#------------------------------------------------------------------------------ #$Date: 2020-02-05 01:38:20 +0200 (Wed, 05 Feb 2020) $ #$Revision: 247848 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/72/1557224.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557224 loop_ _publ_author_name 'Nohara, Isaak' 'Keller, Aramis' 'Tarassenko, Nikolai' 'Prescimone, Alessandro' 'Constable, Edwin C.' 'Housecroft, Catherine E.' _publ_section_title ; Heteroleptic [Cu(P^P)(N^N)][PF6] Compounds with Isomeric Dibromo-1,10-Phenanthroline Ligands ; _journal_issue 1 _journal_name_full Inorganics _journal_page_first 4 _journal_paper_doi 10.3390/inorganics8010004 _journal_volume 8 _journal_year 2020 _chemical_formula_moiety 'C48 H34 Br2 Cu N2 O P2, F6 P, 1[CH2Cl2]' _chemical_formula_sum 'C49 H36 Br2 Cl2 Cu F6 N2 O P3' _chemical_formula_weight 1169.97 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2019-09-30 _audit_creation_method ; Olex2 1.2 (compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 70.330(3) _cell_angle_beta 77.791(3) _cell_angle_gamma 87.292(3) _cell_formula_units_Z 4 _cell_length_a 12.4032(9) _cell_length_b 18.9805(14) _cell_length_c 22.0591(17) _cell_measurement_reflns_used 9774 _cell_measurement_temperature 130 _cell_measurement_theta_max 70.343 _cell_measurement_theta_min 3.802 _cell_volume 4777.9(6) _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection 'Apex2 (Bruker AXS, 2006)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 130 _diffrn_measured_fraction_theta_full 0.988 _diffrn_measured_fraction_theta_max 0.958 _diffrn_measurement_device Area _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f & \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0261 _diffrn_reflns_av_unetI/netI 0.0293 _diffrn_reflns_Laue_measured_fraction_full 0.988 _diffrn_reflns_Laue_measured_fraction_max 0.958 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 42627 _diffrn_reflns_point_group_measured_fraction_full 0.988 _diffrn_reflns_point_group_measured_fraction_max 0.958 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 70.417 _diffrn_reflns_theta_min 3.647 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 5.128 _exptl_absorpt_correction_T_max 0.7533 _exptl_absorpt_correction_T_min 0.6714 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0640 before and 0.0349 after correction. The Ratio of minimum to maximum transmission is 0.8913. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.626 _exptl_crystal_description block _exptl_crystal_F_000 2336 _exptl_crystal_recrystallization_method 'The material was recrystallised from a mixture of DCM and ethanol by solvent layering' _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.1 _refine_diff_density_max 1.283 _refine_diff_density_min -0.900 _refine_diff_density_rms 0.065 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.008 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1135 _refine_ls_number_reflns 17481 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.008 _refine_ls_R_factor_all 0.0350 _refine_ls_R_factor_gt 0.0327 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0367P)^2^+6.2344P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0817 _refine_ls_wR_factor_ref 0.0834 _reflns_Friedel_coverage 0.000 _reflns_number_gt 16297 _reflns_number_total 17481 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ISN164_130K_0m.cif _cod_data_source_block isn164_130k_0m _cod_database_code 1557224 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.628 _shelx_estimated_absorpt_t_min 0.427 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C57(H57), C56(H56), C49(H49), C44(H44), C10(H10), C14(H14), C11(H11), C50(H50), C59(H59), C60(H60), C12(H12), C20(H20), C62(H62), C38(H38), C92(H92), C2(H2), C86(H86), C9(H9), C66(H66), C81(H81), C42(H42), C90(H90), C45(H45), C15(H15), C87(H87), C48(H48), C16(H16), C18(H18), C68(H68), C1(H1), C65(H65), C75(H75), C24(H24), C41(H41), C78(H78), C72(H72), C94(H94), C21(H21), C29(H29), C96(H96), C63(H63), C17(H17), C82(H82), C64(H64), C27(H27), C33(H33), C93(H93), C84(H84), C36(H36), C76(H76), C88(H88), C46(H46), C28(H28), C77(H77), C47(H47), C34(H34), C35(H35), C95(H95), C30(H30), C39(H39), C83(H83), C22(H22), C71(H71), C23(H23), C40(H40), C89(H89), C69(H69), C70(H70) ; _shelx_res_file ; isn164_130k_0m.res created by SHELXL-2014/7 TITL isn164_130k_0m_a.res in P-1 REM Old TITL ISN164_130K_0m in P-1 REM SHELXT solution in P-1 REM R1 0.162, Rweak 0.008, Alpha 0.059, Orientation as input REM Formula found by SHELXT: C101 N3 O5 F12 P6 Cu2 Br4 CELL 1.54178 12.4032 18.9805 22.0591 70.33 77.791 87.292 ZERR 4 0.0009 0.0014 0.0017 0.003 0.003 0.003 LATT 1 SFAC Br C Cl Cu F H N O P UNIT 8 196 8 4 24 144 8 4 12 L.S. 10 PLAN 10 SIZE 0.1 0.15 0.2 TEMP -143.15 BOND $H list 4 ABIN fmap 2 53 acta OMIT 0 0 1 OMIT 0 1 0 OMIT -1 1 1 OMIT 0 -1 1 OMIT 0 -2 1 OMIT 2 0 3 OMIT 2 -1 4 OMIT -1 2 1 OMIT 1 2 0 REM REM REM WGHT 0.036700 6.234400 FVAR 0.18411 BR2 1 0.031837 0.290767 0.797314 11.00000 0.03410 0.03141 = 0.01660 -0.00782 -0.00604 0.00653 BR1 1 -0.199159 0.486773 0.479833 11.00000 0.03218 0.03491 = 0.02466 -0.00808 -0.00980 0.01779 BR4 1 0.822065 0.163994 0.784533 11.00000 0.02922 0.02645 = 0.03673 -0.00609 -0.00856 0.00863 BR3 1 0.442638 0.411547 0.565587 11.00000 0.04416 0.05867 = 0.01516 -0.00664 -0.01044 0.01795 CU1 4 0.218573 0.247433 0.503191 11.00000 0.02502 0.01643 = 0.01726 -0.00424 -0.00088 0.00463 CU2 4 0.344826 0.306016 0.895815 11.00000 0.02606 0.02242 = 0.01437 -0.00258 -0.00266 -0.00010 P4 9 0.412258 0.394290 0.927293 11.00000 0.02555 0.02188 = 0.01541 -0.00356 -0.00244 -0.00058 P3 9 0.204315 0.238664 0.971560 11.00000 0.02429 0.02165 = 0.01583 -0.00026 -0.00442 -0.00016 P1 9 0.132134 0.144784 0.503840 11.00000 0.02308 0.01606 = 0.01836 -0.00292 -0.00184 0.00303 P2 9 0.375214 0.277333 0.426898 11.00000 0.02506 0.01700 = 0.01795 -0.00402 0.00004 0.00301 P5 9 -0.031311 0.466968 0.237630 11.00000 0.03574 0.02712 = 0.01913 -0.00699 -0.00709 0.00712 P6 9 0.452128 0.080892 0.723997 11.00000 0.02505 0.02321 = 0.03071 -0.00317 -0.00502 0.00238 O1 8 0.209134 0.248772 0.364206 11.00000 0.03100 0.01938 = 0.02307 -0.00588 -0.00064 0.00123 O2 8 0.381986 0.260552 1.040448 11.00000 0.02981 0.02592 = 0.01683 -0.00293 -0.00148 -0.00313 F10 5 0.451062 -0.007378 0.759655 11.00000 0.05617 0.02470 = 0.05216 -0.00573 -0.00333 0.00896 F3 5 -0.043565 0.521467 0.280201 11.00000 0.08584 0.03144 = 0.03162 -0.01441 -0.01968 0.01559 F7 5 0.451384 0.168873 0.687748 11.00000 0.05394 0.02738 = 0.08112 0.00759 -0.03052 -0.00506 F6 5 -0.022343 0.411917 0.196522 11.00000 0.08872 0.05548 = 0.04749 -0.03408 -0.02106 0.01398 N1 7 0.104770 0.332111 0.485344 11.00000 0.02732 0.01710 = 0.01783 -0.00403 -0.00351 0.00487 N2 7 0.179369 0.260242 0.594384 11.00000 0.02451 0.01961 = 0.01993 -0.00588 -0.00323 0.00411 N4 7 0.481877 0.245326 0.871135 11.00000 0.03106 0.01827 = 0.01839 -0.00135 -0.00544 0.00217 N3 7 0.355492 0.337365 0.795358 11.00000 0.02520 0.02187 = 0.01827 -0.00412 -0.00530 0.00059 F1 5 -0.096053 0.521669 0.188524 11.00000 0.14528 0.10727 = 0.06334 -0.05156 -0.07210 0.09099 F8 5 0.329834 0.082532 0.762393 11.00000 0.05615 0.05308 = 0.10500 -0.00085 0.03110 0.01741 C4 2 -0.040027 0.390963 0.543962 11.00000 0.02435 0.01980 = 0.02008 -0.00543 -0.00500 0.00451 C54 2 0.518137 0.264827 0.804701 11.00000 0.02714 0.01498 = 0.01805 -0.00322 -0.00625 -0.00119 C52 2 0.480912 0.333894 0.694756 11.00000 0.02707 0.01716 = 0.01863 -0.00376 -0.00665 -0.00149 C53 2 0.448914 0.313005 0.763874 11.00000 0.02509 0.01510 = 0.01841 -0.00375 -0.00512 -0.00134 C6 2 0.092895 0.306033 0.600153 11.00000 0.02165 0.01659 = 0.01808 -0.00333 -0.00343 0.00197 F12 5 0.404151 0.070313 0.667193 11.00000 0.16809 0.07055 = 0.06521 -0.02104 -0.06326 -0.00333 C7 2 0.043542 0.318076 0.659635 11.00000 0.02405 0.02014 = 0.01786 -0.00552 -0.00368 0.00116 C5 2 0.051589 0.343970 0.541256 11.00000 0.02310 0.01697 = 0.01724 -0.00423 -0.00337 0.00258 C61 2 0.124452 0.178626 0.946762 11.00000 0.03053 0.02278 = 0.01863 0.00048 -0.00839 0.00001 C57 2 0.583590 0.308735 0.666403 11.00000 0.03229 0.02132 = 0.01674 -0.00578 -0.00384 0.00079 AFIX 43 H57 6 0.605099 0.322115 0.619919 11.00000 -1.20000 AFIX 0 C73 2 0.247971 0.170925 1.043384 11.00000 0.02745 0.02618 = 0.01657 0.00044 -0.00372 0.00040 C55 2 0.620071 0.242168 0.775075 11.00000 0.02726 0.01506 = 0.02321 -0.00468 -0.00624 0.00021 C51 2 0.408265 0.381008 0.658680 11.00000 0.03379 0.02738 = 0.01512 -0.00331 -0.00790 0.00056 C56 2 0.650589 0.266149 0.704791 11.00000 0.02707 0.01912 = 0.02453 -0.00744 -0.00303 0.00329 AFIX 43 H56 6 0.719540 0.251849 0.684554 11.00000 -1.20000 AFIX 0 C85 2 0.557575 0.379002 0.931086 11.00000 0.02685 0.01915 = 0.02148 -0.00492 -0.00335 -0.00102 C13 2 0.367093 0.373395 0.372564 11.00000 0.02413 0.01859 = 0.01919 -0.00313 0.00095 0.00221 C49 2 0.291832 0.382807 0.758658 11.00000 0.02365 0.02940 = 0.02226 -0.00697 -0.00574 0.00305 AFIX 43 H49 6 0.227367 0.400747 0.780142 11.00000 -1.20000 AFIX 0 C74 2 0.332119 0.189400 1.069050 11.00000 0.02891 0.02589 = 0.01724 -0.00139 -0.00177 -0.00086 C3 2 -0.074353 0.425450 0.484043 11.00000 0.02762 0.02094 = 0.02435 -0.00562 -0.00851 0.00952 C44 2 0.228010 0.027432 0.459640 11.00000 0.02611 0.02287 = 0.02548 -0.00640 -0.00200 -0.00010 AFIX 43 H44 6 0.180003 0.039101 0.429467 11.00000 -1.20000 AFIX 0 C8 2 0.089411 0.279437 0.714948 11.00000 0.02786 0.02293 = 0.01730 -0.00606 -0.00353 0.00046 C10 2 0.219329 0.225522 0.647877 11.00000 0.02880 0.02561 = 0.02296 -0.00558 -0.00725 0.00984 AFIX 43 H10 6 0.279773 0.193465 0.644335 11.00000 -1.20000 AFIX 0 C14 2 0.365965 0.429331 0.400259 11.00000 0.03131 0.02396 = 0.01975 -0.00604 -0.00443 0.00257 AFIX 43 H14 6 0.374944 0.416658 0.444362 11.00000 -1.20000 AFIX 0 C11 2 -0.047722 0.367015 0.660199 11.00000 0.02541 0.02853 = 0.02118 -0.01130 -0.00265 0.00660 AFIX 43 H11 6 -0.080879 0.375544 0.699991 11.00000 -1.20000 AFIX 0 C50 2 0.314922 0.405663 0.689796 11.00000 0.02847 0.03293 = 0.02164 -0.00506 -0.01127 0.00579 AFIX 43 H50 6 0.266575 0.437666 0.665286 11.00000 -1.20000 AFIX 0 C59 2 0.647746 0.177220 0.885214 11.00000 0.03731 0.02303 = 0.02780 -0.00079 -0.01427 0.00837 AFIX 43 H59 6 0.691142 0.146799 0.914317 11.00000 -1.20000 AFIX 0 C58 2 0.683473 0.197111 0.818588 11.00000 0.02738 0.01629 = 0.03089 -0.00647 -0.00719 0.00210 C60 2 0.545362 0.202854 0.909557 11.00000 0.03955 0.02560 = 0.01992 -0.00018 -0.00760 0.00317 AFIX 43 H60 6 0.520378 0.189053 0.955884 11.00000 -1.20000 AFIX 0 C43 2 0.224888 0.068318 0.501752 11.00000 0.02004 0.01730 = 0.02141 -0.00169 0.00243 0.00208 C80 2 0.343499 0.389128 1.010414 11.00000 0.02401 0.03286 = 0.01905 -0.00928 -0.00294 -0.00141 F5 5 0.077529 0.507935 0.193801 11.00000 0.06308 0.17856 = 0.10435 -0.09352 0.03189 -0.05689 C12 2 -0.087844 0.401390 0.605416 11.00000 0.02607 0.02683 = 0.02252 -0.00937 -0.00611 0.01040 AFIX 43 H12 6 -0.149029 0.433141 0.607652 11.00000 -1.20000 AFIX 0 C20 2 0.520331 0.232302 0.511821 11.00000 0.03259 0.02119 = 0.02829 -0.00813 -0.00369 0.00489 AFIX 43 H20 6 0.458546 0.204265 0.542318 11.00000 -1.20000 AFIX 0 F4 5 0.037751 0.413407 0.285386 11.00000 0.25973 0.09097 = 0.08440 -0.05847 -0.11774 0.11751 C31 2 0.106192 0.215227 0.373648 11.00000 0.03247 0.01928 = 0.02465 -0.00589 -0.00534 0.00315 C62 2 0.010936 0.164770 0.970445 11.00000 0.02983 0.03927 = 0.02594 -0.00637 -0.00482 -0.00304 AFIX 43 H62 6 -0.028543 0.188427 0.999831 11.00000 -1.20000 AFIX 0 C37 2 0.020605 0.100833 0.574277 11.00000 0.02546 0.02534 = 0.01885 -0.00637 -0.00244 0.00046 C38 2 0.017966 0.025642 0.612005 11.00000 0.03221 0.02973 = 0.02586 -0.00302 0.00000 -0.00067 AFIX 43 H38 6 0.077312 -0.005206 0.602753 11.00000 -1.20000 AFIX 0 F11 5 0.572905 0.078842 0.686613 11.00000 0.04052 0.09015 = 0.15999 0.03064 0.03696 0.01744 C92 2 0.486200 0.545893 0.877691 11.00000 0.03398 0.02864 = 0.02261 -0.00720 -0.00433 -0.00144 AFIX 43 H92 6 0.544755 0.530097 0.900482 11.00000 -1.20000 AFIX 0 C91 2 0.409013 0.493659 0.879977 11.00000 0.03217 0.02329 = 0.01737 -0.00420 -0.00222 0.00050 C2 2 -0.019061 0.415311 0.427123 11.00000 0.03594 0.02606 = 0.01885 -0.00343 -0.00872 0.00991 AFIX 43 H2 6 -0.041387 0.439830 0.386665 11.00000 -1.20000 AFIX 0 C86 2 0.629782 0.378633 0.873196 11.00000 0.03096 0.02526 = 0.02392 -0.00668 -0.00085 -0.00258 AFIX 43 H86 6 0.602224 0.387898 0.834254 11.00000 -1.20000 AFIX 0 F9 5 0.497702 0.091826 0.781366 11.00000 0.20902 0.05121 = 0.10768 -0.01534 -0.11282 -0.00314 C67 2 0.100564 0.293868 1.006145 11.00000 0.02445 0.02933 = 0.02635 -0.00850 -0.00589 0.00039 C9 2 0.177026 0.233668 0.709328 11.00000 0.03225 0.02715 = 0.01946 -0.00405 -0.00854 0.00685 AFIX 43 H9 6 0.208479 0.207988 0.746256 11.00000 -1.20000 AFIX 0 C26 2 0.302864 0.209843 0.348749 11.00000 0.03527 0.01708 = 0.01624 -0.00174 0.00332 0.00128 C19 2 0.508912 0.276146 0.448871 11.00000 0.02708 0.02234 = 0.02617 -0.00849 -0.00244 0.00469 C66 2 0.181114 0.144364 0.903119 11.00000 0.03128 0.02662 = 0.02814 -0.00469 -0.00914 0.00260 AFIX 43 H66 6 0.257927 0.154242 0.885999 11.00000 -1.20000 AFIX 0 C81 2 0.295314 0.449698 1.026613 11.00000 0.02866 0.03400 = 0.02881 -0.01137 -0.00264 -0.00076 AFIX 43 H81 6 0.302864 0.498042 0.994059 11.00000 -1.20000 AFIX 0 C42 2 -0.067006 0.145556 0.589289 11.00000 0.03058 0.03496 = 0.03027 -0.01405 -0.00432 0.00539 AFIX 43 H42 6 -0.064783 0.197552 0.564960 11.00000 -1.20000 AFIX 0 C90 2 0.599274 0.364728 0.987773 11.00000 0.03325 0.03735 = 0.02359 -0.00842 -0.00641 -0.00044 AFIX 43 H90 6 0.551580 0.364699 1.027624 11.00000 -1.20000 AFIX 0 C32 2 0.061088 0.163059 0.435089 11.00000 0.02819 0.01882 = 0.02230 -0.00635 -0.00555 0.00636 C45 2 0.301499 -0.030541 0.461772 11.00000 0.03472 0.02560 = 0.03953 -0.01414 0.00041 0.00298 AFIX 43 H45 6 0.305409 -0.057460 0.432064 11.00000 -1.20000 AFIX 0 C15 2 0.351928 0.503176 0.364354 11.00000 0.03493 0.02180 = 0.02478 -0.00914 0.00078 0.00052 AFIX 43 H15 6 0.353658 0.541129 0.383318 11.00000 -1.20000 AFIX 0 C25 2 0.393826 0.221501 0.372344 11.00000 0.03430 0.01711 = 0.01739 -0.00255 0.00199 0.00291 C87 2 0.740337 0.365044 0.871698 11.00000 0.03322 0.03269 = 0.03702 -0.01432 0.00214 0.00104 AFIX 43 H87 6 0.788641 0.365517 0.831899 11.00000 -1.20000 AFIX 0 C48 2 0.295272 0.050423 0.546242 11.00000 0.02705 0.02464 = 0.03094 -0.00720 -0.00562 0.00235 AFIX 43 H48 6 0.294545 0.079012 0.574345 11.00000 -1.20000 AFIX 0 C79 2 0.330050 0.318606 1.059397 11.00000 0.02457 0.03120 = 0.02122 -0.00898 -0.00357 -0.00212 C16 2 0.335299 0.521898 0.300573 11.00000 0.04473 0.01875 = 0.02240 -0.00028 -0.00069 0.00257 AFIX 43 H16 6 0.323799 0.572472 0.276239 11.00000 -1.20000 AFIX 0 C18 2 0.353034 0.392971 0.307816 11.00000 0.04615 0.02195 = 0.01914 -0.00681 -0.00196 -0.00189 AFIX 43 H18 6 0.355465 0.355598 0.287792 11.00000 -1.20000 AFIX 0 C68 2 0.044774 0.270476 1.071656 11.00000 0.03531 0.04655 = 0.02749 -0.01086 -0.00425 0.00277 AFIX 43 H68 6 0.058937 0.223087 1.101141 11.00000 -1.20000 AFIX 0 C1 2 0.071046 0.368067 0.429788 11.00000 0.03572 0.02383 = 0.01559 -0.00542 -0.00306 0.00686 AFIX 43 H1 6 0.109891 0.361346 0.390193 11.00000 -1.20000 AFIX 0 C65 2 0.125361 0.095592 0.884492 11.00000 0.04614 0.02795 = 0.03785 -0.01139 -0.01671 0.00822 AFIX 43 H65 6 0.164228 0.071766 0.855079 11.00000 -1.20000 AFIX 0 C75 2 0.374032 0.137775 1.119338 11.00000 0.03228 0.03849 = 0.02267 0.00070 -0.00797 0.00039 AFIX 43 H75 6 0.431771 0.151937 1.135485 11.00000 -1.20000 AFIX 0 C24 2 0.600338 0.318288 0.404908 11.00000 0.03203 0.03784 = 0.03031 -0.00198 -0.00176 0.00062 AFIX 43 H24 6 0.593522 0.349077 0.361966 11.00000 -1.20000 AFIX 0 C41 2 -0.157074 0.114233 0.639565 11.00000 0.02849 0.05784 = 0.03658 -0.02698 0.00016 0.00415 AFIX 43 H41 6 -0.217382 0.144503 0.648575 11.00000 -1.20000 AFIX 0 C78 2 0.205980 0.097375 1.071688 11.00000 0.04244 0.02916 = 0.03107 0.00167 -0.01207 -0.00646 AFIX 43 H78 6 0.148170 0.082671 1.055930 11.00000 -1.20000 AFIX 0 C72 2 0.077479 0.362983 0.963336 11.00000 0.02863 0.03054 = 0.03917 -0.00857 -0.00746 0.00125 AFIX 43 H72 6 0.115434 0.379317 0.918612 11.00000 -1.20000 AFIX 0 C94 2 0.393078 0.644629 0.808917 11.00000 0.05112 0.02250 = 0.03468 -0.00060 -0.00502 0.00280 AFIX 43 H94 6 0.387830 0.696134 0.784692 11.00000 -1.20000 AFIX 0 C21 2 0.621118 0.229030 0.530635 11.00000 0.04296 0.03131 = 0.03611 -0.01285 -0.01468 0.00968 AFIX 43 H21 6 0.628223 0.198500 0.573597 11.00000 -1.20000 AFIX 0 C29 2 0.495774 0.139662 0.318466 11.00000 0.05171 0.03115 = 0.03035 -0.01146 0.00309 0.01559 AFIX 43 H29 6 0.562321 0.115416 0.307881 11.00000 -1.20000 AFIX 0 C96 2 0.324235 0.517891 0.846045 11.00000 0.03921 0.02865 = 0.04102 -0.00416 -0.01509 -0.00110 AFIX 43 H96 6 0.271507 0.482701 0.846852 11.00000 -1.20000 AFIX 0 C63 2 -0.044161 0.116819 0.951319 11.00000 0.03393 0.04456 = 0.03822 -0.00716 -0.00887 -0.00825 AFIX 43 H63 6 -0.121372 0.107875 0.967300 11.00000 -1.20000 AFIX 0 C17 2 0.335515 0.466889 0.272623 11.00000 0.05744 0.02599 = 0.01755 -0.00214 -0.00592 -0.00060 AFIX 43 H17 6 0.323622 0.479641 0.229092 11.00000 -1.20000 AFIX 0 C82 2 0.236111 0.440417 1.089956 11.00000 0.03635 0.04282 = 0.03501 -0.02016 0.00212 0.00029 AFIX 43 H82 6 0.203212 0.482186 1.100496 11.00000 -1.20000 AFIX 0 C64 2 0.013197 0.081928 0.908941 11.00000 0.04651 0.03096 = 0.04073 -0.00915 -0.01910 -0.00307 AFIX 43 H64 6 -0.024613 0.048328 0.896499 11.00000 -1.20000 AFIX 0 C27 2 0.306841 0.164775 0.310268 11.00000 0.04866 0.02431 = 0.02149 -0.00669 -0.00170 -0.00016 AFIX 43 H27 6 0.244116 0.158476 0.294065 11.00000 -1.20000 AFIX 0 C33 2 -0.044583 0.134290 0.442994 11.00000 0.03147 0.02224 = 0.02928 -0.00520 -0.00581 0.00135 AFIX 43 H33 6 -0.077268 0.097903 0.483694 11.00000 -1.20000 AFIX 0 C93 2 0.477753 0.621080 0.842141 11.00000 0.04329 0.02662 = 0.03020 -0.00928 -0.00104 -0.00558 AFIX 43 H93 6 0.530671 0.656501 0.840714 11.00000 -1.20000 AFIX 0 C84 2 0.272363 0.308560 1.122739 11.00000 0.03879 0.03812 = 0.02092 -0.00561 -0.00002 -0.00740 AFIX 43 H84 6 0.265096 0.260363 1.155506 11.00000 -1.20000 AFIX 0 C36 2 0.049100 0.239584 0.323461 11.00000 0.04984 0.02841 = 0.02826 0.00099 -0.01194 -0.00075 AFIX 43 H36 6 0.081779 0.275594 0.282534 11.00000 -1.20000 AFIX 0 C76 2 0.330518 0.065176 1.145751 11.00000 0.04562 0.03410 = 0.02677 0.00790 -0.01196 0.00388 AFIX 43 H76 6 0.358652 0.029199 1.180074 11.00000 -1.20000 AFIX 0 C88 2 0.780511 0.350713 0.928512 11.00000 0.02915 0.04571 = 0.05431 -0.01747 -0.00785 0.00542 AFIX 43 H88 6 0.856515 0.340973 0.927831 11.00000 -1.20000 AFIX 0 C46 2 0.369067 -0.049095 0.507208 11.00000 0.02740 0.02640 = 0.05418 -0.01249 -0.00463 0.00843 AFIX 43 H46 6 0.417686 -0.089661 0.509329 11.00000 -1.20000 AFIX 0 C28 2 0.403990 0.129144 0.295923 11.00000 0.06115 0.02700 = 0.02564 -0.01247 0.00020 0.00579 AFIX 43 H28 6 0.407627 0.097223 0.270397 11.00000 -1.20000 AFIX 0 C77 2 0.246724 0.045395 1.122210 11.00000 0.05405 0.02780 = 0.03478 0.00697 -0.01175 -0.00453 AFIX 43 H77 6 0.216529 -0.004186 1.140658 11.00000 -1.20000 AFIX 0 C47 2 0.366199 -0.008835 0.549623 11.00000 0.02674 0.02799 = 0.04423 -0.00485 -0.01198 0.00421 AFIX 43 H47 6 0.412522 -0.021786 0.580769 11.00000 -1.20000 AFIX 0 C34 2 -0.102759 0.157650 0.392796 11.00000 0.03571 0.03484 = 0.04206 -0.00955 -0.01486 0.00228 AFIX 43 H34 6 -0.174305 0.137079 0.399193 11.00000 -1.20000 AFIX 0 C35 2 -0.056443 0.211123 0.333157 11.00000 0.05056 0.04039 = 0.03992 -0.00260 -0.02554 0.00371 AFIX 43 H35 6 -0.096956 0.228160 0.299092 11.00000 -1.20000 AFIX 0 C95 2 0.316168 0.593602 0.810815 11.00000 0.04893 0.03363 = 0.04862 -0.00005 -0.02226 0.00433 AFIX 43 H95 6 0.257574 0.609919 0.788139 11.00000 -1.20000 AFIX 0 C30 2 0.491298 0.185502 0.356531 11.00000 0.03895 0.02734 = 0.02596 -0.00761 0.00019 0.00832 AFIX 43 H30 6 0.554735 0.192390 0.371858 11.00000 -1.20000 AFIX 0 C39 2 -0.071623 -0.004711 0.663463 11.00000 0.04488 0.04061 = 0.02827 0.00188 0.00105 -0.00981 AFIX 43 H39 6 -0.072248 -0.056009 0.689701 11.00000 -1.20000 AFIX 0 C83 2 0.225300 0.370029 1.137622 11.00000 0.04189 0.05090 = 0.02611 -0.01653 0.00837 -0.00670 AFIX 43 H83 6 0.185240 0.363829 1.180930 11.00000 -1.20000 AFIX 0 C22 2 0.711234 0.270470 0.486492 11.00000 0.03215 0.04048 = 0.05501 -0.01586 -0.01637 0.00693 AFIX 43 H22 6 0.780235 0.268194 0.499188 11.00000 -1.20000 AFIX 0 C71 2 -0.001020 0.408146 0.985917 11.00000 0.03500 0.03643 = 0.07070 -0.02083 -0.01659 0.00733 AFIX 43 H71 6 -0.017612 0.454858 0.956440 11.00000 -1.20000 AFIX 0 F2 5 -0.138737 0.425916 0.282858 11.00000 0.14830 0.19199 = 0.09514 -0.09293 0.08025 -0.12335 C23 2 0.700778 0.315244 0.423820 11.00000 0.03026 0.04719 = 0.05073 -0.00783 -0.00180 -0.00364 AFIX 43 H23 6 0.762491 0.343875 0.393792 11.00000 -1.20000 AFIX 0 C40 2 -0.159271 0.038966 0.676635 11.00000 0.03650 0.06235 = 0.02589 -0.01251 0.00807 -0.01232 AFIX 43 H40 6 -0.220984 0.017552 0.711010 11.00000 -1.20000 AFIX 0 C89 2 0.710335 0.350550 0.986151 11.00000 0.03947 0.05247 = 0.04107 -0.01520 -0.01813 0.00652 AFIX 43 H89 6 0.738338 0.340645 1.025022 11.00000 -1.20000 AFIX 0 C69 2 -0.032212 0.317311 1.093641 11.00000 0.03874 0.07408 = 0.04338 -0.03348 -0.00031 0.00272 AFIX 43 H69 6 -0.069336 0.302058 1.138513 11.00000 -1.20000 AFIX 0 C70 2 -0.054671 0.385164 1.050974 11.00000 0.03302 0.05926 = 0.07657 -0.04394 -0.01133 0.01123 AFIX 43 H70 6 -0.107506 0.416430 1.066411 11.00000 -1.20000 AFIX 0 HKLF 4 REM isn164_130k_0m_a.res in P-1 REM R1 = 0.0327 for 16297 Fo > 4sig(Fo) and 0.0350 for all 17481 data REM 1135 parameters refined using 0 restraints END WGHT 0.0367 6.2347 REM Highest difference peak 1.283, deepest hole -0.900, 1-sigma level 0.065 Q1 1 -0.0408 0.3992 0.2999 11.00000 0.05 1.28 Q2 1 0.4107 0.1036 0.7800 11.00000 0.05 1.06 Q3 1 0.3320 0.0732 0.7163 11.00000 0.05 1.02 Q4 1 0.5009 0.0620 0.6610 11.00000 0.05 1.01 Q5 1 -0.1714 0.4604 0.2593 11.00000 0.05 0.99 Q6 1 0.5614 0.0848 0.7373 11.00000 0.05 0.91 Q7 1 -0.1210 0.4018 0.2818 11.00000 0.05 0.89 Q8 1 0.0757 0.4651 0.2336 11.00000 0.05 0.86 Q9 1 0.0630 0.4249 0.2802 11.00000 0.05 0.84 Q10 1 -0.0216 0.5330 0.1786 11.00000 0.05 0.65 ; _shelx_res_checksum 24976 _shelx_hkl_file ; -1 0 0 1.10 0.20 -1 0 0 -0.10 0.20 1 0 0 0.20 0.20 1 0 0 0.20 0.20 1 0 0 0.00 0.10 -2 0 0 494.45 17.30 -2 0 0 424.66 20.90 2 0 0 442.16 20.20 2 0 0 443.86 20.90 2 0 0 464.75 18.10 -3 0 0 809.32 29.80 3 0 0 735.53 35.90 3 0 0 797.62 29.00 3 0 0 751.82 34.70 3 0 0 815.72 31.20 -4 0 0 5.30 0.80 4 0 0 0.80 0.60 4 0 0 0.80 0.60 4 0 0 0.20 0.50 4 0 0 2.50 0.50 -5 0 0 960.40 37.90 5 0 0 971.60 44.40 5 0 0 1040.10 34.30 5 0 0 1006.90 36.70 5 0 0 985.90 39.70 6 0 0 196.48 7.00 6 0 0 179.08 9.80 -7 0 0 755.82 23.10 7 0 0 724.43 25.80 -8 0 0 521.95 16.40 8 0 0 508.55 18.30 -9 0 0 69.19 2.90 9 0 0 63.49 3.20 -10 0 0 1.20 0.80 -10 0 0 4.40 0.70 10 0 0 3.30 1.00 10 0 0 2.30 0.80 -11 0 0 0.00 0.70 -11 0 0 0.10 0.60 11 0 0 0.30 0.70 11 0 0 0.10 0.70 -12 0 0 120.79 3.90 -12 0 0 114.89 4.50 12 0 0 117.69 4.70 -13 0 0 48.70 1.90 13 0 0 48.50 2.30 -14 0 0 0.30 0.40 -14 1 0 -0.20 0.40 13 -1 0 0.70 0.60 -13 1 0 -0.50 0.50 12 -1 0 22.40 1.60 -12 1 0 21.10 1.60 -12 1 0 21.00 1.40 11 -1 0 36.50 2.10 11 -1 0 38.10 2.40 -11 1 0 38.00 1.80 -11 1 0 36.60 2.10 10 -1 0 108.49 4.50 10 -1 0 124.69 5.00 -10 1 0 109.59 3.80 -10 1 0 110.39 4.30 9 -1 0 27.40 2.00 -9 1 0 27.20 1.70 8 -1 0 81.49 3.60 -8 1 0 84.09 3.20 7 -1 0 28.90 1.80 7 -1 0 32.50 3.20 -7 1 0 30.70 1.50 6 -1 0 414.66 14.80 6 -1 0 424.16 20.10 5 -1 0 15.40 1.80 5 -1 0 20.60 1.20 5 -1 0 20.60 2.10 -5 1 0 19.90 1.40 4 -1 0 1.30 0.70 4 -1 0 1.30 0.70 4 -1 0 1.20 0.50 4 -1 0 1.90 0.60 4 -1 0 1.50 0.50 -4 1 0 1.40 0.60 -4 1 0 1.50 0.50 3 -1 0 86.09 3.70 3 -1 0 86.29 4.50 3 -1 0 90.79 4.10 3 -1 0 79.29 4.50 -3 1 0 83.09 4.50 2 -1 0 424.86 16.90 2 -1 0 389.06 19.70 2 -1 0 459.15 19.10 2 -1 0 443.66 18.30 -2 1 0 416.46 19.70 1 -1 0 1150.98 44.80 1 -1 0 1010.80 48.10 1 -1 0 1025.50 46.20 -1 1 0 1124.39 44.90 -1 1 0 1038.50 48.10 -1 1 0 984.70 46.80 0 -1 0 188.88 7.90 0 1 0 167.88 6.80 -1 -1 0 2081.69 76.49 -1 -1 0 1941.61 89.89 1 1 0 2037.40 79.99 1 1 0 2027.20 76.39 -2 -1 0 151.98 5.80 2 1 0 139.19 6.80 2 1 0 155.38 6.20 -3 -1 0 1429.16 52.29 3 1 0 1423.66 54.89 3 1 0 1320.87 60.69 3 1 0 1289.57 62.99 3 1 0 1452.25 51.19 -4 -1 0 19.80 1.30 4 1 0 20.90 1.50 4 1 0 19.20 1.70 4 1 0 23.50 1.20 4 1 0 20.10 1.70 -5 -1 0 164.08 7.00 5 1 0 183.98 6.30 5 1 0 177.08 6.70 5 1 0 159.28 8.50 5 1 0 169.28 7.50 6 1 0 9.90 1.80 6 1 0 10.70 1.50 6 1 0 11.00 0.80 6 1 0 12.40 1.10 -7 -1 0 44.60 2.00 7 1 0 47.60 2.30 -8 -1 0 365.36 11.90 8 1 0 366.76 13.20 -9 -1 0 117.89 4.40 9 1 0 117.79 4.90 -10 -1 0 282.27 9.80 -10 -1 0 296.47 8.80 10 1 0 301.57 11.00 -11 -1 0 17.10 1.60 -11 -1 0 17.30 1.30 11 1 0 13.40 1.60 11 1 0 16.20 1.40 -12 -1 0 1.10 0.60 -12 -1 0 1.30 0.70 12 1 0 1.60 0.70 -13 -1 0 141.89 4.40 13 1 0 138.59 5.30 -14 -1 0 4.80 0.70 14 1 0 5.50 0.80 -14 2 0 1.90 0.50 -13 2 0 0.80 0.50 -12 2 0 24.30 1.40 -12 2 0 27.50 1.70 11 -2 0 170.08 6.50 11 -2 0 168.68 7.00 11 -2 0 170.78 5.10 -11 2 0 172.18 5.40 -11 2 0 177.38 6.10 10 -2 0 7.60 1.20 10 -2 0 7.70 1.40 -10 2 0 7.90 1.20 9 -2 0 107.99 4.70 -9 2 0 108.59 4.10 8 -2 0 50.69 2.60 8 -2 0 52.69 5.20 -8 2 0 49.80 2.20 7 -2 0 7.80 1.00 7 -2 0 10.50 2.20 -7 2 0 5.80 0.80 6 -2 0 215.98 8.00 6 -2 0 222.08 11.50 5 -2 0 23.50 1.60 5 -2 0 26.90 2.50 5 -2 0 25.00 1.40 -5 2 0 23.70 2.50 -5 2 0 23.50 1.70 4 -2 0 16.50 1.80 4 -2 0 13.80 1.00 4 -2 0 15.60 1.10 4 -2 0 14.20 1.00 -4 2 0 14.40 1.50 -4 2 0 17.80 1.80 3 -2 0 86.79 3.80 3 -2 0 97.09 4.20 3 -2 0 83.89 4.80 -3 2 0 87.19 4.90 -3 2 0 93.89 4.90 2 -2 0 265.27 12.30 -2 2 0 263.07 12.70 -2 2 0 266.17 12.30 1 -2 0 231.88 10.70 1 -2 0 241.08 10.70 -1 2 0 231.88 10.70 0 -2 0 293.07 13.10 0 -2 0 291.17 13.40 0 2 0 280.67 13.30 0 2 0 322.07 11.90 -1 -2 0 382.56 13.80 -1 -2 0 343.57 16.20 1 2 0 374.66 14.40 1 2 0 326.47 16.20 -2 -2 0 1.50 0.70 -2 -2 0 2.60 0.50 2 2 0 2.70 0.70 2 2 0 1.80 0.70 -3 -2 0 379.06 15.40 3 2 0 404.56 17.90 3 2 0 404.76 16.30 3 2 0 410.56 15.10 -4 -2 0 3.40 0.60 4 2 0 3.60 0.80 4 2 0 4.00 0.70 4 2 0 2.40 0.60 4 2 0 2.60 0.70 5 2 0 81.89 4.50 5 2 0 81.49 3.40 5 2 0 76.29 4.00 6 2 0 16.00 1.30 6 2 0 15.10 1.10 6 2 0 15.00 1.70 -7 -2 0 611.84 18.70 7 2 0 589.04 22.10 7 2 0 580.04 20.80 -8 -2 0 154.48 5.50 8 2 0 160.78 6.20 -9 -2 0 1.60 0.70 9 2 0 1.90 0.80 -10 -2 0 48.80 2.50 -10 -2 0 51.89 2.20 10 2 0 51.79 2.80 10 2 0 55.79 2.60 -11 -2 0 54.89 2.20 -11 -2 0 54.69 2.70 11 2 0 52.79 2.60 -12 -2 0 110.69 4.40 -12 -2 0 110.69 3.70 12 2 0 117.19 4.50 -13 -2 0 15.60 1.10 13 2 0 17.40 1.30 -14 -2 0 4.00 0.60 14 2 0 4.80 0.80 -14 3 0 19.20 1.00 -13 3 0 0.60 0.50 12 -3 0 3.10 0.50 -12 3 0 2.40 0.60 -12 3 0 2.70 0.70 11 -3 0 132.29 4.00 11 -3 0 124.59 5.60 -11 3 0 133.79 4.80 10 -3 0 122.09 3.80 10 -3 0 126.99 5.40 -10 3 0 123.89 4.60 9 -3 0 1.60 0.80 -9 3 0 1.90 0.60 8 -3 0 127.69 5.30 -8 3 0 132.89 4.60 7 -3 0 62.29 2.90 7 -3 0 67.19 5.00 -7 3 0 61.09 2.40 6 -3 0 2825.12 121.69 6 -3 0 2676.03 94.09 5 -3 0 46.30 3.70 5 -3 0 48.30 2.20 -5 3 0 46.40 3.40 4 -3 0 183.18 8.50 4 -3 0 205.78 7.10 4 -3 0 197.28 9.90 -4 3 0 205.08 9.80 3 -3 0 2065.29 91.39 -3 3 0 2186.28 92.39 -3 3 0 1984.70 94.99 2 -3 0 368.56 16.70 2 -3 0 361.76 16.70 -2 3 0 367.76 17.30 -2 3 0 351.06 16.60 1 -3 0 1811.72 81.29 1 -3 0 1850.11 80.39 -1 3 0 1754.12 81.29 -1 3 0 1926.31 72.69 0 -3 0 1.20 0.40 0 -3 0 1.10 0.40 0 3 0 2.40 0.60 0 3 0 1.20 0.50 -1 -3 0 -0.50 0.50 -1 -3 0 -0.40 0.50 1 3 0 -0.60 0.50 1 3 0 -0.10 0.50 -2 -3 0 4269.97 190.78 -2 -3 0 4310.37 162.88 2 3 0 4333.67 191.08 2 3 0 4344.77 171.08 -3 -3 0 1221.28 46.90 3 3 0 1341.27 46.00 3 3 0 1268.27 49.30 3 3 0 1118.09 54.09 -4 -3 0 28.20 1.60 4 3 0 27.40 2.00 4 3 0 23.80 1.80 4 3 0 35.30 1.70 5 3 0 18.30 1.80 5 3 0 19.30 1.40 6 3 0 308.57 12.40 6 3 0 340.37 11.50 6 3 0 316.27 13.80 -7 -3 0 70.09 2.80 7 3 0 71.69 3.00 7 3 0 65.29 3.00 7 3 0 67.89 4.00 -8 -3 0 84.89 3.40 8 3 0 89.19 3.80 -9 -3 0 5.40 1.00 -10 -3 0 62.39 2.90 -10 -3 0 63.89 2.40 10 3 0 59.09 2.90 10 3 0 59.29 2.40 -11 -3 0 55.99 2.20 -11 -3 0 53.59 2.60 11 3 0 46.50 2.00 -12 -3 0 1.60 0.80 -12 -3 0 0.90 0.60 12 3 0 2.20 0.70 -13 -3 0 1.50 0.50 13 3 0 1.30 0.60 -14 -3 0 1.20 0.40 14 3 0 1.30 0.50 -14 4 0 6.50 0.60 -13 4 0 30.30 1.40 12 -4 0 2.50 0.50 -12 4 0 3.10 0.70 -12 4 0 2.30 0.60 11 -4 0 3.50 0.60 -11 4 0 4.60 0.80 10 -4 0 61.79 3.20 10 -4 0 60.79 2.10 -10 4 0 61.09 2.70 9 -4 0 127.49 5.40 -9 4 0 127.09 4.60 8 -4 0 9.10 1.20 -8 4 0 6.00 0.90 7 -4 0 62.19 5.00 7 -4 0 57.69 2.80 -7 4 0 56.59 2.30 6 -4 0 749.03 26.50 6 -4 0 772.62 35.30 5 -4 0 31.10 1.70 5 -4 0 30.90 3.10 -5 4 0 30.40 2.80 4 -4 0 959.10 45.40 4 -4 0 1028.20 34.80 -4 4 0 1037.20 45.60 3 -4 0 10.20 1.60 -3 4 0 8.70 1.30 2 -4 0 17.40 1.80 2 -4 0 9.20 1.20 -2 4 0 10.30 1.30 1 -4 0 508.15 23.20 1 -4 0 516.45 23.10 -1 4 0 532.35 20.40 -1 4 0 494.05 23.20 0 -4 0 4.50 1.00 0 -4 0 8.00 1.10 0 4 0 8.20 1.10 0 4 0 7.60 1.10 -1 -4 0 95.89 4.60 -1 -4 0 87.69 4.90 -1 -4 0 89.49 4.10 1 4 0 96.29 4.90 1 4 0 100.59 4.30 -2 -4 0 1401.36 54.59 2 4 0 1513.25 64.29 2 4 0 1402.46 57.19 -3 -4 0 31.30 1.80 3 4 0 31.50 2.00 3 4 0 32.00 1.70 -4 -4 0 51.29 2.60 4 4 0 49.60 2.50 4 4 0 50.99 2.90 5 4 0 291.77 11.70 5 4 0 314.67 13.00 6 4 0 173.38 6.30 6 4 0 162.88 6.90 6 4 0 173.48 7.90 -7 -4 0 1740.33 52.69 7 4 0 1673.33 63.49 7 4 0 1709.93 68.59 -8 -4 0 51.99 2.40 8 4 0 52.29 2.40 -9 -4 0 34.50 2.10 -10 -4 0 98.19 3.30 -10 -4 0 94.79 3.90 10 4 0 90.39 4.00 10 4 0 94.79 3.40 -11 -4 0 7.90 1.30 -11 -4 0 9.20 1.10 11 4 0 6.70 0.90 11 4 0 7.80 1.20 -12 -4 0 236.08 8.10 -12 -4 0 225.88 7.10 12 4 0 246.48 8.60 -13 -4 0 44.90 1.70 13 4 0 44.90 2.20 -14 -4 0 0.10 0.30 14 4 0 0.20 0.40 -14 5 0 60.49 2.00 13 -5 0 64.69 2.20 -13 5 0 68.29 2.30 12 -5 0 34.60 1.40 -12 5 0 34.80 1.80 11 -5 0 16.20 1.00 -11 5 0 17.20 1.40 10 -5 0 1.40 0.40 10 -5 0 0.80 0.80 -10 5 0 2.10 0.70 9 -5 0 69.39 3.50 -9 5 0 73.59 2.90 8 -5 0 23.80 1.70 -8 5 0 22.70 1.30 7 -5 0 251.07 13.90 7 -5 0 262.27 9.50 -7 5 0 252.37 8.20 6 -5 0 7.90 1.00 6 -5 0 6.00 1.70 5 -5 0 83.19 3.40 5 -5 0 82.19 5.40 -5 5 0 81.89 5.10 4 -5 0 267.27 13.50 4 -5 0 267.47 9.70 -4 5 0 281.87 13.30 3 -5 0 695.73 32.80 3 -5 0 714.43 25.00 -3 5 0 762.22 32.90 2 -5 0 99.39 4.90 2 -5 0 97.29 5.40 -2 5 0 99.29 5.20 1 -5 0 110.39 6.00 1 -5 0 118.99 6.10 1 -5 0 116.59 5.70 -1 5 0 131.49 5.00 -1 5 0 109.59 5.90 0 -5 0 26.20 1.90 0 -5 0 24.60 1.70 0 -5 0 25.20 1.80 0 5 0 27.10 1.60 0 5 0 23.50 1.90 -1 -5 0 1819.22 79.59 1 5 0 1753.82 72.29 1 5 0 1897.01 81.19 -2 -5 0 32.30 1.90 2 5 0 31.50 2.00 2 5 0 33.60 2.40 -3 -5 0 97.29 4.60 3 5 0 108.59 4.40 3 5 0 103.99 4.90 -4 -5 0 395.86 15.80 4 5 0 407.76 15.40 4 5 0 400.46 16.80 5 5 0 181.58 7.40 5 5 0 180.38 8.30 -6 -5 0 763.92 23.70 6 5 0 764.62 31.10 6 5 0 742.93 28.60 -7 -5 0 52.99 2.40 7 5 0 58.39 2.90 7 5 0 56.89 3.70 -8 -5 0 2.50 0.70 8 5 0 0.80 0.60 -9 -5 0 59.59 2.80 -10 -5 0 -0.20 0.60 -10 -5 0 1.30 0.80 10 5 0 1.40 0.70 10 5 0 0.70 0.50 -11 -5 0 5.10 0.70 -11 -5 0 3.90 0.90 11 5 0 7.20 0.90 11 5 0 6.10 1.20 -12 -5 0 13.40 1.10 -12 -5 0 13.10 1.30 12 5 0 15.50 1.00 12 5 0 14.20 1.30 -13 -5 0 63.59 2.20 13 5 0 61.99 2.70 14 5 0 5.20 0.70 13 -6 0 48.20 1.70 12 -6 0 5.00 0.80 -12 6 0 6.20 0.90 11 -6 0 15.40 1.00 -11 6 0 17.00 1.30 10 -6 0 3.40 1.00 10 -6 0 4.40 0.50 -10 6 0 3.60 0.70 -10 6 0 3.10 0.90 9 -6 0 598.94 21.70 -9 6 0 591.94 19.10 -9 6 0 629.14 20.80 8 -6 0 53.09 2.70 -8 6 0 48.80 2.10 7 -6 0 14.90 1.40 -7 6 0 17.00 1.00 6 -6 0 67.29 3.00 6 -6 0 71.49 5.40 5 -6 0 98.49 6.20 5 -6 0 90.99 3.80 4 -6 0 1083.09 37.60 4 -6 0 1122.79 49.40 -4 6 0 1069.89 49.30 3 -6 0 438.96 21.10 3 -6 0 458.25 15.70 -3 6 0 437.46 15.00 -3 6 0 461.75 20.90 2 -6 0 116.89 6.40 2 -6 0 114.19 5.80 -2 6 0 125.39 6.20 1 -6 0 188.88 8.80 1 -6 0 186.48 9.30 -1 6 0 185.68 7.80 -1 6 0 198.68 9.30 0 -6 0 2.60 0.80 0 6 0 2.40 0.80 0 6 0 2.70 0.70 -1 -6 0 219.78 10.50 1 6 0 236.78 11.10 1 6 0 228.78 9.70 -2 -6 0 465.45 21.50 2 6 0 483.05 19.60 2 6 0 490.45 22.30 -3 -6 0 517.95 20.30 3 6 0 517.75 21.30 -4 -6 0 14.00 1.50 4 6 0 13.60 1.80 4 6 0 14.40 1.40 5 6 0 134.59 5.70 5 6 0 129.99 6.50 -6 -6 0 182.88 6.10 6 6 0 175.18 8.50 6 6 0 176.68 7.40 -7 -6 0 5.70 1.00 7 6 0 6.50 1.20 -8 -6 0 1.50 0.70 8 6 0 0.60 0.70 -9 -6 0 44.50 2.00 -9 -6 0 44.30 2.40 9 6 0 46.10 2.40 -10 -6 0 7.80 1.40 -10 -6 0 9.30 1.40 -10 -6 0 7.80 1.10 10 6 0 9.30 1.20 10 6 0 8.40 1.10 -11 -6 0 11.90 1.40 -11 -6 0 10.10 1.30 -11 -6 0 11.60 1.10 11 6 0 13.90 1.40 11 6 0 12.20 1.10 -12 -6 0 77.79 3.20 -12 -6 0 83.69 2.80 12 6 0 85.09 3.00 12 6 0 88.69 3.50 -13 -6 0 44.10 1.60 13 6 0 45.00 2.10 13 -7 0 1.90 0.40 12 -7 0 0.80 0.40 11 -7 0 13.40 0.90 -11 7 0 10.60 1.10 10 -7 0 122.29 3.60 10 -7 0 117.09 5.20 -10 7 0 114.49 4.30 -10 7 0 121.99 5.10 9 -7 0 103.19 3.20 9 -7 0 104.59 4.60 -9 7 0 106.19 3.90 -9 7 0 107.99 4.50 8 -7 0 20.30 1.70 -8 7 0 19.60 1.20 -8 7 0 19.70 1.60 7 -7 0 7.40 1.10 -7 7 0 6.20 1.10 6 -7 0 52.39 4.70 6 -7 0 49.40 2.40 -6 7 0 49.90 2.30 5 -7 0 2.50 1.40 5 -7 0 4.30 0.70 -5 7 0 3.60 0.60 4 -7 0 1176.38 52.09 4 -7 0 1137.39 39.60 -4 7 0 1157.38 51.99 -4 7 0 1126.19 37.80 3 -7 0 318.07 15.40 3 -7 0 314.27 11.00 -3 7 0 299.67 10.50 -3 7 0 317.57 15.00 2 -7 0 233.48 11.20 2 -7 0 233.38 11.90 -2 7 0 253.37 11.70 1 -7 0 136.59 7.10 1 -7 0 139.69 6.60 -1 7 0 123.79 5.80 -1 7 0 143.89 7.00 0 -7 0 78.79 4.10 0 7 0 74.99 3.70 0 7 0 83.09 4.60 -1 -7 0 1119.39 52.79 1 7 0 1279.97 54.19 1 7 0 1210.28 48.00 -2 -7 0 309.47 14.60 2 7 0 312.87 13.40 2 7 0 328.47 15.30 -3 -7 0 1.40 0.90 3 7 0 1.50 1.00 4 7 0 1417.26 56.99 5 7 0 2.80 0.50 5 7 0 2.30 1.10 5 7 0 2.10 0.90 6 7 0 563.64 23.90 6 7 0 588.34 21.80 6 7 0 544.75 17.80 7 7 0 151.08 6.50 -8 -7 0 45.60 2.50 8 7 0 49.10 2.70 -9 -7 0 260.57 8.80 -9 -7 0 259.77 7.90 9 7 0 266.07 8.60 9 7 0 275.97 9.60 -10 -7 0 42.40 1.90 -10 -7 0 42.90 2.30 10 7 0 46.20 2.10 10 7 0 45.60 2.40 -11 -7 0 62.99 2.70 -11 -7 0 61.49 2.30 11 7 0 60.79 2.40 11 7 0 61.79 2.90 -12 -7 0 3.20 0.70 -12 -7 0 4.60 0.80 12 7 0 4.30 0.70 12 7 0 3.90 0.70 -13 -7 0 16.10 1.10 13 7 0 17.10 1.20 13 -8 0 19.40 0.90 12 -8 0 24.60 1.10 11 -8 0 0.80 0.40 10 -8 0 464.85 13.00 9 -8 0 12.10 0.80 9 -8 0 13.40 1.50 -9 8 0 11.80 1.60 8 -8 0 49.10 2.70 -8 8 0 51.69 2.60 7 -8 0 260.47 9.70 7 -8 0 252.27 8.60 -7 8 0 264.27 9.30 -6 8 0 5.20 0.90 5 -8 0 996.90 45.30 5 -8 0 977.00 33.80 -5 8 0 955.60 32.30 4 -8 0 14.90 2.50 4 -8 0 10.70 1.00 -4 8 0 10.80 1.00 3 -8 0 54.49 2.30 3 -8 0 57.09 4.20 -3 8 0 50.39 2.20 2 -8 0 720.93 33.80 2 -8 0 756.82 34.80 -2 8 0 805.92 34.90 1 -8 0 23.10 2.30 1 -8 0 22.10 1.90 -1 8 0 24.00 2.20 0 -8 0 184.78 8.60 0 8 0 184.78 9.20 0 8 0 167.98 7.70 -1 -8 0 1.40 0.80 1 8 0 0.50 0.80 1 8 0 2.00 1.00 -2 -8 0 19.30 1.90 2 8 0 23.30 2.40 2 8 0 19.50 2.00 -3 -8 0 837.82 38.00 3 8 0 867.21 34.70 -4 -8 0 2.30 1.00 4 8 0 1.60 1.00 4 8 0 1.50 0.40 -5 -8 0 79.59 5.10 5 8 0 88.19 3.20 5 8 0 90.19 5.00 5 8 0 86.49 4.20 6 8 0 141.09 5.00 6 8 0 150.58 6.40 7 8 0 122.89 5.60 8 8 0 34.80 2.00 8 8 0 31.50 2.20 -9 -8 0 100.99 3.50 -9 -8 0 105.09 4.10 9 8 0 105.09 3.80 9 8 0 104.99 4.30 -10 -8 0 4.10 0.70 -10 -8 0 4.40 0.90 10 8 0 5.60 0.90 10 8 0 6.40 0.80 -11 -8 0 28.40 1.50 -11 -8 0 29.50 1.80 11 8 0 31.90 1.90 11 8 0 29.00 1.50 -12 -8 0 52.19 2.30 12 8 0 51.29 2.00 12 8 0 50.99 2.40 -13 -8 0 2.90 0.50 13 8 0 4.70 0.70 13 -9 0 11.50 0.70 12 -9 0 131.49 3.90 11 -9 0 3.00 0.50 10 -9 0 10.30 0.80 9 -9 0 5.10 0.70 9 -9 0 3.50 0.90 -9 9 0 4.20 1.00 8 -9 0 51.49 2.90 8 -9 0 54.19 2.20 -8 9 0 62.49 2.90 7 -9 0 300.37 9.90 7 -9 0 301.77 11.10 -7 9 0 293.57 10.60 6 -9 0 2.40 0.50 6 -9 0 2.90 0.70 -6 9 0 2.90 0.70 5 -9 0 193.88 10.80 5 -9 0 177.48 6.80 -5 9 0 174.08 6.50 4 -9 0 3.10 1.30 3 -9 0 255.87 13.40 2 -9 0 387.06 18.10 2 -9 0 400.36 19.00 1 -9 0 201.68 9.80 -1 9 0 207.88 10.60 0 -9 0 1219.98 55.19 0 9 0 1285.47 56.59 -1 -9 0 38.20 2.70 1 9 0 40.10 2.60 -2 -9 0 331.97 15.60 2 9 0 335.07 14.30 -3 -9 0 84.99 4.80 3 9 0 81.49 3.00 3 9 0 80.29 4.50 -4 -9 0 75.39 4.60 4 9 0 73.49 2.80 4 9 0 70.99 4.30 -5 -9 0 55.49 4.00 5 9 0 55.49 2.30 -6 -9 0 59.39 4.20 6 9 0 52.29 3.10 6 9 0 50.49 2.20 -7 -9 0 186.28 9.90 7 9 0 171.38 7.70 -8 -9 0 18.50 2.90 -8 -9 0 19.20 1.60 8 9 0 19.70 1.60 8 9 0 20.70 1.40 -9 -9 0 91.39 3.60 9 9 0 87.39 3.70 9 9 0 84.99 3.30 -10 -9 0 0.10 0.60 10 9 0 0.40 0.50 10 9 0 0.10 0.60 -11 -9 0 37.60 2.00 11 9 0 35.60 1.70 11 9 0 38.20 2.00 -12 -9 0 38.30 1.80 12 9 0 42.90 1.60 12 9 0 38.00 2.00 -13 -9 0 33.70 1.50 13 9 0 32.90 1.50 13 -10 0 51.59 1.70 12 -10 0 63.69 2.10 11 -10 0 6.90 0.70 10 -10 0 23.30 1.10 9 -10 0 17.00 0.90 9 -10 0 17.90 1.70 8 -10 0 186.88 7.50 8 -10 0 195.38 5.50 8 -10 0 194.58 6.60 7 -10 0 265.57 8.80 7 -10 0 260.97 9.90 6 -10 0 21.00 1.10 5 -10 0 14.40 0.80 5 -10 0 16.90 0.90 4 -10 0 537.95 26.30 3 -10 0 67.19 5.10 2 -10 0 889.71 39.80 1 -10 0 0.50 0.70 0 -10 0 74.19 4.40 0 10 0 81.89 2.80 -1 -10 0 272.57 12.80 1 10 0 266.47 8.60 1 10 0 260.67 11.50 -2 -10 0 237.88 11.40 2 10 0 241.28 7.60 2 10 0 220.98 10.40 -3 -10 0 980.30 44.10 3 10 0 1008.70 30.60 3 10 0 967.20 40.20 -4 -10 0 46.00 3.60 4 10 0 48.70 2.10 4 10 0 55.59 3.60 -5 -10 0 1.60 1.10 5 10 0 1.00 0.50 -6 -10 0 4.10 1.40 6 10 0 5.40 1.20 6 10 0 4.60 0.90 -7 -10 0 0.60 1.30 7 10 0 3.00 1.10 7 10 0 1.90 0.50 -8 -10 0 1.10 0.80 8 10 0 0.60 0.60 8 10 0 1.40 0.70 -9 -10 0 150.98 5.40 9 10 0 152.68 5.20 9 10 0 150.18 5.80 -10 -10 0 10.80 1.30 10 10 0 8.90 1.20 10 10 0 10.60 1.10 -11 -10 0 6.80 1.00 11 10 0 5.20 0.80 11 10 0 5.10 1.00 -12 -10 0 -0.20 0.50 12 10 0 0.40 0.40 12 10 0 -0.10 0.50 12 -11 0 45.20 1.50 11 -11 0 5.90 0.60 11 -11 0 5.10 0.60 10 -11 0 47.50 2.00 10 -11 0 47.40 1.70 9 -11 0 37.90 1.70 9 -11 0 37.50 1.40 8 -11 0 332.87 9.20 8 -11 0 323.57 10.90 7 -11 0 19.00 1.00 6 -11 0 1.40 0.40 5 -11 0 174.38 5.90 4 -11 0 308.37 10.10 -2 11 0 9.30 0.70 -1 11 0 98.29 3.40 0 -11 0 80.39 4.70 0 11 0 77.69 2.90 -1 -11 0 18.70 2.00 1 11 0 18.80 1.10 -2 -11 0 72.29 4.40 2 11 0 67.89 2.60 2 11 0 66.99 4.00 -3 -11 0 44.90 3.40 3 11 0 45.50 2.00 3 11 0 42.40 3.20 -4 -11 0 40.90 3.40 4 11 0 43.80 1.90 -5 -11 0 17.50 2.50 5 11 0 18.10 1.20 -6 -11 0 1.90 1.30 6 11 0 0.60 0.50 -7 -11 0 6.60 1.00 7 11 0 6.30 1.10 7 11 0 8.40 0.80 7 11 0 8.30 1.30 -8 -11 0 27.10 1.90 8 11 0 30.00 1.90 8 11 0 30.50 1.70 -9 -11 0 33.70 1.90 9 11 0 32.20 1.70 9 11 0 30.50 1.90 -10 -11 0 -0.40 0.50 10 11 0 0.10 0.60 10 11 0 0.10 0.50 -11 -11 0 33.90 1.70 11 11 0 36.10 1.60 11 11 0 38.10 1.90 -12 -11 0 21.80 1.20 12 11 0 22.10 1.00 12 11 0 22.20 1.20 12 -12 0 1.80 0.30 11 -12 0 182.48 5.20 11 -12 0 176.58 6.00 10 -12 0 1.50 0.40 10 -12 0 2.00 0.40 9 -12 0 89.69 2.70 9 -12 0 86.79 3.20 8 -12 0 75.59 2.40 8 -12 0 74.29 2.80 7 -12 0 1.60 0.40 7 -12 0 1.30 0.40 6 -12 0 163.78 5.60 5 -12 0 184.58 6.30 5 -12 0 184.68 6.30 4 -12 0 31.90 1.40 -2 12 0 2.10 0.50 -1 12 0 223.48 7.30 0 12 0 359.56 11.50 1 12 0 0.50 0.40 2 12 0 384.66 12.30 -3 -12 0 451.15 21.40 3 12 0 451.85 14.40 -4 -12 0 -0.10 1.00 4 12 0 0.80 0.50 -5 -12 0 29.20 3.00 5 12 0 28.40 1.60 -6 -12 0 59.59 2.60 -6 -12 0 57.69 4.50 6 12 0 59.39 2.10 6 12 0 55.99 2.50 -7 -12 0 11.60 1.30 7 12 0 10.60 1.20 7 12 0 11.50 0.90 7 12 0 13.50 1.40 -8 -12 0 115.59 4.20 8 12 0 116.29 4.10 8 12 0 110.29 4.50 8 12 0 110.39 3.50 -9 -12 0 69.39 2.90 9 12 0 69.29 2.70 9 12 0 66.29 3.00 -10 -12 0 62.99 2.60 10 12 0 69.09 2.90 10 12 0 63.79 2.50 -11 -12 0 0.80 0.50 11 12 0 1.30 0.50 11 12 0 0.70 0.50 -12 -12 0 0.90 0.40 12 12 0 0.70 0.30 12 -13 0 16.00 0.70 11 -13 0 50.09 1.70 10 -13 0 2.40 0.40 10 -13 0 2.60 0.40 9 -13 0 5.90 0.60 9 -13 0 5.60 0.60 8 -13 0 124.69 4.20 8 -13 0 112.59 5.00 8 -13 0 117.69 3.50 7 -13 0 16.60 0.80 7 -13 0 15.70 1.00 6 -13 0 29.10 1.40 6 -13 0 30.20 1.20 5 -13 0 214.18 7.30 4 -13 0 67.19 2.60 -2 13 0 18.50 1.10 -1 13 0 22.40 1.20 0 13 0 365.46 11.70 1 13 0 8.50 0.90 2 13 0 58.39 2.40 3 13 0 0.60 0.50 4 13 0 36.60 1.80 -5 -13 0 55.29 2.40 5 13 0 53.29 2.00 5 13 0 53.69 2.40 -6 -13 0 39.10 2.00 6 13 0 37.60 2.00 6 13 0 39.20 1.60 -7 -13 0 4.00 0.80 7 13 0 3.10 0.70 7 13 0 3.00 0.50 7 13 0 6.80 1.00 7 13 0 3.80 0.80 -8 -13 0 1.90 0.70 8 13 0 1.10 0.60 8 13 0 0.80 0.60 8 13 0 0.80 0.40 -9 -13 0 14.30 1.20 9 13 0 14.70 1.20 9 13 0 16.20 1.30 -10 -13 0 24.30 1.40 10 13 0 24.20 1.40 10 13 0 20.90 1.20 -11 -13 0 2.50 0.50 11 13 0 1.80 0.40 11 13 0 4.20 0.70 11 -14 0 62.59 1.90 10 -14 0 28.80 1.20 10 -14 0 30.40 1.10 9 -14 0 2.70 0.40 9 -14 0 2.10 0.40 8 -14 0 36.40 1.60 8 -14 0 38.10 1.40 8 -14 0 36.40 2.20 7 -14 0 60.69 2.00 7 -14 0 56.39 2.30 6 -14 0 23.30 1.20 6 -14 0 23.40 1.00 5 -14 0 6.00 0.60 5 -14 0 7.20 0.70 4 -14 0 13.10 0.80 4 -14 0 15.60 1.00 -2 14 0 168.08 5.70 -1 14 0 124.59 4.40 0 14 0 10.90 1.00 1 14 0 18.10 1.20 2 14 0 16.10 1.20 3 14 0 50.29 2.30 3 14 0 55.99 2.00 -4 -14 0 162.08 5.50 4 14 0 169.58 5.10 4 14 0 161.08 5.80 -5 -14 0 40.10 2.00 5 14 0 40.50 2.00 5 14 0 40.70 1.70 -6 -14 0 82.89 3.20 6 14 0 80.49 2.80 6 14 0 86.89 3.30 -7 -14 0 14.00 1.30 7 14 0 12.40 1.30 7 14 0 13.10 0.90 7 14 0 12.30 1.10 7 14 0 11.50 1.20 -8 -14 0 65.19 2.70 8 14 0 70.79 2.30 8 14 0 71.29 2.70 8 14 0 69.59 3.00 -9 -14 0 14.70 1.10 9 14 0 16.40 1.30 9 14 0 14.90 1.10 -10 -14 0 78.29 2.80 10 14 0 81.19 2.80 10 14 0 76.29 3.10 -11 -14 0 1.60 0.40 11 14 0 1.00 0.30 11 -15 0 39.80 1.30 10 -15 0 4.30 0.50 9 -15 0 159.68 5.40 9 -15 0 163.88 4.70 8 -15 0 132.79 4.50 8 -15 0 126.79 3.90 8 -15 0 136.69 5.40 7 -15 0 39.10 1.40 7 -15 0 39.40 1.60 7 -15 0 34.20 2.20 6 -15 0 111.99 4.10 6 -15 0 117.49 3.50 5 -15 0 25.70 1.10 5 -15 0 25.60 1.30 4 -15 0 19.50 1.00 3 -15 0 561.94 15.60 2 -15 0 91.39 2.80 -2 15 0 84.99 3.30 1 -15 0 295.17 8.40 -1 15 0 295.67 9.70 0 -15 0 53.79 2.00 0 15 0 57.99 2.40 -1 -15 0 3.70 0.60 1 15 0 2.90 0.60 -2 -15 0 130.59 4.10 2 15 0 134.29 4.20 2 15 0 131.29 4.80 3 15 0 90.39 3.00 3 15 0 89.19 3.50 4 15 0 53.79 2.40 4 15 0 55.59 2.10 -5 -15 0 93.49 3.50 5 15 0 97.29 3.70 5 15 0 99.19 3.20 -6 -15 0 3.80 0.70 6 15 0 3.20 0.50 6 15 0 2.40 0.70 6 15 0 3.10 0.70 -7 -15 0 15.10 1.20 7 15 0 14.70 0.90 7 15 0 14.10 1.30 7 15 0 12.80 1.10 -8 -15 0 24.90 1.40 8 15 0 25.20 1.50 8 15 0 22.50 1.30 -9 -15 0 61.19 2.30 9 15 0 60.49 2.30 9 15 0 60.69 2.50 -10 -15 0 0.80 0.40 10 15 0 0.80 0.40 10 15 0 -0.10 0.40 10 -16 0 17.10 0.70 9 -16 0 4.70 0.50 8 -16 0 3.60 0.50 8 -16 0 3.40 0.50 8 -16 0 2.90 0.70 7 -16 0 127.79 4.30 7 -16 0 122.49 5.20 7 -16 0 123.39 3.70 6 -16 0 5.70 0.60 6 -16 0 5.10 0.60 5 -16 0 149.29 4.40 5 -16 0 146.19 5.20 4 -16 0 127.79 3.80 3 -16 0 11.60 0.80 2 -16 0 131.09 3.90 -2 16 0 119.49 4.40 1 -16 0 3.10 0.50 -1 16 0 2.60 0.60 0 -16 0 14.90 1.00 0 16 0 15.90 1.20 -1 -16 0 220.18 6.50 1 16 0 227.48 7.60 2 16 0 79.19 3.20 2 16 0 77.69 2.70 3 16 0 0.10 0.50 3 16 0 0.60 0.40 4 16 0 52.49 2.40 4 16 0 52.09 2.00 5 16 0 103.39 3.80 5 16 0 99.39 3.30 6 16 0 4.30 0.70 6 16 0 2.90 0.50 -7 -16 0 33.10 1.50 7 16 0 33.40 1.30 -8 -16 0 6.50 0.80 8 16 0 8.40 0.80 8 16 0 6.30 0.90 9 16 0 37.80 1.50 9 16 0 33.80 1.60 9 -17 0 21.30 0.80 8 -17 0 67.09 3.10 8 -17 0 72.39 2.20 7 -17 0 4.80 0.50 7 -17 0 5.80 1.10 7 -17 0 4.50 0.50 6 -17 0 0.40 0.30 6 -17 0 1.20 0.30 6 -17 0 0.40 0.60 5 -17 0 9.20 0.70 5 -17 0 9.10 0.80 4 -17 0 12.30 0.80 3 -17 0 0.00 0.40 2 -17 0 82.19 2.70 -2 17 0 81.19 3.10 1 -17 0 116.99 3.60 -1 17 0 115.29 4.20 0 -17 0 32.70 1.40 0 17 0 31.10 1.70 -1 -17 0 11.90 0.90 1 17 0 12.10 1.10 1 17 0 12.40 0.90 2 17 0 7.30 0.80 2 17 0 7.30 1.00 3 17 0 75.29 2.60 3 17 0 75.39 3.00 4 17 0 74.59 2.50 4 17 0 71.39 2.90 5 17 0 47.50 1.80 5 17 0 51.59 2.20 6 17 0 -0.50 0.30 7 17 0 43.10 1.50 8 17 0 5.70 0.70 8 -18 0 1.90 0.30 7 -18 0 68.59 2.10 7 -18 0 66.99 3.00 6 -18 0 55.29 1.80 6 -18 0 52.89 2.00 6 -18 0 56.19 2.70 5 -18 0 36.70 1.60 5 -18 0 42.10 2.30 5 -18 0 38.10 1.40 4 -18 0 119.89 3.60 3 -18 0 9.20 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27.40 1.00 7 16 -4 57.79 2.10 6 16 -4 1.60 0.50 5 16 -4 8.50 0.70 4 16 -4 0.30 0.50 4 16 -4 0.90 0.40 3 16 -4 27.80 1.30 3 16 -4 32.10 1.70 2 16 -4 55.69 2.50 2 16 -4 59.89 2.10 1 16 -4 1.90 0.60 1 16 -4 1.20 0.40 0 16 -4 73.49 3.00 0 16 -4 72.89 2.50 -1 16 -4 32.60 1.40 -1 16 -4 36.10 1.80 1 -16 4 30.00 1.50 -2 16 -4 121.69 3.90 -2 16 -4 128.49 4.50 2 -16 4 117.19 3.80 -3 16 -4 8.30 0.90 3 -16 4 7.50 0.80 -4 16 -4 0.40 0.40 4 -16 4 -0.20 0.40 -5 16 -4 0.60 0.50 5 -16 4 1.40 0.40 6 -16 4 53.99 1.90 7 -16 4 15.00 0.80 8 -16 4 26.80 1.10 8 -16 4 26.50 1.60 9 -16 4 49.00 1.60 8 15 -4 2.50 0.50 -8 -15 4 2.50 0.50 7 15 -4 42.80 1.80 -7 -15 4 47.30 1.90 6 15 -4 10.20 0.70 6 15 -4 8.90 1.00 -6 -15 4 10.30 1.00 5 15 -4 64.29 2.70 5 15 -4 67.69 2.30 -5 -15 4 67.89 2.60 4 15 -4 113.59 4.20 4 15 -4 113.29 3.60 -4 -15 4 111.19 3.90 3 15 -4 0.20 0.50 3 15 -4 0.10 0.40 2 15 -4 77.59 2.70 2 15 -4 77.29 3.10 1 15 -4 122.39 4.40 1 15 -4 112.69 3.80 0 15 -4 2.30 0.60 0 15 -4 2.00 0.50 -1 15 -4 118.99 3.80 -1 15 -4 115.99 4.30 1 -15 4 115.79 3.70 -2 15 -4 91.09 3.50 2 -15 4 88.89 2.90 -3 15 -4 287.67 9.50 3 -15 4 290.67 8.30 -4 15 -4 118.79 4.30 4 -15 4 116.49 3.70 -5 15 -4 0.90 0.50 5 -15 4 1.10 0.40 -6 15 -4 63.09 2.60 6 -15 4 68.99 2.20 7 -15 4 4.10 0.60 8 -15 4 108.09 4.40 8 -15 4 101.69 3.20 9 -15 4 172.88 5.00 10 -15 4 27.20 1.00 9 14 -4 15.30 0.90 -9 -14 4 14.40 0.90 8 14 -4 32.60 1.50 -8 -14 4 31.00 1.50 7 14 -4 19.60 1.20 -7 -14 4 18.00 1.30 6 14 -4 60.69 2.10 6 14 -4 63.09 2.50 -6 -14 4 62.69 2.50 5 14 -4 2.80 0.50 5 14 -4 4.80 0.80 -5 -14 4 4.30 0.70 4 14 -4 4.90 0.80 4 14 -4 5.20 0.70 -4 -14 4 4.20 0.70 3 14 -4 32.00 1.50 3 14 -4 31.00 1.70 -3 -14 4 31.00 1.70 2 14 -4 9.10 1.00 2 14 -4 7.90 0.80 1 14 -4 60.69 2.70 1 14 -4 63.39 2.30 0 14 -4 0.10 0.50 0 14 -4 0.50 0.40 -1 14 -4 50.49 1.90 -1 14 -4 48.10 2.20 1 -14 4 47.00 1.80 -2 14 -4 3.70 0.70 2 -14 4 2.00 0.50 -3 14 -4 103.39 3.90 3 -14 4 103.49 3.30 -4 14 -4 14.10 1.10 4 -14 4 12.70 0.90 -5 14 -4 2.10 0.60 5 -14 4 1.80 0.40 -6 14 -4 40.80 1.90 6 -14 4 41.50 1.60 7 -14 4 4.60 0.70 8 -14 4 16.90 0.90 9 -14 4 97.69 3.00 10 -14 4 6.00 0.60 11 -14 4 5.40 0.50 10 13 -4 25.60 1.10 -10 -13 4 25.70 1.20 9 13 -4 2.80 0.50 -9 -13 4 1.50 0.50 8 13 -4 7.60 0.90 -8 -13 4 9.40 1.10 7 13 -4 -0.10 0.50 -7 -13 4 1.50 0.60 6 13 -4 12.10 0.80 6 13 -4 14.20 1.20 -6 -13 4 10.20 1.30 5 13 -4 8.70 1.10 5 13 -4 7.60 1.10 5 13 -4 8.70 0.80 -5 -13 4 9.80 1.20 4 13 -4 11.30 1.10 4 13 -4 10.00 0.90 -4 -13 4 11.80 1.20 3 13 -4 89.59 3.00 3 13 -4 84.69 3.40 -3 -13 4 88.49 3.40 2 13 -4 29.30 1.70 2 13 -4 30.10 1.40 -2 -13 4 32.10 1.70 1 13 -4 137.59 5.10 1 13 -4 146.59 4.50 0 13 -4 7.70 1.00 0 13 -4 9.90 0.90 -1 13 -4 8.90 1.00 -2 13 -4 62.79 2.60 -3 13 -4 117.99 4.40 3 -13 4 122.39 3.70 -4 13 -4 42.30 2.00 4 -13 4 43.20 1.60 -5 13 -4 13.70 1.10 5 -13 4 11.90 0.90 -6 13 -4 51.99 2.30 6 -13 4 54.89 1.90 -7 13 -4 9.50 0.90 7 -13 4 10.50 0.80 8 -13 4 57.59 2.00 9 -13 4 3.60 0.50 10 -13 4 38.00 1.40 11 -13 4 0.40 0.30 10 12 -4 21.40 1.10 -10 -12 4 22.00 1.20 9 12 -4 8.30 0.90 -9 -12 4 8.90 1.10 8 12 -4 126.39 4.40 -8 -12 4 127.49 4.50 7 12 -4 187.78 6.30 -7 -12 4 188.38 6.40 6 12 -4 3.80 0.70 6 12 -4 2.80 0.50 -6 -12 4 2.90 0.70 5 12 -4 80.89 3.10 5 12 -4 76.79 3.10 5 12 -4 74.19 2.60 -5 -12 4 78.69 3.20 4 12 -4 16.60 1.00 4 12 -4 17.70 1.30 -4 -12 4 19.70 1.50 3 12 -4 66.49 2.90 3 12 -4 71.79 2.50 2 12 -4 288.47 9.50 1 12 -4 37.20 1.90 0 12 -4 478.15 15.30 -1 12 -4 11.10 1.00 -2 12 -4 72.89 2.90 -3 12 -4 70.89 2.80 -4 12 -4 17.90 1.20 -5 12 -4 190.08 6.30 5 -12 4 181.58 5.40 -6 12 -4 240.08 8.10 6 -12 4 249.48 7.10 -7 12 -4 11.40 1.00 7 -12 4 10.30 0.80 -8 12 -4 12.20 1.00 8 -12 4 13.60 0.90 9 -12 4 65.49 2.20 10 -12 4 5.00 0.60 11 -12 4 21.30 1.00 12 -12 4 20.40 0.80 11 11 -4 11.60 0.70 -11 -11 4 11.30 0.90 10 11 -4 38.30 1.80 10 11 -4 37.60 1.60 -10 -11 4 38.20 1.80 9 11 -4 3.80 0.60 9 11 -4 5.00 0.90 -9 -11 4 3.30 0.70 8 11 -4 43.60 2.00 8 11 -4 42.20 2.20 -8 -11 4 46.40 2.20 7 11 -4 0.10 0.50 -7 -11 4 0.80 0.70 6 11 -4 60.29 2.50 6 11 -4 58.59 2.10 -6 -11 4 61.59 2.70 5 11 -4 20.50 1.10 5 11 -4 17.50 2.10 5 11 -4 18.40 1.40 5 11 -4 20.50 1.40 -5 -11 4 19.30 1.60 4 11 -4 59.09 2.50 3 11 -4 85.09 3.30 2 11 -4 262.57 8.70 1 11 -4 112.29 4.10 0 11 -4 2.30 0.50 -1 11 -4 42.80 1.90 -2 11 -4 175.08 5.90 -3 11 -4 781.92 24.40 -4 11 -4 0.90 0.50 -5 11 -4 53.99 2.30 -6 11 -4 257.27 8.70 6 -11 4 271.37 7.60 -7 11 -4 84.99 3.30 7 -11 4 90.79 2.80 -8 11 -4 56.09 2.40 8 -11 4 54.89 2.00 -9 11 -4 3.30 0.60 9 -11 4 3.30 0.50 10 -11 4 253.77 7.30 11 -11 4 50.39 1.80 11 10 -4 13.80 0.80 11 10 -4 11.90 0.90 -11 -10 4 13.90 1.00 10 10 -4 8.50 0.80 10 10 -4 6.60 1.00 -10 -10 4 6.20 1.00 9 10 -4 49.99 2.40 9 10 -4 48.50 2.10 -9 -10 4 48.40 2.30 8 10 -4 35.50 1.70 8 10 -4 31.20 1.90 -8 -10 4 32.70 1.90 7 10 -4 84.09 3.70 7 10 -4 92.19 3.40 -7 -10 4 92.29 3.60 6 10 -4 189.88 5.60 6 10 -4 182.58 6.30 -6 -10 4 193.08 6.50 5 10 -4 16.70 1.20 5 10 -4 14.70 1.80 4 10 -4 45.30 2.10 3 10 -4 12.00 1.00 2 10 -4 136.79 4.80 1 10 -4 154.18 5.30 0 10 -4 17.50 1.10 -1 10 -4 238.88 7.80 -2 10 -4 526.45 16.60 -3 10 -4 108.09 3.80 -4 10 -4 0.60 0.40 -5 10 -4 90.39 3.80 -5 10 -4 92.29 3.40 -6 10 -4 5.00 0.90 -6 10 -4 6.60 0.80 -7 10 -4 43.60 2.50 -7 10 -4 49.10 2.10 7 -10 4 47.60 1.70 -8 10 -4 1.10 0.80 -8 10 -4 1.10 0.50 8 -10 4 0.10 0.40 -9 10 -4 3.10 0.60 9 -10 4 5.00 0.70 -10 10 -4 2.70 0.60 10 -10 4 2.80 0.50 11 -10 4 45.60 1.70 12 -10 4 71.59 2.30 -12 -9 4 10.70 0.80 11 9 -4 0.90 0.50 11 9 -4 0.80 0.40 -11 -9 4 0.50 0.50 10 9 -4 58.89 2.30 10 9 -4 61.99 2.70 -10 -9 4 57.29 2.50 9 9 -4 34.40 2.00 9 9 -4 35.60 1.70 -9 -9 4 38.70 2.00 8 9 -4 184.18 6.20 8 9 -4 179.88 6.90 -8 -9 4 193.88 6.40 7 9 -4 3.60 0.80 7 9 -4 4.00 0.70 -7 -9 4 4.90 0.90 6 9 -4 5.00 1.10 5 9 -4 4.00 1.10 4 9 -4 350.46 11.10 4 9 -4 335.37 13.70 3 9 -4 352.96 11.40 2 9 -4 2.00 0.50 1 9 -4 413.96 13.20 0 9 -4 181.28 6.00 -1 9 -4 376.56 12.00 -2 9 -4 46.80 2.00 -2 9 -4 42.40 1.80 -3 9 -4 2.30 0.50 -3 9 -4 1.20 0.50 -4 9 -4 7.00 0.70 -4 9 -4 6.00 0.90 -5 9 -4 171.38 6.30 -5 9 -4 168.58 5.70 -6 9 -4 37.20 1.70 -6 9 -4 33.70 2.00 -7 9 -4 19.20 1.60 -7 9 -4 22.40 1.30 -8 9 -4 1.90 0.60 -8 9 -4 1.40 0.80 8 -9 4 1.70 0.50 -9 9 -4 23.90 1.40 -9 9 -4 23.80 1.90 9 -9 4 27.10 1.20 -10 9 -4 81.49 3.20 10 -9 4 86.69 2.70 -11 9 -4 4.50 0.80 11 -9 4 2.50 0.50 12 -9 4 15.40 0.90 13 -9 4 0.60 0.30 12 8 -4 4.30 0.70 -12 -8 4 5.80 0.80 11 8 -4 39.70 1.90 11 8 -4 37.60 1.60 -11 -8 4 37.10 1.80 10 8 -4 42.20 1.80 10 8 -4 40.40 2.20 -10 -8 4 44.60 1.70 -10 -8 4 41.10 2.10 9 8 -4 54.39 2.60 9 8 -4 51.69 2.20 -9 -8 4 54.09 2.10 -9 -8 4 52.89 2.50 8 8 -4 226.58 8.30 8 8 -4 232.48 7.50 -8 -8 4 221.38 7.60 -8 -8 4 225.48 6.80 7 8 -4 15.20 1.20 7 8 -4 12.40 1.30 7 8 -4 13.00 1.40 -7 -8 4 15.10 1.50 -7 -8 4 13.40 1.20 6 8 -4 23.90 2.00 5 8 -4 9.40 1.40 4 8 -4 0.40 0.80 4 8 -4 1.00 0.40 3 8 -4 149.09 5.10 2 8 -4 219.88 7.20 1 8 -4 51.29 2.10 0 8 -4 896.41 26.80 0 8 -4 834.12 28.70 -1 8 -4 11.40 0.90 -1 8 -4 13.30 0.90 -2 8 -4 0.30 0.40 -2 8 -4 1.20 0.40 -3 8 -4 14.30 0.90 -3 8 -4 12.60 1.00 -4 8 -4 371.26 12.10 -4 8 -4 382.66 13.10 4 -8 4 394.96 19.10 -5 8 -4 644.24 21.70 -5 8 -4 612.94 20.10 5 -8 4 681.93 31.00 -6 8 -4 34.70 1.60 -6 8 -4 34.40 1.90 -7 8 -4 155.08 5.20 -7 8 -4 143.89 5.70 -8 8 -4 38.70 1.90 -8 8 -4 37.20 2.30 -9 8 -4 71.89 2.90 -9 8 -4 72.59 3.40 9 -8 4 69.09 2.40 -10 8 -4 96.09 3.70 10 -8 4 102.59 3.20 -11 8 -4 62.49 2.50 11 -8 4 57.89 2.10 12 -8 4 92.19 2.90 -13 8 -4 56.19 1.90 13 -8 4 55.19 1.80 12 7 -4 55.59 2.30 -12 -7 4 51.99 2.10 11 7 -4 7.60 0.80 11 7 -4 6.70 1.00 -11 -7 4 9.60 1.10 -11 -7 4 7.90 0.90 10 7 -4 59.69 2.30 10 7 -4 60.39 2.80 -10 -7 4 56.19 2.20 -10 -7 4 62.89 2.70 9 7 -4 10.40 1.00 9 7 -4 9.00 1.20 -9 -7 4 8.20 1.10 -9 -7 4 9.20 1.40 8 7 -4 -0.20 0.60 8 7 -4 0.40 0.50 -8 -7 4 0.00 0.60 -8 -7 4 0.80 0.80 -8 -7 4 -0.30 0.70 7 7 -4 450.05 17.10 -7 -7 4 434.46 14.40 6 7 -4 79.49 3.80 -6 -7 4 74.19 3.20 5 7 -4 101.19 4.70 4 7 -4 11.00 1.40 4 7 -4 11.90 1.00 4 7 -4 11.00 0.90 4 7 -4 10.00 1.70 3 7 -4 3.00 1.10 3 7 -4 2.00 0.50 3 7 -4 3.40 0.90 3 7 -4 5.20 0.70 2 7 -4 25.30 1.40 1 7 -4 288.47 9.90 0 7 -4 0.90 0.40 -1 7 -4 7.10 0.80 -2 7 -4 129.99 4.70 -3 7 -4 53.89 2.30 3 -7 4 49.30 3.90 -4 7 -4 5.50 0.60 -4 7 -4 6.90 0.90 4 -7 4 5.60 1.50 -5 7 -4 634.54 20.00 -5 7 -4 631.44 21.50 5 -7 4 658.73 30.60 -6 7 -4 61.69 2.80 -6 7 -4 64.69 2.40 -7 7 -4 4.40 0.80 -7 7 -4 4.60 0.70 7 -7 4 5.10 0.90 -8 7 -4 11.60 1.40 -8 7 -4 10.30 1.00 8 -7 4 9.40 1.30 -9 7 -4 119.99 4.90 -9 7 -4 122.79 4.40 9 -7 4 112.89 5.10 9 -7 4 121.39 3.70 -10 7 -4 28.30 2.00 -10 7 -4 26.30 1.60 10 -7 4 28.80 1.30 10 -7 4 26.80 2.00 -11 7 -4 32.90 1.70 11 -7 4 30.20 1.40 -12 7 -4 5.80 0.80 12 -7 4 6.40 0.80 -13 7 -4 12.00 0.80 13 -7 4 13.40 0.80 13 6 -4 0.90 0.40 12 6 -4 51.79 2.30 -12 -6 4 49.99 1.80 11 6 -4 156.48 5.10 11 6 -4 151.08 5.80 -11 -6 4 158.98 4.80 10 6 -4 23.90 1.70 10 6 -4 21.50 1.30 -10 -6 4 21.30 1.70 -10 -6 4 22.10 1.40 9 6 -4 17.10 1.20 9 6 -4 18.00 1.50 -9 -6 4 15.70 1.30 -9 -6 4 15.90 1.60 8 6 -4 7.90 1.10 8 6 -4 9.60 1.20 -8 -6 4 8.20 1.40 -8 -6 4 10.30 1.20 7 6 -4 155.78 6.50 -7 -6 4 164.28 5.80 6 6 -4 14.60 1.40 -6 -6 4 15.70 1.30 5 6 -4 60.19 2.60 5 6 -4 56.69 3.00 5 6 -4 51.49 3.60 -5 -6 4 59.89 2.50 4 6 -4 61.59 3.60 4 6 -4 52.79 2.40 4 6 -4 56.99 2.90 3 6 -4 1.10 0.80 3 6 -4 1.90 0.70 3 6 -4 2.10 0.50 2 6 -4 281.57 11.00 2 6 -4 285.97 12.00 2 6 -4 272.27 9.60 1 6 -4 25.00 1.30 0 6 -4 129.99 4.80 0 6 -4 138.59 7.40 -1 6 -4 86.39 5.10 -1 6 -4 79.09 3.10 -2 6 -4 12.40 0.90 -2 6 -4 11.80 1.80 2 -6 4 12.30 1.80 -3 6 -4 86.19 3.30 3 -6 4 86.59 5.30 -4 6 -4 241.48 8.60 4 -6 4 255.27 12.70 -5 6 -4 31.10 1.40 -5 6 -4 33.00 1.70 5 -6 4 32.20 3.40 -6 6 -4 197.08 7.20 -6 6 -4 196.58 6.60 6 -6 4 212.78 11.50 6 -6 4 203.28 7.50 -7 6 -4 527.95 16.20 -7 6 -4 501.75 17.50 7 -6 4 506.15 18.20 -8 6 -4 30.20 1.60 -8 6 -4 30.10 1.90 8 -6 4 31.50 2.00 -9 6 -4 32.90 2.10 -9 6 -4 30.90 1.70 9 -6 4 29.10 2.10 -10 6 -4 3.50 0.70 -10 6 -4 3.80 1.00 10 -6 4 3.20 0.50 10 -6 4 3.20 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3 14 4 15.80 1.20 -4 -14 -4 1.00 1.20 4 14 4 -0.70 0.50 -5 -14 -4 396.26 19.90 5 14 4 402.86 13.10 5 14 4 415.06 11.70 -6 -14 -4 61.49 2.50 6 14 4 57.09 2.60 6 14 4 61.49 2.20 -7 -14 -4 3.70 0.70 7 14 4 3.70 0.80 7 14 4 3.90 0.60 -8 -14 -4 31.30 1.70 8 14 4 30.90 1.40 8 14 4 32.30 1.80 -9 -14 -4 52.99 2.30 9 14 4 54.59 2.30 9 14 4 50.49 2.50 9 14 4 53.19 1.90 -10 -14 -4 80.89 2.90 10 14 4 75.39 2.90 10 14 4 78.09 3.20 -11 -14 -4 46.30 1.80 11 14 4 46.10 1.80 11 14 4 44.30 2.00 10 -15 -4 27.60 1.00 9 -15 -4 105.49 3.10 8 -15 -4 73.99 2.30 8 -15 -4 77.39 3.50 7 -15 -4 0.30 0.20 7 -15 -4 0.00 0.20 7 -15 -4 0.90 0.30 7 -15 -4 0.30 0.60 6 -15 -4 9.20 1.40 6 -15 -4 11.10 0.60 6 -15 -4 10.50 0.60 6 -15 -4 10.40 0.70 5 -15 -4 101.79 3.60 5 -15 -4 109.29 4.70 5 -15 -4 103.69 3.60 4 -15 -4 8.60 0.60 4 -15 -4 8.70 1.40 3 -15 -4 366.06 12.20 3 -15 -4 377.96 13.70 2 -15 -4 15.70 0.90 1 -15 -4 20.70 1.10 1 -15 -4 17.60 2.60 0 -15 -4 5.30 1.60 0 15 4 5.10 0.70 -1 -15 -4 16.60 2.50 1 15 4 17.50 1.20 -2 -15 -4 15.20 2.40 2 15 4 13.50 1.10 -3 -15 -4 24.00 2.90 3 15 4 28.40 1.60 4 15 4 76.19 2.60 4 15 4 71.79 3.00 5 15 4 2.90 0.70 5 15 4 3.60 0.60 6 15 4 40.70 1.70 6 15 4 42.00 2.10 -7 -15 -4 62.39 2.60 7 15 4 67.29 2.80 7 15 4 65.59 2.30 -8 -15 -4 130.09 4.30 8 15 4 120.69 4.40 8 15 4 116.59 3.80 8 15 4 119.69 4.80 -9 -15 -4 0.30 0.50 9 15 4 0.00 0.60 9 15 4 0.20 0.50 9 15 4 -0.20 0.30 -10 -15 -4 1.10 0.50 10 15 4 1.60 0.60 10 15 4 0.20 0.40 -11 -15 -4 63.69 2.20 11 15 4 66.39 2.30 11 15 4 62.49 2.50 10 -16 -4 50.29 1.50 9 -16 -4 8.40 0.50 8 -16 -4 38.90 2.10 8 -16 -4 37.60 1.30 7 -16 -4 17.70 1.60 7 -16 -4 17.00 0.80 6 -16 -4 113.49 5.20 6 -16 -4 128.59 4.20 6 -16 -4 121.89 3.60 6 -16 -4 125.49 4.10 5 -16 -4 15.40 0.80 5 -16 -4 16.30 0.90 5 -16 -4 15.00 1.60 5 -16 -4 16.50 0.80 4 -16 -4 56.19 2.90 4 -16 -4 56.09 1.80 4 -16 -4 57.89 3.00 4 -16 -4 54.49 2.10 3 -16 -4 65.79 2.10 3 -16 -4 65.79 3.20 3 -16 -4 65.79 2.50 2 -16 -4 1.60 0.40 2 -16 -4 1.80 0.40 2 -16 -4 3.10 0.90 1 -16 -4 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0.90 6 -19 -4 72.59 2.10 6 -19 -4 68.89 3.20 5 -19 -4 -0.20 0.20 5 -19 -4 0.60 0.60 4 -19 -4 15.10 0.80 4 -19 -4 15.10 1.50 4 -19 -4 14.20 0.80 4 -19 -4 14.40 0.70 3 -19 -4 0.20 0.30 3 -19 -4 0.30 0.30 3 -19 -4 0.50 0.60 2 -19 -4 20.60 1.10 2 -19 -4 24.10 1.00 2 -19 -4 20.20 1.70 1 -19 -4 72.59 2.30 1 -19 -4 67.79 3.30 0 -19 -4 2.30 0.40 -1 -19 -4 0.60 0.40 1 19 4 0.50 0.40 -2 -19 -4 265.07 7.70 2 19 4 266.37 8.70 -3 -19 -4 18.30 1.00 3 19 4 19.50 1.00 3 19 4 19.00 1.30 4 19 4 17.10 1.20 4 19 4 17.40 1.00 5 19 4 1.70 0.40 6 19 4 28.90 1.20 6 19 4 27.10 1.50 7 19 4 7.10 0.60 7 19 4 7.20 0.80 6 -20 -4 4.20 0.40 6 -20 -4 4.50 0.90 5 -20 -4 13.80 1.30 5 -20 -4 14.20 0.70 4 -20 -4 5.10 0.50 4 -20 -4 6.20 1.10 3 -20 -4 111.69 3.90 3 -20 -4 115.19 4.70 3 -20 -4 112.09 3.40 2 -20 -4 10.60 0.70 2 -20 -4 7.50 1.20 2 -20 -4 10.60 0.70 1 -20 -4 9.00 0.70 0 -20 -4 5.10 0.60 -1 -20 -4 60.49 2.10 -2 -20 -4 14.60 0.80 2 20 4 14.10 0.90 3 20 4 100.09 3.20 4 20 4 16.30 0.90 5 20 4 8.30 0.70 6 20 4 5.70 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0.30 0.40 3 -17 5 1.10 0.40 -4 17 -5 34.30 1.40 4 -17 5 30.80 1.30 5 -17 5 101.79 3.10 6 -17 5 1.10 0.30 7 -17 5 126.19 5.00 7 -17 5 129.29 3.80 8 -17 5 10.50 0.60 7 16 -5 12.70 0.80 6 16 -5 12.00 0.90 5 16 -5 6.80 0.60 4 16 -5 3.80 0.60 3 16 -5 65.19 2.70 3 16 -5 67.29 2.30 2 16 -5 10.20 1.00 2 16 -5 8.00 0.80 1 16 -5 16.70 1.00 1 16 -5 16.50 1.20 0 16 -5 92.29 3.50 0 16 -5 88.49 3.00 -1 16 -5 2.10 0.50 -1 16 -5 2.10 0.60 -2 16 -5 2.10 0.50 -2 16 -5 1.30 0.50 -3 16 -5 107.79 3.50 -3 16 -5 110.39 4.00 3 -16 5 107.99 3.40 -4 16 -5 19.90 1.30 4 -16 5 19.70 1.10 5 -16 5 277.57 7.90 6 -16 5 1.60 0.40 7 -16 5 15.00 0.80 8 -16 5 1.50 0.30 8 -16 5 0.10 0.50 9 -16 5 25.90 1.00 8 15 -5 7.70 0.60 -8 -15 5 5.40 0.60 7 15 -5 50.79 2.00 -7 -15 5 51.19 2.00 6 15 -5 23.90 1.30 -6 -15 5 26.30 1.40 5 15 -5 24.10 1.10 5 15 -5 21.80 1.30 -5 -15 5 24.40 1.30 4 15 -5 19.00 1.00 4 15 -5 19.10 1.30 -4 -15 5 18.70 1.20 3 15 -5 0.20 0.40 3 15 -5 0.50 0.50 2 15 -5 12.60 0.90 2 15 -5 8.40 1.00 1 15 -5 117.89 3.90 1 15 -5 125.09 4.50 0 15 -5 14.70 1.20 0 15 -5 13.10 1.00 -1 15 -5 10.40 1.10 -1 15 -5 10.40 0.90 -2 15 -5 116.29 4.20 -2 15 -5 113.39 3.70 2 -15 5 112.49 3.60 -3 15 -5 2.60 0.70 -3 15 -5 2.60 0.50 3 -15 5 0.90 0.40 -4 15 -5 3.10 0.60 4 -15 5 2.30 0.50 -5 15 -5 78.19 3.00 5 -15 5 70.59 2.50 -6 15 -5 30.80 1.50 6 -15 5 29.10 1.30 7 -15 5 15.60 0.90 8 -15 5 2.70 0.40 8 -15 5 2.90 0.70 9 -15 5 1.10 0.30 10 -15 5 54.79 1.80 9 14 -5 1.00 0.30 -9 -14 5 0.80 0.40 8 14 -5 0.30 0.40 -8 -14 5 0.80 0.50 7 14 -5 1.00 0.50 -7 -14 5 1.40 0.60 6 14 -5 1.30 0.50 -6 -14 5 1.50 0.60 5 14 -5 99.99 3.60 5 14 -5 94.79 3.10 -5 -14 5 98.59 3.60 4 14 -5 96.99 3.70 4 14 -5 94.69 3.10 -4 -14 5 92.39 3.50 3 14 -5 68.09 2.80 3 14 -5 63.49 2.30 -3 -14 5 62.69 2.60 2 14 -5 11.40 0.90 2 14 -5 10.00 1.10 1 14 -5 18.60 1.40 1 14 -5 17.90 1.10 0 14 -5 0.80 0.50 0 14 -5 1.20 0.60 -1 14 -5 167.58 5.90 -1 14 -5 169.18 5.20 -2 14 -5 42.00 2.10 -2 14 -5 44.80 1.80 2 -14 5 44.90 1.80 -3 14 -5 284.17 9.40 3 -14 5 283.37 8.20 -4 14 -5 288.97 9.60 4 -14 5 291.67 8.40 -5 14 -5 40.20 1.90 5 -14 5 35.70 1.50 -6 14 -5 162.28 5.60 6 -14 5 163.58 4.90 -7 14 -5 0.90 0.50 7 -14 5 0.30 0.40 8 -14 5 18.20 1.00 9 -14 5 65.99 2.20 10 -14 5 25.50 1.00 9 13 -5 2.30 0.40 -9 -13 5 1.70 0.50 8 13 -5 4.80 0.80 -8 -13 5 6.80 1.00 7 13 -5 1.70 0.50 -7 -13 5 1.10 0.60 6 13 -5 1.20 0.50 -6 -13 5 0.50 0.60 5 13 -5 2.00 0.60 5 13 -5 1.60 0.40 -5 -13 5 1.60 0.70 4 13 -5 16.10 1.00 4 13 -5 15.80 1.20 -4 -13 5 16.40 1.30 3 13 -5 0.30 0.40 3 13 -5 1.60 0.60 -3 -13 5 0.50 0.60 2 13 -5 1.70 0.60 2 13 -5 3.00 0.50 -2 -13 5 1.50 0.60 1 13 -5 216.98 7.60 1 13 -5 233.98 6.80 0 13 -5 26.50 1.60 0 13 -5 25.40 1.30 -1 13 -5 100.09 3.90 -1 13 -5 104.59 3.40 -2 13 -5 184.88 5.60 -2 13 -5 175.68 6.30 2 -13 5 186.38 5.50 -3 13 -5 28.00 1.60 3 -13 5 29.60 1.30 -4 13 -5 2.50 0.60 4 -13 5 2.80 0.50 -5 13 -5 37.00 1.90 5 -13 5 41.70 1.60 -6 13 -5 10.60 1.10 6 -13 5 12.30 0.90 -7 13 -5 215.08 7.10 7 -13 5 205.38 6.10 -8 13 -5 24.10 1.40 8 -13 5 23.90 1.10 9 -13 5 45.50 1.60 10 -13 5 102.19 3.10 11 -13 5 1.50 0.30 10 12 -5 16.10 0.90 -10 -12 5 14.90 1.00 9 12 -5 42.50 1.80 -9 -12 5 42.60 1.90 8 12 -5 13.00 1.00 -8 -12 5 11.10 1.20 7 12 -5 1.60 0.60 -7 -12 5 1.60 0.60 6 12 -5 7.00 0.70 6 12 -5 8.30 1.00 -6 -12 5 6.40 1.20 5 12 -5 3.50 0.50 5 12 -5 6.00 1.00 -5 -12 5 5.20 0.90 4 12 -5 113.69 4.20 4 12 -5 110.99 3.60 -4 -12 5 111.69 4.10 3 12 -5 108.99 4.10 3 12 -5 109.59 3.50 -3 -12 5 107.99 4.00 2 12 -5 10.50 0.90 2 12 -5 7.30 1.00 1 12 -5 518.75 16.60 0 12 -5 12.50 1.10 -1 12 -5 36.50 1.80 -2 12 -5 231.78 7.80 -3 12 -5 46.00 2.10 -4 12 -5 154.18 5.40 -5 12 -5 1.80 0.60 5 -12 5 0.30 0.40 -6 12 -5 13.30 1.10 6 -12 5 13.40 0.90 -7 12 -5 67.89 2.70 7 -12 5 66.79 2.30 -8 12 -5 12.50 1.10 8 -12 5 13.00 0.90 -9 12 -5 1.00 0.50 9 -12 5 0.20 0.40 10 -12 5 0.80 0.40 11 -12 5 17.90 0.90 10 11 -5 2.00 0.40 -10 -11 5 2.30 0.60 9 11 -5 45.10 1.90 -9 -11 5 44.50 2.10 8 11 -5 0.70 0.50 -8 -11 5 0.50 0.60 7 11 -5 190.28 6.40 -7 -11 5 195.98 6.60 6 11 -5 52.29 2.40 -6 -11 5 57.89 2.60 5 11 -5 8.70 0.80 5 11 -5 8.30 1.10 -5 -11 5 10.70 1.30 4 11 -5 38.80 1.90 4 11 -5 37.00 1.60 -4 -11 5 39.80 2.10 3 11 -5 8.60 1.00 2 11 -5 769.92 24.20 1 11 -5 0.40 0.50 0 11 -5 474.55 15.10 -1 11 -5 94.09 3.50 -2 11 -5 59.19 2.50 -3 11 -5 58.79 2.50 -4 11 -5 14.00 1.10 -5 11 -5 500.75 15.90 -6 11 -5 446.86 14.50 6 -11 5 459.15 12.70 -7 11 -5 8.30 1.00 7 -11 5 8.00 0.80 -8 11 -5 2.70 0.60 8 -11 5 1.60 0.50 -9 11 -5 3.40 0.70 9 -11 5 2.20 0.50 10 -11 5 29.60 1.30 11 -11 5 90.09 2.80 12 -11 5 8.80 0.60 11 10 -5 12.50 0.70 11 10 -5 11.30 0.90 -11 -10 5 13.60 0.90 10 10 -5 6.20 0.90 10 10 -5 3.60 0.50 -10 -10 5 2.90 0.60 9 10 -5 116.69 4.30 9 10 -5 105.59 3.80 -9 -10 5 108.69 4.00 8 10 -5 29.80 1.50 -8 -10 5 24.70 1.70 7 10 -5 9.90 1.10 -7 -10 5 10.10 1.30 6 10 -5 113.49 4.10 -6 -10 5 116.59 4.30 5 10 -5 205.48 6.10 5 10 -5 187.68 8.70 -5 -10 5 218.88 7.00 4 10 -5 545.25 16.90 4 10 -5 515.45 20.70 3 10 -5 147.49 5.20 2 10 -5 108.39 4.00 1 10 -5 39.20 1.80 0 10 -5 0.40 0.40 -1 10 -5 64.99 2.60 -2 10 -5 0.70 0.40 -3 10 -5 79.09 3.00 -4 10 -5 86.79 3.60 -4 10 -5 87.19 3.30 -5 10 -5 27.70 1.50 -5 10 -5 26.10 1.70 -6 10 -5 114.39 4.10 -6 10 -5 111.99 4.60 -7 10 -5 86.69 3.80 -7 10 -5 87.59 3.40 7 -10 5 87.39 2.80 -8 10 -5 87.49 3.90 -8 10 -5 87.59 3.40 8 -10 5 88.59 2.80 -9 10 -5 1.20 0.60 9 -10 5 0.70 0.40 -10 10 -5 84.89 3.20 10 -10 5 81.09 2.70 11 -10 5 125.29 3.80 12 -10 5 15.10 0.80 11 9 -5 16.70 0.90 11 9 -5 17.20 1.10 -11 -9 5 15.50 1.10 10 9 -5 17.60 1.30 10 9 -5 16.30 1.00 -10 -9 5 15.20 1.30 9 9 -5 62.19 2.80 9 9 -5 59.39 2.40 -9 -9 5 61.89 2.70 8 9 -5 8.00 1.10 8 9 -5 6.60 1.00 -8 -9 5 5.20 0.90 7 9 -5 7.20 1.00 -7 -9 5 6.10 0.90 6 9 -5 58.59 2.50 -6 -9 5 58.59 2.60 5 9 -5 143.49 6.40 4 9 -5 11.80 1.00 4 9 -5 9.40 1.50 3 9 -5 35.20 1.70 2 9 -5 114.29 4.10 1 9 -5 430.46 13.70 0 9 -5 23.60 1.30 -1 9 -5 286.87 9.90 -1 9 -5 285.57 9.30 -2 9 -5 28.00 1.40 -2 9 -5 27.20 1.50 -3 9 -5 4.30 0.70 -3 9 -5 4.10 0.70 -4 9 -5 12.70 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1.80 -2 8 -5 36.50 1.60 -3 8 -5 366.96 11.90 -3 8 -5 381.66 12.80 -4 8 -5 7.70 0.80 -4 8 -5 5.40 0.90 -5 8 -5 64.09 2.50 -5 8 -5 63.59 2.80 -6 8 -5 187.88 7.00 -6 8 -5 190.18 6.40 -7 8 -5 34.70 2.10 -7 8 -5 38.20 1.80 -8 8 -5 236.68 8.50 -8 8 -5 221.78 7.60 8 -8 5 226.28 6.70 -9 8 -5 37.50 2.30 -9 8 -5 35.80 1.80 9 -8 5 38.40 1.50 -10 8 -5 31.90 1.70 10 -8 5 32.20 1.40 -11 8 -5 25.60 1.40 11 -8 5 21.10 1.10 -12 8 -5 31.30 1.30 12 -8 5 33.20 1.30 -13 8 -5 6.00 0.60 12 7 -5 -0.40 0.40 -12 -7 5 0.40 0.40 11 7 -5 -0.30 0.50 11 7 -5 0.90 0.40 -11 -7 5 1.30 0.40 -11 -7 5 1.20 0.60 10 7 -5 42.90 2.10 10 7 -5 41.10 1.70 -10 -7 5 38.50 2.10 -10 -7 5 38.50 1.70 9 7 -5 29.80 1.90 9 7 -5 34.90 1.70 -9 -7 5 35.10 1.60 -9 -7 5 32.70 1.90 8 7 -5 117.59 4.00 8 7 -5 106.19 4.50 -8 -7 5 105.99 4.20 -8 -7 5 112.09 4.40 -8 -7 5 115.99 3.70 7 7 -5 52.69 2.60 7 7 -5 54.59 2.70 -7 -7 5 61.09 2.20 -7 -7 5 52.79 2.70 6 7 -5 11.40 1.40 -6 -7 5 16.20 1.50 5 7 -5 130.79 5.20 5 7 -5 140.49 6.00 4 7 -5 411.26 17.00 4 7 -5 451.75 14.90 4 7 -5 447.66 13.90 3 7 -5 61.89 3.20 3 7 -5 64.39 2.70 3 7 -5 62.69 2.50 2 7 -5 106.39 3.70 2 7 -5 104.59 4.00 1 7 -5 180.88 6.40 0 7 -5 1232.78 40.70 -1 7 -5 70.19 2.80 -2 7 -5 139.19 5.10 -3 7 -5 28.30 1.50 -3 7 -5 25.40 1.30 -4 7 -5 132.19 4.50 -4 7 -5 128.89 4.90 4 -7 5 138.69 7.90 -5 7 -5 1781.12 54.39 -5 7 -5 1742.83 58.29 5 -7 5 1783.12 79.59 -6 7 -5 40.50 1.80 -6 7 -5 38.10 2.10 -7 7 -5 74.09 3.40 -7 7 -5 77.39 2.90 -8 7 -5 253.67 9.50 -8 7 -5 268.67 8.70 -9 7 -5 115.09 4.70 -9 7 -5 105.49 4.00 9 -7 5 107.29 3.40 -10 7 -5 73.39 3.00 10 -7 5 73.69 2.50 -11 7 -5 56.99 2.50 11 -7 5 56.79 2.00 -12 7 -5 169.38 5.10 12 -7 5 168.18 5.00 -13 7 -5 35.20 1.40 12 6 -5 58.99 2.50 -12 -6 5 56.09 1.90 11 6 -5 7.20 1.00 -11 -6 5 5.30 0.90 10 6 -5 7.90 0.90 10 6 -5 7.10 1.10 -10 -6 5 8.80 1.30 -10 -6 5 7.20 1.00 9 6 -5 61.19 2.40 9 6 -5 58.79 2.80 -9 -6 5 59.19 2.30 -9 -6 5 59.39 2.90 8 6 -5 26.70 1.70 8 6 -5 24.60 1.50 -8 -6 5 25.30 1.70 -8 -6 5 26.90 1.90 -8 -6 5 25.10 1.50 7 6 -5 63.49 2.90 -7 -6 5 64.79 3.00 6 6 -5 49.40 2.60 -6 -6 5 46.90 2.30 5 6 -5 224.08 8.20 5 6 -5 235.58 9.20 -5 -6 5 224.08 7.70 4 6 -5 36.80 2.30 4 6 -5 40.90 1.90 -4 -6 5 39.40 1.90 3 6 -5 131.19 5.00 3 6 -5 137.29 5.80 2 6 -5 4.20 0.90 2 6 -5 4.60 0.80 1 6 -5 125.59 4.60 0 6 -5 451.95 15.20 -1 6 -5 56.29 2.30 -2 6 -5 58.09 2.40 2 -6 5 55.89 3.80 -3 6 -5 28.70 1.50 3 -6 5 28.60 2.80 -4 6 -5 101.19 3.90 4 -6 5 102.39 6.30 -5 6 -5 271.37 9.70 -5 6 -5 274.67 8.90 5 -6 5 290.77 14.50 -6 6 -5 23.60 1.30 -6 6 -5 25.00 1.50 -7 6 -5 66.79 2.50 -7 6 -5 62.29 2.90 7 -6 5 60.69 2.90 -8 6 -5 8.90 1.20 -8 6 -5 6.90 0.90 8 -6 5 7.50 1.20 -9 6 -5 40.90 2.30 -9 6 -5 38.60 1.90 9 -6 5 39.80 2.40 -10 6 -5 97.39 4.30 -10 6 -5 102.09 3.80 10 -6 5 101.79 4.50 -11 6 -5 0.20 0.50 -11 6 -5 0.10 0.50 11 -6 5 -0.10 0.40 -12 6 -5 13.90 1.00 -12 6 -5 15.40 1.20 12 -6 5 17.20 1.00 -13 6 -5 1.00 0.40 -14 6 -5 43.50 1.50 13 5 -5 3.90 0.70 12 5 -5 0.30 0.50 -12 -5 5 0.90 0.40 11 5 -5 20.40 1.50 -11 -5 5 22.40 1.60 -11 -5 5 19.20 1.20 10 5 -5 39.20 2.20 10 5 -5 42.60 1.80 -10 -5 5 42.80 2.30 -10 -5 5 42.90 1.90 9 5 -5 29.50 1.50 9 5 -5 28.60 1.80 -9 -5 5 30.60 2.00 -9 -5 5 27.30 1.60 8 5 -5 41.80 2.20 8 5 -5 41.30 1.90 -8 -5 5 39.80 2.30 -8 -5 5 42.10 1.90 7 5 -5 0.10 0.40 -7 -5 5 0.10 0.70 6 5 -5 319.17 12.70 -6 -5 5 340.07 10.80 5 5 -5 738.03 28.20 5 5 -5 751.82 25.10 -5 -5 5 754.42 23.50 4 5 -5 10.00 1.00 4 5 -5 11.60 1.20 -4 -5 5 9.90 1.00 3 5 -5 1000.00 37.70 3 5 -5 1010.40 33.30 2 5 -5 0.60 0.50 2 5 -5 1.50 0.70 1 5 -5 675.23 31.80 1 5 -5 701.63 26.00 0 5 -5 352.36 12.10 0 5 -5 365.16 17.20 -1 5 -5 164.38 8.50 -1 5 -5 157.78 5.60 1 -5 5 158.08 7.90 -2 5 -5 398.76 13.50 -2 5 -5 419.76 19.20 2 -5 5 387.46 18.60 -3 5 -5 116.39 4.30 3 -5 5 115.59 6.50 -4 5 -5 384.56 13.10 4 -5 5 385.46 18.60 -5 5 -5 3.90 0.70 -5 5 -5 4.50 0.60 5 -5 5 4.20 0.80 5 -5 5 3.40 1.30 -6 5 -5 2.60 0.70 -6 5 -5 2.70 0.50 6 -5 5 -0.40 1.00 6 -5 5 2.50 0.70 -7 5 -5 63.89 2.60 -7 5 -5 68.79 3.00 7 -5 5 65.89 3.00 -8 5 -5 15.70 1.20 -8 5 -5 18.20 1.50 8 -5 5 14.90 1.50 -9 5 -5 2.60 0.90 -9 5 -5 5.40 0.90 9 -5 5 4.60 1.00 -10 5 -5 0.50 0.60 -10 5 -5 2.30 0.80 10 -5 5 1.90 0.50 10 -5 5 2.20 0.90 -11 5 -5 99.29 3.30 -11 5 -5 104.39 3.90 11 -5 5 100.89 3.20 -12 5 -5 54.49 2.10 -12 5 -5 56.19 2.40 -13 5 -5 18.40 1.00 -14 5 -5 4.90 0.60 13 4 -5 44.10 1.90 -13 -4 5 41.70 1.50 12 4 -5 31.60 1.70 -12 -4 5 31.80 1.40 11 4 -5 48.10 2.30 -11 -4 5 45.90 1.90 -11 -4 5 46.40 2.40 10 4 -5 1.20 0.70 10 4 -5 2.40 0.50 -10 -4 5 2.50 0.90 -10 -4 5 2.40 0.70 9 4 -5 0.60 0.50 9 4 -5 0.20 0.60 -9 -4 5 0.90 0.80 -9 -4 5 -0.20 0.60 8 4 -5 3.20 0.80 -8 -4 5 5.30 1.00 -8 -4 5 6.60 1.10 -7 -4 5 2.00 0.80 6 4 -5 243.98 9.20 -6 -4 5 231.08 8.00 5 4 -5 1.00 0.50 5 4 -5 1.80 0.60 -5 -4 5 2.60 0.70 4 4 -5 153.48 6.40 4 4 -5 159.68 5.70 3 4 -5 5.10 0.80 3 4 -5 3.10 0.70 2 4 -5 55.99 2.70 2 4 -5 51.59 3.80 2 4 -5 56.19 2.30 1 4 -5 257.47 10.00 1 4 -5 248.78 8.80 1 4 -5 267.47 12.70 0 4 -5 8.70 1.50 0 4 -5 9.50 0.70 0 4 -5 8.70 1.00 -1 4 -5 93.49 5.20 -1 4 -5 82.89 3.20 1 -4 5 88.19 4.70 -2 4 -5 3538.95 115.99 -2 4 -5 3638.64 157.68 2 -4 5 3476.65 155.48 -3 4 -5 135.39 4.80 -3 4 -5 133.69 7.20 3 -4 5 126.99 7.10 -4 4 -5 644.04 21.50 4 -4 5 635.04 22.40 4 -4 5 658.23 29.80 -5 4 -5 9.70 1.00 5 -4 5 9.10 1.00 5 -4 5 8.90 2.20 -6 4 -5 251.07 9.00 -6 4 -5 247.58 8.30 6 -4 5 250.57 9.40 6 -4 5 286.47 13.70 -7 4 -5 842.32 25.90 -7 4 -5 832.52 27.90 7 -4 5 823.42 29.10 -8 4 -5 563.64 19.40 -8 4 -5 583.94 18.00 8 -4 5 562.54 20.30 -9 4 -5 72.49 3.40 -9 4 -5 72.49 2.90 9 -4 5 70.09 3.50 -10 4 -5 0.80 0.60 -10 4 -5 0.90 0.50 -10 4 -5 0.40 0.80 10 -4 5 0.70 0.40 10 -4 5 1.00 0.90 -11 4 -5 46.00 1.90 -11 4 -5 41.30 2.10 -12 4 -5 12.30 1.00 -12 4 -5 11.70 1.20 -13 4 -5 15.20 1.00 -14 4 -5 9.10 0.70 13 3 -5 0.70 0.50 -13 -3 5 0.30 0.40 12 3 -5 43.90 2.20 -12 -3 5 43.70 1.80 11 3 -5 40.10 2.20 -11 -3 5 42.70 1.80 -11 -3 5 42.50 2.30 10 3 -5 144.99 5.60 -10 -3 5 142.19 5.40 -10 -3 5 149.88 4.70 9 3 -5 3.50 0.60 9 3 -5 2.00 0.70 -9 -3 5 1.60 0.80 -9 -3 5 3.80 0.70 -8 -3 5 115.69 4.50 -7 -3 5 2.90 0.80 6 3 -5 110.49 4.40 -6 -3 5 114.59 4.10 5 3 -5 144.69 6.20 5 3 -5 163.98 5.80 -5 -3 5 162.38 5.40 4 3 -5 72.69 2.80 4 3 -5 64.99 3.00 3 3 -5 3.60 0.70 3 3 -5 2.40 1.10 3 3 -5 3.30 0.70 2 3 -5 41.00 1.80 2 3 -5 41.00 2.90 2 3 -5 45.10 3.20 2 3 -5 43.50 2.10 1 3 -5 368.86 13.30 1 3 -5 323.37 15.60 1 3 -5 329.87 11.70 1 3 -5 366.46 16.50 0 3 -5 55.19 2.20 0 3 -5 59.39 3.60 0 3 -5 55.59 2.50 0 3 -5 53.49 3.30 -1 3 -5 353.76 16.10 -1 3 -5 372.86 16.90 -1 3 -5 352.36 12.00 -2 3 -5 512.05 22.70 -2 3 -5 481.15 16.30 2 -3 5 474.85 22.20 -3 3 -5 91.89 3.30 -3 3 -5 89.99 5.10 3 -3 5 79.29 4.90 -4 3 -5 94.99 3.60 -4 3 -5 101.69 5.80 4 -3 5 98.09 5.80 -5 3 -5 241.88 8.70 5 -3 5 264.27 12.80 -6 3 -5 145.39 5.40 -6 3 -5 141.79 4.90 -6 3 -5 146.19 7.00 6 -3 5 154.18 5.70 6 -3 5 151.58 8.60 -7 3 -5 95.99 3.90 -7 3 -5 96.19 3.50 -7 3 -5 93.19 5.20 7 -3 5 100.99 4.10 7 -3 5 95.99 6.60 -8 3 -5 79.29 3.00 -8 3 -5 80.99 3.40 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0.60 -4 18 -6 32.50 1.20 -5 18 -6 2.20 0.30 4 17 -6 7.20 0.50 3 17 -6 0.50 0.30 2 17 -6 5.00 0.60 1 17 -6 15.30 0.90 0 17 -6 25.90 1.20 -1 17 -6 19.30 1.00 -2 17 -6 0.70 0.40 -3 17 -6 0.90 0.40 -4 17 -6 2.40 0.40 -5 17 -6 90.79 2.80 5 -17 6 82.29 2.70 -6 17 -6 82.89 2.60 6 -17 6 84.09 2.60 7 -17 6 42.60 1.40 6 16 -6 21.30 1.10 5 16 -6 122.79 4.10 4 16 -6 87.79 2.70 3 16 -6 83.69 2.70 2 16 -6 63.49 2.20 2 16 -6 58.89 2.50 1 16 -6 74.19 2.50 1 16 -6 73.59 3.00 0 16 -6 186.28 5.60 0 16 -6 186.28 6.40 -1 16 -6 137.09 4.40 -1 16 -6 149.39 5.10 -2 16 -6 46.10 1.70 -2 16 -6 40.10 2.00 -3 16 -6 23.60 1.40 -3 16 -6 20.30 1.10 -4 16 -6 3.00 0.50 -4 16 -6 1.90 0.50 4 -16 6 2.80 0.50 -5 16 -6 195.38 5.80 5 -16 6 192.78 5.70 -6 16 -6 53.09 1.90 6 -16 6 52.49 1.80 7 -16 6 28.90 1.20 8 -16 6 113.89 3.40 7 15 -6 20.20 1.00 -7 -15 6 20.40 1.00 6 15 -6 1.50 0.50 -6 -15 6 3.90 0.60 5 15 -6 12.40 0.70 5 15 -6 11.90 1.00 -5 -15 6 13.20 1.00 4 15 -6 21.70 1.00 -4 -15 6 23.80 1.30 3 15 -6 18.40 1.30 3 15 -6 18.60 1.00 2 15 -6 -0.30 0.40 2 15 -6 0.00 0.50 1 15 -6 2.50 0.50 1 15 -6 1.60 0.60 0 15 -6 32.90 1.50 0 15 -6 34.80 1.80 -1 15 -6 25.00 1.30 -1 15 -6 25.90 1.50 -2 15 -6 5.30 0.80 -2 15 -6 3.90 0.70 -3 15 -6 0.00 0.50 -3 15 -6 0.70 0.40 3 -15 6 0.80 0.40 -4 15 -6 33.80 1.70 -4 15 -6 35.20 1.50 4 -15 6 33.40 1.40 -5 15 -6 713.13 21.90 -5 15 -6 691.93 19.80 5 -15 6 685.53 19.30 6 -15 6 57.29 2.00 7 -15 6 21.30 1.00 8 -15 6 36.70 2.00 8 -15 6 39.20 1.40 9 -15 6 29.40 1.10 8 14 -6 2.30 0.40 -8 -14 6 1.70 0.40 7 14 -6 0.70 0.40 -7 -14 6 0.20 0.50 6 14 -6 22.80 1.30 -6 -14 6 23.70 1.40 5 14 -6 31.70 1.30 5 14 -6 30.50 1.60 -5 -14 6 30.00 1.60 4 14 -6 13.70 0.90 4 14 -6 11.00 1.10 -4 -14 6 13.90 1.20 3 14 -6 41.30 1.70 3 14 -6 41.60 2.00 -3 -14 6 40.40 1.90 2 14 -6 3.20 0.70 2 14 -6 3.10 0.50 -2 -14 6 2.40 0.60 1 14 -6 48.20 2.30 1 14 -6 47.30 1.90 0 14 -6 7.50 0.80 0 14 -6 6.10 1.00 -1 14 -6 11.60 1.20 -1 14 -6 14.10 1.00 -2 14 -6 1.90 0.50 -2 14 -6 1.10 0.60 -3 14 -6 18.40 1.30 -3 14 -6 16.90 1.10 3 -14 6 18.00 1.10 -4 14 -6 226.68 6.80 -4 14 -6 236.18 7.70 4 -14 6 223.58 6.70 -5 14 -6 0.50 0.50 5 -14 6 0.70 0.40 -6 14 -6 41.10 1.90 6 -14 6 38.90 1.60 -7 14 -6 55.59 2.30 7 -14 6 50.89 1.90 8 -14 6 60.09 2.00 9 -14 6 0.00 0.30 10 -14 6 1.50 0.30 9 13 -6 3.40 0.50 -9 -13 6 2.50 0.50 8 13 -6 27.20 1.30 -8 -13 6 26.70 1.40 7 13 -6 1.50 0.50 -7 -13 6 1.60 0.60 6 13 -6 127.99 4.40 -6 -13 6 121.89 4.40 5 13 -6 39.60 1.60 5 13 -6 40.90 1.90 -5 -13 6 42.60 2.00 4 13 -6 1.80 0.60 4 13 -6 1.30 0.60 4 13 -6 1.90 0.40 -4 -13 6 2.70 0.70 3 13 -6 15.10 1.20 3 13 -6 15.60 1.00 -3 -13 6 14.80 1.30 2 13 -6 89.79 3.00 2 13 -6 90.99 3.50 -2 -13 6 82.59 3.30 1 13 -6 10.80 1.10 1 13 -6 11.10 0.90 -1 -13 6 13.10 1.20 0 13 -6 0.70 0.50 0 13 -6 1.40 0.50 -1 13 -6 5.80 0.80 -1 13 -6 5.90 1.00 -2 13 -6 208.68 6.20 -2 13 -6 199.98 7.00 -3 13 -6 13.10 1.10 -3 13 -6 11.70 1.00 3 -13 6 12.80 0.90 -4 13 -6 144.39 5.20 4 -13 6 144.39 4.40 -5 13 -6 63.49 2.70 5 -13 6 61.59 2.20 -6 13 -6 5.40 0.90 6 -13 6 6.40 0.80 -7 13 -6 7.40 0.90 7 -13 6 8.40 0.80 -8 13 -6 33.20 1.60 8 -13 6 32.40 1.40 9 -13 6 5.50 0.60 10 -13 6 87.29 2.70 11 -13 6 16.10 0.70 -10 -12 6 16.90 0.90 9 12 -6 72.19 2.50 -9 -12 6 71.99 2.70 8 12 -6 21.10 1.20 -8 -12 6 20.50 1.40 7 12 -6 20.20 1.30 -7 -12 6 20.20 1.40 6 12 -6 18.40 1.20 -6 -12 6 17.50 1.40 5 12 -6 129.89 4.10 5 12 -6 131.69 4.60 -5 -12 6 133.09 4.70 4 12 -6 0.10 0.50 4 12 -6 1.50 0.50 4 12 -6 0.70 0.40 -4 -12 6 -0.40 0.60 3 12 -6 0.20 0.40 3 12 -6 0.30 0.50 -3 -12 6 0.80 0.60 2 12 -6 3.30 0.50 2 12 -6 1.60 0.60 -2 -12 6 2.70 0.70 1 12 -6 253.87 8.50 1 12 -6 249.68 7.50 0 12 -6 10.90 0.90 0 12 -6 9.30 1.00 -1 12 -6 29.70 1.40 -1 12 -6 29.50 1.70 -2 12 -6 555.74 15.40 -2 12 -6 518.35 17.10 -3 12 -6 70.89 2.90 -3 12 -6 70.29 2.50 -4 12 -6 41.50 2.00 4 -12 6 44.50 1.70 -5 12 -6 1.60 0.60 5 -12 6 1.70 0.50 -6 12 -6 101.49 3.90 6 -12 6 104.89 3.30 -7 12 -6 304.57 10.00 7 -12 6 304.77 8.70 -8 12 -6 88.49 3.40 8 -12 6 87.29 2.80 -9 12 -6 12.10 1.00 9 -12 6 12.70 0.80 10 -12 6 96.29 3.00 11 -12 6 32.70 1.20 10 11 -6 -0.50 0.30 -10 -11 6 -0.20 0.40 9 11 -6 29.30 1.40 -9 -11 6 26.80 1.50 8 11 -6 58.39 2.30 -8 -11 6 56.59 2.50 7 11 -6 0.50 0.50 -7 -11 6 -0.40 0.60 6 11 -6 16.20 1.30 -6 -11 6 16.80 1.40 5 11 -6 42.00 1.70 5 11 -6 44.00 2.10 -5 -11 6 47.40 2.30 4 11 -6 325.97 10.50 4 11 -6 319.07 10.70 4 11 -6 320.67 9.50 -4 -11 6 337.97 10.50 3 11 -6 27.30 1.60 3 11 -6 27.50 1.30 2 11 -6 0.70 0.50 1 11 -6 16.40 1.20 0 11 -6 116.59 4.30 -1 11 -6 351.66 11.40 -2 11 -6 80.89 3.20 -3 11 -6 250.77 8.40 -4 11 -6 0.50 0.50 -5 11 -6 20.10 1.30 5 -11 6 16.60 1.00 -6 11 -6 22.80 1.40 6 -11 6 22.70 1.20 -7 11 -6 44.30 2.10 7 -11 6 48.10 1.80 -8 11 -6 -0.30 0.50 8 -11 6 0.10 0.40 -9 11 -6 4.40 0.80 9 -11 6 4.60 0.70 10 -11 6 16.50 0.90 11 -11 6 0.80 0.40 -11 -10 6 18.50 1.00 10 10 -6 58.49 2.10 -10 -10 6 54.49 2.30 9 10 -6 69.39 2.60 -9 -10 6 66.99 2.70 8 10 -6 203.48 6.70 -8 -10 6 204.08 6.80 7 10 -6 2.00 0.60 -7 -10 6 2.90 0.80 6 10 -6 32.30 1.70 -6 -10 6 36.20 2.00 5 10 -6 21.20 1.40 5 10 -6 18.70 1.10 -5 -10 6 21.30 1.60 4 10 -6 0.90 0.40 4 10 -6 1.00 0.90 4 10 -6 0.50 0.50 3 10 -6 2.70 0.60 2 10 -6 108.79 4.00 1 10 -6 48.00 2.10 0 10 -6 46.00 2.10 -1 10 -6 162.68 5.60 -2 10 -6 6.50 0.80 -3 10 -6 8.30 0.90 -3 10 -6 6.60 1.00 -4 10 -6 0.20 0.40 -4 10 -6 0.60 0.60 -5 10 -6 13.30 1.40 -5 10 -6 16.50 1.20 -6 10 -6 506.75 17.60 -6 10 -6 513.55 16.30 -7 10 -6 1.80 0.80 -7 10 -6 0.50 0.50 7 -10 6 0.60 0.40 -8 10 -6 3.50 0.90 -8 10 -6 6.10 0.90 8 -10 6 1.90 0.50 -9 10 -6 111.89 4.10 9 -10 6 108.89 3.50 -10 10 -6 20.60 1.30 10 -10 6 21.90 1.10 -11 10 -6 162.48 5.00 11 -10 6 163.68 4.80 -12 10 -6 0.00 0.30 12 -10 6 -0.70 0.30 11 9 -6 1.70 0.50 -11 -9 6 3.20 0.50 10 9 -6 1.00 0.50 10 9 -6 0.70 0.40 -10 -9 6 0.50 0.50 9 9 -6 27.80 1.60 9 9 -6 26.10 1.40 -9 -9 6 26.10 1.60 8 9 -6 211.28 6.90 -8 -9 6 210.08 7.10 7 9 -6 3.10 0.60 -7 -9 6 3.90 0.80 6 9 -6 17.40 1.30 -6 -9 6 17.20 1.50 5 9 -6 12.30 1.60 5 9 -6 13.00 0.90 4 9 -6 254.27 10.40 4 9 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20.40 1.80 3 8 -6 0.90 0.40 3 8 -6 0.80 0.80 3 8 -6 0.70 0.50 2 8 -6 409.66 14.10 2 8 -6 416.56 13.20 1 8 -6 285.17 10.10 1 8 -6 294.67 9.40 0 8 -6 75.69 2.80 0 8 -6 69.89 3.00 -1 8 -6 115.49 4.40 -1 8 -6 116.79 4.10 -2 8 -6 639.44 21.30 -2 8 -6 629.54 19.90 -3 8 -6 138.49 4.90 -3 8 -6 146.49 5.30 -4 8 -6 0.50 0.50 -4 8 -6 0.80 0.40 -5 8 -6 246.08 7.90 -5 8 -6 233.48 8.60 -6 8 -6 56.19 2.30 -6 8 -6 51.59 2.60 -7 8 -6 118.29 4.20 -7 8 -6 113.49 4.70 -8 8 -6 105.29 4.30 -8 8 -6 96.19 3.80 8 -8 6 99.49 3.20 -9 8 -6 339.97 12.10 -9 8 -6 330.07 11.00 9 -8 6 338.87 9.60 -10 8 -6 0.30 0.50 10 -8 6 0.40 0.40 -11 8 -6 21.10 1.30 -11 8 -6 19.10 1.10 11 -8 6 20.30 1.10 -12 8 -6 24.30 1.10 12 -8 6 22.80 1.10 -13 8 -6 3.20 0.40 11 7 -6 188.88 6.60 -11 -7 6 182.48 6.10 -11 -7 6 182.58 5.40 10 7 -6 1.40 0.60 10 7 -6 2.00 0.50 -10 -7 6 1.80 0.70 -10 -7 6 1.30 0.50 9 7 -6 7.70 0.90 9 7 -6 4.10 0.80 -9 -7 6 5.50 0.70 -9 -7 6 8.40 1.20 8 7 -6 73.49 3.30 8 7 -6 78.89 2.90 -8 -7 6 74.79 2.70 -8 -7 6 70.29 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12 6 22.50 1.50 9 12 6 21.10 1.10 9 12 6 21.60 1.70 -10 -12 -6 3.60 0.70 10 12 6 5.90 1.20 10 12 6 3.10 0.70 -11 -12 -6 1.00 0.60 11 12 6 1.20 0.50 11 12 6 1.20 0.60 -12 -12 -6 29.00 1.50 12 12 6 30.20 1.40 12 12 6 29.10 1.60 -13 -12 -6 13.80 0.80 13 12 6 12.40 0.70 11 -13 -6 1.40 0.30 10 -13 -6 2.10 0.30 9 -13 -6 20.60 0.80 8 -13 -6 1.10 0.30 8 -13 -6 0.20 0.70 7 -13 -6 55.29 2.70 7 -13 -6 53.19 2.80 7 -13 -6 54.49 2.80 6 -13 -6 20.10 1.60 6 -13 -6 20.00 1.80 6 -13 -6 17.20 1.70 6 -13 -6 21.90 1.80 6 -13 -6 24.80 1.80 5 -13 -6 19.90 1.60 5 -13 -6 22.20 1.80 5 -13 -6 21.20 1.80 5 -13 -6 19.10 1.70 5 -13 -6 19.00 1.80 4 -13 -6 48.60 1.80 4 -13 -6 48.90 2.70 4 -13 -6 47.20 2.60 4 -13 -6 52.49 1.70 3 -13 -6 358.36 11.90 3 -13 -6 359.76 13.30 3 -13 -6 384.26 11.90 2 -13 -6 229.78 7.50 1 -13 -6 19.60 2.40 1 -13 -6 17.80 0.90 0 -13 -6 46.50 1.90 0 -13 -6 51.09 3.80 -1 -13 -6 1.60 1.10 1 13 6 2.40 0.50 -2 -13 -6 138.19 7.60 2 13 6 132.09 4.60 -3 -13 -6 74.49 5.00 3 13 6 78.49 2.90 -4 -13 -6 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424.66 14.30 1 -14 -6 460.75 21.30 0 -14 -6 50.59 2.00 0 -14 -6 47.80 3.90 -1 -14 -6 2.50 1.30 1 14 6 3.50 0.60 -2 -14 -6 52.39 4.00 2 14 6 49.60 2.10 -3 -14 -6 5.10 1.50 3 14 6 6.00 0.80 -4 -14 -6 78.89 5.50 4 14 6 80.09 3.10 -5 -14 -6 3.50 1.60 5 14 6 2.20 0.50 5 14 6 1.00 0.60 6 14 6 0.50 0.40 6 14 6 0.60 0.60 -7 -14 -6 102.29 3.90 7 14 6 115.59 4.20 7 14 6 106.29 3.50 -8 -14 -6 34.80 1.80 8 14 6 34.80 1.50 8 14 6 31.00 1.80 -9 -14 -6 1.60 0.60 9 14 6 3.10 0.80 9 14 6 1.50 0.40 9 14 6 1.40 0.60 -10 -14 -6 6.10 1.00 10 14 6 9.00 1.10 10 14 6 6.60 0.90 -11 -14 -6 24.50 1.20 11 14 6 21.70 1.20 11 14 6 22.70 1.40 -12 -14 -6 1.90 0.40 12 14 6 3.60 0.60 12 14 6 2.60 0.40 10 -15 -6 29.90 1.00 9 -15 -6 21.00 0.80 8 -15 -6 81.09 3.60 8 -15 -6 79.29 2.30 7 -15 -6 199.28 7.80 6 -15 -6 1.60 0.70 5 -15 -6 6.00 1.30 5 -15 -6 9.90 1.50 4 -15 -6 190.08 7.20 4 -15 -6 195.28 7.70 4 -15 -6 193.98 6.40 4 -15 -6 191.88 6.30 4 -15 -6 195.28 7.70 3 -15 -6 91.19 4.10 3 -15 -6 90.89 3.20 3 -15 -6 92.79 4.10 3 -15 -6 88.69 3.10 2 -15 -6 25.30 1.80 2 -15 -6 22.40 1.10 2 -15 -6 26.20 1.90 1 -15 -6 21.90 1.10 1 -15 -6 22.20 2.90 0 -15 -6 1.30 0.40 0 -15 -6 1.70 1.20 -1 -15 -6 304.27 15.20 1 15 6 301.17 9.70 -2 -15 -6 188.68 10.20 2 15 6 182.88 6.20 -3 -15 -6 19.70 2.70 3 15 6 21.70 1.30 -4 -15 -6 170.98 9.90 -4 -15 -6 173.18 5.30 4 15 6 182.38 5.40 4 15 6 180.08 6.10 5 15 6 107.09 4.00 5 15 6 107.19 3.50 6 15 6 477.25 15.30 6 15 6 472.65 13.70 7 15 6 16.30 1.40 7 15 6 18.00 1.10 -8 -15 -6 0.60 0.50 8 15 6 0.10 0.50 8 15 6 0.30 0.40 -9 -15 -6 19.10 1.30 9 15 6 22.10 1.30 9 15 6 20.30 1.00 9 15 6 20.60 1.50 -10 -15 -6 20.90 1.10 10 15 6 19.50 1.20 10 15 6 18.10 1.40 -11 -15 -6 1.50 0.40 11 15 6 2.40 0.50 11 15 6 2.10 0.40 9 -16 -6 56.79 1.70 8 -16 -6 4.90 0.40 8 -16 -6 7.00 1.10 7 -16 -6 2.10 0.70 6 -16 -6 1.00 0.70 5 -16 -6 1.40 0.80 5 -16 -6 -0.30 0.70 4 -16 -6 119.49 4.10 4 -16 -6 120.29 5.20 4 -16 -6 129.79 5.30 4 -16 -6 122.89 4.10 3 -16 -6 18.20 1.70 3 -16 -6 17.60 1.70 3 -16 -6 16.60 0.80 2 -16 -6 7.70 0.60 2 -16 -6 7.40 0.60 2 -16 -6 6.80 1.30 2 -16 -6 7.60 1.30 1 -16 -6 32.80 2.10 1 -16 -6 33.10 2.00 1 -16 -6 31.70 1.20 1 -16 -6 33.10 1.50 0 -16 -6 3.70 0.50 0 -16 -6 3.00 1.40 -1 -16 -6 236.08 6.80 -1 -16 -6 232.98 12.40 1 16 6 237.48 7.80 -2 -16 -6 68.69 2.30 2 16 6 67.59 2.70 -3 -16 -6 20.50 1.10 3 16 6 20.40 1.30 -4 -16 -6 71.69 2.50 4 16 6 72.49 2.50 4 16 6 73.49 3.00 5 16 6 48.10 1.90 5 16 6 48.50 2.30 6 16 6 126.49 4.10 6 16 6 137.59 4.80 7 16 6 37.60 2.00 7 16 6 40.30 1.60 8 16 6 49.20 2.20 8 16 6 50.99 1.80 9 16 6 40.40 2.00 9 16 6 37.80 1.40 10 16 6 7.00 0.90 10 16 6 6.00 0.70 11 16 6 7.20 0.80 8 -17 -6 1.10 0.20 8 -17 -6 1.40 0.60 7 -17 -6 167.88 4.80 7 -17 -6 177.78 6.70 6 -17 -6 73.89 3.50 5 -17 -6 1.30 0.70 4 -17 -6 8.00 1.40 4 -17 -6 4.60 0.40 4 -17 -6 4.90 0.50 4 -17 -6 4.10 0.90 4 -17 -6 4.60 0.40 3 -17 -6 3.60 0.40 3 -17 -6 3.10 0.90 3 -17 -6 4.30 0.90 3 -17 -6 2.80 0.40 2 -17 -6 22.20 1.00 2 -17 -6 23.70 1.10 2 -17 -6 24.40 1.80 2 -17 -6 23.30 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18 6 3.90 0.70 -3 -18 -6 365.86 10.80 3 18 6 398.56 12.30 -4 -18 -6 1.50 0.40 4 18 6 0.60 0.50 4 18 6 0.20 0.40 5 18 6 17.30 1.00 5 18 6 16.40 1.20 6 18 6 7.70 1.00 6 18 6 10.20 0.80 7 18 6 16.30 0.90 8 18 6 1.40 0.40 8 18 6 1.40 0.60 9 18 6 33.30 1.20 9 18 6 36.30 1.60 7 -19 -6 50.49 2.40 6 -19 -6 2.40 0.70 6 -19 -6 3.20 0.40 5 -19 -6 0.60 0.20 5 -19 -6 1.40 0.60 4 -19 -6 10.20 1.30 4 -19 -6 9.90 0.60 3 -19 -6 2.30 0.40 3 -19 -6 2.50 0.40 3 -19 -6 2.30 0.70 3 -19 -6 2.20 0.40 2 -19 -6 77.19 2.80 2 -19 -6 80.79 3.60 2 -19 -6 77.79 2.50 1 -19 -6 -0.50 0.60 1 -19 -6 0.60 0.30 1 -19 -6 0.80 0.30 0 -19 -6 6.40 0.70 -1 -19 -6 16.50 0.90 -2 -19 -6 3.00 0.50 2 19 6 3.80 0.60 -3 -19 -6 35.70 1.50 3 19 6 34.50 1.50 3 19 6 36.00 1.70 4 19 6 7.20 0.90 4 19 6 7.80 0.80 5 19 6 30.90 1.30 6 19 6 0.60 0.40 7 19 6 5.90 0.60 7 19 6 4.60 0.70 8 19 6 31.20 1.10 8 19 6 30.80 1.50 6 -20 -6 36.40 1.10 6 -20 -6 39.20 1.90 5 -20 -6 41.30 1.30 5 -20 -6 40.60 2.10 4 -20 -6 0.50 0.60 4 -20 -6 0.00 0.20 3 -20 -6 101.09 3.40 3 -20 -6 104.89 3.40 3 -20 -6 101.39 4.30 3 -20 -6 102.59 3.10 2 -20 -6 25.90 1.80 2 -20 -6 27.00 1.20 2 -20 -6 27.10 1.10 1 -20 -6 65.49 2.10 1 -20 -6 62.89 2.40 0 -20 -6 0.60 0.30 -1 -20 -6 1.20 0.40 -2 -20 -6 2.00 0.40 -3 -20 -6 0.00 0.30 3 20 6 0.60 0.40 4 20 6 0.40 0.30 5 20 6 6.00 0.60 6 20 6 1.20 0.30 7 20 6 2.30 0.50 7 20 6 1.70 0.30 5 -21 -6 30.10 1.00 4 -21 -6 0.10 0.50 4 -21 -6 -0.20 0.20 3 -21 -6 34.70 1.20 3 -21 -6 33.80 1.90 2 -21 -6 3.30 0.70 2 -21 -6 3.30 0.50 1 -21 -6 0.20 0.30 1 -21 -6 0.00 0.20 0 -21 -6 78.09 2.50 -1 -21 -6 10.40 0.70 -2 -21 -6 0.40 0.30 -3 -21 -6 11.40 0.70 3 21 6 14.00 0.80 4 21 6 4.70 0.60 5 21 6 0.70 0.30 6 21 6 48.20 1.60 3 -22 -6 132.79 3.80 2 -22 -6 12.80 0.60 1 -22 -6 6.40 0.50 0 -22 -6 12.10 0.70 -1 -22 -6 27.00 1.10 -2 -22 -6 16.70 0.80 3 22 6 0.00 0.30 2 18 -7 17.40 0.70 1 18 -7 4.80 0.50 0 18 -7 54.69 1.80 -1 18 -7 0.30 0.30 -2 18 -7 64.29 2.10 -3 18 -7 94.69 2.90 -4 18 -7 3.10 0.50 3 17 -7 14.70 0.70 2 17 -7 5.50 0.60 1 17 -7 1.60 0.40 0 17 -7 61.79 2.10 -1 17 -7 19.90 1.00 -2 17 -7 3.60 0.60 -3 17 -7 5.40 0.60 -4 17 -7 14.60 0.80 -5 17 -7 16.10 0.80 -6 17 -7 0.20 0.30 5 16 -7 5.30 0.70 4 16 -7 0.30 0.30 3 16 -7 32.10 1.30 2 16 -7 6.20 0.70 1 16 -7 173.58 5.20 0 16 -7 0.70 0.50 0 16 -7 0.60 0.40 -1 16 -7 1.00 0.40 -1 16 -7 1.10 0.50 -2 16 -7 2.90 0.60 -2 16 -7 2.40 0.40 -3 16 -7 33.60 1.40 -4 16 -7 14.90 0.90 -5 16 -7 2.70 0.40 -6 16 -7 13.40 0.80 6 -16 7 14.20 0.80 -7 16 -7 10.30 0.70 7 -16 7 11.00 0.70 7 15 -7 7.00 0.60 6 15 -7 24.20 1.10 -6 -15 7 22.30 1.10 5 15 -7 38.30 1.70 -5 -15 7 38.20 1.60 4 15 -7 58.79 1.90 4 15 -7 54.59 2.30 -4 -15 7 57.79 2.20 3 15 -7 45.60 1.70 2 15 -7 2.10 0.60 2 15 -7 2.60 0.50 1 15 -7 16.00 1.20 1 15 -7 15.60 1.00 0 15 -7 79.99 2.70 0 15 -7 80.39 3.20 -1 15 -7 54.09 2.40 -1 15 -7 56.29 2.10 -2 15 -7 152.28 5.40 -2 15 -7 149.19 4.70 -3 15 -7 32.00 1.70 -3 15 -7 29.50 1.40 -4 15 -7 4.10 0.70 -4 15 -7 3.00 0.60 -5 15 -7 156.08 5.40 -5 15 -7 158.38 4.80 5 -15 7 151.08 4.60 -6 15 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2.50 -12 -5 7 59.69 2.00 11 5 -7 8.80 1.00 -11 -5 7 6.80 0.90 10 5 -7 6.00 1.00 -10 -5 7 7.30 1.20 -10 -5 7 5.70 0.90 9 5 -7 4.60 0.80 9 5 -7 4.60 0.80 -9 -5 7 5.00 0.70 -9 -5 7 5.70 1.00 8 5 -7 10.80 1.30 8 5 -7 11.80 1.10 -8 -5 7 13.10 1.20 -8 -5 7 13.10 1.50 7 5 -7 13.80 1.30 -7 -5 7 13.10 1.20 -7 -5 7 12.60 1.50 6 5 -7 217.38 8.50 -6 -5 7 224.48 7.60 5 5 -7 150.58 5.90 5 5 -7 154.58 6.40 -5 -5 7 162.48 5.60 4 5 -7 4.30 1.00 4 5 -7 6.20 0.90 -4 -5 7 6.20 1.00 3 5 -7 517.25 20.00 3 5 -7 525.85 17.80 -3 -5 7 528.25 16.60 2 5 -7 1138.29 37.40 2 5 -7 1119.59 42.30 1 5 -7 131.09 5.60 0 5 -7 6.30 1.10 0 5 -7 7.40 0.80 -1 5 -7 329.87 11.30 -2 5 -7 64.49 2.60 -3 5 -7 1216.68 38.90 3 -5 7 1131.49 52.79 -4 5 -7 324.97 11.20 -4 5 -7 317.17 10.40 4 -5 7 335.67 16.20 -5 5 -7 1.50 0.50 -5 5 -7 3.10 0.70 5 -5 7 1.00 1.20 -6 5 -7 112.39 4.00 -6 5 -7 111.99 4.40 -7 5 -7 30.40 1.90 -7 5 -7 34.70 1.70 -8 5 -7 59.09 2.50 -8 5 -7 64.69 3.00 8 -5 7 56.79 3.00 -9 5 -7 179.18 5.40 -9 5 -7 172.98 6.20 -9 5 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0.50 0.60 6 5 -10 0.60 0.50 -6 -5 10 0.50 0.80 -6 -5 10 0.80 0.60 5 5 -10 219.08 7.80 5 5 -10 203.38 7.40 -5 -5 10 201.08 6.30 -5 -5 10 201.68 7.20 4 5 -10 83.29 3.80 4 5 -10 93.39 3.90 -4 -5 10 87.89 3.60 3 5 -10 49.10 2.50 3 5 -10 47.70 2.50 -3 -5 10 45.80 2.30 2 5 -10 75.39 3.50 2 5 -10 69.69 3.20 -2 -5 10 72.49 3.00 1 5 -10 26.20 1.80 1 5 -10 23.70 1.60 0 5 -10 274.97 10.80 0 5 -10 264.27 8.80 0 5 -10 264.77 9.50 -1 5 -10 61.59 2.70 -1 5 -10 58.49 3.10 -1 5 -10 57.19 2.40 -2 5 -10 19.10 1.20 -2 5 -10 19.50 1.40 -3 5 -10 -0.30 0.50 -3 5 -10 0.10 0.40 -4 5 -10 281.67 10.00 -4 5 -10 280.57 9.20 -5 5 -10 167.88 6.30 -5 5 -10 164.98 5.70 -6 5 -10 242.38 8.10 -6 5 -10 244.18 8.80 -7 5 -10 86.79 3.50 -7 5 -10 91.59 3.90 -8 5 -10 4.50 0.60 -8 5 -10 3.70 0.70 -8 5 -10 4.40 0.90 -9 5 -10 217.68 8.20 -9 5 -10 215.58 6.60 -9 5 -10 224.78 7.50 -10 5 -10 1.20 0.50 -10 5 -10 0.80 0.60 -11 5 -10 123.49 4.50 -11 5 -10 121.89 3.90 -12 5 -10 127.19 4.00 -13 5 -10 4.40 0.60 11 4 -10 41.70 1.80 -11 -4 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28.40 1.80 1 2 -14 122.89 4.90 -1 -2 14 115.59 4.50 0 2 -14 36.50 2.10 0 -2 14 38.20 2.00 -1 2 -14 437.56 15.00 1 -2 14 425.66 13.90 -2 2 -14 30.00 1.90 2 -2 14 34.30 1.80 -3 2 -14 0.30 0.60 -4 2 -14 226.68 8.30 -5 2 -14 133.49 5.30 -6 2 -14 83.39 3.40 -6 2 -14 90.39 3.90 -7 2 -14 17.50 1.60 -7 2 -14 16.20 1.00 -7 2 -14 16.30 1.30 -7 2 -14 19.80 1.40 7 -2 14 15.00 1.30 -8 2 -14 11.80 1.20 -8 2 -14 11.40 1.20 -8 2 -14 12.10 1.00 -8 2 -14 10.90 1.40 8 -2 14 13.10 1.10 -9 2 -14 406.86 13.20 -9 2 -14 402.46 11.70 9 -2 14 407.56 12.80 -10 2 -14 7.40 0.80 -10 2 -14 7.70 1.10 10 -2 14 9.90 1.00 -11 2 -14 4.70 0.70 -11 2 -14 4.00 0.70 11 -2 14 5.40 0.80 -12 2 -14 5.00 0.60 -13 2 -14 1.90 0.30 -13 2 -14 0.90 0.60 -10 -1 14 29.30 1.20 -9 -1 14 7.00 0.90 -8 -1 14 22.20 1.50 -8 -1 14 21.40 1.30 -7 -1 14 5.10 1.00 -7 -1 14 6.00 1.00 6 1 -14 27.30 1.80 -6 -1 14 29.10 1.60 -6 -1 14 28.40 1.90 5 1 -14 54.39 2.60 5 1 -14 49.99 2.80 -5 -1 14 52.79 2.60 -5 -1 14 53.99 2.20 4 1 -14 15.80 1.50 4 1 -14 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1.10 5 -4 21 16.80 1.20 -6 4 -21 72.19 2.60 6 -4 21 71.49 2.70 -7 4 -21 27.10 1.30 7 -4 21 28.00 1.30 -8 4 -21 0.70 0.30 8 -4 21 0.20 0.30 3 3 -21 40.80 1.80 2 3 -21 13.80 1.10 -2 -3 21 12.30 1.10 1 3 -21 0.70 0.30 1 3 -21 0.70 0.50 -1 -3 21 1.00 0.50 -1 -3 21 0.00 0.50 0 3 -21 59.99 2.20 0 3 -21 63.19 2.60 0 -3 21 58.69 2.50 -1 3 -21 11.90 0.90 -1 3 -21 11.00 1.10 1 -3 21 8.80 1.10 -2 3 -21 3.20 0.50 2 -3 21 2.80 0.70 -3 3 -21 21.80 1.30 3 -3 21 23.90 1.50 -4 3 -21 53.79 2.20 4 -3 21 53.89 2.30 -5 3 -21 91.59 3.30 5 -3 21 93.29 3.40 -6 3 -21 83.19 3.00 6 -3 21 84.09 3.10 -7 3 -21 30.70 1.40 7 -3 21 29.20 1.40 -8 3 -21 0.90 0.40 8 -3 21 -0.10 0.40 -9 3 -21 6.40 0.60 4 2 -21 157.28 5.30 -4 -2 21 145.89 4.40 3 2 -21 -0.20 0.50 -3 -2 21 1.10 0.40 2 2 -21 3.80 0.70 -2 -2 21 3.10 0.50 1 2 -21 26.50 1.60 1 2 -21 25.80 1.20 -1 -2 21 22.20 1.40 -1 -2 21 25.10 1.20 -1 -2 21 24.10 1.50 0 2 -21 292.47 9.20 0 2 -21 300.57 10.10 0 -2 21 280.07 9.50 0 -2 21 302.37 8.60 -1 2 -21 2.00 0.60 -1 2 -21 2.10 0.50 1 -2 21 1.70 0.50 1 -2 21 1.80 0.70 -2 2 -21 21.60 1.20 2 -2 21 23.50 1.50 -3 2 -21 99.59 3.70 3 -2 21 107.69 3.90 -4 2 -21 14.20 1.10 4 -2 21 14.70 1.30 -5 2 -21 41.20 1.80 5 -2 21 37.40 1.90 -6 2 -21 13.00 1.00 6 -2 21 11.50 1.10 -7 2 -21 0.70 0.40 7 -2 21 1.00 0.50 -8 2 -21 117.19 4.60 -8 2 -21 113.89 3.90 8 -2 21 116.39 3.90 -9 2 -21 7.80 0.70 -9 2 -21 9.40 0.90 9 -2 21 6.20 0.70 4 1 -21 16.30 1.10 -4 -1 21 16.40 0.90 3 1 -21 8.60 1.00 -3 -1 21 11.50 0.90 2 1 -21 0.70 0.50 -2 -1 21 1.20 0.50 1 1 -21 0.60 0.60 -1 -1 21 3.10 0.60 0 1 -21 329.97 10.20 0 1 -21 322.07 11.20 0 -1 21 323.37 9.50 -1 1 -21 94.29 3.80 -1 1 -21 93.99 3.40 1 -1 21 94.69 3.70 1 -1 21 100.39 3.20 -2 1 -21 2.70 0.50 2 -1 21 2.40 0.70 2 -1 21 3.80 0.60 -3 1 -21 13.10 1.10 3 -1 21 16.70 1.40 -4 1 -21 -0.30 0.40 4 -1 21 -0.20 0.60 -5 1 -21 225.28 7.50 5 -1 21 235.38 7.60 -6 1 -21 36.80 1.70 6 -1 21 39.40 1.90 -7 1 -21 5.00 0.80 7 -1 21 3.80 0.60 -8 1 -21 34.70 1.60 -8 1 -21 36.80 2.00 8 -1 21 38.80 1.70 -9 1 -21 11.40 1.10 -9 1 -21 11.70 0.90 9 -1 21 10.80 0.90 -10 1 -21 11.10 0.90 -10 1 -21 10.00 0.80 10 -1 21 10.40 0.70 5 0 -21 0.60 0.40 -5 0 21 1.50 0.40 4 0 -21 -0.10 0.50 -4 0 21 0.30 0.40 3 0 -21 16.00 1.30 -3 0 21 18.00 1.10 2 0 -21 107.49 4.10 -2 0 21 100.69 3.40 1 0 -21 77.59 3.30 -1 0 21 79.19 3.30 -1 0 21 78.69 2.70 0 0 -21 1.40 0.40 0 0 -21 2.50 0.70 0 0 21 0.60 0.70 0 0 21 1.50 0.50 -1 0 -21 138.29 5.30 -1 0 -21 146.79 4.70 1 0 21 141.59 4.40 1 0 21 137.39 5.20 -2 0 -21 115.29 3.90 2 0 21 112.99 4.20 2 0 21 110.19 3.60 -3 0 -21 112.29 3.90 3 0 21 107.79 3.60 3 0 21 115.49 4.20 -4 0 -21 1.20 0.50 4 0 21 1.80 0.70 -5 0 -21 2.30 0.50 5 0 21 2.90 0.70 -6 0 -21 8.70 0.90 6 0 21 11.40 1.10 -7 0 -21 36.00 2.00 -7 0 -21 35.70 1.70 7 0 21 36.90 1.80 -8 0 -21 6.00 1.10 -8 0 -21 5.00 0.80 8 0 21 6.20 0.90 -9 0 -21 59.49 2.30 -9 0 -21 59.29 2.70 9 0 21 58.29 2.30 -10 0 -21 1.30 0.50 -10 0 -21 0.50 0.40 10 0 21 0.30 0.40 5 -1 -21 0.20 0.40 -5 1 21 0.20 0.40 4 -1 -21 12.20 1.10 -4 1 21 13.10 1.00 3 -1 -21 215.88 7.60 -3 1 21 216.88 6.50 2 -1 -21 2.50 0.70 -2 1 21 3.10 0.60 -2 1 21 2.40 0.80 1 -1 -21 6.90 1.10 -1 1 21 6.50 1.20 -1 1 21 6.00 0.90 0 -1 -21 0.90 0.60 0 1 21 2.20 0.80 0 1 21 1.90 0.60 -1 -1 -21 23.30 1.60 -1 -1 -21 20.70 1.20 1 1 21 18.50 1.60 1 1 21 19.20 1.20 -2 -1 -21 150.98 5.20 2 1 21 156.68 4.90 2 1 21 163.28 5.80 -3 -1 -21 8.10 0.90 3 1 21 5.50 1.00 3 1 21 7.00 0.90 3 1 21 6.40 1.10 -4 -1 -21 7.60 0.90 4 1 21 9.40 1.20 4 1 21 8.00 0.90 -5 -1 -21 0.70 0.50 5 1 21 1.20 0.60 -6 -1 -21 0.40 0.50 -6 -1 -21 0.90 0.70 6 1 21 -0.10 0.60 -7 -1 -21 21.20 1.30 -7 -1 -21 20.70 1.60 7 1 21 17.70 1.40 -8 -1 -21 45.20 2.00 -8 -1 -21 50.59 2.50 8 1 21 45.40 2.10 -9 -1 -21 2.80 0.50 -9 -1 -21 2.70 0.70 9 1 21 2.90 0.60 -10 -1 -21 1.00 0.60 -10 -1 -21 0.30 0.40 10 1 21 0.50 0.40 -11 -1 -21 0.50 0.30 -6 2 21 100.39 3.10 5 -2 -21 6.30 0.90 -5 2 21 5.10 0.80 4 -2 -21 147.39 5.50 -4 2 21 157.48 4.70 3 -2 -21 78.29 3.20 -3 2 21 74.09 2.60 2 -2 -21 26.20 1.70 -2 2 21 22.50 1.60 -2 2 21 23.40 1.30 1 -2 -21 173.98 6.60 -1 2 21 174.48 5.50 -1 2 21 192.18 6.50 0 -2 -21 0.30 0.60 0 2 21 0.60 0.50 0 2 21 0.60 0.70 -1 -2 -21 87.69 3.70 1 2 21 93.79 3.70 1 2 21 88.29 3.10 -2 -2 -21 107.19 3.70 2 2 21 110.29 3.60 2 2 21 103.79 4.20 -3 -2 -21 216.88 7.10 3 2 21 218.58 7.70 3 2 21 225.48 6.70 -4 -2 -21 1.90 0.50 4 2 21 1.60 0.70 4 2 21 1.80 0.60 4 2 21 2.20 0.80 -5 -2 -21 70.49 2.80 5 2 21 69.99 2.90 5 2 21 70.89 2.50 -6 -2 -21 111.39 4.70 -6 -2 -21 113.09 4.00 6 2 21 110.59 4.10 -7 -2 -21 82.69 3.60 -7 -2 -21 73.59 3.00 7 2 21 82.39 3.10 -8 -2 -21 142.89 5.90 -8 -2 -21 154.48 5.00 8 2 21 148.29 5.10 -9 -2 -21 1.10 0.70 -9 -2 -21 0.80 0.40 9 2 21 0.10 0.50 -10 -2 -21 47.20 1.90 -10 -2 -21 48.40 2.40 10 2 21 49.40 1.90 -11 -2 -21 16.30 1.10 -11 -2 -21 16.50 0.90 11 2 21 15.70 0.90 -6 3 21 11.50 0.80 5 -3 -21 -0.20 0.50 -5 3 21 0.00 0.40 4 -3 -21 230.88 7.90 -4 3 21 219.38 6.70 3 -3 -21 105.29 4.10 -3 3 21 100.59 3.40 2 -3 -21 16.50 1.50 -2 3 21 21.00 1.50 -2 3 21 18.30 1.20 1 -3 -21 27.40 1.80 -1 3 21 31.10 1.50 -1 3 21 31.20 1.90 0 -3 -21 6.10 1.10 0 3 21 7.60 1.00 0 3 21 6.40 1.00 1 3 21 139.59 5.20 1 3 21 139.39 4.50 2 3 21 63.79 2.40 2 3 21 66.39 3.00 -3 -3 -21 1.40 0.50 3 3 21 2.20 0.80 3 3 21 1.70 0.60 -4 -3 -21 18.80 1.20 4 3 21 20.00 1.20 4 3 21 17.70 1.50 -5 -3 -21 111.29 4.60 -5 -3 -21 107.49 3.80 5 3 21 105.19 4.00 5 3 21 107.49 4.40 5 3 21 106.79 3.50 -6 -3 -21 39.00 1.80 -6 -3 -21 39.20 2.30 6 3 21 40.00 2.00 6 3 21 36.20 1.60 -7 -3 -21 35.80 2.10 -7 -3 -21 30.30 1.60 7 3 21 32.50 1.80 -8 -3 -21 28.10 1.50 -8 -3 -21 31.10 2.00 8 3 21 29.50 1.60 -9 -3 -21 84.09 3.70 -9 -3 -21 82.69 3.00 9 3 21 85.49 3.10 -10 -3 -21 0.30 0.40 -10 -3 -21 0.00 0.60 10 3 21 0.70 0.50 -11 -3 -21 17.40 1.30 -11 -3 -21 18.40 1.00 11 3 21 19.50 1.00 6 -4 -21 9.90 0.90 -6 4 21 9.20 0.80 5 -4 -21 0.30 0.50 -5 4 21 -0.10 0.40 4 -4 -21 5.30 1.00 -4 4 21 6.40 0.90 3 -4 -21 117.69 4.50 -3 4 21 118.59 4.40 -3 4 21 111.49 3.70 2 -4 -21 6.80 1.20 -2 4 21 8.00 1.00 -2 4 21 7.80 1.20 1 -4 -21 24.20 1.70 -1 4 21 27.50 1.80 -1 4 21 29.70 1.50 0 -4 -21 123.09 4.90 0 4 21 132.29 4.90 0 4 21 129.59 4.20 1 4 21 118.49 3.90 1 4 21 119.49 4.60 2 4 21 50.99 2.00 2 4 21 46.90 2.50 -3 -4 -21 43.00 1.90 3 4 21 47.60 1.90 3 4 21 48.20 2.40 3 4 21 47.30 1.90 -4 -4 -21 77.19 2.90 4 4 21 81.49 2.80 4 4 21 81.29 2.80 4 4 21 79.29 3.40 -5 -4 -21 73.99 3.40 -5 -4 -21 74.59 2.80 5 4 21 72.19 3.10 5 4 21 70.79 2.60 5 4 21 69.39 2.60 -6 -4 -21 185.78 7.30 -6 -4 -21 186.88 6.10 6 4 21 179.28 5.60 6 4 21 182.68 5.60 6 4 21 187.28 6.30 -7 -4 -21 13.50 1.10 -7 -4 -21 16.30 1.60 7 4 21 16.10 1.00 7 4 21 14.10 1.00 7 4 21 16.00 1.30 -8 -4 -21 16.20 1.10 -8 -4 -21 16.10 1.50 8 4 21 15.50 1.20 -9 -4 -21 96.99 4.10 -9 -4 -21 97.39 3.40 9 4 21 91.59 3.40 -10 -4 -21 0.50 0.60 -10 -4 -21 0.30 0.40 10 4 21 0.50 0.50 -11 -4 -21 1.40 0.40 -11 -4 -21 0.20 0.50 11 4 21 0.50 0.40 6 -5 -21 25.90 1.40 -6 5 21 26.90 1.20 5 -5 -21 89.29 3.50 -5 5 21 94.59 3.00 4 -5 -21 214.28 7.50 -4 5 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84.09 2.70 5 -6 -21 123.89 3.70 5 -6 -21 128.59 4.70 -5 6 21 126.99 3.90 4 -6 -21 11.70 0.70 4 -6 -21 11.30 1.30 -4 6 21 11.70 1.00 3 -6 -21 35.30 2.00 3 -6 -21 33.10 1.30 -3 6 21 32.30 1.50 -3 6 21 33.50 1.80 2 -6 -21 30.30 1.20 2 -6 -21 27.90 1.80 -2 6 21 26.70 1.40 -2 6 21 28.70 1.80 1 -6 -21 -0.10 0.60 -1 6 21 -0.20 0.70 -1 6 21 1.00 0.60 0 -6 -21 37.30 2.10 0 6 21 40.00 1.70 0 6 21 36.30 2.10 1 6 21 35.00 2.00 1 6 21 32.30 1.60 1 6 21 33.70 1.60 2 6 21 173.78 5.50 2 6 21 183.68 6.40 3 6 21 192.08 6.60 3 6 21 181.08 5.70 -4 -6 -21 16.50 1.60 4 6 21 18.80 1.20 4 6 21 19.70 1.50 -5 -6 -21 10.50 1.40 -5 -6 -21 8.30 0.90 5 6 21 9.20 1.20 5 6 21 7.20 0.90 -6 -6 -21 76.69 3.60 -6 -6 -21 74.99 2.80 6 6 21 75.69 2.60 6 6 21 71.79 3.10 -7 -6 -21 31.80 2.10 -7 -6 -21 29.20 1.50 7 6 21 31.30 1.40 7 6 21 33.70 1.70 -8 -6 -21 76.29 3.60 -8 -6 -21 80.19 2.90 8 6 21 79.89 3.00 8 6 21 80.09 2.60 -9 -6 -21 12.80 1.00 -9 -6 -21 12.10 1.40 9 6 21 13.60 1.10 -10 -6 -21 47.10 1.90 -10 -6 -21 49.30 2.50 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0.40 0.40 0 3 -22 7.60 0.60 0 3 -22 8.80 0.90 0 -3 22 9.80 1.00 0 -3 22 9.50 1.00 -1 3 -22 14.10 0.80 -1 3 -22 14.50 1.10 1 -3 22 15.10 1.10 -2 3 -22 1.50 0.40 2 -3 22 0.60 0.50 -3 3 -22 10.60 0.80 3 -3 22 8.20 1.00 -4 3 -22 42.60 1.80 4 -3 22 44.30 1.90 -5 3 -22 2.50 0.50 5 -3 22 1.90 0.50 -6 3 -22 26.90 1.30 6 -3 22 27.80 1.40 -7 3 -22 1.80 0.40 7 -3 22 1.80 0.50 -8 3 -22 44.80 1.70 8 -3 22 42.90 1.60 3 2 -22 5.80 0.80 2 2 -22 5.40 0.80 1 2 -22 12.90 1.10 -1 -2 22 13.80 1.00 -1 -2 22 12.30 1.00 0 2 -22 2.10 0.60 0 2 -22 2.20 0.40 0 -2 22 2.90 0.60 -1 2 -22 48.00 1.80 -1 2 -22 47.50 2.10 1 -2 22 47.70 2.10 -2 2 -22 6.40 0.70 2 -2 22 5.40 0.80 -3 2 -22 215.38 6.70 3 -2 22 201.28 6.90 -4 2 -22 43.90 1.80 4 -2 22 38.30 1.90 -5 2 -22 20.60 1.10 5 -2 22 19.70 1.30 -6 2 -22 32.50 1.40 6 -2 22 29.30 1.50 -7 2 -22 12.20 0.90 7 -2 22 10.50 0.90 -8 2 -22 23.90 1.10 8 -2 22 24.30 1.20 -9 2 -22 0.50 0.30 3 1 -22 14.50 1.10 -3 -1 22 14.90 0.80 2 1 -22 10.40 1.10 -2 -1 22 11.80 0.80 1 1 -22 8.50 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10 1.5334 0.1252 14 -1 11 0.6354 0.0566 14 -1 12 -0.5012 0.0826 14 0 0 0.1594 0.4019 14 0 1 -0.8035 0.0996 14 0 2 -1.3125 -0.2914 14 0 3 -1.3383 0.1072 14 0 4 -0.9046 0.2630 14 0 5 0.0223 -0.0528 14 0 6 -0.0177 0.0453 14 0 7 -1.4069 0.1288 14 0 8 -0.9520 -0.0673 14 0 9 1.7126 0.0664 14 0 10 2.1018 0.2153 14 0 11 -0.1803 0.0460 14 0 12 -0.9364 0.0353 14 1 0 -0.8952 0.3669 14 1 1 -1.0633 0.0240 14 1 2 -0.4462 -0.1071 14 1 3 -0.2064 0.1893 14 1 4 0.9212 0.2226 14 1 5 1.6436 0.0602 14 1 6 -0.2824 0.0927 14 1 7 -1.7624 0.0294 14 1 8 0.3881 -0.0197 14 1 9 2.6094 0.1317 14 1 10 1.0157 0.1236 14 1 11 -1.5267 -0.0048 14 1 12 -1.0307 -0.0350 14 2 0 -1.2216 0.0767 14 2 1 -0.3640 -0.0051 14 2 2 1.2358 0.1178 14 2 3 1.3339 0.1544 14 2 4 1.6435 0.1159 14 2 5 1.0138 0.1322 14 2 6 -1.4685 0.0465 14 2 7 -1.5916 -0.0655 14 2 8 1.2687 0.0395 14 2 9 1.9644 0.0836 14 2 10 -0.6488 -0.0047 14 2 11 -2.1758 0.0161 14 2 12 -0.5485 -0.0652 14 2 13 1.1205 -0.2115 14 3 0 -0.9469 -0.1235 14 3 1 0.6517 0.0433 14 3 2 2.3001 0.2003 14 3 3 1.4350 0.0065 14 3 4 0.3389 -0.0276 14 3 5 -0.6927 0.1309 14 3 6 -2.0084 -0.0159 14 3 7 -1.0128 -0.1359 14 3 8 1.3714 0.0341 14 3 9 0.9052 0.0217 14 3 10 -1.6450 -0.0291 14 3 11 -1.9358 0.0904 14 3 12 0.1863 -0.0184 14 3 13 1.0162 -0.1396 14 3 14 -0.1706 -0.0085 14 4 0 -0.4085 -0.0919 14 4 1 1.1988 0.0879 14 4 2 1.7360 0.0999 14 4 3 0.0392 -0.1450 14 4 4 -1.2001 -0.0796 14 4 5 -1.4402 0.1037 14 4 6 -1.5680 -0.1006 14 4 7 -0.3491 -0.1845 14 4 8 1.1787 0.0134 14 4 9 0.0914 -0.0094 14 4 10 -1.8314 -0.0037 14 4 11 -1.1730 0.1334 14 4 12 0.5783 0.0334 14 4 13 0.6233 -0.0079 14 4 14 0.0031 0.0874 14 5 0 0.0613 0.0530 14 5 1 0.9285 0.0783 14 5 2 0.3590 -0.0599 14 5 3 -1.0793 -0.1446 14 5 4 -1.2817 -0.0160 14 5 5 -0.7953 0.0042 14 5 6 -0.8141 -0.1691 14 5 7 -0.0621 -0.1329 14 5 8 0.8552 -0.0118 14 5 9 -0.2436 -0.0539 14 5 10 -1.5507 0.0152 14 5 11 -0.7243 0.0859 14 5 12 0.4993 -0.0006 14 5 13 0.5925 0.0516 14 5 14 0.5893 0.0259 14 6 1 0.4395 0.0509 14 6 2 -0.5101 -0.1137 14 6 3 -0.8159 -0.0201 14 6 4 0.0180 0.0099 14 6 5 -0.0377 -0.1064 14 6 6 -0.8018 -0.0955 14 6 7 -0.0652 -0.0266 14 6 8 0.7702 -0.0698 14 6 9 -0.3862 -0.0652 14 6 10 -1.4242 0.0176 14 6 11 -0.6610 -0.0262 14 6 12 0.3288 -0.0401 14 6 13 0.6350 0.0576 14 6 14 0.6312 -0.1035 14 7 3 0.3719 0.0332 14 7 4 0.8656 -0.0387 14 7 5 -0.4194 -0.0842 14 7 6 -1.1417 0.0378 14 7 7 0.1511 0.0011 14 7 8 0.7005 -0.0734 14 7 9 -0.5772 0.0005 14 7 10 -1.3724 -0.0035 14 7 11 -0.7536 -0.0493 14 7 12 0.1921 0.0466 14 7 13 0.6304 0.0687 14 7 14 0.2673 -0.1074 14 8 4 0.3120 -0.0735 14 8 5 -1.2598 -0.0026 14 8 6 -1.0202 0.0501 14 8 7 0.5457 -0.0034 14 8 8 0.5337 0.0417 14 8 9 -0.7392 0.0657 14 8 10 -1.2265 -0.0030 14 8 11 -0.5967 0.0931 14 8 12 0.2994 0.1909 14 8 13 0.6465 0.0729 14 9 6 -0.2788 -0.0051 14 9 7 0.7957 0.0554 14 9 8 0.2110 0.1569 14 9 9 -0.7070 0.0618 14 9 10 -0.8026 0.0437 14 9 11 -0.2963 0.2518 14 9 12 0.3901 0.2304 0 0 0 0.0 0.0 ; _shelx_fab_checksum 85730 _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems' _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn Br2 Br 0.03184(2) 0.29077(2) 0.79731(2) 0.02750(6) Uani 1 1 d . Br1 Br -0.19916(2) 0.48677(2) 0.47983(2) 0.03104(7) Uani 1 1 d . Br4 Br 0.82206(2) 0.16399(2) 0.78453(2) 0.03197(7) Uani 1 1 d . Br3 Br 0.44264(2) 0.41155(2) 0.56559(2) 0.04071(8) Uani 1 1 d . Cu1 Cu 0.21857(3) 0.24743(2) 0.50319(2) 0.02062(7) Uani 1 1 d . Cu2 Cu 0.34483(3) 0.30602(2) 0.89582(2) 0.02209(8) Uani 1 1 d . P4 P 0.41226(5) 0.39429(3) 0.92729(3) 0.02188(12) Uani 1 1 d . P3 P 0.20432(5) 0.23866(3) 0.97156(3) 0.02208(12) Uani 1 1 d . P1 P 0.13213(5) 0.14478(3) 0.50384(3) 0.02037(11) Uani 1 1 d . P2 P 0.37521(5) 0.27733(3) 0.42690(3) 0.02127(11) Uani 1 1 d . P5 P -0.03131(5) 0.46697(3) 0.23763(3) 0.02752(13) Uani 1 1 d . P6 P 0.45213(5) 0.08089(3) 0.72400(3) 0.02802(13) Uani 1 1 d . O1 O 0.20913(14) 0.24877(9) 0.36421(8) 0.0256(3) Uani 1 1 d . O2 O 0.38199(14) 0.26055(9) 1.04045(8) 0.0257(3) Uani 1 1 d . F10 F 0.45106(15) -0.00738(9) 0.75966(9) 0.0477(4) Uani 1 1 d . F3 F -0.04357(17) 0.52147(9) 0.28020(8) 0.0479(4) Uani 1 1 d . F7 F 0.45138(16) 0.16887(9) 0.68775(11) 0.0580(5) Uani 1 1 d . F6 F -0.02234(19) 0.41192(11) 0.19652(9) 0.0589(5) Uani 1 1 d . N1 N 0.10477(16) 0.33211(10) 0.48534(9) 0.0215(4) Uani 1 1 d . N2 N 0.17937(16) 0.26024(10) 0.59438(9) 0.0219(4) Uani 1 1 d . N4 N 0.48188(17) 0.24533(10) 0.87113(9) 0.0238(4) Uani 1 1 d . N3 N 0.35549(16) 0.33737(11) 0.79536(9) 0.0223(4) Uani 1 1 d . F1 F -0.0961(3) 0.52167(16) 0.18852(12) 0.0944(10) Uani 1 1 d . F8 F 0.32983(19) 0.08253(13) 0.76239(14) 0.0861(9) Uani 1 1 d . C4 C -0.04003(19) 0.39096(12) 0.54396(11) 0.0218(4) Uani 1 1 d . C54 C 0.51814(19) 0.26483(12) 0.80470(11) 0.0203(4) Uani 1 1 d . C52 C 0.48091(19) 0.33389(12) 0.69476(11) 0.0212(4) Uani 1 1 d . C53 C 0.44891(18) 0.31300(12) 0.76387(11) 0.0199(4) Uani 1 1 d . C6 C 0.09290(18) 0.30603(12) 0.60015(11) 0.0196(4) Uani 1 1 d . F12 F 0.4042(3) 0.07031(15) 0.66719(13) 0.0954(9) Uani 1 1 d . C7 C 0.04354(19) 0.31808(12) 0.65963(11) 0.0210(4) Uani 1 1 d . C5 C 0.05159(18) 0.34397(12) 0.54126(10) 0.0197(4) Uani 1 1 d . C61 C 0.1245(2) 0.17863(13) 0.94676(11) 0.0254(5) Uani 1 1 d . C57 C 0.5836(2) 0.30873(13) 0.66640(11) 0.0238(5) Uani 1 1 d . H57 H 0.6051 0.3221 0.6199 0.029 Uiso 1 1 calc R C73 C 0.2480(2) 0.17092(13) 1.04338(11) 0.0255(5) Uani 1 1 d . C55 C 0.62007(19) 0.24217(12) 0.77508(11) 0.0221(4) Uani 1 1 d . C51 C 0.4083(2) 0.38101(13) 0.65868(11) 0.0260(5) Uani 1 1 d . C56 C 0.6506(2) 0.26615(12) 0.70479(11) 0.0240(5) Uani 1 1 d . H56 H 0.7195 0.2518 0.6846 0.029 Uiso 1 1 calc R C85 C 0.55758(19) 0.37900(12) 0.93109(11) 0.0232(5) Uani 1 1 d . C13 C 0.36709(19) 0.37339(12) 0.37256(11) 0.0224(4) Uani 1 1 d . C49 C 0.29183(19) 0.38281(14) 0.75866(11) 0.0255(5) Uani 1 1 d . H49 H 0.2274 0.4007 0.7801 0.031 Uiso 1 1 calc R C74 C 0.3321(2) 0.18940(13) 1.06905(11) 0.0259(5) Uani 1 1 d . C3 C -0.0744(2) 0.42545(13) 0.48404(12) 0.0246(5) Uani 1 1 d . C44 C 0.2280(2) 0.02743(13) 0.45964(12) 0.0258(5) Uani 1 1 d . H44 H 0.1800 0.0391 0.4295 0.031 Uiso 1 1 calc R C8 C 0.08941(19) 0.27944(13) 0.71495(11) 0.0230(5) Uani 1 1 d . C10 C 0.2193(2) 0.22552(13) 0.64788(12) 0.0265(5) Uani 1 1 d . H10 H 0.2798 0.1935 0.6443 0.032 Uiso 1 1 calc R C14 C 0.3660(2) 0.42933(13) 0.40026(11) 0.0255(5) Uani 1 1 d . H14 H 0.3749 0.4167 0.4444 0.031 Uiso 1 1 calc R C11 C -0.04772(19) 0.36702(13) 0.66020(11) 0.0248(5) Uani 1 1 d . H11 H -0.0809 0.3755 0.7000 0.030 Uiso 1 1 calc R C50 C 0.3149(2) 0.40566(14) 0.68980(12) 0.0280(5) Uani 1 1 d . H50 H 0.2666 0.4377 0.6653 0.034 Uiso 1 1 calc R C59 C 0.6477(2) 0.17722(14) 0.88521(12) 0.0305(5) Uani 1 1 d . H59 H 0.6911 0.1468 0.9143 0.037 Uiso 1 1 calc R C58 C 0.6835(2) 0.19711(12) 0.81859(12) 0.0251(5) Uani 1 1 d . C60 C 0.5454(2) 0.20285(14) 0.90956(12) 0.0301(5) Uani 1 1 d . H60 H 0.5204 0.1891 0.9559 0.036 Uiso 1 1 calc R C43 C 0.22489(18) 0.06832(12) 0.50175(11) 0.0219(4) Uani 1 1 d . C80 C 0.34350(19) 0.38913(14) 1.01041(11) 0.0253(5) Uani 1 1 d . F5 F 0.0775(2) 0.5079(2) 0.19380(15) 0.1090(12) Uani 1 1 d . C12 C -0.08784(19) 0.40139(13) 0.60542(11) 0.0250(5) Uani 1 1 d . H12 H -0.1490 0.4331 0.6077 0.030 Uiso 1 1 calc R C20 C 0.5203(2) 0.23230(13) 0.51182(12) 0.0279(5) Uani 1 1 d . H20 H 0.4585 0.2043 0.5423 0.034 Uiso 1 1 calc R F4 F 0.0378(4) 0.41341(16) 0.28539(14) 0.1285(16) Uani 1 1 d . C31 C 0.1062(2) 0.21523(13) 0.37365(12) 0.0260(5) Uani 1 1 d . C62 C 0.0109(2) 0.16477(15) 0.97045(13) 0.0329(6) Uani 1 1 d . H62 H -0.0285 0.1884 0.9998 0.039 Uiso 1 1 calc R C37 C 0.02061(19) 0.10083(13) 0.57428(11) 0.0238(5) Uani 1 1 d . C38 C 0.0180(2) 0.02564(15) 0.61200(12) 0.0318(5) Uani 1 1 d . H38 H 0.0773 -0.0052 0.6028 0.038 Uiso 1 1 calc R F11 F 0.57290(19) 0.07884(17) 0.68661(18) 0.1252(15) Uani 1 1 d . C92 C 0.4862(2) 0.54589(14) 0.87769(12) 0.0289(5) Uani 1 1 d . H92 H 0.5448 0.5301 0.9005 0.035 Uiso 1 1 calc R C91 C 0.4090(2) 0.49366(13) 0.87998(11) 0.0254(5) Uani 1 1 d . C2 C -0.0191(2) 0.41531(14) 0.42712(12) 0.0278(5) Uani 1 1 d . H2 H -0.0414 0.4398 0.3867 0.033 Uiso 1 1 calc R C86 C 0.6298(2) 0.37863(13) 0.87320(12) 0.0278(5) Uani 1 1 d . H86 H 0.6022 0.3879 0.8343 0.033 Uiso 1 1 calc R F9 F 0.4977(3) 0.09183(14) 0.78137(15) 0.1128(13) Uani 1 1 d . C67 C 0.1006(2) 0.29387(14) 1.00615(12) 0.0268(5) Uani 1 1 d . C9 C 0.1770(2) 0.23367(14) 0.70933(11) 0.0270(5) Uani 1 1 d . H9 H 0.2085 0.2080 0.7463 0.032 Uiso 1 1 calc R C26 C 0.3029(2) 0.20984(12) 0.34875(11) 0.0252(5) Uani 1 1 d . C19 C 0.5089(2) 0.27615(13) 0.44887(12) 0.0257(5) Uani 1 1 d . C66 C 0.1811(2) 0.14436(14) 0.90312(12) 0.0294(5) Uani 1 1 d . H66 H 0.2579 0.1542 0.8860 0.035 Uiso 1 1 calc R C81 C 0.2953(2) 0.44970(15) 1.02661(13) 0.0307(5) Uani 1 1 d . H81 H 0.3029 0.4980 0.9941 0.037 Uiso 1 1 calc R C42 C -0.0670(2) 0.14556(15) 0.58929(13) 0.0316(5) Uani 1 1 d . H42 H -0.0648 0.1976 0.5650 0.038 Uiso 1 1 calc R C90 C 0.5993(2) 0.36473(15) 0.98777(12) 0.0317(5) Uani 1 1 d . H90 H 0.5516 0.3647 1.0276 0.038 Uiso 1 1 calc R C32 C 0.06109(19) 0.16306(12) 0.43509(11) 0.0234(5) Uani 1 1 d . C45 C 0.3015(2) -0.03054(14) 0.46177(14) 0.0338(6) Uani 1 1 d . H45 H 0.3054 -0.0575 0.4321 0.041 Uiso 1 1 calc R C15 C 0.3519(2) 0.50318(13) 0.36435(12) 0.0279(5) Uani 1 1 d . H15 H 0.3537 0.5411 0.3833 0.033 Uiso 1 1 calc R C25 C 0.3938(2) 0.22150(12) 0.37234(11) 0.0250(5) Uani 1 1 d . C87 C 0.7403(2) 0.36504(15) 0.87170(14) 0.0351(6) Uani 1 1 d . H87 H 0.7886 0.3655 0.8319 0.042 Uiso 1 1 calc R C48 C 0.2953(2) 0.05042(14) 0.54624(12) 0.0282(5) Uani 1 1 d . H48 H 0.2945 0.0790 0.5743 0.034 Uiso 1 1 calc R C79 C 0.33005(19) 0.31861(14) 1.05940(11) 0.0257(5) Uani 1 1 d . C16 C 0.3353(2) 0.52190(14) 0.30057(12) 0.0314(5) Uani 1 1 d . H16 H 0.3238 0.5725 0.2762 0.038 Uiso 1 1 calc R C18 C 0.3530(2) 0.39297(14) 0.30782(12) 0.0298(5) Uani 1 1 d . H18 H 0.3555 0.3556 0.2878 0.036 Uiso 1 1 calc R C68 C 0.0448(2) 0.27048(17) 1.07166(13) 0.0373(6) Uani 1 1 d . H68 H 0.0589 0.2231 1.1011 0.045 Uiso 1 1 calc R C1 C 0.0710(2) 0.36807(13) 0.42979(11) 0.0259(5) Uani 1 1 d . H1 H 0.1099 0.3613 0.3902 0.031 Uiso 1 1 calc R C65 C 0.1254(2) 0.09559(15) 0.88449(14) 0.0362(6) Uani 1 1 d . H65 H 0.1642 0.0718 0.8551 0.043 Uiso 1 1 calc R C75 C 0.3740(2) 0.13778(16) 1.11934(12) 0.0336(6) Uani 1 1 d . H75 H 0.4318 0.1519 1.1355 0.040 Uiso 1 1 calc R C24 C 0.6003(2) 0.31829(16) 0.40491(14) 0.0366(6) Uani 1 1 d . H24 H 0.5935 0.3491 0.3620 0.044 Uiso 1 1 calc R C41 C -0.1571(2) 0.11423(18) 0.63957(14) 0.0393(6) Uani 1 1 d . H41 H -0.2174 0.1445 0.6486 0.047 Uiso 1 1 calc R C78 C 0.2060(2) 0.09737(15) 1.07169(13) 0.0363(6) Uani 1 1 d . H78 H 0.1482 0.0827 1.0559 0.044 Uiso 1 1 calc R C72 C 0.0775(2) 0.36298(15) 0.96334(14) 0.0335(6) Uani 1 1 d . H72 H 0.1154 0.3793 0.9186 0.040 Uiso 1 1 calc R C94 C 0.3931(3) 0.64463(15) 0.80892(14) 0.0391(6) Uani 1 1 d . H94 H 0.3878 0.6961 0.7847 0.047 Uiso 1 1 calc R C21 C 0.6211(2) 0.22903(15) 0.53064(14) 0.0357(6) Uani 1 1 d . H21 H 0.6282 0.1985 0.5736 0.043 Uiso 1 1 calc R C29 C 0.4958(3) 0.13966(15) 0.31847(13) 0.0398(7) Uani 1 1 d . H29 H 0.5623 0.1154 0.3079 0.048 Uiso 1 1 calc R C96 C 0.3242(2) 0.51789(15) 0.84604(14) 0.0371(6) Uani 1 1 d . H96 H 0.2715 0.4827 0.8469 0.045 Uiso 1 1 calc R C63 C -0.0442(2) 0.11682(17) 0.95132(14) 0.0401(6) Uani 1 1 d . H63 H -0.1214 0.1079 0.9673 0.048 Uiso 1 1 calc R C17 C 0.3355(3) 0.46689(14) 0.27262(12) 0.0352(6) Uani 1 1 d . H17 H 0.3236 0.4796 0.2291 0.042 Uiso 1 1 calc R C82 C 0.2361(2) 0.44042(17) 1.08996(14) 0.0377(6) Uani 1 1 d . H82 H 0.2032 0.4822 1.1005 0.045 Uiso 1 1 calc R C64 C 0.0132(2) 0.08193(15) 0.90894(14) 0.0384(6) Uani 1 1 d . H64 H -0.0246 0.0483 0.8965 0.046 Uiso 1 1 calc R C27 C 0.3068(2) 0.16478(14) 0.31027(12) 0.0326(6) Uani 1 1 d . H27 H 0.2441 0.1585 0.2941 0.039 Uiso 1 1 calc R C33 C -0.0446(2) 0.13429(13) 0.44299(13) 0.0287(5) Uani 1 1 d . H33 H -0.0773 0.0979 0.4837 0.034 Uiso 1 1 calc R C93 C 0.4778(2) 0.62108(15) 0.84214(13) 0.0342(6) Uani 1 1 d . H93 H 0.5307 0.6565 0.8407 0.041 Uiso 1 1 calc R C84 C 0.2724(2) 0.30856(16) 1.12274(12) 0.0344(6) Uani 1 1 d . H84 H 0.2651 0.2604 1.1555 0.041 Uiso 1 1 calc R C36 C 0.0491(3) 0.23958(15) 0.32346(13) 0.0375(6) Uani 1 1 d . H36 H 0.0818 0.2756 0.2825 0.045 Uiso 1 1 calc R C76 C 0.3305(2) 0.06518(16) 1.14575(13) 0.0396(6) Uani 1 1 d . H76 H 0.3587 0.0292 1.1801 0.047 Uiso 1 1 calc R C88 C 0.7805(2) 0.35071(17) 0.92851(16) 0.0431(7) Uani 1 1 d . H88 H 0.8565 0.3410 0.9278 0.052 Uiso 1 1 calc R C46 C 0.3691(2) -0.04909(15) 0.50721(15) 0.0371(6) Uani 1 1 d . H46 H 0.4177 -0.0897 0.5093 0.045 Uiso 1 1 calc R C28 C 0.4040(3) 0.12914(15) 0.29592(13) 0.0386(6) Uani 1 1 d . H28 H 0.4076 0.0972 0.2704 0.046 Uiso 1 1 calc R C77 C 0.2467(3) 0.04539(16) 1.12221(14) 0.0428(7) Uani 1 1 d . H77 H 0.2165 -0.0042 1.1407 0.051 Uiso 1 1 calc R C47 C 0.3662(2) -0.00883(15) 0.54962(14) 0.0343(6) Uani 1 1 d . H47 H 0.4125 -0.0218 0.5808 0.041 Uiso 1 1 calc R C34 C -0.1028(2) 0.15765(16) 0.39280(14) 0.0374(6) Uani 1 1 d . H34 H -0.1743 0.1371 0.3992 0.045 Uiso 1 1 calc R C35 C -0.0564(3) 0.21112(17) 0.33316(15) 0.0440(7) Uani 1 1 d . H35 H -0.0970 0.2282 0.2991 0.053 Uiso 1 1 calc R C95 C 0.3162(3) 0.59360(17) 0.81082(16) 0.0455(7) Uani 1 1 d . H95 H 0.2576 0.6099 0.7881 0.055 Uiso 1 1 calc R C30 C 0.4913(2) 0.18550(14) 0.35653(12) 0.0324(6) Uani 1 1 d . H30 H 0.5547 0.1924 0.3719 0.039 Uiso 1 1 calc R C39 C -0.0716(3) -0.00471(17) 0.66346(14) 0.0424(7) Uani 1 1 d . H39 H -0.0722 -0.0560 0.6897 0.051 Uiso 1 1 calc R C83 C 0.2253(2) 0.37003(18) 1.13762(14) 0.0408(7) Uani 1 1 d . H83 H 0.1852 0.3638 1.1809 0.049 Uiso 1 1 calc R C22 C 0.7112(2) 0.27047(17) 0.48649(16) 0.0416(7) Uani 1 1 d . H22 H 0.7802 0.2682 0.4992 0.050 Uiso 1 1 calc R C71 C -0.0010(2) 0.40815(17) 0.98592(18) 0.0460(7) Uani 1 1 d . H71 H -0.0176 0.4549 0.9564 0.055 Uiso 1 1 calc R F2 F -0.1387(3) 0.4259(2) 0.28286(16) 0.1457(18) Uani 1 1 d . C23 C 0.7008(2) 0.31524(18) 0.42382(16) 0.0458(7) Uani 1 1 d . H23 H 0.7625 0.3439 0.3938 0.055 Uiso 1 1 calc R C40 C -0.1593(2) 0.03897(19) 0.67664(14) 0.0440(7) Uani 1 1 d . H40 H -0.2210 0.0176 0.7110 0.053 Uiso 1 1 calc R C89 C 0.7103(2) 0.35055(18) 0.98615(15) 0.0431(7) Uani 1 1 d . H89 H 0.7383 0.3406 1.0250 0.052 Uiso 1 1 calc R C69 C -0.0322(3) 0.3173(2) 1.09364(16) 0.0498(8) Uani 1 1 d . H69 H -0.0693 0.3021 1.1385 0.060 Uiso 1 1 calc R C70 C -0.0547(3) 0.3852(2) 1.05097(19) 0.0511(8) Uani 1 1 d . H70 H -0.1075 0.4164 1.0664 0.061 Uiso 1 1 calc R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br2 0.03410(13) 0.03141(13) 0.01660(11) -0.00782(9) -0.00604(9) 0.00653(10) Br1 0.03218(13) 0.03491(14) 0.02466(12) -0.00808(10) -0.00980(10) 0.01779(11) Br4 0.02922(13) 0.02645(13) 0.03673(14) -0.00609(10) -0.00856(10) 0.00863(10) Br3 0.04416(16) 0.05867(19) 0.01516(12) -0.00664(11) -0.01044(11) 0.01795(13) Cu1 0.02502(17) 0.01643(15) 0.01726(15) -0.00424(12) -0.00088(12) 0.00463(12) Cu2 0.02606(17) 0.02242(16) 0.01437(15) -0.00258(12) -0.00266(12) -0.00010(13) P4 0.0255(3) 0.0219(3) 0.0154(3) -0.0036(2) -0.0024(2) -0.0006(2) P3 0.0243(3) 0.0216(3) 0.0158(3) -0.0003(2) -0.0044(2) -0.0002(2) P1 0.0231(3) 0.0161(2) 0.0184(3) -0.0029(2) -0.0018(2) 0.0030(2) P2 0.0251(3) 0.0170(3) 0.0180(3) -0.0040(2) 0.0000(2) 0.0030(2) P5 0.0357(3) 0.0271(3) 0.0191(3) -0.0070(2) -0.0071(2) 0.0071(3) P6 0.0250(3) 0.0232(3) 0.0307(3) -0.0032(2) -0.0050(2) 0.0024(2) O2 0.0310(9) 0.0194(8) 0.0231(8) -0.0059(6) -0.0006(7) 0.0012(6) O3 0.0298(9) 0.0259(8) 0.0168(7) -0.0029(6) -0.0015(6) -0.0031(7) F10 0.0562(10) 0.0247(8) 0.0522(10) -0.0057(7) -0.0033(8) 0.0090(7) F3 0.0858(13) 0.0314(8) 0.0316(8) -0.0144(7) -0.0197(8) 0.0156(8) F7 0.0539(11) 0.0274(9) 0.0811(14) 0.0076(9) -0.0305(10) -0.0051(8) F6 0.0887(15) 0.0555(11) 0.0475(11) -0.0341(9) -0.0211(10) 0.0140(10) N1 0.0273(10) 0.0171(9) 0.0178(9) -0.0040(7) -0.0035(7) 0.0049(7) N2 0.0245(9) 0.0196(9) 0.0199(9) -0.0059(7) -0.0032(7) 0.0041(7) N4 0.0311(10) 0.0183(9) 0.0184(9) -0.0013(7) -0.0054(8) 0.0022(8) N3 0.0252(10) 0.0219(9) 0.0183(9) -0.0041(7) -0.0053(7) 0.0006(7) F1 0.145(2) 0.107(2) 0.0633(14) -0.0516(14) -0.0721(16) 0.0910(19) F8 0.0561(13) 0.0531(13) 0.1050(19) -0.0008(12) 0.0311(13) 0.0174(10) C4 0.0244(11) 0.0198(11) 0.0201(11) -0.0054(9) -0.0050(9) 0.0045(9) C54 0.0271(11) 0.0150(10) 0.0180(10) -0.0032(8) -0.0063(9) -0.0012(8) C52 0.0271(11) 0.0172(10) 0.0186(10) -0.0038(8) -0.0066(9) -0.0015(8) C53 0.0251(11) 0.0151(10) 0.0184(10) -0.0037(8) -0.0051(9) -0.0013(8) C6 0.0217(10) 0.0166(10) 0.0181(10) -0.0033(8) -0.0034(8) 0.0020(8) F12 0.168(3) 0.0705(16) 0.0652(15) -0.0210(12) -0.0633(18) -0.0033(17) C7 0.0240(11) 0.0201(10) 0.0179(10) -0.0055(8) -0.0037(9) 0.0012(9) C5 0.0231(11) 0.0170(10) 0.0172(10) -0.0042(8) -0.0034(8) 0.0026(8) C61 0.0305(12) 0.0228(11) 0.0186(11) 0.0005(9) -0.0084(9) 0.0000(9) C57 0.0323(12) 0.0213(11) 0.0167(10) -0.0058(9) -0.0038(9) 0.0008(9) C73 0.0275(12) 0.0262(12) 0.0166(10) 0.0004(9) -0.0037(9) 0.0004(9) C55 0.0273(11) 0.0151(10) 0.0232(11) -0.0047(8) -0.0062(9) 0.0002(8) C51 0.0338(13) 0.0274(12) 0.0151(10) -0.0033(9) -0.0079(9) 0.0006(10) C56 0.0271(12) 0.0191(11) 0.0245(11) -0.0074(9) -0.0030(9) 0.0033(9) C85 0.0268(11) 0.0192(10) 0.0215(11) -0.0049(9) -0.0034(9) -0.0010(9) C13 0.0241(11) 0.0186(10) 0.0192(11) -0.0031(8) 0.0009(9) 0.0022(8) C49 0.0237(11) 0.0294(12) 0.0223(11) -0.0070(9) -0.0057(9) 0.0030(9) C74 0.0289(12) 0.0259(12) 0.0172(11) -0.0014(9) -0.0018(9) -0.0009(9) C3 0.0276(12) 0.0209(11) 0.0244(11) -0.0056(9) -0.0085(9) 0.0095(9) C44 0.0261(12) 0.0229(11) 0.0255(12) -0.0064(9) -0.0020(9) -0.0001(9) C8 0.0279(12) 0.0229(11) 0.0173(10) -0.0061(9) -0.0035(9) 0.0005(9) C10 0.0288(12) 0.0256(12) 0.0230(11) -0.0056(9) -0.0072(9) 0.0098(9) C14 0.0313(12) 0.0240(11) 0.0198(11) -0.0060(9) -0.0044(9) 0.0026(9) C11 0.0254(11) 0.0285(12) 0.0212(11) -0.0113(9) -0.0027(9) 0.0066(9) C50 0.0285(12) 0.0329(13) 0.0216(11) -0.0051(10) -0.0113(9) 0.0058(10) C59 0.0373(14) 0.0230(12) 0.0278(12) -0.0008(10) -0.0143(11) 0.0084(10) C58 0.0274(12) 0.0163(10) 0.0309(12) -0.0065(9) -0.0072(10) 0.0021(9) C60 0.0395(14) 0.0256(12) 0.0199(11) -0.0002(9) -0.0076(10) 0.0032(10) C43 0.0200(10) 0.0173(10) 0.0214(11) -0.0017(8) 0.0024(8) 0.0021(8) C80 0.0240(11) 0.0329(13) 0.0190(11) -0.0093(9) -0.0029(9) -0.0014(9) F5 0.0631(15) 0.179(3) 0.104(2) -0.094(2) 0.0319(14) -0.0569(18) C12 0.0261(11) 0.0268(12) 0.0225(11) -0.0094(9) -0.0061(9) 0.0104(9) C20 0.0326(13) 0.0212(11) 0.0283(12) -0.0081(10) -0.0037(10) 0.0049(9) F4 0.260(4) 0.0910(19) 0.0844(18) -0.0585(16) -0.118(2) 0.118(3) C31 0.0325(12) 0.0193(11) 0.0247(12) -0.0059(9) -0.0053(10) 0.0031(9) C62 0.0298(13) 0.0393(14) 0.0259(12) -0.0064(11) -0.0048(10) -0.0030(11) C37 0.0255(11) 0.0253(11) 0.0188(11) -0.0064(9) -0.0024(9) 0.0005(9) C38 0.0322(13) 0.0297(13) 0.0259(12) -0.0030(10) 0.0000(10) -0.0007(10) F11 0.0405(12) 0.090(2) 0.160(3) 0.0306(19) 0.0370(15) 0.0174(12) C92 0.0340(13) 0.0286(12) 0.0226(12) -0.0072(10) -0.0043(10) -0.0014(10) C91 0.0322(12) 0.0233(11) 0.0174(11) -0.0042(9) -0.0022(9) 0.0005(9) C2 0.0359(13) 0.0261(12) 0.0188(11) -0.0034(9) -0.0087(10) 0.0099(10) C86 0.0310(13) 0.0253(12) 0.0239(12) -0.0067(9) -0.0009(10) -0.0026(10) F9 0.209(4) 0.0512(14) 0.108(2) -0.0153(14) -0.113(2) -0.0031(17) C67 0.0245(11) 0.0293(12) 0.0264(12) -0.0085(10) -0.0059(9) 0.0004(9) C9 0.0323(13) 0.0272(12) 0.0195(11) -0.0041(9) -0.0085(9) 0.0069(10) C26 0.0353(13) 0.0171(10) 0.0162(10) -0.0017(8) 0.0033(9) 0.0013(9) C19 0.0271(12) 0.0223(11) 0.0262(12) -0.0085(9) -0.0024(9) 0.0047(9) C66 0.0313(13) 0.0266(12) 0.0281(12) -0.0047(10) -0.0091(10) 0.0026(10) C81 0.0287(12) 0.0340(13) 0.0288(13) -0.0114(11) -0.0026(10) -0.0008(10) C42 0.0306(13) 0.0350(14) 0.0303(13) -0.0140(11) -0.0043(10) 0.0054(10) C90 0.0333(13) 0.0374(14) 0.0236(12) -0.0084(10) -0.0064(10) -0.0004(11) C32 0.0282(12) 0.0188(10) 0.0223(11) -0.0063(9) -0.0056(9) 0.0064(9) C45 0.0347(14) 0.0256(12) 0.0395(14) -0.0141(11) 0.0004(11) 0.0030(10) C15 0.0349(13) 0.0218(11) 0.0248(12) -0.0091(9) 0.0008(10) 0.0005(10) C25 0.0343(13) 0.0171(10) 0.0174(10) -0.0026(8) 0.0020(9) 0.0029(9) C87 0.0332(14) 0.0327(14) 0.0370(14) -0.0143(11) 0.0021(11) 0.0010(11) C48 0.0270(12) 0.0246(12) 0.0309(13) -0.0072(10) -0.0056(10) 0.0023(9) C79 0.0246(11) 0.0312(12) 0.0212(11) -0.0090(10) -0.0036(9) -0.0021(9) C16 0.0447(15) 0.0188(11) 0.0224(12) -0.0003(9) -0.0007(10) 0.0026(10) C18 0.0461(15) 0.0220(12) 0.0191(11) -0.0068(9) -0.0020(10) -0.0019(10) C68 0.0353(14) 0.0466(16) 0.0275(13) -0.0109(12) -0.0043(11) 0.0028(12) C1 0.0357(13) 0.0238(11) 0.0156(10) -0.0054(9) -0.0031(9) 0.0069(10) C65 0.0461(16) 0.0279(13) 0.0379(14) -0.0114(11) -0.0167(12) 0.0082(11) C75 0.0323(13) 0.0385(14) 0.0227(12) 0.0007(10) -0.0080(10) 0.0004(11) C24 0.0320(14) 0.0378(15) 0.0303(13) -0.0020(11) -0.0018(11) 0.0006(11) C41 0.0285(13) 0.0578(18) 0.0366(15) -0.0270(14) 0.0002(11) 0.0041(12) C78 0.0424(15) 0.0292(13) 0.0311(13) 0.0017(11) -0.0121(11) -0.0065(11) C72 0.0286(13) 0.0305(13) 0.0392(14) -0.0086(11) -0.0075(11) 0.0013(10) C94 0.0511(17) 0.0225(12) 0.0347(14) -0.0006(11) -0.0050(12) 0.0028(11) C21 0.0430(15) 0.0313(13) 0.0361(14) -0.0128(11) -0.0147(12) 0.0097(11) C29 0.0517(17) 0.0311(14) 0.0304(14) -0.0115(11) 0.0031(12) 0.0156(12) C96 0.0392(15) 0.0286(13) 0.0410(15) -0.0042(11) -0.0151(12) -0.0011(11) C63 0.0339(14) 0.0446(16) 0.0382(15) -0.0072(12) -0.0089(12) -0.0082(12) C17 0.0574(17) 0.0260(13) 0.0176(11) -0.0021(10) -0.0059(11) -0.0006(12) C82 0.0364(14) 0.0428(15) 0.0350(14) -0.0202(12) 0.0021(11) 0.0003(12) C64 0.0465(16) 0.0310(14) 0.0407(15) -0.0092(12) -0.0191(13) -0.0031(12) C27 0.0487(16) 0.0243(12) 0.0215(12) -0.0067(10) -0.0017(11) -0.0002(11) C33 0.0315(13) 0.0222(11) 0.0293(12) -0.0052(10) -0.0058(10) 0.0013(9) C93 0.0433(15) 0.0266(13) 0.0302(13) -0.0093(10) -0.0010(11) -0.0056(11) C84 0.0388(14) 0.0381(14) 0.0209(12) -0.0056(10) 0.0000(10) -0.0074(11) C36 0.0498(16) 0.0284(13) 0.0283(13) 0.0010(10) -0.0119(12) -0.0008(12) C76 0.0456(16) 0.0341(14) 0.0268(13) 0.0079(11) -0.0120(12) 0.0039(12) C88 0.0292(14) 0.0457(17) 0.0543(18) -0.0175(14) -0.0079(13) 0.0054(12) C46 0.0274(13) 0.0264(13) 0.0542(17) -0.0125(12) -0.0046(12) 0.0084(10) C28 0.0611(18) 0.0270(13) 0.0256(13) -0.0125(11) 0.0002(12) 0.0058(12) C77 0.0541(18) 0.0278(14) 0.0348(15) 0.0070(11) -0.0118(13) -0.0045(12) C47 0.0267(12) 0.0280(13) 0.0442(15) -0.0048(11) -0.0120(11) 0.0042(10) C34 0.0357(14) 0.0348(14) 0.0421(15) -0.0096(12) -0.0149(12) 0.0023(11) C35 0.0506(17) 0.0404(16) 0.0399(16) -0.0026(13) -0.0255(14) 0.0037(13) C95 0.0489(17) 0.0336(15) 0.0486(17) 0.0000(13) -0.0223(14) 0.0043(13) C30 0.0389(14) 0.0273(12) 0.0260(12) -0.0076(10) 0.0002(10) 0.0083(11) C39 0.0449(16) 0.0406(16) 0.0283(14) 0.0019(12) 0.0011(12) -0.0098(13) C83 0.0419(15) 0.0509(17) 0.0261(13) -0.0165(12) 0.0084(11) -0.0067(13) C22 0.0322(14) 0.0405(16) 0.0550(18) -0.0159(14) -0.0164(13) 0.0069(12) C71 0.0350(15) 0.0364(15) 0.071(2) -0.0208(15) -0.0166(15) 0.0073(12) F2 0.148(3) 0.192(4) 0.095(2) -0.093(2) 0.080(2) -0.123(3) C23 0.0303(14) 0.0472(17) 0.0507(18) -0.0078(14) -0.0018(13) -0.0036(12) C40 0.0365(15) 0.062(2) 0.0259(13) -0.0125(13) 0.0081(11) -0.0123(14) C89 0.0395(16) 0.0525(18) 0.0411(16) -0.0152(14) -0.0181(13) 0.0065(13) C69 0.0387(16) 0.074(2) 0.0434(17) -0.0335(17) -0.0003(13) 0.0027(15) C70 0.0330(15) 0.059(2) 0.077(2) -0.0439(19) -0.0113(15) 0.0112(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle P2 Cu1 P1 112.37(2) N1 Cu1 P1 105.08(6) N1 Cu1 P2 111.47(6) N2 Cu1 P1 110.95(6) N2 Cu1 P2 129.56(6) N2 Cu1 N1 80.22(7) P3 Cu2 P4 112.52(3) N4 Cu2 P4 104.92(6) N4 Cu2 P3 115.62(6) N3 Cu2 P4 113.62(6) N3 Cu2 P3 124.18(6) N3 Cu2 N4 80.34(8) C85 P4 Cu2 110.76(8) C80 P4 Cu2 111.77(8) C80 P4 C85 104.78(11) C80 P4 C91 103.35(11) C91 P4 Cu2 121.01(8) C91 P4 C85 103.69(11) C61 P3 Cu2 117.23(8) C61 P3 C73 101.55(11) C73 P3 Cu2 113.23(8) C67 P3 Cu2 114.52(8) C67 P3 C61 104.12(11) C67 P3 C73 104.59(11) C43 P1 Cu1 112.90(8) C43 P1 C37 103.17(10) C43 P1 C32 107.31(11) C37 P1 Cu1 117.63(8) C37 P1 C32 101.20(11) C32 P1 Cu1 113.35(8) C13 P2 Cu1 108.59(7) C13 P2 C25 104.43(10) C19 P2 Cu1 121.85(8) C19 P2 C13 103.40(11) C19 P2 C25 104.30(11) C25 P2 Cu1 112.65(8) F6 P5 F3 178.44(12) F1 P5 F3 90.96(11) F1 P5 F6 88.94(12) F1 P5 F4 177.9(2) F5 P5 F3 90.93(13) F5 P5 F6 90.63(14) F5 P5 F1 89.0(2) F5 P5 F4 88.9(2) F4 P5 F3 89.12(11) F4 P5 F6 91.04(12) F2 P5 F3 88.18(14) F2 P5 F6 90.26(14) F2 P5 F1 92.1(2) F2 P5 F5 178.60(19) F2 P5 F4 90.0(3) F7 P6 F10 178.93(11) F8 P6 F10 89.31(11) F8 P6 F7 90.19(12) F12 P6 F10 90.83(13) F12 P6 F7 88.21(13) F12 P6 F8 88.30(18) F11 P6 F10 90.36(13) F11 P6 F7 90.14(13) F11 P6 F8 179.57(18) F11 P6 F12 92.0(2) F11 P6 F9 89.1(2) F9 P6 F10 89.38(12) F9 P6 F7 91.58(13) F9 P6 F8 90.6(2) F9 P6 F12 178.9(2) C26 O1 C31 117.93(18) C79 O2 C74 118.12(18) C5 N1 Cu1 112.24(14) C1 N1 Cu1 128.97(16) C1 N1 C5 118.33(19) C6 N2 Cu1 112.79(15) C10 N2 Cu1 129.27(16) C10 N2 C6 117.61(19) C54 N4 Cu2 111.93(15) C60 N4 Cu2 128.81(17) C60 N4 C54 118.1(2) C53 N3 Cu2 112.71(14) C49 N3 Cu2 129.04(16) C49 N3 C53 117.82(19) C5 C4 C12 118.7(2) C3 C4 C5 115.7(2) C3 C4 C12 125.6(2) N4 C54 C53 117.0(2) N4 C54 C55 123.2(2) C55 C54 C53 119.7(2) C53 C52 C57 119.1(2) C53 C52 C51 115.9(2) C51 C52 C57 125.0(2) N3 C53 C54 116.90(19) N3 C53 C52 123.4(2) C52 C53 C54 119.7(2) N2 C6 C7 123.6(2) N2 C6 C5 116.74(19) C7 C6 C5 119.6(2) C6 C7 C8 116.2(2) C6 C7 C11 118.9(2) C8 C7 C11 124.9(2) N1 C5 C4 123.4(2) N1 C5 C6 116.80(19) C4 C5 C6 119.8(2) C62 C61 P3 123.2(2) C66 C61 P3 117.51(19) C66 C61 C62 119.3(2) C52 C57 H57 119.5 C56 C57 C52 121.0(2) C56 C57 H57 119.5 C74 C73 P3 120.75(18) C74 C73 C78 116.6(2) C78 C73 P3 122.47(19) C54 C55 C56 118.7(2) C58 C55 C54 115.8(2) C58 C55 C56 125.4(2) C52 C51 Br3 119.29(18) C50 C51 Br3 119.69(18) C50 C51 C52 121.0(2) C57 C56 C55 121.6(2) C57 C56 H56 119.2 C55 C56 H56 119.2 C86 C85 P4 116.76(18) C90 C85 P4 124.53(19) C90 C85 C86 118.6(2) C14 C13 P2 116.59(17) C14 C13 C18 118.9(2) C18 C13 P2 124.34(18) N3 C49 H49 118.4 N3 C49 C50 123.3(2) C50 C49 H49 118.4 O2 C74 C73 119.4(2) C75 C74 O2 118.0(2) C75 C74 C73 122.4(2) C4 C3 Br1 121.06(17) C2 C3 Br1 117.78(17) C2 C3 C4 121.2(2) C43 C44 H44 120.1 C45 C44 H44 120.1 C45 C44 C43 119.9(2) C7 C8 Br2 120.58(17) C9 C8 Br2 118.97(17) C9 C8 C7 120.4(2) N2 C10 H10 118.2 N2 C10 C9 123.5(2) C9 C10 H10 118.2 C13 C14 H14 119.6 C15 C14 C13 120.7(2) C15 C14 H14 119.6 C7 C11 H11 119.2 C12 C11 C7 121.5(2) C12 C11 H11 119.2 C51 C50 C49 118.6(2) C51 C50 H50 120.7 C49 C50 H50 120.7 C58 C59 H59 120.9 C58 C59 C60 118.3(2) C60 C59 H59 120.9 C55 C58 Br4 119.57(18) C59 C58 Br4 119.08(18) C59 C58 C55 121.3(2) N4 C60 C59 123.2(2) N4 C60 H60 118.4 C59 C60 H60 118.4 C44 C43 P1 123.90(18) C44 C43 C48 119.6(2) C48 C43 P1 116.46(18) C81 C80 P4 123.85(19) C81 C80 C79 118.1(2) C79 C80 P4 117.75(18) C4 C12 H12 119.3 C11 C12 C4 121.4(2) C11 C12 H12 119.3 C19 C20 H20 119.6 C21 C20 H20 119.6 C21 C20 C19 120.8(2) O1 C31 C32 119.2(2) C36 C31 O1 118.2(2) C36 C31 C32 122.4(2) C61 C62 H62 119.8 C63 C62 C61 120.4(3) C63 C62 H62 119.8 C38 C37 P1 123.17(19) C38 C37 C42 119.1(2) C42 C37 P1 117.76(19) C37 C38 H38 120.0 C37 C38 C39 120.1(3) C39 C38 H38 120.0 C91 C92 H92 119.9 C93 C92 H92 119.9 C93 C92 C91 120.1(2) C92 C91 P4 122.78(19) C96 C91 P4 118.16(19) C96 C91 C92 119.0(2) C3 C2 H2 120.7 C3 C2 C1 118.5(2) C1 C2 H2 120.7 C85 C86 H86 119.5 C87 C86 C85 121.1(2) C87 C86 H86 119.5 C68 C67 P3 123.7(2) C68 C67 C72 119.5(2) C72 C67 P3 116.73(19) C8 C9 C10 118.6(2) C8 C9 H9 120.7 C10 C9 H9 120.7 O1 C26 C25 115.5(2) C27 C26 O1 122.2(2) C27 C26 C25 122.2(2) C20 C19 P2 118.71(19) C20 C19 C24 118.9(2) C24 C19 P2 122.41(19) C61 C66 H66 120.0 C61 C66 C65 120.1(2) C65 C66 H66 120.0 C80 C81 H81 119.6 C80 C81 C82 120.8(2) C82 C81 H81 119.6 C37 C42 H42 119.9 C41 C42 C37 120.3(3) C41 C42 H42 119.9 C85 C90 H90 120.0 C89 C90 C85 120.1(2) C89 C90 H90 120.0 C31 C32 P1 119.92(18) C33 C32 P1 122.74(18) C33 C32 C31 116.8(2) C44 C45 H45 120.0 C46 C45 C44 120.0(2) C46 C45 H45 120.0 C14 C15 H15 120.0 C14 C15 C16 120.0(2) C16 C15 H15 120.0 C26 C25 P2 117.88(18) C26 C25 C30 117.9(2) C30 C25 P2 124.1(2) C86 C87 H87 120.2 C86 C87 C88 119.6(2) C88 C87 H87 120.2 C43 C48 H48 119.8 C47 C48 C43 120.4(2) C47 C48 H48 119.8 O2 C79 C80 115.4(2) C84 C79 O2 122.8(2) C84 C79 C80 121.8(2) C15 C16 H16 120.1 C17 C16 C15 119.8(2) C17 C16 H16 120.1 C13 C18 H18 119.9 C17 C18 C13 120.2(2) C17 C18 H18 119.9 C67 C68 H68 120.3 C67 C68 C69 119.4(3) C69 C68 H68 120.3 N1 C1 C2 122.9(2) N1 C1 H1 118.6 C2 C1 H1 118.6 C66 C65 H65 120.1 C64 C65 C66 119.8(3) C64 C65 H65 120.1 C74 C75 H75 120.4 C74 C75 C76 119.1(3) C76 C75 H75 120.4 C19 C24 H24 119.8 C23 C24 C19 120.3(3) C23 C24 H24 119.8 C42 C41 H41 119.9 C40 C41 C42 120.2(3) C40 C41 H41 119.9 C73 C78 H78 119.2 C77 C78 C73 121.5(3) C77 C78 H78 119.2 C67 C72 H72 119.9 C71 C72 C67 120.1(3) C71 C72 H72 119.9 C93 C94 H94 120.0 C95 C94 H94 120.0 C95 C94 C93 120.1(3) C20 C21 H21 120.1 C22 C21 C20 119.8(3) C22 C21 H21 120.1 C28 C29 H29 119.8 C28 C29 C30 120.4(3) C30 C29 H29 119.8 C91 C96 H96 119.8 C91 C96 C95 120.4(3) C95 C96 H96 119.8 C62 C63 H63 120.0 C64 C63 C62 119.9(3) C64 C63 H63 120.0 C16 C17 C18 120.3(2) C16 C17 H17 119.8 C18 C17 H17 119.8 C81 C82 H82 120.1 C83 C82 C81 119.8(3) C83 C82 H82 120.1 C65 C64 H64 119.8 C63 C64 C65 120.5(3) C63 C64 H64 119.8 C26 C27 H27 120.7 C28 C27 C26 118.7(3) C28 C27 H27 120.7 C32 C33 H33 119.3 C34 C33 C32 121.5(2) C34 C33 H33 119.3 C92 C93 H93 119.8 C94 C93 C92 120.4(3) C94 C93 H93 119.8 C79 C84 H84 120.6 C79 C84 C83 118.9(2) C83 C84 H84 120.6 C31 C36 H36 120.3 C31 C36 C35 119.5(2) C35 C36 H36 120.3 C75 C76 H76 120.0 C77 C76 C75 119.9(2) C77 C76 H76 120.0 C87 C88 H88 120.0 C89 C88 C87 120.1(3) C89 C88 H88 120.0 C45 C46 H46 119.8 C45 C46 C47 120.5(2) C47 C46 H46 119.8 C29 C28 C27 120.5(2) C29 C28 H28 119.8 C27 C28 H28 119.8 C78 C77 H77 119.8 C76 C77 C78 120.4(3) C76 C77 H77 119.8 C48 C47 C46 119.6(2) C48 C47 H47 120.2 C46 C47 H47 120.2 C33 C34 H34 120.0 C33 C34 C35 120.0(3) C35 C34 H34 120.0 C36 C35 C34 119.8(3) C36 C35 H35 120.1 C34 C35 H35 120.1 C94 C95 C96 120.0(3) C94 C95 H95 120.0 C96 C95 H95 120.0 C25 C30 H30 119.9 C29 C30 C25 120.3(3) C29 C30 H30 119.9 C38 C39 H39 119.7 C40 C39 C38 120.6(3) C40 C39 H39 119.7 C82 C83 C84 120.7(2) C82 C83 H83 119.7 C84 C83 H83 119.7 C21 C22 H22 119.9 C21 C22 C23 120.1(3) C23 C22 H22 119.9 C72 C71 H71 120.0 C70 C71 C72 120.0(3) C70 C71 H71 120.0 C24 C23 H23 119.9 C22 C23 C24 120.1(3) C22 C23 H23 119.9 C41 C40 H40 120.1 C39 C40 C41 119.7(3) C39 C40 H40 120.1 C90 C89 H89 119.7 C88 C89 C90 120.5(3) C88 C89 H89 119.7 C68 C69 H69 119.7 C70 C69 C68 120.6(3) C70 C69 H69 119.7 C71 C70 H70 119.8 C69 C70 C71 120.3(3) C69 C70 H70 119.8 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Br2 C8 1.886(2) Br1 C3 1.891(2) Br4 C58 1.893(2) Br3 C51 1.894(2) Cu1 P1 2.2622(7) Cu1 P2 2.2377(7) Cu1 N1 2.0797(19) Cu1 N2 2.0607(19) Cu2 P4 2.2694(7) Cu2 P3 2.2370(7) Cu2 N4 2.088(2) Cu2 N3 2.0683(19) P4 C85 1.827(2) P4 C80 1.823(2) P4 C91 1.826(2) P3 C61 1.826(2) P3 C73 1.839(2) P3 C67 1.825(3) P1 C43 1.816(2) P1 C37 1.831(2) P1 C32 1.838(2) P2 C13 1.826(2) P2 C19 1.821(3) P2 C25 1.828(2) P5 F3 1.5980(16) P5 F6 1.5845(18) P5 F1 1.558(2) P5 F5 1.550(2) P5 F4 1.567(2) P5 F2 1.546(2) P6 F10 1.5926(16) P6 F7 1.5909(17) P6 F8 1.578(2) P6 F12 1.569(2) P6 F11 1.555(2) P6 F9 1.567(2) O1 C31 1.398(3) O1 C26 1.391(3) O2 C74 1.395(3) O2 C79 1.390(3) N1 C5 1.355(3) N1 C1 1.330(3) N2 C6 1.360(3) N2 C10 1.329(3) N4 C54 1.363(3) N4 C60 1.323(3) N3 C53 1.365(3) N3 C49 1.326(3) C4 C5 1.415(3) C4 C3 1.409(3) C4 C12 1.435(3) C54 C53 1.443(3) C54 C55 1.414(3) C52 C53 1.411(3) C52 C57 1.431(3) C52 C51 1.412(3) C6 C7 1.413(3) C6 C5 1.444(3) C7 C8 1.415(3) C7 C11 1.431(3) C61 C62 1.399(4) C61 C66 1.391(4) C57 H57 0.9500 C57 C56 1.354(3) C73 C74 1.397(3) C73 C78 1.398(4) C55 C56 1.431(3) C55 C58 1.405(3) C51 C50 1.364(4) C56 H56 0.9500 C85 C86 1.398(3) C85 C90 1.392(3) C13 C14 1.390(3) C13 C18 1.397(3) C49 H49 0.9500 C49 C50 1.401(3) C74 C75 1.387(3) C3 C2 1.367(3) C44 H44 0.9500 C44 C43 1.391(3) C44 C45 1.390(4) C8 C9 1.370(3) C10 H10 0.9500 C10 C9 1.403(3) C14 H14 0.9500 C14 C15 1.382(3) C11 H11 0.9500 C11 C12 1.352(3) C50 H50 0.9500 C59 H59 0.9500 C59 C58 1.366(4) C59 C60 1.402(4) C60 H60 0.9500 C43 C48 1.397(3) C80 C81 1.388(4) C80 C79 1.399(3) C12 H12 0.9500 C20 H20 0.9500 C20 C19 1.391(3) C20 C21 1.391(4) C31 C32 1.399(3) C31 C36 1.377(4) C62 H62 0.9500 C62 C63 1.383(4) C37 C38 1.387(3) C37 C42 1.400(3) C38 H38 0.9500 C38 C39 1.394(4) C92 H92 0.9500 C92 C91 1.392(4) C92 C93 1.389(4) C91 C96 1.390(4) C2 H2 0.9500 C2 C1 1.398(3) C86 H86 0.9500 C86 C87 1.379(4) C67 C68 1.392(4) C67 C72 1.393(4) C9 H9 0.9500 C26 C25 1.394(4) C26 C27 1.386(3) C19 C24 1.402(4) C66 H66 0.9500 C66 C65 1.393(4) C81 H81 0.9500 C81 C82 1.391(4) C42 H42 0.9500 C42 C41 1.388(4) C90 H90 0.9500 C90 C89 1.386(4) C32 C33 1.398(3) C45 H45 0.9500 C45 C46 1.386(4) C15 H15 0.9500 C15 C16 1.388(4) C25 C30 1.398(4) C87 H87 0.9500 C87 C88 1.384(4) C48 H48 0.9500 C48 C47 1.386(4) C79 C84 1.383(3) C16 H16 0.9500 C16 C17 1.379(4) C18 H18 0.9500 C18 C17 1.388(4) C68 H68 0.9500 C68 C69 1.397(4) C1 H1 0.9500 C65 H65 0.9500 C65 C64 1.384(4) C75 H75 0.9500 C75 C76 1.388(4) C24 H24 0.9500 C24 C23 1.388(4) C41 H41 0.9500 C41 C40 1.385(5) C78 H78 0.9500 C78 C77 1.386(4) C72 H72 0.9500 C72 C71 1.391(4) C94 H94 0.9500 C94 C93 1.379(4) C94 C95 1.376(4) C21 H21 0.9500 C21 C22 1.387(4) C29 H29 0.9500 C29 C28 1.382(5) C29 C30 1.390(4) C96 H96 0.9500 C96 C95 1.395(4) C63 H63 0.9500 C63 C64 1.382(4) C17 H17 0.9500 C82 H82 0.9500 C82 C83 1.386(4) C64 H64 0.9500 C27 H27 0.9500 C27 C28 1.384(4) C33 H33 0.9500 C33 C34 1.386(4) C93 H93 0.9500 C84 H84 0.9500 C84 C83 1.386(4) C36 H36 0.9500 C36 C35 1.386(4) C76 H76 0.9500 C76 C77 1.374(4) C88 H88 0.9500 C88 C89 1.380(4) C46 H46 0.9500 C46 C47 1.388(4) C28 H28 0.9500 C77 H77 0.9500 C47 H47 0.9500 C34 H34 0.9500 C34 C35 1.388(4) C35 H35 0.9500 C95 H95 0.9500 C30 H30 0.9500 C39 H39 0.9500 C39 C40 1.377(5) C83 H83 0.9500 C22 H22 0.9500 C22 C23 1.387(4) C71 H71 0.9500 C71 C70 1.376(5) C23 H23 0.9500 C40 H40 0.9500 C89 H89 0.9500 C69 H69 0.9500 C69 C70 1.372(5) C70 H70 0.9500 loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.500 0.000 0.000 622.6 184.4 '2 CH2Cl2' 2 0.438 0.531 0.713 7.3 0.0 ? 3 0.562 0.469 0.287 7.3 0.0 ?