#------------------------------------------------------------------------------ #$Date: 2020-05-04 05:49:44 +0300 (Mon, 04 May 2020) $ #$Revision: 251489 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/78/1557805.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557805 loop_ _publ_author_name 'Cobos, Katherine' 'Rodr\'iguez, Rafael' 'Domarco, Olaya' 'Fern\'andez, Berta' 'Qui\~no\'a, Emilio' 'Riguera, Ricardo' 'Freire, F\'elix' _publ_section_title ; Polymeric Helical Structures \`a la Carte by Rational Design of Monomers ; _journal_issue 8 _journal_name_full Macromolecules _journal_page_first 3182 _journal_paper_doi 10.1021/acs.macromol.0c00085 _journal_volume 53 _journal_year 2020 _chemical_absolute_configuration rmad _chemical_formula_moiety 'C16 H12 Cl N O' _chemical_formula_sum 'C16 H12 Cl N O' _chemical_formula_weight 269.72 _chemical_name_common S-m-ClMA _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_conform_dict_location ftp://ftp.iucr.org/pub/cif_core.dic _audit_conform_dict_name cif_core.dic _audit_conform_dict_version 2.4.3 _audit_creation_date 2016-05-09T10:15:05-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 4.9936(8) _cell_length_b 10.8879(16) _cell_length_c 23.631(3) _cell_measurement_reflns_used 1213 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 21.25 _cell_measurement_theta_min 2.54 _cell_measurement_wavelength 0.71073 _cell_volume 1284.8(3) _computing_cell_refinement 'SAINT V8.37A integration software' _computing_data_collection 'Bruker APEX2 software' _computing_data_reduction 'SORTAV (Blessing, 1995)' _computing_molecular_graphics 'ORTEP-3 for Windows (Farrugia, 2012)' _computing_publication_material 'WinGX publication routines (Farrugia, 2012)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT-2014 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_detector 'APEX-II CCD' _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker APEX-II' _diffrn_measurement_method '\f or \w oscillation scans' _diffrn_orient_matrix_UB_11 -0.002549 _diffrn_orient_matrix_UB_12 0.067203 _diffrn_orient_matrix_UB_13 -0.02884 _diffrn_orient_matrix_UB_21 -0.012017 _diffrn_orient_matrix_UB_22 -0.062537 _diffrn_orient_matrix_UB_23 -0.030889 _diffrn_orient_matrix_UB_31 -0.199878 _diffrn_orient_matrix_UB_32 0.002903 _diffrn_orient_matrix_UB_33 0.002225 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0846 _diffrn_reflns_av_unetI/netI 0.1139 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 10064 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.99 _diffrn_reflns_reduction_process ; Scaled and merged with Sortav R.H. Blessing, (1987) Cryst. Rev. 1, 3-58 R.H. Blessing, (1989) J. Appl. Cryst. 22, 396-397 ; _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.12 _diffrn_reflns_theta_min 1.724 _diffrn_source 'sealed x-ray tube' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.287 _exptl_absorpt_correction_T_max 0.928 _exptl_absorpt_correction_T_min 0.766 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.394 _exptl_crystal_density_method 'not measured' _exptl_crystal_description needle _exptl_crystal_F_000 560 _exptl_crystal_size_max 1 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.311 _refine_diff_density_min -0.293 _refine_diff_density_rms 0.069 _refine_ls_abs_structure_details ; Flack x determined using 571 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.07(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.959 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_constraints 0 _refine_ls_number_parameters 176 _refine_ls_number_reflns 2815 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.959 _refine_ls_R_factor_all 0.0932 _refine_ls_R_factor_gt 0.0501 _refine_ls_shift/su_max 0 _refine_ls_shift/su_mean 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0319P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.08 _refine_ls_wR_factor_ref 0.0921 _reflns_Friedel_coverage 0.68 _reflns_Friedel_fraction_full 1 _reflns_Friedel_fraction_max 0.984 _reflns_number_gt 1944 _reflns_number_total 2815 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ma0c00085_si_004.cif _cod_data_source_block shelx _cod_depositor_comments 'Adding full bibliography for 1557803--1557808.cif.' _cod_database_code 1557805 _shelx_estimated_absorpt_t_min 0.762 _shelx_estimated_absorpt_t_max 0.994 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL shelxt_a.res in P2(1)2(1)2(1) CELL 0.71073 4.9936 10.8879 23.6305 90.000 90.000 90.000 ZERR 4.00 0.0008 0.0016 0.0032 0.000 0.000 0.000 LATT -1 SYMM 1/2 - X, - Y, 1/2 + Z SYMM - X, 1/2 + Y, 1/2 - Z SYMM 1/2 + X, 1/2 - Y, - Z SFAC C H CL N O UNIT 64 48 4 4 4 MERG 2 FMAP 2 PLAN 20 SIZE 0.020 0.030 1.000 ACTA BOND $H REM Instructions for potential hydrogen bonds EQIV $1 x+1, y, z HTAB N4 O3_$1 CONF LIST 4 WPDB -2 L.S. 12 TEMP -173.00 WGHT 0.031900 FVAR 0.91010 CL1 3 0.209077 0.066082 0.219886 11.00000 0.02609 0.01783 = 0.02201 -0.00158 -0.00067 -0.00408 C1 1 0.425114 0.189284 0.242404 11.00000 0.00995 0.01549 = 0.01456 -0.00091 -0.00079 -0.00201 AFIX 13 H1 2 0.608812 0.155397 0.248737 11.00000 -1.20000 AFIX 0 C2 1 0.320435 0.240856 0.298507 11.00000 0.01378 0.01438 = 0.01479 0.00241 -0.00016 -0.00015 O3 5 0.082305 0.245307 0.310617 11.00000 0.01266 0.02664 = 0.02057 -0.00323 0.00245 -0.00120 N4 4 0.518323 0.283408 0.331993 11.00000 0.01282 0.01690 = 0.01437 -0.00394 0.00103 -0.00042 H4 2 0.681032 0.264908 0.321473 11.00000 0.00878 C5 1 0.479947 0.342458 0.385175 11.00000 0.01300 0.01681 = 0.01036 -0.00109 0.00030 -0.00455 C6 1 0.285756 0.432781 0.391751 11.00000 0.01464 0.01842 = 0.01207 0.00062 -0.00076 -0.00353 AFIX 43 H6 2 0.174335 0.454944 0.360807 11.00000 -1.20000 AFIX 0 C7 1 0.255242 0.490691 0.443953 11.00000 0.01132 0.01447 = 0.01829 0.00057 0.00378 -0.00325 C8 1 0.420707 0.456511 0.489070 11.00000 0.01891 0.01947 = 0.01375 -0.00276 0.00398 -0.00567 AFIX 43 H8 2 0.400757 0.495124 0.524873 11.00000 -1.20000 AFIX 0 C9 1 0.612255 0.367089 0.481688 11.00000 0.02015 0.02504 = 0.01114 0.00315 -0.00304 -0.00632 AFIX 43 H9 2 0.723911 0.344488 0.512527 11.00000 -1.20000 AFIX 0 C10 1 0.644287 0.309519 0.429726 11.00000 0.01469 0.01671 = 0.01869 0.00249 0.00179 -0.00156 AFIX 43 H10 2 0.777611 0.248188 0.424837 11.00000 -1.20000 AFIX 0 C11 1 0.057973 0.586848 0.450468 11.00000 0.01969 0.02183 = 0.01310 -0.00412 0.00121 -0.00795 C12 1 -0.101937 0.663775 0.454760 11.00000 0.02975 0.02204 = 0.03228 -0.00473 0.00560 -0.00097 AFIX 163 H12 2 -0.232710 0.726685 0.458270 11.00000 -1.20000 AFIX 0 C13 1 0.441209 0.288417 0.197397 11.00000 0.01359 0.01840 = 0.00946 -0.00209 -0.00154 -0.00174 C14 1 0.262320 0.385432 0.196236 11.00000 0.01474 0.01987 = 0.01698 -0.00308 0.00482 -0.00081 AFIX 43 H14 2 0.123995 0.389743 0.223765 11.00000 -1.20000 AFIX 0 C15 1 0.282298 0.476232 0.155505 11.00000 0.02426 0.01367 = 0.02831 -0.00132 -0.00757 -0.00202 AFIX 43 H15 2 0.159484 0.542863 0.155123 11.00000 -1.20000 AFIX 0 C16 1 0.484497 0.468835 0.115073 11.00000 0.02169 0.01951 = 0.02100 0.00702 -0.00275 -0.00403 AFIX 43 H16 2 0.502901 0.531801 0.087516 11.00000 -1.20000 AFIX 0 C17 1 0.657419 0.370724 0.114933 11.00000 0.02054 0.02765 = 0.01462 0.00049 0.00419 -0.00458 AFIX 43 H17 2 0.790893 0.364629 0.086423 11.00000 -1.20000 AFIX 0 C18 1 0.638353 0.280805 0.156034 11.00000 0.01816 0.02170 = 0.01808 -0.00031 -0.00074 0.00296 AFIX 43 H18 2 0.760100 0.213759 0.156006 11.00000 -1.20000 REM ##### AFIX 0 HKLF 4 REM shelxt_a.res in P2(1)2(1)2(1) REM R1 = 0.0501 for 1944 Fo > 4sig(Fo) and 0.0932 for all 2815 data REM 176 parameters refined using 0 restraints END WGHT 0.0319 0.0000 REM Highest difference peak 0.311, deepest hole -0.293, 1-sigma level 0.069 Q1 1 0.0210 0.3546 0.2201 11.00000 0.05 0.31 Q2 1 -0.0933 0.7961 0.5207 11.00000 0.05 0.27 Q3 1 0.4070 0.2333 0.4232 11.00000 0.05 0.24 Q4 1 -0.2551 0.6924 0.5123 11.00000 0.05 0.24 Q5 1 -0.0693 0.5748 0.4587 11.00000 0.05 0.24 Q6 1 0.0357 0.4851 0.1011 11.00000 0.05 0.24 Q7 1 0.0688 0.5243 0.2189 11.00000 0.05 0.23 Q8 1 0.8619 0.3940 0.2833 11.00000 0.05 0.23 Q9 1 0.6705 0.2833 0.2382 11.00000 0.05 0.23 Q10 1 0.3154 0.5235 0.4674 11.00000 0.05 0.23 Q11 1 -0.0797 0.4447 0.2068 11.00000 0.05 0.22 Q12 1 0.2345 0.5802 0.3580 11.00000 0.05 0.22 Q13 1 0.4044 0.4972 0.3266 11.00000 0.05 0.22 Q14 1 0.1276 0.0163 0.2697 11.00000 0.05 0.22 Q15 1 -0.1113 0.8447 0.4718 11.00000 0.05 0.22 Q16 1 0.4157 0.2831 0.4585 11.00000 0.05 0.22 Q17 1 0.2641 0.3469 0.1193 11.00000 0.05 0.22 Q18 1 0.9133 0.2786 0.4479 11.00000 0.05 0.22 Q19 1 0.0018 0.2822 0.2095 11.00000 0.05 0.22 Q20 1 0.3109 0.5965 0.0662 11.00000 0.05 0.21 ; _shelx_res_checksum 47234 _shelx_hkl_file ; 0 0 1-3.88944 1.51258 1 0 0 1-3.59145 1.58609 1 0 0 2 2910.45 77.7295 1 0 0 2 2575.84 76.3619 1 0 0 3 1.89789 8.05029 1 0 0 -3-5.15028 6.91191 1 0 0 -3-1.59959 5.88193 1 0 0 3-3.04621 7.62626 1 0 0 4 243.839 21.3465 1 0 0 -4 202.455 19.2012 1 0 0 -4 206.043 19.5241 1 0 0 4 228.523 21.608 1 0 0 -5 2.56641 12.2281 1 0 0 5-1.70896 14.1846 1 0 0 -5 7.21613 5.74607 1 0 0 5-6.28187 14.9033 1 0 0 -5-0.98198 13.7662 1 0 0 -6 313.572 13.7209 1 0 0 6 323.688 29.4735 1 0 0 -6 287.093 28.1404 1 0 0 6 302.858 28.5107 1 0 0 -6 313.004 27.8581 1 0 0 -7-2.31844 5.68416 1 0 0 -7 13.89 13.026 1 0 0 -7 13.769 15.1238 1 0 0 7 4.78551 16.5354 1 0 0 7 1.06616 16.6073 1 0 0 -8 875.799 27.8669 1 0 0 -8 844.433 50.1032 1 0 0 8 966.766 48.7154 1 0 0 8 974.11 54.5938 1 0 0 -8 922.564 46.7201 1 0 0 -9-13.1383 4.63812 1 0 0 9 10.9466 17.794 1 0 0 9 16.8698 18.5701 1 0 0 -9 4.76063 13.1131 1 0 0 -9 6.13827 18.0426 1 0 0 10 790.414 49.8232 1 0 0 -10 842.90 55.7541 1 0 0 -10 768.412 47.1635 1 0 0 10 835.84 55.7939 1 0 0 -11 14.7272 15.9902 1 0 0 11-11.4232 17.7132 1 0 0 11-3.53669 19.529 1 0 0 -11-18.1167 18.0061 1 0 0 12 1333.68 68.9743 1 0 0 -12 1370.18 68.4414 1 0 0 -12 1394.74 75.1692 1 0 0 12 1499.67 78.2914 1 0 0 13 0.16314 19.0316 1 0 0 -13-4.91104 14.5846 1 0 0 -13-18.4944 18.9112 1 0 0 13 24.9773 23.5619 1 0 0 -14 34.7996 24.3095 1 0 0 -14 19.4996 19.2717 1 0 0 14 27.3937 23.3342 1 0 0 -15-0.36085 16.2558 1 0 0 -15 0.73969 19.5142 1 0 0 15-17.6871 18.7377 1 0 0 16 2.09049 21.1594 1 0 0 -16-10.1949 16.9385 1 0 0 -16 40.8972 27.6485 1 0 0 17 4.77852 25.5123 1 0 0 -17 3.40839 24.0135 1 0 0 -17 8.6415 18.5054 1 0 0 -18 1642.54 99.5715 1 0 0 -18 1515.11 87.166 1 0 0 18 1591.71 89.4804 1 0 0 -19 7.3101 19.8786 1 0 0 -19-21.0058 28.2088 1 0 0 19-7.89318 25.451 1 0 0 20 68.3824 33.7638 1 0 0 -20 62.5857 30.4373 1 0 0 -20 144.886 39.9124 1 0 0 21 26.1271 33.9474 1 0 0 -21-30.2071 27.7203 1 0 0 -22 750.541 85.9567 1 0 0 22 646.513 75.1565 1 0 0 23-9.29652 31.2654 1 0 0 -23-14.5069 32.9668 1 0 0 -24 51.2868 42.7825 1 0 0 24 35.6223 39.6025 1 0 0 25 8.83039 38.5403 1 0 0 -25-16.0919 37.9063 1 0 0 -26 195.904 60.0285 1 0 0 26 216.237 54.8296 1 0 0 27-0.92358 38.7509 1 0 0 -27 42.2043 50.184 1 0 0 28 95.6221 50.5912 1 0 0 -28 107.894 57.6118 1 0 0 -29 4.68066 50.6995 1 0 0 29-24.0365 41.8273 1 0 0 30 302.819 70.9585 1 0 0 -30 370.394 87.0821 1 0 1 0-4.51694 4.70135 1 0 -1 0-1.09019 2.50907 1 0 -1 0 4.03494 3.86186 1 0 1 0 4.05833 5.58161 1 0 -1 -1 251.837 14.4763 1 0 1 -1 255.286 16.0312 1 0 1 1 277.629 15.0865 1 0 -1 1 288.079 17.2176 1 0 1 1 235.915 14.1549 1 0 1 -1 298.743 14.6583 1 0 1 -2 315.626 17.2661 1 0 1 2 360.884 18.456 1 0 -1 2 380.899 20.9317 1 0 1 2 344.658 19.4526 1 0 -1 -2 352.311 19.1528 1 0 -1 -2 338.37 17.3202 1 0 1 -2 345.747 20.977 1 0 -1 2 294.045 16.9353 1 0 -1 3 11.9003 10.6497 1 0 1 3 11.3883 9.88202 1 0 1 -3 13.7485 11.2563 1 0 -1 -3 14.2401 9.53059 1 0 -1 3 27.8183 11.093 1 0 1 -3 14.2805 8.5646 1 0 1 3 30.782 12.3722 1 0 -1 -3 19.4941 8.76951 1 0 -1 -3 9.06514 10.0142 1 0 -1 -4 2487.34 79.248 1 0 1 -4 2498.70 82.941 1 0 1 4 2552.54 83.4068 1 0 1 4 2570.38 80.3884 1 0 -1 4 2526.83 80.2319 1 0 -1 -4 2479.46 83.0027 1 0 -1 4 2523.49 82.9325 1 0 1 5 6.89988 15.713 1 0 -1 5 2.80961 13.3996 1 0 1 5 21.0986 15.7583 1 0 -1 -5 25.4708 12.8671 1 0 1 -5 13.0659 12.4825 1 0 -1 -5-6.61886 14.5917 1 0 -1 5 12.3581 16.1291 1 0 1 -5 0.91688 14.6197 1 0 -1 6 7467.48 210.423 1 0 -1 -6 7263.17 209.534 1 0 1 6 7638.29 211.511 1 0 -1 -6 7262.67 212.843 1 0 -1 6 7545.56 214.453 1 0 1 -6 7095.52 212.267 1 0 1 -6 7679.83 211.625 1 0 1 6 7361.08 213.933 1 0 1 -7 477.464 33.5449 1 0 -1 -7 344.057 31.6063 1 0 -1 -7 444.112 32.7122 1 0 -1 7 443.805 34.0806 1 0 1 7 433.064 35.7341 1 0 -1 7 367.10 34.4259 1 0 1 -7 394.884 36.2421 1 0 1 7 389.229 35.8715 1 0 -1 -8 394.39 32.9486 1 0 -1 8 365.695 18.1617 1 0 1 8 337.428 34.6176 1 0 -1 8 378.703 35.8793 1 0 1 -8 352.276 36.2106 1 0 -1 8 353.883 34.2265 1 0 -1 -8 356.352 35.3776 1 0 1 8 333.60 32.8136 1 0 1 -8 403.622 32.6604 1 0 1 9 111.901 25.5548 1 0 -1 9 104.33 24.3147 1 0 -1 -9 88.1321 22.7151 1 0 1 -9 193.664 29.8666 1 0 -1 9 123.681 10.8279 1 0 -1 9 124.252 25.4671 1 0 1 9 165.658 27.9243 1 0 1 -9 121.594 25.8538 1 0 -1 10 1863.27 84.1306 1 0 1 -10 1942.31 79.3568 1 0 1 -10 1771.87 83.1926 1 0 1 10 1834.46 79.6377 1 0 -1 -10 1885.20 83.6436 1 0 1 10 1883.82 85.0619 1 0 -1 10 1873.71 79.1755 1 0 -1 -10 1838.77 78.1206 1 0 -1 -11 3642.20 131.16 1 0 -1 11 3919.03 134.113 1 0 -1 11 3894.16 139.964 1 0 1 -11 3668.27 137.268 1 0 1 11 3925.94 134.137 1 0 1 11 3832.97 139.663 1 0 1 -11 4040.42 134.672 1 0 -1 -11 3589.67 136.069 1 0 -1 -12 916.507 61.6671 1 0 1 12 936.859 64.0457 1 0 -1 -12 982.171 57.1424 1 0 -1 12 931.147 57.7099 1 0 -1 12 913.857 63.7169 1 0 1 12 968.415 59.1821 1 0 1 -12 886.042 61.9211 1 0 1 -12 885.837 55.5135 1 0 -1 13 87.4989 28.6624 1 0 -1 13 118.363 28.0897 1 0 -1 -13 96.3081 25.3058 1 0 1 13 85.1848 29.5594 1 0 1 -13 60.5803 26.5981 1 0 1 13 61.5371 25.0856 1 0 -1 -13 99.7898 27.5293 1 0 1 -13 134.215 27.2057 1 0 1 -14 122.857 27.6547 1 0 -1 -14 163.237 16.745 1 0 1 -14 109.115 31.0794 1 0 -1 -14 188.526 32.5367 1 0 -1 14 172.237 33.7753 1 0 -1 -14 112.493 32.1786 1 0 1 14 159.42 31.9923 1 0 -1 15 267.45 43.5942 1 0 -1 -15 236.636 37.3536 1 0 1 -15 164.25 31.8477 1 0 1 -15 205.25 38.8869 1 0 1 15 299.251 46.8122 1 0 -1 -15 262.953 42.1404 1 0 -1 -15 233.96 18.9354 1 0 -1 -16 184.63 36.8059 1 0 1 -16 219.105 40.5576 1 0 -1 -16 230.722 37.0815 1 0 -1 -16 212.109 15.6263 1 0 1 -16 216.731 39.3629 1 0 -1 16 207.136 35.9633 1 0 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114.553 18.8855 1 1 -2 16 69.4979 27.5702 1 -1 -2 -16 115.835 34.2355 1 -1 2 -16 148.798 36.2928 1 1 2 16 103.673 35.0931 1 1 -2 -16 66.6045 28.1211 1 -1 -2 16 126.171 23.1698 1 -1 2 16 103.565 28.7431 1 -1 -2 -17 253.486 45.4496 1 1 2 -17 272.502 43.2777 1 1 2 -17 261.087 45.5524 1 -1 -2 -17 272.056 26.0453 1 1 2 17 241.132 43.1968 1 -1 -2 -17 253.238 37.7688 1 1 -2 -17 205.347 42.6241 1 1 -2 -17 346.387 41.7875 1 -1 -2 17 234.634 40.0107 1 -1 2 -17 331.958 51.4234 1 1 -2 -17 323.67 47.2714 1 1 -2 17 251.623 45.7884 1 -1 -2 -18 706.851 34.7797 1 1 -2 18 794.487 70.8405 1 -1 2 18 808.493 64.5649 1 -1 2 -18 734.145 72.9117 1 1 -2 -18 752.257 76.2432 1 -1 -2 -18 790.967 60.3919 1 1 -2 -18 799.229 69.3029 1 1 2 -18 783.075 66.2836 1 -1 -2 18 739.561 58.1036 1 1 2 -18 866.766 80.5859 1 1 -2 -18 670.251 51.4027 1 -1 -2 -18 703.011 69.5436 1 1 2 18 652.567 71.5583 1 1 -2 19 283.061 51.0783 1 1 2 -19 253.901 48.7285 1 1 -2 -19 229.67 48.952 1 -1 2 19 215.232 41.4124 1 -1 -2 -19 244.41 47.5591 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49.0614 1 -1 -2 24 44.7514 32.0818 1 -1 2 24 10.6126 30.9101 1 -1 2 -24-16.5067 40.5394 1 1 -2 -24 22.0173 41.6107 1 1 2 -24 37.2587 41.4467 1 -1 -2 -24-0.35528 41.5535 1 1 -2 -25 177.13 56.4486 1 1 2 -25 106.13 55.7194 1 -1 2 25 34.0375 34.2459 1 -1 -2 25 139.468 41.0064 1 -1 2 -25 253.667 63.1735 1 -1 -2 -25 66.4103 46.6318 1 1 -2 -26 75.1581 54.7745 1 -1 2 26 70.8194 37.4064 1 1 2 -26 86.2851 56.5946 1 -1 -2 26 51.6362 34.2153 1 -1 2 -26 88.4734 51.5954 1 -1 -2 -26 71.913 51.172 1 -1 2 27 270.629 51.7115 1 1 2 -27 230.412 70.4947 1 -1 -2 27 289.552 56.2408 1 1 -2 -27 264.325 71.031 1 -1 -2 -27 221.868 66.5221 1 -1 2 -27 310.081 70.8612 1 -1 2 28 193.563 50.9224 1 -1 -2 -28 127.917 64.2465 1 -1 2 -28 120.635 64.6472 1 -1 -2 28 169.586 46.9844 1 -1 -2 28 137.125 39.7497 1 1 -2 -28 253.095 78.1552 1 1 2 -28 189.759 72.4133 1 -1 2 -29 114.019 70.6909 1 1 2 -29 122.709 72.9491 1 -1 2 29 60.5378 41.5506 1 -1 -2 29 77.7818 41.0203 1 1 -2 -29 106.738 65.1329 1 -1 -2 -29 146.883 71.5011 1 -1 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601.398 41.3813 1 1 -3 -3 634.104 45.8938 1 1 -3 3 619.161 37.8696 1 -1 -3 -3 599.505 31.8967 1 1 3 -3 591.648 39.1684 1 1 3 -3 618.199 43.1757 1 1 3 -3 654.72 37.7035 1 1 3 3 632.639 37.8711 1 -1 -3 3 668.182 29.6547 1 1 3 3 644.723 34.4704 1 -1 3 -3 689.277 41.4433 1 -1 -3 3 701.499 31.0122 1 1 -3 -3 704.105 35.319 1 -1 3 3 588.312 46.2086 1 -1 -3 -3 616.823 31.1931 1 -1 3 -3 671.442 42.2914 1 -1 -3 -4 282.791 23.0807 1 1 3 -4 207.872 27.9472 1 1 -3 4 355.30 33.6723 1 1 3 -4 315.819 32.0365 1 -1 -3 4 434.294 24.6274 1 -1 -3 4 290.064 29.6967 1 -1 3 -4 299.837 30.9673 1 1 -3 -4 283.129 26.9592 1 -1 3 4 283.353 28.824 1 -1 -3 -4 296.445 25.5156 1 1 3 4 326.728 31.962 1 1 3 4 349.633 27.0214 1 1 3 -4 367.939 33.6679 1 1 -3 4 271.612 26.5306 1 1 -3 -4 294.739 37.8329 1 -1 3 -4 351.053 32.8326 1 1 -3 5 492.541 33.5816 1 -1 -3 -5 480.222 27.2439 1 -1 3 5 517.227 39.1461 1 1 -3 5 491.197 40.9248 1 1 3 -5 428.797 39.3502 1 -1 -3 -5 501.062 32.7089 1 -1 -3 5 509.294 30.5744 1 -1 -3 5 417.31 36.8995 1 1 -3 -5 478.856 34.7003 1 1 3 5 482.063 38.7063 1 -1 3 -5 447.451 39.5067 1 1 3 5 459.738 30.5176 1 1 -3 -5 495.288 46.0416 1 -1 3 -5 480.936 37.1934 1 1 -3 6 2002.47 72.425 1 -1 -3 6 2022.29 70.0496 1 -1 -3 -6 1985.22 65.73 1 -1 -3 6 2110.89 72.0106 1 1 -3 -6 2069.00 77.3336 1 1 -3 6 2065.13 82.7074 1 -1 3 6 2170.75 83.0718 1 -1 -3 6 2076.34 82.9687 1 -1 3 -6 2085.57 84.6816 1 1 3 6 2075.13 81.4354 1 -1 3 -6 2118.90 77.9787 1 1 -3 -6 1959.07 88.4928 1 -1 3 6 1988.13 67.0974 1 -1 -3 -6 1950.12 72.7692 1 1 3 6 2008.54 71.7323 1 1 3 -6 1872.50 77.6079 1 1 3 -6 1913.36 82.5296 1 1 3 7 253.339 26.4802 1 1 -3 7 281.396 34.1402 1 1 3 -7 237.971 29.9338 1 -1 -3 -7 230.079 21.3298 1 1 -3 7 209.904 25.5578 1 1 3 -7 211.549 31.6225 1 -1 -3 7 238.735 30.501 1 -1 -3 7 250.917 25.8256 1 -1 3 -7 199.644 29.2892 1 1 -3 -7 361.007 33.4068 1 -1 3 7 285.132 25.8459 1 -1 3 7 209.626 31.082 1 -1 -3 7 243.169 23.6113 1 1 -3 -7 253.306 34.2761 1 1 3 7 255.578 34.2897 1 -1 3 -7 312.007 32.5402 1 1 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987.614 63.5647 1 -1 -3 -10 894.882 43.4945 1 -1 3 10 984.204 62.4853 1 -1 -3 10 970.107 53.7105 1 1 -3 -10 846.824 62.6885 1 1 -3 -10 1007.41 59.5065 1 -1 -3 10 993.225 61.7608 1 -1 -3 10 903.435 47.0601 1 -1 3 -10 981.111 62.1795 1 1 3 10 663.093 53.3911 1 1 3 10 928.025 65.6121 1 1 -3 10 947.991 63.3078 1 1 3 -10 940.961 56.0538 1 -1 3 10 930.894 48.3932 1 -1 -3 10 868.898 48.7216 1 1 -3 11 4.46109 20.1016 1 1 3 11-5.29459 14.8322 1 -1 3 11-18.3189 14.908 1 -1 -3 11 17.4505 15.4795 1 -1 -3 11 14.4669 18.1394 1 -1 3 -11 12.6149 21.0838 1 -1 -3 11 22.3339 20.653 1 1 3 -11 1.93802 19.4001 1 -1 3 11 10.5836 21.0052 1 -1 -3 -11 16.8595 14.5211 1 1 3 -11 17.7419 18.0011 1 1 3 11 4.38892 23.6414 1 -1 -3 11 8.12832 17.1365 1 1 -3 -11 28.3689 19.7252 1 -1 -3 -11 23.4139 15.4952 1 1 -3 -11 14.8593 20.4255 1 1 3 12 188.968 38.8427 1 -1 -3 12 191.045 30.9403 1 1 3 -12 210.08 35.7618 1 1 3 -12 169.599 34.9914 1 -1 3 12 177.521 29.8457 1 -1 -3 12 229.299 31.6737 1 1 -3 -12 187.407 33.8092 1 1 -3 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1 -1 -3 15 1113.47 63.0969 1 -1 -3 -15 1101.95 64.8922 1 -1 3 15 1228.37 66.5786 1 -1 -3 -15 1190.35 78.7585 1 1 -3 -15 993.24 74.8744 1 1 -3 -15 1064.71 68.8638 1 1 3 15 1123.32 76.7972 1 -1 3 -15 1180.46 80.9602 1 1 -3 16 138.591 36.6055 1 1 -3 16 139.619 16.7545 1 -1 -3 16 113.116 28.5932 1 -1 -3 16 139.999 27.3097 1 -1 3 -16 167.054 39.7306 1 1 -3 -16 114.59 33.832 1 1 -3 -16 134.985 36.653 1 -1 3 16 103.752 30.7058 1 1 3 -16 92.8096 35.5294 1 -1 -3 -16 130.536 30.7372 1 1 3 -16 167.379 36.0213 1 -1 -3 -16 114.727 34.8977 1 -1 -3 -16 91.7514 24.3619 1 1 3 16 131.368 39.7915 1 -1 -3 16 83.1577 28.349 1 -1 -3 17 1137.68 59.0607 1 -1 3 17 1197.98 73.2862 1 -1 -3 -17 1205.91 72.2665 1 -1 -3 -17 1187.65 62.2208 1 -1 3 -17 1128.82 85.3063 1 1 3 17 1173.75 83.7474 1 -1 -3 17 1114.75 67.2347 1 -1 -3 17 1066.81 67.9744 1 1 3 -17 1285.91 89.1651 1 -1 -3 -17 1109.21 83.213 1 1 3 -17 1149.92 79.2695 1 1 -3 17 1275.66 83.0108 1 1 -3 -17 1290.26 87.823 1 1 -3 -17 992.31 73.812 1 -1 -3 -18 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1 -4 -27 193.721 69.7197 1 1 -4 -27 306.297 71.3594 1 1 4 -27 360.736 82.5666 1 -1 4 27 162.284 48.7827 1 -1 -4 27 205.602 49.1737 1 -1 -4 27 180.526 43.6558 1 -1 4 -27 295.066 83.3139 1 1 -4 -28 33.054 54.0838 1 -1 -4 28 6.35954 32.2555 1 -1 4 28 39.6462 41.5004 1 1 -4 -28-5.58291 55.7686 1 -1 -4 28-8.65144 32.5127 1 1 4 -28-40.4007 62.8892 1 -1 4 -28 89.7528 75.5945 1 1 5 0 14.557 20.3221 1 1 -5 0 11.513 20.5595 1 -1 -5 0 18.831 16.812 1 -1 -5 0 14.3166 15.2603 1 1 -5 0 29.4632 17.9229 1 -1 5 0 19.3502 21.146 1 -1 -5 -1 2505.38 95.2848 1 -1 -5 1 2529.48 97.5995 1 -1 5 1 2638.46 106.559 1 1 5 1 2624.98 101.698 1 1 -5 1 2615.44 101.057 1 1 -5 1 2614.65 99.0446 1 1 5 -1 2731.48 111.827 1 1 5 -1 2784.86 102.683 1 -1 -5 -1 2721.05 93.5841 1 -1 -5 1 2744.91 93.7318 1 -1 5 -1 2781.97 108.096 1 1 -5 -1 2651.58 97.6232 1 -1 -5 2 419.612 33.2092 1 1 -5 2 445.403 38.588 1 -1 5 2 264.692 35.4971 1 1 5 -2 398.623 45.6454 1 1 -5 2 417.336 40.4172 1 1 5 2 456.52 44.7944 1 -1 -5 -2 453.489 36.1053 1 1 5 -2 522.096 48.2475 1 -1 -5 -2 418.988 33.7691 1 -1 -5 2 429.02 42.5871 1 -1 5 -2 376.574 41.5905 1 1 -5 -2 419.702 37.9314 1 1 -5 -2 374.339 40.4573 1 -1 -5 3 211.72 32.0354 1 1 -5 3 259.515 35.6799 1 1 5 -3 219.581 34.6231 1 1 -5 3 246.998 32.3184 1 -1 -5 -3 206.832 25.3854 1 1 5 -3 222.347 37.3608 1 1 -5 -3 247.418 34.1781 1 -1 5 -3 206.345 33.5675 1 1 -5 -3 246.128 30.6672 1 -1 -5 3 271.102 29.1083 1 1 5 3 225.207 34.2322 1 -1 -5 -3 235.342 27.6472 1 1 5 -4 40.3589 25.4739 1 1 -5 -4 55.4323 23.6835 1 1 5 4 47.7316 23.3806 1 -1 5 -4 33.3273 22.2803 1 1 -5 4 46.9224 23.9804 1 1 -5 4 28.9237 18.1347 1 -1 -5 -4 73.2909 20.578 1 -1 -5 -4 64.4346 18.2849 1 -1 -5 4 71.3434 19.5524 1 1 -5 -4 43.1929 19.6577 1 1 5 -4 42.5259 27.2789 1 -1 -5 4 56.8303 17.6149 1 -1 -5 5 164.565 24.9662 1 1 5 -5 129.027 34.6388 1 -1 -5 -5 130.84 23.1467 1 1 -5 5 111.597 23.4309 1 1 -5 5 118.189 31.2389 1 1 5 -5 135.241 29.7719 1 -1 -5 -5 109.098 20.6019 1 -1 -5 5 157.761 25.6219 1 1 -5 -5 146.059 26.5247 1 1 5 5 103.724 28.5979 1 -1 5 -5 69.9725 26.8568 1 1 -5 -5 153.402 30.3381 1 -1 -5 -6 42.3286 16.7937 1 1 -5 6 9.68126 20.5686 1 1 -5 -6 19.1654 20.7097 1 -1 -5 -6 53.7009 17.7586 1 -1 5 6 23.5912 20.543 1 1 5 -6 70.4287 27.2544 1 1 -5 6 68.9532 20.3983 1 -1 5 6 46.7527 20.4761 1 1 5 -6 53.5838 28.3685 1 -1 -5 6 78.1206 24.164 1 1 -5 -6 56.2664 22.0875 1 -1 5 -6 43.2557 23.4774 1 -1 -5 6 71.8307 18.8308 1 -1 -5 6 88.528 21.8531 1 1 5 6 57.5703 23.5743 1 1 -5 7 180.46 33.1298 1 1 -5 -7 218.366 36.3393 1 1 -5 -7 211.171 31.81 1 -1 -5 -7 174.104 27.8485 1 -1 5 7 203.909 29.7984 1 -1 -5 -7 184.181 25.0323 1 1 5 -7 138.275 32.6356 1 -1 5 7 110.286 27.5809 1 1 -5 7 188.808 28.4825 1 -1 -5 7 181.015 36.8517 1 -1 -5 7 194.833 28.3124 1 -1 -5 7 204.499 27.5299 1 -1 5 -7 186.941 34.9927 1 1 -5 8 96.8429 23.4171 1 -1 -5 -8 142.992 23.0611 1 -1 5 8 94.7101 26.2247 1 1 -5 8 183.90 37.5908 1 1 -5 -8 114.763 29.6269 1 -1 -5 8 129.231 26.0347 1 -1 -5 8 151.272 25.4912 1 -1 -5 -8 162.364 28.1363 1 1 -5 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22.2871 17.3904 1 2 0 -11 579.457 48.497 1 -2 0 -11 603.448 50.8631 1 2 0 11 591.675 53.009 1 -2 0 11 611.794 46.1033 1 -2 0 -11 586.873 42.7481 1 2 0 12 412.386 54.9242 1 -2 0 -12 358.997 39.9737 1 -2 0 -12 442.983 41.0629 1 2 0 -12 350.634 41.5845 1 2 0 12 345.035 44.5307 1 -2 0 12 345.096 38.5796 1 2 0 -13 46.6767 23.0549 1 -2 0 -13 49.8619 23.1243 1 2 0 13 2.36969 23.8353 1 2 0 13 21.825 23.9797 1 -2 0 -14 1654.07 86.7085 1 2 0 14 1666.21 94.3695 1 2 0 -14 1708.69 88.9909 1 2 0 14 1718.34 88.4492 1 2 0 15 194.531 40.6265 1 2 0 -15 173.124 37.5887 1 -2 0 -15 266.671 42.5237 1 -2 0 -16 860.53 69.0941 1 2 0 16 878.297 72.9712 1 2 0 -16 988.525 74.3091 1 2 0 -17 -23.95 26.1997 1 -2 0 -17-11.3208 13.3757 1 2 0 17-5.05004 36.4721 1 -2 0 -17 6.84347 23.7902 1 2 0 -18 161.901 41.9996 1 -2 0 -18 143.665 39.4068 1 -2 0 -19 825.677 77.5638 1 2 0 -19 655.258 73.8802 1 2 0 -20 3.82268 30.1888 1 -2 0 -20 41.3211 33.997 1 -2 0 -21 182.09 49.2999 1 2 0 -21 190.137 47.8361 1 2 0 -22-24.5946 32.4963 1 -2 0 -22-0.65649 36.1986 1 2 0 -23 274.645 59.251 1 -2 0 -23 308.938 61.6375 1 -2 0 -24 138.514 56.5227 1 2 0 -24 198.887 57.5863 1 -2 0 -25-29.2257 44.7996 1 2 0 -25-35.2719 39.6594 1 -2 0 -26 16.863 47.3935 1 2 0 -26 25.946 51.1958 1 -2 0 -27 212.561 68.1716 1 2 0 -27 212.993 64.4486 1 -2 0 -28 38.9025 60.6441 1 2 0 -28 40.8242 55.2267 1 -2 -1 0 1530.63 75.7946 1 2 -1 0 1462.22 45.193 1 2 -1 1 293.507 18.8145 1 2 -1 1 265.452 30.8617 1 -2 -1 -1 265.814 41.1011 1 -2 -1 1 248.062 37.574 1 2 -1 -1 287.21 16.4324 1 2 -1 2 286.459 30.2873 1 2 1 -2 254.616 20.5907 1 2 -1 2 215.676 18.211 1 -2 -1 -2 290.436 39.4095 1 2 -1 -2 272.181 18.5567 1 -2 -1 2 271.298 39.6519 1 2 -1 3 1419.00 79.5487 1 2 -1 3 1499.12 52.578 1 -2 -1 -3 1359.49 71.2945 1 2 -1 3 1461.71 58.1234 1 2 1 -3 1319.31 50.8361 1 -2 -1 3 1334.17 74.4487 1 2 -1 -3 1483.37 50.1394 1 2 1 4 123.996 20.0028 1 -2 -1 -4 123.641 28.8515 1 2 1 -4 120.575 17.6537 1 2 -1 4 147.331 19.697 1 2 -1 4 117.816 19.3806 1 2 -1 4 101.71 27.931 1 -2 -1 4 116.21 29.2005 1 2 -1 -4 118.223 16.3763 1 -2 1 5 203.021 16.6038 1 2 -1 5 220.107 24.4135 1 2 -1 5 246.285 22.8073 1 2 1 -5 207.331 23.0786 1 2 -1 -5 249.735 23.8718 1 -2 -1 5 242.756 40.4224 1 2 1 5 270.882 42.2108 1 2 1 5 220.42 25.9067 1 -2 1 -5 242.726 21.2634 1 -2 -1 -5 217.238 33.7037 1 2 -1 5 194.488 29.8181 1 2 -1 6 445.945 35.9833 1 -2 -1 -6 496.679 47.1237 1 -2 1 6 413.905 27.3514 1 2 -1 6 464.015 45.2298 1 2 -1 6 412.957 25.6837 1 2 1 -6 453.402 35.1428 1 -2 -1 6 391.447 27.2311 1 2 -1 -6 457.678 34.706 1 -2 -1 6 467.098 50.1276 1 2 1 6 449.661 51.0443 1 2 1 6 424.129 36.2794 1 -2 1 -6 434.576 30.5791 1 -2 -1 7 134.021 18.5812 1 2 1 7 173.704 27.3216 1 -2 -1 -7 128.164 28.295 1 2 -1 7 201.348 31.5884 1 -2 1 7 149.714 19.9243 1 2 -1 7 144.266 16.2565 1 2 -1 7 149.735 24.1313 1 2 1 -7 126.215 22.6102 1 -2 1 -7 148.691 22.1534 1 2 -1 -7 164.696 24.637 1 -2 1 -7 174.496 20.517 1 -2 -1 7 138.681 32.085 1 2 1 -8 2164.69 86.0555 1 2 -1 8 2206.33 89.3737 1 2 -1 8 2328.36 90.0881 1 -2 -1 -8 2175.98 91.2411 1 2 -1 8 2231.03 68.9294 1 -2 1 8 2194.54 80.1952 1 -2 1 -8 2305.48 83.6292 1 2 1 8 2210.90 90.0006 1 2 -1 -8 2157.06 84.7112 1 -2 -1 8 2155.30 79.9547 1 -2 -1 8 2092.79 97.3174 1 -2 1 -8 2205.35 72.2164 1 -2 1 -9 75.6381 14.8389 1 2 1 -9 34.3321 20.3134 1 2 -1 9 64.0034 22.1924 1 -2 -1 -9 18.5553 19.2491 1 2 -1 9 43.7834 21.0766 1 -2 1 9 55.3327 18.82 1 2 -1 -9 72.591 21.9859 1 -2 -1 9 48.6323 25.0905 1 2 1 9 76.9207 24.3567 1 -2 1 -9 22.9963 17.0169 1 -2 -1 9 54.3395 17.5036 1 2 -1 10 674.814 53.3667 1 -2 -1 -10 667.002 46.0866 1 -2 -1 -10 630.637 45.7329 1 2 1 -10 612.958 48.7772 1 2 -1 10 662.809 45.3175 1 -2 1 10 629.834 44.5074 1 2 1 10 686.081 54.1399 1 -2 1 -10 560.50 44.9652 1 -2 -1 10 662.674 44.0961 1 -2 -1 10 715.144 55.4371 1 -2 1 -10 689.867 33.57 1 2 -1 -10 652.165 49.4235 1 -2 -1 -11 167.963 28.3112 1 -2 1 -11 276.418 23.5346 1 2 -1 11 199.645 34.1791 1 -2 1 11 216.509 30.4784 1 -2 -1 -11 177.942 29.4994 1 2 1 -11 169.744 30.1109 1 2 -1 11 208.61 31.0309 1 -2 1 -11 232.738 31.9389 1 2 1 11 238.653 38.7705 1 -2 -1 11 182.967 29.1307 1 -2 -1 11 147.071 33.2731 1 2 -1 -11 148.994 28.7292 1 -2 1 -12 301.985 23.8542 1 -2 -1 -12 314.761 36.6595 1 2 -1 12 280.967 33.2669 1 -2 1 12 306.487 36.3469 1 2 -1 12 262.595 45.356 1 2 1 -12 269.173 37.4212 1 2 -1 12 306.068 41.9952 1 -2 -1 -12 294.792 35.8319 1 2 -1 -12 301.809 40.3224 1 -2 -1 12 282.86 36.0788 1 2 1 12 238.565 38.2065 1 -2 -1 12 311.787 46.0536 1 -2 1 -12 307.49 37.9082 1 2 1 12 278.271 42.0714 1 -2 1 -13 126.82 29.1001 1 2 1 13 42.6198 27.9224 1 -2 -1 -13 70.0311 21.0331 1 2 -1 13 72.5534 29.6557 1 -2 -1 -13 66.6479 24.5474 1 2 -1 13 80.4234 22.0635 1 2 1 -13 58.4484 26.7331 1 2 -1 13 71.8233 30.1213 1 2 1 13 69.606 30.2346 1 2 -1 -13 89.4343 27.8578 1 -2 -1 13 125.597 31.4725 1 -2 1 -13 104.275 18.2968 1 2 1 14 10.0095 26.2386 1 -2 -1 14 28.4122 25.8553 1 2 1 -14 25.7035 26.1056 1 -2 -1 -14-1.98126 18.4753 1 2 1 14 7.42502 26.1517 1 2 -1 14 9.94348 19.1964 1 2 -1 14 21.8911 26.3082 1 -2 -1 -14 2.51039 15.8572 1 -2 1 -14 19.0548 14.5496 1 -2 1 -14 33.3603 22.2023 1 2 -1 -14 35.3613 24.3153 1 2 -1 14 34.8077 29.5269 1 -2 -1 -15 232.292 30.7209 1 2 -1 15 234.195 43.7559 1 -2 -1 -15 283.659 42.9967 1 2 1 -15 201.489 40.2679 1 -2 1 -15 304.953 28.741 1 2 1 15 164.642 40.3672 1 -2 1 -15 279.443 43.5236 1 2 -1 -15 225.374 39.8409 1 2 1 16 170.731 43.938 1 -2 -1 -16 150.496 36.5031 1 -2 -1 -16 146.496 26.0363 1 2 1 -16 203.387 40.4531 1 2 -1 16 142.366 40.4371 1 -2 1 -16 139.505 34.4985 1 2 -1 -16 149.288 37.6377 1 -2 1 -16 177.695 24.5596 1 2 -1 -17 162.085 38.9792 1 2 1 -17 138.282 38.2787 1 -2 -1 -17 179.728 26.812 1 -2 -1 -17 106.292 33.8176 1 -2 1 -17 172.054 25.9383 1 -2 1 -17 173.937 38.7436 1 2 1 17 122.837 58.8916 1 -2 -1 -18 124.323 37.639 1 2 1 -18 126.798 39.1893 1 -2 1 -18 131.851 38.1034 1 2 -1 -18 91.099 36.9441 1 -2 -1 -19-1.66466 24.7667 1 2 -1 -19 28.5736 34.4489 1 -2 1 -19 40.4077 33.5875 1 2 1 -19 32.0194 36.1633 1 2 1 -20 326.624 57.9567 1 -2 -1 -20 531.973 68.435 1 -2 1 -20 441.202 66.0652 1 2 -1 -20 356.314 58.4885 1 -2 -1 -21 169.983 46.5086 1 2 1 -21 190.659 48.725 1 -2 1 -21 255.10 53.5776 1 2 -1 -21 296.766 55.6352 1 2 1 -22 133.982 48.0761 1 -2 -1 -22 148.559 46.7685 1 -2 1 -22 219.644 54.5049 1 2 -1 -22 138.688 48.7492 1 2 1 -23 27.9249 44.4946 1 -2 -1 -23 129.025 47.82 1 2 -1 -23 82.2013 47.1317 1 -2 1 -23 146.687 49.8605 1 -2 -1 -24 449.863 73.6109 1 2 -1 -24 316.507 67.4515 1 2 1 -24 180.091 59.103 1 -2 1 -24 290.867 66.2104 1 -2 -1 -25 17.8348 45.3788 1 2 -1 -25-13.2967 41.7532 1 -2 1 -25 25.5683 48.5568 1 2 1 -25-2.85621 43.9164 1 -2 1 -26 531.951 84.9532 1 -2 -1 -26 607.201 88.3626 1 2 1 -26 558.595 91.6033 1 2 -1 -26 466.258 85.1457 1 -2 1 -27 12.5534 57.0013 1 -2 -1 -27 134.341 60.8923 1 2 1 -27 146.73 58.1476 1 2 -1 -27-9.87332 43.0146 1 -2 -1 -28 63.0719 62.7566 1 2 1 -28-13.5625 51.9233 1 -2 1 -28-21.1158 59.5425 1 2 -1 -28 43.1271 56.9045 1 2 -2 0 3245.78 99.094 1 -2 -2 0 3346.82 126.568 1 2 -2 0 3103.55 113.918 1 2 -2 1 301.133 36.5458 1 2 -2 1 279.491 24.1666 1 -2 -2 -1 327.00 43.0818 1 -2 -2 1 297.615 41.0984 1 2 -2 -1 268.903 35.7667 1 2 2 -2 2113.35 72.5076 1 2 -2 2 1885.24 77.3237 1 -2 -2 -2 2024.28 92.1364 1 2 -2 2 2031.60 69.9735 1 2 -2 -2 1987.42 86.8719 1 2 -2 3 490.38 36.9971 1 2 -2 3 510.759 33.2175 1 -2 2 3 390.699 20.0053 1 -2 -2 -3 612.081 58.593 1 2 2 -3 503.975 34.3504 1 -2 2 3 480.612 21.9812 1 -2 2 -3 545.715 39.2457 1 2 2 3 469.827 27.0175 1 -2 -2 3 380.219 45.0004 1 2 -2 -3 448.979 44.4269 1 2 2 4 25.4377 10.4517 1 2 2 -4-0.87075 15.3541 1 2 -2 4 39.5152 15.2711 1 -2 2 4 25.3988 10.9374 1 -2 -2 -4 58.0732 25.2056 1 2 -2 4 41.3108 17.3967 1 -2 2 -4 72.2601 20.8701 1 -2 2 -4 50.7796 12.6845 1 -2 -2 4 50.2077 27.6369 1 2 -2 5 743.023 39.4885 1 -2 -2 -5 808.073 55.5807 1 -2 2 5 658.891 34.579 1 2 -2 5 749.257 43.547 1 2 2 -5 763.259 44.2122 1 -2 2 -5 739.792 44.0049 1 -2 2 -5 764.036 39.2092 1 -2 -2 5 731.961 58.6064 1 2 2 5 847.303 49.3086 1 2 2 5 781.633 29.3472 1 2 -2 -5 766.254 41.9338 1 2 2 6 1295.97 64.6326 1 2 -2 -6 1316.58 59.8122 1 -2 2 -6 1307.86 57.7509 1 -2 2 6 1431.40 54.3831 1 -2 -2 -6 1215.29 69.2521 1 2 -2 6 1329.53 53.2805 1 2 -2 6 1361.73 62.9406 1 2 2 -6 1306.54 61.3414 1 -2 -2 6 1392.15 77.5174 1 -2 2 -6 1308.76 56.1481 1 2 -2 7 493.816 30.934 1 2 -2 7 556.094 42.8472 1 -2 -2 -7 550.73 52.7911 1 2 2 -7 540.472 42.5902 1 -2 2 7 556.037 35.7697 1 2 -2 -7 490.963 40.7987 1 2 2 7 513.817 45.2487 1 -2 -2 7 596.732 37.7317 1 -2 -2 7 595.081 58.5905 1 -2 2 -7 563.749 37.0239 1 -2 2 -7 510.598 37.0356 1 2 -2 8 343.86 45.851 1 2 2 -8 297.337 34.6053 1 -2 2 8 294.974 29.1739 1 2 -2 8 253.315 32.5852 1 2 -2 8 334.633 27.2155 1 -2 -2 -8 321.828 41.7108 1 -2 -2 8 193.072 37.4741 1 2 -2 -8 271.414 32.1674 1 -2 2 -8 310.173 30.6359 1 -2 2 -8 253.627 29.9294 1 -2 -2 8 256.184 28.7605 1 2 2 8 332.96 37.659 1 -2 -2 9 320.68 45.6007 1 2 2 -9 331.475 37.8336 1 2 -2 9 329.758 27.2332 1 -2 -2 -9 315.952 40.8106 1 2 -2 9 360.793 39.3053 1 2 -2 9 308.051 36.8006 1 -2 2 9 336.709 33.5466 1 2 2 9 377.875 41.9233 1 2 -2 -9 331.367 37.2894 1 -2 2 -9 451.787 36.2609 1 -2 -2 9 267.186 30.9289 1 -2 2 -9 350.018 36.2097 1 -2 -2 -10 47.1094 20.642 1 2 -2 10 39.8666 21.6853 1 2 -2 10 38.0599 14.0856 1 -2 2 10 82.9366 21.4056 1 2 -2 10 98.3201 26.708 1 2 2 -10 54.3807 22.1298 1 2 -2 -10 55.0656 22.1435 1 -2 -2 10 50.4259 19.0648 1 -2 2 -10 57.4741 17.1979 1 -2 2 -10 76.6244 22.167 1 -2 -2 10 64.7585 28.1483 1 2 2 10 25.7724 23.0863 1 -2 2 11 445.077 42.0953 1 -2 -2 -11 468.174 46.7884 1 2 -2 11 481.811 51.0775 1 2 2 -11 440.20 45.272 1 2 -2 11 510.14 39.89 1 2 -2 -11 493.283 47.0361 1 -2 -2 11 520.70 46.0685 1 2 2 11 509.328 53.0787 1 2 2 11 431.469 54.7676 1 -2 2 -11 442.493 44.1328 1 -2 2 -11 534.879 34.7061 1 -2 -2 11 447.90 51.4555 1 -2 2 12 39.2091 23.4822 1 2 2 12 24.4828 25.07 1 2 -2 12 65.636 28.2414 1 2 2 -12 115.203 29.9328 1 2 -2 12 29.9333 20.7764 1 -2 -2 -12 41.7085 21.5083 1 2 2 12 43.9433 30.1344 1 -2 2 -12 90.1718 19.8381 1 2 -2 -12 45.9011 23.1877 1 -2 -2 12 34.9242 25.6692 1 -2 2 -12 25.2093 22.0043 1 2 2 -13 36.0656 24.6175 1 2 -2 13 17.5205 26.5977 1 -2 2 -13 55.0564 20.197 1 -2 -2 13 56.4851 29.1368 1 2 2 13 39.8035 29.482 1 -2 2 -13 25.9043 23.2658 1 2 -2 -13 64.3738 25.6689 1 2 -2 13 42.4743 27.2487 1 -2 -2 -13 65.6406 21.6103 1 2 -2 13 20.4609 21.3665 1 2 2 13 31.6882 28.7359 1 -2 2 -14 72.7312 21.3019 1 2 -2 14 18.3169 29.3673 1 2 -2 14 37.6831 21.2961 1 -2 -2 -14 49.157 20.6917 1 2 2 -14 40.7118 27.794 1 -2 2 -14-10.7203 22.106 1 -2 -2 14-0.85384 23.0515 1 2 -2 -14 17.2244 24.5778 1 2 2 14 52.1539 31.386 1 2 2 15 388.888 53.1594 1 -2 -2 15 521.667 57.3257 1 -2 -2 -15 529.277 48.0168 1 2 2 -15 579.56 61.1255 1 2 -2 15 538.28 44.4292 1 2 -2 15 586.671 64.8133 1 -2 2 -15 534.622 40.7036 1 2 -2 -15 482.386 56.1278 1 -2 2 -15 527.897 55.3771 1 -2 2 -16 517.29 43.5917 1 2 -2 -16 339.566 50.2846 1 2 2 -16 327.933 51.8411 1 2 2 16 439.651 61.6696 1 -2 -2 -16 435.47 43.1019 1 2 -2 16 392.087 54.296 1 2 -2 16 448.789 37.7512 1 -2 -2 16 411.485 51.4259 1 -2 2 -16 379.285 51.0959 1 -2 2 -17 242.269 46.1657 1 -2 -2 -17 303.456 36.2185 1 2 2 -17 297.324 51.72 1 -2 -2 -17 292.149 48.1703 1 2 -2 -17 228.641 46.5694 1 -2 -2 17 242.727 41.1345 1 -2 -2 -18 265.709 33.5227 1 2 2 -18 163.494 43.9871 1 -2 2 -18 359.326 56.3169 1 -2 -2 18 309.245 45.142 1 -2 -2 -18 284.396 49.344 1 2 -2 -18 190.13 44.7584 1 -2 -2 -19 828.387 46.8301 1 -2 -2 -19 666.136 70.4562 1 -2 2 -19 899.668 84.5498 1 2 2 -19 714.645 76.2983 1 2 -2 -19 711.944 75.7817 1 2 -2 -20 104.152 39.6777 1 -2 -2 -20-10.2496 27.9528 1 -2 2 -20 23.097 31.9303 1 2 2 -20 27.3335 35.2387 1 -2 -2 -21 136.879 43.6786 1 2 2 -21 24.9248 38.0885 1 2 -2 -21 168.211 48.9311 1 -2 2 -21 100.276 42.489 1 2 2 -22 90.0408 47.5695 1 -2 -2 -22 124.124 46.3778 1 2 -2 -22 81.3022 45.9962 1 -2 2 -22 112.746 47.2463 1 -2 -2 -23 31.8543 40.919 1 2 2 -23 19.8154 42.8684 1 -2 2 -23-31.7181 34.6458 1 2 -2 -23 40.3213 44.5196 1 2 2 -24 134.968 55.5404 1 -2 -2 -24 116.403 55.6266 1 2 -2 -24 32.0533 46.6791 1 -2 2 -24 112.525 55.5963 1 2 2 -25 107.635 54.8342 1 -2 -2 -25 19.4079 49.5656 1 -2 2 -25 140.063 57.2303 1 2 -2 -25 189.852 64.2604 1 -2 2 -26 128.026 62.192 1 -2 -2 -26 47.8596 56.1047 1 2 2 -26 60.9184 54.9555 1 2 -2 -26-29.1378 45.1455 1 -2 -2 -27 89.9761 61.5694 1 2 2 -27 91.6629 59.7006 1 2 -2 -27 68.633 56.5581 1 -2 2 -27 41.0809 60.179 1 2 2 -28 24.2178 96.0429 1 -2 -2 -28-18.6084 53.5973 1 2 -2 -28-9.55562 87.5489 1 -2 2 -28 33.4167 61.3186 1 2 3 0 22.9367 14.9127 1 -2 -3 0-9.46253 19.785 1 -2 3 0 23.9598 12.2147 1 2 -3 0 27.2517 19.4084 1 2 -3 1 542.719 48.3674 1 -2 -3 -1 617.534 59.6406 1 2 -3 1 609.429 38.9227 1 -2 3 1 495.411 30.5874 1 -2 3 1 519.532 30.3535 1 -2 3 -1 531.468 32.2341 1 2 3 1 626.981 37.0546 1 2 -3 -1 456.691 43.6962 1 -2 -3 1 520.523 53.5118 1 -2 3 2 1922.58 67.129 1 -2 3 2 1897.86 66.5453 1 2 -3 2 1891.95 79.1831 1 2 3 -2 1861.26 76.4435 1 -2 -3 -2 1806.87 89.033 1 2 -3 2 1908.00 74.4567 1 -2 3 -2 1803.06 66.322 1 2 3 2 1825.03 66.5356 1 2 -3 -2 1817.50 84.3119 1 2 -3 3 150.168 23.9936 1 -2 -3 -3 225.163 39.1201 1 2 -3 3 219.394 31.1158 1 -2 3 3 166.586 20.6542 1 2 3 -3 183.548 26.3018 1 -2 3 3 177.951 20.2901 1 2 -3 -3 235.763 36.1562 1 -2 -3 3 240.082 38.4652 1 2 3 3 175.865 21.3971 1 -2 3 -3 312.103 42.685 1 -2 3 -3 161.942 21.7175 1 2 3 4 730.741 34.7866 1 -2 3 -4 743.83 42.0747 1 2 -3 -4 726.233 56.2889 1 2 -3 4 771.805 46.2141 1 -2 3 4 767.323 40.0165 1 2 -3 4 661.489 43.1825 1 2 3 -4 690.458 47.218 1 -2 3 4 675.334 39.0776 1 -2 -3 -4 749.206 56.0483 1 -2 -3 4 722.718 56.0681 1 -2 3 -4 685.115 48.8439 1 -2 -3 -5 1556.36 80.7907 1 -2 3 5 1673.06 65.2943 1 2 3 -5 1678.99 74.7351 1 2 -3 5 1565.49 66.3516 1 2 -3 5 1667.13 71.3409 1 -2 -3 5 1752.66 87.5209 1 2 3 5 1702.32 57.4957 1 -2 3 -5 1605.39 67.9095 1 2 -3 -5 1571.14 85.0927 1 -2 3 -5 1711.74 74.4028 1 2 3 -6 542.423 44.899 1 -2 3 6 513.248 37.9981 1 -2 -3 -6 561.655 56.6128 1 2 -3 6 527.389 43.9994 1 2 -3 6 576.744 37.6487 1 2 -3 -6 649.969 60.812 1 -2 3 -6 716.464 54.3939 1 -2 3 -6 514.676 40.3749 1 -2 -3 6 559.932 57.9481 1 2 3 6 548.651 29.3582 1 -2 -3 -7 1185.96 68.5584 1 2 -3 7 1242.12 64.5728 1 2 -3 7 1188.11 53.7846 1 -2 3 7 1240.98 58.6888 1 2 3 -7 1249.85 65.7914 1 2 3 7 1252.99 68.6741 1 -2 3 -7 1113.67 59.5084 1 2 3 7 1172.57 44.7285 1 -2 -3 7 1213.27 59.119 1 -2 3 -7 1262.08 60.5387 1 -2 -3 7 1307.12 77.0049 1 2 -3 -7 1237.93 76.2824 1 2 -3 8 691.651 51.1716 1 2 3 -8 630.77 49.9518 1 -2 3 8 642.062 44.0559 1 2 -3 8 560.701 36.94 1 -2 -3 -8 566.83 54.4588 1 -2 -3 8 614.505 44.2376 1 -2 3 -8 615.234 44.1526 1 -2 -3 8 553.632 57.1626 1 2 -3 -8 587.963 59.6444 1 2 -3 -8 652.008 48.1171 1 -2 3 -8 666.653 47.7958 1 2 3 8 623.99 54.3776 1 2 -3 9 1526.00 64.9567 1 -2 -3 -9 1640.31 80.9471 1 2 -3 9 1785.15 83.0563 1 -2 3 9 1731.21 75.4043 1 2 -3 -9 1678.70 78.2074 1 -2 -3 9 1611.66 87.4827 1 -2 3 -9 1694.02 71.699 1 -2 3 -9 1565.08 76.6425 1 -2 -3 9 1563.91 73.4618 1 2 3 -9 1726.22 82.0959 1 2 3 9 1606.87 86.3224 1 2 -3 10 569.457 37.2769 1 -2 -3 -10 531.059 53.3872 1 2 -3 10 562.312 51.7148 1 -2 3 10 487.577 45.325 1 2 3 -10 521.301 49.568 1 2 3 10 564.334 52.466 1 2 3 10 442.745 51.9298 1 -2 -3 10 590.097 61.6706 1 -2 3 -10 557.252 48.7307 1 -2 -3 10 569.088 47.2858 1 2 -3 -10 516.85 47.3921 1 -2 3 -10 618.901 48.9788 1 2 -3 11 240.646 38.225 1 -2 3 11 208.496 35.1181 1 -2 -3 -11 254.962 39.4315 1 2 3 -11 225.665 37.5547 1 2 -3 11 290.665 29.9811 1 2 -3 -11 198.765 32.9483 1 2 3 11 197.129 38.4705 1 -2 -3 11 173.435 38.0457 1 2 3 11 256.071 42.6189 1 -2 3 -11 258.92 38.1179 1 -2 -3 -12 362.087 43.993 1 2 -3 12 325.059 45.1055 1 2 3 -12 407.617 47.4949 1 2 3 12 288.667 43.1906 1 -2 3 -12 409.365 46.558 1 2 -3 -12 273.298 41.6169 1 2 3 12 338.881 48.641 1 -2 -3 12 433.078 53.2853 1 2 -3 13 357.45 54.5705 1 -2 -3 -13 404.417 46.3082 1 2 3 -13 420.313 49.8652 1 2 -3 13 494.146 53.9016 1 2 -3 -13 405.474 49.0523 1 -2 3 -13 429.455 49.0825 1 2 3 13 337.805 47.1991 1 -2 -3 13 472.432 56.3367 1 2 -3 14 276.476 47.2726 1 -2 -3 -14 249.669 36.8763 1 2 -3 14 275.988 36.549 1 2 3 -14 199.156 40.6719 1 2 -3 -14 252.079 42.9256 1 -2 3 -14 184.694 38.5106 1 -2 -3 14 284.674 46.412 1 2 3 14 256.541 46.3228 1 -2 -3 15 390.765 52.1004 1 2 -3 15 344.322 53.1784 1 -2 -3 -15 388.64 45.4236 1 2 3 -15 287.461 47.4445 1 2 -3 15 481.526 43.5726 1 -2 3 -15 385.781 50.4747 1 2 3 15 324.544 53.402 1 2 -3 -15 430.447 55.2387 1 -2 -3 16 718.048 68.6672 1 2 3 -16 599.632 65.394 1 2 -3 16 608.331 46.3211 1 -2 -3 -16 626.087 49.2919 1 2 -3 -16 647.231 69.0545 1 -2 3 -16 744.064 73.7223 1 -2 3 -17 359.18 54.4749 1 2 3 -17 294.888 51.8222 1 -2 -3 -17 332.73 41.6732 1 2 -3 -17 374.027 55.5352 1 -2 -3 17 247.92 47.387 1 2 3 -18 36.7871 36.3593 1 -2 -3 -18 33.6595 21.1178 1 -2 -3 18-5.73248 27.8435 1 -2 3 -18 90.8702 38.2486 1 2 -3 -18-25.0823 29.2726 1 2 3 -19 267.183 55.182 1 -2 -3 -19 380.725 42.7234 1 -2 3 -19 293.787 57.7806 1 -2 -3 19 407.253 53.7679 1 2 -3 -19 322.132 55.8435 1 2 3 -20 309.805 59.0194 1 -2 -3 -20 278.60 39.5122 1 2 -3 -20 171.254 47.6726 1 -2 3 -20 347.606 60.0291 1 -2 -3 20 287.513 45.259 1 2 3 -21 128.069 48.9554 1 -2 3 -21 165.668 54.8138 1 2 -3 -21 188.375 51.9864 1 2 3 -22 10.8749 39.368 1 2 -3 -22 21.9667 41.0885 1 -2 3 -22-6.46106 41.3049 1 -2 3 -23 83.3098 51.5617 1 2 3 -23 1.92292 45.0477 1 2 -3 -23 41.8547 45.7726 1 2 -3 -24 20.8132 41.2452 1 -2 3 -24 8.45692 44.0417 1 2 3 -24 67.4261 49.3311 1 2 3 -25 91.7989 53.7324 1 -2 3 -25 20.1506 47.5224 1 2 -3 -25 4.493 45.2428 1 2 3 -26 -7.6643 48.5665 1 -2 3 -26 44.2258 52.4668 1 2 -3 -26-51.3738 44.0757 1 2 3 -27 67.5065 56.3064 1 2 -3 -27 143.245 61.0505 1 -2 3 -27 56.2404 61.1723 1 -2 3 -28-26.9841 63.2665 1 2 -4 0 58.0064 22.8692 1 -2 -4 0-13.5913 21.0797 1 -2 4 0 34.8423 15.7332 1 -2 4 1 34.7602 16.3187 1 2 -4 1 82.9132 21.6831 1 2 -4 1 52.7608 22.9209 1 2 4 1 94.1489 21.4689 1 2 -4 -1 58.7791 25.3751 1 -2 -4 1 84.0103 28.8421 1 -2 4 -1 55.6965 17.4903 1 2 -4 2 539.155 44.1564 1 2 -4 2 501.704 42.6271 1 2 4 -2 575.846 49.1573 1 -2 4 2 507.769 38.4462 1 2 -4 -2 420.996 45.9294 1 -2 4 -2 511.535 38.4684 1 2 4 2 491.008 36.0811 1 -2 -4 2 603.705 60.0227 1 2 4 -3 2083.81 89.9928 1 2 -4 3 2055.29 85.2657 1 -2 4 3 2039.18 80.1384 1 2 -4 3 2096.47 86.3142 1 -2 4 3 2141.97 80.6222 1 2 4 3 2044.95 73.9013 1 -2 -4 3 2025.38 96.2479 1 -2 4 -3 1998.06 79.441 1 2 -4 -3 1954.10 93.4729 1 -2 4 4 1198.73 58.7535 1 2 4 -4 1173.41 66.3159 1 2 -4 4 1126.29 59.5492 1 -2 4 4 1197.73 59.0385 1 2 4 4 1199.90 51.3685 1 -2 4 -4 1152.48 58.6988 1 2 -4 -4 1209.93 72.9751 1 -2 -4 4 1099.61 71.5758 1 2 -4 4 1225.43 64.5087 1 2 -4 5 1023.82 55.3537 1 2 4 -5 1037.96 62.3633 1 -2 4 5 970.29 54.2166 1 2 -4 5 1031.98 60.4628 1 2 -4 -5 1036.56 69.3433 1 -2 4 -5 1018.42 56.5359 1 2 4 5 1052.49 48.2865 1 -2 -4 5 1051.78 69.6032 1 2 -4 6 329.869 34.4625 1 -2 4 6 279.176 33.1703 1 2 4 -6 252.552 35.4637 1 2 -4 6 263.503 35.8087 1 2 4 6 282.215 27.0759 1 2 -4 -6 298.296 41.724 1 -2 -4 6 289.232 42.8832 1 -2 4 -6 332.486 36.0646 1 2 -4 -7 459.683 53.3451 1 -2 4 -7 443.898 42.9691 1 -2 4 7 514.611 43.368 1 2 -4 7 534.737 44.084 1 2 4 -7 392.17 43.9648 1 2 -4 7 495.505 47.1708 1 2 4 7 475.229 33.9167 1 -2 -4 7 527.88 54.6839 1 -2 4 8 150.734 29.1502 1 2 -4 8 172.169 32.6426 1 2 -4 8 211.882 28.3902 1 2 4 -8 161.297 31.724 1 2 -4 -8 225.656 39.699 1 2 4 8 117.32 37.5286 1 2 4 8 162.49 23.4473 1 2 4 8 129.659 33.3301 1 -2 4 -8 161.921 29.787 1 -2 -4 8 190.52 38.5966 1 2 -4 9 80.4145 21.2985 1 2 4 -9 53.2261 26.7081 1 2 -4 9 92.904 28.7775 1 -2 4 9 17.2558 21.3498 1 -2 -4 -9 71.3629 15.8027 1 2 -4 -9 63.9331 28.7565 1 2 4 9 24.9481 25.115 1 -2 -4 9 97.1356 33.2417 1 2 4 9 52.0882 18.9929 1 -2 4 -9 62.4695 24.4472 1 2 4 -10 1058.83 71.3446 1 -2 -4 -10 1043.90 42.1801 1 2 -4 10 979.484 54.4169 1 2 -4 10 1062.41 70.2412 1 -2 -4 -10 959.893 64.239 1 2 -4 -10 1074.65 78.6605 1 2 4 10 986.851 67.4001 1 -2 -4 10 1083.25 73.3305 1 2 4 10 1033.89 76.3068 1 -2 4 -10 890.34 63.339 1 2 4 -11 65.6266 28.1321 1 2 -4 11 35.9849 18.8295 1 -2 -4 -11 24.4654 21.2645 1 -2 -4 -11 47.7501 13.5529 1 2 -4 11 76.5188 29.7898 1 -2 -4 11 26.6427 27.1387 1 2 4 11-4.92641 26.0887 1 2 -4 -11 51.7009 32.3391 1 2 4 11 4.69904 26.9126 1 -2 4 -11 39.3306 24.605 1 2 -4 -12 221.061 45.1164 1 -2 -4 -12 243.678 39.5892 1 -2 -4 -12 265.263 22.2321 1 2 4 -12 240.516 42.6254 1 2 -4 12 362.13 38.9113 1 2 4 12 267.958 47.8271 1 -2 4 -12 299.945 44.052 1 -2 -4 12 240.283 45.1696 1 -2 -4 -13 475.942 27.2738 1 2 -4 -13 411.321 56.2135 1 2 4 13 317.354 53.1552 1 2 4 -13 437.235 55.4337 1 -2 -4 -13 413.367 48.7681 1 -2 -4 13 569.072 62.5801 1 -2 4 -13 455.308 53.226 1 2 -4 -14 330.612 48.0927 1 2 4 -14 242.70 45.7091 1 -2 -4 -14 286.574 42.7073 1 -2 -4 14 290.202 49.5395 1 2 4 14 267.96 54.5931 1 -2 4 -14 332.423 47.8709 1 2 -4 -14 377.176 59.2903 1 -2 4 -15 745.51 70.6562 1 -2 -4 -15 597.178 59.441 1 2 4 -15 567.707 66.896 1 2 -4 -15 639.373 70.1105 1 2 -4 -15 672.429 77.8192 1 -2 -4 15 665.28 69.2805 1 -2 -4 16 91.2183 38.061 1 2 4 -16 22.4448 33.8215 1 -2 -4 -16 64.3462 26.4568 1 -2 4 -16 72.6583 34.4913 1 2 -4 -16 84.2458 34.6254 1 2 -4 -16 105.562 39.2178 1 2 4 -17 145.468 44.5145 1 -2 -4 -17 194.544 36.9728 1 -2 -4 17 230.319 47.6098 1 2 -4 -17 178.089 44.6017 1 2 -4 -17 224.613 53.7895 1 -2 4 -17 166.184 44.124 1 -2 -4 -18 81.9057 27.717 1 2 4 -18 107.122 42.0526 1 -2 -4 18 66.5952 35.9638 1 2 -4 -18 41.0826 33.0568 1 -2 4 -18 109.825 40.462 1 2 -4 -18 126.339 43.7353 1 2 4 -19 195.297 49.2584 1 -2 -4 -19 218.50 38.0596 1 -2 4 -19 297.228 56.2516 1 -2 -4 19 210.395 45.9266 1 2 -4 -19 230.268 53.178 1 2 -4 -19 234.768 52.7831 1 2 4 -20 47.6948 43.4479 1 -2 -4 -20 96.6206 30.4807 1 2 -4 -20 40.9895 37.2468 1 -2 -4 20 34.7686 34.5944 1 -2 4 -20 22.7465 40.1439 1 2 -4 -20 40.6283 40.0063 1 -2 -4 21 314.886 51.0904 1 -2 4 -21 188.803 54.6388 1 2 -4 -21 179.281 53.6817 1 2 -4 -21 270.709 62.3007 1 2 4 -21 241.23 60.2388 1 2 4 -22 29.5819 48.5823 1 -2 4 -22 100.14 53.232 1 2 -4 -22 86.7094 46.4846 1 2 -4 -22 72.3676 47.5348 1 2 4 -23 147.728 52.9219 1 2 -4 -23 74.4563 48.2391 1 2 -4 -23 42.2097 43.8062 1 -2 4 -23 27.8171 51.9279 1 2 4 -24 11.4748 42.8458 1 2 -4 -24 15.6872 44.3656 1 2 -4 -24-25.1867 41.9807 1 -2 4 -24-48.8054 46.3945 1 2 4 -25-15.3544 46.6361 1 2 -4 -25-22.0292 43.0929 1 2 -4 -25-21.2587 43.9618 1 -2 4 -25 96.1262 63.9914 1 2 4 -26 63.9545 56.1933 1 2 -4 -26 167.489 61.8498 1 2 -4 -26 109.259 58.5637 1 -2 4 -26 70.97 65.9157 1 -2 4 -27 285.793 78.2444 1 2 -4 -27 261.395 77.6582 1 2 -5 0 195.781 34.4033 1 -2 5 0 140.704 26.5145 1 2 -5 -1 259.192 38.9961 1 -2 5 1 157.996 28.0896 1 2 -5 1 270.724 37.4343 1 -2 5 -1 210.133 29.9655 1 2 -5 2 1498.65 75.0507 1 -2 5 2 1453.32 72.0282 1 2 5 -2 1598.09 82.6978 1 2 -5 -2 1654.32 83.3017 1 -2 5 -2 1483.03 72.4281 1 2 -5 3 140.325 28.2461 1 -2 5 3 150.157 27.6298 1 2 5 -3 98.0438 29.7392 1 2 -5 3 185.595 32.4218 1 2 -5 -3 209.192 35.9166 1 -2 5 -3 165.339 29.2729 1 2 -5 4 505.707 50.3007 1 2 -5 4 654.249 55.5702 1 -2 5 4 431.453 42.5601 1 2 5 -4 514.915 50.2241 1 -2 5 4 512.702 44.7075 1 -2 5 -4 460.473 43.713 1 2 -5 -4 468.199 51.905 1 2 -5 5 1765.29 86.5071 1 2 5 -5 1730.62 88.9561 1 -2 5 5 1646.54 79.7229 1 -2 5 5 1843.49 82.5193 1 2 -5 5 1793.77 80.0708 1 2 -5 -5 1704.78 91.2368 1 -2 5 -5 1752.22 81.7245 1 2 5 5 1700.81 71.3396 1 2 5 5 1646.36 111.272 1 -2 -5 5 1773.20 92.5057 1 2 -5 6 144.83 32.8803 1 2 -5 6 108.77 26.0351 1 -2 -5 -6 115.268 21.8008 1 -2 5 6 106.846 27.0734 1 2 5 -6 102.299 30.6996 1 2 5 6 108.407 22.9608 1 2 5 6 99.2566 31.6799 1 -2 -5 6 114.235 32.7639 1 2 -5 -6 182.957 41.0142 1 -2 5 -6 111.443 27.3181 1 -2 -5 -7 242.169 26.7656 1 2 5 -7 204.298 38.0761 1 2 -5 7 178.39 29.5956 1 2 -5 7 224.186 37.6649 1 2 5 7 230.737 30.1443 1 -2 -5 7 251.20 41.6031 1 2 5 7 208.142 37.9373 1 2 -5 -7 326.478 48.1153 1 -2 5 -7 201.167 34.1761 1 2 5 -8 36.5247 24.5231 1 -2 -5 -8 92.3042 19.563 1 2 -5 -8 100.935 35.5945 1 2 5 8 77.304 31.2761 1 -2 -5 8 88.7637 30.3255 1 2 5 8 78.4285 22.4756 1 -2 5 -8 98.3344 26.955 1 2 -5 8 105.185 25.4186 1 2 -5 8 72.972 29.918 1 2 5 -9-6.76191 63.2398 1 2 -5 9 3.83289 24.616 1 -2 -5 -9 53.1299 16.8577 1 2 -5 9 15.4492 19.038 1 2 5 9 58.1458 30.8766 1 2 5 9 25.8113 19.9875 1 -2 -5 9-22.3183 22.5922 1 2 -5 -9 72.1009 32.3638 1 2 5 9 34.2001 30.2496 1 -2 5 -9 36.6435 24.0835 1 2 5 -9 17.2922 26.4873 1 2 -5 10 98.6063 35.7792 1 -2 -5 -10 65.8375 18.096 1 2 5 -10 94.789 33.8184 1 2 -5 10 91.9566 25.508 1 -2 5 -10 47.3824 26.9904 1 2 5 10 56.3457 31.8734 1 -2 -5 10 49.0346 31.446 1 2 5 10 116.467 28.5149 1 2 -5 -10 54.4277 31.6717 1 2 5 -11 383.344 52.6625 1 2 -5 11 504.64 46.3657 1 -2 -5 -11 399.294 31.9273 1 -2 5 -11 540.53 56.1062 1 2 5 11 373.754 50.7341 1 -2 -5 11 470.689 59.2063 1 2 -5 -11 471.264 64.3975 1 -2 5 -12 109.349 33.4182 1 2 5 -12 139.403 39.7869 1 2 -5 12 101.194 26.8607 1 -2 -5 -12 145.219 21.4776 1 -2 -5 12 116.007 36.8211 1 2 -5 -12 116.56 38.9527 1 2 5 12 114.728 40.8506 1 -2 -5 13 1279.77 86.0889 1 2 5 -13 1310.14 91.7607 1 2 -5 13 1284.49 70.1571 1 -2 -5 -13 1268.02 54.3409 1 2 5 13 1273.13 102.006 1 2 -5 -13 1375.98 95.5852 1 -2 5 -13 1224.97 85.7216 1 -2 -5 14 976.374 77.348 1 -2 -5 -14 1028.99 48.0322 1 2 5 -14 1033.07 85.8379 1 2 -5 -14 995.925 89.8094 1 -2 5 -14 1016.17 81.6808 1 -2 -5 -15 218.375 24.5133 1 2 5 -15 268.215 52.8111 1 -2 5 -15 312.144 53.6261 1 -2 -5 15 241.388 49.4331 1 2 -5 -15 250.272 51.5836 1 -2 -5 16 175.217 45.2397 1 2 5 -16 133.888 41.9949 1 -2 -5 -16 126.832 21.5855 1 -2 -5 -16 136.221 34.8218 1 2 -5 -16 139.624 43.78 1 -2 5 -16 153.548 45.7535 1 -2 -5 -17 50.5009 21.1636 1 2 5 -17 86.403 42.8836 1 -2 -5 -17 51.0609 29.192 1 -2 -5 17 31.8298 34.3422 1 -2 5 -17 64.4166 37.6626 1 2 -5 -17 71.258 40.2448 1 2 5 -18 9.99654 34.4147 1 -2 -5 -18 59.7826 29.1454 1 -2 -5 18 60.2463 36.63 1 -2 5 -18 39.7489 38.1086 1 2 -5 -18-21.8458 33.7144 1 -2 -5 -19 25.7032 26.6233 1 -2 5 -19 86.3596 41.9995 1 -2 -5 19 16.6891 36.251 1 2 -5 -19 0.91014 38.4095 1 2 5 -19 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605.733 77.0172 1 4 -5 5 69.0509 33.3252 1 4 5 -5 67.7366 34.1172 1 -4 -5 -5 128.053 50.9661 1 4 -5 -5 85.6333 40.2213 1 -4 -5 5 36.7096 46.7332 1 4 -5 6 58.1056 29.0044 1 -4 -5 -6 44.6227 45.5891 1 4 5 -6 34.218 31.9078 1 4 -5 -6-6.39188 31.2183 1 -4 -5 6-4.45387 39.4985 1 4 5 -7 137.394 40.5833 1 4 -5 7 76.7847 33.3146 1 -4 -5 -7 131.821 49.8341 1 4 -5 -7 76.6095 39.9545 1 -4 -5 7 74.1942 47.391 1 4 -5 8 133.731 35.3142 1 -4 -5 -8 144.864 54.2634 1 4 5 -8 199.536 44.0866 1 4 -5 -8 309.578 67.7547 1 -4 -5 8 195.152 57.7588 1 -4 -5 -9 429.144 78.5021 1 4 -5 9 465.988 52.159 1 4 5 -9 347.737 53.6425 1 -4 -5 9 302.611 69.5468 1 4 -5 -9 436.617 71.1909 1 4 -5 10 99.5952 30.3506 1 -4 -5 -10 111.902 48.8531 1 4 5 -10 101.536 40.2092 1 4 -5 -10 69.6227 40.6034 1 -4 -5 10 108.359 50.3141 1 -4 -5 -11 353.217 71.5777 1 4 5 -11 324.838 55.7897 1 4 -5 11 329.491 42.7116 1 -4 -5 11 275.833 65.5049 1 4 -5 -11 229.791 62.4013 1 4 -5 12 37.1319 27.309 1 4 5 -12 34.9099 37.7009 1 -4 -5 -12 14.8326 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-9-18.2036 38.325 1 -5 -5 9-3.06161 56.9961 1 5 -5 -9-25.2446 40.2194 1 5 5 -10 46.4671 44.1732 1 -5 -5 -10 5.7442 42.7311 1 5 -5 -10 28.2859 52.798 1 -5 -5 10 6.82125 56.1798 1 -5 -5 -11 23.422 46.3154 1 5 5 -11-23.8001 42.646 1 5 -5 -11-8.79932 41.5412 1 -5 -5 11 3.99917 52.3674 1 -5 -5 -12-19.6321 41.7176 1 5 5 -12-29.2007 41.8245 1 -5 -5 12 6.8211 55.9687 1 5 -5 -12 13.1496 43.0592 1 5 5 -13-32.7725 45.9541 1 -5 -5 -13-11.4929 41.7447 1 -5 -5 13-33.6385 56.7954 1 5 -5 -13 0.65963 42.9418 1 -5 -5 -14 94.0678 54.6742 1 5 5 -14 41.5401 51.9168 1 5 -5 -14 90.0443 56.9438 1 -5 -5 14 136.805 75.9227 1 5 5 -15 6.00029 52.423 1 -5 -5 -15-13.3987 41.2794 1 -5 -5 15-21.4352 59.9555 1 5 -5 -15 53.0974 53.1483 1 5 -6 0 175.026 54.3128 1 -5 -6 0 167.815 69.1933 1 5 6 0 134.081 49.3139 1 -5 -6 -1 79.5209 54.7226 1 5 6 -1 34.7147 42.0465 1 5 -6 1 8.78412 36.4457 1 5 -6 -1 13.285 42.5913 1 -5 -6 1 29.3013 56.4304 1 5 6 1 -19.18 41.0241 1 5 6 -2 92.6873 47.0842 1 5 -6 2 71.4151 43.6631 1 -5 -6 -2 97.8793 62.8165 1 -5 -6 2 73.8753 61.2885 1 5 -6 -2 137.154 55.0813 1 5 6 2 56.8045 43.6311 1 5 -6 3 31.1439 38.0781 1 -5 -6 -3 92.0631 59.0614 1 5 6 -3 85.3276 45.5133 1 -5 -6 3 0.57268 49.4674 1 5 -6 -3 51.4787 45.3924 1 5 -6 4-16.0166 35.674 1 -5 -6 -4-11.5079 42.3218 1 5 6 -4 7.44045 40.9688 1 -5 -6 4 63.8418 58.691 1 5 -6 -4-16.8434 37.7334 1 5 6 -5-10.7223 42.196 1 -5 -6 -5 18.0825 52.4198 1 5 -6 5-21.6421 33.8116 1 -5 -6 5 20.7973 55.6624 1 5 -6 -5-53.4886 37.4812 1 5 6 -6 102.783 47.6978 1 5 -6 6 52.4991 38.6756 1 -5 -6 -6 25.4336 51.9832 1 -5 -6 6 29.4149 57.6993 1 5 -6 -6 158.169 58.7956 1 -5 -6 -7 131.725 63.0451 1 5 -6 7 208.388 51.8097 1 5 6 -7 189.312 51.8703 1 -5 -6 7 157.121 67.5759 1 5 -6 -7 251.153 61.75 1 5 6 -8 79.7999 49.9703 1 -5 -6 -8 4.81883 47.3314 1 5 -6 8 29.1084 36.6861 1 5 -6 -8 36.0209 48.7817 1 -5 -6 8-41.4614 43.9381 1 -5 -6 -9 180.02 69.6195 1 5 6 -9 194.458 53.6345 1 5 -6 -9 162.164 58.7131 1 -5 -6 9 92.7202 67.0372 1 5 6 -10-3.74925 45.5693 1 -5 -6 -10 0.49739 47.9076 1 5 -6 -10 44.7741 50.4813 1 -5 -6 10 54.8796 59.6971 1 -5 -6 -11-24.5873 45.7707 1 5 6 -11-2.96714 49.2585 1 5 -6 -11-11.2589 39.5825 1 -5 -6 11 84.6572 64.0009 1 5 6 -12-49.9168 49.8275 1 -5 -6 -12-30.0534 40.8771 1 5 -6 -12 72.679 57.0932 1 -5 -6 12-49.3782 46.9949 1 -5 -6 -13 96.1751 54.8088 1 5 6 -13 22.0829 56.2446 1 5 -6 -13 105.923 55.9009 1 -5 -6 13 140.653 74.4216 1 5 7 0 17.3122 47.6649 1 5 -7 0 9.06493 38.2815 1 -5 -7 0 23.6682 63.7241 1 5 7 -1 20.6339 45.946 1 -5 -7 -1 48.0908 62.8472 1 5 -7 1 10.5362 41.1749 1 -5 -7 1 -1.1006 55.3822 1 5 -7 -1 86.1922 49.3432 1 5 7 1 43.0064 48.5688 1 5 7 -2 37.461 48.5044 1 -5 -7 -2 117.565 68.2138 1 5 -7 2 65.4108 41.8511 1 -5 -7 2 60.6046 58.0177 1 5 -7 -2 3.08606 38.4217 1 5 7 2 5.05418 47.195 1 -5 -7 -3 99.8649 62.558 1 5 7 -3 14.8395 45.5689 1 5 -7 3 28.3418 40.8993 1 5 -7 -3 -10.511 41.439 1 -5 -7 3 109.762 63.7006 1 5 -7 4 15.5067 37.6293 1 -5 -7 -4-0.26742 57.5092 1 5 7 -4 8.67628 50.1964 1 5 -7 -4 15.3264 43.609 1 -5 -7 4-17.0378 51.9892 1 5 -7 5 208.069 54.4971 1 5 7 -5 119.153 54.5568 1 -5 -7 -5 213.116 76.8438 1 5 -7 -5 103.698 56.6064 1 -5 -7 5 168.575 67.7932 1 5 -7 6 41.118 41.6388 1 5 7 -6 -38.277 44.4353 1 -5 -7 -6 31.1908 59.6604 1 -5 -7 6-0.69967 55.6058 1 5 -7 -6 34.0881 48.9756 1 5 -7 7 235.417 56.1976 1 -5 -7 -7 253.699 78.9218 1 5 7 -7 313.317 68.167 1 5 -7 -7 460.387 79.5883 1 -5 -7 7 290.193 83.8285 1 5 -7 8 93.6847 46.1001 1 5 7 -8 58.6067 54.5201 1 -5 -7 -8 34.1249 55.4036 1 5 -7 -8 136.924 60.1066 1 -5 -7 8 124.60 72.2629 1 -5 -7 -9 151.378 70.6478 1 5 7 -9 170.023 60.0171 1 -5 -7 9 355.632 89.9989 1 5 -7 -9 208.929 73.7345 1 5 7 -10 71.5789 55.497 1 -5 -7 -10 38.5345 52.1383 1 -5 -7 10 15.4254 60.7327 1 5 -7 -10 -17.12 46.7243 1 -5 -7 -11 106.50 61.2942 1 5 7 -11 126.956 64.2993 1 5 -7 -11 265.815 68.9414 1 -5 -7 11 267.684 83.1213 1 5 8 0-21.4066 52.0542 1 5 -8 0 64.8395 49.7409 1 -5 -8 0-62.6621 51.2556 1 5 -8 1 416.173 73.5881 1 -5 -8 -1 584.159 114.825 1 5 8 -1 450.373 81.0612 1 5 -8 -1 576.971 85.894 1 -5 -8 1 397.361 102.426 1 5 8 1 488.222 84.5239 1 5 -8 2 47.5898 44.4671 1 -5 -8 -2-45.8788 56.765 1 5 8 -2-15.3224 54.8466 1 -5 -8 2-20.3496 59.3642 1 5 -8 -2 16.3276 47.2598 1 5 8 2-24.8774 54.8781 1 -5 -8 -3 320.46 89.9608 1 5 -8 3 481.267 80.8355 1 5 8 -3 410.505 78.4557 1 5 -8 -3 383.383 75.2341 1 -5 -8 3 157.268 70.9107 1 5 8 3 389.923 76.233 1 5 8 -4 187.174 69.5358 1 -5 -8 -4 268.158 83.7233 1 5 -8 4 127.094 54.6404 1 5 -8 -4 102.971 54.969 1 -5 -8 4 134.707 67.622 1 5 8 -5 149.264 66.3032 1 5 -8 5 83.2167 47.6299 1 -5 -8 -5-29.0476 54.0021 1 -5 -8 5 61.7213 70.0139 1 5 -8 -5 104.781 54.1016 1 5 -8 6 57.9001 47.199 1 -5 -8 -6 -48.091 53.4835 1 5 8 -6 68.8903 61.6695 1 -5 -8 6 38.7148 67.1957 1 5 -8 -6 12.1624 49.2598 1 -5 -8 -7 -37.987 49.1488 1 5 8 -7-12.6841 55.569 1 5 -8 7 8.66954 42.2663 1 5 -8 -7 39.7953 52.91 1 -5 -8 7 6.79998 60.3048 1 6 0 -1 28.2476 46.7865 1 6 0 -2 48.6514 47.6678 1 6 0 -3 19.9184 48.018 1 6 0 -4 380.01 80.234 1 6 0 -5 25.0816 48.3377 1 6 -1 0 202.804 73.416 1 6 -1 -1 232.72 62.5073 1 6 -1 -2 103.193 52.7259 1 6 -1 -3 7.18627 47.2452 1 6 -1 -4 109.482 56.9959 1 6 -1 -5 21.3583 49.8279 1 6 -1 -6 26.6376 50.8854 1 6 -1 -7 63.2656 58.7003 1 6 -1 -8 48.357 58.9783 1 6 -1 -9 25.8102 57.5593 1 6 -1 -10 65.7826 59.2259 1 -6 -2 0 39.1691 62.0088 1 6 -2 0 52.1109 47.018 1 -6 -2 -1 43.8155 60.5917 1 -6 -2 1 17.1277 52.3465 1 6 -2 -1 -19.086 49.4182 1 -6 -2 -2 14.3965 52.5947 1 6 -2 -2-17.7121 43.7205 1 -6 -2 2-24.5254 61.8114 1 -6 -2 -3 73.4271 62.5884 1 -6 -2 3 53.1058 62.4066 1 6 -2 -3 85.0536 57.5245 1 -6 -2 -4 412.568 94.852 1 -6 -2 4 490.75 109.432 1 6 -2 -4 379.641 77.2296 1 -6 -2 -5 185.504 73.1391 1 -6 -2 5 38.3501 62.6683 1 6 -2 -5 52.4983 49.7843 1 -6 -2 -6 76.0134 55.4218 1 6 -2 -6 89.9566 60.7899 1 -6 -2 6 82.2688 68.9333 1 -6 -2 -7 54.1168 53.2359 1 -6 -2 7 260.842 89.4305 1 6 -2 -7 141.571 65.1854 1 -6 -2 -8 81.0817 56.0267 1 -6 -2 8 158.402 87.8281 1 6 -2 -8-2.50589 55.303 1 -6 -2 -9 71.2854 51.3756 1 -6 -2 9 0.70058 63.1586 1 6 -2 -9 180.141 70.6229 1 6 -3 0 5.02212 47.1253 1 -6 -3 0 -60.443 53.795 1 -6 -3 -1 -38.481 48.8413 1 6 -3 1 9.73383 62.6019 1 6 -3 -1-22.9361 43.7031 1 -6 -3 1-41.8326 56.2463 1 -6 -3 -2 362.523 97.3983 1 -6 -3 2 280.699 84.6798 1 6 -3 -2 301.357 73.7473 1 -6 -3 -3-77.7721 47.5337 1 6 -3 -3 62.5206 54.2481 1 -6 -3 3-27.4121 54.9129 1 -6 -3 -4 169.828 73.4608 1 6 -3 -4 104.551 61.3852 1 -6 -3 4 125.211 72.6365 1 -6 -3 -5 3.23358 56.0825 1 6 -3 -5-46.1328 46.8047 1 -6 -3 5 0.78844 57.7095 1 -6 -3 -6-5.01465 51.1019 1 -6 -3 6-32.9031 52.5524 1 6 -3 -6 122.951 61.4491 1 -6 -3 -7 4.78106 50.0714 1 6 -3 -7-5.33449 49.3213 1 -6 -3 7 53.2618 66.8647 1 -6 -3 -8-37.0391 46.4299 1 -6 -3 8 20.8573 60.9664 1 6 -3 -8-31.2844 50.9405 1 6 -4 0 15.6281 47.7818 1 -6 -4 0 26.6402 61.3959 1 6 -4 1 91.2609 52.6825 1 -6 -4 -1 125.568 73.7171 1 -6 -4 1 66.8025 62.9208 1 6 -4 -1 47.2432 50.0092 1 -6 -4 -2-5.60476 55.7537 1 -6 -4 2 56.0977 63.0574 1 6 -4 -2 27.8822 51.4338 1 -6 -4 -3 41.3605 69.0622 1 -6 -4 3 41.7703 66.4256 1 6 -4 -3 34.8286 49.3459 1 -6 -4 -4 64.9141 60.8285 1 -6 -4 4 128.689 74.7192 1 6 -4 -4 13.4457 50.6254 1 -6 -4 -5-11.2594 52.6874 1 -6 -4 5-16.9909 55.3971 1 6 -4 -5 34.4028 51.859 1 0 0 0 0.00 0.00 1 ; _shelx_hkl_checksum 85044 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.2091(2) 0.06608(9) 0.21989(4) 0.0220(3) Uani 1 1 d . . . . . C1 C 0.4251(8) 0.1893(3) 0.24240(15) 0.0133(10) Uani 1 1 d . . . . . H1 H 0.6088 0.1554 0.2487 0.016 Uiso 1 1 calc R U . . . C2 C 0.3204(9) 0.2409(3) 0.29851(16) 0.0143(9) Uani 1 1 d . . . . . O3 O 0.0823(6) 0.2453(3) 0.31062(11) 0.0200(7) Uani 1 1 d . . . . . N4 N 0.5183(8) 0.2834(3) 0.33199(14) 0.0147(8) Uani 1 1 d . . . . . H4 H 0.681(8) 0.265(3) 0.3215(13) 0.009(11) Uiso 1 1 d . . . . . C5 C 0.4799(8) 0.3425(4) 0.38518(16) 0.0134(9) Uani 1 1 d . . . . . C6 C 0.2858(8) 0.4328(3) 0.39175(14) 0.0150(8) Uani 1 1 d . . . . . H6 H 0.1743 0.4549 0.3608 0.018 Uiso 1 1 calc R U . . . C7 C 0.2552(9) 0.4907(3) 0.44395(15) 0.0147(9) Uani 1 1 d . . . . . C8 C 0.4207(8) 0.4565(3) 0.48907(16) 0.0174(10) Uani 1 1 d . . . . . H8 H 0.4008 0.4951 0.5249 0.021 Uiso 1 1 calc R U . . . C9 C 0.6123(9) 0.3671(4) 0.48169(17) 0.0188(11) Uani 1 1 d . . . . . H9 H 0.7239 0.3445 0.5125 0.023 Uiso 1 1 calc R U . . . C10 C 0.6443(8) 0.3095(4) 0.42973(15) 0.0167(10) Uani 1 1 d . . . . . H10 H 0.7776 0.2482 0.4248 0.02 Uiso 1 1 calc R U . . . C11 C 0.0580(10) 0.5868(4) 0.45047(16) 0.0182(10) Uani 1 1 d . . . . . C12 C -0.1019(11) 0.6638(4) 0.45476(17) 0.0280(12) Uani 1 1 d . . . . . H12 H -0.2327 0.7267 0.4583 0.034 Uiso 1 1 calc R U . . . C13 C 0.4412(8) 0.2884(4) 0.19740(15) 0.0138(9) Uani 1 1 d . . . . . C14 C 0.2623(9) 0.3854(3) 0.19624(15) 0.0172(10) Uani 1 1 d . . . . . H14 H 0.124 0.3897 0.2238 0.021 Uiso 1 1 calc R U . . . C15 C 0.2823(10) 0.4762(3) 0.15550(16) 0.0221(10) Uani 1 1 d . . . . . H15 H 0.1595 0.5429 0.1551 0.026 Uiso 1 1 calc R U . . . C16 C 0.4845(9) 0.4688(4) 0.11507(18) 0.0207(10) Uani 1 1 d . . . . . H16 H 0.5029 0.5318 0.0875 0.025 Uiso 1 1 calc R U . . . C17 C 0.6574(9) 0.3707(3) 0.11493(16) 0.0209(11) Uani 1 1 d . . . . . H17 H 0.7909 0.3646 0.0864 0.025 Uiso 1 1 calc R U . . . C18 C 0.6384(8) 0.2808(4) 0.15603(16) 0.0193(10) Uani 1 1 d . . . . . H18 H 0.7601 0.2138 0.156 0.023 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0261(6) 0.0178(5) 0.0220(5) -0.0016(4) -0.0007(5) -0.0041(5) C1 0.010(2) 0.015(2) 0.015(2) -0.0009(17) -0.0008(18) -0.0020(19) C2 0.014(2) 0.014(2) 0.015(2) 0.0024(16) 0.000(2) 0.000(2) O3 0.0127(17) 0.0266(17) 0.0206(17) -0.0032(13) 0.0024(14) -0.0012(14) N4 0.013(2) 0.0169(18) 0.0144(18) -0.0039(15) 0.0010(17) -0.0004(18) C5 0.013(2) 0.0168(19) 0.010(2) -0.0011(18) 0.0003(19) -0.0045(19) C6 0.015(2) 0.0184(18) 0.0121(18) 0.0006(17) -0.0008(19) -0.004(2) C7 0.011(3) 0.0145(18) 0.018(2) 0.0006(15) 0.004(2) -0.0032(19) C8 0.019(2) 0.019(2) 0.014(2) -0.0028(18) 0.004(2) -0.006(2) C9 0.020(3) 0.025(2) 0.011(2) 0.0031(18) -0.003(2) -0.006(2) C10 0.015(3) 0.017(2) 0.019(2) 0.0025(17) 0.002(2) -0.0016(19) C11 0.020(3) 0.022(3) 0.013(2) -0.0041(18) 0.001(2) -0.008(2) C12 0.030(3) 0.022(2) 0.032(3) -0.005(2) 0.006(2) -0.001(2) C13 0.014(2) 0.018(2) 0.0095(19) -0.0021(17) -0.0015(19) -0.0017(19) C14 0.015(3) 0.0199(19) 0.0170(19) -0.0031(16) 0.005(2) -0.001(2) C15 0.024(3) 0.0137(19) 0.028(2) -0.0013(17) -0.008(2) -0.002(2) C16 0.022(3) 0.020(2) 0.021(2) 0.0070(19) -0.003(2) -0.0040(19) C17 0.021(3) 0.028(2) 0.015(2) 0.0005(19) 0.004(2) -0.005(2) C18 0.018(3) 0.022(2) 0.018(2) -0.0003(18) -0.001(2) 0.003(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C13 C1 C2 111.3(3) . . ? C13 C1 Cl1 110.8(3) . . ? C2 C1 Cl1 108.9(3) . . ? C13 C1 H1 108.6 . . ? C2 C1 H1 108.6 . . ? Cl1 C1 H1 108.6 . . ? O3 C2 N4 124.1(4) . . ? O3 C2 C1 123.3(4) . . ? N4 C2 C1 112.6(4) . . ? C2 N4 C5 125.1(4) . . ? C2 N4 H4 116(2) . . ? C5 N4 H4 119(2) . . ? C10 C5 C6 120.8(4) . . ? C10 C5 N4 118.4(4) . . ? C6 C5 N4 120.8(4) . . ? C5 C6 C7 119.7(4) . . ? C5 C6 H6 120.2 . . ? C7 C6 H6 120.2 . . ? C6 C7 C8 119.3(4) . . ? C6 C7 C11 119.8(4) . . ? C8 C7 C11 120.9(3) . . ? C9 C8 C7 120.1(4) . . ? C9 C8 H8 119.9 . . ? C7 C8 H8 119.9 . . ? C8 C9 C10 120.8(4) . . ? C8 C9 H9 119.6 . . ? C10 C9 H9 119.6 . . ? C5 C10 C9 119.2(4) . . ? C5 C10 H10 120.4 . . ? C9 C10 H10 120.4 . . ? C12 C11 C7 178.8(5) . . ? C11 C12 H12 180 . . ? C14 C13 C18 119.3(4) . . ? C14 C13 C1 121.5(3) . . ? C18 C13 C1 119.2(4) . . ? C15 C14 C13 120.9(4) . . ? C15 C14 H14 119.6 . . ? C13 C14 H14 119.6 . . ? C14 C15 C16 119.2(4) . . ? C14 C15 H15 120.4 . . ? C16 C15 H15 120.4 . . ? C17 C16 C15 120.2(4) . . ? C17 C16 H16 119.9 . . ? C15 C16 H16 119.9 . . ? C16 C17 C18 120.4(4) . . ? C16 C17 H17 119.8 . . ? C18 C17 H17 119.8 . . ? C17 C18 C13 120.0(4) . . ? C17 C18 H18 120 . . ? C13 C18 H18 120 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C1 1.802(4) . ? C1 C13 1.517(5) . ? C1 C2 1.532(5) . ? C1 H1 1 . ? C2 O3 1.224(5) . ? C2 N4 1.348(5) . ? N4 C5 1.425(5) . ? N4 H4 0.87(4) . ? C5 C10 1.382(5) . ? C5 C6 1.390(5) . ? C6 C7 1.394(4) . ? C6 H6 0.95 . ? C7 C8 1.399(5) . ? C7 C11 1.446(6) . ? C8 C9 1.376(5) . ? C8 H8 0.95 . ? C9 C10 1.388(5) . ? C9 H9 0.95 . ? C10 H10 0.95 . ? C11 C12 1.162(6) . ? C12 H12 0.95 . ? C13 C14 1.384(5) . ? C13 C18 1.390(5) . ? C14 C15 1.383(5) . ? C14 H14 0.95 . ? C15 C16 1.392(6) . ? C15 H15 0.95 . ? C16 C17 1.374(5) . ? C16 H16 0.95 . ? C17 C18 1.382(5) . ? C17 H17 0.95 . ? C18 H18 0.95 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N4 H4 O3 0.87(4) 2.03(4) 2.891(5) 168(3) 1_655 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C13 C1 C2 O3 89.1(5) . . . . ? Cl1 C1 C2 O3 -33.3(5) . . . . ? C13 C1 C2 N4 -89.2(4) . . . . ? Cl1 C1 C2 N4 148.4(3) . . . . ? O3 C2 N4 C5 -1.9(6) . . . . ? C1 C2 N4 C5 176.4(3) . . . . ? C2 N4 C5 C10 136.2(4) . . . . ? C2 N4 C5 C6 -45.1(6) . . . . ? C10 C5 C6 C7 -0.2(6) . . . . ? N4 C5 C6 C7 -178.9(4) . . . . ? C5 C6 C7 C8 -0.2(5) . . . . ? C5 C6 C7 C11 178.4(4) . . . . ? C6 C7 C8 C9 0.4(6) . . . . ? C11 C7 C8 C9 -178.3(4) . . . . ? C7 C8 C9 C10 -0.1(6) . . . . ? C6 C5 C10 C9 0.5(6) . . . . ? N4 C5 C10 C9 179.2(3) . . . . ? C8 C9 C10 C5 -0.4(6) . . . . ? C2 C1 C13 C14 -32.0(5) . . . . ? Cl1 C1 C13 C14 89.3(4) . . . . ? C2 C1 C13 C18 148.7(4) . . . . ? Cl1 C1 C13 C18 -89.9(4) . . . . ? C18 C13 C14 C15 -1.8(6) . . . . ? C1 C13 C14 C15 178.9(3) . . . . ? C13 C14 C15 C16 0.4(6) . . . . ? C14 C15 C16 C17 1.6(6) . . . . ? C15 C16 C17 C18 -2.3(6) . . . . ? C16 C17 C18 C13 0.9(6) . . . . ? C14 C13 C18 C17 1.2(6) . . . . ? C1 C13 C18 C17 -179.5(4) . . . . ?