#------------------------------------------------------------------------------ #$Date: 2020-02-27 02:13:47 +0200 (Thu, 27 Feb 2020) $ #$Revision: 248463 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/73/1557375.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557375 loop_ _publ_author_name 'Fu, Yifan' 'Ding, Xiaoyu' 'Zhang, Xianglei' 'Shao, Xingcheng' 'Zhao, Jihui' 'Xu, Yechun' 'Luo, Xiaomin' 'Zhao, Weimin' _publ_section_title ; Diterpenoids from the Root Bark of Pinus massoniana and Evaluation of Their Phosphodiesterase Type 4D Inhibitory Activity ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.9b01269 _journal_year 2020 _chemical_absolute_configuration rmad _chemical_formula_moiety 'H2 O, C17 H24 O4' _chemical_formula_sum 'C17 H26 O5' _chemical_formula_weight 310.38 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2019-10-15 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 91.0550(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.8562(2) _cell_length_b 7.7464(2) _cell_length_c 10.3400(2) _cell_measurement_reflns_used 8326 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 74.545 _cell_measurement_theta_min 4.277 _cell_volume 789.33(3) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 173.0 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'D8 VENTURE' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0334 _diffrn_reflns_av_unetI/netI 0.0301 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 10969 _diffrn_reflns_point_group_measured_fraction_full 0.961 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 74.643 _diffrn_reflns_theta_min 4.276 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.777 _exptl_absorpt_correction_T_max 0.7538 _exptl_absorpt_correction_T_min 0.6369 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1477 before and 0.0568 after correction. The Ratio of minimum to maximum transmission is 0.8449. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.306 _exptl_crystal_description block _exptl_crystal_F_000 336 _exptl_crystal_size_max 0.19 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.225 _refine_diff_density_min -0.134 _refine_diff_density_rms 0.033 _refine_ls_abs_structure_details ; Flack x determined using 1257 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.05(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.058 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 211 _refine_ls_number_reflns 3087 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.057 _refine_ls_R_factor_all 0.0316 _refine_ls_R_factor_gt 0.0299 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0445P)^2^+0.0802P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0760 _refine_ls_wR_factor_ref 0.0779 _reflns_Friedel_coverage 0.778 _reflns_Friedel_fraction_full 0.919 _reflns_Friedel_fraction_max 0.904 _reflns_number_gt 2979 _reflns_number_total 3087 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 220191038_0m_a.res in P2(1) 220191038_0m.res created by SHELXL-2018/3 at 13:28:00 on 15-Oct-2019 REM Old TITL 220191038_0m in P2(1) REM SHELXT solution in P2(1) REM R1 0.098, Rweak 0.026, Alpha 0.002, Orientation as input REM Flack x = 0.028 ( 0.087 ) from Parsons' quotients REM Formula found by SHELXT: C17 O5 CELL 1.54178 9.8562 7.7464 10.34 90 91.055 90 ZERR 2 0.0002 0.0002 0.0002 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H O UNIT 34 52 10 L.S. 4 0 2 PLAN 20 SIZE 0.19 0.15 0.12 TEMP -100.15 BOND $H list 4 fmap 2 ACTA REM REM REM WGHT 0.044500 0.080200 FVAR 1.65648 O3 3 0.108888 0.537997 0.057157 11.00000 0.02907 0.02685 = 0.02562 0.00360 -0.01185 -0.00356 O5 3 0.944350 0.698463 0.865052 11.00000 0.03056 0.02565 = 0.02699 -0.00385 -0.01071 -0.00113 O2 3 0.365615 0.618320 0.259849 11.00000 0.02458 0.03896 = 0.03113 -0.00662 -0.00598 0.00620 O1 3 0.381592 0.507253 0.062220 11.00000 0.02511 0.04176 = 0.02376 -0.00011 -0.00775 0.00174 AFIX 147 H1 2 0.297734 0.526700 0.060776 11.00000 -1.50000 AFIX 0 O4 3 0.964920 0.360122 0.836467 11.00000 0.04417 0.02538 = 0.03380 0.00488 -0.01991 0.00091 AFIX 147 H4 2 0.940115 0.260250 0.857068 11.00000 -1.50000 AFIX 0 C12 1 0.742843 0.672444 0.574923 11.00000 0.01747 0.01900 = 0.02195 0.00007 0.00031 0.00135 C10 1 0.877176 0.633980 0.776042 11.00000 0.01956 0.02362 = 0.02201 -0.00167 -0.00159 -0.00083 C13 1 0.653648 0.786693 0.491910 11.00000 0.02864 0.01637 = 0.02823 -0.00308 -0.00758 0.00421 AFIX 23 H13A 2 0.685525 0.907297 0.501440 11.00000 -1.20000 H13B 2 0.560079 0.781389 0.524894 11.00000 -1.20000 AFIX 0 C4 1 0.754623 0.449289 0.393655 11.00000 0.01798 0.01643 = 0.01970 -0.00049 -0.00233 0.00131 C8 1 0.862401 0.390936 0.620344 11.00000 0.02628 0.01796 = 0.02366 -0.00051 -0.00726 0.00425 AFIX 23 H8A 2 0.851070 0.264393 0.612200 11.00000 -1.20000 H8B 2 0.951287 0.422101 0.583882 11.00000 -1.20000 AFIX 0 C11 1 0.804923 0.739497 0.680729 11.00000 0.02231 0.01820 = 0.02567 -0.00246 -0.00284 0.00067 AFIX 43 H11 2 0.801395 0.860814 0.693689 11.00000 -1.20000 AFIX 0 C14 1 0.649494 0.741371 0.348559 11.00000 0.02503 0.01785 = 0.02594 0.00379 -0.00552 0.00100 AFIX 23 H14A 2 0.735206 0.777428 0.308057 11.00000 -1.20000 H14B 2 0.573675 0.803298 0.304882 11.00000 -1.20000 AFIX 0 C5 1 0.630256 0.546607 0.332909 11.00000 0.01794 0.01726 = 0.01771 0.00076 -0.00212 -0.00019 AFIX 13 H5 2 0.552641 0.517251 0.389839 11.00000 -1.20000 AFIX 0 C15 1 0.890501 0.514685 0.343070 11.00000 0.01906 0.03119 = 0.02632 0.00148 -0.00038 0.00096 AFIX 137 H15A 2 0.887810 0.514600 0.248280 11.00000 -1.50000 H15B 2 0.963755 0.438900 0.374107 11.00000 -1.50000 H15C 2 0.906809 0.632364 0.374480 11.00000 -1.50000 AFIX 0 C17 1 0.433460 0.549619 0.177639 11.00000 0.02422 0.02069 = 0.02157 0.00358 -0.00327 -0.00133 C7 1 0.748869 0.482030 0.542831 11.00000 0.01794 0.01756 = 0.02007 -0.00022 -0.00317 0.00054 AFIX 13 H7 2 0.661535 0.430862 0.572219 11.00000 -1.20000 AFIX 0 C6 1 0.581975 0.493144 0.194392 11.00000 0.02157 0.02198 = 0.01932 0.00133 -0.00242 -0.00033 C3 1 0.742092 0.254154 0.368264 11.00000 0.02680 0.01830 = 0.02584 -0.00165 -0.00623 0.00385 AFIX 23 H3A 2 0.827442 0.196739 0.396226 11.00000 -1.20000 H3B 2 0.667880 0.206991 0.420963 11.00000 -1.20000 AFIX 0 C16 1 0.664432 0.573254 0.084195 11.00000 0.02871 0.03852 = 0.02255 0.00632 -0.00045 -0.00077 AFIX 137 H16A 2 0.666097 0.699097 0.093820 11.00000 -1.50000 H16B 2 0.622160 0.543006 0.000712 11.00000 -1.50000 H16C 2 0.757440 0.528570 0.088024 11.00000 -1.50000 AFIX 0 C9 1 0.860942 0.440972 0.763155 11.00000 0.02668 0.02149 = 0.02327 0.00325 -0.00786 -0.00069 AFIX 13 H9 2 0.771412 0.407100 0.799380 11.00000 -1.20000 AFIX 0 C2 1 0.713612 0.212378 0.226603 11.00000 0.03299 0.02303 = 0.02704 -0.00678 -0.00585 0.00651 AFIX 23 H2A 2 0.708724 0.085664 0.214963 11.00000 -1.20000 H2B 2 0.788445 0.256700 0.173344 11.00000 -1.20000 AFIX 0 C1 1 0.579707 0.294424 0.181939 11.00000 0.02960 0.02588 = 0.02350 -0.00635 -0.00689 0.00245 AFIX 23 H1A 2 0.505120 0.247716 0.234384 11.00000 -1.20000 H1B 2 0.561218 0.262799 0.090536 11.00000 -1.20000 AFIX 0 H3C 2 0.063155 0.552551 -0.011849 11.00000 0.05784 H3D 2 0.089841 0.445382 0.084083 11.00000 0.04932 HKLF 4 REM 220191038_0m_a.res in P2(1) REM wR2 = 0.0779, GooF = S = 1.058, Restrained GooF = 1.057 for all data REM R1 = 0.0299 for 2979 Fo > 4sig(Fo) and 0.0316 for all 3087 data REM 211 parameters refined using 1 restraints END WGHT 0.0445 0.0808 REM Highest difference peak 0.225, deepest hole -0.134, 1-sigma level 0.033 Q1 1 0.6136 0.5178 0.2575 11.00000 0.05 0.23 Q2 1 0.7547 0.4645 0.4707 11.00000 0.05 0.20 Q3 1 0.5129 0.5252 0.1845 11.00000 0.05 0.18 Q4 1 0.8557 0.4121 0.6924 11.00000 0.05 0.18 Q5 1 0.6992 0.4946 0.3566 11.00000 0.05 0.17 Q6 1 0.8444 0.6789 0.7213 11.00000 0.05 0.16 Q7 1 0.8033 0.4352 0.5817 11.00000 0.05 0.15 Q8 1 0.6449 0.2478 0.2093 11.00000 0.05 0.15 Q9 1 0.6378 0.6465 0.3368 11.00000 0.05 0.15 Q10 1 0.7536 0.5827 0.5571 11.00000 0.05 0.14 Q11 1 0.8790 0.5378 0.7603 11.00000 0.05 0.14 Q12 1 0.6275 0.9055 0.5240 11.00000 0.05 0.14 Q13 1 0.5917 0.3994 0.1857 11.00000 0.05 0.13 Q14 1 0.6195 0.5329 0.1472 11.00000 0.05 0.13 Q15 1 0.8024 0.7049 0.6177 11.00000 0.05 0.12 Q16 1 0.7304 0.2235 0.2997 11.00000 0.05 0.12 Q17 1 0.7490 0.6923 0.6449 11.00000 0.05 0.11 Q18 1 0.7616 0.3504 0.3851 11.00000 0.05 0.11 Q19 1 0.3981 0.6879 0.1984 11.00000 0.05 0.11 Q20 1 0.6553 0.7615 0.4172 11.00000 0.05 0.11 REM The information below was added by Olex2. REM REM R1 = 0.0299 for 2979 Fo > 4sig(Fo) and 0.0316 for all 10980 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.23, deepest hole -0.13 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0316 REM R1_gt = 0.0299 REM wR_ref = 0.0779 REM GOOF = 1.058 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 10980 REM Reflections_gt = 2979 REM Parameters = n/a REM Hole = -0.13 REM Peak = 0.23 REM Flack = 0.04(8) ; _cod_data_source_file np9b01269_si_001.cif _cod_data_source_block 220191038_0m _cod_database_code 1557375 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.913 _shelx_estimated_absorpt_t_min 0.866 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Ternary CH refined with riding coordinates: C5(H5), C7(H7), C9(H9) 2.b Secondary CH2 refined with riding coordinates: C13(H13A,H13B), C8(H8A,H8B), C14(H14A,H14B), C3(H3A,H3B), C2(H2A,H2B), C1(H1A, H1B) 2.c Aromatic/amide H refined with riding coordinates: C11(H11) 2.d Idealised Me refined as rotating group: C15(H15A,H15B,H15C), C16(H16A,H16B,H16C) 2.e Idealised tetrahedral OH refined as rotating group: O1(H1), O4(H4) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O3 O 0.10889(15) 0.5380(2) 0.05716(14) 0.0273(3) Uani 1 1 d . . . . . O5 O 0.94435(15) 0.69846(19) 0.86505(14) 0.0279(3) Uani 1 1 d . . . . . O2 O 0.36561(14) 0.6183(2) 0.25985(14) 0.0316(4) Uani 1 1 d . . . . . O1 O 0.38159(14) 0.5073(2) 0.06222(13) 0.0303(3) Uani 1 1 d . . . . . H1 H 0.297734 0.526700 0.060776 0.045 Uiso 1 1 calc GR . . . . O4 O 0.96492(17) 0.3601(2) 0.83647(15) 0.0347(4) Uani 1 1 d . . . . . H4 H 0.940115 0.260250 0.857068 0.052 Uiso 1 1 calc GR . . . . C12 C 0.74284(17) 0.6724(2) 0.57492(17) 0.0195(4) Uani 1 1 d . . . . . C10 C 0.87718(18) 0.6340(3) 0.77604(18) 0.0218(4) Uani 1 1 d . . . . . C13 C 0.6536(2) 0.7867(2) 0.49191(19) 0.0245(4) Uani 1 1 d . . . . . H13A H 0.685525 0.907297 0.501440 0.029 Uiso 1 1 calc R . . . . H13B H 0.560079 0.781389 0.524894 0.029 Uiso 1 1 calc R . . . . C4 C 0.75462(17) 0.4493(2) 0.39366(17) 0.0181(4) Uani 1 1 d . . . . . C8 C 0.8624(2) 0.3909(3) 0.62034(18) 0.0227(4) Uani 1 1 d . . . . . H8A H 0.851070 0.264393 0.612200 0.027 Uiso 1 1 calc R . . . . H8B H 0.951287 0.422101 0.583882 0.027 Uiso 1 1 calc R . . . . C11 C 0.80492(18) 0.7395(3) 0.68073(18) 0.0221(4) Uani 1 1 d . . . . . H11 H 0.801395 0.860814 0.693689 0.027 Uiso 1 1 calc R . . . . C14 C 0.64949(19) 0.7414(2) 0.34856(18) 0.0230(4) Uani 1 1 d . . . . . H14A H 0.735206 0.777428 0.308057 0.028 Uiso 1 1 calc R . . . . H14B H 0.573675 0.803298 0.304882 0.028 Uiso 1 1 calc R . . . . C5 C 0.63026(17) 0.5466(2) 0.33291(16) 0.0177(3) Uani 1 1 d . . . . . H5 H 0.552641 0.517251 0.389839 0.021 Uiso 1 1 calc R . . . . C15 C 0.89050(18) 0.5147(3) 0.34307(18) 0.0255(4) Uani 1 1 d . . . . . H15A H 0.887810 0.514600 0.248280 0.038 Uiso 1 1 calc GR . . . . H15B H 0.963755 0.438900 0.374107 0.038 Uiso 1 1 calc GR . . . . H15C H 0.906809 0.632364 0.374480 0.038 Uiso 1 1 calc GR . . . . C17 C 0.43346(18) 0.5496(3) 0.17764(17) 0.0222(4) Uani 1 1 d . . . . . C7 C 0.74887(18) 0.4820(2) 0.54283(17) 0.0186(4) Uani 1 1 d . . . . . H7 H 0.661535 0.430862 0.572219 0.022 Uiso 1 1 calc R . . . . C6 C 0.58198(18) 0.4931(2) 0.19439(17) 0.0210(4) Uani 1 1 d . . . . . C3 C 0.7421(2) 0.2542(2) 0.36826(19) 0.0237(4) Uani 1 1 d . . . . . H3A H 0.827442 0.196739 0.396226 0.028 Uiso 1 1 calc R . . . . H3B H 0.667880 0.206991 0.420963 0.028 Uiso 1 1 calc R . . . . C16 C 0.6644(2) 0.5733(3) 0.08420(19) 0.0299(4) Uani 1 1 d . . . . . H16A H 0.666097 0.699097 0.093820 0.045 Uiso 1 1 calc GR . . . . H16B H 0.622160 0.543006 0.000712 0.045 Uiso 1 1 calc GR . . . . H16C H 0.757440 0.528570 0.088024 0.045 Uiso 1 1 calc GR . . . . C9 C 0.8609(2) 0.4410(3) 0.76316(18) 0.0239(4) Uani 1 1 d . . . . . H9 H 0.771412 0.407100 0.799380 0.029 Uiso 1 1 calc R . . . . C2 C 0.7136(2) 0.2124(3) 0.22660(19) 0.0278(4) Uani 1 1 d . . . . . H2A H 0.708724 0.085664 0.214963 0.033 Uiso 1 1 calc R . . . . H2B H 0.788445 0.256700 0.173344 0.033 Uiso 1 1 calc R . . . . C1 C 0.5797(2) 0.2944(3) 0.18194(19) 0.0264(4) Uani 1 1 d . . . . . H1A H 0.505120 0.247716 0.234384 0.032 Uiso 1 1 calc R . . . . H1B H 0.561218 0.262799 0.090536 0.032 Uiso 1 1 calc R . . . . H3C H 0.063(3) 0.553(5) -0.012(3) 0.058(9) Uiso 1 1 d . . . . . H3D H 0.090(3) 0.445(5) 0.084(3) 0.049(9) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O3 0.0291(7) 0.0269(8) 0.0256(7) 0.0036(6) -0.0119(5) -0.0036(6) O5 0.0306(7) 0.0256(8) 0.0270(7) -0.0039(6) -0.0107(6) -0.0011(6) O2 0.0246(7) 0.0390(9) 0.0311(8) -0.0066(6) -0.0060(6) 0.0062(6) O1 0.0251(7) 0.0418(9) 0.0238(7) -0.0001(6) -0.0078(5) 0.0017(6) O4 0.0442(9) 0.0254(8) 0.0338(8) 0.0049(6) -0.0199(7) 0.0009(6) C12 0.0175(8) 0.0190(9) 0.0220(8) 0.0001(7) 0.0003(7) 0.0014(6) C10 0.0196(8) 0.0236(10) 0.0220(9) -0.0017(7) -0.0016(7) -0.0008(7) C13 0.0286(9) 0.0164(9) 0.0282(10) -0.0031(7) -0.0076(7) 0.0042(7) C4 0.0180(8) 0.0164(9) 0.0197(8) -0.0005(6) -0.0023(6) 0.0013(6) C8 0.0263(9) 0.0180(9) 0.0237(9) -0.0005(7) -0.0073(7) 0.0043(7) C11 0.0223(9) 0.0182(8) 0.0257(10) -0.0025(7) -0.0028(7) 0.0007(7) C14 0.0250(9) 0.0178(9) 0.0259(9) 0.0038(7) -0.0055(7) 0.0010(7) C5 0.0179(8) 0.0173(9) 0.0177(8) 0.0008(7) -0.0021(6) -0.0002(6) C15 0.0191(9) 0.0312(11) 0.0263(9) 0.0015(8) -0.0004(7) 0.0010(7) C17 0.0242(9) 0.0207(9) 0.0216(8) 0.0036(7) -0.0033(7) -0.0013(7) C7 0.0179(8) 0.0176(9) 0.0201(9) -0.0002(6) -0.0032(6) 0.0005(6) C6 0.0216(8) 0.0220(9) 0.0193(8) 0.0013(7) -0.0024(6) -0.0003(7) C3 0.0268(9) 0.0183(10) 0.0258(9) -0.0016(7) -0.0062(7) 0.0039(7) C16 0.0287(10) 0.0385(12) 0.0225(9) 0.0063(8) -0.0004(7) -0.0008(8) C9 0.0267(9) 0.0215(10) 0.0233(9) 0.0033(7) -0.0079(7) -0.0007(7) C2 0.0330(10) 0.0230(10) 0.0270(10) -0.0068(8) -0.0058(8) 0.0065(8) C1 0.0296(10) 0.0259(10) 0.0235(9) -0.0064(7) -0.0069(8) 0.0025(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H3C O3 H3D 107(3) . . ? C17 O1 H1 109.5 . . ? C9 O4 H4 109.5 . . ? C13 C12 C7 118.23(15) . . ? C11 C12 C13 119.21(17) . . ? C11 C12 C7 122.32(17) . . ? O5 C10 C11 121.89(18) . . ? O5 C10 C9 121.54(18) . . ? C11 C10 C9 116.52(16) . . ? C12 C13 H13A 108.5 . . ? C12 C13 H13B 108.5 . . ? C12 C13 C14 115.12(16) . . ? H13A C13 H13B 107.5 . . ? C14 C13 H13A 108.5 . . ? C14 C13 H13B 108.5 . . ? C5 C4 C7 106.01(13) . . ? C15 C4 C5 112.81(15) . . ? C15 C4 C7 109.30(14) . . ? C15 C4 C3 109.53(16) . . ? C3 C4 C5 110.23(14) . . ? C3 C4 C7 108.85(15) . . ? H8A C8 H8B 108.0 . . ? C7 C8 H8A 109.3 . . ? C7 C8 H8B 109.3 . . ? C9 C8 H8A 109.3 . . ? C9 C8 H8B 109.3 . . ? C9 C8 C7 111.61(16) . . ? C12 C11 C10 122.83(18) . . ? C12 C11 H11 118.6 . . ? C10 C11 H11 118.6 . . ? C13 C14 H14A 109.8 . . ? C13 C14 H14B 109.8 . . ? C13 C14 C5 109.36(15) . . ? H14A C14 H14B 108.2 . . ? C5 C14 H14A 109.8 . . ? C5 C14 H14B 109.8 . . ? C4 C5 H5 104.9 . . ? C14 C5 C4 109.82(14) . . ? C14 C5 H5 104.9 . . ? C14 C5 C6 113.27(15) . . ? C6 C5 C4 117.78(15) . . ? C6 C5 H5 104.9 . . ? C4 C15 H15A 109.5 . . ? C4 C15 H15B 109.5 . . ? C4 C15 H15C 109.5 . . ? H15A C15 H15B 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? O2 C17 O1 121.91(17) . . ? O2 C17 C6 125.63(16) . . ? O1 C17 C6 112.39(16) . . ? C12 C7 C4 112.10(14) . . ? C12 C7 C8 111.38(14) . . ? C12 C7 H7 106.4 . . ? C4 C7 H7 106.4 . . ? C8 C7 C4 113.61(15) . . ? C8 C7 H7 106.4 . . ? C17 C6 C5 107.62(15) . . ? C17 C6 C16 108.45(15) . . ? C17 C6 C1 105.21(15) . . ? C16 C6 C5 114.60(15) . . ? C16 C6 C1 110.27(17) . . ? C1 C6 C5 110.21(15) . . ? C4 C3 H3A 109.0 . . ? C4 C3 H3B 109.0 . . ? H3A C3 H3B 107.8 . . ? C2 C3 C4 112.71(16) . . ? C2 C3 H3A 109.0 . . ? C2 C3 H3B 109.0 . . ? C6 C16 H16A 109.5 . . ? C6 C16 H16B 109.5 . . ? C6 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? O4 C9 C10 108.52(15) . . ? O4 C9 C8 112.79(17) . . ? O4 C9 H9 108.6 . . ? C10 C9 C8 109.51(16) . . ? C10 C9 H9 108.6 . . ? C8 C9 H9 108.6 . . ? C3 C2 H2A 109.6 . . ? C3 C2 H2B 109.6 . . ? C3 C2 C1 110.21(16) . . ? H2A C2 H2B 108.1 . . ? C1 C2 H2A 109.6 . . ? C1 C2 H2B 109.6 . . ? C6 C1 H1A 109.2 . . ? C6 C1 H1B 109.2 . . ? C2 C1 C6 112.21(16) . . ? C2 C1 H1A 109.2 . . ? C2 C1 H1B 109.2 . . ? H1A C1 H1B 107.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O3 H3C 0.84(4) . ? O3 H3D 0.79(4) . ? O5 C10 1.230(2) . ? O2 C17 1.214(2) . ? O1 H1 0.8400 . ? O1 C17 1.331(2) . ? O4 H4 0.8400 . ? O4 C9 1.410(2) . ? C12 C13 1.505(2) . ? C12 C11 1.348(3) . ? C12 C7 1.513(3) . ? C10 C11 1.456(3) . ? C10 C9 1.509(3) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C14 1.523(3) . ? C4 C5 1.561(2) . ? C4 C15 1.533(3) . ? C4 C7 1.565(2) . ? C4 C3 1.539(3) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C8 C7 1.536(2) . ? C8 C9 1.527(3) . ? C11 H11 0.9500 . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C14 C5 1.529(3) . ? C5 H5 1.0000 . ? C5 C6 1.557(2) . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C17 C6 1.535(3) . ? C7 H7 1.0000 . ? C6 C16 1.542(3) . ? C6 C1 1.545(3) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C3 C2 1.521(3) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C9 H9 1.0000 . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C2 C1 1.529(3) . ? C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 1 0 0 68.8203 3.10593 11 -1 0 0 72.0158 4.30383 10 -1 0 0 68.9047 3.237 11 1 0 0 71.0221 4.26648 10 2 0 0 2083.77 58.7896 10 -2 0 0 2121.74 58.8994 10 2 0 0 1932.94 54.0778 11 -2 0 0 2117 55.2238 11 3 0 0 2882.62 76.2914 11 3 0 0 2815.46 82.8717 10 -3 0 0 2942.49 83.5365 10 4 0 0 4712.57 123.285 11 -4 0 0 4531.14 139.447 10 4 0 0 4940.86 134.913 10 5 0 0 11.3072 3.00819 11 5 0 0 9.39869 3.70742 10 6 0 0 1143.49 53.9687 10 -6 0 0 1156.58 47.0988 4 6 0 0 1228.53 40.2079 11 -7 0 0 4.62689 4.85954 3 7 0 0 0.87662 4.23431 7 -7 0 0 9.25006 6.2831 4 7 0 0 7.64651 2.71654 12 7 0 0 6.70612 4.16295 3 7 0 0 4.74007 4.33652 1 7 0 0 3.25806 2.14019 11 -8 0 0 1125.57 57.2678 3 8 0 0 1128.19 37.6589 1 8 0 0 1090.5 41.4844 11 8 0 0 1222.52 65.6463 7 -9 0 0 22.3913 5.7932 3 10 0 0 498.264 25.8101 7 -10 0 0 488.262 25.7476 3 11 0 0 4.53179 2.78715 7 -11 0 0 1.75345 2.6801 3 -12 0 0 2.08485 1.59637 3 -12 0 0 6.94117 3.99032 7 12 0 0 0.27282 1.29027 7 -1 1 0 4582.85 115.399 11 2 -1 0 2589.5 67.8005 11 -2 -1 0 2700.77 70.8549 10 -2 -1 0 2505.76 67.0874 11 2 -1 0 2417.87 71.2568 10 -2 1 0 2725.12 72.4369 10 2 1 0 2516.79 70.4417 10 -2 1 0 2606.3 65.6167 4 2 1 0 2471.17 65.8824 11 3 -1 0 101.253 8.88879 10 -3 -1 0 112.047 8.91276 10 3 -1 0 110.44 6.87343 11 -3 1 0 107.216 9.32923 10 3 1 0 108.389 8.78805 10 3 1 0 112.767 5.7737 11 -4 -1 0 332.994 19.2024 10 4 -1 0 326.023 14.7671 11 4 -1 0 318.057 19.3841 10 4 1 0 334.926 13.2423 11 -4 1 0 336.928 20.3015 10 4 1 0 327.962 19.1154 10 5 -1 0 890.501 31.1162 11 -5 -1 0 827.826 38.7097 10 5 -1 0 839.622 39.7439 10 5 1 0 931.342 29.0774 11 5 1 0 832.854 38.3597 10 -5 1 0 792.104 30.9045 4 -5 1 0 888.05 42.352 10 -6 -1 0 370.533 24.5265 4 6 -1 0 285.424 39.8747 10 6 -1 0 353.564 17.9031 11 -6 1 0 348.694 19.7632 4 -6 1 0 294.09 37.0892 10 6 1 0 369.362 16.7281 11 -7 -1 0 203.24 25.4267 4 -7 -1 0 199.378 16.7881 3 7 -1 0 197.115 11.4733 12 7 -1 0 178.842 13.149 11 7 -1 0 173.829 16.9473 7 -7 1 0 195.213 11.6442 8 7 1 0 170.839 15.4282 7 -7 1 0 204.162 17.8709 4 -7 1 0 159.899 14.39 3 8 -1 0 611.306 29.1072 11 -8 -1 0 606.241 31.4336 3 -8 1 0 583.733 29.6702 3 8 1 0 572.327 24.4793 1 8 1 0 596.696 30.9399 7 9 -1 0 327.157 21.7342 7 -9 -1 0 323.065 21.8717 3 9 -1 0 320.699 12.8339 12 9 1 0 334.725 21.0642 7 9 1 0 341.125 16.4759 1 -9 1 0 333.923 20.8977 3 -9 1 0 366.082 18.2492 2 -10 -1 0 231.75 16.9372 3 10 -1 0 213.563 16.4211 7 -10 1 0 212.224 15.2402 3 10 1 0 219 15.9465 7 -11 -1 0 122.584 10.4122 3 11 -1 0 132.482 10.5562 7 11 1 0 114.808 9.39187 7 -11 1 0 117.095 8.82281 3 12 -1 0 23.5293 3.51645 7 -12 1 0 21.7072 3.62377 7 12 1 0 22.0254 3.77735 9 12 1 0 28.504 3.7331 7 0 -2 0 2008.89 55.9419 4 0 2 0 2107.67 55.1055 2 1 -2 0 908.297 27.3123 11 1 -2 0 901.262 24.3936 4 1 -2 0 925.555 27.1703 10 -1 -2 0 956.004 23.9655 10 1 2 0 960.843 28.8207 2 -1 2 0 913.556 26.1855 2 1 2 0 965.505 24.9146 10 -1 2 0 971.504 28.1461 10 -2 -2 0 532.152 17.9863 10 2 -2 0 518.41 20.157 10 2 -2 0 524.699 18.4036 11 -2 2 0 536.726 20.9648 10 -2 2 0 499.848 15.5096 2 2 2 0 513.624 19.6297 2 2 2 0 518.552 18.5278 10 3 -2 0 821.514 32.0821 10 -3 -2 0 816.728 29.5491 10 3 -2 0 871.421 28.4842 11 3 2 0 858.094 30.467 10 -3 2 0 842.054 23.9346 2 4 -2 0 3313.58 98.8944 10 4 -2 0 3282.82 100.365 11 -4 -2 0 3205.34 95.1566 10 -4 2 0 3405.77 101.08 10 -4 2 0 3316.88 84.2166 4 -4 2 0 3079.03 81.7472 4 4 2 0 3166.55 95.6892 10 -4 2 0 3365.25 84.6085 2 -5 -2 0 228.712 18.8398 4 5 -2 0 229.644 19.7798 10 5 -2 0 247.23 14.4526 11 -5 2 0 241.857 20.3375 10 -5 2 0 241.334 10.1761 2 -5 2 0 235.693 10.3581 4 6 -2 0 434.859 24.3913 3 6 -2 0 479.515 23.0638 11 -6 -2 0 443.632 29.971 4 6 -2 0 441.009 20.004 12 6 2 0 428.333 23.379 7 6 2 0 431.02 21.3837 1 -6 2 0 441.531 23.5518 3 -6 2 0 443.509 16.6929 2 -6 2 0 453.238 20.5057 8 7 -2 0 315.981 18.9587 11 7 -2 0 302.826 20.0176 3 7 -2 0 317.482 16.3583 12 -7 -2 0 292.98 21.3254 3 7 -2 0 269.485 21.2307 7 7 2 0 318.134 19.8184 7 -7 2 0 305.132 16.8742 8 -7 2 0 307.773 14.099 2 -7 2 0 300.24 18.8106 3 7 2 0 330.421 17.8878 1 -8 -2 0 706.489 34.7029 3 8 -2 0 655.845 31.9897 11 8 -2 0 705.416 34.953 7 8 -2 0 709.553 26.6463 12 -8 2 0 695.014 27.3997 8 8 2 0 675.753 28.1709 1 -8 2 0 695.626 26.1167 2 -8 2 0 710.271 31.2432 3 8 2 0 696.898 32.386 7 9 -2 0 135.214 8.68583 12 -9 -2 0 143.46 14.3022 3 9 -2 0 141.9 13.5413 7 9 2 0 139.852 10.7258 1 9 2 0 132.053 12.4258 7 -9 2 0 139.708 11.9254 3 10 -2 0 38.3614 5.13108 12 -10 -2 0 49.4284 7.75844 3 10 -2 0 37.2486 6.43096 7 10 2 0 37.3496 5.97283 7 10 2 0 36.0928 4.82998 1 -10 2 0 35.706 5.96861 3 -10 2 0 43.4068 5.85974 5 11 -2 0 168.256 11.2229 7 -11 -2 0 174.195 12.237 3 11 2 0 170.984 10.1627 7 -12 -2 0 25.8911 4.30319 3 -12 2 0 30.284 3.22247 7 12 2 0 31.2395 2.60095 7 12 2 0 30.1907 3.46421 9 0 -3 0 0.69568 0.96183 4 1 -3 0 1429.1 43.5181 11 1 -3 0 1577.19 39.942 10 1 -3 0 1525.95 40.0395 4 -1 -3 0 1526.81 48.5223 4 -1 3 0 1538.75 41.0951 10 1 3 0 1502.05 45.4507 2 -1 3 0 1494.41 43.0167 2 -2 -3 0 1805.73 44.9546 10 2 -3 0 1716.83 50.9028 10 -2 -3 0 1801.8 58.7043 4 2 -3 0 1765.29 51.9532 11 2 3 0 1772.65 53.8181 2 -2 3 0 1742.57 48.7393 2 2 3 0 1775.83 45.8131 10 -2 3 0 1789.4 52.9331 10 -3 -3 0 1930.74 66.7206 4 3 -3 0 2015.54 58.9394 11 3 -3 0 1915.94 61.05 10 -3 -3 0 1939.29 54.7664 10 3 3 0 1927.87 56.4547 10 -3 3 0 2018.72 53.887 2 3 3 0 2055.3 61.7459 2 -3 3 0 1981.35 62.8784 10 4 -3 0 81.2309 7.89001 11 4 -3 0 71.3611 9.30395 10 -4 -3 0 79.5356 10.7812 4 -4 3 0 73.7778 10.1297 10 5 -3 0 274.824 16.4746 11 -5 -3 0 273.977 22.0334 4 -5 3 0 273.181 11.8456 2 5 3 0 276.573 17.493 1 -5 3 0 250.505 15.6846 8 6 -3 0 258.698 15.042 12 6 -3 0 255.97 18.2865 3 6 -3 0 284.318 18.0181 11 -6 -3 0 273.07 24.8874 4 -6 -3 0 264.613 19.7704 3 -6 3 0 266.028 12.5423 2 6 3 0 268.49 16.4985 7 -6 3 0 263.536 16.0798 8 6 3 0 243.528 15.1443 5 6 3 0 285.224 17.5635 1 -6 3 0 270.32 17.3231 9 7 -3 0 53.9551 9.11542 11 -7 -3 0 52.6212 10.5786 3 7 -3 0 50.4725 12.3082 3 -7 3 0 63.8604 9.18794 3 7 3 0 63.4871 8.71707 1 -7 3 0 48.8395 8.60078 6 7 3 0 45.2104 10.1714 7 8 -3 0 104.002 13.8929 7 8 -3 0 116.953 9.48923 12 -8 -3 0 117.659 13.3803 3 8 3 0 111.97 10.4431 1 -8 3 0 106.353 9.37256 8 8 3 0 112.878 10.7466 7 -8 3 0 115.115 10.2075 3 9 -3 0 94.3859 11.6016 7 -9 -3 0 105.99 11.919 3 9 -3 0 104.878 8.00793 12 9 3 0 110.879 10.0256 7 9 3 0 107.137 8.74892 1 -9 3 0 91.6445 9.54653 5 10 -3 0 27.74 5.94005 7 -10 -3 0 25.3732 5.92222 3 10 -3 0 26.5065 3.36974 12 10 3 0 33.6147 5.28437 9 -10 3 0 19.9586 4.3534 5 10 3 0 32.1407 4.54688 7 10 3 0 32.6633 5.96177 1 11 -3 0 35.2482 6.19862 7 -11 -3 0 45.1417 5.6252 3 11 3 0 41.5487 4.90227 9 11 3 0 40.6991 3.61312 7 0 -4 0 3540.08 96.6238 11 0 -4 0 3660.3 97.5366 4 0 4 0 3559.52 98.5723 2 1 -4 0 2333.85 61.9556 4 -1 -4 0 2498.32 73.4932 4 1 -4 0 2345.34 68.4287 11 1 4 0 2366.68 70.9701 2 -1 4 0 2415.54 68.0695 2 -2 -4 0 1239.04 46.5903 4 2 -4 0 1195.77 40.1302 11 -2 4 0 1186.29 39.7729 2 2 4 0 1174.08 42.3954 2 -2 4 0 1231.09 35.6943 10 3 -4 0 172.343 12.353 11 -3 -4 0 187.704 16.2869 4 3 -4 0 177.063 10.8985 10 -3 4 0 163.186 12.3777 10 -3 4 0 173.864 9.81646 2 4 -4 0 1170.45 42.624 11 -4 -4 0 1130.62 51.8457 4 4 4 0 1161.99 44.1521 1 -4 4 0 1097.24 45.0428 6 4 4 0 1230.3 50.2425 9 -4 4 0 1207.46 42.7464 5 -4 4 0 1147.86 36.3718 2 -4 4 0 1095.2 41.3924 8 5 -4 0 115.018 11.1716 11 5 -4 0 113.381 18.8501 3 -5 -4 0 111.934 16.2097 4 5 4 0 124.186 10.9065 9 5 4 0 130.619 12.0731 1 -5 4 0 112.449 11.3201 5 5 4 0 111.939 8.96343 5 -5 4 0 144.792 12.3135 8 -5 4 0 99.629 12.3224 6 6 -4 0 525.079 28.2684 3 6 -4 0 503.236 23.5322 12 -6 -4 0 527.227 29.7594 3 6 -4 0 508.971 28 11 -6 -4 0 510.2 25.5424 12 -6 4 0 569.61 27.8577 6 6 4 0 541.277 22.349 7 -6 4 0 529.814 26.2588 9 -6 4 0 537.073 26.6702 5 6 4 0 462.538 21.9333 5 -6 4 0 542.655 25.6775 8 6 4 0 531.937 26.3253 1 7 -4 0 55.1938 7.39549 12 -7 -4 0 42.578 10.713 3 -7 4 0 54.5822 7.24109 8 -7 4 0 47.7737 7.73422 6 7 4 0 42.5618 5.88213 7 -7 4 0 48.2044 7.83688 5 8 -4 0 30.288 5.46055 12 -8 -4 0 38.4708 10.8642 3 -8 4 0 32.4704 5.43003 8 8 4 0 33.5665 6.12491 1 8 4 0 29.0039 5.37305 7 -8 4 0 21.6157 4.95892 5 -8 4 0 34.7663 8.39067 6 -9 -4 0 202.167 14.8658 3 9 -4 0 214.135 11.5876 12 9 4 0 210.87 14.0967 9 -9 4 0 214.037 13.7712 5 9 4 0 199.916 12.5097 1 9 4 0 204.125 10.3577 7 10 -4 0 82.8583 5.34494 12 -10 -4 0 81.9659 8.06926 3 -10 4 0 86.735 6.85817 5 10 4 0 82.3941 7.32225 9 10 4 0 81.0638 6.21398 1 -11 -4 0 86.0552 6.52071 3 11 4 0 85.6095 5.78922 9 -11 4 0 93.3292 5.39679 7 0 -5 0 -2.3075 1.77707 11 0 -5 0 -0.9631 1.5037 4 0 5 0 -1.5876 4.33997 5 0 5 0 -0.6369 1.76992 2 1 -5 0 276.2 15.7022 11 -1 -5 0 269.422 14.4421 11 -1 -5 0 273.781 16.7707 4 -1 5 0 246.208 18.2666 6 1 5 0 268.956 16.6445 2 -1 5 0 269.291 14.8922 5 -1 5 0 273.713 15.3057 2 2 -5 0 572.95 25.9228 11 -2 -5 0 554.569 29.6567 4 2 5 0 563.12 21.6673 5 -2 5 0 573.354 23.8595 2 -2 5 0 583.449 26.6282 8 2 5 0 575.088 29.4184 1 -3 -5 0 151.192 16.5597 4 3 -5 0 158.864 13.3028 11 3 5 0 147.546 13.7411 1 -3 5 0 156.794 10.7015 2 -3 5 0 133.591 13.7703 9 3 5 0 167.453 9.33847 5 -3 5 0 157.193 14.9182 6 -3 5 0 147.863 11.7322 5 -3 5 0 143.263 12.8486 8 4 -5 0 164.512 14.2357 11 -4 5 0 162.509 14.2304 8 -4 5 0 202.44 15.6563 9 -4 5 0 189.398 16.2419 6 4 5 0 168.3 9.63197 5 4 5 0 192.861 13.4938 9 4 5 0 174.458 14.8021 1 -4 5 0 170.819 13.388 5 5 -5 0 1326.81 52.3402 11 5 -5 0 1304.34 46.6639 12 5 5 0 1344.37 50.9876 1 -5 5 0 1382.49 49.4083 9 -5 5 0 1401.82 54.0933 6 -5 5 0 1448.26 50.5418 8 5 5 0 1335.21 42.7523 5 -5 5 0 1480.23 50.8418 5 6 -5 0 1176.76 42.1369 12 6 5 0 1145.44 43.3694 9 -6 5 0 1195.44 44.0849 8 6 5 0 1113.16 38.9795 5 -6 5 0 1204.09 44.8851 5 -6 5 0 1175.01 43.4002 9 6 5 0 1234.69 46.3216 1 -6 5 0 1172.13 45.8187 6 -7 -5 0 693.606 35.0497 3 7 -5 0 700.021 28.6944 12 7 5 0 700.742 30.3607 9 -7 5 0 720.554 31.1707 5 -7 5 0 676.535 29.2626 8 -7 5 0 699.74 30.5184 6 7 5 0 703.101 30.5907 1 8 -5 0 106.242 8.43744 12 -8 -5 0 93.4773 10.9288 3 -8 5 0 92.928 7.93741 6 8 5 0 106.329 9.67081 1 -8 5 0 95.8327 8.5359 8 -8 5 0 101.748 9.45156 5 8 5 0 98.9308 9.04985 9 -9 -5 0 38.6232 6.09777 3 9 -5 0 34.9463 4.24083 12 -9 5 0 32.9215 7.61842 7 9 5 0 35.4188 5.51531 1 -9 5 0 33.4197 8.73858 5 -10 -5 0 52.0782 6.20849 3 10 -5 0 59.7441 3.76581 12 10 5 0 43.5891 4.82291 1 -10 5 0 58.8905 3.65485 7 -10 5 0 57.9516 4.46572 5 10 5 0 57.2945 5.59088 9 0 -6 0 283.259 17.9755 11 0 6 0 305.102 19.8717 1 0 6 0 297.795 20.4619 6 0 6 0 294.278 18.5508 8 0 6 0 292.908 18.6494 2 0 6 0 267.108 18.825 9 0 6 0 287.879 15.9405 5 1 -6 0 319.59 19.6444 11 -1 -6 0 352.682 20.5977 11 -1 6 0 324.561 19.5992 8 -1 6 0 318.279 17.0208 5 1 6 0 313.338 19.5195 9 1 6 0 313.844 20.9973 6 -1 6 0 294.231 19.9422 9 -1 6 0 336.431 22.0931 6 1 6 0 333.915 16.3582 5 1 6 0 352.278 21.2491 1 -1 6 0 314.121 20.3485 1 1 6 0 332.723 19.6006 8 1 6 0 331.663 20.8639 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23.36 8 -6 6 0 361.54 12.4825 7 7 -6 0 40.6039 5.99116 12 7 6 0 32.8656 5.92137 1 -7 6 0 42.0794 6.03423 5 7 6 0 38.3467 6.09807 9 -7 6 0 38.8673 6.27775 6 -7 6 0 41.5096 4.07611 7 -7 6 0 46.422 6.20699 8 8 -6 0 111.431 7.55564 12 -8 6 0 95.7989 7.53366 8 -8 6 0 105.624 8.57545 5 8 6 0 104.875 8.51197 1 -8 6 0 91.7679 6.82265 6 8 6 0 101.283 7.83752 9 9 -6 0 44.446 3.9548 12 9 6 0 40.6435 4.44613 9 9 6 0 43.2648 4.05484 1 -9 6 0 48.1687 4.32856 5 0 7 0 13.0134 6.42241 9 0 7 0 8.77618 4.50301 1 0 7 0 7.96905 4.68191 6 0 7 0 5.21123 3.97367 8 1 7 0 1.69148 1.84815 5 -1 7 0 4.50995 2.43067 5 1 7 0 0.30776 4.0758 6 -1 7 0 -1.8463 3.14657 8 -1 7 0 17.3344 5.92895 1 -1 7 0 10.4092 4.58819 6 1 7 0 8.32539 3.7212 1 1 7 0 9.62988 5.55187 9 2 7 0 16.0156 6.16319 6 -2 7 0 24.4789 7.59 6 -2 7 0 32.6222 6.20289 5 2 7 0 28.1588 3.9249 5 -2 7 0 41.0812 8.09919 8 2 7 0 17.2335 5.39209 1 2 7 0 30.4556 7.16064 9 3 7 0 0.12078 2.8853 1 -3 7 0 0.38747 1.90812 5 3 7 0 3.24193 2.1844 5 -3 7 0 4.50335 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32.4946 4.86287 5 -2 8 0 46.1404 7.41988 6 2 8 0 39.2452 4.02323 5 2 8 0 40.934 6.32309 1 -2 8 0 27.7557 6.0612 8 -3 8 0 43.9625 5.88852 5 3 8 0 42.6606 6.16038 1 3 8 0 48.9276 5.02834 5 -3 8 0 53.6138 7.56536 6 -3 8 0 58.1127 8.47663 8 4 8 0 357.355 17.9215 1 -4 8 0 378.945 17.2078 5 -4 8 0 408.791 20.1823 8 -4 8 0 380.568 19.7737 6 -5 8 0 36.913 4.29684 5 5 8 0 31.9674 4.58517 1 -5 8 0 43.9218 5.90916 6 -5 8 0 39.0141 4.65755 8 6 -8 0 13.7592 2.29101 12 6 8 0 13.294 2.75217 1 -6 8 0 8.41194 1.77769 8 -6 8 0 8.88157 2.25505 6 0 9 0 -0.3488 0.9934 5 0 9 0 -2.8283 2.62395 6 -1 9 0 43.9924 3.51959 5 1 9 0 46.9974 3.92387 5 -1 9 0 44.054 4.63069 6 2 9 0 100.473 6.44395 1 -2 9 0 120.687 6.09353 5 -2 9 0 117.844 7.50473 6 3 9 0 130.52 6.94652 1 -3 9 0 129.362 6.27718 5 -3 9 0 117.23 7.19936 6 -4 9 0 150.963 6.68138 5 4 9 0 176.894 10.0444 1 -4 9 0 161.906 8.24316 6 12 0 -1 137.896 8.46066 7 -12 0 1 134.916 7.32432 3 11 0 -1 0.55479 2.49235 7 -11 0 1 6.40692 3.37423 3 -10 0 1 343.863 20.9064 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59.7353 2.89524 11 1 0 1 48.9112 3.38713 10 -1 0 -1 55.6704 3.58602 4 -1 0 -1 52.724 3.91998 10 -2 0 -1 -1.1836 0.72511 10 2 0 1 1.12551 0.77755 11 -2 0 -1 -0.629 0.54968 11 2 0 1 0.72628 0.89386 10 -3 0 -1 838.349 32.6009 10 3 0 1 843.454 26.09 11 3 0 1 849.552 31.1658 10 -4 0 -1 1302.98 48.801 10 4 0 1 1226.92 38.8686 11 4 0 1 1366.49 49.8293 10 -5 0 -1 291.049 21.718 10 5 0 1 275.437 19.5518 10 5 0 1 246.868 13.1852 11 6 0 1 447.153 20.19 11 7 0 1 94.7671 10.7689 11 7 0 1 92.0659 11.0175 7 -7 0 -1 69.6348 10.1176 3 7 0 1 89.1883 6.0996 12 8 0 1 636.547 28.7076 11 -8 0 -1 707.902 33.3712 3 8 0 1 668.528 34.4455 7 8 0 1 665.906 26.1039 1 9 0 1 292.079 19.3746 7 -9 0 -1 296.359 19.7957 3 10 0 1 240.309 16.5287 7 -10 0 -1 239.574 16.5435 3 -11 0 -1 208.235 14.1198 3 11 0 1 222.663 13.3232 7 12 0 1 21.2189 2.82112 9 12 0 1 21.8483 3.44433 7 -12 0 -1 21.7808 2.7564 3 12 -1 -1 100.841 6.62465 7 -12 -1 1 111.079 8.24317 3 12 1 -1 100.212 7.47523 9 12 1 -1 111.475 7.74589 7 -11 -1 1 34.2028 6.26604 3 11 -1 -1 35.5564 6.36331 7 11 1 -1 51.7385 6.02637 7 -11 1 1 37.8251 5.1363 5 -11 1 1 35.5501 5.67404 3 -10 -1 1 161.723 14.1966 3 10 -1 -1 156.144 14.4269 7 10 1 -1 177.811 14.2636 7 -10 1 1 149.469 12.749 3 9 -1 -1 86.9568 6.00414 12 9 -1 -1 77.5614 11.9477 7 9 1 -1 78.6642 11.3564 7 -9 1 1 78.2264 8.23415 2 9 1 -1 67.8777 7.4463 1 -9 1 1 98.3906 11.3713 3 -8 -1 1 273.083 21.3448 3 8 -1 -1 283.51 20.1785 3 8 -1 -1 268.01 14.7455 12 8 -1 -1 314.927 24.1897 11 8 1 -1 260.51 20.9592 7 8 1 -1 303.75 15.6262 1 -8 1 1 311.601 20.323 3 -7 -1 1 599.969 30.7744 3 7 -1 -1 612.792 33.4025 7 7 -1 -1 600.624 30.562 3 7 -1 -1 611.477 23.989 12 -7 -1 1 622.163 39.0153 4 7 -1 -1 639.086 27.4996 11 7 1 -1 601.938 24.9271 1 7 1 -1 592.967 30.9443 7 7 1 -1 579.932 27.7365 3 -7 1 1 576.69 23.9486 8 -7 1 1 627.483 30.3885 3 -6 -1 1 482.158 27.5014 4 6 -1 -1 458.471 21.0122 11 -6 1 1 466.956 21.2563 4 -5 -1 1 266.582 19.0144 10 5 -1 -1 289.853 14.2998 11 -5 -1 1 313.195 19.8222 4 5 -1 -1 287.26 22.8033 10 -5 1 1 250.232 26.1651 10 5 1 -1 292.758 13.2595 11 5 1 -1 276.063 20.8828 10 -4 -1 1 2022.42 63.2956 4 4 -1 -1 1818.71 55.6278 11 4 -1 -1 1941.58 66.8159 10 -4 -1 1 2009.7 63.2109 10 4 1 -1 1911.41 54.281 11 -4 1 1 1960.66 55.5805 4 4 1 -1 1971.55 65.8204 10 -4 1 1 2021.16 64.9301 10 3 -1 -1 673.828 22.3561 11 -3 -1 1 674.859 25.8201 10 -3 -1 1 707.314 27.0743 4 3 -1 -1 688.897 28.885 10 3 1 -1 656.409 27.5284 10 -3 1 1 691.015 27.226 10 -3 1 1 671.885 21.0495 4 2 -1 -1 3663.33 96.0974 11 -2 -1 1 3792.19 100.769 4 -2 -1 1 3802.78 98.7607 10 2 -1 -1 3954.08 102.174 10 -2 1 1 3578.39 99.7029 10 2 1 -1 3660.99 100.559 10 1 -1 1 415.209 14.3961 10 1 -1 1 452.085 14.1307 11 -1 -1 -1 458.409 12.2648 11 -1 -1 -1 467.867 14.8272 10 1 -1 1 429.887 13.208 4 1 1 1 444.736 13.5622 10 -1 1 -1 458.999 12.9646 4 1 1 1 430.828 14.7895 2 2 -1 1 1030.71 30.5394 11 -2 -1 -1 1083.48 33.5687 10 2 -1 1 1033.87 33.0638 10 2 1 1 1082.54 31.9331 2 -2 1 -1 1043.23 28.6619 4 -2 1 -1 986.66 34.1394 10 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2 159.671 14.4336 8 4 7 -2 157.778 13.9765 1 -4 7 2 175.274 16.1272 6 -4 7 2 168.149 15.3944 9 -4 7 2 192.203 13.2827 5 4 7 -2 165.198 10.0155 5 -3 7 2 29.5658 7.60076 6 3 7 -2 48.7252 8.88046 1 -3 7 2 45.2613 9.78201 9 -3 7 2 57.4889 11.8184 8 -2 7 2 60.2265 10.6698 6 2 7 -2 62.0264 5.68619 5 -2 7 2 59.025 9.79197 9 2 7 -2 57.8681 8.8872 1 -2 7 2 53.7908 9.8491 8 -2 7 2 61.4199 7.32734 5 -1 7 2 33.8055 5.71203 5 1 7 -2 17.9933 5.68224 1 -1 7 2 54.2191 11.3356 6 1 7 -2 32.2803 4.59875 5 -1 7 2 24.2395 5.77696 8 1 7 -2 25.9018 5.2975 6 -1 7 2 26.6798 8.70906 2 -1 7 2 47.8066 9.71473 9 0 7 -2 15.6692 4.44645 6 0 7 -2 15.0402 5.01828 1 0 7 2 16.4427 5.50746 9 0 7 2 13.5308 5.09957 6 0 7 2 20.4815 6.10161 8 0 7 2 4.07163 6.34351 2 0 7 2 18.3662 3.97073 5 0 7 -2 13.9322 3.27501 5 1 7 2 45.8124 5.10934 5 1 7 2 57.6769 10.7795 6 -1 7 -2 48.1888 7.45436 6 1 7 2 31.1405 6.61394 8 -1 7 -2 43.2255 6.19234 5 -1 7 -2 29.6472 7.02733 1 1 7 2 35.0701 6.9909 9 1 7 2 33.4256 6.32049 1 -2 7 -2 62.793 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476.177 24.2406 12 5 -4 -3 448.744 28.7064 3 -5 -4 3 456.663 21.5705 12 5 -4 -3 453.875 21.7247 11 -5 -4 3 464.559 27.7676 3 -5 4 3 483.36 22.6662 2 -5 4 3 448.051 25.6266 9 5 4 -3 512.452 27.4926 1 5 4 -3 472.547 24.4606 7 -5 4 3 481.833 25.2386 8 -5 4 3 504.777 29.3142 6 5 4 -3 477.156 20.4337 5 -4 -4 3 305.497 21.4157 4 4 -4 -3 343.905 16.636 11 -4 4 3 349.43 17.9062 2 -4 4 3 328.63 20.0118 8 -4 4 3 338.972 24.0395 6 4 4 -3 314.647 18.8385 7 4 4 -3 323.721 14.7112 5 -4 4 3 306.745 20.0486 9 4 4 -3 321.51 21.2107 1 3 -4 -3 922.562 30.1496 11 -3 -4 3 893.683 36.8852 4 -3 4 3 796.914 34.7434 8 -3 4 3 841.839 40.819 6 3 4 -3 864.453 37.7506 1 3 4 -3 868.02 28.0398 5 -3 4 3 837.955 35.8467 9 -3 4 3 811.634 41.2806 2 2 -4 -3 563.742 25.1503 10 -2 -4 3 574.878 26.2002 4 2 -4 -3 596.076 20.7704 11 -2 4 3 618.386 25.4961 2 2 4 -3 622.982 24.556 10 1 -4 -3 1621.94 43.1919 11 -1 -4 3 1623.11 50.0923 4 1 -4 -3 1479.94 42.3985 4 1 -4 -3 1556.22 44.3963 4 -1 4 3 1622.39 52.1362 2 1 4 -3 1563.84 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8.89404 6 -5 -5 3 293.584 26.6642 3 5 -5 -3 283.585 19.1374 12 5 -5 -3 294.914 22.5041 3 -5 -5 3 272.802 16.8395 12 -5 5 3 287.644 21.0857 9 -5 5 3 281.364 18.8577 2 -5 5 3 285.804 19.3409 8 -5 5 3 287.355 22.0614 6 5 5 -3 292.511 14.9605 7 5 5 -3 276.569 15.0523 5 5 5 -3 291.225 20.4779 1 -5 5 3 310.239 19.524 5 4 -5 -3 359.203 20.8889 12 4 -5 -3 316.428 20.3157 11 4 5 -3 363.918 32.3713 1 -4 5 3 392.236 28.0203 8 -4 5 3 378.4 21.5842 2 4 5 -3 362.198 16.8497 7 -3 5 3 539.852 28.0001 9 -3 5 3 523.586 26.5371 2 3 5 -3 549.545 20.4439 5 -3 5 3 518.444 27.1495 8 3 5 -3 508.117 28.5723 1 -3 5 3 527.964 25.6154 5 -3 5 3 540.221 32.4206 6 -2 -5 3 178.1 13.8301 4 2 5 -3 165.337 15.8533 1 -2 5 3 173.446 14.7493 9 2 5 -3 173.833 9.70819 5 -2 5 3 168.699 13.8131 2 -2 5 3 172.132 12.3881 5 -2 5 3 188.574 15.4367 8 -2 5 3 213.035 19.674 6 -1 -5 3 96.108 8.73259 4 -1 5 3 95.5777 11.1027 2 -1 5 3 111.319 9.5932 5 1 5 -3 90.7309 11.6787 1 1 5 -3 103.211 8.10602 5 -1 5 3 84.6863 13.1282 6 -1 5 3 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344.41 22.0717 8 -1 7 -3 361.057 18.315 6 1 7 3 337.322 21.9671 9 -1 7 -3 329.46 22.6636 1 -1 7 -3 367.674 17.3177 5 1 7 3 357.941 23.7361 6 2 7 3 85.8586 8.03005 1 2 7 3 65.5808 11.5111 2 -2 7 -3 84.4148 8.27224 5 2 7 3 74.8062 11.8861 6 3 -7 3 1.72069 3.07937 12 -3 7 -3 11.4077 3.24778 5 -3 7 -3 4.84476 3.49636 1 3 7 3 12.4768 4.89556 8 3 7 3 8.58436 3.60147 1 -3 7 -3 11.3877 3.49521 8 3 7 3 14.249 4.36485 9 3 7 3 -1.2594 8.86235 6 -3 7 -3 9.61643 3.82277 6 4 -7 3 41.7064 5.55886 12 -4 7 -3 37.5368 5.28027 5 -4 7 -3 43.2371 5.98392 6 4 7 3 46.0381 7.80679 9 4 7 3 49.8639 5.96973 1 4 7 3 32.6828 6.3228 8 -4 7 -3 23.2917 6.49321 1 -4 7 -3 34.8552 4.71606 8 5 -7 3 4.68438 2.34075 12 -5 7 -3 4.63328 2.16818 5 5 7 3 3.84414 2.39163 9 -5 7 -3 3.11732 2.17507 6 -5 7 -3 6.24506 2.54107 8 5 7 3 2.36663 4.06118 8 5 7 3 1.73639 2.28295 1 6 -7 3 106.704 6.98144 12 6 7 3 99.2907 9.45034 9 -6 7 -3 105.759 7.28111 5 -6 7 -3 114.868 8.21534 6 6 7 3 91.9419 7.2244 1 7 -7 3 46.1307 4.15204 12 7 7 3 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91.4967 8.3863 7 7 4 4 108.446 10.3764 9 7 4 4 99.323 8.88806 1 7 4 4 114.159 11.3981 8 -7 4 -4 103.161 7.97585 6 8 -4 4 243.109 12.2618 12 -8 -4 -4 239.41 14.6622 3 8 4 4 241.818 14.625 9 -8 4 -4 231.855 12.8125 7 8 4 4 236.177 13.4721 1 -8 4 -4 235.481 11.3578 6 8 4 4 245.967 10.3491 7 8 4 4 229.02 14.0564 8 9 -4 4 27.9163 3.95228 12 -9 -4 -4 20.6891 4.13522 3 9 4 4 29.4221 4.17209 1 9 4 4 30.0866 5.02532 8 -9 4 -4 23.423 3.40485 7 9 4 4 22.6824 4.72517 9 -10 -4 -4 78.1634 5.24343 3 -10 4 -4 68.327 4.51234 7 10 4 4 75.4557 5.9052 9 -9 -5 4 -3.24 3.92754 3 9 -5 -4 -0.3294 1.536 12 -9 5 4 -0.3556 1.17523 5 8 -5 -4 185.622 14.6254 3 8 -5 -4 198.403 12.072 12 -8 -5 4 191.171 15.3629 3 -8 5 4 190.525 13.2001 5 -8 5 4 174.122 10.9839 8 8 5 -4 167.04 10.3134 1 -7 -5 4 165.579 15.5682 3 7 -5 -4 194.175 16.3761 3 7 -5 -4 184.293 13.116 12 7 5 -4 198.097 13.5936 1 -7 5 4 196.263 14.2464 6 7 5 -4 197.305 9.65807 7 -7 5 4 202.74 13.3183 8 -7 5 4 187.225 14.5273 9 7 5 -4 199.089 13.1995 5 -6 -5 4 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4 1058.14 35.4295 12 3 -5 4 1144.21 48.7325 11 -3 5 -4 1286.36 49.9572 6 3 5 4 1084.93 49.6144 2 -3 5 -4 1051.15 45.5213 5 -3 5 -4 1147.58 35.4005 7 3 5 4 1054.27 48.5858 6 -3 5 -4 1145.15 37.1763 8 3 5 4 1106.35 39.2121 1 4 -5 4 211.024 11.6779 12 4 -5 4 215.901 19.5988 11 4 5 4 204.717 20.0572 6 -4 5 -4 213.294 10.9499 7 4 5 4 215.358 15.3589 8 -4 5 -4 222.9 13.9886 6 4 5 4 197.186 14.4826 9 4 5 4 201.353 13.4785 1 4 5 4 202.555 19.5446 2 -4 5 -4 219.744 12.4833 8 -4 5 -4 210.154 12.9017 5 5 -5 4 384.874 16.9809 12 -5 5 -4 377.876 17.0931 8 -5 5 -4 410.951 16.6554 7 5 5 4 404.383 21.7425 9 -5 5 -4 376.127 18.1667 5 5 5 4 414.305 22.2156 8 -5 5 -4 388.885 19.3048 6 5 5 4 377.787 19.2287 1 6 -5 4 36.1543 5.45728 12 6 5 4 18.9925 6.60751 8 6 5 4 44.0855 6.84876 1 -6 5 -4 39.4078 6.00331 6 -6 5 -4 34.5873 5.78852 5 6 5 4 47.7272 7.44146 9 7 -5 4 24.3387 4.00474 12 -7 -5 -4 26.8369 5.54378 3 7 5 4 37.3771 6.23286 8 7 5 4 32.2344 5.62914 9 -7 5 -4 22.15 3.88852 6 -7 5 -4 25.9459 3.64875 7 7 5 4 28.1381 4.50377 1 -7 5 -4 21.4498 3.62563 5 -8 -5 -4 193.843 10.9974 3 8 -5 4 194.407 10.2404 12 -8 5 -4 190.267 9.46974 7 8 5 4 188.608 12.1392 9 8 5 4 204.562 12.3008 8 8 5 4 198.064 11.4079 1 -8 5 -4 216.527 11.5753 6 9 -5 4 83.6339 4.8776 12 -9 -5 -4 75.9735 8.31012 3 9 5 4 78.068 5.58219 1 -9 5 -4 85.6611 4.66841 7 9 5 4 73.814 6.38862 9 8 -6 -4 52.2717 5.32289 12 -8 6 4 56.9689 5.6664 5 8 6 -4 73.4851 7.6382 1 -8 6 4 56.4996 4.73556 8 -7 -6 4 10.7053 6.87919 3 7 -6 -4 2.01356 3.54305 3 7 -6 -4 7.13045 3.19556 12 -7 6 4 2.44788 2.91594 6 -7 6 4 -1.4036 2.16781 9 -7 6 4 5.98675 2.93885 5 7 6 -4 6.42245 2.89921 5 -7 6 4 3.38693 2.0776 8 -6 -6 4 280.274 20.6412 3 6 -6 -4 300.524 19.5409 3 6 -6 -4 311.187 17.4239 12 -6 -6 4 305.021 16.5896 12 -6 6 4 334.906 19.5859 8 -6 6 4 318.472 17.3218 5 6 6 -4 294.456 16.0308 5 -6 6 4 314.111 20.0593 6 6 6 -4 340.445 19.2447 1 -6 6 4 285.266 18.3024 9 -5 -6 4 157.942 11.7547 12 5 -6 -4 112.115 14.0357 3 5 -6 -4 140.922 12.333 12 -5 6 4 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750.496 37.7392 1 0 6 -4 783.744 28.0022 5 0 6 -4 764.982 28.709 6 0 6 4 762.598 36.5005 9 1 6 4 27.0651 6.62268 9 1 6 4 22.7352 6.8843 2 -1 6 -4 44.2139 9.50802 1 -1 6 -4 34.1965 5.69898 6 1 6 4 41.4531 8.1483 8 -1 6 -4 41.4707 5.11072 5 1 6 4 23.5549 6.80236 6 2 -6 4 797.41 29.1107 12 2 6 4 902.336 38.4149 9 2 6 4 831.297 30.4571 1 2 6 4 769.235 40.8829 6 -2 6 -4 848.571 30.9198 5 2 6 4 834.823 37.5144 8 2 6 4 776.54 41.7525 2 -2 6 -4 815.229 39.1589 1 -2 6 -4 874.994 32.7543 6 3 -6 4 267.448 13.5682 12 -3 6 -4 270.212 13.1335 8 3 6 4 269.96 15.0272 1 -3 6 -4 266.373 14.7139 5 3 6 4 270.701 21.5617 6 -3 6 -4 270.975 20.0634 1 -3 6 -4 274.595 16.2238 6 -3 6 -4 276.303 11.763 7 3 6 4 261.166 18.1747 9 3 6 4 278.951 18.6547 8 3 6 4 233.016 21.3118 2 4 -6 4 378.982 16.7526 12 -4 6 -4 379.953 17.9819 5 4 6 4 348.937 20.799 9 -4 6 -4 340.004 22.8068 1 -4 6 -4 368.268 18.7587 6 4 6 4 353.872 18.2816 1 4 6 4 356.188 20.9393 8 5 -6 4 181.498 10.6192 12 -5 6 -4 178.496 15.2868 1 -5 6 -4 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9 -6 5 5 30.5811 6.87713 6 -6 5 5 49.915 7.30846 5 6 5 -5 41.4111 6.14184 5 -5 -5 5 97.6207 9.58138 12 5 -5 -5 100.869 14.6486 3 -5 -5 5 80.2049 12.5437 3 5 -5 -5 96.9656 11.2052 12 5 5 -5 107.755 9.45634 5 -5 5 5 102.903 14.047 6 5 5 -5 113.611 11.8837 1 -5 5 5 115.725 24.7844 2 5 5 -5 111.8 10.3093 7 -5 5 5 108.074 11.247 8 -5 5 5 101.793 13.2978 9 -5 5 5 98.8931 10.3402 5 4 -5 -5 252.197 21.1633 3 4 -5 -5 282.897 17.3539 12 -4 -5 5 253.883 15.0257 12 -4 -5 5 242.405 19.6693 3 -4 5 5 256.76 19.7751 9 4 5 -5 238.658 16.027 7 -4 5 5 268.657 22.5575 6 4 5 -5 262.211 14.296 5 -4 5 5 247.604 16.4138 5 -4 5 5 292.922 19.6185 8 -4 5 5 275.633 19.9597 2 4 5 -5 275.478 20.3931 1 -3 -5 5 40.2497 6.59675 12 3 -5 -5 77.9894 10.8722 12 -3 5 5 52.5668 7.9453 5 -3 5 5 47.8005 9.53873 9 3 5 -5 42.3343 7.40531 7 -3 5 5 39.3449 9.65055 6 3 5 -5 39.2708 8.55378 1 -3 5 5 49.073 8.03573 2 3 5 -5 48.9335 5.46054 5 -3 5 5 70.0627 10.2138 8 -2 -5 5 81.8121 8.26293 12 -2 5 5 86.0709 11.876 9 2 5 -5 90.4314 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25.308 2 3 5 5 374.457 21.3651 9 3 5 5 366.527 21.8422 8 -3 5 -5 353.049 17.4506 6 3 5 5 307.703 16.1212 1 3 5 5 344.905 25.4888 6 4 -5 5 32.1797 5.17259 12 -4 5 -5 30.7874 4.39703 7 -4 5 -5 32.7689 5.14839 6 4 5 5 29.202 6.42755 9 4 5 5 36.5169 8.92577 6 -4 5 -5 46.0298 5.57374 5 4 5 5 24.1567 8.41062 2 5 -5 5 23.6117 4.18199 12 -5 5 -5 23.3634 4.88357 5 5 5 5 18.8689 4.43931 9 5 5 5 20.3623 4.74685 8 5 5 5 22.8293 4.68659 1 -5 5 -5 21.6526 3.86433 7 -5 5 -5 24.2747 4.34961 6 6 -5 5 76.0893 7.17257 12 -6 -5 -5 86.5486 8.4778 3 6 5 5 87.8069 9.31502 8 -6 5 -5 73.8271 6.55873 6 -6 5 -5 70.3948 6.12411 5 6 5 5 72.0007 8.43109 9 6 5 5 70.3277 7.41441 1 -6 5 -5 78.0184 6.2536 7 -7 -5 -5 9.489 3.42126 3 7 -5 5 13.0666 2.89592 12 7 5 5 20.8225 4.6174 8 7 5 5 10.1489 3.08073 9 -7 5 -5 17.8237 3.1356 6 7 5 5 14.9511 3.30185 1 -7 5 -5 17.0706 2.93029 7 8 -5 5 49.5067 4.4193 12 -8 -5 -5 39.7223 4.71288 3 8 5 5 37.9955 5.15373 9 8 5 5 30.5491 4.92793 8 8 5 5 47.43 4.51334 1 -8 5 -5 49.8774 4.03292 7 -9 5 -5 20.1305 2.05179 7 8 -6 -5 190.318 9.04881 12 -8 6 5 164.037 7.38182 8 -8 6 5 157.788 10.3112 5 7 -6 -5 125.062 9.96196 3 -7 -6 5 105.701 10.7822 3 7 -6 -5 128.305 8.73396 12 7 6 -5 108.889 7.86243 1 -7 6 5 107.308 7.81435 8 -7 6 5 114.266 8.32027 6 -7 6 5 114.516 8.20598 5 -7 6 5 115.568 9.55963 9 7 6 -5 106.858 8.1653 5 -6 -6 5 54.4428 6.47257 12 -6 -6 5 44.3808 8.3703 3 6 -6 -5 50.688 8.5872 3 6 -6 -5 55.3438 7.06945 12 6 6 -5 63.871 7.44402 1 -6 6 5 51.727 7.77836 9 6 6 -5 51.968 6.12259 5 -6 6 5 34.8457 6.6859 6 -6 6 5 59.5194 6.48605 5 -6 6 5 60.2168 7.88458 8 5 -6 -5 208.947 17.3952 3 -5 -6 5 181.564 12.7051 12 -5 -6 5 209.485 17.5139 3 5 -6 -5 207.015 14.4734 12 5 6 -5 213.057 15.6959 1 -5 6 5 193.907 16.9736 9 -5 6 5 191.291 12.5834 5 -5 6 5 186.906 16.6501 6 -5 6 5 175.804 14.1772 8 5 6 -5 189.676 12.0104 5 -4 -6 5 91.9407 14.4272 3 -4 -6 5 94.5231 8.52708 12 4 -6 -5 73.226 9.95265 12 -4 6 5 85.0568 12.0684 9 4 6 -5 89.739 7.59779 5 4 6 -5 76.4175 10.2737 1 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3 6 2.54738 1.96206 1 -6 3 -6 8.96722 3.29631 3 -6 3 -6 3.37042 2.08101 6 -6 3 -6 0.13686 1.48787 7 6 3 6 0.26344 2.10664 9 6 3 6 4.29452 2.2065 7 7 -3 6 1881.87 61.6942 7 -7 -3 -6 1937.78 59.9757 3 7 -3 6 1943.11 55.6442 12 -7 3 -6 2023.68 58.7358 7 7 3 6 2009.73 59.5214 1 7 3 6 1916.5 60.6859 9 -7 3 -6 1972.08 55.2469 3 7 3 6 1952.96 58.2358 7 -8 -3 -6 529.374 21.7552 3 8 -3 6 590.856 25.2899 7 8 -3 6 562.948 18.9628 12 -8 3 -6 527.967 20.9561 7 8 3 6 521.918 20.5494 7 8 3 6 556.263 24.0282 8 8 3 6 557.124 22.8911 9 -9 -3 -6 61.3171 5.30677 3 9 -3 6 69.9182 7.60402 7 9 3 6 53.3398 5.63932 9 9 3 6 56.1048 4.13962 7 -9 3 -6 56.7552 4.80836 7 9 3 6 51.3041 5.5332 8 -10 -3 -6 120.179 5.91399 3 -10 -3 -6 113.325 4.39165 12 10 3 6 114.418 6.36807 8 -10 3 -6 115.695 5.82934 7 -9 -4 6 21.7657 5.17618 3 9 -4 -6 13.1476 3.2838 3 9 -4 -6 10.6144 2.08561 12 9 4 -6 8.76468 2.26298 7 -9 4 6 16.0943 3.39945 5 8 -4 -6 57.9295 7.80113 3 -8 -4 6 34.8723 7.83074 3 8 -4 -6 49.3762 5.56157 12 8 4 -6 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188.081 10.9892 6 -5 4 -6 194.726 11.2511 7 5 4 6 195.634 10.9383 7 5 4 6 198.751 14.3194 9 5 4 6 198.931 14.4885 8 5 4 6 206.823 18.4977 6 -6 -4 -6 206.478 12.2383 3 6 -4 6 206.256 11.4824 12 6 4 6 205.364 13.9155 9 -6 4 -6 196.405 10.9819 6 6 4 6 210.924 10.4878 7 -6 4 -6 202.014 11.3306 7 6 4 6 200.362 11.972 1 6 4 6 198.763 14.4083 8 -7 -4 -6 273.943 13.7288 3 7 -4 6 283.281 12.9236 12 7 4 6 288.621 15.9226 9 7 4 6 290.009 14.4831 1 -7 4 -6 285.192 13.3622 7 7 4 6 287.367 16.8322 8 7 4 6 257.783 11.6133 7 8 -4 6 137.524 6.80772 12 -8 -4 -6 134.932 8.20793 3 8 4 6 141.939 13.0894 1 8 4 6 119.281 9.07857 9 8 4 6 131.743 9.96352 8 -8 4 -6 121.538 8.4081 7 -9 -4 -6 114.97 6.26536 3 -9 -4 -6 128.204 5.92318 12 -9 4 -6 119.506 6.29813 7 9 4 6 116.495 10.4003 9 9 4 6 151.119 9.6927 8 -8 -5 6 117.478 9.76024 3 8 -5 -6 104.773 7.25007 12 8 -5 -6 115.763 9.59701 3 -8 5 6 113.638 7.67041 5 7 -5 -6 92.3103 9.8962 3 -7 -5 6 72.0619 7.34315 12 -7 -5 6 71.8896 9.79834 3 7 -5 -6 70.4287 7.35893 12 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282.58 14.3867 12 -1 5 -6 265.434 15.5701 7 -1 5 -6 260.5 20.9044 1 -1 5 -6 281.463 13.0268 5 1 5 6 268.728 19.1849 8 1 5 6 296.766 19.8185 9 -1 5 -6 269.866 13.385 6 1 5 6 269.664 22.1766 2 1 5 6 297.68 24.6552 6 2 -5 6 2.5675 2.57867 12 -2 5 -6 -1.8777 1.40308 7 2 5 6 -0.8677 4.59671 6 2 5 6 -1.0073 3.54592 9 -2 5 -6 3.16003 2.078 6 2 5 6 5.78803 4.9172 2 -2 5 -6 -0.5848 1.47578 5 2 5 6 1.29825 2.7558 8 3 -5 6 231.705 12.8809 12 -3 5 -6 211.359 11.9768 6 -3 5 -6 216.545 12.4827 7 3 5 6 209.154 19.578 6 3 5 6 223.426 16.4756 9 3 5 6 227.987 12.5275 1 3 5 6 254.838 21.5116 2 -3 5 -6 206.721 10.9558 5 3 5 6 224.427 16.77 8 4 -5 6 906.823 31.7283 12 4 5 6 896.841 36.8784 9 -4 5 -6 924.827 30.7817 7 4 5 6 820.583 44.6419 2 4 5 6 895.233 37.8118 8 -5 -5 -6 12.3342 3.33666 3 5 -5 6 16.4975 3.56797 12 -5 5 -6 13.7537 2.8465 6 -5 5 -6 17.9585 2.8554 5 5 5 6 9.12453 3.54443 8 5 5 6 14.0307 7.97412 6 5 5 6 10.3372 4.06755 9 -5 5 -6 21.572 3.86607 7 5 5 6 18.7814 3.8884 1 6 -5 6 25.9278 3.86619 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32.8396 6.28732 1 5 4 -7 16.688 5.11233 7 -5 4 7 36.6643 8.28386 9 4 -4 -7 4.46524 4.3287 3 4 -4 -7 8.92271 4.28347 12 -4 -4 7 6.32078 3.12657 12 4 4 -7 3.4128 3.60004 7 -4 4 7 0.29997 3.84972 6 -4 4 7 8.63765 5.14892 9 4 4 -7 6.02417 2.54909 5 4 4 -7 2.11142 4.08704 1 -4 4 7 12.0889 5.98129 2 -4 4 7 13.9594 5.48578 8 3 -4 -7 513.606 24.862 12 3 -4 -7 535.375 31.3731 3 -3 -4 7 562.196 23.1941 12 -3 4 7 548.502 29.4746 9 3 4 -7 565.403 30.5404 1 -3 4 7 595.431 35.9379 6 3 4 -7 547.542 29.3653 7 -3 4 7 593.391 30.7924 2 -3 4 7 531.757 27.8564 8 3 4 -7 564.35 23.1406 5 2 -4 -7 218.139 19.0938 3 -2 -4 7 215.445 12.5391 12 2 -4 -7 204.922 13.8339 12 -2 4 7 189.621 16.337 8 -2 4 7 208.07 17.1388 9 2 4 -7 216.962 16.481 7 -2 4 7 215.768 21.5052 6 2 4 -7 209.089 18.5983 1 2 4 -7 217.928 12.0946 5 -2 4 7 220.305 17.6909 2 -1 -4 7 685.415 25.1303 12 1 -4 -7 650.641 32.8358 3 1 -4 -7 716.698 26.7722 12 -1 4 7 667.553 39.0334 6 -1 4 7 717.028 35.671 2 1 4 -7 688.13 35.1647 1 1 4 -7 688.629 31.772 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9 -3 4 -7 497.267 21.4059 7 -3 4 -7 491.53 17.9739 5 -3 4 -7 526.679 20.7152 6 3 4 7 528.899 21.0186 1 -4 -4 -7 137.273 9.99929 3 4 -4 7 128.669 9.2158 12 4 4 7 130.115 12.0867 9 4 4 7 141.881 12.6194 8 4 4 7 165.682 17.2438 6 4 4 7 119.559 9.11514 1 -4 4 -7 129.49 9.32908 7 4 4 7 110.464 19.207 2 -4 4 -7 131.538 9.138 6 -5 -4 -7 36.9721 5.36509 3 5 -4 7 35.8772 4.81202 12 5 4 7 36.2673 7.94091 6 5 4 7 33.3768 4.99833 1 5 4 7 31.5145 6.35646 8 -5 4 -7 36.6945 4.76757 7 5 4 7 34.9556 6.23784 9 -6 -4 -7 223.802 11.8393 3 6 -4 7 215.62 10.8241 12 6 4 7 235.123 15.0924 8 6 4 7 206.715 13.5367 9 -6 4 -7 218.511 11.5725 7 -7 -4 -7 203.371 10.5756 3 -7 -4 -7 207.113 9.45256 12 -7 4 -7 212.385 10.6421 7 7 4 7 240.969 15.0851 9 7 4 7 198.925 12.6389 8 -8 -4 -7 37.2664 6.32918 3 -8 -4 -7 41.8889 3.3663 12 8 4 7 47.0018 5.14804 8 -8 4 -7 42.6907 3.99097 7 8 4 7 39.7234 5.11708 9 8 -5 -7 248.315 12.279 3 -8 -5 7 243.152 12.5689 3 8 -5 -7 240.539 10.248 12 -8 5 7 228.361 10.5914 5 -7 -5 7 43.7768 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5 -7 85.2935 7.35671 7 6 5 7 91.0286 8.63618 8 -7 -5 -7 8.64858 4.45022 3 -7 -5 -7 1.45716 1.03997 12 7 -5 7 3.79374 1.13788 12 7 5 7 5.44429 1.82605 9 -7 5 -7 2.1416 2.80333 1 -8 -5 -7 36.2361 2.53775 12 8 5 7 28.6736 4.04625 8 8 5 7 25.0748 4.70622 9 7 -6 -7 25.2447 3.30149 12 6 -6 -7 14.365 2.79813 12 -6 -6 7 3.06105 3.79244 3 -6 -6 7 13.904 3.03646 12 6 -6 -7 4.21995 3.98086 3 6 6 -7 11.9351 2.75529 5 -6 6 7 10.2229 2.53521 8 -6 6 7 12.8209 3.2635 9 -6 6 7 7.30676 2.93816 6 6 6 -7 13.9201 3.03874 1 -5 -6 7 85.6623 9.89271 3 -5 -6 7 77.7648 7.15565 12 5 -6 -7 87.5893 7.93156 12 5 6 -7 85.0186 7.7419 5 5 6 -7 65.3541 7.07481 1 -5 6 7 80.3387 8.94805 9 -5 6 7 75.4794 8.91438 6 -5 6 7 82.9881 7.87756 8 -4 -6 7 169.573 14.3755 3 4 -6 -7 167.718 14.8637 3 -4 -6 7 194.269 11.6004 12 4 6 -7 172.412 10.6215 5 -4 6 7 163.072 12.4667 8 -4 6 7 169.741 14.3597 9 4 6 -7 174.816 12.8658 1 -4 6 7 156.835 14.8846 6 3 -6 -7 175.095 12.3343 12 -3 -6 7 190.96 11.5796 12 -3 -6 7 176.562 17.7702 3 -3 6 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