#------------------------------------------------------------------------------ #$Date: 2020-03-27 03:33:39 +0200 (Fri, 27 Mar 2020) $ #$Revision: 249762 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/76/1557663.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557663 loop_ _publ_author_name 'Chen, Xue' 'Liu, Zheng-Fei' 'Jin, Wei Jun' _publ_section_title ; The Effect of Electron Donation and Intermolecular Interactions on Ultralong Phosphorescence Lifetime of 4-Carnoyl Phenylboronic Acids. ; _journal_name_full 'The journal of physical chemistry. A' _journal_paper_doi 10.1021/acs.jpca.9b11943 _journal_year 2020 _chemical_formula_moiety 'C8 H10 B N O3' _chemical_formula_sum 'C8 H10 B N O3' _chemical_formula_weight 179.00 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_Int_Tables_number 14 _atom_sites_solution_primary direct _audit_creation_date 2020-02-17 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 98.767(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 4.98445(16) _cell_length_b 24.1243(7) _cell_length_c 7.0635(2) _cell_measurement_reflns_used 2743 _cell_measurement_temperature 100.0(3) _cell_measurement_theta_max 71.7020 _cell_measurement_theta_min 6.5770 _cell_volume 839.44(4) _computing_cell_refinement 'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.0(3) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.3127 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.9818 _diffrn_measured_fraction_theta_max 0.9818 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -86.00 -11.00 1.00 1.40 -- -41.49 125.00 0.00 75 2 \w -114.00 -60.00 1.00 1.40 -- -41.49 -37.00-150.00 54 3 \w -61.00 29.00 1.00 1.40 -- -41.49 57.00 -60.00 90 4 \w 23.00 118.00 1.00 1.40 -- 41.49 77.00 150.00 95 5 \w 73.00 124.00 1.00 5.61 -- 104.69 -61.00 -60.00 51 6 \w 25.00 50.00 1.00 5.61 -- 104.69 -94.00 90.00 25 7 \w 86.00 134.00 1.00 5.61 -- 104.69 -61.00 60.00 48 8 \w 78.00 112.00 1.00 5.61 -- 104.69-125.00 90.00 34 9 \w 96.00 178.00 1.00 5.61 -- 104.69 125.00 -30.00 82 10 \w 53.00 118.00 1.00 5.61 -- 104.69-125.00 -60.00 65 11 \w 40.00 131.00 1.00 5.61 -- 104.69 -45.00-120.00 91 12 \w 76.00 146.00 1.00 5.61 -- 104.69 30.00 150.00 70 13 \w 35.00 80.00 1.00 5.61 -- 104.69 -61.00 60.00 45 14 \w 81.00 107.00 1.00 5.61 -- 104.69 -94.00 90.00 26 15 \w 37.00 71.00 1.00 5.61 -- 104.69 -30.00-180.00 34 16 \w 97.00 127.00 1.00 5.61 -- 104.69 -30.00-180.00 30 17 \w 150.00 178.00 1.00 5.61 -- 104.69 125.00 90.00 28 18 \w 77.00 178.00 1.00 5.61 -- 104.69 30.00 60.00 101 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.3080908000 _diffrn_orient_matrix_UB_12 0.0062694000 _diffrn_orient_matrix_UB_13 0.0636604000 _diffrn_orient_matrix_UB_21 -0.0489496000 _diffrn_orient_matrix_UB_22 0.0117092000 _diffrn_orient_matrix_UB_23 0.2064074000 _diffrn_orient_matrix_UB_31 0.0216160000 _diffrn_orient_matrix_UB_32 -0.0624703000 _diffrn_orient_matrix_UB_33 0.0450728000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0354 _diffrn_reflns_av_unetI/netI 0.0329 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 5239 _diffrn_reflns_theta_full 71.9548 _diffrn_reflns_theta_max 71.95 _diffrn_reflns_theta_min 3.66 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.883 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.83616 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46e (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_density_diffrn 1.4161 _exptl_crystal_description needle _exptl_crystal_F_000 377.3510 _exptl_crystal_size_max 0.9 _exptl_crystal_size_mid 0.6 _exptl_crystal_size_min 0.3 _refine_diff_density_max 0.3539 _refine_diff_density_min -0.2941 _refine_diff_density_rms 0.0517 _refine_ls_d_res_high 0.8108 _refine_ls_d_res_low 12.0622 _refine_ls_goodness_of_fit_ref 1.0645 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 18 _refine_ls_number_parameters 121 _refine_ls_number_reflns 1620 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0645 _refine_ls_R_factor_all 0.0407 _refine_ls_R_factor_gt 0.0360 _refine_ls_shift/su_max 0.0000 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0409P)^2^+0.3488P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0917 _refine_ls_wR_factor_ref 0.0948 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 5 _reflns_limit_h_min -6 _reflns_limit_k_max 29 _reflns_limit_k_min 0 _reflns_limit_l_max 8 _reflns_limit_l_min 0 _reflns_number_gt 1453 _reflns_number_total 1620 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL 20190601a_a.res in P2(1)/c REM Old TITL 20190601a in P21/c #14 REM SHELXT solution in P2(1)/c REM R1 0.104, Rweak 0.161, Alpha 0.018, Orientation as input REM Formula found by SHELXT: C8 N O3 CELL 1.54184 4.984451 24.124343 7.063539 90 98.7668 90 ZERR 4 0.000156 0.000649 0.000196 0 0.0027 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H B N O UNIT 32 40 4 4 12 L.S. 4 PLAN 5 BOND $H LIST 6 fmap 2 MORE -1 CONF ACTA WGHT 0.040892 0.348784 FVAR 0.941778 REM REM REM O1 5 0.29632 0.53806 0.12432 11.00000 0.01160 0.02305 0.01292 = -0.00420 0.00182 0.00080 AFIX 147 H1 2 0.16666 0.54428 0.18000 11.00000 -1.50000 AFIX 0 O2 5 0.76777 0.52755 0.19606 11.00000 0.01354 0.02438 0.01401 = -0.00694 0.00092 -0.00050 AFIX 147 H2 2 0.73269 0.50780 0.10102 11.00000 -1.50000 AFIX 0 O3 5 0.32898 0.68541 1.01470 11.00000 0.01292 0.03246 0.01895 = -0.00871 0.00378 0.00002 N1 4 0.78589 0.68148 1.07388 11.00000 0.01347 0.01948 0.01196 = -0.00369 0.00164 0.00087 AFIX 43 H1a 2 0.93218 0.66804 1.04158 11.00000 -1.20000 AFIX 0 C3 1 0.55291 0.63814 0.78585 11.00000 0.01458 0.01590 0.01174 = -0.00063 0.00313 -0.00322 C6 1 0.54029 0.58016 0.43908 11.00000 0.01296 0.01657 0.01193 = 0.00029 0.00248 -0.00230 C7 1 0.54662 0.67003 0.96846 11.00000 0.01420 0.01635 0.01279 = 0.00083 0.00262 -0.00075 C4 1 0.75814 0.60080 0.76343 11.00000 0.01423 0.01839 0.01209 = 0.00094 -0.00021 -0.00032 AFIX 43 H4 2 0.89995 0.59494 0.86325 11.00000 -1.20000 AFIX 0 C2 1 0.34166 0.64685 0.63497 11.00000 0.01332 0.01816 0.01590 = -0.00113 0.00224 0.00190 AFIX 43 H2a 2 0.20418 0.67191 0.64877 11.00000 -1.20000 AFIX 0 C1 1 0.33675 0.61806 0.46412 11.00000 0.01350 0.02020 0.01295 = 0.00002 -0.00074 0.00040 AFIX 43 H1b 2 0.19507 0.62416 0.36439 11.00000 -1.20000 AFIX 0 C5 1 0.75150 0.57219 0.59167 11.00000 0.01432 0.01677 0.01411 = -0.00031 0.00229 0.00141 AFIX 43 H5 2 0.88984 0.54732 0.57800 11.00000 -1.20000 AFIX 0 C8 1 0.80138 0.71653 1.24318 11.00000 0.01883 0.02180 0.01488 = -0.00540 0.00074 -0.00005 AFIX 137 H8a 2 0.69868 0.74980 1.21136 11.00000 -1.50000 H8b 2 0.72821 0.69696 1.34208 11.00000 -1.50000 H8c 2 0.98747 0.72593 1.28765 11.00000 -1.50000 AFIX 0 B1 3 0.53274 0.54735 0.24650 11.00000 0.01375 0.01564 0.01223 = 0.00143 0.00165 -0.00064 HKLF 4 END Q1 1 0.933333 0.686667 1 11 0.05 0.35 Q2 1 0.533333 0.56 0.333333 11 0.05 0.26 Q3 1 0.466667 0.646667 0.708333 11 0.05 0.21 Q4 1 0.666667 0.58 0.5 11 0.05 0.19 Q5 1 0.133333 0.673333 1 11 0.05 0.19 Q6 1 0.066667 0.54 0.125 11 0.05 0.18 Q7 1 0.6 0.66 0.875 11 0.05 0.17 Q8 1 0.6 0.613333 0.791667 11 0.05 0.16 Q9 1 0.8 0.7 1.166667 11 0.05 0.16 Q10 1 0.866667 0.486667 0.333333 11 0.05 0.15 Q11 1 0.733333 0.593333 0.666667 11 0.05 0.15 Q12 1 -0.133333 0.653333 0.666667 11 0.05 0.15 Q13 1 0.4 0.586667 0.458333 11 0.05 0.14 Q14 1 0.133333 0.533333 0 11 0.05 0.14 Q15 1 0.4 0.706667 1.25 11 0.05 0.14 Q16 1 0.333333 0.626667 0.541667 11 0.05 0.14 Q17 1 0.666667 0.686667 1 11 0.05 0.13 Q18 1 0.066667 0.586667 0.458333 11 0.05 0.13 Q19 1 0.333333 0.593333 0.083333 11 0.05 0.12 Q20 1 0.866667 0.606667 0.958333 11 0.05 0.12 REM The information below was added by Olex2. REM REM R1 = 0.0360 for 1453 Fo > 4sig(Fo) and 0.0407 for all 1620 data REM 121 parameters refined using 0 restraints REM Highest difference peak 0.3539, deepest hole -0.2941 REM Mean Shift 0.0000, Max Shift 0.0000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0407 REM R1_gt = 0.0360 REM wR_ref = 0.0948 REM GOOF = 1.0645 REM Shift_max = 0.0000 REM Shift_mean = 0.0000 REM Reflections_all = 1620 REM Reflections_gt = 1453 REM Parameters = 121 REM Hole = -0.2941 REM Peak = 0.3539 REM Flack = n/a ; _cod_data_source_file jp9b11943_si_005.cif _cod_data_source_block 20190601a _cod_database_code 1557663 _chemical_oxdiff_formula C1H1N1O1B1 _reflns_odcompleteness_completeness 99.94 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: N1(H1a), C4(H4), C2(H2a), C1(H1b), C5(H5) 2.b Idealised Me refined as rotating group: C8(H8a,H8b,H8c) 2.c Idealised tetrahedral OH refined as rotating group: O1(H1), O2(H2) ; _iucr_refine_fcf_details ; data_20190601a _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_Int_Tables_number 14 _cell_length_a 4.98445(16) _cell_length_b 24.1243(7) _cell_length_c 7.0635(2) _cell_angle_alpha 90 _cell_angle_beta 98.767(3) _cell_angle_gamma 90 _cell_volume 839.44(4) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -6 1 3 1.546 1.749 1.246 259.992 o -6 2 3 4.087 4.803 1.026 212.520 o -5 0 2 289.584 325.330 13.563 1.249 o -5 0 4 95.513 102.904 6.314 6.116 o -5 0 6 33.461 27.544 2.153 31.889 o -5 1 1 0.918 2.187 1.236 275.811 o -5 1 2 97.298 108.716 9.645 3.790 o -5 1 3 3.418 4.421 1.327 178.100 o -5 1 4 196.834 197.337 6.536 3.125 o -5 1 5 0.921 3.184 0.991 350.549 o -5 1 6 6.590 5.085 1.082 164.126 o -5 2 1 10.027 10.818 1.377 97.300 o -5 2 2 1.735 2.912 2.120 105.102 o -5 2 3 0.846 3.783 1.459 198.801 o -5 2 4 132.623 133.364 5.094 5.412 o -5 2 5 230.729 223.676 7.836 2.414 o -5 2 6 56.848 54.197 3.134 15.933 o -5 3 1 368.527 412.893 9.145 1.190 o -5 3 2 103.287 109.912 6.274 5.814 o -5 3 3 261.335 265.848 8.164 2.012 o -5 3 4 38.475 39.496 2.608 24.105 o -5 3 5 127.310 134.871 10.395 3.035 o -5 3 6 31.149 30.182 2.277 31.435 o -5 4 1 884.303 954.655 17.429 0.276 o -5 4 2 20.137 26.992 1.900 44.900 o -5 4 3 428.582 423.396 12.588 0.900 o -5 4 4 73.140 75.407 3.582 11.542 o -5 4 5 7.849 8.952 3.078 44.246 o -5 5 1 226.270 239.753 7.640 2.418 o -5 5 2 178.709 178.031 5.075 3.900 o -5 5 3 14.623 11.505 1.625 71.667 o -5 5 4 43.900 47.984 2.379 22.155 o -5 5 5 4.299 5.178 1.173 182.951 o -5 6 1 127.344 143.064 4.508 5.742 o -5 6 2 21.502 19.329 1.599 52.351 o -5 6 3 5.583 6.156 0.964 183.681 o -5 6 4 10.526 9.161 1.060 114.653 o -5 6 5 188.421 178.072 7.678 3.050 o -5 7 1 56.135 61.164 2.563 17.048 o -5 7 2 1.254 1.264 0.781 524.446 o -5 7 3 4.826 2.479 0.789 267.400 o -5 7 4 3.392 2.978 1.315 191.186 o -5 7 5 8.994 11.162 1.804 81.014 o -5 8 1 42.368 44.840 2.471 22.683 o -5 8 2 5.709 5.642 1.026 178.302 o -5 8 3 38.543 33.727 1.858 29.594 o -5 8 4 42.353 46.366 2.340 23.047 o -5 8 5 59.587 59.868 3.642 13.763 o -5 9 1 51.968 50.388 3.845 14.831 o -5 9 2 695.300 685.530 11.310 0.471 o -5 9 3 150.172 154.092 5.262 4.635 o -5 9 4 37.430 41.553 1.886 28.097 o -5 9 5 48.449 51.751 3.157 17.573 o -5 10 1 6.670 5.832 1.679 107.713 o -5 10 2 3.924 9.811 1.242 150.813 o -5 10 3 586.552 605.548 12.548 0.579 o -5 10 4 10.810 12.260 1.455 87.902 o -5 11 1 9.228 10.104 1.616 90.549 o -5 11 2 69.430 64.463 3.572 12.501 o -5 11 3 157.347 166.259 4.465 4.637 o -5 11 4 44.771 35.126 1.897 26.260 o -5 12 1 146.866 161.594 6.477 4.130 o -5 12 2 4.528 7.410 1.360 144.469 o -5 12 3 0.244 0.951 1.533 218.742 o -5 12 4 52.627 42.956 2.965 18.302 o -5 13 1 181.080 189.646 6.526 3.374 o -5 13 2 123.534 117.929 4.753 6.137 o -5 13 3 1.284 0.707 1.150 323.096 o -5 13 4 60.226 48.876 3.022 16.137 o -5 14 1 21.489 25.833 2.159 40.696 o -5 14 2 15.566 13.033 1.555 69.599 o -5 14 3 6.446 6.096 1.488 122.731 o -5 15 1 62.744 59.351 3.099 14.716 o -5 15 2 30.657 37.672 3.456 21.804 o -5 15 3 10.607 11.485 1.291 97.231 o -5 16 1 29.510 22.050 1.810 39.580 o -5 16 2 25.274 25.756 1.843 41.269 o -5 17 1 2.563 1.894 0.795 378.155 o -5 17 2 169.562 162.479 6.404 3.772 o -4 0 2 18.909 25.117 2.344 40.673 o -4 0 4 0.626 3.446 1.342 234.442 o -4 0 6 1273.020 1281.040 37.804 0.120 o -4 1 1 275.521 286.218 6.474 2.044 o -4 1 2 57.791 47.090 2.489 18.352 o -4 1 3 2.930 1.119 0.697 421.735 o -4 1 4 109.374 107.759 3.503 7.867 o -4 1 5 267.731 276.165 5.982 2.182 o -4 1 6 7.220 11.360 1.432 106.501 o -4 1 7 5.347 4.485 0.852 217.482 o -4 2 1 44.030 46.965 2.076 23.552 o -4 2 2 6.929 6.143 0.807 180.555 o -4 2 3 14.585 19.047 2.152 51.642 o -4 2 4 78.946 74.333 2.863 12.186 o -4 2 5 321.762 319.549 6.552 1.684 o -4 2 6 31.298 31.749 1.831 34.494 o -4 2 7 7.258 8.236 0.988 148.209 o -4 3 1 101.563 98.639 3.071 8.969 o -4 3 2 65.047 58.169 2.645 15.534 o -4 3 3 85.164 74.831 2.882 11.486 o -4 3 4 23.655 25.304 1.709 44.642 o -4 3 5 1.659 3.251 1.013 306.576 o -4 3 6 0.489 2.790 0.868 461.667 o -4 3 7 0.084 0.789 0.599 1172.800 o -4 4 1 383.397 368.204 7.401 1.293 o -4 4 2 49.001 62.360 2.483 18.622 o -4 4 3 253.430 244.856 5.690 2.451 o -4 4 4 22.018 24.937 1.631 47.645 o -4 4 5 72.266 73.212 3.127 12.551 o -4 4 6 394.604 394.357 11.255 1.050 o -4 4 7 1.631 2.108 1.026 327.482 o -4 5 1 421.823 428.494 7.030 1.106 o -4 5 2 666.115 683.592 10.186 0.504 o -4 5 3 204.838 211.718 5.190 3.224 o -4 5 4 1.334 2.151 0.770 475.848 o -4 5 5 62.661 72.898 3.117 13.754 o -4 5 6 30.275 29.303 1.693 37.194 o -4 5 7 232.015 230.048 8.580 2.260 o -4 6 1 12.490 11.866 1.052 97.662 o -4 6 2 117.977 118.522 4.131 6.750 o -4 6 3 123.501 123.070 3.429 6.868 o -4 6 4 50.651 54.675 2.473 19.153 o -4 6 5 133.433 138.086 4.383 5.695 o -4 6 6 35.409 34.375 2.900 24.279 o -4 6 7 75.878 76.532 4.059 10.456 o -4 7 1 7.258 8.687 0.979 146.710 o -4 7 2 8.391 10.669 1.087 122.112 o -4 7 3 2.447 4.436 0.822 310.010 o -4 7 4 52.593 50.082 2.276 19.882 o -4 7 5 126.151 127.054 3.494 6.634 o -4 7 6 0.010 1.847 0.924 513.821 o -4 7 7 3.448 2.232 0.846 307.491 o -4 8 1 2.459 2.813 0.728 382.561 o -4 8 2 187.438 177.538 4.225 3.971 o -4 8 3 11.669 8.862 0.971 112.931 o -4 8 4 18.926 19.706 1.737 53.371 o -4 8 5 13.871 13.272 1.319 80.776 o -4 8 6 8.302 8.909 1.295 115.631 o -4 9 1 2.147 2.693 0.765 391.713 o -4 9 2 404.647 367.561 6.750 1.253 o -4 9 3 0.005 0.736 0.841 694.375 o -4 9 4 11.908 12.513 1.428 84.650 o -4 9 5 48.877 51.572 2.469 19.962 o -4 9 6 36.613 37.982 2.300 26.857 o -4 10 1 380.724 381.521 7.797 1.263 o -4 10 2 99.362 93.037 3.334 9.055 o -4 10 3 260.023 282.093 7.506 2.047 o -4 10 4 7.235 8.595 1.617 102.146 o -4 10 5 3.703 3.801 0.838 271.520 o -4 10 6 44.041 38.788 2.127 24.749 o -4 11 1 89.740 85.274 5.959 6.947 o -4 11 2 128.435 137.895 4.090 6.016 o -4 11 3 135.920 137.900 7.650 4.011 o -4 11 4 73.671 79.599 3.234 11.872 o -4 11 5 0.003 1.513 0.732 773.317 o -4 11 6 25.062 20.547 1.058 53.681 o -4 12 1 201.678 191.098 7.347 2.919 o -4 12 2 31.717 29.531 2.227 31.716 o -4 12 3 12.155 13.063 1.320 86.797 o -4 12 4 7.095 8.339 1.209 131.980 o -4 12 5 1.401 0.429 0.604 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355.670 o -4 18 1 44.854 38.517 2.879 20.989 o -4 18 2 30.945 26.373 2.422 31.352 o -4 18 3 120.782 115.155 4.757 6.280 o -4 18 4 0.046 0.248 0.501 1895.440 o -4 19 1 18.478 13.342 1.702 59.797 o -4 19 2 14.273 18.725 1.934 57.093 o -4 19 3 89.574 88.201 3.887 9.264 o -4 19 4 39.699 48.255 2.465 23.010 o -4 20 1 7.427 9.471 1.406 112.119 o -4 20 2 9.115 8.450 1.295 112.219 o -4 20 3 82.604 83.826 8.140 5.162 o -4 21 1 30.641 32.418 1.859 34.477 o -4 21 2 1.209 0.960 0.688 634.104 o -4 21 3 0.241 0.728 0.597 1106.860 o -4 22 1 10.992 12.088 1.550 83.749 o -4 22 2 17.301 11.621 1.411 70.986 o -3 0 2 2601.430 2816.330 90.039 0.026 o -3 0 4 81.887 78.707 3.293 11.029 o -3 0 6 1645.930 1638.930 33.930 0.088 o -3 0 8 26.727 25.875 2.086 37.373 o -3 1 1 0.275 1.530 1.562 205.357 o -3 1 2 269.244 258.623 12.762 1.475 o -3 1 3 70.564 70.757 2.094 14.747 o -3 1 4 2.437 6.601 0.831 268.905 o -3 1 5 169.640 164.917 3.777 4.587 o -3 1 6 74.772 78.559 3.556 11.284 o -3 1 7 419.883 392.798 8.229 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107.066 o -3 9 2 45.557 41.054 2.113 23.878 o -3 9 3 21.959 24.063 1.722 46.982 o -3 9 4 100.814 106.141 3.386 8.497 o -3 9 5 71.112 81.973 3.342 11.830 o -3 9 6 779.423 760.677 16.487 0.358 o -3 9 7 77.320 72.115 2.325 13.333 o -3 10 1 2.962 2.281 1.208 227.260 o -3 10 2 44.200 37.905 3.386 18.927 o -3 10 3 263.112 257.659 7.723 2.080 o -3 10 4 826.190 822.864 13.682 0.342 o -3 10 5 67.276 69.640 2.752 14.107 o -3 10 6 13.605 12.088 1.136 89.658 o -3 10 7 2.182 2.225 0.634 468.354 o -3 11 1 2.806 4.734 1.109 224.634 o -3 11 2 3.749 1.717 0.975 270.501 o -3 11 3 425.894 429.740 9.867 0.999 o -3 11 4 490.099 498.686 10.760 0.794 o -3 11 5 65.909 64.232 2.633 14.945 o -3 11 6 136.215 129.319 4.049 5.919 o -3 11 7 0.091 0.246 0.530 1668.480 o -3 12 1 6.221 5.998 1.033 168.314 o -3 12 2 84.777 72.872 3.659 10.496 o -3 12 3 240.071 247.118 7.904 2.246 o -3 12 4 784.217 808.412 15.550 0.351 o -3 12 5 4.843 5.601 1.174 172.243 o -3 12 6 45.472 46.279 2.258 22.444 o -3 12 7 163.478 162.078 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163.526 6.945 3.537 o -3 17 3 36.090 40.900 2.784 23.672 o -3 17 4 73.171 76.823 3.645 11.364 o -3 17 5 60.092 59.292 2.487 16.678 o -3 17 6 43.311 43.468 2.110 24.248 o -3 18 1 2.006 2.785 1.077 281.425 o -3 18 2 26.259 26.450 2.604 32.182 o -3 18 3 13.926 14.225 1.959 60.816 o -3 18 4 26.195 22.314 1.588 44.999 o -3 18 5 108.199 107.168 3.219 8.171 o -3 18 6 101.660 90.130 4.341 7.990 o -3 19 1 332.229 305.326 8.884 1.504 o -3 19 2 79.164 72.050 3.329 11.544 o -3 19 3 35.032 27.555 2.284 30.050 o -3 19 4 34.428 39.101 1.961 29.683 o -3 19 5 21.044 22.235 1.592 51.099 o -3 20 1 1.707 1.866 1.015 333.917 o -3 20 2 103.686 101.369 4.648 7.326 o -3 20 3 207.332 187.439 5.397 3.310 o -3 20 4 141.031 141.593 4.961 5.139 o -3 20 5 1.513 0.780 0.584 700.598 o -3 21 1 0.243 1.252 0.852 593.454 o -3 21 2 1.151 1.831 1.074 336.686 o -3 21 3 519.259 520.020 12.720 0.694 o -3 21 4 41.535 30.295 2.325 26.269 o -3 21 5 8.260 9.068 1.008 134.010 o -3 22 1 13.865 11.979 1.246 85.276 o -3 22 2 0.483 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159.411 o -2 2 7 200.685 200.171 6.532 3.064 o -2 2 8 28.846 27.084 1.462 41.335 o -2 3 1 87.319 83.861 5.496 7.582 o -2 3 2 510.603 577.568 17.209 0.576 o -2 3 3 737.151 714.496 24.646 0.314 o -2 3 4 290.831 285.651 15.097 1.176 o -2 3 5 289.834 280.554 8.070 1.821 o -2 3 6 141.781 137.486 6.297 4.533 o -2 3 7 28.522 21.248 1.939 39.354 o -2 3 8 27.404 18.781 1.201 50.068 o -2 4 1 187.358 248.232 17.876 1.187 o -2 4 2 229.980 236.798 9.740 2.071 o -2 4 3 111.965 110.873 8.799 4.017 o -2 4 4 13.871 18.745 4.142 23.995 o -2 4 5 949.807 976.978 21.904 0.234 o -2 4 6 37.014 42.095 2.968 22.202 o -2 4 7 25.187 21.706 1.968 41.682 o -2 4 8 12.199 11.233 1.220 93.925 o -2 5 1 1867.240 1915.690 42.984 0.065 o -2 5 2 1307.310 1336.490 27.796 0.133 o -2 5 3 1.672 3.457 2.672 69.399 o -2 5 4 7.966 12.658 1.967 75.000 o -2 5 5 36.492 35.772 2.604 25.482 o -2 5 6 25.409 23.156 2.356 36.322 o -2 5 7 13.764 10.869 1.155 90.757 o -2 5 8 11.645 10.287 0.924 110.945 o -2 6 1 48.914 86.405 5.811 8.960 o 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107.437 3.775 8.204 o -2 9 6 12.222 11.108 2.531 51.135 o -2 9 7 42.565 41.854 2.673 22.126 o -2 9 8 10.990 11.119 1.088 105.233 o -2 10 1 2483.610 2444.660 58.744 0.038 o -2 10 2 708.408 802.704 28.237 0.280 o -2 10 3 85.425 81.472 4.611 8.826 o -2 10 4 1159.860 1183.230 18.597 0.182 o -2 10 5 3.269 4.571 1.147 209.552 o -2 10 6 30.357 30.201 2.535 29.731 o -2 10 7 66.674 63.751 3.828 12.303 o -2 10 8 14.044 12.188 1.477 76.895 o -2 11 1 21.285 23.218 4.213 21.026 o -2 11 2 159.201 178.808 12.435 2.133 o -2 11 3 379.306 387.521 9.245 1.191 o -2 11 4 1046.950 1056.520 19.977 0.211 o -2 11 5 29.285 30.496 3.653 21.888 o -2 11 6 5.769 6.348 1.439 130.907 o -2 11 7 51.950 52.545 2.307 19.638 o -2 12 1 37.485 43.761 5.545 11.680 o -2 12 2 119.155 129.728 5.896 5.364 o -2 12 3 1003.950 967.577 21.987 0.223 o -2 12 4 295.261 296.285 8.164 1.744 o -2 12 5 20.026 21.030 2.244 42.949 o -2 12 6 2.775 1.984 1.052 276.375 o -2 12 7 9.329 10.700 1.037 118.524 o -2 13 1 811.886 819.307 28.125 0.252 o -2 13 2 135.262 137.724 7.706 3.998 o -2 13 3 62.232 49.482 3.133 15.452 o -2 13 4 29.935 38.541 2.693 26.885 o -2 13 5 13.406 13.871 1.849 65.155 o -2 13 6 50.695 53.896 2.560 18.941 o -2 13 7 45.515 56.242 2.193 21.223 o -2 14 1 4.227 7.046 0.896 207.933 o -2 14 2 3.686 6.516 1.163 183.451 o -2 14 3 80.016 78.468 3.335 11.149 o -2 14 4 54.761 51.383 3.402 15.702 o -2 14 5 11.261 10.327 1.636 82.304 o -2 14 6 1.551 1.407 0.721 526.018 o -2 14 7 54.505 52.107 2.511 18.453 o -2 15 1 151.538 141.732 4.045 5.256 o -2 15 2 809.555 799.382 12.389 0.362 o -2 15 3 167.699 160.623 5.020 4.285 o -2 15 4 0.751 0.124 1.080 406.035 o -2 15 5 10.537 11.704 1.704 79.684 o -2 15 6 74.186 77.709 3.506 11.461 o -2 15 7 40.039 43.588 2.509 23.434 o -2 16 1 31.050 31.991 1.908 33.959 o -2 16 2 541.358 536.656 8.564 0.736 o -2 16 3 2416.080 2456.630 44.990 0.043 o -2 16 4 0.033 2.339 1.239 303.353 o -2 16 5 6.959 7.107 1.174 141.131 o -2 16 6 7.119 5.775 1.383 127.762 o -2 16 7 19.985 26.986 1.781 46.731 o -2 17 1 38.808 38.608 2.162 26.622 o -2 17 2 12.738 11.693 1.336 86.612 o -2 17 3 325.643 327.549 8.628 1.504 o -2 17 4 3.423 4.441 1.795 120.894 o -2 17 5 0.000 0.625 3.016 60.093 o -2 17 6 19.081 23.322 1.641 52.252 o -2 18 1 0.574 2.642 1.050 356.580 o -2 18 2 151.210 152.209 5.431 4.563 o -2 18 3 86.221 94.804 4.103 9.007 o -2 18 4 27.404 28.602 3.285 25.296 o -2 18 5 152.591 149.924 5.986 4.331 o -2 18 6 115.252 138.335 4.682 6.117 o -2 19 1 365.154 349.869 7.054 1.405 o -2 19 2 0.191 1.689 1.088 386.513 o -2 19 3 11.314 11.904 1.336 91.493 o -2 19 4 24.192 23.067 1.952 42.171 o -2 19 5 6.298 7.974 1.202 140.732 o -2 19 6 118.743 133.555 4.321 6.305 o -2 20 1 58.104 56.966 2.952 16.008 o -2 20 2 31.002 34.100 2.229 30.851 o -2 20 3 26.890 29.973 1.914 37.470 o -2 20 4 2.660 3.896 0.996 264.978 o -2 20 5 46.953 49.099 2.774 19.594 o -2 20 6 7.432 6.208 2.075 80.601 o -2 21 1 16.310 19.603 1.863 54.838 o -2 21 2 211.113 211.376 5.032 3.174 o -2 21 3 169.653 177.893 4.963 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1 6 3 94.437 97.913 5.566 6.922 o 1 6 4 127.085 121.557 7.605 4.313 o 1 6 5 47.622 50.013 3.791 15.661 o 1 6 6 3.263 3.523 0.853 287.720 o 1 6 7 396.174 390.162 8.640 1.168 o 1 6 8 187.639 194.880 12.340 1.975 o 1 7 0 38.080 35.398 2.819 23.721 o 1 7 1 0.164 1.928 0.835 573.171 o 1 7 2 46.512 46.491 3.255 18.105 o 1 7 3 241.505 260.326 11.995 1.655 o 1 7 4 2.401 1.646 0.740 422.131 o 1 7 5 285.290 298.148 8.019 1.803 o 1 7 6 9.190 9.211 1.109 120.342 o 1 7 7 54.773 55.445 2.495 18.087 o 1 7 8 412.372 404.544 7.457 1.150 o 1 8 0 101.221 102.181 4.331 7.715 o 1 8 1 4.119 2.578 0.851 275.076 o 1 8 2 81.959 64.543 3.918 10.676 o 1 8 3 456.591 502.861 17.943 0.641 o 1 8 4 20.996 15.825 2.094 46.976 o 1 8 5 1.032 0.679 0.853 525.752 o 1 8 6 35.504 31.891 1.843 31.796 o 1 8 7 261.443 257.658 5.450 2.358 o 1 9 0 793.694 775.841 17.483 0.341 o 1 9 1 329.162 300.187 8.735 1.537 o 1 9 2 1.798 -1.314 1.786 152.611 o 1 9 3 146.571 164.718 9.956 2.880 o 1 9 4 1387.170 1391.260 24.197 0.128 o 1 9 5 6.370 4.812 1.213 154.401 o 1 9 6 120.587 119.055 3.800 6.850 o 1 9 7 6.351 8.604 0.938 160.126 o 1 10 0 459.928 524.509 11.974 0.788 o 1 10 1 33.647 31.887 2.769 26.205 o 1 10 2 16.692 16.072 3.146 34.218 o 1 10 3 94.611 103.651 7.994 4.838 o 1 10 4 42.485 38.285 3.012 21.009 o 1 10 5 312.071 334.988 8.451 1.557 o 1 10 6 230.556 240.198 5.701 2.682 o 1 10 7 10.351 11.494 1.013 111.035 o 1 11 0 0.063 0.587 0.986 522.336 o 1 11 1 52.621 47.262 3.692 15.440 o 1 11 2 1167.700 1204.090 43.928 0.118 o 1 11 3 165.085 185.049 7.881 3.216 o 1 11 4 236.425 237.085 5.865 2.617 o 1 11 5 99.895 110.919 4.467 7.444 o 1 11 6 17.940 18.848 1.788 54.456 o 1 11 7 123.451 133.821 3.774 6.449 o 1 12 0 3.177 2.721 1.373 186.394 o 1 12 1 261.982 246.279 8.472 2.029 o 1 12 2 34.156 48.457 5.230 12.679 o 1 12 3 84.691 76.846 3.725 10.248 o 1 12 4 9.737 9.593 1.456 97.436 o 1 12 5 30.243 29.829 2.126 33.318 o 1 12 6 318.263 333.251 6.854 1.647 o 1 12 7 311.685 329.737 5.889 1.753 o 1 13 0 315.445 307.209 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3.588 20.413 o 2 9 3 54.855 51.691 3.200 16.279 o 2 9 4 2361.970 2290.570 58.896 0.041 o 2 9 5 3.899 2.158 0.726 323.558 o 2 9 6 0.036 0.734 0.646 1076.750 o 2 9 7 0.692 0.688 0.413 1337.670 o 2 10 0 381.089 414.591 11.960 1.026 o 2 10 1 157.647 128.809 7.756 3.712 o 2 10 2 5.497 8.165 3.968 30.539 o 2 10 3 263.042 266.944 6.924 2.144 o 2 10 4 603.862 613.723 12.222 0.564 o 2 10 5 21.449 26.093 1.554 48.677 o 2 10 6 193.031 190.782 5.261 3.519 o 2 10 7 0.919 1.015 0.846 525.678 o 2 11 0 498.893 523.199 20.887 0.528 o 2 11 1 188.357 148.889 8.510 2.981 o 2 11 2 0.685 1.252 1.289 279.964 o 2 11 3 1.080 -0.086 0.983 452.585 o 2 11 4 35.769 41.895 3.440 20.100 o 2 11 5 8.664 8.959 1.123 123.937 o 2 11 6 13.696 14.234 1.137 85.370 o 2 12 0 293.447 278.068 15.153 1.174 o 2 12 1 759.459 709.449 21.081 0.339 o 2 12 2 76.904 78.509 3.126 11.771 o 2 12 3 326.814 312.964 9.746 1.446 o 2 12 4 124.078 124.577 6.050 5.210 o 2 12 5 2.048 1.427 1.133 285.207 o 2 12 6 292.962 282.318 6.565 1.939 o 2 13 0 16.232 13.334 4.707 19.769 o 2 13 1 108.217 103.254 4.726 7.020 o 2 13 2 35.829 37.496 2.575 25.587 o 2 13 3 903.104 868.530 19.197 0.274 o 2 13 4 119.212 113.396 5.720 5.703 o 2 13 5 4.986 3.803 1.018 206.188 o 2 13 6 28.149 32.295 2.329 32.065 o 2 14 0 698.274 688.012 10.760 0.473 o 2 14 1 1.558 1.935 1.051 324.660 o 2 14 2 6.413 3.699 1.448 135.458 o 2 14 3 165.478 161.693 6.766 3.719 o 2 14 4 26.294 28.704 4.160 19.687 o 2 14 5 0.248 0.110 1.308 309.379 o 2 14 6 9.541 8.579 1.151 117.629 o 2 15 0 91.394 102.605 3.637 8.953 o 2 15 1 33.052 31.532 3.834 19.804 o 2 15 2 293.094 280.372 7.152 1.891 o 2 15 3 970.515 896.966 18.279 0.255 o 2 15 4 116.295 120.303 5.831 5.613 o 2 15 5 7.710 7.002 1.467 113.541 o 2 15 6 16.802 18.208 1.597 60.739 o 2 16 0 43.870 46.869 2.130 23.393 o 2 16 1 37.727 47.378 3.158 20.365 o 2 16 2 1185.750 1145.620 19.465 0.179 o 2 16 3 532.995 530.911 14.496 0.634 o 2 16 4 15.024 18.802 2.323 47.824 o 2 16 5 19.568 20.029 1.650 53.742 o 2 16 6 4.748 7.352 1.014 181.239 o 2 17 0 5.414 1.697 0.838 251.834 o 2 17 1 59.238 58.471 3.728 13.676 o 2 17 2 273.610 275.262 7.411 1.995 o 2 17 3 149.049 159.049 5.799 4.387 o 2 17 4 73.174 62.347 3.920 11.545 o 2 17 5 106.257 112.598 4.752 6.886 o 2 17 6 193.591 195.841 4.405 3.665 o 2 18 0 65.574 71.939 3.303 13.061 o 2 18 1 64.922 63.915 3.097 14.095 o 2 18 2 49.545 49.274 2.989 18.201 o 2 18 3 38.037 42.564 3.019 21.586 o 2 18 4 8.064 11.190 1.904 79.400 o 2 18 5 123.179 132.086 4.721 5.931 o 2 19 0 5.071 9.531 1.640 109.168 o 2 19 1 40.836 37.309 2.252 25.588 o 2 19 2 46.014 42.836 3.522 17.514 o 2 19 3 12.188 13.465 1.833 68.671 o 2 19 4 282.751 291.204 8.365 1.801 o 2 19 5 4.441 3.480 0.685 284.786 o 2 20 0 82.043 88.635 3.724 9.996 o 2 20 1 407.005 391.616 10.022 1.079 o 2 20 2 32.275 29.904 1.952 33.495 o 2 20 3 196.195 203.307 4.622 3.520 o 2 20 4 9.319 8.592 1.046 125.264 o 2 20 5 48.806 47.901 1.879 22.598 o 2 21 0 2.932 3.801 2.233 89.900 o 2 21 1 315.109 312.583 7.766 1.644 o 2 21 2 325.727 316.129 6.666 1.665 o 2 21 3 125.737 123.572 4.409 6.179 o 2 21 4 8.720 8.572 0.861 141.622 o 2 22 0 52.050 51.578 3.971 14.359 o 2 22 1 215.885 216.946 6.068 2.893 o 2 22 2 24.749 20.206 1.639 47.121 o 2 22 3 362.804 360.469 9.390 1.271 o 2 22 4 104.122 106.897 3.298 8.353 o 2 23 0 6.104 5.564 1.629 115.326 o 2 23 1 1.038 1.595 1.025 372.454 o 2 23 2 2.969 2.233 0.989 283.870 o 2 23 3 10.693 13.315 1.746 75.418 o 2 23 4 0.670 1.161 0.913 489.292 o 2 24 0 230.665 215.527 7.051 2.580 o 2 24 1 5.646 7.913 1.197 147.549 o 2 24 2 0.308 0.501 0.776 751.656 o 2 24 3 182.035 178.206 5.832 3.632 o 2 25 0 166.549 167.161 6.887 3.623 o 2 25 1 4.347 5.436 0.947 213.876 o 2 25 2 108.955 112.095 4.467 7.014 o 2 25 3 61.525 55.096 2.629 16.437 o 2 26 0 31.454 28.976 2.652 28.570 o 2 26 1 149.618 157.553 6.244 4.210 o 2 26 2 29.075 29.021 3.202 25.276 o 2 27 0 0.321 2.106 1.486 217.850 o 2 27 1 43.825 47.861 4.025 15.579 o 2 28 0 219.746 224.061 9.132 2.273 o 3 0 0 0.192 2.097 2.774 69.026 o 3 0 2 15.260 7.116 1.651 74.806 o 3 0 4 353.991 297.268 14.544 1.067 o 3 0 6 11.617 14.003 2.323 55.203 o 3 1 0 26.872 25.208 3.808 22.184 o 3 1 1 13.441 12.949 4.194 24.470 o 3 1 2 0.115 0.323 0.780 818.513 o 3 1 3 148.149 133.745 5.558 4.781 o 3 1 4 11.947 6.219 1.641 86.622 o 3 1 5 25.334 24.162 2.583 33.575 o 3 1 6 106.392 107.902 3.842 7.744 o 3 2 0 8.093 6.914 2.077 77.600 o 3 2 1 95.578 107.014 8.589 4.410 o 3 2 2 4.991 5.620 1.348 149.917 o 3 2 3 5.251 5.768 1.495 131.908 o 3 2 4 10.378 7.818 1.883 78.506 o 3 2 5 31.117 29.426 5.169 14.149 o 3 2 6 79.959 75.965 2.994 11.792 o 3 3 0 9.008 1.363 2.001 87.085 o 3 3 1 420.550 407.342 17.997 0.726 o 3 3 2 54.795 61.412 2.826 16.547 o 3 3 3 3.076 4.197 1.316 186.517 o 3 3 4 0.062 0.893 0.889 605.793 o 3 3 5 1.204 1.308 1.556 192.960 o 3 3 6 18.961 15.907 1.376 63.399 o 3 4 0 37.606 34.230 4.878 14.221 o 3 4 1 0.334 1.729 1.935 136.879 o 3 4 2 41.801 44.916 2.421 23.079 o 3 4 3 81.182 85.469 4.936 8.531 o 3 4 4 11.743 12.405 1.446 84.724 o 3 4 5 55.377 57.022 2.959 16.453 o 3 4 6 29.872 26.808 1.690 38.506 o 3 5 0 95.858 83.754 7.373 5.483 o 3 5 1 215.219 225.946 7.889 2.521 o 3 5 2 54.167 58.716 2.803 16.973 o 3 5 3 34.864 43.148 2.787 23.691 o 3 5 4 355.968 320.210 10.529 1.285 o 3 5 5 67.361 59.079 2.984 14.343 o 3 5 6 0.008 -0.129 0.544 1851.450 o 3 6 0 91.250 68.839 7.047 6.081 o 3 6 1 82.493 60.847 2.685 12.832 o 3 6 2 3.403 3.846 0.909 264.073 o 3 6 3 146.104 129.515 8.261 3.665 o 3 6 4 41.122 39.316 2.307 24.820 o 3 6 5 85.326 71.094 2.843 11.711 o 3 6 6 60.869 62.920 2.348 16.538 o 3 7 0 20.447 24.239 2.449 38.372 o 3 7 1 1087.760 1127.660 16.309 0.206 o 3 7 2 33.460 31.147 2.483 28.468 o 3 7 3 26.732 30.535 3.157 26.183 o 3 7 4 0.869 1.384 0.845 510.344 o 3 7 5 84.569 71.809 2.807 11.803 o 3 7 6 5.979 5.823 0.820 196.889 o 3 8 0 86.571 92.663 4.141 9.006 o 3 8 1 18.642 12.225 1.531 64.411 o 3 8 2 68.618 62.998 4.625 10.571 o 3 8 3 0.001 0.187 1.470 252.495 o 3 8 4 214.469 205.954 4.879 3.194 o 3 8 5 27.553 29.365 1.754 38.739 o 3 8 6 39.490 45.684 1.631 27.494 o 3 9 0 132.233 131.540 4.355 5.853 o 3 9 1 118.667 107.205 4.251 6.872 o 3 9 2 152.911 151.550 6.757 4.001 o 3 9 3 12.748 10.807 1.942 66.878 o 3 9 4 13.021 11.801 1.159 91.708 o 3 9 5 0.056 0.717 0.739 857.748 o 3 9 6 0.499 0.896 0.428 1362.980 o 3 10 0 1.996 2.136 0.892 363.735 o 3 10 1 0.992 0.568 0.848 541.399 o 3 10 2 3.721 8.605 1.460 136.190 o 3 10 3 130.283 131.674 5.947 5.029 o 3 10 4 99.684 109.259 3.785 8.114 o 3 10 5 62.831 62.191 2.876 15.026 o 3 10 6 86.423 88.324 7.041 5.949 o 3 11 0 207.274 215.371 6.588 2.894 o 3 11 1 170.318 161.522 5.192 4.168 o 3 11 2 303.267 319.594 8.221 1.647 o 3 11 3 121.093 115.141 5.551 5.735 o 3 11 4 117.269 114.585 4.125 6.866 o 3 11 5 248.201 230.627 5.967 2.524 o 3 11 6 71.691 56.734 2.445 15.020 o 3 12 0 93.218 98.951 3.972 8.597 o 3 12 1 224.289 195.376 5.797 2.970 o 3 12 2 1113.650 1091.240 19.664 0.195 o 3 12 3 35.839 40.547 2.661 24.522 o 3 12 4 59.607 63.351 2.698 15.880 o 3 12 5 22.024 24.458 2.196 40.345 o 3 13 0 139.157 137.825 4.752 5.342 o 3 13 1 8.701 8.044 1.380 110.575 o 3 13 2 419.857 416.130 10.275 1.012 o 3 13 3 340.686 330.920 8.444 1.452 o 3 13 4 131.449 135.553 4.743 5.604 o 3 13 5 4.893 4.830 1.657 122.828 o 3 14 0 86.482 83.773 4.986 8.229 o 3 14 1 1.749 0.743 0.932 403.397 o 3 14 2 140.869 152.543 6.586 4.274 o 3 14 3 194.015 201.923 6.151 3.220 o 3 14 4 59.514 63.214 3.944 12.839 o 3 14 5 23.376 21.771 1.970 43.311 o 3 15 0 43.895 50.952 3.057 18.966 o 3 15 1 4.988 5.669 1.277 157.622 o 3 15 2 0.246 0.337 0.962 538.855 o 3 15 3 344.928 365.261 8.830 1.352 o 3 15 4 79.622 84.233 4.405 9.382 o 3 15 5 21.234 21.221 1.778 48.679 o 3 16 0 65.444 69.908 3.579 12.625 o 3 16 1 0.748 1.436 1.052 380.042 o 3 16 2 0.871 1.182 0.828 536.474 o 3 16 3 70.963 70.231 4.340 10.624 o 3 16 4 103.073 114.804 5.254 6.555 o 3 16 5 3.306 1.730 0.623 401.889 o 3 17 0 23.070 23.531 2.695 33.876 o 3 17 1 6.229 6.678 1.316 136.882 o 3 17 2 64.843 60.444 3.702 12.956 o 3 17 3 510.674 528.350 22.662 0.483 o 3 17 4 144.362 149.150 5.650 4.652 o 3 17 5 1.008 3.608 1.116 289.137 o 3 18 0 23.148 25.592 2.211 38.785 o 3 18 1 35.814 37.358 2.541 25.829 o 3 18 2 86.521 79.507 3.278 10.604 o 3 18 3 46.733 54.545 5.017 11.862 o 3 18 4 40.886 45.259 2.858 21.244 o 3 19 0 62.478 56.734 3.105 14.934 o 3 19 1 14.311 10.275 1.754 69.936 o 3 19 2 216.974 229.059 7.157 2.624 o 3 19 3 309.680 301.209 7.267 1.737 o 3 19 4 19.096 21.504 1.378 57.985 o 3 20 0 51.037 44.110 2.625 19.781 o 3 20 1 57.018 58.633 3.506 14.536 o 3 20 2 217.099 219.539 11.170 1.967 o 3 20 3 0.680 1.286 0.757 624.237 o 3 20 4 15.345 14.059 1.736 64.147 o 3 21 0 57.535 49.222 3.233 15.938 o 3 21 1 184.085 194.840 6.878 3.210 o 3 21 2 16.673 14.419 1.614 64.207 o 3 21 3 1.392 1.720 0.804 469.576 o 3 22 0 23.441 20.243 2.023 43.263 o 3 22 1 4.681 3.661 1.635 130.621 o 3 22 2 34.821 39.522 2.239 27.661 o 3 22 3 31.805 35.924 2.159 30.482 o 3 23 0 2.562 2.716 1.009 283.963 o 3 23 1 1.855 0.936 0.858 430.139 o 3 23 2 38.964 39.230 1.989 27.377 o 3 24 0 46.251 40.786 2.953 20.023 o 3 24 1 0.418 -0.187 1.104 418.543 o 3 24 2 0.108 -0.350 1.082 460.402 o 3 25 0 181.617 156.274 5.595 3.884 o 3 25 1 137.381 138.716 6.286 4.617 o 4 0 0 1042.600 1079.890 21.598 0.204 o 4 0 2 681.692 761.051 26.293 0.310 o 4 0 4 89.816 75.991 6.122 6.945 o 4 1 0 1816.590 1860.330 25.336 0.080 o 4 1 1 39.955 40.435 1.977 26.756 o 4 1 2 86.880 93.153 12.972 2.593 o 4 1 3 309.071 358.416 12.549 1.229 o 4 1 4 268.616 230.238 8.047 2.092 o 4 1 5 10.934 8.233 1.257 104.995 o 4 2 0 354.456 370.628 9.449 1.277 o 4 2 1 84.500 81.044 2.754 11.414 o 4 2 2 100.069 88.332 5.592 6.864 o 4 2 3 5.158 6.538 1.792 105.520 o 4 2 4 54.040 47.212 3.341 16.351 o 4 2 5 0.073 1.480 0.957 498.128 o 4 3 0 295.926 299.048 8.246 1.727 o 4 3 1 274.854 285.865 5.813 2.114 o 4 3 2 23.839 27.087 2.714 32.229 o 4 3 3 0.414 2.342 2.802 67.029 o 4 3 4 2.954 2.732 1.178 228.978 o 4 3 5 180.943 180.094 5.810 3.641 o 4 4 0 73.113 67.767 2.595 13.733 o 4 4 1 244.656 247.049 8.182 2.175 o 4 4 2 93.741 109.707 13.518 2.358 o 4 4 3 564.107 548.018 22.093 0.457 o 4 4 4 10.441 7.966 1.556 92.944 o 4 4 5 45.149 37.735 1.930 25.444 o 4 5 0 10.953 12.520 1.171 98.487 o 4 5 1 40.509 42.474 2.694 22.538 o 4 5 2 0.254 0.497 1.207 349.841 o 4 5 3 6.480 4.451 1.571 121.114 o 4 5 4 129.342 112.559 4.176 6.391 o 4 5 5 36.073 35.169 1.786 30.943 o 4 6 0 51.815 53.474 2.237 19.780 o 4 6 1 1426.410 1414.230 25.328 0.122 o 4 6 2 81.457 78.065 8.834 4.716 o 4 6 3 57.744 57.716 2.941 16.035 o 4 6 4 39.467 40.753 2.373 24.809 o 4 6 5 48.669 36.847 2.177 23.264 o 4 7 0 635.310 647.778 10.377 0.543 o 4 7 1 926.000 991.623 28.922 0.206 o 4 7 2 195.332 191.675 9.488 2.496 o 4 7 3 17.648 17.923 1.839 54.577 o 4 7 4 59.136 59.475 2.324 17.254 o 4 7 5 24.671 21.049 2.576 35.002 o 4 8 0 171.242 177.593 4.329 4.256 o 4 8 1 1084.880 1064.010 24.874 0.188 o 4 8 2 3.839 4.324 1.729 124.934 o 4 8 3 6.153 5.919 1.218 150.391 o 4 8 4 59.160 59.184 3.944 13.103 o 4 8 5 0.533 -0.812 0.691 916.526 o 4 9 0 14.311 18.081 1.525 67.519 o 4 9 1 7.432 10.519 1.667 94.207 o 4 9 2 280.833 276.081 11.515 1.529 o 4 9 3 18.876 15.701 1.690 57.391 o 4 9 4 180.618 165.512 4.840 4.045 o 4 9 5 0.957 -0.586 1.105 381.543 o 4 10 0 0.094 0.742 1.071 438.641 o 4 10 1 2.244 4.457 1.259 208.754 o 4 10 2 8.226 6.016 1.262 128.153 o 4 10 3 392.126 396.927 14.059 0.927 o 4 10 4 1.155 2.025 0.926 403.746 o 4 11 0 37.448 33.059 2.471 26.464 o 4 11 1 21.331 22.453 2.090 43.299 o 4 11 2 0.138 0.433 1.203 360.042 o 4 11 3 14.156 18.217 1.670 64.066 o 4 11 4 1.052 2.015 0.711 557.797 o 4 12 0 8.180 6.596 1.414 115.608 o 4 12 1 196.439 202.903 6.494 3.106 o 4 12 2 414.136 411.522 10.030 1.039 o 4 12 3 60.038 54.675 2.385 17.392 o 4 12 4 1.609 3.133 0.744 423.892 o 4 13 0 1.705 1.745 1.144 287.914 o 4 13 1 2.287 4.142 1.260 210.685 o 4 13 2 381.847 379.543 15.993 0.872 o 4 13 3 71.638 79.825 3.155 12.206 o 4 13 4 44.414 47.559 2.683 20.784 o 4 14 0 59.131 58.736 3.205 15.025 o 4 14 1 6.271 3.675 1.486 133.049 o 4 14 2 349.331 346.342 10.982 1.238 o 4 14 3 31.730 34.336 2.342 29.574 o 4 14 4 1.517 1.492 0.677 557.331 o 4 15 0 24.304 25.880 2.193 38.001 o 4 15 1 0.671 1.587 1.161 326.221 o 4 15 2 335.544 327.991 9.545 1.403 o 4 15 3 2.464 4.198 0.828 312.843 o 4 15 4 83.157 82.621 4.837 8.629 o 4 16 0 86.301 82.749 3.698 9.932 o 4 16 1 127.432 128.873 4.585 5.925 o 4 16 2 119.807 123.474 4.079 6.611 o 4 16 3 11.759 12.709 1.480 82.911 o 4 17 0 0.123 -0.440 0.927 620.230 o 4 17 1 0.047 -0.801 0.760 936.512 o 4 17 2 128.093 134.825 4.114 6.069 o 4 17 3 75.036 72.567 3.308 11.968 o 4 18 0 16.396 16.983 1.588 62.836 o 4 18 1 0.005 0.634 1.359 286.777 o 4 18 2 8.438 10.761 1.522 97.163 o 4 18 3 9.844 11.737 1.295 99.916 o 4 19 0 13.671 13.913 1.423 77.195 o 4 19 1 5.948 4.064 0.868 207.482 o 4 19 2 182.685 191.362 11.466 2.171 o 4 20 0 58.802 55.944 2.225 17.934 o 4 20 1 179.928 157.828 3.993 4.376 o 4 20 2 70.999 64.579 2.920 13.614 o 4 21 0 279.197 273.545 13.321 1.368 o 4 21 1 62.364 70.808 3.085 14.000 o 4 22 0 2.040 3.709 1.443 183.683 o 5 0 0 18.467 39.330 4.470 18.408 o 5 0 2 32.983 51.040 4.645 14.606 o 5 1 0 1069.830 1162.960 20.634 0.194 o 5 1 1 0.475 1.014 1.996 130.830 o 5 1 2 19.747 16.019 1.931 51.239 o 5 1 3 0.866 0.246 0.657 832.085 o 5 2 0 93.977 129.543 4.441 7.311 o 5 2 1 5.367 7.110 1.153 159.053 o 5 2 2 21.944 25.490 4.989 16.277 o 5 2 3 0.798 1.535 0.713 630.025 o 5 3 0 630.801 684.124 16.395 0.460 o 5 3 1 90.938 108.529 4.892 7.511 o 5 3 2 5.588 6.715 1.117 162.656 o 5 3 3 35.306 27.940 1.703 34.091 o 5 4 0 6.171 7.255 1.708 104.603 o 5 4 1 52.090 51.601 4.966 11.652 o 5 4 2 7.853 9.307 3.219 41.163 o 5 4 3 88.820 68.642 3.444 10.644 o 5 5 0 32.094 31.040 2.442 29.431 o 5 5 1 43.582 46.139 3.133 19.255 o 5 5 2 7.186 14.189 2.046 71.934 o 5 5 3 155.532 163.013 5.619 4.289 o 5 6 0 1.056 0.990 2.858 64.583 o 5 6 1 53.336 50.108 3.180 16.743 o 5 6 2 31.748 29.677 2.435 29.984 o 5 6 3 89.894 97.697 4.059 8.740 o 5 7 0 90.469 83.823 4.431 8.686 o 5 7 1 15.817 16.696 2.965 37.115 o 5 7 2 24.784 22.728 2.086 40.139 o 5 7 3 0.001 0.558 0.884 650.941 o 5 8 0 7.695 7.354 1.555 106.819 o 5 8 1 204.598 205.577 14.065 1.623 o 5 8 2 35.061 34.984 2.556 26.486 o 5 8 3 2.396 2.049 0.935 328.177 o 5 9 0 0.559 3.204 1.416 219.434 o 5 9 1 0.036 2.022 1.297 286.178 o 5 9 2 64.184 59.269 3.169 14.348 o 5 9 3 133.940 142.139 4.674 5.469 o 5 10 0 78.820 88.043 7.035 6.172 o 5 10 1 38.150 37.449 2.611 24.549 o 5 10 2 122.737 120.253 4.894 6.033 o 5 11 0 7.120 6.408 1.432 121.642 o 5 11 1 7.872 9.502 1.422 108.576 o 5 11 2 37.959 35.549 2.025 28.448 o 5 12 0 15.460 17.851 1.993 54.642 o 5 12 1 155.165 154.504 4.285 4.896 o 5 12 2 17.722 18.303 1.290 65.218 o 5 13 0 30.924 25.323 2.252 33.155 o 5 13 1 41.902 41.171 2.431 23.605 o 5 13 2 0.732 0.710 0.868 546.934 o 5 14 0 31.509 30.614 2.320 30.789 o 5 14 1 16.311 13.179 1.311 74.113 o 5 15 0 0.086 1.085 1.657 190.439 o 5 15 1 7.030 5.091 1.370 132.098 o 5 16 0 4.286 7.731 1.143 169.492 o ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.332 _oxdiff_exptl_absorpt_empirical_full_min 0.668 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn O1 O 0.29632(19) 0.53806(4) 0.12432(12) 0.0159(2) Uani 1.000000 . H1 H 0.16666(19) 0.5443(8) 0.1800(8) 0.0238(3) Uiso 1.000000 GR O2 O 0.76777(19) 0.52755(4) 0.19606(13) 0.0174(2) Uani 1.000000 . H2 H 0.7327(3) 0.5078(6) 0.1010(16) 0.0261(4) Uiso 1.000000 GR O3 O 0.3290(2) 0.68541(4) 1.01470(14) 0.0213(3) Uani 1.000000 . N1 N 0.7859(2) 0.68148(5) 1.07388(16) 0.0150(3) Uani 1.000000 . H1a H 0.9322(2) 0.66804(5) 1.04158(16) 0.0180(3) Uiso 1.000000 R C3 C 0.5529(3) 0.63814(5) 0.78585(17) 0.0140(3) Uani 1.000000 . C6 C 0.5403(3) 0.58016(5) 0.43908(18) 0.0138(3) Uani 1.000000 . C7 C 0.5466(3) 0.67003(5) 0.96846(18) 0.0144(3) Uani 1.000000 . C4 C 0.7581(3) 0.60080(5) 0.76343(18) 0.0151(3) Uani 1.000000 . H4 H 0.8999(3) 0.59494(5) 0.86325(18) 0.0182(3) Uiso 1.000000 R C2 C 0.3417(3) 0.64685(5) 0.63497(19) 0.0158(3) Uani 1.000000 . H2a H 0.2042(3) 0.67191(5) 0.64877(19) 0.0190(3) Uiso 1.000000 R C1 C 0.3368(3) 0.61806(6) 0.46412(18) 0.0158(3) Uani 1.000000 . H1b H 0.1951(3) 0.62416(6) 0.36439(18) 0.0190(3) Uiso 1.000000 R C5 C 0.7515(3) 0.57219(6) 0.59167(18) 0.0151(3) Uani 1.000000 . H5 H 0.8898(3) 0.54732(6) 0.57800(18) 0.0181(3) Uiso 1.000000 R C8 C 0.8014(3) 0.71653(6) 1.24318(19) 0.0187(3) Uani 1.000000 . H8a H 0.6987(19) 0.7498(2) 1.2114(4) 0.0280(4) Uiso 1.000000 GR H8b H 0.728(2) 0.69696(18) 1.3421(6) 0.0280(4) Uiso 1.000000 GR H8c H 0.9875(4) 0.7259(4) 1.2877(10) 0.0280(4) Uiso 1.000000 GR B1 B 0.5327(3) 0.54735(6) 0.2465(2) 0.0139(3) Uani 1.000000 . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0116(5) 0.0230(5) 0.0129(4) 0.0008(4) 0.0018(3) -0.0042(3) O2 0.0135(5) 0.0244(5) 0.0140(5) -0.0005(4) 0.0009(3) -0.0069(4) O3 0.0129(5) 0.0325(6) 0.0189(5) 0.0000(4) 0.0038(4) -0.0087(4) N1 0.0135(6) 0.0195(6) 0.0120(5) 0.0009(4) 0.0016(4) -0.0037(4) C3 0.0146(7) 0.0159(6) 0.0117(6) -0.0032(5) 0.0031(5) -0.0006(5) C6 0.0130(7) 0.0166(6) 0.0119(6) -0.0023(5) 0.0025(5) 0.0003(5) C7 0.0142(7) 0.0163(6) 0.0128(6) -0.0008(5) 0.0026(5) 0.0008(5) C4 0.0142(6) 0.0184(7) 0.0121(6) -0.0003(5) -0.0002(5) 0.0009(5) C2 0.0133(7) 0.0182(6) 0.0159(6) 0.0019(5) 0.0022(5) -0.0011(5) C1 0.0135(7) 0.0202(7) 0.0130(6) 0.0004(5) -0.0007(5) 0.0000(5) C5 0.0143(7) 0.0168(6) 0.0141(6) 0.0014(5) 0.0023(5) -0.0003(5) C8 0.0188(7) 0.0218(7) 0.0149(6) -0.0001(5) 0.0007(5) -0.0054(5) B1 0.0137(7) 0.0156(7) 0.0122(6) -0.0006(5) 0.0016(5) 0.0014(5) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.01920 0.00962 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' B 0.00963 0.00408 2.05450 1.33260 1.09790 0.70680 23.21850 1.02100 60.34980 0.14030 -0.193200007081 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.05239 0.03377 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.03256 0.01839 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag B1 O1 H1 109.5 . . ? B1 O2 H2 109.5 . . ? C7 N1 H1a 119.70(7) . . ? C8 N1 H1a 119.70(7) . . ? C8 N1 C7 120.59(11) . . ? C4 C3 C7 122.70(11) . . ? C2 C3 C7 117.74(12) . . ? C2 C3 C4 119.56(12) . . ? C5 C6 C1 117.89(12) . . ? B1 C6 C1 121.20(11) . . ? B1 C6 C5 120.91(12) . . ? N1 C7 O3 122.39(12) . . ? C3 C7 O3 120.86(12) . . ? C3 C7 N1 116.73(11) . . ? H4 C4 C3 119.98(7) . . ? C5 C4 C3 120.04(12) . . ? C5 C4 H4 119.98(8) . . ? H2a C2 C3 120.01(7) . . ? C1 C2 C3 119.97(12) . . ? C1 C2 H2a 120.01(8) . . ? C2 C1 C6 121.35(12) . . ? H1b C1 C6 119.33(7) . . ? H1b C1 C2 119.33(8) . . ? C4 C5 C6 121.19(12) . . ? H5 C5 C6 119.40(8) . . ? H5 C5 C4 119.40(8) . . ? H8a C8 N1 109.5 . . ? H8b C8 N1 109.5 . . ? H8b C8 H8a 109.5 . . ? H8c C8 N1 109.5 . . ? H8c C8 H8a 109.5 . . ? H8c C8 H8b 109.5 . . ? O2 B1 O1 118.02(11) . . ? C6 B1 O1 122.26(12) . . ? C6 B1 O2 119.72(12) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 H1 0.8200 . ? O1 B1 1.3688(17) . ? O2 H2 0.8200 . ? O2 B1 1.3619(18) . ? O3 C7 1.2366(17) . ? N1 H1a 0.8600 . ? N1 C7 1.3350(18) . ? N1 C8 1.4570(16) . ? C3 C7 1.5063(17) . ? C3 C4 1.3901(19) . ? C3 C2 1.3952(19) . ? C6 C1 1.3969(19) . ? C6 C5 1.4004(18) . ? C6 B1 1.5693(18) . ? C4 H4 0.9300 . ? C4 C5 1.3919(18) . ? C2 H2a 0.9300 . ? C2 C1 1.3893(18) . ? C1 H1b 0.9300 . ? C5 H5 0.9300 . ? C8 H8a 0.9600 . ? C8 H8b 0.9600 . ? C8 H8c 0.9600 . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 -1 0.43 0.96 0 0 -2 0.55 1.32 0 0 -3 -0.21 1.48 0 0 4 574.03 26.85 0 0 -5 2.73 1.46 0 0 5 1.71 2.91 0 0 5 0.27 1.35 0 0 6 232.37 30.48 0 0 -6 289.62 12.16 0 0 -7 0.91 1.09 0 0 -8 64.09 3.86 0 0 8 60.04 4.09 0 1 -1 113.33 5.05 0 -1 -1 114.84 6.1 0 -1 -2 610.31 22.33 0 1 -2 604.97 20.84 0 -1 -3 826.49 29.96 0 1 -3 804.16 27.92 0 -1 -4 32.33 4.8 0 -1 4 40.19 6.04 0 1 5 487.55 27.7 0 1 5 500.45 18.1 0 1 -5 526.46 17.56 0 -1 5 459.15 40.1 0 -1 5 453.79 17.72 0 -1 -5 490.02 17.36 0 1 -6 222.33 10.27 0 -1 -6 226.42 10.4 0 1 6 206.33 29.44 0 -1 6 193.26 28.55 0 -1 -7 4.16 1.39 0 1 -7 4.02 1.43 0 1 -8 13.66 1.75 0 -1 -8 13.39 1.79 0 -2 0 440.46 14.64 0 -2 0 429.35 12.9 0 -2 -1 47.75 4.03 0 -2 1 45.52 2.59 0 -2 1 44.64 5.25 0 -2 -2 938.12 32.18 0 2 -2 957.67 28.97 0 -2 -3 602.51 25.39 0 2 -3 665.07 22.52 0 -2 3 633.86 24.43 0 -2 -4 603.57 26.92 0 -2 4 653.53 27.72 0 -2 5 181.32 9.1 0 2 5 153.35 8.4 0 -2 -5 168.29 8.3 0 -2 5 149.71 23.03 0 2 -5 175.01 8.32 0 2 5 191.06 16.31 0 -2 -5 166.57 7.65 0 -2 -6 34.59 3.67 0 2 -6 36.05 3.67 0 -2 6 32.33 4.05 0 -2 -7 77.51 5.29 0 2 -7 79.38 5.22 0 -2 -8 5.24 1.23 0 2 -8 6.19 1.27 0 -2 8 6.83 1.5 0 -3 0 1.43 1.41 0 -3 0 0.29 0.64 0 -3 1 594.93 16.16 0 -3 1 647.08 24.65 0 -3 -1 597.7 20.19 0 3 -2 199.27 8.14 0 -3 2 189.62 8.66 0 -3 2 204.34 15.66 0 -3 -2 201.5 11.56 0 -3 3 3271.32 88.75 0 -3 -3 2906.21 91.34 0 -3 4 165.42 11.8 0 -3 4 160.02 20.11 0 -3 -4 131.65 11.29 0 3 5 85.51 11.18 0 -3 -5 84.7 5.16 0 -3 5 81.92 16.31 0 -3 -5 90.82 5.77 0 -3 5 92.51 6.19 0 3 -5 101.31 5.89 0 3 -6 514.75 18.22 0 -3 -6 503.56 18.39 0 -3 -6 504.24 17.4 0 -3 6 510.35 19.5 0 -3 6 444.91 43.18 0 -3 -7 112.79 6.65 0 3 -7 117.77 6.5 0 3 -8 7.78 1.29 0 -3 -8 8.13 1.51 0 -3 8 8.42 1.71 0 -4 0 1331.89 38.71 0 -4 0 1442.4 42.68 0 -4 1 363.97 19.31 0 -4 -1 373.52 15.43 0 4 1 375.05 10.49 0 -4 2 1008.79 42.92 0 -4 2 1026.59 30.34 0 4 -2 1005.22 28.74 0 -4 -2 1052.15 35.72 0 -4 -3 11.24 3.31 0 -4 3 19.11 7.92 0 -4 3 14.17 2.72 0 -4 -4 47.97 7.07 0 -4 4 47.5 11.72 0 4 -5 230.79 9.78 0 4 5 185.93 17.27 0 -4 5 183.13 25.43 0 -4 5 220.71 10.49 0 -4 -5 220.21 9.86 0 -4 -5 204.92 9.16 0 -4 6 6.11 2.29 0 4 -6 3.04 1.55 0 -4 -6 4.69 1.61 0 -4 -6 5.33 1.81 0 4 -7 61.92 4.42 0 -4 -7 67.28 4.94 0 -4 -8 5.96 1.32 0 -4 8 5.23 1.31 0 -5 0 -1.43 2.15 0 -5 0 0.21 1.16 0 -5 -1 9184.45 242.58 0 5 1 8942.06 235.46 0 -5 1 9349.19 250.4 0 -5 -2 873.76 30.75 0 -5 2 808.19 23.6 0 -5 2 849.41 38.1 0 -5 3 642.38 38.07 0 -5 3 702.33 24.27 0 -5 -3 670.96 29.44 0 -5 4 253.75 26.42 0 -5 -4 268.03 17.84 0 5 5 10.57 4.17 0 -5 -5 4.74 1.53 0 5 -5 6.33 1.6 0 -5 5 4.41 1.73 0 -5 -5 5.25 1.39 0 -5 -6 98.55 6.03 0 -5 6 100.6 7.12 0 -5 -6 104.06 6.63 0 5 -6 108.1 6.31 0 -5 -7 9.04 1.7 0 5 -7 7.89 1.55 0 -5 7 12.17 2.42 0 -5 -7 11.54 2.05 0 -5 -8 58.1 3.69 0 -5 8 52.88 3.75 0 -6 0 1133.88 39.26 0 -6 0 1107.64 33.92 0 -6 1 9597.65 250.93 0 -6 -1 9999 242.16 0 -6 -2 564.83 24.26 0 -6 2 529.23 30.33 0 -6 3 723.89 40.95 0 -6 -3 710.53 31.07 0 -6 -4 1.21 2.04 0 -6 4 1.45 5.67 0 -6 5 24.63 9.63 0 -6 5 17.42 2.82 0 -6 -5 17.47 2.4 0 -6 -5 22.71 2.88 0 6 5 17.17 5.75 0 -6 6 360.09 15.69 0 -6 -6 372.77 14.67 0 -6 -6 373.88 14.12 0 -6 -7 210.39 9.53 0 -6 7 201.18 9.92 0 -6 -7 193.36 8.56 0 -6 8 0.51 0.8 0 -6 8 -1.08 0.89 0 -6 -8 0.56 0.79 0 -7 0 4.11 3.44 0 -7 0 1.15 1.54 0 -7 -1 101.75 8.19 0 -7 1 110.5 11.48 0 7 1 106.18 4.73 0 -7 2 3996.17 133.62 0 -7 -2 4452.87 123.79 0 -7 3 7.93 4.61 0 -7 -3 7.78 3.4 0 -7 4 8.64 5.79 0 -7 -4 6.23 3.56 0 -7 5 0.2 1.39 0 -7 -5 0.28 1 0 -7 -5 -0.73 1.35 0 -7 -5 3.83 2.87 0 7 5 -0.09 3 0 -7 -6 85.25 5.9 0 -7 -6 88.48 5.67 0 -7 6 95.92 6.86 0 -7 -7 294.59 11.72 0 -7 7 288.28 12.26 0 -7 -7 268.82 10.87 0 -7 -8 27.03 2.36 0 -7 8 24.49 2.36 0 -7 8 22.37 2.13 0 -8 0 2363.71 68.64 0 -8 0 2460.19 77.04 0 8 1 391.83 13.35 0 -8 -1 447.32 19.55 0 -8 1 465.1 25.48 0 -8 2 1982.06 76.6 0 -8 -2 2078.3 66.51 0 -8 -3 26.93 5.93 0 -8 3 29.94 9.05 0 -8 4 1.03 4.18 0 -8 -4 -1 2.73 0 -8 -5 90.98 5.75 0 -8 -5 88.27 5.75 0 -8 -5 87.08 11.48 0 -8 5 90.66 6.51 0 -8 5 88.44 18.5 0 8 5 92.47 13.09 0 -8 6 65.6 5.56 0 -8 6 68.59 5.7 0 -8 -6 61.68 4.87 0 -8 -6 63 4.85 0 -8 -7 71.98 4.77 0 -8 -7 80.22 5.21 0 -8 7 87.71 5.9 0 -8 8 1.11 0.78 0 -8 -8 1.28 0.7 0 -8 8 1.95 1 0 -9 0 0.58 2.7 0 -9 0 1.92 1.76 0 -9 1 1379.41 52.12 0 -9 -1 1349.56 44 0 -9 -2 625.91 27.86 0 -9 2 519.16 33.31 0 -9 3 512.96 36.54 0 -9 -3 521.6 27.42 0 -9 4 307.76 30.96 0 -9 -4 322.42 22.53 0 -9 -5 18.08 5.78 0 -9 5 26.58 3.47 0 -9 5 27.06 11.03 0 -9 5 29.21 3.66 0 -9 -5 26.82 3.17 0 -9 -5 23.58 2.91 0 9 5 24.77 7.58 0 -9 6 55.24 5.14 0 -9 -6 54.88 4.6 0 -9 6 65.83 5.57 0 -9 -6 58.57 4.6 0 -9 -7 29.54 2.87 0 -9 7 28.49 3.3 0 -9 -7 26.41 2.84 0 -9 8 21.1 1.94 0 -9 -8 19.66 1.87 0 -9 8 22.23 2.16 0 -10 0 96.98 11.4 0 -10 0 84.96 7.23 0 -10 1 909.95 42.4 0 10 1 878.17 27.53 0 -10 2 364.76 27.57 0 -10 -2 371.62 21.28 0 -10 3 66.12 13.23 0 -10 -3 72.68 9.73 0 -10 4 517.3 18.34 0 -10 4 463.58 39.61 0 -10 -4 473.38 29.04 0 -10 4 510.99 18.26 0 -10 -4 514.07 17.43 0 -10 -5 18.4 2.63 0 -10 -5 20.13 2.66 0 -10 5 21.66 3.12 0 10 5 21.68 6.75 0 -10 -5 12.22 5.83 0 -10 5 19.59 3.05 0 -10 -6 4.82 1.59 0 -10 -6 5.13 1.63 0 -10 6 6.64 2.34 0 -10 6 5.23 2.09 0 -10 -7 4.53 1.5 0 -10 -7 5.32 1.48 0 -10 7 4.91 1.59 0 -10 8 24.99 1.99 0 -10 -8 25.22 2.01 0 -11 0 -0.3 3.75 0 -11 0 0.72 1.52 0 -11 1 533.3 31.35 0 -11 -1 525.21 24.51 0 -11 -2 -0.23 2.23 0 -11 2 2.7 4.75 0 -11 3 876.38 52.19 0 -11 -3 970.34 42.41 0 -11 -4 89.89 5.37 0 -11 4 85.71 5.9 0 -11 -4 103.73 12.71 0 -11 4 82.56 5.72 0 -11 4 73.48 15.07 0 -11 5 8.61 2.31 0 -11 -5 7.97 1.97 0 -11 -5 5.34 1.8 0 -11 -5 4.58 3.12 0 -11 5 15.18 11.83 0 -11 5 10.07 2.45 0 11 5 3.15 4.29 0 -11 -6 52.84 4.53 0 -11 6 65.7 5.48 0 -11 6 56.6 5 0 -11 -6 59.55 4.58 0 -11 -7 63.8 4.22 0 -11 7 61.87 4.3 0 -11 -7 59.3 4.12 0 -11 7 65.79 4.8 0 -11 8 3.45 0.84 0 -12 0 207.14 12.94 0 -12 0 229.36 19.58 0 -12 1 534.82 32.73 0 -12 -1 495.47 24.7 0 -12 2 1310.35 61.25 0 -12 -2 1334.25 51.59 0 -12 3 737.81 47.23 0 -12 -3 759.2 37.44 0 -12 4 13.92 2.42 0 -12 -4 10.35 1.96 0 -12 4 11 6.88 0 -12 4 11.09 2.23 0 -12 -4 4.9 2.84 0 -12 -4 11.83 1.9 0 -12 -5 25.96 7.18 0 -12 -5 32.79 3.52 0 -12 5 38.94 4.23 0 -12 -5 36.24 3.54 0 -12 5 31.35 3.78 0 -12 -6 3.78 1.69 0 -12 6 4.87 1.99 0 -12 -6 1.42 1.23 0 -12 6 6.71 2.22 0 -12 -7 79.86 4.69 0 -12 7 89.38 5.45 0 -12 -7 78.21 4.71 0 -12 7 85.88 4.98 0 -13 0 0.98 1.77 0 -13 -1 1597.79 56.98 0 -13 1 1670.12 68.61 0 -13 -2 43.19 7.6 0 -13 2 59.15 11.95 0 -13 3 182.12 10.25 0 -13 3 187.81 10.63 0 -13 -3 174.71 16.54 0 -13 3 148.4 20.29 0 -13 3 192.1 8.9 0 -13 -4 74.87 4.86 0 -13 -4 71.64 11.22 0 -13 -4 65.39 4.85 0 -13 4 71.81 5.47 0 -13 4 66.79 14.68 0 -13 4 73.41 5.49 0 -13 5 77.02 5.99 0 -13 -5 72.71 5.1 0 -13 5 76.83 5.86 0 -13 -5 73.36 5.36 0 -13 -6 61.85 4.53 0 -13 -6 62.79 4.79 0 -13 6 67.46 4.88 0 -13 6 67.42 5.34 0 -13 6 62.66 5.17 0 -13 -7 -0.24 0.75 0 -13 7 1.17 0.9 0 -13 -7 0.01 0.84 0 -14 0 961.53 36.91 0 -14 -1 21.25 5.1 0 -14 1 59.31 10.95 0 -14 -2 236.23 18.33 0 -14 2 246.01 24.68 0 -14 -3 60.46 4.29 0 -14 3 52.48 5.76 0 -14 -3 65.64 10.35 0 -14 3 69.21 5 0 -14 3 50.66 5.48 0 -14 3 52.67 13.24 0 -14 3 62.66 4.24 0 -14 -4 103.15 13.69 0 -14 4 98.99 6.49 0 -14 4 91.05 18.09 0 -14 -4 88.62 5.74 0 -14 4 90.32 6.29 0 -14 -5 32.64 3.48 0 -14 -5 32.79 3.25 0 -14 5 35.18 4.05 0 -14 5 29.39 3.2 0 -14 5 33.79 3.93 0 -14 -6 67.51 4.89 0 -14 -6 59.85 4.23 0 -14 6 61.71 4.96 0 -14 6 66.68 4.73 0 -14 6 68.34 5.25 0 -14 -7 5.38 1.42 0 -14 -7 4.55 1.18 0 -14 7 4.68 1.27 0 -15 0 1.28 1.59 0 -15 1 944.96 50.7 0 -15 -1 912.65 39.42 0 -15 2 14.5 3.08 0 -15 2 16.04 7.75 0 -15 -2 8.43 4.08 0 -15 2 16.49 3.14 0 -15 3 101.45 17.75 0 -15 3 104.7 5.89 0 -15 3 135.34 9.09 0 -15 3 93.52 8.07 0 -15 -3 106.48 13.66 0 -15 -3 116.17 6.31 0 -15 -4 116.92 14.98 0 -15 4 135.99 7.9 0 -15 -4 127.42 7.08 0 -15 4 138.93 7.21 0 -15 4 126.2 7.47 0 -15 -5 24.87 2.77 0 -15 5 23.67 3.22 0 -15 5 21.97 2.86 0 -15 5 23.78 3.28 0 -15 -5 23.04 3.04 0 -15 -6 9.61 2.05 0 -15 6 8.76 1.73 0 -15 -6 9.05 1.7 0 -15 6 10.87 2.27 0 -15 -7 3.4 0.79 0 -15 -7 4.2 1.14 0 -15 7 3.9 1.02 0 -16 0 72.39 8.55 0 -16 -1 198.51 11.9 0 -16 1 216.45 11.17 0 -16 1 224.14 12.24 0 -16 1 236.25 10.55 0 -16 1 240.68 12.41 0 -16 -1 233.97 17.6 0 -16 1 269.25 26.21 0 -16 2 1211.12 38.42 0 -16 2 1203.37 39.96 0 -16 -2 1191.48 37.91 0 -16 2 1237.45 64.64 0 -16 -2 1281.91 52.79 0 -16 2 1222.12 40.31 0 -16 3 44.55 12.22 0 -16 -3 52.12 9.91 0 -16 -3 61.56 4.37 0 -16 3 48.79 5.91 0 -16 3 51.5 3.94 0 -16 -4 21.45 2.81 0 -16 4 25.7 2.96 0 -16 -5 21.21 2.84 0 -16 5 21.71 2.76 0 -16 5 22.57 3.11 0 -16 6 2.89 1.18 0 -16 6 0.44 0.93 0 -16 6 4.33 1.4 0 -16 -6 3.96 1.55 0 -16 7 89.14 4.19 0 -16 -7 89.39 4.42 0 -17 0 -0.88 1.13 0 -17 0 -1.52 1.41 0 -17 0 0.26 1.82 0 -17 0 -1.36 2.32 0 -17 0 -2.43 2.15 0 -17 0 5.52 1.87 0 -17 -1 100.27 6.35 0 -17 -1 99.89 11.49 0 -17 1 103.42 8 0 -17 -1 98.41 7.15 0 -17 1 89.05 6.27 0 -17 -1 104.36 7.71 0 -17 -1 97.67 5.64 0 -17 -1 95.89 8.11 0 -17 1 77.58 7.09 0 -17 1 92.46 7.14 0 -17 2 2.41 2.38 0 -17 2 0.59 1.85 0 -17 2 1.88 1.38 0 -17 -2 2.99 1.93 0 -17 -2 7.78 3.29 0 -17 2 2.17 2.07 0 -17 2 8.2 6.66 0 -17 -3 247.22 12.1 0 -17 3 217.99 26.9 0 -17 3 240.32 13.53 0 -17 -3 269.46 22.81 0 -17 -3 263.19 10.69 0 -17 -4 63.31 4.72 0 -17 4 63.58 4.59 0 -17 5 84.87 5.61 0 -17 5 76.34 5.01 0 -17 -5 74.94 5.17 0 -17 6 17.27 2.06 0 -17 -6 19.09 2.33 0 -17 6 16.53 2.29 0 -17 -7 9.03 2.05 0 -18 0 231.56 12.29 0 -18 0 244.2 10.18 0 -18 0 240.46 11.16 0 -18 0 234.69 12.98 0 -18 0 226.21 13.26 0 -18 -1 1.74 1.8 0 -18 -1 1.43 2.08 0 -18 -1 7.08 4.59 0 -18 1 5.13 2.69 0 -18 -1 3.82 1.69 0 -18 1 1.57 1.75 0 -18 1 2.18 2.27 0 -18 -1 0.13 2.61 0 -18 1 3.49 1.66 0 -18 -1 5.22 1.69 0 -18 -2 4.57 3.04 0 -18 2 9.91 2.85 0 -18 -2 4.61 3.12 0 -18 2 7.21 3.07 0 -18 2 6.59 1.9 0 -18 2 5.89 5.39 0 -18 2 6.17 2.76 0 -18 -2 14.63 3.08 0 -18 -3 45.19 3.74 0 -18 3 40.82 4.5 0 -18 -3 32.3 8.38 0 -18 3 42.48 5.47 0 -18 -3 31.94 4.21 0 -18 4 153.62 7.55 0 -18 -4 155.22 7.84 0 -18 -5 51.02 4.09 0 -18 5 46.43 4.42 0 -18 5 52.23 3.9 0 -18 6 37.3 2.78 0 -18 -6 38.86 3.09 0 -18 6 28.91 2.8 0 -19 0 0.93 1.53 0 -19 0 1.27 2.07 0 -19 0 1.52 2.34 0 -19 0 0.98 2.98 0 -19 0 0.43 1.29 0 -19 -1 77.32 6.84 0 -19 1 71.34 7.31 0 -19 -1 76.62 5.29 0 -19 -1 71.61 7.34 0 -19 -1 74.09 6.71 0 -19 -1 79.7 11.01 0 -19 1 75.16 7.2 0 -19 -1 77.68 5.93 0 -19 1 80.54 6.13 0 -19 1 72.33 6.65 0 -19 2 99.28 8.56 0 -19 2 86.43 7.77 0 -19 -2 107.09 9.21 0 -19 2 98.13 6.94 0 -19 -2 87.3 7.22 0 -19 2 107.63 18.97 0 -19 2 104.47 7.78 0 -19 -2 104.23 13.77 0 -19 -3 4.78 2.96 0 -19 -3 6.28 1.67 0 -19 -3 7.04 2.04 0 -19 3 13.72 3.92 0 -19 3 9.86 2.52 0 -19 -4 11.14 1.94 0 -19 4 9.95 2.29 0 -19 -5 115.08 6.21 0 -19 5 110.03 6.77 0 -19 5 120.28 5.97 0 -19 -6 29.86 4.07 0 -19 6 24.83 2.11 0 -19 6 24.94 2.38 0 -19 -6 27.51 2.41 0 -20 0 327.56 12.94 0 -20 0 327.73 16.37 0 -20 0 315.55 16.78 0 -20 0 323.75 14.08 0 -20 0 316.32 15.55 0 -20 -1 7.43 3.94 0 -20 -1 6.15 2.78 0 -20 1 13.49 4.19 0 -20 -1 7 2.94 0 -20 1 6.61 1.91 0 -20 1 7.86 3.07 0 -20 -1 5.48 3.05 0 -20 -1 11.7 2.5 0 -20 1 8.13 2.97 0 -20 2 399.29 18.79 0 -20 2 408.09 16.56 0 -20 -2 359.73 16.98 0 -20 2 398.88 19.26 0 -20 -2 375.44 19.39 0 -20 2 420.96 17.89 0 -20 -3 313.74 14.49 0 -20 -3 326.11 17.61 0 -20 3 359.98 17.17 0 -20 3 334.12 14.65 0 -20 -4 1.68 1.13 0 -20 -4 3.63 3.07 0 -20 4 3.29 1.76 0 -20 -5 -0.18 0.8 0 -20 5 1.24 1.05 0 -20 6 0.48 0.87 0 -20 -6 2.79 1.88 0 -21 0 0.08 2.17 0 -21 0 -1.58 3.39 0 -21 0 2.22 2.56 0 -21 0 -1.11 1.54 0 -21 0 0.74 1.68 0 -21 -1 153.46 10.19 0 -21 1 155.63 10.29 0 -21 -1 158.47 8.07 0 -21 -1 163.07 11.62 0 -21 1 148.46 8.96 0 -21 1 148.58 10.71 0 -21 1 160.09 8.1 0 -21 -1 146.24 9.99 0 -21 1 143.25 10.71 0 -21 -2 52.23 5.74 0 -21 2 65.46 6.9 0 -21 -2 67.18 7.51 0 -21 2 72.46 5.94 0 -21 -3 48.43 6.44 0 -21 3 63.19 6.75 0 -21 -3 59.56 5.37 0 -21 3 54.35 5.12 0 -21 4 -0.15 1.27 0 -21 -4 -0.46 0.96 0 -21 5 8.65 1.81 0 -21 -5 7.43 2.63 0 -21 -5 7.73 1.44 0 -21 -6 1.69 1.46 0 -22 0 198.5 12.17 0 -22 0 198.73 11.88 0 -22 0 187.54 9.1 0 -22 0 190.62 12.57 0 -22 0 184.96 10.14 0 -22 1 482.97 17.35 0 -22 1 495.72 21.76 0 -22 1 472.57 18.77 0 -22 1 456.07 20.12 0 -22 1 476.99 21.45 0 -22 -1 480.62 22.29 0 -22 -1 473.86 20.33 0 -22 -1 511.65 20.74 0 -22 -2 5.11 2.42 0 -22 -2 5.57 3.49 0 -22 2 8.26 2.4 0 -22 2 9.49 3.44 0 -22 -3 6.24 2.19 0 -22 -3 7.06 3.54 0 -22 3 5.72 2.26 0 -22 3 15.04 4.03 0 -22 4 29.44 3.39 0 -22 -4 27.51 4.94 0 -22 5 5.2 1.51 0 -22 -5 0.59 1.72 0 -23 0 4.74 2.55 0 -23 0 -1.21 2.14 0 -23 0 0.06 1.59 0 -23 0 4 1.92 0 -23 0 1.79 2.69 0 -23 1 147.26 10.58 0 -23 1 126.96 7.11 0 -23 -1 126.4 10.12 0 -23 1 143.69 9.75 0 -23 -1 131.1 9.31 0 -23 1 136.19 8.44 0 -23 2 -3.75 2.87 0 -23 2 0.39 1.04 0 -23 -2 2.25 2.09 0 -23 2 1.48 1.87 0 -23 -2 2.24 2.88 0 -23 -3 4.24 2.11 0 -23 3 2.66 1.54 0 -23 4 322.38 12.71 0 -23 -4 314.05 15.18 0 -23 5 34.44 2.79 0 -23 -5 40.74 4.08 0 -24 0 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3 5.56 1.94 1 -22 -3 6.86 2.99 -1 -22 2 311.34 15.46 1 -22 -2 328.47 17.33 1 -22 -2 304.54 14 -1 -22 2 311.03 14.87 1 -22 -2 301.63 14.87 -1 -22 2 332.67 13.25 -1 -22 2 313.16 13.96 -1 -22 1 15.39 2.93 1 -22 -1 16.48 3.2 -1 -22 1 18.33 3.65 -1 -22 1 14.08 3.93 1 -22 -1 18.78 4.74 1 -22 -1 15.14 3.47 -1 -22 1 14.84 2.42 1 -22 0 72.64 7.23 -1 -22 0 79.93 5.84 -1 -22 0 71.45 7.01 1 -22 0 83.66 8.17 -1 -22 0 76.94 7.35 1 -22 0 75.4 5.87 1 -22 1 1.05 1.71 -1 -22 -1 3.16 2.5 1 -22 1 -1.83 2.62 1 -22 1 -1.3 2.33 1 -22 2 1.49 1.6 -1 -22 -2 -1.49 1.82 1 -22 2 2.44 2.9 -1 -22 -2 2.15 2.82 1 -22 2 -0.54 2.22 1 -22 3 209.47 10.27 -1 -22 -3 195.82 11.93 -1 -22 -3 187.54 10.33 1 -22 4 10.2 2.01 -1 -22 -4 11.99 2.93 1 -22 5 52.35 3.62 -1 -22 -5 53.74 4.43 -1 -22 -5 54.29 2.92 1 -23 -5 169.47 8.9 -1 -23 5 185.72 7.32 1 -23 -4 34.46 4.71 -1 -23 4 39.96 3.51 1 -23 -3 26.73 4.44 -1 -23 3 25.15 3.24 -1 -23 3 29.05 3.13 -1 -23 2 33.37 3.97 1 -23 -2 41.1 6.16 -1 -23 2 35.81 3.65 -1 -23 2 31.78 4.47 -1 -23 2 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103.63 7.98 -1 -26 1 109.32 7.39 -1 -26 1 106.09 6 -1 -26 0 9.11 2.7 1 -26 0 10.68 3.02 -1 -26 0 14.93 3.12 1 -26 0 11.57 2.98 -1 -26 -1 71.84 5.93 1 -26 1 76.09 6.6 -1 -26 -1 74.45 6.17 1 -26 1 74.26 5.01 -1 -26 -2 22.8 3.24 -1 -26 -2 32.5 3.56 1 -26 2 31.05 3.02 -1 -26 -3 27.79 2.77 -1 -26 -3 31.87 3.33 1 -27 -3 22.36 2.99 -1 -27 3 28.42 2.31 1 -27 -2 28.63 3.81 -1 -27 2 33.02 2.88 -1 -27 1 14.6 2.57 1 -27 -1 17.14 3.19 1 -27 0 330.25 14.52 -1 -27 0 301.52 13.25 -1 -27 0 323.9 13.6 -1 -27 -1 33.13 3.7 1 -27 1 39.9 4.39 -1 -27 -1 37.32 4.04 -1 -27 -2 25.3 3.01 -1 -27 -2 22.97 2.79 1 -27 2 25.03 2.54 1 -27 3 6.84 1.22 1 -28 -2 -0.06 1.41 -1 -28 1 85.79 5.33 1 -28 -1 84.91 6.06 -1 -28 0 0.5 1.29 1 -28 0 0.39 1.64 -1 -28 0 4.36 1.86 1 -28 1 25.41 3.3 -1 -28 -1 20.21 2.63 -1 -28 -1 23.91 2.75 1 -29 -1 3.09 1.31 1 -29 0 14.63 2.27 2 0 -8 21.99 2.2 2 0 -8 20.01 1.92 2 0 -7 0.73 0.97 2 0 -6 7.07 1.96 2 0 -5 0.03 1.06 2 0 -5 -13.45 5.61 2 0 -4 125.16 14.94 2 0 -3 -0.26 1.36 2 0 -2 835.02 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23.06 -2 1 -4 147.19 8.71 -2 1 -5 -0.7 1.48 -2 -1 -5 2.11 1.85 2 -1 5 -1.21 1.55 2 -1 6 64.02 5.04 -2 1 -6 66 5.2 -2 -1 -6 63.7 5.28 -2 1 -7 77.12 4.74 -2 -1 -7 76.34 4.72 2 -2 -8 25.01 2.24 2 -2 -8 23.71 2.23 2 2 -8 23.26 2.27 2 2 -7 179.23 8 2 -2 -7 175.64 8.4 -2 -2 6 6.71 1.62 2 -2 -6 5.95 1.5 2 2 -6 5.68 1.68 -2 -2 5 15.47 2.25 2 -2 -5 16.19 5.81 2 2 -5 18.93 2.46 2 -2 -5 16.23 2.34 2 -2 -4 468.87 30.99 2 2 -4 380.53 27 2 2 -4 417.26 21.82 2 -2 -3 0.49 1.14 2 2 -3 -1.59 1.64 2 -2 -2 70.15 6.27 2 2 -2 60.62 6.74 2 -2 -1 8.45 2.32 2 2 -1 8.61 2.63 2 2 0 151.67 10.22 2 -2 0 156.83 10.27 2 -2 1 56.5 9.17 2 2 1 63.78 7.95 2 2 1 55.52 6.28 2 -2 1 58.71 6.85 2 -2 2 120.53 10.83 2 -2 2 98.09 10.91 2 2 2 121.44 12.17 2 2 2 131.89 10.66 2 -2 3 131.09 19.79 2 2 3 116.65 13.33 2 -2 3 102.77 12.16 2 -2 4 113.66 7.2 2 -2 4 74.7 18.48 -2 -2 -4 100.47 6.74 2 -2 4 102.27 13.44 2 -2 4 85.86 6.11 2 2 4 92.75 13.39 -2 2 -4 95.45 6.67 -2 2 -5 13.58 2.9 -2 -2 -5 13.71 2.68 2 -2 5 10.85 2.44 -2 2 -6 192.8 9.68 2 -2 6 201.03 9.83 -2 -2 -6 201.34 9.96 -2 -2 -7 112.32 5.9 -2 2 -7 109 5.7 2 -3 -8 15.66 1.68 2 3 -8 18.65 2.11 2 -3 -8 16.08 1.82 2 -3 -7 18.32 2.59 -2 -3 7 19.24 2.3 -2 -3 6 127.19 6.86 2 -3 -6 116.02 6.96 -2 -3 5 252.72 10.53 2 -3 -5 253.8 23.26 2 -3 -5 243.53 10.75 2 -3 -4 263.99 22.81 2 3 -4 247.39 16.54 2 3 -3 630.42 27.81 2 -3 -3 638.98 35.36 2 -3 -2 525.33 20.49 2 3 -2 494.99 22.88 2 -3 -1 73.27 6.52 2 3 -1 75.74 7.34 2 -3 0 1.3 1.74 2 3 0 0.08 1.75 2 -3 0 -0.02 2.52 2 3 0 4.86 2.86 2 3 1 244.98 14.02 2 3 1 218.02 15.29 2 -3 1 233.41 19.54 2 -3 1 238.57 14.55 2 -3 2 837.14 46.32 2 3 2 849.5 32.84 2 3 2 806.05 36.45 2 -3 2 758.16 35.25 2 -3 3 406.38 25.79 2 -3 3 451.14 37.55 2 3 3 449.44 27.62 2 -3 4 75.22 17.82 2 -3 4 93.65 6.35 2 -3 4 80 5.8 2 3 4 68.48 11.62 -2 -3 -4 77.24 5.93 2 -3 4 70.43 11.29 -2 3 -4 81.64 6.11 -2 -3 -5 974.47 31.47 -2 3 -5 916.76 31.29 2 -3 5 988.7 31.41 2 -3 6 2.01 1.56 -2 -3 -6 -0.75 1.4 -2 3 -6 0.61 1.22 -2 -3 -7 101.1 5.5 -2 3 -7 100.54 5.3 2 4 -8 10.42 1.53 2 -4 -8 9.46 1.53 -2 -4 7 17.67 2.32 2 -4 -7 20.99 2.65 2 -4 -6 36.05 3.79 -2 -4 6 38.46 3.66 -2 -4 5 891.13 27.4 2 -4 -5 817.66 45.79 2 -4 -5 857.57 27.51 2 4 -4 15.81 4.45 2 -4 -4 18.04 6.51 2 -4 -3 99.25 12.95 2 4 -3 97.81 9.78 2 -4 -2 213.03 11.18 2 4 -2 205.41 13.61 2 -4 -1 234.2 12.36 2 4 -1 202.49 12.9 2 -4 0 365.97 21.3 2 -4 0 409.28 18.81 2 4 0 378.4 19.87 2 4 0 409.62 18.85 2 4 1 412.06 22.35 2 -4 1 445.88 21.78 2 -4 1 427.55 27.76 2 4 1 462.55 20.45 2 4 2 34.77 5.42 2 4 2 42.29 7.59 2 -4 2 25.68 7.76 2 -4 3 521.82 41.06 2 4 3 501.11 30.25 2 -4 4 20.43 3.03 -2 -4 -4 23.33 3.35 2 -4 4 27.87 3.53 2 4 4 18.98 6.84 -2 4 -4 18.77 2.95 2 -4 4 23.81 12.61 -2 4 -5 1353.32 42.68 2 -4 5 1394.2 42.92 -2 -4 -5 1460.11 43.11 -2 4 -6 4.57 1.7 2 -4 6 5.93 2.06 -2 -4 -6 3.5 1.79 2 -4 7 29.96 2.85 -2 4 -7 31.62 2.68 -2 -4 -7 28.91 2.78 2 5 -8 10.29 1.66 -2 -5 8 7.84 1.2 2 -5 -8 9.75 1.52 -2 -5 7 9.5 1.74 2 -5 -7 8.99 1.66 2 -5 -7 10.57 1.96 -2 -5 6 22.6 2.94 2 -5 -6 18.42 2.69 -2 -5 5 31.01 3.31 2 -5 -5 31.86 3.44 2 -5 -5 35.74 9.25 2 -5 -4 11.41 2 2 5 -4 14.09 4.25 2 -5 -4 6.87 4.74 2 5 -3 1.12 2.34 2 -5 -3 5.86 3.36 2 -5 -2 1201.9 49.72 2 -5 -2 1187.16 37.75 2 5 -2 1170.33 43.07 2 -5 -1 1686 52.52 2 5 -1 1713.48 55.43 2 -5 0 20.78 4.09 2 5 0 24.25 4.12 2 5 0 13.56 3.67 2 -5 0 19.78 5.26 2 -5 1 59.99 10.31 2 5 1 57.86 7.8 2 -5 1 69.99 7.92 2 5 1 72.99 7.16 2 5 2 7.06 2.75 2 5 2 7.45 3.92 2 -5 2 4.88 4.79 2 5 3 144.01 15.48 2 -5 3 158.92 22.36 -2 5 -4 22.83 3.34 2 -5 4 26.45 3.28 2 5 4 18.13 6.66 2 -5 4 27.63 3.49 -2 -5 -4 24.44 3.27 2 -5 4 28.28 11.24 2 -5 5 24.5 3.6 -2 5 -5 21.46 3.09 -2 5 -6 34.46 3.62 2 -5 6 38.77 4 -2 -5 -6 35.07 3.73 2 -5 7 0.47 0.91 -2 -5 -7 -1.04 0.98 -2 5 -7 0.07 0.89 -2 -6 8 8.97 1.2 2 6 -8 8.99 1.43 2 -6 -8 7.8 1.38 -2 -6 7 12.71 2.03 2 -6 -7 14.48 2.26 -2 -6 6 65.72 4.93 2 -6 -6 60.92 4.94 -2 -6 5 150.31 7.78 2 -6 -5 126.77 17.12 2 -6 -5 143.02 7.73 2 6 -5 131.86 13.86 -2 -6 4 40.07 3.44 2 6 -4 31.5 6.35 2 -6 -4 38.76 3.45 2 -6 -4 42.21 9.79 2 -6 -4 38.71 3.53 2 6 -3 20.53 4.88 2 -6 -3 18.88 6.18 2 -6 -2 705.78 36.54 2 -6 -2 717.22 25.22 2 6 -2 729.86 31.14 2 -6 -1 74.85 6.71 2 6 -1 79.07 8.05 2 -6 0 106.99 11.3 2 6 0 97.01 9.2 2 6 0 114.23 9.22 2 -6 0 104.29 8.92 2 -6 1 2828.18 99.15 2 6 1 2763.37 88.15 2 6 1 2833.68 83.68 2 6 2 27.55 4.75 2 -6 2 11.94 5.93 2 6 2 25.17 5.91 -2 -6 -3 7.91 2.45 2 6 3 4.5 3.52 2 6 3 6.28 2.34 2 -6 3 9.95 7.29 -2 -6 -4 114.22 7.09 2 -6 4 123.22 7.19 2 -6 4 107.73 7.12 2 6 4 98.83 14.5 -2 6 -4 110.69 7.27 -2 -6 -5 1.49 1.29 2 -6 5 0.49 1.58 -2 6 -5 -0.34 1.29 -2 6 -6 1.34 1.04 2 -6 6 0.18 1.44 -2 -6 -6 0.92 1.23 2 -6 7 0.42 0.9 -2 -6 -7 1.14 0.94 -2 6 -7 1.3 0.86 -2 -7 8 -0.47 0.6 2 7 -8 -0.71 0.8 2 -7 -8 0.66 0.9 -2 -7 7 59.56 4.25 2 -7 -7 59.68 4.43 -2 -7 6 33.02 3.46 -2 -7 6 31.85 3.35 2 -7 -6 33.25 3.57 -2 -7 5 0.96 1.32 2 7 -5 2.31 3.66 -2 -7 5 3.96 1.65 2 -7 -5 -2.85 3.7 2 -7 -5 2.55 1.23 -2 -7 4 108.14 6.11 2 -7 -4 109.64 6.24 2 -7 -4 101.57 14.62 2 -7 -4 111.33 6.26 2 7 -4 99.5 11.75 2 7 -3 16.45 4.9 2 -7 -3 19.11 6.38 2 -7 -2 806.07 39.18 2 7 -2 771.71 33.4 2 -7 -1 177.63 14.97 2 -7 -1 172.55 10.83 2 7 -1 198.45 13.33 2 -7 0 345.33 22.01 2 -7 0 320.16 19.28 2 7 0 320.27 18.22 2 7 0 360.59 18.07 2 -7 1 108.4 14.68 2 7 1 118.7 11.44 2 7 1 131.18 9.97 2 7 2 1348.52 52.95 2 7 2 1284.76 45.26 2 -7 2 1171.67 62.16 2 -7 3 11.18 8.36 -2 -7 -3 15.95 2.95 2 -7 3 14.79 2.17 2 7 3 17.9 5.85 2 -7 4 27.13 3.25 -2 -7 -4 20.37 2.88 2 7 4 18.01 6.14 2 -7 4 33.19 11.35 2 -7 4 17.96 3.08 -2 7 -4 21.39 3.17 -2 7 -5 215.97 10.75 2 -7 5 228.65 11.38 -2 -7 -5 224.83 10.84 -2 -7 -5 237.6 11.3 2 -7 6 75.35 5.33 2 -7 6 74.42 5.61 -2 -7 -6 75.61 5.31 -2 7 -6 73.32 4.97 2 -7 7 23.76 2.3 -2 -7 -7 25.04 2.29 -2 7 -7 19.59 1.9 -2 -7 -7 22.54 1.91 2 8 -8 31.8 2.43 2 -8 -8 35.39 2.53 -2 -8 8 28.02 2.12 2 -8 -7 16.19 2.36 -2 -8 7 19.03 2.44 -2 -8 6 36.37 3.7 -2 -8 6 41.83 3.93 2 -8 -6 34.79 3.75 -2 -8 5 39.24 3.87 2 8 -5 36.51 7.93 -2 -8 5 44.2 4.01 2 -8 -5 38.55 3.9 -2 -8 4 73.73 5.09 -2 -8 4 81.88 5.32 2 -8 -4 86.25 5.46 2 -8 -4 84.73 13.01 2 -8 -4 82.24 5.32 2 8 -4 78.65 10.94 2 -8 -3 134.84 16.05 2 8 -3 118.65 12.37 2 -8 -2 327.9 23.9 2 8 -2 329.18 20.07 2 -8 -1 1169.36 47.77 2 8 -1 1193.31 43.58 2 8 0 101.69 9.1 2 -8 0 86.6 11.03 2 -8 0 91.26 9.76 2 8 0 97.95 9.54 2 -8 1 610.71 37.93 2 8 1 635.46 30.55 2 8 1 689.92 27.66 2 8 2 0.29 1.31 2 -8 2 2.57 5.34 2 8 2 2.5 3.59 -2 -8 -3 143.22 9.41 2 -8 3 143.22 22.55 2 -8 3 162.41 7.65 2 8 3 148.54 16.64 2 -8 4 871.3 26.3 2 8 4 723.23 43.73 2 -8 4 763.7 26.61 -2 -8 -4 791.03 25.9 -2 8 -4 741.86 26.16 2 -8 4 664.62 56.07 -2 -8 -5 2.15 1.42 2 -8 5 0.93 1.46 -2 8 -5 2.53 1.59 -2 -8 -5 3.66 1.56 2 -8 6 106.08 6.3 2 -8 6 100.43 6.59 -2 -8 -6 101.71 6.09 -2 8 -6 104.37 5.91 2 -8 7 41.46 2.87 -2 -8 -7 38.14 2.76 2 9 -8 10.16 1.37 2 -9 -8 9.55 1.36 -2 -9 7 36.78 3.28 2 -9 -7 37.49 3.43 -2 -9 6 11.86 2.35 2 -9 -6 7.37 2.06 2 9 -5 92.55 12.48 -2 -9 5 101.24 6.38 2 -9 -5 90.57 6.02 2 -9 -5 87.46 13.9 -2 -9 5 96.18 6.27 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3 37.26 4.78 -2 -18 -3 31.76 4.29 2 -18 4 10.24 2.29 -2 -18 -4 9.52 2.5 2 -18 5 115.41 6.16 -2 -18 -5 118.61 5.71 2 -19 -6 121.05 5.39 -2 -19 6 115.68 5.45 -2 -19 5 7.98 1.79 2 -19 -5 6.89 1.64 2 -19 -5 5.72 2.26 -2 -19 4 18.07 2.67 2 -19 -4 22.81 2.86 2 -19 -4 20.11 3.75 -2 -19 3 11.09 2.27 -2 -19 3 7.57 1.99 2 -19 -3 11.3 2.27 2 -19 -3 13.6 3.75 2 -19 -2 3.83 2.81 2 -19 -2 1.56 1.73 -2 -19 2 2.45 2 -2 -19 2 -0.73 1.66 -2 -19 1 324.21 14.51 2 -19 -1 313.63 12.41 2 -19 -1 283.38 15.62 -2 -19 1 300.9 14.82 -2 -19 1 319.2 13.3 -2 -19 0 10.64 2.78 2 -19 0 8.65 3.52 -2 -19 0 7.14 2.81 -2 -19 0 6.85 2.71 2 -19 1 35.84 3.83 -2 -19 -1 36.2 4.56 2 -19 1 30.46 4.85 2 -19 1 27.43 4.6 -2 -19 -1 32.13 4.73 -2 -19 -2 37.07 4.57 2 -19 2 41 5.15 2 -19 2 27.79 4.33 -2 -19 -2 45.5 5.31 2 -19 3 12.19 2.93 2 -19 3 9.14 2.38 -2 -19 -3 15.16 3.42 2 -19 4 272.72 11.19 -2 -19 -4 241.26 11.42 -2 -19 -4 258.3 10.12 2 -19 5 2.47 1.09 2 -19 5 2.5 1.05 -2 -19 -5 3.97 1.02 2 -20 -6 7.52 1.2 -2 -20 6 3.84 0.78 2 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3.09 2 -21 -3 161.43 7.82 2 -21 -3 139.35 9.83 2 -21 -3 162.76 9.5 -2 -21 3 161.22 8.34 -2 -21 2 188.42 10.26 2 -21 -2 192.73 8.81 2 -21 -2 168.32 11.5 -2 -21 2 187.41 10.36 -2 -21 2 192.13 9.56 -2 -21 1 15.54 3.13 2 -21 -1 18.13 4.03 -2 -21 1 17.9 3.42 -2 -21 1 18.01 2.92 -2 -21 0 0.13 1.49 2 -21 0 -1.24 2.21 2 -21 0 5.56 3.03 -2 -21 0 7.99 3.04 -2 -21 0 8.52 2.69 2 -21 1 271.39 14.29 -2 -21 -1 291.84 14.49 2 -21 1 268.1 14.84 2 -21 1 276.52 12.06 2 -21 2 288.24 14.35 2 -21 2 276.09 11.81 -2 -21 -2 274.96 13.87 2 -21 2 281.94 14.54 2 -21 2 282.1 12.26 2 -21 3 106.97 6.59 2 -21 3 114.32 6.46 -2 -21 -3 106.31 7.37 2 -21 4 6.07 1.58 2 -21 4 7.83 1.51 -2 -21 -4 7.35 1.79 -2 -21 -4 8.35 1.33 2 -22 -5 46.96 2.95 -2 -22 5 52.95 3.31 2 -22 -4 2.01 1.15 -2 -22 4 0.06 1.12 2 -22 -3 9.26 2.48 2 -22 -3 7.57 1.57 -2 -22 3 6.48 1.94 2 -22 -2 305.41 15.1 -2 -22 2 327.91 13.92 2 -22 -2 323.29 15.89 -2 -22 2 317.99 14.17 -2 -22 2 332.34 13.39 -2 -22 1 164.39 9.05 2 -22 -1 153.54 10.37 -2 -22 1 166.02 9.99 2 -22 -1 148.56 10.48 -2 -22 1 153.67 8.54 2 -22 0 37.92 5.33 2 -22 0 50.34 6.08 -2 -22 0 48.27 5.39 2 -22 1 191.63 11.9 2 -22 1 199.67 11.48 -2 -22 -1 191.7 11.16 2 -22 1 188.47 9.19 2 -22 2 17.72 2.65 -2 -22 -2 21 3.65 2 -22 2 18.4 2.47 2 -22 2 13.12 3.3 2 -22 3 335.41 12.18 -2 -22 -3 307.76 13.51 2 -22 3 312.03 12.51 2 -22 4 98.53 4.78 -2 -22 -4 88.85 5.26 2 -22 4 95.69 5.2 -2 -23 5 162.53 6.28 -2 -23 4 4.59 1.4 2 -23 -4 1.68 0.79 2 -23 -4 0.75 1.57 -2 -23 4 1.13 0.92 -2 -23 3 2.92 1.5 2 -23 -3 2.36 1.02 2 -23 -3 0.86 1.73 -2 -23 3 2.03 1.25 2 -23 -2 152.71 9.64 -2 -23 2 164.9 8.67 2 -23 -2 170.41 10.4 -2 -23 2 165.19 9.1 -2 -23 2 178.13 8.63 2 -23 -1 99.55 7.91 -2 -23 1 106.74 7.64 2 -23 -1 105.59 8.21 -2 -23 1 103.94 6.65 2 -23 0 5.05 2.56 2 -23 0 5.39 2.5 -2 -23 0 4.38 2.45 2 -23 1 1.91 1.25 2 -23 1 3.22 2.33 2 -23 1 1.21 2.12 -2 -23 -1 -1.24 2.47 2 -23 2 1.12 1.07 -2 -23 -2 3.86 2.23 2 -23 2 1.9 2.11 2 -23 3 10.92 1.94 -2 -23 -3 13.11 2.57 2 -23 4 1.03 0.81 2 -24 -4 36.66 3.45 -2 -24 4 44.89 3.13 -2 -24 3 16.55 2.19 2 -24 -3 13.72 2.62 -2 -24 3 19.7 2.4 2 -24 -2 16.58 3.28 -2 -24 2 19.02 2.93 2 -24 -2 15.99 2.79 -2 -24 2 20.26 2.67 2 -24 -1 7.34 2.7 2 -24 -1 1.4 2.03 -2 -24 1 8.1 2.52 -2 -24 1 11.53 2.62 2 -24 0 196.33 10.92 -2 -24 0 191.79 10.57 2 -24 0 184.86 11.02 2 -24 1 5.8 1.52 2 -24 1 6.19 2.76 2 -24 1 7.62 2.39 -2 -24 -1 9.31 2.6 2 -24 2 0.13 0.83 -2 -24 -2 0.97 1.75 2 -24 2 0.58 1.74 -2 -24 -3 160.37 7.76 2 -24 3 156.16 6.94 -2 -25 4 16.87 1.68 2 -25 -3 -0.71 1.51 -2 -25 3 0.67 1.19 2 -25 -2 12.3 2.36 2 -25 -2 16.9 2.98 2 -25 -1 16.63 3.24 2 -25 -1 22.22 3.65 -2 -25 1 18.53 2.96 -2 -25 0 135.68 8.31 2 -25 0 156.46 9.07 2 -25 0 153.4 9.29 2 -25 1 3.71 1.1 -2 -25 -1 5.63 2.25 2 -25 1 6.72 2.4 2 -25 1 4.79 2.13 -2 -25 -2 97.49 6.22 2 -25 2 100.7 5.14 -2 -25 -3 48.16 3.57 2 -25 3 49.38 3.08 -2 -26 3 118.65 5.41 2 -26 -2 87.55 5.77 2 -26 -2 75.04 5.02 -2 -26 2 88.41 4.93 2 -26 -1 10.41 2.5 2 -26 -1 12.78 2.47 -2 -26 1 10.05 2.17 2 -26 0 23.31 3.28 2 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335.34 13.54 4 -9 -2 322.36 13.25 4 -9 -1 0.87 1.21 4 9 -1 2.85 1.4 -4 -9 1 3.59 2.25 4 -9 -1 3.68 1.68 4 -9 -1 1.81 1.53 4 9 0 17.07 2.47 -4 -9 0 16.66 3.27 4 -9 0 14.64 2.46 -4 -9 0 15.79 2.84 -4 -9 -1 8.54 2.99 4 -9 1 8.94 2.15 -4 -9 -1 10.47 2.78 -4 -9 -2 219.29 13.02 4 -9 2 254.89 11.16 -4 -9 -2 252.6 12.46 4 -9 3 15.23 2.51 4 -9 3 12.17 2.35 -4 -9 -3 14.4 3.08 4 -9 4 143.79 6.93 -4 9 -4 143.16 7.33 -4 -9 -4 154.94 8.21 -4 -9 -5 -0.52 0.98 4 10 -6 38.5 2.85 4 -10 -6 32.15 2.41 4 -10 -6 32.75 2.79 4 10 -5 2.89 1.2 4 -10 -5 4.11 1.33 4 -10 -5 3.14 1.35 4 10 -4 10.24 2.07 4 -10 -4 7.01 1.76 4 -10 -4 4.77 1.76 4 10 -3 249.86 10.73 -4 -10 3 275.34 12.92 4 -10 -3 244.29 11.14 4 -10 -3 235.47 10.92 4 10 -2 83.61 5.49 -4 -10 2 83.93 6.84 4 -10 -2 81.21 5.88 4 -10 -2 81.53 5.69 4 10 -1 355.22 13.22 -4 -10 1 331.32 15.54 4 -10 -1 335.31 13.77 4 -10 -1 328.33 13.16 -4 -10 0 -0.6 1.82 4 -10 0 1.03 1.4 -4 -10 0 1.44 1.84 -4 -10 -1 4.32 2.46 4 -10 1 4.73 1.91 -4 -10 -1 3.03 1.66 -4 -10 -2 8.1 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320.76 14.48 4 -13 3 64.93 4.45 4 -13 3 74.42 5.03 -4 13 -3 68.06 4.73 -4 -13 -3 77.96 5.74 4 -13 4 41.44 3.09 -4 -13 -4 43.22 3.73 -4 -14 5 47.36 4.04 4 -14 -5 43.62 3.2 4 -14 -5 42.56 3.21 -4 -14 4 1.37 1.52 4 -14 -4 0.98 1.36 4 -14 -4 0.71 1.16 -4 -14 3 6.27 2.38 4 -14 -3 8.43 2.22 4 -14 -3 6.18 1.59 -4 -14 2 3.47 2.29 4 -14 -2 2.08 1.58 4 -14 -2 5.74 1.8 -4 -14 1 8.54 2.84 4 -14 -1 7.67 2.02 -4 -14 0 48.59 5.59 4 -14 0 50.71 4.37 -4 -14 0 56.22 5.04 -4 -14 -1 6.68 3.21 4 -14 1 3.35 1.39 -4 -14 -1 1.18 1.84 -4 -14 -2 296.79 14.69 4 -14 2 324.12 12.16 -4 -14 -2 293.19 13.41 4 -14 3 33.03 2.97 4 -14 3 29.29 3.04 -4 14 -3 33.5 3 -4 -14 -3 22.85 3.17 4 -14 4 0.98 0.69 -4 -14 -4 1.93 1.22 -4 -15 5 45.93 3.8 4 -15 -5 48.39 3.22 4 -15 -5 40.36 2.92 -4 -15 4 1.93 1.68 4 -15 -4 -0.59 1.16 4 -15 -4 0.85 1.07 -4 -15 3 42.61 4.6 4 -15 -3 37.61 3.68 4 -15 -3 42.67 3.51 -4 -15 2 87.69 6.95 4 -15 -2 91.35 5.89 4 -15 -2 78.9 4.98 -4 -15 1 353.69 16.21 4 -15 -1 353.74 13.87 -4 -15 0 23.29 4.04 4 -15 0 22.36 2.91 -4 -15 0 23.5 3.43 -4 -15 -1 -0.29 2 4 -15 1 1.04 1.31 -4 -15 -1 3.71 2.04 4 -15 2 286.57 11.2 -4 -15 -2 296.5 12.93 4 -15 3 3.71 1.05 4 -15 3 3.21 1.26 -4 -15 -3 4.47 1.77 -4 -15 -4 73.28 4.29 -4 -16 5 50 3.73 4 -16 -5 50.31 3.15 4 -16 -5 48.48 2.97 -4 -16 4 7.97 2.13 4 -16 -4 4.91 1.54 4 -16 -4 7.38 1.4 -4 -16 3 3.65 1.99 4 -16 -3 3.59 1.39 4 -16 -3 2.76 1.24 -4 -16 2 1.27 1.92 4 -16 -2 -0.28 1.51 -4 -16 1 147.67 9.66 4 -16 -1 170.01 8.24 -4 -16 0 73.67 6.64 4 -16 0 76.21 5.12 -4 -16 0 69.52 5.58 -4 -16 -1 106.01 7.86 4 -16 1 114.57 6.16 -4 -16 -1 120.52 7.47 4 -16 2 105.16 5.59 4 -16 2 111.16 6.42 -4 -16 -2 113.97 7.05 4 -16 3 11.93 1.76 -4 -16 -3 10.32 1.97 -4 -17 5 2.96 1.1 4 -17 -5 2.35 0.73 -4 -17 4 2.43 1.58 4 -17 -4 4.14 1.4 4 -17 -4 2.47 0.98 4 -17 -3 164.73 7.67 4 -17 -3 152.08 6.73 -4 -17 2 26.56 3.84 4 -17 -2 26.75 3.1 -4 -17 1 3.25 2.25 4 -17 -1 4.97 1.72 -4 -17 0 -0.7 2.17 4 -17 0 0.16 1.15 -4 -17 0 -0.86 1.4 -4 -17 -1 -0.26 1.8 4 -17 1 -0.9 0.94 4 -17 1 1 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3.79 4 -20 0 54.04 4.76 -4 -20 -1 144.18 7.69 4 -20 1 144.36 6.68 -4 -20 -1 142.55 7.04 4 -20 1 127.69 7.03 4 -20 2 56.83 3.5 -4 -20 -2 57.81 3.85 -4 -21 3 0.08 1.02 4 -21 -3 0.99 0.62 -4 -21 2 1.54 1.34 4 -21 -2 0.75 0.81 4 -21 -2 0.35 1.29 -4 -21 1 29.75 3.31 4 -21 -1 27.52 2.26 4 -21 -1 30.36 3.52 -4 -21 0 253.98 10.69 4 -21 0 230.35 10.58 4 -21 1 61.26 3.72 -4 -21 -1 64.53 4.04 -4 -22 2 10.83 1.76 4 -22 -2 9.71 1.78 -4 -22 1 11.35 1.91 4 -22 -1 9.95 1.98 4 -22 0 3.29 1.28 5 0 -6 24.43 1.91 5 0 -5 1.41 1.06 5 0 -4 91.27 5.6 5 0 -3 2.5 1.43 5 0 -2 288.55 12.03 5 0 -1 -1.89 1.72 5 0 0 39.38 4.61 5 0 0 31.45 3.6 5 0 1 -0.94 1.33 5 0 2 45.27 4.12 -5 0 -3 -0.62 1.05 5 1 -6 4.51 0.96 5 -1 -5 3.51 1.4 5 1 -5 2.27 1.13 5 -1 -4 171.96 8.09 5 1 -4 178.15 8.31 5 -1 -3 3.46 1.65 5 1 -3 4.39 1.68 5 -1 -2 87.53 6.31 5 1 -2 104.64 6.63 5 -1 -1 1.75 1.55 5 1 -1 2.13 1.55 5 -1 0 1026.77 31.81 5 1 0 1040.65 31.86 5 -1 0 1027.05 31.43 5 1 1 2.86 1.39 5 -1 1 -0.68 1.12 5 -1 2 15.42 2.5 -5 -1 -2 12.93 2.35 -5 -1 -3 -0.79 0.86 -5 1 -3 0.64 0.95 -5 -1 -3 1.26 1.43 5 2 -6 48.07 2.78 5 -2 -5 191.53 7.89 5 2 -5 205.43 8.28 5 -2 -4 118.95 6.33 5 2 -4 117.59 6.45 5 -2 -3 4.63 2.03 5 2 -3 2.3 1.68 5 -2 -2 0.94 1.49 5 2 -2 4.7 1.92 5 -2 -1 10.12 2.51 5 2 -1 8.6 2.04 5 -2 -1 10.04 1.92 5 -2 0 121.73 7.01 5 2 0 107.24 6.8 5 -2 0 115.22 6.67 5 2 1 5.23 1.6 5 -2 1 8.1 2.1 -5 -2 -1 5.74 1.72 5 -2 2 26.9 3.08 -5 -2 -2 18.05 2.6 -5 -2 -3 2.3 1.09 -5 2 -3 0.46 0.95 -5 -2 -3 1.48 1.35 5 3 -6 26.77 2.02 5 -3 -5 110.58 5.44 5 3 -5 129.02 5.99 5 -3 -4 33.68 3.11 5 3 -4 36.57 3.46 5 -3 -3 240.12 10.24 5 3 -3 231.3 10.24 5 -3 -2 91.81 6.06 5 3 -2 102.94 6.29 5 -3 -1 363.03 14.23 5 3 -1 379.67 14.33 5 -3 -1 356.23 13.62 5 3 0 595.38 20.54 5 -3 0 617.82 20.59 5 -3 1 94.07 5.95 -5 -3 -1 98.63 6.34 5 -3 2 4.95 1.95 -5 -3 -2 5.93 1.39 -5 -3 -2 6.94 2.05 -5 -3 -3 23.87 2.34 -5 3 -3 23.94 2.68 -5 -3 -3 26.94 2.93 5 -4 -5 5.55 1.14 5 4 -5 11.01 1.82 5 -4 -4 66.98 4.36 5 4 -4 66.77 4.64 5 -4 -3 364.47 13.76 5 4 -3 386.8 14.31 5 -4 -2 21.77 2.96 5 4 -2 25.38 3.15 5 -4 -2 24.45 2.7 5 -4 -1 848.36 26.9 5 4 -1 860.88 26.94 5 -4 -1 830.93 26.49 5 4 0 8.13 2.22 5 -4 0 5.1 1.56 5 -4 1 49.96 4.2 -5 -4 -1 41.15 4 5 -4 2 10.6 2.07 -5 -4 -2 4.89 1.74 -5 4 -3 60.06 4.21 -5 -4 -3 61.77 4.44 5 -5 -5 3.61 1.04 5 5 -5 5.69 1.38 5 -5 -4 38.37 3.19 5 5 -4 46.16 3.74 5 -5 -4 43.72 3.6 5 -5 -3 10.66 2 5 5 -3 9.66 2.08 5 -5 -2 155.17 7.78 5 5 -2 167.17 8.11 5 -5 -2 151.72 7.53 5 -5 -1 207.57 9.62 5 5 -1 226.95 9.92 5 -5 -1 203.28 9.39 5 5 0 28.65 3.12 5 -5 0 26.4 3.01 5 -5 1 42.48 3.91 -5 -5 -1 39.2 3.95 5 -5 2 14.29 2.43 -5 -5 -2 10.66 2.23 -5 5 -3 144.72 6.97 -5 -5 -3 144.44 7.13 5 6 -5 157.94 6.81 5 -6 -4 7 1.39 5 6 -4 9.35 1.8 5 -6 -4 8.34 1.81 5 -6 -3 6.11 1.44 5 6 -3 6.42 1.77 5 -6 -3 3.74 1.33 5 -6 -2 16.73 2.37 5 6 -2 17.44 2.69 5 -6 -2 17.31 2.35 5 -6 -1 121.71 6.81 5 6 -1 127.45 6.97 5 -6 -1 131.41 7 -5 -6 0 -1.48 1.6 5 -6 0 3.59 1.84 5 -6 1 43.38 3.83 -5 -6 -1 45.64 4.17 5 -6 2 27.38 3.03 -5 -6 -2 25.13 3.08 -5 6 -3 84.43 4.98 -5 -6 -3 88.96 5.21 5 7 -5 9.9 1.6 5 -7 -4 0.73 0.78 5 7 -4 4.56 1.37 5 -7 -4 3.76 1.25 5 -7 -3 2.01 1 5 7 -3 3.08 1.45 5 -7 -3 1.64 1.33 5 -7 -2 1.94 1.19 5 7 -2 1.68 1.28 5 -7 -2 -0.16 1.14 5 -7 -1 51.23 4.12 5 7 -1 61.91 4.52 -5 -7 1 53.58 5.11 5 -7 -1 49.85 4.15 -5 -7 0 71.31 5.97 5 -7 0 76.51 5.22 5 -7 1 17.16 2.44 -5 -7 -1 11.9 2.26 5 -7 2 21.16 2.54 -5 -7 -2 18.89 2.7 -5 7 -3 0.66 1.08 -5 -7 -3 0.32 1.14 5 8 -5 53.1 3.23 5 8 -4 45.19 3.36 5 -8 -4 37.09 2.82 5 -8 -4 41.83 3.41 5 -8 -3 28.27 2.64 5 8 -3 31.08 3.03 5 -8 -3 30.68 2.94 5 -8 -2 4.12 1.41 5 8 -2 5.56 1.69 5 -8 -2 5.42 1.68 5 8 -1 39.88 3.48 -5 -8 1 37 4.2 5 -8 -1 41.67 3.81 -5 -8 0 6.02 2.22 5 -8 0 6.83 1.76 5 -8 1 194.04 8.65 -5 -8 -1 169.09 8.59 5 -8 2 29.24 3.02 -5 -8 -2 33.07 3.43 -5 8 -3 1.3 1.03 -5 -8 -3 2.52 1.4 5 9 -5 45.9 2.8 5 9 -4 37.2 2.92 5 -9 -4 36.98 2.74 5 -9 -4 36.31 3.06 5 9 -3 135.99 6.59 5 -9 -3 137.35 6.61 5 -9 -2 602.32 19.23 5 9 -2 617.24 19.73 -5 -9 2 596 21.52 5 -9 -2 614.63 19.98 5 9 -1 47.27 3.65 -5 -9 1 35.86 4.11 5 -9 -1 47.75 3.9 -5 -9 0 2.83 2.17 5 -9 0 2.85 1.54 5 -9 1 0.66 1.39 -5 -9 -1 2.96 1.43 5 -9 2 52.92 3.87 -5 -9 -2 52.17 4.09 -5 9 -3 128.55 5.77 -5 -9 -3 123.31 5.96 5 10 -4 13.26 1.71 5 -10 -4 10.52 1.49 5 -10 -4 8.14 1.56 5 10 -3 559.1 17.36 -5 -10 3 524.65 18.68 5 -10 -3 524.32 17.39 5 10 -2 9.41 1.59 -5 -10 2 7 2.35 5 -10 -2 8.48 2.01 5 10 -1 6.23 1.46 -5 -10 1 1.7 1.39 5 -10 -1 6.96 1.68 -5 -10 0 70.35 6.1 5 -10 0 82.83 5.18 5 -10 1 33.43 3.25 -5 -10 -1 32.99 3.3 5 -10 2 116.18 5.75 5 -10 2 100.36 4.97 -5 -10 -2 104.06 5.86 5 11 -4 32.49 2.39 5 -11 -4 29.72 2.37 5 11 -3 153.16 6.44 -5 -11 3 149.85 7.69 5 -11 -3 138.89 6.63 -5 -11 2 56.16 4.99 5 -11 -2 57.84 4.1 -5 -11 1 8.17 2.17 5 -11 -1 9.49 1.91 -5 -11 0 5.83 2.11 5 -11 0 5.59 1.59 5 -11 1 7.55 1.63 -5 -11 -1 9.47 1.99 5 -11 2 34.01 2.84 5 -11 2 28.14 2.38 -5 -11 -2 33.28 3.02 5 -12 -4 38.1 2.63 -5 -12 3 2.6 1.55 5 -12 -3 -0.12 0.85 -5 -12 2 6.36 2.11 5 -12 -2 6.67 1.47 -5 -12 1 136.42 8.32 5 -12 -1 147.91 7.06 -5 -12 0 16.97 3.02 5 -12 0 15.17 2.18 5 -12 1 142.56 6.62 5 -12 1 130.34 6.41 -5 -12 -1 138.11 6.73 5 -12 2 17.15 1.93 -5 12 -2 15.7 1.92 -5 -12 -2 15.68 2.11 5 -13 -4 43.35 2.68 -5 -13 3 1.9 1.36 5 -13 -3 -0.14 0.82 -5 -13 2 103.16 6.53 5 -13 -2 105.6 5.52 -5 -13 1 163.71 8.98 5 -13 -1 171.26 7.57 -5 -13 0 24.17 3.45 5 -13 0 21.49 2.45 5 -13 1 38.4 3.08 -5 -13 -1 34.5 3.02 5 -13 2 0.63 0.77 -5 -14 3 6.98 1.71 5 -14 -3 4.34 1.11 -5 -14 2 11.45 2.31 5 -14 -2 11.62 1.72 -5 -14 1 21.99 3.13 5 -14 -1 23.43 2.42 -5 -14 0 29.17 3.41 5 -14 0 25.85 2.58 5 -14 1 12.11 1.64 5 -14 1 11.23 1.65 -5 -15 3 8.69 1.76 5 -15 -3 10.98 1.44 -5 -15 2 37.14 3.53 5 -15 -2 31.01 2.59 -5 -15 1 52.47 4.4 5 -15 -1 52.75 3.52 -5 -15 0 -0.69 1.27 5 -15 0 2.25 0.99 5 -15 1 5.5 1.14 5 -15 1 3.07 1.04 -5 -16 2 24.88 2.77 5 -16 -2 21.61 2.01 -5 -16 1 19.65 2.6 5 -16 -1 19.5 2.04 -5 -16 0 6.21 1.6 5 -16 0 7.23 1.31 5 -17 -2 144.11 5.68 -5 -17 1 0.94 0.96 5 -17 -1 2.35 0.87 6 0 -3 -0.04 0.58 6 -1 -3 2.61 0.71 6 1 -3 0.4 0.63 6 2 -3 4.26 0.91