#------------------------------------------------------------------------------ #$Date: 2020-03-04 08:13:49 +0200 (Wed, 04 Mar 2020) $ #$Revision: 248737 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/74/1557436.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1557436 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.0195 _cell_length_b 18.7418 _cell_length_c 19.7401 _exptl_crystal_F_000 3352.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file wm4124Isup2.hkl _cod_data_source_block I _shelx_title ' 1a in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 711.16 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 74943.16 62611.27 1242.96 o 6 0 0 200588.14 181294.44 4282.83 o 8 0 0 62089.69 61277.73 1426.42 o 10 0 0 33569.88 35671.68 847.86 o 12 0 0 73150.83 80187.19 2068.42 o 14 0 0 46616.55 54291.52 1368.52 o 16 0 0 16464.01 19170.44 550.22 o 18 0 0 60128.29 74410.13 1968.10 o 20 0 0 924.03 1105.96 296.82 o 4 1 0 9212.72 9358.06 163.51 o 6 1 0 23651.25 22601.29 382.31 o 8 1 0 20007.83 18726.56 449.37 o 10 1 0 77590.01 81866.58 1830.67 o 12 1 0 51144.55 57684.41 1070.77 o 14 1 0 5731.85 5901.98 186.78 o 16 1 0 75625.50 89488.62 1545.91 o 18 1 0 61.65 -177.81 177.81 o 20 1 0 364.71 107.36 236.79 o 2 2 0 1440.75 1286.33 49.48 o 4 2 0 52156.71 56762.84 694.43 o 6 2 0 28058.20 27013.96 425.12 o 8 2 0 16840.90 15826.96 301.76 o 10 2 0 95631.95 99766.92 1924.40 o 12 2 0 44994.27 46082.46 1172.53 o 14 2 0 88.46 -111.61 111.61 o 16 2 0 5644.65 6305.49 207.61 o 18 2 0 31033.35 36383.75 739.07 o 20 2 0 10201.65 11646.19 442.22 o 2 3 0 39093.54 40849.91 472.89 o 4 3 0 4328.63 4759.10 85.62 o 6 3 0 18184.14 18163.87 294.47 o 8 3 0 27123.05 26706.19 461.12 o 10 3 0 570.37 232.65 76.61 o 12 3 0 7400.53 7199.04 201.15 o 14 3 0 565.13 236.29 124.65 o 16 3 0 9439.00 10046.45 270.50 o 18 3 0 2693.63 2943.48 215.92 o 20 3 0 1285.95 1154.25 235.07 o 0 4 0 9224.66 10061.28 169.86 o 2 4 0 155.69 262.03 24.37 o 4 4 0 82590.30 89165.71 1269.42 o 6 4 0 22005.65 22309.39 338.93 o 8 4 0 66767.27 63088.02 1044.78 o 10 4 0 136473.50 133753.41 2190.28 o 12 4 0 37710.78 37032.97 818.09 o 14 4 0 32969.58 32601.80 949.16 o 16 4 0 21159.14 23893.81 690.77 o 18 4 0 189.11 -191.80 191.80 o 20 4 0 1209.41 1160.89 230.55 o 2 5 0 20558.31 21239.78 274.90 o 4 5 0 106040.92 113064.35 1546.17 o 6 5 0 497.84 458.67 50.29 o 8 5 0 2665.50 3083.96 101.46 o 10 5 0 6256.74 6087.77 181.49 o 12 5 0 3189.24 2831.71 128.09 o 14 5 0 21660.65 20434.13 566.36 o 16 5 0 6030.38 6628.05 271.06 o 18 5 0 9155.22 10427.83 393.52 o 20 5 0 848.94 953.39 264.41 o 0 6 0 189092.70 200209.81 3665.67 o 2 6 0 7460.70 8268.25 123.72 o 4 6 0 13795.02 13489.34 204.61 o 6 6 0 255601.62 270170.62 3906.26 o 8 6 0 4953.02 5042.83 125.22 o 10 6 0 4309.89 4044.55 135.16 o 12 6 0 30915.26 28227.60 570.02 o 14 6 0 4628.91 4554.76 237.57 o 16 6 0 13822.48 14850.56 517.14 o 18 6 0 4502.25 4398.70 248.31 o 20 6 0 318.18 274.34 239.62 o 2 7 0 15646.23 17220.23 236.89 o 4 7 0 1131.68 1053.09 49.44 o 6 7 0 28494.72 29257.07 441.76 o 8 7 0 29000.61 28436.27 437.56 o 10 7 0 18188.82 18601.47 344.75 o 12 7 0 6430.37 6082.00 180.38 o 14 7 0 8583.49 7695.35 240.02 o 16 7 0 12243.67 11068.81 414.91 o 18 7 0 8717.04 8303.17 325.96 o 20 7 0 525.05 225.41 265.26 o 0 8 0 21770.13 23081.26 494.12 o 2 8 0 68144.88 68423.01 943.74 o 4 8 0 107039.41 108865.19 1522.45 o 6 8 0 8942.65 8882.40 167.97 o 8 8 0 950.02 1155.54 68.39 o 10 8 0 1795.75 1780.37 102.47 o 12 8 0 5489.83 5357.48 178.02 o 14 8 0 18609.76 17072.93 392.86 o 16 8 0 19324.15 18651.51 767.13 o 18 8 0 3030.77 2809.38 257.23 o 20 8 0 7131.65 7597.66 356.47 o 2 9 0 81477.47 83263.53 1191.95 o 4 9 0 74232.38 74241.96 1026.44 o 6 9 0 47819.54 50618.36 751.33 o 8 9 0 13270.00 14325.75 252.18 o 10 9 0 39277.63 39689.96 635.47 o 12 9 0 24503.10 22535.43 593.99 o 14 9 0 26343.97 24920.89 479.58 o 16 9 0 5391.53 4923.79 285.11 o 18 9 0 1611.44 1535.05 242.34 o 0 10 0 70307.51 67798.78 1409.05 o 2 10 0 103703.41 104740.46 1529.13 o 4 10 0 83885.72 84818.84 1171.24 o 6 10 0 8963.87 8713.16 184.73 o 8 10 0 59755.55 59577.26 904.16 o 10 10 0 35.24 -14.17 98.36 o 12 10 0 39611.76 37783.09 790.11 o 14 10 0 65269.34 60406.74 1153.63 o 16 10 0 4982.79 4371.58 267.84 o 18 10 0 4521.26 4176.92 332.53 o 2 11 0 130921.70 131869.77 1921.63 o 4 11 0 11607.86 11519.86 201.68 o 6 11 0 9829.65 10242.09 212.36 o 8 11 0 1786.12 1889.36 91.48 o 10 11 0 50051.46 49717.44 848.48 o 12 11 0 23612.66 23605.54 508.22 o 14 11 0 273.10 65.24 144.12 o 16 11 0 30696.06 28440.75 686.52 o 18 11 0 129.26 -337.19 337.19 o 0 12 0 61001.59 60612.52 1388.46 o 2 12 0 1270.56 1790.38 112.94 o 4 12 0 930.75 920.82 79.49 o 6 12 0 12129.66 12333.05 254.47 o 8 12 0 10131.18 9835.23 213.76 o 10 12 0 2764.69 2697.71 128.47 o 12 12 0 17595.56 16964.55 423.28 o 14 12 0 18383.66 18127.73 675.06 o 16 12 0 22.57 -225.37 225.37 o 18 12 0 457.74 -344.71 344.71 o 2 13 0 819.41 664.19 91.91 o 4 13 0 7000.46 6423.80 154.02 o 6 13 0 25523.99 26125.05 468.78 o 8 13 0 19274.13 19172.31 369.23 o 10 13 0 329.99 275.53 131.36 o 12 13 0 3908.77 3761.45 174.73 o 14 13 0 15211.27 14357.88 495.87 o 16 13 0 7221.31 7158.72 361.18 o 0 14 0 3012.78 3077.79 173.71 o 2 14 0 2770.29 3147.60 126.77 o 4 14 0 485.55 462.12 96.08 o 6 14 0 62.54 103.40 98.55 o 8 14 0 5337.12 5539.21 175.72 o 10 14 0 10289.17 10234.07 260.55 o 12 14 0 4092.27 3951.55 185.07 o 14 14 0 673.29 205.07 216.37 o 16 14 0 613.23 170.59 322.65 o 2 15 0 51.94 310.95 115.71 o 4 15 0 52718.10 52268.05 887.09 o 6 15 0 1691.00 1682.47 116.99 o 8 15 0 4729.39 4969.13 185.37 o 10 15 0 11733.44 11766.39 301.22 o 12 15 0 102.02 -112.59 174.03 o 14 15 0 29.17 -222.99 222.99 o 0 16 0 1332.41 1308.00 167.73 o 2 16 0 55995.82 54841.63 953.71 o 4 16 0 130.29 355.45 117.63 o 6 16 0 54231.78 52422.35 976.65 o 8 16 0 2953.20 3448.90 172.91 o 10 16 0 52.09 82.80 172.26 o 12 16 0 19360.76 18597.05 473.10 o 14 16 0 1260.96 732.35 269.84 o 2 17 0 1340.34 2023.28 136.32 o 4 17 0 44743.97 44619.70 794.54 o 6 17 0 1590.02 1604.24 167.82 o 8 17 0 1666.14 1794.62 168.15 o 10 17 0 7304.92 7122.19 258.61 o 12 17 0 193.00 221.39 195.69 o 0 18 0 6709.55 6617.43 299.82 o 2 18 0 4964.27 4975.04 178.50 o 4 18 0 3722.60 3879.69 179.50 o 6 18 0 2654.72 2745.95 188.79 o 8 18 0 53.24 -135.22 197.46 o 10 18 0 1965.59 2344.46 207.46 o 12 18 0 168.12 475.88 209.63 o 2 19 0 6077.20 6201.45 208.50 o 4 19 0 955.40 1075.47 154.53 o 6 19 0 268.33 462.91 184.55 o 8 19 0 4238.12 4386.78 250.39 o 10 19 0 1958.33 2165.59 240.84 o 0 20 0 56.59 693.24 218.80 o 2 20 0 23117.28 22718.79 487.21 o 4 20 0 10907.93 10962.90 304.58 o 6 20 0 7481.73 7558.55 294.90 o 8 20 0 2626.72 3035.08 248.69 o 2 21 0 4167.15 4618.34 216.85 o 4 21 0 13396.95 13578.32 380.44 o 6 21 0 4088.22 4123.08 257.67 o 0 22 0 7972.55 8124.10 407.98 o 2 22 0 6400.11 5950.52 278.40 o 3 1 1 6041.06 6405.86 72.00 o 4 1 1 7425.60 7465.73 81.57 o 5 1 1 6298.25 5956.75 80.79 o 6 1 1 191.23 149.19 33.80 o 7 1 1 14006.02 13438.61 179.14 o 8 1 1 1391.88 1225.28 52.46 o 9 1 1 26246.16 26939.53 372.93 o 10 1 1 8862.21 8629.94 172.76 o 11 1 1 3411.48 3770.17 98.39 o 12 1 1 758.56 477.85 66.49 o 13 1 1 7844.58 8148.90 177.07 o 14 1 1 1007.30 941.00 90.58 o 15 1 1 87.11 -77.22 77.22 o 16 1 1 6447.14 6688.51 146.17 o 17 1 1 163.26 223.62 124.83 o 18 1 1 214.45 -46.78 130.93 o 19 1 1 952.79 881.02 141.90 o 20 1 1 45.91 -148.39 148.39 o 21 1 1 7806.83 8663.95 246.17 o 2 2 1 3807.13 3833.76 49.69 o 3 2 1 93785.24 100543.20 898.78 o 4 2 1 4646.11 4982.47 56.01 o 5 2 1 80194.67 84208.29 847.87 o 6 2 1 2047.32 1881.93 46.31 o 7 2 1 8156.00 7907.46 117.55 o 8 2 1 48.88 -41.91 41.91 o 9 2 1 1028.62 764.10 50.96 o 10 2 1 9554.38 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392.39 o 0 4 1 24876.36 25915.15 311.36 o 1 4 1 512.25 630.12 17.99 o 2 4 1 104734.59 110865.51 902.19 o 3 4 1 25209.21 26687.72 249.97 o 4 4 1 9846.91 10360.31 113.92 o 5 4 1 48533.92 49917.48 516.64 o 6 4 1 25254.45 25044.30 273.23 o 7 4 1 52733.96 52448.73 577.51 o 8 4 1 48004.75 47400.51 546.13 o 9 4 1 525.91 432.42 47.43 o 10 4 1 14212.20 13431.17 218.51 o 11 4 1 19719.82 18337.77 284.75 o 12 4 1 51.04 -61.66 61.66 o 13 4 1 14530.44 14275.80 263.11 o 14 4 1 7367.54 7092.08 154.46 o 15 4 1 3114.26 3130.87 111.95 o 16 4 1 1689.67 1728.62 110.01 o 17 4 1 846.92 850.20 131.29 o 18 4 1 2551.59 2343.06 157.08 o 19 4 1 10808.19 12602.89 273.60 o 20 4 1 17476.24 21463.69 438.19 o 21 4 1 4758.61 6207.38 235.28 o 1 5 1 30086.24 31678.49 292.69 o 2 5 1 22775.10 24495.91 222.76 o 3 5 1 69804.64 73393.95 675.11 o 4 5 1 61185.09 62019.51 598.03 o 5 5 1 55662.41 56054.91 600.00 o 6 5 1 24877.61 25516.40 278.80 o 7 5 1 810.68 889.92 42.19 o 8 5 1 67553.75 69714.58 783.87 o 9 5 1 128834.62 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6 1 14563.83 15968.66 397.21 o 1 7 1 17047.41 17602.17 176.49 o 2 7 1 642.22 626.17 28.10 o 3 7 1 4266.47 4611.15 64.18 o 4 7 1 4961.29 5331.89 73.67 o 5 7 1 5631.30 5449.43 79.41 o 6 7 1 1574.27 1937.56 48.50 o 7 7 1 9946.29 10650.71 135.44 o 8 7 1 10060.91 10619.86 141.51 o 9 7 1 83043.17 83537.84 950.57 o 10 7 1 42.97 -62.19 65.15 o 11 7 1 5230.41 4813.08 108.86 o 12 7 1 142.26 -75.93 75.93 o 13 7 1 5695.34 5061.52 138.59 o 14 7 1 733.42 340.38 89.07 o 15 7 1 4554.40 4354.82 173.47 o 16 7 1 685.42 496.08 130.62 o 17 7 1 10033.69 10074.31 259.59 o 18 7 1 175.42 -81.85 150.19 o 19 7 1 462.77 89.72 171.72 o 20 7 1 162.02 -210.91 216.88 o 0 8 1 66796.02 68932.92 987.66 o 1 8 1 3717.36 3686.26 57.10 o 2 8 1 7238.74 7720.16 91.87 o 3 8 1 31.35 58.77 31.02 o 4 8 1 13292.14 14102.01 151.41 o 5 8 1 556.33 626.37 39.13 o 6 8 1 39685.09 40925.86 436.47 o 7 8 1 14301.13 14805.54 178.24 o 8 8 1 797.67 762.95 51.76 o 9 8 1 46.20 -8.66 56.03 o 10 8 1 10936.92 10675.47 160.41 o 11 8 1 2.70 -69.69 69.69 o 12 8 1 40043.61 37978.20 477.35 o 13 8 1 1361.66 872.03 86.23 o 14 8 1 41.64 -85.24 85.24 o 15 8 1 10291.42 9064.57 236.68 o 16 8 1 5380.46 5002.05 199.42 o 17 8 1 28.09 -155.84 155.84 o 18 8 1 5440.86 5733.19 221.75 o 19 8 1 2.99 -170.91 170.91 o 20 8 1 57.71 -204.36 204.36 o 1 9 1 1366.34 1250.63 40.64 o 2 9 1 4927.48 5148.48 73.98 o 3 9 1 29222.87 30046.88 311.46 o 4 9 1 8168.38 8374.62 106.43 o 5 9 1 896.90 793.21 44.85 o 6 9 1 504.02 676.29 45.19 o 7 9 1 737.04 807.44 48.71 o 8 9 1 7454.94 7665.83 115.68 o 9 9 1 4530.81 4630.59 89.22 o 10 9 1 2043.85 2136.65 75.98 o 11 9 1 1941.26 1999.37 83.67 o 12 9 1 80.33 -78.71 78.71 o 13 9 1 857.43 632.21 87.46 o 14 9 1 106.42 -93.77 93.77 o 15 9 1 3785.65 3265.02 162.64 o 16 9 1 2598.59 2179.93 145.24 o 17 9 1 624.81 133.07 162.19 o 18 9 1 1761.53 1461.36 186.99 o 19 9 1 5638.54 5605.32 262.82 o 0 10 1 2789.83 2769.74 78.32 o 1 10 1 578.93 663.71 43.11 o 2 10 1 22962.49 23437.84 251.42 o 3 10 1 3273.73 2897.28 58.41 o 4 10 1 29263.88 29415.09 308.37 o 5 10 1 36787.21 37060.07 399.91 o 6 10 1 15920.33 16198.66 196.74 o 7 10 1 5022.27 5330.63 90.69 o 8 10 1 14593.62 14895.39 186.04 o 9 10 1 25230.28 25887.17 309.16 o 10 10 1 126.02 114.81 69.15 o 11 10 1 7337.71 7131.87 134.24 o 12 10 1 1491.39 1301.02 91.27 o 13 10 1 34406.65 32322.89 549.50 o 14 10 1 8458.63 7986.56 219.43 o 15 10 1 1579.43 1013.42 132.26 o 16 10 1 8158.53 7221.29 252.01 o 17 10 1 1684.83 1315.34 165.36 o 18 10 1 3256.01 3328.03 195.20 o 19 10 1 2621.67 2179.39 207.02 o 1 11 1 6785.66 6690.49 98.57 o 2 11 1 16525.73 16079.54 188.87 o 3 11 1 71066.50 71393.77 743.70 o 4 11 1 6926.64 7013.33 101.77 o 5 11 1 3291.82 3272.00 72.89 o 6 11 1 315.68 373.30 52.19 o 7 11 1 191.87 207.61 55.56 o 8 11 1 3365.77 3651.70 80.30 o 9 11 1 11446.50 11666.04 169.46 o 10 11 1 1387.31 1537.56 76.54 o 11 11 1 27988.43 27323.37 358.30 o 12 11 1 13249.96 13393.77 267.82 o 13 11 1 934.56 550.46 101.15 o 14 11 1 1354.36 1180.35 122.07 o 15 11 1 10548.14 9758.95 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14675.21 14364.44 367.85 o 15 8 5 3500.05 3271.90 150.34 o 16 8 5 1814.77 1323.03 140.10 o 17 8 5 125.41 -156.66 156.66 o 18 8 5 3648.09 3614.65 265.31 o 19 8 5 7983.64 8311.39 352.21 o 1 9 5 103112.30 103892.01 1071.45 o 2 9 5 17556.70 17491.46 195.90 o 3 9 5 2752.85 3094.30 64.84 o 4 9 5 79520.58 81651.93 916.51 o 5 9 5 28561.20 27978.78 330.91 o 6 9 5 2454.20 2343.31 65.42 o 7 9 5 7533.98 7018.52 115.36 o 8 9 5 5137.30 5101.25 96.04 o 9 9 5 4115.08 4070.97 87.82 o 10 9 5 28502.88 28271.75 351.56 o 11 9 5 26255.57 26342.61 344.65 o 12 9 5 5730.15 5300.69 123.92 o 13 9 5 1378.19 1264.37 107.47 o 14 9 5 1362.17 900.70 119.52 o 15 9 5 306.04 -124.91 124.91 o 16 9 5 3632.52 3194.87 165.38 o 17 9 5 28407.69 29477.62 916.77 o 18 9 5 6653.69 6519.70 382.46 o 19 9 5 2895.71 3115.52 370.62 o 0 10 5 2357.82 2348.40 79.25 o 1 10 5 10187.56 9987.64 130.54 o 2 10 5 532.34 491.38 42.67 o 3 10 5 29977.38 29165.77 338.86 o 4 10 5 4951.45 5521.06 103.66 o 5 10 5 10348.24 10252.32 155.62 o 6 10 5 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296.32 o 1 12 5 1051.73 999.68 51.71 o 2 12 5 135.08 276.14 54.80 o 3 12 5 17432.95 17206.20 225.79 o 4 12 5 6702.02 6671.20 121.95 o 5 12 5 8666.76 8384.10 145.75 o 6 12 5 55.11 -34.18 57.47 o 7 12 5 9799.36 9668.77 157.80 o 8 12 5 1737.15 1503.81 79.18 o 9 12 5 782.87 870.27 93.25 o 10 12 5 445.06 365.31 92.69 o 11 12 5 7978.91 8395.89 171.78 o 12 12 5 163.91 115.16 105.19 o 13 12 5 512.58 188.75 125.25 o 14 12 5 9098.70 9048.27 228.64 o 15 12 5 9.77 -142.92 142.92 o 16 12 5 1842.18 1206.66 164.84 o 17 12 5 1431.42 1086.88 242.63 o 1 13 5 11579.50 11239.99 160.03 o 2 13 5 3169.74 3226.22 81.43 o 3 13 5 17635.58 17280.99 236.21 o 4 13 5 209.23 191.91 69.49 o 5 13 5 1915.18 1906.43 87.33 o 6 13 5 3581.65 3668.27 96.90 o 7 13 5 7021.08 7044.27 143.26 o 8 13 5 2004.27 2010.18 99.67 o 9 13 5 33946.26 34239.21 462.44 o 10 13 5 1852.48 1889.61 109.55 o 11 13 5 36714.55 36946.62 504.74 o 12 13 5 2017.41 2077.67 132.44 o 13 13 5 9213.93 9283.29 212.79 o 14 13 5 1310.08 990.70 147.61 o 15 13 5 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6 47553.94 47070.80 725.58 o 1 6 6 16761.94 17260.17 192.88 o 2 6 6 397.70 399.01 27.39 o 3 6 6 178.58 274.08 32.59 o 4 6 6 2460.53 2697.70 54.09 o 5 6 6 20759.25 22968.50 269.20 o 6 6 6 56400.68 58433.07 661.63 o 7 6 6 546.15 677.48 51.51 o 8 6 6 8.59 -20.49 44.51 o 9 6 6 1516.39 1536.12 67.36 o 10 6 6 12346.53 12156.38 170.16 o 11 6 6 186.23 -19.29 73.61 o 12 6 6 31085.87 30848.05 400.04 o 13 6 6 7627.08 7478.49 161.44 o 14 6 6 5766.63 5089.92 136.75 o 15 6 6 162.03 -122.06 122.06 o 16 6 6 380.44 -42.30 141.46 o 17 6 6 1136.15 268.84 165.59 o 18 6 6 6200.99 6165.23 280.74 o 19 6 6 327.32 -183.47 183.47 o 1 7 6 74800.16 74077.34 790.89 o 2 7 6 68456.73 69043.89 764.29 o 3 7 6 11881.25 12932.84 151.80 o 4 7 6 129.60 243.68 38.64 o 5 7 6 9042.17 9868.85 136.11 o 6 7 6 2358.28 2154.91 56.30 o 7 7 6 1272.80 1146.38 54.07 o 8 7 6 20002.67 20014.71 250.86 o 9 7 6 11323.30 10888.98 151.86 o 10 7 6 14794.79 14551.71 208.32 o 11 7 6 18930.68 18650.35 253.38 o 12 7 6 1296.32 1014.29 89.33 o 13 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6 9 6 16828.57 16477.56 216.55 o 7 9 6 510.88 454.13 66.49 o 8 9 6 6170.99 6359.37 125.66 o 9 9 6 29168.24 29604.74 367.67 o 10 9 6 1711.60 1526.07 84.25 o 11 9 6 1316.65 1031.93 81.64 o 12 9 6 1283.07 923.60 96.07 o 13 9 6 2568.89 2453.54 125.42 o 14 9 6 2148.21 2010.89 131.82 o 15 9 6 611.51 221.71 139.79 o 16 9 6 11365.78 11512.44 335.90 o 17 9 6 10.95 -171.62 171.62 o 18 9 6 3134.36 2800.24 214.73 o 0 10 6 8805.92 8811.09 174.39 o 1 10 6 2391.99 2648.67 62.80 o 2 10 6 5390.69 5168.90 85.34 o 3 10 6 2474.96 2450.08 66.62 o 4 10 6 4729.37 4837.01 94.49 o 5 10 6 9157.07 9024.95 149.27 o 6 10 6 685.00 567.48 64.26 o 7 10 6 14819.08 14495.21 203.72 o 8 10 6 1760.01 1588.81 82.23 o 9 10 6 677.24 604.29 71.03 o 10 10 6 124.51 -68.65 73.97 o 11 10 6 13060.29 12544.81 205.61 o 12 10 6 1972.10 1799.12 116.56 o 13 10 6 64.72 -120.23 120.23 o 14 10 6 1551.71 961.64 135.43 o 15 10 6 100.79 -148.08 148.08 o 16 10 6 31.01 -148.82 148.82 o 17 10 6 3.01 -181.02 181.02 o 18 10 6 172.04 -274.69 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6417.83 248.54 o 1 10 18 12686.13 13078.39 250.90 o 2 10 18 1909.51 2111.08 146.58 o 3 10 18 830.37 898.48 137.71 o 4 10 18 136.69 198.59 134.34 o 5 10 18 13503.99 13323.82 312.86 o 6 10 18 3636.44 3656.47 185.19 o 7 10 18 8710.51 9465.52 243.81 o 8 10 18 6788.10 6890.92 212.33 o 9 10 18 1859.97 1966.17 183.14 o 1 11 18 3341.95 4014.66 162.21 o 2 11 18 807.15 1194.39 139.25 o 3 11 18 5149.26 5807.06 195.56 o 4 11 18 856.45 1102.08 148.86 o 5 11 18 2543.31 2874.09 164.01 o 6 11 18 320.01 410.99 155.62 o 7 11 18 27.45 -44.71 156.29 o 8 11 18 124.20 241.47 163.47 o 0 12 18 1419.00 2017.71 213.34 o 1 12 18 5116.57 5197.45 193.69 o 2 12 18 4487.31 4797.20 185.94 o 3 12 18 4671.73 4713.28 193.47 o 4 12 18 1524.95 1807.56 165.60 o 5 12 18 1091.66 1409.09 169.51 o 6 12 18 991.10 893.00 172.01 o 7 12 18 9294.97 9082.41 248.48 o 1 13 18 2024.21 2369.38 161.34 o 2 13 18 252.41 539.36 161.60 o 3 13 18 4476.78 4892.12 202.46 o 4 13 18 5291.44 5465.86 216.97 o 5 13 18 255.60 266.08 171.96 o 0 14 18 3213.82 3471.58 262.70 o 1 14 18 38.57 405.54 154.29 o 2 14 18 3684.04 3877.15 188.64 o 3 14 18 58.37 184.61 271.52 o 1 1 19 459.74 960.93 101.06 o 2 1 19 11902.21 12106.58 197.79 o 3 1 19 9216.22 9143.77 168.70 o 4 1 19 3285.87 3472.08 121.74 o 5 1 19 938.24 981.48 115.88 o 6 1 19 5051.77 5154.84 154.69 o 7 1 19 2231.20 2292.74 128.72 o 8 1 19 927.97 945.69 122.31 o 9 1 19 133.77 122.23 133.67 o 10 1 19 1459.57 1491.49 158.65 o 11 1 19 609.92 470.35 175.98 o 12 1 19 10.73 137.72 213.80 o 0 2 19 28791.68 28761.33 528.30 o 1 2 19 610.92 1147.71 108.37 o 2 2 19 4820.44 4911.35 133.00 o 3 2 19 269.85 368.51 98.97 o 4 2 19 316.50 507.99 105.85 o 5 2 19 1307.11 1147.51 116.59 o 6 2 19 2121.22 2186.82 132.31 o 7 2 19 411.31 390.04 118.33 o 8 2 19 7775.90 8051.18 199.19 o 9 2 19 67.57 -59.36 137.07 o 10 2 19 2065.57 1850.47 170.39 o 11 2 19 398.62 -9.72 166.11 o 12 2 19 7193.34 7370.03 279.81 o 1 3 19 1661.13 1930.98 107.00 o 2 3 19 2857.94 3143.05 121.17 o 3 3 19 691.32 829.32 105.61 o 4 3 19 7576.61 7999.05 163.16 o 5 3 19 977.49 1223.39 117.19 o 6 3 19 3277.35 3353.02 141.77 o 7 3 19 616.04 433.17 130.44 o 8 3 19 73.86 17.56 155.86 o 9 3 19 302.85 365.52 148.66 o 10 3 19 376.22 208.30 154.92 o 11 3 19 468.41 382.22 182.28 o 12 3 19 127.97 131.45 189.63 o 0 4 19 4543.77 5306.06 240.42 o 1 4 19 16374.54 15589.64 307.85 o 2 4 19 2475.01 2829.61 126.20 o 3 4 19 304.69 574.04 111.17 o 4 4 19 2017.12 1918.86 115.03 o 5 4 19 422.28 471.56 115.01 o 6 4 19 32488.23 31657.99 474.28 o 7 4 19 4965.02 4772.77 178.37 o 8 4 19 1065.43 1006.33 129.25 o 9 4 19 1768.76 1804.17 168.18 o 10 4 19 13.14 52.42 160.19 o 11 4 19 599.71 427.04 174.44 o 12 4 19 4461.32 5153.76 246.35 o 1 5 19 2899.57 2928.61 128.38 o 2 5 19 6023.39 6442.80 156.48 o 3 5 19 22033.86 21094.19 330.56 o 4 5 19 5635.01 5746.66 157.22 o 5 5 19 85.23 348.96 118.78 o 6 5 19 11391.39 11991.85 252.82 o 7 5 19 2.49 121.16 131.17 o 8 5 19 19214.68 19177.89 341.21 o 9 5 19 3872.40 4108.18 179.97 o 10 5 19 8517.16 9193.14 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5 12 19 48.56 -97.21 163.40 o 1 13 19 2086.16 2422.10 180.70 o 0 0 20 477.63 843.84 193.11 o 1 0 20 3676.27 4504.53 176.93 o 2 0 20 28693.45 28353.90 529.35 o 3 0 20 25390.81 24633.84 493.26 o 4 0 20 17983.36 17841.43 402.18 o 5 0 20 18313.87 17591.70 429.72 o 6 0 20 4189.98 4634.51 230.00 o 7 0 20 207.92 287.22 178.75 o 8 0 20 18567.86 18243.76 454.58 o 9 0 20 78.19 478.83 202.26 o 10 0 20 31.04 216.95 269.02 o 11 0 20 637.67 486.82 298.12 o 1 1 20 4971.14 5502.56 132.90 o 2 1 20 6925.41 7350.03 152.99 o 3 1 20 12290.92 12524.58 237.80 o 4 1 20 17419.70 17050.75 277.66 o 5 1 20 6098.52 6056.16 166.93 o 6 1 20 238.10 313.80 124.81 o 7 1 20 15231.40 14571.63 262.44 o 8 1 20 1321.47 1286.00 137.82 o 9 1 20 5792.15 6514.18 192.29 o 10 1 20 6857.41 7093.32 265.14 o 11 1 20 3253.58 3216.90 210.69 o 0 2 20 40.86 551.00 144.72 o 1 2 20 4608.16 4958.03 143.01 o 2 2 20 3590.08 4013.45 132.78 o 3 2 20 3302.11 3325.47 132.65 o 4 2 20 12131.36 12602.36 224.98 o 5 2 20 484.23 527.21 117.12 o 6 2 20 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1878.83 146.15 o 6 5 20 814.33 1102.46 148.41 o 7 5 20 1899.75 1869.39 153.34 o 8 5 20 994.75 1194.22 167.22 o 9 5 20 21.51 58.32 171.62 o 10 5 20 552.60 880.56 189.70 o 0 6 20 3.53 430.69 172.51 o 1 6 20 3647.50 3626.69 139.37 o 2 6 20 8002.35 7948.90 189.20 o 3 6 20 2699.80 2945.65 144.54 o 4 6 20 4239.90 4443.51 161.80 o 5 6 20 389.52 616.84 147.00 o 6 6 20 2.20 140.73 146.61 o 7 6 20 16.94 109.72 145.16 o 8 6 20 12184.74 12173.17 284.16 o 9 6 20 782.82 1007.13 183.36 o 1 7 20 1757.18 1865.02 132.76 o 2 7 20 504.86 586.88 133.65 o 3 7 20 107.39 261.35 131.66 o 4 7 20 4304.83 4287.48 159.46 o 5 7 20 287.18 415.69 139.28 o 6 7 20 180.51 325.45 146.68 o 7 7 20 6727.45 6632.08 219.02 o 8 7 20 908.55 1090.27 176.83 o 9 7 20 6332.76 6583.49 235.80 o 0 8 20 4365.31 4702.09 238.29 o 1 8 20 151.38 398.47 130.96 o 2 8 20 2020.44 2321.66 144.77 o 3 8 20 97.29 135.35 131.46 o 4 8 20 2146.92 2200.05 152.08 o 5 8 20 5279.75 5651.92 185.16 o 6 8 20 857.36 1139.28 167.13 o 7 8 20 8850.18 8277.78 247.61 o 8 8 20 7.16 -29.87 183.08 o 1 9 20 601.09 988.54 140.05 o 2 9 20 10305.86 10416.21 230.98 o 3 9 20 593.37 932.46 146.02 o 4 9 20 1795.20 2107.69 166.61 o 5 9 20 1566.43 1538.98 158.71 o 6 9 20 1705.72 1758.41 178.90 o 7 9 20 4265.00 4364.90 211.48 o 0 10 20 27348.43 27741.46 637.58 o 1 10 20 928.39 1495.14 163.51 o 2 10 20 1540.70 2091.82 167.34 o 3 10 20 250.18 485.35 146.98 o 4 10 20 15.31 311.03 160.09 o 5 10 20 445.25 700.82 168.91 o 1 11 20 8531.96 9000.15 249.18 o 2 11 20 5833.85 6386.57 223.23 o 3 11 20 918.94 964.21 173.49 o 1 1 21 106.28 430.81 107.08 o 2 1 21 63.83 389.71 116.76 o 3 1 21 102.84 675.46 125.87 o 4 1 21 12507.50 13205.88 306.23 o 5 1 21 446.95 582.61 128.91 o 6 1 21 2088.33 1859.67 138.09 o 7 1 21 489.82 410.33 139.52 o 8 1 21 87.20 -72.56 142.73 o 9 1 21 625.24 758.09 172.85 o 0 2 21 1424.51 1674.90 170.13 o 1 2 21 60.50 350.13 119.41 o 2 2 21 22273.91 22578.84 348.83 o 3 2 21 226.33 406.59 122.01 o 4 2 21 3178.35 3645.97 153.94 o 5 2 21 305.42 382.34 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493.56 127.46 o 2 6 21 5212.28 5043.16 172.47 o 3 6 21 3776.71 3946.02 163.73 o 4 6 21 1680.13 1712.28 154.73 o 5 6 21 3300.80 3643.66 170.47 o 6 6 21 6261.03 6293.82 206.58 o 7 6 21 9198.92 9361.03 249.32 o 1 7 21 1403.76 1639.45 142.48 o 2 7 21 371.35 609.91 140.64 o 3 7 21 77.20 253.37 150.63 o 4 7 21 46.32 308.95 136.65 o 5 7 21 10857.77 10546.04 246.52 o 6 7 21 2836.41 3274.65 187.21 o 0 8 21 3196.39 3606.23 241.61 o 1 8 21 737.73 758.71 145.61 o 2 8 21 1915.39 2282.72 154.67 o 3 8 21 234.35 226.48 141.16 o 4 8 21 365.80 495.72 159.41 o 5 8 21 1500.03 1613.07 182.73 o 1 9 21 5907.17 5829.35 190.26 o 2 9 21 582.86 815.49 144.82 o 3 9 21 1723.97 1931.42 169.67 o 4 9 21 1655.67 1985.10 179.23 o 0 10 21 17987.96 18374.34 534.42 o 0 0 22 737.21 1051.53 252.92 o 1 0 22 7771.86 7564.57 246.84 o 2 0 22 3053.26 3162.72 194.82 o 3 0 22 9920.92 10511.02 323.27 o 4 0 22 668.94 931.24 195.03 o 5 0 22 21069.27 20647.36 497.09 o 6 0 22 3321.39 2962.99 222.38 o 7 0 22 8.68 -135.99 186.66 o 1 1 22 14447.88 14744.23 256.26 o 2 1 22 756.35 1239.36 129.02 o 3 1 22 29075.66 28012.12 411.89 o 4 1 22 77.27 174.34 135.77 o 5 1 22 2723.17 2876.55 151.43 o 6 1 22 3390.45 3630.89 180.35 o 7 1 22 3340.72 3519.16 181.23 o 0 2 22 10747.21 11706.76 393.00 o 1 2 22 677.69 853.23 132.56 o 2 2 22 497.23 1060.19 140.08 o 3 2 22 344.89 464.78 134.22 o 4 2 22 3446.10 3494.51 151.68 o 5 2 22 61.10 167.19 132.89 o 6 2 22 3301.18 3620.48 172.02 o 7 2 22 7.15 225.77 165.02 o 1 3 22 254.58 396.74 139.08 o 2 3 22 6062.65 6433.29 186.05 o 3 3 22 4600.73 4683.93 172.69 o 4 3 22 144.45 430.92 133.38 o 5 3 22 9499.80 10199.62 221.29 o 6 3 22 593.82 837.29 158.59 o 0 4 22 7452.68 7961.45 300.86 o 1 4 22 50.42 197.17 140.98 o 2 4 22 31.06 276.93 145.94 o 3 4 22 2662.01 2996.04 155.73 o 4 4 22 1013.86 1116.77 134.64 o 5 4 22 9521.55 9988.05 225.56 o 6 4 22 895.81 1319.50 154.75 o 1 5 22 40.75 283.77 144.37 o 2 5 22 14.88 64.67 154.16 o 3 5 22 3391.63 3450.07 160.27 o 4 5 22 3.87 322.36 146.30 o 5 5 22 2911.95 3483.13 168.83 o 0 6 22 8758.56 8715.27 295.89 o 1 6 22 986.25 992.92 147.78 o 2 6 22 525.91 602.35 154.43 o 3 6 22 3.08 129.60 145.41 o 4 6 22 4854.00 4709.60 189.98 o 1 7 22 9305.85 9345.10 230.21 o 2 7 22 12242.98 12636.78 276.50 o 3 7 22 15265.52 15736.27 328.23 o 1 1 23 251.54 798.79 150.03 o 2 1 23 3559.49 3659.43 159.47 o 3 1 23 4623.71 5393.90 177.10 o 4 1 23 20.49 324.11 144.38 o 0 2 23 8656.16 8886.29 337.31 o 1 2 23 2353.15 3112.77 168.47 o 2 2 23 2523.53 2912.47 157.21 o 3 2 23 1886.21 2322.95 152.56 o 1 3 23 10.59 252.85 147.44 o 2 3 23 1565.24 1962.16 166.45 o 3 3 23 3452.09 4174.70 169.43 o 0 4 23 354.92 799.04 226.44 o 1 4 23 2485.14 2523.94 170.27 o 2 4 23 2.15 271.13 151.28 o