#------------------------------------------------------------------------------
#$Date: 2020-02-08 12:30:02 +0200 (Sat, 08 Feb 2020) $
#$Revision: 247986 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/55/72/1557272.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1557272
loop_
_publ_author_name
'Fu, Yifan'
'Zhao, Weimin'
_publ_section_title
;
Polyesterified Sesquiterpenoids from the Seeds of Celastrus
paniculatus as Lifespan-Extending Agents for the Nematode
Caenorhabditis elegans.
;
_journal_name_full 'Journal of natural products'
_journal_paper_doi 10.1021/acs.jnatprod.9b01199
_journal_year 2020
_chemical_absolute_configuration rmad
_chemical_formula_moiety 'C35 H40 O12'
_chemical_formula_sum 'C35 H40 O12'
_chemical_formula_weight 652.67
_space_group_crystal_system triclinic
_space_group_IT_number 1
_space_group_name_Hall 'P 1'
_space_group_name_H-M_alt 'P 1'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary dual
_audit_creation_date 2019-02-26
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_cell_angle_alpha 100.1590(10)
_cell_angle_beta 99.8180(10)
_cell_angle_gamma 90.9320(10)
_cell_formula_units_Z 1
_cell_length_a 8.5050(3)
_cell_length_b 9.1711(4)
_cell_length_c 10.7701(4)
_cell_measurement_reflns_used 9605
_cell_measurement_temperature 100
_cell_measurement_theta_max 74.364
_cell_measurement_theta_min 7.045
_cell_volume 813.86(5)
_computing_cell_refinement 'SAINT V8.38A (?, 2016)'
_computing_data_reduction 'SAINT V8.38A (?, 2016)'
_computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material 'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement 'ShelXL (Sheldrick, 2015)'
_computing_structure_solution 'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature 100.0
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type 'Bruker APEX-II CCD'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type CuK\a
_diffrn_radiation_wavelength 1.54178
_diffrn_reflns_av_R_equivalents 0.0471
_diffrn_reflns_av_unetI/netI 0.0473
_diffrn_reflns_Laue_measured_fraction_full 0.987
_diffrn_reflns_Laue_measured_fraction_max 0.984
_diffrn_reflns_limit_h_max 10
_diffrn_reflns_limit_h_min -10
_diffrn_reflns_limit_k_max 11
_diffrn_reflns_limit_k_min -11
_diffrn_reflns_limit_l_max 12
_diffrn_reflns_limit_l_min -13
_diffrn_reflns_number 19295
_diffrn_reflns_point_group_measured_fraction_full 0.949
_diffrn_reflns_point_group_measured_fraction_max 0.928
_diffrn_reflns_theta_full 67.679
_diffrn_reflns_theta_max 74.434
_diffrn_reflns_theta_min 7.044
_diffrn_standards_number 0
_exptl_absorpt_coefficient_mu 0.838
_exptl_absorpt_correction_T_max 0.7538
_exptl_absorpt_correction_T_min 0.6122
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1302 before and 0.0849 after correction. The Ratio of minimum to maximum transmission is 0.8122. The \l/2 correction factor is Not present.'
_exptl_crystal_colour colourless
_exptl_crystal_colour_primary colourless
_exptl_crystal_density_diffrn 1.332
_exptl_crystal_description block
_exptl_crystal_F_000 346
_exptl_crystal_size_max 0.19
_exptl_crystal_size_mid 0.15
_exptl_crystal_size_min 0.12
_refine_diff_density_max 0.365
_refine_diff_density_min -0.289
_refine_diff_density_rms 0.048
_refine_ls_abs_structure_details
;
Flack x determined using 2824 quotients [(I+)-(I-)]/[(I+)+(I-)]
(Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack -0.01(7)
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.064
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 430
_refine_ls_number_reflns 6196
_refine_ls_number_restraints 3
_refine_ls_restrained_S_all 1.064
_refine_ls_R_factor_all 0.0409
_refine_ls_R_factor_gt 0.0407
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0592P)^2^+0.2235P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1084
_refine_ls_wR_factor_ref 0.1087
_reflns_Friedel_coverage 0.887
_reflns_Friedel_fraction_full 0.911
_reflns_Friedel_fraction_max 0.873
_reflns_number_gt 6152
_reflns_number_total 6196
_reflns_threshold_expression 'I > 2\s(I)'
_iucr_refine_instructions_details
;
TITL 22019164_0m_a.res in P1
22019164_0m.res
created by SHELXL-2018/3 at 09:18:29 on 26-Feb-2019
REM Old TITL 22019164_0m in P1
REM SHELXT solution in P1
REM R1 0.099, Rweak 0.038, Alpha 0.000, Orientation as input
REM Flack x = 0.069 ( 0.068 ) from Parsons' quotients
REM Formula found by SHELXT: C35 O12
CELL 1.54178 8.505 9.1711 10.7701 100.159 99.818 90.932
ZERR 1 0.0003 0.0004 0.0004 0.001 0.001 0.001
LATT -1
SFAC C H O
UNIT 35 40 12
L.S. 20
PLAN 20
SIZE 0.19 0.15 0.12
TEMP -173.15
BOND $H
list 4
fmap 2
ACTA
REM
REM
REM
WGHT 0.059200 0.223500
FVAR 2.19872
O3 3 0.599962 0.146238 0.391231 11.00000 0.01874 0.01820 =
0.02623 -0.00069 0.00674 -0.00131
O6 3 0.707382 0.619082 0.571159 11.00000 0.02787 0.01746 =
0.02413 0.00077 0.00816 -0.00308
O7 3 0.554312 0.576267 0.290097 11.00000 0.02622 0.01956 =
0.02129 0.00482 0.00617 0.00092
O11 3 0.842509 0.426218 0.230091 11.00000 0.02865 0.02279 =
0.02459 0.00314 0.01273 -0.00137
O4 3 0.355374 0.545492 0.460988 11.00000 0.02174 0.02045 =
0.02426 0.00180 0.00571 0.00476
O2 3 0.538068 0.242406 0.660836 11.00000 0.02844 0.02181 =
0.02297 0.00606 0.01062 0.00208
O9 3 0.789926 0.838125 0.530844 11.00000 0.03626 0.02157 =
0.02540 0.00380 0.00793 -0.00181
O5 3 0.186378 0.631348 0.306128 11.00000 0.03166 0.02924 =
0.02717 0.00700 0.00470 0.00496
O10 3 0.723683 0.942727 0.170958 11.00000 0.04962 0.02986 =
0.03649 0.01000 0.01710 0.00047
O12 3 0.849770 0.238301 0.065669 11.00000 0.05582 0.02620 =
0.03388 -0.00126 0.02105 0.00140
O8 3 0.455195 0.486594 0.081780 11.00000 0.06913 0.03418 =
0.02660 0.00345 -0.00522 -0.00850
O1 3 0.373969 0.405724 0.746540 11.00000 0.07298 0.04620 =
0.04034 0.01956 0.03195 0.03391
C6 1 0.538230 0.326592 0.558706 11.00000 0.02328 0.02023 =
0.02089 0.00551 0.00702 -0.00111
AFIX 13
H6 2 0.550603 0.435532 0.593306 11.00000 -1.20000
AFIX 0
C15 1 0.792873 0.541399 0.476852 11.00000 0.02047 0.01993 =
0.02514 0.00073 0.00679 0.00016
AFIX 23
H15A 2 0.899068 0.517477 0.520131 11.00000 -1.20000
H15B 2 0.809730 0.606750 0.415823 11.00000 -1.20000
AFIX 0
C16 1 0.719683 0.769157 0.591567 11.00000 0.02536 0.01761 =
0.02263 0.00014 0.00174 -0.00136
C25 1 0.208826 0.699531 0.644995 11.00000 0.02059 0.02198 =
0.03216 0.00387 0.00773 -0.00120
AFIX 43
H25 2 0.274179 0.618911 0.659005 11.00000 -1.20000
AFIX 0
C9 1 0.541117 0.430678 0.321267 11.00000 0.02394 0.01604 =
0.02376 0.00225 0.00905 0.00134
AFIX 13
H9 2 0.528531 0.358963 0.238316 11.00000 -1.20000
AFIX 0
C5 1 0.670396 0.275733 0.482999 11.00000 0.01953 0.01701 =
0.02127 -0.00005 0.00567 -0.00210
C24 1 0.179182 0.725846 0.525071 11.00000 0.02135 0.01952 =
0.03360 0.00487 0.00759 0.00052
AFIX 43
H24 2 0.117559 0.807948 0.508362 11.00000 -1.20000
AFIX 0
C8 1 0.385794 0.414501 0.374141 11.00000 0.02188 0.01953 =
0.02224 0.00079 0.00661 0.00157
AFIX 13
H8 2 0.294035 0.392726 0.300942 11.00000 -1.20000
AFIX 0
C23 1 0.237678 0.633445 0.418166 11.00000 0.01930 0.02012 =
0.03183 0.00717 0.00628 0.00012
C10 1 0.702287 0.397658 0.402724 11.00000 0.02036 0.01734 =
0.02213 0.00124 0.00759 -0.00168
C33 1 0.583740 0.726730 0.141389 11.00000 0.03119 0.02600 =
0.02595 0.00828 0.01036 0.00531
C18 1 0.863483 0.368990 0.109915 11.00000 0.02882 0.02703 =
0.02496 0.00067 0.01226 0.00176
C32 1 0.521743 0.585092 0.164253 11.00000 0.03239 0.02886 =
0.02101 0.00536 0.00404 0.00400
C1 1 0.809377 0.321598 0.310097 11.00000 0.02107 0.01998 =
0.02354 0.00433 0.00865 0.00040
AFIX 13
H1 2 0.749308 0.232361 0.254314 11.00000 -1.20000
AFIX 0
C7 1 0.391519 0.289647 0.452872 11.00000 0.02087 0.01898 =
0.02529 0.00224 0.00672 -0.00117
AFIX 13
H7 2 0.291832 0.283058 0.489591 11.00000 -1.20000
AFIX 0
C4 1 0.822262 0.222844 0.558970 11.00000 0.02247 0.02068 =
0.02651 0.00407 0.00601 0.00028
AFIX 13
H4 2 0.787202 0.134464 0.591791 11.00000 -1.20000
AFIX 0
C34 1 0.676605 0.832938 0.227530 11.00000 0.03990 0.02260 =
0.03412 0.00942 0.01535 0.00241
AFIX 43
H34 2 0.705015 0.830566 0.316344 11.00000 -1.20000
AFIX 0
C12 1 0.378487 0.008812 0.438372 11.00000 0.02733 0.02168 =
0.03827 0.00340 0.01207 -0.00158
AFIX 137
H12A 2 0.416956 -0.083562 0.395512 11.00000 -1.50000
H12B 2 0.261824 0.000661 0.428626 11.00000 -1.50000
H12C 2 0.425568 0.026692 0.529650 11.00000 -1.50000
AFIX 0
C2 1 0.966438 0.273580 0.379176 11.00000 0.02037 0.02539 =
0.03164 0.00432 0.01047 0.00144
AFIX 23
H2A 2 1.029835 0.361971 0.430591 11.00000 -1.20000
H2B 2 1.029029 0.224924 0.315301 11.00000 -1.20000
AFIX 0
C26 1 0.151713 0.781222 0.757181 11.00000 0.02401 0.02327 =
0.03055 0.00014 0.00884 -0.00361
C11 1 0.427035 0.137770 0.378031 11.00000 0.02001 0.02100 =
0.02740 0.00152 0.00755 -0.00147
C27 1 0.082556 0.919286 0.758877 11.00000 0.02984 0.02428 =
0.03247 0.00007 0.00539 0.00229
AFIX 43
H27 2 0.071029 0.963837 0.684809 11.00000 -1.20000
AFIX 0
C21 1 0.450843 0.295881 0.750289 11.00000 0.03447 0.02788 =
0.02532 0.00469 0.01123 0.00678
C31 1 0.170452 0.720071 0.868822 11.00000 0.03091 0.02623 =
0.03204 0.00244 0.00949 0.00002
AFIX 43
H31 2 0.218082 0.627176 0.869554 11.00000 -1.20000
AFIX 0
C3 1 0.935713 0.165835 0.467263 11.00000 0.02163 0.02394 =
0.03101 0.00586 0.00753 0.00389
AFIX 23
H3A 2 0.890287 0.070592 0.413724 11.00000 -1.20000
H3B 2 1.038999 0.146156 0.518109 11.00000 -1.20000
AFIX 0
C36 1 0.655739 0.903901 0.043891 11.00000 0.03905 0.03574 =
0.04630 0.02189 0.02004 0.01049
AFIX 43
H36 2 0.667469 0.961312 -0.019552 11.00000 -1.20000
AFIX 0
C13 1 0.354120 0.102397 0.235374 11.00000 0.02574 0.02384 =
0.03036 -0.00382 0.00362 -0.00203
AFIX 137
H13A 2 0.391128 0.178377 0.192021 11.00000 -1.50000
H13B 2 0.237362 0.101042 0.225295 11.00000 -1.50000
H13C 2 0.387188 0.005125 0.197474 11.00000 -1.50000
AFIX 0
C20 1 0.906579 0.332649 0.677573 11.00000 0.02874 0.03150 =
0.02746 0.00500 0.00179 -0.00028
AFIX 137
H20A 2 0.984993 0.395913 0.652312 11.00000 -1.50000
H20B 2 0.961063 0.277483 0.741098 11.00000 -1.50000
H20C 2 0.827352 0.394444 0.714802 11.00000 -1.50000
AFIX 0
C28 1 0.030903 0.991072 0.868303 11.00000 0.03162 0.03019 =
0.03460 -0.00442 0.00618 0.00293
AFIX 43
H28 2 -0.017595 1.083639 0.868147 11.00000 -1.20000
AFIX 0
C17 1 0.638734 0.834039 0.699089 11.00000 0.03587 0.02842 =
0.03132 -0.00380 0.01251 -0.00073
AFIX 137
H17A 2 0.528020 0.794194 0.682377 11.00000 -1.50000
H17B 2 0.639800 0.942131 0.706656 11.00000 -1.50000
H17C 2 0.695035 0.808552 0.779096 11.00000 -1.50000
AFIX 0
C22 1 0.457712 0.201780 0.851112 11.00000 0.04366 0.02910 =
0.02903 0.00941 0.01600 0.00628
AFIX 137
H22A 2 0.406287 0.104032 0.812796 11.00000 -1.50000
H22B 2 0.401870 0.249353 0.918826 11.00000 -1.50000
H22C 2 0.569478 0.190308 0.887763 11.00000 -1.50000
AFIX 0
C30 1 0.120015 0.793869 0.979270 11.00000 0.03423 0.03434 =
0.03446 0.00443 0.00990 -0.00336
AFIX 43
H30 2 0.133968 0.751839 1.054743 11.00000 -1.20000
AFIX 0
C35 1 0.570664 0.774510 0.020787 11.00000 0.03637 0.04604 =
0.02642 0.01149 0.00715 0.00918
AFIX 43
H35 2 0.513356 0.724729 -0.059435 11.00000 -1.20000
AFIX 0
C29 1 0.049601 0.928666 0.977617 11.00000 0.02792 0.03672 =
0.03248 -0.00658 0.01107 0.00042
AFIX 43
H29 2 0.013867 0.978687 1.051999 11.00000 -1.20000
AFIX 0
C19 1 0.906540 0.488019 0.041936 11.00000 0.05918 0.03419 =
0.03177 0.00587 0.02182 -0.00076
AFIX 137
H19A 2 0.809549 0.519521 -0.007578 11.00000 -1.50000
H19B 2 0.979593 0.449989 -0.016061 11.00000 -1.50000
H19C 2 0.958785 0.572798 0.104757 11.00000 -1.50000
AFIX 0
HKLF 4
REM 22019164_0m_a.res in P1
REM wR2 = 0.1087, GooF = S = 1.064, Restrained GooF = 1.064 for all data
REM R1 = 0.0407 for 6152 Fo > 4sig(Fo) and 0.0409 for all 6196 data
REM 430 parameters refined using 3 restraints
END
WGHT 0.0592 0.2235
REM Highest difference peak 0.365, deepest hole -0.289, 1-sigma level 0.048
Q1 1 0.6059 0.8411 -0.0193 11.00000 0.05 0.37
Q2 1 0.4662 0.4531 0.7850 11.00000 0.05 0.20
Q3 1 0.6963 0.6265 0.4344 11.00000 0.05 0.19
Q4 1 0.8064 0.8194 0.4001 11.00000 0.05 0.18
Q5 1 0.2027 0.6838 0.4726 11.00000 0.05 0.18
Q6 1 0.6614 0.5789 0.6810 11.00000 0.05 0.18
Q7 1 0.7722 0.6855 0.4994 11.00000 0.05 0.17
Q8 1 0.4408 0.5482 0.3545 11.00000 0.05 0.17
Q9 1 0.3838 0.1354 0.2945 11.00000 0.05 0.17
Q10 1 1.0865 0.4131 0.3853 11.00000 0.05 0.16
Q11 1 0.6563 0.8034 0.3974 11.00000 0.05 0.16
Q12 1 0.3710 0.4498 0.1789 11.00000 0.05 0.16
Q13 1 0.7506 0.1966 0.1592 11.00000 0.05 0.16
Q14 1 0.8766 0.5979 0.0832 11.00000 0.05 0.16
Q15 1 0.3925 0.6986 0.4255 11.00000 0.05 0.16
Q16 1 0.8189 0.9940 0.0822 11.00000 0.05 0.16
Q17 1 0.2134 0.9435 0.6786 11.00000 0.05 0.15
Q18 1 0.0561 0.7574 1.0775 11.00000 0.05 0.15
Q19 1 0.5879 1.0564 0.1886 11.00000 0.05 0.15
Q20 1 0.2864 0.7867 0.8245 11.00000 0.05 0.15
REM The information below was added by Olex2.
REM
REM R1 = 0.0407 for 6152 Fo > 4sig(Fo) and 0.0409 for all 19295 data
REM n/a parameters refined using n/a restraints
REM Highest difference peak 0.37, deepest hole -0.29
REM Mean Shift 0, Max Shift 0.000.
REM +++ Tabular Listing of Refinement Information +++
REM R1_all = 0.0409
REM R1_gt = 0.0407
REM wR_ref = 0.1087
REM GOOF = 1.064
REM Shift_max = 0.000
REM Shift_mean = 0
REM Reflections_all = 19295
REM Reflections_gt = 6152
REM Parameters = n/a
REM Hole = -0.29
REM Peak = 0.37
REM Flack = -0.01(7)
;
_cod_data_source_file np9b01199_si_002.cif
_cod_data_source_block 22019164_0m
_cod_database_code 1557272
_shelx_shelxl_version_number 2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max 0.906
_shelx_estimated_absorpt_t_min 0.857
_olex2_refinement_description
;
1. Fixed Uiso
At 1.2 times of:
All C(H) groups, All C(H,H) groups
At 1.5 times of:
All C(H,H,H) groups
2.a Ternary CH refined with riding coordinates:
C6(H6), C9(H9), C8(H8), C1(H1), C7(H7), C4(H4)
2.b Secondary CH2 refined with riding coordinates:
C15(H15A,H15B), C2(H2A,H2B), C3(H3A,H3B)
2.c Aromatic/amide H refined with riding coordinates:
C25(H25), C24(H24), C34(H34), C27(H27), C31(H31), C36(H36), C28(H28),
C30(H30), C35(H35), C29(H29)
2.d Idealised Me refined as rotating group:
C12(H12A,H12B,H12C), C13(H13A,H13B,H13C), C20(H20A,H20B,H20C), C17(H17A,H17B,
H17C), C22(H22A,H22B,H22C), C19(H19A,H19B,H19C)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
O3 O 0.6000(2) 0.14624(19) 0.39123(18) 0.0213(4) Uani 1 1 d .
O6 O 0.7074(2) 0.6191(2) 0.57116(18) 0.0231(4) Uani 1 1 d .
O7 O 0.5543(2) 0.57627(19) 0.29010(17) 0.0220(4) Uani 1 1 d .
O11 O 0.8425(2) 0.4262(2) 0.23009(19) 0.0246(4) Uani 1 1 d .
O4 O 0.3554(2) 0.5455(2) 0.46099(18) 0.0222(4) Uani 1 1 d .
O2 O 0.5381(2) 0.2424(2) 0.66084(18) 0.0234(4) Uani 1 1 d .
O9 O 0.7899(2) 0.8381(2) 0.53084(19) 0.0275(4) Uani 1 1 d .
O5 O 0.1864(2) 0.6313(2) 0.30613(19) 0.0291(4) Uani 1 1 d .
O10 O 0.7237(3) 0.9427(2) 0.1710(2) 0.0370(5) Uani 1 1 d .
O12 O 0.8498(3) 0.2383(2) 0.0657(2) 0.0379(5) Uani 1 1 d .
O8 O 0.4552(4) 0.4866(3) 0.0818(2) 0.0453(6) Uani 1 1 d .
O1 O 0.3740(4) 0.4057(3) 0.7465(3) 0.0488(7) Uani 1 1 d .
C6 C 0.5382(3) 0.3266(3) 0.5587(2) 0.0209(5) Uani 1 1 d .
H6 H 0.550603 0.435532 0.593306 0.025 Uiso 1 1 calc R
C15 C 0.7929(3) 0.5414(3) 0.4769(3) 0.0219(5) Uani 1 1 d .
H15A H 0.899068 0.517477 0.520131 0.026 Uiso 1 1 calc R
H15B H 0.809730 0.606750 0.415823 0.026 Uiso 1 1 calc R
C16 C 0.7197(3) 0.7692(3) 0.5916(3) 0.0226(5) Uani 1 1 d .
C25 C 0.2088(3) 0.6995(3) 0.6450(3) 0.0247(5) Uani 1 1 d .
H25 H 0.274179 0.618911 0.659005 0.030 Uiso 1 1 calc R
C9 C 0.5411(3) 0.4307(3) 0.3213(3) 0.0208(5) Uani 1 1 d .
H9 H 0.528531 0.358963 0.238316 0.025 Uiso 1 1 calc R
C5 C 0.6704(3) 0.2757(3) 0.4830(3) 0.0195(5) Uani 1 1 d .
C24 C 0.1792(3) 0.7258(3) 0.5251(3) 0.0245(5) Uani 1 1 d .
H24 H 0.117559 0.807948 0.508362 0.029 Uiso 1 1 calc R
C8 C 0.3858(3) 0.4145(3) 0.3741(3) 0.0213(5) Uani 1 1 d .
H8 H 0.294035 0.392726 0.300942 0.026 Uiso 1 1 calc R
C23 C 0.2377(3) 0.6334(3) 0.4182(3) 0.0232(5) Uani 1 1 d .
C10 C 0.7023(3) 0.3977(3) 0.4027(3) 0.0198(5) Uani 1 1 d .
C33 C 0.5837(3) 0.7267(3) 0.1414(3) 0.0266(6) Uani 1 1 d .
C18 C 0.8635(3) 0.3690(3) 0.1099(3) 0.0265(6) Uani 1 1 d .
C32 C 0.5217(3) 0.5851(3) 0.1643(3) 0.0274(6) Uani 1 1 d .
C1 C 0.8094(3) 0.3216(3) 0.3101(3) 0.0209(5) Uani 1 1 d .
H1 H 0.749308 0.232361 0.254314 0.025 Uiso 1 1 calc R
C7 C 0.3915(3) 0.2896(3) 0.4529(3) 0.0216(5) Uani 1 1 d .
H7 H 0.291832 0.283058 0.489591 0.026 Uiso 1 1 calc R
C4 C 0.8223(3) 0.2228(3) 0.5590(3) 0.0231(5) Uani 1 1 d .
H4 H 0.787202 0.134464 0.591791 0.028 Uiso 1 1 calc R
C34 C 0.6766(4) 0.8329(3) 0.2275(3) 0.0306(6) Uani 1 1 d .
H34 H 0.705015 0.830566 0.316344 0.037 Uiso 1 1 calc R
C12 C 0.3785(3) 0.0088(3) 0.4384(3) 0.0286(6) Uani 1 1 d .
H12A H 0.416956 -0.083562 0.395512 0.043 Uiso 1 1 calc GR
H12B H 0.261824 0.000661 0.428626 0.043 Uiso 1 1 calc GR
H12C H 0.425568 0.026692 0.529650 0.043 Uiso 1 1 calc GR
C2 C 0.9664(3) 0.2736(3) 0.3792(3) 0.0252(6) Uani 1 1 d .
H2A H 1.029835 0.361971 0.430591 0.030 Uiso 1 1 calc R
H2B H 1.029029 0.224924 0.315301 0.030 Uiso 1 1 calc R
C26 C 0.1517(3) 0.7812(3) 0.7572(3) 0.0261(6) Uani 1 1 d .
C11 C 0.4270(3) 0.1378(3) 0.3780(3) 0.0228(5) Uani 1 1 d .
C27 C 0.0826(3) 0.9193(3) 0.7589(3) 0.0295(6) Uani 1 1 d .
H27 H 0.071029 0.963837 0.684809 0.035 Uiso 1 1 calc R
C21 C 0.4508(4) 0.2959(3) 0.7503(3) 0.0285(6) Uani 1 1 d .
C31 C 0.1705(4) 0.7201(3) 0.8688(3) 0.0296(6) Uani 1 1 d .
H31 H 0.218082 0.627176 0.869554 0.036 Uiso 1 1 calc R
C3 C 0.9357(3) 0.1658(3) 0.4673(3) 0.0250(6) Uani 1 1 d .
H3A H 0.890287 0.070592 0.413724 0.030 Uiso 1 1 calc R
H3B H 1.038999 0.146156 0.518109 0.030 Uiso 1 1 calc R
C36 C 0.6557(4) 0.9039(4) 0.0439(4) 0.0370(7) Uani 1 1 d .
H36 H 0.667469 0.961312 -0.019552 0.044 Uiso 1 1 calc R
C13 C 0.3541(3) 0.1024(3) 0.2354(3) 0.0279(6) Uani 1 1 d .
H13A H 0.391128 0.178377 0.192021 0.042 Uiso 1 1 calc GR
H13B H 0.237362 0.101042 0.225295 0.042 Uiso 1 1 calc GR
H13C H 0.387188 0.005125 0.197474 0.042 Uiso 1 1 calc GR
C20 C 0.9066(4) 0.3326(3) 0.6776(3) 0.0297(6) Uani 1 1 d .
H20A H 0.984993 0.395913 0.652312 0.045 Uiso 1 1 calc GR
H20B H 0.961063 0.277483 0.741098 0.045 Uiso 1 1 calc GR
H20C H 0.827352 0.394444 0.714802 0.045 Uiso 1 1 calc GR
C28 C 0.0309(4) 0.9911(3) 0.8683(3) 0.0334(7) Uani 1 1 d .
H28 H -0.017595 1.083639 0.868147 0.040 Uiso 1 1 calc R
C17 C 0.6387(4) 0.8340(3) 0.6991(3) 0.0323(6) Uani 1 1 d .
H17A H 0.528020 0.794194 0.682377 0.048 Uiso 1 1 calc GR
H17B H 0.639800 0.942131 0.706656 0.048 Uiso 1 1 calc GR
H17C H 0.695035 0.808552 0.779096 0.048 Uiso 1 1 calc GR
C22 C 0.4577(4) 0.2018(3) 0.8511(3) 0.0322(6) Uani 1 1 d .
H22A H 0.406287 0.104032 0.812796 0.048 Uiso 1 1 calc GR
H22B H 0.401870 0.249353 0.918826 0.048 Uiso 1 1 calc GR
H22C H 0.569478 0.190308 0.887763 0.048 Uiso 1 1 calc GR
C30 C 0.1200(4) 0.7939(4) 0.9793(3) 0.0342(7) Uani 1 1 d .
H30 H 0.133968 0.751839 1.054743 0.041 Uiso 1 1 calc R
C35 C 0.5707(4) 0.7745(4) 0.0208(3) 0.0354(7) Uani 1 1 d .
H35 H 0.513356 0.724729 -0.059435 0.042 Uiso 1 1 calc R
C29 C 0.0496(4) 0.9287(4) 0.9776(3) 0.0333(6) Uani 1 1 d .
H29 H 0.013867 0.978687 1.051999 0.040 Uiso 1 1 calc R
C19 C 0.9065(5) 0.4880(4) 0.0419(3) 0.0401(8) Uani 1 1 d .
H19A H 0.809549 0.519521 -0.007578 0.060 Uiso 1 1 calc GR
H19B H 0.979593 0.449989 -0.016061 0.060 Uiso 1 1 calc GR
H19C H 0.958785 0.572798 0.104757 0.060 Uiso 1 1 calc GR
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
O3 0.0187(8) 0.0182(8) 0.0262(9) -0.0007(7) 0.0067(7) -0.0013(7)
O6 0.0279(9) 0.0175(8) 0.0241(10) 0.0008(7) 0.0082(8) -0.0031(7)
O7 0.0262(9) 0.0196(9) 0.0213(9) 0.0048(7) 0.0062(7) 0.0009(7)
O11 0.0286(9) 0.0228(9) 0.0246(9) 0.0031(7) 0.0127(8) -0.0014(7)
O4 0.0217(9) 0.0205(9) 0.0243(9) 0.0018(7) 0.0057(7) 0.0048(7)
O2 0.0284(9) 0.0218(9) 0.0230(9) 0.0061(7) 0.0106(7) 0.0021(7)
O9 0.0363(11) 0.0216(9) 0.0254(10) 0.0038(7) 0.0079(8) -0.0018(8)
O5 0.0317(10) 0.0292(10) 0.0272(11) 0.0070(8) 0.0047(8) 0.0050(8)
O10 0.0496(13) 0.0299(11) 0.0365(12) 0.0100(9) 0.0171(10) 0.0005(9)
O12 0.0558(14) 0.0262(11) 0.0339(11) -0.0013(9) 0.0210(10) 0.0014(10)
O8 0.0691(17) 0.0342(12) 0.0266(11) 0.0035(9) -0.0052(11) -0.0085(11)
O1 0.0730(18) 0.0462(14) 0.0403(14) 0.0196(11) 0.0319(13) 0.0339(13)
C6 0.0233(12) 0.0202(12) 0.0209(12) 0.0055(10) 0.0070(10) -0.0011(9)
C15 0.0205(11) 0.0199(12) 0.0251(13) 0.0007(10) 0.0068(10) 0.0002(9)
C16 0.0254(12) 0.0176(12) 0.0226(13) 0.0001(10) 0.0017(10) -0.0014(10)
C25 0.0206(12) 0.0220(12) 0.0322(15) 0.0039(10) 0.0077(10) -0.0012(9)
C9 0.0239(12) 0.0160(12) 0.0238(13) 0.0023(9) 0.0090(10) 0.0013(9)
C5 0.0195(11) 0.0170(11) 0.0213(12) 0.0000(9) 0.0057(9) -0.0021(9)
C24 0.0214(12) 0.0195(12) 0.0336(15) 0.0049(10) 0.0076(11) 0.0005(9)
C8 0.0219(12) 0.0195(12) 0.0222(12) 0.0008(9) 0.0066(10) 0.0016(9)
C23 0.0193(12) 0.0201(12) 0.0318(15) 0.0072(10) 0.0063(10) 0.0001(9)
C10 0.0204(11) 0.0173(11) 0.0221(12) 0.0012(9) 0.0076(10) -0.0017(9)
C33 0.0312(14) 0.0260(13) 0.0260(14) 0.0083(10) 0.0104(11) 0.0053(11)
C18 0.0288(13) 0.0270(14) 0.0250(13) 0.0007(11) 0.0123(11) 0.0018(11)
C32 0.0324(14) 0.0289(14) 0.0210(13) 0.0054(11) 0.0040(11) 0.0040(11)
C1 0.0211(12) 0.0200(12) 0.0235(13) 0.0043(10) 0.0087(10) 0.0004(9)
C7 0.0209(12) 0.0190(12) 0.0253(13) 0.0022(10) 0.0067(10) -0.0012(9)
C4 0.0225(12) 0.0207(12) 0.0265(13) 0.0041(10) 0.0060(10) 0.0003(10)
C34 0.0399(16) 0.0226(13) 0.0341(16) 0.0094(11) 0.0153(13) 0.0024(11)
C12 0.0273(14) 0.0217(13) 0.0383(16) 0.0034(11) 0.0121(12) -0.0016(10)
C2 0.0204(12) 0.0254(13) 0.0316(14) 0.0043(11) 0.0105(11) 0.0014(10)
C26 0.0240(12) 0.0233(13) 0.0306(15) 0.0001(11) 0.0088(11) -0.0036(10)
C11 0.0200(12) 0.0210(12) 0.0274(14) 0.0015(10) 0.0076(10) -0.0015(9)
C27 0.0298(14) 0.0243(14) 0.0325(15) 0.0001(11) 0.0054(12) 0.0023(11)
C21 0.0345(15) 0.0279(14) 0.0253(14) 0.0047(11) 0.0112(12) 0.0068(11)
C31 0.0309(14) 0.0262(14) 0.0320(15) 0.0024(12) 0.0095(12) 0.0000(11)
C3 0.0216(12) 0.0239(13) 0.0310(15) 0.0059(11) 0.0075(11) 0.0039(10)
C36 0.0390(16) 0.0357(16) 0.0463(19) 0.0219(14) 0.0200(14) 0.0105(13)
C13 0.0257(13) 0.0238(12) 0.0304(14) -0.0038(10) 0.0036(11) -0.0020(10)
C20 0.0287(13) 0.0315(14) 0.0275(14) 0.0050(11) 0.0018(11) -0.0003(11)
C28 0.0316(14) 0.0302(15) 0.0346(16) -0.0044(13) 0.0062(12) 0.0029(12)
C17 0.0359(15) 0.0284(15) 0.0313(16) -0.0038(12) 0.0125(13) -0.0007(12)
C22 0.0437(17) 0.0291(15) 0.0290(15) 0.0094(12) 0.0160(13) 0.0063(12)
C30 0.0342(15) 0.0343(15) 0.0345(16) 0.0044(13) 0.0099(13) -0.0034(12)
C35 0.0364(16) 0.0460(18) 0.0264(15) 0.0115(13) 0.0071(12) 0.0092(13)
C29 0.0279(14) 0.0367(16) 0.0325(15) -0.0066(12) 0.0111(12) 0.0004(12)
C19 0.059(2) 0.0342(17) 0.0318(16) 0.0059(13) 0.0218(15) -0.0008(15)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C5 O3 C11 111.68(18)
C16 O6 C15 116.7(2)
C32 O7 C9 116.6(2)
C18 O11 C1 117.0(2)
C23 O4 C8 118.0(2)
C21 O2 C6 115.8(2)
C34 O10 C36 105.4(2)
O2 C6 H6 111.1
O2 C6 C5 109.9(2)
O2 C6 C7 112.9(2)
C5 C6 H6 111.1
C7 C6 H6 111.1
C7 C6 C5 100.2(2)
O6 C15 H15A 109.2
O6 C15 H15B 109.2
O6 C15 C10 111.9(2)
H15A C15 H15B 107.9
C10 C15 H15A 109.2
C10 C15 H15B 109.2
O6 C16 C17 110.8(2)
O9 C16 O6 123.4(2)
O9 C16 C17 125.7(2)
C24 C25 H25 116.4
C24 C25 C26 127.3(3)
C26 C25 H25 116.4
O7 C9 H9 106.3
O7 C9 C8 109.4(2)
O7 C9 C10 109.14(19)
C8 C9 H9 106.3
C8 C9 C10 118.6(2)
C10 C9 H9 106.3
O3 C5 C6 104.54(19)
O3 C5 C10 106.48(19)
O3 C5 C4 105.51(19)
C6 C5 C10 108.45(19)
C6 C5 C4 116.5(2)
C4 C5 C10 114.4(2)
C25 C24 H24 118.5
C25 C24 C23 122.9(2)
C23 C24 H24 118.5
O4 C8 C9 112.8(2)
O4 C8 H8 109.1
O4 C8 C7 104.7(2)
C9 C8 H8 109.1
C7 C8 C9 112.0(2)
C7 C8 H8 109.1
O4 C23 C24 111.4(2)
O5 C23 O4 123.6(2)
O5 C23 C24 124.9(2)
C15 C10 C9 111.3(2)
C15 C10 C5 116.9(2)
C15 C10 C1 106.8(2)
C9 C10 C5 109.14(19)
C1 C10 C9 108.2(2)
C1 C10 C5 103.92(19)
C34 C33 C32 127.3(3)
C34 C33 C35 105.7(3)
C35 C33 C32 126.8(3)
O11 C18 C19 111.1(2)
O12 C18 O11 123.5(3)
O12 C18 C19 125.4(3)
O7 C32 C33 111.3(2)
O8 C32 O7 123.8(3)
O8 C32 C33 124.9(3)
O11 C1 C10 107.62(19)
O11 C1 H1 108.8
O11 C1 C2 109.5(2)
C10 C1 H1 108.8
C2 C1 C10 113.2(2)
C2 C1 H1 108.8
C6 C7 C8 106.1(2)
C6 C7 H7 111.2
C6 C7 C11 103.4(2)
C8 C7 H7 111.2
C8 C7 C11 113.4(2)
C11 C7 H7 111.2
C5 C4 H4 105.9
C3 C4 C5 109.4(2)
C3 C4 H4 105.9
C3 C4 C20 112.5(2)
C20 C4 C5 116.3(2)
C20 C4 H4 105.9
O10 C34 C33 111.4(3)
O10 C34 H34 124.3
C33 C34 H34 124.3
H12A C12 H12B 109.5
H12A C12 H12C 109.5
H12B C12 H12C 109.5
C11 C12 H12A 109.5
C11 C12 H12B 109.5
C11 C12 H12C 109.5
C1 C2 H2A 109.5
C1 C2 H2B 109.5
C1 C2 C3 110.8(2)
H2A C2 H2B 108.1
C3 C2 H2A 109.5
C3 C2 H2B 109.5
C27 C26 C25 123.1(3)
C31 C26 C25 118.4(3)
C31 C26 C27 118.5(3)
O3 C11 C7 102.76(19)
O3 C11 C12 108.6(2)
O3 C11 C13 108.8(2)
C12 C11 C7 112.3(2)
C12 C11 C13 107.3(2)
C13 C11 C7 116.7(2)
C26 C27 H27 119.8
C28 C27 C26 120.3(3)
C28 C27 H27 119.8
O2 C21 C22 111.9(2)
O1 C21 O2 123.2(3)
O1 C21 C22 124.9(3)
C26 C31 H31 119.5
C30 C31 C26 120.9(3)
C30 C31 H31 119.5
C4 C3 C2 113.7(2)
C4 C3 H3A 108.8
C4 C3 H3B 108.8
C2 C3 H3A 108.8
C2 C3 H3B 108.8
H3A C3 H3B 107.7
O10 C36 H36 124.3
C35 C36 O10 111.3(3)
C35 C36 H36 124.3
C11 C13 H13A 109.5
C11 C13 H13B 109.5
C11 C13 H13C 109.5
H13A C13 H13B 109.5
H13A C13 H13C 109.5
H13B C13 H13C 109.5
C4 C20 H20A 109.5
C4 C20 H20B 109.5
C4 C20 H20C 109.5
H20A C20 H20B 109.5
H20A C20 H20C 109.5
H20B C20 H20C 109.5
C27 C28 H28 119.8
C29 C28 C27 120.4(3)
C29 C28 H28 119.8
C16 C17 H17A 109.5
C16 C17 H17B 109.5
C16 C17 H17C 109.5
H17A C17 H17B 109.5
H17A C17 H17C 109.5
H17B C17 H17C 109.5
C21 C22 H22A 109.5
C21 C22 H22B 109.5
C21 C22 H22C 109.5
H22A C22 H22B 109.5
H22A C22 H22C 109.5
H22B C22 H22C 109.5
C31 C30 H30 120.3
C29 C30 C31 119.4(3)
C29 C30 H30 120.3
C33 C35 H35 127.0
C36 C35 C33 106.1(3)
C36 C35 H35 127.0
C28 C29 H29 119.8
C30 C29 C28 120.4(3)
C30 C29 H29 119.8
C18 C19 H19A 109.5
C18 C19 H19B 109.5
C18 C19 H19C 109.5
H19A C19 H19B 109.5
H19A C19 H19C 109.5
H19B C19 H19C 109.5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
O3 C5 1.452(3)
O3 C11 1.453(3)
O6 C15 1.443(3)
O6 C16 1.354(3)
O7 C9 1.440(3)
O7 C32 1.353(3)
O11 C18 1.351(3)
O11 C1 1.452(3)
O4 C8 1.443(3)
O4 C23 1.366(3)
O2 C6 1.451(3)
O2 C21 1.345(4)
O9 C16 1.205(3)
O5 C23 1.208(3)
O10 C34 1.353(4)
O10 C36 1.373(4)
O12 C18 1.205(4)
O8 C32 1.206(4)
O1 C21 1.213(4)
C6 H6 1.0000
C6 C5 1.530(3)
C6 C7 1.528(4)
C15 H15A 0.9900
C15 H15B 0.9900
C15 C10 1.534(3)
C16 C17 1.487(4)
C25 H25 0.9500
C25 C24 1.338(4)
C25 C26 1.466(4)
C9 H9 1.0000
C9 C8 1.540(3)
C9 C10 1.561(4)
C5 C10 1.576(3)
C5 C4 1.540(4)
C24 H24 0.9500
C24 C23 1.468(4)
C8 H8 1.0000
C8 C7 1.537(4)
C10 C1 1.548(3)
C33 C32 1.470(4)
C33 C34 1.356(4)
C33 C35 1.430(4)
C18 C19 1.491(4)
C1 H1 1.0000
C1 C2 1.526(4)
C7 H7 1.0000
C7 C11 1.543(4)
C4 H4 1.0000
C4 C3 1.529(4)
C4 C20 1.540(4)
C34 H34 0.9500
C12 H12A 0.9800
C12 H12B 0.9800
C12 H12C 0.9800
C12 C11 1.529(4)
C2 H2A 0.9900
C2 H2B 0.9900
C2 C3 1.533(4)
C26 C27 1.403(4)
C26 C31 1.400(4)
C11 C13 1.531(4)
C27 H27 0.9500
C27 C28 1.388(4)
C21 C22 1.496(4)
C31 H31 0.9500
C31 C30 1.399(4)
C3 H3A 0.9900
C3 H3B 0.9900
C36 H36 0.9500
C36 C35 1.342(5)
C13 H13A 0.9800
C13 H13B 0.9800
C13 H13C 0.9800
C20 H20A 0.9800
C20 H20B 0.9800
C20 H20C 0.9800
C28 H28 0.9500
C28 C29 1.384(5)
C17 H17A 0.9800
C17 H17B 0.9800
C17 H17C 0.9800
C22 H22A 0.9800
C22 H22B 0.9800
C22 H22C 0.9800
C30 H30 0.9500
C30 C29 1.384(5)
C35 H35 0.9500
C29 H29 0.9500
C19 H19A 0.9800
C19 H19B 0.9800
C19 H19C 0.9800
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_scale_group_code
-2 0 0 35.1567 3.09365 1
-2 0 0 39.2628 3.22667 1
2 0 0 34.978 3.16664 6
2 0 0 37.9413 4.48454 17
2 0 0 44.9837 3.0514 9
-3 0 0 1861.08 119.61 1
-3 0 0 1883.22 119.694 3
-3 0 0 1689.5 119.178 14
-3 0 0 1943.61 119.775 1
3 0 0 1989.69 119.15 9
3 0 0 1774.55 119.616 6
3 0 0 1903.81 122.944 17
-4 0 0 1242.3 83.4014 1
-4 0 0 1281.51 82.9062 1
-4 0 0 1242.26 82.2694 14
4 0 0 1341.06 82.956 6
-5 0 0 1184.86 78.654 7
-5 0 0 1213.89 79.3505 11
-5 0 0 1253.14 79.503 3
-5 0 0 1159.23 78.6791 14
5 0 0 1262.37 79.5734 6
-6 0 0 2097.47 156.255 14
-6 0 0 2596.5 160.17 8
-6 0 0 2059.8 157.041 13
-6 0 0 2454.98 155.68 11
-6 0 0 2446.85 155.566 3
6 0 0 2491.41 159.027 20
6 0 0 2522.86 165.257 15
6 0 0 2528.46 158.676 2
6 0 0 2326.03 159.488 19
6 0 0 2407.48 158.262 8
6 0 0 2470.53 155.552 6
-7 0 0 541.672 39.0941 8
-7 0 0 517.663 36.7847 13
-7 0 0 498.773 34.619 3
-7 0 0 442.016 33.3803 14
7 0 0 525.595 37.1602 2
7 0 0 405.329 36.1443 19
7 0 0 497.426 39.6396 15
7 0 0 464.948 34.0506 6
7 0 0 463.442 37.0043 5
7 0 0 479.728 37.4766 20
-8 0 0 461.973 33.0706 3
-8 0 0 454.815 34.7441 13
-8 0 0 461.121 37.0045 8
8 0 0 448.469 35.1776 5
8 0 0 436.796 34.2663 15
8 0 0 457.603 34.7702 2
-9 0 0 110.771 10.3267 3
-9 0 0 121.081 11.4857 13
-9 0 0 119.014 13.1175 8
9 0 0 96.1216 9.93586 15
9 0 0 99.5969 10.6173 2
9 0 0 114.009 11.5118 5
-10 0 0 31.3319 4.63795 8
10 0 0 20.1801 3.50214 18
10 0 0 22.3877 2.84881 2
10 0 0 24.0118 3.2275 5
10 -1 0 46.0348 6.35855 5
10 -1 0 49.6356 5.56281 18
-10 1 0 47.9376 6.25914 8
-10 1 0 56.8747 5.46746 13
9 -1 0 70.0383 8.74024 5
9 -1 0 82.0399 8.62193 2
-9 1 0 76.6776 8.32246 3
-9 1 0 75.5559 8.83805 13
-9 1 0 80.1826 10.287 8
8 -1 0 10.3772 5.05289 19
8 -1 0 12.8049 4.02278 5
8 -1 0 9.79872 4.05357 20
8 -1 0 14.2595 4.73149 15
8 -1 0 10.2984 3.36125 2
-8 1 0 6.55713 2.75418 3
-8 1 0 14.6629 4.33242 13
-8 1 0 8.5271 3.65797 8
7 -1 0 759.586 52.2312 20
7 -1 0 690.679 51.6105 2
7 -1 0 688.541 48.5495 6
7 -1 0 676.093 52.2128 19
-7 1 0 668.46 50.426 13
-7 1 0 747.573 48.7517 3
-7 1 0 727.604 52.9784 8
6 -1 0 864.653 62.6936 15
6 -1 0 959.4 63.5207 20
6 -1 0 902.087 63.2535 2
6 -1 0 903.527 60.2271 6
6 -1 0 848.056 64.7413 19
-6 1 0 863.774 58.9145 14
-6 1 0 843.372 62.0208 13
-6 1 0 930.618 60.1696 3
-6 1 0 962.17 64.3618 8
-6 1 0 926.113 59.9777 11
5 -1 0 1059.22 68.0415 6
-5 1 0 1064.46 67.8697 11
-5 1 0 1014.96 67.0841 14
-5 1 0 997.878 67.8949 3
4 -1 0 679.442 44.4694 6
4 -1 0 742.097 44.0803 9
-4 1 0 614.38 43.7361 14
-4 1 0 723.966 45.0173 1
-4 1 0 631.531 43.2942 7
-4 1 0 648.131 44.3118 11
3 -1 0 4578.89 308.075 1
-3 1 0 4605.24 307.019 7
-3 1 0 5005.71 308.109 3
-3 1 0 5112.29 307.932 1
1 -1 0 1031.37 68.4353 1
1 -1 0 1111.65 68.1396 14
1 -1 0 1005.17 67.9693 7
1 -1 0 1053.39 68.4447 6
-1 1 0 1096.48 68.3693 1
-1 1 0 1052.55 68.3206 11
-1 1 0 1125.81 68.6889 9
3 1 0 7183.43 457.394 9
-4 -1 0 858.317 61.2516 14
-4 -1 0 934.846 62.051 1
-4 -1 0 961.626 62.0167 1
-4 -1 0 992.861 62.1023 3
4 1 0 880.273 61.8795 6
4 1 0 1038.56 67.1256 17
-5 -1 0 754.313 50.4732 14
-5 -1 0 803.746 51.4363 3
5 1 0 745.011 51.2682 6
-6 -1 0 700.854 49.0545 7
-6 -1 0 763.257 49.855 11
-6 -1 0 750.693 54.0999 8
-6 -1 0 712.964 48.9396 14
-6 -1 0 661.61 51.7916 13
6 1 0 752.088 52.3745 2
6 1 0 792.376 53.5829 20
6 1 0 767.157 52.9023 15
6 1 0 727.424 49.9596 6
6 1 0 735.722 53.0824 19
6 1 0 756.486 52.8909 5
-7 -1 0 548.428 36.4067 11
-7 -1 0 495.754 35.2672 14
-7 -1 0 519.471 40.8018 8
-7 -1 0 506.697 36.7659 3
-7 -1 0 499.061 38.6625 13
7 1 0 479.829 38.4458 2
7 1 0 520.098 36.4893 6
7 1 0 543.914 42.4459 19
7 1 0 465.648 38.4286 15
7 1 0 542.279 40.2414 20
7 1 0 560.03 39.6138 5
-8 -1 0 33.0367 6.88284 8
-8 -1 0 37.7485 6.46674 13
-8 -1 0 22.9965 5.12285 3
8 1 0 24.962 5.6535 15
8 1 0 43.6038 6.56581 2
8 1 0 38.8657 7.23304 5
-9 -1 0 12.4227 3.63615 13
-9 -1 0 12.4068 3.26271 3
-9 -1 0 13.3231 3.89962 8
9 1 0 14.8332 3.28915 2
9 1 0 12.2484 3.85968 5
-10 -1 0 40.0927 5.31747 8
10 1 0 41.6844 3.88787 2
10 1 0 51.0151 5.73543 18
10 -2 0 8.09101 3.00388 18
10 -2 0 6.14025 1.80721 5
10 -2 0 5.95686 1.36864 2
-10 2 0 7.00897 2.45277 8
-10 2 0 11.0221 2.86983 13
9 -2 0 31.3764 5.08533 2
9 -2 0 44.2442 6.44475 5
-9 2 0 43.943 6.16647 13
-9 2 0 49.0874 6.07199 3
-9 2 0 45.0821 7.28617 8
8 -2 0 50.1191 8.09802 20
8 -2 0 42.3462 6.70799 19
-8 2 0 47.3105 8.34502 8
-8 2 0 46.431 6.1572 3
-8 2 0 52.4438 7.61847 13
7 -2 0 49.5536 7.44077 20
7 -2 0 32.6936 6.01725 15
7 -2 0 37.5967 7.31901 19
7 -2 0 46.8013 7.21595 2
7 -2 0 39.291 8.97512 4
-7 2 0 41.7221 5.22998 3
-7 2 0 45.248 7.48626 8
-7 2 0 38.1093 5.16796 11
-7 2 0 31.6017 6.46254 13
6 -2 0 890.607 60.2287 20
6 -2 0 866.604 57.2886 6
6 -2 0 753.033 63.628 4
6 -2 0 906.187 60.8288 15
6 -2 0 823.949 62.8325 19
6 -2 0 786.227 57.7092 8
6 -2 0 912.982 61.4755 2
-6 2 0 847.27 57.1747 3
-6 2 0 950.452 61.5188 8
-6 2 0 782.992 58.7924 13
-6 2 0 851.225 56.726 11
5 -2 0 1538.06 95.8708 2
5 -2 0 1204.16 87.2504 6
-5 2 0 1263.35 87.2606 3
-5 2 0 1364.58 87.1135 11
4 -2 0 108.027 8.21592 9
4 -2 0 86.2192 8.07388 1
4 -2 0 94.1099 7.89415 6
-4 2 0 93.839 7.8522 1
3 -2 0 3516.52 223.243 6
3 -2 0 3389.52 223.385 1
-3 2 0 3430.49 222.918 11
-3 2 0 3617.63 223.155 1
2 -2 0 3646.59 240.372 1
2 -2 0 3782.54 239.827 14
-2 2 0 3644.58 240.314 3
-2 2 0 3986.62 240.327 1
-1 -2 0 4503.05 289.701 17
-2 -2 0 3415.57 210.76 3
-2 -2 0 2948.55 210.388 1
2 2 0 3511.37 210.458 1
3 2 0 8482.12 541.616 9
-4 -2 0 2245.49 136.742 14
-4 -2 0 1985.22 137.317 3
-4 -2 0 2114.97 137.713 1
-4 -2 0 1886.12 139.381 1
4 2 0 2431.3 143.113 17
4 2 0 2080.14 137.482 6
-5 -2 0 1012.38 79.2086 13
-5 -2 0 1068.02 70.9257 14
-5 -2 0 1053.87 72.0199 3
5 2 0 1068.35 74.4564 20
5 2 0 1112.39 73.9626 2
5 2 0 1109.86 74.8734 15
5 2 0 1176.63 72.3947 6
-6 -2 0 140.41 14.9513 13
-6 -2 0 165.923 13.6921 3
-6 -2 0 160.697 12.3604 14
-6 -2 0 159.963 12.8291 7
-6 -2 0 162.376 16.465 8
6 2 0 180.14 15.5471 2
6 2 0 132.915 13.2648 8
6 2 0 166.913 15.1426 5
6 2 0 151.77 15.1553 19
6 2 0 172.255 13.4743 6
6 2 0 172.453 15.578 15
-7 -2 0 729.29 55.222 13
-7 -2 0 786.901 57.8791 8
-7 -2 0 782.705 53.479 3
7 2 0 858.309 56.1393 2
7 2 0 737.461 52.9572 6
7 2 0 792.246 55.9357 15
7 2 0 795.621 55.4328 5
7 2 0 715.778 54.6395 19
-8 -2 0 662.461 49.9478 8
-8 -2 0 663.168 45.8169 3
-8 -2 0 617.118 47.3763 13
8 2 0 678.626 47.503 5
8 2 0 676.935 47.9037 2
8 2 0 646.751 47.8036 15
-9 -2 0 22.412 4.91768 8
-9 -2 0 25.45 4.52741 3
9 2 0 24.2825 4.00415 15
9 2 0 23.5097 3.86071 5
9 2 0 32.7191 6.07845 18
9 2 0 22.1731 4.05716 2
-10 -2 0 43.6021 5.86053 8
-10 -2 0 51.6109 4.74651 13
10 2 0 45.8646 5.43412 18
10 -3 0 83.1011 7.89992 5
-10 3 0 92.0053 7.93306 13
9 -3 0 9.33499 3.10339 18
9 -3 0 9.10476 2.41191 2
9 -3 0 11.4208 3.3051 5
-9 3 0 11.4904 3.18876 13
-9 3 0 9.67457 2.97414 3
-9 3 0 13.4375 4.15697 8
8 -3 0 76.0454 10.3134 19
8 -3 0 78.8486 9.95436 2
8 -3 0 102.145 10.9268 20
-8 3 0 94.7592 10.3537 13
-8 3 0 92.694 9.0597 3
-8 3 0 103.844 11.993 8
7 -3 0 643.481 53.1679 19
7 -3 0 760.599 51.4399 20
-7 3 0 700.113 52.3173 8
-7 3 0 686.194 50.3151 13
-7 3 0 729.261 48.3835 3
6 -3 0 2029.17 130.402 19
6 -3 0 1709.67 130.367 4
6 -3 0 1959.8 127.768 2
6 -3 0 1615.42 125.085 15
6 -3 0 1590.6 123.097 8
6 -3 0 1906.23 125.878 20
-6 3 0 1992.42 123.133 3
-6 3 0 1852.2 124.931 13
-6 3 0 2052.52 122.792 11
-6 3 0 2153.8 127.926 8
5 -3 0 369.232 39.1496 2
-5 3 0 423.767 32.2922 13
-5 3 0 471.886 34.2307 8
-5 3 0 464.543 30.4266 11
-5 3 0 462.622 30.8589 3
4 -3 0 582.959 40.6852 9
-4 3 0 583.986 39.3572 11
-4 3 0 606.535 39.825 3
3 -3 0 48.7546 5.09186 9
3 -3 0 48.2944 4.58362 1
-3 3 0 39.722 4.02806 11
-3 3 0 44.0844 4.37796 3
2 -3 0 999.868 66.924 1
2 -3 0 1098.63 68.092 9
-2 3 0 1043.08 66.8083 1
-2 3 0 1003.36 66.7986 3
-2 3 0 1002.7 66.5768 11
0 -3 0 933.158 62.2512 9
0 -3 0 1063.72 61.1602 1
0 -3 0 921.009 60.3961 14
0 3 0 950.399 61.3502 1
0 3 0 848.48 63.7303 17
-1 -3 0 2176.11 133.699 14
-1 -3 0 1979.66 135.255 9
-1 -3 0 2115.15 134.378 1
-1 -3 0 2078.56 134.498 3
1 3 0 2036.79 137.125 17
1 3 0 2176.37 134.699 1
-2 -3 0 168.326 13.1439 1
-2 -3 0 197.082 12.5994 14
-2 -3 0 166.426 13.2338 3
2 3 0 185.024 13.1908 6
2 3 0 173.978 13.1669 1
2 3 0 205.345 16.0636 17
-3 -3 0 446.748 32.3456 1
-3 -3 0 463.171 32.3961 3
-3 -3 0 490.532 31.5285 14
3 3 0 459.232 32.3504 6
3 3 0 509.633 35.8974 17
3 3 0 481.422 32.3389 1
-4 -3 0 3430.94 236.31 3
-4 -3 0 3471.73 235.282 14
4 3 0 3818.39 236.8 6
4 3 0 3988.44 241.92 17
-5 -3 0 471.519 32.2719 3
-5 -3 0 460.796 32.1145 14
-5 -3 0 478.142 36.0375 8
-5 -3 0 429.626 34.0248 13
5 3 0 431.825 33.6884 2
5 3 0 491.282 38.156 17
5 3 0 433.008 32.7972 8
5 3 0 475.678 34.7398 15
5 3 0 412.328 32.0272 6
-6 -3 0 1250.47 87.3302 8
-6 -3 0 1280.05 81.7266 14
-6 -3 0 1100.55 87.6113 13
-6 -3 0 1322.04 83.2266 3
6 3 0 1045.37 82.3706 8
6 3 0 1323.89 85.5513 19
6 3 0 1384.43 86.4809 15
6 3 0 1206.93 84.5392 5
6 3 0 1281.98 88.2072 2
6 3 0 1245.71 83.1516 6
-7 -3 0 268.844 21.4497 7
-7 -3 0 306.176 22.2435 3
-7 -3 0 299.024 24.1762 13
-7 -3 0 274.456 25.2772 8
7 3 0 264.691 22.0636 6
7 3 0 285.874 24.418 15
7 3 0 266.294 23.0111 5
7 3 0 302.701 24.2096 2
-8 -3 0 136.613 11.698 3
-8 -3 0 136.607 14.4231 8
-8 -3 0 140.305 13.0513 13
8 3 0 148.76 13.4099 2
8 3 0 109.073 11.6153 5
8 3 0 117.825 12.9812 15
-9 -3 0 251.796 20.2546 8
-9 -3 0 276.005 18.9403 13
9 3 0 218.43 20.7238 18
9 3 0 230.07 18.8002 2
9 -4 0 216.955 17.0887 2
9 -4 0 216.861 18.7569 5
-9 4 0 198.526 18.4926 8
-9 4 0 245.869 17.5475 13
8 -4 0 146.372 14.0294 2
8 -4 0 117.346 12.8163 20
-8 4 0 156.965 15.6893 8
-8 4 0 146.08 13.4677 13
-8 4 0 154.247 12.3934 3
7 -4 0 99.4597 11.0938 20
7 -4 0 97.138 12.9905 19
7 -4 0 89.7658 14.0323 4
7 -4 0 113.616 12.7079 2
-7 4 0 111.258 11.5442 13
-7 4 0 120.099 13.271 8
-7 4 0 104.763 10.1862 3
6 -4 0 209.734 23.823 4
6 -4 0 235.577 21.4156 2
6 -4 0 217.779 19.4775 20
-6 4 0 234.511 21.2313 8
-6 4 0 223.147 19.4947 13
-6 4 0 247.02 18.1115 3
-6 4 0 250.178 17.8796 11
5 -4 0 392.134 31.3715 20
5 -4 0 366.25 29.8676 8
5 -4 0 387.871 31.5023 2
5 -4 0 397.333 34.7589 4
5 -4 0 389.436 29.8388 9
-5 4 0 436.96 27.9678 11
-5 4 0 358.081 29.3925 13
-5 4 0 434.696 31.9103 8
-5 4 0 411.093 28.5018 3
4 -4 0 248.034 22.4368 2
4 -4 0 301.541 22.0986 9
-4 4 0 286.417 19.7428 11
-4 4 0 270.228 20.0719 3
3 -4 0 493.241 34.2134 1
3 -4 0 529.583 35.7323 9
-3 4 0 500.033 33.4382 11
-3 4 0 516.287 34.2246 1
-3 4 0 453.07 33.6309 3
2 -4 0 605.228 39.2005 9
2 -4 0 510.484 36.7575 3
2 -4 0 564.474 37.5218 1
-2 4 0 553.097 37.4372 1
-2 4 0 546.753 37.2436 3
-2 4 0 570.927 37.0842 11
1 -4 0 1054.75 68.1995 1
1 -4 0 1019.52 69.7207 9
-1 4 0 1107.39 68.5757 1
-1 4 0 1087.64 68.6134 3
-1 4 0 957.657 67.7327 11
0 -4 0 17.0888 2.33986 3
0 -4 0 21.4627 3.38038 9
0 4 0 17.7778 2.18154 11
0 4 0 17.3264 2.37832 3
0 4 0 18.0102 4.14174 17
-1 -4 0 801.046 51.4105 1
-1 -4 0 732.524 52.6929 9
-1 -4 0 772.077 50.4616 14
1 4 0 821.669 52.0707 1
1 4 0 824.245 51.771 3
1 4 0 738.897 54.7609 17
-2 -4 0 1488 99.9895 1
-2 -4 0 1523.34 99.9512 3
2 4 0 1557.02 100.314 1
2 4 0 1565.91 99.9722 6
2 4 0 1448.95 99.2003 3
2 4 0 1656.8 103.858 17
-3 -4 0 684.071 50.6423 1
-3 -4 0 750.24 49.4863 14
-3 -4 0 754.381 50.5659 3
3 4 0 745.572 50.6716 6
3 4 0 843.664 54.9334 17
3 4 0 749.346 50.8074 1
-4 -4 0 102.342 9.91736 3
-4 -4 0 97.5848 11.4025 13
-4 -4 0 104.24 12.1879 8
4 4 0 131.994 12.3073 8
4 4 0 118.128 13.492 17
4 4 0 115.592 10.364 6
4 4 0 134.8 12.7171 15
4 4 0 138.914 12.1765 2
-5 -4 0 840.127 57.6796 14
-5 -4 0 880.75 62.8262 8
-5 -4 0 796.54 60.6765 13
-5 -4 0 843.653 58.8656 3
5 4 0 942.283 61.8288 19
5 4 0 939.248 61.5126 2
5 4 0 781.724 59.2973 8
5 4 0 779.548 59.131 6
5 4 0 952.023 62.4628 15
5 4 0 963.463 68.3746 17
-6 -4 0 418.872 30.887 14
-6 -4 0 442.896 33.9674 13
-6 -4 0 420.189 31.8648 3
-6 -4 0 449.751 35.7767 8
6 4 0 413.121 33.5691 19
6 4 0 462.109 32.9939 6
6 4 0 463.647 35.326 15
6 4 0 486.362 34.6598 2
-7 -4 0 436.721 33.2001 7
-7 -4 0 409.654 32.1391 13
-7 -4 0 443.053 30.8497 3
-7 -4 0 427.281 34.1862 8
7 4 0 431.165 33.1429 2
7 4 0 444.548 33.9991 15
7 4 0 381.261 31.4997 6
-8 -4 0 324.464 23.9807 13
-8 -4 0 342.848 23.1845 3
-8 -4 0 277.679 25.1113 8
8 4 0 304.425 25.2691 15
8 4 0 316.656 26.0678 18
8 4 0 317.847 24.73 2
-9 -4 0 393.611 27.4737 8
-9 -4 0 402.817 25.6561 13
9 4 0 351.912 27.681 18
9 4 0 341.99 26.0111 2
9 -5 0 268.077 22.1995 2
9 -5 0 342.644 24.2373 5
-9 5 0 348.199 24.7514 8
-9 5 0 318.227 22.3166 13
8 -5 0 130.672 12.6173 2
8 -5 0 111.708 13.6189 19
-8 5 0 126.026 11.9425 13
-8 5 0 134.94 11.5395 3
-8 5 0 153.236 14.3177 8
7 -5 0 168.973 18.1315 2
7 -5 0 131.095 15.9435 19
-7 5 0 152.9 17.6941 8
-7 5 0 137.097 12.1656 3
6 -5 0 24.8349 7.87124 4
6 -5 0 27.738 6.93506 19
6 -5 0 28.7537 5.26793 20
6 -5 0 38.294 6.43253 2
-6 5 0 28.7404 4.66237 3
-6 5 0 34.9061 5.64227 13
-6 5 0 33.2241 6.40877 8
5 -5 0 371.014 34.3009 4
5 -5 0 403.169 31.1243 9
5 -5 0 388.613 29.8529 20
5 -5 0 403.472 31.8257 2
5 -5 0 367.208 29.3851 8
-5 5 0 414.87 31.7736 8
-5 5 0 399.734 28.2258 3
-5 5 0 364.537 29.3795 13
-5 5 0 361.279 32.0614 2
-5 5 0 449.596 28.2125 11
4 -5 0 186.327 20.3169 4
4 -5 0 228.89 23.158 12
4 -5 0 194.143 17.7546 9
4 -5 0 207.645 18.3387 2
4 -5 0 196.931 17.2408 8
-4 5 0 197.189 17.7755 8
-4 5 0 163.187 23.696 2
-4 5 0 210.71 15.0886 11
-4 5 0 196.001 15.3665 3
-4 5 0 183.918 16.4657 13
3 -5 0 282.77 23.2959 2
3 -5 0 306.377 28.3563 12
3 -5 0 289.647 23.1332 9
-3 5 0 297.171 20.377 11
-3 5 0 277.643 22.6518 8
-3 5 0 266.51 21.7838 13
-3 5 0 269.448 20.4988 3
2 -5 0 1178.39 82.7864 9
2 -5 0 1161.48 79.7275 3
2 -5 0 1227.05 80.9613 1
-2 5 0 1246.12 80.2032 11
-2 5 0 1328.29 80.6002 3
1 -5 0 602.302 43.0421 9
1 -5 0 680.498 38.9962 14
1 -5 0 531.286 40.4049 1
-1 5 0 636.105 41.445 1
-1 5 0 570.597 46.0454 17
-1 5 0 577.058 40.0423 11
0 -5 0 1037.44 62.3799 14
0 -5 0 969.913 63.907 1
0 -5 0 1022.27 63.4216 3
0 -5 0 954.551 65.9274 9
0 5 0 979.883 63.3735 3
0 5 0 966.761 64.6659 1
0 5 0 868.428 68.3266 17
0 5 0 931.158 63.3428 11
-1 -5 0 365.48 22.3758 14
-1 -5 0 312.016 25.1404 9
-1 -5 0 338.775 23.3078 3
-1 -5 0 323.383 23.5659 1
1 5 0 320.439 27.2081 17
1 5 0 340.862 24.3495 1
-2 -5 0 182.088 14.0518 3
-2 -5 0 175.046 13.0966 14
2 5 0 169.859 13.6296 3
2 5 0 212.011 14.6388 6
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1 -1 -12 23.8429 6.37715 12
-1 1 12 26.72 3.64228 13
0 -1 -12 173.125 14.1754 20
0 -1 -12 153.35 13.5426 10
0 -1 -12 190.782 15.2998 16
0 -1 -12 138.854 16.5171 12
-1 -1 -12 243.908 20.5582 12
-1 -1 -12 188.169 15.9364 20
-2 -1 -12 132.795 12.1705 4
2 1 12 121.204 9.35212 13
4 -2 -12 11.5446 3.378 12
4 -2 -12 17.7479 2.74848 20
3 -2 -12 93.9884 12.3517 12
3 -2 -12 88.6438 9.6927 20
3 -2 -12 110.917 11.5369 4
2 -2 -12 34.3603 6.59173 12
2 -2 -12 28.4049 4.5137 16
2 -2 -12 30.4193 4.35447 20
1 -2 -12 19.4395 3.47326 20
1 -2 -12 18.5988 4.65672 12
1 -2 -12 15.2904 4.51693 4
-1 2 12 19.9977 2.71393 13
0 -2 -12 22.878 3.76644 16
0 -2 -12 19.3225 3.28209 20
0 2 12 27.9014 3.00227 13
-1 -2 -12 35.957 4.29439 16
-1 -2 -12 43.6676 6.19254 4
1 2 12 36.495 3.6677 13
3 -3 -12 258.394 19.1876 4
3 -3 -12 206.26 16.9939 20
2 -3 -12 97.2921 8.83908 20
2 -3 -12 94.5029 8.93387 16
2 -3 -12 118.666 11.346 12
1 -3 -12 92.5225 9.29382 4
1 -3 -12 85.2042 9.41326 12
-1 3 12 97.7712 8.1873 13
3 4 -13 92.3497 8.67543 16
3 4 -13 90.8331 8.21834 10
2 4 -13 59.441 7.67684 12
2 4 -13 49.56 5.77629 16
2 4 -13 40.9582 4.34338 18
1 4 -13 0.95532 1.14053 18
1 4 -13 2.60828 1.3143 16
1 4 -13 0.68045 1.36099 10
1 4 -13 0.98141 1.85795 12
0 4 -13 112.198 9.40641 16
0 4 -13 96.0619 8.89979 10
3 3 -13 64.4807 7.01713 16
3 3 -13 71.0069 8.12903 12
3 3 -13 59.5403 6.26875 10
2 3 -13 209.569 16.6279 16
2 3 -13 190.825 22.3663 12
2 3 -13 189.338 15.6454 10
1 3 -13 78.3476 8.04725 16
1 3 -13 65.5979 9.83566 12
0 3 -13 70.7135 11.2801 12
0 3 -13 77.8416 7.72829 16
3 2 -13 158.448 13.328 10
3 2 -13 195.296 15.0397 16
2 2 -13 8.30755 2.21473 16
2 2 -13 11.8362 3.83167 12
2 2 -13 8.17742 2.06584 10
1 2 -13 69.0678 7.91526 16
1 2 -13 77.3187 7.46211 10
1 2 -13 65.9192 9.93332 12
0 2 -13 30.1532 6.24489 12
0 2 -13 35.8787 6.04534 16
3 1 -13 21.1957 4.54783 12
3 1 -13 21.2617 3.55813 16
2 1 -13 85.6213 9.14575 16
2 1 -13 102.871 8.57751 10
1 1 -13 81.9125 10.498 12
1 1 -13 63.9462 7.39073 10
0 1 -13 51.1829 7.73872 12
0 1 -13 45.2697 5.10412 10
3 0 -13 176.769 16.1603 12
3 0 -13 199.819 14.8101 4
3 0 -13 155.471 13.6599 16
2 0 -13 182.996 14.7646 4
2 0 -13 143.432 15.6825 12
1 0 -13 211.305 21.3957 12
1 0 -13 207.48 17.2965 16
0 0 -13 333.74 24.3134 16
0 0 -13 342.216 23.5992 10
0 0 -13 335.799 26.2491 12