#------------------------------------------------------------------------------ #$Date: 2020-04-17 00:22:41 +0300 (Fri, 17 Apr 2020) $ #$Revision: 250865 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/78/1557810.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557810 loop_ _publ_author_name 'Anstis, Daniel G.' 'Lindsay, Ashley C.' 'S\"ohnel, Tilo' 'Sperry, Jonathan' _publ_section_title ; Synthesis of the 1,2,4-Thiadiazole Alkaloid Polyaurine B ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.0c00166 _journal_year 2020 _chemical_formula_moiety 'C12 H15 N3 O4' _chemical_formula_sum 'C12 H15 N3 O4' _chemical_formula_weight 265.27 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_date 2020-02-05 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3510 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 99.673(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.63730(10) _cell_length_b 13.1251(2) _cell_length_c 14.4267(2) _cell_measurement_reflns_used 8386 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 73.8210 _cell_measurement_theta_min 6.2020 _cell_volume 1238.92(3) _computing_cell_refinement 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.8140 _diffrn_detector_type 'Pilatus 200K' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.980 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -64.00 14.00 0.50 0.50 -- -47.48 38.00 120.00 156 2 \w -50.00 -25.00 0.50 2.00 -- -90.25 118.00 149.00 50 3 \w -70.00 -45.00 0.50 0.50 -- -47.48 118.00 149.00 50 4 \w -95.00 -70.00 0.50 0.50 -- -47.48 160.00 -58.00 50 5 \w 78.00 103.00 0.50 0.50 -- 47.48 160.00 -58.00 50 6 \w 103.00 129.00 0.50 2.00 -- 101.53 160.00 -58.00 52 7 \w 115.00 149.00 0.50 2.00 -- 101.53 178.00 0.00 68 8 \w 120.00 174.00 0.50 2.00 -- 101.53 118.00 149.00 108 9 \w 82.00 154.00 0.50 2.00 -- 101.53 30.00 90.00 144 10 \w 69.00 105.00 0.50 2.00 -- 101.53 -45.00 30.00 72 11 \w 60.00 89.00 0.50 0.50 -- 47.48-118.00 62.00 58 12 \w 87.00 114.00 0.50 2.00 -- 101.53-118.00 62.00 54 13 \w 82.00 111.00 0.50 2.00 -- 101.53-111.00 150.00 58 14 \w 36.00 63.00 0.50 2.00 -- 101.53 -45.00 30.00 54 15 \w 25.00 109.00 0.50 2.00 -- 101.53 -95.00 60.00 168 16 \w 61.00 86.00 0.50 0.50 -- 47.48-160.00 -89.00 50 17 \w 97.00 129.00 0.50 2.00 -- 101.53-160.00 -89.00 64 18 \w 29.00 106.00 0.50 2.00 -- 101.53 -61.00 -90.00 154 19 \w 73.00 157.00 0.50 2.00 -- 101.53 15.00-150.00 168 20 \w 130.00 173.00 0.50 2.00 -- 101.53 61.00-120.00 86 21 \w 108.00 161.00 0.50 2.00 -- 101.53 111.00-150.00 106 22 \w 84.00 110.00 0.50 0.50 -- 47.48 77.00-150.00 52 23 \w 80.00 121.00 0.50 2.00 -- 101.53 61.00-120.00 82 24 \w 59.00 133.00 0.50 2.00 -- 101.53 178.00-120.00 148 25 \w 61.00 87.00 0.50 2.00 -- 101.53 178.00 0.00 52 26 \w 23.00 60.00 0.50 0.50 -- 47.48 77.00-150.00 74 27 \w -73.00 -37.00 0.50 0.50 -- -47.48 -57.00 90.00 72 28 \w -120.00 -78.00 0.50 0.50 -- -47.48-118.00 62.00 84 29 \w -123.00 -86.00 0.50 0.50 -- -47.48-125.00 90.00 74 30 \w -146.00 -97.00 0.50 2.00 -- -90.25-118.00 62.00 98 31 \w -159.00-133.00 0.50 2.00 -- -90.25 -77.00 -60.00 52 32 \w -130.00-105.00 0.50 2.00 -- -90.25 -77.00 -60.00 50 33 \w -120.00 -40.00 0.50 0.50 -- -47.48 -57.00 -90.00 160 34 \w -110.00 -85.00 0.50 0.50 -- -47.48-160.00 -89.00 50 35 \w -90.00 -46.00 0.50 2.00 -- -90.25-160.00 -89.00 88 36 \w -123.00 -73.00 0.50 0.50 -- -47.48-125.00-180.00 100 37 \w -144.00 -82.00 0.50 2.00 -- -90.25 -95.00-180.00 124 38 \w -164.00 -75.00 0.50 2.00 -- -90.25 -45.00-120.00 178 39 \w -168.00-125.00 0.50 2.00 -- -90.25-111.00 90.00 86 40 \w -87.00 -62.00 0.50 2.00 -- -90.25 111.00 -60.00 50 41 \w -48.00 -22.00 0.50 2.00 -- -90.25 111.00 -60.00 52 42 \w -95.00 -70.00 0.50 2.00 -- -90.25 160.00 -58.00 50 43 \w 28.00 53.00 0.50 2.00 -- 101.53-111.00 150.00 50 44 \w 36.00 109.00 0.50 2.00 -- 101.53-111.00 -60.00 146 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 200K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1392978000 _diffrn_orient_matrix_UB_12 0.0322841000 _diffrn_orient_matrix_UB_13 -0.0701631000 _diffrn_orient_matrix_UB_21 0.0124818000 _diffrn_orient_matrix_UB_22 -0.1116901000 _diffrn_orient_matrix_UB_23 -0.0314331000 _diffrn_orient_matrix_UB_31 -0.1893965000 _diffrn_orient_matrix_UB_32 0.0163718000 _diffrn_orient_matrix_UB_33 -0.0762747000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0364 _diffrn_reflns_av_unetI/netI 0.0240 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.980 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 15882 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.980 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.392 _diffrn_reflns_theta_min 4.584 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.912 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.97504 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 1.422 _exptl_crystal_description plate _exptl_crystal_F_000 560 _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.248 _refine_diff_density_min -0.179 _refine_diff_density_rms 0.041 _refine_ls_extinction_coef 0.0008(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 184 _refine_ls_number_reflns 2487 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.041 _refine_ls_R_factor_all 0.0373 _refine_ls_R_factor_gt 0.0323 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0445P)^2^+0.3827P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0856 _refine_ls_wR_factor_ref 0.0889 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2190 _reflns_number_total 2487 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL dap6_3_a.res in P2(1)/c dap6_3.res created by SHELXL-2016/6 at 12:03:36 on 05-Feb-2020 REM colourless irregular CELL 1.54184 6.6373 13.1251 14.4267 90 99.673 90 ZERR 4 0.0001 0.0002 0.0002 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O UNIT 48 60 12 16 L.S. 10 PLAN 5 SIZE 0.14 0.12 0.1 TEMP 100 MORE -1 BOND $H CONF fmap 2 acta MERG 2 OMIT 0 2 0 REM REM REM WGHT 0.044500 0.382700 EXTI 0.000801 FVAR 3.33085 C1 1 1.612883 0.532961 0.891414 11.00000 0.01977 0.02228 = 0.02740 -0.00129 0.00040 -0.00163 AFIX 137 H1A 2 1.613352 0.551657 0.827118 11.00000 -1.50000 H1B 2 1.750522 0.532541 0.925102 11.00000 -1.50000 H1C 2 1.533285 0.581339 0.919722 11.00000 -1.50000 AFIX 0 C2 1 1.330349 0.419875 0.848931 11.00000 0.01787 0.02111 = 0.01997 -0.00182 0.00313 0.00098 C3 1 1.251922 0.321515 0.853645 11.00000 0.02275 0.01875 = 0.02562 0.00252 0.00273 0.00453 AFIX 43 H3 2 1.331853 0.271064 0.886931 11.00000 -1.20000 AFIX 0 C4 1 1.056307 0.298950 0.809097 11.00000 0.02315 0.01688 = 0.02453 -0.00025 0.00480 -0.00021 AFIX 43 H4 2 1.006058 0.233089 0.811993 11.00000 -1.20000 AFIX 0 C5 1 1.210590 0.495739 0.799801 11.00000 0.02139 0.01681 = 0.02180 -0.00037 0.00459 -0.00098 AFIX 43 H5 2 1.261678 0.561370 0.796435 11.00000 -1.20000 AFIX 0 C6 1 1.013410 0.471984 0.755811 11.00000 0.02037 0.01737 = 0.02134 0.00143 0.00350 0.00176 AFIX 43 H6 2 0.933159 0.522626 0.722996 11.00000 -1.20000 AFIX 0 C7 1 0.932767 0.374200 0.759595 11.00000 0.01951 0.01828 = 0.01919 -0.00107 0.00487 0.00062 C8 1 0.720577 0.348898 0.712865 11.00000 0.02192 0.01727 = 0.01932 -0.00133 0.00599 -0.00014 C9 1 0.428717 0.421279 0.622149 11.00000 0.02028 0.01823 = 0.01819 -0.00130 0.00503 -0.00197 C10 1 0.431475 0.603213 0.592366 11.00000 0.02336 0.01779 = 0.02614 0.00088 0.00089 -0.00210 AFIX 137 H10A 2 0.407636 0.633334 0.650191 11.00000 -1.50000 H10B 2 0.373599 0.645816 0.540598 11.00000 -1.50000 H10C 2 0.575886 0.596570 0.593436 11.00000 -1.50000 AFIX 0 C11 1 0.133474 0.310841 0.564512 11.00000 0.02116 0.01889 = 0.02063 -0.00211 0.00420 -0.00209 C12 1 -0.112969 0.181097 0.529564 11.00000 0.02112 0.02121 = 0.02933 -0.00140 0.00160 -0.00573 AFIX 137 H12A 2 -0.216477 0.214866 0.557346 11.00000 -1.50000 H12B 2 -0.125781 0.108722 0.536235 11.00000 -1.50000 H12C 2 -0.129175 0.198229 0.464038 11.00000 -1.50000 AFIX 0 N1 3 0.616447 0.430317 0.670302 11.00000 0.01841 0.01823 = 0.02090 -0.00035 0.00200 -0.00124 N2 3 0.336560 0.503177 0.581578 11.00000 0.01908 0.01838 = 0.02270 0.00076 -0.00070 -0.00199 N3 3 0.327247 0.328931 0.612063 11.00000 0.02001 0.01720 = 0.02372 0.00117 0.00055 -0.00133 O1 4 1.525534 0.433448 0.894847 11.00000 0.01929 0.02119 = 0.02806 0.00115 -0.00099 0.00009 O2 4 0.657038 0.259406 0.715885 11.00000 0.02291 0.01663 = 0.03169 0.00088 0.00145 -0.00235 O3 4 0.023406 0.372288 0.518042 11.00000 0.02225 0.02000 = 0.02946 0.00147 -0.00210 -0.00156 O4 4 0.086790 0.213464 0.576403 11.00000 0.02157 0.01759 = 0.02954 0.00024 -0.00062 -0.00399 H2 2 0.211209 0.497106 0.551401 11.00000 0.03200 H3A 2 0.395560 0.279575 0.643444 11.00000 0.02986 HKLF 4 REM dap6_3_a.res in P2(1)/c REM R1 = 0.0323 for 2190 Fo > 4sig(Fo) and 0.0373 for all 2487 data REM 184 parameters refined using 0 restraints END WGHT 0.0445 0.3826 REM Highest difference peak 0.248, deepest hole -0.179, 1-sigma level 0.041 Q1 1 0.9964 0.3371 0.7773 11.00000 0.05 0.25 Q2 1 0.9637 0.4168 0.7625 11.00000 0.05 0.24 Q3 1 0.8415 0.3618 0.7316 11.00000 0.05 0.22 Q4 1 1.2575 0.4604 0.8397 11.00000 0.05 0.21 Q5 1 1.1580 0.3198 0.8299 11.00000 0.05 0.20 REM The information below was added by Olex2. REM REM R1 = 0.0323 for 2190 Fo > 4sig(Fo) and 0.0373 for all 16347 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.25, deepest hole -0.18 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0373 REM R1_gt = 0.0323 REM wR_ref = 0.0889 REM GOOF = 1.041 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 16347 REM Reflections_gt = 2190 REM Parameters = n/a REM Hole = -0.18 REM Peak = 0.25 REM Flack = n/a ; _cod_data_source_file np0c00166_si_002.cif _cod_data_source_block dap6_3 _cod_database_code 1557810 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula C12H15N3O4 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.914 _shelx_estimated_absorpt_t_min 0.883 _diffrn_oxdiff_digest_frames ; 01b650aea8e520ae187e48b7c4df075a2c000478f59 ; _diffrn_oxdiff_digest_hkl ; 010e4b780b7035a148ecd538caa25d5d8d2e9c ; _reflns_odcompleteness_completeness 100.00 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 68.13 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C5(H5), C6(H6) 2.b Idealised Me refined as rotating group: C1(H1A,H1B,H1C), C10(H10A,H10B,H10C), C12(H12A,H12B,H12C) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.402 _oxdiff_exptl_absorpt_empirical_full_min 0.839 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 1.61288(18) 0.53296(9) 0.89141(9) 0.0236(3) Uani 1 1 d . . . . . H1A H 1.613352 0.551657 0.827118 0.035 Uiso 1 1 calc GR . . . . H1B H 1.750522 0.532541 0.925102 0.035 Uiso 1 1 calc GR . . . . H1C H 1.533285 0.581339 0.919722 0.035 Uiso 1 1 calc GR . . . . C2 C 1.33035(17) 0.41988(9) 0.84893(8) 0.0197(2) Uani 1 1 d . . . . . C3 C 1.25192(19) 0.32151(9) 0.85365(9) 0.0225(3) Uani 1 1 d . . . . . H3 H 1.331853 0.271064 0.886931 0.027 Uiso 1 1 calc R . . . . C4 C 1.05631(18) 0.29895(9) 0.80910(8) 0.0214(3) Uani 1 1 d . . . . . H4 H 1.006058 0.233089 0.811993 0.026 Uiso 1 1 calc R . . . . C5 C 1.21059(17) 0.49574(9) 0.79980(8) 0.0199(2) Uani 1 1 d . . . . . H5 H 1.261678 0.561370 0.796435 0.024 Uiso 1 1 calc R . . . . C6 C 1.01341(17) 0.47198(9) 0.75581(8) 0.0197(2) Uani 1 1 d . . . . . H6 H 0.933159 0.522626 0.722996 0.024 Uiso 1 1 calc R . . . . C7 C 0.93277(17) 0.37420(9) 0.75959(8) 0.0188(2) Uani 1 1 d . . . . . C8 C 0.72058(17) 0.34890(9) 0.71287(8) 0.0192(2) Uani 1 1 d . . . . . C9 C 0.42872(17) 0.42128(9) 0.62215(8) 0.0187(2) Uani 1 1 d . . . . . C10 C 0.43147(18) 0.60321(9) 0.59237(9) 0.0228(3) Uani 1 1 d . . . . . H10A H 0.407636 0.633334 0.650191 0.034 Uiso 1 1 calc GR . . . . H10B H 0.373599 0.645816 0.540598 0.034 Uiso 1 1 calc GR . . . . H10C H 0.575886 0.596570 0.593436 0.034 Uiso 1 1 calc GR . . . . C11 C 0.13347(18) 0.31084(9) 0.56451(8) 0.0201(2) Uani 1 1 d . . . . . C12 C -0.11297(18) 0.18110(9) 0.52956(9) 0.0242(3) Uani 1 1 d . . . . . H12A H -0.216477 0.214866 0.557346 0.036 Uiso 1 1 calc GR . . . . H12B H -0.125781 0.108722 0.536235 0.036 Uiso 1 1 calc GR . . . . H12C H -0.129175 0.198229 0.464038 0.036 Uiso 1 1 calc GR . . . . N1 N 0.61645(15) 0.43032(7) 0.67030(7) 0.0193(2) Uani 1 1 d . . . . . N2 N 0.33656(16) 0.50318(7) 0.58158(7) 0.0205(2) Uani 1 1 d . . . . . N3 N 0.32725(15) 0.32893(8) 0.61206(7) 0.0207(2) Uani 1 1 d . . . . . O1 O 1.52553(12) 0.43345(6) 0.89485(6) 0.0234(2) Uani 1 1 d . . . . . O2 O 0.65704(13) 0.25941(6) 0.71589(6) 0.0241(2) Uani 1 1 d . . . . . O3 O 0.02341(13) 0.37229(6) 0.51804(6) 0.0246(2) Uani 1 1 d . . . . . O4 O 0.08679(12) 0.21346(6) 0.57640(6) 0.0235(2) Uani 1 1 d . . . . . H2 H 0.211(3) 0.4971(12) 0.5514(11) 0.032(4) Uiso 1 1 d . . . . . H3A H 0.396(2) 0.2796(13) 0.6434(11) 0.030(4) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0198(6) 0.0223(6) 0.0274(6) -0.0013(5) 0.0004(5) -0.0016(5) C2 0.0179(5) 0.0211(6) 0.0200(5) -0.0018(4) 0.0031(4) 0.0010(4) C3 0.0227(6) 0.0187(6) 0.0256(6) 0.0025(4) 0.0027(5) 0.0045(5) C4 0.0232(6) 0.0169(5) 0.0245(6) -0.0003(5) 0.0048(5) -0.0002(4) C5 0.0214(6) 0.0168(5) 0.0218(6) -0.0004(4) 0.0046(4) -0.0010(4) C6 0.0204(6) 0.0174(6) 0.0213(6) 0.0014(4) 0.0035(4) 0.0018(4) C7 0.0195(5) 0.0183(6) 0.0192(5) -0.0011(4) 0.0049(4) 0.0006(4) C8 0.0219(6) 0.0173(5) 0.0193(5) -0.0013(4) 0.0060(4) -0.0001(4) C9 0.0203(5) 0.0182(5) 0.0182(5) -0.0013(4) 0.0050(4) -0.0020(4) C10 0.0234(6) 0.0178(6) 0.0261(6) 0.0009(5) 0.0009(5) -0.0021(5) C11 0.0212(6) 0.0189(6) 0.0206(6) -0.0021(4) 0.0042(4) -0.0021(5) C12 0.0211(6) 0.0212(6) 0.0293(6) -0.0014(5) 0.0016(5) -0.0057(5) N1 0.0184(5) 0.0182(5) 0.0209(5) -0.0003(4) 0.0020(4) -0.0012(4) N2 0.0191(5) 0.0184(5) 0.0227(5) 0.0008(4) -0.0007(4) -0.0020(4) N3 0.0200(5) 0.0172(5) 0.0237(5) 0.0012(4) 0.0006(4) -0.0013(4) O1 0.0193(4) 0.0212(4) 0.0281(4) 0.0012(3) -0.0010(3) 0.0001(3) O2 0.0229(4) 0.0166(4) 0.0317(5) 0.0009(3) 0.0014(3) -0.0023(3) O3 0.0222(4) 0.0200(4) 0.0295(5) 0.0015(3) -0.0021(3) -0.0016(3) O4 0.0216(4) 0.0176(4) 0.0295(5) 0.0002(3) -0.0006(3) -0.0040(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? O1 C1 H1A 109.5 . . ? O1 C1 H1B 109.5 . . ? O1 C1 H1C 109.5 . . ? C5 C2 C3 120.01(11) . . ? O1 C2 C3 115.34(10) . . ? O1 C2 C5 124.65(11) . . ? C2 C3 H3 119.9 . . ? C4 C3 C2 120.28(11) . . ? C4 C3 H3 119.9 . . ? C3 C4 H4 119.7 . . ? C3 C4 C7 120.69(11) . . ? C7 C4 H4 119.7 . . ? C2 C5 H5 120.5 . . ? C6 C5 C2 119.03(11) . . ? C6 C5 H5 120.5 . . ? C5 C6 H6 119.1 . . ? C5 C6 C7 121.75(11) . . ? C7 C6 H6 119.1 . . ? C4 C7 C8 120.03(10) . . ? C6 C7 C4 118.24(11) . . ? C6 C7 C8 121.73(10) . . ? N1 C8 C7 113.44(10) . . ? O2 C8 C7 119.40(10) . . ? O2 C8 N1 127.15(11) . . ? N1 C9 N3 122.13(10) . . ? N2 C9 N1 118.87(10) . . ? N2 C9 N3 119.00(10) . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? N2 C10 H10A 109.5 . . ? N2 C10 H10B 109.5 . . ? N2 C10 H10C 109.5 . . ? O3 C11 N3 126.04(11) . . ? O3 C11 O4 125.29(11) . . ? O4 C11 N3 108.67(10) . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? O4 C12 H12A 109.5 . . ? O4 C12 H12B 109.5 . . ? O4 C12 H12C 109.5 . . ? C9 N1 C8 121.81(10) . . ? C9 N2 C10 121.77(10) . . ? C9 N2 H2 118.4(11) . . ? C10 N2 H2 119.6(11) . . ? C9 N3 H3A 113.3(10) . . ? C11 N3 C9 127.10(10) . . ? C11 N3 H3A 119.5(10) . . ? C2 O1 C1 117.32(9) . . ? C11 O4 C12 115.85(9) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 H1A 0.9600 . ? C1 H1B 0.9600 . ? C1 H1C 0.9600 . ? C1 O1 1.4332(14) . ? C2 C3 1.3979(17) . ? C2 C5 1.3915(16) . ? C2 O1 1.3640(14) . ? C3 H3 0.9300 . ? C3 C4 1.3806(17) . ? C4 H4 0.9300 . ? C4 C7 1.4004(16) . ? C5 H5 0.9300 . ? C5 C6 1.3906(16) . ? C6 H6 0.9300 . ? C6 C7 1.3952(16) . ? C7 C8 1.4931(16) . ? C8 N1 1.3616(15) . ? C8 O2 1.2512(14) . ? C9 N1 1.3260(15) . ? C9 N2 1.3236(15) . ? C9 N3 1.3824(15) . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C10 N2 1.4533(15) . ? C11 N3 1.3728(15) . ? C11 O3 1.2120(15) . ? C11 O4 1.3330(14) . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? C12 O4 1.4470(14) . ? N2 H2 0.875(17) . ? N3 H3A 0.872(17) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 C3 C4 C7 -0.78(18) . . . . ? C2 C5 C6 C7 -0.05(17) . . . . ? C3 C2 C5 C6 -0.09(17) . . . . ? C3 C2 O1 C1 179.60(10) . . . . ? C3 C4 C7 C6 0.62(17) . . . . ? C3 C4 C7 C8 -179.19(10) . . . . ? C4 C7 C8 N1 177.83(10) . . . . ? C4 C7 C8 O2 -2.26(17) . . . . ? C5 C2 C3 C4 0.50(18) . . . . ? C5 C2 O1 C1 -0.42(17) . . . . ? C5 C6 C7 C4 -0.21(17) . . . . ? C5 C6 C7 C8 179.60(10) . . . . ? C6 C7 C8 N1 -1.98(16) . . . . ? C6 C7 C8 O2 177.94(11) . . . . ? C7 C8 N1 C9 177.30(10) . . . . ? N1 C9 N2 C10 -3.13(16) . . . . ? N1 C9 N3 C11 179.62(11) . . . . ? N2 C9 N1 C8 -179.29(10) . . . . ? N2 C9 N3 C11 -1.16(18) . . . . ? N3 C9 N1 C8 -0.07(17) . . . . ? N3 C9 N2 C10 177.62(11) . . . . ? N3 C11 O4 C12 -179.29(9) . . . . ? O1 C2 C3 C4 -179.52(10) . . . . ? O1 C2 C5 C6 179.94(10) . . . . ? O2 C8 N1 C9 -2.61(19) . . . . ? O3 C11 N3 C9 5.1(2) . . . . ? O3 C11 O4 C12 -0.37(17) . . . . ? O4 C11 N3 C9 -175.99(10) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 0 0 -1 6.15132 9.46755 22 0 0 -1 2.41715 12.2451 1 0 0 -1 -5.56186 8.43568 36 0 0 -2 5704.1 216.705 22 0 0 -2 5659.01 214.737 36 0 0 2 5579.61 211.758 27 0 0 -2 5860.16 223.675 1 0 0 -3 -3.71209 35.0664 1 0 0 -4 20114.3 754.386 1 0 0 -5 -6.59346 47.0835 1 0 0 -6 28070.9 1063.14 1 0 0 -7 -2.70786 25.1922 35 0 0 -7 10.1178 50.4115 1 0 0 -8 90.9293 33.2447 35 0 0 -8 200.368 73.4092 34 0 0 -8 170.516 59.2132 1 0 0 -8 154.886 31.642 38 0 0 -9 7.2422 26.3685 38 0 0 -9 -5.00211 35.2502 18 0 0 -9 -14.8698 63.2918 34 0 0 -9 49.8651 30.1411 35 0 0 -9 3.95976 34.1764 44 0 0 -9 57.6237 60.1712 1 0 0 -10 6213.87 354.305 1 0 0 -10 6164.4 263.763 44 0 0 -10 6488.44 262.823 38 0 0 -10 6447.35 363.02 34 0 0 -10 6169.63 261.874 8 0 0 -10 6571.69 277.807 18 0 0 -11 -39.4215 64.5816 34 0 0 -11 39.7401 47.9151 18 0 0 -11 -32.4157 38.0689 15 0 0 -11 19.1295 36.1163 8 0 0 -11 -13.8987 33.73 38 0 0 -12 108.083 77.4504 34 0 0 -12 181.733 59.8934 18 0 0 -12 140.31 47.12 15 0 0 -12 239.679 50.0079 8 0 0 -12 207.24 44.9262 38 0 0 -13 135.049 86.4761 34 0 0 -13 -5.39331 38.0031 8 0 0 -13 -29.9554 44.7085 15 0 0 -13 37.9487 52.3844 18 0 0 -13 10.933 40.794 42 0 0 -14 73.2059 42.295 8 0 0 -14 74.2222 43.4773 15 0 0 -14 132.385 57.55 18 0 0 -14 89.8955 42.1064 42 0 0 -15 41.9622 39.17 8 0 0 -15 54.6025 38.8231 15 0 0 -15 47.1297 37.8618 42 0 0 -16 179.739 37.4904 15 0 0 -16 218.735 41.4895 8 0 0 -16 220.514 39.9182 42 0 0 -17 28.4788 21.7575 15 0 0 -17 29.4203 25.3802 8 0 -1 0 1.5299 14.0108 33 0 1 0 1.23706 11.9895 27 0 -1 -1 4502.12 178.794 33 0 1 -1 4577.26 176.191 36 0 1 -2 20129.4 702.822 36 0 -1 -2 17888.5 704.395 22 0 -1 -2 20006.8 710.737 33 0 1 2 20257.4 704.911 27 0 1 -2 19610.9 704.67 1 0 -1 -2 18379.5 706.445 1 0 1 -3 10915.4 423.614 36 0 1 3 11479 426.647 27 0 -1 -3 11361.2 429.782 22 0 -1 -3 11729.5 434.738 1 0 1 -3 10678.7 430.195 1 0 1 -4 21672.2 822.096 36 0 -1 -4 22754.7 828.919 22 0 -1 -4 22850.8 836.94 1 0 1 -4 22353 833.752 1 0 -1 -5 388.016 59.2578 1 0 1 -5 363.549 61.8535 1 0 1 -5 346.521 47.9472 36 0 -1 -6 22535.5 892.582 1 0 1 -6 23780.8 892.343 1 0 -1 -7 62.7437 56.8224 1 0 1 -7 -10.0631 48.7696 1 0 1 -7 30.0485 25.7163 38 0 1 -7 5.42596 25.1507 35 0 -1 -7 -2.71581 25.3727 35 0 -1 -7 57.7476 31.2116 31 0 1 -8 2557.21 123.72 35 0 -1 -8 2921.1 126.838 35 0 -1 -8 2685.25 122.365 38 0 1 -8 2455.16 121.499 38 0 -1 -8 2749.85 188.433 34 0 1 -8 2457.55 182.829 34 0 -1 -8 2620.06 129.064 31 0 1 -8 2733.48 118.135 41 0 -1 -8 2445.33 180.524 1 0 1 -8 2863.32 185.985 1 0 -1 -9 450.505 46.6543 38 0 -1 -9 491.718 50.3704 35 0 1 -9 529.446 51.301 38 0 -1 -9 513.695 59.415 18 0 1 -9 424.646 54.759 18 0 -1 -9 685.267 99.9883 34 0 1 -9 595.119 96.844 34 0 1 -9 479.793 48.0221 35 0 1 -9 534.558 43.5798 41 0 1 -9 563.997 53.178 44 0 1 -9 641.954 95.1737 1 0 -1 -9 503.239 87.5705 1 0 -1 -10 2005.37 176.666 1 0 1 -10 2064.77 102.139 41 0 1 -10 1938.06 110.994 44 0 -1 -10 2094.99 109.63 38 0 1 -10 2000.72 110.8 38 0 -1 -10 1942.38 180.099 34 0 1 -10 1922.85 177.107 34 0 -1 -10 2242.29 112.687 8 0 1 -10 1972.31 109.303 8 0 -1 -10 2151.67 124.665 18 0 1 -10 2143.55 124.836 18 0 1 -11 1294.07 98.716 18 0 -1 -11 1306.64 101.866 18 0 1 -11 1328.46 87.5992 38 0 -1 -11 1219.88 83.271 38 0 1 -11 1239.56 88.3597 15 0 -1 -11 1319.47 94.7571 15 0 -1 -11 1122.36 145.094 34 0 1 -11 1317.98 150.244 34 0 -1 -11 1658.51 165.875 1 0 -1 -11 1318.42 90.393 8 0 1 -11 1333.42 88.2834 8 0 1 -12 -107.649 72.7138 34 0 -1 -12 -86.1844 70.5961 34 0 -1 -12 -6.07138 41.3124 15 0 1 -12 -33.3919 38.6838 15 0 -1 -12 102.514 54.3151 18 0 1 -12 -29.0664 50.1557 18 0 -1 -12 -20.8834 68.4248 1 0 -1 -12 25.9633 39.6753 8 0 1 -12 -20.7848 38.0718 8 0 -1 -12 19.0316 33.9784 38 0 1 -13 491.946 113.475 34 0 -1 -13 402.697 107.451 34 0 1 -13 265.919 53.0595 42 0 -1 -13 315.106 53.3011 42 0 1 -13 385.004 69.5054 18 0 -1 -13 366.978 61.3349 15 0 -1 -13 318.297 70.3191 18 0 1 -13 322.579 54.0504 15 0 1 -13 284.537 51.3991 8 0 -1 -13 316.452 52.0995 8 0 -1 -13 259.202 92.6286 4 0 1 -13 366.758 100.603 4 0 1 -14 78.4886 43.7205 42 0 -1 -14 15.7117 36.916 42 0 1 -14 26.694 34.7241 15 0 1 -14 58.6911 59.1932 18 0 -1 -14 -5.94284 40.1534 15 0 1 -14 62.1571 41.3655 8 0 -1 -14 -10.3462 40.2112 8 0 -1 -15 185.961 41.6034 42 0 1 -15 144.016 39.0597 42 0 -1 -15 171.413 45.0052 15 0 1 -15 188.962 53.4259 18 0 1 -15 200.385 43.5764 15 0 1 -15 147.245 41.8699 8 0 -1 -15 142.396 44.1056 8 0 1 -16 134.233 33.7951 42 0 -1 -16 164.175 35.8294 42 0 -1 -16 162.702 39.4061 15 0 1 -16 178.511 35.1376 15 0 1 -16 137.05 35.9608 8 0 -1 -16 203.237 39.5223 8 0 -1 -17 74.8288 25.7543 15 0 1 -17 85.9126 25.0051 8 0 -1 -17 62.2542 25.2747 8 0 -2 0 2582.5 121.893 33 0 -2 0 2603.36 110.863 22 0 2 0 2661.96 116.217 27 0 -2 -1 143534 4918.81 33 0 2 -1 141091 4903.35 27 0 2 1 136439 4917.73 27 0 -2 1 138366 4894.98 22 0 -2 -2 3220.41 146.349 33 0 2 -2 2828.68 113.252 27 0 2 -2 3010.47 138.304 36 0 -2 -3 4743.34 218.24 33 0 -2 -3 4915.36 214.21 1 0 2 3 4491.29 211.335 27 0 2 -3 4830.34 208.212 36 0 2 -4 14958.9 592 36 0 -2 -4 15248.3 599.971 22 0 -2 -4 16079 610.795 33 0 -2 -4 16195.5 604.572 1 0 2 4 15417.1 596.337 27 0 -2 -5 8280.27 355.122 1 0 2 -5 7960.33 339.088 36 0 -2 -6 1504.72 120.97 1 0 2 -6 1543.11 112.805 36 0 -2 -7 499.481 85.6365 1 0 -2 -7 444.374 47.5668 31 0 2 -7 445.403 42.6432 38 0 2 -7 398.606 41.2929 35 0 -2 -7 415.847 40.5084 35 0 2 -8 5187.95 281.568 34 0 -2 -8 5101.84 215.172 31 0 -2 -8 5051.31 277.088 34 0 -2 -8 5162.48 208.192 35 0 2 -8 4937.2 207.477 35 0 -2 -8 5227.84 206.618 38 0 2 -8 4807.82 207.453 38 0 -2 -8 5316.78 286.011 1 0 2 -8 4754.17 202.245 41 0 2 -9 8009.92 313.151 41 0 2 -9 8009.74 319.702 38 0 -2 -9 7746.55 314.839 38 0 2 -9 8021.43 405.166 34 0 -2 -9 8146.78 407.552 34 0 -2 -9 8438.84 328.502 31 0 -2 -9 8115.93 410.626 1 0 -2 -9 8400.66 334.119 18 0 2 -9 7717.42 329.35 18 0 -2 -10 360.338 44.7559 38 0 -2 -10 377.185 60.9229 18 0 2 -10 446.44 49.7325 15 0 2 -10 385.036 56.3508 18 0 -2 -10 451.055 99.3884 34 0 2 -10 294.249 84.9754 34 0 2 -10 318.42 46.4833 44 0 2 -10 442.318 44.5488 41 0 -2 -10 380.214 49.6044 8 0 -2 -10 480.298 103.929 1 0 2 -10 397.45 50.2439 8 0 2 -11 538.526 52.2978 41 0 2 -11 674.153 60.3217 44 0 -2 -11 508.133 53.9718 38 0 -2 -11 549.161 106.029 34 0 2 -11 665.555 117.352 34 0 -2 -11 478.046 110.069 1 0 2 -11 527.353 56.8719 8 0 -2 -11 621.698 59.7984 8 0 -2 -11 634.943 75.8315 18 0 2 -11 560.885 59.5536 15 0 2 -11 601.479 71.2553 18 0 -2 -11 568.881 66.0227 15 0 -2 -12 2494.53 135.783 42 0 2 -12 2415.3 133.355 42 0 2 -12 2534.15 124.572 41 0 -2 -12 2378.44 141.719 15 0 2 -12 2547.21 135.372 15 0 2 -12 2712.26 223.32 4 0 -2 -12 2637.35 227.002 4 0 -2 -12 2333.07 221.032 1 0 -2 -12 2215.74 208.809 34 0 2 -12 2701.75 226.023 34 0 -2 -12 2607.89 135.678 8 0 2 -12 2426.97 133.365 8 0 -2 -12 2565.54 151.351 18 0 2 -12 2522.36 151.883 18 0 2 -13 -21.9158 69.5262 34 0 -2 -13 -109.681 82.3411 34 0 2 -13 126.656 79.2372 4 0 -2 -13 5.24615 39.1499 8 0 -2 -13 -21.1617 64.8577 4 0 2 -13 -10.5132 36.0253 8 0 -2 -13 -21.7922 71.4016 1 0 2 -13 37.1962 41.5214 42 0 -2 -13 5.32556 36.2361 42 0 2 -13 -7.51034 52.5617 18 0 -2 -13 -12.7153 46.5792 15 0 2 -13 20.8518 35.9803 15 0 -2 -14 3708.9 172.032 42 0 2 -14 3504.35 170.314 42 0 2 -14 3445.48 165.964 15 0 -2 -14 3703.4 179.705 15 0 2 -14 3351.4 167.918 8 0 -2 -14 3437.66 169.01 8 0 2 -14 3383.4 186.322 18 0 -2 -15 218.34 43.2302 42 0 2 -15 271.394 46.4275 42 0 2 -15 192.309 56.93 18 0 -2 -15 263.14 50.418 15 0 2 -15 225.2 44.795 8 0 -2 -15 259.568 47.0442 8 0 -2 -16 14.0716 28.1087 42 0 2 -16 3.51242 27.3177 42 0 -2 -16 49.5296 33.996 15 0 -2 -16 104.389 32.517 8 0 2 -16 13.9899 29.5169 8 0 -2 -17 33.0634 24.2378 15 0 2 -17 57.099 23.8238 8 0 -2 -17 23.5955 22.4113 8 0 3 0 -23.0976 39.3845 27 0 -3 0 29.2926 31.832 22 0 -3 0 -4.71107 45.0024 33 0 3 -1 2463.05 115.463 27 0 3 1 2632.03 130.694 27 0 -3 1 2285.98 101.202 22 0 -3 -1 2098.49 120.184 22 0 3 -1 2298.11 91.9371 34 0 -3 -1 2397.56 92.9721 34 0 -3 -1 2399.91 130.203 33 0 -3 -2 8877.87 356.852 33 0 3 -2 8501.84 349.461 36 0 3 -2 8539.38 325.67 27 0 -3 -3 1972.5 123.852 33 0 3 3 1686.37 114.39 27 0 3 -3 1812.82 113.116 36 0 3 -4 13793.1 550.964 36 0 -3 -4 14619.1 561.572 1 0 -3 -4 13833.5 564.177 33 0 3 4 13955 558.776 27 0 -3 -4 13896.1 559.906 22 0 -3 -5 224.17 60.2778 33 0 3 -5 224.184 51.9079 36 0 -3 -5 230.661 59.0802 1 0 3 -6 132.927 52.4619 36 0 -3 -6 121.721 54.6661 1 0 -3 -7 264.484 65.0873 34 0 -3 -7 278.725 43.5845 31 0 -3 -7 253.793 35.3537 35 0 3 -7 308.02 35.6839 35 0 3 -7 263.197 63.6202 34 0 -3 -7 265.133 71.9265 1 0 -3 -7 335.33 35.6926 38 0 3 -7 324.347 34.1699 37 0 3 -7 245.627 62.2793 36 0 3 -8 18633.4 673.046 37 0 -3 -8 18263.2 676.961 38 0 3 -8 18686.6 677.449 41 0 -3 -8 19413.6 689.181 31 0 -3 -8 18270.7 763.228 34 0 3 -8 18646.5 763.908 34 0 -3 -8 17842.8 691.591 18 0 3 -8 17634.4 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766.696 67.8602 18 0 -5 -7 998.035 99.6701 34 0 5 -7 937.073 96.6295 34 0 -5 -7 811.522 108.882 1 0 -5 -7 813.156 63.8659 19 0 5 -8 7.73323 30.8712 41 0 5 -8 10.8622 28.6022 37 0 5 -8 28.0211 57.3818 36 0 -5 -8 12.5587 47.1419 34 0 5 -8 12.4606 46.7736 34 0 -5 -8 33.6227 56.7775 1 0 -5 -8 17.0114 32.3064 19 0 -5 -8 -19.7464 29.8256 21 0 5 -9 8.59339 31.6759 41 0 5 -9 -14.347 27.2462 42 0 5 -9 139.318 33.0956 37 0 -5 -9 -15.3005 33.4213 15 0 -5 -9 -14.6178 53.5482 34 0 5 -9 14.518 51.8358 34 0 -5 -9 -17.2844 32.0518 21 0 -5 -9 -18.934 58.0301 1 0 5 -9 -14.011 48.6915 4 0 -5 -9 -3.56432 26.2769 8 0 -5 -9 -28.3251 51.8804 4 0 -5 -10 1708.12 160.834 4 0 5 -10 1976.12 169.208 4 0 -5 -10 1979.92 193.64 1 0 5 -10 1850.98 99.6199 42 0 -5 -10 1644.87 98.7308 42 0 5 -10 1773.66 104.172 41 0 5 -10 1848.8 100.5 37 0 -5 -10 1766.2 113.088 15 0 -5 -10 1811.32 116.918 31 0 -5 -10 1915.26 169.334 34 0 5 -10 1510.14 155.075 34 0 5 -10 1831.22 100.019 8 0 -5 -10 1753.05 100.4 8 0 -5 -10 1972.54 106.226 21 0 5 -11 1448.15 89.438 42 0 5 -11 1475.82 93.9439 41 0 -5 -11 1568.65 93.1992 42 0 -5 -11 1453.67 102.671 15 0 -5 -11 1736.3 183.169 1 0 5 -11 1268.54 148.169 4 0 -5 -11 1371.57 104.007 31 0 5 -11 1123.65 145.604 34 0 -5 -11 1361.83 89.3869 8 0 5 -11 1588.61 92.8888 8 0 -5 -11 1563.16 94.3121 21 0 5 -12 2234.2 119.565 41 0 5 -12 2123.51 113.133 42 0 -5 -12 1973.78 112.026 42 0 -5 -12 1932.19 199.923 1 0 -5 -12 2093.05 112.306 8 0 5 -12 2131.92 113.855 8 0 -5 -12 2136.88 128.953 15 0 -5 -12 1943.16 112.54 21 0 -5 -13 2016.49 121.306 15 0 -5 -13 1877.87 104.537 8 0 5 -13 1875.64 104.571 8 0 -5 -13 1991.94 104.868 21 0 5 -13 1709.83 127.08 18 0 -5 -13 1808.82 103.527 42 0 5 -13 1853.88 103.881 42 0 5 -14 6.44823 51.2102 18 0 -5 -14 21.7303 40.5416 15 0 -5 -14 18.4332 29.8959 8 0 5 -14 26.0872 31.5782 8 0 5 14 70.3644 35.7212 9 0 5 -14 -22.3349 30.0321 42 0 -5 -14 -14.992 30.238 42 0 -5 -15 -4.43687 32.3066 14 0 -5 -15 31.2612 35.6583 15 0 5 -15 42.8048 44.6986 18 0 -5 -15 34.3166 25.0159 8 0 5 15 -24.746 28.1053 9 0 5 -15 34.8127 25.2659 8 0 5 -16 193.862 39.2032 18 0 -5 -16 176.211 33.3748 15 0 -5 -16 149.842 29.8774 14 0 6 0 853.144 90.5147 27 0 -6 0 933.484 100.89 33 0 6 1 4303.3 228.915 27 0 -6 -1 4173.55 234.993 33 0 -6 1 4386.9 240.165 33 0 6 -1 3992.84 220.512 36 0 6 2 3025.07 186.341 27 0 -6 2 2995.26 197.321 33 0 -6 -2 2815.97 188.071 33 0 -6 -3 531.474 81.198 1 0 -6 -3 472.738 86.0279 33 0 6 -3 463.702 43.5038 37 0 -6 -4 6657.85 351.54 33 0 -6 -4 6918.15 268.734 38 0 6 -4 7321.31 348.095 36 0 -6 -5 8746.35 436.96 33 0 -6 -5 9201.08 346.892 38 0 6 -5 8989.45 350.512 37 0 6 -5 9472.9 428.634 36 0 -6 -6 1155.22 132.906 33 0 6 -6 1178.11 80.0564 18 0 -6 -6 1062.26 70.0442 23 0 6 -6 1340.77 76.8463 37 0 6 -6 1169.46 126.519 36 0 -6 -7 44.2787 33.1422 15 0 6 -7 10.1199 33.6769 18 0 -6 -7 -16.5366 60.5796 1 0 -6 -7 10.7856 27.1573 23 0 6 -7 7.69101 29.3868 37 0 6 -7 58.8624 59.0542 36 0 -6 -8 848.434 123.861 1 0 6 -8 785.282 73.6643 18 0 -6 -8 726.361 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6214.23 382.887 33 1 -9 -5 6022.44 255.69 23 1 -9 -5 6294.5 356.562 1 1 9 -4 1982.15 183.995 36 1 9 -4 2215.55 119.176 37 1 -9 -4 2118.57 182.666 1 -1 -9 4 2270.25 201.031 33 1 -9 -4 2383.09 214.661 33 1 -9 -4 2224.41 121.471 38 -1 9 4 2287.31 120.242 9 1 9 -4 2070.35 120.683 9 1 9 -3 529.897 53.9953 37 -1 9 3 366.795 49.3008 9 1 -9 -3 509.203 109.595 33 -1 -9 3 354.067 91.5805 33 1 -9 -3 433.334 49.2975 23 1 -9 -3 437.2 89.2898 1 1 -9 -2 7567.17 374.788 1 1 9 -2 6662.91 377.434 36 1 9 -2 6624.63 280.411 37 -1 9 2 6597.78 336.287 36 -1 -9 2 6656.54 275.488 20 -1 -9 2 7297.4 389.683 33 1 -9 -2 7244.29 406.69 33 1 -9 -2 7385.83 285.288 23 -1 9 2 7020.53 285.388 9 1 -9 -1 1679.01 151.84 1 -1 -9 1 1664.08 95.5647 20 1 -9 -1 1719.56 184.698 33 -1 -9 1 1600.52 160.641 33 1 9 -1 1745.81 95.6037 37 1 9 -1 1904.37 168.347 36 -1 9 1 1928.9 150.459 36 1 -9 -1 1813.76 97.5589 23 -1 9 1 1796.61 100.667 9 1 9 -1 1699.14 100.587 9 -1 -9 0 6571.24 270.892 20 -1 9 0 6237.33 340.465 36 1 9 0 6521.09 264.582 37 -1 9 0 6376.04 261.575 37 -1 -9 0 6493.34 362.311 33 1 -9 0 6691.34 394.381 33 1 9 0 7694.01 376.129 27 1 -9 0 6687.73 266.558 23 -1 9 0 6701.54 271.909 9 1 9 0 6599.62 273.844 9 -1 9 -1 2710.9 125.625 37 -1 9 -1 2550.6 191.602 36 1 9 1 2653.82 121.962 37 -1 -9 -1 2476.58 133.335 14 1 -9 1 2085.15 207.44 33 -1 -9 -1 2751.35 207.061 33 1 -9 1 2437.55 121.142 23 1 9 1 2876.54 213.406 27 -1 9 -1 2720.94 131.357 9 1 9 1 2698.08 132.127 9 -1 9 -2 170.76 38.2436 37 -1 9 -2 371.049 85.9613 36 -1 -9 -2 244.617 47.8621 14 1 -9 2 235.182 94.6021 33 -1 -9 -2 221.021 77.8939 33 -1 9 -2 277.11 41.121 25 1 9 2 239.399 78.7319 27 -1 9 -2 188.987 40.4931 9 1 9 2 146.885 41.1722 9 -1 9 -3 2768.83 126.977 41 -1 9 -3 2856.44 136.526 37 -1 9 -3 2176.09 196.972 36 -1 -9 -3 2549.98 143.835 14 1 -9 3 2709.24 236.713 33 -1 -9 -3 3190.72 224.537 33 -1 -9 -3 2934.36 146.824 32 -1 9 -3 2837.61 136.845 25 1 9 3 2798.28 138.899 9 -1 9 -3 2715.89 135.962 9 -1 9 -4 1070.59 74.8678 9 1 9 4 1104.34 78.5058 9 -1 -9 -4 987.269 139.872 1 -1 9 -4 1010.17 69.3956 41 -1 9 -4 1221.76 78.2466 44 -1 9 -4 904.485 128.965 36 -1 9 -4 1024.23 74.83 37 -1 -9 -4 1045.23 84.9858 14 1 -9 4 860.797 143.395 33 -1 -9 -4 957.178 127.263 33 -1 -9 -4 962.222 81.4013 32 -1 9 -4 981.329 70.9094 25 -1 -9 -4 1037.38 75.0137 21 1 9 5 4298.57 188.949 9 -1 -9 -5 3939.02 283.681 1 -1 9 -5 3924.85 177.702 41 -1 9 -5 3896.27 184.178 44 -1 9 -5 4089.92 186.9 37 -1 9 -5 3370.1 265.495 36 -1 -9 -5 4396.48 202.975 14 1 -9 5 3819.46 299.544 33 -1 -9 -5 3828.13 193.876 32 -1 9 -5 3861.99 178.131 25 -1 -9 -5 4115.94 185.528 21 -1 -9 -5 4133.08 190.557 20 -1 -9 -6 87.4055 80.1797 1 -1 9 -6 112.815 37.7605 44 -1 9 -6 127.877 36.2358 41 -1 -9 -6 115.956 51.1118 14 -1 -9 -6 149.864 51.3577 32 1 9 6 179.573 46.2699 9 -1 -9 -6 148.006 45.1401 20 -1 -9 -6 122.452 41.4209 21 -1 -9 -7 3149.65 256.476 1 -1 9 -7 3257.92 158.775 41 -1 9 -7 3448.59 162.293 44 -1 9 -7 3238.42 162.631 37 -1 9 -7 3287.59 254.477 36 -1 -9 -7 3371.9 179.169 14 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4590.29 190.456 18 -1 -9 -14 4915.78 189.349 14 1 -10 -14 401.733 37.1703 14 -1 10 14 249.892 26.5809 9 1 -10 -13 478.816 50.4959 14 1 10 -13 426.515 45.7196 18 -1 10 13 538.108 44.814 9 1 -10 -13 397.512 38.3896 21 1 10 -12 3308.91 145.589 41 1 -10 -12 3039.13 154.779 14 1 -10 -12 2961.62 148.348 31 -1 10 12 3124.92 147.705 9 1 -10 -12 3299.82 145.407 21 1 10 -12 3265.44 153.221 18 1 10 -11 2332.9 119.424 41 1 10 -11 2332.22 119.266 37 1 -10 -11 2364.24 134.398 14 1 -10 -11 2465.73 130.671 31 -1 10 11 2259.23 124.52 9 1 -10 -11 2436.61 122.726 21 1 -10 -11 2354.62 117.001 20 1 10 -11 2273.43 127.513 18 1 10 -10 13.9757 32.3811 37 1 10 -10 11.4761 44.8376 18 1 10 -10 4.51054 32.6324 41 1 -10 -10 29.2521 37.8872 21 1 -10 -10 -5.8361 40.2824 31 1 10 -9 16270.3 622.972 37 1 -10 -9 16686.2 635.654 31 1 10 -9 16407 620.165 41 1 10 -9 15985.4 631.994 18 1 -10 -9 16634.8 625.441 21 1 10 -8 7534.4 304.228 41 1 -10 -8 7017.58 302.848 38 1 10 -8 6938.97 412.963 36 1 10 -8 7586.52 309.632 37 1 10 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145.849 23 -1 10 5 3121.97 154.575 9 1 -10 -4 1247.64 153.321 1 1 -10 -4 1245.62 87.9867 38 1 10 -4 1295.3 88.2056 37 1 10 -4 1384.97 92.0221 18 1 -10 -4 1150.23 165.061 33 -1 -10 4 1022.06 151.227 33 1 -10 -4 1233.15 88.3167 23 -1 10 4 1217.64 88.3775 9 1 10 -4 1249.84 91.3597 9 1 10 -3 1847.36 184.088 36 1 10 -3 2246.36 120.581 37 -1 10 3 2327.73 123.364 9 1 10 -3 1987.97 122.367 9 -1 -10 3 2194.46 201.288 33 1 -10 -3 1981.3 207.63 33 1 -10 -3 2168.08 119.398 23 1 -10 -3 2059.84 184.713 1 1 -10 -2 69.0695 56.6011 1 1 10 -2 53.9466 34.7806 37 1 10 -2 38.3345 68.4562 36 -1 -10 2 20.1049 29.1378 20 -1 -10 2 60.4849 66.0803 33 1 -10 -2 23.4763 74.4958 33 1 -10 -2 60.5668 35.4308 23 -1 10 2 76.1111 39.4659 9 1 -10 -1 20425.2 844.354 1 1 10 -1 20261.7 857.659 36 1 10 -1 19570.6 729.626 37 -1 10 1 18917 818.235 36 -1 -10 1 20109.5 731.901 20 -1 -10 1 19302.3 858.527 33 1 -10 -1 18085.3 878.253 33 1 -10 -1 19589.4 732.217 23 -1 10 1 19697 736.885 9 1 -10 0 4251.93 271.103 1 -1 -10 0 4468.26 200.148 20 1 -10 0 4166.03 308.828 33 -1 -10 0 4531.38 295.834 33 1 10 0 4088.48 280.887 36 -1 10 0 4398.23 190.323 37 -1 10 0 4352.14 272.366 36 1 10 0 4623.57 194.732 37 1 -10 0 4574.35 195.923 23 1 10 0 4603.51 204.542 9 -1 10 0 4366.72 201.387 9 -1 -10 -1 2093.01 121.95 20 -1 10 -1 2496.27 118.108 37 1 10 1 1934.21 182.095 36 -1 10 -1 2576.68 195.931 36 1 -10 1 2679.86 236.647 33 -1 -10 -1 1904.24 183.528 33 1 -10 1 2257.67 114.072 23 1 10 1 2243.58 125.281 9 -1 10 -1 2153.58 121.562 9 -1 -10 -2 2115.52 201.229 1 -1 -10 -2 2000.61 111.427 21 -1 -10 -2 2272.46 125.649 20 -1 10 -2 2254.3 117.566 37 -1 -10 -2 2368.65 130.999 14 1 -10 2 2420.77 228.157 33 -1 -10 -2 2415.11 203.836 33 -1 10 -2 2313.94 123.766 25 -1 10 -2 2077.63 119.503 9 1 10 2 2185.48 124.245 9 -1 -10 -3 4.37361 31.8431 21 -1 -10 -3 -10.8329 35.4948 20 -1 10 -3 38.2435 66.4526 36 -1 10 -3 46.8121 30.9155 37 -1 -10 -3 47.9974 45.0422 14 1 -10 3 -99.1904 90.8387 33 -1 -10 -3 11.9025 38.3847 32 -1 10 -3 -4.75801 35.9329 25 -1 10 -3 4.91471 32.953 9 1 10 3 5.26099 35.2747 9 -1 10 -4 706.572 64.1894 9 1 10 4 640.578 64.5625 9 -1 10 -4 568.375 61.5846 44 -1 10 -4 503.725 109.348 36 -1 10 -4 765.24 65.4007 37 -1 -10 -4 738.634 75.4009 14 -1 -10 -4 688.862 71.4885 32 1 -10 4 408.246 125.718 33 -1 10 -4 600.114 57.9722 25 -1 -10 -4 649.953 62.5293 21 -1 10 -5 1310.15 92.014 44 -1 10 -5 1566.91 98.0302 37 -1 10 -5 1491.07 171.056 36 1 -10 5 1628.13 197.939 33 -1 -10 -5 1339.7 101.67 32 -1 -10 -5 1490.65 94.7313 21 -1 -10 -5 1577.52 101 20 1 10 5 1462.14 96.5774 9 -1 -10 -5 1494.76 107.336 14 -1 -10 -6 710.267 127.744 1 -1 10 -6 679.951 63.0153 44 -1 -10 -6 570.722 73.547 14 -1 -10 -6 611.962 71.2436 32 1 -10 6 831.37 148.944 33 1 10 6 658.488 64.0662 9 -1 -10 -6 536.245 62.4836 20 -1 -10 -6 579.747 65.25 21 -1 -10 -7 321.014 98.3626 1 -1 10 -7 294.292 46.9742 44 -1 10 -7 328.805 54.7433 37 -1 10 -7 237.529 83.8654 36 -1 -10 -7 432.156 69.023 14 1 10 7 413.767 53.5673 9 -1 -10 -7 350.465 54.3978 20 -1 -10 -7 389.626 53.1654 21 -1 -10 -8 160.534 37.0133 43 -1 -10 -8 135.194 47.3033 31 -1 -10 -8 182.405 60.8797 14 1 10 8 162.172 38.5787 9 -1 -10 -8 222.293 49.2724 21 -1 -10 -8 256.776 46.1917 20 -1 -10 -9 348.396 58.8408 31 -1 -10 -9 442.286 66.5737 14 -1 -10 -9 316.915 48.6386 20 1 10 9 348.577 50.3032 9 -1 -10 -10 995.655 80.1112 31 1 10 10 909.558 70.3899 9 -1 -10 -10 1124.39 71.9317 20 -1 -10 -11 522.009 56.9276 31 1 10 11 494.43 45.6448 9 -1 -10 -11 454.592 50.2418 21 -1 10 -11 533.31 62.4229 18 -1 10 -12 69.1127 25.6735 40 -1 -10 -12 140.913 32.4532 21 -1 10 -12 123.063 37.6197 18 -1 -10 -12 122.515 38.8661 14 -1 -10 -13 9368.43 354.185 21 -1 10 -13 9635.9 363.438 18 -1 -10 -13 9593.08 362.545 14 1 -11 -13 319.065 34.3646 14 1 -11 -13 351.987 29.0967 21 1 -11 -12 -10.4951 28.801 14 1 11 -12 -12.4455 28.2674 18 1 -11 -12 -3.3189 24.4698 31 -1 11 12 -6.06545 25.214 9 1 -11 -12 -19.4295 24.384 21 1 11 -11 408.796 41.8036 41 1 11 -11 373.103 41.1204 37 1 11 -11 424.825 48.5924 18 1 -11 -11 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33 1 -11 -6 383.375 109.378 33 1 -11 -6 150.439 50.6931 32 1 -11 -6 293.471 54.6213 23 -1 11 6 271.109 52.1491 9 1 11 -5 422.215 46.8503 41 1 11 -5 493.312 112.287 36 1 -11 -5 380.981 54.9968 38 1 11 -5 468.957 58.0336 37 1 11 -5 544.167 63.107 18 1 -11 -5 433.536 65.6893 32 -1 -11 5 630.072 121.972 33 1 -11 -5 464.996 120.79 33 -1 11 5 501.407 60.5955 9 1 -11 -5 546.147 111.091 1 1 11 -4 23.5178 42.0088 9 -1 11 4 68.4179 46.4897 9 1 -11 -4 43.8499 35.3814 38 1 11 -4 51.7265 38.6273 37 1 11 -4 11.1999 38.1295 18 -1 -11 4 45.7537 70.1286 33 1 -11 -4 -51.8505 82.2581 33 1 -11 -4 58.9391 45.2222 32 1 -11 -4 64.3549 44.6054 23 1 -11 -4 78.9268 62.6135 1 1 -11 -3 1157.18 83.3324 38 1 11 -3 776.405 131.749 36 1 11 -3 963.211 75.4345 37 1 11 -3 902.501 79.7708 9 -1 11 3 897.023 78.5508 9 -1 -11 3 646.542 122.945 33 1 -11 -3 1105.61 166.501 33 1 -11 -3 1030.45 78.1428 23 1 -11 -3 843.18 130.859 1 1 11 -2 3167.25 249.464 36 1 11 -2 3447.64 160.848 37 -1 11 2 3159.63 164.623 9 -1 -11 2 3429.47 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117.168 33 2 -7 -4 971.564 69.63 23 2 -7 -4 991.598 108.23 1 2 -7 -3 3231.01 195.827 1 2 7 -3 3561.21 154.26 37 2 -7 -3 3366.25 154.671 19 2 -7 -3 3772.03 228.932 22 -2 -7 3 3367.52 207.852 33 2 -7 -3 3467.23 245.832 33 -2 7 3 3268.48 207.303 29 2 7 -3 3446.27 207.33 27 2 -7 -3 3359.61 152.446 23 2 7 -3 3312.72 152.294 9 -2 7 3 3260.26 149.453 9 -2 -7 3 3101.63 157.259 10 2 -7 -2 696.604 81.4624 1 -2 7 2 774.927 81.0244 36 2 -7 -2 831.545 103.609 22 -2 7 2 774.552 90.9249 29 2 -7 -2 616.64 111.581 33 2 7 -2 847.343 101.974 27 2 -7 -2 763.237 57.2701 23 2 7 -2 728.257 56.7572 9 -2 -7 2 815.444 66.8403 10 2 -7 -1 25.7905 42.8402 1 2 -7 -1 123.768 55.3033 22 2 -7 -1 -13.0009 26.5004 23 2 -7 -1 98.3079 65.753 33 -2 7 1 31.1377 39.884 29 -2 7 1 68.04 49.727 36 2 7 -1 -13.2711 52.1388 27 2 7 -1 6.91486 27.7584 9 -2 -7 1 39.8207 35.8856 10 -2 7 0 3016.11 190.275 36 2 -7 0 2543.61 209.88 33 -2 7 0 3086.47 184.734 29 2 7 0 3286.36 217.481 27 -2 -7 0 3090.91 141.363 20 2 -7 0 3251.51 189.281 22 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32.3425 15 -2 -7 -13 13.2757 29.1546 21 -2 7 -13 35.1919 26.8539 40 -2 -7 -14 927.266 59.4491 15 -2 7 -14 1125.67 65.2718 18 2 8 -14 31.2432 32.0735 18 2 -8 -14 49.3024 26.3808 15 2 8 -14 33.473 25.2101 41 2 8 -13 2458.61 118.568 41 2 -8 -13 2269.42 114.399 38 2 -8 -13 2210.25 114.698 15 -2 8 13 2299.52 121.705 9 2 -8 -13 2350.05 110.942 21 2 8 -13 2213.35 120.788 18 2 8 -12 5204.67 215.193 41 2 8 -12 4553.3 203.335 37 2 -8 -12 4610.8 211.968 38 2 -8 -12 4884.71 211.682 15 2 -8 -12 4820.75 215.959 31 2 -8 -12 5056.05 209.931 21 2 8 -12 4702.76 218.473 18 -2 8 12 5141.92 220.803 9 -2 8 11 4103.44 194.236 9 2 8 -11 4354.84 192.4 41 2 -8 -11 3926.72 191.176 38 2 8 -11 4198.73 186.431 37 2 -8 -11 4182.01 189.165 15 2 -8 -11 4082.28 193.709 31 2 -8 -11 4008.96 180.402 23 2 8 -11 4233.12 198.801 18 2 -8 -11 3969.47 186.379 21 2 -8 -10 1822.52 186.538 1 2 8 -10 1651.04 108.916 18 2 -8 -10 1797.07 110.498 38 2 8 -10 1713.04 102.528 37 2 -8 -10 1781.97 111.1 31 2 -8 -10 1693.53 99.6268 23 -2 8 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-5 6323.33 357.869 22 2 -8 -5 6119.84 261.293 19 -2 -8 5 5602.26 334.914 33 2 -8 -5 6065.67 258.688 32 2 -8 -5 6016.09 255.545 23 -2 8 5 6158.52 256.4 9 2 -8 -4 59.16 36.664 38 2 8 -4 97.6378 39.4112 37 2 8 -4 119.195 66.9435 36 2 -8 -4 49.5732 59.0589 22 2 -8 -4 41.9854 84.2818 33 -2 8 4 55.1374 50.5644 29 -2 8 4 72.7814 33.3745 9 2 8 -4 102.267 35.6143 9 -2 -8 4 58.2602 40.3196 10 2 -8 -4 81.5565 53.4627 1 2 -8 -3 184.822 59.3166 1 2 8 -3 235.18 41.6594 37 2 -8 -3 196.571 69.3592 22 2 -8 -3 200.881 94.8146 33 2 8 -3 183.696 63.1077 27 2 -8 -3 235.308 41.3901 23 -2 8 3 229.521 38.8963 9 2 8 -3 132.484 40.6387 9 -2 -8 3 283.924 50.2254 10 2 -8 -2 135.209 51.6946 1 2 -8 -2 261.311 70.5779 22 -2 -8 2 136.874 32.4179 20 2 -8 -2 254.221 90.7873 33 2 8 -2 150.755 37.6179 37 2 8 -2 199.164 72.989 27 2 -8 -2 200.272 39.5349 23 -2 8 2 126.135 34.4735 9 2 8 -2 185.942 41.0523 9 -2 -8 2 146.678 43.2238 10 2 -8 -1 1873.78 148.699 22 -2 -8 1 1601.96 97.1098 20 2 -8 -1 1738.09 177.933 33 2 8 -1 1771.69 98.2831 37 -2 8 1 1801.24 141.344 36 2 -8 -1 1812.91 98.2924 23 2 8 -1 2011.1 167.687 27 2 8 -1 1953.18 102.109 9 -2 8 1 1858.71 98.1405 9 -2 -8 1 2117.59 112.038 10 2 -8 0 308.008 65.8951 22 -2 -8 0 344.098 44.5925 20 2 8 0 284.869 40.0081 37 -2 8 0 467.761 82.273 36 2 -8 0 387.211 102.135 33 -2 8 0 219.108 45.3013 25 2 8 0 372.94 85.7494 27 2 -8 0 360.292 41.6657 23 2 8 0 287.944 42.2332 9 -2 -8 -1 392.743 48.0693 20 2 8 1 416.809 43.0713 37 -2 8 -1 222.606 69.8424 36 -2 -8 -1 461.851 57.3111 14 2 -8 1 492.037 111.435 33 2 -8 1 461.896 44.4207 23 -2 -8 -1 358.091 42.0859 24 2 8 1 551.863 107.596 27 -2 8 -1 390.369 48.8963 25 2 8 1 421.294 46.8511 9 -2 -8 -2 2548.91 123.891 21 -2 -8 -2 2980.18 137.863 20 -2 8 -2 2266.91 189.359 36 -2 -8 -2 2575.76 141.827 14 2 -8 2 3013.51 235.233 33 -2 -8 -2 2632.34 132.682 32 2 8 2 2309.96 203.966 27 -2 8 -2 2808.05 136.841 25 -2 -8 -2 2553.1 125.181 24 2 8 2 2785.39 131.611 9 -2 -8 -3 697.867 111.812 1 -2 -8 -3 506.311 57.0471 20 -2 -8 -3 679.914 55.4058 21 -2 8 -3 562.492 104.766 36 -2 -8 -3 703.827 71.9674 14 2 -8 3 843.512 132.346 33 -2 -8 -3 654.944 61.0423 32 -2 -8 -3 610.47 52.264 24 2 8 3 718.206 120.053 27 -2 8 -3 706.094 60.7977 25 2 8 3 648.762 58.3245 9 2 8 4 3985.96 178.162 9 -2 -8 -4 3471.76 261.133 1 -2 8 -4 4048.3 187.938 44 -2 8 -4 3790.82 264.467 36 -2 -8 -4 4027.93 196.857 14 2 -8 4 3631.77 282.589 33 -2 -8 -4 4096.89 187.273 32 -2 8 -4 3756.34 180.977 25 -2 -8 -4 3862.31 178.842 21 -2 -8 -4 4386.41 188.551 20 2 8 5 667.379 58.0482 9 -2 8 -5 618.045 64.529 44 -2 8 -5 693.475 72.6041 18 -2 -8 -5 660.011 113.431 1 2 -8 5 490.738 118.648 33 -2 -8 -5 804.887 70.3277 32 2 8 5 687.875 119.005 27 -2 -8 -5 659.278 61.4751 21 -2 -8 -5 544.346 60.6817 20 2 8 6 934.577 70.055 9 -2 8 -6 1009.55 82.2025 44 -2 8 -6 1068.51 86.3293 18 -2 -8 -6 900.734 89.509 14 -2 -8 -6 931.416 134.542 1 2 -8 6 1104.1 159.301 33 2 8 6 1068.41 148.609 27 -2 -8 -6 987.296 75.5001 21 -2 -8 -6 877.723 73.806 20 -2 -8 -7 1146 155.326 1 -2 -8 -7 1111.51 82.2645 15 -2 8 -7 1230.47 97.6517 18 -2 -8 -7 1366.05 105.632 14 -2 8 -7 1279.81 92.2513 44 -2 -8 -7 1153.55 84.3871 43 -2 -8 -7 1274.69 93.2001 31 2 -8 7 1067.82 165.387 33 2 8 7 1245.36 80.5566 9 -2 -8 -7 1057.03 84.8243 21 -2 -8 -7 1235.21 88.5775 20 -2 -8 -8 4578.8 212.677 15 -2 -8 -8 4821.2 235.323 14 -2 8 -8 4536.69 225.137 18 -2 -8 -8 4722.69 208.81 43 -2 8 -8 5076.57 222.443 44 2 -8 8 5251.41 352.703 33 -2 -8 -8 4436.37 219.772 31 -2 -8 -8 5253.52 334.013 1 -2 -8 -8 4641.29 217.254 21 -2 -8 -8 4801.93 213.668 20 -2 -8 -9 104.83 45.448 31 -2 8 -9 189.054 54.132 18 -2 -8 -9 99.8561 52.8137 14 -2 -8 -9 98.1656 43.8514 15 -2 -8 -9 158.334 37.2598 43 -2 8 -9 170.595 49.2147 44 -2 -8 -9 164.296 40.6296 20 -2 -8 -10 23850.4 900.634 31 -2 8 -10 23746.7 892.206 44 -2 -8 -10 23378.9 893.324 21 -2 8 -10 25049 908.378 18 -2 -8 -10 24088.8 891.91 15 -2 -8 -10 24796.1 910.31 14 -2 8 -11 2008.46 110.589 44 -2 8 -11 2121.12 123.516 18 -2 -8 -11 2019.64 112.468 21 -2 -8 -11 1938.09 122.109 14 -2 -8 -11 2132.84 113.814 15 -2 8 -12 53.0876 30.1465 40 -2 8 -12 19.4095 27.5583 44 -2 -8 -12 22.6268 30.9087 21 -2 8 -12 33.7991 40.734 18 -2 -8 -12 52.069 41.9535 14 -2 -8 -12 18.426 29.7493 15 -2 8 -13 186.522 29.1476 40 -2 -8 -13 241.246 33.2564 21 -2 8 -13 252.278 39.8628 18 -2 -8 -13 199.535 36.9808 14 -2 -8 -13 202.104 31.861 15 2 9 -14 821.512 51.8021 41 2 -9 -14 876.09 61.3563 14 2 9 -13 5704.21 233.548 41 2 -9 -13 5943.6 229.557 21 -2 9 13 5608.08 237.412 9 2 -9 -12 11331.2 457.747 38 2 9 -12 11852.4 455.201 37 2 -9 -12 12702.7 459.999 21 2 9 -12 11665.7 462.817 18 -2 9 12 12204.8 467.027 9 2 -9 -12 12702.7 465.196 31 2 9 -11 5004.22 214.186 37 2 -9 -11 4818.95 217.925 38 2 -9 -11 5402.64 224.584 31 2 9 -11 4538.49 217.622 18 2 -9 -11 5165.85 218.176 21 -2 9 11 4976.83 222.302 9 2 9 -10 264.681 49.3991 41 2 9 -10 304.202 46.0488 37 2 -9 -10 248.192 46.1108 38 2 9 -10 308.819 50.9672 18 2 -9 -10 266.73 51.334 31 2 -9 -10 253.632 45.0274 23 -2 9 10 219.164 48.6098 9 2 -9 -9 6472.09 272.511 38 2 9 -9 6240.76 268.593 37 2 9 -9 5882.51 267.222 18 2 -9 -9 6488.99 275.33 31 2 -9 -9 6361.53 267.348 23 -2 9 9 6084.15 271.871 9 2 -9 -8 1356.26 156.84 1 2 -9 -8 1655.16 107.455 38 2 9 -8 1866.91 175.839 36 2 9 -8 1654.88 104.277 37 2 9 -8 1538.61 99.6929 18 2 -9 -8 1786.25 209.343 33 2 -9 -8 1594.45 105.292 32 2 -9 -8 1499.74 99.7453 23 -2 9 8 1562.27 101.998 9 2 9 -7 39.1181 71.6488 36 2 9 -7 27.1318 41.9327 37 2 -9 -7 -5.81239 38.385 38 -2 9 7 -5.50493 41.081 9 2 -9 -7 -17.6667 39.7776 32 2 -9 -7 15.6849 40.8537 23 2 -9 -7 37.6487 65.4187 1 2 -9 -6 1432.98 96.263 38 2 9 -6 1354.5 157.533 36 2 9 -6 1313.45 92.7503 37 -2 9 6 1492.41 95.527 9 2 -9 -6 1393.74 96.7226 32 2 -9 -6 1304.03 91.1695 23 2 -9 -6 1285.53 145.798 1 2 -9 -5 1190.2 137.437 1 2 -9 -5 1490.68 97.0784 38 2 9 -5 1349.37 152.784 36 2 -9 -5 1479.47 154.44 22 2 -9 -5 1345.93 92.5696 32 2 -9 -5 1228.42 89.1777 23 -2 9 5 1494.02 94.2487 9 2 -9 -4 106.769 66.955 22 -2 9 4 129.732 40.7838 9 2 9 -4 182.511 46.8235 9 2 -9 -4 150.484 68.7858 1 2 9 -4 59.0095 42.8777 37 2 -9 -4 197.145 47.9068 38 2 9 -4 77.0125 78.9878 36 2 -9 -3 4555.33 275.319 22 2 9 -3 4096.39 282.632 36 2 9 -3 4604.06 198.174 37 2 -9 -3 4459.23 198.12 23 -2 9 3 4343.49 194.766 9 -2 -9 3 3934.81 199.908 10 2 9 -3 4416.38 199.556 9 2 -9 -2 14.818 47.0096 22 -2 -9 2 20.6223 30.5939 20 2 -9 -2 67.3606 90.1024 33 2 9 -2 -22.2328 35.5012 37 2 -9 -2 44.1424 35.2431 23 2 9 -2 15.8758 56.6843 27 2 9 -2 -4.85081 33.7162 9 -2 -9 2 11.1567 38.2306 10 -2 9 2 -4.3856 31.9303 9 -2 -9 1 26.4126 31.4502 20 2 -9 -1 22.2435 77.307 33 2 9 -1 42.069 33.2459 37 -2 9 1 -12.8201 46.9726 36 2 9 -1 17.1369 56.1569 27 2 -9 -1 54.5147 31.8692 23 2 9 -1 -4.70824 33.8557 9 -2 9 1 33.7762 29.5643 9 -2 -9 1 44.5608 38.4573 10 -2 -9 0 13.9681 32.5862 20 2 -9 0 44.6378 73.1273 33 2 9 0 27.7374 31.6365 37 -2 9 0 -14.2638 53.542 36 -2 -9 0 15.7694 28.3375 24 2 -9 0 -3.9571 30.0598 23 2 9 0 -36.5832 58.0291 27 -2 9 0 5.06583 36.1753 25 2 9 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107.969 20 -2 -9 -9 946.575 77.5736 31 -2 -9 -9 754.655 82.8081 14 -2 9 -9 695.273 76.2557 18 -2 9 -9 818.401 71.2063 44 -2 -9 -9 800.69 62.5042 43 -2 -9 -9 696.941 68.6769 21 -2 -9 -9 973.169 70.5933 20 -2 -9 -10 528.3 63.2018 31 -2 9 -10 654.845 61.0897 44 -2 9 -10 601.624 57.4948 40 -2 -9 -10 672.859 72.4661 14 -2 9 -11 811.551 59.9277 44 -2 9 -11 900.157 63.5176 40 -2 -9 -11 846.853 66.3722 21 -2 9 -11 849.759 72.5527 18 -2 -9 -11 749.415 70.9101 14 -2 -9 -12 282.843 37.5187 21 -2 9 -12 304.602 42.4374 18 -2 -9 -12 311.77 44.1877 14 -2 -9 -13 30.2 20.8715 21 -2 9 -13 46.9594 26.418 18 2 -10 -13 2920.32 129.293 14 -2 10 13 2645.22 124.284 9 2 -10 -13 2757.13 117.827 21 2 10 -12 1354.82 74.9656 41 2 -10 -12 1348.96 83.8537 14 2 -10 -12 1190.34 74.3471 31 -2 10 12 1386.73 80.8592 9 2 -10 -12 1351.66 74.5216 21 2 -10 -11 490.454 49.9259 38 2 10 -11 480.876 49.1282 37 2 10 -11 476.039 49.8776 41 2 -10 -11 533.314 53.7032 31 -2 10 11 522.967 55.1502 9 2 -10 -11 509.047 52.4178 21 2 10 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2 10 -4 4231.91 296.974 36 2 10 -4 4308.31 200.281 37 -2 10 4 4328.1 199.59 9 2 -10 -3 165.65 45.9886 23 2 10 -3 103.839 78.2903 36 2 10 -3 216.535 46.3155 37 2 -10 -3 198.474 50.8944 38 2 10 -3 264.615 48.7541 9 -2 10 3 226.323 43.8095 9 2 10 -2 2051.91 114.418 37 2 -10 -2 1894.39 111.332 23 2 10 -2 1998.28 118.442 9 -2 -10 2 2046.58 120.677 10 -2 10 2 2087.95 115.208 9 -2 -10 2 1887.87 106.786 20 2 10 -1 760.44 64.4056 37 -2 -10 1 687.178 61.5275 20 2 -10 -1 744.104 63.5769 23 -2 10 1 662.37 59.8477 9 2 10 -1 643.234 64.8233 9 -2 -10 1 620.367 67.9053 10 2 10 0 88.7685 36.1247 37 -2 10 0 124.072 63.5988 36 -2 -10 0 91.1125 39.6812 20 2 -10 0 24.8931 79.0358 33 -2 -10 0 78.7522 34.2699 24 2 10 0 159.147 81.5376 27 2 -10 0 77.2131 35.9751 23 -2 10 0 55.5966 41.1105 25 -2 -10 0 146.297 47.213 10 2 10 0 98.3876 39.2362 9 -2 10 0 100.567 35.071 9 2 10 1 403.297 47.5145 37 -2 10 -1 355.604 89.0239 36 -2 -10 -1 483.734 56.6234 20 2 -10 1 577.632 127.714 33 -2 -10 -1 482.481 58.7782 32 2 -10 1 403.7 45.8303 23 2 10 1 358.558 94.2624 27 -2 10 -1 450.977 59.987 25 -2 10 -1 523.111 55.1925 9 2 10 1 357.914 51.9893 9 -2 -10 -2 44.4391 77.2181 1 -2 -10 -2 22.1431 40.3041 20 -2 10 -2 -18.2147 65.035 36 2 -10 2 178.239 106.35 33 -2 -10 -2 5.46413 38.503 32 2 10 2 -44.3237 83.1883 27 -2 10 -2 -10.859 37.9995 25 2 10 2 25.3438 35.7173 9 2 10 3 1992.76 114.903 9 -2 -10 -3 2207.03 206.395 1 -2 10 -3 1837.01 117.728 44 -2 10 -3 1973.9 187.026 36 -2 -10 -3 1975.79 127.249 14 2 -10 3 2018.9 218.011 33 -2 -10 -3 2200.27 121.389 32 2 10 3 1776.66 195.054 27 -2 10 -3 1992.19 118.733 25 -2 -10 -3 1935.2 107.685 21 -2 -10 -4 1704.04 183.525 1 -2 -10 -4 1532.23 112.52 14 -2 10 -4 1668.72 107.494 44 -2 10 -4 1637.31 90.661 40 2 -10 4 1888.25 207.094 33 -2 -10 -4 1623.15 106.343 32 2 10 4 1571.57 98.3558 9 -2 -10 -4 1593.86 97.2261 21 -2 -10 -4 1595.68 106.42 20 -2 -10 -5 204.7 87.8526 1 -2 10 -5 336.019 62.7015 18 -2 -10 -5 214.531 60.1343 14 -2 10 -5 239.582 52.1907 44 2 -10 5 264.075 106.355 33 -2 -10 -5 249.932 51.2289 32 2 10 5 218.952 46.5078 9 -2 -10 -5 328.083 48.8136 21 -2 -10 -5 257.01 49.1645 20 -2 10 -6 1303.63 91.265 44 -2 -10 -6 1379.94 96.6922 31 2 -10 6 1129.98 171.276 33 -2 -10 -6 1171.75 101.588 14 -2 10 -6 1490.2 105.462 18 2 10 6 1237.25 84.7988 9 -2 -10 -6 1555.05 94.8365 21 -2 -10 -6 1202.17 92.1148 20 -2 10 -7 164.653 47.3135 44 -2 -10 -7 167.162 42.5986 43 -2 10 -7 128.699 37.5096 40 -2 -10 -7 129.097 46.1128 31 -2 10 -7 140.39 52.4665 18 2 10 7 164.845 38.9087 9 -2 -10 -7 101.074 44.2759 21 -2 -10 -7 119.473 44.0832 20 -2 10 -8 1276.24 86.8608 44 -2 10 -8 1354.77 83.6186 40 -2 -10 -8 1342.3 83.5879 43 -2 -10 -8 1139.44 89.0106 31 -2 10 -8 1334.16 99.8047 18 2 10 8 1093.26 75.8343 9 -2 -10 -8 1394.72 90.3229 21 -2 -10 -8 1387.92 89.9659 20 -2 -10 -9 23987.6 901.26 31 -2 -10 -9 23829.9 911.197 14 -2 10 -9 23988.3 893.373 44 -2 -10 -9 24215.1 887.213 43 -2 10 -9 24296.1 890.822 40 -2 -10 -9 25430.8 898.577 21 -2 10 -9 25429.1 911.424 18 -2 -10 -9 23869.5 892.776 20 -2 -10 -10 606.666 58.4242 31 -2 10 -10 601.691 50.9873 40 -2 10 -10 511.527 48.1038 44 -2 -10 -10 540.489 55.2728 21 -2 -10 -10 525.192 46.3241 20 -2 10 -10 635.502 63.9219 18 -2 -10 -10 613.495 65.398 14 -2 10 -11 1074.4 64.686 40 -2 10 -11 1134.85 75.8693 18 -2 -10 -11 1129.29 76.4913 14 -2 -10 -12 64.3614 22.4977 21 -2 10 -12 27.3302 26.1434 18 -2 11 13 67.7604 19.9342 9 2 11 -12 277.132 31.1922 41 2 -11 -12 177.211 31.0861 14 -2 11 12 253.875 33.6623 9 2 -11 -12 193.226 29.3898 21 2 11 -11 2469.52 114.898 41 2 11 -11 2483.29 115.738 37 2 -11 -11 2212.43 116.636 14 2 -11 -11 2373.73 116.868 31 2 -11 -11 2465.73 116.506 21 2 -11 -11 2384.16 112.831 20 -2 11 11 2674.2 121.703 9 -2 11 10 308.746 46.0215 9 2 11 -10 367.057 43.5108 41 2 -11 -10 223.857 37.3206 38 2 11 -10 295.365 42.273 37 2 -11 -10 253.401 43.8635 14 2 -11 -10 305.046 44.186 31 -2 11 10 204.821 34.4336 25 2 -11 -10 344.007 45.2604 21 2 -11 -9 330.31 43.8866 38 2 11 -9 327.041 46.8556 37 2 -11 -9 185.229 41.0302 14 2 -11 -9 233.333 46.5279 31 -2 11 9 277.729 47.4385 9 2 11 -9 221.302 39.4798 41 2 -11 -8 363.168 50.1028 38 2 11 -8 444.305 53.1168 37 2 11 -8 328.122 46.0619 41 2 -11 -8 470.654 55.4926 23 -2 11 8 390.506 55.4628 9 2 -11 -7 1199.38 85.9818 38 2 11 -7 1031.29 74.0096 41 2 -11 -7 1186.85 87.2246 32 2 -11 -7 1139.11 83.6912 23 -2 11 7 1192.19 86.1371 9 2 -11 -6 922.007 76.7697 38 2 11 -6 858.456 74.3918 37 2 11 -6 742.668 61.9196 41 2 -11 -6 1047.83 82.8245 32 2 -11 -6 888.479 74.8845 23 -2 11 6 798.522 71.2466 9 2 -11 -5 2573.01 238.695 33 2 -11 -5 2204.63 126.294 32 -2 11 5 1958.29 117.436 9 2 11 -5 1469.43 175.811 36 2 -11 -5 1922.24 120.288 38 2 11 -5 2166.32 120.922 37 2 -11 -4 3256.31 276.396 33 2 -11 -4 3358.55 167.645 32 2 -11 -4 3049.93 157.174 23 -2 11 4 2825.76 153.648 9 2 -11 -4 3223.22 162.813 38 2 11 -4 3284.35 255.185 36 2 11 -4 3114.68 157.22 37 2 -11 -3 7561.95 335.102 38 2 -11 -3 8347.32 330.93 23 -2 11 3 7967.87 329.04 9 2 11 -3 8025.79 334.988 9 2 11 -3 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38.1821 30 -5 3 4 21.2474 35.3671 30 -5 3 4 63.8047 67.4817 28 -5 -3 4 -43.081 66.0286 28 -5 -3 4 33.4943 30.3107 24 5 3 -4 137.04 70.1669 26 5 3 -4 66.1971 40.179 19 -5 -3 3 2127.61 197.394 16 -5 3 3 1974.13 191.008 16 -5 -3 3 2009.6 114.835 2 -5 3 3 2367.44 120.434 2 -5 -3 3 2347.27 202.601 5 -5 3 3 2210.5 194.415 5 -5 -3 3 2033.89 119.396 30 -5 3 3 1990.23 118.029 30 -5 -3 3 2122.55 112.417 24 5 3 -3 2177.6 186.22 26 5 3 -3 2065.35 118.565 19 -5 -3 2 1142.21 100.517 10 -5 -3 2 1435.65 83.7293 39 -5 -3 2 1276.78 151.185 16 -5 3 2 1261.15 150.763 16 -5 -3 2 1524.23 92.578 2 -5 3 2 1496.93 92.6519 2 -5 -3 2 1679.42 169.697 5 -5 3 2 1635.22 164.964 5 -5 -3 2 1173.25 90.3559 30 -5 3 2 1401.07 95.3128 30 -5 -3 2 1275.79 86.3541 24 5 -3 -2 1558.76 165.502 26 5 3 -2 1297.88 144.583 26 5 3 -2 1360.59 88.2791 19 -5 -3 1 1496.11 91.7631 39 -5 3 1 1718.88 104.437 39 -5 -3 1 1658.63 172.084 16 -5 3 1 1583.76 167.02 16 -5 -3 1 1486.92 93.6591 6 -5 3 1 1678.11 96.1452 6 -5 -3 1 1688.71 99.0188 2 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-5 3 -2 16218 757.82 3 -5 3 -2 17439.5 643.743 7 -5 -3 -2 17183.3 637.414 6 -5 3 -2 17040 638.314 6 -5 3 -2 16996.2 640.636 44 -5 3 -2 16745.2 648.007 39 -5 -3 -2 16154.1 651.451 15 -5 -3 -2 17610.3 642.749 24 5 -3 2 16359.9 748.668 26 -5 3 -2 17494.9 644.949 13 -5 -3 -2 15953.1 650.354 10 -5 3 -3 48.2615 43.7159 7 -5 -3 -3 79.3929 65.0399 3 -5 3 -3 -39.6597 66.979 3 -5 -3 -3 28.2167 32.0145 6 -5 3 -3 89.8158 38.3453 6 -5 3 -3 31.5328 37.0457 44 -5 3 -3 57.6335 44.2973 39 -5 3 -3 69.5131 41.3329 15 -5 -3 -3 -4.99978 35.9516 17 -5 3 -3 20.0498 34.1205 17 -5 -3 -3 6.30978 42.3179 15 5 -3 3 36.1074 51.2375 26 -5 -3 -3 -5.13524 40.3589 24 -5 3 -3 32.7027 40.6868 13 -5 -3 -3 6.02724 43.3341 12 -5 3 -3 29.9616 41.3715 12 -5 3 -4 363.344 56.525 7 -5 3 -4 297.243 53.0465 39 -5 3 -4 277.192 53.5456 44 -5 3 -4 352.366 53.4728 15 -5 -3 -4 239.696 47.655 17 -5 3 -4 332.245 51.4669 17 -5 -3 -4 356.298 53.9075 24 -5 3 -4 342.439 57.0431 13 -5 -3 -4 227.086 54.1286 12 -5 3 -4 452.169 59.4264 12 -5 3 -5 1965.36 118.998 7 -5 3 -5 1870.12 120.236 44 5 3 5 2031.2 192.62 27 -5 -3 -5 2133.33 118.021 17 -5 3 -5 1941.83 116.118 17 -5 3 -5 2036.97 117.595 15 -5 -3 -5 2229.14 127.721 12 -5 3 -5 2123.89 126.251 12 -5 -3 -6 385.259 50.9909 17 -5 3 -6 335.136 52.4111 17 -5 3 -6 241.382 43.9643 15 -5 3 -6 327.039 56.2207 44 -5 3 -6 346.308 56.5197 13 -5 -3 -6 334.804 57.8745 12 -5 3 -6 237.021 51.91 12 -5 3 -7 889.861 75.5649 7 -5 3 -7 853.756 77.0664 44 -5 -3 -7 835.148 71.4269 17 -5 3 -7 899.56 72.0617 17 -5 -3 -7 993.347 77.801 24 -5 -3 -7 914.746 80.3025 12 -5 3 -7 862.213 76.6681 12 -5 3 -7 1021.43 79.6365 13 -5 3 -8 89.219 41.8072 7 -5 3 -8 96.9414 44.0855 44 -5 -3 -8 125.006 37.6973 17 -5 3 -8 210.083 40.8137 17 -5 -3 -8 102.965 45.8539 15 -5 -3 -8 205.755 43.87 24 -5 3 -8 114.637 40.8675 13 -5 -3 -8 32.1524 43.4258 12 -5 3 -8 75.1448 40.0245 12 -5 -3 -9 307.26 51.4242 15 -5 3 -9 289.241 49.6082 44 -5 3 -9 282.705 42.9179 13 -5 -3 -9 293.421 44.9012 13 -5 -3 -9 215.243 44.0676 12 -5 3 -9 286.532 48.0786 12 -5 3 -9 248.568 43.6204 7 -5 -3 -10 209.529 35.1627 13 -5 -3 -10 239.944 38.983 12 -5 3 -10 187.966 37.4505 12 -5 3 -10 230.434 43.4862 44 -5 -3 -10 249.862 43.5684 15 -5 -3 -11 257.127 35.0193 15 -5 -3 -11 162.691 23.6076 13 -5 3 -11 255.465 34.0952 12 5 -4 -15 1023.04 58.114 19 -5 -4 14 1428.21 78.8819 30 5 -4 -14 1587.96 84.3508 38 5 -4 -14 1662.14 88.8034 19 5 4 -14 1706.97 85.4807 19 5 -4 -13 25.9272 25.6006 35 5 4 -13 -12.905 25.8927 35 -5 -4 13 29.0625 29.9053 30 -5 4 13 -10.2926 26.5121 30 5 -4 -13 -12.042 30.8435 38 5 4 -13 16.6124 33.8481 19 5 -4 -13 -26.0432 35.554 19 -5 -4 12 2079.04 110.186 30 5 -4 -12 1930.32 109.566 38 5 -4 -12 2099.33 105.883 35 5 4 -12 1945.34 104.136 35 5 4 -12 2106.22 115.96 19 -5 -4 11 9.88011 33.1735 30 -5 4 11 57.1073 36.197 30 5 -4 -11 113.997 40.7528 38 5 -4 -11 66.6043 34.1693 35 5 4 -11 26.5038 36.9457 35 5 4 -11 58.0204 43.0758 19 5 -4 -11 62.1939 46.5805 19 -5 -4 10 53.158 38.538 30 -5 4 10 72.029 39.1627 30 5 -4 -10 28.8346 36.1661 35 5 -4 -10 49.2645 40.9259 38 5 4 -10 81.2207 35.0936 35 5 -4 -10 119.318 36.072 23 5 4 -10 87.6929 46.2453 19 5 -4 -10 89.5473 49.2079 19 -5 -4 9 38.6227 36.7528 30 -5 4 9 26.768 35.1197 30 -5 4 9 94.4112 79.7303 29 5 4 -9 72.3262 33.1011 37 5 -4 -9 72.3678 37.6366 38 5 -4 -9 5.02851 34.0048 35 5 4 -9 44.9621 39.2842 35 -5 -4 9 30.9174 29.741 24 5 -4 -9 36.4282 44.2324 19 5 -4 -9 108.217 77.2937 22 5 4 -9 110.793 53.1409 19 5 -4 -8 119.334 47.4594 19 -5 -4 8 72.4657 41.4315 30 -5 4 8 97.7158 40.8406 30 -5 4 8 -47.6473 75.6249 29 5 -4 -8 107.884 39.5639 35 5 4 -8 102.018 42.281 35 5 -4 -8 76.8041 41.5142 38 -5 -4 8 -22.6274 64.2596 28 -5 4 8 44.0877 65.1572 28 -5 -4 8 83.1265 33.9779 24 -5 -4 8 145.159 74.0874 5 -5 4 8 63.1386 75.1908 5 5 -4 -7 22.8791 42.1851 19 5 4 -7 39.0525 45.8798 19 -5 -4 7 38.7823 35.7557 30 -5 4 7 27.0378 36.2782 30 5 -4 -7 79.2274 42.6289 38 -5 -4 7 -22.3991 66.1644 28 -5 4 7 -43.7303 67.0251 28 -5 -4 7 69.3135 34.4269 24 -5 -4 7 20.4692 64.9491 5 -5 4 7 83.0876 79.8152 5 5 4 -6 6.32661 45.4789 19 5 -4 -6 37.5069 39.5063 19 -5 -4 6 59.9969 39.2096 30 -5 4 6 -21.3278 35.7558 30 5 -4 -6 15.0852 35.9138 38 -5 -4 6 21.9928 72.0616 28 -5 4 6 43.0032 68.2154 28 -5 -4 6 13.3187 33.1373 24 -5 -4 6 60.2555 67.837 5 -5 4 6 40.7393 68.7977 5 5 -4 -5 270.353 45.5255 19 5 4 -5 291.91 57.774 19 5 -4 -5 241.352 42.6662 38 -5 -4 5 256.74 47.8434 30 -5 4 5 251.505 45.9021 30 -5 -4 5 64.505 70.8902 28 -5 4 5 231.579 81.2684 28 -5 -4 5 211.856 41.3747 24 -5 -4 5 218.36 42.7931 2 -5 4 5 274.017 46.6252 2 -5 -4 5 137.122 75.6733 5 -5 4 5 39.7175 71.3425 5 5 4 -4 406.156 57.7499 19 5 -4 -4 365.936 47.8438 38 -5 -4 4 267.858 45.9564 30 -5 4 4 335.007 51.0848 30 -5 4 4 247.343 89.1771 29 -5 -4 4 425.065 53.0516 2 -5 -4 4 326.029 91.07 5 -5 4 4 441.794 52.4168 2 -5 4 4 174.898 78.9384 5 -5 -4 4 294.697 93.657 28 -5 4 4 475.002 103.626 28 -5 -4 4 337.63 49.8264 24 5 4 -4 616.874 102.018 26 -5 -4 4 258.342 91.4555 16 -5 4 4 259.654 90.4439 16 5 4 -3 297.315 53.7789 19 -5 -4 3 451.154 88.4875 16 -5 4 3 374.53 88.919 16 -5 -4 3 167.758 57.6493 10 -5 4 3 332.565 101.535 29 -5 -4 3 160.68 46.2629 30 -5 4 3 300.635 47.9351 30 -5 -4 3 263.315 47.8576 24 5 4 -3 314.926 85.2859 26 -5 -4 3 227.296 78.1237 5 -5 4 3 479.539 99.799 5 -5 -4 3 208.111 44.8135 2 -5 4 3 285.551 44.4773 2 -5 -4 2 11953.4 459.678 2 -5 4 2 12342.1 459.881 2 -5 4 2 12684.6 584.588 5 -5 4 2 11595.4 451.821 13 -5 -4 2 12132.4 583.139 16 -5 4 2 11621 574.266 16 -5 4 2 11826.4 467.483 39 -5 4 2 11506.6 591.225 29 -5 -4 2 12029.9 465.146 30 -5 4 2 11833.8 463.258 30 5 -4 -2 11301.5 571.896 26 -5 -4 2 11975.6 460.276 24 5 4 -2 11453.3 563.523 26 -5 -4 2 10934.1 480.46 10 -5 -4 1 6622.46 358.589 3 -5 4 1 6444.55 358.614 3 -5 -4 1 6088.98 251.771 6 -5 4 1 6280.74 253.406 6 -5 -4 1 5918.09 254.471 2 -5 4 1 6515.58 256.361 2 -5 4 1 5794.63 250.991 13 -5 -4 1 5502.01 349.12 16 -5 4 1 6059.57 358.624 16 -5 4 1 5712.44 261.723 39 -5 -4 1 6303.66 262.07 30 -5 4 1 6011.3 258.645 30 -5 -4 1 6118.62 256.765 24 5 -4 -1 6407.68 362.213 26 5 4 -1 6033.41 353.821 26 -5 -4 1 5015.99 270.038 10 -5 -4 0 163.402 70.0704 3 -5 4 0 126.812 72.9998 3 -5 -4 0 192.954 40.5943 6 -5 4 0 186.148 43.6482 6 -5 -4 0 173.843 45.2703 15 -5 -4 0 118.189 77.6661 16 -5 4 0 98.884 74.5325 16 -5 4 0 226.596 51.4487 39 -5 -4 0 208.246 46.0148 30 -5 4 0 200.947 45.7456 30 -5 -4 0 235.688 45.9871 24 5 -4 0 188.819 77.6174 26 -5 4 0 188.41 42.0833 13 -5 -4 0 207.644 57.8482 10 -5 -4 -1 13577.5 646.701 3 -5 4 -1 14358.2 653.468 3 -5 -4 -1 14257.2 536.079 6 -5 4 -1 14160.1 535.826 6 -5 4 -1 14749.2 542.765 13 -5 -4 -1 13952.8 550.187 15 -5 4 -1 14191.8 540.675 44 -5 4 -1 13746.5 547.002 39 -5 -4 -1 13993.5 543.713 30 -5 -4 -1 14279.7 542.837 24 5 -4 1 13316.9 643.517 26 -5 -4 -1 13199.7 556.203 10 -5 4 -2 1373.23 91.1297 44 -5 4 -2 1129.87 89.2373 39 -5 -4 -2 1339.47 98.2582 15 -5 -4 -2 1385.89 157.056 3 -5 4 -2 1215.08 145.142 3 -5 -4 -2 1476.21 88.4509 6 -5 4 -2 1309.55 84.8997 6 -5 -4 -2 1177.82 89.4495 24 5 -4 2 1256.74 146.021 26 -5 -4 -2 1239.59 99.2759 10 -5 4 -2 1370.51 92.0923 13 -5 4 -3 15874.1 614.946 44 -5 4 -3 16116.5 617.814 39 -5 -4 -3 16630 624.099 15 -5 -4 -3 16506.4 610.166 17 -5 4 -3 15748.8 607.635 17 -5 4 -3 16238.4 616.82 7 -5 -4 -3 14676.1 609.214 24 -5 4 -3 16212.1 616.507 13 -5 -4 -3 16676.2 626.592 10 -5 4 -4 1833.29 113.673 44 -5 4 -4 1635.61 112.068 39 -5 -4 -4 2021.09 123.945 15 -5 -4 -4 1919.23 109.238 17 -5 4 -4 2032.39 111.189 17 -5 4 -4 1932.88 116.667 7 5 4 4 1843.21 189.458 27 -5 -4 -4 2076.14 118.173 12 -5 4 -4 1853.34 114.905 12 -5 -4 -4 1691.06 114.997 10 -5 4 -4 1646.3 112.258 13 -5 4 -5 1571.56 101.931 44 -5 -4 -5 1628.61 106.451 15 -5 -4 -5 1214.34 86.9124 17 -5 4 -5 1314.66 88.9619 17 -5 -4 -5 1231.76 92.2422 24 5 4 5 1294.37 161.036 27 -5 -4 -5 1360.74 97.0324 12 -5 4 -5 1331.42 95.0563 12 -5 4 -6 157.803 48.2631 44 -5 -4 -6 169.346 39.5813 17 -5 4 -6 165.03 42.3985 17 -5 -4 -6 137.675 51.6238 15 -5 4 -6 197.694 49.8923 7 -5 -4 -6 163.901 47.6744 24 -5 4 -6 142.116 47.3551 13 -5 -4 -6 293.851 49.3674 12 -5 4 -6 157.84 43.5015 12 -5 4 -7 536.697 66.032 44 -5 -4 -7 701.847 73.1448 15 -5 -4 -7 655.042 60.1029 17 -5 4 -7 616.454 58.7664 17 -5 4 -7 674.644 65.6125 13 -5 -4 -7 576.577 62.5098 24 -5 -4 -7 738.706 67.6565 12 -5 4 -7 738.633 66.3783 12 -5 4 -7 468.211 61.4835 7 -5 4 -8 511.996 62.0754 44 -5 -4 -8 420.488 50.8313 24 -5 4 -8 437.989 54.2487 7 -5 4 -8 367.711 51.6704 13 -5 -4 -8 559.433 58.9057 12 -5 4 -8 536.913 56.9193 12 -5 4 -9 3.67955 31.8997 7 -5 -4 -9 -28.3609 32.1786 12 -5 4 -9 -8.15459 33.233 12 -5 4 -9 -13.7733 39.2643 44 -5 -4 -10 338.017 38.2822 13 -5 4 -10 374.954 41.0199 12 -5 4 -10 437.128 49.1012 44 5 -5 -14 256.595 31.9248 38 5 5 -14 234.595 31.0752 19 5 -5 -14 221.044 34.3969 19 -5 -5 13 25.4822 23.3488 30 5 -5 -13 33.1219 27.8269 38 5 5 -13 80.7275 34.1661 19 -5 -5 12 1254.45 75.9241 30 5 -5 -12 1292.44 83.2369 38 5 -5 -12 1194.98 72.1697 35 5 5 -12 1226.08 72.5364 35 5 -5 -12 1467.57 90.8225 19 5 5 -12 1241.33 86.0498 19 -5 -5 11 101.941 34.5595 30 5 -5 -11 79.5386 33.1015 35 5 5 -11 90.1314 31.4992 35 5 -5 -11 64.7251 34.9602 38 5 5 -11 98.0356 45.1457 19 5 -5 -11 42.3362 43.4407 19 -5 -5 10 37.564 35.6735 30 -5 5 10 22.3183 31.0309 30 5 -5 -10 54.7136 32.7115 35 5 5 -10 -4.17125 28.999 35 5 -5 -10 58.9867 41.4431 38 -5 -5 10 -25.5603 29.1595 24 5 -5 -10 11.9552 30.8014 23 5 5 -10 54.1428 45.4355 19 5 -5 -10 22.6693 44.7722 19 -5 -5 9 4.97756 34.6054 30 -5 5 9 57.1349 35.9651 30 5 5 -9 22.023 32.0774 37 5 -5 -9 40.481 34.3741 35 5 5 -9 -31.1848 33.8502 35 5 -5 -9 5.55881 35.8617 38 -5 -5 9 24.7001 32.1771 24 5 -5 -9 49.9449 37.0137 23 5 5 -9 57.4461 53.3247 19 5 -5 -9 64.1058 48.4537 19 -5 -5 8 -5.1203 33.037 30 -5 5 8 24.5981 37.3813 30 -5 5 8 71.4352 70.3304 29 5 5 -8 48.0678 37.9809 37 5 -5 -8 38.98 36.5017 38 5 -5 -8 42.0989 35.7498 35 5 5 -8 18.5201 31.7435 35 -5 -5 8 22.1771 32.9118 24 5 -5 -8 22.4685 71.2851 22 5 -5 -8 17.3801 41.651 19 5 5 -7 203.87 56.4249 19 5 -5 -7 273.99 52.2973 19 -5 -5 7 185.673 43.6573 30 -5 5 7 184.029 41.3475 30 -5 5 7 262.828 92.0692 29 5 -5 -7 208.734 41.3616 35 5 5 -7 239.339 44.2266 35 5 -5 -7 251.861 49.2265 38 -5 -5 7 272.614 86.1746 28 -5 -5 7 190.294 41.7237 24 -5 -5 7 204.725 40.4093 2 -5 5 7 117.33 37.4499 2 -5 5 7 174.488 81.2827 5 5 5 -6 84.1949 48.4423 19 5 -5 -6 52.6239 39.171 19 5 -5 -6 42.4081 38.4889 38 -5 -5 6 128.251 39.778 30 -5 5 6 59.5239 36.2623 30 -5 5 6 118.585 82.4871 29 -5 -5 6 186.736 77.9515 28 -5 -5 6 166.681 44.2552 24 -5 -5 6 126.955 38.1981 2 -5 5 6 85.4532 36.2446 2 -5 5 6 76.5307 76.8461 5 5 -5 -5 855.013 70.5949 19 5 5 -5 938.613 85.439 19 5 -5 -5 906.548 73.7615 38 -5 5 5 907.082 129.669 16 -5 -5 5 871.702 71.9104 30 -5 5 5 1032.12 74.3408 30 -5 5 5 888.959 144.56 29 -5 -5 5 592.467 114.505 28 -5 -5 5 1204.91 79.1826 24 -5 -5 5 965.453 71.4235 2 -5 5 5 949.385 71.2865 2 -5 5 5 771.54 123.795 5 5 5 -4 1489.01 102.82 19 5 -5 -4 1395.32 91.3395 38 -5 5 4 1408.75 158.23 16 -5 -5 4 1425.88 94.2343 30 -5 5 4 1522.67 95.7935 30 -5 5 4 1174.17 160.57 29 -5 -5 4 1427.71 93.6019 24 -5 -5 4 1694.7 94.2974 2 -5 5 4 1448.93 91.2265 2 -5 5 4 1596.5 164.851 5 -5 -5 3 1358.99 117.14 10 5 -5 -3 1582.2 96.2406 38 -5 5 3 1681.13 187.625 29 -5 -5 3 1668.99 102.006 30 -5 5 3 1703.82 100.877 30 -5 -5 3 1782.59 98.9117 2 -5 5 3 1801.99 100.459 2 -5 5 3 1694.81 174.474 5 -5 -5 3 1565.75 99.7917 24 -5 5 3 1583.32 163.421 16 -5 -5 2 17064.8 759.442 3 -5 5 2 16743.7 755.952 3 -5 -5 2 17325.6 649.191 6 -5 5 2 17101.9 650.17 6 -5 -5 2 18184.9 654.197 2 -5 5 2 17751.8 652.804 2 -5 5 2 16502.2 770.281 16 -5 5 2 18376 666.89 39 -5 5 2 17630 806.637 29 -5 -5 2 17364.7 657.67 30 -5 5 2 17190 656.055 30 -5 -5 2 17842 659.714 24 5 5 -2 16078.2 757.93 26 -5 -5 2 16342.3 681.896 10 -5 -5 1 618.961 98.9252 3 -5 5 1 564.102 94.3109 3 -5 -5 1 674.26 56.265 6 -5 5 1 675.925 58.3349 6 -5 5 1 649.469 60.2627 44 -5 5 1 592.343 66.1985 39 -5 -5 1 511.944 57.6684 30 -5 5 1 608.803 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3 9 462.846 43.7129 30 7 -3 -9 492.479 39.9126 23 7 3 -9 630.574 50.4575 19 7 -3 -8 16.751 28.3863 35 7 3 -8 -6.62336 27.7965 35 -7 3 8 39.5888 27.1581 39 -7 -3 8 -22.0791 28.2761 30 -7 3 8 -10.6608 28.2214 30 -7 -3 8 9.00413 26.3644 6 -7 3 8 9.13831 25.1996 6 -7 -3 8 -13.0385 26.0241 2 -7 3 8 19.3551 27.2048 2 7 3 -8 -6.95312 30.0026 19 7 -3 -7 1728.32 94.3579 35 7 3 -7 1671.61 93.4183 35 -7 -3 7 1606.6 94.8064 30 -7 3 7 1652.28 94.8649 30 -7 -3 7 1780.76 92.4127 6 -7 3 7 1750.12 92.7785 6 -7 -3 7 1908.55 95.6198 2 -7 3 7 1796.17 93.6416 2 -7 3 7 1578.06 92.1812 39 7 3 -7 1706.34 93.3531 19 -7 -3 6 1163.03 74.9525 30 -7 3 6 993.782 71.8849 30 -7 -3 6 1119.62 69.5194 6 -7 3 6 924.976 67.308 6 -7 -3 6 1087.97 71.3166 2 -7 3 6 905.388 66.2007 2 -7 3 6 962.069 71.7113 39 7 3 -6 983.627 66.7974 19 -7 -3 5 103.693 33.3165 6 -7 3 5 37.5093 30.6647 6 -7 3 5 17.6255 34.5146 39 -7 -3 5 104.106 37.3383 30 -7 3 5 92.8702 35.9408 30 -7 -3 4 494.947 49.9897 6 -7 3 4 457.888 50.4641 6 -7 3 4 510.828 55.9284 39 -7 -3 4 437.85 52.5462 30 -7 3 4 456.4 51.5914 30 -7 -3 3 -7.70915 30.7756 6 -7 3 3 15.5766 30.0939 6 -7 3 3 -42.598 34.8941 39 -7 -3 3 -18.8986 34.3991 30 -7 3 3 -4.63469 31.3071 30 -7 3 2 1219.6 81.5323 39 -7 -3 2 1219.9 75.6655 6 -7 3 2 1154.38 74.809 6 -7 -3 2 1000.51 64.6479 24 -7 3 1 100.089 43.5043 39 -7 -3 1 128.929 36.0707 6 -7 3 1 118.713 36.6908 6 -7 -3 1 127.252 31.983 24 -7 -3 0 797.194 61.7614 17 -7 3 0 763.484 61.3643 17 -7 -3 0 716.8 54.9141 24 -7 3 0 717.569 55.5245 7 -7 -3 -1 1935.01 99.0093 17 -7 3 -1 1811.45 97.0604 17 -7 -3 -1 1740.05 92.9128 13 -7 -3 -1 1766.19 93.2456 24 -7 3 -1 1808.47 94.2817 7 -7 -3 -2 76.8041 30.9666 17 -7 3 -2 48.9717 30.2234 17 -7 -3 -2 32.7579 28.9372 13 -7 -3 -2 33.9847 26.8228 24 -7 3 -2 23.2428 30.444 7 -7 -3 -3 164.183 32.5332 17 -7 3 -3 117.052 33.0054 17 -7 -3 -3 133.149 31.9321 13 -7 -3 -3 132.533 30.67 24 -7 3 -3 117.403 32.4844 7 -7 -3 -4 120.52 28.1422 17 -7 3 -4 186.651 31.9003 17 -7 -3 -4 125.296 31.2758 13 -7 -3 -4 165.165 29.5947 24 -7 -3 -5 25.2051 22.9137 13 -7 -3 -5 46.8114 21.2326 17 -7 3 -5 8.93917 20.8894 17 -7 -3 -6 693.064 42.9037 13 -7 4 10 6746.64 256.499 6 7 4 -10 7084.9 265.974 19 -7 -4 9 620.577 42.1895 6 -7 4 9 693.197 44.8212 6 -7 4 9 513.791 44.138 39 7 -4 -9 674.917 43.9816 23 7 4 -9 809.984 53.0546 19 -7 -4 8 2073.12 96.11 6 -7 4 8 2272.09 98.3673 6 -7 -4 8 2147.43 98.7184 2 -7 4 8 2213.36 98.8289 2 7 -4 -8 1796.99 95.8639 35 7 4 -8 2042.87 97.6865 35 -7 4 8 2082.02 102.17 39 -7 -4 8 1975.53 99.8394 30 -7 4 8 1987.83 98.5684 30 7 -4 -8 2015.24 98.9547 23 7 4 -8 2180.44 105.001 19 7 4 -7 32.3458 26.6098 37 7 -4 -7 3.13625 25.4372 35 7 4 -7 27.8607 28.1274 35 -7 4 7 7.31072 27.2836 39 -7 -4 7 34.5691 28.6031 30 -7 4 7 3.28687 26.5219 30 -7 -4 7 8.35538 24.1496 6 -7 4 7 51.2629 26.8073 6 7 4 -7 -20.5126 29.2417 19 7 -4 -6 202.153 36.3665 35 7 4 -6 226.741 36.7832 35 -7 -4 6 150.038 34.9989 30 -7 4 6 240.761 38.296 30 -7 -4 6 184.676 33.3483 6 -7 4 6 213.091 35.1881 6 -7 4 6 308.544 41.2632 39 7 4 -6 194.96 36.4136 19 -7 -4 5 845.309 57.2729 6 -7 4 5 841.376 58.1075 6 -7 4 5 652.721 61.4645 39 -7 -4 5 788.758 60.9531 30 -7 4 5 641.163 57.5318 30 -7 -4 4 447.185 44.8899 6 -7 4 4 394.318 44.5768 6 -7 4 4 444.195 51.8362 39 -7 -4 4 389.779 47.495 30 -7 4 4 404.515 47.7463 30 -7 4 3 1212.39 85.4548 39 -7 -4 3 1399.34 78.9805 6 -7 4 3 1337.84 78.6261 6 -7 -4 3 1356.54 74.4634 24 -7 -4 2 1398.11 78.7856 6 -7 4 2 1287.7 79.2077 6 -7 -4 2 1395.91 77.911 24 -7 -4 1 187.663 35.9738 24 -7 -4 1 306.896 40.7214 17 -7 4 1 247.849 38.5362 17 -7 -4 0 3142.69 146.058 17 -7 4 0 3451.26 148.967 17 -7 4 0 3107.81 153.903 39 -7 -4 0 3254.33 146.178 24 -7 4 0 3366.57 145.076 7 -7 4 -1 6.37031 27.9213 7 -7 4 -1 66.5946 33.458 39 -7 -4 -1 41.8001 27.6885 17 -7 4 -1 100.028 30.8814 17 -7 -4 -1 47.7153 29.6551 24 -7 -4 -1 79.6009 28.2263 13 -7 -4 -2 170.903 31.4256 17 -7 4 -2 136.077 30.5044 17 -7 -4 -2 179.316 31.953 13 -7 -4 -2 166.156 32.4778 24 -7 4 -2 159.743 33.8325 7 -7 -4 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232.166 19 -7 -6 5 5756.4 228.444 24 -7 -6 4 1125.3 63.0755 24 -7 6 4 1054.37 69.2691 39 -7 -6 3 1854.96 88.5314 24 -7 6 3 1625.42 92.7053 39 -7 -6 2 34.5524 24.8855 24 -7 6 2 44.3715 29.2398 39 -7 -6 1 75.5705 28.3018 24 -7 6 1 3.58919 27.1378 39 -7 6 0 17.9571 25.7337 7 -7 6 0 60.9531 28.3634 39 -7 -6 0 82.8942 28.6559 24 7 -6 0 77.9237 23.7803 23 -7 -6 -1 304.751 35.6724 24 -7 6 -1 254.823 34.2841 7 -7 -6 -2 1484.33 75.464 24 -7 6 -2 1440.53 74.1551 7 -7 -6 -2 1386.4 70.1373 13 -7 -6 -3 98.4718 23.2582 24 -7 6 -3 60.0435 23.1344 7 -7 -6 -3 78.2999 21.0263 13 -7 -6 -4 563.122 37.1723 24 -7 6 -4 566.645 38.4091 7 7 -7 -8 287.292 25.9261 23 7 7 -7 1071.61 60.0823 19 7 -7 -7 1251.88 62.0756 23 -7 7 6 1158.03 65.6046 39 7 -7 -6 1299.89 66.1898 23 7 7 -6 1121.9 61.644 19 -7 -7 5 7214.49 279.687 24 7 7 -5 7076.63 280.848 19 7 7 -5 7691.41 287.977 37 -7 -7 4 688.794 46.1405 24 7 -7 -4 730.508 50.3986 23 -7 7 4 713.382 51.9743 39 7 7 -4 845.458 53.5351 37 -7 7 3 181.05 31.5914 39 -7 -7 3 275.221 31.0235 24 7 -7 -3 221.34 32.1236 23 -7 -7 2 1090.25 62.7699 24 7 -7 -2 1014.25 61.281 23 -7 7 2 1168.26 67.1543 39 7 7 -2 1183.62 66.2531 37 -7 -7 1 876.037 53.8478 24 7 -7 -1 801.033 49.0911 23 -7 7 1 775.358 53.9154 39 7 7 -1 838.165 54.2506 37 -7 7 0 -14.7799 22.8135 7 -7 -7 0 17.1738 23.263 24 -7 7 -1 540.54 40.1539 7 -7 -7 -1 590.62 42.0109 24 -7 7 -2 9.75684 20.4796 7 -7 -7 -2 26.5208 19.5698 24 -7 -7 -3 351.663 28.699 24 7 -8 -5 174.103 25.7848 23 7 -8 -4 -12.1379 19.255 23 -7 -8 4 -3.57864 16.6487 24 7 -8 -3 -11.613 18.8966 23 -7 -8 3 35.2707 18.9276 24 7 -8 -2 -3.38963 16.6618 23 -7 -8 2 26.4323 19.7787 24 -7 -8 1 304.538 29.2121 24 -7 -8 0 409.357 32.3293 24 -7 -8 -1 1841.21 81.2116 24 -8 0 7 16.2133 18.2611 6 -8 0 6 1518.32 73.0281 6 -8 0 5 -22.2738 21.9835 6 -8 0 4 9.33967 22.2244 6 -8 0 3 -10.0798 22.1381 17 -8 0 2 39.8934 22.7852 17 -8 0 1 4.79114 21.4062 17 -8 0 0 -17.768 21.3029 17 -8 0 -1 19.661 18.9995 17 -8 -1 7 502.263 34.7272 6 -8 1 7 524.484 35.7719 6 -8 -1 6 929.294 51.435 6 -8 1 6 892.908 50.8325 6 -8 -1 5 3767.25 157.71 6 -8 1 5 4112.74 159.575 6 -8 -1 4 554.766 41.5994 6 -8 1 4 655.818 43.89 6 -8 -1 3 -12.2071 21.8222 17 -8 1 3 -19.5539 20.91 17 -8 -1 2 2.41459 21.0249 17 -8 1 2 4.83452 22.3139 17 -8 -1 1 944.923 54.3222 17 -8 1 1 925.093 54.2605 17 -8 -1 0 79.1693 22.0179 17 -8 1 0 147.811 24.4279 17 -8 -1 -1 1.88128 16.8882 17 -8 1 -1 28.2567 17.6006 17 -8 -2 6 280.886 26.1618 6 -8 2 6 238.983 25.9061 6 -8 -2 5 34.3864 19.5214 6 -8 2 5 36.8998 20.5338 6 -8 -2 4 60.3841 21.3263 17 -8 2 4 73.8934 22.4903 6 -8 -2 3 57.2934 21.779 17 -8 2 3 72.9282 22.2131 17 -8 -2 2 258.691 29.7039 17 -8 2 2 233.248 28.2405 17 -8 -2 1 20.7161 19.5237 17 -8 2 1 39.4707 20.0169 17 -8 -2 0 -1.88781 17.7719 17 -8 2 0 30.2969 17.4854 17 -8 -3 4 6.88262 16.1956 17 -8 3 4 10.4067 16.8726 17 -8 -3 3 684.942 40.0308 17 -8 3 3 589.86 38.7647 17 -8 -3 2 224.387 24.0992 17 -8 3 2 229.388 24.6216 17