#------------------------------------------------------------------------------ #$Date: 2020-03-06 02:55:56 +0200 (Fri, 06 Mar 2020) $ #$Revision: 249096 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/74/1557490.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557490 loop_ _publ_author_name 'Ptak, Maciej' 'Svane, Katrine L.' 'Collings, Ines E.' 'Paraguassu, Waldeci' _publ_section_title ; Effect of Alkali and Trivalent Metal Ions on the High-Pressure Phase Transition of [C2H5NH3]MI0.5MIII0.5(HCOO)3 (MI = Na, K and MIII = Cr, Al) Heterometallic Perovskites ; _journal_name_full 'The Journal of Physical Chemistry C' _journal_paper_doi 10.1021/acs.jpcc.0c00372 _journal_year 2020 _chemical_formula_moiety 'C6 H6 Cr K O12, 2(C2 H8 N)' _chemical_formula_sum 'C10 H22 Cr K N2 O12' _chemical_formula_weight 453.39 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 90 _cell_angle_beta 90.098(6) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.0498(6) _cell_length_b 9.9049(8) _cell_length_c 12.4534(6) _cell_measurement_reflns_used 434 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 18.5700 _cell_measurement_theta_min 1.7400 _cell_volume 992.94(12) _computing_cell_refinement 'CrysAlisPro (Agilent Technologies, 2013)' _computing_data_reduction 'CrysAlisPro (Agilent Technologies, 2013)' _computing_molecular_graphics 'SHELXLE-2011 (Huebschle, 2011)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_pressure '0 GPa' _diffrn_ambient_temperature 293(2) _diffrn_detector_area_resol_mean 7 _diffrn_measured_fraction_theta_full 0.515 _diffrn_measured_fraction_theta_max 0.312 _diffrn_measurement_device_type 'ID15B beamline, ESRF' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.41115 _diffrn_reflns_av_R_equivalents 0.0424 _diffrn_reflns_av_unetI/netI 0.0570 _diffrn_reflns_Laue_measured_fraction_full 0.515 _diffrn_reflns_Laue_measured_fraction_max 0.312 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 3252 _diffrn_reflns_point_group_measured_fraction_full 0.515 _diffrn_reflns_point_group_measured_fraction_max 0.312 _diffrn_reflns_theta_full 14.282 _diffrn_reflns_theta_max 22.076 _diffrn_reflns_theta_min 1.741 _diffrn_source synchrotron _exptl_absorpt_coefficient_mu 0.193 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.94487 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'dark blue' _exptl_crystal_density_diffrn 1.516 _exptl_crystal_description block _exptl_crystal_F_000 470 _exptl_crystal_size_max 0.050 _exptl_crystal_size_mid 0.050 _exptl_crystal_size_min 0.050 _refine_diff_density_max 0.325 _refine_diff_density_min -0.503 _refine_diff_density_rms 0.064 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.108 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 123 _refine_ls_number_reflns 1978 _refine_ls_number_restraints 12 _refine_ls_restrained_S_all 1.105 _refine_ls_R_factor_all 0.0976 _refine_ls_R_factor_gt 0.0630 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0828P)^2^+0.3974P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1644 _refine_ls_wR_factor_ref 0.2113 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1116 _reflns_number_total 1978 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jp0c00372_si_002.cif _cod_data_source_block EtaKCrF_c6_p0 _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1557490 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL EtaKCrD_c6_f2_76_R10_RO_a.res in P2(1)/n EtaKCrD_c6_f2_76_R10_RO_a.res created by SHELXL-2016/6 at 10:59:45 on 08-Nov-2018 REM Old TITL EtaKCrD_c6_f2_76_R10_RO in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.173, Rweak 0.054, Alpha 0.024, Orientation as input REM Formula found by SHELXT: C10 O12 K Cr CELL 0.41115 8.0498 9.9049 12.4534 90.000 90.098 90.000 ZERR 2.000 0.0006 0.0008 0.0006 0.000 0.006 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O K CR DISP $C -0.00006 0.00048 5.14168!source kissel DISP $H -0.00003 0.00000 0.64129!source kissel DISP $N 0.00062 0.00099 7.19180!source kissel DISP $O 0.00180 0.00183 10.15742!source kissel DISP $K 0.08048 0.08446 216.06612!source kissel DISP $Cr 0.16119 0.22192 542.61250!source kissel UNIT 20.00 44.00 4.00 24.00 2.00 2.00 OMIT 0 0 4 OMIT -1 0 3 L.S. 50 BOND $H ACTA LIST 4 DELU O1 C1 O2 DELU O3 C2 O4 DELU O5 C3 O6 DELU N1 C4 C5 FMAP 2 PLAN 20 WGHT 0.082800 0.397400 FVAR 1.16948 CR1 6 0.500000 0.500000 0.500000 10.50000 0.02489 0.03282 = 0.02801 0.00161 -0.00025 -0.00047 K1 5 0.500000 0.500000 1.000000 10.50000 0.03388 0.03569 = 0.03278 -0.00021 0.00278 0.00178 C1 1 0.776912 0.310948 0.476984 11.00000 0.03699 0.04863 = 0.04556 0.01059 0.00163 0.00690 AFIX 43 H1 2 0.743074 0.277379 0.543170 11.00000 -1.20000 AFIX 0 C2 1 0.294549 0.262608 0.542892 11.00000 0.04144 0.04639 = 0.04397 0.00651 -0.00437 -0.00731 AFIX 43 H2 2 0.222727 0.298520 0.491766 11.00000 -1.20000 AFIX 0 C3 1 0.577016 0.526796 0.728240 11.00000 0.03758 0.07684 = 0.03189 0.00318 -0.00110 -0.00547 AFIX 43 H3 2 0.469833 0.494386 0.738720 11.00000 -1.20000 AFIX 0 O1 4 0.696692 0.409464 0.439079 11.00000 0.03495 0.04406 = 0.04016 0.00358 0.00512 0.00576 O2 4 0.897616 0.254827 0.433264 11.00000 0.04485 0.05303 = 0.06594 0.01281 0.01228 0.01553 O3 4 0.423886 0.328966 0.564942 11.00000 0.03617 0.03900 = 0.04384 0.00620 -0.00130 -0.00528 O4 4 0.256063 0.153830 0.583906 11.00000 0.05700 0.05734 = 0.06997 0.01506 -0.00975 -0.02548 O5 4 0.627740 0.536998 0.631574 11.00000 0.03357 0.05130 = 0.03124 0.00063 -0.00339 -0.00228 O6 4 0.657437 0.556029 0.808138 11.00000 0.04428 0.09868 = 0.03479 -0.00594 -0.00119 -0.00450 N1 3 1.002125 0.399777 0.248736 11.00000 0.04394 0.05419 = 0.04983 0.00451 -0.00327 -0.00677 AFIX 137 H1A 2 0.985170 0.350680 0.307560 11.00000 -1.50000 H1B 2 1.108778 0.395244 0.230368 11.00000 -1.50000 H1C 2 0.939765 0.367873 0.195387 11.00000 -1.50000 AFIX 0 C4 1 0.956214 0.543413 0.270386 11.00000 0.05462 0.06403 = 0.10177 -0.00431 0.01576 0.00144 AFIX 23 H4A 2 0.838759 0.548259 0.287222 11.00000 -1.20000 H4B 2 1.017562 0.575232 0.332534 11.00000 -1.20000 AFIX 0 C5 1 0.990711 0.630518 0.180351 11.00000 0.10661 0.09051 = 0.19549 0.06702 -0.02983 -0.00822 AFIX 137 H5A 2 0.937793 0.595195 0.117180 11.00000 -1.50000 H5B 2 1.108517 0.634968 0.169020 11.00000 -1.50000 H5C 2 0.948789 0.719374 0.194918 11.00000 -1.50000 AFIX 0 HKLF 4 REM EtaKCrD_c6_f2_76_R10_RO_a.res in P2(1)/n REM R1 = 0.0630 for 1116 Fo > 4sig(Fo) and 0.0976 for all 1978 data REM 123 parameters refined using 12 restraints END WGHT 0.0828 0.4002 REM Highest difference peak 0.325, deepest hole -0.503, 1-sigma level 0.064 Q1 1 0.4972 0.4968 1.0668 11.00000 0.05 0.32 Q2 1 0.5144 0.5049 0.4283 11.00000 0.05 0.24 Q3 1 1.1000 0.2480 0.2789 11.00000 0.05 0.24 Q4 1 0.8780 0.2780 0.2627 11.00000 0.05 0.23 Q5 1 0.6130 0.5410 0.4434 11.00000 0.05 0.23 Q6 1 1.0938 0.2143 0.2360 11.00000 0.05 0.23 Q7 1 1.0968 0.7604 0.2783 11.00000 0.05 0.22 Q8 1 0.6144 0.4607 0.4412 11.00000 0.05 0.22 Q9 1 0.4675 0.5779 1.0653 11.00000 0.05 0.21 Q10 1 0.6157 0.4879 0.3980 11.00000 0.05 0.21 Q11 1 1.0381 0.3380 0.1998 11.00000 0.05 0.21 Q12 1 0.8904 0.7446 0.2367 11.00000 0.05 0.20 Q13 1 0.7048 0.6614 0.7752 11.00000 0.05 0.20 Q14 1 0.7525 0.3434 0.5830 11.00000 0.05 0.20 Q15 1 0.2867 0.2611 0.4629 11.00000 0.05 0.20 Q16 1 0.4163 0.5466 1.0413 11.00000 0.05 0.20 Q17 1 0.2173 0.0411 0.5746 11.00000 0.05 0.20 Q18 1 0.9642 0.6663 0.3189 11.00000 0.05 0.20 Q19 1 0.7664 0.6179 0.6743 11.00000 0.05 0.19 Q20 1 0.6019 0.5537 0.4761 11.00000 0.05 0.19 ; _shelx_res_checksum 29273 _shelx_hkl_file ; 0 0 3 -0.02 0.12 0 0 -3 0.18 0.43 0 0 4 7280.35 71.85 0 0 5 0.11 0.49 0 0 -5 -0.03 0.37 0 0 6 4.19 3.11 0 0 -6 7.63 2.69 0 0 -7 -0.04 0.90 0 0 7 0.61 1.45 0 0 8 196.08 16.48 0 0 9 -0.10 0.89 0 0 -9 0.10 0.39 0 0 -10 246.62 21.09 0 0 -11 0.06 12.34 0 0 -13 0.08 1.13 0 0 -14 553.02 39.19 0 0 -15 0.65 1.94 0 0 -16 552.55 41.54 0 0 -17 -0.85 2.70 0 0 -18 62.19 13.33 0 0 -19 68.29 18.25 0 0 -20 4.72 2.93 0 -1 -3 1008.96 26.92 0 -1 -4 56.11 7.51 0 -1 4 76.97 6.07 0 1 -4 72.87 6.11 0 1 -5 72.04 7.44 0 -1 -5 55.61 8.60 0 -1 -6 42.30 7.18 0 -1 6 37.24 5.47 0 1 -6 27.44 5.69 0 -1 -7 35.65 8.54 0 -1 7 41.38 7.34 0 1 -8 119.29 12.13 0 -1 -8 121.22 13.43 0 -1 -9 95.44 13.41 0 -1 9 110.41 11.84 0 1 -9 131.18 13.11 0 -1 10 40.25 8.22 0 1 -10 43.60 8.51 0 -1 -10 28.37 8.62 0 1 -11 398.68 27.60 0 -1 11 344.05 24.57 0 1 -12 -0.13 0.99 0 -1 -12 -1.47 3.05 0 1 -13 178.56 19.81 0 -1 -13 141.99 20.81 0 1 -14 0.98 2.71 0 -1 -14 1.68 1.95 0 1 -15 52.02 14.52 0 -1 -15 30.74 9.66 0 -1 -16 2.31 1.46 0 1 -16 31.64 13.20 0 -1 -17 46.60 12.39 0 1 -17 38.86 11.15 0 1 -18 0.71 2.27 0 -1 -18 2.88 3.25 0 1 -19 -0.11 2.04 0 1 -20 1.86 4.22 0 1 -21 -0.37 3.56 0 1 -22 -2.56 5.41 0 -2 4 3768.26 37.58 0 2 -5 754.16 19.76 0 2 -7 73.76 7.73 0 -2 7 52.34 6.67 0 2 -8 4278.54 66.44 0 -2 9 14.97 4.58 0 2 -9 9.75 3.25 0 -2 10 1504.96 43.47 0 2 -10 1421.50 44.55 0 2 -11 1.02 1.56 0 -2 11 0.47 1.12 0 2 -12 431.76 27.61 0 2 -13 1.82 2.54 0 2 -15 0.38 2.26 0 2 -16 353.84 28.74 0 2 -17 22.91 8.16 0 2 -18 81.09 14.50 0 2 -19 -1.58 3.29 0 2 -20 39.47 9.48 0 2 -21 -1.85 3.33 0 -3 5 15.06 2.68 0 -3 6 198.19 10.52 0 3 -8 195.78 12.80 0 3 -9 701.80 27.23 0 -3 9 753.12 26.60 0 3 -10 70.22 8.60 0 -3 10 72.24 9.00 0 -3 11 0.82 1.65 0 3 -11 0.13 0.79 0 3 -12 100.61 12.38 0 -3 12 82.88 11.35 0 3 -13 91.46 12.55 0 -3 13 89.24 11.42 0 3 -14 4.49 3.70 0 3 -15 5.44 3.80 0 3 -16 5.96 4.96 0 3 -17 0.38 1.74 0 3 -18 1.54 1.51 0 3 -19 -0.93 2.87 0 3 -20 1.95 2.88 0 3 -21 2.44 4.09 0 -4 7 31.18 4.33 0 4 -9 8.82 2.66 0 -4 9 1.81 1.88 0 -4 10 729.25 26.17 0 -4 11 71.36 9.02 0 4 -11 57.28 9.48 0 4 -12 116.05 12.29 0 -4 12 117.23 11.71 0 4 -13 119.41 13.16 0 -4 13 110.04 12.31 0 4 -14 286.71 21.58 0 4 -15 40.44 8.99 0 4 -16 111.19 14.21 0 4 -17 22.65 6.10 0 4 -18 105.78 14.70 0 4 -19 0.22 1.33 0 4 -20 20.88 6.47 0 -5 7 86.32 7.16 0 -5 8 98.10 8.15 0 -5 10 13.06 3.36 0 -5 11 3.48 1.40 0 5 -13 9.72 4.13 0 -5 13 1.01 2.34 0 5 -14 0.04 0.71 0 -5 14 0.17 0.92 0 5 -15 0.05 2.05 0 5 -16 0.40 1.34 0 5 -17 0.49 1.10 0 5 -18 3.06 3.06 0 5 -19 0.44 1.01 0 -6 7 38.74 5.20 0 -6 9 27.22 4.40 0 -6 10 1068.54 28.23 0 -6 11 63.50 8.12 0 -6 13 0.03 0.64 0 -7 8 85.37 7.67 0 -7 10 423.89 17.01 0 -7 11 49.73 5.65 0 -7 12 16.94 3.53 0 -7 13 5.99 2.95 0 -8 9 4.86 2.18 0 -8 10 202.94 12.07 0 -8 11 51.86 5.83 0 -8 12 265.30 12.95 0 -8 13 0.76 0.91 0 -9 10 -0.10 0.27 0 -9 11 10.41 3.19 0 -9 12 1.66 0.57 0 -10 11 0.62 0.46 0 -11 11 20.38 3.66 0 -11 12 0.02 0.46 0 -12 12 17.87 3.11 1 0 -20 0.14 3.39 1 0 -19 5.28 7.16 1 0 -18 1.21 3.74 1 0 -17 71.19 15.53 1 0 -16 0.83 1.94 -1 0 15 7.82 5.34 1 0 -15 4.54 11.66 1 0 -14 18.77 9.73 -1 0 14 -0.08 17.15 1 0 -13 75.04 16.85 -1 0 13 83.92 14.45 1 0 -12 -0.08 2.35 -1 0 12 0.14 0.68 -1 0 11 19.95 8.22 1 0 -11 28.62 8.01 1 0 -10 0.13 0.93 -1 0 10 0.18 0.72 1 0 -9 126.02 15.79 -1 0 9 138.67 15.42 1 0 -8 0.21 0.75 -1 0 8 -0.10 1.66 -1 0 7 13.56 4.67 1 0 -7 21.41 5.95 -1 0 6 0.04 0.87 1 0 -6 0.04 0.21 1 0 -5 7560.16 88.59 1 0 -4 -0.48 0.91 -1 0 4 -1.21 1.29 -1 0 3 7214.48 70.23 -1 0 2 -0.21 0.60 1 0 -2 0.07 0.40 1 0 -1 1760.32 26.97 -1 0 1 1737.07 27.47 -1 0 -11 402.88 28.25 -1 0 -12 -0.20 13.60 -1 0 -13 90.18 14.83 -1 0 -14 -0.63 1.53 -1 0 -15 36.64 10.21 -1 0 -16 -0.57 3.02 1 1 -21 -0.39 2.55 1 1 -20 7.97 5.99 1 -1 -19 -1.20 3.15 1 1 -19 1.18 1.91 1 -1 -18 148.18 25.17 1 1 -18 94.68 18.32 1 1 -17 3.13 2.93 1 -1 -17 2.52 9.88 1 1 -16 278.70 28.77 1 -1 -16 249.55 30.39 -1 -1 15 4.07 4.31 1 1 -15 15.24 5.75 1 -1 -15 2.27 3.87 -1 -1 14 843.27 44.74 1 1 -14 831.53 47.42 -1 -1 13 0.21 14.97 1 1 -13 0.62 1.45 -1 1 13 -0.60 2.83 1 -1 -13 1.96 3.81 1 -1 -12 164.11 22.16 -1 1 12 175.45 21.66 -1 -1 11 113.89 16.04 -1 1 11 128.18 18.42 1 -1 -11 140.27 19.01 1 1 -11 137.27 17.42 1 -1 -10 2108.30 68.90 -1 -1 10 2238.25 59.79 -1 1 9 -0.30 1.43 1 -1 -9 0.26 0.71 -1 -1 9 1.14 1.17 1 1 -9 1.37 1.64 -1 1 8 984.28 39.84 1 -1 -8 903.67 39.84 1 -1 -7 0.10 0.79 -1 1 7 0.15 0.37 -1 -1 7 0.04 0.83 1 1 -7 0.04 0.59 -1 -1 6 361.72 19.70 -1 1 6 346.08 21.40 1 1 -5 711.76 25.88 1 1 -4 1585.85 34.00 1 1 -3 956.30 24.48 -1 1 1 27.95 3.88 -1 1 -7 0.38 1.31 -1 1 -8 1501.62 40.75 -1 1 -9 0.37 0.86 -1 1 -11 71.68 10.62 -1 1 -13 0.39 2.22 -1 1 -14 402.48 29.40 -1 1 -15 0.08 1.04 -1 1 -17 0.18 0.49 -1 1 -18 102.68 17.86 -1 1 -19 30.60 16.71 -1 1 -20 23.30 12.32 1 2 -22 -2.62 4.18 1 2 -21 -0.23 1.62 1 2 -20 -1.86 4.53 1 2 -19 1.88 4.70 1 -2 -19 1.20 2.80 1 -2 -18 -0.14 1.73 1 2 -18 0.99 2.40 1 2 -17 47.00 11.50 1 -2 -17 50.31 13.88 -1 -2 16 6.08 4.70 1 2 -16 5.11 4.15 1 -2 -16 8.23 4.44 1 -2 -15 3.30 4.51 -1 -2 15 2.36 3.19 1 2 -15 1.33 2.62 1 2 -14 1.23 1.44 -1 -2 14 4.55 3.40 1 -2 -14 0.88 1.03 1 -2 -13 33.46 10.82 -1 -2 13 36.08 9.32 1 2 -13 54.13 10.63 -1 -2 12 0.18 0.32 1 -2 -12 -0.37 0.72 1 2 -12 0.52 1.72 -1 2 12 0.70 2.37 -1 -2 11 0.59 0.71 1 2 -11 0.94 1.82 1 -2 -11 1.19 1.03 -1 2 11 0.32 1.16 -1 -2 10 60.53 10.05 1 -2 -10 40.94 10.99 1 2 -10 66.22 10.47 -1 2 10 36.26 10.79 1 -2 -9 228.35 21.28 -1 2 9 248.78 22.26 -1 -2 9 181.99 16.55 -1 2 8 105.11 14.69 1 -2 -8 105.89 14.21 1 2 -8 90.85 10.71 -1 -2 8 78.85 10.67 1 -2 -7 596.01 32.05 -1 2 7 641.99 32.56 1 2 -6 914.46 29.58 1 -2 -6 911.77 37.89 -1 -2 5 1.19 1.10 1 2 -5 0.03 0.57 -1 2 5 0.26 0.74 1 -2 -5 0.62 1.21 -1 2 4 18.07 5.04 1 -2 -4 12.29 4.38 -1 -2 4 13.34 3.41 -1 2 3 1839.95 42.04 1 -2 -2 1308.15 32.65 -1 2 2 1260.54 31.53 -1 2 1 5793.72 60.84 -1 2 -5 372.52 11.57 -1 2 -6 32.59 4.86 -1 2 -7 13.90 3.29 -1 2 -8 9.54 3.39 -1 2 -9 108.18 10.57 -1 2 -10 196.04 15.11 -1 2 -11 66.13 9.82 -1 2 -12 71.90 11.38 -1 2 -13 95.14 13.88 -1 2 -14 0.69 0.97 -1 2 -15 15.02 5.95 -1 2 -16 24.33 9.91 -1 2 -17 0.46 1.90 -1 2 -18 0.77 2.98 -1 2 -19 1.18 1.21 -1 2 -20 0.88 3.07 -1 2 -21 2.04 1.11 1 3 -21 -2.68 4.66 1 3 -20 47.69 11.55 1 3 -19 4.65 4.47 1 3 -18 107.31 17.32 -1 -3 17 0.24 1.20 1 3 -17 1.66 1.85 -1 -3 16 130.46 19.42 1 3 -16 182.21 20.63 -1 -3 15 0.21 1.53 1 -3 -15 1.80 2.09 1 3 -15 0.22 1.24 1 -3 -14 216.39 27.53 -1 -3 14 172.08 19.58 1 -3 -13 198.06 25.15 1 3 -13 222.24 19.62 1 -3 -12 217.58 25.23 -1 -3 12 203.97 18.76 1 3 -12 234.52 20.36 1 3 -11 11.85 4.43 -1 -3 11 10.59 4.08 1 -3 -11 6.13 5.58 1 -3 -10 1972.07 70.97 1 3 -10 2140.32 54.27 1 3 -9 289.69 19.32 -1 -3 9 305.68 19.62 1 3 -8 4214.36 70.25 -1 3 8 4444.31 97.82 1 3 -7 6.12 2.80 -1 3 7 6.08 3.25 -1 -3 7 11.53 3.35 1 -3 -7 6.79 4.08 1 -3 -4 4846.02 80.32 -1 3 4 4702.77 79.96 -1 3 -8 1586.46 32.10 -1 3 -9 23.96 4.19 -1 3 -10 397.94 20.56 -1 3 -11 -0.34 1.02 -1 3 -12 686.38 31.25 -1 3 -13 1.71 1.24 -1 3 -14 270.88 21.19 -1 3 -15 0.36 0.33 -1 3 -16 159.24 18.08 -1 3 -17 1.97 3.12 -1 3 -18 32.78 8.34 -1 3 -19 -0.89 1.95 -1 3 -20 24.80 6.20 1 4 -20 1.91 3.61 1 4 -19 3.39 4.92 1 4 -18 49.96 10.74 -1 -4 17 17.26 6.70 1 4 -17 8.41 4.53 -1 -4 16 -0.81 1.46 1 4 -16 1.04 2.36 1 4 -15 0.90 1.67 -1 -4 15 1.36 1.64 1 4 -14 0.78 1.46 -1 -4 14 2.98 3.07 -1 -4 13 1.17 1.80 1 4 -13 -0.56 0.74 -1 -4 12 79.21 11.05 1 4 -12 79.21 10.90 1 4 -11 10.70 3.51 -1 -4 11 8.24 3.91 1 4 -10 26.37 6.70 -1 -4 10 33.72 6.48 -1 -4 6 4.48 2.06 1 -4 -5 51.99 10.84 1 -4 -1 1.46 1.38 1 -4 2 66.12 6.06 -1 4 -10 260.76 13.57 -1 4 -11 3.51 1.87 -1 4 -12 150.40 12.97 -1 4 -13 15.21 4.93 -1 4 -14 4.31 2.29 -1 4 -15 1.79 1.71 -1 4 -16 1.27 2.10 -1 4 -17 -0.11 0.69 -1 4 -18 -0.12 1.61 -1 4 -19 3.05 2.38 1 5 -19 2.04 2.58 1 5 -18 81.45 13.96 1 5 -17 2.07 3.06 -1 -5 17 0.58 1.39 -1 -5 16 118.10 16.87 1 5 -16 164.43 17.95 -1 -5 15 9.34 3.76 1 5 -15 14.03 4.99 -1 -5 14 150.08 15.94 -1 -5 13 0.60 1.24 -1 -5 12 314.71 21.12 -1 -5 11 156.50 14.78 -1 -5 10 264.22 18.33 -1 -5 9 34.87 6.89 -1 -5 8 1080.81 33.73 -1 5 -13 26.25 5.24 -1 5 -14 332.13 18.64 -1 5 -15 1.14 1.76 -1 5 -16 175.82 15.55 -1 5 -17 2.92 2.47 -1 5 -18 62.86 9.90 -1 5 -19 0.05 0.59 -1 -6 17 0.06 1.04 -1 -6 16 1.24 0.58 -1 -6 15 1.01 13.97 -1 -6 14 0.24 0.26 -1 -6 13 0.45 0.60 -1 -6 12 0.61 0.33 -1 -6 11 0.58 1.12 -1 -6 10 87.03 10.04 -1 -6 9 31.23 6.13 -1 -6 8 0.28 1.21 -1 -7 17 -1.90 1.69 -1 -7 16 62.04 9.98 -1 -7 15 18.85 5.30 -1 -7 13 20.88 5.34 -1 -7 12 251.84 19.06 -1 -7 11 29.21 6.63 -1 -7 9 74.91 9.28 -1 -8 16 7.87 3.61 -1 -8 15 -0.16 0.66 -1 -8 14 0.04 0.38 -1 -8 13 5.77 2.07 -1 -8 12 1.33 2.42 -1 -8 11 29.55 6.32 -1 -8 10 168.33 13.68 -1 -9 15 0.04 0.70 -1 -9 14 103.81 10.93 -1 -9 13 0.69 1.31 -1 -9 12 135.93 12.92 -1 -9 11 24.98 5.53 -1 -10 15 1.86 0.25 -1 -10 14 -0.14 0.81 -1 -10 13 17.47 4.70 -1 -10 12 0.75 1.41 -1 -11 14 53.40 7.78 -1 -11 13 1.86 2.93 2 0 -20 36.43 12.36 2 0 -19 2.91 3.26 -2 0 18 173.55 25.25 2 0 -18 174.38 26.50 -2 0 17 1.35 3.95 2 0 -17 0.74 2.66 -2 0 16 170.59 25.32 2 0 -16 229.92 28.43 2 0 -15 1.19 2.61 -2 0 15 0.30 1.19 2 0 -14 734.55 48.74 2 0 -13 0.84 2.95 -2 0 13 -0.85 2.47 2 0 -12 541.84 38.46 -2 0 12 516.87 35.30 -2 0 11 -1.12 0.81 2 0 -11 -0.16 1.61 2 0 -10 2272.24 71.51 2 0 -9 -0.13 0.81 -2 0 9 0.44 1.44 2 0 -8 3483.87 80.81 2 0 -7 -0.16 1.35 -2 0 7 1.45 2.14 2 0 -6 54.42 9.18 -2 0 6 50.56 9.20 -2 0 5 15.61 6.25 2 0 -5 0.56 1.53 -2 0 4 5876.01 82.86 2 0 -4 6210.67 82.74 -2 0 3 -0.13 0.48 2 0 -3 0.29 0.74 2 0 -2 807.57 26.14 -2 0 1 0.05 0.26 2 1 -20 13.90 9.62 2 1 -19 0.12 1.34 -2 -1 19 1.51 2.88 2 -1 -19 0.60 2.82 2 1 -18 0.95 2.93 2 -1 -18 1.83 3.74 -2 -1 18 2.87 3.73 2 -1 -17 11.60 6.65 -2 1 17 8.63 5.46 -2 -1 17 19.71 8.58 2 1 -17 24.96 9.56 2 1 -16 14.99 7.02 2 -1 -16 -1.72 20.12 -2 1 16 4.24 3.66 -2 -1 16 13.70 8.17 2 -1 -15 -2.03 4.96 2 1 -15 0.80 2.02 -2 1 15 -1.51 23.35 -2 -1 15 -1.18 1.55 -2 -1 14 0.51 2.19 2 1 -14 3.73 4.00 -2 1 14 8.76 6.21 2 -1 -14 0.74 2.05 -2 -1 13 7.51 4.56 -2 1 13 25.61 8.76 2 -1 -13 21.21 7.38 2 1 -13 7.96 4.82 -2 1 12 4.53 3.67 -2 -1 12 18.03 5.83 2 1 -12 13.22 5.58 2 -1 -12 22.67 15.32 -2 -1 11 328.65 25.89 -2 1 11 341.43 28.59 2 -1 -11 356.04 31.16 2 1 -11 312.52 27.56 2 1 -10 0.13 0.89 -2 -1 10 0.82 2.53 -2 1 10 -0.15 1.19 2 1 -9 455.43 30.23 -2 -1 9 504.93 29.31 2 -1 -8 110.76 15.68 2 1 -8 120.97 13.54 -2 1 8 102.50 13.98 -2 -1 8 109.06 13.38 2 1 -7 112.13 12.44 -2 -1 7 100.42 12.27 -2 1 7 70.79 12.09 2 -1 -7 100.09 13.93 2 -1 -6 63.46 10.23 2 1 -6 55.89 8.55 -2 -1 6 56.99 8.58 -2 1 6 40.63 8.77 2 1 -5 158.28 13.84 -2 -1 4 0.60 0.90 -2 1 4 0.17 1.23 2 1 -4 0.32 0.78 2 -1 -4 0.17 0.90 -2 1 3 1619.42 40.84 -2 1 2 194.17 13.34 2 -1 -1 4309.38 57.20 -2 1 1 4408.85 58.76 2 -1 0 4472.82 53.02 2 2 -21 8.19 7.25 2 2 -20 33.37 11.57 -2 -2 19 0.21 3.89 2 2 -19 -3.38 3.85 -2 -2 18 111.03 19.53 2 2 -18 135.53 20.68 2 -2 -18 109.40 23.18 -2 -2 17 0.10 0.52 2 -2 -17 5.60 13.96 2 2 -17 -1.21 3.48 -2 2 16 42.89 14.41 -2 -2 16 35.69 11.45 2 2 -16 41.02 11.23 -2 -2 15 5.02 4.00 2 -2 -15 3.28 8.28 2 2 -15 2.04 1.51 -2 2 15 0.81 2.59 -2 2 14 247.03 29.08 2 -2 -14 219.86 28.75 2 2 -14 282.51 25.49 -2 2 13 -2.42 3.93 2 -2 -13 1.19 2.75 -2 -2 13 0.68 1.79 2 2 -13 0.08 15.33 2 -2 -12 196.85 24.58 -2 2 12 186.86 23.28 2 2 -12 181.87 20.87 -2 -2 11 50.60 10.01 -2 2 11 40.98 10.93 2 2 -11 53.64 9.71 2 -2 -11 35.31 11.51 -2 -2 10 1975.35 61.03 2 -2 -10 2113.81 73.48 -2 -2 9 170.99 17.54 2 -2 -9 133.01 18.80 2 2 -9 167.86 16.70 2 2 -8 3536.82 72.92 2 -2 -8 3340.81 86.18 2 -2 -7 689.60 36.53 -2 -2 7 651.28 30.75 2 -2 -6 815.63 37.95 2 2 -6 792.13 31.82 -2 -2 5 0.04 0.21 2 -2 -5 0.98 2.13 -2 2 5 0.05 0.66 2 2 -5 0.64 1.02 2 -2 -4 5780.18 89.16 -2 2 4 6075.57 89.00 -2 -2 4 5933.75 79.71 -2 2 -1 348.31 14.50 -2 2 -9 258.03 16.68 -2 2 -11 27.58 6.57 -2 2 -13 47.30 9.05 -2 2 -14 168.61 17.26 -2 2 -15 4.38 3.82 -2 2 -16 81.13 14.08 -2 2 -17 0.61 1.84 -2 2 -18 59.25 12.91 -2 2 -19 4.93 13.92 2 3 -21 2.25 3.21 -2 -3 20 1.97 2.91 2 3 -20 -0.54 0.58 -2 -3 19 0.10 1.93 2 3 -19 1.94 1.99 2 3 -18 3.01 3.89 -2 -3 18 8.05 5.28 -2 -3 17 8.54 5.45 2 -3 -17 4.85 4.02 2 3 -16 -0.09 1.14 -2 -3 16 0.17 1.41 2 -3 -16 0.87 1.11 2 3 -15 -0.08 0.88 -2 -3 15 0.70 1.26 -2 3 15 0.38 3.84 2 -3 -15 1.90 2.84 2 -3 -14 13.68 7.81 2 3 -14 10.92 5.55 -2 -3 14 14.43 6.77 -2 3 14 18.42 7.64 -2 3 13 27.68 10.63 2 -3 -13 38.33 11.83 2 3 -13 28.39 8.64 -2 -3 13 28.84 8.68 2 -3 -12 97.59 17.98 -2 -3 12 76.62 13.06 -2 3 12 96.52 18.24 2 3 -12 86.70 14.17 -2 -3 11 5.77 3.42 -2 3 11 3.59 4.48 2 3 -11 4.73 4.20 2 -3 -11 16.24 6.99 2 3 -10 58.98 11.53 2 -3 -10 63.08 14.13 -2 3 10 47.38 13.79 -2 -3 10 72.66 12.09 2 -3 -9 173.22 21.27 2 3 -9 180.09 16.29 -2 3 9 166.29 20.15 -2 -3 9 159.72 17.26 2 -3 -8 269.89 26.06 2 3 -8 302.76 20.24 -2 -3 8 272.64 20.19 2 -3 -7 156.36 18.12 -2 3 7 119.08 16.29 2 -3 -6 1173.45 47.62 -2 3 5 2568.60 65.34 2 -3 -5 2502.24 66.81 -2 3 4 143.85 14.90 -2 3 3 173.63 15.14 2 -3 -3 191.59 16.06 2 -3 -2 1208.51 37.57 2 -3 -1 2167.10 46.53 -2 3 -7 397.25 12.63 -2 3 -8 130.89 8.53 -2 3 -11 10.82 2.96 -2 3 -12 9.38 4.08 -2 3 -13 66.93 10.37 -2 3 -14 8.68 3.59 -2 3 -15 0.11 1.85 -2 3 -16 31.40 8.83 -2 3 -17 -0.51 2.49 -2 3 -18 0.35 0.53 -2 3 -19 0.67 2.45 -2 3 -20 0.32 1.60 2 4 -21 -0.50 2.38 -2 -4 20 20.52 7.67 2 4 -20 16.45 7.64 -2 -4 19 0.55 0.99 2 4 -19 5.51 5.05 2 4 -18 214.78 24.28 -2 -4 18 155.43 21.58 -2 -4 17 0.57 2.48 2 4 -17 6.91 3.50 2 4 -16 153.76 20.33 -2 -4 16 127.69 19.16 2 -4 -16 169.91 26.78 2 4 -15 31.04 8.69 -2 -4 15 30.84 9.34 2 -4 -15 34.75 11.65 2 -4 -14 419.80 40.63 -2 -4 13 18.67 5.87 2 -4 -13 10.86 5.94 -2 4 13 16.75 7.07 2 4 -13 20.93 5.70 -2 -4 12 162.62 17.01 2 -4 -12 144.12 22.89 2 4 -12 121.00 16.72 -2 4 12 145.29 23.48 -2 4 11 35.09 9.90 -2 -4 11 24.96 7.29 2 4 -11 34.55 8.69 2 -4 -11 32.05 10.28 -2 -4 10 777.90 37.14 -2 -4 9 70.34 10.72 -2 4 9 75.41 14.73 2 -4 -9 78.08 14.40 -2 -4 8 461.71 26.75 -2 4 7 974.46 46.04 2 -4 -7 955.09 46.46 -2 -4 7 905.89 36.39 -2 4 5 429.07 29.41 2 -4 -2 9999.00 113.58 -2 4 1 759.97 28.88 2 -4 -1 769.50 29.24 2 -4 1 422.16 18.26 -2 4 -1 409.64 17.65 2 -4 2 1385.35 28.89 -2 4 -2 1392.41 28.83 -2 4 -3 44.96 4.46 2 -4 3 44.92 4.29 -2 4 -9 337.06 11.60 -2 4 -10 1172.80 25.85 -2 4 -11 38.99 5.31 -2 4 -12 1124.89 32.37 -2 4 -13 82.71 9.26 -2 4 -14 458.93 25.28 -2 4 -15 -0.49 1.18 -2 4 -16 76.65 11.53 -2 4 -17 1.18 2.10 -2 4 -18 56.51 10.15 -2 4 -19 1.46 2.40 -2 -5 20 -2.86 2.70 -2 -5 19 3.87 4.29 -2 -5 18 9.70 6.03 -2 -5 17 18.00 6.70 -2 -5 16 1.22 2.32 -2 -5 15 18.86 6.45 -2 -5 14 0.78 1.53 -2 -5 13 22.53 7.36 2 -5 -13 33.79 12.21 2 -5 -12 10.18 6.27 -2 -5 12 33.15 7.85 2 -5 -11 -0.80 2.98 -2 -5 11 11.82 6.44 -2 5 11 9.74 6.96 -2 -5 10 6.77 3.52 -2 5 10 8.32 6.03 2 -5 -10 6.83 4.82 2 -5 -9 30.71 11.12 -2 -5 9 41.72 8.16 -2 5 9 30.51 9.50 -2 -5 8 18.58 6.67 -2 5 8 27.37 7.96 2 -5 -8 34.24 9.78 2 -5 -7 82.34 15.46 -2 5 7 92.44 15.32 -2 5 6 13.93 5.73 2 -5 -6 9.88 5.13 -2 5 5 -0.21 1.78 2 -5 -5 2.99 4.20 -2 5 4 127.58 16.52 2 -5 -4 110.82 15.90 -2 5 3 0.28 0.68 2 -5 -3 0.05 0.98 -2 5 2 2.78 2.21 2 -5 -2 1.17 2.61 -2 5 1 786.00 31.87 2 -5 -1 806.37 32.07 -2 5 0 828.00 30.37 -2 5 -1 73.23 8.15 2 -5 1 42.62 7.53 2 -5 2 110.69 9.43 2 -5 3 -0.14 0.55 2 -5 4 28.70 3.34 -2 5 -12 33.04 4.11 -2 5 -13 85.64 7.16 -2 5 -14 1.95 1.17 -2 5 -15 16.49 3.73 -2 5 -16 2.52 1.93 -2 5 -17 14.01 4.89 -2 5 -18 -0.04 1.62 -2 -6 19 2.20 2.32 -2 -6 18 75.89 14.41 -2 -6 17 0.14 3.06 -2 -6 16 95.15 15.60 -2 -6 15 0.58 1.55 -2 -6 13 17.17 6.14 -2 -6 12 220.64 20.25 -2 -6 11 26.28 7.14 -2 -6 9 21.54 6.15 2 -6 -7 -0.27 18.38 -2 6 6 1269.68 56.70 2 -6 -6 1222.38 55.00 -2 6 5 50.49 12.58 2 -6 -5 52.25 12.74 2 -6 -4 713.08 39.55 2 -6 -3 160.12 16.90 2 -6 1 145.05 12.58 2 -6 3 206.32 12.38 2 -6 4 2559.93 39.01 -2 -7 18 -2.37 1.47 -2 -7 17 0.70 2.07 -2 -7 16 10.61 4.06 -2 -7 15 1.26 1.80 -2 -7 14 2.17 2.90 -2 -7 13 6.06 4.07 -2 -7 12 0.17 1.01 -2 -7 11 -0.72 1.08 -2 -7 10 0.05 1.02 2 -7 -2 -1.42 2.66 2 -7 -1 304.70 24.28 2 -7 2 11.06 4.23 2 -7 5 10.33 2.94 -2 -8 17 -0.06 1.02 -2 -8 16 67.05 11.39 -2 -8 15 2.31 1.97 -2 -8 14 49.78 10.21 -2 -8 13 26.04 8.15 -2 -8 12 162.72 16.84 -2 -8 11 26.53 6.66 2 -8 1 -0.34 1.00 2 -8 3 5.38 3.47 -2 -9 16 -0.16 0.96 -2 -9 15 0.89 2.33 -2 -9 14 3.44 2.68 -2 -9 13 0.06 0.30 2 -9 4 17.04 6.20 2 -9 5 3.54 2.54 2 -9 6 12.88 4.29 -2 -10 15 0.48 1.94 -2 -10 14 62.90 10.60 2 -10 5 73.72 9.34 2 -10 6 49.45 9.14 2 -10 7 5.14 1.93 2 -11 6 0.18 1.18 2 -11 7 7.97 2.90 2 -11 8 9.78 3.64 2 -12 7 3.79 2.34 2 -12 8 14.93 3.68 2 -13 8 0.06 0.47 2 -13 9 1.82 1.65 -3 0 19 -1.38 1.98 3 0 -19 -3.36 3.79 -3 0 18 3.50 4.21 3 0 -18 2.22 4.51 -3 0 17 0.12 3.67 3 0 -17 0.66 1.42 3 0 -16 0.50 3.30 -3 0 16 -1.26 3.03 -3 0 15 2.26 3.19 3 0 -15 5.61 4.09 3 0 -14 -3.61 5.58 -3 0 14 0.71 2.80 3 0 -13 0.61 1.10 -3 0 13 11.38 5.09 3 0 -12 0.57 1.03 -3 0 12 1.44 2.47 -3 0 11 947.78 48.36 3 0 -11 795.75 48.01 -3 0 10 0.47 1.69 3 0 -10 -0.08 0.98 3 0 -8 -0.68 1.16 -3 0 8 0.21 1.41 3 0 -7 0.37 0.47 -3 0 7 0.12 1.43 3 0 -6 -0.17 0.31 -3 0 6 -0.94 1.67 3 0 -5 906.13 37.52 -3 0 5 944.18 38.98 -3 0 4 1.18 1.78 3 0 -4 0.05 0.91 -3 0 3 4.68 1.91 3 0 -3 2.68 2.55 -3 0 2 -0.76 2.09 3 0 -2 0.55 1.08 3 1 -19 -0.13 2.50 -3 -1 19 1.66 5.47 3 -1 -18 180.17 29.03 3 1 -18 209.71 28.52 -3 1 18 178.75 27.94 -3 -1 18 165.96 25.63 3 -1 -17 3.72 3.00 3 1 -17 4.66 6.06 -3 1 17 2.63 2.85 -3 -1 17 0.23 2.29 -3 1 16 26.12 10.45 3 -1 -16 29.88 11.01 -3 -1 16 20.20 9.44 3 1 -16 23.76 9.25 3 -1 -15 3.41 4.47 -3 1 15 2.31 3.47 3 1 -15 2.00 4.73 -3 -1 15 -1.93 3.06 -3 1 14 289.25 30.69 -3 -1 14 291.92 29.40 3 -1 -14 298.21 33.57 3 1 -14 324.30 31.38 3 -1 -13 0.99 1.98 -3 1 13 1.12 2.90 3 1 -13 -1.02 2.29 -3 -1 13 -1.44 3.97 -3 -1 12 501.10 35.49 3 -1 -12 474.95 39.03 3 1 -12 503.00 36.36 3 -1 -11 68.75 15.38 -3 -1 11 65.46 12.58 3 1 -11 61.36 13.21 -3 1 11 61.63 13.21 3 1 -10 2041.59 68.34 3 -1 -10 2116.72 75.51 -3 -1 10 2184.53 72.63 -3 1 9 0.23 0.82 3 -1 -9 0.89 2.32 3 1 -9 -0.07 1.49 -3 -1 9 1.36 1.89 -3 1 8 2277.65 71.61 3 1 -8 2431.38 68.43 -3 -1 7 0.06 0.33 3 1 -7 -0.06 0.32 -3 1 7 2.24 2.91 3 -1 -7 0.21 1.89 3 1 -6 1997.75 58.04 3 1 -5 65.69 10.41 -3 1 5 98.84 13.62 -3 -1 5 74.09 10.48 3 -1 -5 79.87 11.35 3 1 -4 2499.41 56.78 3 -1 -4 2635.46 62.35 -3 1 4 2517.36 62.37 -3 -1 4 2415.88 58.19 3 -1 -3 69.26 10.05 -3 1 3 71.03 10.29 -3 1 2 9790.71 111.84 -3 1 1 7.21 2.72 3 -1 -1 8.59 2.66 -3 -2 20 1.26 2.72 3 2 -20 0.13 1.57 -3 -2 19 13.57 7.76 3 2 -19 2.23 3.42 -3 -2 18 0.45 0.85 3 2 -18 1.41 4.80 3 -2 -17 8.49 5.78 -3 -2 17 5.29 4.68 -3 2 17 5.13 6.07 3 2 -17 11.49 5.59 -3 2 16 -1.33 4.07 3 2 -16 -0.32 3.32 -3 -2 16 0.30 1.63 3 -2 -16 4.18 5.23 3 2 -15 -0.20 1.61 -3 -2 15 -0.20 1.30 -3 2 15 -0.12 1.16 3 -2 -15 1.21 4.11 -3 2 14 2.55 3.65 3 -2 -14 1.88 3.96 -3 -2 14 1.18 3.39 3 2 -14 0.75 3.87 -3 -2 13 106.90 16.19 -3 2 13 96.38 18.89 3 2 -13 117.20 18.23 3 -2 -13 105.33 19.49 -3 -2 12 45.96 10.26 -3 2 12 39.56 12.31 3 2 -12 39.70 10.66 3 -2 -12 36.99 12.24 -3 2 11 1.71 3.28 -3 -2 11 3.37 3.39 3 2 -11 4.07 2.41 3 -2 -11 0.60 1.88 -3 -2 10 56.12 11.73 3 2 -10 56.00 11.13 3 -2 -10 49.59 12.94 -3 2 10 32.29 12.01 -3 -2 9 -0.87 2.50 3 2 -9 -0.33 1.66 3 -2 -9 -0.17 1.60 -3 2 9 0.57 2.38 -3 -2 8 57.68 10.16 3 2 -8 46.27 9.55 3 -2 -8 30.15 9.52 -3 2 8 35.37 10.66 -3 2 7 -0.55 1.90 3 2 -7 0.33 0.97 -3 -2 7 0.42 1.29 3 -2 -7 0.65 1.47 3 -2 -5 1223.80 46.80 -3 2 5 1173.03 46.69 3 -2 -3 734.01 32.32 -3 2 3 677.12 31.40 3 -2 -1 279.17 17.50 -3 2 -2 12.86 3.32 3 3 -21 1.14 3.34 -3 -3 21 0.24 2.55 3 3 -20 47.57 12.65 -3 -3 20 27.54 12.10 3 3 -19 3.78 4.99 -3 -3 19 0.88 2.72 3 3 -18 197.46 25.05 -3 -3 18 128.70 22.18 -3 -3 17 26.88 9.68 3 3 -17 56.46 13.28 -3 3 16 96.42 20.85 3 -3 -16 102.06 21.73 -3 -3 16 104.27 18.31 3 3 -16 146.42 19.24 3 3 -15 6.94 5.39 -3 3 15 10.73 7.43 3 -3 -15 5.94 5.17 -3 -3 15 12.14 5.14 3 3 -14 209.39 23.71 -3 -3 14 160.33 21.85 3 -3 -14 209.00 32.76 -3 3 14 201.12 27.63 3 3 -13 -2.40 2.97 -3 3 13 0.12 1.09 -3 3 12 216.95 26.36 3 -3 -12 292.52 32.57 3 3 -12 207.28 22.67 -3 -3 12 250.94 24.15 3 3 -11 159.76 19.01 -3 -3 11 155.06 18.89 3 -3 -11 186.21 27.44 -3 3 11 190.88 23.05 3 -3 -10 354.30 33.72 -3 -3 10 366.04 28.01 -3 3 10 350.26 33.89 3 -3 -9 2.52 1.82 -3 -3 9 7.78 4.26 3 3 -9 3.87 2.54 -3 3 9 8.23 4.78 -3 -3 8 400.51 27.35 3 -3 -7 32.01 12.09 -3 3 7 16.20 6.24 -3 -3 7 18.03 5.80 -3 3 6 1107.36 48.08 3 -3 -6 1219.09 50.25 -3 3 5 165.05 17.95 3 -3 -5 148.47 16.64 -3 3 4 6218.53 103.80 -3 3 1 3721.72 67.43 3 -3 -1 3585.28 67.66 -3 3 -1 35.30 6.12 3 -3 1 34.59 5.57 3 -3 2 236.92 13.07 -3 3 -4 1415.78 28.93 -3 3 -12 975.43 35.05 -3 3 -13 29.98 6.20 -3 3 -14 217.17 17.96 -3 3 -15 40.14 9.02 -3 3 -16 107.17 13.55 -3 3 -17 0.06 1.53 -3 3 -18 45.61 10.05 3 4 -21 -4.04 3.54 -3 -4 21 1.13 4.06 3 4 -20 -0.32 1.40 -3 -4 20 1.50 1.00 -3 -4 19 -0.71 1.83 3 4 -19 0.51 4.03 3 4 -18 2.33 4.39 -3 -4 18 2.05 2.84 3 4 -17 3.88 3.87 -3 -4 17 0.10 1.36 -3 -4 16 1.98 4.07 3 4 -16 0.87 2.62 3 -4 -15 8.57 6.46 -3 4 15 4.35 5.32 -3 -4 15 5.31 3.47 3 4 -15 6.85 3.09 -3 -4 14 -1.66 1.91 3 4 -14 -0.23 1.12 3 -4 -14 -0.28 2.31 -3 4 14 -0.14 1.28 -3 -4 13 28.32 8.37 3 -4 -13 6.07 2.06 -3 4 13 9.23 6.27 3 4 -13 24.13 7.68 -3 -4 12 99.85 15.65 3 -4 -12 114.78 21.34 -3 4 12 108.87 18.94 3 -4 -11 188.11 24.63 -3 4 11 192.15 25.24 -3 -4 11 130.12 18.32 -3 -4 10 0.07 0.84 -3 4 10 0.51 3.58 3 -4 -10 0.86 2.80 -3 -4 9 96.13 13.70 3 -4 -9 70.12 16.61 -3 4 9 45.36 15.31 -3 4 8 241.92 24.99 3 -4 -8 239.64 26.54 -3 -4 8 237.69 21.35 3 -4 -7 15.11 7.17 -3 4 7 17.26 6.00 -3 4 6 31.61 7.94 3 -4 -6 31.10 8.18 3 -4 -5 97.23 14.41 -3 4 5 88.37 13.71 -3 4 4 602.03 33.33 3 -4 -4 555.63 33.18 3 -4 -3 0.83 1.44 -3 4 3 -0.39 1.34 -3 4 2 326.82 22.81 3 -4 -2 415.67 24.85 -3 4 1 63.55 11.52 3 -4 -1 124.39 12.78 3 -4 0 1.07 1.49 -3 4 0 0.44 1.44 3 -4 1 153.76 12.72 -3 4 -1 142.97 12.65 -3 4 -2 1074.47 30.38 -3 4 -3 1025.40 26.60 -3 4 -5 170.87 8.56 -3 4 -9 44.77 4.58 -3 4 -10 82.29 6.41 -3 4 -11 18.93 3.82 -3 4 -12 0.19 0.60 -3 4 -13 59.37 8.08 -3 4 -14 1.13 1.74 -3 4 -15 26.43 7.59 -3 4 -16 1.71 3.86 -3 4 -17 19.91 6.02 -3 4 -18 0.16 1.66 -3 -5 20 20.32 9.35 -3 -5 19 3.32 3.37 -3 -5 18 48.92 14.18 -3 -5 17 4.67 3.70 -3 -5 16 136.77 20.11 -3 -5 15 6.64 3.76 3 -5 -14 311.28 37.99 -3 -5 14 281.89 26.46 -3 5 14 281.44 35.72 -3 5 13 0.14 1.81 -3 -5 13 1.40 3.00 3 -5 -13 1.02 2.73 -3 -5 12 603.43 36.18 -3 5 12 668.56 50.27 -3 -5 11 1.08 2.90 3 -5 -11 0.38 1.36 -3 5 11 -0.47 2.31 3 -5 -10 823.66 53.95 3 -5 -9 53.98 17.18 -3 5 9 67.83 17.12 -3 -5 9 98.22 13.36 3 -5 -8 815.20 51.11 -3 5 8 842.25 49.15 3 -5 -7 58.22 12.90 -3 5 7 56.05 12.09 3 -5 -6 679.30 41.48 -3 5 6 669.80 40.00 3 -5 -5 299.97 26.24 -3 5 5 284.51 25.02 -3 5 4 1708.36 58.58 3 -5 -4 1703.62 59.82 -3 5 2 1351.98 47.25 3 -5 -2 1340.85 47.70 3 -5 -1 2.83 2.37 -3 5 1 7.47 3.52 -3 5 0 4457.39 81.38 3 -5 0 4814.83 77.18 3 -5 1 406.23 21.12 -3 5 -3 302.04 15.16 3 -5 3 288.48 14.78 3 -5 4 4537.62 49.76 -3 5 -4 4468.63 51.45 -3 5 -13 7.18 2.06 -3 5 -14 97.49 7.78 -3 5 -15 0.34 0.50 -3 5 -16 152.10 11.83 -3 5 -17 18.00 4.15 -3 5 -18 44.28 7.05 -3 -6 20 1.28 2.16 -3 -6 19 0.53 2.14 -3 -6 18 0.53 1.64 -3 -6 17 3.93 4.15 -3 -6 16 1.61 2.04 -3 -6 15 15.75 6.38 -3 -6 14 -1.57 3.57 3 -6 -13 56.96 15.92 -3 6 13 58.88 15.47 -3 -6 13 61.84 12.38 3 -6 -12 35.99 12.36 -3 -6 12 30.26 8.32 -3 6 12 37.65 14.10 -3 -6 11 7.16 4.27 3 -6 -11 10.05 6.97 -3 6 11 5.79 6.71 -3 6 10 1.08 2.52 3 -6 -10 5.79 5.23 -3 -6 10 10.88 5.39 3 -6 -9 1.28 3.62 -3 6 9 -0.78 2.64 -3 6 8 93.47 16.06 3 -6 -8 81.27 15.79 3 -6 -7 23.85 9.20 -3 6 7 29.32 9.40 3 -6 -6 155.04 20.17 -3 6 6 142.80 18.79 3 -6 -5 11.84 5.65 -3 6 5 5.58 4.05 3 -6 -4 15.01 6.05 -3 6 4 19.97 6.38 -3 6 3 301.56 24.66 3 -6 -3 308.40 25.05 3 -6 -2 199.73 20.05 -3 6 2 240.01 20.68 -3 6 1 423.68 25.71 3 -6 -1 441.87 26.60 -3 6 0 136.92 15.47 3 -6 1 192.80 15.73 3 -6 2 19.08 4.87 -3 6 -2 29.98 5.49 -3 6 -3 397.36 19.06 3 -6 3 466.55 20.24 3 -6 4 0.29 0.62 -3 -7 19 3.47 2.09 -3 -7 18 37.47 10.36 -3 -7 17 -0.40 0.43 -3 -7 16 90.42 15.17 -3 -7 15 -1.56 2.34 -3 -7 14 164.83 18.53 -3 -7 13 -1.10 1.63 -3 -7 12 229.58 22.62 3 -7 -11 26.88 10.92 -3 7 10 450.99 40.04 3 -7 -10 393.95 39.57 3 -7 -9 7.64 4.76 -3 7 9 17.65 7.54 3 -7 -8 334.14 34.03 -3 7 8 355.74 34.41 3 -7 -7 -0.10 2.75 -3 7 7 0.21 0.56 3 -7 -5 94.08 15.80 -3 7 5 134.82 17.51 3 -7 -4 354.12 29.11 3 -7 -3 167.06 19.31 -3 7 3 167.00 19.47 -3 7 2 601.22 36.01 -3 7 1 366.52 25.61 3 -7 -1 374.09 26.58 -3 7 -1 233.90 19.59 3 -7 2 1826.25 48.79 3 -7 3 55.61 8.28 -3 -8 18 0.30 0.41 -3 -8 17 0.07 0.90 -3 -8 16 0.38 2.41 -3 -8 15 0.08 0.70 -3 -8 14 1.48 6.25 -3 -8 13 1.10 0.56 3 -8 -7 3.55 4.65 3 -8 -6 187.89 22.85 3 -8 -5 3.98 4.52 3 -8 -4 14.68 5.71 3 -8 -3 -0.63 3.09 3 -8 -2 0.57 2.12 3 -8 -1 0.39 1.87 3 -8 1 6.16 3.17 3 -8 2 -0.05 0.72 3 -8 3 12.59 4.01 3 -8 4 0.85 2.25 3 -8 5 0.49 0.65 3 -8 6 0.93 0.75 -3 -9 17 0.07 2.14 -3 -9 16 38.81 9.91 -3 -9 15 0.14 1.93 -3 -9 14 88.29 14.28 3 -9 -3 104.78 17.72 3 -9 -2 707.75 41.30 3 -9 -1 293.26 26.09 3 -9 1 35.54 8.02 3 -9 3 53.77 10.02 3 -10 -1 14.16 7.16 3 -10 0 33.45 8.27 3 -10 1 7.67 3.77 3 -10 2 145.05 15.76 3 -10 3 4.36 1.66 3 -10 4 1.38 1.96 3 -10 5 1.34 1.22 3 -10 6 43.60 6.33 3 -10 7 27.71 3.46 3 -11 1 8.02 3.97 3 -11 3 1.83 2.40 3 -11 5 3.12 2.45 3 -11 7 0.19 0.65 3 -12 3 9.59 5.62 3 -12 4 -2.09 1.86 3 -12 5 0.24 0.79 3 -12 6 0.19 1.09 3 -12 7 6.92 2.91 3 -12 8 0.09 0.55 3 -13 5 0.38 1.79 3 -13 6 35.78 8.25 3 -13 7 0.77 1.33 3 -13 8 72.87 7.21 3 -14 7 0.23 2.39 -4 0 17 -0.53 1.02 4 0 -17 -0.14 3.71 4 0 -16 5.03 6.03 -4 0 16 8.43 6.06 4 0 -15 -1.12 2.52 -4 0 15 -2.11 2.92 4 0 -14 66.76 14.44 -4 0 14 61.99 14.18 -4 0 13 0.11 1.17 4 0 -13 1.54 2.72 4 0 -12 482.65 39.08 -4 0 12 507.70 39.94 -4 0 11 -0.30 22.31 4 0 -11 -0.58 2.21 -4 0 10 603.87 42.39 4 0 -9 -0.42 1.11 -4 0 9 -0.52 1.76 -4 0 8 1153.13 52.04 4 0 -8 1048.22 49.67 4 0 -7 -0.36 0.55 -4 0 7 -0.53 1.79 4 0 -5 -0.76 1.18 -4 0 5 -0.53 1.48 -4 0 4 5659.24 100.97 4 0 -3 1.28 1.90 -4 0 3 -0.22 0.86 -4 -1 18 -0.40 3.36 4 1 -18 -0.28 2.26 4 1 -17 1.58 1.75 -4 1 17 1.00 3.36 4 -1 -17 0.92 2.19 -4 -1 17 -1.52 2.98 4 1 -16 1.75 4.16 4 -1 -16 5.62 5.40 -4 1 16 4.97 4.05 -4 -1 16 0.87 2.60 4 1 -15 4.12 3.87 4 -1 -15 1.08 2.93 -4 1 15 0.13 4.13 -4 -1 15 -1.15 3.35 4 1 -14 24.40 9.33 4 -1 -14 40.04 13.73 -4 1 14 22.88 6.62 -4 -1 14 15.78 8.51 -4 -1 13 4.96 3.62 4 1 -13 3.13 3.95 4 -1 -13 10.60 5.97 -4 1 13 4.55 4.17 -4 -1 12 0.61 0.55 4 1 -12 0.10 0.53 4 -1 -12 1.78 23.78 -4 1 12 2.69 4.15 -4 1 11 33.26 10.70 -4 -1 11 36.34 10.05 4 -1 -11 45.77 11.70 4 1 -11 27.19 10.12 -4 1 10 55.50 14.03 -4 -1 10 41.82 13.59 4 1 -10 53.19 12.79 4 -1 -10 58.79 14.03 -4 1 9 49.61 10.92 4 -1 -9 48.52 11.18 -4 -1 9 36.36 10.92 4 1 -9 28.94 10.99 4 1 -8 379.04 29.23 -4 -1 8 331.90 29.20 -4 -1 7 74.51 13.41 4 1 -7 84.49 13.34 4 -1 -7 84.55 14.24 -4 1 7 69.10 14.07 -4 -1 6 432.65 30.68 4 1 -5 2111.63 60.63 4 -1 -5 2077.73 64.37 -4 -1 5 2063.54 62.53 -4 1 5 2012.96 65.93 4 -1 -4 101.58 14.07 -4 1 4 103.60 14.54 -4 1 3 164.81 16.93 4 -1 -2 944.84 37.16 -4 1 2 964.58 38.94 -4 1 1 13.87 4.67 -4 -2 19 -1.70 3.47 4 2 -19 -2.98 2.07 4 2 -18 196.40 27.51 -4 -2 18 164.60 25.26 4 2 -17 5.27 4.73 -4 -2 17 4.81 6.50 4 -2 -16 159.83 25.86 -4 -2 16 129.85 20.85 4 2 -16 153.63 23.49 -4 2 16 136.35 24.55 -4 -2 15 6.45 4.77 4 -2 -15 1.91 2.24 -4 2 15 4.98 7.98 4 2 -15 7.92 5.95 4 -2 -14 332.23 37.68 -4 2 14 360.24 37.62 4 2 -14 347.99 34.18 4 -2 -13 4.89 4.34 -4 -2 13 5.24 3.56 -4 2 13 4.14 5.31 4 2 -13 1.88 2.82 4 2 -12 705.37 43.80 -4 -2 12 640.22 43.80 4 -2 -12 576.72 46.67 4 -2 -11 19.37 7.94 4 2 -11 4.60 5.43 -4 -2 11 23.12 7.97 -4 2 11 22.22 8.41 -4 -2 10 527.90 36.57 4 2 -9 160.08 18.94 -4 2 9 141.16 20.80 -4 -2 9 165.64 19.93 4 -2 -9 151.27 21.71 4 -2 -8 304.91 27.83 -4 2 8 274.26 26.84 -4 -2 8 240.02 23.56 4 2 -8 236.37 22.76 4 -2 -7 178.98 20.87 -4 -2 7 166.57 18.41 -4 2 7 163.84 21.02 4 -2 -6 1279.60 55.06 -4 -2 6 1303.66 51.02 -4 2 6 1224.66 54.16 -4 2 5 1031.28 46.57 4 -2 -5 1024.60 46.34 4 -2 -4 2285.43 65.67 -4 2 4 2136.28 64.71 -4 2 3 149.14 17.07 4 -2 -3 123.46 15.14 4 -2 -2 3941.64 78.87 4 -2 0 1263.19 39.97 4 3 -19 27.19 9.58 -4 -3 19 11.48 6.54 4 3 -18 0.24 3.10 -4 -3 18 -0.12 3.20 -4 -3 17 0.11 1.75 4 3 -17 1.03 1.38 4 3 -16 -0.11 2.35 -4 -3 16 -0.33 1.57 4 -3 -15 17.09 8.18 -4 -3 15 22.97 10.16 -4 3 15 30.35 10.78 4 3 -15 33.97 9.43 4 -3 -14 3.08 3.81 -4 -3 14 8.29 5.93 4 3 -14 3.18 3.42 -4 3 14 2.02 3.79 4 -3 -13 5.90 5.35 4 3 -13 1.90 1.62 -4 3 13 7.48 4.89 4 -3 -12 8.45 6.61 -4 -3 12 7.45 4.81 -4 3 12 1.91 3.10 4 3 -12 2.46 4.02 4 -3 -11 53.44 14.85 -4 -3 11 53.74 13.49 4 3 -11 71.89 14.87 -4 3 11 43.81 15.17 -4 -3 10 1.19 2.73 -4 3 10 -0.10 0.80 4 -3 -9 3.60 4.17 -4 -3 9 1.54 1.76 -4 3 9 5.40 4.28 -4 3 8 0.09 1.10 4 -3 -8 0.48 1.26 -4 -3 8 -0.52 2.22 4 -3 -7 202.67 22.88 4 -3 -5 415.07 31.31 -4 3 5 441.62 32.07 -4 3 4 5.56 2.80 4 -3 -4 1.75 2.25 4 -3 -3 68.50 12.01 -4 3 3 55.08 11.36 -4 3 2 89.74 12.56 4 -3 -2 91.55 11.82 -4 3 1 396.55 26.02 -4 3 0 10.01 4.65 4 -3 0 10.45 4.37 -4 3 -1 7.12 3.79 4 -3 1 7.09 3.33 -4 3 -2 620.14 26.31 -4 3 -3 3.12 1.34 -4 -4 20 13.86 7.90 4 4 -20 33.93 12.57 4 4 -19 1.92 5.66 -4 -4 19 1.05 1.79 -4 -4 18 70.68 16.84 4 4 -18 89.13 17.89 4 4 -17 3.42 4.19 -4 -4 17 4.15 4.26 -4 -4 16 45.29 13.17 4 4 -16 49.14 11.95 -4 -4 15 -0.21 2.32 -4 4 14 163.62 27.42 -4 -4 14 195.47 24.39 4 -4 -14 186.20 29.41 -4 -4 13 8.98 6.01 -4 4 13 11.07 5.21 4 -4 -13 5.32 4.92 -4 -4 12 167.37 22.20 -4 4 12 205.10 27.85 4 -4 -12 226.32 28.44 -4 -4 11 12.51 6.16 -4 4 11 24.33 10.80 4 -4 -11 33.87 11.36 -4 -4 9 0.31 0.83 4 -4 -9 0.43 1.30 -4 4 9 -0.32 1.90 4 -4 -7 -0.55 1.57 -4 4 7 0.27 0.68 4 -4 -6 3139.42 89.84 -4 4 6 3174.64 88.81 4 -4 -5 4.42 4.05 -4 4 5 3.93 4.42 4 -4 -3 94.71 13.96 -4 4 3 97.84 14.66 4 -4 -2 3137.90 74.77 4 -4 -1 543.38 29.48 -4 4 0 93.92 12.04 4 -4 0 97.72 11.60 4 -4 1 212.09 16.26 4 -4 2 1999.96 46.02 -4 4 -5 285.14 15.59 -4 4 -14 119.20 11.19 -4 4 -15 12.11 4.31 -4 4 -16 80.65 11.21 -4 4 -17 2.17 2.06 -4 -5 21 1.05 0.89 -4 -5 20 0.11 29.44 -4 -5 19 1.35 2.64 -4 -5 18 9.23 6.39 -4 -5 17 0.31 0.79 -4 -5 16 1.45 2.17 -4 -5 15 1.70 4.09 -4 -5 14 -2.60 4.20 4 -5 -14 -2.38 3.09 -4 5 13 6.38 5.87 -4 -5 13 3.11 3.53 -4 -5 12 9.12 4.34 -4 5 12 11.26 7.26 -4 -5 11 67.81 13.94 -4 5 11 71.58 16.35 4 -5 -10 73.28 19.47 -4 5 10 11.62 8.13 4 -5 -9 74.00 19.38 -4 5 9 28.69 9.62 4 -5 -8 127.68 24.11 -4 5 8 80.50 17.13 4 -5 -7 32.51 14.63 -4 5 7 2.79 1.04 4 -5 -6 3.93 11.15 -4 5 6 0.54 1.09 4 -5 -5 37.09 9.05 -4 5 5 43.38 10.05 4 -5 -4 17.69 6.92 -4 5 4 10.97 4.96 4 -5 -3 3.29 3.49 -4 5 3 2.05 2.79 -4 5 2 158.78 17.02 4 -5 -2 158.47 17.65 -4 5 1 39.71 8.58 4 -5 -1 39.22 8.61 -4 5 0 71.45 10.82 4 -5 0 56.76 10.49 4 -5 1 37.73 6.92 -4 5 -1 33.68 7.63 4 -5 2 78.64 9.19 -4 5 -2 70.28 9.87 4 -5 3 995.85 31.76 -4 5 -4 10.08 3.45 -4 5 -6 -0.12 0.70 -4 5 -7 221.45 10.80 -4 5 -8 0.89 0.28 -4 5 -13 0.39 2.77 -4 5 -14 15.78 4.62 -4 5 -15 -0.39 0.89 -4 5 -16 1.01 0.48 -4 5 -17 10.72 3.20 -4 -6 20 4.08 3.76 -4 -6 19 -0.21 3.72 -4 -6 18 21.45 9.44 -4 -6 17 2.49 4.73 -4 -6 16 43.55 12.87 -4 -6 15 -1.16 2.51 -4 -6 14 304.91 29.30 -4 6 13 11.23 8.07 4 -6 -13 7.23 5.21 -4 -6 13 9.07 4.46 4 -6 -12 403.48 42.74 -4 -6 12 394.67 32.40 4 -6 -11 3.81 3.32 -4 6 11 0.95 3.74 -4 6 10 916.75 60.14 4 -6 -10 976.56 62.41 4 -6 -9 2.60 1.34 -4 6 9 10.08 5.91 4 -6 -8 186.99 24.44 -4 6 8 181.15 24.72 4 -6 -7 35.84 12.77 -4 6 7 71.80 14.92 4 -6 -6 137.87 22.86 -4 6 6 201.03 23.87 4 -6 -5 16.61 6.58 -4 6 5 1.98 3.16 4 -6 -4 21.92 11.89 -4 6 4 13.82 7.74 -4 6 3 20.89 7.79 4 -6 -3 32.21 11.03 4 -6 -1 136.33 15.26 -4 6 1 106.56 13.88 -4 6 0 1604.64 52.22 4 -6 0 1610.05 52.22 -4 6 -1 387.31 23.89 4 -6 1 396.54 24.58 4 -6 2 3151.91 64.64 4 -6 3 49.62 7.31 -4 6 -3 39.60 6.49 4 -6 4 2385.35 45.45 -4 6 -4 2333.96 46.42 -4 6 -5 9.18 2.61 -4 6 -6 1627.03 31.88 -4 -7 19 4.47 3.68 -4 -7 18 1.16 2.92 -4 -7 17 6.09 6.08 -4 -7 16 -0.97 3.94 -4 -7 15 5.30 4.69 -4 -7 14 0.09 2.70 -4 -7 13 20.20 7.46 -4 7 12 0.63 2.56 4 -7 -12 2.48 4.65 4 -7 -11 47.88 13.78 -4 7 11 47.54 13.43 -4 7 10 -0.69 1.49 4 -7 -10 3.15 4.38 4 -7 -9 33.42 11.25 -4 7 9 27.21 10.13 4 -7 -8 0.74 3.66 -4 7 8 -1.89 5.41 4 -7 -7 109.62 19.22 -4 7 7 96.86 17.77 -4 7 6 225.56 26.22 4 -7 -6 205.64 25.59 -4 7 5 17.73 5.68 4 -7 -5 7.16 4.38 4 -7 -4 41.73 11.24 -4 7 4 44.61 11.82 4 -7 -3 25.97 10.20 -4 7 3 44.17 10.24 4 -7 -2 11.19 5.37 -4 7 2 18.01 6.52 4 -7 -1 69.30 13.38 -4 7 1 52.51 10.10 -4 7 0 -0.87 0.95 4 -7 0 0.06 0.97 4 -7 1 14.17 5.51 -4 7 -1 13.67 4.70 4 -7 2 9.25 3.71 -4 7 -2 8.36 3.53 4 -7 4 54.85 8.44 -4 7 -4 57.88 8.53 4 -7 5 152.93 11.00 -4 -8 18 19.35 7.65 -4 -8 17 -0.67 3.09 -4 -8 16 69.13 14.56 -4 -8 15 2.02 6.73 4 -8 -11 -1.16 2.82 -4 8 11 -0.16 35.14 -4 8 10 219.94 31.18 4 -8 -10 209.28 31.11 4 -8 -9 43.77 15.89 -4 8 9 17.58 9.54 -4 8 8 413.45 39.43 4 -8 -8 411.13 40.76 4 -8 -7 18.48 8.73 -4 8 7 19.29 9.24 -4 8 6 732.03 50.19 4 -8 -6 756.33 51.19 4 -8 -5 0.63 1.59 -4 8 5 1.23 2.28 -4 8 4 1025.83 55.73 4 -8 -3 114.92 17.76 -4 8 3 95.59 16.24 -4 8 2 604.11 37.63 4 -8 -2 568.64 37.77 -4 8 1 37.86 9.98 4 -8 -1 24.74 8.83 4 -8 0 597.31 35.18 -4 8 -1 58.50 10.67 4 -8 1 73.57 11.24 4 -8 2 150.15 15.70 -4 8 -2 154.61 15.48 -4 8 -3 48.28 8.54 4 -8 3 44.22 8.36 4 -8 4 77.97 9.71 4 -8 5 11.57 3.37 4 -9 -10 4.28 6.73 4 -9 -9 2.00 3.89 4 -9 -8 11.67 6.25 -4 9 8 4.11 3.63 4 -9 -7 52.75 13.77 -4 9 7 49.29 14.40 4 -9 -6 15.49 8.26 -4 9 6 19.51 8.24 4 -9 -5 4.16 3.94 -4 9 5 3.83 3.19 4 -9 -4 86.78 16.18 -4 9 4 65.64 14.61 -4 9 3 163.83 21.38 4 -9 -3 186.38 22.72 4 -9 -2 29.75 9.06 -4 9 2 33.57 9.99 4 -9 -1 155.63 19.17 4 -9 0 36.77 9.14 4 -9 1 36.40 10.10 4 -9 2 161.07 16.36 4 -9 3 11.29 4.33 4 -9 4 32.34 6.42 4 -9 5 61.44 8.30 4 -9 6 0.17 0.72 4 -10 -7 6.93 6.84 4 -10 -6 160.38 25.73 4 -10 -5 18.99 9.06 4 -10 -4 343.27 35.06 4 -10 -3 2.88 3.09 4 -10 -2 311.47 29.33 4 -10 -1 -0.51 0.46 4 -10 0 618.47 38.33 4 -10 1 90.77 13.91 4 -10 2 376.73 26.42 4 -10 3 37.77 8.13 4 -10 4 285.30 20.00 4 -10 5 0.58 1.25 4 -11 -4 2.28 28.69 4 -11 -3 1.88 3.11 4 -11 -2 3.15 3.56 4 -11 -1 17.28 6.72 4 -11 0 1.77 2.73 4 -11 1 40.71 9.22 4 -11 2 -0.61 2.01 4 -11 3 23.16 7.10 4 -11 4 26.96 7.08 4 -11 5 24.01 5.23 4 -11 6 2.99 1.86 4 -12 -1 2.71 3.43 4 -12 0 172.18 21.74 4 -12 1 1.07 1.89 4 -12 2 142.16 18.53 4 -12 3 0.45 0.49 4 -12 4 53.49 11.14 4 -12 5 3.63 2.25 4 -12 6 106.79 11.74 4 -12 7 0.32 1.33 4 -13 1 4.01 4.00 4 -13 2 0.16 1.69 4 -13 3 2.07 2.25 4 -13 4 7.76 5.47 4 -13 5 0.75 1.56 4 -13 6 12.91 3.72 4 -13 7 -0.03 0.34 4 -14 3 -0.08 1.56 4 -14 4 9.14 5.41 4 -14 5 0.06 1.22 4 -14 6 40.26 8.35 4 -14 7 10.79 3.48 5 0 -16 -1.75 2.73 -5 0 16 -1.00 4.44 5 0 -15 13.80 5.83 -5 0 15 6.83 6.97 -5 0 14 -2.05 0.98 5 0 -14 0.91 3.07 -5 0 13 2.24 3.29 5 0 -13 14.00 6.30 -5 0 12 0.48 1.72 5 0 -12 0.12 2.25 -5 0 11 -0.57 2.61 5 0 -11 0.11 1.75 5 0 -10 -0.20 1.81 -5 0 10 0.21 1.88 5 0 -9 56.71 12.38 -5 0 9 44.57 12.51 5 0 -8 -0.09 0.48 -5 0 8 -0.29 2.62 5 0 -7 199.14 22.59 -5 0 7 162.18 21.39 -5 0 6 -0.60 2.12 5 0 -6 -0.16 2.02 -5 0 5 34.69 8.14 5 0 -5 32.84 7.63 -5 0 4 -2.11 2.12 5 1 -17 -0.14 32.98 -5 -1 17 0.58 2.48 5 1 -16 121.93 22.22 -5 -1 16 110.93 21.76 -5 -1 15 0.26 2.61 5 1 -15 0.78 2.89 -5 1 15 8.81 6.48 5 -1 -15 3.05 2.94 5 1 -14 244.20 30.48 -5 -1 14 244.00 31.11 5 -1 -14 224.05 29.81 -5 1 14 242.64 30.59 -5 1 13 53.58 15.40 -5 -1 13 67.77 15.76 5 1 -13 68.55 14.83 5 -1 -13 54.58 13.48 5 1 -12 521.22 41.72 -5 1 12 488.20 42.96 -5 -1 12 502.78 42.15 5 -1 -12 542.81 44.27 5 -1 -11 123.60 19.00 5 1 -11 114.91 19.02 -5 1 11 102.98 20.09 -5 -1 11 84.03 18.95 5 1 -10 377.25 33.79 -5 -1 10 342.01 32.87 5 -1 -10 366.10 34.66 -5 -1 9 98.99 17.88 5 -1 -9 109.66 19.21 -5 1 9 62.40 17.73 5 1 -9 105.73 18.07 5 1 -8 60.97 12.93 -5 -1 8 66.51 13.61 5 -1 -8 62.67 13.42 -5 1 8 64.38 19.34 5 1 -7 315.33 27.58 -5 1 7 310.35 28.97 -5 -1 7 293.27 28.76 5 -1 -6 2575.41 79.08 -5 1 6 2565.11 82.28 -5 -1 6 2428.24 78.14 5 -1 -5 172.57 19.80 -5 1 5 140.14 18.59 -5 1 4 681.68 40.70 5 -1 -3 501.27 30.58 -5 1 3 467.12 31.02 5 2 -17 0.27 3.14 -5 -2 17 -0.41 4.20 -5 -2 16 1.68 2.32 5 2 -16 -0.91 3.86 -5 -2 15 14.48 9.37 5 2 -15 9.29 6.17 5 -2 -15 31.23 12.83 -5 2 15 10.03 7.79 -5 -2 14 9.92 6.00 5 2 -14 16.58 6.95 5 -2 -14 5.72 4.69 -5 2 14 6.89 5.91 -5 -2 13 30.15 10.44 5 -2 -13 32.37 12.40 5 2 -13 10.01 7.67 -5 2 13 11.37 7.34 -5 2 12 58.99 15.06 -5 -2 12 55.47 13.00 5 -2 -12 59.94 14.77 5 2 -12 60.92 14.73 -5 2 11 40.69 14.21 5 2 -11 43.75 12.49 5 -2 -11 55.43 15.13 -5 -2 11 53.51 12.84 -5 -2 10 5.44 4.96 -5 2 10 4.15 5.25 5 2 -10 7.05 5.72 5 -2 -10 3.47 4.37 -5 -2 9 0.59 2.11 -5 2 9 6.98 6.21 5 2 -9 0.34 1.13 -5 2 8 4.90 5.12 -5 -2 8 2.90 2.81 5 -2 -8 2.62 3.24 5 -2 -7 138.06 19.29 -5 2 7 116.19 18.47 -5 -2 7 132.55 18.67 -5 2 6 184.75 25.20 5 -2 -6 173.91 21.40 5 -2 -4 204.72 20.98 -5 2 4 190.02 21.73 5 -2 -3 617.46 35.56 -5 2 3 649.83 37.77 -5 2 2 64.80 12.18 5 -2 -2 76.36 11.69 -5 2 1 196.15 18.79 -5 2 0 111.05 14.61 5 3 -18 37.49 13.68 -5 -3 18 51.07 14.85 -5 -3 17 0.13 3.92 5 3 -17 1.86 3.67 5 3 -16 92.84 20.42 -5 -3 16 92.68 19.62 -5 -3 15 3.38 6.17 5 3 -15 1.35 3.56 5 -3 -14 195.40 30.86 -5 -3 14 185.92 26.05 -5 3 14 177.05 27.98 5 3 -14 190.85 25.56 5 -3 -13 1.19 3.61 -5 -3 13 2.99 4.02 5 3 -13 -0.82 2.21 -5 3 13 -0.29 1.35 5 -3 -12 493.72 45.93 -5 3 12 432.13 43.52 -5 -3 11 -0.85 1.51 5 -3 -11 3.40 5.47 -5 3 11 2.00 4.00 -5 3 10 456.22 41.24 -5 -3 10 468.98 38.55 5 -3 -10 488.10 41.78 5 -3 -9 9.02 5.21 -5 -3 9 2.73 2.79 -5 3 8 627.61 44.21 5 -3 -8 572.24 42.39 -5 3 7 594.70 43.20 5 -3 -7 621.87 42.44 -5 3 5 87.38 16.24 5 -3 -5 110.90 16.21 -5 3 4 1694.10 64.69 -5 3 3 124.23 17.45 5 -3 -3 128.27 16.50 5 -3 -1 84.01 11.58 -5 3 1 74.59 12.21 5 -3 0 2537.72 64.57 -5 3 0 2462.94 64.97 -5 3 -1 49.02 9.09 -5 -4 18 1.82 4.81 -5 -4 17 1.76 3.66 -5 -4 16 11.43 4.90 -5 -4 15 1.94 2.85 -5 -4 14 -0.46 0.87 5 -4 -13 -2.05 4.00 -5 -4 13 4.68 5.86 -5 4 13 5.61 7.09 -5 -4 12 -1.41 2.81 5 -4 -12 -1.92 3.29 -5 4 12 -3.39 2.16 5 -4 -11 5.51 5.00 -5 4 11 0.13 1.02 -5 -4 11 0.94 1.87 5 -4 -10 1.41 1.55 -5 4 10 0.37 1.33 5 -4 -9 40.39 12.38 -5 4 9 33.24 11.56 -5 4 8 -0.11 1.16 5 -4 -8 1.34 0.85 -5 4 7 -0.20 1.22 5 -4 -7 -0.21 1.59 -5 4 6 172.13 22.57 5 -4 -6 154.89 21.46 -5 4 5 105.60 16.62 5 -4 -5 101.00 16.08 -5 4 4 3.51 3.99 5 -4 -4 3.70 1.57 5 -4 -2 28.42 9.35 -5 4 2 69.53 15.17 5 -4 -1 147.43 16.52 5 -4 0 10.93 3.98 -5 4 0 7.90 4.32 5 -4 1 138.56 14.87 -5 4 -2 1.18 1.96 -5 4 -3 226.59 17.36 -5 4 -5 0.04 1.52 -5 -5 19 -1.03 4.12 -5 -5 18 15.79 9.29 -5 -5 17 1.37 2.52 -5 -5 16 61.00 16.14 -5 -5 15 7.38 6.88 -5 -5 14 102.73 19.94 5 -5 -13 10.59 7.66 -5 -5 13 4.08 2.38 -5 5 12 332.35 39.07 5 -5 -12 316.06 38.40 -5 -5 12 298.96 31.85 5 -5 -11 0.58 0.79 -5 5 11 -0.14 2.57 -5 5 10 295.80 35.72 5 -5 -10 357.93 38.67 5 -5 -9 63.07 15.54 -5 5 9 63.19 14.82 -5 5 8 493.74 42.46 5 -5 -7 23.87 8.14 -5 5 7 15.16 7.23 -5 5 6 533.17 40.19 5 -5 -6 482.06 40.53 -5 5 5 137.89 20.87 5 -5 -5 180.12 22.78 -5 5 4 743.88 43.72 5 -5 -4 666.56 41.32 -5 5 3 25.64 8.36 5 -5 -3 28.57 8.43 -5 5 2 132.67 19.65 5 -5 -2 143.78 18.45 -5 5 1 24.25 7.09 5 -5 -1 28.55 7.20 -5 5 0 663.70 35.57 5 -5 0 663.88 34.92 5 -5 1 155.20 16.64 -5 5 -2 815.33 35.26 -5 5 -3 1.11 0.75 -5 5 -4 1445.98 43.41 -5 5 -5 366.04 20.57 -5 5 -6 974.75 31.56 -5 5 -7 3.71 2.57 -5 5 -8 1031.64 28.73 -5 5 -15 0.22 0.85 -5 5 -16 71.81 7.71 -5 -6 19 -0.12 2.56 -5 -6 18 0.12 1.86 -5 -6 17 0.73 3.00 -5 -6 16 0.71 1.42 -5 -6 15 27.75 12.41 -5 -6 14 0.22 3.89 -5 6 12 0.31 35.82 5 -6 -12 0.49 5.01 -5 6 11 105.42 20.68 5 -6 -11 98.59 21.66 -5 6 10 0.14 1.64 5 -6 -10 1.99 2.98 -5 6 9 169.01 24.90 5 -6 -9 169.82 25.35 -5 6 8 -3.70 5.00 5 -6 -8 -2.73 4.39 -5 6 7 241.43 29.02 5 -6 -7 286.46 31.96 -5 6 6 34.76 11.87 5 -6 -6 29.28 11.09 5 -6 -5 3.89 3.45 -5 6 5 5.67 5.43 5 -6 -4 106.60 17.56 -5 6 4 112.75 17.23 -5 6 3 308.33 28.01 5 -6 -3 270.03 27.27 -5 6 2 20.68 7.75 5 -6 -2 28.37 7.86 -5 6 1 435.02 30.94 5 -6 -1 534.21 32.79 -5 6 0 17.43 5.94 5 -6 0 19.12 6.41 -5 6 -1 234.82 19.94 5 -6 1 205.68 19.39 5 -6 2 98.01 12.11 -5 6 -2 85.95 12.42 5 -6 3 78.25 10.47 -5 6 -3 94.70 11.67 -5 6 -4 7.17 3.81 -5 6 -6 48.09 7.69 -5 6 -7 217.46 13.17 -5 6 -8 -0.02 0.47 -5 6 -9 104.71 7.01 -5 -7 19 -0.35 1.98 -5 -7 18 6.21 5.25 -5 -7 17 0.82 2.68 -5 -7 16 39.87 12.48 -5 7 11 3.74 4.54 5 -7 -11 -0.16 1.47 -5 7 10 352.14 38.36 5 -7 -10 325.79 38.77 -5 7 9 1.62 4.44 5 -7 -9 -0.68 2.44 5 -7 -8 650.99 49.41 -5 7 8 679.65 50.64 -5 7 7 72.99 16.28 5 -7 -7 73.38 15.32 -5 7 6 745.16 49.83 5 -7 -6 721.55 49.01 -5 7 5 0.81 2.12 5 -7 -5 0.31 1.38 5 -7 -4 966.71 53.16 5 -7 -3 24.26 7.85 -5 7 3 16.02 6.38 -5 7 2 575.52 37.44 5 -7 -2 600.88 38.12 5 -7 -1 -0.15 1.63 -5 7 1 2.47 2.86 -5 7 0 222.26 21.43 5 -7 0 249.31 22.17 5 -7 1 1.53 1.88 -5 7 -1 1.45 2.14 -5 7 -2 267.75 21.38 5 -7 2 325.52 22.61 5 -7 3 64.85 9.70 -5 7 -3 59.97 9.82 5 -7 4 356.35 20.48 -5 7 -4 339.17 20.80 -5 7 -5 36.21 6.43 -5 7 -7 99.56 8.39 -5 7 -8 602.77 16.63 -5 8 10 -1.56 2.80 5 -8 -10 47.88 18.63 -5 8 9 1.31 6.47 5 -8 -9 53.64 19.92 -5 8 8 -3.51 5.51 5 -8 -8 50.22 18.33 -5 8 7 0.13 3.18 5 -8 -7 -10.49 3.24 -5 8 6 3.95 4.57 5 -8 -6 59.58 18.39 -5 8 5 39.27 12.22 5 -8 -5 35.97 11.89 -5 8 4 33.83 10.91 5 -8 -4 13.65 8.02 -5 8 3 114.88 17.27 5 -8 -3 101.62 17.13 -5 8 2 -0.84 2.58 5 -8 -2 1.05 2.00 -5 8 1 530.45 35.13 5 -8 -1 539.54 36.78 5 -8 0 -0.29 2.08 -5 8 0 1.62 2.49 -5 8 -1 154.82 16.89 5 -8 1 138.68 16.75 -5 8 -2 33.31 7.58 5 -8 2 26.06 7.08 5 -8 3 42.77 7.89 -5 8 -3 34.55 7.56 5 -8 4 81.17 10.50 -5 8 -4 68.10 9.74 -5 8 -5 0.82 0.40 -5 8 -6 0.03 0.56 -5 9 9 -0.16 1.70 5 -9 -9 0.16 1.48 -5 9 8 124.14 23.15 5 -9 -8 83.44 20.11 -5 9 7 4.77 5.90 5 -9 -7 2.32 2.76 -5 9 6 208.58 28.09 5 -9 -6 175.38 25.62 -5 9 5 0.93 1.78 5 -9 -5 7.84 16.49 5 -9 -4 273.76 31.56 -5 9 4 270.33 30.85 -5 9 3 50.37 12.38 5 -9 -3 42.37 12.19 -5 9 2 756.28 45.28 5 -9 -2 735.77 45.00 -5 9 1 4.09 4.62 5 -9 -1 3.05 2.63 -5 9 0 699.07 39.92 5 -9 0 653.34 39.62 5 -9 1 -0.35 3.22 -5 9 -1 0.48 1.58 -5 9 -2 736.27 37.78 5 -9 2 790.17 39.13 -5 9 -3 3.96 2.79 5 -9 3 3.15 2.40 -5 9 -4 262.82 19.47 5 -9 4 274.78 19.45 5 -9 5 0.15 0.41 -5 10 8 -1.55 3.66 5 -10 -8 0.64 1.93 5 -10 -7 -1.18 3.20 -5 10 7 7.94 7.57 -5 10 6 4.29 5.28 5 -10 -6 1.92 1.82 -5 10 5 0.12 0.95 5 -10 -5 0.50 0.95 -5 10 4 28.12 9.39 5 -10 -4 40.83 11.85 -5 10 3 0.11 2.37 5 -10 -3 3.66 10.65 -5 10 2 0.78 2.25 5 -10 -2 29.57 11.55 -5 10 1 28.98 9.23 5 -10 -1 36.72 10.12 -5 10 0 -4.52 3.29 5 -10 0 0.25 2.64 5 -10 1 1.89 2.16 5 -10 2 46.00 9.89 5 -10 3 1.00 2.08 5 -10 4 0.25 1.60 5 -10 5 3.12 1.92 5 -10 6 0.13 0.45 5 -11 -7 1.42 31.95 5 -11 -6 95.79 19.40 5 -11 -5 12.73 7.71 5 -11 -4 48.01 11.92 5 -11 -3 0.11 0.61 5 -11 -2 163.11 23.89 5 -11 -1 18.24 8.48 5 -11 0 149.48 20.20 5 -11 1 61.20 12.47 5 -11 2 146.13 18.29 5 -11 3 0.06 14.89 5 -11 4 82.39 12.07 5 -11 5 1.59 1.99 5 -11 6 198.59 14.98 5 -12 -5 1.59 4.69 5 -12 -4 1.74 3.15 5 -12 -3 -2.21 3.46 5 -12 -2 -0.11 1.04 5 -12 -1 33.29 13.36 5 -12 0 6.97 9.42 5 -12 1 21.54 8.02 5 -12 2 1.32 2.05 5 -12 3 20.58 7.05 5 -12 4 0.18 1.41 5 -12 5 15.93 5.16 5 -12 6 -0.75 1.82 5 -13 -3 21.40 10.11 5 -13 -2 168.73 23.25 5 -13 -1 -0.98 1.02 5 -13 0 180.08 23.91 5 -13 1 1.88 2.37 5 -13 2 86.74 14.49 5 -13 3 27.20 7.79 5 -13 4 87.30 13.36 5 -13 5 0.75 2.33 5 -13 6 84.48 10.64 5 -14 0 5.74 13.53 5 -14 1 4.77 10.69 5 -14 2 1.22 4.75 5 -14 3 -0.63 1.36 5 -14 4 0.69 2.32 5 -14 5 1.11 1.73 5 -14 6 1.08 1.08 5 -15 2 6.03 5.32 5 -15 3 0.76 2.98 5 -15 4 17.31 6.78 6 0 -15 -3.03 4.41 -6 0 14 264.21 35.54 6 0 -14 240.85 32.65 -6 0 13 4.61 5.88 6 0 -13 1.09 3.74 6 0 -12 585.32 47.66 -6 0 12 560.75 50.14 6 0 -11 1.34 0.66 -6 0 11 -1.02 3.15 6 0 -10 847.70 55.17 -6 0 10 720.18 53.42 6 0 -9 0.76 1.66 -6 0 9 -0.12 0.63 -6 0 7 1.48 3.80 6 0 -7 -0.65 1.94 -6 0 6 1900.92 74.52 -6 0 5 -0.73 2.33 -6 -1 15 44.60 14.18 6 1 -15 45.27 13.41 -6 1 14 7.66 6.98 -6 -1 14 3.94 5.35 6 -1 -14 1.67 3.67 6 1 -14 1.38 2.47 -6 1 13 61.36 16.79 6 -1 -13 83.26 18.93 -6 -1 13 59.93 16.83 6 1 -13 77.68 16.80 -6 1 12 1.56 4.19 6 -1 -12 1.75 2.92 -6 -1 12 -0.13 1.99 6 1 -12 -1.84 3.03 6 1 -11 39.33 11.83 -6 1 11 33.28 12.18 6 -1 -11 30.22 10.51 -6 -1 11 18.11 9.73 6 1 -10 20.77 8.66 -6 1 10 26.77 11.42 6 -1 -10 22.29 8.03 -6 -1 10 4.11 4.03 -6 -1 9 -0.12 2.64 6 1 -9 1.01 1.64 6 -1 -9 2.01 2.95 6 1 -8 35.35 10.63 -6 -1 8 32.47 10.58 -6 1 8 24.55 9.09 6 -1 -8 40.40 11.00 -6 1 7 77.26 14.55 6 -1 -7 71.56 14.46 -6 -1 7 62.38 16.35 -6 1 6 62.86 14.27 6 -1 -6 70.79 14.45 6 -1 -5 -0.34 1.72 -6 1 5 -1.34 2.87 6 -1 -4 1.27 3.09 -6 1 4 -0.44 1.90 -6 1 3 0.17 1.10 -6 -2 15 -3.10 1.96 6 2 -15 -1.59 3.73 -6 -2 14 175.15 27.78 6 2 -14 152.40 26.26 6 -2 -13 -3.74 3.87 -6 2 13 0.89 5.58 6 2 -13 2.53 4.65 -6 -2 13 0.39 2.24 -6 2 12 204.71 31.10 6 2 -12 220.67 28.58 -6 -2 12 229.54 28.74 6 -2 -12 232.27 31.25 6 -2 -11 64.00 15.39 -6 2 11 48.97 16.18 6 2 -11 62.58 14.43 -6 -2 11 60.42 14.45 -6 2 10 260.07 31.51 -6 -2 10 232.63 29.22 6 -2 -10 235.45 29.90 6 -2 -9 9.59 6.96 -6 2 9 1.60 2.40 -6 -2 9 2.37 3.56 6 -2 -8 97.83 17.66 -6 2 8 82.42 16.74 6 -2 -7 0.10 1.46 -6 2 7 0.31 0.98 -6 2 6 1322.26 65.92 -6 2 5 2.15 1.18 6 -2 -5 0.27 0.69 6 -2 -4 1146.85 54.06 -6 2 4 1133.22 56.01 -6 2 3 12.12 6.14 6 -2 -3 16.63 5.49 -6 2 1 128.33 16.65 -6 -3 16 -2.69 3.43 -6 -3 15 1.72 2.69 -6 -3 14 -1.22 3.26 6 -3 -13 3.59 4.05 -6 -3 13 3.09 3.62 -6 3 13 1.09 4.99 -6 3 12 59.81 16.27 6 -3 -12 67.62 17.75 -6 -3 12 80.01 18.05 -6 3 11 1.38 4.15 -6 -3 11 -0.25 2.10 6 -3 -11 4.68 4.94 -6 3 10 53.14 13.38 6 -3 -10 52.14 14.36 -6 3 9 27.32 11.81 6 -3 -9 11.55 6.86 6 -3 -8 0.23 1.38 -6 3 8 1.20 3.31 6 -3 -7 45.14 12.53 -6 3 7 40.75 13.22 6 -3 -6 2.60 3.67 -6 3 6 0.41 1.76 6 -3 -5 113.66 19.06 -6 3 5 164.79 21.20 -6 3 3 63.69 15.46 6 -3 -3 86.74 14.97 -6 3 2 67.41 12.67 6 -3 -2 64.60 11.85 -6 3 1 108.21 15.89 6 -3 -1 88.65 13.83 -6 3 -1 249.04 22.15 -6 -4 16 50.53 15.14 -6 -4 15 1.78 3.62 -6 -4 14 170.82 26.65 -6 -4 13 0.91 2.62 -6 -4 12 176.11 26.00 6 -4 -12 159.34 27.79 -6 4 12 180.60 30.45 6 -4 -11 3.86 5.51 -6 4 11 0.87 3.53 -6 4 10 353.09 38.89 6 -4 -10 368.39 38.71 -6 4 9 0.51 0.98 6 -4 -9 0.90 1.21 -6 4 8 227.46 30.34 6 -4 -8 236.47 29.57 -6 4 7 0.94 3.36 6 -4 -7 0.11 0.84 6 -4 -6 1140.48 59.31 6 -4 -5 0.58 1.48 -6 4 5 5.44 4.68 6 -4 -4 324.13 29.92 6 -4 -3 7.08 4.50 -6 4 3 10.73 11.71 6 -4 -2 1164.58 52.08 -6 4 2 1174.78 54.86 6 -4 -1 594.78 36.14 -6 4 1 554.52 37.86 6 -4 0 545.50 32.21 -6 4 0 542.61 34.19 -6 4 -1 92.19 15.08 -6 4 -3 19.77 5.63 -6 -5 16 7.02 5.88 -6 -5 15 32.92 15.46 -6 -5 14 20.32 7.95 6 -5 -11 43.45 12.08 -6 5 11 45.31 14.38 6 -5 -10 15.92 8.36 -6 5 10 16.12 8.31 6 -5 -9 32.66 11.37 -6 5 9 30.02 11.44 -6 5 8 34.71 12.14 6 -5 -8 35.18 11.90 -6 5 7 151.58 24.33 6 -5 -7 178.92 25.19 -6 5 6 163.60 23.21 6 -5 -6 153.81 22.95 -6 5 5 96.39 18.74 6 -5 -5 97.51 18.09 -6 5 4 118.43 19.02 6 -5 -4 101.38 17.48 6 -5 -3 -0.09 1.49 -6 5 3 -1.12 2.89 -6 5 2 231.53 24.76 6 -5 -2 213.11 23.54 -6 5 1 2.48 3.28 6 -5 -1 2.52 3.44 6 -5 1 15.90 5.33 -6 5 -1 13.29 5.91 -6 5 -3 0.24 0.78 -6 5 -4 0.05 1.06 -6 5 -5 0.39 0.96 -6 5 -6 44.18 8.45 -6 5 -7 36.66 7.83 -6 -6 17 -5.34 5.21 6 -6 -10 264.53 34.54 -6 6 10 230.59 33.24 6 -6 -9 -0.88 2.50 -6 6 9 -1.73 2.69 -6 6 8 502.96 45.32 6 -6 -8 495.49 46.56 6 -6 -7 77.76 18.66 -6 6 7 89.52 19.35 6 -6 -6 1324.56 68.86 -6 6 5 43.21 13.45 6 -6 -5 52.43 13.39 -6 6 4 963.13 53.84 6 -6 -4 862.38 53.16 -6 6 3 31.76 9.41 6 -6 -3 26.37 8.37 -6 6 2 959.72 50.99 6 -6 -2 945.67 49.08 6 -6 -1 17.71 6.76 -6 6 1 16.36 6.58 -6 6 0 85.82 14.56 6 -6 0 75.07 13.66 6 -6 1 5.75 3.22 -6 6 -1 4.79 3.49 6 -6 2 360.67 25.00 -6 6 -2 371.28 26.94 -6 6 -3 98.19 13.26 -6 6 -4 107.88 13.84 -6 6 -5 32.25 6.66 -6 6 -7 5.69 2.45 -6 6 -8 302.33 17.73 -6 6 -9 40.96 7.18 -6 6 -10 273.19 14.65 -6 6 -11 14.31 3.29 6 -7 -10 -0.66 2.19 -6 7 10 3.13 1.47 6 -7 -9 -0.93 3.01 -6 7 9 -4.12 5.09 6 -7 -8 15.51 9.09 -6 7 8 7.87 6.55 6 -7 -7 17.09 9.02 -6 7 7 43.63 13.51 6 -7 -6 -2.48 5.37 -6 7 6 2.59 4.00 6 -7 -5 32.46 9.49 -6 7 5 56.71 13.39 6 -7 -4 34.27 10.66 -6 7 4 8.77 7.41 6 -7 -3 79.42 16.31 -6 7 3 80.97 16.03 6 -7 -2 6.71 5.40 -6 7 2 3.77 3.82 -6 7 1 117.08 17.57 6 -7 -1 115.46 17.70 -6 7 0 -0.08 1.36 6 -7 0 0.07 0.98 -6 7 -1 31.09 8.17 6 -7 1 42.88 8.53 -6 7 -2 98.59 14.38 6 -7 2 134.39 15.56 -6 7 -3 -2.53 2.60 6 -7 3 0.43 1.89 -6 7 -4 174.24 17.34 -6 7 -5 0.86 0.26 -6 7 -6 9.50 3.79 -6 7 -7 0.04 9.61 -6 7 -8 19.12 4.34 -6 7 -9 19.44 3.92 -6 7 -10 2.90 1.46 6 -8 -9 1.95 4.03 -6 8 9 2.79 5.17 6 -8 -8 199.11 30.80 -6 8 8 222.89 31.91 6 -8 -7 74.98 18.02 -6 8 7 76.00 17.62 6 -8 -6 117.33 21.61 -6 8 6 112.97 20.56 6 -8 -5 1.58 0.66 -6 8 5 2.34 3.70 -6 8 4 241.86 28.73 6 -8 -4 275.53 29.72 6 -8 -3 0.10 1.38 -6 8 3 1.03 2.43 -6 8 2 338.78 30.82 6 -8 -2 333.89 31.67 6 -8 -1 4.14 3.62 -6 8 1 3.02 2.49 6 -8 0 498.51 33.88 6 -8 1 25.34 7.44 -6 8 -1 38.15 9.12 6 -8 2 607.67 35.29 -6 8 -2 644.52 36.59 6 -8 3 69.09 11.34 -6 8 -3 62.37 11.07 6 -8 4 545.49 28.39 -6 8 -4 487.18 28.95 -6 8 -5 3.17 2.56 -6 8 -6 398.41 22.63 -6 8 -7 0.06 0.90 -6 8 -8 251.07 13.79 -6 9 8 0.31 2.89 6 -9 -8 28.35 9.67 -6 9 7 0.86 3.01 6 -9 -7 1.63 5.19 -6 9 6 2.66 4.61 6 -9 -6 -1.24 3.74 6 -9 -5 -1.42 3.19 -6 9 5 -0.25 1.89 6 -9 -4 11.18 3.34 -6 9 4 0.69 1.75 6 -9 -3 14.72 6.14 -6 9 3 26.11 9.92 6 -9 -2 1.93 1.45 -6 9 2 4.90 4.37 6 -9 -1 13.47 7.14 -6 9 1 3.70 2.24 6 -9 0 0.58 2.51 -6 9 0 1.90 2.41 -6 9 -1 21.81 6.89 6 -9 1 20.45 7.23 6 -9 2 2.23 2.81 -6 9 -2 0.89 1.28 6 -9 3 0.60 0.46 -6 9 -3 1.59 2.37 -6 9 -4 0.54 13.95 6 -9 4 0.78 1.53 -6 9 -5 65.07 9.70 -6 9 -6 22.16 5.99 -6 10 7 0.16 1.19 6 -10 -7 -0.31 2.79 -6 10 6 11.84 7.87 6 -10 -6 8.96 5.79 -6 10 5 14.84 9.34 6 -10 -5 2.43 5.40 6 -10 -4 216.75 29.09 -6 10 4 223.59 28.82 6 -10 -3 3.38 4.67 -6 10 3 7.94 5.82 -6 10 2 269.73 29.44 6 -10 -2 301.69 31.27 6 -10 -1 2.36 3.14 -6 10 1 3.47 5.05 -6 10 0 322.46 30.03 6 -10 0 385.63 32.28 -6 10 -1 8.89 4.68 6 -10 1 21.82 7.17 -6 10 -2 161.19 18.92 6 -10 2 154.74 18.93 6 -10 3 -0.45 0.77 -6 10 -3 0.13 1.43 -6 10 -4 109.53 14.14 6 -10 4 128.38 14.13 6 -10 5 15.52 5.62 -6 11 6 -2.43 3.85 6 -11 -6 -0.30 0.81 -6 11 5 3.10 5.11 6 -11 -5 1.42 2.76 -6 11 4 0.13 2.83 6 -11 -4 -5.41 4.57 -6 11 3 -0.85 1.73 6 -11 -3 0.61 1.33 6 -11 -2 2.38 2.94 -6 11 2 2.01 2.89 6 -11 -1 1.66 2.69 -6 11 1 -0.10 2.66 6 -11 0 -2.09 3.75 -6 11 0 1.41 1.97 6 -11 1 8.31 4.84 -6 11 -1 5.83 3.91 6 -11 2 -1.06 2.83 6 -11 3 0.20 1.74 6 -11 4 0.64 1.45 6 -11 5 28.99 7.09 6 -12 -5 2.66 4.79 6 -12 -4 76.38 18.19 6 -12 -3 0.13 0.70 6 -12 -2 53.55 13.91 6 -12 -1 2.09 3.27 6 -12 0 63.49 13.43 6 -12 1 -0.82 1.98 6 -12 2 102.53 15.36 6 -12 3 5.24 2.84 6 -12 4 208.98 20.56 6 -12 5 2.88 2.40 6 -13 -3 2.03 3.95 6 -13 -2 1.51 1.92 6 -13 -1 2.32 3.07 6 -13 0 -0.21 2.93 6 -13 1 0.97 1.38 6 -13 2 -0.43 1.87 6 -13 3 1.65 3.94 6 -13 4 4.73 4.02 6 -13 5 29.74 6.50 6 -14 -2 55.35 14.84 6 -14 -1 5.51 4.49 6 -14 0 52.15 13.16 6 -14 1 -0.41 2.06 6 -14 2 41.94 10.44 6 -14 3 0.80 1.37 6 -14 4 24.66 7.65 6 -14 5 0.42 2.65 6 -15 -1 6.67 6.72 6 -15 0 -0.36 1.28 6 -15 1 1.29 3.17 6 -15 2 0.29 0.91 6 -15 3 -0.51 3.21 -7 0 13 17.64 9.80 7 0 -13 12.95 4.66 -7 0 12 0.91 3.77 7 0 -12 -4.14 6.59 -7 0 11 78.81 22.54 7 0 -11 17.90 8.61 7 0 -10 -0.38 1.51 -7 0 10 0.28 4.47 7 0 -9 3.54 2.92 -7 0 9 5.42 3.66 -7 0 8 0.39 2.51 7 0 -8 -0.45 1.04 -7 0 7 720.14 53.23 -7 -1 13 -0.16 2.52 7 1 -13 2.67 4.63 7 -1 -12 169.66 26.95 7 1 -12 162.14 26.18 -7 1 12 120.72 24.07 -7 -1 12 133.14 30.61 7 -1 -11 12.36 7.53 -7 1 11 8.33 6.70 7 1 -11 9.51 6.43 -7 -1 11 3.62 5.42 7 -1 -10 534.72 47.14 -7 1 10 553.84 51.00 -7 -1 10 487.85 46.97 -7 -1 9 -0.94 2.89 7 -1 -9 -1.64 2.82 -7 1 9 -0.80 2.16 7 -1 -8 727.45 50.26 -7 1 8 682.85 53.99 -7 1 7 73.99 18.58 7 -1 -7 76.66 16.26 -7 1 5 0.99 4.31 -7 -2 13 6.08 14.03 -7 2 12 -4.62 4.73 7 -2 -12 3.57 3.75 -7 -2 12 0.89 5.68 -7 -2 11 6.47 7.38 -7 2 11 2.19 2.80 7 -2 -11 10.37 7.07 -7 2 10 1.48 2.40 7 -2 -10 0.55 1.05 -7 2 9 0.27 4.98 7 -2 -9 1.17 3.30 7 -2 -8 2.59 3.20 -7 2 8 15.72 15.57 7 -2 -7 183.95 25.33 -7 2 7 153.23 24.73 -7 2 6 2.28 2.25 7 -2 -6 18.58 6.37 -7 2 5 140.21 21.88 7 -2 -5 126.58 20.24 -7 2 4 12.57 6.59 7 -2 -4 4.95 4.97 -7 2 3 -1.19 3.19 -7 -3 14 151.30 29.87 -7 -3 13 -4.26 4.35 -7 3 11 7.24 6.21 7 -3 -11 11.05 7.78 -7 3 10 89.27 20.52 7 -3 -10 74.90 17.79 -7 3 9 76.44 19.35 7 -3 -9 131.76 23.36 -7 3 8 147.74 27.70 7 -3 -8 140.48 24.00 -7 3 7 29.76 11.47 7 -3 -7 32.19 11.16 7 -3 -6 334.00 33.41 -7 3 6 331.45 34.52 -7 3 5 456.97 39.88 -7 3 4 568.23 43.45 -7 3 3 1.34 2.48 7 -3 -3 -0.63 1.87 7 -3 -2 577.39 38.64 -7 3 2 572.99 40.59 -7 3 1 146.77 19.57 7 -4 -11 -8.00 6.76 7 -4 -10 0.45 3.14 -7 4 10 0.62 4.19 7 -4 -9 1.27 3.95 -7 4 9 -0.15 1.81 7 -4 -8 -0.13 2.02 -7 4 8 -0.70 3.64 7 -4 -7 49.08 14.03 -7 4 7 54.60 15.17 7 -4 -6 319.85 33.31 -7 4 6 321.43 35.03 -7 4 5 -0.23 2.38 7 -4 -5 3.24 3.79 -7 4 4 124.79 20.99 7 -4 -4 130.88 21.20 7 -4 -3 100.32 17.29 -7 4 3 95.73 17.24 -7 4 2 0.49 1.41 7 -4 -2 0.26 1.40 7 -4 -1 60.25 12.38 -7 4 1 79.42 14.54 -7 4 0 35.09 9.90 -7 4 -1 162.78 19.50 -7 5 10 89.03 20.70 7 -5 -10 107.86 22.58 -7 5 9 6.80 6.24 7 -5 -9 5.28 5.32 -7 5 8 522.68 49.52 7 -5 -8 579.14 48.11 7 -5 -7 115.07 20.41 -7 5 7 128.58 23.06 -7 5 6 629.93 49.58 7 -5 -6 603.24 46.65 7 -5 -5 3.50 3.76 -7 5 5 9.16 4.88 -7 5 4 879.56 55.57 -7 5 3 7.28 5.79 7 -5 -3 21.29 8.06 7 -5 -2 655.00 43.29 -7 5 2 692.32 45.34 -7 5 1 49.07 11.40 7 -5 -1 44.62 9.81 -7 5 0 878.42 49.01 -7 5 -1 27.07 8.71 -7 5 -2 528.19 35.07 -7 5 -3 22.65 6.67 -7 5 -4 358.19 26.54 -7 5 -5 109.38 14.70 7 -6 -9 -0.78 3.04 -7 6 9 5.89 6.66 7 -6 -8 76.59 18.32 -7 6 8 78.53 18.34 -7 6 7 37.75 11.70 7 -6 -7 33.48 14.23 -7 6 6 -2.19 3.11 7 -6 -6 -1.13 2.14 7 -6 -5 73.19 15.25 -7 6 5 92.80 17.75 7 -6 -4 5.78 4.53 -7 6 4 9.93 4.81 -7 6 3 115.07 20.05 7 -6 -3 114.17 19.50 -7 6 2 47.69 13.13 7 -6 -2 49.47 11.96 7 -6 -1 71.65 14.50 -7 6 1 76.49 15.58 -7 6 0 2.52 1.94 7 -6 0 3.87 4.67 7 -6 1 58.73 11.47 -7 6 -1 73.78 15.92 -7 6 -2 48.59 13.68 -7 6 -3 4.15 2.77 -7 6 -4 154.29 17.37 -7 6 -5 21.91 6.53 -7 6 -6 1.24 3.11 -7 6 -7 37.05 8.35 -7 6 -8 1.00 2.55 -7 6 -9 7.84 3.55 7 -7 -8 174.54 30.45 -7 7 8 207.07 31.76 7 -7 -7 1.86 5.20 -7 7 7 0.28 4.61 7 -7 -6 152.60 25.34 -7 7 6 197.01 28.00 -7 7 5 1.00 2.43 7 -7 -5 0.85 1.61 -7 7 4 260.36 29.55 7 -7 -4 229.57 28.35 7 -7 -3 2.85 2.74 -7 7 3 13.41 6.75 -7 7 2 396.98 35.80 7 -7 -2 459.40 37.30 -7 7 1 80.62 15.65 7 -7 -1 97.84 16.23 7 -7 0 385.20 30.42 -7 7 -1 -0.59 2.18 7 -7 1 0.99 2.55 -7 7 -3 30.72 8.50 -7 7 -5 14.07 6.45 -7 7 -6 126.43 16.80 -7 7 -7 0.47 2.28 -7 7 -8 146.95 15.40 -7 7 -9 2.24 4.07 -7 7 -10 96.43 10.53 -7 7 -11 1.03 1.44 -7 7 -12 82.09 6.62 7 -8 -7 5.51 5.55 -7 8 7 -4.15 4.24 7 -8 -6 -0.28 1.08 -7 8 6 -6.11 4.98 7 -8 -5 16.29 8.18 -7 8 5 4.86 5.86 7 -8 -4 2.74 5.39 -7 8 4 1.45 0.92 7 -8 -3 5.25 5.23 -7 8 3 2.03 2.19 7 -8 -2 5.51 4.55 -7 8 2 2.09 2.65 7 -8 -1 4.44 4.74 -7 8 1 2.44 3.38 7 -8 0 5.70 4.10 -7 8 0 6.02 4.15 -7 8 -1 0.08 2.53 7 -8 1 -0.16 1.56 -7 8 -2 2.51 2.69 7 -8 2 16.46 5.18 7 -8 3 1.59 2.28 -7 8 -3 0.62 2.86 -7 8 -4 7.19 4.83 -7 8 -5 1.57 3.11 -7 8 -6 23.23 6.89 -7 8 -7 3.05 1.38 -7 8 -8 0.55 1.02 -7 8 -9 0.03 0.60 -7 8 -10 -0.68 1.09 7 -9 -7 5.79 9.76 7 -9 -6 94.94 19.05 -7 9 6 77.72 19.35 7 -9 -5 3.71 3.64 -7 9 5 -1.88 4.11 7 -9 -4 104.42 21.09 -7 9 4 102.13 20.48 7 -9 -3 6.65 5.54 -7 9 3 0.70 3.69 -7 9 2 419.25 36.66 7 -9 -2 373.26 35.36 -7 9 1 3.98 4.51 7 -9 -1 0.20 1.41 7 -9 0 135.27 19.26 -7 9 0 159.30 21.37 7 -9 1 3.87 2.82 -7 9 -1 21.86 8.05 7 -9 2 270.58 24.86 -7 9 -2 233.89 23.41 7 -9 3 29.33 7.87 -7 9 -3 35.22 8.36 -7 9 -4 155.39 17.51 -7 9 -5 -0.57 0.43 -7 9 -6 96.96 12.32 -7 9 -7 14.90 4.43 -7 9 -8 50.72 7.81 7 -10 -6 -2.67 5.02 7 -10 -5 -2.04 3.95 -7 10 5 2.68 5.00 7 -10 -4 2.03 3.35 -7 10 4 0.13 2.35 7 -10 -3 3.60 3.85 -7 10 3 0.12 1.47 7 -10 -2 0.23 2.52 -7 10 2 0.11 1.22 -7 10 1 6.77 3.52 7 -10 -1 4.70 5.38 7 -10 0 -0.09 1.35 -7 10 0 -5.95 5.03 7 -10 1 25.96 7.47 -7 10 -1 16.17 6.60 7 -10 2 4.83 3.88 -7 10 -2 0.56 2.21 7 -10 3 63.13 11.59 -7 10 -3 64.17 11.62 -7 10 -4 1.56 2.97 7 -10 4 4.22 2.90 -7 10 -5 44.45 9.04 -7 10 -6 1.91 1.61 7 -11 -5 1.68 3.88 7 -11 -4 108.42 21.71 -7 11 4 108.35 20.79 7 -11 -3 -1.18 3.26 -7 11 3 0.13 2.09 7 -11 -2 136.35 21.86 -7 11 2 86.66 19.27 -7 11 1 0.11 2.07 7 -11 -1 1.42 3.59 -7 11 0 32.27 9.44 7 -11 0 32.06 8.84 7 -11 1 -0.90 3.08 -7 11 -1 5.67 4.60 7 -11 2 104.13 15.61 -7 11 -2 94.65 16.09 -7 11 -3 -0.08 1.44 7 -11 3 -0.73 0.56 7 -11 4 200.92 19.73 -7 11 -4 169.23 18.84 7 -12 -4 16.24 11.14 7 -12 -3 -0.69 3.73 -7 12 3 3.81 3.53 7 -12 -2 1.15 2.92 -7 12 2 1.13 5.69 -7 12 1 -0.23 1.98 7 -12 -1 0.34 0.88 -7 12 0 4.47 4.27 7 -12 0 1.86 4.00 -7 12 -1 1.85 3.87 7 -12 1 8.55 4.13 7 -12 2 -0.09 2.72 7 -12 3 -0.38 2.25 7 -12 4 0.81 1.63 7 -12 5 15.08 5.10 7 -13 -2 38.17 13.84 7 -13 -1 0.73 3.88 7 -13 0 36.66 11.70 7 -13 1 -0.29 1.18 7 -13 2 27.61 9.18 7 -13 3 1.60 3.14 7 -13 4 47.10 10.01 7 -13 5 1.52 1.51 7 -14 -1 5.52 5.37 7 -14 0 -4.03 11.40 7 -14 1 0.41 2.23 7 -14 2 2.13 4.04 7 -14 3 -1.24 2.77 7 -14 4 0.94 0.68 7 -15 0 27.40 11.63 7 -15 1 2.17 3.98 7 -15 2 10.69 6.18 8 0 -11 -0.59 1.12 -8 0 11 0.33 2.18 8 0 -10 245.80 30.63 -8 0 10 212.90 33.31 -8 0 9 2.17 4.44 -8 -1 11 0.17 1.81 8 -1 -10 3.05 3.68 -8 1 10 0.16 3.39 8 -1 -9 -1.23 3.69 -8 1 9 0.16 4.54 -8 1 8 -2.40 1.63 8 -1 -8 0.90 2.42 8 -2 -10 143.57 25.93 -8 2 10 142.20 26.90 8 -2 -9 10.98 7.20 -8 2 9 95.01 26.14 8 -2 -8 473.72 45.24 -8 2 8 457.89 45.82 -8 2 7 19.91 11.03 8 -2 -7 28.34 9.73 -8 2 6 439.78 42.93 -8 2 5 43.75 14.34 8 -3 -9 4.84 5.49 -8 3 9 -3.09 3.73 8 -3 -8 53.47 14.50 -8 3 8 53.67 17.15 8 -3 -7 28.45 10.37 -8 3 7 13.97 7.70 -8 3 6 77.57 18.69 8 -3 -6 66.22 16.59 -8 3 5 23.72 8.98 8 -3 -5 13.86 6.92 -8 3 4 75.42 17.29 8 -3 -4 71.40 16.66 -8 3 3 5.24 5.31 -8 3 2 94.03 17.68 -8 4 9 75.32 19.79 8 -4 -9 74.00 19.74 8 -4 -8 262.77 33.98 -8 4 8 252.01 35.36 -8 4 7 10.29 7.90 8 -4 -7 7.01 5.10 8 -4 -6 237.53 30.86 -8 4 6 232.83 31.51 8 -4 -5 1.47 2.19 -8 4 5 1.91 2.84 8 -4 -4 78.58 15.86 -8 4 4 70.89 16.62 8 -4 -3 227.59 26.88 -8 4 3 257.53 30.34 -8 4 2 544.77 43.25 -8 4 1 58.67 13.58 -8 4 0 417.56 35.62 -8 5 8 2.77 5.36 8 -5 -8 3.97 5.28 -8 5 7 7.21 6.09 8 -5 -7 2.70 4.91 -8 5 6 30.72 12.46 8 -5 -6 41.36 14.63 -8 5 5 2.04 2.44 8 -5 -5 0.75 2.71 8 -5 -4 12.79 8.07 -8 5 4 7.84 6.49 -8 5 3 69.92 18.56 8 -5 -3 22.21 10.09 8 -5 -2 21.00 8.43 -8 5 2 2.89 3.06 8 -5 -1 16.79 7.80 -8 5 1 28.85 9.08 -8 5 0 3.58 4.56 -8 5 -1 57.83 12.71 -8 5 -2 30.41 8.53 -8 5 -3 6.70 4.89 -8 6 7 1.71 3.66 8 -6 -7 -0.59 1.13 8 -6 -6 243.96 32.37 -8 6 6 235.40 31.72 -8 6 5 -0.84 2.01 8 -6 -5 2.96 2.70 -8 6 4 190.30 28.54 8 -6 -4 210.89 28.09 8 -6 -3 45.14 12.37 -8 6 3 40.58 11.74 8 -6 -2 618.44 43.97 -8 6 2 613.53 46.38 8 -6 -1 68.78 13.99 -8 6 1 66.55 14.62 8 -6 0 346.88 30.10 -8 6 0 429.26 35.93 -8 6 -1 32.65 9.62 -8 6 -2 384.17 32.12 -8 6 -3 20.25 7.73 -8 6 -4 158.89 20.20 -8 6 -5 48.86 10.42 -8 6 -6 270.74 25.11 -8 7 7 0.16 1.48 8 -7 -7 5.37 6.75 -8 7 6 1.47 3.29 8 -7 -6 -0.72 3.20 -8 7 5 -1.11 1.99 8 -7 -5 4.98 6.13 -8 7 4 9.66 2.77 8 -7 -4 14.08 6.80 -8 7 3 7.93 6.28 8 -7 -3 5.58 5.10 8 -7 -2 -0.22 1.87 -8 7 2 3.09 3.40 -8 7 1 -0.78 1.34 8 -7 -1 -0.92 2.69 8 -7 0 1.19 2.71 -8 7 0 2.17 2.56 -8 7 -1 42.48 11.77 8 -7 1 42.38 10.65 -8 7 -2 6.29 5.32 -8 7 -3 5.08 4.96 -8 7 -4 7.74 9.48 -8 7 -5 60.24 13.06 -8 7 -6 0.63 4.59 -8 7 -7 6.43 3.22 -8 7 -8 -1.15 1.15 -8 7 -9 -0.49 2.28 -8 7 -10 -1.51 2.66 -8 7 -11 0.04 1.19 -8 8 6 81.66 19.32 8 -8 -6 101.81 20.53 8 -8 -5 0.84 2.72 -8 8 5 -2.30 3.12 8 -8 -4 155.39 25.03 -8 8 4 165.13 26.18 -8 8 3 84.42 17.57 8 -8 -3 88.03 18.18 -8 8 2 192.97 25.51 8 -8 -2 180.73 25.86 -8 8 1 4.49 4.92 8 -8 -1 2.20 3.63 8 -8 0 290.51 28.04 -8 8 0 244.09 28.14 -8 8 -1 0.10 2.54 8 -8 1 -2.32 3.19 -8 8 -2 179.34 22.55 -8 8 -3 95.19 16.09 -8 8 -4 194.42 21.94 -8 8 -5 0.28 0.66 -8 8 -6 66.19 12.78 -8 8 -7 0.81 1.62 -8 8 -8 41.30 8.01 -8 8 -9 0.93 1.60 -8 8 -10 39.83 6.65 -8 8 -11 0.98 1.23 -8 9 5 1.50 4.45 8 -9 -5 -1.16 1.36 8 -9 -4 0.14 0.73 -8 9 4 0.14 2.17 8 -9 -3 2.89 3.52 -8 9 3 11.52 6.53 8 -9 -2 4.32 4.51 -8 9 2 3.37 4.17 8 -9 -1 -1.72 3.07 -8 9 1 0.11 2.26 8 -9 0 16.32 7.60 -8 9 0 21.92 9.28 8 -9 1 33.99 9.93 -8 9 -1 37.67 10.06 8 -9 2 6.16 4.09 -8 9 -2 3.65 2.50 -8 9 -3 7.19 5.27 -8 9 -4 0.60 1.80 -8 9 -5 8.63 5.36 -8 9 -6 2.28 2.17 -8 9 -7 -0.05 0.90 -8 9 -8 19.35 5.95 -8 9 -9 -1.77 1.95 -8 10 4 151.79 25.84 8 -10 -4 176.33 26.91 -8 10 3 -5.84 4.76 8 -10 -3 -3.65 6.23 8 -10 -2 51.70 14.07 -8 10 2 43.86 13.16 8 -10 -1 0.11 1.71 -8 10 1 0.11 0.62 8 -10 0 75.94 14.96 -8 10 0 73.53 16.04 8 -10 1 -1.62 2.82 -8 10 -1 0.88 2.37 -8 10 -2 63.39 13.13 8 -10 2 72.55 12.98 -8 10 -3 0.74 1.53 8 -10 3 0.30 2.04 -8 10 -4 183.73 20.41 -8 10 -5 0.73 1.56 -8 10 -6 101.88 13.58 -8 10 -7 1.01 1.15 -8 11 3 0.97 2.24 8 -11 -3 6.78 5.96 -8 11 2 0.51 3.53 8 -11 -2 0.38 3.60 8 -11 -1 -0.12 0.89 -8 11 1 0.59 0.64 8 -11 0 0.95 2.07 -8 11 0 0.66 1.45 -8 11 -1 0.30 2.49 8 -11 1 3.98 4.40 8 -11 2 3.30 3.23 -8 11 -2 4.69 5.58 8 -11 3 -0.08 0.60 -8 11 -3 -0.84 1.43 -8 11 -4 1.44 1.92 -8 11 -5 2.16 2.50 -8 11 -6 -0.59 1.90 -8 12 2 34.08 12.23 8 -12 -2 34.32 12.28 8 -12 -1 -3.49 5.04 -8 12 1 2.74 4.31 8 -12 0 29.59 10.84 -8 12 0 33.03 10.76 8 -12 1 -0.50 1.72 -8 12 -1 -3.29 3.30 -8 12 -2 30.72 9.21 8 -12 2 27.36 9.19 -8 12 -3 0.96 3.46 8 -12 3 0.90 2.08 -8 12 -4 36.27 8.80 8 -12 4 39.34 10.20 -8 13 1 0.52 2.89 8 -13 -1 -3.25 3.70 8 -13 0 -0.34 3.22 -8 13 0 2.50 3.81 8 -13 1 -0.73 1.70 8 -13 2 -0.85 1.69 8 -13 3 -2.04 2.95 8 -13 4 -0.36 1.62 8 -14 0 24.79 12.17 8 -14 1 0.98 3.05 8 -14 2 17.88 9.07 8 -14 3 0.09 0.82 8 -15 1 -0.78 1.60 9 -2 -8 5.80 5.91 -9 2 7 2.32 5.45 9 -3 -7 0.29 3.40 -9 3 7 2.43 2.90 9 -3 -6 35.95 14.18 -9 3 6 61.70 17.07 -9 3 5 3.93 3.92 -9 3 4 154.42 26.15 -9 4 7 42.58 15.36 9 -4 -7 39.23 13.23 9 -4 -6 14.75 7.82 -9 4 6 38.42 25.55 9 -4 -5 1.05 2.56 -9 4 5 -1.05 2.44 9 -4 -4 3.60 4.03 -9 4 4 2.75 2.92 -9 4 3 48.96 13.49 -9 4 2 1.57 3.67 9 -5 -6 69.18 18.30 -9 5 6 89.70 20.79 -9 5 5 2.12 5.48 9 -5 -5 1.92 4.32 -9 5 4 322.83 39.19 9 -5 -4 194.32 28.36 9 -5 -3 6.42 6.49 -9 5 3 5.64 5.43 -9 5 2 122.52 21.59 -9 5 1 25.65 9.52 -9 5 0 257.63 31.31 -9 5 -1 -0.11 2.76 9 -6 -6 19.82 12.46 9 -6 -5 13.42 6.41 -9 6 5 4.56 5.95 -9 6 4 2.07 4.00 9 -6 -4 -2.67 4.62 9 -6 -3 -0.24 0.94 -9 6 3 3.48 5.00 -9 6 2 0.77 3.16 9 -6 -2 4.00 5.39 -9 6 1 58.74 18.98 -9 6 0 0.11 2.31 -9 6 -1 3.08 3.21 -9 6 -2 -0.10 3.04 -9 6 -3 6.12 4.24 -9 6 -4 19.88 7.80 -9 7 5 1.44 1.50 9 -7 -5 0.15 1.13 9 -7 -4 149.38 24.21 -9 7 4 163.14 26.73 -9 7 3 44.89 13.10 9 -7 -3 57.03 14.14 9 -7 -2 130.74 21.52 -9 7 2 113.62 22.17 -9 7 1 1.01 1.92 9 -7 -1 14.94 7.80 -9 7 0 153.93 23.02 -9 7 -1 0.76 1.55 -9 7 -2 117.13 22.55 -9 7 -3 31.32 12.24 -9 7 -4 159.99 21.18 -9 7 -5 -1.01 2.44 -9 7 -6 179.15 21.11 -9 7 -7 1.62 2.67 -9 8 4 -0.15 1.60 9 -8 -4 4.54 4.41 9 -8 -3 19.12 9.78 -9 8 3 2.94 2.01 -9 8 2 11.99 7.38 9 -8 -2 16.43 8.67 9 -8 -1 9.85 5.81 -9 8 1 3.80 4.28 -9 8 0 10.13 5.58 9 -8 0 10.57 6.47 -9 8 -1 25.43 9.71 -9 8 -2 1.45 3.76 -9 8 -3 28.56 9.25 -9 8 -4 1.26 1.61 -9 8 -5 0.83 1.00 -9 8 -6 11.27 5.11 -9 8 -7 2.51 1.46 -9 8 -8 29.80 8.55 -9 8 -9 0.06 1.99 -9 8 -10 0.05 1.18 9 -9 -3 0.27 2.45 -9 9 3 0.14 0.78 9 -9 -2 112.65 21.74 -9 9 2 122.57 22.05 -9 9 1 -0.12 0.67 9 -9 -1 1.78 2.49 -9 9 0 102.09 20.08 9 -9 0 91.90 17.93 -9 9 -1 -0.11 2.02 9 -9 1 -0.68 0.75 -9 9 -2 155.58 22.58 -9 9 -3 11.23 5.97 -9 9 -4 116.63 17.54 -9 9 -5 5.03 4.42 -9 9 -6 57.17 12.86 -9 9 -7 -0.13 2.15 -9 9 -8 15.44 6.09 9 -10 -3 6.34 8.58 9 -10 -2 -0.13 1.58 -9 10 2 3.36 3.21 9 -10 -1 2.45 4.13 -9 10 1 -1.56 2.54 9 -10 0 5.91 5.72 -9 10 0 0.12 2.51 9 -10 1 -0.30 2.65 -9 10 -1 0.67 3.93 -9 10 -2 0.10 0.78 -9 10 -3 1.88 2.60 -9 10 -4 5.60 4.73 -9 10 -5 1.50 2.63 -9 10 -6 1.28 1.76 -9 10 -7 0.25 1.42 9 -11 -2 41.90 13.59 -9 11 2 45.63 14.03 -9 11 1 -3.23 5.41 9 -11 -1 0.12 0.95 9 -11 0 23.46 10.13 -9 11 0 8.02 5.53 -9 11 -1 0.99 2.32 9 -11 1 -0.42 2.51 9 -11 2 41.64 11.56 -9 11 -2 34.38 9.11 -9 11 -3 -1.21 2.75 -9 11 -4 5.56 3.59 -9 11 -5 1.75 2.81 -9 11 -6 13.88 4.45 9 -12 -1 -2.06 3.18 -9 12 1 1.74 3.96 -9 12 0 1.48 3.65 9 -12 0 -1.79 3.70 9 -12 1 0.11 1.44 -9 12 -1 -5.91 4.43 9 -12 2 1.25 2.01 -9 12 -2 1.25 4.87 -9 12 -3 -1.61 3.33 -9 12 -4 -1.29 2.13 -9 13 0 15.96 9.34 9 -13 0 27.93 10.32 9 -13 1 -0.34 4.78 -9 13 -1 -3.29 4.72 -9 13 -2 13.70 6.85 9 -13 2 14.88 6.74 9 -13 3 -0.70 1.96 9 -14 1 2.52 3.62 -10 4 4 66.03 18.68 -10 5 4 5.37 4.67 -10 5 3 2.17 3.94 -10 5 2 -1.49 2.42 -10 6 3 0.46 4.05 -10 6 2 168.60 28.86 -10 6 1 0.82 1.82 -10 6 0 17.46 8.85 -10 6 -1 0.13 1.94 10 -7 -3 15.32 7.20 -10 7 3 15.95 9.64 -10 7 2 -3.76 4.81 -10 7 1 0.28 1.53 -10 7 0 5.24 6.21 -10 7 -1 56.52 17.15 -10 7 -2 8.26 15.41 -10 7 -3 -2.82 2.99 -10 7 -4 0.73 1.86 10 -8 -2 36.23 11.62 -10 8 2 48.12 15.73 -10 8 1 5.01 4.77 -10 8 0 163.71 26.11 -10 8 -1 3.27 3.60 -10 8 -2 138.20 23.15 -10 8 -3 8.92 5.39 -10 8 -4 113.44 18.64 -10 8 -5 3.73 4.48 -10 8 -6 44.55 12.33 -10 8 -7 2.83 4.19 -10 9 1 -0.14 2.47 10 -9 -1 -0.13 1.52 -10 9 0 0.78 3.23 -10 9 -1 12.98 7.35 -10 9 -2 3.57 4.70 -10 9 -3 11.64 7.74 -10 9 -4 5.45 5.06 -10 9 -5 7.04 4.54 -10 9 -6 0.60 0.93 -10 9 -7 0.63 1.13 10 -10 -1 1.03 0.70 -10 10 1 -8.31 5.85 -10 10 0 51.67 14.48 10 -10 0 58.84 14.33 -10 10 -1 0.25 2.81 -10 10 -2 37.88 12.16 -10 10 -3 1.58 3.37 -10 10 -4 31.68 10.10 -10 10 -5 0.89 3.46 -10 10 -6 5.86 5.28 10 -11 0 0.84 1.60 -10 11 0 -1.32 3.92 10 -11 1 1.11 3.12 -10 11 -1 0.25 1.62 -10 11 -2 0.57 2.81 -10 11 -3 0.10 1.49 -10 11 -4 -0.48 1.86 10 -12 1 1.70 3.35 -10 12 -1 -0.74 2.75 -10 12 -2 16.66 9.21 -10 12 -3 3.94 4.42 -11 7 0 120.68 27.42 -11 7 -1 36.57 18.22 -11 8 -1 0.14 1.87 -11 8 -2 -0.13 4.07 -11 8 -3 3.74 4.91 -11 9 -1 0.14 3.24 -11 9 -2 37.41 11.72 -11 9 -3 0.99 5.35 -11 9 -4 15.44 7.53 -11 9 -5 -2.14 3.05 -11 9 -6 1.09 2.93 -11 10 -2 0.13 1.52 -11 10 -3 2.58 2.10 -11 10 -4 0.11 3.21 -11 11 -2 44.70 13.17 -11 11 -3 -1.06 1.91 0 0 0 0.00 0.00 TITL EtaKCrD_c6_f2_76_R10_RO in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 0.41115 8.049763 9.904915 12.453413 90.0000 90.0982 90.0000 ZERR 2.00 0.000627 0.000804 0.000592 0.0000 0.0056 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O K Cr UNIT 20.00 44.00 4.00 24.00 2.00 2.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 9385 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cr1 Cr 0.500000 0.500000 0.500000 0.0286(2) Uani 1 2 d S . P . . K1 K 0.500000 0.500000 1.000000 0.0341(3) Uani 1 2 d S . P . . C1 C 0.7769(5) 0.3109(4) 0.4770(3) 0.0437(9) Uani 1 1 d . U . . . H1 H 0.743074 0.277379 0.543170 0.052 Uiso 1 1 calc R U . . . C2 C 0.2945(5) 0.2626(4) 0.5429(3) 0.0439(9) Uani 1 1 d . U . . . H2 H 0.222727 0.298520 0.491766 0.053 Uiso 1 1 calc R U . . . C3 C 0.5770(6) 0.5268(5) 0.7282(3) 0.0488(10) Uani 1 1 d . U . . . H3 H 0.469833 0.494386 0.738720 0.059 Uiso 1 1 calc R U . . . O1 O 0.6967(3) 0.4095(3) 0.43908(19) 0.0397(6) Uani 1 1 d . U . . . O2 O 0.8976(4) 0.2548(3) 0.4333(2) 0.0546(9) Uani 1 1 d . U . . . O3 O 0.4239(3) 0.3290(3) 0.56494(19) 0.0397(6) Uani 1 1 d . U . . . O4 O 0.2561(5) 0.1538(4) 0.5839(3) 0.0615(9) Uani 1 1 d . U . . . O5 O 0.6277(3) 0.5370(3) 0.63157(18) 0.0387(6) Uani 1 1 d . U . . . O6 O 0.6574(5) 0.5560(4) 0.8081(2) 0.0592(9) Uani 1 1 d . U . . . N1 N 1.0021(5) 0.3998(5) 0.2487(3) 0.0493(9) Uani 1 1 d . U . . . H1A H 0.985170 0.350680 0.307560 0.074 Uiso 1 1 calc R U . . . H1B H 1.108778 0.395244 0.230368 0.074 Uiso 1 1 calc R U . . . H1C H 0.939765 0.367873 0.195387 0.074 Uiso 1 1 calc R U . . . C4 C 0.9562(8) 0.5434(7) 0.2704(6) 0.0735(17) Uani 1 1 d . U . . . H4A H 0.838759 0.548259 0.287222 0.088 Uiso 1 1 calc R U . . . H4B H 1.017562 0.575232 0.332534 0.088 Uiso 1 1 calc R U . . . C5 C 0.9907(13) 0.6305(11) 0.1804(11) 0.131(4) Uani 1 1 d . U . . . H5A H 0.937793 0.595195 0.117180 0.196 Uiso 1 1 calc R U . . . H5B H 1.108517 0.634968 0.169020 0.196 Uiso 1 1 calc R U . . . H5C H 0.948789 0.719374 0.194918 0.196 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cr1 0.0249(5) 0.0328(5) 0.0280(3) 0.0016(2) -0.0003(3) -0.00047(19) K1 0.0339(7) 0.0357(7) 0.0328(4) -0.0002(3) 0.0028(5) 0.0018(3) C1 0.037(3) 0.049(3) 0.0456(16) 0.0106(16) 0.0016(18) 0.0069(13) C2 0.041(3) 0.046(3) 0.0440(16) 0.0065(15) -0.0044(18) -0.0073(13) C3 0.038(3) 0.077(3) 0.0319(14) 0.0032(16) -0.0011(17) -0.0055(17) O1 0.0350(19) 0.0441(18) 0.0402(11) 0.0036(10) 0.0051(12) 0.0058(9) O2 0.045(2) 0.053(2) 0.0659(16) 0.0128(14) 0.0123(17) 0.0155(12) O3 0.0362(18) 0.0390(18) 0.0438(12) 0.0062(10) -0.0013(12) -0.0053(8) O4 0.057(2) 0.057(2) 0.0700(18) 0.0151(16) -0.0097(18) -0.0255(14) O5 0.0336(17) 0.0513(18) 0.0312(10) 0.0006(10) -0.0034(11) -0.0023(10) O6 0.044(2) 0.099(3) 0.0348(12) -0.0059(14) -0.0012(15) -0.0045(15) N1 0.044(3) 0.054(3) 0.0498(17) 0.0045(13) -0.0033(19) -0.0068(12) C4 0.055(4) 0.064(4) 0.102(4) -0.004(3) 0.016(4) 0.001(2) C5 0.107(8) 0.091(7) 0.195(9) 0.067(7) -0.030(7) -0.008(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C -0.0001 0.0005 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0006 0.0010 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0018 0.0018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.0805 0.0845 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.1612 0.2219 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O5 Cr1 O5 180.0 . 3_666 ? O5 Cr1 O1 89.21(12) . . ? O5 Cr1 O1 90.79(12) 3_666 . ? O5 Cr1 O1 90.79(12) . 3_666 ? O5 Cr1 O1 89.21(12) 3_666 3_666 ? O1 Cr1 O1 180.0 . 3_666 ? O5 Cr1 O3 88.90(11) . . ? O5 Cr1 O3 91.10(11) 3_666 . ? O1 Cr1 O3 90.99(11) . . ? O1 Cr1 O3 89.01(11) 3_666 . ? O5 Cr1 O3 91.10(11) . 3_666 ? O5 Cr1 O3 88.90(11) 3_666 3_666 ? O1 Cr1 O3 89.01(11) . 3_666 ? O1 Cr1 O3 90.99(11) 3_666 3_666 ? O3 Cr1 O3 180.0 . 3_666 ? O6 K1 O6 180.00(14) . 3_667 ? O6 K1 O4 95.43(11) . 4_666 ? O6 K1 O4 84.57(11) 3_667 4_666 ? O6 K1 O4 84.57(11) . 2_556 ? O6 K1 O4 95.43(11) 3_667 2_556 ? O4 K1 O4 180.0 4_666 2_556 ? O6 K1 O2 86.56(10) . 2_656 ? O6 K1 O2 93.44(10) 3_667 2_656 ? O4 K1 O2 99.60(12) 4_666 2_656 ? O4 K1 O2 80.40(12) 2_556 2_656 ? O6 K1 O2 93.44(10) . 4_566 ? O6 K1 O2 86.56(10) 3_667 4_566 ? O4 K1 O2 80.40(12) 4_666 4_566 ? O4 K1 O2 99.60(12) 2_556 4_566 ? O2 K1 O2 180.0 2_656 4_566 ? O6 K1 C3 161.22(12) . 3_667 ? O6 K1 C3 18.78(11) 3_667 3_667 ? O4 K1 C3 73.88(10) 4_666 3_667 ? O4 K1 C3 106.12(10) 2_556 3_667 ? O2 K1 C3 80.24(10) 2_656 3_667 ? O2 K1 C3 99.76(10) 4_566 3_667 ? O6 K1 C3 18.78(11) . . ? O6 K1 C3 161.22(12) 3_667 . ? O4 K1 C3 106.12(10) 4_666 . ? O4 K1 C3 73.88(10) 2_556 . ? O2 K1 C3 99.76(10) 2_656 . ? O2 K1 C3 80.24(10) 4_566 . ? C3 K1 C3 180.00(16) 3_667 . ? O2 C1 O1 125.5(3) . . ? O2 C1 H1 117.2 . . ? O1 C1 H1 117.2 . . ? O4 C2 O3 125.0(4) . . ? O4 C2 H2 117.5 . . ? O3 C2 H2 117.5 . . ? O6 C3 O5 125.5(4) . . ? O6 C3 K1 46.77(18) . . ? O5 C3 K1 171.7(3) . . ? O6 C3 H3 117.3 . . ? O5 C3 H3 117.3 . . ? K1 C3 H3 70.6 . . ? C1 O1 Cr1 128.2(2) . . ? C1 O2 K1 120.4(2) . 2_646 ? C2 O3 Cr1 127.9(3) . . ? C2 O4 K1 120.8(3) . 2_546 ? C3 O5 Cr1 127.1(3) . . ? C3 O6 K1 114.4(3) . . ? C4 N1 H1A 109.5 . . ? C4 N1 H1B 109.5 . . ? H1A N1 H1B 109.5 . . ? C4 N1 H1C 109.5 . . ? H1A N1 H1C 109.5 . . ? H1B N1 H1C 109.5 . . ? C5 C4 N1 112.4(6) . . ? C5 C4 H4A 109.1 . . ? N1 C4 H4A 109.1 . . ? C5 C4 H4B 109.1 . . ? N1 C4 H4B 109.1 . . ? H4A C4 H4B 107.9 . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cr1 O5 1.967(3) . ? Cr1 O5 1.967(3) 3_666 ? Cr1 O1 1.973(2) . ? Cr1 O1 1.973(2) 3_666 ? Cr1 O3 1.975(3) . ? Cr1 O3 1.975(3) 3_666 ? K1 O6 2.763(2) . ? K1 O6 2.763(2) 3_667 ? K1 O4 2.767(3) 4_666 ? K1 O4 2.767(3) 2_556 ? K1 O2 2.782(3) 2_656 ? K1 O2 2.782(3) 4_566 ? K1 C3 3.452(3) 3_667 ? K1 C3 3.452(3) . ? C1 O2 1.246(4) . ? C1 O1 1.261(5) . ? C1 H1 0.9300 . ? C2 O4 1.232(5) . ? C2 O3 1.261(5) . ? C2 H2 0.9300 . ? C3 O6 1.221(6) . ? C3 O5 1.276(4) . ? C3 H3 0.9300 . ? N1 C4 1.495(8) . ? N1 H1A 0.8900 . ? N1 H1B 0.8900 . ? N1 H1C 0.8900 . ? C4 C5 1.442(11) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C5 H5A 0.9600 . ? C5 H5B 0.9600 . ? C5 H5C 0.9600 . ?