#------------------------------------------------------------------------------ #$Date: 2020-10-04 06:44:43 +0300 (Sun, 04 Oct 2020) $ #$Revision: 257165 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/78/1557808.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557808 loop_ _publ_author_name 'Cobos, Katherine' 'Rodr\'iguez, Rafael' 'Domarco, Olaya' 'Fern\'andez, Berta' 'Qui\~no\'a, Emilio' 'Riguera, Ricardo' 'Freire, F\'elix' _publ_section_title ; Polymeric Helical Structures \`a la Carte by Rational Design of Monomers ; _journal_issue 8 _journal_name_full Macromolecules _journal_page_first 3182 _journal_page_last 3193 _journal_paper_doi 10.1021/acs.macromol.0c00085 _journal_volume 53 _journal_year 2020 _chemical_absolute_configuration syn _chemical_formula_moiety 'C16 H13 N O2' _chemical_formula_sum 'C16 H13 N O2' _chemical_formula_weight 251.27 _chemical_name_common R-m-MA _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_conform_dict_location ftp://ftp.iucr.org/pub/cif_core.dic _audit_conform_dict_name cif_core.dic _audit_conform_dict_version 2.4.3 _audit_creation_date 2016-04-29T13:21:38-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' _cell_angle_alpha 90 _cell_angle_beta 108.302(7) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.4442(12) _cell_length_b 7.7559(11) _cell_length_c 10.4879(13) _cell_measurement_reflns_used 4870 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 27.03 _cell_measurement_theta_min 2.54 _cell_measurement_wavelength 0.71073 _cell_volume 652.13(16) _computing_cell_refinement 'SAINT V8.37A integration software' _computing_data_collection 'Bruker APEX2 software' _computing_data_reduction 'SORTAV (Blessing, 1995)' _computing_molecular_graphics 'ORTEP-3 for Windows (Farrugia, 2012)' _computing_publication_material 'WinGX publication routines (Farrugia, 2012)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT-2014 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_detector 'APEX-II CCD' _diffrn_measured_fraction_theta_full 1 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker APEX-II' _diffrn_measurement_method '\f or \w oscillation scans' _diffrn_orient_matrix_UB_11 -0.124345 _diffrn_orient_matrix_UB_12 -0.00101 _diffrn_orient_matrix_UB_13 -0.038933 _diffrn_orient_matrix_UB_21 0.000964 _diffrn_orient_matrix_UB_22 0.126437 _diffrn_orient_matrix_UB_23 -0.018416 _diffrn_orient_matrix_UB_31 0.009805 _diffrn_orient_matrix_UB_32 -0.025232 _diffrn_orient_matrix_UB_33 -0.090724 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0482 _diffrn_reflns_av_unetI/netI 0.0551 _diffrn_reflns_Laue_measured_fraction_full 1 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 11985 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.957 _diffrn_reflns_reduction_process ; Scaled and merged with Sortav R.H. Blessing, (1987) Cryst. Rev. 1, 3-58 R.H. Blessing, (1989) J. Appl. Cryst. 22, 396-397 ; _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.567 _diffrn_reflns_theta_min 2.045 _diffrn_source 'sealed x-ray tube' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.085 _exptl_absorpt_correction_T_max 0.97 _exptl_absorpt_correction_T_min 0.86 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.28 _exptl_crystal_density_method 'not measured' _exptl_crystal_description Needle _exptl_crystal_F_000 264 _exptl_crystal_size_max 0.46 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.189 _refine_diff_density_min -0.253 _refine_diff_density_rms 0.049 _refine_ls_abs_structure_details ; Flack x determined using 848 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.5(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.066 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_constraints 0 _refine_ls_number_parameters 178 _refine_ls_number_reflns 2858 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.066 _refine_ls_R_factor_all 0.0613 _refine_ls_R_factor_gt 0.0421 _refine_ls_shift/su_max 0 _refine_ls_shift/su_mean 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0494P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0868 _refine_ls_wR_factor_ref 0.0955 _reflns_Friedel_coverage 0.804 _reflns_Friedel_fraction_full 0.995 _reflns_Friedel_fraction_max 0.921 _reflns_number_gt 2227 _reflns_number_total 2858 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ma0c00085_si_003.cif _cod_data_source_block shelx _cod_depositor_comments ;Adding full bibliography for 1557803--1557808.cif. Adding full bibliography for 1557803--1557808.cif. ; _cod_original_sg_symbol_H-M 'P 21' _cod_database_code 1557808 _shelx_estimated_absorpt_t_min 0.962 _shelx_estimated_absorpt_t_max 0.993 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL shelxt_a.res in P2(1) CELL 0.71073 8.4442 7.7559 10.4879 90.000 108.302 90.000 ZERR 2.00 0.0012 0.0011 0.0013 0.000 0.007 0.000 LATT -1 SYMM - X, 1/2 + Y, - Z SFAC C H N O UNIT 32 26 2 4 MERG 2 FMAP 2 PLAN 20 SIZE 0.080 0.120 0.460 ACTA BOND $H REM Instructions for potential hydrogen bonds EQIV $1 -x+1, y+1/2, -z HTAB O1 O3_$1 HTAB N4 O1 CONF LIST 4 WPDB -2 L.S. 20 TEMP -173.00 WGHT 0.049400 FVAR 1.12603 O1 4 0.444614 0.870758 0.115096 11.00000 0.02852 0.02208 = 0.02347 0.00326 0.01233 0.00762 AFIX 148 H1O 2 0.371548 0.931411 0.045138 11.00000 -1.50000 AFIX 0 C1 1 0.545665 0.760016 0.063459 11.00000 0.02338 0.01840 = 0.01643 -0.00045 0.00831 0.00057 AFIX 13 H1 2 0.472452 0.702743 -0.019591 11.00000 -1.20000 AFIX 0 C2 1 0.623038 0.622123 0.166265 11.00000 0.02281 0.01098 = 0.02232 -0.00025 0.00704 -0.00532 O3 4 0.704085 0.503461 0.136965 11.00000 0.02795 0.01370 = 0.02323 -0.00111 0.00973 0.00174 N4 3 0.598044 0.639470 0.286222 11.00000 0.02885 0.01322 = 0.01912 0.00173 0.00984 0.00320 H4 2 0.535015 0.729602 0.294226 11.00000 0.03915 C5 1 0.649750 0.530111 0.399651 11.00000 0.02030 0.01658 = 0.02069 0.00320 0.00634 -0.00156 C6 1 0.709849 0.363555 0.394340 11.00000 0.02463 0.01914 = 0.01680 -0.00249 0.00917 -0.00215 AFIX 43 H6 2 0.717605 0.318861 0.312174 11.00000 -1.20000 AFIX 0 C7 1 0.758406 0.263252 0.510409 11.00000 0.02109 0.01574 = 0.02667 0.00105 0.00830 -0.00177 C8 1 0.746650 0.326899 0.631229 11.00000 0.02973 0.01911 = 0.02180 0.00478 0.00733 -0.00121 AFIX 43 H8 2 0.780185 0.258191 0.710178 11.00000 -1.20000 AFIX 0 C9 1 0.685092 0.492534 0.634617 11.00000 0.03264 0.02254 = 0.02053 0.00089 0.01013 -0.00258 AFIX 43 H9 2 0.675891 0.536752 0.716469 11.00000 -1.20000 AFIX 0 C10 1 0.637225 0.593418 0.520579 11.00000 0.02815 0.01598 = 0.02476 -0.00160 0.01122 -0.00076 AFIX 43 H10 2 0.595574 0.706431 0.524421 11.00000 -1.20000 AFIX 0 C11 1 0.821237 0.090144 0.504258 11.00000 0.02728 0.02066 = 0.02041 0.00394 0.00920 -0.00422 C12 1 0.872179 -0.049594 0.499888 11.00000 0.03125 0.02798 = 0.02906 0.00230 0.01067 0.00371 AFIX 163 H12 2 0.913463 -0.162840 0.496346 11.00000 -1.20000 AFIX 0 C13 1 0.681244 0.858310 0.027899 11.00000 0.02387 0.01046 = 0.02228 0.00268 0.00754 0.00365 C14 1 0.791736 0.963244 0.123019 11.00000 0.03308 0.02061 = 0.02479 0.00444 0.00833 -0.00263 AFIX 43 H14 2 0.782715 0.972709 0.210784 11.00000 -1.20000 AFIX 0 C15 1 0.914476 1.053600 0.089818 11.00000 0.03185 0.02590 = 0.04151 0.00744 0.00262 -0.00805 AFIX 43 H15 2 0.989083 1.124928 0.155265 11.00000 -1.20000 AFIX 0 C16 1 0.930170 1.041713 -0.036770 11.00000 0.02770 0.02984 = 0.05607 0.02074 0.01855 0.00136 AFIX 43 H16 2 1.014954 1.104241 -0.058537 11.00000 -1.20000 AFIX 0 C17 1 0.821001 0.937602 -0.132012 11.00000 0.03927 0.02688 = 0.03864 0.01459 0.02446 0.01234 AFIX 43 H17 2 0.831514 0.927569 -0.219272 11.00000 -1.20000 AFIX 0 C18 1 0.696046 0.847793 -0.099885 11.00000 0.03320 0.01558 = 0.02448 0.00455 0.01363 0.00684 AFIX 43 H18 2 0.620096 0.778568 -0.166136 11.00000 -1.20000 REM ##### AFIX 0 HKLF 4 REM shelxt_a.res in P2(1) REM R1 = 0.0421 for 2227 Fo > 4sig(Fo) and 0.0613 for all 2858 data REM 178 parameters refined using 1 restraints END WGHT 0.0494 0.0000 REM Highest difference peak 0.189, deepest hole -0.253, 1-sigma level 0.049 Q1 1 0.6721 0.8616 -0.0387 11.00000 0.05 0.19 Q2 1 1.0281 0.0772 0.4765 11.00000 0.05 0.18 Q3 1 0.8574 0.8688 -0.2845 11.00000 0.05 0.18 Q4 1 0.9096 0.5306 0.5980 11.00000 0.05 0.17 Q5 1 0.4286 0.8752 0.2031 11.00000 0.05 0.16 Q6 1 0.6825 0.9290 0.0374 11.00000 0.05 0.16 Q7 1 0.7184 0.9450 -0.1204 11.00000 0.05 0.16 Q8 1 1.1407 1.0261 -0.0966 11.00000 0.05 0.16 Q9 1 0.6280 1.0566 0.2602 11.00000 0.05 0.16 Q10 1 0.8886 0.9521 0.1195 11.00000 0.05 0.15 Q11 1 1.0375 1.0222 0.2625 11.00000 0.05 0.15 Q12 1 0.6981 0.3901 0.8206 11.00000 0.05 0.15 Q13 1 0.9581 0.8363 0.1192 11.00000 0.05 0.15 Q14 1 0.6406 1.0297 -0.3205 11.00000 0.05 0.15 Q15 1 0.6909 0.2627 0.7665 11.00000 0.05 0.15 Q16 1 0.7209 0.4911 0.8034 11.00000 0.05 0.15 Q17 1 0.8782 0.3694 0.4631 11.00000 0.05 0.15 Q18 1 0.7250 -0.0725 0.4603 11.00000 0.05 0.15 Q19 1 0.7185 -0.0342 0.5443 11.00000 0.05 0.15 Q20 1 0.7728 0.6010 0.0862 11.00000 0.05 0.14 ; _shelx_res_checksum 20998 _shelx_hkl_file ; -10 0 1 41.2351 10.8149 1 -10 0 2 32.3265 9.24784 1 -10 0 2 29.7368 13.5325 1 -10 0 3-3.78084 10.3475 1 -10 0 3 5.45563 7.70327 1 -10 0 4 25.6245 12.5801 1 -10 0 4 18.9962 8.62917 1 -10 0 5 40.7868 13.3185 1 -10 0 5 30.3937 8.1416 1 -10 0 6 0.58118 10.2697 1 -10 0 6 2.02725 6.55908 1 -10 0 7 4.73616 10.4422 1 -10 0 8 4.96716 10.2628 1 -10 0 9-5.19324 9.72498 1 -10 1 1 11.7641 7.66294 1 10 -1 -1 18.9951 8.78772 1 -10 -1 1 0.98904 8.27816 1 -10 -1 2 4.5111 12.7339 1 -10 1 2 6.39268 7.01376 1 -10 -1 2 8.50372 7.48187 1 -10 1 2 15.6471 12.7359 1 -10 1 3 19.0994 8.71019 1 -10 -1 3 17.2733 11.8172 1 -10 1 3 2.57372 11.4575 1 -10 -1 3 11.2075 7.56514 1 -10 1 4 16.4047 11.3172 1 -10 -1 4 0.73663 6.39795 1 -10 1 4 1.73514 6.95518 1 -10 -1 4 9.009 11.2475 1 -10 1 5 14.066 8.50733 1 -10 -1 5 24.6928 11.9243 1 -10 1 5 12.9949 11.7566 1 -10 -1 5 21.0897 8.34651 1 -10 1 6 79.1997 11.1862 1 -10 -1 6 107.437 17.1371 1 -10 -1 6 67.818 10.7304 1 -10 1 6 107.316 17.2185 1 -10 -1 7 20.7791 11.374 1 -10 1 7 22.9376 12.0498 1 -10 1 8 14.6423 10.8959 1 -10 -1 8 25.3633 11.8094 1 -10 -1 9 26.0477 11.9218 1 10 -2 -1 5.2379 8.12454 1 -10 2 1 3.92401 8.21939 1 10 -2 -2-0.76548 7.15349 1 -10 -2 2 4.57552 8.79549 1 -10 2 2 6.95701 13.2713 1 -10 2 2-1.11474 7.10933 1 -10 2 3 19.0752 13.6101 1 -10 -2 3 33.1724 13.1443 1 -10 -2 3 19.0543 9.48361 1 -10 2 3 12.1013 7.08402 1 -10 -2 4-0.10488 6.99865 1 -10 2 4 14.8167 12.799 1 -10 2 4 4.47001 6.86522 1 -10 -2 4 15.2099 12.1161 1 -10 2 5 134.359 19.2821 1 -10 -2 5 105.388 17.1068 1 -10 2 5 93.2985 12.0305 1 -10 -2 5 83.884 12.628 1 -10 2 6 24.2708 12.624 1 -10 -2 6 3.87577 8.99131 1 -10 -2 6 26.5818 12.5957 1 -10 2 7 31.3205 13.1077 1 -10 -2 7 21.2792 12.0451 1 -10 2 8 18.249 12.1018 1 -10 -2 8 26.8415 12.2918 1 10 -3 -1 12.9818 8.67358 1 -10 3 1 9.84442 9.61448 1 -10 -3 2 47.0662 10.9116 1 -10 3 2 45.4074 10.2471 1 10 -3 -2 49.8622 10.3696 1 -10 3 2 42.6678 16.8474 1 -10 3 3 1.70648 7.65454 1 -10 -3 3-8.11733 7.39116 1 10 -3 -3 1.17902 7.51761 1 -10 3 3 1.6557 13.2236 1 -10 -3 4 26.5547 9.19745 1 -10 -3 4 58.2287 15.3961 1 -10 3 4 55.4285 16.5136 1 -10 3 4 37.5407 11.0209 1 -10 -3 5 11.4402 7.55237 1 -10 -3 5 27.8099 13.4537 1 -10 3 5 33.8304 14.4509 1 -10 -3 6 12.0371 12.1115 1 -10 3 6 4.3769 12.4489 1 -10 -3 7 34.2427 13.9249 1 -10 3 7 32.0319 13.642 1 -10 -4 4 4.45238 9.48767 1 -10 4 4 6.68554 14.3907 1 -10 -4 4 11.6847 19.5878 1 -9 0 1 13.3061 10.2056 1 -9 0 1 24.1167 7.22086 1 -9 0 2 6.82779 9.53068 1 -9 0 2 8.72958 5.59833 1 -9 0 3 -1.8422 5.88113 1 -9 0 3 4.22146 8.71396 1 -9 0 4 2.83777 5.69938 1 -9 0 4 8.28926 8.71746 1 -9 0 5-2.95954 5.00656 1 -9 0 5-0.18909 8.18989 1 -9 0 6 101.801 12.032 1 -9 0 6 87.6868 13.6337 1 -9 0 7 14.2599 6.07851 1 -9 0 7 40.827 10.1256 1 -9 0 8-5.47282 5.01373 1 -9 0 8-4.66407 7.25401 1 -9 0 9 83.9793 10.3152 1 -9 0 9 102.865 14.2793 1 -9 0 10 4.7893 8.27728 1 -9 -1 1 10.0341 10.2166 1 -9 1 1 7.63838 10.6584 1 -9 1 1 17.3903 8.12919 1 9 -1 -1 2.91788 6.46967 1 -9 -1 1 11.3881 7.54785 1 -9 1 2 21.5276 7.29741 1 -9 1 2 10.363 10.047 1 -9 -1 2 7.43261 9.7259 1 -9 -1 2 11.8667 6.1673 1 9 -1 -2 17.793 6.92985 1 -9 -1 3 58.5169 12.8266 1 -9 1 3 66.9284 13.0787 1 -9 1 3 65.8186 10.1726 1 -9 -1 3 66.4459 9.6479 1 -9 -1 4 7.8666 8.98045 1 -9 -1 4 6.48826 5.52542 1 -9 1 4 5.74124 8.76739 1 -9 1 4 6.38495 5.76626 1 -9 1 5 18.7233 9.83334 1 -9 -1 5 26.5246 7.88172 1 -9 1 5 22.4949 6.68713 1 -9 -1 5 17.9454 9.36393 1 -9 1 6 7.5018 8.66531 1 -9 -1 6 11.979 6.21798 1 -9 -1 6 16.2183 8.77214 1 9 1 -6 10.9028 11.5215 1 -9 1 6 6.47879 5.42917 1 -9 -1 7 16.8852 6.84766 1 -9 1 7 23.8287 6.33069 1 -9 -1 7 15.0554 8.86145 1 9 1 -7 10.9649 11.0659 1 -9 1 7 21.8953 9.73131 1 9 -1 -8 23.8102 15.0964 1 9 1 -8 31.7001 12.7532 1 -9 -1 8 27.0897 9.78776 1 -9 1 8 45.4234 10.6924 1 -9 1 8 31.448 6.49342 1 -9 -1 8 33.5846 7.79102 1 -9 1 9 6.89256 5.79176 1 -9 1 9 33.1085 10.3765 1 -9 -1 9 28.1375 9.20349 1 9 1 -9 19.7066 12.504 1 -9 -1 9 43.9046 11.2092 1 -9 1 10 4.9018 8.55103 1 9 1 -10 7.3024 11.013 1 -9 -1 10 3.7043 8.69155 1 -9 -2 1 36.6163 15.233 1 -9 2 1 40.3278 8.42834 1 -9 -2 1 28.8903 8.37224 1 -9 2 1 35.1361 12.8412 1 9 -2 -1 48.6536 9.41708 1 -9 2 2 49.5801 9.55218 1 9 -2 -2 37.257 8.34661 1 -9 -2 2 24.3792 7.94248 1 -9 -2 2 38.4017 11.6007 1 -9 2 2 40.0067 13.2787 1 -9 2 3 6.64486 9.98339 1 -9 -2 3 2.02681 6.03338 1 -9 -2 3 10.8314 9.84333 1 9 -2 -3 4.16768 5.91395 1 -9 2 3 5.49513 6.10948 1 -9 2 4 1.12504 5.23423 1 -9 -2 4 6.99108 9.02293 1 -9 -2 4 1.69749 5.87354 1 -9 2 4 10.6283 9.74749 1 -9 2 5 80.33 10.3862 1 -9 2 5 88.936 14.8512 1 -9 -2 5 75.4413 13.2212 1 -9 -2 5 59.3202 10.3658 1 -9 2 6 286.568 23.9086 1 -9 -2 6 242.864 19.4382 1 -9 -2 6 317.783 24.4274 1 -9 2 6 262.722 18.1123 1 -9 -2 7-0.48111 8.20025 1 -9 -2 7 3.38677 6.05303 1 -9 2 7 11.7132 9.43612 1 9 2 -7 18.9979 12.7024 1 -9 2 7 11.4885 6.06956 1 -9 -2 8 79.5617 13.1956 1 -9 2 8 55.4002 8.31657 1 9 2 -8 72.2712 16.768 1 9 -2 -8 32.9534 15.065 1 -9 -2 8 53.9176 10.0321 1 -9 2 8 74.7365 13.4155 1 9 2 -9-0.33022 11.8851 1 -9 -2 9 10.6603 9.26777 1 9 -2 -9 9.05996 10.7412 1 -9 2 9 9.54256 9.12853 1 -9 2 10 44.3748 11.7866 1 9 2 -10 41.6736 15.0839 1 9 -2 -10 27.956 12.045 1 9 -3 -1 66.5273 10.4572 1 -9 -3 1 37.3721 9.26059 1 -9 3 1 53.5645 14.589 1 -9 3 1 57.2898 9.03032 1 -9 3 2 51.54 14.1304 1 9 -3 -2 46.7952 8.85225 1 -9 3 2 34.5821 9.08517 1 -9 -3 2 49.648 10.8001 1 -9 -3 2 37.6278 11.9522 1 -9 3 3 31.3628 8.48978 1 -9 -3 3 27.0864 11.2688 1 -9 3 3 18.2213 11.8711 1 9 -3 -3 29.5611 7.69958 1 -9 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3.88315 1 5 -4 -3 4.71387 2.9354 1 -5 4 3-1.11604 3.51557 1 5 -4 -3 5.53096 3.81491 1 5 -4 -3 0.8826 2.59029 1 5 4 -3 7.12614 3.84105 1 -5 4 3 1.47981 3.12628 1 5 4 -3 4.34242 3.83797 1 5 4 -3 1.46289 7.21881 1 -5 4 3 6.52307 5.98565 1 -5 -4 3-9.56357 6.90883 1 -5 4 3-1.57861 3.33529 1 -5 -4 3 1.50564 4.18167 1 5 -4 -4 118.743 15.3266 1 -5 4 4 123.033 10.1499 1 -5 4 4 134.354 9.98788 1 5 4 -4 134.059 10.0449 1 -5 4 4 138.453 13.1283 1 5 4 -4 131.526 16.6129 1 5 4 -4 152.815 11.0398 1 -5 -4 4 114.076 10.6411 1 -5 -4 4 102.96 10.4632 1 -5 -4 4 123.486 16.3054 1 -5 -4 4 120.202 10.6267 1 5 -4 -4 116.954 7.43053 1 -5 4 4 131.418 9.94191 1 5 4 -5 178.181 18.6686 1 5 4 -5 176.313 12.6181 1 -5 4 5 151.33 11.2986 1 -5 4 5 162.112 14.5062 1 -5 -4 5 179.389 13.1591 1 -5 -4 5 153.712 12.8345 1 -5 4 5 183.104 11.5684 1 -5 4 5 181.799 11.3224 1 5 -4 -5 195.011 17.5334 1 -5 -4 5 184.612 13.1123 1 5 -4 -5 181.173 9.26703 1 -5 -4 6 165.023 13.689 1 5 -4 -6 227.669 18.2642 1 5 4 -6 211.051 10.6242 1 5 4 -6 191.334 13.7081 1 -5 4 6 193.051 12.2277 1 -5 -4 6 188.223 13.9092 1 -5 -4 6 202.856 14.1655 1 5 4 -6 222.853 21.3512 1 -5 4 6 190.018 14.9274 1 -5 4 6 195.798 12.3746 1 -5 4 6 210.05 12.5607 1 5 4 -7 108.068 16.256 1 -5 4 7 91.5644 8.00693 1 5 4 -7 83.1377 9.18812 1 -5 4 7 84.7425 7.90468 1 5 -4 -7 82.9343 12.1548 1 -5 -4 7 84.8087 9.93362 1 -5 4 7 92.2456 10.2241 1 -5 4 8 21.2829 4.51879 1 5 -4 -8 21.7181 7.97719 1 -5 -4 8 23.1174 6.0529 1 -5 4 8 22.4224 6.12658 1 5 4 -8 24.0251 11.9779 1 5 4 -8 20.0839 5.67799 1 -5 4 8 25.7775 5.14534 1 -5 4 9 34.6973 6.63342 1 5 -4 -9 9.11334 6.58032 1 -5 4 9 25.8944 4.69416 1 5 4 -9 35.6862 13.7164 1 5 4 -9 26.2169 7.39232 1 -5 -4 9 31.2626 6.84769 1 5 -4 -10 2.90775 5.75859 1 -5 4 10 9.78394 4.16692 1 5 4 -10 14.1082 12.6187 1 -5 -4 10 11.9865 6.2661 1 -5 4 10 7.54091 4.92368 1 -5 4 11 10.8207 5.14551 1 5 -4 -11 4.74779 5.19457 1 5 4 -11 26.0195 14.1067 1 -5 -4 11 13.9896 7.11202 1 -5 4 11 11.6324 4.44985 1 5 4 -12 74.7103 17.9053 1 5 -4 -12 65.2724 7.28159 1 -5 4 12 62.4818 7.39241 1 -5 4 12 61.2426 6.80583 1 5 -5 -1 103.949 10.2871 1 -5 -5 1 109.903 13.1315 1 5 -5 -1 91.7761 8.97358 1 5 -5 -1 97.4369 9.02929 1 -5 -5 1 80.6099 9.70794 1 -5 -5 1 72.2778 9.33259 1 -5 5 1 87.3101 14.8444 1 -5 5 1 89.9878 9.59306 1 -5 5 1 122.55 15.2467 1 5 5 -1 85.6921 15.7857 1 -5 5 1 63.8384 8.63764 1 -5 5 1 104.998 10.1776 1 5 5 -1 80.1531 9.75925 1 5 5 -1 103.636 10.5498 1 5 5 -2 192.453 13.8932 1 -5 5 2 172.394 13.7674 1 -5 5 2 173.046 13.5859 1 -5 -5 2 175.401 14.0841 1 5 -5 -2 176.812 11.6574 1 5 -5 -2 173.809 11.7212 1 5 -5 -2 180.562 13.1718 1 -5 -5 2 182.38 14.2693 1 5 -5 -2 172.987 19.215 1 5 5 -2 156.943 13.3023 1 -5 5 2 166.514 12.5177 1 -5 5 2 170.721 19.6916 1 -5 5 2 164.143 12.7205 1 5 5 -2 177.936 19.8482 1 -5 5 2 177.202 18.7643 1 -5 5 3 30.9914 9.73763 1 -5 -5 3 27.0204 6.63317 1 5 -5 -3 34.6785 4.93113 1 -5 5 3 43.124 7.41867 1 5 -5 -3 47.0135 12.3927 1 -5 -5 3 34.4901 6.74747 1 5 -5 -3 43.9611 5.55709 1 5 5 -3 37.9591 6.56722 1 -5 5 3 36.0158 6.14018 1 -5 5 3 35.5465 6.33182 1 -5 -5 3 33.1747 15.652 1 5 5 -3 23.4347 5.61698 1 5 5 -3 39.0342 11.8838 1 -5 5 4 86.3917 12.6348 1 5 5 -4 68.5908 8.96794 1 -5 5 4 84.4561 8.76092 1 -5 -5 4 81.516 10.5204 1 5 5 -4 92.5498 9.2829 1 5 5 -4 88.7352 15.2604 1 5 -5 -4 84.2839 6.65444 1 -5 -5 4 79.0271 21.4603 1 5 -5 -4 94.9879 15.4926 1 -5 5 4 82.2118 8.91681 1 -5 -5 4 70.8447 8.76388 1 -5 5 4 72.2541 8.75698 1 -5 5 5 30.8685 5.56955 1 5 5 -5 26.5075 11.3597 1 -5 5 5 20.281 7.91689 1 5 -5 -5 20.6118 9.69606 1 -5 -5 5 26.859 6.81316 1 -5 5 5 14.2562 5.22695 1 5 -5 -5 27.0723 3.67333 1 -5 5 6 187.182 17.0195 1 -5 5 6 177.677 12.7012 1 5 5 -6 217.393 23.4519 1 5 -5 -6 179.411 18.3041 1 -5 -5 6 175.488 14.8199 1 -5 -5 7 5.19664 5.87309 1 5 -5 -7 9.83411 8.72084 1 5 5 -7 11.9001 11.7937 1 -5 5 7 34.4813 8.98881 1 -5 5 7 15.5214 4.97993 1 5 -5 -8 52.1855 11.4885 1 -5 5 8 76.5637 11.3381 1 -5 -5 8 69.3444 10.0735 1 5 5 -8 69.0035 16.3674 1 -5 5 8 80.0715 8.42773 1 -5 5 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153.149 9.08405 1 -2 0 2 141.548 7.18618 1 -2 0 2 141.082 7.33824 1 -2 0 2 159.319 9.03309 1 2 0 -3 93.1034 5.92257 1 -2 0 3 81.4103 5.4382 1 2 0 -3 85.0888 6.17359 1 2 0 -3 99.4185 4.77628 1 -2 0 3 95.4925 4.93921 1 2 0 -4 348.726 14.7299 1 2 0 -4 393.267 16.3298 1 -2 0 4 342.157 15.0438 1 2 0 -4 287.375 16.0318 1 -2 0 5 0.86503 1.05601 1 2 0 -5 -1.4276 1.8145 1 2 0 -6 26.0228 3.71849 1 -2 0 6 34.8207 2.34904 1 2 0 -7 117.808 7.62321 1 2 0 -8 38.2381 5.42724 1 2 0 -8 44.3321 5.60589 1 -2 0 9 16.3692 3.50868 1 2 0 -9 23.2971 5.03526 1 2 0 -9 23.4892 5.14401 1 -2 0 10 5.2742 3.53885 1 2 0 -10 -1.0273 4.48772 1 -2 0 11 6.52481 3.96885 1 2 0 -11 3.96574 5.296 1 -2 0 11 9.45059 2.75623 1 2 0 -12 6.63146 6.214 1 -2 0 12 27.4284 4.49307 1 2 0 -13-1.69063 5.80687 1 2 0 -13-1.91001 5.83333 1 2 0 -13 1.87606 5.36173 1 2 -1 -1 49.4082 3.678 1 2 -1 -1 46.8793 6.68472 1 2 -1 -1 40.4824 4.10966 1 2 1 -1 38.7739 3.81864 1 -2 1 1 37.6995 3.44195 1 -2 -1 1 37.3518 3.74582 1 2 -1 -1 42.2389 3.40532 1 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42.3094 1 2 4 -3 980.662 42.5545 1 -2 4 4 124.806 8.41181 1 2 4 -4 133.387 14.0873 1 -2 -4 4 115.946 9.41038 1 -2 -4 4 129.543 9.39732 1 -2 -4 4 124.964 13.9803 1 2 -4 -4 109.722 11.7916 1 -2 -4 4 132.787 9.6615 1 2 -4 -4 125.471 8.15276 1 -2 4 4 119.959 8.12311 1 -2 4 4 118.276 8.47266 1 2 4 -4 123.586 8.26798 1 -2 4 4 116.418 11.0385 1 2 4 -4 138.756 9.84431 1 -2 4 4 127.686 8.53215 1 -2 -4 5 181.872 11.4404 1 -2 -4 5 178.384 11.8488 1 2 4 -5 175.785 11.5965 1 2 4 -5 176.372 16.6467 1 -2 4 5 166.216 9.71393 1 -2 4 5 175.37 10.0691 1 2 -4 -5 168.219 9.732 1 -2 -4 5 156.275 11.191 1 2 -4 -5 170.468 14.2287 1 2 -4 -5 170.64 8.49593 1 -2 4 5 168.925 11.8156 1 -2 4 5 180.032 10.2305 1 2 4 -5 148.248 9.17489 1 -2 -4 6 218.471 13.3651 1 -2 -4 6 221.463 13.6271 1 2 -4 -6 202.801 15.6446 1 2 -4 -6 195.16 10.769 1 2 -4 -6 195.932 9.5173 1 -2 4 6 210.807 13.2352 1 -2 4 6 224.397 11.5983 1 2 4 -6 204.764 10.1368 1 -2 -4 6 229.337 13.427 1 -2 4 6 189.054 11.1092 1 2 4 -6 226.115 19.5637 1 2 4 -6 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1 -2 5 6 505.112 25.5869 1 2 5 -6 551.016 35.2381 1 -2 -5 7 327.714 19.1062 1 2 -5 -7 300.863 15.1052 1 2 5 -7 296.709 19.1537 1 2 5 -7 348.393 19.5894 1 -2 5 7 307.308 17.2701 1 2 -5 -7 258.54 21.2803 1 2 5 -7 334.126 27.5297 1 -2 -5 8 59.0626 8.95721 1 2 -5 -8 68.6365 12.4122 1 2 -5 -8 62.2218 5.37217 1 -2 5 8 76.0156 7.82809 1 2 5 -8 93.1028 17.44 1 2 5 -8 85.0409 9.56595 1 2 5 -9 23.2913 13.0528 1 -2 5 9 12.4582 4.56997 1 -2 -5 9 17.1954 6.98471 1 2 5 -9 17.217 5.925 1 2 -5 -9 14.5724 9.17677 1 2 5 -10-5.02975 12.4741 1 -2 -5 10-3.09725 6.19051 1 2 -5 -10 9.37117 8.78117 1 2 -5 -11 24.9581 10.1989 1 2 5 -11 28.5992 16.1199 1 -2 5 11 26.895 6.1481 1 2 6 -1 81.8093 14.9165 1 2 6 -1 71.8685 8.8862 1 -2 6 1 80.8937 9.67287 1 -2 -6 1 74.2608 8.51141 1 2 -6 -1 85.8574 8.87862 1 -2 -6 1 85.3952 9.6434 1 2 -6 -1 75.7748 7.74994 1 -2 -6 1 54.782 12.4999 1 2 -6 -1 85.9892 15.4877 1 -2 6 1 88.4259 14.4517 1 -2 6 1 89.184 9.67985 1 -2 6 1 88.6412 9.74542 1 2 6 -1 87.2587 10.0063 1 -2 6 1 78.1506 8.915 1 -2 6 2 59.6261 10.6297 1 -2 -6 2 96.9727 10.1226 1 2 6 -2 77.6768 8.845 1 -2 6 2 99.4868 9.98895 1 -2 6 2 75.7538 9.29717 1 2 6 -2 79.0716 9.34291 1 -2 6 2 77.3211 8.90302 1 2 6 -2 85.4522 13.7413 1 2 -6 -2 86.9262 15.0806 1 -2 -6 2 53.4476 7.86966 1 -2 -6 2 76.7179 15.1186 1 2 -6 -2 108.437 10.2304 1 2 -6 -2 66.0991 7.00435 1 -2 6 2 77.7554 8.93904 1 -2 6 3 103.584 10.1593 1 2 6 -3 110.965 11.1553 1 -2 6 3 98.7451 10.3319 1 2 6 -3 120.442 16.3306 1 -2 -6 3 82.294 14.3691 1 2 6 -3 126.549 10.5073 1 -2 6 3 118.337 10.4163 1 2 -6 -3 110.601 9.65015 1 -2 -6 3 98.9564 10.175 1 -2 -6 3 117.607 11.5102 1 2 -6 -3 121.16 17.401 1 2 -6 -3 97.5787 7.29916 1 -2 6 3 119.45 10.9445 1 2 -6 -4 192.569 19.5306 1 -2 6 4 234.377 14.7559 1 -2 6 4 198.612 14.2473 1 2 6 -4 195.851 21.7736 1 -2 -6 4 193.63 21.9409 1 -2 -6 4 209.474 15.0768 1 -2 -6 4 191.378 14.4127 1 2 -6 -4 214.599 13.5215 1 -2 6 4 229.297 14.9503 1 2 6 -4 211.459 13.9422 1 2 6 -4 212.964 15.5933 1 2 -6 -5 21.6848 4.88921 1 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13.829 1 -2 -7 2 59.6225 8.98217 1 2 -7 -2 77.677 17.8654 1 2 -7 -2 58.7163 8.36297 1 -2 -7 2 57.9739 9.15744 1 2 7 -2 65.3811 9.25863 1 -2 7 2 60.2279 9.30846 1 -2 -7 3 309.002 20.8432 1 2 -7 -3 339.118 20.1564 1 2 -7 -3 324.921 28.0416 1 -2 -7 3 348.946 21.4806 1 -2 7 3 324.242 20.6419 1 2 7 -3 338.588 20.353 1 2 -7 -4 177.425 13.9444 1 2 -7 -4 212.077 22.4461 1 -2 7 4 252.004 16.7661 1 2 7 -4 194.368 15.1557 1 -2 -7 4 184.076 15.8551 1 2 -7 -5 4.06354 10.3115 1 -2 -7 5 7.66691 6.28608 1 2 -7 -5 3.05127 4.33757 1 -2 7 5 6.98861 5.71733 1 -2 -7 6 155.932 16.0283 1 -2 7 6 144.612 13.5974 1 2 -7 -6 139.624 11.7377 1 2 7 -6 149.913 14.7002 1 -2 -7 7 11.1578 7.54859 1 2 -7 -7 2.20789 11.2418 1 2 7 -7 8.35107 7.16332 1 -2 7 7 9.13374 6.24261 1 -2 -7 8 6.89051 8.43943 1 2 -7 -8 13.7225 13.1815 1 -2 7 8 27.1635 7.69131 1 2 7 -8 17.5451 8.7421 1 2 -7 -9 22.6101 14.3312 1 -2 8 1 142.153 14.4873 1 2 8 -1 154.955 15.1787 1 2 -8 -1 159.55 14.4365 1 -2 -8 1 140.125 14.8838 1 -2 -8 1 142.085 14.6972 1 2 -8 -2 4.73446 5.5809 1 -2 -8 2 10.9039 6.30984 1 2 8 -2 2.87539 6.0406 1 -2 8 2 3.26359 5.98329 1 -2 -8 3 60.2682 10.4719 1 2 -8 -3 61.3481 9.13636 1 -2 8 3 68.1394 11.0799 1 2 -8 -4 3.56615 5.41187 1 -2 -8 4 6.23602 6.41998 1 -2 8 4 2.61822 6.59625 1 -2 -8 5 6.06613 6.6211 1 2 -8 -5 1.31669 6.26781 1 -2 8 5-1.54483 6.57127 1 -2 -8 6 33.3984 9.2465 1 2 8 -6 39.6591 10.2629 1 -2 8 6 48.5659 10.122 1 -2 -8 7 36.8235 10.5484 1 2 8 -7 42.012 10.3754 1 2 9 -1 20.3886 9.361 1 2 -9 -1 7.97275 7.47321 1 -2 9 1 14.0483 8.00502 1 2 -9 -2 5.64559 7.26871 1 -2 9 2 3.25497 7.19731 1 -2 9 3 4.54941 7.64855 1 2 -9 -3 18.0915 8.26968 1 -2 -9 4 14.9529 9.89888 1 -2 9 4 9.22264 8.98149 1 -2 -9 5 1.77082 9.15309 1 -2 -9 6 16.8398 9.84532 1 1 0 -1 316.818 15.2015 1 -1 0 1 326.288 15.253 1 1 0 -1 304.934 14.2708 1 -1 0 1 362.50 14.6541 1 1 0 -1 378.299 15.379 1 1 0 -1 388.78 14.6984 1 1 0 -1 295.899 14.2292 1 -1 0 1 316.47 14.4127 1 -1 0 1 367.527 15.3552 1 -1 0 2 4.46084 0.80491 1 1 0 -2 3.13769 1.28754 1 1 0 -2 4.44869 0.75354 1 1 0 -2 6.05095 1.2305 1 -1 0 3 72.8533 3.2269 1 1 0 -3 54.1944 3.65848 1 -1 0 4 443.987 17.5197 1 1 0 -4 346.129 18.1834 1 1 0 -4 433.123 18.3127 1 1 0 -5 2.27955 2.34254 1 -1 0 5 3.63218 1.06977 1 1 0 -6 39.7628 5.00862 1 -1 0 7 69.6574 5.44265 1 1 0 -7 62.9837 6.94969 1 1 0 -8 379.605 21.9085 1 -1 0 8 460.277 20.3358 1 -1 0 9 122.903 8.64602 1 -1 0 9 137.164 6.89358 1 -1 0 9 117.335 6.36575 1 -1 0 10 75.5824 7.32766 1 1 0 -10 51.5405 8.62531 1 -1 0 10 75.7799 5.86543 1 -1 0 10 67.5656 5.17444 1 -1 0 11-0.41531 4.02559 1 1 0 -11-1.40457 6.22892 1 -1 0 11 1.91007 3.23997 1 -1 0 12 101.597 8.38859 1 1 0 -12 82.9554 11.5245 1 1 0 -12 62.1484 11.1911 1 1 0 -13 5.05556 8.36362 1 1 0 -13 9.10866 7.71212 1 1 -1 -1 2110.86 87.3261 1 -1 -1 1 2106.73 87.553 1 1 -1 -1 1941.63 88.4662 1 1 -1 -1 2073.34 86.8291 1 -1 -1 1 2079.31 87.3312 1 1 1 -1 2330.53 88.6737 1 -1 1 1 1999.39 88.6706 1 1 1 -1 2106.19 88.6562 1 -1 1 1 2251.05 88.3447 1 1 1 -1 2093.05 90.525 1 -1 1 1 2154.79 88.7396 1 -1 1 1 1956.11 88.3012 1 -1 1 1 2013.47 88.6598 1 -1 -1 1 2217.12 87.3257 1 1 -1 -1 2067.99 87.3012 1 -1 -1 1 2028.90 89.0394 1 1 -1 -1 2096.54 87.0315 1 -1 -1 2 1076.74 45.4902 1 1 -1 -2 959.053 45.806 1 -1 -1 2 1084.59 45.1191 1 1 1 -2 1133.39 46.5042 1 -1 1 2 1018.28 47.1707 1 1 1 -2 1163.83 47.2622 1 -1 1 2 1045.17 46.6735 1 1 1 -2 1093.91 48.7182 1 1 1 -2 1201.11 46.5291 1 1 -1 -2 1128.90 44.9628 1 -1 -1 2 1053.19 46.9227 1 -1 -1 2 1102.00 45.1308 1 -1 -1 3 692.784 27.8997 1 -1 -1 3 658.909 28.4832 1 -1 -1 3 671.606 27.7697 1 -1 -1 3 669.996 29.6528 1 1 -1 -3 577.547 28.0897 1 -1 1 3 615.638 28.4559 1 1 1 -3 700.058 29.309 1 1 1 -3 670.306 31.0655 1 -1 1 3 716.504 28.4965 1 1 1 -4 407.889 20.64 1 1 1 -4 431.61 18.7405 1 -1 -1 4 404.756 18.4698 1 1 -1 -4 463.288 18.6078 1 -1 -1 4 422.729 18.3771 1 -1 -1 4 428.973 19.328 1 1 -1 -4 421.779 18.5209 1 -1 -1 4 435.287 20.1909 1 1 1 -4 370.308 20.4389 1 -1 1 4 424.975 17.6972 1 1 1 -4 398.426 18.545 1 -1 1 4 464.102 18.2122 1 -1 1 5 681.691 27.3365 1 1 1 -5 561.418 29.5617 1 -1 -1 5 615.127 27.931 1 1 -1 -5 624.716 27.3838 1 -1 -1 5 661.01 27.128 1 -1 -1 5 636.58 26.9229 1 -1 1 5 629.993 26.4221 1 1 1 -5 608.66 27.2861 1 1 1 -5 646.318 27.4516 1 -1 -1 6 20.0045 2.07224 1 1 -1 -6 18.8586 2.44793 1 -1 -1 6 20.8088 2.27373 1 -1 1 6 18.4738 1.77796 1 -1 1 6 23.9851 2.86956 1 1 1 -6 20.4687 2.48835 1 1 1 -6 18.8002 2.64199 1 1 1 -6 17.2832 4.97546 1 -1 -1 6 19.4684 2.6812 1 -1 -1 7 307.388 14.5436 1 -1 -1 7 330.936 14.1676 1 -1 -1 7 304.659 13.6237 1 1 -1 -7 291.96 14.7537 1 1 1 -7 304.783 13.9389 1 -1 1 7 295.301 13.1046 1 1 1 -7 285.074 17.5231 1 1 -1 -7 275.367 14.9236 1 -1 1 7 301.602 14.344 1 1 1 -7 288.421 13.6667 1 -1 -1 8 160.327 8.6079 1 1 -1 -8 134.533 9.68571 1 1 1 -8 145.86 7.78417 1 -1 1 8 152.646 8.92126 1 1 1 -8 153.497 8.06258 1 1 -1 -8 147.805 9.41362 1 -1 -1 8 151.291 8.60724 1 1 1 -8 164.669 13.1321 1 -1 -1 8 161.182 8.01262 1 -1 -1 9 28.4618 4.06128 1 -1 -1 9 33.9477 5.39924 1 1 -1 -9 37.7504 5.81534 1 -1 -1 9 38.4847 3.98574 1 1 1 -9 40.2275 3.05192 1 1 1 -9 39.7471 8.40431 1 1 1 -9 32.2344 3.14996 1 -1 1 9 36.9025 4.71062 1 -1 1 10 1.42034 1.98992 1 1 -1 -10 0.89994 4.54448 1 -1 -1 10 8.05258 3.63163 1 1 -1 -10 0.63062 4.46716 1 -1 -1 10 4.00727 3.98458 1 1 1 -10 -3.2516 6.5109 1 -1 1 10 6.98674 3.56191 1 -1 1 10 1.32713 1.97042 1 1 1 -11 39.3128 9.95682 1 -1 -1 11 53.9294 7.34921 1 -1 1 11 60.546 5.44129 1 1 -1 -11 50.4529 8.01308 1 -1 -1 11 57.6717 6.51472 1 1 1 -12 2.89153 8.5583 1 1 1 -12 1.11801 8.57553 1 -1 -1 12 0.72124 4.60855 1 1 -1 -12 2.71567 6.75336 1 -1 -1 12 7.17794 5.32139 1 1 -1 -12 5.86743 5.95165 1 -1 1 12-0.37361 3.3274 1 1 -1 -13 30.7538 8.76037 1 1 1 -13 32.978 11.2242 1 1 -1 -13 43.1465 8.29768 1 -1 1 13 43.2412 5.96596 1 -1 -2 1 191.826 10.7098 1 -1 -2 1 216.604 10.8078 1 -1 -2 1 202.685 13.2193 1 1 -2 -1 211.708 9.9853 1 -1 -2 1 196.83 10.7094 1 1 2 -1 205.331 13.0338 1 -1 2 1 191.08 10.0576 1 1 2 -1 220.551 10.5209 1 1 2 -1 193.795 10.3744 1 -1 2 1 208.684 10.0491 1 -1 2 1 197.511 10.2777 1 1 -2 -1 198.681 10.1816 1 1 -2 -1 233.586 11.0352 1 -1 2 1 185.372 12.2832 1 1 -2 -1 209.911 10.5218 1 1 2 -1 209.58 10.5834 1 -1 -2 2 0.86498 1.77166 1 1 -2 -2 0.89286 0.55605 1 -1 -2 2 1.2969 1.67652 1 1 -2 -2 0.68866 3.14575 1 -1 -2 2 1.44682 1.89868 1 1 -2 -2 1.91836 0.6017 1 -1 -2 2 2.80011 3.69062 1 1 -2 -2-0.09839 1.40524 1 1 2 -2 5.80522 3.68336 1 -1 2 2 1.89566 1.47879 1 -1 2 2-0.32621 1.33368 1 1 2 -2 0.49452 1.70212 1 1 2 -2 4.01199 1.90395 1 -1 2 2 0.30742 1.47343 1 1 2 -2 2.19901 1.5865 1 -1 2 2-0.00981 2.31242 1 -1 2 3 170.629 10.5625 1 1 -2 -3 183.195 11.319 1 -1 2 3 203.542 8.96485 1 -1 2 3 212.087 8.9835 1 1 2 -3 195.644 13.4488 1 -1 2 3 198.788 8.94502 1 1 2 -3 206.02 10.637 1 1 2 -3 209.931 9.75822 1 -1 -2 3 195.947 10.1651 1 -1 -2 3 197.956 10.3312 1 -1 -2 3 187.171 12.5468 1 1 -2 -3 188.108 9.30245 1 -1 -2 3 195.327 9.89664 1 -1 2 3 186.317 9.66357 1 1 -2 -4 689.975 30.2338 1 -1 -2 4 700.495 33.8611 1 1 -2 -4 651.643 32.1467 1 -1 -2 4 704.403 31.571 1 -1 -2 4 722.771 31.3406 1 1 -2 -4 771.635 30.1968 1 -1 -2 4 685.401 30.932 1 1 2 -4 727.447 32.7859 1 1 2 -4 759.572 30.9405 1 -1 2 4 699.313 31.7103 1 1 2 -4 739.157 30.8767 1 1 2 -4 741.575 36.1728 1 1 -2 -5 178.901 10.9193 1 1 2 -5 198.507 14.2363 1 -1 -2 5 206.779 10.0236 1 1 -2 -5 179.342 8.60788 1 -1 -2 5 198.588 10.5746 1 -1 -2 5 203.24 12.9582 1 -1 -2 5 198.725 10.429 1 1 2 -5 201.256 10.5894 1 -1 2 5 194.712 9.39445 1 1 2 -5 191.659 10.7486 1 -1 -2 6 79.73 5.40117 1 -1 -2 6 77.4881 6.121 1 -1 -2 6 78.0003 6.05019 1 1 -2 -6 71.8443 6.8164 1 1 2 -6 76.9541 6.22982 1 1 2 -6 67.5042 9.64712 1 1 2 -6 69.8896 5.65729 1 -1 2 6 87.7425 4.71718 1 1 -2 -7 18.0298 4.32272 1 1 2 -7 25.383 3.91087 1 1 2 -7 21.3467 3.30443 1 -1 -2 7 22.9128 3.20097 1 -1 -2 7 20.5399 3.54015 1 -1 -2 7 24.6227 3.98189 1 -1 2 7 19.5482 2.29186 1 1 2 -7 28.848 7.61848 1 -1 2 7 24.2129 3.20373 1 1 -2 -8 55.3572 5.71573 1 1 -2 -8 49.2176 6.82837 1 1 2 -8 74.0085 11.2234 1 1 2 -8 53.2224 5.50408 1 -1 -2 8 50.6884 5.5184 1 1 2 -8 55.0408 5.30289 1 -1 2 8 50.6487 4.91825 1 -1 -2 8 63.6711 5.37857 1 -1 -2 8 70.3638 6.43119 1 1 -2 -9 153.918 10.6501 1 -1 -2 9 171.664 10.7536 1 -1 -2 9 157.487 9.81528 1 1 -2 -9 148.431 11.0641 1 1 2 -9 147.595 9.12165 1 1 2 -9 179.85 16.4247 1 -1 2 9 136.992 9.04774 1 1 2 -9 161.91 9.75324 1 -1 -2 9 151.975 10.0133 1 -1 -2 10 36.05 5.82508 1 1 -2 -10 20.3366 5.3433 1 1 2 -10 26.4146 3.85817 1 -1 2 10 27.3606 4.84987 1 1 2 -10 31.7448 4.40861 1 -1 2 10 28.2954 2.80856 1 1 2 -10 38.8733 10.4777 1 1 2 -11 24.1027 3.4307 1 -1 -2 11 16.3667 5.9916 1 1 -2 -11 9.84685 6.26491 1 -1 -2 11 24.3716 5.7997 1 1 -2 -11 17.5433 6.43739 1 1 2 -11 20.831 10.1218 1 -1 2 11 24.487 3.54817 1 1 2 -11 17.3397 2.89472 1 1 2 -12 45.3643 12.4632 1 1 -2 -12 45.2597 7.9682 1 -1 -2 12 43.0964 8.25092 1 -1 -2 12 55.5091 7.60932 1 -1 2 12 49.2598 5.27488 1 1 -2 -12 27.5567 7.78327 1 1 -2 -13 2.36266 7.04216 1 1 -2 -13 12.3454 6.79208 1 1 2 -13 14.4795 11.9637 1 -1 2 13 7.67506 4.2563 1 1 -3 -1 672.216 30.8916 1 -1 -3 1 680.474 31.6404 1 -1 -3 1 692.123 31.4694 1 -1 -3 1 693.451 31.5011 1 1 -3 -1 694.32 34.7142 1 1 -3 -1 682.47 30.558 1 1 -3 -1 675.131 31.2883 1 -1 -3 1 755.289 35.7826 1 1 3 -1 725.22 31.5776 1 -1 3 1 693.186 31.0462 1 -1 3 1 675.735 34.4073 1 1 3 -1 717.909 31.7502 1 -1 3 1 681.844 31.3761 1 -1 3 1 644.231 31.0187 1 1 3 -1 715.30 35.2342 1 1 3 -1 686.15 31.4146 1 -1 -3 2 108.866 10.9245 1 -1 -3 2 103.331 7.53977 1 1 -3 -2 97.9261 10.0843 1 1 3 -2 134.062 8.02387 1 -1 3 2 101.96 7.05795 1 1 -3 -2 112.376 6.17058 1 1 -3 -2 106.71 6.97675 1 -1 3 2 117.375 9.71787 1 1 3 -2 111.601 7.55619 1 1 3 -2 114.725 10.7352 1 1 3 -2 115.801 7.5939 1 -1 3 2 104.775 6.98236 1 -1 3 2 106.911 7.3042 1 -1 -3 2 107.266 7.63798 1 1 -3 -2 110.091 5.86413 1 -1 -3 2 106.767 7.40112 1 -1 -3 3 358.982 18.3319 1 1 -3 -3 332.548 20.4107 1 -1 -3 3 364.856 21.8103 1 -1 -3 3 405.094 18.4516 1 -1 -3 3 383.677 18.5638 1 1 -3 -3 371.625 17.5666 1 1 3 -3 389.09 22.7547 1 -1 3 3 363.48 17.6399 1 1 3 -3 397.394 18.8845 1 -1 3 3 378.473 20.1684 1 -1 3 3 342.40 17.8128 1 -1 3 3 371.922 17.5776 1 1 3 -3 388.999 17.9953 1 1 3 -3 396.192 18.3265 1 -1 3 4 67.7123 5.22394 1 -1 -3 4 77.6918 9.91075 1 -1 -3 4 69.9042 6.12691 1 -1 -3 4 72.6588 6.47882 1 -1 -3 4 71.8206 6.01447 1 1 -3 -4 69.0026 5.14637 1 1 -3 -4 72.4511 4.53226 1 -1 3 4 72.8374 4.91814 1 1 3 -4 76.4775 10.3801 1 1 3 -4 69.2558 5.39068 1 1 3 -4 68.0462 6.29748 1 -1 3 4 68.617 4.80321 1 1 -3 -4 69.7432 8.02841 1 -1 3 4 70.5262 6.50589 1 -1 3 5 54.1916 4.17803 1 1 3 -5 58.8456 9.7395 1 -1 3 5 50.9666 4.48904 1 1 -3 -5 48.0786 4.1522 1 -1 -3 5 48.7286 5.41068 1 -1 -3 5 50.6022 5.63267 1 1 -3 -5 46.3367 3.62199 1 -1 -3 5 40.7462 8.34903 1 -1 -3 5 49.6502 5.08012 1 1 -3 -5 51.2989 7.16734 1 1 3 -5 45.5148 5.30733 1 -1 3 5 42.6733 3.68312 1 1 3 -5 50.8018 3.91756 1 1 3 -5 46.5762 5.50569 1 1 3 -5 50.1978 3.51811 1 -1 3 5 37.3428 4.63549 1 -1 3 5 46.7072 3.84148 1 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2.66441 1 1 3 -9 9.65896 3.67593 1 1 -3 -10 69.0903 9.94934 1 1 -3 -10 68.8958 8.61001 1 1 3 -10 64.3855 7.46187 1 1 3 -10 83.3042 14.3203 1 -1 3 10 66.3474 5.59781 1 -1 3 10 82.3732 6.63381 1 1 3 -10 57.8843 6.63035 1 -1 -3 10 70.6873 8.61349 1 -1 -3 11 20.1688 6.57044 1 1 -3 -11 6.39414 5.84098 1 1 3 -11 19.7097 5.44427 1 -1 3 11 19.9775 3.82561 1 1 3 -11 23.4515 11.8913 1 1 3 -12 31.2181 8.87555 1 1 3 -12 19.7245 13.1466 1 -1 -3 12 15.6121 7.58756 1 1 -3 -12 11.4432 6.97378 1 -1 3 12 23.494 4.73319 1 1 -3 -12 43.0294 8.96143 1 1 4 -1 120.037 8.76989 1 1 4 -1 124.934 8.75831 1 -1 -4 1 121.382 8.74057 1 -1 -4 1 114.024 12.4292 1 1 4 -1 121.269 12.2698 1 -1 4 1 113.566 8.40219 1 1 -4 -1 115.834 12.2352 1 -1 -4 1 129.055 8.64478 1 1 -4 -1 108.94 8.22601 1 -1 -4 1 102.356 8.24341 1 1 -4 -1 107.277 7.43813 1 1 -4 -1 115.644 7.83577 1 -1 4 1 110.562 11.6901 1 -1 4 1 119.485 8.50024 1 -1 4 1 114.106 8.5821 1 1 4 -1 123.91 8.92751 1 -1 -4 2 563.488 26.6605 1 1 -4 -2 529.529 25.9058 1 1 -4 -2 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128.449 7.56892 1 -1 1 -5 124.538 7.84737 1 -1 1 -5 122.392 8.21611 1 1 1 5 132.089 7.35816 1 1 1 6 59.3175 5.91985 1 1 -1 6 44.444 5.12366 1 1 -1 6 52.4853 5.31077 1 -1 -1 -6 47.4679 4.59503 1 -1 -1 -6 49.0586 4.57188 1 1 -1 6 49.1761 5.86095 1 1 1 6 42.0448 4.42762 1 -1 1 -6 46.3503 8.6886 1 1 1 6 48.5035 5.50472 1 -1 1 -6 45.5831 5.02732 1 -1 1 -6 47.4882 4.68016 1 1 1 6 40.0762 4.41206 1 1 1 6 50.6171 4.60859 1 1 -1 6 44.2546 4.51221 1 -1 -1 -6 45.1048 6.70762 1 -1 -1 -6 50.0802 7.66179 1 1 1 7 55.8005 5.96019 1 1 1 7 50.0474 5.05506 1 -1 -1 -7 63.8226 8.91759 1 1 -1 7 55.6548 7.93735 1 -1 -1 -7 51.4967 5.27767 1 -1 -1 -7 63.9717 5.57968 1 1 -1 7 54.9833 5.78796 1 1 -1 7 57.3166 5.4937 1 1 -1 7 66.732 6.36463 1 -1 1 -7 64.6023 6.37109 1 1 1 7 46.9514 4.86463 1 -1 1 -7 55.0477 5.32311 1 1 1 7 50.7505 6.27878 1 -1 1 -7 58.6254 10.4833 1 1 -1 8 51.8165 6.49941 1 1 -1 8 48.1842 7.67913 1 1 -1 8 40.5941 5.18561 1 -1 -1 -8 51.3635 5.06199 1 1 -1 8 40.7757 5.46204 1 -1 -1 -8 41.3574 4.62557 1 1 1 8 37.7164 4.93929 1 1 1 8 40.2473 4.83935 1 1 1 8 54.7611 6.38301 1 -1 1 -8 44.1081 10.8328 1 1 1 8 50.9404 6.76548 1 -1 1 -8 34.3373 4.78268 1 -1 1 -8 44.4548 5.69896 1 -1 -1 -8 41.0361 8.2699 1 -1 -1 -8 45.1129 8.09008 1 1 1 9 203.457 15.2065 1 -1 1 -9 225.993 12.6781 1 1 1 9 207.287 12.0071 1 -1 -1 -9 211.573 11.2623 1 -1 -1 -9 204.954 16.9358 1 1 -1 9 199.528 13.3817 1 1 -1 9 210.41 12.9104 1 -1 -1 -9 170.744 16.671 1 -1 -1 -9 218.427 11.2406 1 -1 1 -9 175.809 18.7942 1 -1 1 -9 181.885 11.6763 1 1 1 9 209.938 13.1827 1 -1 -1 -10 36.7122 10.2027 1 -1 -1 -10 54.1706 5.16191 1 1 -1 10 45.0024 6.39376 1 -1 -1 -10 49.8246 4.88852 1 1 -1 10 58.5537 7.84544 1 -1 1 -10 41.6226 13.0551 1 -1 1 -10 51.6675 6.45369 1 -1 1 -10 52.3946 5.88452 1 1 1 10 50.0173 7.47819 1 1 1 10 56.632 6.56495 1 -1 -1 -10 18.5809 9.289 1 1 1 11 4.78196 5.69783 1 1 1 11-0.60073 3.83565 1 1 -1 11-1.45742 4.50557 1 -1 -1 -11 3.4349 8.42065 1 1 -1 11 2.13038 5.30678 1 -1 -1 -11-1.88368 7.22559 1 -1 1 -11 5.39197 9.72021 1 -1 1 -11-0.74731 4.45224 1 1 -1 12 6.50281 6.78303 1 -1 1 -12 10.5998 10.5607 1 -1 1 -12 10.3868 10.4245 1 -1 -1 -12 19.4064 10.3388 1 1 1 12 14.0687 7.11097 1 -1 -1 -12 3.7621 9.97197 1 1 -2 0 840.438 36.6443 1 -1 -2 0 813.215 37.0602 1 -1 -2 0 842.616 36.9445 1 1 -2 0 916.059 37.6778 1 1 -2 0 847.071 36.8423 1 -1 -2 0 806.901 36.7767 1 -1 2 0 913.06 39.9605 1 -1 2 0 847.143 36.9655 1 1 2 0 796.084 37.0104 1 1 2 0 844.559 37.2379 1 -1 2 0 835.825 37.2558 1 1 2 0 818.956 37.1022 1 -1 2 0 863.178 36.9899 1 -1 2 0 845.225 37.1775 1 1 2 0 884.534 39.8369 1 1 -2 0 847.692 37.068 1 -1 -2 -1 3901.83 168.281 1 1 -2 1 4475.02 172.645 1 1 -2 1 3715.76 169.171 1 -1 -2 -1 4236.57 171.911 1 1 -2 1 3924.39 168.469 1 1 -2 1 3979.11 169.12 1 1 -2 1 4080.62 168.58 1 -1 -2 -1 3906.34 168.16 1 -1 -2 -1 3889.17 168.892 1 1 -2 1 4122.44 169.237 1 -1 2 -1 4071.54 172.184 1 1 2 1 4185.91 174.441 1 -1 2 -1 4011.98 171.469 1 1 2 1 3997.13 171.816 1 -1 2 -1 4542.91 175.689 1 1 2 1 4008.55 171.492 1 -1 2 -1 4022.58 172.036 1 -1 2 -1 4151.84 171.448 1 1 2 1 3861.26 171.297 1 1 -2 2 1905.26 82.8568 1 -1 -2 -2 1913.60 82.4327 1 1 -2 2 2118.67 86.2311 1 -1 -2 -2 1893.27 82.0332 1 1 -2 2 1859.65 82.3387 1 -1 -2 -2 1888.19 81.4849 1 1 -2 2 1907.91 82.8214 1 -1 -2 -2 1986.77 82.6526 1 1 -2 2 1965.59 82.3453 1 -1 -2 -2 2050.22 85.2803 1 1 -2 2 1835.45 83.2855 1 1 2 2 1897.34 82.075 1 -1 2 -2 2043.16 86.4203 1 1 2 2 1976.69 84.69 1 1 2 2 1942.30 82.4829 1 1 2 2 1936.45 82.855 1 1 2 2 1878.98 82.2268 1 -1 2 -2 1845.11 82.7554 1 -1 2 -2 2009.63 82.2063 1 -1 2 -2 1923.01 82.421 1 1 -2 3 192.816 11.0656 1 1 -2 3 195.955 10.9229 1 1 -2 3 209.22 11.0845 1 -1 -2 -3 219.057 10.5736 1 1 -2 3 220.618 14.4027 1 -1 -2 -3 215.619 13.8803 1 -1 -2 -3 193.043 8.90257 1 -1 -2 -3 171.265 8.79122 1 1 -2 3 207.219 10.5768 1 -1 -2 -3 212.695 10.6992 1 -1 2 -3 231.453 15.6091 1 1 2 3 197.423 10.7186 1 -1 2 -3 224.568 10.6324 1 -1 2 -3 197.19 11.2102 1 -1 2 -3 198.849 10.8376 1 1 2 3 220.512 11.3557 1 1 2 3 219.842 12.9095 1 1 2 3 193.918 10.3987 1 -1 2 -3 206.785 11.5647 1 1 2 3 202.542 10.7599 1 -1 -2 -4 90.6319 6.23891 1 1 -2 4 102.43 10.2448 1 1 -2 4 95.5295 6.94471 1 1 -2 4 85.3715 6.1187 1 1 -2 4 85.3896 6.66085 1 -1 -2 -4 92.2883 9.40068 1 -1 -2 -4 89.2488 6.29648 1 1 -2 4 94.619 6.85367 1 1 2 4 93.9051 6.2086 1 -1 2 -4 100.08 6.23286 1 1 2 4 85.9374 6.05478 1 1 2 4 85.837 5.83809 1 1 2 4 94.5254 6.80034 1 1 2 4 86.8566 6.29501 1 -1 2 -4 89.7699 7.09196 1 -1 2 -4 84.4681 6.49945 1 -1 2 -4 111.319 11.5861 1 1 2 5 593.782 26.8221 1 -1 2 -5 548.686 24.9134 1 1 -2 5 550.185 26.002 1 1 -2 5 569.698 26.6605 1 1 -2 5 561.089 26.4722 1 -1 -2 -5 551.101 28.8075 1 1 -2 5 581.355 26.9737 1 1 -2 5 606.972 30.5105 1 -1 -2 -5 583.811 26.2948 1 1 -2 5 531.148 25.9032 1 -1 -2 -5 570.126 25.8725 1 1 2 5 561.725 26.1253 1 1 2 5 565.067 26.2937 1 -1 2 -5 549.68 26.8739 1 -1 2 -5 596.797 25.2959 1 -1 2 -5 600.122 27.5069 1 1 2 5 590.005 26.9646 1 -1 2 -5 612.029 32.4497 1 1 2 5 567.992 25.9774 1 1 -2 6 403.326 19.6333 1 1 2 6 367.313 18.0032 1 1 2 6 366.838 18.1037 1 1 -2 6 380.139 19.1373 1 -1 -2 -6 369.09 18.1043 1 1 -2 6 360.804 18.4464 1 -1 -2 -6 366.13 21.6394 1 1 -2 6 380.007 19.1189 1 -1 -2 -6 359.244 19.0513 1 -1 -2 -6 402.926 21.2051 1 -1 2 -6 388.036 19.4217 1 -1 2 -6 359.571 18.6471 1 -1 2 -6 377.05 24.6014 1 1 2 6 356.947 17.6942 1 1 2 6 380.321 18.6764 1 1 2 6 389.084 18.8621 1 1 2 7 288.273 15.7545 1 1 -2 7 311.693 16.127 1 1 -2 7 272.437 15.1282 1 -1 -2 -7 284.656 14.5111 1 -1 -2 -7 285.915 17.8926 1 1 -2 7 289.695 15.7533 1 1 2 7 309.407 15.202 1 -1 2 -7 286.166 22.3866 1 1 2 7 291.105 15.9759 1 1 2 7 298.787 14.8261 1 -1 2 -7 310.936 16.5467 1 -1 2 -7 268.177 15.5543 1 -1 -2 -7 283.237 18.5864 1 1 -2 8 6.00744 4.10843 1 -1 -2 -8 4.28053 3.01886 1 1 2 8 5.78223 2.97495 1 -1 -2 -8 4.15426 6.09689 1 -1 -2 -8 5.94187 4.84314 1 -1 2 -8 7.75762 4.24606 1 1 2 8 5.90243 3.98144 1 1 2 8 9.377 3.99715 1 -1 2 -8 5.23951 8.20606 1 1 2 8 9.2049 3.63733 1 -1 2 -8 10.4463 3.62147 1 -1 -2 -8 5.94328 2.8888 1 1 -2 8 7.79908 4.07159 1 1 -2 8 4.06232 3.40484 1 -1 2 -9 14.1395 9.28074 1 -1 2 -9 7.49183 4.68897 1 1 2 9 16.9956 3.99475 1 -1 -2 -9 14.7581 3.4948 1 1 -2 9 15.0952 5.17638 1 -1 -2 -9 3.9624 5.56915 1 -1 -2 -9 19.5075 7.80212 1 -1 2 -9 11.8288 4.0967 1 1 2 9 22.3614 5.34201 1 -1 -2 -9 12.4266 3.22894 1 1 -2 9 14.5912 4.73201 1 -1 2 -10 11.2685 4.54302 1 1 -2 10 12.3855 5.04303 1 -1 -2 -10 10.7068 8.44364 1 1 -2 10 9.51281 5.41913 1 -1 -2 -10 3.76413 6.59152 1 -1 -2 -10 9.1552 2.05476 1 1 2 10 14.3116 5.43317 1 -1 2 -10 12.1001 5.5169 1 -1 -2 -10 9.70108 2.32774 1 -1 2 -10 9.8003 9.75822 1 1 2 10 12.3616 4.16705 1 1 -2 11 13.0292 6.02578 1 1 -2 11 26.8147 7.12752 1 -1 -2 -11 19.9812 9.4584 1 1 2 11 14.6621 4.98873 1 -1 2 -11 15.1543 11.2384 1 -1 2 -11 18.0198 7.07745 1 -1 -2 -11 14.5087 9.45395 1 -1 -2 -12 13.8552 10.7045 1 1 -2 12 9.87667 6.82997 1 -1 -2 -12-2.02335 9.31279 1 -1 2 -12 21.9649 13.7073 1 -1 -3 0 670.53 30.8064 1 1 -3 0 685.639 34.2581 1 1 -3 0 718.07 31.2584 1 1 -3 0 702.647 30.9121 1 -1 -3 0 629.204 30.9256 1 -1 -3 0 672.675 30.8049 1 1 -3 0 695.741 30.6227 1 -1 3 0 701.627 32.8503 1 1 3 0 721.624 32.8405 1 -1 3 0 760.692 36.7111 1 -1 3 0 703.981 32.4946 1 1 3 0 739.901 32.9074 1 -1 3 0 712.731 32.7929 1 1 3 0 722.453 32.7283 1 1 3 0 731.878 36.2201 1 -1 3 0 718.047 32.56 1 1 -3 1 188.563 14.0108 1 -1 -3 -1 167.652 9.51937 1 1 -3 1 164.385 10.0883 1 -1 -3 -1 167.537 9.43319 1 -1 -3 -1 170.184 9.96337 1 1 -3 1 170.103 9.90739 1 -1 -3 -1 168.29 13.1446 1 1 -3 1 163.891 9.81273 1 1 3 1 156.988 9.77996 1 -1 3 -1 174.512 10.1468 1 -1 3 -1 180.839 10.1595 1 -1 3 -1 176.396 10.4255 1 1 3 1 168.452 9.91486 1 -1 3 -1 164.90 9.72598 1 1 3 1 156.972 9.77103 1 -1 3 -1 176.903 13.7829 1 1 3 1 183.689 13.7824 1 -1 -3 -2 329.299 16.4846 1 -1 -3 -2 331.853 15.6588 1 -1 -3 -2 300.997 16.0939 1 -1 -3 -2 331.267 19.9122 1 -1 -3 -2 307.137 15.3928 1 1 -3 2 337.066 16.8853 1 1 -3 2 371.593 21.4688 1 1 -3 2 332.514 16.5267 1 1 3 2 297.516 16.0502 1 -1 3 -2 341.78 21.0834 1 -1 3 -2 331.238 16.8048 1 -1 3 -2 332.81 16.5521 1 -1 3 -2 337.305 17.161 1 1 3 2 327.93 16.3697 1 1 3 2 312.587 16.2532 1 1 3 2 348.464 19.5543 1 -1 3 -2 322.203 16.1584 1 1 -3 3 461.282 22.276 1 -1 -3 -3 424.822 20.1242 1 1 -3 3 494.018 26.8477 1 -1 -3 -3 451.208 21.844 1 -1 3 -3 462.701 21.7503 1 -1 3 -3 446.017 22.5196 1 1 3 3 456.00 22.0212 1 -1 3 -3 489.803 27.3801 1 1 3 3 457.809 21.7957 1 1 3 3 443.779 21.9124 1 1 3 3 484.45 24.7576 1 -1 3 -3 470.924 22.2177 1 -1 -3 -3 464.252 21.5353 1 -1 -3 -3 444.381 20.4176 1 -1 -3 -3 448.308 20.2834 1 1 -3 3 468.73 22.4789 1 1 -3 3 461.859 22.0128 1 -1 -3 -3 476.59 25.5894 1 1 -3 4 22.4523 4.02006 1 1 -3 4 31.8927 7.93463 1 -1 -3 -4 24.201 6.88927 1 1 -3 4 29.4194 4.23543 1 -1 -3 -4 23.4585 3.80406 1 -1 -3 -4 25.6775 3.77638 1 1 -3 4 25.2278 4.16272 1 1 3 4 18.0058 3.30 1 -1 3 -4 19.4028 3.11261 1 1 3 4 20.132 3.32142 1 1 3 4 28.4714 5.57834 1 1 3 4 24.5897 4.2123 1 -1 3 -4 21.9389 3.89446 1 -1 3 -4 30.2985 8.55716 1 1 3 4 19.6613 3.33275 1 -1 3 -4 21.2483 3.78234 1 -1 3 -4 29.4201 5.07154 1 1 3 5 297.878 16.3375 1 -1 3 -5 311.144 17.0537 1 1 -3 5 294.704 16.092 1 -1 -3 -5 286.73 15.1571 1 1 -3 5 292.344 15.6513 1 -1 -3 -5 297.18 19.5981 1 1 -3 5 302.565 16.2692 1 -1 -3 -5 300.533 15.2909 1 1 -3 5 284.403 20.1523 1 -1 3 -5 311.851 16.5318 1 -1 3 -5 346.892 22.9422 1 -1 3 -5 284.617 14.535 1 1 3 5 301.564 15.6781 1 1 3 5 316.11 15.8082 1 1 3 5 286.893 15.2282 1 -1 -3 -6 13.175 6.98556 1 1 -3 6 6.75463 3.34319 1 1 -3 6 6.13997 2.90116 1 -1 -3 -6 3.71441 2.75318 1 1 -3 6 4.08654 3.51045 1 1 3 6 4.66187 3.27029 1 -1 3 -6 2.00707 7.7359 1 -1 3 -6 4.92026 3.78532 1 -1 3 -6 1.93729 2.52395 1 1 3 6 5.92365 2.71896 1 -1 3 -6 2.50496 3.11732 1 1 3 6 5.37137 3.09081 1 -1 3 -6 3.76158 1.95164 1 -1 -3 -7 6.80313 5.08064 1 -1 -3 -7 21.9302 7.70323 1 -1 -3 -7 11.8007 3.35066 1 1 -3 7 7.35312 3.61285 1 1 3 7 11.30 4.36317 1 1 -3 7 8.79537 3.84363 1 1 -3 7 3.96701 3.87075 1 1 3 7 2.30122 3.53954 1 1 3 7 10.1892 3.2473 1 -1 3 -7 6.29353 4.35571 1 -1 3 -7 14.7734 9.70033 1 -1 3 -7 18.3362 4.39202 1 -1 -3 -8 62.7128 9.09193 1 -1 -3 -8 69.8951 11.5403 1 1 -3 8 50.187 7.27726 1 -1 3 -8 66.3384 7.44423 1 -1 3 -8 67.038 13.516 1 -1 3 -8 62.4995 7.75528 1 1 3 8 52.9662 6.09892 1 -1 -3 -8 58.2748 6.1911 1 1 3 8 53.6078 7.95909 1 -1 3 -9 39.4387 7.21103 1 1 -3 9 30.4874 6.84699 1 1 -3 9 30.4575 6.51046 1 -1 -3 -9 29.8052 4.34247 1 -1 -3 -9 33.7412 4.36021 1 -1 -3 -9 36.9905 8.32824 1 1 3 9 27.2429 5.09422 1 -1 3 -9 28.3012 5.46721 1 -1 3 -9 35.8313 13.3216 1 -1 -3 -9 35.0887 10.0522 1 1 -3 10 14.6394 6.24918 1 1 -3 10 12.4069 5.84728 1 -1 -3 -10 5.85378 6.91334 1 -1 -3 -10 9.44458 9.32972 1 -1 -3 -10 7.5092 2.54478 1 1 3 10 4.96761 3.93816 1 -1 3 -10 14.0735 11.8851 1 -1 3 -11 -3.0159 12.0631 1 -1 -3 -11 1.26785 10.0238 1 1 -3 11 3.90516 5.90914 1 1 3 11 9.76628 4.91632 1 -1 -3 -11 1.40009 7.85881 1 -1 -4 0 228.421 13.8559 1 1 -4 0 252.949 13.8265 1 1 -4 0 239.47 13.8824 1 1 -4 0 257.174 13.4576 1 -1 -4 0 236.60 13.5132 1 -1 -4 0 237.933 13.5167 1 1 -4 0 277.141 18.1643 1 1 4 0 244.489 13.9695 1 1 4 0 249.202 14.1659 1 -1 4 0 251.392 14.0132 1 -1 4 0 301.548 19.0048 1 -1 4 0 240.388 14.1988 1 1 4 0 247.448 14.1248 1 -1 4 0 234.563 13.8287 1 1 4 0 241.871 17.6575 1 1 4 1 105.461 11.58 1 -1 -4 -1 91.6608 7.13642 1 1 -4 1 103.449 7.8872 1 -1 -4 -1 100.665 7.41941 1 1 -4 1 99.5974 7.90525 1 1 -4 1 101.014 8.05722 1 -1 -4 -1 107.283 8.052 1 1 -4 1 126.975 12.5162 1 -1 -4 -1 91.1618 11.4441 1 -1 4 -1 107.05 8.06041 1 1 4 1 92.6795 7.79379 1 1 4 1 96.8393 8.01142 1 -1 4 -1 105.007 8.65137 1 -1 4 -1 105.476 8.21338 1 -1 4 -1 114.696 12.7373 1 1 4 1 114.886 8.19981 1 -1 4 -1 114.212 8.3942 1 -1 -4 -2 311.467 15.4625 1 -1 -4 -2 276.675 15.9599 1 1 -4 2 324.964 17.0097 1 1 -4 2 318.043 16.7087 1 1 -4 2 319.71 16.7468 1 1 -4 2 305.928 21.1988 1 -1 -4 -2 295.514 16.3384 1 -1 -4 -2 327.621 21.20 1 -1 -4 -2 308.411 15.3894 1 -1 4 -2 311.239 17.02 1 1 4 2 298.058 20.1236 1 1 4 2 287.778 16.4867 1 -1 4 -2 330.942 17.6067 1 -1 4 -2 307.199 16.4585 1 1 4 2 317.842 16.7129 1 -1 4 -2 331.559 16.9637 1 1 4 2 320.224 16.7735 1 -1 4 -2 340.217 22.4946 1 -1 -4 -3 122.813 8.15931 1 -1 -4 -3 100.068 12.3038 1 -1 -4 -3 110.642 7.65529 1 -1 -4 -3 112.533 8.37846 1 1 -4 3 122.359 9.20544 1 1 4 3 122.182 11.8656 1 -1 4 -3 124.241 9.66103 1 1 4 3 114.832 8.50526 1 -1 4 -3 133.963 8.55313 1 -1 4 -3 127.048 12.9133 1 -1 4 -3 106.474 8.92232 1 -1 4 -3 133.026 14.7313 1 1 4 3 113.534 8.60092 1 1 4 3 106.11 8.32594 1 1 -4 3 131.894 14.3773 1 -1 -4 -3 111.676 6.91815 1 1 -4 3 115.829 8.77965 1 -1 -4 -3 102.748 6.71165 1 1 -4 3 111.778 8.78843 1 1 -4 4 2.11073 2.96194 1 1 -4 4 4.2932 2.8158 1 -1 -4 -4 4.08803 5.41692 1 -1 -4 -4 7.84524 3.12254 1 -1 -4 -4 3.50135 3.57397 1 1 -4 4 2.32247 5.89332 1 1 -4 4 2.90898 3.29851 1 1 4 4 1.8841 2.70161 1 -1 4 -4 10.9144 8.05832 1 1 4 4 3.32847 2.86271 1 -1 4 -4 0.08786 2.35817 1 1 4 4 3.92479 2.51149 1 -1 4 -4-4.88891 2.36483 1 -1 4 -4 2.57941 3.07033 1 -1 4 -5 177.722 11.8333 1 1 -4 5 177.411 18.6888 1 1 -4 5 169.972 11.7203 1 1 -4 5 172.776 12.0557 1 -1 -4 -5 181.14 15.9865 1 -1 -4 -5 174.79 11.037 1 1 -4 5 183.875 12.5354 1 -1 4 -5 165.799 10.0863 1 1 4 5 181.811 11.0951 1 1 4 5 165.753 11.0064 1 1 4 5 159.031 10.6988 1 -1 4 -5 198.236 19.1519 1 -1 4 -5 166.36 12.2681 1 -1 -4 -6 101.928 13.3631 1 1 -4 6 98.4553 8.87607 1 1 -4 6 102.799 9.92527 1 1 -4 6 97.1956 9.21903 1 -1 -4 -6 94.4854 7.89474 1 -1 4 -6 100.159 7.01739 1 -1 4 -6 118.141 17.4522 1 -1 4 -6 100.666 9.23548 1 1 4 6 97.1298 8.72744 1 1 4 6 90.9991 7.96862 1 -1 4 -6 99.7205 10.0974 1 1 -4 7 0.36269 4.02114 1 1 -4 7 6.45627 4.77271 1 -1 -4 -7 4.78364 3.40314 1 -1 -4 -7 7.93833 7.99151 1 -1 4 -7 5.25906 10.2698 1 1 4 7 9.73543 3.82456 1 -1 4 -7 12.1592 5.42966 1 1 -4 7 5.48054 4.14705 1 -1 4 -7 7.62887 4.34315 1 1 -4 8 15.669 5.8891 1 -1 -4 -8 19.1711 4.42133 1 1 4 8 13.9076 4.35565 1 -1 4 -8 19.5403 12.549 1 -1 4 -8 8.09869 4.52501 1 -1 -4 -8 22.0492 9.69297 1 -1 -4 -9 7.32571 6.27568 1 -1 -4 -9 6.23629 3.72008 1 1 -4 9 10.8997 6.37494 1 -1 4 -9 2.87802 12.0095 1 -1 -4 -9-0.23309 8.80289 1 -1 4 -9 6.60761 5.1672 1 1 4 9 5.98948 4.21227 1 -1 4 -10 72.7596 17.3891 1 -1 -4 -10 88.9071 7.48507 1 1 -4 10 71.3126 10.7046 1 -1 -4 -10 94.1869 13.3846 1 -1 -4 -10 89.0732 15.2407 1 1 4 10 54.2846 7.55823 1 -1 -4 -11-3.87349 7.61977 1 1 -4 11 1.97427 6.67634 1 -1 -4 -11 13.5286 11.2371 1 -1 4 -11-10.7916 14.1143 1 -1 -5 0 148.711 10.5155 1 1 -5 0 149.833 10.962 1 1 -5 0 149.835 10.2999 1 -1 -5 0 144.01 10.8623 1 1 5 0 159.31 11.3216 1 -1 5 0 162.459 11.2483 1 -1 5 0 143.262 11.316 1 -1 5 0 161.637 11.2062 1 1 5 0 162.30 15.2787 1 1 5 0 168.614 11.4351 1 -1 5 0 162.759 15.8359 1 1 -5 0 181.916 16.0977 1 1 5 0 160.852 11.3195 1 -1 -5 -1 170.02 17.2294 1 -1 -5 -1 174.53 12.0751 1 1 -5 1 189.484 17.3167 1 1 -5 1 183.292 11.8536 1 -1 -5 -1 172.316 11.1204 1 1 -5 1 186.941 12.3351 1 -1 5 -1 183.373 12.1772 1 -1 5 -1 179.207 11.9347 1 1 5 1 179.838 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8.24621 1 -6 4 -5 14.1059 7.22378 1 6 4 5 12.4525 7.86085 1 6 -4 6 6.58308 7.73164 1 6 -4 6 -6.6005 6.56613 1 -6 4 -6 10.1004 7.81187 1 6 4 6 1.2687 7.56481 1 6 -4 7 1.23435 14.9695 1 6 -4 7 7.81871 8.16603 1 6 -5 0 75.2798 9.14779 1 6 -5 0 72.9738 9.04325 1 -6 -5 0 90.7527 15.2477 1 -6 -5 0 72.1629 9.7538 1 -6 -5 0 71.8071 10.374 1 -6 5 0 90.5344 15.045 1 6 5 0 70.2398 10.0251 1 -6 5 0 78.9259 10.0399 1 -6 -5 -1 15.5966 6.45861 1 6 -5 1 16.3952 6.194 1 -6 -5 -1 14.2168 6.74333 1 -6 5 -1 8.45535 5.90435 1 6 5 1 13.185 6.20882 1 6 -5 2 12.5938 6.13377 1 -6 -5 -2 16.2624 6.86286 1 6 -5 2 2.01031 5.83587 1 6 5 2 13.0842 6.86677 1 -6 5 -2 11.9396 5.93357 1 -6 -5 -3 6.46276 6.45889 1 6 -5 3 16.8646 7.54315 1 6 -5 3 11.2822 6.7196 1 6 5 3 1.80422 6.17422 1 -6 -5 -4 25.6725 8.3681 1 6 -5 4 32.6832 8.62158 1 6 -5 4 23.5302 8.27345 1 6 5 4 17.1694 7.6694 1 -6 -5 -5 5.32672 8.54724 1 6 -5 5 10.835 8.39056 1 6 -5 5 28.015 9.58025 1 6 5 5 17.7615 8.52473 1 6 -5 6 16.6517 9.365 1 6 -5 6 7.57182 8.88968 1 6 -6 0-4.00647 5.02179 1 -6 -6 0-1.91587 11.5702 1 -6 6 0-1.24327 5.05712 1 6 6 0 3.36767 6.67228 1 6 -6 1 96.2489 11.3622 1 -6 -6 -1 69.0198 11.0456 1 6 6 1 71.40 10.7778 1 -6 6 -1 76.1832 10.1151 1 -6 -6 -2 0.79259 7.24532 1 6 -6 2 4.22202 6.43139 1 -6 6 -2 2.60784 6.68112 1 6 6 2 3.75025 6.83992 1 -6 -6 -3 29.4853 9.25963 1 6 -6 3 50.2596 9.97573 1 6 6 3 47.0727 10.1787 1 6 -6 4 26.5416 10.5789 1 -6 -6 -4 14.7946 8.55947 1 6 -6 4 31.6715 9.17749 1 6 6 4 29.0196 8.92739 1 6 -6 5 42.0897 11.4625 1 6 -6 5 43.5037 10.3121 1 6 -7 0 19.4204 7.58996 1 -6 7 0 13.5585 7.4436 1 6 7 0 15.6999 8.09641 1 6 -7 1 46.2971 10.0756 1 6 7 1 25.7072 9.51338 1 -6 7 -1 39.4112 9.17892 1 6 -7 2 8.76103 8.16447 1 6 7 2 15.6998 8.5335 1 6 -7 3 9.94486 8.33031 1 6 7 3 18.5379 9.67349 1 6 -8 0 30.3408 9.82921 1 -6 8 0 13.6779 8.66076 1 6 -8 1 17.2059 9.54354 1 6 8 1 9.04661 14.2911 1 7 0 0 0.08731 4.09375 1 -7 0 0-0.44225 4.03218 1 7 0 0 3.47242 9.29751 1 -7 0 0-4.76101 8.27211 1 7 0 0 1.46438 3.9103 1 7 0 0 0.82214 4.38192 1 -7 0 0 3.06353 8.23792 1 -7 0 0 0.69847 6.71271 1 -7 0 0 0.82999 4.15334 1 -7 0 -1 7.68616 7.99318 1 7 0 1 20.1282 6.14159 1 -7 0 -1 21.3536 6.00485 1 7 0 1 15.221 5.34445 1 7 0 1 19.576 6.01016 1 -7 0 -1 15.767 5.95393 1 -7 0 -2 51.0219 8.64707 1 7 0 2 61.8203 11.2791 1 7 0 2 57.316 8.3754 1 -7 0 -2 73.4957 8.93788 1 -7 0 -2 49.469 12.5124 1 7 0 2 58.4158 8.7573 1 7 0 3 16.2445 6.84947 1 7 0 3 10.8883 6.24478 1 -7 0 -3 13.9472 6.36925 1 -7 0 -4 8.35666 6.3177 1 7 0 4 17.1369 7.19446 1 7 0 4 15.324 6.39351 1 7 0 5-2.65289 6.07867 1 7 0 5 8.66548 6.45145 1 -7 0 -5 1.70254 6.09097 1 7 0 6 13.8967 7.20111 1 -7 0 -6 19.3082 8.38244 1 7 0 6 21.104 8.91198 1 7 0 7 14.0976 8.22005 1 -7 -1 0 27.9958 8.64098 1 -7 -1 0 26.2446 5.87376 1 7 -1 0 32.9258 6.29785 1 7 -1 0 30.1468 14.3677 1 7 -1 0 34.7722 6.49227 1 7 -1 0 31.2732 6.49989 1 -7 -1 0 36.7021 7.05528 1 -7 -1 0 4.70339 11.1493 1 -7 1 0 42.1319 10.1342 1 7 1 0 39.5596 7.13022 1 -7 1 0 31.6047 6.7798 1 -7 1 0 4.04479 11.7155 1 7 1 0 29.1373 6.64422 1 -7 1 0 30.5966 6.16161 1 7 1 0 41.6927 7.60623 1 -7 1 0 34.3512 6.57784 1 7 -1 1 45.7088 7.40605 1 7 -1 1 40.4837 7.25647 1 7 -1 1 17.9076 5.69135 1 -7 -1 -1 32.6647 6.54113 1 -7 -1 -1 36.8173 7.34349 1 -7 -1 -1 34.3981 9.1618 1 7 1 1 38.7802 7.53047 1 7 1 1 23.9253 6.11506 1 -7 1 -1 31.1304 6.89147 1 -7 1 -1 42.1143 7.03729 1 7 1 1 36.5013 7.04001 1 -7 1 -1 16.856 8.81531 1 -7 1 -1 37.7873 7.15744 1 -7 -1 -2 39.3437 7.53989 1 7 -1 2 38.6943 7.60517 1 -7 -1 -2 40.1327 8.04815 1 7 -1 2 38.1977 7.53763 1 7 1 2 43.4784 8.23652 1 -7 1 -2 35.3023 11.3565 1 -7 1 -2 48.263 7.86819 1 7 1 2 36.0524 7.34609 1 -7 1 -2 28.0411 6.7667 1 7 1 2 19.879 8.09716 1 7 -1 3 21.0238 6.72738 1 7 -1 3 27.9787 7.31733 1 -7 -1 -3 11.2083 6.13153 1 -7 1 -3 21.9333 6.81957 1 -7 1 -3 14.0496 8.5121 1 7 1 3 20.4563 6.92511 1 7 1 3 9.48974 6.12219 1 7 -1 4 38.6781 7.67881 1 -7 -1 -4 35.8491 8.14392 1 7 -1 4 46.6349 9.07422 1 -7 1 -4 17.7067 7.29241 1 7 1 4 42.2802 8.69195 1 7 1 4 41.4618 8.8106 1 7 -1 5 12.2045 7.4125 1 7 -1 5 2.23028 5.35784 1 -7 -1 -5 3.1453 6.35268 1 -7 1 -5-4.99059 5.95165 1 7 1 5 4.13312 7.10795 1 7 1 5 1.06107 5.57882 1 7 -1 6 6.72206 7.26738 1 -7 -1 -6 4.93984 7.48234 1 7 -1 6 16.8741 8.70408 1 7 1 6 8.80418 6.53529 1 7 1 6 17.3449 8.71673 1 -7 1 -6 16.537 7.8993 1 7 -1 7 8.37046 7.35467 1 7 1 7 20.3504 8.70931 1 7 -2 0 222.599 15.2461 1 7 -2 0 232.845 19.2919 1 -7 -2 0 216.712 15.9392 1 -7 -2 0 224.196 19.2364 1 7 -2 0 246.439 15.6924 1 7 2 0 249.849 16.7407 1 -7 2 0 240.206 20.8347 1 -7 2 0 228.784 16.4219 1 -7 2 0 253.699 17.5357 1 7 2 0 216.60 16.0225 1 7 -2 1 65.4244 8.64085 1 -7 -2 -1 32.4246 9.50827 1 -7 -2 -1 65.39 9.01811 1 7 -2 1 40.1315 7.39225 1 -7 -2 -1 44.9288 7.81569 1 -7 2 -1 52.8446 7.82407 1 -7 2 -1 46.0401 7.67516 1 7 2 1 55.9088 8.62683 1 -7 2 -1 47.2894 11.3949 1 7 2 1 38.7414 8.74078 1 -7 -2 -2 4.28669 5.37653 1 7 -2 2 6.66828 5.46761 1 -7 -2 -2 1.7045 5.10119 1 7 -2 2-0.26757 4.95601 1 7 2 2 0.84757 5.27924 1 -7 2 -2 10.1621 5.63722 1 -7 2 -2 0.91819 5.13461 1 -7 2 -2 21.884 11.5991 1 7 -2 3 83.3558 10.9953 1 7 -2 3 90.2606 11.2096 1 -7 -2 -3 82.4591 10.8101 1 -7 2 -3 68.2718 10.3229 1 7 2 3 77.5304 10.5521 1 7 -2 4 6.45761 6.68056 1 7 -2 4-2.24757 6.03376 1 -7 -2 -4 1.85475 5.80854 1 -7 2 -4-1.79978 6.05798 1 7 2 4-1.99174 5.88355 1 7 2 4 0.78851 6.09139 1 -7 -2 -5 5.0348 6.84093 1 7 -2 5 9.03897 7.54716 1 7 -2 5 7.2132 7.15761 1 7 2 5 9.42879 7.33897 1 7 2 5 7.86164 6.89129 1 -7 2 -5 8.52615 7.1327 1 7 -2 6 1.01174 7.96032 1 7 -2 6 4.76372 8.29548 1 7 2 6 18.4351 9.08612 1 7 2 6 5.6347 7.41522 1 -7 2 -6 11.1674 8.06916 1 -7 -3 0 262.888 18.7565 1 -7 -3 0 292.716 22.2791 1 -7 -3 0 279.357 18.9188 1 7 -3 0 287.681 18.0245 1 7 -3 0 295.15 17.8597 1 7 3 0 304.721 19.6629 1 -7 3 0 294.883 18.5947 1 -7 3 0 309.917 24.1234 1 -7 3 0 292.53 19.4524 1 -7 3 0 289.731 20.7088 1 -7 -3 -1 60.5384 9.17994 1 7 -3 1 77.6335 9.62183 1 -7 -3 -1 65.1348 9.38133 1 7 -3 1 84.16 10.1525 1 -7 3 -1 94.4329 14.7671 1 -7 3 -1 79.2185 10.7022 1 7 3 1 91.1448 10.9779 1 -7 3 -1 79.6387 9.75047 1 7 -3 2 107.666 11.6205 1 -7 -3 -2 69.6584 10.0677 1 7 -3 2 109.053 11.6678 1 -7 3 -2 131.091 12.0367 1 7 3 2 120.159 12.9562 1 -7 3 -2 82.6674 11.2719 1 -7 -3 -3 44.6865 8.72072 1 7 -3 3 52.4089 9.69748 1 7 -3 3 58.6144 9.62454 1 7 3 3 57.4591 9.97055 1 -7 3 -3 36.4694 8.75788 1 7 -3 4 19.4149 8.58983 1 7 -3 4 37.6904 8.8515 1 -7 -3 -4 17.9614 7.99436 1 7 3 4 29.9726 8.64454 1 -7 3 -4 25.0965 8.50524 1 7 -3 5 31.4421 9.57274 1 7 -3 5 23.9308 8.97831 1 -7 -3 -5 13.478 8.01191 1 -7 3 -5 1.6914 9.50217 1 7 3 5 28.8309 8.65612 1 7 -3 6 65.7276 12.5167 1 7 -3 6 33.3863 10.2158 1 -7 -4 0 31.3658 16.3629 1 -7 -4 0 40.4145 8.03582 1 -7 -4 0 41.4275 8.71121 1 7 -4 0 39.5362 7.6527 1 7 -4 0 50.8282 9.17127 1 7 4 0 42.1049 8.52774 1 -7 4 0 42.6514 12.773 1 -7 4 0 41.8081 7.72139 1 7 -4 1 78.2268 10.0441 1 -7 -4 -1 57.888 10.0416 1 -7 -4 -1 82.0434 11.5784 1 7 -4 1 68.6997 9.69792 1 -7 4 -1 92.9011 15.8126 1 7 4 1 81.7127 11.3635 1 -7 4 -1 80.8171 9.78518 1 7 -4 2 91.716 11.4734 1 7 -4 2 100.271 11.7499 1 -7 -4 -2 89.9216 12.3139 1 7 4 2 86.1194 12.0006 1 -7 4 -2 103.726 11.0188 1 7 -4 3 4.37634 6.87741 1 7 -4 3 5.23959 6.76137 1 -7 -4 -3 1.11989 6.89914 1 7 4 3 9.53146 6.90102 1 -7 -4 -4 18.9819 8.21233 1 7 -4 4 36.8275 9.09856 1 7 -4 4 23.4036 9.01116 1 7 4 4 21.5585 8.83765 1 7 -4 5 1.13074 8.09375 1 7 -4 5-4.17507 8.01892 1 7 4 5-2.08878 7.94498 1 -7 -5 0 38.1517 9.72935 1 7 -5 0 38.4522 7.96461 1 -7 5 0 54.118 8.96531 1 7 5 0 37.6407 8.62997 1 -7 5 0 57.9658 14.8199 1 7 -5 1 19.0993 7.45608 1 -7 5 -1 13.9122 6.78261 1 7 5 1 13.5824 7.44803 1 7 -5 2 74.9458 11.132 1 -7 -5 -2 41.3329 10.7039 1 7 5 2 79.7457 12.534 1 7 -5 3 12.2456 8.26288 1 -7 -5 -3 4.66736 7.96689 1 7 5 3 12.6798 8.12952 1 -7 -5 -4 9.25439 8.73468 1 7 -5 4 6.95295 13.813 1 7 -5 4 6.05193 8.36868 1 7 5 4-1.33408 7.75845 1 7 -6 0 42.9487 9.22184 1 7 6 0 29.7898 9.29097 1 -7 6 0 44.0691 9.42154 1 7 -6 1 10.8097 7.86182 1 7 6 1 14.2266 7.90801 1 -7 6 -1 8.23188 7.88056 1 7 -6 2 5.95983 8.1418 1 7 6 2 7.58757 8.67902 1 7 -6 3 28.1731 9.7536 1 7 6 3 54.4909 12.0495 1 7 -7 0 10.4498 7.81257 1 -7 7 0 21.4625 8.90182 1 7 -7 1 29.6108 9.60108 1 -8 0 0 85.9606 10.9382 1 -8 0 0 74.3696 13.0363 1 8 0 0 88.1866 10.6933 1 8 0 0 93.1795 10.8371 1 -8 0 0 70.6511 15.8711 1 8 0 1 221.188 16.6212 1 -8 0 -1 194.167 15.7209 1 8 0 1 193.485 15.6259 1 -8 0 -1 168.055 22.9643 1 8 0 2 44.0357 8.45689 1 -8 0 -2 58.5466 14.0405 1 8 0 2 52.7578 9.41649 1 -8 0 -3 74.4492 16.99 1 8 0 3 57.1314 9.73289 1 8 0 3 75.8465 11.1598 1 8 0 4 28.3726 8.90236 1 8 0 4 21.037 8.76562 1 8 0 5 4.2057 6.6606 1 8 0 5 6.57746 8.64126 1 8 -1 0 17.5554 6.48818 1 8 -1 0 11.6815 5.99142 1 -8 -1 0 17.4045 9.21562 1 -8 -1 0 17.1428 9.05735 1 -8 -1 0 5.85792 5.48355 1 8 1 0 16.1559 6.78543 1 -8 1 0 10.2552 6.37461 1 -8 1 0 22.6762 10.3335 1 8 -1 1 19.6564 7.26929 1 -8 -1 -1 9.29189 5.75525 1 -8 -1 -1 30.896 9.17306 1 8 -1 1 21.9423 6.85657 1 8 1 1 23.3706 7.44436 1 -8 1 -1 19.4342 7.25036 1 -8 1 -1 19.215 14.2136 1 8 1 1 24.4329 7.3541 1 8 -1 2-2.41478 5.83117 1 8 -1 2 1.9376 6.29336 1 -8 -1 -2 5.21526 6.93152 1 8 1 2 2.17827 6.07411 1 -8 1 -2 5.21484 10.1678 1 -8 -1 -3 -7.3915 6.24999 1 8 -1 3 1.43149 6.51284 1 8 -1 3 7.1439 6.85915 1 8 1 3 5.02796 7.04442 1 8 1 3 3.95396 6.76373 1 8 -1 4 25.7411 8.37705 1 -8 -1 -4 26.154 9.9616 1 8 -1 4 23.732 8.74866 1 8 1 4 20.3571 9.15646 1 8 1 4 17.8823 8.02015 1 8 -1 5 0.42246 8.64223 1 -8 -1 -5 4.70296 8.86449 1 8 -1 5-1.02111 6.06624 1 8 1 5 7.56644 7.65445 1 8 1 5 2.63966 8.57847 1 -8 -2 0 82.7284 10.4244 1 8 -2 0 104.113 11.5919 1 -8 -2 0 102.625 14.5159 1 8 -2 0 86.8788 10.354 1 8 2 0 103.892 11.8821 1 -8 2 0 98.3595 11.2702 1 -8 2 0 118.193 15.7213 1 8 -2 1 96.3594 11.4052 1 -8 -2 -1 71.3385 10.5241 1 8 -2 1 78.3598 10.674 1 -8 2 -1 66.7777 10.647 1 -8 2 -1 91.3135 21.3699 1 8 2 1 94.8637 11.4007 1 8 -2 2 1.256 6.60718 1 8 -2 2 4.02975 6.10185 1 8 2 2-3.14285 6.20155 1 8 -2 3 36.9185 9.63505 1 8 -2 3 32.704 9.03334 1 -8 -2 -3 18.371 11.4264 1 8 2 3 28.7605 8.90322 1 -8 -2 -4 14.0147 11.007 1 8 -2 4 10.798 8.54648 1 8 -2 4 32.191 8.84776 1 8 2 4 29.5207 9.69979 1 8 -2 5 0.62611 8.77116 1 8 -2 5 2.86092 7.84096 1 8 2 5 8.65403 9.48841 1 -8 -3 0-2.91264 5.98429 1 8 -3 0-2.38216 5.86993 1 -8 3 0-3.93637 4.93907 1 -8 3 0-3.52902 9.58057 1 8 3 0 4.66548 6.17288 1 8 -3 1 70.2292 10.1239 1 -8 3 -1 53.5047 8.82014 1 8 3 1 56.0344 10.1919 1 8 -3 2 92.9999 12.3958 1 8 -3 2 116.989 16.3832 1 8 3 2 93.8481 13.1904 1 8 -3 3 65.6494 11.6016 1 8 -3 3 55.4552 11.1873 1 8 3 3 57.9775 11.1401 1 8 -3 4-3.44533 7.73573 1 8 -3 4 3.77059 8.36091 1 8 3 4 7.41717 8.94687 1 8 -4 0 7.92488 6.90987 1 8 4 0 3.1242 7.19137 1 -8 4 0-1.39335 6.18958 1 -8 4 0-0.91404 11.442 1 8 -4 1 47.0706 9.63201 1 8 4 1 38.6568 9.47104 1 -8 4 -1 50.0502 8.72302 1 8 -4 2 46.2573 9.66323 1 8 4 2 47.2946 10.563 1 8 -4 3 19.6886 8.7897 1 8 4 3 4.12246 8.50808 1 8 -4 4 40.6226 10.5897 1 8 4 4 20.6552 10.4051 1 8 -5 0-1.33194 6.81409 1 -8 5 0 9.99944 7.44915 1 -8 5 0 14.1852 19.9539 1 8 -5 1 7.2941 7.87793 1 8 5 1 12.1636 9.09163 1 8 -5 2 39.6864 10.279 1 8 5 2 33.1136 10.373 1 8 5 3 13.6066 10.1159 1 8 -6 0 92.4775 12.6589 1 -8 6 0 78.7909 11.9462 1 8 -6 1 13.4684 9.07204 1 -9 0 0-1.38327 5.71821 1 9 0 0 1.5151 6.75997 1 9 0 1-5.40064 6.55083 1 9 0 2 26.7147 10.0946 1 9 0 3 4.97851 10.8885 1 9 0 3-1.46081 8.54736 1 9 -1 0 37.1725 9.07748 1 -9 -1 0 34.5155 8.09935 1 -9 1 0 41.8095 8.36477 1 9 -1 1 88.7427 12.6924 1 9 -1 2 115.07 14.4977 1 9 1 2 110.281 15.968 1 9 -1 3 49.6138 11.8393 1 9 1 3 31.4487 10.6434 1 9 1 3 44.6927 10.2115 1 -9 -2 0 28.2644 10.0814 1 9 -2 0 52.9625 9.65611 1 -9 2 0 46.3044 9.85845 1 9 -2 1 27.1485 8.69396 1 9 -2 2 119.202 15.4207 1 9 2 2 98.2523 17.3815 1 9 -2 3 10.0152 8.05281 1 9 2 3 8.76805 9.70248 1 -9 3 0 44.7859 10.3039 1 9 -3 0 39.8698 9.61745 1 9 -3 1 65.3619 11.2453 1 9 -3 2 32.3115 9.84359 1 9 -4 0 13.5745 8.75531 1 -9 4 0 22.2507 9.22555 1 9 -4 1 20.0915 8.98525 1 9 -5 0 48.9998 11.0273 1 10 0 1 3.32276 8.56544 1 10 -1 0-8.21257 7.43708 1 10 -1 1 3.83595 8.9761 1 10 -2 0 24.4289 9.52502 1 0 0 0 0.00 0.00 1 ; _shelx_hkl_checksum 47674 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.4446(2) 0.8708(2) 0.11510(17) 0.0237(5) Uani 1 1 d . . . . . H1O H 0.372(3) 0.931(4) 0.045(2) 0.036 Uiso 1 1 calc R U . . . C1 C 0.5457(3) 0.7600(3) 0.0635(2) 0.0189(6) Uani 1 1 d . . . . . H1 H 0.4725 0.7027 -0.0196 0.023 Uiso 1 1 calc R U . . . C2 C 0.6230(3) 0.6221(3) 0.1663(2) 0.0187(6) Uani 1 1 d . . . . . O3 O 0.7041(2) 0.5035(2) 0.13696(16) 0.0212(4) Uani 1 1 d . . . . . N4 N 0.5980(3) 0.6395(3) 0.28622(19) 0.0199(5) Uani 1 1 d . . . . . H4 H 0.535(4) 0.730(5) 0.294(3) 0.039(9) Uiso 1 1 d . . . . . C5 C 0.6498(3) 0.5301(4) 0.3997(2) 0.0192(6) Uani 1 1 d . . . . . C6 C 0.7098(3) 0.3636(4) 0.3943(2) 0.0196(6) Uani 1 1 d . . . . . H6 H 0.7176 0.3189 0.3122 0.023 Uiso 1 1 calc R U . . . C7 C 0.7584(3) 0.2633(3) 0.5104(2) 0.0210(6) Uani 1 1 d . . . . . C8 C 0.7467(3) 0.3269(4) 0.6312(2) 0.0237(6) Uani 1 1 d . . . . . H8 H 0.7802 0.2582 0.7102 0.028 Uiso 1 1 calc R U . . . C9 C 0.6851(3) 0.4925(4) 0.6346(2) 0.0248(6) Uani 1 1 d . . . . . H9 H 0.6759 0.5368 0.7165 0.03 Uiso 1 1 calc R U . . . C10 C 0.6372(3) 0.5934(3) 0.5206(2) 0.0223(6) Uani 1 1 d . . . . . H10 H 0.5956 0.7064 0.5244 0.027 Uiso 1 1 calc R U . . . C11 C 0.8212(3) 0.0901(4) 0.5043(2) 0.0224(6) Uani 1 1 d . . . . . C12 C 0.8722(3) -0.0496(4) 0.4999(3) 0.0291(7) Uani 1 1 d . . . . . H12 H 0.9135 -0.1628 0.4963 0.035 Uiso 1 1 calc R U . . . C13 C 0.6812(3) 0.8583(3) 0.0279(2) 0.0188(6) Uani 1 1 d . . . . . C14 C 0.7917(3) 0.9632(4) 0.1230(3) 0.0263(7) Uani 1 1 d . . . . . H14 H 0.7827 0.9727 0.2108 0.032 Uiso 1 1 calc R U . . . C15 C 0.9145(4) 1.0536(4) 0.0898(3) 0.0351(8) Uani 1 1 d . . . . . H15 H 0.9891 1.1249 0.1553 0.042 Uiso 1 1 calc R U . . . C16 C 0.9302(3) 1.0417(4) -0.0368(3) 0.0366(8) Uani 1 1 d . . . . . H16 H 1.015 1.1042 -0.0585 0.044 Uiso 1 1 calc R U . . . C17 C 0.8210(4) 0.9376(4) -0.1320(3) 0.0321(7) Uani 1 1 d . . . . . H17 H 0.8315 0.9276 -0.2193 0.039 Uiso 1 1 calc R U . . . C18 C 0.6960(3) 0.8478(4) -0.0999(2) 0.0234(6) Uani 1 1 d . . . . . H18 H 0.6201 0.7786 -0.1661 0.028 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0285(10) 0.0221(11) 0.0235(8) 0.0033(8) 0.0123(7) 0.0076(9) C1 0.0234(14) 0.0184(15) 0.0164(12) -0.0004(11) 0.0083(10) 0.0006(11) C2 0.0228(13) 0.0110(14) 0.0223(13) -0.0002(11) 0.0070(11) -0.0053(11) O3 0.0280(10) 0.0137(10) 0.0232(8) -0.0011(8) 0.0097(7) 0.0017(8) N4 0.0289(13) 0.0132(12) 0.0191(10) 0.0017(10) 0.0098(9) 0.0032(11) C5 0.0203(13) 0.0166(14) 0.0207(12) 0.0032(11) 0.0063(10) -0.0016(12) C6 0.0246(13) 0.0191(15) 0.0168(11) -0.0025(11) 0.0092(10) -0.0021(12) C7 0.0211(13) 0.0157(15) 0.0267(14) 0.0011(11) 0.0083(11) -0.0018(11) C8 0.0297(15) 0.0191(16) 0.0218(13) 0.0048(12) 0.0073(11) -0.0012(13) C9 0.0326(15) 0.0225(17) 0.0205(12) 0.0009(11) 0.0101(11) -0.0026(13) C10 0.0282(15) 0.0160(15) 0.0248(13) -0.0016(11) 0.0112(11) -0.0008(12) C11 0.0273(14) 0.0207(16) 0.0204(12) 0.0039(11) 0.0092(11) -0.0042(12) C12 0.0312(15) 0.0280(18) 0.0291(14) 0.0023(13) 0.0107(12) 0.0037(14) C13 0.0239(13) 0.0105(14) 0.0223(12) 0.0027(11) 0.0075(10) 0.0037(12) C14 0.0331(16) 0.0206(17) 0.0248(13) 0.0044(12) 0.0083(11) -0.0026(13) C15 0.0318(16) 0.0259(18) 0.0415(17) 0.0074(14) 0.0026(13) -0.0081(13) C16 0.0277(16) 0.0298(19) 0.0561(19) 0.0207(16) 0.0186(14) 0.0014(14) C17 0.0393(17) 0.0269(17) 0.0386(15) 0.0146(14) 0.0245(14) 0.0123(15) C18 0.0332(15) 0.0156(14) 0.0245(13) 0.0046(12) 0.0136(11) 0.0068(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 O1 H1O 109.5 . . ? O1 C1 C2 109.25(19) . . ? O1 C1 C13 112.2(2) . . ? C2 C1 C13 109.9(2) . . ? O1 C1 H1 108.5 . . ? C2 C1 H1 108.5 . . ? C13 C1 H1 108.5 . . ? O3 C2 N4 124.5(2) . . ? O3 C2 C1 119.7(2) . . ? N4 C2 C1 115.8(2) . . ? C2 N4 C5 129.0(2) . . ? C2 N4 H4 115.9(19) . . ? C5 N4 H4 115.1(19) . . ? C10 C5 C6 119.6(2) . . ? C10 C5 N4 117.5(2) . . ? C6 C5 N4 122.8(2) . . ? C7 C6 C5 119.5(2) . . ? C7 C6 H6 120.2 . . ? C5 C6 H6 120.2 . . ? C8 C7 C6 120.8(2) . . ? C8 C7 C11 120.0(2) . . ? C6 C7 C11 119.3(2) . . ? C9 C8 C7 119.0(2) . . ? C9 C8 H8 120.5 . . ? C7 C8 H8 120.5 . . ? C10 C9 C8 120.8(2) . . ? C10 C9 H9 119.6 . . ? C8 C9 H9 119.6 . . ? C9 C10 C5 120.2(3) . . ? C9 C10 H10 119.9 . . ? C5 C10 H10 119.9 . . ? C12 C11 C7 179.7(3) . . ? C11 C12 H12 180 . . ? C18 C13 C14 118.9(2) . . ? C18 C13 C1 120.8(2) . . ? C14 C13 C1 120.3(2) . . ? C15 C14 C13 120.1(3) . . ? C15 C14 H14 119.9 . . ? C13 C14 H14 119.9 . . ? C16 C15 C14 121.0(3) . . ? C16 C15 H15 119.5 . . ? C14 C15 H15 119.5 . . ? C15 C16 C17 119.3(3) . . ? C15 C16 H16 120.3 . . ? C17 C16 H16 120.3 . . ? C16 C17 C18 120.0(3) . . ? C16 C17 H17 120 . . ? C18 C17 H17 120 . . ? C13 C18 C17 120.7(3) . . ? C13 C18 H18 119.7 . . ? C17 C18 H18 119.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.432(3) . ? O1 H1O 0.93(3) . ? C1 C2 1.514(4) . ? C1 C13 1.516(4) . ? C1 H1 1 . ? C2 O3 1.242(3) . ? C2 N4 1.346(3) . ? N4 C5 1.414(3) . ? N4 H4 0.90(3) . ? C5 C10 1.395(3) . ? C5 C6 1.395(4) . ? C6 C7 1.393(3) . ? C6 H6 0.95 . ? C7 C8 1.392(3) . ? C7 C11 1.452(4) . ? C8 C9 1.390(4) . ? C8 H8 0.95 . ? C9 C10 1.379(3) . ? C9 H9 0.95 . ? C10 H10 0.95 . ? C11 C12 1.172(4) . ? C12 H12 0.95 . ? C13 C18 1.387(3) . ? C13 C14 1.394(4) . ? C14 C15 1.383(4) . ? C14 H14 0.95 . ? C15 C16 1.378(4) . ? C15 H15 0.95 . ? C16 C17 1.386(4) . ? C16 H16 0.95 . ? C17 C18 1.391(4) . ? C17 H17 0.95 . ? C18 H18 0.95 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1 H1O O3 0.93 1.9 2.746(2) 151.4 2_655 N4 H4 O1 0.90(3) 2.10(3) 2.580(3) 112(2) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 O3 173.8(2) . . . . ? C13 C1 C2 O3 -62.7(3) . . . . ? O1 C1 C2 N4 -6.5(3) . . . . ? C13 C1 C2 N4 116.9(2) . . . . ? O3 C2 N4 C5 -2.4(4) . . . . ? C1 C2 N4 C5 178.0(2) . . . . ? C2 N4 C5 C10 167.5(2) . . . . ? C2 N4 C5 C6 -13.2(4) . . . . ? C10 C5 C6 C7 -0.7(4) . . . . ? N4 C5 C6 C7 -180.0(2) . . . . ? C5 C6 C7 C8 0.4(4) . . . . ? C5 C6 C7 C11 -179.8(2) . . . . ? C6 C7 C8 C9 0.2(4) . . . . ? C11 C7 C8 C9 -179.6(2) . . . . ? C7 C8 C9 C10 -0.4(4) . . . . ? C8 C9 C10 C5 0.1(4) . . . . ? C6 C5 C10 C9 0.5(4) . . . . ? N4 C5 C10 C9 179.7(2) . . . . ? O1 C1 C13 C18 -124.7(2) . . . . ? C2 C1 C13 C18 113.6(3) . . . . ? O1 C1 C13 C14 54.3(3) . . . . ? C2 C1 C13 C14 -67.5(3) . . . . ? C18 C13 C14 C15 -0.6(4) . . . . ? C1 C13 C14 C15 -179.5(2) . . . . ? C13 C14 C15 C16 -0.1(4) . . . . ? C14 C15 C16 C17 0.0(4) . . . . ? C15 C16 C17 C18 0.7(4) . . . . ? C14 C13 C18 C17 1.3(4) . . . . ? C1 C13 C18 C17 -179.7(2) . . . . ? C16 C17 C18 C13 -1.3(4) . . . . ?