#------------------------------------------------------------------------------ #$Date: 2020-02-01 02:11:12 +0200 (Sat, 01 Feb 2020) $ #$Revision: 247420 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/72/1557205.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557205 loop_ _publ_author_name 'Wang, Rong' 'Fan, Run-Zhu' 'Ni, Fu-Qiang' 'Sang, Jun' 'Xie, Xing-Lin' 'Luo, Si-Yuan' 'Tang, Gui-Hua' 'Yin, Sheng' _publ_section_title ; 19-nor-, 20-nor-, and tetranor-Halimane-Type Furanoditerpenoids from Croton crassifolius ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.9b00634 _journal_year 2020 _chemical_absolute_configuration ad _chemical_formula_moiety 'C23 H28 O8' _chemical_formula_sum 'C23 H28 O8' _chemical_formula_weight 432.45 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2019-04-23 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.90190(10) _cell_length_b 10.29550(10) _cell_length_c 25.9952(4) _cell_measurement_reflns_used 18716 _cell_measurement_temperature 100.01(10) _cell_measurement_theta_max 77.1920 _cell_measurement_theta_min 3.3940 _cell_volume 2114.81(5) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.01(10) _diffrn_detector 'CCD plate' _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 31.00 120.00 0.50 0.05 -- 46.62 53.00 -27.00 178 2 \w -173.00 -76.00 0.50 0.20 -- -100.00-117.00 -43.00 194 3 \w 87.00 178.00 0.50 0.20 -- 107.00 68.00 163.00 182 4 \w -119.00 -71.00 0.50 0.05 -- -46.62-125.00-180.00 96 5 \w -119.00 -71.00 0.50 0.05 -- -46.62-125.00 -30.00 96 6 \w -25.00 63.00 0.50 0.05 -- 46.62 -57.00 -30.00 176 7 \w -114.00 -27.00 0.50 0.20 -- -100.00 45.00 90.00 174 8 \w 32.00 123.00 0.50 0.20 -- 107.00 -30.00 0.00 182 9 \w 31.00 125.00 0.50 0.20 -- 107.00 -15.00 0.00 188 10 \w 34.00 109.00 0.50 0.20 -- 107.00 -94.00-150.00 150 11 \w 34.00 117.00 0.50 0.20 -- 107.00-125.00 90.00 166 12 \w 31.00 125.00 0.50 0.20 -- 107.00 -15.00-180.00 188 13 \w 93.00 178.00 0.50 0.20 -- 107.00 45.00 150.00 170 14 \w 34.00 123.00 0.50 0.20 -- 107.00 -53.00-171.00 178 15 \w -119.00 -71.00 0.50 0.05 -- -46.62-125.00 60.00 96 16 \w 31.00 120.00 0.50 0.05 -- 46.62 57.00 60.00 178 17 \w 23.00 120.00 0.50 0.05 -- 46.62 77.00-150.00 194 18 \w -173.00-140.00 0.50 0.20 -- -100.00 -68.00 30.00 66 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0201094000 _diffrn_orient_matrix_UB_12 0.0154560000 _diffrn_orient_matrix_UB_13 -0.0586526000 _diffrn_orient_matrix_UB_21 -0.1496500000 _diffrn_orient_matrix_UB_22 0.0957803000 _diffrn_orient_matrix_UB_23 -0.0008172000 _diffrn_orient_matrix_UB_31 0.1232696000 _diffrn_orient_matrix_UB_32 0.1138834000 _diffrn_orient_matrix_UB_33 0.0086061000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0371 _diffrn_reflns_av_unetI/netI 0.0235 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 20943 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.116 _diffrn_reflns_theta_min 3.400 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.855 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.71010 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.358 _exptl_crystal_description block _exptl_crystal_F_000 920 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.200 _refine_diff_density_min -0.277 _refine_diff_density_rms 0.055 _refine_ls_abs_structure_details ; Flack x determined using 1672 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.11(5) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.106 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 284 _refine_ls_number_reflns 4161 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.106 _refine_ls_R_factor_all 0.0368 _refine_ls_R_factor_gt 0.0353 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0509P)^2^+0.8917P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0976 _refine_ls_wR_factor_ref 0.0988 _reflns_Friedel_coverage 0.734 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.996 _reflns_number_gt 4062 _reflns_number_total 4161 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file np9b00634_si_004.cif _cod_data_source_block wangr_41_190419 _cod_database_code 1557205 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.919 _shelx_estimated_absorpt_t_min 0.784 _reflns_odcompleteness_completeness 99.88 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 71.98 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Ternary CH refined with riding coordinates: C4(H4), C12(H12), C2(H2) 2.b Secondary CH2 refined with riding coordinates: C29(H29A,H29B), C13(H13A,H13B), C7(H7A,H7B), C8(H8A,H8B), C3(H3A,H3B), C9(H9A, H9B) 2.c Aromatic/amide H refined with riding coordinates: C16(H16), C19(H19), C18(H18) 2.d Idealised Me refined as rotating group: C31(H31A,H31B,H31C), C28(H28A,H28B,H28C), C23(H23A,H23B,H23C) 2.e Idealised tetrahedral OH refined as rotating group: O30(H30) ; _shelx_res_file ; TITL wangr_41_190419_a.res in P2(1)2(1)2(1) wangr_41_190419.res created by SHELXL-2016/6 at 11:22:04 on 23-Apr-2019 REM Old TITL wangr_41_190419 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.092, Rweak 0.026, Alpha 0.001 REM 0.699 for 25 systematic absences, Orientation as input REM Flack x = -0.773 ( 0.296 ) from 1758 Parsons' quotients REM Formula found by SHELXT: C23 O8 CELL 1.54184 7.9019 10.2955 25.9952 90 90 90 ZERR 4 0.0001 0.0001 0.0004 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H O UNIT 92 112 32 L.S. 4 PLAN 5 SIZE 0.3 0.2 0.1 BOND $h htab conf acta LIST 6 fmap 2 acta SHEL 999 0.81 OMIT 9 0 9 REM REM REM WGHT 0.050900 0.891700 FVAR 0.55626 O25 3 0.272648 0.768729 0.358503 11.00000 0.02384 0.01577 = 0.01984 0.00271 -0.00188 -0.00002 O22 3 0.674296 0.613469 0.336407 11.00000 0.01840 0.02503 = 0.02259 0.00144 0.00108 -0.00330 O17 3 0.405092 0.163763 0.663147 11.00000 0.02540 0.02587 = 0.01809 0.00378 0.00118 0.00400 O20 3 0.019013 0.511687 0.485388 11.00000 0.02049 0.02370 = 0.02138 -0.00083 -0.00045 0.00212 O11 3 0.154489 0.356292 0.528047 11.00000 0.01703 0.02222 = 0.02136 0.00356 -0.00054 -0.00129 O24 3 0.527463 0.652052 0.264062 11.00000 0.03308 0.02683 = 0.01900 0.00479 0.00106 -0.00441 O30 3 0.256365 0.472833 0.246511 11.00000 0.03052 0.02754 = 0.01773 -0.00244 -0.00353 -0.00029 AFIX 147 H30 2 0.334379 0.508225 0.231142 11.00000 -1.50000 AFIX 0 O27 3 0.479378 0.918454 0.349582 11.00000 0.03452 0.02568 = 0.04868 0.01233 -0.00635 -0.00834 C10 1 0.346895 0.466283 0.423004 11.00000 0.01590 0.01793 = 0.01650 -0.00175 -0.00112 0.00046 C21 1 0.537219 0.603194 0.306213 11.00000 0.02095 0.01698 = 0.01908 -0.00179 0.00049 0.00234 C16 1 0.390680 0.157683 0.610840 11.00000 0.02558 0.02270 = 0.01729 0.00057 0.00254 0.00316 AFIX 43 H16 2 0.407598 0.083095 0.591326 11.00000 -1.20000 AFIX 0 C15 1 0.348484 0.274882 0.591363 11.00000 0.02130 0.01967 = 0.01910 0.00092 0.00208 -0.00042 C14 1 0.152155 0.461673 0.497091 11.00000 0.02273 0.01602 = 0.01448 -0.00337 -0.00154 0.00031 C4 1 0.367665 0.699852 0.398295 11.00000 0.02110 0.01628 = 0.01738 0.00177 -0.00133 0.00036 AFIX 13 H4 2 0.484876 0.730961 0.398339 11.00000 -1.20000 AFIX 0 C5 1 0.366004 0.555706 0.385856 11.00000 0.01586 0.01635 = 0.01788 -0.00176 -0.00140 0.00028 C29 1 0.239838 0.528623 0.296398 11.00000 0.02185 0.02030 = 0.01859 0.00003 -0.00032 0.00098 AFIX 23 H29A 2 0.146771 0.486528 0.314121 11.00000 -1.20000 H29B 2 0.211367 0.619798 0.292720 11.00000 -1.20000 AFIX 0 C13 1 0.441848 0.415624 0.515279 11.00000 0.01765 0.02128 = 0.01520 -0.00019 -0.00174 0.00004 AFIX 23 H13A 2 0.535315 0.379394 0.495805 11.00000 -1.20000 H13B 2 0.487294 0.466384 0.543518 11.00000 -1.20000 AFIX 0 C7 1 0.470251 0.376531 0.327450 11.00000 0.02330 0.01771 = 0.01691 -0.00096 0.00133 0.00111 AFIX 23 H7A 2 0.481090 0.349792 0.291822 11.00000 -1.20000 H7B 2 0.581674 0.373617 0.343067 11.00000 -1.20000 AFIX 0 C12 1 0.326924 0.306938 0.535674 11.00000 0.01805 0.01914 = 0.01978 0.00008 0.00001 0.00117 AFIX 13 H12 2 0.343283 0.228356 0.514989 11.00000 -1.20000 AFIX 0 C8 1 0.353097 0.284156 0.355435 11.00000 0.02685 0.01514 = 0.01890 -0.00180 -0.00025 0.00013 AFIX 23 H8A 2 0.394641 0.195926 0.351995 11.00000 -1.20000 H8B 2 0.240966 0.288214 0.340335 11.00000 -1.20000 AFIX 0 C6 1 0.400672 0.516926 0.329830 11.00000 0.02015 0.01673 = 0.01589 0.00025 0.00051 -0.00136 C3 1 0.286856 0.731575 0.449454 11.00000 0.02394 0.01581 = 0.01904 -0.00222 0.00159 0.00031 AFIX 23 H3A 2 0.165879 0.716292 0.447608 11.00000 -1.20000 H3B 2 0.304958 0.822475 0.457579 11.00000 -1.20000 AFIX 0 C1 1 0.329344 0.501221 0.480337 11.00000 0.02002 0.01581 = 0.01619 -0.00037 -0.00147 0.00014 C2 1 0.364259 0.646765 0.491365 11.00000 0.02322 0.01670 = 0.01692 -0.00143 0.00052 -0.00275 AFIX 13 H2 2 0.487122 0.659339 0.490094 11.00000 -1.20000 AFIX 0 C19 1 0.333066 0.360788 0.634588 11.00000 0.03112 0.02101 = 0.02060 -0.00097 0.00193 0.00098 AFIX 43 H19 2 0.303940 0.448288 0.633837 11.00000 -1.20000 AFIX 0 C9 1 0.343821 0.320889 0.412336 11.00000 0.02098 0.01581 = 0.01808 0.00209 -0.00165 0.00058 AFIX 23 H9A 2 0.240684 0.284921 0.426708 11.00000 -1.20000 H9B 2 0.438357 0.280874 0.430096 11.00000 -1.20000 AFIX 0 C18 1 0.369211 0.289219 0.676313 11.00000 0.02670 0.02570 = 0.01856 -0.00154 0.00410 0.00076 AFIX 43 H18 2 0.369758 0.320900 0.709816 11.00000 -1.20000 AFIX 0 C31 1 0.304403 0.689836 0.544867 11.00000 0.02945 0.02064 = 0.01776 -0.00296 0.00227 -0.00192 AFIX 137 H31A 2 0.325000 0.781121 0.549051 11.00000 -1.50000 H31B 2 0.365295 0.642438 0.570728 11.00000 -1.50000 H31C 2 0.185469 0.672893 0.548293 11.00000 -1.50000 AFIX 0 C26 1 0.341696 0.877862 0.338295 11.00000 0.02889 0.01573 = 0.02328 0.00065 0.00253 -0.00034 C28 1 0.225663 0.936583 0.299345 11.00000 0.03688 0.02262 = 0.02654 0.00624 -0.00191 0.00048 AFIX 137 H28A 2 0.236740 0.890892 0.267329 11.00000 -1.50000 H28B 2 0.254700 1.026260 0.294398 11.00000 -1.50000 H28C 2 0.110976 0.930337 0.311276 11.00000 -1.50000 AFIX 0 C23 1 0.812517 0.689184 0.315508 11.00000 0.02313 0.02919 = 0.02913 0.00014 0.00562 -0.00638 AFIX 137 H23A 2 0.852645 0.649135 0.284469 11.00000 -1.50000 H23B 2 0.902859 0.693117 0.340151 11.00000 -1.50000 H23C 2 0.773707 0.775511 0.308046 11.00000 -1.50000 AFIX 0 HKLF 4 REM wangr_41_190419_a.res in P2(1)2(1)2(1) REM R1 = 0.0353 for 4062 Fo > 4sig(Fo) and 0.0368 for all 4161 data REM 284 parameters refined using 0 restraints END WGHT 0.0510 0.8883 REM Instructions for potential hydrogen bonds HTAB O30 O24 EQIV $1 x+1/2, -y+1/2, -z+1 HTAB C16 O20_$1 HTAB C4 O22 EQIV $2 x-1/2, -y+1/2, -z+1 HTAB C29 O17_$2 HTAB C29 O25 HTAB C3 O20 EQIV $3 -x+1/2, -y+1, z+1/2 HTAB C18 O30_$3 EQIV $4 -x+1, y+1/2, -z+1/2 HTAB C28 O24_$4 HTAB C23 O30_$4 REM Highest difference peak 0.200, deepest hole -0.277, 1-sigma level 0.055 Q1 1 0.3672 0.0354 0.5956 11.00000 0.05 0.20 Q2 1 0.4530 0.0541 0.6058 11.00000 0.05 0.20 Q3 1 0.2939 0.3851 0.4217 11.00000 0.05 0.18 Q4 1 0.4122 0.6296 0.3911 11.00000 0.05 0.18 Q5 1 0.3093 0.5754 0.4863 11.00000 0.05 0.18 ; _shelx_res_checksum 1208 _shelx_hkl_file ; 0 0 2 108.48 3.61 0 0 3 0.80 0.40 0 0 4 14.08 1.28 0 0 -4 16.20 1.31 0 0 -5 0.21 0.57 0 0 5 0.86 0.70 0 0 -5 0.27 0.57 0 0 -6 8881.09 239.06 0 0 -6 9218.30 239.12 0 0 -7 0.64 0.77 0 0 -7 0.10 0.70 0 0 7 0.30 0.78 0 0 -8 161.22 6.90 0 0 8 169.42 7.13 0 0 -8 154.80 6.69 0 0 9 0.53 0.86 0 0 -9 -0.12 0.70 0 0 -9 -0.12 0.69 0 0 10 144.70 7.12 0 0 -10 145.11 6.85 0 0 -10 139.36 6.64 0 0 11 0.51 1.08 0 0 -11 0.14 0.76 0 0 -11 0.78 1.03 0 0 12 2206.87 61.06 0 0 -12 2074.52 60.01 0 0 -12 2098.82 60.34 0 0 12 2092.06 58.69 0 0 -13 -0.19 0.92 0 0 13 0.90 0.73 0 0 13 -0.21 1.05 0 0 -13 0.88 1.03 0 0 14 337.57 14.19 0 0 -14 333.59 13.79 0 0 -14 338.19 13.49 0 0 14 334.74 15.90 0 0 14 314.32 12.02 0 0 15 0.26 1.33 0 0 -15 -0.23 0.91 0 0 15 1.07 1.48 0 0 -15 1.45 1.06 0 0 16 212.38 13.09 0 0 16 213.85 9.40 0 0 -16 220.27 9.44 0 0 -16 227.90 11.27 0 0 16 241.25 12.12 0 0 -16 230.44 10.83 0 0 -17 0.24 0.84 0 0 -17 0.08 0.58 0 0 17 0.32 0.63 0 0 17 -0.32 1.25 0 0 17 -0.43 1.62 0 0 -17 -0.27 1.07 0 0 -18 30.53 4.02 0 0 -18 30.54 2.31 0 0 18 32.23 5.35 0 0 -18 29.38 2.24 0 0 -18 25.32 3.50 0 0 18 28.01 4.23 0 0 -19 0.09 0.63 0 0 19 0.75 1.49 0 0 -19 -0.26 0.93 0 0 19 -0.52 1.71 0 0 -19 1.23 0.77 0 0 -19 0.62 1.09 0 0 20 204.40 14.57 0 0 -20 207.84 7.77 0 0 -20 170.95 10.12 0 0 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7.27 0 1 -4 221.30 6.56 0 1 4 209.49 7.69 0 1 -4 197.68 6.12 0 -1 5 678.00 19.26 0 1 -5 677.03 19.13 0 1 5 664.34 19.98 0 1 -5 652.10 19.54 0 1 5 613.19 18.62 0 1 5 653.86 19.25 0 1 -5 652.23 18.02 0 1 6 106.57 4.66 0 1 6 89.70 3.85 0 -1 6 102.91 4.60 0 1 -6 93.44 4.67 0 1 -6 92.19 4.29 0 1 -6 91.12 3.45 0 1 6 96.90 5.08 0 -1 7 305.41 10.54 0 1 -7 297.53 10.82 0 1 7 279.44 9.38 0 1 -7 288.05 10.15 0 1 -7 309.47 9.16 0 1 7 304.88 10.57 0 1 7 304.87 11.48 0 1 -8 232.42 7.55 0 1 8 234.49 9.04 0 1 -8 227.76 9.19 0 -1 8 233.73 9.03 0 1 8 232.84 9.98 0 1 -8 222.81 8.66 0 1 -9 6.54 1.54 0 1 -9 7.76 1.35 0 -1 9 5.74 1.37 0 1 9 8.54 1.59 0 1 -9 7.58 0.96 0 1 9 9.66 2.03 0 1 -10 503.15 17.25 0 1 10 489.52 17.02 0 1 10 470.21 18.26 0 1 -10 511.04 16.57 0 1 -10 495.18 14.90 0 -1 -10 482.45 16.87 0 -1 10 487.97 16.94 0 1 11 727.10 24.45 0 -1 -11 671.56 22.35 0 1 11 684.66 22.47 0 -1 -11 686.52 21.97 0 -1 11 673.24 21.67 0 1 -11 630.92 21.47 0 1 -11 663.52 19.91 0 -1 11 744.00 22.74 0 1 -11 664.29 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4.84 0 4 -19 104.63 8.83 0 4 -19 103.15 4.82 0 -4 -20 84.06 7.86 0 -4 -20 97.15 4.70 0 4 20 84.57 10.16 0 4 -20 99.96 4.73 0 4 20 95.13 4.75 0 4 -20 96.36 5.10 0 4 -20 89.57 8.40 0 -4 20 92.48 7.94 0 4 -20 104.66 5.35 0 -4 -21 52.52 3.27 0 4 -21 52.98 3.20 0 4 -21 52.44 3.66 0 4 -21 49.66 3.50 0 4 21 46.97 7.51 0 -4 -21 47.48 5.68 0 -4 21 46.85 5.61 0 4 22 70.21 9.19 0 4 -22 90.41 4.96 0 4 -22 90.35 4.90 0 -4 22 86.07 7.48 0 4 -22 85.69 4.25 0 -4 22 88.74 9.74 0 -4 -22 86.48 4.41 0 -4 -23 16.74 1.79 0 4 -23 15.85 2.00 0 4 -23 15.34 2.03 0 4 -23 16.02 1.70 0 -4 -24 11.04 1.50 0 4 -24 11.19 1.76 0 4 -24 9.91 1.71 0 4 -24 14.62 1.50 0 -4 -25 21.52 1.91 0 4 -25 16.97 1.98 0 4 -25 17.69 1.59 0 4 -25 16.93 1.98 0 -4 -26 126.78 5.46 0 -4 -26 119.27 5.02 0 4 -26 125.35 5.61 0 4 -26 124.27 5.61 0 -4 -27 73.92 3.35 0 4 -27 73.63 3.84 0 4 -27 74.45 3.81 0 -4 -27 75.08 3.74 0 4 -28 71.96 3.63 0 4 -28 72.80 3.64 0 -4 -28 81.67 3.68 0 -4 -28 69.76 3.09 0 -4 -29 0.04 0.35 0 -4 -29 -0.42 0.63 0 4 -29 0.07 0.63 0 4 -29 0.32 0.61 0 4 -30 136.88 4.00 0 4 -30 124.28 3.95 0 -4 -30 132.08 3.95 0 4 -31 0.11 0.34 0 -4 -31 0.17 0.32 0 -5 0 0.31 0.80 0 5 0 0.31 1.57 0 5 -1 334.47 15.35 0 -5 -1 316.57 11.98 0 -5 1 312.35 12.48 0 5 1 319.88 15.32 0 -5 2 440.89 15.61 0 5 2 396.19 18.20 0 5 -2 430.74 18.07 0 -5 -2 397.36 14.20 0 -5 3 1139.36 34.18 0 5 -3 1052.79 36.57 0 -5 -3 1079.53 31.86 0 -5 4 58.42 4.80 0 5 -4 71.05 6.08 0 5 -4 56.50 5.17 0 -5 -4 56.08 3.52 0 5 4 62.49 6.18 0 5 -5 55.44 5.18 0 -5 -5 49.95 3.16 0 -5 5 52.69 4.60 0 5 5 60.73 6.07 0 5 -6 6.29 1.96 0 5 6 6.31 2.31 0 -5 6 2.04 1.27 0 5 -7 162.34 9.98 0 -5 7 181.30 9.70 0 5 -7 185.40 10.23 0 5 7 191.47 11.31 0 5 -8 33.24 4.25 0 5 8 43.88 5.28 0 5 -8 40.91 4.59 0 -5 8 42.53 4.51 0 5 -9 73.67 6.33 0 5 -9 73.78 6.21 0 -5 9 73.64 5.97 0 5 -10 61.57 5.90 0 5 -10 64.83 6.08 0 -5 10 60.18 5.74 0 5 -11 280.77 9.72 0 5 -11 284.87 14.34 0 5 -11 273.81 9.81 0 5 -11 290.01 14.63 0 5 -12 82.74 7.04 0 5 -12 78.81 4.11 0 5 -12 71.54 3.88 0 5 -12 68.02 3.64 0 5 -12 79.08 7.20 0 5 -13 724.01 27.45 0 5 13 650.72 20.02 0 5 13 633.98 19.75 0 5 -13 671.09 20.08 0 5 -13 705.06 20.85 0 5 -13 700.29 20.56 0 5 -13 710.05 26.67 0 5 -14 360.19 12.58 0 -5 14 389.38 17.94 0 5 -14 363.99 12.08 0 5 -14 371.86 12.42 0 5 14 340.07 11.91 0 5 -14 388.36 18.35 0 5 -14 407.07 18.15 0 5 14 362.09 11.84 0 5 -15 10.66 1.67 0 5 -15 11.39 1.67 0 5 -15 8.31 1.35 0 -5 15 10.28 2.90 0 5 15 10.45 1.46 0 5 -15 6.21 2.29 0 5 -15 11.47 3.04 0 5 15 8.90 1.32 0 5 16 413.40 13.63 0 -5 16 443.37 20.20 0 5 -16 414.05 19.36 0 5 -16 424.65 13.80 0 5 -16 454.32 14.74 0 5 -16 440.66 14.43 0 5 16 394.86 13.70 0 5 -16 448.50 20.69 0 -5 17 184.25 12.13 0 5 -17 176.14 11.42 0 5 -17 179.09 12.29 0 5 17 182.28 7.39 0 5 -17 190.92 7.90 0 5 -17 198.61 7.49 0 5 -17 192.50 8.07 0 5 17 177.55 7.18 0 5 18 28.44 2.45 0 5 18 28.99 2.38 0 5 -18 34.80 2.96 0 5 -18 27.84 2.63 0 5 -18 28.51 2.41 0 -5 18 26.43 4.46 0 5 -18 30.31 4.89 0 -5 -18 26.13 4.52 0 -5 19 9.34 2.83 0 5 -19 9.75 1.74 0 5 -19 7.92 1.41 0 5 19 11.43 1.63 0 -5 -19 10.29 3.05 0 5 19 9.67 1.49 0 5 -19 11.27 3.16 0 -5 -19 10.39 1.48 0 5 -19 8.30 1.69 0 5 -20 285.67 10.46 0 5 -20 271.94 9.54 0 -5 -20 234.25 14.24 0 -5 -20 257.78 9.32 0 5 -20 260.71 15.23 0 5 -20 258.99 10.04 0 5 20 257.79 9.38 0 -5 20 226.39 14.00 0 -5 21 82.04 7.63 0 5 -21 86.31 4.87 0 5 -21 80.68 4.69 0 -5 -21 77.07 4.10 0 5 -21 84.24 4.29 0 5 -22 139.78 6.48 0 -5 -22 136.70 5.83 0 5 -22 143.39 5.97 0 5 -22 146.70 6.73 0 5 -23 38.23 2.99 0 -5 -23 41.06 2.65 0 5 -23 36.49 2.99 0 5 -23 36.75 2.56 0 5 -24 15.50 1.88 0 5 -24 13.49 1.46 0 -5 -24 13.98 1.53 0 5 -24 11.43 1.74 0 5 -25 12.99 1.71 0 -5 -25 15.77 1.53 0 5 -25 14.55 1.44 0 5 -25 12.40 1.73 0 5 -25 14.30 1.76 0 -5 -26 3.47 0.97 0 5 -26 1.40 0.79 0 5 -26 1.22 0.56 0 5 -26 1.65 0.92 0 -5 -26 2.65 0.76 0 5 -26 2.31 0.99 0 5 -27 18.17 1.61 0 -5 -27 25.89 1.94 0 5 -27 23.21 1.93 0 -5 -27 25.08 1.60 0 5 -27 23.48 1.96 0 5 -28 1.72 0.75 0 5 -28 1.37 0.68 0 -5 -28 1.31 0.67 0 5 28 0.65 0.45 0 -5 -29 13.76 1.17 0 5 -29 13.94 1.21 0 -5 -30 0.82 0.39 0 5 -30 1.86 0.46 0 -6 0 944.77 30.85 0 6 0 961.78 28.11 0 6 1 18.37 3.87 0 -6 -1 16.14 2.35 0 -6 1 12.68 2.25 0 6 -1 12.82 1.63 0 6 -1 16.67 3.63 0 -6 -2 146.73 7.30 0 6 -2 134.57 5.79 0 6 2 155.82 10.91 0 -6 2 139.17 7.94 0 6 -2 155.32 10.68 0 6 2 134.60 5.78 0 6 3 74.69 3.80 0 -6 -3 57.95 4.18 0 6 -3 63.36 3.55 0 -6 3 61.83 5.16 0 6 -4 807.20 23.69 0 -6 -4 794.72 24.88 0 6 4 797.68 23.67 0 -6 4 838.55 28.06 0 6 -5 120.68 8.66 0 -6 5 131.71 8.14 0 6 -5 114.39 5.20 0 6 5 120.84 5.31 0 -6 6 4.66 1.75 0 6 -6 4.58 1.09 0 6 6 5.37 1.13 0 6 -6 6.86 2.27 0 6 6 7.24 2.76 0 -6 7 83.30 6.69 0 6 -7 74.27 3.98 0 6 -7 72.24 3.82 0 6 7 76.65 3.92 0 6 -7 78.95 3.96 0 6 -7 73.02 6.75 0 6 -8 103.70 4.80 0 6 -8 104.37 4.72 0 -6 8 102.45 7.70 0 6 8 100.56 4.71 0 6 -8 95.95 7.96 0 6 -9 571.73 17.62 0 6 -9 550.46 17.30 0 6 9 567.67 17.37 0 -6 9 590.31 23.14 0 -6 10 25.34 3.94 0 6 10 19.80 1.83 0 6 -10 23.57 2.15 0 6 10 20.24 1.87 0 6 -10 23.83 2.01 0 6 -10 22.98 4.04 0 6 11 103.74 4.84 0 -6 11 122.39 9.01 0 6 -11 124.61 9.49 0 6 -11 116.36 5.32 0 6 -11 115.16 5.09 0 6 11 102.47 4.59 0 6 11 109.38 4.81 0 6 12 143.88 6.03 0 6 -12 162.40 11.17 0 6 -12 143.63 6.35 0 -6 12 153.51 10.42 0 6 12 138.91 5.74 0 6 -12 149.40 6.21 0 6 -13 153.69 11.14 0 6 13 140.25 5.91 0 6 -13 154.46 6.35 0 6 -13 162.34 6.96 0 6 13 141.55 6.15 0 6 -13 154.13 6.69 0 6 14 288.73 10.55 0 6 -14 335.81 17.46 0 6 -14 312.24 11.44 0 6 -14 313.08 11.22 0 6 14 306.49 10.41 0 6 -14 310.02 10.79 0 6 -15 191.65 8.11 0 -6 15 214.71 13.25 0 6 -15 194.14 8.41 0 6 15 189.51 7.61 0 6 -15 198.17 13.30 0 6 -15 203.34 7.81 0 6 15 194.22 7.45 0 6 -16 6.64 1.35 0 6 -16 8.38 1.61 0 6 -16 7.92 1.70 0 6 -16 8.76 2.82 0 6 16 7.06 1.27 0 6 16 6.34 1.27 0 -6 16 8.66 2.97 0 6 17 559.07 17.52 0 -6 17 601.37 25.58 0 6 -17 578.95 18.57 0 6 -17 573.55 25.56 0 6 -17 585.66 18.05 0 6 -17 575.66 18.87 0 6 17 550.53 17.79 0 6 18 11.85 1.52 0 6 18 9.22 1.46 0 -6 -18 10.46 2.99 0 6 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0.90 0 7 0 0.31 0.71 0 7 0 0.33 0.72 0 -7 0 -0.24 0.72 0 7 0 -0.33 0.69 0 7 -1 125.14 5.92 0 -7 -1 130.40 7.59 0 7 -1 134.84 6.05 0 7 -1 126.77 5.33 0 -7 1 137.22 8.25 0 7 1 127.88 5.83 0 7 1 125.32 5.32 0 7 -1 120.89 5.61 0 7 -2 210.91 8.20 0 -7 -2 218.60 10.18 0 7 -2 216.86 8.62 0 7 2 215.34 8.27 0 7 2 220.42 8.57 0 7 2 207.46 7.75 0 7 -2 216.83 7.84 0 7 -2 219.38 8.55 0 -7 2 217.18 11.24 0 -7 3 131.91 8.57 0 7 -3 135.24 5.97 0 7 3 135.50 5.65 0 7 3 149.95 6.38 0 7 -3 146.63 6.36 0 7 -3 138.87 5.70 0 7 3 130.78 5.88 0 7 -3 134.21 6.35 0 7 4 313.79 10.89 0 -7 4 348.85 15.30 0 7 4 302.39 10.55 0 7 -4 319.23 11.08 0 7 4 325.95 11.34 0 7 -4 316.31 11.59 0 7 -4 317.22 11.30 0 7 -4 320.79 10.68 0 7 5 34.06 2.72 0 7 5 32.38 2.39 0 7 -5 34.60 2.75 0 -7 5 37.31 4.53 0 7 -5 37.04 2.73 0 7 -5 33.65 2.93 0 7 6 147.66 6.36 0 -7 6 145.96 9.50 0 7 6 137.65 5.82 0 7 -6 141.41 6.77 0 7 -6 149.85 6.42 0 7 -6 142.08 6.20 0 7 7 77.40 4.26 0 7 -7 87.04 4.97 0 7 -7 72.13 4.17 0 7 -7 82.79 4.36 0 -7 7 82.71 7.05 0 7 7 76.19 3.95 0 -7 8 101.98 8.14 0 7 -8 111.80 9.29 0 7 -8 110.24 5.23 0 7 8 100.38 5.06 0 7 -8 109.79 5.31 0 7 8 105.48 4.87 0 7 -8 114.87 5.95 0 -7 9 261.75 14.19 0 7 9 251.89 9.27 0 7 -9 260.19 10.34 0 7 -9 253.86 9.46 0 7 -9 240.25 9.15 0 7 -9 260.85 15.16 0 7 9 239.44 8.89 0 7 -10 0.21 0.76 0 7 10 0.10 0.72 0 7 -10 0.90 1.49 0 7 -10 -0.15 0.99 0 -7 10 -0.38 1.36 0 7 10 0.73 0.78 0 7 -10 0.92 0.93 0 7 11 0.30 0.70 0 7 -11 0.10 0.68 0 -7 11 2.00 1.73 0 7 11 -0.20 0.69 0 7 -11 1.39 1.42 0 7 -11 0.24 0.92 0 7 12 55.75 3.43 0 7 12 56.59 3.39 0 -7 12 63.07 6.86 0 7 -12 59.11 7.05 0 7 -12 59.08 3.85 0 7 13 203.19 7.99 0 7 -13 208.13 8.55 0 7 -13 213.48 14.17 0 -7 13 203.67 13.19 0 7 -13 213.37 8.25 0 7 -14 423.89 21.32 0 -7 14 437.05 20.67 0 7 -14 422.18 13.80 0 7 -14 403.69 14.11 0 7 14 389.30 13.42 0 7 -15 0.22 0.90 0 7 -15 1.18 1.03 0 7 -15 -0.49 1.50 0 7 -15 1.44 1.36 0 7 15 0.94 0.81 0 7 -16 36.31 3.03 0 7 16 32.34 2.56 0 7 -16 26.77 4.90 0 7 -16 30.54 2.63 0 7 -16 32.82 3.14 0 7 -17 65.36 4.40 0 7 17 66.01 3.76 0 -7 17 55.62 6.75 0 7 -17 68.24 3.95 0 7 -17 67.86 7.59 0 7 -17 62.26 4.13 0 7 -18 62.56 3.83 0 7 18 66.91 3.72 0 7 -18 69.70 4.28 0 7 -18 66.59 4.41 0 7 -18 67.47 4.73 0 -7 -19 46.98 2.91 0 7 -19 37.91 3.31 0 7 -19 47.00 3.84 0 7 -19 46.27 3.12 0 7 -19 46.00 3.39 0 7 -20 75.19 4.34 0 7 -20 69.02 4.38 0 -7 -20 70.59 3.64 0 7 -20 69.07 4.59 0 7 -20 73.26 3.95 0 7 -21 6.35 1.51 0 -7 -21 6.46 1.11 0 7 -21 6.77 1.47 0 7 -21 6.40 1.24 0 -7 -22 16.45 1.51 0 7 -22 15.18 1.80 0 7 -22 14.48 1.95 0 7 -22 13.51 1.53 0 7 -23 5.11 1.24 0 7 -23 7.26 1.11 0 -7 -23 6.28 0.93 0 7 -23 6.61 1.29 0 7 -24 32.49 2.02 0 7 -24 32.59 2.38 0 7 -24 31.47 2.28 0 -7 -24 31.07 1.78 0 7 -25 96.43 4.13 0 7 -25 91.44 3.97 0 7 -25 90.80 3.61 0 -7 -26 107.11 4.06 0 7 -26 95.65 3.95 0 -7 -27 32.05 1.67 0 7 -27 31.80 1.71 0 8 0 53.28 3.78 0 8 0 49.70 3.54 0 8 0 51.06 3.20 0 -8 0 46.93 4.81 0 8 -1 0.83 1.15 0 8 1 0.12 0.73 0 8 -1 0.68 0.72 0 -8 1 1.14 1.13 0 8 1 0.39 0.69 0 8 -1 0.91 0.82 0 8 -2 5.23 1.15 0 8 -2 8.63 1.69 0 8 -2 6.15 1.47 0 8 2 4.09 1.06 0 8 -2 4.58 1.30 0 8 2 4.84 1.26 0 -8 3 50.82 5.44 0 8 3 56.47 3.89 0 8 3 54.72 3.35 0 8 3 56.58 3.62 0 8 -3 48.83 3.55 0 8 -3 56.08 3.88 0 8 -3 58.52 4.00 0 8 -3 58.02 3.42 0 8 4 58.64 3.92 0 8 4 49.90 3.21 0 -8 4 51.81 5.60 0 8 4 56.35 3.54 0 8 -4 52.52 3.30 0 8 -4 55.85 3.97 0 8 -4 54.87 3.06 0 8 -4 52.02 3.61 0 8 -4 54.31 3.80 0 8 5 93.48 4.62 0 8 -5 100.07 4.77 0 8 -5 97.27 5.48 0 8 5 94.36 5.15 0 8 -5 92.34 4.29 0 8 -5 88.15 5.04 0 -8 5 102.39 8.03 0 8 -5 92.67 5.07 0 8 6 298.90 10.96 0 8 -6 308.21 11.61 0 8 -6 283.71 9.83 0 8 -6 299.07 10.41 0 8 -6 283.36 10.80 0 -8 6 316.73 15.63 0 8 6 275.20 10.14 0 8 -6 300.02 11.00 0 8 -7 12.92 1.73 0 8 7 16.01 1.79 0 8 7 16.05 2.02 0 -8 7 16.05 3.42 0 8 -7 17.87 2.38 0 8 -7 13.15 1.90 0 8 -7 15.99 2.03 0 8 -8 35.39 2.94 0 8 -8 36.45 2.99 0 8 8 30.76 2.50 0 -8 8 34.82 4.94 0 8 8 33.01 2.80 0 8 -8 40.33 3.51 0 8 -9 471.49 15.20 0 8 -9 455.55 15.47 0 8 -9 467.03 15.31 0 8 -9 470.54 16.52 0 8 9 448.03 14.82 0 8 9 447.68 15.18 0 -8 9 488.15 21.55 0 8 -10 93.68 4.92 0 8 10 97.10 4.76 0 8 -10 98.42 5.87 0 8 -10 87.59 4.76 0 -8 10 94.52 8.45 0 8 10 97.27 4.96 0 8 -10 97.31 5.19 0 8 11 35.40 2.82 0 -8 11 41.57 5.67 0 8 11 36.89 2.78 0 8 -11 41.39 3.22 0 8 -11 46.56 3.19 0 8 -11 41.62 3.70 0 8 -11 34.40 2.75 0 8 -12 115.07 5.55 0 -8 12 144.42 10.78 0 8 -12 139.59 6.47 0 8 -12 142.76 7.35 0 8 12 134.64 5.89 0 8 12 129.84 5.83 0 8 13 243.90 9.10 0 -8 13 250.67 14.94 0 8 -13 256.77 10.70 0 8 -13 246.09 9.75 0 8 14 22.42 2.14 0 8 -14 23.91 2.86 0 8 -14 23.80 2.53 0 -8 14 23.97 4.44 0 8 15 191.18 7.38 0 8 -15 187.05 8.82 0 8 -15 190.14 7.66 0 8 -15 184.40 7.99 0 8 -16 0.42 0.92 0 8 -16 -0.25 1.04 0 8 16 0.92 0.78 0 8 -17 27.97 2.44 0 8 -17 29.71 2.70 0 8 17 27.23 2.15 0 8 -18 1.85 1.13 0 8 -18 2.71 1.03 0 -8 -18 1.45 0.74 0 8 -19 2.73 1.34 0 8 -19 4.70 1.16 0 -8 -19 3.74 0.89 0 8 -19 4.54 1.27 0 -8 -20 60.99 3.08 0 8 -20 68.08 3.80 0 8 -20 65.67 3.48 0 8 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-19 50.36 3.50 2 7 -19 56.28 3.43 2 7 -18 131.98 6.52 -2 7 18 143.25 6.26 2 7 -18 131.99 6.26 -2 7 18 144.32 6.48 2 7 -18 128.32 6.07 2 7 -17 18.32 2.36 -2 7 17 15.20 1.95 -2 7 17 19.99 2.32 2 7 -17 13.66 2.00 2 7 -17 19.57 2.13 -2 7 16 103.55 5.28 2 7 -16 107.85 10.23 2 7 -16 104.40 5.36 2 7 -16 109.93 5.94 -2 -7 -16 110.37 10.52 -2 7 16 102.72 5.48 2 -7 16 101.53 9.03 2 7 -16 107.41 5.54 2 7 -15 61.95 3.79 2 7 -15 51.05 7.11 2 7 -15 65.65 4.51 2 -7 15 64.98 7.09 -2 7 15 61.34 3.85 -2 7 15 59.60 4.02 2 7 -15 60.79 3.94 2 7 -15 54.76 3.74 2 -7 14 178.34 12.34 2 7 -14 201.55 14.12 2 7 -14 181.73 8.38 -2 7 14 177.75 7.54 2 7 -14 192.36 7.60 -2 7 14 185.98 7.95 2 7 -14 164.12 7.52 2 7 -14 176.00 7.58 2 7 -13 488.22 15.27 2 7 -13 488.92 16.52 -2 7 13 415.45 22.75 2 7 -13 441.90 15.36 -2 7 13 447.06 15.22 -2 7 13 470.80 15.73 2 7 -13 456.53 15.35 2 7 -12 15.72 1.91 2 7 -12 14.03 1.89 2 7 -12 11.94 1.66 2 7 -12 12.78 2.08 -2 7 12 12.97 1.71 -2 7 12 14.94 1.91 -2 7 12 10.57 3.63 -2 7 12 14.34 2.04 2 7 -12 12.52 1.75 -2 7 11 40.65 6.52 2 7 -11 36.83 2.74 2 7 -11 42.59 6.23 2 7 -11 27.09 2.45 2 7 -11 34.13 3.24 -2 7 11 35.91 2.79 -2 7 11 35.47 2.94 2 7 -11 32.92 2.79 2 -7 11 35.07 5.13 -2 7 11 33.64 2.71 2 7 -11 33.56 2.77 2 7 -10 111.59 5.15 -2 7 10 107.14 5.23 2 7 -10 112.86 5.38 2 7 -10 93.70 5.04 2 7 -10 119.71 10.33 2 7 -10 114.09 6.10 -2 7 10 107.43 5.49 -2 7 10 107.42 10.53 -2 7 10 105.67 5.27 2 -7 10 107.54 8.96 2 7 -9 21.74 2.03 2 7 -9 20.11 2.14 -2 7 9 19.99 2.15 -2 7 9 19.26 2.18 2 7 -9 22.25 2.57 2 7 -9 23.86 4.63 -2 7 9 19.54 2.07 -2 7 9 19.19 4.81 2 -7 9 19.67 3.84 2 7 -9 20.00 2.11 2 7 -8 120.27 5.21 -2 7 8 102.57 5.31 2 7 -8 101.86 5.33 2 7 -8 138.05 10.58 -2 7 8 114.89 5.37 -2 7 8 113.35 5.57 -2 7 8 117.59 10.99 2 -7 8 116.16 8.98 2 7 -8 119.34 5.51 2 7 -7 415.24 14.68 2 -7 7 440.79 20.09 2 7 -7 475.84 21.79 -2 7 7 437.44 14.77 -2 7 7 446.41 14.55 -2 7 7 442.72 14.81 2 7 -7 446.52 14.63 2 7 -7 464.98 14.25 2 -7 6 128.39 9.20 2 7 -6 118.67 9.53 -2 7 6 121.77 5.49 -2 7 6 120.25 11.03 2 7 -6 108.58 5.56 -2 7 6 121.62 5.77 2 7 -6 115.15 5.46 -2 7 6 117.23 5.63 2 7 -6 121.94 5.16 2 7 -5 63.62 4.00 2 7 -5 67.11 6.92 2 7 -5 63.23 4.24 -2 7 5 64.55 3.74 -2 7 5 69.49 8.27 -2 7 5 63.42 3.86 2 7 -5 66.11 3.83 2 -7 5 68.41 6.50 -2 7 5 66.58 4.03 2 7 -5 69.26 3.51 2 7 -4 25.65 2.46 2 7 -4 24.82 2.52 2 -7 4 20.58 3.63 2 7 -4 18.45 3.71 -2 7 4 25.47 2.44 -2 7 4 25.40 2.23 2 7 -4 25.31 1.95 2 7 -4 23.30 2.15 -2 7 4 23.09 2.24 -2 7 3 63.25 3.64 2 7 -3 59.30 3.81 2 -7 3 52.71 5.62 2 7 -3 61.14 6.48 2 7 -3 64.07 4.12 -2 7 3 57.63 3.68 -2 7 3 64.18 7.85 -2 7 3 59.37 3.84 2 7 -3 64.86 3.72 2 7 -3 63.11 3.21 2 7 -2 53.70 3.63 2 7 -2 60.12 3.56 2 7 -2 56.54 3.84 -2 7 2 60.09 3.66 -2 7 2 65.22 7.88 -2 7 2 60.80 3.52 2 -7 2 58.42 5.78 2 7 -2 57.76 3.00 2 7 -1 85.00 4.79 2 7 -1 73.41 4.43 -2 7 1 79.62 8.75 -2 7 1 81.39 4.39 -2 7 1 85.23 4.31 2 -7 1 76.65 6.64 2 -7 0 6.31 2.09 -2 7 0 3.73 1.30 -2 7 0 5.06 1.17 -2 7 0 5.10 1.27 2 7 0 4.46 1.24 2 7 0 6.51 1.49 -2 7 0 3.19 2.49 2 7 1 79.42 4.61 -2 7 -1 84.77 4.32 -2 7 -1 79.80 8.78 2 -7 -1 85.53 6.74 -2 7 -1 79.58 4.55 -2 -7 1 73.76 5.87 2 -7 -2 52.89 5.29 -2 7 -2 57.06 7.23 -2 -7 2 53.21 5.17 -2 7 -2 63.45 3.95 -2 7 -2 63.67 3.61 2 7 2 60.21 3.88 -2 7 -2 55.18 3.47 -2 7 -3 60.31 3.88 -2 -7 3 61.93 5.65 2 7 3 52.91 3.68 -2 7 -3 63.73 3.84 2 7 3 61.08 3.95 -2 7 -3 57.88 3.50 -2 7 -3 63.91 7.63 2 -7 -3 70.29 5.89 -2 7 -3 61.79 3.68 2 7 4 24.22 2.45 -2 7 -4 26.12 2.45 2 7 4 23.98 2.39 -2 7 -4 35.85 5.67 2 -7 -4 24.42 3.42 -2 7 -4 23.37 2.40 -2 7 -4 25.96 2.27 -2 -7 4 22.02 3.56 2 7 5 66.53 4.14 -2 7 -5 62.42 3.72 2 7 5 67.32 4.08 -2 7 -5 75.12 8.16 -2 -7 5 70.31 6.38 -2 7 -5 64.32 3.98 -2 7 -6 119.23 10.34 -2 -7 6 140.75 9.47 2 7 6 118.99 5.79 -2 7 -6 125.47 5.65 -2 7 -6 114.29 5.66 2 7 6 121.24 5.83 -2 -7 7 477.12 20.42 2 7 7 438.54 14.80 -2 7 -7 443.39 21.88 2 7 7 449.97 14.86 -2 7 -7 430.03 14.62 -2 7 -7 436.06 14.45 -2 7 -8 103.44 9.42 2 7 8 124.22 5.76 2 7 8 119.55 5.71 -2 -7 8 122.21 9.27 -2 7 -8 104.93 5.44 -2 7 -8 119.78 5.53 -2 7 -9 14.77 3.58 2 7 9 20.83 2.21 -2 -7 9 18.23 3.76 -2 7 -9 20.55 2.22 2 7 9 21.73 2.25 -2 7 -9 22.32 2.17 2 7 10 106.07 5.39 2 7 10 112.78 5.40 -2 -7 10 101.95 8.91 -2 7 -10 105.26 5.24 -2 7 -10 111.39 5.35 2 7 11 37.39 2.93 2 7 11 33.56 2.67 -2 -7 11 35.67 5.31 2 7 11 28.39 2.17 -2 7 -11 31.67 2.58 -2 7 -11 33.65 2.75 2 7 12 14.72 1.88 2 7 12 12.42 1.47 -2 7 -12 13.91 1.84 2 7 12 9.36 1.52 -2 -7 12 14.58 3.57 2 7 13 434.66 14.27 -2 -7 13 503.39 22.92 2 7 13 470.35 15.30 -2 7 -13 470.01 15.37 -2 7 -14 184.65 7.46 2 7 14 176.52 6.90 -2 -7 14 197.46 13.32 -2 7 -14 177.03 7.62 2 7 15 60.65 3.41 -2 7 -15 64.71 3.88 -2 7 -15 65.91 4.04 2 7 16 94.68 4.64 -2 -7 16 108.59 9.79 -2 7 -16 119.94 5.66 -2 7 -16 106.81 5.17 2 7 17 15.91 1.69 -2 7 -17 17.88 2.08 -2 7 -17 14.82 1.82 2 7 18 129.55 5.55 -2 7 -18 143.51 6.33 -2 7 -18 138.92 5.92 -2 7 -19 50.16 3.08 2 7 19 48.90 2.90 -2 7 -19 52.69 3.41 -2 7 -20 25.00 2.05 2 -7 -20 25.36 2.16 2 7 20 23.16 1.86 -2 7 -20 24.61 2.24 -2 7 -21 35.17 2.27 2 7 21 31.00 2.08 2 -7 -21 32.35 2.40 -2 7 -21 36.85 2.58 2 -7 -22 39.38 2.51 -2 7 -22 40.53 2.27 2 7 22 37.29 2.14 -2 7 -22 39.76 2.58 2 -7 -23 47.33 2.53 -2 7 -23 41.11 2.06 -2 7 -23 47.30 2.56 2 -7 -24 10.99 1.18 -2 7 -24 9.83 1.10 2 -7 -25 27.21 1.71 -2 7 -25 42.88 2.50 2 -7 -25 40.91 2.02 -2 7 -25 32.57 1.85 -2 7 -25 43.30 2.18 2 -7 -26 9.87 0.84 -2 7 -26 17.61 1.36 2 -7 -26 17.01 1.07 -2 7 -26 9.92 0.86 -2 7 -26 17.98 1.19 -2 -8 -24 17.07 1.13 2 8 -24 20.75 1.27 2 8 -23 6.88 0.85 2 8 -23 6.57 0.83 2 8 -22 38.87 2.16 2 8 -22 33.21 2.01 2 8 -22 39.51 2.19 2 8 -21 1.88 0.71 2 8 -21 1.06 0.73 2 8 -21 0.50 0.71 -2 8 20 2.14 0.79 2 8 -20 1.57 0.83 2 8 -20 2.50 0.89 -2 8 19 4.72 1.03 2 8 -19 4.05 1.19 2 8 -19 5.74 1.20 -2 8 19 7.58 1.32 -2 8 18 2.72 0.96 2 8 -18 2.28 1.15 2 8 -18 2.93 1.05 -2 8 18 1.14 0.91 2 8 -17 22.54 2.13 -2 8 17 25.51 2.22 2 8 -17 21.35 2.40 -2 8 17 23.40 2.35 2 8 -17 22.53 2.17 2 8 -16 58.75 4.07 2 8 -16 58.23 3.54 -2 8 16 57.50 3.53 -2 8 16 58.50 3.84 2 8 -16 61.34 3.76 2 8 -15 140.60 6.12 2 8 -15 141.04 6.95 -2 8 15 138.12 6.12 -2 8 15 142.59 6.54 2 8 -15 132.04 6.19 2 8 -14 123.37 5.79 2 8 -14 133.94 6.82 2 8 -14 130.70 6.14 -2 8 14 128.12 5.92 -2 8 14 137.80 6.42 2 8 -13 189.86 7.65 2 8 -13 191.40 8.61 -2 8 13 190.21 7.70 -2 8 13 197.32 8.18 2 8 -13 194.35 7.93 -2 8 13 175.40 7.17 2 8 -12 85.41 4.45 2 8 -12 79.05 8.76 2 8 -12 88.30 5.38 2 -8 12 80.03 7.96 -2 8 12 86.52 4.55 -2 8 12 88.10 4.90 2 8 -12 86.49 4.72 -2 8 12 84.09 4.37 2 -8 11 228.16 13.93 2 8 -11 248.08 15.67 2 8 -11 226.42 9.63 -2 8 11 215.92 8.45 -2 8 11 232.11 8.62 -2 8 11 222.30 8.98 2 8 -11 226.38 8.81 2 8 -11 243.13 8.58 2 8 -10 152.87 6.36 -2 8 10 140.10 12.69 2 8 -10 113.48 6.07 2 8 -10 163.58 12.45 2 8 -10 141.93 6.58 2 8 -10 149.94 5.84 2 -8 10 144.22 10.79 -2 8 10 151.90 6.88 -2 8 10 145.40 6.39 -2 8 10 150.70 6.65 2 8 -9 30.26 2.50 -2 8 9 31.42 2.85 2 8 -9 31.22 2.78 2 8 -9 33.11 5.55 -2 8 9 28.29 2.51 2 -8 9 32.81 5.02 2 8 -9 29.35 2.70 -2 8 9 39.86 3.09 2 8 -8 160.91 6.54 -2 8 8 156.19 6.75 -2 8 8 171.39 7.29 2 8 -8 141.29 6.87 2 8 -8 152.38 11.83 -2 8 8 152.00 13.48 2 8 -8 165.17 7.08 2 -8 8 150.89 10.93 -2 8 8 148.88 6.96 -2 8 7 71.96 4.10 2 8 -7 73.45 3.91 2 8 -7 58.33 4.11 2 8 -7 70.91 7.80 2 8 -7 74.07 4.78 -2 8 7 65.61 8.94 2 -8 7 57.74 6.62 -2 8 7 79.81 4.57 -2 8 7 77.26 4.58 2 8 -7 73.15 4.28 2 8 -6 47.87 3.02 -2 8 6 51.45 7.79 -2 8 6 53.14 3.65 2 -8 6 44.17 5.69 2 8 -6 44.05 3.50 2 8 -6 50.65 3.48 -2 8 6 47.45 3.24 2 8 -6 52.36 3.94 -2 8 6 52.32 3.75 -2 8 5 203.46 8.39 2 8 -5 201.99 8.64 2 8 -5 199.58 8.83 2 8 -5 208.28 8.35 2 8 -5 204.53 7.64 -2 8 5 213.13 8.78 -2 8 5 209.12 15.91 -2 8 5 198.73 8.03 2 -8 5 212.40 12.70 2 8 -4 244.08 8.73 2 8 -4 248.26 10.02 2 -8 4 253.86 14.06 2 8 -4 249.56 9.60 2 8 -4 242.68 10.09 -2 8 4 249.46 10.05 -2 8 4 254.98 9.77 -2 8 4 254.36 9.39 2 8 -3 13.26 1.97 2 -8 3 11.05 2.85 -2 8 3 13.34 1.76 -2 8 3 12.50 4.12 -2 8 3 13.47 2.06 2 8 -3 12.83 1.45 -2 8 3 11.67 1.84 2 8 -3 14.46 2.11 -2 8 2 43.13 3.03 2 8 -2 39.22 3.28 -2 8 2 35.28 6.61 2 8 -2 41.25 3.45 -2 8 2 40.54 3.21 2 -8 2 36.35 4.89 2 8 -2 39.15 2.48 -2 8 1 103.52 11.10 2 8 -1 109.67 5.83 -2 8 1 114.79 5.63 2 8 -1 102.29 5.71 2 -8 1 101.03 8.15 -2 8 1 102.04 5.11 -2 8 0 15.34 4.45 2 8 0 12.17 1.94 -2 8 0 13.11 1.92 2 8 0 9.89 1.81 2 -8 0 13.25 2.99 -2 8 0 13.73 2.13 -2 8 0 12.56 1.66 2 8 1 111.11 5.87 -2 8 -1 112.91 5.32 2 -8 -1 100.97 7.92 -2 8 -1 106.61 5.49 -2 8 -1 119.96 11.55 -2 8 -1 98.96 5.68 -2 8 -2 33.52 6.29 2 8 2 45.64 3.50 -2 8 -2 43.12 3.26 -2 8 -2 39.39 2.95 -2 8 -2 44.29 3.55 2 -8 -2 31.28 4.29 -2 8 -3 13.34 1.96 2 8 3 15.87 2.16 -2 8 -3 10.85 1.71 -2 8 -3 8.54 3.42 -2 8 -3 16.07 2.21 2 8 3 11.40 1.95 -2 8 -3 13.90 1.83 -2 8 -4 249.91 10.07 2 8 4 264.42 10.32 2 8 4 258.00 10.06 -2 8 -4 250.31 9.75 -2 8 -4 262.41 17.32 -2 -8 4 246.48 13.23 -2 8 -4 251.98 9.67 -2 8 -4 247.15 9.41 -2 8 -4 245.99 9.62 2 8 5 208.19 8.74 -2 8 -5 198.85 8.43 -2 8 -5 187.26 14.37 2 8 5 199.41 8.46 -2 8 -5 197.91 7.99 -2 -8 5 194.71 11.74 -2 8 -5 198.31 8.16 -2 8 -5 204.26 8.58 2 8 6 49.55 3.71 2 8 6 47.24 3.54 -2 8 -6 47.07 3.25 -2 8 -6 45.54 3.54 -2 8 -6 51.08 3.70 -2 8 -6 54.09 7.35 -2 -8 6 46.92 5.57 -2 8 -6 46.86 3.37 -2 -8 7 72.84 7.17 2 8 7 73.05 4.50 -2 8 -7 69.87 4.53 2 8 7 76.23 4.50 -2 8 -7 83.28 4.68 -2 8 -7 69.77 4.23 2 8 8 162.07 7.23 -2 8 -8 158.63 7.56 -2 -8 8 162.00 11.29 -2 8 -8 162.85 7.25 2 8 8 169.75 7.37 -2 8 -8 155.34 6.99 2 8 9 29.03 2.69 2 8 9 28.71 2.71 -2 8 -9 32.05 3.10 -2 -8 9 33.86 5.10 -2 8 -9 31.30 2.73 -2 8 -9 27.65 2.62 2 8 10 148.74 6.70 2 8 10 144.40 6.74 -2 -8 10 159.63 11.44 -2 8 -10 140.55 6.49 -2 8 -10 148.84 6.71 2 8 11 222.90 8.90 2 8 11 224.05 8.85 -2 -8 11 242.68 14.71 -2 8 -11 231.76 9.02 -2 8 -11 221.47 8.67 2 8 12 86.79 4.65 2 8 12 80.06 4.36 -2 8 -12 87.46 4.79 -2 -8 12 84.33 8.46 -2 8 -12 80.14 4.27 2 8 13 193.27 7.72 -2 8 -13 189.30 7.88 -2 8 -13 176.06 7.54 -2 8 -14 130.60 5.99 -2 8 -14 107.72 5.46 -2 8 -15 137.02 6.28 -2 8 -15 133.65 6.03 -2 8 -16 53.28 3.53 -2 8 -16 54.80 3.41 -2 8 -17 19.91 2.08 -2 8 -17 18.95 1.95 -2 8 -18 2.54 0.93 -2 8 -18 2.05 1.25 -2 8 -18 0.70 0.83 2 -8 -19 4.60 1.08 -2 8 -19 5.85 1.14 -2 8 -19 4.67 1.43 -2 8 -19 5.23 1.14 -2 8 -20 1.39 0.70 -2 8 -20 1.03 0.90 2 -8 -20 2.43 0.87 -2 8 -20 1.71 0.83 -2 8 -20 0.60 0.85 -2 8 -21 0.87 0.61 -2 8 -21 1.53 0.97 -2 8 -21 0.56 0.64 2 -8 -21 0.65 0.69 -2 8 -21 1.20 0.77 2 -8 -22 41.03 2.21 -2 8 -22 36.79 1.97 -2 8 -22 40.44 2.37 -2 8 -22 36.15 2.61 -2 8 -22 36.79 2.18 -2 8 -23 6.86 0.96 2 -8 -23 5.51 0.76 -2 8 -23 6.06 0.77 2 -8 -24 27.71 1.38 -2 8 -24 17.29 1.16 2 -8 -24 18.49 1.18 -2 8 -24 26.81 1.53 -2 8 -25 16.71 1.17 -2 8 -25 16.29 1.03 2 9 -21 3.47 0.66 2 9 -21 3.21 0.64 2 9 -20 16.75 1.44 2 9 -20 14.23 1.33 2 9 -19 48.32 2.61 2 9 -19 46.11 2.52 2 9 -19 44.38 2.70 2 9 -18 12.93 1.36 2 9 -18 12.05 1.52 -2 9 18 9.29 1.01 -2 9 18 12.06 1.40 2 9 -18 13.67 1.44 2 9 -17 46.79 2.87 -2 9 17 45.65 2.48 2 9 -17 45.43 3.09 -2 9 17 42.61 2.78 2 9 -17 46.80 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2.12 4 -3 -19 18.30 1.69 -4 3 -19 19.33 4.40 4 3 19 21.49 2.34 4 -3 -19 17.00 4.10 -4 -3 19 13.80 3.32 4 -3 -19 18.40 4.10 4 -3 -20 156.25 6.66 4 -3 -20 155.71 6.77 4 -3 -20 156.86 6.03 4 3 20 171.06 7.25 4 -3 -21 9.74 1.52 4 -3 -21 9.29 1.55 4 -3 -21 9.18 1.18 4 3 21 12.10 1.82 4 -3 -22 100.28 4.82 4 -3 -22 104.16 4.95 4 -3 -22 96.29 4.18 4 3 22 106.24 5.25 4 -3 -23 157.21 6.46 4 -3 -23 161.65 6.57 4 -3 -23 153.91 5.69 4 3 23 175.88 6.93 4 3 24 46.53 3.00 4 -3 -24 43.18 2.79 4 3 25 76.38 3.87 4 -3 -25 76.93 3.76 4 -3 -26 2.52 0.82 4 3 26 3.52 0.92 4 -3 -27 1.06 0.61 4 3 27 0.67 0.58 4 3 27 0.36 0.51 4 3 28 47.29 2.05 4 -3 -28 40.70 1.88 4 -3 -29 3.37 0.51 4 3 29 2.96 0.50 4 4 -27 21.41 1.35 4 4 -27 20.20 1.30 4 4 -26 7.43 0.94 4 -4 26 4.97 0.68 4 4 -26 7.53 0.95 4 4 -25 56.52 2.86 4 -4 25 54.16 2.62 4 4 -25 54.24 2.82 4 4 -24 3.05 0.85 4 4 -24 3.98 0.93 4 -4 24 3.40 0.82 4 4 -23 54.83 3.21 -4 4 23 59.29 3.50 4 -4 23 57.08 3.07 4 4 -23 54.90 3.14 4 4 -22 110.29 4.93 -4 4 22 116.91 5.33 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0.37 1.03 4 4 -13 1.05 0.80 4 4 -13 1.94 1.71 -4 4 13 0.86 1.52 -4 -4 -13 1.46 1.92 -4 4 13 1.42 1.09 4 4 -13 0.09 0.63 -4 4 13 0.49 0.96 -4 4 13 0.37 1.21 4 4 -12 69.73 3.72 4 4 -12 70.05 7.62 -4 4 12 66.24 6.52 -4 4 12 56.47 6.82 -4 4 12 72.51 4.15 -4 4 12 60.01 3.40 -4 -4 -12 64.03 7.38 4 -4 12 70.24 6.76 -4 4 12 68.42 4.09 4 4 -12 69.99 3.63 4 4 -12 60.86 3.44 4 4 -11 153.08 6.19 -4 4 11 162.14 6.72 4 4 -11 151.33 11.26 -4 4 11 171.80 10.58 -4 4 11 142.58 11.01 -4 4 11 125.29 5.83 -4 -4 -11 160.72 11.62 4 -4 11 151.05 10.17 -4 4 11 165.53 6.85 4 4 -11 165.21 6.24 4 4 -10 78.23 3.91 4 4 -10 83.88 3.95 4 4 -10 69.71 3.92 4 4 -10 80.59 7.81 -4 4 10 94.03 8.57 -4 4 10 80.75 4.30 -4 4 10 91.80 7.36 -4 4 10 74.85 3.94 -4 -4 -10 93.92 8.42 4 -4 10 84.51 7.29 -4 4 10 81.07 4.39 4 -4 10 80.24 3.95 4 4 -9 166.90 6.23 -4 4 9 158.66 9.92 4 4 -9 149.29 6.30 4 4 -9 168.31 11.31 4 4 -9 156.75 6.23 -4 4 9 142.78 11.36 -4 4 9 137.50 6.16 -4 -4 -9 161.59 11.41 -4 4 9 164.44 6.74 4 4 -9 165.83 6.15 4 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6.01 4 -4 2 95.52 4.34 4 4 -2 95.17 6.59 -4 4 2 101.63 7.17 -4 -4 -2 109.76 7.66 4 -4 2 99.05 6.60 4 -4 2 109.63 7.93 4 4 -1 571.63 21.22 -4 -4 -1 589.63 22.48 4 -4 1 669.23 23.90 4 -4 1 596.88 22.12 -4 4 1 590.64 23.90 -4 4 1 646.82 23.10 -4 -4 0 178.92 9.71 -4 4 0 195.40 10.42 4 4 0 175.29 8.72 4 -4 0 184.38 10.66 -4 4 0 186.78 11.10 -4 -4 0 188.17 9.74 4 -4 0 150.71 9.24 4 4 1 599.92 20.09 -4 4 -1 604.55 24.09 4 -4 -1 605.44 23.40 4 -4 -1 569.42 22.35 -4 -4 1 617.87 22.31 -4 -4 2 105.09 7.12 -4 4 -2 109.46 8.33 4 -4 -2 104.35 7.76 4 -4 -2 96.73 7.37 4 -4 -3 97.53 4.46 4 4 3 99.84 4.81 -4 -4 3 108.91 7.13 4 -4 -3 108.09 7.85 4 4 3 101.58 4.46 -4 4 -3 100.92 8.07 4 -4 -4 55.45 3.12 -4 -4 4 56.10 5.07 4 4 4 51.25 3.29 4 4 4 57.79 3.12 -4 4 -4 63.56 6.33 4 -4 -4 47.80 5.37 -4 -4 5 73.43 5.83 4 -4 -5 70.63 3.63 4 4 5 64.83 3.81 4 4 5 69.95 3.61 -4 4 -5 76.34 7.20 4 -4 -5 62.55 6.27 4 -4 -6 73.42 3.83 4 4 6 76.20 3.87 -4 4 -6 77.29 7.32 4 -4 -6 76.23 7.10 -4 4 -6 91.36 7.84 -4 -4 6 75.58 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7.43 4 -4 -12 62.79 3.54 -4 4 -13 0.54 1.64 4 -4 -13 0.74 0.86 4 4 13 0.82 0.91 4 -4 -13 2.39 2.23 4 -4 -13 0.38 0.69 -4 -4 13 1.76 1.58 4 -4 -14 57.17 3.63 -4 -4 14 61.92 6.36 -4 4 -14 59.38 7.74 4 -4 -14 63.32 3.56 4 -4 -15 122.53 5.74 -4 -4 15 127.23 9.49 4 -4 -16 64.70 3.91 -4 -4 16 68.05 6.90 4 -4 -16 63.73 7.67 4 -4 -17 96.83 4.84 -4 -4 17 81.74 7.66 4 -4 -17 95.97 4.91 4 -4 -17 102.83 9.82 -4 4 -17 91.59 9.67 4 -4 -17 94.81 9.40 4 -4 -18 72.33 4.01 4 -4 -18 69.70 4.05 -4 4 -18 59.75 7.76 4 -4 -18 56.34 7.34 4 -4 -18 58.61 7.41 4 -4 -19 1.45 1.04 4 -4 -19 0.96 0.97 4 -4 -19 2.48 0.76 4 -4 -20 66.92 3.78 4 -4 -20 61.08 3.73 4 -4 -20 61.70 3.15 4 -4 -21 118.20 5.25 4 -4 -21 120.12 5.32 4 -4 -22 111.85 5.00 4 -4 -22 109.69 4.91 4 -4 -22 100.36 4.16 4 -4 -23 54.00 3.14 4 -4 -24 5.02 1.04 4 4 24 3.00 0.81 4 4 25 45.78 2.47 4 -4 -25 60.51 2.94 4 -4 -26 6.17 0.94 4 4 26 3.92 0.65 4 -4 -27 24.92 1.56 4 -4 -28 7.62 0.76 4 5 -26 18.47 1.28 4 5 -25 3.41 0.69 4 5 -25 4.54 0.82 4 5 -24 1.36 0.59 4 5 -24 2.52 0.77 4 5 -23 37.60 2.41 4 5 -23 36.70 2.33 4 5 -22 50.74 2.96 -4 5 22 46.61 3.10 4 5 -22 46.82 2.83 4 5 -21 109.08 4.84 -4 5 21 112.88 5.22 4 5 -21 103.04 4.66 -4 5 20 38.42 3.06 -4 5 20 42.51 3.11 4 5 -20 38.79 2.67 4 5 -20 34.49 2.27 -4 5 19 95.72 5.02 -4 5 19 94.03 4.92 4 5 -19 79.37 4.22 4 5 -19 79.59 3.86 4 5 -18 2.80 0.98 4 5 -18 2.93 0.82 -4 5 18 3.32 1.33 -4 5 18 2.40 1.16 4 5 -17 48.28 3.17 -4 5 17 42.76 3.38 -4 5 17 47.90 3.52 4 5 -17 47.34 3.12 4 5 -17 39.31 2.64 4 5 -16 47.13 3.13 4 5 -16 39.07 5.99 -4 5 16 49.27 3.60 4 -5 16 38.34 5.27 -4 5 16 41.02 3.32 -4 -5 -16 45.65 6.67 4 5 -16 42.69 2.97 4 5 -16 39.94 2.65 4 5 -15 332.85 11.23 4 5 -15 300.34 10.82 4 5 -15 339.32 18.87 -4 5 15 318.26 11.75 -4 -5 -15 332.52 18.82 4 -5 15 309.22 16.52 -4 5 15 327.82 11.91 4 5 -15 328.20 11.15 4 5 -14 67.83 3.83 4 5 -14 59.61 3.62 4 5 -14 64.08 7.68 -4 5 14 54.69 6.92 -4 5 14 70.35 4.29 -4 -5 -14 62.59 7.60 4 -5 14 65.02 6.86 -4 5 14 68.24 4.31 4 5 -14 67.14 3.74 4 5 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6.49 4 5 -8 56.92 3.29 -4 5 8 60.93 5.48 -4 5 8 57.47 7.10 -4 5 8 54.82 3.43 -4 5 8 59.97 3.61 -4 -5 -8 60.63 6.77 4 -5 8 58.64 6.23 -4 5 8 52.78 3.49 4 5 -7 12.44 1.40 4 5 -7 10.92 1.64 4 5 -7 12.99 1.54 -4 5 7 16.58 2.89 4 5 -7 12.86 3.08 -4 5 7 14.31 1.79 -4 5 7 12.65 1.64 -4 5 7 13.35 3.72 -4 -5 -7 9.37 2.94 -4 5 7 10.72 1.58 4 5 -6 68.24 3.36 4 5 -6 64.55 3.91 4 5 -6 67.54 6.64 4 5 -6 72.59 3.71 -4 5 6 72.07 7.83 -4 5 6 75.65 4.09 -4 5 6 67.00 3.82 -4 5 6 62.36 5.43 -4 5 6 63.80 3.81 4 5 -5 185.72 6.69 4 5 -5 181.01 7.58 4 5 -5 189.72 11.38 4 5 -5 204.10 7.32 -4 5 5 204.65 13.67 -4 5 5 194.10 7.70 4 -5 5 189.94 11.57 -4 5 5 185.42 9.87 -4 5 5 182.24 7.42 -4 5 5 183.07 7.36 4 -5 4 4.12 1.02 4 5 -4 2.65 0.68 4 5 -4 2.29 0.94 -4 5 4 3.50 1.14 4 5 -4 3.11 1.55 4 5 -4 4.46 1.04 -4 5 4 3.72 1.06 4 -5 4 5.67 2.22 -4 5 4 3.47 1.42 -4 5 4 3.61 1.02 -4 5 3 5.37 2.59 -4 5 3 1.37 1.03 4 -5 3 2.15 0.75 4 5 -3 1.30 0.81 -4 5 3 3.09 1.12 4 5 -3 1.15 1.08 4 5 -3 2.71 0.89 -4 5 3 1.78 0.85 4 -5 3 3.16 1.70 -4 5 3 1.82 0.87 -4 5 2 184.30 9.71 4 -5 2 195.24 7.29 4 -5 2 207.59 11.94 4 5 -2 186.26 7.68 4 5 -2 192.55 10.52 4 5 -2 198.68 7.27 -4 5 2 221.36 14.23 -4 5 2 187.60 7.39 -4 5 2 192.24 7.48 4 -5 1 68.06 3.51 4 5 -1 68.66 5.55 4 5 -1 65.31 3.83 -4 5 1 62.29 5.21 4 5 -1 63.07 3.40 -4 5 1 65.83 7.46 -4 5 1 59.15 3.47 4 -5 1 60.52 6.11 4 -5 1 59.39 5.30 -4 5 1 62.36 3.55 4 -5 0 138.56 5.65 4 5 0 146.13 8.07 4 5 0 129.60 6.03 4 5 0 142.92 5.66 -4 5 0 131.98 6.10 -4 5 0 125.76 7.86 -4 5 0 131.85 5.72 4 -5 0 140.06 9.50 4 -5 0 143.69 8.82 -4 5 0 128.38 5.70 4 -5 -1 64.38 3.44 -4 5 -1 68.67 5.49 4 5 1 61.39 3.79 4 5 1 62.88 3.36 -4 5 -1 58.67 7.07 -4 5 -1 67.15 3.94 -4 5 -1 78.40 7.60 4 -5 -1 62.61 6.12 -4 5 -1 59.05 3.45 4 -5 -1 56.61 5.53 -4 5 -1 61.06 3.48 -4 5 -2 188.34 10.21 4 -5 -2 190.57 7.32 4 5 2 192.93 7.89 4 -5 -2 214.50 12.07 4 5 2 200.43 7.36 -4 5 -2 217.76 13.83 -4 5 -2 230.94 8.25 -4 5 -2 208.85 13.17 -4 5 -2 188.71 7.47 4 -5 -2 181.70 10.94 -4 5 -2 189.26 7.42 4 -5 -3 2.09 0.80 4 5 3 1.90 0.89 -4 5 -3 2.59 1.13 4 5 3 4.25 0.93 -4 5 -3 3.13 2.01 -4 5 -3 1.28 1.68 -4 5 -3 2.07 0.84 4 -5 -3 2.02 1.46 4 -5 -3 4.01 1.86 -4 5 -3 1.26 0.78 4 -5 -4 2.76 0.88 -4 5 -4 3.51 1.08 4 5 4 2.86 0.87 -4 5 -4 2.19 1.97 -4 5 -4 2.48 0.96 -4 5 -4 2.60 1.87 4 -5 -4 3.17 1.82 -4 5 -4 2.53 0.94 4 -5 -5 192.03 7.47 -4 5 -5 211.07 13.50 4 5 5 191.64 7.40 -4 5 -5 203.60 12.97 -4 5 -5 213.98 7.92 4 -5 -5 188.00 11.93 -4 5 -5 190.30 7.46 4 -5 -6 64.87 3.66 4 5 6 66.65 3.69 -4 5 -6 65.71 7.07 -4 5 -6 70.01 3.88 -4 5 -6 71.84 7.63 4 -5 -6 58.20 6.40 -4 5 -6 66.60 3.68 4 -5 -7 12.95 3.17 4 -5 -7 15.49 1.69 4 5 7 13.48 1.84 4 5 7 14.40 1.68 -4 5 -7 13.48 3.32 -4 5 -7 12.40 1.67 -4 5 -7 14.68 3.75 -4 5 -7 12.69 1.56 -4 5 -8 56.53 7.07 4 -5 -8 56.08 3.39 4 5 8 56.22 3.77 4 5 8 63.44 3.58 -4 5 -8 54.31 6.20 -4 5 -8 51.73 3.30 4 -5 -8 58.00 6.59 -4 5 -8 56.12 3.40 4 -5 -9 18.41 1.92 4 5 9 19.22 2.15 4 5 9 16.96 1.89 -4 5 -9 13.69 1.68 -4 5 -9 14.61 3.25 -4 5 -9 19.96 4.40 4 -5 -9 14.81 3.59 -4 5 -9 16.00 1.84 4 -5 -10 18.27 1.92 4 5 10 12.33 1.82 4 5 10 15.04 1.83 -4 5 -10 15.00 1.71 -4 5 -10 15.48 4.07 4 -5 -10 16.65 3.79 4 -5 -11 103.15 5.15 4 -5 -11 126.75 10.28 4 5 11 107.11 5.67 4 5 11 118.52 5.54 -4 5 -11 121.49 10.95 -4 5 -11 106.71 4.94 4 -5 -12 34.65 2.73 4 5 12 37.15 3.10 4 -5 -12 37.29 5.65 4 5 12 39.35 3.00 -4 5 -12 37.12 6.17 4 -5 -13 183.61 7.58 4 5 13 192.37 7.93 -4 5 -13 221.60 15.49 4 -5 -13 193.33 13.48 4 -5 -14 64.81 3.88 4 5 14 69.85 4.18 -4 5 -14 63.39 8.25 4 -5 -14 62.12 7.50 4 5 14 67.48 3.62 4 -5 -15 331.35 11.52 4 5 15 337.70 11.94 4 -5 -15 305.08 18.10 4 5 15 321.02 10.97 4 -5 -16 44.02 3.07 4 5 16 40.01 3.18 4 5 16 39.89 2.72 -4 5 -16 36.88 2.49 4 -5 -17 43.15 3.07 4 -5 -17 46.10 3.12 4 5 17 42.13 3.23 4 5 17 42.28 2.78 4 -5 -18 2.28 1.05 4 -5 -18 2.55 1.00 4 5 18 2.62 1.08 4 5 18 2.68 0.96 4 -5 -19 87.87 4.53 4 -5 -19 85.11 4.43 4 5 19 95.19 4.86 4 5 19 91.92 4.25 4 -5 -20 41.03 2.80 4 -5 -20 40.88 2.78 4 -5 -20 36.33 2.20 4 5 20 42.36 3.00 4 5 20 36.19 2.40 4 -5 -21 109.26 4.84 4 -5 -21 107.64 4.70 4 5 21 108.51 4.99 4 5 21 98.55 4.22 4 -5 -22 48.24 2.90 4 -5 -22 53.06 2.93 4 5 22 46.25 3.00 4 5 22 44.42 2.41 4 -5 -23 37.37 2.40 4 5 23 35.13 2.39 -4 5 -23 31.87 2.03 4 -5 -24 1.69 0.71 4 5 24 1.85 0.77 -4 5 -24 2.00 0.58 4 5 25 3.77 0.78 4 5 26 17.80 1.30 4 5 27 4.58 0.58 4 6 -25 14.05 1.05 4 -6 25 8.72 0.86 4 6 -24 11.52 1.10 4 6 -23 2.84 0.77 -4 6 23 2.98 0.84 4 6 -21 5.10 0.94 -4 6 20 40.71 2.88 4 6 -20 39.01 2.50 4 6 -19 64.12 3.50 -4 6 19 63.91 3.81 4 6 -19 55.93 2.94 4 6 -19 62.41 3.36 4 6 -18 15.21 1.76 -4 6 18 12.70 1.85 4 6 -18 12.51 1.39 4 6 -18 15.36 1.68 4 6 -17 43.78 2.84 -4 6 17 50.62 3.57 4 6 -17 52.76 2.93 4 6 -17 50.78 3.13 4 6 -16 67.66 3.78 4 6 -16 61.39 3.56 -4 6 16 68.61 4.24 4 6 -16 64.33 3.40 4 6 -16 60.53 3.53 4 6 -15 187.83 7.33 4 6 -15 173.19 7.21 -4 6 15 184.34 7.92 4 6 -15 179.06 6.83 4 6 -15 181.34 7.12 4 6 -14 42.28 2.91 4 6 -14 41.79 3.03 4 6 -14 51.84 6.92 -4 -6 -14 38.47 5.85 4 -6 14 41.09 5.61 -4 6 14 48.02 3.47 4 6 -14 42.90 2.72 4 6 -14 41.72 2.84 4 6 -13 62.13 3.57 4 6 -13 65.20 3.91 4 6 -13 51.03 6.90 -4 6 13 42.71 6.47 -4 -6 -13 51.48 6.85 4 -6 13 53.98 6.47 -4 6 13 63.27 3.53 -4 6 13 59.99 4.00 4 6 -13 59.22 3.29 4 6 -13 56.25 3.35 4 6 -12 75.09 3.96 4 6 -12 72.12 4.27 4 6 -12 71.41 8.02 -4 6 12 59.94 7.79 -4 -6 -12 70.69 7.89 4 -6 12 76.22 7.64 -4 6 12 68.98 3.90 -4 6 12 73.43 4.45 4 6 -11 17.92 1.80 -4 6 11 11.48 3.57 4 -6 11 12.77 3.22 4 6 -11 15.06 1.94 4 6 -11 16.34 3.91 -4 6 11 17.11 2.14 -4 -6 -11 16.12 3.86 -4 6 11 15.34 1.87 -4 6 11 16.87 2.08 4 6 -10 6.11 1.14 4 6 -10 4.77 1.32 -4 6 10 3.88 1.33 4 -6 10 3.37 1.90 4 6 -10 5.12 2.47 -4 6 10 3.61 1.11 -4 6 10 3.85 2.38 -4 6 10 4.58 1.35 -4 -6 -10 5.55 2.59 4 6 -9 48.17 2.89 4 6 -9 45.40 3.40 4 6 -9 49.10 6.21 -4 6 9 40.82 6.42 -4 6 9 47.75 3.40 -4 6 9 41.84 3.07 -4 -6 -9 42.17 5.88 -4 6 9 41.35 3.20 4 6 -8 83.98 4.03 4 6 -8 88.41 4.90 4 6 -8 84.35 8.09 -4 6 8 81.89 4.57 -4 6 8 95.05 9.58 -4 6 8 82.20 4.47 -4 -6 -8 80.32 7.97 -4 6 8 76.68 4.52 4 6 -7 176.97 6.62 -4 6 7 166.91 7.32 4 6 -7 177.14 7.69 4 6 -7 178.95 11.87 4 6 -7 179.44 6.96 -4 6 7 192.08 13.92 -4 6 7 185.63 7.50 -4 6 7 164.17 7.19 4 -6 7 174.47 11.67 4 6 -6 238.47 8.22 4 -6 6 249.41 8.90 4 6 -6 231.28 9.34 4 6 -6 258.93 14.18 4 6 -6 239.14 8.65 -4 6 6 244.65 15.99 -4 6 6 237.24 9.11 -4 6 6 227.98 9.02 4 -6 6 239.23 14.00 -4 6 6 232.55 9.09 4 6 -5 59.81 3.13 4 -6 5 66.73 3.69 4 6 -5 52.57 5.98 4 6 -5 68.29 4.18 4 6 -5 63.72 3.55 -4 6 5 74.20 8.48 -4 6 5 65.92 3.99 -4 6 5 68.78 3.96 4 -6 5 68.69 6.98 -4 6 5 59.52 3.78 4 -6 4 213.12 7.97 4 6 -4 210.15 12.20 4 6 -4 205.83 8.55 4 6 -4 220.39 7.95 4 -6 4 216.67 13.03 -4 6 4 201.62 8.30 -4 6 4 204.98 8.24 -4 6 4 211.72 8.31 4 -6 3 109.65 5.06 4 6 -3 118.41 8.49 4 6 -3 112.34 5.69 4 6 -3 116.81 5.09 -4 6 3 110.73 10.42 -4 6 3 113.94 5.54 -4 6 3 104.77 5.28 4 -6 3 121.12 9.33 -4 6 3 108.18 5.34 -4 6 2 21.63 2.17 4 -6 2 23.58 2.11 4 6 -2 25.44 2.48 4 6 -2 27.39 2.13 4 6 -2 17.69 3.19 -4 6 2 17.76 4.45 -4 6 2 21.41 2.17 4 -6 2 30.86 4.61 4 -6 1 219.84 8.11 4 6 -1 213.11 11.41 4 6 -1 213.19 8.74 4 6 -1 202.55 8.66 4 6 -1 215.31 7.97 -4 6 1 225.14 15.00 -4 6 1 223.34 8.51 4 -6 1 215.82 12.89 -4 6 1 218.00 8.38 4 -6 0 337.45 11.33 4 6 0 328.44 12.04 4 6 0 303.95 11.91 4 6 0 345.96 11.29 -4 6 0 382.13 20.12 -4 6 0 342.10 11.96 -4 6 0 332.66 11.66 4 -6 0 348.58 17.10 -4 6 0 337.63 11.67 4 -6 -1 216.92 8.02 4 6 1 209.69 8.66 -4 6 -1 210.04 8.31 4 6 1 220.56 7.99 -4 6 -1 223.08 14.79 -4 6 -1 216.93 8.58 4 -6 -1 213.84 12.74 4 -6 -1 194.97 11.42 -4 6 -1 216.03 8.32 4 -6 -2 24.10 2.11 -4 6 -2 22.08 2.15 4 6 2 20.81 1.91 -4 6 -2 22.47 2.34 -4 6 -2 20.86 4.62 4 -6 -2 18.69 3.60 4 -6 -2 19.38 3.49 -4 6 -2 24.94 2.28 4 -6 -3 116.92 5.21 4 6 3 110.63 5.07 -4 6 -3 122.15 10.42 -4 6 -3 119.14 5.67 -4 6 -3 112.21 5.44 4 -6 -3 102.23 8.37 4 -6 -3 119.36 9.11 -4 6 -3 116.33 5.43 4 -6 -4 216.38 8.03 -4 6 -4 210.50 8.32 4 6 4 210.43 7.89 -4 6 -4 200.86 13.87 -4 6 -4 215.77 14.53 -4 6 -4 197.55 8.18 4 -6 -4 205.54 12.52 -4 6 -4 222.13 8.31 4 -6 -5 62.75 3.58 4 6 5 59.15 3.98 4 6 5 58.28 3.41 -4 6 -5 58.67 7.13 4 -6 -5 60.07 6.57 -4 6 -5 60.47 7.44 -4 6 -5 62.43 3.80 -4 6 -5 61.26 3.78 -4 6 -5 60.49 3.68 4 -6 -6 235.62 8.67 -4 6 -6 223.50 8.78 4 6 6 234.24 9.34 4 6 6 222.51 8.48 -4 6 -6 236.08 14.79 -4 6 -6 242.84 15.72 4 -6 -6 227.38 13.81 -4 6 -6 227.35 8.89 -4 6 -6 239.91 8.88 4 -6 -7 171.34 7.14 4 6 7 181.06 7.96 4 6 7 180.57 7.19 -4 6 -7 171.20 12.34 -4 6 -7 177.42 13.46 -4 6 -7 193.59 7.56 4 -6 -7 174.39 12.04 -4 6 -7 184.96 7.46 4 -6 -8 82.09 4.30 4 6 8 81.51 4.77 4 6 8 82.03 4.29 -4 6 -8 76.75 7.91 -4 6 -8 97.30 9.85 4 -6 -8 77.48 7.92 -4 6 -8 75.43 4.27 -4 6 -8 81.41 4.41 4 -6 -9 45.46 3.07 4 6 9 47.38 3.51 4 6 9 47.43 3.15 -4 6 -9 52.90 7.38 -4 6 -9 40.34 2.97 4 -6 -9 37.36 5.64 -4 6 -9 45.69 3.19 4 -6 -10 4.24 1.16 4 6 10 4.78 1.32 -4 6 -10 2.12 1.01 4 6 10 3.96 1.09 -4 6 -10 4.14 2.56 4 -6 -10 6.07 2.61 -4 6 -10 4.56 1.23 4 -6 -11 15.53 1.82 4 6 11 19.24 2.26 4 6 11 17.14 1.97 -4 6 -11 15.70 4.42 -4 6 -11 15.09 1.81 4 -6 -11 13.85 3.60 -4 6 -11 15.19 1.93 4 -6 -12 79.64 4.21 4 -6 -12 79.31 8.34 4 6 12 78.34 4.74 4 6 12 72.11 4.18 -4 6 -12 84.15 9.63 -4 6 -12 68.43 3.88 -4 -6 12 87.28 8.74 -4 6 -12 77.20 4.35 4 -6 -13 61.00 3.66 4 6 13 62.57 3.85 -4 6 -13 68.07 8.73 4 -6 -13 53.76 6.92 -4 -6 13 71.71 8.01 -4 6 -13 67.97 3.99 4 -6 -14 44.03 3.03 4 -6 -14 41.79 6.19 4 6 14 42.11 3.11 -4 -6 14 41.57 6.09 -4 6 -14 44.13 3.18 4 -6 -15 179.86 7.28 4 6 15 185.19 7.62 -4 6 -15 188.53 7.65 4 -6 -16 63.60 3.67 4 6 16 67.86 3.98 -4 6 -16 69.46 3.96 -4 6 -16 63.02 3.42 4 -6 -17 53.71 3.21 4 6 17 56.53 3.50 -4 6 -17 53.05 3.39 -4 6 -17 45.29 2.75 4 -6 -18 13.72 1.72 4 -6 -18 14.27 1.63 4 6 18 13.02 1.68 -4 6 -18 11.45 1.62 -4 6 -18 13.83 1.38 4 -6 -19 56.72 3.39 4 -6 -19 58.43 3.21 4 6 19 54.61 3.35 -4 6 -19 62.94 3.51 4 -6 -20 43.85 2.80 4 -6 -20 41.00 2.53 4 6 20 39.70 2.68 -4 6 -20 43.99 2.75 4 -6 -21 6.31 1.11 4 -6 -21 5.75 0.98 4 6 21 6.27 1.08 -4 6 -21 5.60 1.04 4 6 22 1.98 0.73 -4 6 -22 1.72 0.70 4 6 23 2.43 0.68 -4 6 -23 2.56 0.67 4 6 24 10.77 1.02 -4 6 -24 8.98 0.83 4 6 25 11.63 0.90 -4 6 -25 11.60 1.00 -4 6 -26 0.59 0.40 4 -7 23 2.79 0.50 4 -7 22 28.42 1.74 -4 7 22 37.27 2.15 4 7 -21 51.22 2.61 4 -7 21 43.43 2.39 -4 7 21 49.13 2.75 4 7 -20 15.65 1.50 -4 7 20 16.95 1.71 -4 7 20 16.37 1.71 4 7 -19 8.83 1.21 -4 7 19 11.36 1.59 -4 7 19 9.76 1.48 4 7 -18 109.97 4.68 -4 7 18 111.92 5.17 -4 7 18 110.41 5.08 4 7 -17 14.25 1.60 4 7 -17 9.84 1.31 -4 7 17 16.49 1.96 -4 7 17 12.01 1.75 4 7 -16 91.21 4.33 4 7 -16 80.73 4.19 -4 7 16 95.35 4.95 -4 7 16 92.37 4.85 4 7 -16 83.04 3.87 4 7 -15 14.64 1.68 4 7 -15 16.40 1.84 -4 7 15 15.66 2.03 -4 7 15 16.26 2.09 4 7 -15 13.50 1.48 4 7 -14 2.50 0.93 4 7 -14 3.20 1.02 4 7 -14 2.23 0.83 -4 7 14 2.47 1.17 -4 7 14 2.26 1.19 4 7 -13 90.42 4.45 4 7 -13 92.24 4.94 -4 7 13 94.75 5.11 -4 7 13 93.69 4.48 4 7 -13 88.92 4.22 4 7 -12 42.86 2.84 4 7 -12 44.31 3.31 -4 7 12 43.43 3.37 -4 7 12 42.40 2.98 4 7 -12 41.12 2.67 4 7 -11 102.76 4.66 4 -7 11 97.44 4.71 4 7 -11 79.19 8.41 4 7 -11 91.55 5.15 -4 7 11 73.44 9.02 -4 -7 -11 77.94 8.25 4 -7 11 86.67 8.43 -4 7 11 107.29 5.05 -4 7 11 95.26 5.19 4 7 -11 91.40 4.36 4 7 -10 200.50 7.56 4 -7 10 208.61 7.89 4 7 -10 209.59 13.69 4 7 -10 197.96 8.52 -4 7 10 178.84 14.24 -4 -7 -10 175.28 12.70 -4 7 10 208.28 8.19 -4 7 10 206.04 8.47 4 7 -10 199.75 7.44 4 7 -9 31.90 2.33 4 -7 9 31.94 2.52 4 7 -9 35.87 3.06 4 7 -9 27.81 4.85 -4 7 9 30.43 5.84 -4 -7 -9 28.43 4.82 -4 7 9 32.44 2.75 4 -7 9 26.26 4.72 -4 7 9 31.00 2.80 4 7 -8 45.09 2.81 4 -7 8 49.27 3.16 4 7 -8 56.02 6.51 4 7 -8 51.68 3.75 -4 -7 -8 44.62 6.05 -4 7 8 41.84 6.90 4 -7 8 49.07 6.27 -4 7 8 49.96 3.50 -4 7 8 46.57 3.43 4 7 -7 18.14 1.69 4 -7 7 18.09 1.85 4 7 -7 20.01 2.35 4 7 -7 20.09 3.97 -4 7 7 12.36 4.04 -4 7 7 18.58 2.24 4 -7 7 14.10 3.51 -4 7 7 16.58 2.09 4 7 -6 59.20 3.11 4 -7 6 57.45 3.41 4 7 -6 53.47 6.41 4 7 -6 55.90 4.01 4 7 -6 58.76 3.31 -4 7 6 57.57 8.13 4 -7 6 51.61 6.40 -4 7 6 57.81 3.83 -4 7 6 59.24 3.89 4 -7 5 469.24 14.71 4 7 -5 426.81 20.37 4 7 -5 464.26 15.84 4 7 -5 458.21 14.44 -4 7 5 447.38 24.34 -4 7 5 452.45 15.41 4 -7 5 440.23 21.22 -4 7 5 448.03 15.29 4 -7 4 7.80 1.27 4 7 -4 7.54 1.57 4 7 -4 10.99 2.79 -4 7 4 8.04 1.66 4 7 -4 6.93 1.26 4 -7 4 8.96 2.77 -4 7 4 7.63 1.56 4 -7 3 6.70 1.22 4 7 -3 6.68 1.49 -4 7 3 7.69 1.66 4 7 -3 6.69 1.18 -4 7 3 8.58 3.34 4 -7 3 5.49 2.30 -4 7 3 9.68 1.67 -4 7 2 67.79 4.22 4 -7 2 76.05 3.96 4 7 -2 74.52 4.62 4 7 -2 70.82 3.77 -4 7 2 61.38 8.31 4 -7 2 75.34 7.48 4 -7 1 107.44 5.00 4 7 -1 111.06 5.87 4 7 -1 107.79 5.78 4 7 -1 113.24 4.99 -4 7 1 113.65 10.99 4 -7 1 107.32 9.03 -4 7 1 101.71 5.37 4 -7 0 1.04 0.73 -4 7 0 -0.40 1.00 4 7 0 0.90 0.66 4 -7 0 1.23 1.36 -4 7 0 1.19 2.34 -4 7 0 0.85 1.05 4 7 0 -0.43 1.02 -4 7 0 0.97 0.92 4 -7 -1 108.84 5.01 4 7 1 107.88 4.92 4 -7 -1 112.46 9.14 -4 7 -1 116.36 11.02 -4 7 -1 107.83 5.61 -4 7 -1 110.26 5.55 -4 7 -1 105.01 5.42 4 -7 -2 73.20 3.92 4 7 2 74.53 3.86 -4 7 -2 59.89 7.87 -4 7 -2 73.46 4.49 -4 7 -2 73.74 4.36 4 -7 -2 76.86 7.44 -4 7 -2 71.17 4.31 -4 7 -3 5.09 2.74 4 -7 -3 7.10 1.26 4 7 3 8.69 1.74 -4 7 -3 8.83 1.70 4 7 3 7.71 1.27 -4 7 -3 5.80 1.44 -4 7 -3 7.45 1.51 4 -7 -4 7.81 1.34 4 7 4 5.57 1.47 -4 7 -4 6.94 1.56 4 7 4 7.70 1.25 4 -7 -4 7.43 2.50 -4 7 -4 5.55 2.86 -4 7 -4 7.73 1.57 -4 7 -4 7.64 1.54 4 -7 -5 434.67 14.24 4 7 5 466.92 15.59 4 7 5 449.41 14.24 4 -7 -5 408.80 20.27 -4 7 -5 432.27 14.91 -4 7 -5 462.11 15.16 -4 -7 5 451.66 20.06 -4 7 -5 449.87 14.90 4 -7 -6 53.40 3.28 4 7 6 51.19 3.86 4 -7 -6 44.52 6.02 4 7 6 61.23 3.42 -4 7 -6 46.74 6.71 -4 7 -6 54.69 3.74 -4 7 -6 50.58 3.61 -4 -7 6 56.78 6.38 -4 7 -6 57.64 3.71 4 -7 -7 18.52 1.89 4 7 7 18.16 2.26 4 7 7 20.32 1.95 -4 7 -7 16.56 3.96 -4 7 -7 18.09 2.15 -4 7 -7 22.18 2.31 -4 -7 7 23.22 4.20 4 -7 -7 14.61 3.57 -4 7 -7 22.09 2.31 4 -7 -8 41.90 2.89 -4 7 -8 47.76 3.39 4 7 8 47.75 3.65 4 7 8 45.58 2.99 4 -7 -8 46.32 6.17 -4 7 -8 44.57 3.31 -4 7 -8 49.83 3.39 -4 -7 8 48.74 6.24 4 -7 -9 34.59 2.58 4 7 9 33.27 3.00 4 7 9 35.60 2.59 4 -7 -9 32.93 5.32 -4 7 -9 35.00 2.94 -4 7 -9 36.52 2.88 -4 -7 9 42.51 5.91 -4 7 -9 35.74 2.86 4 -7 -10 172.89 7.36 -4 7 -10 208.47 8.22 4 7 10 211.07 8.71 4 7 10 202.09 7.70 4 -7 -10 191.59 13.29 -4 -7 10 226.00 14.15 -4 7 -10 201.82 8.00 4 -7 -11 92.49 4.59 4 7 11 104.38 5.55 4 -7 -11 93.16 9.01 4 7 11 99.84 4.76 -4 7 -11 83.73 9.92 -4 -7 11 112.42 9.81 -4 7 -11 93.04 4.81 -4 7 -11 102.35 5.16 4 -7 -12 40.19 2.76 4 7 12 47.07 3.54 4 7 12 43.67 2.92 -4 7 -12 40.26 2.89 -4 7 -12 42.31 3.13 4 -7 -13 90.50 4.39 -4 7 -13 94.59 4.93 4 7 13 91.49 4.55 4 -7 -14 2.40 0.85 4 7 14 2.88 0.97 -4 7 -14 3.19 1.18 4 -7 -15 15.90 1.65 -4 7 -15 19.02 2.04 4 7 15 17.14 1.80 -4 7 -15 15.22 1.66 4 -7 -16 81.06 3.90 4 7 16 90.19 4.28 -4 7 -16 91.44 4.57 -4 7 -16 82.08 3.99 4 -7 -17 12.89 1.37 4 7 17 13.23 1.52 -4 7 -17 12.97 1.64 -4 7 -17 12.37 1.36 4 -7 -18 113.04 4.84 4 -7 -18 102.61 4.24 4 7 18 105.47 4.55 -4 7 -18 107.07 4.82 -4 7 -18 95.94 4.12 4 -7 -19 10.31 1.33 4 -7 -19 7.36 0.97 4 7 19 7.77 1.12 -4 7 -19 8.67 1.28 4 7 20 14.95 1.36 -4 7 -20 13.12 1.40 4 7 21 45.48 2.33 -4 7 -21 49.39 2.52 4 7 22 29.97 1.63 -4 7 -22 29.88 1.75 -4 7 -23 2.84 0.77 -4 7 -23 4.60 0.72 -4 7 -23 3.43 0.54 -4 7 -24 22.71 1.50 -4 7 -24 24.41 1.35 4 8 -21 2.74 0.55 -4 8 21 2.59 0.61 4 8 -20 37.18 1.89 -4 8 20 38.17 2.05 4 -8 19 1.32 0.54 4 8 -19 2.24 0.65 4 8 -18 37.81 2.01 4 -8 18 33.20 1.74 -4 8 18 39.97 2.36 4 8 -17 40.25 2.36 4 -8 17 36.15 2.15 4 8 -17 32.73 2.12 -4 8 17 40.25 2.73 4 8 -16 13.27 1.35 4 -8 16 11.75 1.27 4 8 -16 10.05 1.34 -4 8 16 10.91 1.58 -4 8 16 13.13 1.69 4 8 -15 174.01 6.50 4 -8 15 161.85 6.29 4 8 -15 171.64 6.79 -4 8 15 191.89 7.31 -4 8 15 182.26 7.26 4 8 -14 54.16 3.04 4 -8 14 56.37 3.01 4 8 -14 49.60 3.26 -4 8 14 55.56 3.56 -4 8 14 53.86 3.56 4 8 -13 56.72 3.08 4 -8 13 54.04 3.02 4 8 -13 51.33 3.43 -4 8 13 51.12 3.49 -4 8 13 55.47 3.65 4 8 -12 23.53 1.96 4 -8 12 25.38 2.01 4 8 -12 23.93 2.40 -4 8 12 20.71 2.27 -4 8 12 24.64 2.47 -4 8 12 20.38 2.01 4 -8 11 6.09 1.11 4 8 -11 7.12 1.16 4 8 -11 4.99 1.38 -4 8 11 6.76 1.37 -4 8 11 7.96 1.61 -4 8 11 6.68 1.63 4 8 -10 99.48 4.50 4 -8 10 105.42 4.68 4 8 -10 103.58 5.51 -4 8 10 103.23 5.31 -4 8 10 104.55 5.47 -4 8 10 97.53 5.03 4 8 -9 137.39 5.66 4 -8 9 141.01 5.89 4 8 -9 152.98 7.01 -4 8 9 151.11 6.69 -4 8 9 145.08 6.76 -4 8 9 150.57 6.63 4 8 -8 58.42 3.17 4 -8 8 63.84 3.46 4 8 -8 69.12 4.40 -4 8 8 63.60 4.03 -4 8 8 59.57 3.96 -4 8 8 62.95 4.09 4 8 -7 66.62 3.32 4 -8 7 71.09 3.68 4 8 -7 66.63 4.40 -4 8 7 67.06 4.17 -4 8 7 65.31 4.20 -4 8 7 68.84 4.26 4 -8 6 100.43 4.65 4 8 -6 103.41 5.69 -4 8 6 100.27 5.28 4 -8 6 84.61 8.34 -4 8 6 100.34 5.44 -4 8 6 106.06 5.51 4 -8 5 36.45 2.56 4 8 -5 43.50 3.51 -4 8 5 41.11 3.21 4 -8 5 37.05 5.45 -4 8 5 41.60 3.35 -4 8 5 40.12 3.20 -4 8 4 66.00 4.14 4 -8 4 64.62 3.53 4 8 -4 66.76 4.41 -4 8 4 64.30 4.28 -4 8 4 65.41 4.19 4 -8 3 50.11 3.03 4 8 -3 49.01 3.83 4 8 -3 48.48 2.83 -4 8 3 51.85 3.66 -4 8 3 42.65 7.13 4 -8 3 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225.16 8.78 -5 5 11 208.72 8.10 5 5 -10 7.97 1.30 5 5 -10 8.86 1.30 -5 5 10 6.95 1.46 5 5 -10 7.18 2.69 -5 5 10 5.43 2.80 -5 -5 -10 4.91 2.31 -5 5 10 9.17 1.58 5 -5 10 5.94 2.44 -5 5 10 7.93 1.60 5 5 -9 162.78 6.33 5 5 -9 148.74 6.46 5 5 -9 158.59 11.44 -5 5 9 162.80 12.77 -5 5 9 157.66 6.86 -5 5 9 159.29 6.93 -5 -5 -9 162.74 11.67 5 -5 9 146.11 10.94 -5 5 9 159.18 7.02 5 5 -8 60.10 3.25 5 -5 8 59.43 3.65 5 5 -8 59.51 3.57 5 5 -8 51.28 6.24 5 5 -8 55.91 3.46 -5 5 8 62.60 7.91 -5 5 8 50.71 3.49 -5 5 8 58.77 3.74 -5 -5 -8 58.55 6.72 5 -5 8 51.03 6.23 -5 5 8 58.32 3.77 5 5 -7 209.54 7.60 5 -5 7 233.11 8.49 5 5 -7 199.93 8.17 5 5 -7 211.26 12.88 5 5 -7 207.37 8.18 -5 5 7 225.36 15.55 -5 5 7 234.33 8.79 -5 5 7 207.87 8.37 -5 -5 -7 214.14 13.22 5 -5 7 199.95 12.95 -5 5 7 208.25 8.43 5 5 -6 45.83 2.67 5 -5 6 47.89 3.21 5 5 -6 44.05 3.14 5 5 -6 48.00 5.69 5 5 -6 53.83 3.30 -5 5 6 54.96 7.56 -5 5 6 39.93 3.24 -5 5 6 45.44 3.20 -5 -5 -6 40.26 5.37 -5 5 6 47.36 3.32 5 -5 5 60.53 3.65 5 5 -5 56.14 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8.40 -5 5 -7 211.06 13.89 -5 5 -7 220.06 8.54 -5 5 -7 227.43 15.06 -5 5 -7 224.13 8.53 5 -5 -7 205.78 13.68 -5 5 -7 204.97 7.99 5 -5 -8 55.91 3.63 5 5 8 64.21 3.78 -5 5 -8 51.52 6.54 -5 5 -8 59.33 3.69 -5 5 -8 61.81 7.66 -5 5 -8 58.82 3.73 5 -5 -8 59.56 7.10 -5 5 -8 56.98 3.42 5 -5 -9 156.31 6.83 5 5 9 160.85 6.91 -5 5 -9 162.85 6.78 -5 5 -9 154.72 12.72 -5 5 -9 158.80 6.88 5 -5 -9 166.00 12.17 -5 5 -9 151.95 6.43 5 -5 -10 9.20 1.56 5 5 10 6.79 1.59 -5 5 -10 6.73 1.34 5 5 10 8.12 1.46 -5 5 -10 4.00 2.58 5 -5 -10 2.96 1.95 -5 5 -10 8.11 1.37 5 -5 -11 220.27 8.59 5 5 11 226.45 8.68 -5 5 -11 219.73 15.66 -5 5 -11 216.67 8.14 5 -5 -11 183.47 13.65 5 5 11 215.74 7.83 -5 5 -11 210.27 8.10 5 -5 -12 147.36 6.60 5 5 12 149.87 6.70 -5 5 -12 151.73 6.17 5 -5 -12 128.18 11.01 5 -5 -12 144.93 5.96 5 5 12 150.83 6.01 -5 5 -12 152.78 6.29 5 -5 -13 42.71 3.11 5 5 13 38.67 3.08 -5 5 -13 42.05 6.87 5 -5 -13 30.41 5.43 5 5 13 40.63 2.64 -5 5 -13 37.99 2.72 5 -5 -14 2.69 1.13 5 5 14 2.15 1.14 5 5 14 3.06 0.93 -5 5 -14 1.50 0.83 5 -5 -15 166.76 6.69 5 -5 -15 162.77 6.95 5 5 15 166.89 7.17 5 5 15 161.88 6.37 -5 5 -15 166.66 6.58 5 -5 -16 197.04 7.55 5 -5 -16 202.96 7.85 5 5 16 201.05 8.10 5 5 16 202.10 7.29 -5 5 -16 188.35 7.29 5 -5 -17 96.24 4.55 5 -5 -17 92.05 4.70 5 5 17 100.86 5.04 5 5 17 96.70 4.31 -5 5 -17 102.42 4.45 5 -5 -18 35.35 2.49 5 -5 -18 38.78 2.75 5 5 18 40.10 2.90 5 5 18 37.47 2.32 5 -5 -19 13.84 1.49 5 -5 -19 14.52 1.62 5 5 19 13.69 1.70 5 5 19 10.57 1.21 5 -5 -20 36.40 2.36 5 -5 -20 38.39 2.51 5 5 20 35.24 2.53 5 -5 -21 5.52 0.97 5 -5 -21 4.82 1.00 5 5 21 6.71 1.13 5 -5 -22 32.14 2.00 5 -5 -22 33.88 2.09 5 5 22 33.17 2.18 -5 5 -22 32.00 2.00 5 5 23 16.63 1.39 -5 5 -23 12.85 1.13 5 -5 -23 15.36 1.27 5 5 24 8.80 0.95 -5 5 -24 6.74 0.70 5 -5 -24 8.14 0.85 5 5 25 29.60 1.50 5 -5 -25 26.41 1.34 5 6 -23 100.58 3.43 5 -6 23 76.84 3.22 5 6 -22 14.94 1.26 5 -6 22 14.59 1.26 -5 6 22 16.54 1.39 5 6 -21 84.54 3.55 5 -6 21 75.99 3.48 -5 6 21 80.85 3.67 5 6 -20 19.87 1.64 5 -6 20 20.98 1.69 -5 6 20 19.75 1.75 5 6 -19 36.67 2.36 5 -6 19 39.93 2.50 -5 6 19 36.13 2.57 5 6 -18 25.93 2.01 -5 6 18 25.52 2.25 -5 6 18 22.96 2.12 5 6 -17 18.12 1.73 -5 6 17 19.53 2.08 -5 6 17 17.36 1.95 5 6 -16 12.31 1.48 -5 6 16 10.75 1.67 -5 6 16 9.41 1.57 5 6 -15 39.01 2.64 -5 6 15 40.24 3.08 -5 6 15 38.29 3.00 5 6 -14 97.44 4.60 -5 6 14 105.36 5.28 -5 6 14 99.32 5.18 5 6 -13 53.96 3.11 5 6 -13 45.51 2.85 -5 6 13 46.51 3.46 -5 6 13 51.87 3.07 -5 6 13 50.02 3.53 5 6 -12 98.72 4.56 5 -6 12 103.66 4.96 5 6 -12 89.10 4.49 -5 6 12 91.57 5.02 -5 6 12 100.35 4.73 -5 6 12 104.10 5.33 5 6 -11 145.59 5.91 5 -6 11 142.46 6.24 5 6 -11 130.58 5.95 -5 6 11 146.98 6.61 -5 6 11 149.47 6.26 -5 6 11 145.72 6.68 5 6 -10 55.89 3.14 5 -6 10 55.26 3.44 5 6 -10 52.32 3.35 5 6 -10 43.46 5.95 -5 6 10 51.56 3.56 -5 6 10 36.12 6.17 -5 -6 -10 42.09 5.73 -5 6 10 58.58 3.54 5 -6 10 50.71 6.30 -5 6 10 50.23 3.57 5 6 -9 20.97 1.82 5 -6 9 21.13 2.13 5 6 -9 17.86 2.00 5 6 -9 17.70 3.75 -5 6 9 21.27 2.31 -5 6 9 9.76 3.62 -5 6 9 18.45 2.06 -5 -6 -9 19.34 3.89 5 -6 9 14.93 3.50 -5 6 9 21.35 2.28 5 6 -8 37.98 2.47 5 -6 8 35.24 2.76 5 6 -8 37.35 2.90 5 6 -8 30.67 4.79 -5 6 8 35.88 2.96 -5 6 8 39.26 3.02 -5 6 8 34.40 6.08 -5 -6 -8 29.77 4.80 5 -6 8 33.87 5.24 -5 6 8 37.61 3.03 5 6 -7 259.45 8.81 5 -6 7 265.05 9.69 5 6 -7 259.84 9.87 5 6 -7 241.88 14.15 5 6 -7 268.42 9.56 -5 6 7 294.00 18.18 -5 6 7 258.79 9.83 -5 6 7 257.00 9.85 -5 6 7 244.04 9.77 5 -6 6 25.61 2.35 5 6 -6 29.65 2.62 5 6 -6 28.28 2.45 -5 6 6 27.27 2.60 -5 6 6 33.55 6.30 -5 6 6 27.76 2.62 -5 6 6 34.69 2.84 5 -6 5 118.73 5.46 5 6 -5 106.44 5.55 5 6 -5 110.12 5.25 -5 6 5 96.61 10.41 -5 6 5 125.77 5.88 -5 6 5 107.61 5.45 5 -6 5 108.67 9.34 -5 6 5 106.99 5.48 5 -6 4 2.51 0.97 5 6 -4 1.65 0.99 -5 6 4 2.06 1.25 5 6 -4 3.79 1.13 -5 6 4 1.52 1.09 5 -6 4 2.22 1.66 -5 6 4 2.50 1.13 5 -6 3 48.23 3.27 5 6 -3 46.25 3.46 5 6 -3 53.32 3.31 -5 6 3 60.21 7.96 -5 6 3 55.18 3.81 -5 6 3 47.60 3.42 5 -6 3 47.13 6.14 -5 6 3 47.55 3.35 5 -6 2 41.64 2.96 5 6 -2 39.52 3.15 5 6 -2 35.68 2.74 -5 6 2 35.86 6.29 -5 6 2 36.55 2.96 5 -6 2 30.82 5.08 -5 6 2 40.15 3.05 5 -6 1 46.86 3.17 5 6 -1 43.11 3.31 5 6 -1 39.48 2.89 -5 6 1 44.70 7.13 -5 6 1 45.66 3.26 5 -6 1 44.64 5.96 -5 6 1 45.02 3.22 5 -6 0 36.96 2.84 5 6 0 34.51 2.99 5 6 0 37.68 2.79 -5 6 0 40.01 6.57 -5 6 0 35.54 3.14 -5 6 0 40.33 3.05 -5 6 0 36.85 2.91 5 -6 -1 43.05 3.05 5 6 1 49.19 3.53 5 6 1 46.41 3.10 -5 6 -1 38.14 6.53 -5 6 -1 42.55 3.39 -5 6 -1 46.81 3.30 -5 6 -1 40.30 3.07 5 -6 -2 40.58 2.95 5 6 2 38.98 3.18 5 6 2 41.36 2.94 -5 6 -2 37.81 3.19 -5 6 -2 34.59 6.06 -5 6 -2 41.35 3.13 -5 6 -2 36.38 2.88 5 -6 -3 50.76 3.39 5 6 3 46.18 3.53 5 6 3 49.83 3.26 -5 6 -3 42.63 6.69 -5 6 -3 51.75 3.64 -5 6 -3 48.81 3.46 -5 6 -3 49.43 3.37 5 -6 -4 2.44 1.05 5 6 4 1.37 0.97 -5 6 -4 1.78 1.08 5 6 4 1.91 0.95 -5 6 -4 2.73 2.46 -5 6 -4 1.31 1.07 5 -6 -4 0.81 1.52 -5 6 -4 1.56 0.91 5 -6 -5 111.75 5.42 5 6 5 117.53 5.99 5 6 5 108.34 5.26 -5 6 -5 89.42 9.49 -5 6 -5 112.78 5.63 -5 6 -5 122.84 5.77 5 -6 -5 84.19 8.36 -5 6 -5 115.38 5.48 5 -6 -6 27.52 2.48 5 6 6 29.97 2.52 -5 6 -6 29.13 2.65 -5 6 -6 23.54 4.80 -5 6 -6 28.70 5.56 -5 6 -6 33.95 2.81 5 -6 -6 23.42 4.51 -5 6 -6 30.89 2.57 5 -6 -7 253.23 9.52 5 6 7 262.51 9.57 -5 6 -7 233.65 16.27 -5 6 -7 261.82 9.72 -5 6 -7 255.21 9.77 5 -6 -7 237.04 14.83 -5 6 -7 268.62 9.65 5 -6 -8 36.73 2.88 5 6 8 41.26 2.97 -5 6 -8 35.40 2.82 -5 6 -8 30.63 5.90 -5 6 -8 35.27 2.92 5 -6 -8 32.68 5.27 -5 6 -8 39.39 2.90 5 -6 -9 23.79 2.30 5 6 9 18.50 2.34 5 6 9 22.99 2.20 -5 6 -9 19.28 2.08 -5 6 -9 22.44 5.14 -5 6 -9 25.56 2.45 5 -6 -9 13.77 3.60 -5 6 -9 20.89 2.15 5 -6 -10 50.23 3.41 5 6 10 56.83 4.00 5 6 10 54.21 3.50 -5 6 -10 64.41 8.41 -5 6 -10 54.99 3.42 -5 6 -10 47.40 3.48 5 -6 -10 39.84 5.97 -5 6 -10 56.12 3.47 5 -6 -11 143.85 6.34 5 6 11 154.28 6.50 -5 6 -11 140.13 6.53 -5 6 -11 140.06 6.10 -5 6 -11 142.11 6.26 5 -6 -12 99.47 4.98 5 6 12 104.41 5.12 -5 6 -12 103.63 5.28 -5 6 -12 96.42 4.67 -5 6 -12 101.85 4.95 5 -6 -13 53.21 3.39 5 6 13 48.66 3.33 -5 6 -13 57.63 3.69 -5 6 -13 52.27 3.30 5 -6 -14 95.23 4.79 5 6 14 100.16 4.99 -5 6 -14 103.52 4.85 5 -6 -15 38.77 2.66 5 -6 -15 36.41 2.64 5 6 15 37.73 2.83 -5 6 -15 36.95 2.61 -5 6 -15 31.18 2.15 5 -6 -16 9.79 1.38 5 -6 -16 10.23 1.44 5 6 16 11.20 1.58 -5 6 -16 10.32 1.39 5 -6 -17 18.47 1.73 5 -6 -17 16.57 1.71 5 6 17 17.87 1.85 -5 6 -17 18.23 1.68 5 -6 -18 25.62 1.97 5 -6 -18 21.22 1.85 5 6 18 22.23 1.96 -5 6 -18 26.67 2.16 -5 6 -18 24.94 1.87 5 -6 -19 34.38 2.20 5 -6 -19 37.21 2.27 5 6 19 31.85 2.23 -5 6 -19 33.58 2.39 -5 6 -19 29.34 1.91 5 -6 -20 21.26 1.61 5 -6 -20 16.91 1.45 5 6 20 18.02 1.58 -5 6 -20 16.32 1.58 5 -6 -21 75.43 3.27 5 6 21 76.94 3.36 -5 6 -21 76.17 3.38 5 -6 -22 16.06 1.22 5 6 22 14.34 1.20 -5 6 -22 15.66 1.25 5 6 23 84.14 3.17 -5 6 -23 86.49 3.12 5 -6 -23 85.50 3.15 5 7 -21 19.91 1.24 5 -7 21 13.99 1.07 5 7 -20 112.99 3.97 5 -7 20 93.15 3.79 5 7 -19 8.30 1.00 5 -7 19 7.75 0.99 5 7 -18 21.89 1.63 5 -7 18 22.53 1.70 -5 7 18 21.49 1.90 -5 7 18 22.70 1.89 5 7 -17 31.14 2.04 5 -7 17 28.15 2.03 -5 7 17 33.18 2.44 -5 7 17 31.17 2.30 5 7 -16 22.89 1.78 5 -7 16 24.03 1.89 -5 7 16 24.25 2.20 -5 7 16 22.39 2.08 5 7 -15 51.82 2.84 5 -7 15 47.21 2.87 -5 7 15 55.63 3.40 -5 7 15 51.53 3.27 5 -7 14 3.54 0.94 5 7 -14 3.20 0.88 5 7 -14 2.70 0.78 -5 7 14 2.55 1.06 -5 7 14 4.33 1.20 5 7 -13 13.69 1.47 5 -7 13 12.09 1.52 5 7 -13 11.80 1.45 -5 7 13 12.67 1.82 -5 7 13 16.22 1.94 5 7 -12 11.21 1.34 5 -7 12 11.55 1.51 5 7 -12 8.53 1.35 -5 7 12 11.67 1.75 -5 7 12 10.52 1.50 -5 7 12 8.99 1.67 5 -7 11 2.56 0.94 5 7 -11 3.14 0.88 5 7 -11 3.15 1.03 -5 7 11 3.05 1.09 -5 7 11 4.62 1.33 -5 7 11 4.14 1.22 5 7 -10 26.82 2.00 5 -7 10 26.97 2.29 5 7 -10 22.61 2.23 -5 7 10 25.59 2.48 -5 7 10 31.38 2.49 -5 7 10 27.14 2.58 5 7 -9 362.87 11.43 5 -7 9 368.67 12.15 5 7 -9 358.53 12.46 -5 7 9 356.85 12.52 -5 7 9 348.64 12.31 -5 7 9 349.11 12.57 5 7 -8 70.73 3.42 5 -7 8 75.14 4.06 5 7 -8 69.83 4.23 -5 7 8 76.89 4.43 -5 7 8 71.72 4.23 -5 7 8 67.99 4.24 5 -7 7 91.14 4.63 5 7 -7 89.49 4.90 -5 7 7 89.86 4.91 -5 7 7 92.22 4.90 -5 7 7 80.81 4.74 5 -7 6 0.21 0.72 5 7 -6 0.13 0.97 -5 7 6 -0.13 0.95 -5 7 6 -0.12 0.98 -5 7 6 -0.25 0.94 5 -7 5 43.78 3.04 5 7 -5 43.64 3.33 5 7 -5 42.39 2.87 -5 7 5 40.16 3.17 -5 7 5 37.18 6.58 -5 7 5 46.02 3.42 5 -7 5 40.93 5.83 -5 7 5 43.36 3.30 5 -7 4 413.50 13.68 5 7 -4 420.77 14.37 5 7 -4 407.84 13.33 -5 7 4 407.61 14.00 -5 7 4 416.16 14.25 5 -7 4 362.88 19.57 -5 7 4 403.05 13.99 5 -7 3 209.42 8.15 5 7 -3 205.54 8.69 5 7 -3 216.93 8.03 -5 7 3 194.84 15.22 -5 7 3 207.24 8.50 -5 7 3 209.31 8.68 5 -7 3 186.57 13.01 -5 7 3 207.58 8.48 5 -7 2 469.07 15.14 5 7 -2 458.26 15.78 5 7 -2 466.68 14.91 -5 7 2 441.49 24.68 -5 7 2 474.95 15.61 5 -7 2 462.46 22.08 -5 7 2 454.58 15.45 5 -7 1 6.49 1.32 5 7 -1 6.20 1.53 5 7 -1 4.52 1.13 -5 7 1 1.90 2.09 -5 7 1 8.75 1.66 -5 7 1 5.86 1.45 5 -7 0 100.62 4.97 5 7 0 98.55 5.48 5 7 0 101.87 4.87 -5 7 0 95.00 10.32 -5 7 0 98.46 5.22 -5 7 0 95.49 5.39 -5 7 0 98.70 5.20 5 -7 -1 5.88 1.33 5 7 1 7.69 1.59 -5 7 -1 6.98 1.59 5 7 1 7.34 1.37 -5 7 -1 2.46 2.43 -5 7 -1 7.66 1.57 -5 7 -1 5.20 1.42 5 -7 -2 470.01 15.20 5 7 2 453.53 15.92 5 7 2 459.19 14.93 -5 7 -2 418.81 23.54 -5 7 -2 502.17 16.10 -5 7 -2 474.62 15.66 -5 7 -2 451.00 15.40 5 -7 -3 206.13 8.13 5 7 3 211.60 8.94 5 7 3 205.20 7.96 -5 7 -3 212.54 8.72 -5 7 -3 213.59 8.56 -5 7 -3 209.47 8.40 5 -7 -4 402.38 13.64 5 7 4 416.48 13.58 -5 7 -4 434.37 14.42 -5 7 -4 428.13 14.22 -5 7 -4 411.74 13.96 5 -7 -5 39.90 2.89 5 7 5 42.28 2.92 -5 7 -5 38.22 3.14 -5 7 -5 43.63 3.27 -5 7 -5 39.36 3.06 5 -7 -6 0.31 0.76 -5 7 -6 0.25 0.89 5 7 6 0.81 0.83 -5 7 -6 -0.60 0.97 -5 7 -6 -0.12 0.95 5 -7 -7 89.67 4.59 5 7 7 93.53 5.31 5 7 7 84.91 4.45 -5 7 -7 92.89 4.96 -5 7 -7 89.41 4.84 -5 7 -7 91.44 4.79 5 -7 -8 67.83 3.85 5 7 8 72.73 4.58 5 7 8 66.76 3.83 -5 7 -8 74.60 4.36 -5 7 -8 68.24 4.10 -5 7 -8 68.64 4.02 5 -7 -9 351.26 11.95 5 7 9 370.77 13.06 5 7 9 343.01 11.92 -5 7 -9 361.02 12.53 -5 7 -9 354.25 12.24 -5 7 -9 358.14 12.27 5 -7 -10 25.83 2.26 5 7 10 29.55 2.84 5 7 10 30.71 2.45 -5 7 -10 27.42 2.58 -5 7 -10 32.48 2.54 -5 7 -10 29.79 2.53 5 -7 -11 3.62 1.03 5 7 11 2.13 0.92 -5 7 -11 2.46 1.04 -5 7 -11 3.28 1.26 -5 7 -11 3.77 1.12 5 -7 -12 10.57 1.42 5 7 12 11.11 1.50 -5 7 -12 10.34 1.71 -5 7 -12 8.83 1.44 -5 7 -12 10.74 1.60 5 -7 -13 14.79 1.60 5 7 13 14.48 1.65 -5 7 -13 14.68 1.89 -5 7 -13 14.42 1.74 5 -7 -14 3.46 0.91 5 7 14 2.78 0.93 -5 7 -14 1.73 0.98 -5 7 -14 3.37 1.02 5 -7 -15 53.66 3.01 5 -7 -15 51.04 2.84 5 7 15 47.64 2.90 -5 7 -15 52.86 3.31 -5 7 -15 55.59 3.11 -5 7 -15 47.31 2.62 5 -7 -16 22.29 1.82 5 -7 -16 23.33 1.77 5 7 16 23.59 1.88 -5 7 -16 24.66 2.14 -5 7 -16 22.94 1.88 -5 7 -16 18.71 1.48 5 -7 -17 31.71 2.11 5 -7 -17 31.15 1.96 5 7 17 33.13 2.15 -5 7 -17 31.05 2.33 -5 7 -17 32.20 2.11 5 -7 -18 22.05 1.64 5 -7 -18 20.28 1.47 5 7 18 21.34 1.62 -5 7 -18 22.32 1.85 -5 7 -18 20.27 1.54 5 -7 -19 7.03 0.92 5 -7 -19 6.51 0.79 5 7 19 7.74 0.93 -5 7 -19 8.82 1.14 -5 7 -19 5.48 0.77 5 -7 -20 103.72 3.82 -5 7 -20 111.71 4.08 5 -7 -21 18.12 1.18 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7.55 0.81 7 7 13 7.29 0.83 7 -7 -14 74.51 2.66 7 7 14 60.22 2.58 -7 8 11 12.74 0.99 7 -8 10 15.83 1.07 -7 8 10 16.13 1.22 7 -8 9 8.42 0.84 -7 8 9 9.27 0.99 7 -8 8 11.63 1.02 -7 8 8 12.23 1.16 7 -8 7 22.73 1.49 -7 8 7 20.53 1.54 7 -8 6 64.95 2.86 -7 8 6 67.91 3.09 -7 8 6 60.71 3.02 7 -8 5 0.99 0.56 -7 8 5 0.69 0.67 -7 8 5 0.73 0.67 7 -8 4 47.40 2.41 -7 8 4 44.77 2.52 -7 8 4 46.27 2.71 7 -8 3 69.67 3.12 -7 8 3 67.63 3.24 -7 8 3 71.71 3.56 7 -8 2 2.65 0.76 -7 8 2 2.23 0.80 7 -8 1 54.61 2.71 -7 8 1 54.72 2.82 7 -8 0 48.09 2.55 -7 8 0 51.60 2.72 -7 8 0 53.85 3.12 7 -8 -1 52.62 2.67 -7 8 -1 54.22 2.81 -7 8 -1 60.05 3.24 7 -8 -2 2.23 0.64 7 8 2 2.12 0.68 -7 8 -2 0.49 0.80 -7 8 -2 1.98 0.74 7 -8 -3 67.64 3.07 7 8 3 65.01 2.91 -7 8 -3 75.37 3.31 -7 8 -3 71.00 3.56 7 -8 -4 41.22 2.24 7 8 4 43.15 2.16 -7 8 -4 44.73 2.41 -7 8 -4 46.04 2.69 7 -8 -5 0.20 0.50 7 8 5 0.73 0.48 -7 8 -5 1.09 0.70 -7 8 -5 0.85 0.63 7 -8 -6 60.36 2.70 7 8 6 60.14 2.63 -7 8 -6 65.15 2.90 -7 8 -6 60.46 2.98 7 -8 -7 21.74 1.42 7 8 7 22.37 1.39 -7 8 -7 23.62 1.59 -7 8 -7 21.63 1.54 7 -8 -8 10.27 0.89 7 8 8 8.44 0.84 -7 8 -8 10.55 1.03 7 -8 -9 7.44 0.74 7 8 9 7.01 0.70 -7 8 -9 8.80 0.86 -7 9 5 6.21 0.70 -7 9 4 29.10 1.54 -7 9 3 8.70 0.85 -7 9 2 36.29 1.82 -7 9 1 1.34 0.48 -7 9 0 9.22 0.89 -7 9 0 7.62 0.96 -7 9 -1 1.25 0.59 -7 9 -1 2.25 0.54 -7 9 -2 36.52 1.80 -7 9 -3 9.76 0.87 -7 9 -4 26.89 1.42 8 0 0 98.87 4.30 8 0 0 92.78 4.18 8 0 0 104.86 5.12 8 0 -1 2.47 0.79 8 0 1 1.84 0.71 8 0 -1 2.43 0.81 8 0 1 1.62 0.69 8 0 -1 2.56 1.16 8 0 1 1.89 1.15 8 0 -2 35.49 2.34 8 0 2 35.73 2.35 8 0 2 37.38 2.32 8 0 -2 39.25 3.00 8 0 2 43.58 3.11 8 0 -3 21.95 1.81 8 0 3 20.51 1.73 8 0 3 23.55 1.79 8 0 -3 24.26 2.40 8 0 3 21.04 2.21 8 0 -4 22.15 1.82 8 0 4 23.24 1.77 8 0 -4 21.63 2.24 8 0 4 23.42 2.29 8 0 -5 137.57 5.38 8 0 5 130.66 5.14 8 0 5 134.68 6.01 8 0 -6 32.79 2.22 8 0 6 37.01 2.80 8 0 -7 38.30 2.37 8 0 7 36.16 2.76 8 0 -8 119.16 4.81 8 0 8 120.72 5.41 8 0 -9 5.58 0.97 8 0 9 7.55 1.33 8 0 -10 60.45 2.91 8 0 10 51.64 3.22 8 0 -11 27.63 1.81 8 0 11 24.27 2.08 8 0 -12 26.51 1.70 8 0 12 20.93 1.89 8 0 -13 5.39 0.79 8 0 13 3.35 0.96 8 0 -14 1.59 0.47 8 0 14 2.04 0.79 8 0 -15 -0.04 0.16 8 0 15 6.42 1.03 8 0 16 2.83 0.76 8 0 17 51.32 2.54 8 0 18 2.59 0.60 8 0 19 6.59 0.70 8 -1 19 0.03 0.30 8 -1 18 24.76 1.48 8 -1 17 11.39 1.10 8 -1 16 2.20 0.68 8 -1 15 5.10 0.94 8 1 -14 3.91 0.92 8 -1 14 3.88 0.92 8 -1 13 8.35 1.18 8 1 -13 7.52 1.24 8 1 -12 16.15 1.63 8 -1 12 16.61 1.61 8 1 -11 18.03 1.83 8 -1 11 22.13 1.92 8 1 -10 76.86 4.14 8 -1 10 81.33 4.15 8 1 -9 100.79 4.86 8 -1 9 91.59 4.60 8 -1 8 22.48 1.79 8 1 -8 16.84 1.92 8 -1 8 20.52 2.07 8 -1 7 34.14 2.26 8 1 -7 30.88 2.53 8 -1 7 32.24 2.52 8 -1 6 27.23 2.05 8 1 -6 25.36 2.34 8 -1 6 24.12 2.23 8 -1 5 76.29 3.79 8 1 -5 79.91 4.30 8 -1 5 81.59 4.28 8 -1 4 48.51 2.90 8 1 -4 54.24 3.46 8 -1 4 46.22 3.19 8 -1 3 77.53 3.90 8 1 -3 83.13 4.40 8 -1 3 80.47 4.37 8 -1 2 18.41 1.79 8 1 -2 14.15 1.59 8 1 -2 15.05 1.87 8 -1 2 15.60 1.95 8 -1 1 83.13 4.11 8 1 -1 82.89 4.05 8 1 -1 85.49 4.57 8 -1 1 87.76 4.59 8 -1 0 115.37 5.12 8 1 0 114.67 5.02 8 1 0 125.88 5.68 8 -1 0 120.15 5.64 8 -1 -1 86.20 4.19 8 1 1 81.31 4.02 8 -1 -1 90.71 4.65 8 1 1 80.79 4.48 8 -1 -2 14.55 1.65 8 1 2 14.42 1.54 8 -1 -2 14.36 1.86 8 1 2 16.54 1.95 8 -1 -3 83.50 4.07 8 1 3 77.83 3.86 8 -1 -3 81.36 4.43 8 1 3 78.62 4.34 8 -1 -4 49.99 3.04 8 1 4 50.67 2.96 8 -1 -4 56.83 3.58 8 1 4 58.59 3.55 8 -1 -5 74.77 3.82 8 1 5 73.66 3.68 8 -1 -5 77.50 4.27 8 1 5 78.43 4.20 8 -1 -6 27.85 2.15 8 1 6 27.18 2.05 8 -1 -6 26.96 2.39 8 1 6 28.88 2.41 8 -1 -7 37.49 2.48 8 1 7 35.89 2.32 8 -1 -7 30.19 2.61 8 1 7 34.62 2.66 8 -1 -8 21.78 1.87 8 1 8 20.24 1.71 8 -1 -8 22.78 2.19 8 1 8 18.37 1.95 8 -1 -9 124.75 5.02 8 1 9 116.51 4.71 8 -1 -9 112.58 5.26 8 1 9 108.41 5.14 8 -1 -10 96.78 4.15 8 1 10 91.65 3.91 8 -1 -10 82.68 4.32 8 1 10 85.29 4.28 8 -1 -11 31.86 2.03 8 1 11 27.97 1.80 8 -1 -11 28.50 2.21 8 -1 -12 29.23 1.95 8 1 12 29.24 1.79 8 -1 -12 18.30 1.85 8 1 12 16.34 1.72 8 -1 -13 15.82 1.36 8 1 13 15.55 1.27 8 1 13 8.45 1.24 8 -1 -13 7.55 1.26 8 -1 -14 7.17 0.94 8 1 14 6.88 0.85 8 -1 -14 3.51 0.93 8 1 14 2.64 0.86 8 -1 -15 8.89 0.97 8 1 15 8.44 0.84 8 -1 -16 3.68 0.62 8 1 16 2.34 0.73 8 1 17 9.35 1.03 8 1 18 27.48 1.58 8 1 19 0.13 0.30 8 -2 18 0.40 0.34 8 -2 17 2.69 0.56 8 -2 16 3.19 0.45 8 -2 16 8.08 0.94 8 -2 15 10.80 0.94 8 -2 15 5.96 0.93 8 -2 14 43.10 2.01 8 -2 14 19.69 1.72 8 2 -13 7.16 1.12 8 -2 13 5.92 1.05 8 2 -12 11.00 1.39 8 -2 12 11.64 1.39 8 2 -11 98.26 3.66 8 -2 11 87.51 3.41 8 2 -10 33.02 2.28 8 -2 10 29.20 2.13 8 -2 9 21.49 1.73 8 2 -9 16.45 1.77 8 -2 9 21.20 1.86 8 -2 8 14.16 1.49 8 2 -8 10.99 1.51 8 -2 8 12.93 1.57 8 -2 7 32.56 2.31 8 2 -7 31.30 2.47 8 -2 7 33.97 2.53 8 -2 6 71.34 3.65 8 2 -6 69.43 3.85 8 -2 6 72.75 3.87 8 -2 5 25.08 2.06 8 2 -5 22.17 2.14 8 -2 5 20.03 1.99 8 -2 4 92.03 4.38 8 2 -4 86.24 4.51 8 -2 4 93.57 4.60 8 -2 3 13.73 1.60 8 2 -3 12.81 1.57 8 2 -3 12.28 1.65 8 -2 3 11.08 1.62 8 -2 2 38.21 2.69 8 2 -2 38.21 2.63 8 2 -2 36.68 2.75 8 -2 2 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26.72 2.24 8 3 -2 31.83 2.39 8 3 -2 25.64 2.17 8 -3 2 23.41 2.10 8 -3 1 47.45 3.00 8 3 -1 44.97 2.93 8 3 -1 46.33 2.95 8 -3 1 42.01 2.88 8 -3 0 124.54 5.56 8 3 0 131.33 5.57 8 3 0 126.74 5.50 8 -3 0 125.06 5.56 8 -3 -1 47.38 3.06 8 3 1 44.94 2.95 8 -3 -1 42.62 2.89 8 3 1 47.36 2.97 8 -3 -2 29.68 2.37 8 3 2 28.13 2.29 8 -3 -2 23.33 2.14 8 3 2 24.92 2.15 8 -3 -3 0.67 0.80 8 3 3 0.98 0.84 8 -3 -3 1.70 0.84 8 3 3 1.27 0.81 8 -3 -4 99.77 4.68 8 3 4 98.36 4.55 -8 3 -4 83.37 4.95 8 -3 -4 100.06 4.68 8 3 4 98.02 4.55 8 -3 -5 16.88 1.73 8 3 5 16.45 1.74 -8 3 -5 13.95 1.95 8 -3 -5 14.77 1.72 8 3 5 15.64 1.70 8 -3 -6 5.50 1.16 -8 3 -6 3.34 1.31 8 3 6 6.76 1.20 8 -3 -6 7.33 1.26 8 3 6 7.04 1.22 8 -3 -7 14.48 1.64 8 3 7 15.54 1.60 -8 3 -7 8.66 1.48 8 -3 -7 13.12 1.56 8 3 7 13.68 1.53 8 -3 -8 22.66 1.96 8 3 8 24.77 1.95 -8 3 -8 19.55 1.90 8 -3 -8 17.78 1.79 8 3 8 22.39 1.90 8 -3 -9 11.31 1.45 8 3 9 10.57 1.33 -8 3 -9 7.52 1.24 8 -3 -9 9.93 1.36 8 3 9 9.05 1.29 8 -3 -10 74.35 3.49 8 3 10 85.21 3.55 -8 3 -10 48.08 2.84 8 -3 -10 46.50 2.93 8 3 10 60.91 3.14 8 -3 -11 14.52 1.49 8 3 11 14.85 1.43 8 3 11 13.11 1.37 8 -3 -12 18.61 1.60 8 3 12 18.92 1.54 8 3 12 13.93 1.37 8 -3 -13 19.65 1.56 8 3 13 20.04 1.53 8 -3 -14 21.53 1.52 8 3 14 21.77 1.50 8 -3 -15 17.68 1.33 8 3 15 19.28 1.31 8 -3 -16 21.58 1.30 8 3 16 19.56 1.19 8 -3 -17 16.11 1.06 8 3 17 13.90 0.94 8 -4 16 1.70 0.40 8 -4 15 33.05 1.69 8 -4 14 0.86 0.49 8 -4 13 54.47 2.27 8 -4 13 18.35 1.27 8 -4 12 14.08 1.25 8 -4 12 5.48 0.76 8 -4 11 19.05 1.49 8 -4 11 10.53 0.99 -8 4 10 9.60 1.15 8 -4 10 14.32 1.24 8 -4 9 19.51 1.64 -8 4 9 13.11 1.41 8 4 -9 19.64 1.42 8 -4 9 15.29 1.34 -8 4 8 11.38 1.40 8 4 -8 14.14 1.29 8 -4 8 13.02 1.32 8 -4 7 89.90 3.94 8 4 -7 82.32 3.48 8 -4 6 6.98 1.14 -8 4 6 5.16 1.19 8 4 -6 8.40 1.09 8 -4 6 5.43 0.97 8 -4 5 25.24 2.07 -8 4 5 23.04 2.21 8 4 -5 26.03 1.86 8 -4 5 20.79 1.74 8 -4 4 25.85 2.11 -8 4 4 23.15 2.27 8 4 -4 26.54 1.93 8 -4 4 24.44 1.90 8 -4 3 2.11 0.93 -8 4 3 2.25 1.21 8 4 -3 3.10 1.01 8 4 -3 2.13 0.72 8 -4 3 2.09 0.80 8 -4 2 117.29 5.09 8 4 -2 112.41 4.93 8 4 -2 108.49 4.57 8 -4 2 98.69 4.54 8 -4 1 1.73 0.96 8 4 -1 1.55 0.87 8 4 -1 1.89 0.68 8 -4 1 1.24 0.77 8 -4 0 80.36 4.06 8 4 0 82.35 4.01 -8 4 0 74.31 4.35 8 4 0 74.67 3.63 8 -4 0 73.24 3.68 8 -4 -1 1.56 0.95 -8 4 -1 0.57 0.97 8 4 1 0.96 0.85 8 -4 -1 1.49 0.72 8 4 1 2.34 0.75 8 -4 -2 111.99 5.03 -8 4 -2 98.76 5.19 8 -4 -2 102.16 4.59 8 4 2 104.62 4.51 8 -4 -3 1.54 0.88 -8 4 -3 2.26 1.12 8 4 3 1.54 0.84 8 -4 -3 2.17 0.79 8 4 3 1.94 0.75 8 -4 -4 25.27 2.13 8 4 4 27.23 2.16 -8 4 -4 19.92 2.14 8 -4 -4 21.41 1.82 8 4 4 23.56 1.84 8 -4 -5 23.63 2.08 8 4 5 27.78 2.15 -8 4 -5 22.19 2.14 8 -4 -5 22.46 1.85 8 4 5 25.55 1.87 8 -4 -6 8.52 1.31 8 4 6 8.89 1.30 -8 4 -6 5.79 1.28 8 -4 -6 9.81 1.25 8 4 6 8.40 1.12 8 -4 -7 91.07 4.19 8 4 7 93.82 4.13 -8 4 -7 84.92 4.08 8 -4 -7 73.24 3.64 8 4 7 80.77 3.66 8 -4 -8 15.48 1.63 8 4 8 18.69 1.67 -8 4 -8 14.74 1.54 8 -4 -8 11.89 1.32 8 4 8 15.10 1.39 8 -4 -9 25.18 1.94 8 4 9 23.07 1.82 -8 4 -9 18.38 1.61 8 -4 -9 14.35 1.42 8 4 9 19.65 1.51 8 -4 -10 24.45 1.86 8 4 10 24.49 1.81 -8 4 -10 20.32 1.57 8 4 10 22.37 1.52 8 -4 -11 18.05 1.58 8 4 11 20.95 1.64 8 -4 -12 13.78 1.30 8 4 12 15.36 1.37 8 -4 -13 57.93 2.33 8 4 13 57.14 2.28 8 -4 -14 1.08 0.54 8 4 14 0.39 0.53 8 -4 -15 35.52 1.85 8 4 15 35.35 1.82 8 -4 -16 1.56 0.44 8 4 16 0.90 0.38 8 -5 14 0.61 0.38 8 -5 13 59.11 2.57 8 -5 12 9.66 1.01 8 -5 11 0.97 0.58 8 -5 10 22.27 1.64 8 -5 9 2.81 0.76 -8 5 9 2.46 0.71 8 -5 8 8.42 1.12 -8 5 8 5.36 0.94 8 -5 7 4.59 0.93 -8 5 7 3.07 0.87 8 -5 6 12.71 1.40 -8 5 6 11.99 1.42 -8 5 5 21.52 1.89 -8 5 4 18.88 1.84 -8 5 3 39.65 2.71 8 5 -2 101.07 4.49 8 5 -1 36.22 2.45 8 5 0 28.99 2.19 -8 5 0 30.77 2.43 8 5 1 32.57 2.30 -8 5 -1 30.87 2.50 8 5 2 99.09 4.35 -8 5 -2 86.57 4.41 8 5 3 46.41 2.77 -8 5 -3 41.30 2.79 8 5 4 19.46 1.77 -8 5 -4 18.38 1.81 8 5 5 26.37 2.01 -8 5 -5 25.87 2.09 8 5 6 13.92 1.48 -8 5 -6 12.91 1.46 -8 5 -7 5.12 1.02 8 5 7 4.21 0.96 8 5 8 8.60 1.16 -8 5 -8 8.94 1.17 -8 5 -9 3.11 0.76 8 5 9 3.06 0.81 8 5 10 19.39 1.54 8 5 11 0.61 0.59 8 5 12 9.33 1.03 8 5 13 57.21 2.53 8 -5 -14 0.85 0.44 8 5 14 0.56 0.41 8 -5 -15 44.40 1.77 8 5 15 33.34 1.62 8 -6 9 24.22 1.59 8 -6 8 28.93 1.72 -8 6 8 14.69 1.26 8 -6 7 23.55 1.63 -8 6 7 16.91 1.42 8 -6 6 9.99 1.15 -8 6 6 6.65 1.06 8 -6 5 42.01 2.32 -8 6 5 33.12 2.19 8 -6 4 50.49 2.66 -8 6 4 43.34 2.62 8 -6 3 34.16 2.22 -8 6 3 38.53 2.43 8 -6 2 17.82 1.58 8 -6 1 24.02 1.83 8 -6 0 10.59 1.25 -8 6 0 9.17 1.33 8 -6 -1 17.80 1.58 -8 6 -1 19.97 1.82 8 -6 -2 15.88 1.50 -8 6 -2 15.28 1.60 8 -6 -3 34.68 2.21 -8 6 -3 32.48 2.24 8 -6 -4 49.53 2.66 -8 6 -4 46.49 2.68 8 -6 -5 41.25 2.35 -8 6 -5 35.90 2.26 8 -6 -6 10.05 1.15 -8 6 -6 7.49 1.06 8 -6 -7 21.52 1.62 -8 6 -7 20.99 1.54 8 -6 -8 25.81 1.69 -8 6 -8 22.65 1.51 8 -6 -9 24.76 1.61 8 -6 -10 21.77 1.42 8 -6 -11 10.81 0.93 8 -6 -12 47.60 2.03 8 -7 8 3.55 0.54 8 -7 7 52.74 2.24 8 -7 6 52.02 2.29 8 -7 5 81.21 3.19 8 -7 4 39.54 2.00 -8 7 4 38.29 2.08 8 -7 3 11.90 1.06 -8 7 3 10.35 1.14 8 -7 2 19.87 1.39 -8 7 2 21.51 1.61 8 -7 1 18.01 1.33 8 -7 0 47.27 2.31 -8 7 0 47.30 2.52 8 -7 -1 20.34 1.40 -8 7 -1 16.81 1.50 8 -7 -2 18.21 1.33 -8 7 -2 17.88 1.49 8 -7 -3 10.18 0.99 -8 7 -3 11.07 1.16 8 -7 -4 37.73 1.95 8 7 4 36.04 1.87 -8 7 -4 41.29 2.14 8 -7 -5 73.82 3.02 8 7 5 81.13 3.04 8 -7 -6 44.90 2.07 8 7 6 46.70 2.06 8 -7 -7 49.50 2.11 8 7 7 47.76 2.05 8 -7 -8 3.33 0.49 8 7 8 2.97 0.47 9 0 2 103.05 4.53 9 0 3 0.60 0.83 9 0 4 0.87 0.68 9 0 5 0.70 0.74 9 0 6 10.84 1.27 9 0 7 11.33 1.26 9 0 8 17.48 1.50 -9 0 9 1.77 0.64 -9 0 -9 0.35 0.56 9 0 10 -0.11 0.58 9 0 11 1.47 0.59 9 0 12 1.98 0.59 9 0 13 12.74 1.00 9 0 14 3.86 0.53 9 -1 13 7.46 0.75 9 -1 12 13.61 1.08 9 1 -11 13.66 1.17 9 -1 11 14.98 1.20 9 1 -10 19.08 1.45 9 -1 10 17.80 1.37 -9 1 9 0.37 0.44 9 1 -9 2.64 0.73 9 -1 9 2.17 0.67 9 1 -8 11.59 1.20 9 -1 8 9.84 1.08 -9 1 7 1.52 0.76 9 1 -7 2.22 0.80 9 -1 7 1.50 0.67 9 1 -6 6.24 1.07 9 -1 6 5.89 0.97 9 1 -5 0.43 0.65 9 -1 5 -0.14 0.66 9 1 -4 5.27 1.04 9 -1 4 4.58 0.98 9 1 -3 13.96 1.48 9 -1 3 11.95 1.44 9 1 -2 28.42 2.12 9 -1 2 26.57 2.04 9 1 -1 30.66 2.19 9 -1 1 24.43 2.00 9 1 0 79.72 3.84 9 -1 0 78.55 3.78 9 -1 -1 31.30 2.22 9 1 1 27.61 2.13 9 -1 -2 23.69 1.92 9 1 2 23.88 1.93 9 -1 -3 12.35 1.47 9 1 3 11.22 1.37 9 -1 -4 4.34 0.99 9 1 4 5.61 1.04 9 -1 -5 -0.14 0.70 9 1 5 0.34 0.63 9 -1 -6 6.37 1.07 9 1 6 6.66 1.02 -9 1 -7 1.13 0.79 9 -1 -7 2.78 0.83 9 1 7 2.52 0.79 9 -1 -8 9.72 1.15 9 1 8 10.39 1.14 9 -1 -9 2.63 0.74 9 1 9 2.91 0.71 9 -1 -10 17.48 1.45 9 1 10 18.67 1.40 9 -1 -11 15.55 1.24 9 1 11 15.26 1.21 9 1 12 14.67 1.10 9 1 13 8.81 0.80 9 -2 12 1.04 0.39 9 -2 11 8.74 0.86 9 2 -10 3.15 0.64 9 -2 10 3.25 0.65 9 2 -9 22.24 1.50 9 -2 9 23.31 1.54 9 2 -8 7.02 0.93 9 -2 8 6.50 0.88 9 -2 7 0.03 0.14 -9 2 7 2.25 0.74 9 2 -7 5.76 0.90 9 -2 7 5.61 0.88 9 -2 6 3.62 0.54 -9 2 6 3.04 0.85 9 2 -6 6.34 0.98 9 -2 6 5.97 0.95 9 2 -5 21.67 1.68 9 -2 5 17.62 1.54 -9 2 4 8.89 1.38 9 -2 4 11.24 1.30 -9 2 3 17.49 1.91 9 -2 3 24.52 1.88 9 -2 2 5.72 0.81 9 2 -2 4.13 0.91 9 -2 2 3.63 0.91 9 2 -1 14.60 1.49 9 -2 1 10.99 1.33 9 2 0 26.61 1.95 9 -2 0 25.70 1.97 -9 2 -1 9.97 1.62 9 -2 -1 12.08 1.39 9 2 1 12.87 1.39 9 -2 -2 5.85 0.86 -9 2 -2 3.07 1.13 9 -2 -2 2.40 0.87 9 2 2 5.11 0.97 9 -2 -3 52.06 2.25 9 2 3 49.38 2.13 -9 2 -3 16.87 1.95 9 -2 -3 24.02 1.93 9 2 3 31.48 2.10 9 -2 -4 26.33 1.58 9 2 4 32.27 1.65 -9 2 -4 9.58 1.50 9 -2 -4 13.22 1.42 9 2 4 16.70 1.49 9 -2 -5 38.22 1.85 9 2 5 38.58 1.77 -9 2 -5 11.85 1.54 9 -2 -5 17.75 1.61 9 2 5 22.70 1.72 9 -2 -6 14.16 1.08 9 2 6 13.23 1.02 -9 2 -6 4.04 1.00 9 -2 -6 6.95 1.02 9 2 6 5.70 0.98 9 -2 -7 11.01 0.96 9 2 7 10.79 0.88 -9 2 -7 4.14 0.90 9 -2 -7 4.72 0.90 9 2 7 5.86 0.93 9 -2 -8 13.53 1.00 9 2 8 13.47 0.94 -9 2 -8 3.20 0.78 9 -2 -8 6.97 0.96 9 2 8 8.36 0.99 9 -2 -9 45.63 1.81 9 2 9 43.22 1.68 9 -2 -9 23.43 1.69 9 2 9 23.08 1.64 9 -2 -10 3.05 0.65 9 2 10 3.70 0.67 9 2 11 7.90 0.80 9 2 12 0.87 0.37 9 -3 9 20.12 1.21 9 3 -8 8.68 0.88 9 -3 8 17.75 1.19 -9 3 7 2.37 0.61 9 3 -7 2.03 0.55 -9 3 6 23.27 1.74 9 3 -6 25.12 1.58 -9 3 5 16.29 1.46 9 3 -5 14.80 1.24 9 -3 5 16.62 1.31 9 3 -4 64.60 2.90 9 -3 4 60.58 2.92 9 3 -3 49.79 2.47 9 -3 3 46.03 2.47 9 3 -2 21.66 1.53 9 -3 2 16.91 1.46 9 3 -1 3.26 0.69 9 -3 1 3.40 0.78 9 -3 0 3.20 0.68 -9 3 0 0.31 0.81 9 3 0 1.83 0.64 9 -3 0 1.46 0.62 -9 3 -1 3.69 1.07 9 -3 -1 3.37 0.76 9 3 1 3.96 0.78 -9 3 -2 15.03 1.59 9 -3 -2 17.23 1.44 9 3 2 17.55 1.40 9 -3 -3 90.44 3.19 9 3 3 91.95 3.12 -9 3 -3 54.76 3.07 9 -3 -3 44.39 2.59 9 3 3 46.48 2.54 9 -3 -4 136.15 4.03 9 3 4 138.65 3.95 -9 3 -4 72.20 3.68 9 -3 -4 59.77 3.25 9 3 4 69.98 3.29 9 -3 -5 36.52 1.82 9 3 5 36.33 1.76 -9 3 -5 18.29 1.60 9 -3 -5 15.40 1.37 9 3 5 19.44 1.41 9 -3 -6 74.06 2.61 9 3 6 69.42 2.46 -9 3 -6 44.09 2.34 9 -3 -6 28.95 1.93 9 3 6 31.13 1.91 9 -3 -7 9.29 0.90 9 3 7 9.40 0.86 -9 3 -7 3.39 0.71 9 -3 -7 4.33 0.71 9 3 7 3.61 0.65 9 -3 -8 43.54 1.80 9 3 8 45.13 1.74 9 -3 -8 18.29 1.30 9 3 8 15.02 1.19 9 -3 -9 49.98 1.82 9 3 9 49.63 1.74 9 -3 -9 21.52 1.35 9 3 9 15.30 1.16 9 -3 -10 3.86 0.53 9 -4 8 17.24 1.04 9 -4 7 3.94 0.56 9 -4 6 8.69 0.83 9 -4 5 21.96 1.29 -9 4 5 8.96 1.02 9 -4 4 14.76 1.10 -9 4 4 6.46 0.93 -9 4 3 4.18 0.85 9 -4 3 2.12 0.48 9 -4 2 4.54 0.72 9 -4 2 0.94 0.40 9 -4 1 48.38 2.02 9 -4 1 15.07 1.11 -9 4 0 26.19 1.79 9 -4 0 12.48 1.03 -9 4 -1 30.88 1.95 9 -4 -1 14.36 1.12 -9 4 -2 2.92 0.82 9 -4 -2 1.09 0.42 9 -4 -3 9.70 0.95 9 4 3 10.08 0.94 -9 4 -3 7.50 1.01 9 -4 -4 15.05 1.19 9 4 4 15.97 1.17 9 -4 -5 23.71 1.45 9 4 5 21.98 1.37 9 -4 -6 9.98 0.92 9 4 6 8.66 0.86 9 -4 -7 3.26 0.58 9 4 7 3.56 0.58 9 -4 -8 19.71 1.19 9 4 8 20.40 1.17 9 -4 -9 0.60 0.31 9 4 9 0.57 0.31 9 -5 5 30.31 1.48 9 -5 4 4.87 0.61 9 -5 3 19.48 1.21 9 -5 2 12.23 0.95 -9 5 2 7.23 0.88 9 -5 1 34.62 1.73 9 -5 0 89.73 3.05 -9 5 0 58.84 2.90 9 -5 -1 35.49 1.71 -9 5 -1 24.99 1.65 9 -5 -2 13.05 1.00 -9 5 -2 9.71 0.99 9 -5 -3 19.80 1.24 9 -5 -4 4.87 0.60 9 -5 -5 28.38 1.45 9 -5 -6 14.56 0.95 0 0 0 0.00 0.00 TITL wangr_41_190419 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 7.901886 10.295521 25.995202 90.0000 90.0000 90.0000 ZERR 9.00 0.000122 0.000144 0.000370 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 99.00 90.00 9.00 9.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 89053 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 3.592 _oxdiff_exptl_absorpt_empirical_full_min 0.800 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O25 O 0.2726(2) 0.76873(16) 0.35850(6) 0.0198(4) Uani 1 1 d . O22 O 0.6743(2) 0.61347(17) 0.33641(7) 0.0220(4) Uani 1 1 d . O17 O 0.4051(2) 0.16376(17) 0.66315(7) 0.0231(4) Uani 1 1 d . O20 O 0.0190(2) 0.51169(17) 0.48539(7) 0.0219(4) Uani 1 1 d . O11 O 0.1545(2) 0.35629(17) 0.52805(6) 0.0202(4) Uani 1 1 d . O24 O 0.5275(3) 0.65205(18) 0.26406(6) 0.0263(4) Uani 1 1 d . O30 O 0.2564(3) 0.47283(18) 0.24651(6) 0.0253(4) Uani 1 1 d . H30 H 0.334379 0.508225 0.231142 0.038 Uiso 1 1 calc GR O27 O 0.4794(3) 0.91845(19) 0.34958(9) 0.0363(5) Uani 1 1 d . C10 C 0.3469(3) 0.4663(2) 0.42300(9) 0.0168(5) Uani 1 1 d . C21 C 0.5372(3) 0.6032(2) 0.30621(9) 0.0190(5) Uani 1 1 d . C16 C 0.3907(3) 0.1577(3) 0.61084(9) 0.0219(5) Uani 1 1 d . H16 H 0.407598 0.083095 0.591326 0.026 Uiso 1 1 calc R C15 C 0.3485(3) 0.2749(2) 0.59136(9) 0.0200(5) Uani 1 1 d . C14 C 0.1522(3) 0.4617(2) 0.49709(8) 0.0177(5) Uani 1 1 d . C4 C 0.3677(3) 0.6999(2) 0.39829(9) 0.0183(5) Uani 1 1 d . H4 H 0.484876 0.730961 0.398339 0.022 Uiso 1 1 calc R C5 C 0.3660(3) 0.5557(2) 0.38586(9) 0.0167(5) Uani 1 1 d . C29 C 0.2398(3) 0.5286(2) 0.29640(9) 0.0202(5) Uani 1 1 d . H29A H 0.146771 0.486528 0.314121 0.024 Uiso 1 1 calc R H29B H 0.211367 0.619798 0.292720 0.024 Uiso 1 1 calc R C13 C 0.4418(3) 0.4156(2) 0.51528(9) 0.0180(5) Uani 1 1 d . H13A H 0.535315 0.379394 0.495805 0.022 Uiso 1 1 calc R H13B H 0.487294 0.466384 0.543518 0.022 Uiso 1 1 calc R C7 C 0.4703(3) 0.3765(2) 0.32745(9) 0.0193(5) Uani 1 1 d . H7A H 0.481090 0.349792 0.291822 0.023 Uiso 1 1 calc R H7B H 0.581674 0.373617 0.343067 0.023 Uiso 1 1 calc R C12 C 0.3269(3) 0.3069(2) 0.53567(9) 0.0190(5) Uani 1 1 d . H12 H 0.343283 0.228356 0.514989 0.023 Uiso 1 1 calc R C8 C 0.3531(3) 0.2842(2) 0.35543(9) 0.0203(5) Uani 1 1 d . H8A H 0.394641 0.195926 0.351995 0.024 Uiso 1 1 calc R H8B H 0.240966 0.288214 0.340335 0.024 Uiso 1 1 calc R C6 C 0.4007(3) 0.5169(2) 0.32983(9) 0.0176(5) Uani 1 1 d . C3 C 0.2869(3) 0.7316(2) 0.44945(9) 0.0196(5) Uani 1 1 d . H3A H 0.165879 0.716292 0.447608 0.024 Uiso 1 1 calc R H3B H 0.304958 0.822475 0.457579 0.024 Uiso 1 1 calc R C1 C 0.3293(3) 0.5012(2) 0.48034(9) 0.0173(5) Uani 1 1 d . C2 C 0.3643(3) 0.6468(2) 0.49136(9) 0.0189(5) Uani 1 1 d . H2 H 0.487122 0.659339 0.490094 0.023 Uiso 1 1 calc R C19 C 0.3331(4) 0.3608(3) 0.63459(9) 0.0242(5) Uani 1 1 d . H19 H 0.303940 0.448288 0.633837 0.029 Uiso 1 1 calc R C9 C 0.3438(3) 0.3209(2) 0.41234(9) 0.0183(5) Uani 1 1 d . H9A H 0.240684 0.284921 0.426708 0.022 Uiso 1 1 calc R H9B H 0.438357 0.280874 0.430096 0.022 Uiso 1 1 calc R C18 C 0.3692(3) 0.2892(3) 0.67631(10) 0.0237(5) Uani 1 1 d . H18 H 0.369758 0.320900 0.709816 0.028 Uiso 1 1 calc R C31 C 0.3044(4) 0.6898(2) 0.54487(9) 0.0226(5) Uani 1 1 d . H31A H 0.325000 0.781121 0.549051 0.034 Uiso 1 1 calc GR H31B H 0.365295 0.642438 0.570728 0.034 Uiso 1 1 calc GR H31C H 0.185469 0.672893 0.548293 0.034 Uiso 1 1 calc GR C26 C 0.3417(4) 0.8779(2) 0.33829(10) 0.0226(5) Uani 1 1 d . C28 C 0.2257(4) 0.9366(3) 0.29934(11) 0.0287(6) Uani 1 1 d . H28A H 0.236740 0.890892 0.267329 0.043 Uiso 1 1 calc GR H28B H 0.254700 1.026260 0.294398 0.043 Uiso 1 1 calc GR H28C H 0.110976 0.930337 0.311276 0.043 Uiso 1 1 calc GR C23 C 0.8125(4) 0.6892(3) 0.31551(11) 0.0271(6) Uani 1 1 d . H23A H 0.852645 0.649135 0.284469 0.041 Uiso 1 1 calc GR H23B H 0.902859 0.693117 0.340151 0.041 Uiso 1 1 calc GR H23C H 0.773707 0.775511 0.308046 0.041 Uiso 1 1 calc GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O25 0.0238(9) 0.0158(8) 0.0198(8) 0.0027(6) -0.0019(7) 0.0000(7) O22 0.0184(8) 0.0250(8) 0.0226(8) 0.0014(7) 0.0011(7) -0.0033(7) O17 0.0254(9) 0.0259(9) 0.0181(8) 0.0038(7) 0.0012(7) 0.0040(8) O20 0.0205(9) 0.0237(8) 0.0214(8) -0.0008(7) -0.0004(7) 0.0021(7) O11 0.0170(8) 0.0222(8) 0.0214(8) 0.0036(7) -0.0005(7) -0.0013(7) O24 0.0331(10) 0.0268(9) 0.0190(8) 0.0048(7) 0.0011(8) -0.0044(8) O30 0.0305(10) 0.0275(10) 0.0177(8) -0.0024(7) -0.0035(7) -0.0003(8) O27 0.0345(11) 0.0257(9) 0.0487(12) 0.0123(9) -0.0063(10) -0.0083(9) C10 0.0159(11) 0.0179(11) 0.0165(10) -0.0017(9) -0.0011(9) 0.0005(9) C21 0.0210(12) 0.0170(10) 0.0191(11) -0.0018(9) 0.0005(10) 0.0023(9) C16 0.0256(12) 0.0227(12) 0.0173(11) 0.0006(10) 0.0025(9) 0.0032(10) C15 0.0213(12) 0.0197(11) 0.0191(11) 0.0009(9) 0.0021(10) -0.0004(10) C14 0.0227(12) 0.0160(11) 0.0145(10) -0.0034(8) -0.0015(9) 0.0003(10) C4 0.0211(12) 0.0163(11) 0.0174(11) 0.0018(9) -0.0013(9) 0.0004(9) C5 0.0159(11) 0.0163(11) 0.0179(11) -0.0018(9) -0.0014(9) 0.0003(9) C29 0.0218(12) 0.0203(12) 0.0186(11) 0.0000(9) -0.0003(10) 0.0010(10) C13 0.0176(12) 0.0213(11) 0.0152(10) -0.0002(9) -0.0017(9) 0.0000(9) C7 0.0233(12) 0.0177(11) 0.0169(10) -0.0010(9) 0.0013(10) 0.0011(10) C12 0.0180(11) 0.0191(11) 0.0198(11) 0.0001(9) 0.0000(9) 0.0012(10) C8 0.0269(13) 0.0151(10) 0.0189(11) -0.0018(9) -0.0002(10) 0.0001(10) C6 0.0202(11) 0.0167(10) 0.0159(11) 0.0003(9) 0.0005(9) -0.0014(9) C3 0.0239(12) 0.0158(11) 0.0190(11) -0.0022(9) 0.0016(9) 0.0003(10) C1 0.0200(11) 0.0158(11) 0.0162(10) -0.0004(9) -0.0015(9) 0.0001(9) C2 0.0232(12) 0.0167(11) 0.0169(10) -0.0014(9) 0.0005(9) -0.0027(10) C19 0.0311(13) 0.0210(11) 0.0206(11) -0.0010(10) 0.0019(11) 0.0010(11) C9 0.0210(12) 0.0158(11) 0.0181(11) 0.0021(9) -0.0017(9) 0.0006(9) C18 0.0267(14) 0.0257(12) 0.0186(11) -0.0015(10) 0.0041(10) 0.0008(11) C31 0.0294(14) 0.0206(12) 0.0178(11) -0.0030(9) 0.0023(10) -0.0019(10) C26 0.0289(13) 0.0157(11) 0.0233(11) 0.0006(9) 0.0025(11) -0.0003(10) C28 0.0369(15) 0.0226(12) 0.0265(13) 0.0062(10) -0.0019(12) 0.0005(12) C23 0.0231(13) 0.0292(14) 0.0291(13) 0.0001(11) 0.0056(11) -0.0064(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C26 O25 C4 118.02(19) C21 O22 C23 115.6(2) C18 O17 C16 106.0(2) C14 O11 C12 111.79(18) C29 O30 H30 109.5 C5 C10 C1 123.1(2) C5 C10 C9 123.0(2) C9 C10 C1 113.87(19) O22 C21 C6 112.41(19) O24 C21 O22 123.3(2) O24 C21 C6 124.2(2) O17 C16 H16 124.7 C15 C16 O17 110.7(2) C15 C16 H16 124.7 C16 C15 C12 126.1(2) C16 C15 C19 106.1(2) C19 C15 C12 127.8(2) O20 C14 O11 120.2(2) O20 C14 C1 127.9(2) O11 C14 C1 111.89(19) O25 C4 H4 109.1 O25 C4 C5 108.60(19) O25 C4 C3 107.51(19) C5 C4 H4 109.1 C3 C4 H4 109.1 C3 C4 C5 113.3(2) C10 C5 C4 121.2(2) C10 C5 C6 121.6(2) C4 C5 C6 117.04(19) O30 C29 H29A 108.8 O30 C29 H29B 108.8 O30 C29 C6 113.9(2) H29A C29 H29B 107.7 C6 C29 H29A 108.8 C6 C29 H29B 108.8 H13A C13 H13B 108.7 C12 C13 H13A 110.5 C12 C13 H13B 110.5 C12 C13 C1 106.14(19) C1 C13 H13A 110.5 C1 C13 H13B 110.5 H7A C7 H7B 108.1 C8 C7 H7A 109.5 C8 C7 H7B 109.5 C8 C7 C6 110.5(2) C6 C7 H7A 109.5 C6 C7 H7B 109.5 O11 C12 C15 108.25(19) O11 C12 C13 104.48(18) O11 C12 H12 109.5 C15 C12 C13 115.3(2) C15 C12 H12 109.5 C13 C12 H12 109.5 C7 C8 H8A 109.7 C7 C8 H8B 109.7 C7 C8 C9 109.8(2) H8A C8 H8B 108.2 C9 C8 H8A 109.7 C9 C8 H8B 109.7 C21 C6 C5 110.88(19) C21 C6 C29 108.06(19) C21 C6 C7 106.04(19) C5 C6 C29 111.5(2) C5 C6 C7 110.14(18) C29 C6 C7 110.04(19) C4 C3 H3A 109.7 C4 C3 H3B 109.7 C4 C3 C2 109.6(2) H3A C3 H3B 108.2 C2 C3 H3A 109.7 C2 C3 H3B 109.7 C10 C1 C13 112.56(19) C10 C1 C2 112.88(19) C14 C1 C10 107.30(19) C14 C1 C13 102.02(18) C14 C1 C2 111.68(19) C13 C1 C2 109.87(19) C3 C2 C1 110.49(19) C3 C2 H2 107.3 C3 C2 C31 111.0(2) C1 C2 H2 107.3 C31 C2 C1 113.1(2) C31 C2 H2 107.3 C15 C19 H19 127.0 C18 C19 C15 106.0(2) C18 C19 H19 127.0 C10 C9 C8 114.76(19) C10 C9 H9A 108.6 C10 C9 H9B 108.6 C8 C9 H9A 108.6 C8 C9 H9B 108.6 H9A C9 H9B 107.6 O17 C18 H18 124.4 C19 C18 O17 111.2(2) C19 C18 H18 124.4 C2 C31 H31A 109.5 C2 C31 H31B 109.5 C2 C31 H31C 109.5 H31A C31 H31B 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 O25 C26 C28 110.6(2) O27 C26 O25 123.9(2) O27 C26 C28 125.5(2) C26 C28 H28A 109.5 C26 C28 H28B 109.5 C26 C28 H28C 109.5 H28A C28 H28B 109.5 H28A C28 H28C 109.5 H28B C28 H28C 109.5 O22 C23 H23A 109.5 O22 C23 H23B 109.5 O22 C23 H23C 109.5 H23A C23 H23B 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O25 C4 1.462(3) O25 C26 1.355(3) O22 C21 1.342(3) O22 C23 1.448(3) O17 C16 1.366(3) O17 C18 1.366(3) O20 C14 1.210(3) O11 C14 1.351(3) O11 C12 1.468(3) O24 C21 1.208(3) O30 H30 0.8200 O30 C29 1.424(3) O27 C26 1.202(4) C10 C5 1.343(3) C10 C1 1.539(3) C10 C9 1.523(3) C21 C6 1.526(3) C16 H16 0.9300 C16 C15 1.350(4) C15 C12 1.495(3) C15 C19 1.435(3) C14 C1 1.522(3) C4 H4 0.9800 C4 C5 1.519(3) C4 C3 1.511(3) C5 C6 1.535(3) C29 H29A 0.9700 C29 H29B 0.9700 C29 C6 1.544(3) C13 H13A 0.9700 C13 H13B 0.9700 C13 C12 1.536(3) C13 C1 1.547(3) C7 H7A 0.9700 C7 H7B 0.9700 C7 C8 1.514(3) C7 C6 1.548(3) C12 H12 0.9800 C8 H8A 0.9700 C8 H8B 0.9700 C8 C9 1.528(3) C3 H3A 0.9700 C3 H3B 0.9700 C3 C2 1.524(3) C1 C2 1.550(3) C2 H2 0.9800 C2 C31 1.534(3) C19 H19 0.9300 C19 C18 1.342(4) C9 H9A 0.9700 C9 H9B 0.9700 C18 H18 0.9300 C31 H31A 0.9600 C31 H31B 0.9600 C31 H31C 0.9600 C26 C28 1.494(4) C28 H28A 0.9600 C28 H28B 0.9600 C28 H28C 0.9600 C23 H23A 0.9600 C23 H23B 0.9600 C23 H23C 0.9600 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion O25 C4 C5 C10 -139.7(2) O25 C4 C5 C6 44.8(3) O25 C4 C3 C2 171.65(18) O22 C21 C6 C5 48.9(3) O22 C21 C6 C29 171.44(19) O22 C21 C6 C7 -70.6(2) O17 C16 C15 C12 177.9(2) O17 C16 C15 C19 -0.8(3) O20 C14 C1 C10 -70.8(3) O20 C14 C1 C13 170.7(2) O20 C14 C1 C2 53.4(3) O11 C14 C1 C10 108.2(2) O11 C14 C1 C13 -10.3(2) O11 C14 C1 C2 -127.6(2) O24 C21 C6 C5 -134.4(2) O24 C21 C6 C29 -11.9(3) O24 C21 C6 C7 106.1(3) O30 C29 C6 C21 68.2(3) O30 C29 C6 C5 -169.64(19) O30 C29 C6 C7 -47.1(3) C10 C5 C6 C21 -136.9(2) C10 C5 C6 C29 102.6(3) C10 C5 C6 C7 -19.8(3) C10 C1 C2 C3 40.3(3) C10 C1 C2 C31 165.4(2) C16 O17 C18 C19 0.1(3) C16 C15 C12 O11 121.8(3) C16 C15 C12 C13 -121.6(3) C16 C15 C19 C18 0.8(3) C15 C19 C18 O17 -0.6(3) C14 O11 C12 C15 136.5(2) C14 O11 C12 C13 13.1(2) C14 C1 C2 C3 -80.7(2) C14 C1 C2 C31 44.4(3) C4 O25 C26 O27 3.2(4) C4 O25 C26 C28 -178.6(2) C4 C5 C6 C21 38.5(3) C4 C5 C6 C29 -81.9(3) C4 C5 C6 C7 155.6(2) C4 C3 C2 C1 -62.0(3) C4 C3 C2 C31 171.7(2) C5 C10 C1 C14 114.4(3) C5 C10 C1 C13 -134.2(2) C5 C10 C1 C2 -9.1(3) C5 C10 C9 C8 -3.7(4) C5 C4 C3 C2 51.7(3) C13 C1 C2 C3 166.84(19) C13 C1 C2 C31 -68.0(3) C7 C8 C9 C10 37.0(3) C12 O11 C14 O20 177.4(2) C12 O11 C14 C1 -1.7(3) C12 C15 C19 C18 -177.9(3) C12 C13 C1 C10 -97.2(2) C12 C13 C1 C14 17.5(2) C12 C13 C1 C2 136.1(2) C8 C7 C6 C21 173.58(19) C8 C7 C6 C5 53.6(3) C8 C7 C6 C29 -69.8(2) C6 C7 C8 C9 -62.6(3) C3 C4 C5 C10 -20.4(3) C3 C4 C5 C6 164.2(2) C1 C10 C5 C4 -1.4(4) C1 C10 C5 C6 173.9(2) C1 C10 C9 C8 177.4(2) C1 C13 C12 O11 -18.9(2) C1 C13 C12 C15 -137.6(2) C19 C15 C12 O11 -59.7(3) C19 C15 C12 C13 56.8(3) C9 C10 C5 C4 179.8(2) C9 C10 C5 C6 -5.0(4) C9 C10 C1 C14 -66.7(3) C9 C10 C1 C13 44.8(3) C9 C10 C1 C2 169.9(2) C18 O17 C16 C15 0.4(3) C26 O25 C4 C5 -134.0(2) C26 O25 C4 C3 103.1(2) C23 O22 C21 O24 0.6(3) C23 O22 C21 C6 177.3(2)