#------------------------------------------------------------------------------ #$Date: 2020-03-05 11:42:52 +0200 (Thu, 05 Mar 2020) $ #$Revision: 249077 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/74/1557484.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1557484 loop_ _publ_author_name 'Ranjan, Subham' 'Devarapalli, Ramesh' 'Kundu, Sudeshna' 'Saha, Subhankar' 'Deolka, Shubham' 'Vangala, Venu R.' 'Reddy, C. Malla' _publ_section_title ; Isomorphism: `molecular similarity to crystal structure similarity' in multicomponent forms of analgesic drugs tolfenamic and mefenamic acid ; _journal_issue 2 _journal_name_full IUCrJ _journal_page_first 173 _journal_page_last 183 _journal_paper_doi 10.1107/S205225251901604X _journal_volume 7 _journal_year 2020 _chemical_formula_moiety 'C14 H12 Cl N O2' _chemical_formula_sum 'C14 H12 Cl N O2' _chemical_formula_weight 261.70 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2019-10-09 _audit_creation_method ; Olex2 1.3 (compiled 2019.09.11 svn.r3662 for OlexSys, GUI svn.r5938) ; _cell_angle_alpha 77.167(4) _cell_angle_beta 79.908(3) _cell_angle_gamma 65.487(4) _cell_formula_units_Z 2 _cell_length_a 6.7049(3) _cell_length_b 7.2778(3) _cell_length_c 14.1630(6) _cell_measurement_reflns_used 6423 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 26.4300 _cell_measurement_theta_min 2.9290 _cell_volume 610.42(5) _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 7.9580 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -9.00 105.00 1.00 10.00 -- 29.32 57.00 120.00 114 2 \w 35.00 124.00 1.00 10.00 -- 29.32 178.00 30.00 89 3 \w -14.00 114.00 1.00 10.00 -- 29.32 77.00-150.00 128 4 \w -14.00 114.00 1.00 10.00 -- 29.32 77.00 -30.00 128 5 \w -55.00 73.00 1.00 10.00 -- 29.32 -77.00 90.00 128 6 \w 35.00 124.00 1.00 10.00 -- 29.32 178.00 120.00 89 7 \w -31.00 26.00 1.00 10.00 -- -23.50 -90.00 -53.00 57 8 \w -55.00 116.00 1.00 10.00 -- 29.32 19.00-180.00 171 9 \w -9.00 105.00 1.00 10.00 -- 29.32 57.00 -90.00 114 10 \w -47.00 67.00 1.00 10.00 -- 29.32 -57.00 -90.00 114 11 \w -52.00 85.00 1.00 10.00 -- 29.32 -38.00 120.00 137 12 \w -9.00 21.00 1.00 10.00 -- 29.32 57.00-150.00 30 13 \w -14.00 114.00 1.00 10.00 -- 29.32 77.00 90.00 128 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0569663000 _diffrn_orient_matrix_UB_12 -0.0103875000 _diffrn_orient_matrix_UB_13 -0.0469491000 _diffrn_orient_matrix_UB_21 0.0084794000 _diffrn_orient_matrix_UB_22 0.0953342000 _diffrn_orient_matrix_UB_23 -0.0036364000 _diffrn_orient_matrix_UB_31 0.1015917000 _diffrn_orient_matrix_UB_32 -0.0510437000 _diffrn_orient_matrix_UB_33 0.0210758000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0314 _diffrn_reflns_av_unetI/netI 0.0198 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 11414 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.027 _diffrn_reflns_theta_max 25.027 _diffrn_reflns_theta_min 2.963 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.305 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.37641 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.424 _exptl_crystal_description plate _exptl_crystal_F_000 272 _exptl_crystal_size_max 0.6 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.406 _refine_diff_density_min -1.389 _refine_diff_density_rms 0.096 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.060 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 168 _refine_ls_number_reflns 2133 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.060 _refine_ls_R_factor_all 0.0842 _refine_ls_R_factor_gt 0.0792 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1132P)^2^+1.7122P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2157 _refine_ls_wR_factor_ref 0.2204 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1931 _reflns_number_total 2133 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL tfa_form-vi_a.res in P-1 tfa_form-vi.res created by SHELXL-2018/3 at 23:02:12 on 09-Oct-2019 REM Old TITL tfa_form-vi_a.res in P-1 REM SHELXT solution in P-1 REM R1 0.230, Rweak 0.013, Alpha 0.044, Orientation as input REM Formula found by SHELXT: C14 Cl N O2 CELL 0.71073 6.7049 7.2778 14.163 77.167 79.908 65.487 ZERR 2 0.0003 0.0003 0.0006 0.004 0.003 0.004 LATT 1 SFAC C H Cl N O UNIT 28 24 2 2 4 DFIX 0.87 N1 H1a L.S. 10 PLAN 5 SIZE 0.2 0.3 0.6 CONF BOND $H list 4 MORE -1 fmap 2 acta SHEL 100 0.84 OMIT -1 1 0 OMIT 0 -3 3 OMIT -1 3 3 OMIT 0 3 3 OMIT 0 0 6 OMIT 3 6 9 OMIT 3 3 12 OMIT 3 6 12 OMIT 2 -1 2 REM REM REM WGHT 0.113200 1.712200 FVAR 0.83087 CL1 3 0.189732 1.265158 0.484616 11.00000 0.10099 0.07181 = 0.04035 -0.00762 -0.01072 0.03161 O1 5 0.275300 0.291176 1.004334 11.00000 0.01243 0.01645 = 0.02315 0.00024 0.00079 -0.00449 AFIX 147 H1 2 0.146287 0.323866 1.026784 11.00000 -1.50000 AFIX 0 O2 5 0.134452 0.601678 0.915692 11.00000 0.01221 0.01570 = 0.02280 -0.00080 -0.00139 -0.00390 N1 4 0.402929 0.744427 0.794628 11.00000 0.01069 0.01398 = 0.02572 0.00102 0.00119 -0.00289 AFIX 2 H1A 2 0.272964 0.749678 0.816604 11.00000 -1.20000 AFIX 0 C1 1 0.296141 0.442621 0.938300 11.00000 0.01556 0.01409 = 0.01575 -0.00407 -0.00352 -0.00574 C2 1 0.520840 0.408255 0.894007 11.00000 0.01354 0.01278 = 0.01674 -0.00481 -0.00239 -0.00402 C3 1 0.693107 0.219426 0.921981 11.00000 0.01730 0.01452 = 0.01560 -0.00235 -0.00226 -0.00319 AFIX 43 H3 2 0.662320 0.119839 0.968388 11.00000 -1.20000 AFIX 0 C4 1 0.906388 0.179485 0.881877 11.00000 0.01406 0.01638 = 0.02179 -0.00434 -0.00352 0.00151 AFIX 43 H4 2 1.018891 0.054134 0.900907 11.00000 -1.20000 AFIX 0 C5 1 0.951242 0.328685 0.812714 11.00000 0.01202 0.02225 = 0.01830 -0.00801 0.00085 -0.00493 AFIX 43 H5 2 1.095154 0.302015 0.785483 11.00000 -1.20000 AFIX 0 C6 1 0.787367 0.515375 0.783506 11.00000 0.01553 0.01608 = 0.01769 -0.00447 0.00097 -0.00654 AFIX 43 H6 2 0.821793 0.612520 0.736797 11.00000 -1.20000 AFIX 0 C7 1 0.567416 0.560680 0.823851 11.00000 0.01470 0.01309 = 0.01601 -0.00526 -0.00221 -0.00393 C8 1 0.425630 0.912798 0.728848 11.00000 0.01524 0.01215 = 0.01753 -0.00496 0.00506 -0.00106 C9 1 0.308843 0.986801 0.646358 11.00000 0.01787 0.01991 = 0.01935 -0.00676 0.00134 0.00580 C10 1 0.322104 1.161063 0.586159 11.00000 0.03705 0.01749 = 0.02226 -0.00634 0.00964 0.00688 C11 1 0.445764 1.255280 0.605992 11.00000 0.05172 0.01343 = 0.03006 -0.00254 0.02467 -0.00038 AFIX 43 H11 2 0.451334 1.371880 0.564411 11.00000 -1.20000 AFIX 0 C12 1 0.562656 1.178901 0.687282 11.00000 0.03681 0.01895 = 0.04148 -0.01502 0.01975 -0.01454 AFIX 43 H12 2 0.647623 1.242863 0.699809 11.00000 -1.20000 AFIX 0 C13 1 0.552154 1.006730 0.749747 11.00000 0.02114 0.01977 = 0.02445 -0.00855 0.00562 -0.00615 AFIX 43 H13 2 0.628654 0.954618 0.804919 11.00000 -1.20000 AFIX 0 C14 1 0.179526 0.879151 0.623600 11.00000 0.02281 0.04059 = 0.03400 -0.01448 -0.00892 -0.00039 AFIX 137 H14A 2 0.233774 0.739617 0.656296 11.00000 -1.50000 H14B 2 0.194903 0.881956 0.554676 11.00000 -1.50000 H14C 2 0.027015 0.946879 0.645243 11.00000 -1.50000 AFIX 0 HKLF 4 REM tfa_form-vi_a.res in P-1 REM wR2 = 0.2204, GooF = S = 1.060, Restrained GooF = 1.060 for all data REM R1 = 0.0792 for 1931 Fo > 4sig(Fo) and 0.0842 for all 2133 data REM 168 parameters refined using 1 restraints END WGHT 0.1132 1.7125 REM Highest difference peak 0.406, deepest hole -1.389, 1-sigma level 0.096 Q1 1 0.5877 0.3379 0.9053 11.00000 0.05 0.41 Q2 1 0.5385 0.4908 0.8553 11.00000 0.05 0.40 Q3 1 0.4295 0.4223 0.9188 11.00000 0.05 0.38 Q4 1 0.4983 0.6458 0.8163 11.00000 0.05 0.37 Q5 1 0.2998 1.0740 0.6208 11.00000 0.05 0.36 REM The information below was added by Olex2. REM REM R1 = 0.0792 for 1931 Fo > 4sig(Fo) and 0.0842 for all 12761 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.41, deepest hole -1.39 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0842 REM R1_gt = 0.0792 REM wR_ref = 0.2204 REM GOOF = 1.060 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 12761 REM Reflections_gt = 1931 REM Parameters = n/a REM Hole = -1.39 REM Peak = 0.41 REM Flack = n/a ; _cod_data_source_file ed5019.cif _cod_data_source_block tfa_form-vi _cod_database_code 1557484 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C H N O Cl' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.942 _shelx_estimated_absorpt_t_min 0.838 _reflns_odcompleteness_completeness 92.81 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 27.04 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2. Restrained distances N1-H1A 0.87 with sigma of 0.02 3.a Fixed occupancy and ADP/Uiso: H1A 3.b Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C5(H5), C6(H6), C11(H11), C12(H12), C13(H13) 3.c Idealised Me refined as rotating group: C14(H14A,H14B,H14C) 3.d Idealised tetrahedral OH refined as rotating group: O1(H1) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.567 _oxdiff_exptl_absorpt_empirical_full_min 0.366 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.1897(3) 1.2652(3) 0.48462(10) 0.0931(8) Uani 1 1 d . . . . . O1 O 0.2753(3) 0.2912(3) 1.00433(16) 0.0187(6) Uani 1 1 d . . . . . H1 H 0.146287 0.323866 1.026784 0.028 Uiso 1 1 calc R U . . . O2 O 0.1345(3) 0.6017(3) 0.91569(16) 0.0179(5) Uani 1 1 d . . . . . N1 N 0.4029(4) 0.7444(4) 0.7946(2) 0.0186(6) Uani 1 1 d D . . . . H1A H 0.273(4) 0.750(6) 0.817(3) 0.022 Uiso 1 1 d D U . . . C1 C 0.2961(5) 0.4426(4) 0.9383(2) 0.0146(7) Uani 1 1 d . . . . . C2 C 0.5208(5) 0.4083(4) 0.8940(2) 0.0142(7) Uani 1 1 d . . . . . C3 C 0.6931(5) 0.2194(5) 0.9220(2) 0.0168(7) Uani 1 1 d . . . . . H3 H 0.662320 0.119839 0.968388 0.020 Uiso 1 1 calc R U . . . C4 C 0.9064(5) 0.1795(5) 0.8819(2) 0.0195(7) Uani 1 1 d . . . . . H4 H 1.018891 0.054134 0.900907 0.023 Uiso 1 1 calc R U . . . C5 C 0.9512(5) 0.3287(5) 0.8127(2) 0.0176(7) Uani 1 1 d . . . . . H5 H 1.095154 0.302015 0.785483 0.021 Uiso 1 1 calc R U . . . C6 C 0.7874(5) 0.5154(5) 0.7835(2) 0.0164(7) Uani 1 1 d . . . . . H6 H 0.821793 0.612520 0.736797 0.020 Uiso 1 1 calc R U . . . C7 C 0.5674(5) 0.5607(5) 0.8239(2) 0.0145(7) Uani 1 1 d . . . . . C8 C 0.4256(5) 0.9128(5) 0.7288(2) 0.0169(7) Uani 1 1 d . . . . . C9 C 0.3088(5) 0.9868(5) 0.6464(2) 0.0233(8) Uani 1 1 d . . . . . C10 C 0.3221(7) 1.1611(5) 0.5862(3) 0.0327(9) Uani 1 1 d . . . . . C11 C 0.4458(7) 1.2553(5) 0.6060(3) 0.0399(11) Uani 1 1 d . . . . . H11 H 0.451334 1.371880 0.564411 0.048 Uiso 1 1 calc R U . . . C12 C 0.5627(7) 1.1789(5) 0.6873(3) 0.0326(9) Uani 1 1 d . . . . . H12 H 0.647623 1.242863 0.699809 0.039 Uiso 1 1 calc R U . . . C13 C 0.5522(5) 1.0067(5) 0.7497(2) 0.0226(7) Uani 1 1 d . . . . . H13 H 0.628654 0.954618 0.804919 0.027 Uiso 1 1 calc R U . . . C14 C 0.1795(6) 0.8792(6) 0.6236(3) 0.0343(9) Uani 1 1 d . . . . . H14A H 0.233774 0.739617 0.656296 0.051 Uiso 1 1 calc R U . . . H14B H 0.194903 0.881956 0.554676 0.051 Uiso 1 1 calc R U . . . H14C H 0.027015 0.946879 0.645243 0.051 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.1010(13) 0.0718(11) 0.0403(8) -0.0076(7) -0.0107(8) 0.0316(9) O1 0.0124(11) 0.0165(11) 0.0231(12) 0.0002(9) 0.0008(9) -0.0045(9) O2 0.0122(11) 0.0157(11) 0.0228(12) -0.0008(9) -0.0014(9) -0.0039(9) N1 0.0107(13) 0.0140(13) 0.0257(15) 0.0010(11) 0.0012(11) -0.0029(11) C1 0.0156(15) 0.0141(15) 0.0157(15) -0.0041(12) -0.0035(12) -0.0057(13) C2 0.0135(15) 0.0128(14) 0.0167(15) -0.0048(12) -0.0024(12) -0.0040(12) C3 0.0173(16) 0.0145(15) 0.0156(15) -0.0023(11) -0.0023(12) -0.0032(12) C4 0.0141(15) 0.0164(15) 0.0218(16) -0.0043(12) -0.0035(12) 0.0015(12) C5 0.0120(15) 0.0223(16) 0.0183(16) -0.0080(12) 0.0008(12) -0.0049(13) C6 0.0155(15) 0.0161(15) 0.0177(15) -0.0045(12) 0.0010(12) -0.0065(13) C7 0.0147(15) 0.0131(15) 0.0160(15) -0.0053(11) -0.0022(12) -0.0039(12) C8 0.0152(15) 0.0122(14) 0.0175(15) -0.0050(12) 0.0051(12) -0.0011(12) C9 0.0179(16) 0.0199(16) 0.0193(16) -0.0068(13) 0.0013(13) 0.0058(13) C10 0.037(2) 0.0175(17) 0.0223(18) -0.0063(14) 0.0096(15) 0.0069(15) C11 0.052(3) 0.0134(17) 0.030(2) -0.0025(15) 0.0247(19) -0.0004(17) C12 0.037(2) 0.0190(17) 0.041(2) -0.0150(16) 0.0198(17) -0.0145(16) C13 0.0211(17) 0.0198(16) 0.0245(17) -0.0086(13) 0.0056(13) -0.0061(14) C14 0.0228(19) 0.041(2) 0.034(2) -0.0145(17) -0.0089(16) -0.0004(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 O1 H1 109.5 . . ? C7 N1 H1A 114(3) . . ? C7 N1 C8 127.0(3) . . ? C8 N1 H1A 119(3) . . ? O1 C1 C2 115.5(3) . . ? O2 C1 O1 121.3(3) . . ? O2 C1 C2 123.2(3) . . ? C3 C2 C1 119.1(3) . . ? C3 C2 C7 119.5(3) . . ? C7 C2 C1 121.4(3) . . ? C2 C3 H3 119.4 . . ? C4 C3 C2 121.2(3) . . ? C4 C3 H3 119.4 . . ? C3 C4 H4 120.4 . . ? C3 C4 C5 119.1(3) . . ? C5 C4 H4 120.4 . . ? C4 C5 H5 119.3 . . ? C6 C5 C4 121.4(3) . . ? C6 C5 H5 119.3 . . ? C5 C6 H6 119.7 . . ? C5 C6 C7 120.6(3) . . ? C7 C6 H6 119.7 . . ? N1 C7 C2 120.7(3) . . ? N1 C7 C6 121.1(3) . . ? C6 C7 C2 118.1(3) . . ? C9 C8 N1 118.2(3) . . ? C13 C8 N1 119.8(3) . . ? C13 C8 C9 122.0(3) . . ? C8 C9 C14 121.0(3) . . ? C10 C9 C8 117.1(3) . . ? C10 C9 C14 121.9(3) . . ? C9 C10 Cl1 121.7(3) . . ? C11 C10 Cl1 116.7(3) . . ? C11 C10 C9 121.5(4) . . ? C10 C11 H11 119.6 . . ? C10 C11 C12 120.8(3) . . ? C12 C11 H11 119.6 . . ? C11 C12 H12 120.2 . . ? C13 C12 C11 119.6(4) . . ? C13 C12 H12 120.2 . . ? C8 C13 H13 120.5 . . ? C12 C13 C8 119.1(3) . . ? C12 C13 H13 120.5 . . ? C9 C14 H14A 109.5 . . ? C9 C14 H14B 109.5 . . ? C9 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C10 1.684(4) . ? O1 H1 0.8200 . ? O1 C1 1.316(4) . ? O2 C1 1.238(4) . ? N1 H1A 0.860(19) . ? N1 C7 1.366(4) . ? N1 C8 1.411(4) . ? C1 C2 1.467(4) . ? C2 C3 1.407(4) . ? C2 C7 1.416(4) . ? C3 H3 0.9300 . ? C3 C4 1.377(5) . ? C4 H4 0.9300 . ? C4 C5 1.387(5) . ? C5 H5 0.9300 . ? C5 C6 1.377(5) . ? C6 H6 0.9300 . ? C6 C7 1.412(4) . ? C8 C9 1.400(5) . ? C8 C13 1.391(5) . ? C9 C10 1.389(5) . ? C9 C14 1.498(5) . ? C10 C11 1.369(7) . ? C11 H11 0.9300 . ? C11 C12 1.385(6) . ? C12 H12 0.9300 . ? C12 C13 1.384(5) . ? C13 H13 0.9300 . ? C14 H14A 0.9600 . ? C14 H14B 0.9600 . ? C14 H14C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl1 C10 C11 C12 -179.2(3) . . . . ? O1 C1 C2 C3 1.8(4) . . . . ? O1 C1 C2 C7 -178.3(2) . . . . ? O2 C1 C2 C3 -177.8(3) . . . . ? O2 C1 C2 C7 2.1(5) . . . . ? N1 C8 C9 C10 175.8(3) . . . . ? N1 C8 C9 C14 -5.5(4) . . . . ? N1 C8 C13 C12 -176.3(3) . . . . ? C1 C2 C3 C4 179.5(3) . . . . ? C1 C2 C7 N1 -0.6(4) . . . . ? C1 C2 C7 C6 -179.2(3) . . . . ? C2 C3 C4 C5 0.0(5) . . . . ? C3 C2 C7 N1 179.3(3) . . . . ? C3 C2 C7 C6 0.7(4) . . . . ? C3 C4 C5 C6 0.1(5) . . . . ? C4 C5 C6 C7 0.3(5) . . . . ? C5 C6 C7 N1 -179.2(3) . . . . ? C5 C6 C7 C2 -0.7(4) . . . . ? C7 N1 C8 C9 122.8(3) . . . . ? C7 N1 C8 C13 -60.6(4) . . . . ? C7 C2 C3 C4 -0.4(4) . . . . ? C8 N1 C7 C2 177.2(3) . . . . ? C8 N1 C7 C6 -4.3(5) . . . . ? C8 C9 C10 Cl1 179.9(2) . . . . ? C8 C9 C10 C11 0.7(5) . . . . ? C9 C8 C13 C12 0.2(5) . . . . ? C9 C10 C11 C12 0.1(5) . . . . ? C10 C11 C12 C13 -0.8(5) . . . . ? C11 C12 C13 C8 0.6(5) . . . . ? C13 C8 C9 C10 -0.8(5) . . . . ? C13 C8 C9 C14 178.0(3) . . . . ? C14 C9 C10 Cl1 1.1(5) . . . . ? C14 C9 C10 C11 -178.1(3) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 2 18.18 0.94 0 0 2 22.1 1.1 0 0 -2 17.58 0.86 0 0 2 16.04 0.72 0 0 -2 17.89 0.64 0 0 -2 18.96 0.89 0 0 3 121.68 3.59 0 0 3 145.33 4.11 0 0 -3 146.57 3.77 0 0 -3 142.34 3.08 0 0 -3 147.53 3.96 0 0 3 152.59 4.4 0 0 -3 147.02 3.36 0 0 -4 13.18 0.95 0 0 -4 13.19 1.02 0 0 -4 12.57 0.71 0 0 4 9.51 0.79 0 0 4 11.89 1.06 0 0 4 13.79 1.22 0 0 -4 11.79 0.52 0 0 -5 1.65 0.45 0 0 5 0.9 0.53 0 0 5 1.58 0.54 0 0 5 1.18 0.35 0 0 -5 1.56 0.22 0 0 -5 1.72 0.3 0 0 -5 1.53 0.44 0 0 6 20.61 1.47 0 0 -6 27.51 1.66 0 0 -6 27.06 1.86 0 0 -6 24.35 1.27 0 0 6 22.95 1.98 0 0 -6 24.54 0.99 0 0 -7 669.18 14.7 0 0 7 647.51 16.29 0 0 -7 646.65 15.19 0 0 7 651.69 15.67 0 0 -8 43.29 2.51 0 0 8 45.96 3.26 0 0 -8 44.17 2.81 0 0 8 45.4 3.05 0 0 -9 13.92 1.68 0 0 9 13.55 1.74 0 0 9 14.8 2 0 0 -9 14.56 1.49 0 0 10 459.01 14.08 0 0 10 474.12 14.65 0 0 -10 464.62 12.79 0 0 -10 490.81 13.68 0 0 11 78.28 4.95 0 0 -11 87.41 4.32 0 0 11 71.82 5.03 0 0 -11 76.24 4.58 0 0 12 68.2 4.84 0 0 -12 68.2 3.95 0 0 12 66.99 4.99 0 0 -12 63.31 4.35 0 0 -13 4.04 1.12 0 0 13 5.45 1.64 0 0 -13 4.06 1.24 0 0 13 8.14 1.79 0 0 -14 7.94 1.5 0 0 -14 11.42 2.07 0 0 14 6.44 1.75 0 0 14 8.92 1.96 0 0 -15 19.17 2.82 0 0 -15 18.35 2.38 0 0 15 18.87 3.11 0 0 15 16.43 2.78 0 0 16 12.62 2.7 0 0 -16 12 2.33 0 0 -16 11.41 2.01 0 0 16 8.07 2.11 0 0 -16 13.21 2.71 0 0 -17 15.22 2.74 0 0 17 11.34 2.66 0 0 -17 10.2 2.01 0 0 -17 13.01 2.79 0 1 -16 1.65 1.22 0 -1 16 1.66 1.26 0 1 -16 1.78 1.26 0 1 -16 1.62 1.13 0 1 -15 93.8 6.97 0 1 -15 92.67 5.82 0 1 -15 95.74 6.43 0 -1 15 91.15 6.99 0 1 -14 6.26 1.49 0 -1 14 6.62 1.87 0 1 -14 4.71 1.55 0 1 -14 7.05 1.75 0 1 -13 2.82 0.97 0 -1 13 2.95 1.28 0 1 -13 1.92 1.06 0 1 -13 3.58 1.14 0 1 -12 8.25 1.64 0 1 -12 5.88 1.21 0 1 -12 9.08 1.91 0 -1 12 5.39 1.6 0 1 -11 21.25 2.74 0 1 -11 24.61 2.64 0 1 -11 21.07 2.24 0 -1 11 22.57 2.82 0 -1 10 376.23 12.59 0 1 -10 376.25 11.91 0 1 -10 363.19 12.84 0 -1 10 348.78 12.74 0 -1 9 149.38 6.91 0 1 -9 154.21 7.17 0 -1 9 155.3 7.17 0 1 -9 170.37 6.23 0 1 -9 161.71 6.56 0 -1 8 13.62 1.84 0 1 -8 13.58 1.56 0 -1 8 14.13 1.95 0 1 -8 14.28 1.65 0 1 -8 13 1.87 0 -1 7 657.07 15.93 0 -1 7 634.33 17.02 0 1 -7 652.25 15.55 0 -1 7 640.78 16.71 0 1 -7 616.3 17.01 0 1 -7 638.37 16.08 0 1 -6 3.03 0.73 0 -1 6 2.6 0.65 0 -1 6 2.62 0.9 0 1 -6 2.46 0.87 0 1 -6 3.3 0.64 0 -1 6 2.73 0.68 0 1 -5 53.98 3.25 0 -1 5 64.1 2.98 0 1 -5 58.13 2.67 0 1 -5 59.04 2.92 0 -1 5 59.26 3.36 0 1 -4 237.82 7.44 0 -1 4 247.12 6.92 0 -1 4 253.25 7.64 0 1 -4 250.46 6.55 0 1 -4 239.97 6.86 0 -1 3 56.7 2.41 0 1 -3 53.04 2.24 0 -1 3 52.07 2.71 0 1 -3 48.86 2.6 0 -1 2 417.63 9.81 0 1 -2 411.27 10.31 0 -1 2 416.74 8.48 0 -1 2 413.94 10.45 0 1 -2 431.49 9.53 0 -1 2 424.94 9.95 0 1 -1 2525.91 52.07 0 -1 1 2543.04 51.52 0 -1 1 2672.62 51.55 0 -1 1 2496.58 52.1 0 1 -1 2572.52 51.19 0 -1 1 2557.7 51.12 0 -1 0 24.9 0.82 0 -1 0 26.16 1.14 0 1 0 25.17 1.11 0 -1 0 24.37 1.22 0 1 0 25.23 1.46 0 -1 0 24.82 0.82 0 -1 0 24.6 1.25 0 -1 0 20.39 1.38 0 1 1 1308.98 27.76 0 -1 -1 1348.8 26.57 0 1 1 1347 27.77 0 -1 -1 1273.18 27.24 0 -1 -1 1325.64 26.51 0 1 1 1298.65 26.96 0 1 1 1290.81 26.88 0 -1 -1 1324.23 27.02 0 -1 -2 251.32 5.42 0 -1 -2 246.35 5.86 0 -1 -2 239.66 6.08 0 -1 -2 234.15 5.45 0 1 2 246.48 6.55 0 1 2 251.43 6.56 0 -1 -2 252.36 5.69 0 1 2 238.18 6.4 0 1 2 245.27 5.72 0 1 3 2760.83 58.33 0 1 3 2856.33 59.48 0 -1 -3 2864.85 58.46 0 -1 -3 2995.63 58.7 0 -1 -3 3030.24 58.12 0 -1 -3 2950.45 59.08 0 -1 -3 3063.59 58.32 0 -1 -3 2917.46 58.72 0 1 3 2989.56 59.67 0 -1 -4 83.65 2.85 0 1 4 86.75 2.7 0 1 4 89 3.44 0 1 4 94.18 3.63 0 -1 -4 90.4 2.66 0 -1 -4 86.24 2.83 0 -1 -4 92.98 3.27 0 -1 -4 91.8 2.49 0 -1 -4 85.7 2.99 0 -1 -5 134.54 3.94 0 -1 -5 129.81 4.39 0 1 5 118.63 3.63 0 -1 -5 122.1 3.92 0 -1 -5 129.43 3.36 0 -1 -5 128.91 4.13 0 1 5 129.98 4.76 0 1 5 127.53 4.6 0 -1 -5 125.33 3.58 0 -1 -6 35.95 1.82 0 -1 -6 33.56 2.09 0 1 6 32.73 1.65 0 -1 -6 33.57 2 0 1 6 30.29 2.28 0 -1 -6 34.56 1.64 0 -1 -6 33.33 1.42 0 1 6 33.66 2.25 0 -1 -6 32.98 1.8 0 -1 -7 4.62 0.75 0 1 7 3.92 0.63 0 -1 -7 4.33 0.63 0 -1 -7 3.86 0.9 0 1 7 4.92 0.98 0 -1 -7 4.53 0.53 0 1 7 4.71 0.89 0 -1 -7 4.46 0.64 0 1 8 701.75 16.69 0 -1 -8 764.91 16.57 0 1 8 724.17 18.46 0 -1 -8 739.32 16.72 0 1 8 749.84 19.1 0 -1 -8 751.39 18.04 0 -1 -8 732.66 15.92 0 -1 -8 777.64 17.14 0 -1 -9 341.98 9.29 0 1 9 342.93 10.72 0 -1 -9 336.38 8.18 0 1 9 329.32 9.01 0 -1 -9 345.87 8.83 0 1 9 352.6 11.36 0 -1 -9 349.59 10.32 0 1 10 1.11 0.67 0 -1 -10 1.08 0.42 0 -1 -10 0.69 0.51 0 1 10 0.4 0.47 0 -1 -10 0.71 0.51 0 1 10 1.19 0.89 0 -1 -11 57.24 3.18 0 1 11 50.32 3.79 0 -1 -11 52.53 3.68 0 1 11 61.15 4.45 0 1 12 -0.43 0.57 0 -1 -12 1.35 0.79 0 -1 -12 0.64 0.68 0 1 12 2.08 0.9 0 -1 -13 42.35 3.7 0 1 13 40.26 3.73 0 -1 -13 40.54 3.03 0 1 13 43.15 4.25 0 -1 -14 2.84 1.01 0 1 14 2.19 1 0 -1 -14 2.53 1.1 0 1 14 2.29 1.17 0 1 15 76.73 6.27 0 1 15 89.08 6.35 0 -1 -15 88.94 5.98 0 -1 -15 82 4.92 0 1 16 2.02 1 0 -1 -16 4.55 1.57 0 -1 -16 3.17 1 0 1 16 3.8 1.7 0 1 17 17.73 3.3 0 1 17 12.24 2.71 0 -1 -17 18.68 2.46 0 -1 -17 19.14 3.09 0 2 -15 94.16 6.3 0 -2 15 82.46 6.98 0 2 -15 90.24 7.13 0 2 -14 12.52 2.61 0 2 -14 12.22 2.15 0 -2 14 10.19 2.31 0 -2 13 56.24 5.26 0 2 -13 56.2 5.17 0 2 -13 53.61 4.35 0 -2 12 6.32 1.66 0 2 -12 6.69 1.63 0 2 -12 9.71 1.81 0 2 -11 27.67 3.32 0 -2 11 24.7 3.17 0 2 -11 26.65 2.76 0 -2 10 480.64 16.22 0 2 -10 512.81 14.56 0 2 -10 481.82 16.16 0 -2 9 41.49 3.9 0 -2 9 47.04 3.34 0 2 -9 44.25 3.3 0 2 -9 42.86 3.89 0 -2 8 6.56 1.56 0 2 -8 7.82 1.33 0 2 -8 7.08 1.55 0 -2 8 7.93 1.37 0 2 -7 19 2.3 0 2 -7 18.57 1.85 0 -2 7 17.66 2.29 0 -2 7 16.38 1.86 0 -2 6 125.47 5.1 0 -2 6 113.04 5.76 0 2 -6 115.26 4.68 0 -2 6 93.98 2.79 0 2 -6 105.71 5.48 0 -2 5 42.95 2.69 0 -2 5 35.88 2.96 0 -2 5 30.36 1.11 0 2 -5 35.16 2.87 0 2 -5 35.04 2.32 0 -2 5 32.79 2.52 0 -2 4 196.88 6.76 0 -2 4 192.46 4.47 0 2 -4 201.8 7.4 0 -2 4 203.09 7.6 0 -2 4 198.21 6.58 0 2 -4 205.58 6.27 0 -2 4 198.65 5.91 0 -2 3 2.73 0.69 0 -2 3 2.44 0.22 0 2 -3 2.71 0.8 0 -2 3 2.61 0.55 0 -2 3 1.84 0.62 0 2 -3 2.88 0.69 0 -2 3 2.81 0.82 0 -2 3 2.49 0.28 0 -2 2 1632.43 35.14 0 2 -2 1659.57 36.18 0 -2 2 1715.28 32.89 0 2 -2 1602.03 34.48 0 -2 2 1709.32 32.67 0 -2 2 1669.16 35.19 0 -2 2 1643.95 34.33 0 -2 2 1641.21 36.2 0 -2 1 122.96 2.92 0 -2 1 115.61 4.36 0 -2 1 123.81 3.98 0 -2 1 116.76 3.04 0 -2 1 118.94 4.3 0 2 -1 105.09 3.87 0 2 -1 113.61 4.9 0 -2 1 103.56 4.68 0 2 0 652.89 16.17 0 -2 0 655.29 13.58 0 2 0 649.05 14.68 0 -2 0 616.96 15.12 0 -2 0 662.03 15.14 0 2 0 662.06 16.2 0 -2 0 670.82 13.51 0 -2 0 654.36 14.72 0 -2 -1 222.93 6.14 0 2 1 221.55 7.24 0 2 1 208.8 6.08 0 -2 -1 216.61 5.48 0 2 1 220.45 6.01 0 -2 -1 221.35 5.24 0 -2 -1 215.19 6.4 0 2 1 234.99 7.31 0 -2 -1 230 5.24 0 -2 -2 497.55 12.42 0 -2 -2 534.38 12.21 0 2 2 519.18 12.03 0 2 2 544.41 13.39 0 -2 -2 502.74 11.41 0 -2 -2 524.12 11.21 0 -2 -2 545.03 11.26 0 2 2 495.53 11.85 0 2 2 502.21 13.38 0 -2 -3 392.06 10.14 0 2 3 401.93 9.59 0 -2 -3 389.07 8.97 0 2 3 390.95 10.74 0 -2 -3 416.69 9.92 0 -2 -3 395.5 9.32 0 2 3 404.88 11.08 0 -2 -3 409.23 9.06 0 -2 -4 41.81 2.2 0 2 4 38.23 2.64 0 2 4 43.81 2.81 0 -2 -4 39.78 2.33 0 -2 -4 37.95 1.99 0 -2 -4 45.83 1.83 0 -2 -4 40.6 1.96 0 2 4 38.95 1.88 0 -2 -4 41.69 1.71 0 2 4 40.75 2.58 0 -2 -5 6.86 0.74 0 -2 -5 10.03 1.07 0 2 5 9.25 0.87 0 2 5 7.47 1.19 0 -2 -5 7.6 0.77 0 -2 -5 7.48 0.99 0 -2 -5 6.63 0.84 0 -2 -5 8.41 0.77 0 -2 -5 7.15 0.86 0 2 5 7.23 1.13 0 -2 -6 734.79 15.92 0 2 6 736.76 18.25 0 2 6 705.34 17.71 0 -2 -6 668.19 15.94 0 -2 -6 786.18 16.86 0 -2 -6 728.92 17.3 0 2 6 705.79 15.83 0 -2 -6 688.65 16.44 0 -2 -6 731.82 15.58 0 -2 -7 0.47 0.37 0 2 7 0.76 0.71 0 -2 -7 -0.01 0.42 0 -2 -7 1.2 0.44 0 -2 -7 0.46 0.31 0 -2 -7 0.44 0.3 0 2 7 0.18 0.19 0 -2 -7 0.33 0.26 0 2 7 0.25 0.54 0 -2 -8 54.97 2.69 0 2 8 53.57 2.53 0 2 8 57.27 3.59 0 -2 -8 55.86 2.39 0 -2 -8 58.37 3.4 0 2 8 55.15 3.73 0 -2 -8 52.43 2.57 0 -2 -8 56.65 2.97 0 -2 -8 53.02 2.93 0 2 9 33.03 2.82 0 2 9 38.33 2.13 0 -2 -9 39.11 2 0 -2 -9 38.45 2.2 0 -2 -9 38.48 2.44 0 2 9 37.62 3.22 0 -2 -9 40.86 2.93 0 -2 -9 36.99 2.23 0 2 10 275.75 9.79 0 2 10 267.17 7.84 0 -2 -10 278.16 9.41 0 2 10 281.92 10.49 0 -2 -10 276.33 8.01 0 -2 -10 270.03 7.34 0 -2 -10 265.36 7.84 0 2 11 25 2.91 0 -2 -11 23.16 1.87 0 2 11 24.14 1.96 0 2 11 21.99 2.48 0 -2 -11 21.72 1.86 0 -2 -11 19.43 2.26 0 -2 -11 21.13 1.6 0 2 12 57 3.31 0 -2 -12 59.13 3.29 0 2 12 57.91 4.68 0 -2 -12 56.67 3.24 0 2 12 58.69 4.37 0 -2 -12 62.34 4.27 0 -2 -13 24.88 2.85 0 2 13 19.67 2.81 0 2 13 21.23 2.67 0 -2 -13 19.91 2.02 0 -2 -14 1.26 0.67 0 2 14 0.64 0.85 0 2 14 1.57 0.88 0 -2 -14 1.35 0.85 0 2 15 1.04 1.35 0 -2 -15 0.47 0.69 0 2 15 2.68 1.17 0 2 16 14.78 2.64 0 -2 -16 11.07 2.29 0 2 16 8.96 2.38 0 -2 -17 23.17 3.39 0 2 17 20.03 3.27 0 2 17 20.13 3.49 0 -3 14 35.1 4.6 0 3 -14 40.89 4.95 0 3 -14 39.66 4.11 0 3 -13 4.33 1.47 0 3 -13 5.02 1.81 0 -3 13 7.42 2.01 0 -3 12 72.22 6.2 0 3 -12 73.44 5.24 0 3 -12 70 6.1 0 -3 11 1.23 1.05 0 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1.08 0 -3 2 7.48 1.23 0 -3 2 6.17 1.31 0 -3 2 9.33 0.74 0 -3 2 8.2 1.09 0 3 -1 232.01 7.28 0 -3 1 235.31 7.21 0 3 -1 226.97 8.78 0 -3 1 234.58 5.77 0 -3 1 216.77 8.62 0 -3 1 235.93 5.49 0 -3 1 227.98 7.73 0 -3 1 224.21 7.69 0 3 0 4.03 0.82 0 3 0 2.39 0.95 0 -3 0 5.33 0.53 0 -3 0 3.78 0.91 0 -3 0 4.98 0.94 0 -3 0 4.1 0.79 0 3 0 4.94 1.24 0 -3 0 5.21 0.64 0 3 1 167.12 6.93 0 -3 -1 166.9 4.31 0 -3 -1 163.25 4.44 0 3 1 159.61 5.51 0 3 1 161.01 5.69 0 -3 -1 142.49 5.77 0 -3 -1 154.59 5.77 0 -3 -1 156.43 5.55 0 3 1 159.95 6.86 0 -3 -2 93.52 3.25 0 -3 -2 103.72 4.19 0 3 2 98.48 5.06 0 3 2 98.32 4.12 0 -3 -2 100.24 4.35 0 -3 -2 105.46 3.19 0 3 2 97.93 5.12 0 3 2 100.16 3.98 0 -3 -2 101.46 3.22 0 -3 -3 22.5 1.94 0 -3 -3 21.87 1.4 0 3 3 34.91 2.91 0 3 3 29.09 2.81 0 -3 -3 27.12 2.24 0 3 3 26.09 1.95 0 3 4 42.93 2.41 0 3 4 47.81 3.3 0 -3 -4 42.47 2.74 0 -3 -4 47.4 2.08 0 -3 -4 47.34 2.72 0 -3 -4 41.34 2.03 0 3 4 46.06 3.35 0 -3 -4 46.85 2.11 0 3 5 155.73 5.09 0 3 5 164.51 6.91 0 -3 -5 146.96 4.83 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8.56 0 4 -5 163.25 7.13 0 -4 5 180.76 7.74 0 -4 5 159.52 7.34 0 -4 5 165.68 6.65 0 -4 5 154.36 8.5 0 -4 4 719.66 15.72 0 -4 4 708.11 19.47 0 4 -4 709.01 18.93 0 -4 4 675.68 21.29 0 -4 4 728.3 19.63 0 4 -4 713.42 21.44 0 -4 4 701.44 18.22 0 4 -3 20.42 2.67 0 -4 3 18.92 2.3 0 -4 3 19.46 2.74 0 -4 3 16.64 2.14 0 4 -3 21.06 2.27 0 -4 3 22.02 1.37 0 -4 3 23.68 2.22 0 4 -2 30.61 2.67 0 -4 2 30.5 2.78 0 -4 2 32.26 1.37 0 -4 2 24.01 3.04 0 -4 2 28.67 2.43 0 -4 2 31.32 1.67 0 -4 2 28.81 2.7 0 4 -2 34.81 3.56 0 -4 1 0.46 0.63 0 4 -1 -0.54 0.81 0 4 -1 -0.3 0.62 0 -4 1 0.34 0.31 0 -4 1 -0.01 0.37 0 -4 1 -0.2 0.49 0 -4 1 0.72 0.26 0 4 -1 1.06 0.69 0 4 0 248.53 10.22 0 4 0 244.65 8.37 0 -4 0 241.82 8.88 0 -4 0 233.48 8.42 0 -4 0 237.75 6.52 0 -4 0 238.7 8.17 0 4 0 244.02 9.9 0 -4 0 254.48 6.15 0 -4 -1 215.84 5.65 0 -4 -1 211.83 7.49 0 -4 -1 204.69 8.03 0 4 1 215.09 9.28 0 4 1 206.07 7.56 0 4 1 210.53 9.07 0 -4 -1 205.29 5.89 0 4 1 210.87 7.46 0 -4 -1 223.65 7.94 0 -4 -2 21.76 1.47 0 -4 -2 20.98 1.35 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18.61 2.21 0 5 2 6.35 1.64 0 5 2 8.29 1.84 0 5 2 7.2 1.38 0 -5 -2 6.35 0.81 0 -5 -2 6.03 1.38 0 -5 -2 7.07 1.4 0 -5 -2 10.12 1.87 0 -5 -2 6.34 0.94 0 -5 -3 102.22 3.72 0 -5 -3 99.47 5.25 0 -5 -3 93.97 5.7 0 -5 -3 92 3.88 0 5 3 102.55 6.76 0 5 3 96.26 6.31 0 -5 -3 87.88 5.01 0 5 4 2.39 1.2 0 -5 -4 6.83 1.58 0 -5 -4 7 1 0 5 4 8.29 1.92 0 -5 -4 5.8 1.31 0 -5 -4 6.59 1.33 0 -5 -4 7.09 0.94 0 5 5 167.07 8.48 0 -5 -5 176.78 7.48 0 -5 -5 184.36 6.14 0 5 5 180.95 9.07 0 -5 -5 185.59 7.68 0 -5 -5 183.6 5.89 0 -5 -6 108.24 4.43 0 5 6 97.59 6.44 0 -5 -6 108.75 5.68 0 5 6 98.25 6.52 0 -5 -6 105.56 4.27 0 5 6 101.93 6.29 0 -5 -6 109.47 5.65 0 -5 -7 212.2 8.63 0 5 7 212.28 9.57 0 -5 -7 221.18 7.15 0 5 7 212.93 10.11 0 5 7 213.46 10.1 0 -5 -7 226.2 7.09 0 -5 -7 226.75 8.8 0 5 8 5.21 1.6 0 5 8 1.98 1.02 0 -5 -8 4.33 1.13 0 -5 -8 5.16 0.97 0 -5 -8 4.46 1.25 0 -5 -8 4.27 0.88 0 5 8 4.04 1.42 0 -5 -9 34.59 3.16 0 -5 -9 32.71 2.46 0 5 9 27.78 3.44 0 -5 -9 30.43 3.01 0 5 9 30.13 3.29 0 -5 -9 25.97 2.18 0 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38.53 3.54 0 6 6 3.65 1.35 0 -6 -6 2.07 0.76 0 -6 -6 4.17 1.67 0 6 6 5.99 2.01 0 -6 -6 4.21 1.42 0 -6 -6 1.89 0.65 0 6 6 5.77 2.05 0 -6 -6 4.66 1.33 0 -6 -7 35.45 2.73 0 -6 -7 38.23 3.59 0 6 7 38.43 4.38 0 -6 -7 39.8 2.73 0 6 7 39.99 4.42 0 6 7 39.08 4.12 0 -6 -7 41.01 3.62 0 -6 -8 4.26 1.32 0 6 8 5.25 1.62 0 6 8 6.54 1.96 0 6 8 6.36 1.94 0 -6 -8 5.6 1.43 0 -6 -8 5.68 1.1 0 -6 -8 8.14 1.34 0 -6 -9 105.63 6.25 0 -6 -9 122.23 6.76 0 6 9 115.06 7.71 0 -6 -9 107.02 5.13 0 -6 -9 103.65 4.98 0 6 9 96.43 6.64 0 -6 -10 29.5 2.59 0 -6 -10 27.75 3.18 0 6 10 28.91 3.82 0 6 10 31.98 3.72 0 -6 -10 27.41 2.53 0 -6 -10 31.5 3.39 0 -6 -11 -0.67 0.67 0 6 11 0.73 0.56 0 6 11 0.63 1.01 0 -6 -11 0.7 0.5 0 -6 -11 0.71 0.59 0 -6 -12 1.59 0.7 0 6 12 0.46 0.82 0 6 12 1.16 0.86 0 -6 -12 1.18 0.74 0 -6 -12 2.01 1.19 0 -6 -13 3.61 1.45 0 -6 -13 2.51 0.93 0 -6 -13 -0.27 0.64 0 6 13 4.96 1.83 0 6 13 0.91 0.98 0 -7 6 35.73 4.41 0 7 -6 27.53 4.71 0 7 -6 21 4.03 0 -7 6 27.43 3.47 0 7 -5 0.03 0.8 0 7 -5 1.27 1.22 0 -7 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1 90.72 3.78 1 -4 1 80.39 4.46 -1 4 -1 85.73 4.23 -1 4 -1 83.7 5.98 1 -4 1 85.1 5.24 1 -4 2 167.8 6.85 -1 4 -2 161.89 8.37 1 -4 2 160.98 8.22 -1 4 -2 163.49 6.47 1 -4 2 168.24 7.82 -1 4 -2 169.3 9.03 1 -4 3 51.23 4.09 -1 4 -3 51.6 4.81 1 -4 3 47.46 3.33 1 -4 3 37.12 3.87 -1 4 -3 46.72 3.2 -1 4 -3 47.76 4.46 -1 4 -4 3.84 0.98 -1 4 -4 4.57 1.41 1 -4 4 0.8 0.68 1 -4 4 3.65 1.04 1 -4 4 4.32 1.47 1 -4 5 783.43 19.82 1 -4 5 786.87 22.07 1 -4 5 756.1 23.05 -1 4 -5 709.97 19.42 -1 4 -5 768.19 23.3 1 -4 6 125.77 7.71 1 -4 6 129.88 7.13 -1 4 -6 115.43 7.56 -1 4 -6 115.35 5.7 -1 4 -7 62.67 4.18 1 -4 7 60.33 3.91 -1 4 -7 55.91 5.3 1 -4 7 59.79 5.42 1 -4 7 61.42 4.95 -1 4 -8 168.91 9.87 1 -4 8 194.16 9.42 1 -4 8 159.55 9.52 -1 4 -8 153.95 7.37 1 -4 8 184.87 7.44 1 -4 9 89.74 6.35 -1 4 -9 91.69 7.24 1 -4 9 83.8 6.81 -1 4 -9 81.38 5.25 1 -4 10 117.5 8.42 -1 4 -10 118.39 8.56 1 -4 10 132.76 7.95 -1 4 -10 113.62 6.6 -1 4 -11 3.83 1.42 1 -4 11 2.41 1.63 -1 4 -11 0.25 0.82 -1 4 -12 39.26 4.03 -1 4 -12 42.15 5.31 1 -4 12 34.57 4.7 -1 4 -13 10.3 2.2 1 -4 13 11.18 2.9 -1 4 -13 16.15 3.45 1 -3 -16 -0.41 0.61 -1 3 16 -0.33 0.81 -1 3 15 1.61 1 -1 3 15 0.25 0.97 1 -3 -15 0.66 0.84 -1 3 14 43.64 4.56 -1 3 14 38.57 4.07 1 -3 -14 37.42 3.9 1 -3 -13 97.39 6.07 -1 3 13 90.81 6.13 -1 3 13 96.54 6.64 1 -3 -12 40.64 3.65 -1 3 12 36.32 3.83 -1 3 12 43.96 4.19 1 -3 -11 8.13 1.58 1 -3 -11 9.61 1.76 -1 3 11 11.89 2.1 -1 3 11 8.49 1.73 -1 3 10 124.79 6.68 1 -3 -10 116.06 5.88 1 -3 -10 104.94 4.81 -1 3 10 110.03 6.44 1 -3 -10 133.2 6.28 1 -3 -9 5.51 1 1 -3 -9 9.38 1.64 -1 3 9 6.67 1.49 -1 3 9 7.16 1.48 1 -3 -9 8.55 1.52 1 -3 -9 5.14 0.94 -1 3 8 127.45 6.77 1 -3 -8 133.59 5.88 1 -3 -8 130.26 5.2 -1 3 8 136.41 6.57 1 -3 -8 132.58 5.16 1 -3 -8 151.56 6.42 1 -3 -8 123.35 5.85 -1 3 7 15.71 2.05 1 -3 -7 16.62 1.81 1 -3 -7 15.32 1.86 1 -3 -7 14.06 1.48 1 -3 -7 15.23 1.88 -1 3 7 11.88 1.91 1 -3 -7 12.28 1.34 1 -3 -6 36.27 2.81 1 -3 -6 33.56 2.52 1 -3 -6 33.14 1.84 1 -3 -6 33.34 2.64 -1 3 6 29.87 2.77 -1 3 6 32.3 3.12 1 -3 -6 34.02 2.19 1 -3 -6 33.41 2.23 1 -3 -5 140.46 4.92 -1 3 5 131.01 6.1 1 -3 -5 125.35 5.5 1 -3 -5 136.02 5.78 1 -3 -5 134.21 4.06 -1 3 5 133.89 6.2 1 -3 -5 134.61 4.73 1 -3 -5 134.56 5.3 -1 3 5 130.9 6.66 1 -3 -4 298.03 9.81 -1 3 4 320.34 11.22 -1 3 4 277.92 6.94 1 -3 -4 333.01 9.85 1 -3 -4 314.96 7.27 -1 3 4 305.19 10.13 1 -3 -4 298.79 8.35 1 -3 -4 312.7 8.18 -1 3 4 310.39 10.32 1 -3 -4 298.89 9.21 1 -3 -4 306.09 8.88 1 -3 -3 56.28 3.59 1 -3 -3 56.29 2.75 1 -3 -3 52.49 2.86 1 -3 -3 54.44 2.52 1 -3 -3 56.6 2.01 -1 3 3 58 2.35 -1 3 3 55.41 3.76 1 -3 -3 53.64 3.15 -1 3 3 57.76 4.24 1 -3 -3 55.48 3.34 -1 3 2 1369.4 32.66 -1 3 2 1353.05 28.19 -1 3 2 1300.98 27.63 1 -3 -2 1356.25 29.97 1 -3 -2 1337.58 30.63 1 -3 -2 1305.6 29.35 1 -3 -2 1304.16 28.63 1 -3 -2 1311.21 28.32 1 -3 -2 1300.55 27.79 -1 3 2 1320.88 31.48 1 -3 -1 24.36 2.31 -1 3 1 24.83 2.58 -1 3 1 24.81 1.64 1 -3 -1 23.83 1.97 1 -3 -1 25.95 1.79 1 -3 -1 26.07 2.17 1 -3 -1 24.81 1.48 -1 3 1 26.39 2.9 1 -3 -1 25.08 1.69 -1 3 0 63.95 2.9 -1 3 0 64.12 4.61 -1 3 0 68.14 4.41 1 -3 0 62.69 2.81 1 -3 0 63.2 3.34 1 -3 0 65.13 3.96 1 -3 0 58.47 2.88 1 -3 0 65.6 3.54 1 -3 0 62.27 2.39 1 -3 1 328.9 8.82 -1 3 -1 358.35 12.53 1 -3 1 369.54 9.41 1 -3 1 335.92 10.95 -1 3 -1 344.17 8.51 -1 3 -1 331.31 9.16 1 -3 1 369.39 10.21 1 -3 1 345.19 10.06 -1 3 -1 321.59 11.39 -1 3 -2 14.04 2.23 1 -3 2 14.22 1.4 1 -3 2 12.42 1.91 1 -3 2 14.75 1.93 -1 3 -2 13.42 1.1 -1 3 -2 16 2.16 1 -3 2 12.88 1.5 -1 3 -2 12.9 1.33 1 -3 3 2.67 1 -1 3 -3 3.74 0.84 -1 3 -3 3.11 1 -1 3 -3 3.2 0.53 1 -3 3 1.99 0.6 1 -3 3 1.72 0.58 1 -3 3 3.14 1.12 1 -3 4 2.11 0.72 -1 3 -4 2.53 0.76 1 -3 4 1.48 0.88 1 -3 4 1.26 0.76 1 -3 4 2.52 0.7 -1 3 -4 1.77 0.92 1 -3 5 2.98 0.79 1 -3 5 3.08 1.17 1 -3 5 4.24 1.19 -1 3 -5 3.29 0.78 1 -3 5 3.85 0.93 -1 3 -5 4.28 1.28 -1 3 -6 0.33 0.44 1 -3 6 0.54 0.93 1 -3 6 0.66 0.47 1 -3 6 -0.32 0.72 -1 3 -6 0.87 1 1 -3 7 44.29 4.17 -1 3 -7 49.4 3.3 -1 3 -7 50.23 4.54 1 -3 7 52.14 4.15 1 -3 7 49.34 3.14 -1 3 -8 1518.36 36.17 1 -3 8 1655.72 35.72 1 -3 8 1544.51 39.89 1 -3 8 1672.97 39.12 -1 3 -8 1625.99 40.41 -1 3 -9 86.36 4.93 1 -3 9 87.64 6.31 1 -3 9 89.33 5.88 -1 3 -9 92.16 6.61 1 -3 10 41.1 4.38 -1 3 -10 41.29 3.48 -1 3 -10 43.02 4.67 1 -3 10 45.34 4.19 1 -3 11 1.08 1.14 -1 3 -11 -0.03 0.91 1 -3 11 1.13 0.78 -1 3 -11 1.9 0.95 1 -3 12 12.19 2.58 -1 3 -12 11.99 2.7 -1 3 -12 14.7 2.27 -1 3 -13 48.06 4.22 1 -3 13 48.81 5.32 -1 3 -13 50.6 5.56 1 -3 14 25.41 3.96 -1 3 -14 27.57 4.29 -1 3 -14 29 3.45 -1 2 16 14.14 2.69 -1 2 16 8.26 2.39 1 -2 -16 8.26 1.93 1 -2 -15 0.77 0.79 -1 2 15 1.64 1.13 -1 2 15 0.19 0.67 1 -2 -14 22.55 2.94 -1 2 14 22.03 3.05 -1 2 14 22.54 3.3 1 -2 -13 1.07 0.64 -1 2 13 0.13 0.76 -1 2 13 1.83 1.04 -1 2 12 33.37 3.45 -1 2 12 39.14 3.88 1 -2 -12 35.35 3.36 -1 2 11 21.82 2.71 -1 2 11 25.27 2.97 1 -2 -11 22.04 2.49 1 -2 -10 446.3 13.69 1 -2 -10 475.91 13.54 -1 2 10 439.78 14.27 -1 2 10 461.24 14.56 -1 2 9 1.81 0.81 1 -2 -9 2.58 0.85 -1 2 9 2.54 0.98 1 -2 -9 3.98 1 1 -2 -9 3.38 0.64 1 -2 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519.63 15.75 -4 -3 -4 524.7 14.66 4 3 4 541.2 15.21 4 3 4 519.32 14.39 4 3 4 506.23 15.99 -4 -3 -4 541.39 15.46 -4 -3 -5 318.16 11.18 -4 -3 -5 318.18 10.2 4 3 5 327.11 10.43 4 3 5 304.88 10.04 -4 -3 -5 332.65 10.89 4 3 5 296.99 11.38 -4 -3 -6 76.5 4.8 -4 -3 -6 70.27 4.05 4 3 6 71.51 4.03 4 3 6 71.99 4.18 -4 -3 -6 74.43 4.49 4 3 6 61.44 4.52 -4 -3 -7 9.45 1.62 -4 -3 -7 10.05 1.72 4 3 7 10.44 1.48 4 3 7 11.24 1.68 -4 -3 -7 10.42 1.55 4 3 7 9.49 1.79 -4 -3 -8 24.42 2.61 4 3 8 27.64 2.34 -4 -3 -8 24.23 2.2 -4 -3 -8 26.92 2.51 4 3 8 25.52 2.63 4 3 8 24.69 2.81 -4 -3 -9 453.41 13.17 -4 -3 -9 435.01 12.6 4 3 9 463.45 14.39 4 3 9 436.53 14.61 -4 -3 -10 18.22 2.23 -4 -3 -10 16.38 1.73 -4 -3 -10 21 2.12 -4 -3 -10 23.92 2.95 4 3 10 21.4 2.63 4 3 10 18.38 2.52 -4 -3 -11 -0.21 0.9 -4 -3 -11 0.99 0.55 -4 -3 -11 0.36 0.46 -4 -3 -11 0.06 0.64 4 3 11 1.18 0.8 -4 -3 -11 0.77 0.65 4 3 11 0.63 0.71 -4 -3 -12 26.01 2.74 -4 -3 -12 26.76 2.25 -4 -3 -12 31.58 3.43 4 3 12 29.74 3.43 4 3 12 28.98 3.12 -4 -3 -12 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1.97 1.23 -4 -4 -14 3.66 1.27 -4 -4 -14 3.78 1.01 -4 -4 -14 6.55 1.76 4 4 14 3.45 1.41 4 4 14 2.69 1.16 -4 -4 -15 0.75 1.2 -4 -4 -15 0.01 0.52 -4 -4 -15 3.03 1.7 4 4 15 3.8 1.74 4 4 15 0.21 0.74 -4 -4 -16 13.83 2.54 -4 -4 -16 16.68 2.83 4 4 16 15.6 3.13 4 4 16 14.46 2.43 -4 -5 10 0.92 1.24 -4 -5 10 1.92 1.36 4 5 -10 1.77 1.42 4 5 -10 -0.41 0.93 -4 -5 9 35.5 4.81 -4 -5 9 25.86 3.84 4 5 -9 28.52 4.46 4 5 -9 27.9 4.21 -4 -5 8 7.46 2.25 -4 -5 8 6.1 1.87 4 5 -8 7.54 2.07 4 5 -8 5.21 1.97 -4 -5 7 0.02 1.18 -4 -5 7 0.11 0.76 4 5 -7 2.65 1.41 4 5 -7 -0.34 0.85 -4 -5 6 -0.25 0.75 -4 -5 6 0.01 0.9 4 5 -6 0.42 0.96 4 5 -6 1.76 1.27 4 5 -6 1.1 0.97 -4 -5 5 0.36 0.71 -4 -5 5 -0.21 0.9 -4 -5 5 -0.35 0.78 4 5 -5 -0.1 1.13 4 5 -5 2.05 1.08 4 5 -5 1.75 0.89 -4 -5 4 38.51 4.5 4 5 -4 40.46 4.51 -4 -5 4 36.43 4.29 -4 -5 4 37.15 2.62 4 5 -4 38.14 4.39 -4 -5 4 36.17 3.33 4 5 -4 39.96 4.06 -4 -5 3 4.95 1.37 -4 -5 3 5.15 1.82 -4 -5 3 4 0.91 -4 -5 3 5.26 1.68 4 5 -3 4.27 1.51 4 5 -3 3.03 1.44 4 5 -3 6.92 1.69 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7 29.63 4.13 5 4 -7 37.64 4.45 5 4 -7 31.17 4.06 -5 -4 6 50.92 5.2 5 4 -6 45.42 4.93 5 4 -6 38.75 4.52 -5 -4 6 42.52 4.15 -5 -4 5 24.28 3.61 -5 -4 5 22.41 3.02 -5 -4 5 24.59 2.52 5 4 -5 25.75 3.57 5 4 -5 26.98 3.52 5 4 -5 24.04 3.5 -5 -4 4 -0.49 0.83 -5 -4 4 0.11 0.68 5 4 -4 0.35 0.96 5 4 -4 1.64 1.3 -5 -4 4 -0.24 0.76 5 4 -4 0.46 1.04 -5 -4 3 1181.23 32.3 -5 -4 3 1112.48 27.95 5 4 -3 1154.41 31.66 5 4 -3 1146.45 31.3 5 4 -3 1160.32 31.34 -5 -4 3 1133.5 29.98 -5 -4 2 258.86 11.85 -5 -4 2 250.55 9.36 5 4 -2 252.27 11.41 5 4 -2 255.31 11.28 5 4 -2 243.96 11.09 -5 -4 2 245.25 10.51 -5 -4 1 5.43 1.82 -5 -4 1 3.83 1.08 5 4 -1 5.24 1.67 -5 -4 1 3.14 1.18 5 4 -1 4.52 1.39 5 4 -1 5.5 1.56 -5 -4 0 25.63 3.41 -5 -4 0 33.81 3.02 5 4 0 34.09 3.61 5 4 0 31.32 3.54 5 4 0 30.33 3.5 -5 -4 0 33.48 3.45 -5 -4 -1 82.06 5.93 -5 -4 -1 84.36 4.95 5 4 1 88.12 5.75 5 4 1 81.79 5.9 -5 -4 -1 90.32 5.73 -5 -4 -2 0.18 0.81 -5 -4 -2 -0.29 0.83 -5 -4 -2 1.68 0.86 5 4 2 0.79 0.71 5 4 2 0.4 0.94 -5 -4 -3 0.91 0.62 -5 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-5 -4 -13 9.93 1.66 5 4 13 11.98 2.35 5 4 13 9.17 2.02 -5 -4 -14 4.69 1.71 -5 -4 -14 2.58 1.29 5 4 14 7.29 1.95 5 4 14 6.05 1.65 -5 -4 -15 2.03 1.28 -5 -4 -15 2.67 1.44 5 4 15 1.28 0.9 5 4 15 1.72 1.06 -5 -5 9 17.73 3.52 5 5 -9 17.26 3.46 5 5 -9 18.82 3.43 -5 -5 8 1.39 1.49 5 5 -8 1.45 1.69 5 5 -8 -0.4 0.82 -5 -5 7 22.93 3.68 5 5 -7 28.13 4.27 5 5 -7 25.69 3.83 -5 -5 6 18.22 3.36 -5 -5 6 24.17 3.47 5 5 -6 19.09 3.42 -5 -5 6 22.57 3.01 5 5 -6 21.22 3.51 -5 -5 5 46.37 5.23 5 5 -5 38.95 4.67 -5 -5 5 38.27 4.25 5 5 -5 37.57 4.57 -5 -5 5 36.81 3.76 -5 -5 4 187.93 10.78 -5 -5 4 190.6 7.53 5 5 -4 206.55 10.94 -5 -5 4 173.44 9.49 5 5 -4 170.28 9.91 -5 -5 4 179.05 8.83 -5 -5 3 0.96 0.89 -5 -5 3 2.81 1.15 -5 -5 3 5.52 1.24 5 5 -3 2.25 0.97 5 5 -3 4.45 1.69 5 5 -3 3.99 1.56 -5 -5 2 125.46 8.28 -5 -5 2 119.31 5.83 5 5 -2 133.96 8.41 5 5 -2 123.74 7.44 5 5 -2 122.22 7.95 -5 -5 2 119.03 6.9 -5 -5 1 53.68 5.3 -5 -5 1 56.42 3.79 5 5 -1 52.59 5.16 5 5 -1 53.53 4.68 5 5 -1 45.88 4.74 -5 -5 1 49.48 4.32 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24.29 3.35 -5 -5 -10 3.68 1.2 -5 -5 -10 2.54 0.92 5 5 10 2.29 1.08 -5 -5 -10 2.3 0.83 5 5 10 3.21 1.35 -5 -5 -11 0.26 0.66 -5 -5 -11 0 0.45 5 5 11 0.07 0.68 -5 -5 -11 1.34 0.84 5 5 11 -1.65 1.03 -5 -5 -12 5.92 1.72 -5 -5 -12 4.56 1.12 -5 -5 -12 6.85 1.76 5 5 12 3.82 1.44 -5 -5 -12 6.17 1.45 5 5 12 5.73 1.66 -5 -5 -13 -0.16 0.78 -5 -5 -13 0.57 0.73 -5 -5 -13 -1.11 1 -5 -5 -13 0.99 0.65 5 5 13 0.98 0.92 5 5 13 0.8 1.08 -5 -5 -14 -0.02 1.18 -5 -5 -14 3.56 1.37 -5 -5 -14 4.82 1.74 -5 -5 -14 3.04 1.05 5 5 14 4.73 1.84 5 5 14 3.68 1.53 -5 -5 -15 1.03 1.02 -5 -5 -15 -0.31 0.56 -5 -5 -15 2.16 1.35 5 5 15 1.59 1.19 5 5 15 2.49 1.28 -5 -6 8 7 2.44 -5 -6 8 5.6 2.14 5 6 -8 4.69 1.66 -5 -6 7 7.97 2.5 -5 -6 7 4.3 1.67 5 6 -7 6.04 2.15 5 6 -7 4.87 1.8 -5 -6 6 5.26 2.29 -5 -6 6 1.47 0.94 5 6 -6 4.39 2.09 5 6 -6 3.19 1.62 -5 -6 5 5.38 2.11 -5 -6 5 7.08 2.17 5 6 -5 4.57 2.01 5 6 -5 6.52 2.14 -5 -6 4 0.36 1.02 5 6 -4 -0.27 0.87 -5 -6 4 0.15 0.96 5 6 -4 -0.25 0.86 -5 -6 3 0.8 1.02 -5 -6 3 1.22 0.74 5 6 -3 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4.56 6 -3 2 30.93 4.5 6 -3 2 30.25 3.94 -6 2 6 95.4 7.69 -6 2 6 99.45 5.53 6 -2 -6 88.08 8.18 6 -2 -6 94.56 7.37 -6 2 5 114.45 8.54 -6 2 5 138.04 6.71 6 -2 -5 127.97 9.7 6 -2 -5 122.56 8.29 -6 2 4 25.42 3.87 -6 2 4 26.57 2.84 6 -2 -4 23.85 4.08 6 -2 -4 22.26 3.37 -6 2 3 5.14 1.83 -6 2 3 6.52 1.48 6 -2 -3 4.38 1.88 6 -2 -3 8.97 2.2 -6 2 2 5.17 1.91 -6 2 2 5.41 1.35 6 -2 -2 5.63 2.25 6 -2 -2 5.91 1.76 -6 2 1 31.68 4.45 -6 2 1 35.91 3.3 6 -2 -1 31.29 4.51 6 -2 -1 25.71 3.59 6 -2 -1 31.76 3.87 -6 2 0 17.46 2.34 -6 2 0 16.07 3.17 6 -2 0 16.7 3.29 6 -2 0 11.95 2.58 6 -2 0 10.94 2.25 -6 2 -1 10.21 2.7 -6 2 -1 16.02 2.25 6 -2 1 15.95 3.11 6 -2 1 18.33 3.24 6 -2 1 12.23 2.38 -6 2 -2 5.44 2.07 -6 2 -2 13.09 2.04 6 -2 2 12.32 2.82 6 -2 2 11.27 2.5 6 -2 2 9.65 2.07 -6 2 -3 17.98 2.36 -6 2 -3 13.86 3.21 6 -2 3 10.71 2.7 6 -2 3 12.34 2.66 6 -2 3 13.43 2.43 -6 2 -4 32.57 3.11 -6 2 -4 34.48 4.99 6 -2 4 30.62 4.12 6 -2 4 25.85 4.01 -6 2 -5 -1.62 1.25 -6 2 -5 0.73 0.67 6 -2 5 2.63 1.46 6 -2 5 0.52 1.03 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6 -3 4.77 2.03 7 6 -3 5.09 1.98 -7 -6 2 1.2 1.01 -7 -6 2 1.51 1.44 -7 -6 2 1.24 0.72 7 6 -2 3.61 1.78 7 6 -2 -0.58 1.39 7 6 -2 0.12 0.81 -7 -6 1 25.22 4.32 -7 -6 1 23.87 2.94 7 6 -1 34.37 4.71 -7 -6 1 27.67 3.76 -7 -6 0 26.82 4.31 -7 -6 0 22.11 2.83 -7 -6 0 26.4 3.66 7 6 0 24.99 3.94 -7 -6 -1 2.14 1.34 -7 -6 -1 3.07 1.07 -7 -6 -1 0.1 1.09 7 6 1 -0.02 1.09 -7 -6 -2 2.74 1.22 -7 -6 -2 1.99 0.94 -7 -6 -2 3.23 1.21 7 6 2 3.66 1.73 -7 -6 -3 17.11 3.29 -7 -6 -3 22.17 2.9 -7 -6 -3 17.91 2.99 7 6 3 16.2 3.29 -7 -6 -4 6.64 2.09 -7 -6 -4 7.34 1.72 -7 -6 -4 5.21 1.8 7 6 4 5.9 2.09 -7 -6 -5 47.51 5.36 -7 -6 -5 43.83 4.03 -7 -6 -5 46.76 4.78 7 6 5 44.67 5.19 -7 -6 -6 7.55 2.37 -7 -6 -6 8.2 2.19 -7 -6 -6 7.3 1.57 7 6 6 7.84 2.28 -7 -6 -7 1.34 1.24 -7 -6 -7 1.07 1.08 -7 -6 -7 1.12 0.74 7 6 7 0.14 0.96 -7 -6 -8 1.23 1.06 -7 -6 -8 -0.21 1.02 -7 -6 -8 -0.4 0.89 7 6 8 0.35 0.89 -7 -6 -9 6.06 1.79 -7 -6 -9 3.4 1.29 7 6 9 4.9 1.85 -7 -6 -10 10.64 2.01 7 6 10 10.4 2.45 -7 -6 -10 12.7 2.16 -7 -7 1 6.7 2.42 -7 -7 1 3.9 1.13 -7 -7 1 5.05 1.76 7 7 -1 3.37 1.99 7 7 -1 7.19 2.45 -7 -7 0 56.14 6.47 -7 -7 0 55.5 4.38 -7 -7 0 60.61 5.59 7 7 0 61.04 6.52 -7 -7 -1 26.85 4.45 -7 -7 -1 25.58 2.99 -7 -7 -1 28.86 3.92 7 7 1 29.12 4.55 -7 -7 -2 5.02 1.84 -7 -7 -2 8.35 2.08 -7 -7 -2 7.75 1.65 7 7 2 9.18 2.59 -7 -7 -3 4.16 1.73 -7 -7 -3 1.92 1.22 -7 -7 -3 2.74 1.11 7 7 3 4.12 1.97 -7 -7 -4 132.84 9.66 -7 -7 -4 128.05 7.04 -7 -7 -4 129.14 8.27 7 7 4 122.51 9.27 -7 -7 -5 150.79 10.3 -7 -7 -5 143.21 7.53 -7 -7 -5 157.85 9.15 7 7 5 146.19 10.07 -7 -7 -6 49.5 5.72 -7 -7 -6 49.05 4.16 -7 -7 -6 45.62 4.77 7 7 6 46.72 5.65 -7 -7 -7 20.23 3.73 -7 -7 -7 20.84 2.71 -7 -7 -7 26.38 3.64 7 7 7 23.69 4.1 -7 -7 -8 36.52 4.82 -7 -7 -8 37.22 3.64 -7 -7 -8 29.15 3.72 7 7 8 37.57 4.95 -8 -2 1 11.11 2.45 8 2 -1 7.3 2.52 -8 -2 1 7.08 2.12 -8 -2 0 0.84 0.86 -8 -2 0 2.38 1.92 8 2 0 -1.57 1.49 -8 -2 -1 7.09 2.19 8 2 1 14.64 3.36 -8 -2 -1 13.83 2.76 -8 -2 -2 29.24 4.08 -8 -2 -2 36.1 4.37 8 2 2 25.76 4.29 -8 -2 -3 10.93 2.39 8 2 3 13.95 3.13 -8 -2 -3 11 2.54 -8 -2 -4 9.73 2.37 -8 -2 -4 6.92 2.06 8 2 4 8.04 2.4 -8 -2 -5 3.23 1.39 -8 -2 -5 3.41 1.64 8 2 5 1.33 1.32 -8 -2 -6 1.55 1.18 8 2 6 2.31 1.43 -8 -3 2 59.33 5.47 8 3 -2 46.65 6.22 -8 -3 2 41.18 4.98 -8 -3 1 0.01 0.84 8 3 -1 1.59 1.5 -8 -3 1 0.39 1.14 -8 -3 0 4.33 1.76 -8 -3 0 2.49 1.32 8 3 0 1.59 1.58 -8 -3 -1 4.64 1.69 -8 -3 -1 4.54 1.58 8 3 1 5.21 2 -8 -3 -2 3.51 1.71 8 3 2 3.04 1.41 -8 -3 -2 2.3 1.08 -8 -3 -3 3.49 1.2 -8 -3 -3 6.82 2.02 8 3 3 5.83 1.76 -8 -3 -4 -0.63 0.93 -8 -3 -4 -1.12 1.17 8 3 4 -0.58 1.09 -8 -3 -5 10.64 2.37 -8 -3 -5 2.4 1.31 8 3 5 9.37 2.5 -8 -3 -6 2.41 1.11 8 3 6 -0.86 1.01 8 3 6 -0.6 1.02 -8 -3 -6 -0.66 0.91 -8 -3 -7 2.78 1.38 8 3 7 1.89 1.39 8 3 7 1.5 0.81 -8 -4 1 10.6 2.32 8 4 -1 11.42 3.08 -8 -4 1 12.77 2.95 -8 -4 0 0.3 0.67 8 4 0 -0.09 1.01 -8 -4 0 -0.32 0.86 -8 -4 -1 1.91 1.07 8 4 1 4.08 1.68 -8 -4 -1 3.08 1.56 -8 -4 -2 24.3 3.74 -8 -4 -2 22.1 3.3 8 4 2 26.18 4.22 8 4 2 25.49 3.76 -8 -4 -3 24.27 3.61 -8 -4 -3 22.06 3.3 8 4 3 23.65 3.89 8 4 3 22.61 3.52 -8 -4 -4 0.72 1.24 8 4 4 3.46 1.72 8 4 4 1.13 1.29 -8 -4 -4 1.53 1.36 -8 -4 -5 22.42 3.3 8 4 5 20.59 3.43 8 4 5 25.47 3.72 -8 -4 -5 19.08 3.2 -8 -4 -6 19.62 3.01 -8 -4 -6 21.05 3.36 8 4 6 22.54 3.47 -8 -4 -7 8.17 2.03 -8 -4 -7 8.21 2.13 8 4 7 5.67 1.63 -8 -4 -8 12.46 2.48 -8 -4 -8 9.68 2.21 8 4 8 12.87 2.7 -8 -5 0 2.79 1.44 8 5 0 0.34 0.83 8 5 0 1.89 1.37 -8 -5 -1 11.86 2.62 -8 -5 -1 9.13 2.14 8 5 1 7.11 2.3 8 5 1 12.04 2.78 -8 -5 -2 0.42 1.17 -8 -5 -2 -0.94 1.07 8 5 2 -0.57 1.18 -8 -5 -3 6.85 2.03 8 5 3 4.49 1.87 -8 -5 -3 2.87 1.43 -8 -5 -4 3.97 1.37 -8 -5 -4 3.61 1.48 8 5 4 3.07 1.57 -8 -5 -5 13.76 2.49 -8 -5 -5 12.47 2.68 8 5 5 19.59 3.54 -8 -5 -6 45.98 4.64 -8 -5 -6 41.17 4.7 8 5 6 48.93 5.36 -8 -5 -7 0.35 1.03 -8 -5 -7 0.64 1.15 8 5 7 0.77 1.14 -8 -6 -3 1.14 1.12 -8 -6 -3 2.9 1.29 -8 -6 -3 4.43 1.85 8 6 3 1.22 1.45 -8 -6 -4 4.31 1.61 -8 -6 -4 0.93 1.31 8 6 4 2.53 1.63 8 6 5 2.48 1.49