#------------------------------------------------------------------------------ #$Date: 2020-04-20 23:32:45 +0300 (Mon, 20 Apr 2020) $ #$Revision: 250943 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/78/1557821.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557821 loop_ _publ_author_name 'Yang, Wei-Qun' 'Shao, Xue-Hua' 'Deng, Fang' 'Hu, Li-Jun' 'Xiong, Yu' 'Huang, Xiao-Jun' 'Fan, Chun-Lin' 'Jiang, Ren-Wang' 'Ye, Wen-Cai' 'Wang, Ying' _publ_section_title ; Unprecedented Quassinoids from Eurycoma longifolia: Biogenetic Evidence and Antifeedant Effects ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.0c00244 _journal_year 2020 _chemical_absolute_configuration ad _chemical_formula_moiety 'C20 H28 O8' _chemical_formula_sum 'C20 H28 O8' _chemical_formula_weight 396.42 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2019-06-17 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.26550(10) _cell_length_b 10.19270(10) _cell_length_c 24.3238(3) _cell_measurement_reflns_used 9645 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 73.6330 _cell_measurement_theta_min 4.2990 _cell_volume 1801.30(4) _computing_cell_refinement 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 100.00(10) _diffrn_detector_area_resol_mean 5.2684 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -69.00 32.00 1.00 1.00 -- -41.11 57.00-180.00 101 2 \w 23.00 97.00 1.00 1.00 -- 41.11-125.00 90.00 74 3 \w 1.00 82.00 1.00 1.00 -- 41.11 -99.00 -60.00 81 4 \w 94.00 178.00 1.00 1.00 -- 106.95 125.00 -30.00 84 5 \w 94.00 178.00 1.00 1.00 -- 106.95 125.00 60.00 84 6 \w 94.00 178.00 1.00 1.00 -- 106.95 125.00-180.00 84 7 \w 28.00 113.00 1.00 1.00 -- 106.95-105.00 110.00 85 8 \w 31.00 135.00 1.00 1.00 -- 106.95 -30.00-180.00 104 9 \w 81.00 178.00 1.00 1.00 -- 106.95 45.00 150.00 97 10 \w -113.00 -13.00 1.00 1.00 -- -41.11 -57.00 60.00 100 11 \w -113.00 -13.00 1.00 1.00 -- -41.11 -57.00-150.00 100 12 \w 79.00 178.00 1.00 1.00 -- 106.95 30.00 -60.00 99 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0243 _diffrn_reflns_av_unetI/netI 0.0203 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 11355 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.978 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.762 _diffrn_reflns_theta_min 3.634 _exptl_absorpt_coefficient_mu 0.943 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.69247 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43f (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.462 _exptl_crystal_description block _exptl_crystal_F_000 848 _exptl_crystal_size_max 0.17 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.11 _refine_diff_density_max 0.225 _refine_diff_density_min -0.232 _refine_diff_density_rms 0.048 _refine_ls_abs_structure_details ; Flack x determined using 1440 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.05(6) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.072 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 261 _refine_ls_number_reflns 3565 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.072 _refine_ls_R_factor_all 0.0318 _refine_ls_R_factor_gt 0.0315 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0514P)^2^+0.4118P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0832 _refine_ls_wR_factor_ref 0.0836 _reflns_Friedel_coverage 0.711 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.967 _reflns_number_gt 3526 _reflns_number_total 3565 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file np0c00244_si_002.cif _cod_data_source_block 19-el2 _cod_database_code 1557821 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Ternary CH refined with riding coordinates: C1(H1), C4(H4), C5(H5), C9(H9), C11(H11), C12(H12), C13(H13), C15(H15) 2.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C6(H6A,H6B) 2.c Idealised Me refined as rotating group: C18(H18A,H18B,H18C), C19(H19A,H19B,H19C), C29(H29A,H29B,H29C), C30(H30A,H30B, H30C) 2.d Idealised tetrahedral OH refined as rotating group: O2(H2), O3(H3), O7(H7), O8(H8) ; _shelx_res_file ; TITL 19-el2_a.res in P2(1)2(1)2(1) 19-el2.res created by SHELXL-2017/1 at 22:45:59 on 16-Jun-2019 REM Old TITL REM SHELXT solution in P2(1)2(1)2(1): R1 0.078, Rweak 0.019, Alpha 0.002 REM 4.066 for 24 systematic absences, Orientation as input REM Flack x = -0.034 ( 0.058 ) from 1462 Parsons' quotients REM Formula found by SHELXT: C30 O8 CELL 1.54184 7.2655 10.1927 24.3238 90 90 90 ZERR 4 0.0001 0.0001 0.0003 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H O UNIT 80 112 32 L.S. 20 PLAN 20 list 4 fmap 2 acta REM REM REM WGHT 0.051400 0.411800 FVAR 0.63881 C1 1 0.646314 0.384867 0.708561 11.00000 0.00893 0.01706 = 0.01142 0.00125 -0.00079 0.00136 AFIX 13 H1 2 0.546651 0.445882 0.717690 11.00000 -1.20000 AFIX 0 C2 1 0.568543 0.245608 0.705315 11.00000 0.00955 0.01792 = 0.01420 0.00123 0.00371 0.00160 C3 1 0.427803 0.220873 0.661504 11.00000 0.01601 0.01535 = 0.01991 0.00290 -0.00244 -0.00217 AFIX 23 H3A 2 0.317520 0.271323 0.669135 11.00000 -1.20000 H3B 2 0.395002 0.128629 0.661074 11.00000 -1.20000 AFIX 0 C4 1 0.507051 0.260868 0.605143 11.00000 0.01524 0.01345 = 0.01688 -0.00043 -0.00251 -0.00114 AFIX 13 H4 2 0.614385 0.205439 0.597668 11.00000 -1.20000 AFIX 0 C5 1 0.573100 0.404489 0.608632 11.00000 0.01153 0.01335 = 0.01254 -0.00082 -0.00089 -0.00068 AFIX 13 H5 2 0.467913 0.456302 0.621465 11.00000 -1.20000 AFIX 0 C6 1 0.625313 0.458438 0.551978 11.00000 0.01447 0.01561 = 0.01240 -0.00172 -0.00193 0.00058 AFIX 23 H6A 2 0.714900 0.399774 0.535549 11.00000 -1.20000 H6B 2 0.516563 0.457249 0.528850 11.00000 -1.20000 AFIX 0 C7 1 0.704183 0.596500 0.551637 11.00000 0.01136 0.01445 = 0.01038 0.00095 0.00099 0.00250 C8 1 0.855433 0.623340 0.593718 11.00000 0.01065 0.01348 = 0.01050 0.00049 -0.00085 0.00005 C9 1 0.774167 0.573911 0.650174 11.00000 0.00933 0.01348 = 0.00958 0.00132 -0.00027 0.00134 AFIX 13 H9 2 0.651435 0.613778 0.650665 11.00000 -1.20000 AFIX 0 C10 1 0.730014 0.423736 0.651932 11.00000 0.00968 0.01381 = 0.01154 0.00059 -0.00021 0.00077 C11 1 0.868536 0.638952 0.699280 11.00000 0.01001 0.01695 = 0.01176 -0.00005 -0.00205 -0.00118 AFIX 13 H11 2 0.806849 0.611330 0.733189 11.00000 -1.20000 AFIX 0 C12 1 0.851458 0.788784 0.693285 11.00000 0.01007 0.01703 = 0.01260 -0.00119 -0.00067 -0.00130 AFIX 13 H12 2 0.910397 0.829645 0.725225 11.00000 -1.20000 AFIX 0 C13 1 0.945467 0.839405 0.642014 11.00000 0.01076 0.01427 = 0.01410 0.00000 0.00028 -0.00085 AFIX 13 H13 2 1.073565 0.809338 0.642710 11.00000 -1.20000 AFIX 0 C14 1 0.851884 0.776617 0.593017 11.00000 0.01204 0.01456 = 0.01040 0.00186 0.00221 -0.00059 C15 1 0.644478 0.802896 0.590973 11.00000 0.01253 0.01147 = 0.01400 -0.00084 -0.00003 0.00122 AFIX 13 H15 2 0.622274 0.879167 0.567355 11.00000 -1.20000 AFIX 0 C16 1 0.555316 0.828126 0.647172 11.00000 0.01274 0.01105 = 0.01529 -0.00082 0.00037 -0.00058 C18 1 0.946623 0.989486 0.639801 11.00000 0.01758 0.01475 = 0.01954 -0.00073 0.00023 -0.00279 AFIX 137 H18A 2 1.009371 1.017916 0.607175 11.00000 -1.50000 H18B 2 1.008931 1.023325 0.671585 11.00000 -1.50000 H18C 2 0.822292 1.021342 0.639256 11.00000 -1.50000 AFIX 0 C19 1 0.898349 0.334644 0.642463 11.00000 0.01147 0.01401 = 0.01785 0.00039 0.00128 0.00080 AFIX 137 H19A 2 0.918839 0.324512 0.603705 11.00000 -1.50000 H19B 2 0.876155 0.250254 0.658687 11.00000 -1.50000 H19C 2 1.004947 0.373650 0.659097 11.00000 -1.50000 AFIX 0 C29 1 0.364573 0.235574 0.560275 11.00000 0.02273 0.02113 = 0.02209 -0.00166 -0.00399 -0.00658 AFIX 137 H29A 2 0.322463 0.146477 0.562628 11.00000 -1.50000 H29B 2 0.419377 0.250279 0.524895 11.00000 -1.50000 H29C 2 0.262254 0.294055 0.565078 11.00000 -1.50000 AFIX 0 C30 1 1.045120 0.570229 0.576475 11.00000 0.01173 0.01770 = 0.01633 0.00122 0.00103 0.00091 AFIX 137 H30A 2 1.100527 0.629370 0.550598 11.00000 -1.50000 H30B 2 1.030606 0.485522 0.559773 11.00000 -1.50000 H30C 2 1.122554 0.562662 0.608297 11.00000 -1.50000 AFIX 0 O1 3 0.624466 0.158991 0.735310 11.00000 0.01894 0.01651 = 0.02218 0.00622 -0.00237 -0.00008 O2 3 0.782212 0.390913 0.749945 11.00000 0.01432 0.02291 = 0.01096 0.00405 -0.00253 -0.00227 AFIX 147 H2 2 0.736770 0.370119 0.779548 11.00000 -1.50000 AFIX 0 O3 3 1.056156 0.601027 0.701593 11.00000 0.01104 0.01981 = 0.01985 -0.00161 -0.00575 -0.00068 AFIX 147 H3 2 1.108909 0.643556 0.725480 11.00000 -1.50000 AFIX 0 O4 3 0.655614 0.825807 0.693444 11.00000 0.01064 0.01599 = 0.01467 -0.00240 0.00134 0.00032 O5 3 0.394178 0.855016 0.649810 11.00000 0.01206 0.02594 = 0.01879 -0.00452 0.00163 0.00260 O6 3 0.560806 0.689060 0.565854 11.00000 0.01127 0.01301 = 0.01410 -0.00172 -0.00116 0.00128 O7 3 0.772785 0.625478 0.498219 11.00000 0.01447 0.02018 = 0.00960 0.00111 -0.00035 0.00016 AFIX 147 H7 2 0.686407 0.633552 0.476787 11.00000 -1.50000 AFIX 0 O8 3 0.935721 0.829951 0.544807 11.00000 0.01531 0.01715 = 0.01187 0.00161 0.00223 -0.00209 AFIX 147 H8 2 0.903142 0.787632 0.517838 11.00000 -1.50000 AFIX 0 HKLF 4 REM 19-el2_a.res in P2(1)2(1)2(1) REM R1 = 0.0315 for 3526 Fo > 4sig(Fo) and 0.0318 for all 3565 data REM 261 parameters refined using 0 restraints END WGHT 0.0514 0.4117 REM Highest difference peak 0.225, deepest hole -0.232, 1-sigma level 0.048 Q1 1 0.5471 0.3332 0.6098 11.00000 0.05 0.22 Q2 1 0.7450 0.7899 0.5993 11.00000 0.05 0.20 Q3 1 0.8631 0.6990 0.5957 11.00000 0.05 0.19 Q4 1 0.8594 0.7132 0.7018 11.00000 0.05 0.19 Q5 1 0.7617 0.4934 0.6496 11.00000 0.05 0.19 Q6 1 0.9068 0.8071 0.6193 11.00000 0.05 0.18 Q7 1 0.9466 0.6006 0.5773 11.00000 0.05 0.17 Q8 1 0.9685 0.9050 0.6388 11.00000 0.05 0.16 Q9 1 0.7875 0.4877 0.7379 11.00000 0.05 0.16 Q10 1 0.6107 0.3110 0.6969 11.00000 0.05 0.16 Q11 1 1.1867 0.6350 0.5796 11.00000 0.05 0.16 Q12 1 0.7966 0.6012 0.5727 11.00000 0.05 0.15 Q13 1 0.9024 0.8087 0.6692 11.00000 0.05 0.15 Q14 1 0.4628 0.6728 0.5508 11.00000 0.05 0.15 Q15 1 0.7098 0.1670 0.7602 11.00000 0.05 0.15 Q16 1 0.6111 0.8254 0.6188 11.00000 0.05 0.14 Q17 1 0.8368 0.5922 0.6728 11.00000 0.05 0.14 Q18 1 0.8160 0.3833 0.6478 11.00000 0.05 0.14 Q19 1 0.5983 0.6230 0.5693 11.00000 0.05 0.14 Q20 1 0.3559 0.1373 0.6764 11.00000 0.05 0.14 ; _shelx_res_checksum 56612 _shelx_hkl_file ; 0 0 2 1102.33 9.97 0 0 -2 1137.39 9.91 0 0 3 1.26 0.22 0 0 3 1.47 0.16 0 0 4 2985.02 25.77 0 0 -4 2980.61 25.57 0 0 4 2998.11 24.33 0 0 5 3.26 0.30 0 0 -5 3.62 0.46 0 0 6 40.59 1.69 0 0 6 38.35 1.08 0 0 -7 0.07 0.22 0 0 7 0.11 0.19 0 0 7 0.50 0.15 0 0 8 882.15 8.75 0 0 8 889.95 11.25 0 0 -8 858.48 10.80 0 0 -9 1.56 0.42 0 0 9 2.22 0.30 0 0 -10 836.12 11.25 0 0 10 857.77 11.78 0 0 -11 1.06 0.40 0 0 11 1.16 0.42 0 0 12 0.43 0.35 0 0 -12 0.40 0.36 0 0 13 0.43 0.34 0 0 -13 0.90 0.42 0 0 14 1651.60 20.85 0 0 -14 1601.49 20.61 0 0 15 0.81 0.37 0 0 -15 -0.21 0.35 0 0 16 8.16 1.31 0 0 -16 2.18 0.70 0 0 17 0.46 0.61 0 0 -17 -0.27 0.34 0 0 -18 315.99 9.35 0 0 18 324.52 10.13 0 0 18 321.84 9.64 0 0 19 2.94 1.06 0 0 -19 1.46 0.77 0 0 -20 5257.81 57.50 0 0 20 5436.59 58.66 0 0 21 3.49 1.22 0 0 22 19.44 2.52 0 0 23 3.39 1.13 0 0 24 141.92 6.56 0 0 24 129.76 6.42 0 0 25 -0.11 0.43 0 0 25 0.95 0.63 0 0 26 29.61 2.80 0 0 26 25.22 2.61 0 0 27 0.61 0.42 0 0 27 -0.16 0.57 0 0 28 0.30 0.41 0 0 29 -0.42 0.40 0 0 30 0.49 0.24 0 1 0 1.18 0.15 0 1 0 5.18 0.37 0 -1 -1 4606.02 36.92 0 1 1 4521.03 36.76 0 1 1 4603.72 37.08 0 -1 1 4592.87 37.28 0 -1 -2 1623.37 14.34 0 -1 2 1669.33 14.71 0 1 2 1596.60 14.23 0 1 2 1657.86 14.36 0 -1 -3 3.24 0.36 0 -1 3 3.09 0.36 0 1 3 3.62 0.34 0 -1 3 3.11 0.22 0 -1 -4 765.75 8.42 0 -1 4 772.75 8.63 0 1 4 760.08 7.86 0 -1 4 779.77 7.40 0 1 5 191.94 3.10 0 1 -5 197.33 3.68 0 -1 5 195.65 3.02 0 -1 -5 189.75 3.60 0 -1 5 198.58 3.77 0 -1 -6 1075.95 12.04 0 -1 6 1109.49 11.13 0 -1 6 1099.38 12.26 0 1 6 1109.01 10.98 0 1 -7 223.72 4.46 0 -1 7 227.43 3.97 0 -1 -7 226.16 4.52 0 1 7 229.94 3.74 0 -1 7 222.61 3.47 0 -1 7 225.43 4.65 0 1 -8 725.53 9.69 0 -1 8 708.86 7.80 0 1 8 727.43 8.32 0 -1 8 745.43 10.07 0 -1 8 733.11 8.95 0 -1 -8 716.35 9.71 0 1 -9 318.88 6.13 0 1 9 331.81 4.98 0 -1 9 309.16 4.36 0 -1 9 321.77 6.37 0 -1 -9 312.74 6.08 0 -1 9 318.68 5.59 0 -1 -10 178.34 4.64 0 1 -10 167.90 4.48 0 -1 10 172.69 4.79 0 1 10 166.68 3.42 0 -1 10 167.19 4.13 0 1 11 492.50 6.78 0 1 -11 518.72 8.87 0 -1 -11 524.38 8.95 0 -1 11 530.31 9.43 0 -1 11 525.06 8.44 0 -1 -12 12.33 1.34 0 -1 12 11.24 1.37 0 -1 12 10.49 1.18 0 1 -12 11.26 1.28 0 1 13 1.09 0.52 0 -1 13 0.87 0.45 0 -1 13 1.27 0.54 0 1 -13 0.45 0.42 0 -1 -13 1.44 0.50 0 1 -14 250.42 6.86 0 -1 14 265.45 7.40 0 -1 -14 276.05 7.23 0 1 14 257.10 7.10 0 -1 14 242.76 6.47 0 1 15 1126.55 17.28 0 -1 15 1133.50 17.84 0 -1 -15 1096.66 16.96 0 1 -15 1067.69 16.63 0 -1 15 1058.18 16.12 0 -1 -16 10.19 1.53 0 1 -16 9.69 1.47 0 1 16 8.44 1.40 0 -1 16 9.46 1.42 0 -1 -17 545.93 12.29 0 1 -17 548.18 12.13 0 1 17 570.47 12.80 0 1 18 202.35 7.69 0 1 -18 200.65 7.41 0 1 18 205.56 7.95 0 -1 -18 196.45 7.46 0 1 19 23.38 2.74 0 1 -19 24.88 2.70 0 -1 19 24.44 2.80 0 -1 -19 24.57 2.76 0 1 19 24.43 2.80 0 1 -20 379.10 11.24 0 -1 20 379.66 11.35 0 1 20 399.26 11.63 0 -1 -20 393.41 11.76 0 1 21 1041.99 20.02 0 1 22 4.38 1.14 0 1 23 22.76 2.76 0 1 24 37.09 3.42 0 -1 24 45.67 3.79 0 1 24 39.56 3.47 0 1 25 21.80 2.53 0 -1 25 23.28 2.61 0 1 25 25.30 2.67 0 -1 26 16.28 2.17 0 1 26 13.48 1.91 0 1 26 15.31 2.04 0 -1 27 40.58 3.15 0 1 27 37.30 3.02 0 1 27 34.41 2.90 0 -1 28 2.14 0.76 0 1 28 3.40 0.89 0 1 28 2.60 0.74 0 -1 29 137.86 5.00 0 1 29 139.61 4.99 0 -1 30 0.44 0.39 0 1 30 1.16 0.43 0 2 0 6362.84 51.95 0 2 0 6315.91 51.30 0 2 1 1738.71 15.87 0 -2 -1 1744.35 16.22 0 2 1 1763.67 16.51 0 -2 1 1767.67 16.90 0 2 2 81.31 1.92 0 -2 2 82.51 2.25 0 2 2 84.51 2.15 0 -2 -2 82.73 2.08 0 2 3 164.30 3.21 0 -2 3 168.58 3.49 0 -2 4 86.60 2.53 0 2 4 83.47 2.21 0 -2 -4 86.86 2.40 0 2 4 90.87 2.39 0 -2 5 2288.34 21.57 0 2 5 2281.72 20.76 0 -2 -5 2296.67 21.23 0 -2 6 106.90 3.15 0 2 6 108.96 2.79 0 -2 7 11.21 1.05 0 -2 7 10.58 0.69 0 -2 -7 10.12 0.97 0 2 -7 9.97 0.96 0 -2 -8 871.53 11.58 0 -2 8 891.94 11.80 0 2 -8 906.64 11.57 0 2 8 909.91 10.67 0 2 9 3148.59 28.56 0 -2 -9 3129.67 30.26 0 -2 9 3119.88 30.54 0 2 -9 3156.57 30.07 0 -2 -10 508.85 8.82 0 2 -10 487.41 8.46 0 2 10 521.88 7.66 0 -2 10 474.51 7.28 0 -2 10 498.62 8.96 0 2 -11 15.60 1.45 0 -2 -11 16.61 1.53 0 -2 11 15.35 1.23 0 -2 11 14.56 1.47 0 2 11 13.73 1.11 0 -2 -12 49.36 2.80 0 2 -12 46.33 2.64 0 -2 12 47.61 2.85 0 -2 12 49.05 2.39 0 -2 -13 8.72 1.25 0 -2 13 8.76 1.32 0 2 -13 8.49 1.20 0 -2 -14 7.58 1.23 0 2 14 7.04 1.22 0 2 -14 8.49 1.26 0 -2 14 9.98 1.50 0 -2 15 3.54 1.00 0 2 -15 3.35 0.83 0 -2 -15 5.11 1.04 0 2 15 3.48 0.86 0 -2 16 16.57 2.07 0 2 16 12.23 1.79 0 2 -16 11.95 1.65 0 -2 -16 16.75 2.01 0 -2 -17 1.35 0.75 0 2 17 1.65 0.70 0 2 -17 1.54 0.52 0 2 17 1.00 0.69 0 2 -18 13.11 1.92 0 2 18 13.70 2.06 0 -2 -18 13.24 2.05 0 2 18 16.21 2.27 0 2 -19 705.14 15.43 0 2 19 677.93 15.83 0 2 19 712.72 15.88 0 -2 -19 726.74 16.35 0 2 20 114.71 6.05 0 2 20 92.04 5.82 0 2 -20 99.07 5.71 0 -2 -20 103.95 6.17 0 2 21 65.47 4.62 0 2 22 1.53 0.80 0 2 23 78.96 5.05 0 -2 23 76.78 5.06 0 2 23 77.34 4.96 0 2 24 51.80 4.00 0 2 24 53.96 4.02 0 -2 24 56.72 4.20 0 2 25 0.04 0.50 0 2 25 -0.20 0.48 0 -2 25 0.47 0.49 0 2 26 1.06 0.51 0 -2 26 2.46 0.85 0 2 26 1.70 0.68 0 2 27 44.54 3.17 0 -2 27 39.08 3.06 0 2 27 41.87 3.18 0 2 28 51.43 3.19 0 -2 28 47.01 3.09 0 2 28 53.44 3.32 0 -2 29 560.78 10.32 0 2 29 531.96 10.08 0 2 29 543.64 10.08 0 3 0 1.65 0.32 0 3 -1 1115.50 11.70 0 -3 1 1145.26 13.12 0 3 1 1117.10 11.64 0 3 -2 1211.80 12.69 0 -3 2 1194.42 13.65 0 -3 -2 1184.16 12.99 0 3 2 1233.20 13.16 0 3 2 1171.86 12.31 0 3 3 80.44 2.53 0 -3 -3 77.77 2.53 0 3 3 80.16 2.32 0 -3 3 76.19 2.68 0 3 4 94.23 2.86 0 -3 -4 96.56 2.92 0 -3 4 94.09 3.05 0 3 4 90.44 2.56 0 3 5 376.06 6.37 0 -3 5 381.82 6.80 0 -3 -5 375.88 6.55 0 -3 -6 315.52 6.16 0 -3 6 330.80 6.38 0 3 6 316.30 5.84 0 -3 7 1.30 0.42 0 -3 -7 2.00 0.51 0 3 7 2.32 0.50 0 -3 -8 772.17 11.24 0 3 -8 759.12 10.81 0 -3 8 760.70 11.37 0 -3 -9 21.81 1.73 0 3 -9 24.45 1.79 0 -3 9 27.74 1.96 0 3 9 27.87 1.73 0 3 -10 18.01 1.58 0 -3 10 18.02 1.64 0 -3 -10 18.51 1.67 0 3 10 19.83 1.52 0 3 11 8.94 1.03 0 -3 11 9.31 1.25 0 -3 -11 10.23 1.32 0 3 -11 9.30 1.20 0 -3 12 149.19 5.34 0 -3 -12 143.53 5.23 0 3 -12 142.37 4.91 0 -3 13 199.31 6.54 0 3 -13 194.65 6.10 0 -3 -13 201.51 6.54 0 -3 14 212.92 7.12 0 3 14 204.69 6.86 0 -3 -14 204.26 6.90 0 3 -14 196.05 6.39 0 3 15 284.39 8.53 0 -3 15 286.34 8.74 0 -3 -15 275.40 8.49 0 3 -15 267.53 7.91 0 -3 -16 125.51 5.97 0 3 16 119.64 5.92 0 3 16 123.75 5.78 0 -3 16 134.72 6.17 0 3 -16 115.07 5.33 0 3 17 5.94 1.22 0 -3 -17 7.64 1.59 0 -3 17 8.69 1.69 0 3 -17 7.31 1.40 0 3 17 6.27 1.31 0 3 18 72.27 4.85 0 3 18 65.58 4.52 0 -3 18 74.43 4.94 0 -3 -18 73.53 4.99 0 3 -18 69.93 4.55 0 -3 -19 160.81 7.73 0 3 19 156.27 7.08 0 3 19 152.98 7.38 0 3 -19 154.40 7.06 0 3 20 311.32 10.14 0 3 21 2.86 0.93 0 -3 21 3.34 1.06 0 3 22 198.49 7.99 0 -3 22 214.47 8.61 0 3 22 216.11 8.49 0 -3 23 6.92 1.58 0 3 23 5.87 1.38 0 3 23 4.83 1.25 0 -3 24 5.83 1.33 0 3 24 5.46 1.25 0 3 24 3.88 1.17 0 3 25 53.92 3.84 0 -3 25 55.57 3.87 0 3 25 52.98 3.70 0 3 26 74.40 4.17 0 3 26 71.44 4.23 0 -3 26 71.17 4.14 0 3 27 3.16 0.82 0 3 27 3.36 0.96 0 -3 27 3.66 0.95 0 -3 28 303.49 7.49 0 3 28 292.63 7.28 0 3 29 49.69 2.72 0 4 0 5226.70 44.79 0 -4 0 5208.92 47.43 0 -4 1 891.09 12.36 0 4 1 879.95 10.45 0 4 -1 874.10 10.54 0 4 2 844.03 9.62 0 -4 2 832.18 11.31 0 4 -2 819.91 9.69 0 -4 3 652.48 10.16 0 4 3 650.72 8.78 0 4 -3 647.01 9.00 0 -4 -4 1084.24 13.56 0 -4 4 1069.38 14.07 0 4 -4 1089.82 13.27 0 -4 -5 1362.96 16.56 0 -4 5 1398.04 17.03 0 4 -5 1361.40 16.05 0 -4 6 85.68 3.42 0 -4 -6 84.05 3.36 0 -4 -7 420.93 8.29 0 -4 7 392.32 8.03 0 -4 8 520.31 9.72 0 -4 -8 522.29 9.72 0 4 -8 507.92 9.01 0 -4 -9 154.20 5.19 0 4 -9 158.43 4.95 0 -4 9 151.71 5.09 0 4 -10 73.88 3.46 0 -4 10 72.29 3.57 0 -4 -10 71.97 3.68 0 -4 -11 278.28 7.78 0 -4 11 279.74 7.57 0 4 -11 282.44 7.23 0 -4 12 32.00 2.61 0 -4 -12 35.92 2.81 0 4 -12 30.98 2.42 0 -4 -13 27.62 2.56 0 4 13 30.97 2.69 0 4 -13 27.45 2.37 0 -4 13 28.21 2.56 0 4 -14 176.80 6.39 0 -4 14 191.49 7.06 0 4 14 183.88 6.89 0 -4 -14 191.62 7.21 0 4 -15 230.15 7.64 0 4 15 228.08 8.56 0 -4 -15 230.04 8.33 0 -4 15 238.82 8.28 0 4 15 225.06 7.94 0 -4 15 200.23 7.48 0 4 15 236.97 9.29 0 4 -16 22.76 2.46 0 4 16 21.52 2.52 0 -4 16 25.28 2.78 0 4 16 27.97 3.17 0 -4 -16 22.74 2.69 0 4 16 23.40 2.77 0 -4 16 21.31 2.41 0 4 17 11.75 1.95 0 -4 17 14.15 2.16 0 4 -17 11.66 1.85 0 -4 17 12.70 1.90 0 -4 -17 14.00 2.26 0 4 -18 90.33 5.34 0 -4 18 94.53 5.15 0 4 18 96.18 5.53 0 -4 -18 94.13 6.05 0 -4 18 86.85 5.55 0 4 18 89.08 5.55 0 4 19 1164.02 21.37 0 4 19 1224.51 22.01 0 -4 19 1224.92 22.23 0 -4 19 1126.21 19.86 0 4 20 583.29 14.48 0 -4 20 596.88 14.80 0 4 20 568.65 14.11 0 -4 21 66.24 4.66 0 4 21 67.39 4.63 0 4 21 60.04 4.37 0 4 22 0.17 0.59 0 -4 22 -0.04 0.55 0 4 22 0.91 0.82 0 4 23 164.19 6.99 0 4 23 170.24 6.99 0 -4 23 171.86 7.18 0 4 24 31.18 2.84 0 -4 24 32.83 2.97 0 4 24 36.10 3.12 0 -4 25 6.65 1.28 0 4 25 5.02 1.18 0 4 25 5.69 1.19 0 -4 26 100.31 4.56 0 4 26 108.55 4.92 0 4 27 98.73 4.40 0 4 28 66.21 3.31 0 5 0 3.66 0.58 0 -5 0 26.83 2.07 0 -5 1 2917.89 31.01 0 5 1 2881.66 27.61 0 -5 -1 2941.47 31.46 0 5 -1 2924.30 27.88 0 5 -2 5270.58 46.70 0 -5 2 5318.07 49.74 0 5 2 5305.87 46.57 0 -5 3 180.06 5.48 0 5 -3 169.05 4.37 0 5 3 179.24 4.38 0 5 -4 831.21 11.53 0 5 4 830.85 11.27 0 -5 5 293.47 7.22 0 5 -5 275.61 6.16 0 -5 -6 174.68 5.38 0 -5 6 169.78 5.44 0 5 -6 169.17 4.97 0 -5 7 27.04 2.16 0 -5 -7 24.33 2.04 0 5 -7 29.29 2.23 0 5 -8 104.93 4.29 0 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138.64 6.58 0 5 22 228.71 8.35 0 5 23 36.27 3.18 0 5 24 15.23 1.98 0 5 25 2.56 0.87 0 5 26 143.84 5.39 0 5 -27 2.65 0.82 0 5 27 1.68 0.58 0 -6 0 96.10 4.50 0 -6 -1 56.69 3.51 0 -6 1 55.95 3.36 0 -6 2 12.38 1.58 0 -6 -2 12.61 1.72 0 -6 3 74.83 3.91 0 6 4 5.37 0.97 0 -6 4 11.20 1.53 0 -6 5 34.00 2.66 0 6 5 30.24 2.31 0 6 6 241.91 7.04 0 -6 6 230.23 7.10 0 6 7 13.14 1.68 0 -6 7 11.29 1.59 0 -6 8 61.69 3.74 0 6 8 65.75 3.89 0 6 9 688.99 13.93 0 -6 9 594.62 12.80 0 6 -10 567.02 13.38 0 6 10 633.52 13.74 0 -6 10 589.25 13.20 0 6 10 613.04 15.15 0 6 11 661.86 16.06 0 6 -11 581.20 13.83 0 -6 11 624.92 13.87 0 6 11 700.23 15.04 0 6 12 44.94 4.02 0 6 12 45.40 3.74 0 -6 12 40.46 3.41 0 6 -12 38.68 3.39 0 6 13 10.05 2.02 0 6 -13 7.82 1.57 0 6 13 5.47 1.39 0 6 13 8.54 1.78 0 -6 13 8.16 1.62 0 6 14 104.85 6.35 0 6 14 105.64 6.16 0 -6 14 104.19 5.61 0 6 -14 97.83 5.56 0 6 14 103.17 5.88 0 6 15 32.04 3.55 0 6 15 26.60 3.15 0 -6 15 29.98 3.01 0 6 -15 28.46 2.97 0 6 15 30.15 3.22 0 -6 16 34.40 3.24 0 6 16 34.75 3.49 0 6 16 34.99 3.72 0 -6 17 34.27 3.26 0 6 17 36.13 3.54 0 6 17 36.20 3.80 0 -6 18 262.32 9.09 0 6 18 269.04 9.66 0 6 19 403.22 11.79 0 -6 19 382.30 10.94 0 6 20 19.64 2.51 0 -6 20 17.93 2.24 0 -6 21 73.81 4.37 0 6 21 77.48 4.76 0 6 22 535.22 12.72 0 -6 22 523.79 11.71 0 6 -23 324.49 10.02 0 6 23 294.12 8.79 0 6 24 128.78 5.40 0 6 -24 139.86 6.17 0 6 25 30.51 2.43 0 6 -25 38.70 2.97 0 6 26 36.41 2.38 0 6 -26 42.52 2.81 0 -7 0 0.03 0.63 0 -7 1 201.82 7.37 0 -7 -1 192.42 7.31 0 -7 -2 314.66 9.72 0 -7 -3 359.55 10.56 0 -7 -4 4.73 1.25 0 7 -4 3.59 1.05 0 7 -5 35.36 3.17 0 7 -5 33.20 3.40 0 -7 5 30.54 2.92 0 7 5 32.98 3.31 0 -7 -5 36.50 3.40 0 7 -6 87.56 5.65 0 7 -6 94.07 5.21 0 -7 6 86.45 4.98 0 7 6 86.56 5.46 0 7 -7 22.34 2.85 0 -7 7 19.81 2.37 0 7 -7 24.39 2.70 0 7 7 27.92 3.16 0 -7 8 501.81 12.54 0 7 8 534.16 14.27 0 7 -8 520.90 12.92 0 7 -8 511.64 14.32 0 -7 9 87.08 5.04 0 7 -9 94.29 5.39 0 7 9 91.96 5.80 0 7 -9 87.41 5.79 0 -7 10 104.09 5.54 0 7 10 106.86 6.30 0 7 -10 106.63 5.82 0 7 10 100.29 5.72 0 7 -10 109.85 6.51 0 7 11 10.60 2.07 0 -7 11 9.89 1.79 0 7 -11 10.79 1.92 0 7 11 8.30 1.89 0 7 -11 10.04 1.94 0 7 12 923.68 19.72 0 7 -12 887.73 19.51 0 7 -12 900.19 18.15 0 -7 12 888.84 17.64 0 -7 13 68.82 4.61 0 7 -13 66.52 5.08 0 7 -13 72.52 4.84 0 7 13 67.76 5.11 0 7 -14 10.65 2.04 0 7 -14 12.24 2.00 0 7 14 11.00 2.10 0 -7 14 11.62 1.96 0 -7 15 22.03 2.62 0 7 15 24.01 3.07 0 7 -15 20.46 2.56 0 7 15 24.55 2.83 0 7 -15 18.20 2.63 0 7 16 0.31 0.62 0 7 -16 1.38 0.77 0 -7 16 0.87 0.69 0 7 -16 0.14 0.67 0 7 16 1.38 0.88 0 7 -17 83.50 5.51 0 7 17 94.95 5.95 0 -7 17 92.64 5.31 0 7 17 99.13 5.64 0 7 18 4.65 1.29 0 -7 18 5.81 1.40 0 7 -18 5.41 1.38 0 -7 19 22.66 2.51 0 7 19 22.07 2.60 0 7 -19 24.25 2.86 0 7 -20 2.67 0.98 0 7 20 2.35 0.76 0 -7 20 4.73 1.20 0 7 21 70.92 4.28 0 7 -21 71.65 4.59 0 -7 21 69.45 4.05 0 7 -22 89.61 4.89 0 7 22 81.47 4.37 0 -7 22 81.17 4.09 0 7 -23 157.16 6.13 0 7 23 139.43 5.37 0 7 -24 39.60 2.81 0 7 24 31.91 2.30 0 7 -25 9.61 1.26 0 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4.25 1.48 0 8 -12 4.01 1.30 0 8 -12 4.49 1.37 0 8 -13 1007.96 19.35 0 -8 13 989.93 18.99 0 8 13 974.82 20.37 0 8 -13 982.97 20.50 0 8 -14 4.39 1.25 0 -8 14 5.18 1.40 0 8 14 4.21 1.42 0 8 -14 4.57 1.44 0 8 -15 43.76 3.63 0 8 -15 45.16 3.96 0 -8 15 49.59 3.88 0 8 15 47.15 4.12 0 -8 16 2.35 0.82 0 8 -16 2.02 0.92 0 8 16 2.34 0.84 0 8 -16 2.73 0.88 0 8 17 4.87 1.31 0 8 -17 1.62 0.79 0 -8 17 4.03 1.14 0 8 -17 3.20 0.97 0 8 -18 37.12 3.33 0 -8 18 35.85 3.08 0 -8 19 46.33 3.36 0 8 -19 45.00 3.53 0 8 -20 89.21 4.72 0 -8 20 87.97 4.43 0 8 -21 8.68 1.41 0 -8 21 8.12 1.30 0 8 -22 8.71 1.29 0 8 -22 5.56 1.06 0 -8 22 7.22 1.05 0 8 -23 42.48 2.60 0 9 0 0.36 0.54 0 9 0 0.86 0.81 0 -9 0 2.47 1.03 0 9 1 157.17 7.61 0 9 1 169.78 7.96 0 9 -1 165.83 7.60 0 9 -1 167.95 7.98 0 -9 1 177.84 7.98 0 -9 -1 162.09 7.62 0 9 -2 6.60 1.61 0 9 2 4.86 1.33 0 9 2 5.18 1.46 0 -9 2 7.41 1.60 0 9 -2 6.84 1.60 0 9 -3 -0.44 0.69 0 9 3 0.29 0.49 0 9 -3 0.90 0.73 0 -9 3 0.30 0.48 0 -9 4 70.92 4.97 0 9 4 65.31 4.94 0 9 -4 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2.51 0.86 2 3 -15 2.23 0.79 -2 -3 -15 2.19 0.80 2 3 -15 2.73 0.89 -2 3 14 83.64 4.14 -2 -3 -14 84.87 4.46 2 3 -14 82.90 4.48 2 -3 14 84.81 4.77 2 3 -13 184.96 6.41 -2 3 13 186.02 6.09 2 -3 13 179.98 6.77 -2 -3 -13 177.78 6.19 -2 3 12 159.81 5.46 2 3 -12 165.57 5.72 2 -3 12 159.00 6.08 -2 -3 -12 158.35 5.50 -2 3 11 104.56 4.26 2 -3 11 101.48 4.68 -2 -3 -11 104.21 4.15 2 3 -11 102.86 4.21 2 -3 10 277.15 7.68 2 3 -10 282.61 6.79 2 -3 10 268.13 6.88 -2 3 10 283.59 7.01 -2 -3 -10 276.62 6.54 2 -3 9 29.35 2.33 -2 3 9 28.10 2.02 -2 -3 -9 27.85 1.85 2 3 -9 31.11 2.01 2 -3 8 380.00 8.57 -2 3 8 400.74 7.88 -2 -3 -8 381.08 6.96 2 3 -8 393.24 7.22 2 -3 7 827.64 13.20 -2 -3 -7 838.72 10.76 2 3 -7 840.97 10.96 -2 3 6 52.81 2.50 2 3 -6 47.04 1.91 2 -3 6 49.06 2.79 -2 -3 -6 47.88 1.89 2 3 -5 8.74 1.21 -2 -3 -5 8.92 0.70 -2 3 5 6.37 0.83 2 -3 5 7.30 1.09 2 3 -4 339.76 7.64 2 -3 4 335.76 7.48 -2 3 4 331.69 6.31 2 -3 3 1336.76 17.37 -2 3 3 1389.49 15.74 -2 3 2 144.31 3.80 2 -3 2 135.07 4.44 2 3 -2 136.48 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304.60 7.14 2 4 -7 323.68 8.78 2 -4 7 312.45 8.23 2 4 -6 1.68 0.56 -2 4 6 1.30 0.48 2 -4 6 1.85 0.64 -2 4 5 74.73 3.14 2 4 -5 84.88 4.09 2 -4 5 75.48 3.80 2 4 -4 557.27 10.74 -2 4 4 542.54 9.13 2 -4 4 561.64 10.94 2 -4 3 76.56 3.69 -2 4 3 80.25 3.12 2 4 -3 77.62 3.59 -2 4 2 244.04 5.57 2 4 -2 241.99 6.35 2 -4 2 235.17 6.61 2 4 -1 45.19 2.60 2 -4 1 49.68 2.98 2 4 -1 47.80 2.30 -2 4 1 50.31 2.41 2 -4 0 1119.81 16.41 2 4 0 1154.11 14.51 -2 4 0 1123.76 14.13 2 4 1 49.84 2.73 2 -4 -1 52.81 3.07 2 4 1 49.95 2.56 -2 4 -1 52.55 2.51 2 4 2 259.03 6.56 -2 4 -2 245.99 5.63 2 4 2 268.51 6.39 2 4 3 80.43 3.55 2 4 3 82.88 3.54 -2 4 -3 80.01 3.11 2 4 4 556.39 10.15 -2 4 -4 563.66 9.17 2 4 4 561.91 10.47 2 4 5 76.96 3.52 -2 4 -5 81.76 3.16 2 4 5 75.94 3.69 2 4 6 6.93 1.20 2 4 6 4.73 0.92 2 4 7 308.30 7.65 2 4 7 318.07 8.53 2 -4 -7 317.33 8.42 2 -4 -8 481.27 10.93 2 4 8 485.40 11.19 2 4 8 474.47 9.90 2 -4 -9 250.61 7.94 2 4 9 225.94 7.71 2 4 9 234.55 6.78 2 4 10 226.98 8.00 2 -4 -10 221.71 7.68 2 4 10 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24 59.03 3.73 -2 -4 25 1.03 0.54 2 4 25 2.79 0.87 2 4 26 44.78 3.07 2 4 27 7.30 1.18 -2 5 27 6.72 0.94 2 5 -26 21.51 1.96 -2 5 26 25.51 2.00 2 5 -25 23.69 2.26 -2 5 25 26.89 2.23 2 5 -24 13.96 1.91 -2 5 24 17.37 1.92 -2 5 23 44.67 3.25 -2 5 22 46.34 3.42 -2 5 21 12.74 1.92 2 5 -20 7.09 1.37 -2 5 20 8.81 1.65 2 5 -19 73.14 4.55 -2 5 19 73.29 4.73 2 5 -18 40.77 3.46 -2 5 18 46.27 3.75 2 5 -17 68.59 4.51 -2 5 17 68.96 4.69 -2 5 17 73.85 5.47 2 5 -16 42.77 3.57 -2 5 16 41.86 3.61 -2 5 16 41.81 4.08 2 -5 15 84.93 5.31 2 5 -15 92.78 5.26 2 5 -15 82.92 5.95 2 -5 15 88.80 5.68 -2 5 15 95.60 6.14 -2 5 14 3.49 1.27 2 5 -14 2.32 1.05 2 -5 14 3.62 1.12 2 5 -14 4.22 1.19 2 -5 14 2.41 1.01 -2 5 14 2.15 0.83 2 5 -13 81.08 4.82 2 5 -13 83.10 5.68 2 -5 13 64.68 4.65 -2 5 13 76.61 4.44 2 -5 13 73.23 4.85 -2 5 13 76.94 5.37 2 -5 12 68.16 4.59 2 5 -12 69.46 5.03 -2 5 12 67.22 4.09 2 5 -12 62.87 4.19 -2 5 12 70.21 5.04 2 -5 12 62.80 4.52 2 5 -11 491.13 11.96 2 -5 11 448.25 12.54 2 5 -11 582.78 14.73 2 -5 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61.82 3.62 2 5 8 60.99 4.09 2 5 9 87.18 5.04 2 -5 -9 82.14 4.85 2 5 9 85.51 4.39 2 -5 -10 195.95 7.76 2 5 10 213.79 8.31 -2 -5 11 505.77 11.92 2 5 11 537.84 14.00 2 -5 -11 516.60 13.40 2 5 12 64.95 4.86 2 -5 -12 67.05 4.78 -2 -5 12 62.84 4.03 2 5 12 53.00 4.38 2 5 12 60.15 4.58 -2 -5 13 78.17 4.55 2 -5 -13 79.79 5.42 2 5 13 81.60 5.59 -2 5 -13 82.33 5.11 2 5 13 69.13 4.97 2 5 13 71.09 5.18 2 5 14 3.03 1.22 2 -5 -14 5.47 1.48 -2 -5 14 3.44 1.02 -2 5 -14 3.05 1.03 2 5 14 2.08 0.79 -2 -5 15 92.71 5.11 2 5 15 94.63 6.05 -2 5 -15 94.68 5.79 2 5 15 94.41 6.37 2 -5 -15 89.97 6.13 -2 -5 16 40.43 3.40 2 5 16 42.67 3.98 -2 -5 17 69.79 4.46 2 5 17 66.19 5.03 -2 -5 18 43.42 3.50 2 5 18 46.62 4.19 -2 -5 19 75.85 4.60 2 5 19 78.12 5.36 -2 -5 20 8.04 1.53 2 5 20 7.01 1.57 2 5 21 9.38 1.74 -2 -5 21 8.88 1.49 2 5 22 42.13 3.56 -2 -5 22 39.38 3.01 -2 -5 23 42.89 2.98 2 5 23 48.29 3.68 2 5 24 16.18 2.00 -2 -5 24 14.88 1.64 2 5 25 26.63 2.38 -2 5 -26 26.19 2.25 2 5 26 26.49 2.18 2 5 27 6.99 1.01 2 6 -25 17.71 1.85 -2 6 25 20.61 1.75 2 6 -24 53.47 3.39 -2 6 24 50.36 3.01 2 6 -23 30.38 2.70 -2 6 23 32.40 2.58 2 6 -22 96.67 5.16 -2 6 22 92.27 4.62 2 6 -21 7.85 1.33 -2 6 21 11.24 1.69 2 6 -20 149.10 6.12 -2 6 20 151.34 6.40 2 6 -19 145.06 6.27 -2 6 19 155.63 6.70 2 6 -18 22.74 2.55 -2 6 18 28.12 2.90 2 6 -17 267.57 9.05 -2 6 17 257.14 10.16 -2 6 17 259.28 9.09 2 -6 17 250.17 9.17 2 6 -16 71.46 4.66 -2 6 16 79.92 5.66 2 -6 16 77.08 5.10 -2 6 16 81.63 5.05 2 6 -15 90.99 5.25 2 -6 15 93.75 5.67 -2 6 15 94.05 5.49 -2 6 15 94.87 6.15 2 6 -14 152.07 6.79 2 -6 14 147.04 7.20 -2 6 14 173.66 7.48 -2 6 14 159.97 7.96 -2 6 13 75.69 4.75 2 6 -13 72.65 5.43 2 -6 13 86.07 5.53 2 6 -13 87.72 5.08 -2 6 13 91.00 5.42 -2 6 13 90.89 5.93 2 -6 13 83.54 5.59 -2 6 12 353.46 11.83 2 6 -12 353.03 10.36 2 6 -12 315.65 11.24 2 -6 12 353.50 11.26 2 -6 12 340.63 11.27 -2 6 12 327.50 9.98 2 6 -11 227.46 9.29 2 -6 11 242.80 9.25 2 6 -11 247.62 8.54 2 -6 11 248.55 9.38 -2 6 11 247.08 8.31 -2 6 11 255.64 9.88 2 6 -10 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54.90 3.38 -2 6 -25 17.84 1.82 2 6 25 17.06 1.71 2 7 -24 17.16 1.67 2 7 -23 1.07 0.49 -2 7 23 1.05 0.44 2 7 -22 12.96 1.70 -2 7 22 11.81 1.49 -2 7 21 81.80 4.12 2 7 -21 78.36 4.38 2 7 -20 39.94 2.96 2 7 -20 40.19 3.20 -2 7 20 43.61 3.17 2 -7 19 105.82 5.26 2 7 -19 112.31 5.24 2 7 -19 103.20 5.42 -2 7 19 111.29 5.28 2 -7 18 96.08 5.30 2 7 -18 103.12 5.21 2 7 -18 95.82 5.38 -2 7 18 98.93 5.12 2 7 -17 55.58 3.95 -2 7 17 58.44 4.58 -2 7 17 51.89 3.76 2 -7 17 53.53 4.04 2 -7 16 88.64 5.38 2 7 -16 87.51 5.04 -2 7 16 87.73 5.01 -2 7 16 96.81 6.01 2 7 -15 59.61 4.19 2 -7 15 56.67 4.40 -2 7 15 56.02 4.04 -2 7 15 60.62 4.82 2 7 -14 119.08 5.97 2 -7 14 111.34 6.30 -2 7 14 113.50 6.64 2 7 -13 64.40 4.40 2 -7 13 64.28 4.82 -2 7 13 61.87 4.88 2 -7 12 26.41 3.06 2 7 -12 29.19 2.95 -2 7 12 26.73 3.25 2 -7 11 54.70 4.38 2 7 -11 52.68 3.93 -2 7 11 50.05 4.40 2 7 -11 51.79 4.48 2 -7 10 885.09 18.82 2 7 -10 934.52 20.15 2 7 -10 884.34 17.22 -2 7 10 922.56 19.75 2 -7 9 271.30 10.27 2 7 -9 284.16 10.67 2 7 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164.02 6.32 4 4 6 164.81 7.53 -4 -4 6 156.63 7.09 4 4 7 92.70 5.03 4 4 7 93.78 5.33 4 -4 -7 103.07 6.12 4 4 7 101.66 5.05 4 4 7 98.50 5.97 -4 -4 7 97.15 5.67 4 4 7 88.15 5.69 4 4 8 2.04 0.94 4 4 8 3.03 1.03 4 4 8 2.18 0.95 -4 -4 8 4.95 1.31 4 -4 -8 1.75 0.84 4 4 8 2.58 0.93 4 4 9 142.91 6.63 4 4 9 147.36 7.80 -4 -4 9 144.78 7.14 4 4 9 136.83 7.31 4 4 9 137.31 6.29 4 4 10 70.16 4.63 4 4 10 64.27 5.34 -4 -4 10 64.24 4.82 4 4 10 70.00 5.26 4 4 10 67.66 4.47 4 4 11 136.30 6.54 -4 -4 11 140.59 7.34 -4 -4 11 144.74 6.39 4 4 11 144.26 8.22 4 4 11 143.23 7.62 4 4 11 134.38 6.40 -4 -4 12 123.79 6.97 4 4 12 135.35 8.12 -4 -4 12 134.40 6.18 4 4 12 131.61 7.44 4 4 12 130.02 6.45 4 4 13 94.96 5.76 -4 -4 13 118.58 5.82 -4 -4 13 97.84 6.20 4 4 13 113.10 6.91 4 4 13 122.09 6.25 4 4 14 183.38 8.15 -4 -4 14 212.35 7.82 4 4 14 202.00 9.31 4 4 14 213.89 8.38 -4 -4 15 43.51 3.47 4 4 15 38.92 3.68 4 4 15 41.34 4.22 4 4 16 271.50 9.84 -4 -4 16 291.04 9.07 4 4 16 285.10 10.99 4 -4 -16 285.37 10.56 4 4 17 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-14 63.32 4.26 4 5 -14 65.03 5.20 4 5 -13 186.72 7.37 4 5 -13 196.64 9.15 4 5 -12 400.39 10.96 4 5 -12 408.81 13.33 4 5 -11 111.24 5.65 4 5 -11 114.34 6.89 4 5 -10 182.18 7.21 4 5 -10 176.73 8.54 4 5 -10 178.37 8.91 4 -5 10 168.37 8.05 4 -5 10 165.38 8.08 -4 5 10 164.67 7.01 4 5 -9 474.65 11.97 4 5 -9 477.01 14.17 4 -5 9 471.79 13.68 4 5 -9 501.57 14.86 4 -5 9 440.70 13.64 -4 5 9 456.86 11.75 4 -5 8 600.08 15.19 4 5 -8 594.46 15.75 4 5 -8 586.87 13.47 4 5 -8 612.56 16.15 4 -5 8 551.41 15.37 -4 5 8 587.16 13.07 4 -5 7 389.75 12.00 4 5 -7 395.33 12.58 4 5 -7 405.10 10.85 4 5 -7 393.08 12.44 4 -5 7 396.14 12.78 -4 5 7 371.70 10.05 4 5 -6 96.39 5.98 4 5 -6 103.11 5.32 4 5 -6 102.82 6.07 4 -5 6 96.50 6.12 -4 5 6 98.40 4.97 4 -5 6 99.39 5.89 4 5 -5 40.45 3.81 4 5 -5 38.95 3.65 4 5 -5 36.43 3.16 4 -5 5 35.55 3.72 4 -5 5 33.74 3.37 -4 5 5 35.23 2.91 4 -5 5 35.95 3.51 4 5 -4 25.64 2.90 4 5 -4 25.99 3.01 4 5 -4 22.31 2.44 4 -5 4 24.11 3.04 4 -5 4 22.12 2.73 -4 5 4 28.56 2.58 4 -5 4 24.96 2.90 4 5 -3 194.49 7.97 4 5 -3 173.92 7.82 4 5 -3 172.53 6.86 4 -5 3 195.02 8.58 -4 5 3 200.51 6.90 4 -5 3 160.01 7.49 4 -5 3 201.04 8.34 4 5 -2 81.59 5.03 4 5 -2 83.61 5.32 4 5 -2 71.93 4.34 4 -5 2 86.50 5.46 -4 5 2 78.38 4.26 4 -5 2 68.69 4.86 4 -5 2 85.79 5.66 4 5 -1 47.89 3.82 4 5 -1 52.47 4.20 4 -5 1 47.82 4.15 4 -5 1 50.68 4.17 -4 5 1 52.79 3.50 4 -5 1 42.90 3.86 4 5 0 45.86 3.72 4 5 0 43.76 3.88 4 -5 0 40.09 3.79 4 -5 0 43.76 3.86 -4 5 0 46.76 3.26 4 -5 0 39.32 3.70 4 5 1 54.24 4.00 4 5 1 47.86 4.02 4 -5 -1 50.35 4.21 4 -5 -1 51.33 4.17 -4 5 -1 51.55 3.45 4 -5 -1 48.10 4.10 4 5 2 87.80 5.04 4 5 2 81.78 5.24 4 -5 -2 80.92 5.31 -4 5 -2 87.27 4.49 4 -5 -2 83.59 5.49 4 5 3 192.09 7.53 4 5 3 196.48 8.11 4 -5 -3 195.05 8.49 -4 5 -3 193.38 6.86 4 -5 -3 197.22 8.56 4 5 4 26.92 2.81 4 5 4 25.10 2.87 4 -5 -4 28.09 3.30 4 5 5 37.67 3.33 4 5 5 35.89 3.43 4 -5 -5 38.12 3.89 4 5 5 33.14 3.38 -4 -5 5 41.10 3.39 4 5 6 96.16 5.33 4 5 6 100.09 5.68 4 -5 -6 110.28 6.66 4 5 6 95.27 5.99 -4 -5 6 99.93 5.31 -4 5 -7 343.10 11.72 4 5 7 414.90 11.80 4 -5 -7 388.68 13.06 4 5 7 383.60 12.55 -4 -5 7 421.34 11.24 -4 -5 7 393.48 12.46 4 5 7 364.96 11.83 4 5 7 398.33 11.35 -4 5 -8 525.20 14.82 4 5 8 577.04 14.16 4 -5 -8 618.23 16.97 4 5 8 561.37 15.84 -4 -5 8 627.48 13.98 -4 -5 8 613.97 15.89 4 5 8 537.46 14.77 4 5 8 596.72 14.17 4 5 9 476.97 12.70 -4 5 -9 425.70 13.27 4 -5 -9 468.60 15.11 -4 -5 9 510.08 12.51 4 5 9 444.37 14.46 -4 -5 9 475.35 14.26 4 5 9 476.54 13.94 4 5 9 481.41 12.65 4 5 10 173.68 7.48 -4 5 -10 162.17 8.04 4 -5 -10 162.65 8.95 -4 -5 10 186.33 7.38 -4 -5 10 163.10 8.27 4 5 10 171.18 9.03 4 5 10 190.04 8.62 4 5 10 166.12 7.27 4 5 11 110.02 5.84 -4 5 -11 99.16 6.27 -4 -5 11 111.01 5.69 4 5 11 109.98 6.60 -4 5 -12 401.64 12.86 4 5 12 404.73 13.04 -4 -5 12 431.47 11.44 4 5 12 414.86 11.73 -4 5 -13 192.42 8.77 -4 -5 13 198.34 7.58 4 5 13 189.18 8.87 4 5 13 201.61 8.04 -4 5 -14 60.92 4.86 -4 -5 14 65.41 4.25 4 5 14 68.27 5.28 -4 5 -15 69.00 5.13 -4 -5 15 75.65 4.58 4 5 15 68.40 5.26 -4 5 -16 14.53 2.35 -4 -5 16 15.69 2.05 4 5 16 13.49 2.31 -4 5 -17 70.78 5.02 -4 -5 17 71.75 4.24 4 5 17 76.38 5.34 4 -5 -17 63.85 4.74 -4 5 -18 35.80 3.47 -4 -5 18 40.30 3.04 4 5 18 37.78 3.65 4 -5 -18 37.84 3.46 -4 5 -19 78.29 4.97 -4 -5 19 81.10 4.24 4 5 19 85.90 5.33 4 -5 -19 73.77 4.60 -4 5 -20 12.01 1.86 4 -5 -20 11.03 1.59 -4 -5 20 12.84 1.67 4 5 20 10.17 1.73 -4 5 -21 28.73 2.70 -4 -5 21 29.03 2.37 4 5 21 29.38 2.83 -4 5 -22 15.19 1.85 -4 -5 22 16.83 1.70 4 5 22 15.74 1.93 4 5 23 49.26 3.11 -4 -5 23 47.98 2.65 4 5 24 4.14 0.83 4 6 -22 3.04 0.68 4 6 -22 3.33 0.77 -4 6 22 3.89 0.77 4 6 -21 88.03 4.29 -4 6 21 86.12 3.85 4 6 -20 117.84 5.35 -4 6 20 122.01 4.90 4 6 -19 162.75 6.11 -4 6 19 149.97 5.72 4 6 -18 181.33 6.66 4 6 -18 170.79 7.18 4 6 -17 247.57 8.03 4 6 -17 230.10 8.73 -4 6 17 226.14 7.63 4 6 -16 21.42 2.32 4 6 -16 23.98 2.87 -4 6 16 21.25 2.33 4 6 -15 67.24 4.23 4 6 -15 67.32 4.91 -4 6 14 10.77 1.95 4 6 -14 11.89 1.82 4 6 -14 15.30 2.41 4 6 -13 221.93 7.87 4 6 -13 233.59 9.65 -4 6 13 214.09 8.86 4 6 -12 50.82 3.74 4 6 -12 48.91 4.45 4 -6 12 46.20 4.15 -4 6 12 45.74 4.10 -4 6 11 1.33 0.89 4 6 -11 1.15 0.64 4 6 -11 0.80 0.79 4 -6 11 1.29 0.84 4 6 -10 64.46 4.28 4 6 -10 75.75 5.53 4 -6 10 68.91 5.25 -4 6 10 61.76 4.76 4 6 -9 177.75 7.15 4 6 -9 194.02 8.86 4 -6 9 185.07 8.77 -4 6 9 169.58 8.03 4 6 -8 44.58 3.54 4 6 -8 49.84 4.44 4 -6 8 52.91 4.69 -4 6 8 44.68 4.09 4 -6 7 31.40 3.53 4 6 -7 35.70 3.15 4 6 -7 36.31 3.79 4 -6 7 37.02 3.89 -4 6 7 33.88 3.08 -4 6 7 30.90 3.43 -4 6 6 7.30 1.70 4 6 -6 8.66 1.86 4 6 -6 7.64 1.49 4 6 -6 8.55 1.82 4 -6 6 6.81 1.78 4 -6 6 7.89 1.73 -4 6 6 6.63 1.42 4 6 -5 127.17 7.07 4 6 -5 129.67 7.05 4 6 -5 130.69 6.09 4 -6 5 126.55 7.20 -4 6 5 116.79 5.63 4 -6 5 114.22 6.71 -4 6 5 109.63 6.45 4 6 -4 306.85 10.93 4 6 -4 290.89 10.58 4 6 -4 305.14 9.46 4 -6 4 301.44 11.13 -4 6 4 280.56 8.92 4 -6 4 294.19 10.98 -4 6 4 264.74 10.15 4 6 -3 243.80 9.61 4 6 -3 246.38 9.60 4 6 -3 233.94 8.23 4 -6 3 249.30 10.00 4 -6 3 232.38 9.23 -4 6 3 242.88 8.16 4 -6 3 251.29 9.99 -4 6 3 208.83 8.94 4 6 -2 243.10 9.44 4 6 -2 236.40 9.37 4 6 -2 209.95 7.78 4 -6 2 223.64 9.40 -4 6 2 223.35 7.87 4 -6 2 231.47 9.67 4 -6 2 218.39 9.02 -4 6 2 203.14 8.80 4 6 -1 322.60 10.82 4 6 -1 332.71 11.07 4 -6 1 302.95 10.91 4 -6 1 325.63 11.61 -4 6 1 298.91 9.14 4 -6 1 308.60 10.82 -4 6 1 274.60 10.27 4 6 0 664.23 15.81 4 6 0 664.89 15.98 4 -6 0 624.71 15.88 4 -6 0 647.42 16.68 -4 6 0 601.25 13.51 4 -6 0 632.33 15.92 -4 6 0 580.03 15.37 -4 6 -1 275.32 10.35 4 6 1 315.89 10.43 4 6 1 306.10 10.55 4 -6 -1 294.28 10.58 4 -6 -1 324.25 11.58 -4 6 -1 287.06 9.09 4 -6 -1 326.23 11.32 -4 6 -2 210.69 8.94 4 6 2 235.75 8.94 4 6 2 222.96 8.86 4 -6 -2 228.38 9.68 -4 6 -2 210.24 7.72 4 -6 -2 237.12 9.62 -4 6 -3 231.21 9.41 4 6 3 239.58 9.02 4 6 3 236.10 9.12 4 -6 -3 247.67 10.22 4 -6 -3 253.11 10.02 -4 6 -4 273.45 10.35 4 6 4 293.48 10.03 4 6 4 303.47 10.29 4 -6 -4 315.97 11.87 4 -6 -4 308.30 11.15 4 6 5 123.47 6.41 -4 6 -5 115.53 6.68 4 6 5 120.76 6.37 4 -6 -5 122.50 7.47 4 -6 -6 6.74 1.70 -4 6 -6 7.23 1.68 4 6 6 7.97 1.65 4 6 6 7.72 1.62 -4 -6 6 8.79 1.60 -4 6 -7 37.91 3.79 4 6 7 38.12 3.50 4 -6 -7 35.62 4.16 -4 -6 7 36.96 3.28 -4 6 -8 51.28 4.44 4 6 8 48.75 3.95 -4 -6 8 50.15 3.81 4 6 9 178.34 7.55 -4 6 -9 194.58 8.69 -4 -6 9 193.85 7.61 4 6 10 62.90 4.40 -4 6 -10 66.34 5.05 -4 -6 10 69.12 4.47 4 6 10 67.72 4.93 -4 6 -11 2.93 1.13 4 6 11 1.48 0.65 -4 -6 11 1.35 0.79 4 6 11 0.42 0.77 -4 6 -12 46.49 4.21 -4 -6 12 59.34 4.10 4 6 12 51.31 4.35 4 6 12 47.26 3.78 -4 6 -13 219.69 9.17 -4 -6 13 232.37 8.14 4 6 13 233.53 9.37 4 6 13 219.07 8.13 -4 6 -14 14.79 2.36 -4 -6 14 13.52 1.93 4 6 14 12.10 2.13 -4 6 -15 57.28 4.47 -4 -6 15 60.62 3.94 4 6 15 65.22 4.81 -4 6 -16 23.19 2.77 -4 -6 16 21.66 2.31 4 6 16 19.95 2.62 4 -6 -16 24.23 2.92 -4 6 -17 224.23 8.59 -4 -6 17 232.16 7.41 4 6 17 220.30 8.62 4 -6 -17 222.40 8.53 -4 6 -18 163.30 7.00 -4 -6 18 166.48 6.01 4 6 18 173.04 7.34 4 -6 -18 154.24 6.72 -4 6 -19 148.52 6.36 4 -6 -19 126.98 5.28 -4 -6 19 144.53 5.37 4 6 19 153.72 6.61 4 -6 -19 143.85 6.06 -4 6 -20 122.66 5.43 4 6 20 132.13 5.78 -4 -6 20 132.73 4.94 -4 6 -21 93.03 4.34 -4 -6 21 97.32 3.99 4 6 21 95.25 4.55 -4 -6 22 5.02 0.84 4 6 22 3.48 0.80 4 7 -20 4.31 0.88 4 7 -20 3.79 0.84 4 7 -19 154.84 5.41 4 7 -19 134.30 5.35 4 7 -18 206.03 6.55 4 7 -18 182.79 6.67 4 7 -17 2.46 0.80 4 7 -17 1.99 0.87 -4 7 17 1.51 0.59 4 7 -16 196.63 6.77 4 7 -16 191.22 7.51 4 7 -15 110.81 5.11 4 7 -15 120.01 6.11 -4 7 14 0.52 0.76 4 -7 14 1.38 0.76 4 7 -14 0.64 0.49 4 7 -14 -0.08 0.46 -4 7 14 0.40 0.40 4 7 -13 32.62 2.86 4 7 -13 29.77 3.23 4 -7 13 32.33 3.28 -4 7 13 32.83 3.29 4 7 -12 58.71 3.93 4 7 -12 61.12 4.69 4 -7 12 58.00 4.52 -4 7 12 57.43 4.39 4 7 -11 71.02 4.35 4 7 -11 78.06 5.42 4 -7 11 79.72 5.40 -4 7 11 66.05 4.81 4 7 -10 189.21 7.29 4 7 -10 202.32 8.83 4 -7 10 180.78 8.40 -4 7 10 191.35 8.31 4 7 -9 44.24 3.52 4 7 -9 43.63 4.16 4 -7 9 39.85 4.01 -4 7 9 39.65 3.84 4 7 -8 51.86 3.85 4 7 -8 58.97 4.81 4 -7 8 55.53 4.74 -4 7 8 55.84 4.51 4 7 -7 25.21 2.73 4 7 -7 24.29 3.14 4 -7 7 25.66 3.24 -4 7 7 30.94 3.40 4 7 -6 135.63 6.29 4 7 -6 131.38 7.29 4 -7 6 134.27 7.42 -4 7 6 136.56 7.18 4 7 -5 215.45 9.29 4 7 -5 212.36 7.93 4 -7 5 199.10 9.08 -4 7 5 210.91 8.98 4 7 -4 17.01 2.63 4 7 -4 14.47 2.11 4 -7 4 13.18 2.32 -4 7 4 15.76 2.42 -4 7 3 8.98 1.85 4 7 -3 7.91 1.79 4 7 -3 8.15 1.53 4 -7 3 11.12 2.14 4 7 -2 373.57 12.15 4 7 -2 390.89 10.90 4 -7 2 373.97 12.32 4 -7 2 369.02 11.89 -4 7 2 381.47 12.22 -4 7 1 6.23 1.62 4 7 -1 4.58 1.33 4 -7 1 4.16 1.30 4 -7 1 2.91 1.04 -4 7 0 6.16 1.51 4 7 0 5.80 1.57 4 -7 0 4.46 1.31 4 -7 0 6.09 1.54 -4 7 -1 2.46 1.09 4 7 1 5.61 1.50 4 -7 -1 3.25 1.23 4 7 2 361.86 11.55 4 -7 -2 375.27 12.29 -4 7 -2 378.35 12.23 -4 7 -3 9.10 1.85 4 7 3 7.49 1.69 4 -7 -3 6.58 1.64 4 7 4 15.96 2.35 -4 7 -4 13.16 2.25 4 -7 -4 14.79 2.45 -4 7 -5 206.12 8.89 4 7 5 203.48 8.24 4 -7 -5 207.86 9.25 -4 7 -6 132.64 7.08 4 7 6 124.17 6.33 -4 7 -7 26.09 3.16 4 7 7 25.51 2.87 -4 -7 7 25.85 2.76 -4 7 -8 58.38 4.63 4 7 8 53.90 4.02 -4 -7 8 60.44 4.20 4 7 9 42.74 3.53 -4 7 -9 42.36 3.94 -4 -7 9 44.53 3.59 4 7 10 191.34 7.47 -4 7 -10 190.74 8.36 -4 -7 10 202.38 7.68 -4 7 -11 69.87 4.96 -4 -7 11 77.82 4.65 4 7 11 68.74 4.35 -4 7 -12 61.45 4.58 -4 -7 12 63.28 4.11 4 7 12 63.01 4.09 -4 7 -13 30.22 3.17 -4 -7 13 31.17 2.83 -4 7 -14 0.41 0.71 -4 -7 14 0.42 0.42 -4 7 -15 111.96 5.88 -4 -7 15 119.37 5.28 4 -7 -15 112.47 6.03 -4 7 -16 188.51 7.43 -4 -7 16 198.74 6.67 4 7 16 182.19 7.06 4 -7 -16 190.31 7.64 -4 7 -17 1.71 0.79 -4 -7 17 1.75 0.72 4 7 17 1.49 0.70 4 -7 -17 3.52 0.99 -4 7 -18 175.39 6.52 -4 -7 18 184.11 5.93 4 7 18 164.72 6.17 4 -7 -18 172.23 6.48 4 7 19 115.23 4.80 4 -7 -19 124.33 5.04 -4 7 -20 5.53 1.00 -4 -7 20 4.18 0.82 4 -7 -20 5.15 0.91 -4 -7 21 42.31 2.29 4 8 -19 43.70 2.51 4 8 -18 21.70 1.84 4 8 -18 18.59 1.79 4 8 -17 5.06 0.96 4 8 -17 4.11 0.94 4 8 -16 209.07 6.42 4 8 -16 217.50 7.04 4 8 -15 36.96 2.71 4 8 -15 35.69 2.96 4 8 -14 118.26 4.99 4 8 -14 119.99 5.62 4 -8 14 111.83 5.34 -4 8 14 109.32 5.35 4 8 -13 137.43 5.56 4 8 -13 136.99 6.26 4 -8 13 132.61 6.16 -4 8 13 132.26 6.13 -4 8 12 9.42 1.74 4 8 -12 9.72 1.58 4 8 -12 11.26 1.89 4 -8 12 9.17 1.68 4 8 -11 154.54 6.15 4 8 -11 145.08 6.93 4 -8 11 151.17 7.06 -4 8 11 146.56 6.78 4 8 -10 49.31 3.49 4 8 -10 50.59 4.13 4 -8 10 44.63 3.87 -4 8 10 42.17 3.68 4 8 -9 200.08 7.24 4 8 -9 220.67 8.86 4 -8 9 204.31 8.53 -4 8 9 188.81 7.99 4 8 -8 156.38 6.47 4 8 -8 167.85 7.83 4 -8 8 150.44 7.40 -4 8 8 153.63 7.26 4 8 -7 40.67 3.31 4 8 -7 50.77 4.34 4 -8 7 42.58 3.98 -4 8 7 40.05 3.75 4 8 -6 20.48 2.43 4 8 -6 20.37 2.79 4 -8 6 20.53 2.80 -4 8 6 21.03 2.76 4 8 -5 102.43 6.20 4 8 -5 101.63 5.38 4 -8 5 97.17 6.06 -4 8 5 97.17 5.91 4 8 -4 91.90 5.83 4 8 -4 84.89 4.91 4 -8 4 82.35 5.56 -4 8 4 83.43 5.48 4 8 -3 48.48 4.22 4 8 -3 45.67 3.62 4 -8 3 44.61 4.09 -4 8 3 46.95 4.13 4 8 -2 192.82 8.40 4 8 -2 190.61 7.43 4 -8 2 178.19 8.15 -4 8 2 183.16 8.23 -4 8 1 9.68 1.94 4 8 -1 7.93 1.78 4 -8 1 8.99 1.88 4 -8 1 8.66 1.81 -4 8 0 0.47 0.64 4 8 0 1.12 0.90 4 -8 0 0.79 0.86 -4 8 -1 9.72 1.96 4 8 1 7.35 1.62 4 -8 -1 9.95 1.91 4 8 2 183.59 7.80 4 -8 -2 196.33 8.56 -4 8 -2 185.05 8.25 4 8 3 46.59 3.82 4 -8 -3 42.18 3.96 -4 8 -3 42.92 3.92 4 8 4 84.11 5.06 4 -8 -4 92.03 5.90 -4 8 -4 82.15 5.44 -4 8 -5 99.29 5.95 4 8 5 91.98 5.24 4 -8 -5 107.29 6.34 -4 8 -6 21.58 2.78 4 8 6 16.94 2.20 4 -8 -6 19.24 2.69 -4 8 -7 43.02 3.82 4 8 7 41.14 3.37 4 -8 -7 48.07 4.21 -4 8 -8 152.24 7.17 4 8 8 146.06 6.26 -4 -8 8 163.28 6.66 4 -8 -8 173.68 8.00 4 8 9 195.68 7.09 -4 8 -9 201.81 8.14 -4 -8 9 204.48 7.47 4 -8 -9 207.35 8.63 -4 8 -10 42.78 3.65 -4 -8 10 53.12 3.70 4 -8 -10 45.52 3.95 4 8 10 46.89 3.32 -4 8 -11 151.93 6.83 -4 -8 11 153.67 6.25 4 -8 -11 153.16 7.12 -4 8 -12 10.69 1.82 -4 -8 12 11.47 1.67 4 -8 -12 9.99 1.81 -4 8 -13 134.82 6.15 -4 -8 13 140.23 5.70 4 -8 -13 142.15 6.51 -4 8 -14 114.58 5.49 -4 -8 14 122.61 5.16 4 -8 -14 117.90 5.76 -4 8 -15 32.84 2.81 -4 -8 15 35.82 2.66 4 -8 -15 31.64 2.85 -4 8 -16 211.18 6.93 -4 -8 16 216.22 6.43 4 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1.36 4 10 -12 15.60 1.42 4 10 -11 1.85 0.62 4 10 -11 2.03 0.59 4 10 -10 327.75 7.82 4 10 -10 321.21 7.40 4 10 -9 10.48 1.45 4 10 -9 9.38 1.27 -4 10 9 9.24 1.37 4 10 -8 21.61 2.09 4 10 -8 19.62 1.88 -4 10 8 21.25 2.11 -4 10 7 3.34 0.90 4 10 -7 3.21 0.91 4 10 -7 4.50 0.93 4 10 -6 27.98 2.49 4 10 -6 23.85 2.15 -4 10 6 24.54 2.39 -4 10 5 2.63 0.87 4 10 -5 2.81 0.79 4 10 -5 1.51 0.61 4 10 -4 68.38 3.91 4 10 -4 66.15 3.70 -4 10 4 67.59 4.08 4 10 -3 42.74 3.06 4 10 -3 37.76 2.81 -4 10 3 36.78 3.02 4 10 -2 106.27 4.85 -4 10 2 102.65 5.12 4 10 -1 23.38 2.25 -4 10 1 23.50 2.46 4 10 0 55.51 3.39 -4 10 0 49.77 3.56 4 10 1 20.59 2.03 -4 10 -1 20.62 2.29 -4 10 -2 103.14 5.08 -4 10 -3 39.12 3.10 4 -10 -4 68.61 4.00 -4 10 -4 69.86 4.08 -4 10 -5 2.75 0.83 4 -10 -5 3.61 0.99 4 -10 -6 25.17 2.40 -4 10 -6 23.23 2.28 -4 10 -7 2.41 0.73 4 -10 -7 4.29 1.03 4 -10 -8 20.65 2.14 -4 10 -8 22.36 2.12 4 -10 -9 9.53 1.43 -4 10 -9 9.21 1.38 4 -10 -10 328.37 8.26 -4 10 -10 312.44 7.78 -4 10 -11 1.54 0.55 4 -10 -11 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918.34 20.65 5 5 -10 881.58 17.08 5 5 -9 146.70 7.91 5 5 -9 142.68 6.41 5 5 -8 884.62 20.13 5 5 -8 830.73 16.68 5 5 -7 103.46 6.51 5 5 -7 97.51 5.33 5 -5 7 88.30 5.34 5 5 -6 150.14 7.81 5 5 -6 145.46 6.54 5 -5 6 137.02 6.80 5 5 -5 63.02 4.97 5 5 -5 60.27 4.19 5 -5 5 58.25 4.48 5 5 -4 1.29 0.98 5 5 -4 0.44 0.53 5 -5 4 2.69 1.21 5 -5 4 2.75 1.02 5 5 -3 78.16 5.44 5 5 -3 74.11 4.58 -5 -5 -3 55.75 4.92 5 -5 3 73.08 5.14 -5 5 3 67.73 4.49 5 -5 3 65.35 5.18 5 5 -2 105.75 6.36 5 5 -2 112.91 6.45 -5 -5 -2 105.96 6.84 5 -5 2 117.27 6.55 -5 5 2 100.20 5.49 5 -5 2 107.68 6.75 5 5 -1 78.17 5.39 5 5 -1 90.23 5.68 -5 -5 -1 82.59 6.04 5 -5 1 87.53 5.73 -5 5 1 75.85 4.79 5 -5 1 87.81 6.04 5 5 0 151.22 7.46 5 5 0 149.92 7.31 -5 -5 0 148.05 8.13 5 -5 0 160.10 7.79 -5 5 0 139.56 6.50 5 -5 0 150.66 8.08 5 5 1 88.55 5.59 5 5 1 94.21 5.69 -5 -5 1 79.01 5.85 5 -5 -1 77.96 5.82 5 -5 -1 89.37 5.84 5 5 2 104.80 6.11 5 5 2 110.71 6.15 -5 -5 2 105.05 6.73 5 -5 -2 104.08 6.74 5 -5 -2 114.79 6.66 5 5 3 74.70 4.99 5 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5 -5 -19 1.63 0.66 -5 -5 19 2.59 0.73 5 5 19 3.17 0.93 5 -5 -20 19.44 1.80 -5 -5 20 24.43 1.95 5 5 20 23.22 2.26 -5 -5 21 6.28 0.95 -5 -5 22 24.83 1.68 5 6 -20 78.33 3.37 -5 6 20 45.40 2.42 5 6 -19 24.62 2.10 -5 6 19 21.68 1.84 5 6 -18 25.92 2.38 5 6 -18 29.57 2.32 -5 6 18 21.06 1.95 5 6 -17 62.73 3.97 5 6 -17 69.46 3.67 5 6 -16 84.21 4.88 5 6 -16 83.88 4.18 5 6 -15 4.48 1.25 5 6 -15 2.62 0.84 5 6 -14 8.33 1.69 5 6 -14 6.42 1.25 5 6 -13 117.80 6.47 5 6 -13 110.98 5.16 5 6 -12 123.90 6.81 5 6 -12 124.34 5.61 5 6 -11 66.38 4.99 5 6 -11 63.11 4.02 5 6 -10 49.01 4.33 5 6 -10 41.56 3.32 5 6 -9 1.56 0.84 5 6 -9 1.51 0.85 5 6 -8 86.44 5.84 5 6 -8 85.35 4.88 5 6 -7 433.86 13.34 5 6 -7 431.27 11.43 5 6 -6 17.24 2.66 5 6 -6 17.05 2.19 5 6 -5 78.71 5.48 5 6 -5 82.14 4.84 5 -6 5 75.68 5.00 5 6 -4 143.57 7.39 5 6 -4 148.82 6.56 5 -6 4 150.35 7.26 5 6 -3 76.61 5.32 5 6 -3 71.80 4.52 5 -6 3 67.81 4.93 5 6 -2 105.39 6.18 5 -6 2 110.79 6.40 5 6 -1 125.34 6.73 5 -6 1 134.34 7.09 5 6 0 250.25 9.49 5 -6 0 255.29 10.03 5 6 1 121.03 6.50 5 -6 -1 124.56 6.99 5 6 2 101.08 5.87 5 -6 -2 105.98 6.50 5 6 3 66.25 4.73 5 -6 -3 70.13 5.26 5 6 4 133.54 6.70 5 -6 -4 135.32 7.40 5 6 5 70.23 4.78 5 -6 -5 72.81 5.43 5 6 6 13.78 2.11 5 -6 -6 17.10 2.63 5 6 7 419.08 11.74 5 -6 -7 431.38 13.36 5 6 8 82.26 4.98 -5 -6 8 86.22 4.86 5 -6 -8 88.46 5.94 5 6 9 1.34 0.81 -5 -6 9 2.63 0.92 5 -6 -9 1.08 0.71 5 6 10 45.68 3.59 -5 -6 10 47.92 3.56 5 -6 -10 45.36 4.23 -5 -6 11 63.57 4.06 5 -6 -11 66.00 5.02 5 6 11 63.77 4.19 -5 -6 12 123.39 5.59 5 6 12 122.63 6.33 5 -6 -12 139.04 7.20 5 6 12 126.58 5.86 -5 -6 13 108.71 5.14 5 6 13 111.06 5.92 5 -6 -13 114.37 6.39 -5 -6 14 8.74 1.45 5 6 14 9.58 1.73 5 -6 -14 8.10 1.60 -5 -6 15 3.18 0.88 5 6 15 2.75 0.90 5 -6 -15 2.43 0.91 -5 -6 16 89.39 4.27 5 6 16 84.42 4.77 5 -6 -16 82.20 4.78 -5 -6 17 67.30 3.53 5 6 17 67.20 4.07 5 -6 -17 64.81 3.95 5 -6 -18 25.06 2.17 -5 -6 18 27.46 2.14 5 -6 -18 23.55 2.18 5 -6 -19 20.40 1.74 -5 -6 19 26.36 1.97 -5 -6 20 73.60 3.09 5 7 -18 95.63 3.90 5 7 -18 110.18 4.01 5 7 -17 37.54 2.67 5 7 -17 40.47 2.52 5 7 -16 233.25 7.28 5 7 -16 234.52 6.49 5 7 -15 3.97 1.09 5 7 -15 4.15 0.91 5 7 -14 17.49 2.18 5 7 -14 13.16 1.65 5 7 -13 86.52 5.04 5 7 -13 80.69 4.14 5 7 -12 8.96 1.70 5 7 -12 7.81 1.36 5 7 -11 95.00 5.60 5 7 -11 92.82 4.63 5 7 -10 13.82 2.18 5 7 -10 11.09 1.63 5 7 -9 91.42 5.62 5 7 -9 89.06 4.73 5 7 -8 2.78 0.97 5 7 -8 2.75 0.90 5 7 -7 5.85 1.63 5 7 -7 7.28 1.42 5 7 -6 46.88 4.11 5 7 -6 45.49 3.50 5 7 -5 75.19 5.15 5 7 -5 75.60 4.54 5 7 -4 448.01 12.96 5 7 -4 464.64 11.72 5 7 -3 242.10 9.33 5 7 -3 244.35 8.27 5 -7 3 242.22 9.07 5 7 -2 56.72 4.45 5 -7 2 55.10 4.35 5 7 -1 288.22 10.06 5 -7 1 276.17 10.01 5 7 0 522.76 13.80 5 -7 0 523.61 14.27 5 7 1 291.68 9.98 5 -7 -1 282.68 10.41 5 7 2 61.32 4.45 5 -7 -2 54.65 4.53 5 7 3 241.23 8.84 5 -7 -3 244.52 9.70 5 7 4 431.64 11.89 5 -7 -4 429.71 13.04 5 7 5 69.44 4.56 5 -7 -5 72.59 5.21 5 7 6 47.17 3.69 5 -7 -6 47.37 4.22 5 7 7 5.04 1.22 5 -7 -7 6.03 1.57 5 7 8 4.40 1.18 5 -7 -8 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16.64 2.08 6 7 10 17.78 1.85 6 -7 -11 93.69 4.77 6 -7 -12 33.35 2.71 6 -7 -13 12.68 1.58 6 -7 -14 32.21 2.34 6 -7 -15 38.33 2.21 6 8 -11 5.52 0.92 6 8 -10 76.28 3.61 6 8 -10 58.65 2.80 6 8 -9 0.92 0.55 6 8 -9 0.65 0.38 6 8 -8 23.45 2.14 6 8 -8 18.48 1.68 6 8 -7 92.19 4.41 6 8 -6 65.98 3.76 6 8 -5 37.59 2.87 6 8 -4 76.87 4.15 6 8 -3 33.55 2.73 6 8 -2 34.24 2.80 6 8 -1 130.26 5.43 6 -8 1 122.36 5.12 6 8 0 19.10 2.09 6 -8 0 17.46 1.98 6 8 1 126.10 5.29 6 -8 -1 125.45 5.40 6 8 2 33.81 2.69 6 -8 -2 32.48 2.76 6 8 3 34.05 2.64 6 -8 -3 29.18 2.63 6 8 4 74.68 3.87 6 -8 -4 75.32 4.24 6 8 5 40.89 2.81 6 -8 -5 39.47 3.04 6 -8 -6 61.39 3.76 6 8 6 62.79 3.41 6 -8 -7 92.88 4.54 6 8 7 90.39 3.99 6 -8 -8 22.10 2.18 6 8 8 23.29 1.96 6 -8 -9 0.39 0.44 6 -8 -10 76.80 3.72 6 -8 -11 5.87 1.03 6 -8 -12 42.46 2.45 6 9 -7 44.62 2.37 6 9 -6 5.03 0.85 6 9 -5 85.71 3.56 6 9 -4 67.08 3.20 6 9 -3 42.56 2.58 6 9 -2 38.44 2.46 6 9 -1 73.78 3.42 6 9 0 1.41 0.65 6 9 1 70.18 3.29 6 9 2 40.31 2.45 6 9 3 42.26 2.45 6 9 4 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187.08 7.16 7 1 -13 47.61 3.23 7 -1 13 48.92 3.06 7 -1 13 49.95 3.85 7 1 -12 4.07 1.02 7 -1 12 4.81 1.05 7 1 -11 117.78 5.39 7 -1 11 120.57 5.21 7 1 -10 46.81 3.44 7 -1 10 44.75 3.21 7 1 -9 157.84 6.48 7 -1 9 173.93 7.53 7 -1 9 165.46 6.39 7 1 -8 122.13 5.73 7 -1 8 129.82 5.73 7 1 -7 11.52 1.84 7 -1 7 10.78 1.67 7 1 -6 119.85 5.77 7 -1 6 128.77 5.96 7 1 -6 117.26 5.48 7 1 -5 150.38 6.51 7 1 -5 141.34 6.23 7 -1 5 152.76 6.60 7 1 -4 241.02 8.38 7 -1 4 237.51 8.44 7 1 -3 19.35 2.37 7 -1 3 18.76 2.33 7 1 -2 8.67 1.72 7 -1 2 5.61 1.35 7 1 -1 186.66 7.53 7 -1 1 176.09 7.52 7 1 0 496.62 12.72 7 -1 0 484.96 12.94 7 1 1 186.29 7.55 7 -1 -1 184.60 7.86 7 1 2 7.14 1.54 7 -1 -2 6.92 1.62 7 1 3 23.02 2.64 7 -1 -3 18.98 2.54 7 1 3 19.28 2.35 7 1 4 261.14 8.75 7 -1 -4 251.28 9.24 7 1 4 242.03 8.58 7 -1 -5 149.68 6.76 7 1 5 161.54 6.70 7 -1 -5 147.08 6.92 7 1 5 154.62 6.80 7 -1 -6 121.98 6.08 7 1 6 131.25 5.94 7 -1 -6 119.41 6.14 7 -1 -7 9.94 1.74 7 1 7 12.76 1.84 7 -1 -7 10.56 1.82 7 -1 -8 126.37 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2.12 7 -2 -11 15.96 1.99 7 -2 -12 63.23 3.99 7 2 12 73.51 4.57 7 -2 -13 55.72 3.59 -7 -2 13 57.52 3.37 7 -2 -14 56.63 3.49 -7 -2 14 53.58 3.14 7 -2 -15 90.50 4.25 7 2 15 102.95 4.89 -7 -2 15 92.46 3.97 7 -2 -16 12.02 1.45 -7 -2 16 12.22 1.38 7 -2 -17 89.83 3.72 7 2 17 93.73 4.07 -7 -2 17 87.56 3.47 7 -2 -18 64.33 2.88 7 2 18 66.65 3.07 -7 -2 18 61.60 2.68 7 3 -17 57.42 2.71 7 3 -16 8.72 1.12 7 -3 16 18.93 1.88 7 3 -15 27.43 2.11 7 -3 15 42.02 2.84 7 3 -14 42.09 2.72 7 -3 14 55.17 3.48 7 3 -13 37.35 2.65 7 -3 13 50.53 3.44 7 3 -12 6.20 1.17 7 -3 12 6.64 1.08 7 3 -11 28.14 2.44 7 -3 11 31.71 2.48 7 3 -10 9.39 1.44 7 -3 10 9.54 1.43 7 3 -9 154.95 6.08 7 -3 9 161.22 6.10 7 3 -8 5.14 1.16 7 -3 8 4.81 1.18 7 3 -7 307.95 8.91 7 -3 7 334.23 10.06 7 -3 7 317.40 9.22 7 -3 6 371.41 10.19 7 3 -5 34.65 3.18 7 -3 5 36.14 3.14 7 3 -4 52.72 3.94 7 -3 4 58.58 4.06 7 3 -3 23.60 2.68 7 -3 3 28.91 2.92 7 3 -2 105.42 5.64 7 3 -2 105.95 4.96 7 -3 2 104.03 5.59 7 3 -1 102.51 5.58 7 3 -1 102.50 4.98 7 -3 1 96.27 5.44 7 3 0 87.10 5.10 7 3 0 89.44 4.72 7 -3 0 83.61 5.13 7 3 1 100.44 5.51 7 3 1 115.48 5.42 7 -3 -1 99.85 5.66 7 3 2 107.94 5.68 7 3 2 117.69 5.52 7 -3 -2 108.07 5.96 7 3 3 26.65 2.80 7 3 3 31.13 2.84 7 -3 -3 28.56 3.06 7 3 4 54.32 3.96 7 3 4 62.31 4.03 7 -3 -4 54.38 4.25 7 3 5 46.70 3.48 7 -3 -5 39.27 3.63 7 3 5 39.18 3.31 7 -3 -6 365.21 11.25 7 3 6 372.38 10.56 7 -3 -7 283.24 9.46 7 3 7 358.53 9.56 7 3 7 359.82 10.29 7 -3 -7 309.35 10.17 7 3 7 309.94 9.41 7 3 8 5.74 1.26 7 -3 -8 3.86 1.09 -7 -3 8 5.23 1.12 7 -3 -8 4.88 1.38 7 -3 -9 152.97 6.65 -7 -3 9 157.06 5.82 7 -3 -9 151.72 6.81 7 -3 -10 8.56 1.53 -7 -3 10 9.18 1.38 7 -3 -10 8.78 1.59 7 -3 -11 28.16 2.71 7 -3 -11 28.60 2.73 -7 -3 11 27.55 2.35 7 -3 -12 7.56 1.38 -7 -3 12 5.61 1.03 7 -3 -12 6.05 1.19 7 -3 -13 33.86 2.74 -7 -3 13 32.52 2.41 7 -3 -14 42.83 2.96 -7 -3 14 43.76 2.67 7 -3 -15 26.66 2.20 -7 -3 15 27.55 2.04 7 -3 -16 8.02 1.15 -7 -3 16 9.57 1.15 7 -3 -17 57.33 2.78 -7 -3 17 54.46 2.54 7 4 -16 37.73 2.14 7 4 -15 32.52 2.11 7 4 -14 27.55 2.05 7 4 -13 14.97 1.59 7 4 -12 10.64 1.41 7 4 -11 17.56 1.83 7 4 -10 6.68 1.17 7 -4 10 6.55 1.11 7 4 -9 3.97 1.01 7 -4 9 4.91 1.03 7 4 -8 80.20 4.62 7 4 -8 91.00 4.47 7 -4 8 84.74 4.30 7 4 -7 34.09 3.07 7 4 -7 35.13 2.79 7 -4 7 34.25 2.83 7 4 -6 27.81 2.82 7 -4 6 24.56 2.47 7 4 -5 23.58 2.64 7 -4 5 20.93 2.35 7 4 -4 138.70 6.42 7 -4 4 149.36 6.38 7 4 -3 453.44 12.02 7 -4 3 458.02 11.67 7 4 -2 7.93 1.66 7 -4 2 6.70 1.40 7 4 -1 125.26 6.11 7 -4 1 124.50 6.03 7 4 0 261.65 8.91 7 -4 0 261.03 8.97 7 4 1 131.04 6.17 7 -4 -1 125.73 6.19 7 4 2 8.71 1.66 7 -4 -2 6.08 1.53 7 4 3 472.60 11.88 7 -4 -3 455.41 12.33 7 4 4 150.47 6.43 7 -4 -4 150.48 6.95 7 4 5 22.52 2.46 7 -4 -5 22.04 2.64 7 -4 -6 28.44 3.02 7 4 6 28.46 2.72 7 -4 -7 33.83 3.22 7 4 7 34.79 2.94 7 -4 -8 92.78 5.28 7 4 8 89.97 4.68 7 -4 -9 4.68 1.17 7 -4 -10 4.27 1.07 -7 -4 10 6.80 1.12 7 -4 -10 5.87 1.31 7 -4 -11 17.68 2.07 -7 -4 11 15.67 1.63 7 -4 -11 18.47 2.15 7 -4 -12 9.95 1.51 -7 -4 12 9.73 1.26 7 -4 -12 9.75 1.46 7 -4 -13 12.57 1.62 -7 -4 13 14.16 1.46 7 -4 -13 11.77 1.50 7 -4 -14 22.75 2.04 -7 -4 14 22.89 1.77 7 -4 -15 30.83 2.21 -7 -4 15 29.04 1.88 7 -4 -16 34.82 2.14 7 5 -14 96.70 3.47 7 5 -13 34.72 2.17 7 5 -12 84.82 3.58 7 5 -11 64.89 3.25 7 5 -10 22.25 2.14 7 5 -10 23.09 1.99 7 5 -9 46.64 3.27 7 5 -9 50.27 3.01 7 5 -8 3.62 1.02 7 5 -8 4.58 0.94 7 -5 8 3.69 0.84 7 5 -7 38.98 3.16 7 -5 7 38.77 2.78 7 5 -6 7.87 1.47 7 -5 6 10.24 1.52 7 5 -5 96.62 5.13 7 -5 5 102.88 4.89 7 5 -4 229.20 8.03 7 -5 4 226.97 7.60 7 5 -3 30.49 2.89 7 -5 3 28.73 2.71 7 5 -2 9.16 1.62 7 -5 2 10.74 1.70 7 5 -1 144.85 6.30 7 -5 1 147.59 6.38 7 5 0 1.24 0.78 7 -5 0 0.80 0.72 7 5 1 140.35 6.11 7 -5 -1 139.02 6.32 7 5 2 10.98 1.70 7 -5 -2 10.63 1.79 7 5 3 27.22 2.62 7 -5 -3 28.10 2.85 7 5 4 225.55 7.55 7 -5 -4 226.05 8.10 7 5 5 112.09 5.15 7 -5 -5 96.17 5.27 7 5 6 8.57 1.44 7 -5 -6 8.34 1.57 7 -5 -7 37.40 3.22 7 5 7 34.01 2.74 7 5 8 5.05 1.11 7 -5 -8 4.66 1.14 7 -5 -9 45.55 3.41 7 -5 -10 19.62 2.12 7 -5 -10 24.01 2.43 7 -5 -11 61.68 3.55 7 -5 -11 67.95 3.84 7 -5 -12 79.31 3.88 7 -5 -12 89.74 4.17 7 -5 -13 32.64 2.34 7 -5 -13 31.27 2.21 7 -5 -14 91.12 3.65 7 6 -10 14.87 1.59 7 6 -9 11.63 1.50 7 6 -8 45.28 3.04 7 6 -7 11.05 1.54 7 6 -6 31.53 2.66 7 -6 6 26.42 2.09 7 6 -5 34.74 2.84 7 -6 5 34.46 2.52 7 6 -4 15.24 1.92 7 -6 4 12.33 1.57 7 6 -3 12.42 1.72 7 -6 3 12.38 1.64 7 6 -2 215.24 7.23 7 -6 2 212.78 7.02 7 6 -1 57.95 3.69 7 -6 1 55.59 3.61 7 6 0 2.06 0.76 7 -6 0 1.21 0.73 7 6 1 58.69 3.67 7 -6 -1 60.46 3.83 7 6 2 202.86 6.82 7 -6 -2 219.84 7.49 7 6 3 11.42 1.58 7 -6 -3 12.29 1.80 7 6 4 16.09 1.83 7 -6 -4 15.79 1.98 7 -6 -5 35.58 2.94 7 6 5 35.64 2.66 7 -6 -6 32.34 2.75 7 6 6 29.80 2.37 7 -6 -7 10.89 1.60 7 6 7 10.13 1.38 7 -6 -8 47.94 3.28 7 6 8 48.56 2.92 7 -6 -9 10.35 1.50 7 -6 -10 14.00 1.62 7 -6 -10 19.96 1.94 7 -6 -11 24.19 2.00 7 -6 -11 32.98 2.37 7 -6 -12 29.34 2.04 7 7 -8 26.44 1.94 7 7 -7 23.89 1.94 7 7 -6 70.88 3.45 7 7 -5 16.26 1.71 7 7 -4 66.08 3.47 7 7 -3 182.53 5.87 7 -7 3 144.23 4.68 7 7 -2 18.70 1.87 7 -7 2 13.78 1.50 7 7 -1 171.49 5.70 7 -7 1 164.61 5.41 7 7 0 3.30 0.88 7 -7 0 5.17 1.01 7 7 1 163.97 5.50 7 -7 -1 154.22 5.45 7 7 2 17.88 1.78 7 -7 -2 15.37 1.74 7 7 3 168.98 5.44 7 -7 -3 173.15 5.82 7 -7 -4 69.47 3.64 7 7 4 69.22 3.38 7 -7 -5 12.76 1.55 7 7 5 14.86 1.54 7 -7 -6 72.22 3.57 7 7 6 74.00 3.36 7 -7 -7 24.95 2.04 7 -7 -8 26.96 2.03 7 -7 -9 2.14 0.58 7 8 -2 28.65 1.87 7 8 -1 7.34 0.96 7 8 0 93.78 3.43 7 8 1 7.64 0.97 8 0 0 4.20 0.98 8 0 1 25.68 2.43 8 0 -1 27.59 2.51 8 0 2 7.97 1.37 8 0 -2 9.73 1.49 8 0 3 25.89 2.42 8 0 -3 21.95 2.19 8 0 4 12.89 1.68 8 0 -4 12.83 1.63 8 0 5 101.22 4.53 8 0 -5 91.58 4.28 8 0 6 18.83 1.92 8 0 -6 14.86 1.65 8 0 7 58.56 3.29 8 0 8 43.76 2.79 8 0 -9 0.88 0.43 8 0 9 1.54 0.59 8 0 -10 77.63 3.62 8 0 10 94.16 3.84 8 0 -11 0.64 0.42 8 0 -12 75.41 3.30 8 0 -13 91.72 3.45 -8 0 13 83.75 3.14 8 1 -12 29.50 1.99 8 1 -11 295.10 6.87 8 1 -10 10.77 1.31 8 -1 10 12.36 1.38 8 1 -9 91.17 3.89 8 -1 9 109.66 4.25 8 -1 8 142.79 5.05 8 -1 7 29.34 2.34 8 -1 6 70.95 3.70 8 -1 5 28.87 2.41 8 1 -4 12.21 1.53 8 -1 4 13.06 1.68 8 1 -3 68.76 3.68 8 -1 3 68.03 3.83 8 1 -2 34.11 2.67 8 -1 2 36.06 2.86 8 1 -1 80.81 4.17 8 -1 1 82.11 4.35 8 1 0 1.11 0.58 8 -1 0 0.42 0.54 8 1 1 83.57 4.28 8 -1 -1 79.54 4.36 8 1 2 36.54 2.85 8 -1 -2 31.79 2.75 8 1 3 72.66 3.96 8 -1 -3 68.17 4.00 8 1 4 14.14 1.72 8 -1 -4 13.92 1.81 8 1 5 32.39 2.57 8 -1 -5 28.13 2.47 8 1 6 75.07 3.81 8 -1 -6 69.42 3.76 8 1 7 29.26 2.30 8 -1 -7 25.86 2.20 8 -1 -8 111.75 4.59 8 -1 -8 114.35 4.38 8 -1 -9 98.05 4.19 -8 -1 9 79.14 3.33 8 -1 -10 10.61 1.36 -8 -1 10 9.05 1.12 8 -1 -11 309.73 7.24 -8 -1 11 264.15 6.09 8 -1 -12 33.59 2.20 -8 -1 12 27.26 1.78 8 -1 -13 18.57 1.54 8 -2 10 121.79 4.17 8 -2 9 87.06 3.68 8 -2 8 41.05 2.61 8 -2 7 122.85 4.72 8 -2 6 101.66 4.39 8 -2 5 8.67 1.34 8 -2 4 17.86 1.90 8 2 -3 13.49 1.49 8 -2 3 15.23 1.81 8 2 -2 20.43 1.90 8 -2 2 21.03 2.15 8 2 -1 0.54 0.38 8 -2 1 1.98 0.71 8 2 0 2.65 0.76 8 -2 0 2.55 0.79 8 2 1 1.64 0.66 8 -2 -1 1.88 0.75 8 2 2 23.78 2.21 8 -2 -2 25.58 2.44 8 2 3 18.26 1.93 8 -2 -3 14.67 1.87 8 2 4 19.89 1.98 8 -2 -4 17.83 2.02 8 2 5 9.49 1.42 8 -2 -5 7.49 1.31 8 2 6 114.66 4.66 8 -2 -6 101.89 4.68 8 -2 -7 109.45 4.65 8 -2 -8 30.42 2.35 8 -2 -8 36.19 2.53 8 -2 -9 68.32 3.44 8 -2 -9 70.30 3.31 8 -2 -10 104.78 4.18 8 -2 -11 17.98 1.64 8 -2 -12 12.89 1.31 8 -3 9 43.42 2.39 8 -3 8 47.52 2.64 8 -3 7 71.57 3.40 8 -3 6 137.10 4.91 8 -3 5 118.90 4.72 8 -3 4 142.19 5.29 8 -3 3 66.93 3.66 8 -3 2 9.32 1.40 8 -3 1 7.42 1.27 8 -3 0 39.26 2.88 8 3 1 6.53 1.15 8 -3 -1 10.09 1.49 8 -3 -2 9.12 1.44 8 -3 -3 65.68 3.83 8 -3 -4 151.16 5.85 8 -3 -5 116.94 5.04 8 -3 -6 133.65 5.29 8 -3 -7 72.25 3.74 8 -3 -8 31.99 2.31 8 -3 -8 44.01 2.76 8 -3 -9 31.46 2.23 8 -3 -9 39.03 2.45 8 -3 -10 11.24 1.30 8 -4 7 49.91 2.56 8 -4 6 102.83 3.91 8 -4 5 155.33 5.02 8 -4 4 34.26 2.41 8 -4 3 31.72 2.38 8 -4 2 263.15 7.18 8 -4 1 38.46 2.70 8 4 -1 30.59 2.35 8 4 0 0.81 0.49 8 -4 0 0.51 0.41 8 -4 -1 40.18 2.78 8 4 1 34.05 2.53 8 -4 -2 262.23 7.33 8 4 2 246.56 6.94 8 -4 -3 30.52 2.44 8 4 3 34.58 2.51 8 -4 -4 33.78 2.57 8 -4 -5 157.37 5.57 8 -4 -6 100.21 4.30 8 -4 -7 54.64 3.07 8 -4 -8 25.94 2.02 8 -5 4 20.21 1.63 8 -5 3 134.47 4.42 8 -5 2 36.36 2.32 8 5 -2 30.08 2.10 8 -5 1 10.95 1.32 8 5 -1 9.01 1.17 8 5 0 2.32 0.64 8 -5 0 2.63 0.66 8 -5 -1 9.47 1.27 8 5 1 8.46 1.18 8 -5 -2 34.52 2.36 8 5 2 34.72 2.33 8 -5 -3 132.51 4.68 8 -5 -4 20.54 1.80 8 -5 -5 37.97 2.39 8 -5 -6 23.94 1.87 8 -5 -7 5.68 0.89 0 0 0 0.00 0.00 TITL 19-EL2 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 7.265495 10.192666 24.323825 90.0000 90.0000 90.0000 ZERR 8.00 0.000099 0.000138 0.000321 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 88.00 80.00 8.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 32987 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.6463(3) 0.38487(19) 0.70856(8) 0.0125(4) Uani 1 1 d . . . . . H1 H 0.546651 0.445882 0.717690 0.015 Uiso 1 1 calc R . . . . C2 C 0.5685(3) 0.24561(19) 0.70531(8) 0.0139(4) Uani 1 1 d . . . . . C3 C 0.4278(3) 0.2209(2) 0.66150(8) 0.0171(4) Uani 1 1 d . . . . . H3A H 0.317520 0.271323 0.669135 0.021 Uiso 1 1 calc R . . . . H3B H 0.395002 0.128629 0.661074 0.021 Uiso 1 1 calc R . . . . C4 C 0.5071(3) 0.26087(19) 0.60514(8) 0.0152(4) Uani 1 1 d . . . . . H4 H 0.614385 0.205439 0.597668 0.018 Uiso 1 1 calc R . . . . C5 C 0.5731(3) 0.40449(18) 0.60863(7) 0.0125(4) Uani 1 1 d . . . . . H5 H 0.467913 0.456302 0.621465 0.015 Uiso 1 1 calc R . . . . C6 C 0.6253(3) 0.45844(19) 0.55198(8) 0.0142(4) Uani 1 1 d . . . . . H6A H 0.714900 0.399774 0.535549 0.017 Uiso 1 1 calc R . . . . H6B H 0.516563 0.457249 0.528850 0.017 Uiso 1 1 calc R . . . . C7 C 0.7042(3) 0.59650(19) 0.55164(7) 0.0121(4) Uani 1 1 d . . . . . C8 C 0.8554(3) 0.62334(18) 0.59372(8) 0.0115(4) Uani 1 1 d . . . . . C9 C 0.7742(3) 0.57391(18) 0.65017(7) 0.0108(4) Uani 1 1 d . . . . . H9 H 0.651435 0.613778 0.650665 0.013 Uiso 1 1 calc R . . . . C10 C 0.7300(3) 0.42374(18) 0.65193(7) 0.0117(4) Uani 1 1 d . . . . . C11 C 0.8685(3) 0.63895(19) 0.69928(8) 0.0129(4) Uani 1 1 d . . . . . H11 H 0.806849 0.611330 0.733189 0.015 Uiso 1 1 calc R . . . . C12 C 0.8515(3) 0.78878(19) 0.69329(8) 0.0132(4) Uani 1 1 d . . . . . H12 H 0.910397 0.829645 0.725225 0.016 Uiso 1 1 calc R . . . . C13 C 0.9455(3) 0.83941(19) 0.64201(8) 0.0130(4) Uani 1 1 d . . . . . H13 H 1.073565 0.809338 0.642710 0.016 Uiso 1 1 calc R . . . . C14 C 0.8519(3) 0.77662(19) 0.59302(8) 0.0123(4) Uani 1 1 d . . . . . C15 C 0.6445(3) 0.80290(18) 0.59097(8) 0.0127(4) Uani 1 1 d . . . . . H15 H 0.622274 0.879167 0.567355 0.015 Uiso 1 1 calc R . . . . C16 C 0.5553(3) 0.82813(18) 0.64717(8) 0.0130(4) Uani 1 1 d . . . . . C18 C 0.9466(3) 0.98949(19) 0.63980(8) 0.0173(4) Uani 1 1 d . . . . . H18A H 1.009371 1.017916 0.607175 0.026 Uiso 1 1 calc GR . . . . H18B H 1.008931 1.023325 0.671585 0.026 Uiso 1 1 calc GR . . . . H18C H 0.822292 1.021342 0.639256 0.026 Uiso 1 1 calc GR . . . . C19 C 0.8983(3) 0.33464(19) 0.64246(8) 0.0144(4) Uani 1 1 d . . . . . H19A H 0.918839 0.324512 0.603705 0.022 Uiso 1 1 calc GR . . . . H19B H 0.876155 0.250254 0.658687 0.022 Uiso 1 1 calc GR . . . . H19C H 1.004947 0.373650 0.659097 0.022 Uiso 1 1 calc GR . . . . C29 C 0.3646(3) 0.2356(2) 0.56027(9) 0.0220(5) Uani 1 1 d . . . . . H29A H 0.322463 0.146477 0.562628 0.033 Uiso 1 1 calc GR . . . . H29B H 0.419377 0.250279 0.524895 0.033 Uiso 1 1 calc GR . . . . H29C H 0.262254 0.294055 0.565078 0.033 Uiso 1 1 calc GR . . . . C30 C 1.0451(3) 0.5702(2) 0.57647(8) 0.0153(4) Uani 1 1 d . . . . . H30A H 1.100527 0.629370 0.550598 0.023 Uiso 1 1 calc GR . . . . H30B H 1.030606 0.485522 0.559773 0.023 Uiso 1 1 calc GR . . . . H30C H 1.122554 0.562662 0.608297 0.023 Uiso 1 1 calc GR . . . . O1 O 0.6245(2) 0.15899(14) 0.73531(6) 0.0192(3) Uani 1 1 d . . . . . O2 O 0.78221(19) 0.39091(14) 0.74995(5) 0.0161(3) Uani 1 1 d . . . . . H2 H 0.736770 0.370119 0.779548 0.024 Uiso 1 1 calc GR . . . . O3 O 1.0562(2) 0.60103(14) 0.70159(6) 0.0169(3) Uani 1 1 d . . . . . H3 H 1.108909 0.643556 0.725480 0.025 Uiso 1 1 calc GR . . . . O4 O 0.65561(18) 0.82581(13) 0.69344(5) 0.0138(3) Uani 1 1 d . . . . . O5 O 0.3942(2) 0.85502(15) 0.64981(6) 0.0189(3) Uani 1 1 d . . . . . O6 O 0.56081(19) 0.68906(13) 0.56585(5) 0.0128(3) Uani 1 1 d . . . . . O7 O 0.77279(19) 0.62548(14) 0.49822(5) 0.0147(3) Uani 1 1 d . . . . . H7 H 0.686407 0.633552 0.476787 0.022 Uiso 1 1 calc GR . . . . O8 O 0.9357(2) 0.82995(14) 0.54481(5) 0.0148(3) Uani 1 1 d . . . . . H8 H 0.903142 0.787632 0.517838 0.022 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0089(9) 0.0171(9) 0.0114(8) 0.0012(7) -0.0008(7) 0.0014(7) C2 0.0096(9) 0.0179(9) 0.0142(8) 0.0012(7) 0.0037(7) 0.0016(8) C3 0.0160(10) 0.0154(9) 0.0199(10) 0.0029(7) -0.0024(8) -0.0022(8) C4 0.0152(9) 0.0134(9) 0.0169(10) -0.0004(7) -0.0025(8) -0.0011(7) C5 0.0115(9) 0.0133(9) 0.0125(8) -0.0008(7) -0.0009(7) -0.0007(8) C6 0.0145(10) 0.0156(9) 0.0124(8) -0.0017(7) -0.0019(7) 0.0006(8) C7 0.0114(9) 0.0144(9) 0.0104(8) 0.0010(7) 0.0010(7) 0.0025(8) C8 0.0106(9) 0.0135(9) 0.0105(8) 0.0005(7) -0.0009(7) 0.0001(7) C9 0.0093(9) 0.0135(8) 0.0096(8) 0.0013(7) -0.0003(7) 0.0013(7) C10 0.0097(9) 0.0138(8) 0.0115(8) 0.0006(7) -0.0002(7) 0.0008(7) C11 0.0100(9) 0.0169(9) 0.0118(8) -0.0001(7) -0.0021(7) -0.0012(7) C12 0.0101(9) 0.0170(9) 0.0126(9) -0.0012(7) -0.0007(7) -0.0013(7) C13 0.0108(9) 0.0143(9) 0.0141(9) 0.0000(7) 0.0003(7) -0.0008(7) C14 0.0120(9) 0.0146(9) 0.0104(8) 0.0019(7) 0.0022(7) -0.0006(8) C15 0.0125(9) 0.0115(8) 0.0140(9) -0.0008(7) 0.0000(7) 0.0012(7) C16 0.0127(9) 0.0111(8) 0.0153(9) -0.0008(7) 0.0004(7) -0.0006(7) C18 0.0176(10) 0.0148(9) 0.0195(9) -0.0007(8) 0.0002(8) -0.0028(8) C19 0.0115(9) 0.0140(9) 0.0178(9) 0.0004(8) 0.0013(7) 0.0008(8) C29 0.0227(12) 0.0211(10) 0.0221(10) -0.0017(8) -0.0040(9) -0.0066(9) C30 0.0117(9) 0.0177(9) 0.0163(9) 0.0012(7) 0.0010(7) 0.0009(8) O1 0.0189(7) 0.0165(7) 0.0222(7) 0.0062(6) -0.0024(6) -0.0001(6) O2 0.0143(7) 0.0229(7) 0.0110(6) 0.0041(5) -0.0025(5) -0.0023(6) O3 0.0110(7) 0.0198(7) 0.0199(7) -0.0016(6) -0.0058(5) -0.0007(6) O4 0.0106(7) 0.0160(6) 0.0147(6) -0.0024(5) 0.0013(5) 0.0003(6) O5 0.0121(7) 0.0259(8) 0.0188(7) -0.0045(6) 0.0016(6) 0.0026(6) O6 0.0113(7) 0.0130(6) 0.0141(6) -0.0017(5) -0.0012(5) 0.0013(5) O7 0.0145(7) 0.0202(7) 0.0096(6) 0.0011(5) -0.0003(5) 0.0002(6) O8 0.0153(7) 0.0171(7) 0.0119(6) 0.0016(5) 0.0022(5) -0.0021(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 C10 109.56(15) . . ? O2 C1 C2 109.62(15) . . ? O2 C1 C10 110.28(15) . . ? C3 C2 C1 116.42(16) . . ? O1 C2 C1 121.31(18) . . ? O1 C2 C3 122.20(18) . . ? C2 C3 C4 109.46(17) . . ? C3 C4 C5 108.55(16) . . ? C29 C4 C3 109.75(17) . . ? C29 C4 C5 114.24(17) . . ? C4 C5 C10 112.50(15) . . ? C6 C5 C4 111.61(15) . . ? C6 C5 C10 112.35(16) . . ? C7 C6 C5 115.52(15) . . ? C6 C7 C8 115.71(15) . . ? O6 C7 C6 109.33(15) . . ? O6 C7 C8 103.95(14) . . ? O7 C7 C6 109.23(15) . . ? O7 C7 C8 108.84(15) . . ? O7 C7 O6 109.58(14) . . ? C7 C8 C9 104.89(15) . . ? C7 C8 C14 99.21(15) . . ? C7 C8 C30 113.51(15) . . ? C14 C8 C9 108.82(15) . . ? C30 C8 C9 117.40(15) . . ? C30 C8 C14 111.32(16) . . ? C10 C9 C8 114.40(14) . . ? C11 C9 C8 111.95(16) . . ? C11 C9 C10 119.67(15) . . ? C1 C10 C5 106.20(15) . . ? C1 C10 C9 110.68(14) . . ? C5 C10 C9 104.70(14) . . ? C19 C10 C1 107.00(15) . . ? C19 C10 C5 113.83(15) . . ? C19 C10 C9 114.19(15) . . ? C9 C11 C12 108.67(15) . . ? O3 C11 C9 110.12(16) . . ? O3 C11 C12 110.59(16) . . ? C13 C12 C11 112.34(16) . . ? O4 C12 C11 109.39(15) . . ? O4 C12 C13 110.56(15) . . ? C12 C13 C14 107.58(16) . . ? C12 C13 C18 111.86(16) . . ? C14 C13 C18 113.41(16) . . ? C13 C14 C8 113.99(16) . . ? C13 C14 C15 113.18(16) . . ? C15 C14 C8 101.04(15) . . ? O8 C14 C8 112.48(15) . . ? O8 C14 C13 107.08(15) . . ? O8 C14 C15 109.04(16) . . ? C14 C15 C16 114.57(16) . . ? O6 C15 C14 106.69(15) . . ? O6 C15 C16 109.48(15) . . ? O4 C16 C15 121.02(16) . . ? O5 C16 C15 119.74(17) . . ? O5 C16 O4 119.19(17) . . ? C16 O4 C12 121.84(15) . . ? C15 O6 C7 108.76(14) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.530(3) . ? C1 C10 1.557(2) . ? C1 O2 1.411(2) . ? C2 C3 1.498(3) . ? C2 O1 1.215(2) . ? C3 C4 1.542(3) . ? C4 C5 1.543(3) . ? C4 C29 1.526(3) . ? C5 C6 1.531(3) . ? C5 C10 1.564(3) . ? C6 C7 1.519(3) . ? C7 C8 1.526(3) . ? C7 O6 1.447(2) . ? C7 O7 1.423(2) . ? C8 C9 1.577(2) . ? C8 C14 1.563(3) . ? C8 C30 1.539(3) . ? C9 C10 1.565(3) . ? C9 C11 1.529(2) . ? C10 C19 1.541(3) . ? C11 C12 1.539(3) . ? C11 O3 1.418(2) . ? C12 C13 1.513(3) . ? C12 O4 1.472(2) . ? C13 C14 1.514(3) . ? C13 C18 1.531(3) . ? C14 C15 1.531(3) . ? C14 O8 1.429(2) . ? C15 C16 1.534(3) . ? C15 O6 1.445(2) . ? C16 O4 1.341(2) . ? C16 O5 1.204(3) . ?