#------------------------------------------------------------------------------ #$Date: 2020-04-08 08:38:20 +0300 (Wed, 08 Apr 2020) $ #$Revision: 250494 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/77/1557751.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1557751 _cell_angle_alpha 90.000 _cell_angle_beta 94.548 _cell_angle_gamma 90.000 _cell_length_a 14.6285 _cell_length_b 29.9816 _cell_length_c 20.5191 _exptl_crystal_F_000 3376.00 _reflns_d_resolution_high 0.8301 _cod_data_source_file is4043Isup2.hkl _cod_data_source_block I _shelx_title ' V4-tBuCyOH' _shelx_refln_list_code 4 _shelx_f_calc_maximum 525.63 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 71622.66 89998.98 3449.86 o 3 0 0 21107.54 22371.30 681.27 o 4 0 0 58521.85 69844.77 2812.05 o 5 0 0 375.10 517.69 89.51 o 6 0 0 119.29 -42.60 76.25 o 7 0 0 22137.69 24568.09 773.45 o 8 0 0 48791.59 57163.98 2470.98 o 9 0 0 41229.61 50436.23 2265.93 o 10 0 0 27370.13 35257.55 1600.61 o 11 0 0 11946.38 14254.62 595.98 o 12 0 0 2641.28 3557.28 209.42 o 13 0 0 31.93 121.13 245.89 o 14 0 0 788.55 967.80 175.82 o 15 0 0 126.05 189.21 185.50 o 16 0 0 111.86 58.90 175.98 o 17 0 0 338.01 795.95 247.39 o 2 1 0 63889.24 74123.34 1810.46 o 3 1 0 3332.84 4554.80 86.92 o 4 1 0 14792.09 18147.76 331.53 o 5 1 0 35033.33 43214.21 1041.16 o 6 1 0 4879.90 5398.56 126.01 o 7 1 0 284.30 298.91 53.76 o 8 1 0 5813.38 6192.08 172.14 o 9 1 0 22273.71 26251.03 694.86 o 10 1 0 30566.83 37410.66 1166.88 o 11 1 0 14836.15 18695.49 599.10 o 12 1 0 37.58 184.65 89.62 o 13 1 0 4932.22 5598.97 231.98 o 14 1 0 2200.38 2745.83 162.96 o 15 1 0 259.15 494.20 122.01 o 16 1 0 34.69 -143.60 143.60 o 17 1 0 26.50 67.93 155.01 o 2 2 0 690.28 618.33 38.94 o 3 2 0 13999.61 17124.92 293.38 o 4 2 0 17960.18 21877.76 390.03 o 5 2 0 3274.71 2178.79 72.69 o 6 2 0 5095.13 5371.23 127.13 o 7 2 0 1551.65 1623.90 71.14 o 8 2 0 9744.34 10856.65 243.73 o 9 2 0 10159.04 11224.47 296.06 o 10 2 0 12376.45 13228.44 520.39 o 11 2 0 1663.45 1818.11 102.32 o 12 2 0 142.52 131.95 77.62 o 13 2 0 475.42 923.19 163.72 o 14 2 0 722.03 808.03 173.70 o 15 2 0 35.55 31.81 117.34 o 16 2 0 50.95 356.82 133.95 o 17 2 0 32.99 154.84 133.48 o 1 3 0 8751.00 11505.49 124.50 o 2 3 0 31484.20 39942.69 859.88 o 3 3 0 7576.85 8324.09 143.81 o 4 3 0 302.25 293.00 52.61 o 5 3 0 1721.54 1629.92 66.84 o 6 3 0 252.15 165.91 51.89 o 7 3 0 148.39 231.06 52.46 o 8 3 0 36.34 172.16 66.01 o 9 3 0 6781.81 7842.17 223.04 o 10 3 0 9567.50 11341.25 289.22 o 11 3 0 5623.00 6677.35 224.25 o 12 3 0 542.65 846.37 86.88 o 13 3 0 2213.31 2375.00 176.51 o 14 3 0 505.13 846.77 129.89 o 15 3 0 222.63 650.08 150.15 o 16 3 0 128.89 248.76 136.24 o 17 3 0 716.93 1079.60 167.54 o 0 4 0 35214.00 47849.76 1255.00 o 1 4 0 1709.05 2101.07 47.57 o 2 4 0 30651.33 35107.42 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9 0 715.81 786.56 107.90 o 14 9 0 23.48 97.69 101.38 o 15 9 0 107.51 180.25 117.28 o 16 9 0 693.50 1192.29 160.43 o 17 9 0 672.12 962.89 189.85 o 0 10 0 16665.68 19713.12 492.15 o 1 10 0 3118.22 3073.03 77.39 o 2 10 0 1620.94 1894.45 60.58 o 3 10 0 2745.10 3576.58 80.50 o 4 10 0 818.47 1060.90 52.68 o 5 10 0 150.48 104.19 45.09 o 6 10 0 717.33 809.77 68.17 o 7 10 0 186.05 300.31 57.47 o 8 10 0 2231.98 2319.37 102.37 o 9 10 0 841.57 784.22 81.83 o 10 10 0 26.33 37.51 63.41 o 11 10 0 4.64 -73.02 73.02 o 12 10 0 50.21 127.72 94.84 o 13 10 0 1048.78 1181.43 118.63 o 14 10 0 1070.21 1340.46 127.77 o 15 10 0 52.96 55.85 135.51 o 16 10 0 70.13 363.75 165.79 o 1 11 0 2131.16 2906.92 73.81 o 2 11 0 1978.64 2123.80 71.24 o 3 11 0 3163.68 3923.01 96.62 o 4 11 0 13507.48 14442.55 246.73 o 5 11 0 5387.15 6361.26 139.01 o 6 11 0 3621.23 3415.29 111.55 o 7 11 0 2321.95 3074.27 115.41 o 8 11 0 8094.80 9291.40 340.46 o 9 11 0 7460.84 7862.02 279.32 o 10 11 0 8538.65 9428.37 403.15 o 11 11 0 3277.40 3644.87 146.98 o 12 11 0 458.92 452.94 98.40 o 13 11 0 42.54 204.72 94.24 o 14 11 0 351.08 433.21 103.74 o 15 11 0 1017.63 1259.72 128.68 o 16 11 0 1467.24 1836.92 175.14 o 0 12 0 295.04 757.43 101.72 o 1 12 0 3704.72 4246.15 84.54 o 2 12 0 16521.86 21401.25 392.44 o 3 12 0 27638.18 31379.55 697.69 o 4 12 0 4485.79 4832.54 90.97 o 5 12 0 195.22 170.37 46.34 o 6 12 0 247.65 274.41 61.63 o 7 12 0 28.47 283.83 64.30 o 8 12 0 2276.40 2018.36 94.08 o 9 12 0 3724.61 3435.97 137.52 o 10 12 0 60.38 45.81 79.11 o 11 12 0 865.32 760.54 102.45 o 12 12 0 20.22 24.93 86.38 o 13 12 0 22.45 11.25 95.93 o 14 12 0 129.33 171.27 129.23 o 15 12 0 859.59 859.78 130.04 o 16 12 0 864.53 1089.28 150.22 o 1 13 0 2481.75 2760.17 76.76 o 2 13 0 4656.07 3961.48 95.95 o 3 13 0 165.10 294.02 46.25 o 4 13 0 7565.02 9259.30 176.45 o 5 13 0 2444.58 3113.67 83.92 o 6 13 0 591.09 423.86 62.78 o 7 13 0 2002.88 2112.65 81.26 o 8 13 0 3578.88 3833.65 160.59 o 9 13 0 2791.90 2821.85 113.76 o 10 13 0 1551.50 982.25 95.84 o 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168.01 173.83 74.55 o 11 15 0 1211.73 1326.34 119.08 o 12 15 0 1705.38 1837.04 127.43 o 13 15 0 1660.56 1491.26 150.56 o 14 15 0 235.02 404.31 120.92 o 15 15 0 364.25 292.84 120.08 o 0 16 0 28219.04 34485.52 1118.67 o 1 16 0 46831.20 58797.66 1801.09 o 2 16 0 24710.25 29496.74 656.09 o 3 16 0 469.29 473.42 57.99 o 4 16 0 547.05 654.35 58.18 o 5 16 0 2094.63 1781.38 73.60 o 6 16 0 5310.86 5948.50 195.82 o 7 16 0 8666.92 9327.29 306.57 o 8 16 0 11984.51 12734.07 507.31 o 9 16 0 12072.88 11834.29 612.73 o 10 16 0 8177.87 9033.38 387.38 o 11 16 0 45.09 -4.68 80.87 o 12 16 0 1139.55 1315.91 182.69 o 13 16 0 1533.65 1440.65 125.18 o 14 16 0 1.91 -103.34 176.13 o 15 16 0 868.70 804.15 140.42 o 1 17 0 24052.08 30698.38 742.47 o 2 17 0 21420.99 26062.24 560.83 o 3 17 0 7194.98 7560.31 175.34 o 4 17 0 116.98 151.23 53.70 o 5 17 0 2971.38 3276.88 98.99 o 6 17 0 15745.71 17277.00 440.91 o 7 17 0 13102.17 13615.14 539.48 o 8 17 0 9597.04 10221.92 491.96 o 9 17 0 1234.71 1109.98 111.74 o 10 17 0 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7774.74 252.07 o 4 24 0 8418.58 9402.68 390.07 o 5 24 0 5022.31 5070.95 183.15 o 6 24 0 2210.74 2130.02 122.70 o 7 24 0 31.59 90.94 77.41 o 8 24 0 891.68 821.78 120.01 o 9 24 0 333.89 451.39 142.39 o 10 24 0 0.99 -122.43 124.21 o 11 24 0 204.91 396.30 126.92 o 12 24 0 182.26 334.54 133.64 o 13 24 0 91.20 104.00 132.23 o 1 25 0 116.48 136.27 75.34 o 2 25 0 199.16 175.52 87.54 o 3 25 0 495.76 565.24 89.69 o 4 25 0 1169.33 1404.86 100.65 o 5 25 0 871.54 775.89 106.22 o 6 25 0 780.33 773.33 82.75 o 7 25 0 1110.74 1064.55 100.29 o 8 25 0 124.54 140.83 88.90 o 9 25 0 769.38 688.04 123.87 o 10 25 0 2718.46 2931.77 214.58 o 11 25 0 1931.53 2123.06 164.94 o 12 25 0 2.23 12.85 123.11 o 0 26 0 15371.24 18168.25 739.05 o 1 26 0 15230.87 18919.39 516.29 o 2 26 0 3947.39 5036.65 190.17 o 3 26 0 173.00 164.18 69.64 o 4 26 0 203.48 154.78 89.51 o 5 26 0 1044.29 1014.27 100.14 o 6 26 0 1098.31 1343.86 93.54 o 7 26 0 88.32 89.89 97.12 o 8 26 0 1320.85 1415.52 122.66 o 9 26 0 2750.29 2937.30 173.70 o 10 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