#------------------------------------------------------------------------------ #$Date: 2020-04-20 23:36:21 +0300 (Mon, 20 Apr 2020) $ #$Revision: 250945 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/78/1557823.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557823 loop_ _publ_author_name 'Yang, Wei-Qun' 'Shao, Xue-Hua' 'Deng, Fang' 'Hu, Li-Jun' 'Xiong, Yu' 'Huang, Xiao-Jun' 'Fan, Chun-Lin' 'Jiang, Ren-Wang' 'Ye, Wen-Cai' 'Wang, Ying' _publ_section_title ; Unprecedented Quassinoids from Eurycoma longifolia: Biogenetic Evidence and Antifeedant Effects ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.0c00244 _journal_year 2020 _chemical_absolute_configuration ad _chemical_formula_moiety 'C28 H36 O9, C H Cl3' _chemical_formula_sum 'C29 H37 Cl3 O9' _chemical_formula_weight 635.93 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2020-01-12 _audit_creation_method ; Olex2 1.3 (compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.2039(2) _cell_length_b 13.7078(5) _cell_length_c 24.7447(7) _cell_measurement_reflns_used 7368 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 73.1860 _cell_measurement_theta_min 3.5470 _cell_volume 3461.12(17) _computing_cell_refinement 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _diffrn_ambient_temperature 100.00(10) _diffrn_detector_area_resol_mean 5.2684 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 23.00 69.00 1.00 3.00 -- 40.98 -99.00 -60.00 46 2 \w 34.00 92.00 1.00 3.00 -- 40.98-132.00 -85.00 58 3 \w 43.00 134.00 1.00 10.00 -- 106.95 -61.00 30.00 91 4 \w 75.00 135.00 1.00 10.00 -- 106.95 -30.00 60.00 60 5 \w 106.00 145.00 1.00 10.00 -- 106.95 45.00 0.00 39 6 \w 139.00 164.00 1.00 10.00 -- 106.95 125.00 120.00 25 7 \w 108.00 174.00 1.00 10.00 -- 106.95 125.00 60.00 66 8 \w 80.00 178.00 1.00 10.00 -- 106.95 30.00 120.00 98 9 \w 80.00 149.00 1.00 10.00 -- 106.95 30.00 60.00 69 10 \w 68.00 109.00 1.00 10.00 -- 106.95 -94.00 -30.00 41 11 \w 93.00 120.00 1.00 10.00 -- 106.95-125.00 -90.00 27 12 \w 90.00 119.00 1.00 10.00 -- 106.95-125.00-180.00 29 13 \w 70.00 129.00 1.00 10.00 -- 106.95 -45.00-120.00 59 14 \w 33.00 105.00 1.00 10.00 -- 106.95 -94.00 60.00 72 15 \w 48.00 139.00 1.00 10.00 -- 106.95 -77.00 150.00 91 16 \w 43.00 90.00 1.00 3.00 -- 40.98-137.00 97.00 47 17 \w 45.00 119.00 1.00 10.00 -- 106.95 -30.00 150.00 74 18 \w 20.00 115.00 1.00 3.00 -- 40.98 38.00-180.00 95 19 \w -127.00 40.00 1.00 3.00 -- -40.98 0.00 0.00 167 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0917 _diffrn_reflns_av_unetI/netI 0.0702 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 25004 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.684 _diffrn_reflns_theta_min 4.688 _exptl_absorpt_coefficient_mu 2.784 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.31461 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43f (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.220 _exptl_crystal_description block _exptl_crystal_F_000 1336 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.11 _refine_diff_density_max 1.145 _refine_diff_density_min -0.446 _refine_diff_density_rms 0.119 _refine_ls_abs_structure_details ; Flack x determined using 2172 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.05(2) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.062 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 377 _refine_ls_number_reflns 6895 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.062 _refine_ls_R_factor_all 0.0935 _refine_ls_R_factor_gt 0.0838 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1511P)^2^+2.9858P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2269 _refine_ls_wR_factor_ref 0.2396 _reflns_Friedel_coverage 0.770 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.978 _reflns_number_gt 6000 _reflns_number_total 6895 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file np0c00244_si_004.cif _cod_data_source_block exp_1494 _cod_database_code 1557823 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.749 _shelx_estimated_absorpt_t_min 0.714 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Ternary CH refined with riding coordinates: C5(H5), C7(H7), C9(H9), C11(H11), C17(H17), C20(H20), C2S(H2S) 2.b Secondary CH2 refined with riding coordinates: C6(H6A,H6B), C12(H12A,H12B), C21(H21A,H21B), C22(H22A,H22B), C28(H28A,H28B) 2.c Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C15(H15) 2.d Idealised Me refined as rotating group: C18(H18A,H18B,H18C), C19(H19A,H19B,H19C), C29(H29A,H29B,H29C), C30(H30A,H30B, H30C), C32(H32A,H32B,H32C) 2.e Idealised tetrahedral OH refined as rotating group: O2(H2A), O7(H7A) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL exp_1494_a.res in P2(1)2(1)2(1) exp_1494.res created by SHELXL-2018/3 at 11:02:54 on 12-Jan-2020 REM Old TITL exp_1494 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.176, Rweak 0.028, Alpha 0.001 REM 0.430 for 27 systematic absences, Orientation as input REM Flack x = 0.038 ( 0.017 ) from 2368 Parsons' quotients REM Formula found by SHELXT: C31 N O9 Cl5 CELL 1.54184 10.2039 13.7078 24.7447 90 90 90 ZERR 4 0.0002 0.0005 0.0007 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Cl O UNIT 116 148 12 36 L.S. 20 PLAN 12 SIZE 0.11 0.12 0.13 CONF BOND list 4 fmap 2 53 acta MORE -1 BOND $H ABIN OMIT 2 0 7 OMIT 3 0 8 OMIT 0 0 2 OMIT 0 1 1 REM REM REM WGHT 0.151100 2.985800 FVAR 0.40706 C1 1 0.166029 0.554161 0.780033 11.00000 0.02967 0.04430 = 0.01311 -0.00208 -0.00843 0.00177 C2 1 0.063736 0.569234 0.821692 11.00000 0.03592 0.04564 = 0.02593 -0.01053 0.00094 0.00334 AFIX 43 H2 2 0.076723 0.618593 0.846914 11.00000 -1.20000 AFIX 0 C3 1 -0.044431 0.517197 0.825292 11.00000 0.03616 0.04513 = 0.01823 -0.00738 0.00228 -0.00445 AFIX 43 H3 2 -0.102367 0.531088 0.853266 11.00000 -1.20000 AFIX 0 C4 1 -0.079771 0.435883 0.786360 11.00000 0.03414 0.04489 = 0.02486 -0.00894 0.00516 -0.00549 C5 1 0.016853 0.431221 0.737781 11.00000 0.03142 0.03680 = 0.01551 0.00163 0.00234 -0.00342 AFIX 13 H5 2 -0.011985 0.482342 0.712779 11.00000 -1.20000 AFIX 0 C6 1 0.004318 0.336777 0.706875 11.00000 0.02377 0.03905 = 0.01651 -0.00187 0.00356 -0.00342 AFIX 23 H6A 2 -0.087609 0.324618 0.699506 11.00000 -1.20000 H6B 2 0.036399 0.283793 0.729239 11.00000 -1.20000 AFIX 0 C7 1 0.079537 0.337003 0.653623 11.00000 0.02628 0.03315 = 0.01579 -0.00125 0.00010 0.00018 AFIX 13 H7 2 0.077977 0.270666 0.638871 11.00000 -1.20000 AFIX 0 C8 1 0.221635 0.368092 0.659525 11.00000 0.02918 0.03130 = 0.01528 -0.00783 -0.00244 0.00108 C9 1 0.233988 0.462419 0.695000 11.00000 0.02940 0.02608 = 0.01606 -0.00375 0.00132 0.00646 AFIX 13 H9 2 0.184484 0.511995 0.675061 11.00000 -1.20000 AFIX 0 C10 1 0.162466 0.455158 0.750943 11.00000 0.03075 0.03363 = 0.01534 0.00139 -0.00056 0.00249 C11 1 0.376528 0.501184 0.695297 11.00000 0.02910 0.03243 = 0.01486 -0.00519 -0.00315 0.00346 AFIX 13 H11 2 0.409542 0.501020 0.732488 11.00000 -1.20000 AFIX 0 C12 1 0.473866 0.446723 0.658981 11.00000 0.02691 0.03767 = 0.01302 -0.00463 -0.00440 0.00094 AFIX 23 H12A 2 0.498261 0.386362 0.676795 11.00000 -1.20000 H12B 2 0.552518 0.486013 0.655664 11.00000 -1.20000 AFIX 0 C13 1 0.423555 0.421756 0.600881 11.00000 0.02560 0.03961 = 0.01971 -0.00341 0.00014 -0.00522 C14 1 0.277850 0.397250 0.604543 11.00000 0.03721 0.02792 = 0.01348 -0.00507 -0.00441 -0.00556 C15 1 0.195570 0.408434 0.562601 11.00000 0.03304 0.04016 = 0.01176 -0.00100 -0.00026 0.00151 AFIX 43 H15 2 0.230922 0.413436 0.528070 11.00000 -1.20000 AFIX 0 C16 1 0.055090 0.413057 0.568528 11.00000 0.03372 0.03901 = 0.01264 -0.00507 -0.00485 -0.00063 C17 1 0.500635 0.332294 0.581010 11.00000 0.02972 0.03969 = 0.01279 0.00337 -0.00321 0.00182 AFIX 13 H17 2 0.480868 0.276792 0.604605 11.00000 -1.20000 AFIX 0 C18 1 0.445754 0.509963 0.563412 11.00000 0.03263 0.04062 = 0.01694 -0.00142 0.00253 0.00304 AFIX 137 H18A 2 0.537452 0.525520 0.562404 11.00000 -1.50000 H18B 2 0.397590 0.565017 0.576847 11.00000 -1.50000 H18C 2 0.416055 0.494321 0.527634 11.00000 -1.50000 AFIX 0 C19 1 0.227034 0.383685 0.790681 11.00000 0.03459 0.04851 = 0.01067 0.00533 -0.00068 0.00121 AFIX 137 H19A 2 0.320555 0.386976 0.786865 11.00000 -1.50000 H19B 2 0.197784 0.318571 0.783030 11.00000 -1.50000 H19C 2 0.203104 0.400853 0.826976 11.00000 -1.50000 AFIX 0 C20 1 0.651360 0.345116 0.577737 11.00000 0.02374 0.03573 = 0.01312 -0.00285 -0.00183 0.00117 AFIX 13 H20 2 0.676904 0.407689 0.593736 11.00000 -1.20000 AFIX 0 C21 1 0.720922 0.261738 0.606749 11.00000 0.02388 0.03351 = 0.02805 0.00088 -0.00268 -0.00060 AFIX 23 H21A 2 0.693125 0.199273 0.592331 11.00000 -1.20000 H21B 2 0.815156 0.267372 0.602638 11.00000 -1.20000 AFIX 0 C22 1 0.681405 0.345250 0.516642 11.00000 0.02994 0.04061 = 0.02079 0.00326 -0.00080 0.00176 AFIX 23 H22A 2 0.713674 0.408576 0.505287 11.00000 -1.20000 H22B 2 0.746766 0.296304 0.507979 11.00000 -1.20000 AFIX 0 C23 1 0.554507 0.322408 0.489547 11.00000 0.03091 0.04067 = 0.02146 -0.00186 0.00265 0.01059 C28 1 -0.218741 0.461657 0.764512 11.00000 0.03233 0.05205 = 0.03264 -0.01456 0.00214 -0.00376 AFIX 23 H28A 2 -0.246189 0.413211 0.738277 11.00000 -1.20000 H28B 2 -0.281434 0.461767 0.793979 11.00000 -1.20000 AFIX 0 C29 1 -0.091453 0.342332 0.818153 11.00000 0.04367 0.05578 = 0.01712 -0.00158 0.00414 0.00352 AFIX 137 H29A 2 -0.133732 0.293665 0.796374 11.00000 -1.50000 H29B 2 -0.142409 0.353808 0.850140 11.00000 -1.50000 H29C 2 -0.005648 0.320013 0.828169 11.00000 -1.50000 AFIX 0 C30 1 0.289966 0.274155 0.679806 11.00000 0.03143 0.03603 = 0.01713 -0.00176 0.00548 0.00017 AFIX 137 H30A 2 0.235277 0.242523 0.706064 11.00000 -1.50000 H30B 2 0.372441 0.290763 0.696049 11.00000 -1.50000 H30C 2 0.304557 0.230922 0.649884 11.00000 -1.50000 AFIX 0 C31 1 0.457334 0.663553 0.696777 11.00000 0.02468 0.03636 = 0.03182 -0.00814 0.00159 -0.00040 C32 1 0.444235 0.762561 0.672648 11.00000 0.03445 0.04093 = 0.06567 0.00879 -0.00306 -0.00261 AFIX 137 H32A 2 0.362558 0.767015 0.653552 11.00000 -1.50000 H32B 2 0.515332 0.773819 0.648016 11.00000 -1.50000 H32C 2 0.446368 0.810694 0.700815 11.00000 -1.50000 AFIX 0 O1 4 0.249147 0.613707 0.772737 11.00000 0.03472 0.04144 = 0.02591 -0.00874 0.00251 -0.00313 O2 4 -0.214760 0.554573 0.740084 11.00000 0.02887 0.05871 = 0.04542 0.00215 0.00843 0.00600 AFIX 147 H2A 2 -0.257747 0.593164 0.758165 11.00000 -1.50000 AFIX 0 O3 4 0.002541 0.399798 0.617852 11.00000 0.02492 0.04200 = 0.01698 0.00030 -0.00265 0.00324 O4 4 -0.019930 0.438868 0.532401 11.00000 0.03238 0.05296 = 0.01937 0.00225 -0.00316 0.00086 O5 4 0.371694 0.600644 0.675829 11.00000 0.02645 0.03939 = 0.02096 -0.00240 -0.00317 -0.00123 O6 4 0.539202 0.641176 0.729528 11.00000 0.03621 0.04738 = 0.03252 -0.00659 -0.00878 0.00128 O7 4 0.684234 0.270622 0.662602 11.00000 0.03728 0.03953 = 0.01906 0.00256 -0.00078 0.00157 AFIX 147 H7A 2 0.698094 0.218826 0.678164 11.00000 -1.50000 AFIX 0 O8 4 0.457811 0.309237 0.526304 11.00000 0.03148 0.04567 = 0.01442 -0.00988 -0.00030 -0.00142 O9 4 0.531212 0.317624 0.441980 11.00000 0.04044 0.06213 = 0.01510 -0.01018 0.00099 0.00160 CL4 3 -0.159301 0.554712 0.427203 11.00000 0.04860 0.06290 = 0.02447 0.00599 0.00212 0.00872 CL5 3 0.123323 0.568134 0.429560 11.00000 0.05063 0.08858 = 0.02623 0.00258 -0.00608 -0.02391 CL6 3 -0.003159 0.442714 0.351475 11.00000 0.04562 0.04958 = 0.02308 0.00249 -0.00217 0.00206 C2S 1 -0.010543 0.491687 0.417381 11.00000 0.03572 0.05454 = 0.02134 0.01063 -0.00187 0.00390 AFIX 13 H2S 2 -0.007007 0.437547 0.443205 11.00000 -1.20000 AFIX 0 HKLF 4 REM exp_1494_a.res in P2(1)2(1)2(1) REM wR2 = 0.2396, GooF = S = 1.062, Restrained GooF = 1.062 for all data REM R1 = 0.0838 for 6000 Fo > 4sig(Fo) and 0.0935 for all 6895 data REM 377 parameters refined using 0 restraints END WGHT 0.1562 3.7581 REM Highest difference peak 1.145, deepest hole -0.446, 1-sigma level 0.119 Q1 1 -0.1057 0.1617 0.9202 11.00000 0.05 1.14 Q2 1 -0.1512 0.6336 0.6227 11.00000 0.05 1.02 Q3 1 0.1035 0.2781 0.9610 11.00000 0.05 0.77 Q4 1 0.0538 0.5173 0.4234 11.00000 0.05 0.65 Q5 1 -0.0509 0.5523 0.4246 11.00000 0.05 0.63 Q6 1 -0.1247 0.6198 0.4247 11.00000 0.05 0.61 Q7 1 -0.1262 0.4881 0.4349 11.00000 0.05 0.60 Q8 1 0.1891 0.6202 0.4338 11.00000 0.05 0.49 Q9 1 -0.0040 0.3737 0.3611 11.00000 0.05 0.47 Q10 1 -0.0082 0.3621 0.3488 11.00000 0.05 0.47 Q11 1 0.0981 0.4576 0.3432 11.00000 0.05 0.44 Q12 1 0.0460 0.4979 0.3572 11.00000 0.05 0.44 ; _shelx_res_checksum 43189 _shelx_hkl_file ; 0 0 -2 450.27 17.29 0 0 -3 1.99 2.05 0 0 -3 2.30 2.41 0 0 -4 291.26 15.92 0 0 -4 308.14 20.38 0 0 -5 0.37 3.44 0 0 -5 -0.94 2.92 0 0 -6 2272.27 69.53 0 0 -6 2140.91 54.39 0 0 -7 -1.63 3.74 0 0 -7 0.88 4.75 0 0 -8 8805.45 158.05 0 0 -8 8186.91 125.60 0 0 -9 7.98 6.94 0 0 -9 1.13 4.57 0 0 -10 1535.86 75.80 0 0 -10 1556.99 61.71 0 0 -11 6.55 7.32 0 0 -11 3.10 6.30 0 0 -12 1850.37 92.22 0 0 -12 1800.79 74.28 0 0 -13 -7.10 10.02 0 0 -13 4.49 8.09 0 0 -14 801.65 55.41 0 0 -14 799.05 68.03 0 0 -15 -11.60 11.77 0 0 -15 -1.07 7.28 0 0 -16 46.11 13.33 0 0 -16 44.00 14.39 0 0 -17 1.91 4.49 0 0 -17 0.53 4.24 0 0 -18 17.87 12.24 0 0 -18 -1.19 6.51 0 0 -18 18.84 7.19 0 0 -19 2.95 4.78 0 0 -19 -6.43 8.32 0 0 -19 -4.28 13.60 0 0 -20 874.46 70.72 0 0 -20 979.45 93.58 0 0 -21 -6.82 13.60 0 0 -21 4.38 4.79 0 0 -22 1266.42 59.18 0 0 -23 -0.74 2.98 0 0 -24 164.68 21.26 0 0 -25 2.75 5.18 0 0 -26 345.47 29.14 0 0 -27 -0.02 4.05 0 0 -28 324.20 25.13 0 0 -29 1.78 2.09 0 0 -29 0.77 2.27 0 0 -30 11.16 4.37 0 -1 0 2.21 1.65 0 -1 1 581.76 21.33 0 -1 -1 534.06 17.26 0 -1 -2 1487.58 33.93 0 -1 2 1523.49 39.60 0 -1 3 321.72 20.66 0 -1 -3 320.26 18.13 0 -1 -4 248.20 18.29 0 -1 4 262.02 20.55 0 1 -4 232.51 14.63 0 1 -5 25.22 5.93 0 -1 -5 39.20 8.68 0 1 -6 144.31 14.36 0 -1 -6 170.95 18.22 0 -1 -7 2405.97 73.08 0 1 -7 2215.10 59.90 0 -1 -8 92.15 15.11 0 1 -8 72.61 15.52 0 1 -8 86.15 12.49 0 1 -9 173.06 20.54 0 1 -9 163.08 26.03 0 -1 -9 195.34 20.22 0 -1 -9 179.66 22.66 0 1 -10 1094.34 70.24 0 -1 -10 1097.14 59.63 0 -1 -10 1069.93 50.82 0 1 -10 1118.95 53.33 0 -1 -11 294.06 31.90 0 1 -11 290.99 29.76 0 1 -11 288.87 37.80 0 -1 -11 298.30 28.29 0 -1 -12 2620.39 100.47 0 1 -12 2605.49 92.24 0 -1 -12 2509.77 86.92 0 1 -12 2722.70 119.21 0 -1 -13 264.63 33.60 0 -1 -13 258.82 28.93 0 1 -13 283.66 40.15 0 1 -13 254.77 31.11 0 1 -14 109.11 27.54 0 -1 -14 113.97 19.61 0 -1 -14 121.54 23.08 0 1 -14 133.79 23.06 0 -1 -15 429.71 40.42 0 1 -15 500.99 46.44 0 -1 -15 453.19 49.29 0 1 -15 490.06 57.80 0 1 -16 601.36 54.18 0 1 -16 620.44 68.85 0 -1 -16 603.79 59.10 0 -1 -16 600.07 50.78 0 -1 -17 55.02 18.26 0 -1 -17 68.97 18.35 0 1 -17 59.78 17.73 0 1 -17 65.54 26.86 0 1 -18 6.86 8.68 0 1 -18 14.01 10.37 0 1 -18 10.62 5.73 0 -1 -18 21.59 11.81 0 -1 -18 10.51 4.67 0 -1 -18 9.48 6.66 0 1 -19 491.59 54.24 0 -1 -19 661.13 39.97 0 1 -19 510.84 68.59 0 1 -19 615.97 42.27 0 -1 -19 539.86 64.70 0 -1 -19 495.39 50.39 0 1 -20 3.33 5.68 0 -1 -20 26.48 16.22 0 1 -20 17.61 8.25 0 1 -20 3.62 4.49 0 -1 -20 14.55 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91.00 15.40 6 5 21 76.63 11.90 6 -5 -22 29.32 9.05 6 5 22 24.03 6.37 6 -5 -23 9.18 3.89 6 5 23 6.07 3.03 6 -5 -24 13.47 5.95 6 5 24 5.77 2.58 6 -5 -25 -3.63 2.65 6 -6 24 13.66 5.18 6 6 -24 16.05 5.02 6 -6 24 17.91 5.06 6 6 -23 137.32 14.72 6 6 -23 100.51 12.31 6 -6 23 161.86 20.05 6 -6 22 12.15 5.94 6 6 -22 16.46 6.29 6 -6 22 9.78 4.30 6 -6 21 13.70 8.12 6 6 -21 18.15 6.88 6 -6 21 21.21 6.10 -6 -6 -21 9.84 3.35 6 -6 20 38.39 11.79 6 6 -20 32.55 9.99 6 -6 20 46.23 9.73 -6 -6 -20 26.42 6.95 6 -6 19 37.15 12.05 6 6 -19 28.83 9.61 6 -6 19 35.42 8.86 -6 -6 -19 25.97 6.91 6 -6 18 3.08 4.07 6 6 -18 -0.73 4.45 6 -6 18 0.85 2.35 -6 -6 -18 2.01 2.44 6 -6 17 91.39 19.75 6 6 -17 102.17 19.01 6 -6 17 99.79 14.78 -6 -6 -17 78.51 12.96 -6 -6 -16 34.85 9.89 6 -6 16 37.18 12.89 6 6 -16 38.10 11.89 6 -6 16 39.94 9.20 -6 -6 -15 34.64 10.01 6 -6 15 34.59 12.03 6 6 -15 27.60 8.62 6 -6 15 33.28 9.22 -6 -6 -14 5.27 5.23 6 -6 14 3.70 4.65 6 6 -14 3.03 4.95 6 -6 14 8.25 5.30 6 -6 13 51.88 17.90 6 6 -13 51.08 13.62 6 -6 13 22.00 6.63 6 -6 12 17.83 7.31 6 6 -12 42.23 12.59 6 -6 12 28.58 7.70 6 -6 11 58.02 14.80 6 6 -11 93.28 17.53 6 -6 11 65.15 11.45 6 -6 10 261.12 22.16 6 -6 10 261.38 30.71 6 -6 9 10.83 5.75 6 6 -9 15.79 7.52 6 -6 9 9.77 4.37 6 6 -8 149.73 21.35 6 -6 8 101.32 28.73 6 6 -8 149.33 38.94 6 -6 8 100.86 18.53 6 6 -7 47.50 12.05 6 -6 7 39.41 17.27 6 6 -7 45.51 22.47 6 6 -6 56.79 12.72 6 6 -6 95.44 16.33 6 -6 6 83.24 25.80 6 6 -6 100.00 31.84 6 -6 6 109.48 17.44 6 6 -5 24.03 8.86 6 6 -5 39.25 10.04 6 -6 5 44.94 18.71 6 6 -5 55.33 25.70 6 -6 5 44.17 10.76 6 6 -4 51.00 11.81 6 -6 4 96.63 28.95 6 6 -4 101.30 30.52 6 -6 4 119.35 18.40 6 6 -3 33.28 9.53 6 -6 3 44.29 19.22 6 6 -3 42.65 10.42 6 6 -3 49.65 22.35 6 -6 3 54.51 11.45 6 6 -2 1.84 1.85 6 -6 2 -0.20 7.30 6 6 -2 -1.09 4.52 6 6 -2 8.88 7.63 6 -6 2 4.74 4.64 6 6 -1 -0.60 6.56 6 6 -1 4.53 3.86 6 -6 1 6.68 6.90 6 6 -1 6.05 4.25 6 -6 1 5.61 3.93 6 6 0 20.04 8.03 6 -6 0 40.54 18.73 6 6 0 34.81 9.24 6 6 0 29.25 8.67 6 6 0 23.16 14.17 6 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140.92 16.64 6 6 8 136.16 22.28 6 6 9 20.58 17.06 6 6 9 11.55 7.67 6 -6 -9 2.17 3.55 6 -6 -9 6.20 4.78 6 6 9 1.69 3.17 6 6 9 14.47 6.73 6 -6 -9 8.04 6.66 6 -6 -9 13.14 8.65 6 -6 -9 12.45 5.92 6 -6 -10 294.14 26.80 6 6 10 346.71 29.57 6 -6 -10 230.64 24.65 6 -6 -10 195.35 40.32 6 -6 -10 327.52 24.79 6 6 10 392.85 37.37 6 -6 -11 67.87 13.19 6 6 11 81.51 14.58 6 -6 -11 62.07 12.76 6 -6 -11 68.66 11.19 6 6 11 89.03 18.39 6 6 12 40.66 12.21 6 6 12 57.94 12.81 6 -6 -12 44.30 10.60 6 -6 -12 32.86 8.92 6 -6 -12 48.25 9.50 6 6 13 49.87 13.60 6 6 13 26.80 7.22 6 -6 -13 31.91 9.75 6 -6 -13 30.71 9.07 6 -6 -13 37.99 8.23 6 6 14 13.65 8.16 6 6 14 8.31 6.06 6 -6 -14 2.66 3.08 6 -6 -14 6.77 5.03 6 -6 -14 7.88 4.99 6 6 15 45.38 12.58 6 6 15 63.05 12.79 6 -6 -15 46.31 10.80 6 -6 -15 39.65 9.74 6 -6 -15 50.81 9.73 6 6 16 47.03 12.19 6 -6 -16 27.92 8.50 6 -6 -16 31.79 9.07 6 -6 -16 27.63 6.47 6 -6 -17 113.41 16.87 6 6 17 112.61 16.13 6 -6 -17 76.16 13.19 6 -6 -17 107.03 12.98 6 6 18 0.37 4.12 6 -6 -18 2.85 3.87 6 -6 -18 5.02 3.10 6 -6 -18 4.93 3.89 6 -6 -19 46.66 10.39 6 -6 -19 36.16 8.60 6 -6 -19 60.09 10.25 6 6 19 38.89 8.88 6 -6 -20 42.83 10.32 6 -6 -20 25.80 7.15 6 -6 -20 37.71 7.40 6 6 20 31.36 7.66 6 -6 -21 8.44 3.87 6 -6 -21 9.09 3.87 6 6 21 9.69 4.23 6 -6 -22 20.72 6.67 6 6 22 23.68 6.14 6 -6 -23 186.89 17.95 6 6 23 136.01 12.83 6 -6 -24 18.16 4.94 6 -7 23 4.35 2.79 6 7 -23 2.17 1.94 6 7 -23 3.62 2.11 6 -7 23 5.35 3.42 6 -7 22 40.22 9.37 6 7 -22 45.58 8.98 -6 -7 -22 26.66 5.29 6 -7 22 41.68 9.25 6 -7 21 33.02 9.65 6 7 -21 46.13 10.34 -6 -7 -21 24.64 5.76 6 -7 20 -1.86 5.90 6 7 -20 -9.56 5.52 6 -7 20 2.29 3.67 -6 -7 -20 4.86 2.77 6 -7 19 76.30 16.22 6 -7 19 72.23 11.83 6 7 -19 75.49 14.52 -6 -7 -19 38.36 8.62 6 -7 18 1.21 3.06 6 7 -18 12.00 7.40 6 -7 18 2.53 2.59 -6 -7 -18 7.91 3.95 6 -7 17 60.24 15.22 6 7 -17 61.08 14.23 6 -7 17 55.20 10.70 -6 -7 -17 51.53 10.95 6 7 -16 232.03 26.74 6 -7 16 187.89 19.83 6 -7 16 181.94 26.51 -6 -7 -16 159.39 19.24 -6 -7 -15 22.51 7.40 6 -7 15 25.74 9.11 6 7 -15 27.15 9.86 6 -7 15 22.95 6.92 -6 -7 -14 1.49 2.88 6 -7 14 0.91 5.05 6 7 -14 3.83 7.39 6 -7 14 6.23 2.16 6 -7 13 36.75 11.39 6 7 -13 60.33 14.16 6 -7 13 36.44 8.89 6 -7 12 8.58 5.41 6 7 -12 9.49 6.52 6 -7 12 10.03 4.35 6 7 -11 291.64 30.83 6 -7 11 211.00 20.74 6 -7 11 249.48 30.16 6 -7 10 23.22 8.94 6 7 -10 45.35 13.03 6 -7 10 22.97 7.02 6 7 -9 264.21 28.39 6 -7 9 159.33 17.86 6 -7 9 222.18 28.03 6 -7 9 231.15 24.93 6 -7 8 39.57 11.76 6 7 -8 60.47 13.70 6 -7 8 31.95 14.97 6 7 -8 51.24 23.32 6 -7 8 54.71 12.19 6 -7 7 1.18 2.52 6 7 -7 3.44 3.34 6 -7 7 12.63 11.55 6 7 -7 5.61 10.82 6 -7 7 12.23 4.83 6 7 -6 42.03 11.26 6 -7 6 36.99 16.68 6 7 -6 25.62 17.48 6 -7 6 32.47 9.06 6 7 -5 5.25 3.81 6 -7 5 -8.13 7.82 6 7 -5 -0.35 3.45 6 7 -5 -2.27 5.11 6 -7 5 5.83 5.09 6 7 -4 12.64 6.97 6 -7 4 -3.89 9.87 6 7 -4 -2.15 3.55 6 7 -4 4.75 8.94 6 -7 4 -0.71 4.23 6 -7 3 114.54 30.08 6 7 -3 107.56 15.66 6 7 -3 124.08 34.56 6 -7 3 133.46 18.49 6 -7 2 45.80 20.92 6 7 -2 37.25 8.95 6 7 -2 30.55 16.28 6 -7 2 51.12 11.07 6 -7 1 31.01 16.34 6 7 -1 29.05 8.05 6 7 -1 19.97 14.53 6 -7 1 32.51 8.80 6 7 0 28.90 8.89 6 -7 0 64.13 23.44 6 7 0 50.46 10.39 6 7 0 52.39 13.37 6 7 0 29.77 15.96 6 -7 0 42.20 9.68 6 7 1 18.04 7.36 6 -7 -1 37.01 18.53 6 7 1 28.42 7.81 6 7 1 29.22 9.54 6 -7 -1 13.45 7.39 6 7 1 15.64 9.85 6 -7 -1 30.56 8.56 6 7 2 46.16 11.56 6 -7 -2 55.27 21.76 6 7 2 57.04 11.53 6 7 2 57.69 14.05 6 -7 -2 40.58 11.48 6 7 2 41.51 20.01 6 -7 -2 65.48 12.18 6 7 3 74.89 14.63 6 -7 -3 123.44 32.76 6 7 3 119.19 15.85 6 -7 -3 85.16 15.74 6 7 3 85.47 27.20 6 -7 -3 125.19 16.52 6 7 4 -1.90 3.17 6 -7 -4 0.64 5.87 6 7 4 2.45 2.54 6 -7 -4 -0.64 3.74 6 7 4 1.63 7.66 6 -7 -4 0.06 2.87 6 7 5 8.87 6.12 6 -7 -5 9.68 8.19 6 7 5 5.86 4.48 6 -7 -5 1.59 3.38 6 7 5 -0.94 6.34 6 -7 -5 5.51 4.06 6 7 6 36.42 11.92 6 -7 -6 38.70 16.24 6 -7 -6 38.61 17.11 6 7 6 47.32 10.73 6 -7 -6 39.56 10.71 6 7 6 24.73 14.24 6 -7 -6 47.07 10.27 6 7 7 6.79 5.59 6 -7 -7 -2.85 6.52 6 7 7 10.00 5.77 6 -7 -7 4.96 8.84 6 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-18 13.79 5.38 6 -7 -18 9.26 9.77 6 -7 -18 1.99 1.90 6 -7 -19 83.99 13.31 6 7 19 86.08 12.58 6 -7 -19 57.76 10.15 6 -7 -19 80.06 11.30 6 -7 -20 -1.70 3.34 6 -7 -20 1.20 2.23 6 7 20 -1.46 1.90 6 -7 -21 40.73 8.59 6 -7 -21 27.78 6.48 6 7 21 41.48 7.78 6 -7 -22 58.45 9.63 6 7 22 46.42 7.48 6 -7 -23 4.81 2.44 6 8 -22 18.18 5.53 6 -8 22 12.52 4.25 6 -8 22 24.93 7.18 6 8 -21 7.97 3.57 6 -8 21 16.43 5.14 6 -8 21 13.80 6.16 6 -8 20 6.64 4.42 6 8 -20 6.19 5.10 6 -8 20 6.28 3.91 -6 -8 -20 9.89 3.96 6 -8 19 47.34 12.34 6 8 -19 45.77 9.86 6 -8 19 36.70 8.66 -6 -8 -19 34.49 7.46 6 -8 18 3.17 2.90 6 8 -18 5.54 4.78 6 -8 18 6.00 4.91 -6 -8 -18 8.43 4.06 6 8 -17 79.95 15.33 6 -8 17 101.47 18.84 -6 -8 -17 63.17 11.63 6 -8 17 60.43 13.01 -6 -8 -16 45.22 10.21 6 -8 16 44.02 12.32 6 8 -16 48.20 13.25 6 -8 16 55.24 10.70 6 -8 16 25.95 7.92 6 -8 15 74.43 16.07 6 -8 15 86.31 13.22 6 8 -15 93.63 16.94 -6 -8 -15 66.82 13.48 6 -8 15 74.92 14.20 6 8 -14 135.22 20.92 6 -8 14 105.01 14.32 6 -8 14 110.67 19.47 6 -8 14 95.87 16.26 6 -8 13 3.21 4.41 6 8 -13 10.13 7.26 6 -8 13 7.71 4.63 6 -8 13 -0.02 2.99 6 -8 12 75.23 16.16 6 8 -12 89.15 17.22 6 -8 12 56.25 10.03 6 -8 12 73.88 14.14 6 -8 11 16.72 8.45 6 8 -11 10.87 5.06 6 -8 11 13.02 5.40 6 -8 11 20.57 8.90 6 8 -10 153.94 21.57 6 -8 10 123.09 15.22 6 -8 10 117.29 19.62 6 -8 10 118.40 17.51 6 -8 9 61.24 10.89 6 8 -9 86.09 16.09 6 -8 9 74.91 16.25 6 -8 9 66.81 13.05 6 8 -8 24.73 7.46 6 8 -8 18.04 6.09 6 -8 8 31.20 8.73 6 -8 8 33.40 10.20 6 8 -7 22.28 8.10 6 8 -7 11.34 4.34 6 -8 7 16.28 6.63 6 -8 7 13.21 6.70 6 8 -6 22.00 6.85 6 8 -6 18.77 6.38 6 -8 6 12.90 7.24 6 -8 6 20.09 7.35 6 8 -5 269.06 27.52 6 -8 5 137.79 34.17 6 8 -5 213.85 21.53 6 8 -5 158.55 43.39 6 -8 5 251.15 24.81 6 8 -4 31.43 9.34 6 -8 4 10.49 10.01 6 8 -4 27.42 7.94 6 8 -4 19.49 14.18 6 -8 4 36.68 9.77 6 8 -3 156.38 20.55 6 -8 3 91.28 28.39 6 8 -3 137.88 17.77 6 8 -3 120.67 37.54 6 -8 3 180.66 21.00 6 -8 2 18.29 11.56 6 8 -2 12.34 5.23 6 8 -2 6.24 14.52 6 -8 2 17.42 6.83 6 -8 1 42.85 17.83 6 8 -1 73.99 13.33 6 8 -1 51.23 23.14 6 -8 1 86.51 14.40 6 8 0 129.61 20.97 6 -8 0 119.88 32.51 6 8 0 155.05 18.33 6 -8 0 140.23 22.21 6 8 0 88.60 29.07 6 -8 0 180.87 19.99 6 8 1 62.24 14.41 6 -8 -1 74.57 25.66 6 8 1 93.87 14.17 6 -8 -1 68.85 15.26 6 8 1 46.76 22.46 6 -8 -1 105.24 15.30 6 8 2 7.49 4.76 6 -8 -2 8.17 8.54 6 8 2 15.66 6.08 6 -8 -2 14.26 7.95 6 8 2 11.53 11.96 6 -8 -2 16.94 6.19 6 -8 -3 125.91 33.51 6 8 3 147.60 17.79 6 -8 -3 143.61 21.53 6 8 3 89.40 27.66 6 -8 -3 176.38 19.66 6 8 3 116.87 19.73 6 8 4 19.78 7.98 6 -8 -4 19.69 14.51 6 8 4 29.30 7.47 6 -8 -4 27.19 9.40 6 8 4 28.26 19.00 6 -8 -4 36.41 8.94 6 8 5 284.33 25.08 6 -8 -5 288.00 30.01 6 8 5 188.96 43.62 6 -8 -5 214.68 43.88 6 -8 -5 359.14 27.89 6 8 5 256.48 30.20 6 8 6 10.50 4.90 6 8 6 22.83 7.29 6 -8 -6 18.52 6.44 6 -8 -6 26.55 8.63 6 8 7 22.94 10.68 6 8 7 28.61 8.79 6 -8 -7 16.71 6.71 6 -8 -7 19.38 7.15 6 8 8 31.92 11.91 6 -8 -8 29.24 9.78 6 -8 -8 34.18 8.94 6 8 9 83.27 18.93 6 -8 -9 85.42 16.20 6 -8 -9 87.42 13.35 6 8 10 186.27 23.69 6 -8 -10 134.68 20.11 6 -8 -10 167.97 17.69 6 8 10 140.41 24.44 6 8 11 16.80 9.67 6 8 11 16.50 6.64 6 -8 -11 17.81 7.24 6 -8 -11 18.59 6.36 6 8 12 58.71 15.12 6 8 12 62.63 13.60 6 -8 -12 53.21 12.27 6 -8 -12 57.12 10.40 6 8 13 3.58 3.19 6 8 13 2.55 4.59 6 -8 -13 4.19 4.70 6 -8 -13 5.57 4.15 6 8 14 117.22 18.11 6 -8 -14 81.50 14.16 6 -8 -14 98.87 12.95 6 8 14 133.01 21.44 6 -8 -15 70.52 12.40 6 8 15 95.26 16.55 6 -8 -15 52.82 11.23 6 -8 -15 88.91 12.01 6 8 16 41.87 9.84 6 -8 -16 46.11 9.74 6 -8 -16 28.62 8.64 6 -8 -16 42.45 8.27 6 -8 -17 80.79 12.60 6 8 17 73.93 12.94 6 -8 -17 41.11 9.53 6 -8 -17 69.97 9.90 6 8 18 -0.18 2.41 6 -8 -18 4.24 1.73 6 -8 -18 2.55 2.67 6 -8 -18 8.72 3.99 6 -8 -19 35.90 7.58 6 -8 -19 21.00 6.30 6 -8 -19 31.02 5.88 6 8 19 37.05 7.99 6 -8 -20 12.04 3.98 6 -8 -20 6.64 3.57 6 8 20 12.31 4.07 6 -8 -21 18.68 4.98 6 -8 -21 8.12 3.93 6 8 21 15.10 4.25 6 9 -21 1.20 1.63 6 -9 21 9.38 3.32 6 9 -20 8.34 4.33 6 -9 20 6.58 3.24 -6 -9 -20 3.90 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6.85 6 -9 4 8.24 5.25 6 -9 4 15.66 6.49 6 9 -3 5.81 4.74 6 9 -3 -1.48 3.24 6 -9 3 8.32 6.03 6 9 -2 161.83 18.25 6 -9 2 210.38 22.14 6 9 -1 70.29 12.09 6 9 -1 78.89 16.33 6 -9 1 80.42 13.24 6 9 0 -3.01 2.40 6 -9 0 -1.73 4.66 6 -9 0 0.91 3.54 6 9 1 85.90 13.12 -6 -9 1 79.43 15.13 6 -9 -1 86.82 18.41 6 -9 -1 88.36 14.46 6 9 1 82.90 17.87 6 9 2 201.08 20.05 6 -9 -2 187.92 25.47 6 -9 -2 228.47 22.16 6 9 2 171.84 24.89 6 9 3 3.73 4.71 6 9 3 2.55 3.05 6 -9 -3 18.60 7.72 6 -9 -3 7.61 5.08 6 9 4 22.48 11.23 6 9 4 20.83 6.61 6 -9 -4 22.66 8.40 6 -9 -4 23.47 7.29 6 9 5 -0.04 4.93 6 9 5 4.97 4.18 6 -9 -5 2.67 4.04 6 -9 -5 2.55 3.88 6 -9 -6 211.34 26.60 6 -9 -6 252.88 22.89 6 9 6 178.63 27.17 6 9 7 -2.65 3.15 6 -9 -7 6.29 4.99 6 -9 -7 4.06 2.91 6 9 8 14.23 7.47 6 -9 -8 11.94 6.99 6 -9 -8 17.62 5.59 6 9 9 6.12 6.66 6 -9 -9 6.67 6.14 6 -9 -9 3.94 3.56 6 9 10 56.32 15.56 6 9 10 47.82 11.58 6 -9 -10 43.42 11.23 6 -9 -10 46.01 9.05 6 9 11 80.84 18.62 6 9 11 108.65 18.47 6 -9 -11 63.89 14.36 6 -9 -11 100.38 13.27 6 9 12 294.62 28.94 6 -9 -12 237.26 20.41 6 9 12 281.79 32.83 6 9 13 7.98 5.65 6 9 13 12.05 6.75 6 -9 -13 9.62 4.34 6 -9 -13 10.38 4.35 6 9 14 140.30 19.36 6 -9 -14 93.08 15.19 6 -9 -14 122.55 13.54 6 9 14 132.21 21.00 6 9 15 15.26 7.00 6 -9 -15 17.46 6.28 6 -9 -15 20.07 5.23 6 9 16 126.19 16.49 6 -9 -16 107.83 11.96 6 9 17 5.32 2.97 6 -9 -17 3.33 3.28 6 -9 -17 10.79 3.88 6 -9 -18 -2.67 2.19 6 -9 -18 2.56 1.82 6 9 18 5.51 4.04 6 -9 -19 3.06 1.60 6 9 19 5.70 3.28 6 -9 -20 6.66 3.18 6 9 20 10.82 3.40 -6 -9 21 9.37 5.36 6 10 -20 8.90 3.52 6 -10 19 0.56 1.96 -6 -10 -19 0.20 1.38 6 10 -18 34.51 7.73 6 -10 18 28.58 5.57 6 -10 18 32.07 7.91 -6 -10 -18 20.75 5.14 6 10 -17 73.59 12.07 6 -10 17 70.57 12.63 -6 -10 -17 48.30 9.02 6 -10 17 54.90 8.39 -6 -10 -16 15.10 5.84 6 10 -16 30.21 8.08 6 -10 16 29.99 6.95 6 -10 16 20.15 7.65 -6 -10 -15 11.60 5.49 6 10 -15 20.53 6.58 6 -10 15 25.41 6.83 6 -10 15 24.18 8.13 6 10 -14 100.07 15.59 6 -10 14 103.81 16.19 -6 -10 -14 88.97 14.54 6 -10 14 94.13 13.51 6 10 -13 3.19 3.21 6 -10 13 8.51 4.43 6 -10 13 10.63 5.89 6 10 -12 2.24 3.06 6 -10 12 6.96 4.29 6 -10 12 7.01 4.89 6 10 -11 64.71 12.72 6 -10 11 68.90 13.90 6 -10 11 48.98 9.81 6 10 -10 64.83 13.11 6 -10 10 57.16 10.41 6 -10 10 59.95 12.81 6 10 -9 147.13 19.21 6 -10 9 142.45 19.48 6 -10 9 151.46 17.18 6 10 -9 84.96 16.90 6 10 -8 29.59 9.21 6 -10 8 39.50 10.50 6 -10 8 27.24 8.19 6 10 -7 8.77 5.77 6 -10 7 6.96 4.76 6 -10 7 13.34 6.50 6 10 -6 21.82 7.85 6 -10 6 23.84 8.37 6 -10 6 15.46 5.88 6 10 -5 24.81 8.36 6 -10 5 30.27 9.98 6 -10 5 39.92 9.53 6 10 -4 81.02 14.70 6 -10 4 73.61 14.53 6 -10 4 71.81 12.51 6 10 -3 36.47 10.47 6 -10 3 40.88 10.53 6 -10 3 34.22 8.20 6 10 -2 3.52 3.69 6 -10 2 7.22 2.42 -6 -10 -1 11.31 5.33 6 -10 1 12.13 9.14 6 -10 1 16.98 7.91 -6 -10 0 199.61 23.19 6 -10 0 223.42 28.05 6 -10 0 221.11 21.19 6 10 1 5.37 5.73 -6 -10 1 10.22 7.35 6 -10 -1 15.32 9.25 6 -10 -1 12.37 4.90 6 10 2 -0.38 4.67 -6 -10 2 11.87 6.28 6 -10 -2 8.71 7.25 6 -10 -2 7.05 4.69 6 10 3 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203.84 18.82 7 4 -4 158.39 21.62 7 -4 4 187.83 38.09 7 4 -4 191.09 40.85 7 -4 4 186.06 24.08 7 -4 4 167.77 20.37 7 4 -4 101.59 16.13 7 4 -3 10.66 6.21 7 -4 3 17.46 12.88 7 4 -3 11.66 6.11 7 4 -3 8.05 2.53 7 4 -3 15.25 4.50 7 4 -3 13.85 4.94 7 4 -3 23.40 16.40 7 -4 3 13.25 7.33 7 -4 3 10.64 4.78 7 4 -2 129.58 17.92 7 -4 2 122.15 31.07 7 4 -2 73.74 10.02 7 4 -2 131.61 14.90 7 4 -2 109.20 18.35 7 -4 2 106.68 16.56 7 -4 2 111.93 16.29 7 4 -2 56.83 12.67 7 4 -2 109.69 30.45 7 4 -1 36.53 10.10 7 4 -1 64.37 13.12 7 -4 1 69.11 22.80 7 4 -1 35.46 7.18 7 4 -1 70.73 11.10 7 4 -1 62.91 13.57 7 4 -1 45.31 10.67 7 4 -1 78.22 23.98 7 -4 1 49.53 11.76 7 -4 1 49.52 11.00 7 4 0 50.78 11.38 7 4 0 61.37 14.46 7 -4 0 45.80 17.94 7 -4 0 63.68 13.00 7 4 0 31.01 6.62 7 4 0 66.21 10.62 7 4 0 51.41 12.25 7 4 0 57.40 11.73 7 4 0 56.92 20.42 7 -4 0 55.89 11.61 7 -4 0 54.40 10.95 7 4 1 59.16 13.20 7 -4 -1 92.53 26.09 7 -4 -1 76.84 14.26 7 -4 -1 54.60 10.02 7 4 1 80.18 11.83 7 4 1 84.12 15.88 7 4 1 50.63 10.63 7 -4 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33.99 7.51 7 -6 21 42.09 7.75 7 -6 21 28.56 7.34 7 -6 20 43.81 10.57 7 6 -20 48.57 9.93 7 6 -20 38.28 9.43 7 -6 20 47.02 8.87 7 -6 20 33.50 7.91 7 -6 19 37.41 10.33 7 6 -19 27.68 8.85 7 -6 19 37.51 8.48 7 -6 18 68.01 13.92 7 -6 18 99.53 14.09 7 6 -18 74.84 13.78 7 -6 17 27.73 9.70 7 6 -17 34.35 9.77 7 -6 17 31.21 8.01 7 -6 16 60.83 14.21 7 6 -16 80.99 14.94 7 -6 16 71.25 12.07 7 -6 15 7.02 5.14 7 6 -15 23.21 9.85 7 -6 15 18.56 6.23 7 -6 14 31.09 11.09 7 6 -14 33.93 11.46 7 -6 14 31.56 8.81 7 6 -13 278.22 29.33 7 -6 13 227.72 21.71 7 -6 13 217.21 27.22 7 6 -12 115.54 18.67 7 -6 12 99.84 14.19 7 -6 12 82.69 16.59 7 6 -11 97.85 17.60 7 -6 11 83.25 12.78 7 6 -10 127.45 19.85 7 -6 10 101.78 13.87 7 -6 10 112.40 17.68 7 6 -9 1.09 3.25 7 -6 9 -0.55 3.69 7 6 -8 209.69 24.97 7 -6 8 205.21 23.67 7 6 -7 79.78 15.30 7 -6 7 103.22 16.85 7 -6 6 115.08 31.30 7 6 -6 145.13 40.67 7 -6 6 174.94 22.49 7 6 -5 7.66 4.69 7 -6 5 9.55 7.63 7 6 -5 5.74 9.07 7 -6 5 17.71 7.10 7 6 -4 57.92 13.12 7 -6 4 61.76 23.55 7 6 -4 72.78 13.33 7 6 -4 80.67 29.13 7 -6 4 108.44 16.98 7 6 -3 34.25 10.03 7 -6 3 32.73 14.83 7 6 -3 44.82 10.21 7 6 -3 54.49 13.05 7 6 -3 37.11 21.31 7 -6 3 61.19 13.01 7 -6 2 94.67 29.42 7 6 -2 118.34 20.00 7 6 -2 106.47 15.95 7 6 -2 115.98 33.49 7 -6 2 128.44 18.27 7 6 -2 80.04 15.06 7 6 -1 14.69 6.81 7 -6 1 20.00 13.19 7 6 -1 22.39 7.92 7 6 -1 27.57 8.31 7 6 -1 37.81 19.43 7 -6 1 15.55 6.17 7 6 0 43.76 11.29 7 -6 0 59.18 22.25 7 6 0 47.91 13.38 7 6 0 41.62 10.02 7 6 0 45.80 21.35 7 -6 0 39.29 9.65 7 6 1 17.82 8.04 7 -6 -1 2.73 9.12 7 6 1 8.30 4.06 7 6 1 8.75 4.16 7 6 1 21.23 14.23 7 -6 -1 17.66 5.67 7 -6 -2 132.35 33.53 7 6 2 154.60 23.36 7 6 2 126.42 17.55 7 6 2 129.53 33.59 7 -6 -2 125.82 17.33 7 6 2 100.99 17.17 7 6 3 35.79 10.57 7 -6 -3 29.72 15.68 7 6 3 48.83 13.74 7 6 3 45.32 10.91 7 6 3 37.09 15.80 7 -6 -3 39.50 9.31 7 6 4 54.19 13.43 7 -6 -4 68.29 24.25 7 6 4 109.45 18.81 7 6 4 108.19 16.53 7 6 4 49.29 20.03 7 -6 -4 88.75 14.15 7 6 5 8.82 5.06 7 -6 -5 0.85 8.61 7 6 5 20.47 7.74 7 6 5 14.88 12.63 7 -6 -5 12.86 4.80 7 -6 -6 116.10 30.13 7 -6 -6 96.34 27.16 7 6 6 178.92 20.90 7 6 6 149.03 18.94 7 6 6 91.59 28.77 7 -6 -6 165.13 19.09 7 6 6 138.85 21.72 7 6 7 50.99 13.63 7 -6 -7 62.02 12.82 7 6 7 51.92 10.58 7 6 7 74.16 13.75 7 -6 -7 67.64 12.15 7 -6 -8 173.16 21.25 7 6 8 231.84 24.31 7 6 8 191.44 21.63 7 -6 -8 209.02 20.47 7 6 8 181.17 25.59 7 6 9 8.20 7.15 7 -6 -9 -4.40 5.19 7 6 9 -2.75 5.27 7 6 9 15.98 8.20 7 -6 -9 -2.95 3.75 7 -6 -10 93.88 15.14 7 6 10 112.47 16.86 7 -6 -10 100.56 14.49 7 6 10 127.87 21.25 7 6 11 79.34 17.70 7 -6 -11 76.69 13.52 7 6 11 99.32 15.72 7 -6 -11 50.60 11.41 7 -6 -11 103.11 13.66 7 -6 -12 117.02 16.78 7 6 12 144.62 18.83 7 -6 -12 64.90 12.29 7 -6 -12 122.79 15.07 7 6 12 121.50 20.79 7 -6 -13 223.41 22.62 7 6 13 265.49 25.48 7 -6 -13 250.03 20.33 7 6 13 264.33 29.82 7 6 14 37.16 11.18 7 6 14 37.42 9.45 7 -6 -14 30.84 9.20 7 -6 -14 16.41 6.88 7 -6 -14 33.87 9.20 7 6 15 20.67 8.52 7 6 15 25.64 6.99 7 -6 -15 16.80 6.31 7 -6 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5.44 7 7 -15 11.78 5.94 7 -7 15 3.02 2.11 7 -7 15 2.61 2.87 7 -7 14 2.80 4.42 7 7 -14 11.94 7.33 7 -7 14 2.36 2.94 7 -7 14 -1.25 4.33 7 7 -13 166.32 22.00 7 -7 13 134.40 16.34 7 -7 13 132.30 20.51 7 -7 13 139.71 17.93 7 -7 12 68.27 14.86 7 7 -12 105.76 18.21 7 -7 12 84.07 13.00 7 -7 12 74.21 13.79 7 -7 11 6.96 3.80 7 7 -11 11.20 6.53 7 -7 11 16.29 5.71 7 -7 11 16.11 7.16 7 7 -10 26.43 9.10 7 -7 10 6.75 4.01 7 7 -9 78.21 14.27 7 -7 9 79.15 14.98 7 7 -8 100.70 17.97 7 -7 8 94.85 15.60 7 7 -7 8.35 6.34 7 7 -7 3.14 4.12 7 -7 7 12.08 5.67 7 7 -6 128.69 18.16 7 7 -6 111.13 16.13 7 -7 6 142.63 19.90 7 7 -6 85.52 16.71 7 7 -5 5.91 4.57 7 7 -5 13.53 6.11 7 -7 5 21.09 8.02 7 7 -4 56.88 13.62 7 7 -4 79.08 13.56 7 -7 4 86.86 14.83 7 7 -3 23.65 9.22 7 7 -3 23.78 7.60 7 7 -3 28.30 9.85 7 -7 3 34.29 9.78 7 7 -2 134.21 21.84 7 7 -2 139.01 17.92 7 -7 2 176.19 21.22 7 7 -2 110.36 18.81 7 7 -1 153.89 23.61 7 7 -1 148.95 18.88 7 -7 1 193.30 21.42 7 7 -1 120.05 19.18 7 7 0 4.56 5.29 7 7 0 9.25 6.72 7 7 0 12.39 6.01 7 -7 0 13.58 6.20 7 7 1 195.76 26.17 7 7 1 172.50 20.24 7 -7 -1 183.84 20.70 7 7 1 129.16 19.98 7 7 2 190.60 26.00 7 7 2 177.16 20.65 7 -7 -2 192.98 21.06 7 7 2 130.63 20.58 7 7 3 27.92 10.75 7 7 3 29.67 10.96 7 7 3 32.61 8.71 7 -7 -3 35.45 8.48 7 7 4 51.57 14.11 7 7 4 70.43 12.87 7 -7 -4 83.68 13.41 7 7 5 25.15 10.07 7 7 5 21.62 8.60 7 -7 -5 21.82 6.27 7 7 6 163.41 20.09 7 -7 -6 151.22 18.21 7 7 6 150.87 22.40 7 7 7 9.66 6.59 7 7 7 12.29 6.57 7 7 7 20.85 8.47 7 -7 -7 5.46 4.82 7 -7 -7 15.88 5.85 7 7 8 142.74 18.79 7 7 8 94.95 15.25 7 -7 -8 74.33 13.93 7 -7 -8 111.61 15.62 7 7 8 105.64 19.14 7 7 9 100.65 16.14 7 -7 -9 70.58 14.03 7 -7 -9 104.71 14.25 7 7 9 93.08 18.58 7 7 10 21.00 9.45 7 7 10 25.74 8.19 7 -7 -10 14.97 4.89 7 -7 -10 27.11 6.83 7 7 11 7.70 5.93 7 7 11 6.32 4.02 7 -7 -11 6.97 4.46 7 -7 -11 10.01 5.94 7 -7 -11 17.27 6.39 7 -7 -12 84.69 14.09 7 7 12 113.70 16.97 7 -7 -12 62.19 11.63 7 -7 -12 103.84 13.25 7 7 12 100.95 18.83 7 -7 -13 109.27 15.52 7 7 13 158.69 19.59 7 -7 -13 134.20 15.27 7 7 13 128.95 21.13 7 7 14 5.28 6.03 7 7 14 10.27 6.85 7 -7 -14 -1.12 2.91 7 -7 -14 3.07 3.34 7 -7 -14 1.65 2.42 7 7 15 5.87 3.17 7 7 15 4.17 2.87 7 -7 -15 6.26 3.85 7 -7 -15 2.89 3.35 7 -7 -15 7.19 2.72 7 7 16 23.43 8.32 7 7 16 11.65 3.27 7 -7 -16 10.81 5.63 7 -7 -16 12.07 4.89 7 -7 -16 13.62 4.98 7 7 17 41.37 8.93 7 -7 -17 44.67 9.10 7 -7 -17 25.46 7.37 7 -7 -17 53.39 8.53 7 -7 -18 47.56 9.06 7 -7 -18 30.58 7.13 7 -7 -18 52.35 8.16 7 7 18 55.29 9.61 7 -7 -19 1.24 1.83 7 -7 -19 -2.24 1.94 7 -7 -19 1.52 1.63 7 7 19 2.03 2.17 7 -7 -20 5.41 2.40 7 7 20 5.86 3.01 7 -7 -21 14.22 4.31 7 7 21 15.48 4.23 7 8 -21 1.47 1.65 7 8 -20 31.69 7.09 7 8 -20 32.43 6.86 7 -8 20 30.55 6.38 7 -8 20 31.30 7.03 7 8 -19 41.31 8.26 7 8 -19 49.30 9.65 7 -8 19 50.23 9.21 7 -8 19 45.53 9.04 7 8 -18 44.83 9.77 7 -8 18 29.25 7.21 7 -8 18 33.53 8.57 7 8 -17 54.87 11.26 7 -8 17 45.37 9.87 7 -8 17 43.04 10.29 7 8 -16 22.97 7.11 7 -8 16 17.86 6.93 7 -8 16 19.27 7.24 7 8 -15 40.39 10.64 7 8 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51.65 12.82 8 1 -6 57.59 9.21 8 1 -6 46.16 9.57 8 1 -6 61.81 13.88 8 1 -6 33.14 15.92 8 -1 6 40.62 10.78 8 1 -5 296.87 29.54 8 1 -5 296.59 20.16 8 1 -5 300.23 24.05 8 1 -5 352.11 32.19 8 -1 5 304.71 48.88 8 -1 5 231.14 25.08 8 -1 5 310.84 29.36 8 1 -4 264.63 28.07 8 1 -4 238.43 18.93 8 1 -4 246.49 22.15 8 1 -4 294.04 29.80 8 -1 4 235.54 42.66 8 -1 4 180.50 20.78 8 -1 4 285.91 27.46 8 1 -3 95.34 17.32 8 1 -3 87.41 11.84 8 1 -3 138.04 20.72 8 -1 3 76.00 12.40 8 -1 3 103.25 28.41 8 -1 3 100.50 16.52 8 -1 2 20.65 6.77 8 1 -2 18.59 6.80 8 -1 2 43.76 13.47 8 1 -2 27.24 8.34 8 1 -2 26.88 6.28 8 1 -2 46.19 12.77 8 -1 2 23.19 7.62 8 -1 2 33.32 15.72 8 -1 1 228.81 27.56 8 1 -1 172.34 23.42 8 1 -1 143.85 14.86 8 1 -1 214.69 25.62 8 1 -1 137.53 19.11 8 -1 1 170.09 35.51 8 -1 1 120.56 16.41 8 -1 1 138.92 18.27 8 1 -1 132.92 18.04 8 -1 0 58.51 11.56 8 1 0 59.84 12.33 8 1 0 114.40 18.74 8 -1 0 102.19 19.04 8 -1 0 54.57 11.65 8 1 0 67.51 12.83 8 -1 0 43.53 9.99 8 -1 0 71.68 23.59 8 1 1 231.49 28.28 8 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1 8 105.90 13.84 8 -1 -8 106.74 17.51 8 -1 -8 82.11 26.39 8 1 8 126.80 17.61 8 1 8 89.84 13.15 8 -1 -8 73.66 10.07 8 1 8 106.20 18.19 8 -1 -9 90.17 17.50 8 -1 -9 104.31 16.72 8 1 9 128.14 17.79 8 1 9 100.47 13.91 8 -1 -9 88.29 11.06 8 1 9 133.90 21.09 8 1 10 37.17 11.44 8 -1 -10 25.30 7.58 8 -1 -10 38.52 10.20 8 -1 -10 26.60 5.85 8 1 10 31.49 7.67 8 -1 -11 115.14 18.74 8 -1 -11 114.70 12.73 8 1 11 162.55 18.17 8 -1 -11 117.58 12.55 8 1 11 170.02 22.57 8 -1 -12 406.70 36.18 8 1 12 456.91 30.77 8 -1 -12 359.19 21.54 8 1 13 0.67 3.37 8 -1 -13 -0.95 3.66 8 -1 -13 5.05 2.57 8 1 13 6.30 4.12 8 1 14 49.45 11.82 8 -1 -14 36.80 11.06 8 -1 -14 22.48 5.74 8 1 14 41.03 9.11 8 -1 -15 14.63 8.68 8 -1 -15 7.93 3.24 8 1 15 12.75 5.73 8 1 15 1.40 2.70 8 -1 -16 288.23 29.43 8 1 16 366.29 26.36 8 1 16 328.64 29.05 8 -1 -17 40.00 11.76 8 -1 -17 30.79 6.03 8 1 17 45.72 9.29 8 1 17 42.44 10.36 8 -1 -18 0.89 4.36 8 1 18 17.92 5.47 8 -1 -19 1.05 3.39 8 1 19 6.99 3.66 8 -1 -20 64.75 12.14 8 1 20 75.26 10.66 8 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63.37 9.45 8 -2 11 81.58 13.01 8 2 -11 64.63 13.96 8 -2 11 92.68 16.91 8 2 -10 31.34 9.69 8 2 -10 33.94 7.40 8 2 -10 27.96 9.20 8 -2 10 35.62 8.55 8 -2 10 29.01 10.23 8 2 -9 102.96 18.26 8 2 -9 112.36 13.50 8 -2 9 95.19 13.24 8 2 -9 90.79 16.11 8 -2 9 81.30 17.65 8 -2 9 142.72 20.93 8 2 -8 131.72 19.53 8 2 -8 124.68 14.78 8 2 -8 106.26 17.31 8 -2 8 98.72 18.76 8 -2 8 127.28 20.20 8 2 -7 88.80 15.89 8 2 -7 98.86 13.51 8 2 -7 95.42 16.74 8 -2 7 92.37 17.89 8 -2 7 64.84 23.35 8 -2 7 118.28 19.20 8 2 -6 288.15 29.11 8 2 -6 258.32 18.42 8 2 -6 298.99 23.84 8 2 -6 263.99 27.85 8 -2 6 240.83 43.76 8 -2 6 252.47 28.61 8 -2 6 350.29 31.40 8 2 -5 76.58 15.83 8 2 -5 63.40 9.51 8 2 -5 75.52 11.91 8 2 -5 79.57 15.68 8 -2 5 72.39 15.34 8 -2 5 76.45 15.55 8 -2 5 79.29 24.79 8 -2 4 33.75 9.58 8 2 -4 45.23 11.29 8 2 -4 31.81 7.02 8 2 -4 31.77 7.59 8 2 -4 38.30 11.42 8 -2 4 25.89 9.88 8 -2 4 35.44 17.04 8 -2 3 0.56 2.91 8 2 -3 16.39 8.39 8 2 -3 8.63 2.92 8 2 -3 0.45 3.40 8 2 -3 9.59 6.16 8 2 -3 4.56 10.11 8 -2 3 8.53 4.96 8 -2 3 12.88 11.29 8 -2 2 13.73 6.21 8 -2 2 23.82 14.59 8 2 -2 6.71 4.43 8 -2 2 13.30 5.28 8 2 -2 8.18 4.28 8 2 -2 5.11 1.86 8 2 -2 13.62 4.11 8 2 -2 12.17 6.38 8 2 -2 2.41 3.03 8 2 -2 16.52 15.12 8 -2 2 9.55 4.69 8 -2 1 47.04 10.59 8 -2 1 56.68 21.74 8 2 -1 29.59 8.77 8 -2 1 61.75 15.21 8 2 -1 50.77 12.01 8 2 -1 35.11 7.35 8 2 -1 51.31 9.42 8 2 -1 56.03 13.63 8 2 -1 33.92 8.30 8 2 -1 47.33 19.21 8 -2 1 28.26 8.10 8 2 0 269.89 30.60 8 -2 0 290.84 30.65 8 2 0 170.39 16.81 8 2 0 223.02 20.71 8 2 0 274.12 28.79 8 2 0 185.62 21.98 8 -2 0 210.94 40.59 8 2 0 207.37 43.06 8 -2 0 160.47 19.50 8 -2 0 171.09 19.67 8 2 0 184.44 22.20 8 -2 -1 64.59 21.51 8 2 1 39.46 10.46 8 2 1 79.05 17.19 8 -2 -1 68.25 14.47 8 -2 -1 48.30 9.01 8 2 1 79.92 16.39 8 2 1 53.75 9.47 8 2 1 55.77 12.12 8 2 1 50.90 22.07 8 -2 -1 29.07 17.46 8 -2 -1 36.67 8.91 8 -2 -2 21.21 11.75 8 2 2 14.04 6.17 8 -2 -2 14.13 6.70 8 -2 -2 7.38 2.36 8 2 2 13.46 3.54 8 2 2 16.68 7.17 8 2 2 21.97 12.59 8 -2 -2 10.79 2.47 8 -2 -2 7.61 9.65 8 -2 -3 1.90 6.72 8 2 3 -2.52 4.20 8 -2 -3 11.21 12.10 8 -2 -3 11.77 5.75 8 -2 -3 -0.01 2.29 8 2 3 1.52 2.76 8 2 3 8.26 5.01 8 2 3 10.30 9.75 8 -2 -3 2.31 2.43 8 2 4 22.77 8.40 8 -2 -4 34.23 11.12 8 -2 -4 22.31 12.11 8 -2 -4 25.05 7.10 8 2 4 32.54 7.56 8 2 4 37.56 10.30 8 -2 -4 23.18 6.95 8 -2 -4 19.77 10.34 8 2 5 44.19 11.91 8 -2 -5 63.07 14.40 8 -2 -5 72.97 10.29 8 -2 -5 40.70 17.10 8 2 5 62.25 10.56 8 2 5 85.35 15.48 8 -2 -5 51.40 9.69 8 -2 -5 50.30 19.11 8 -2 -6 271.72 29.01 8 -2 -6 303.77 21.20 8 2 6 322.47 24.07 8 2 6 327.91 29.24 8 -2 -6 254.01 42.97 8 2 6 239.10 21.45 8 -2 -6 257.14 46.23 8 -2 -6 251.34 20.68 8 2 6 282.85 29.92 8 -2 -7 103.79 17.66 8 -2 -7 151.41 15.64 8 2 7 111.94 13.93 8 2 7 131.82 19.10 8 2 7 79.95 12.71 8 -2 -7 80.01 26.46 8 -2 -7 102.60 13.12 8 -2 -7 58.99 20.70 8 2 7 114.93 19.15 8 -2 -8 94.63 16.46 8 2 8 125.38 14.77 8 2 8 139.21 20.07 8 2 8 113.42 15.15 8 -2 -8 94.53 12.53 8 -2 -8 81.42 23.74 8 2 8 126.61 20.33 8 -2 -9 82.12 15.97 8 2 9 146.54 20.47 8 2 9 96.04 14.11 8 -2 -9 99.68 12.55 8 2 9 113.17 19.78 8 2 10 27.38 9.80 8 2 10 28.21 7.53 8 -2 -10 22.92 8.98 8 -2 -10 19.15 5.19 8 2 11 58.79 10.92 8 -2 -11 50.50 12.89 8 -2 -11 67.29 9.88 8 -2 -12 74.92 15.97 8 2 12 83.50 13.14 8 -2 -12 80.84 11.00 8 2 12 116.07 18.99 8 2 13 67.53 14.28 8 -2 -13 50.10 12.80 8 2 13 72.09 12.41 8 -2 -13 74.83 10.06 8 2 14 33.28 10.87 8 -2 -14 36.12 10.93 8 -2 -14 27.86 6.13 8 2 14 38.58 8.55 8 -2 -15 63.80 14.10 8 2 15 92.42 13.38 8 -2 -15 71.67 9.66 8 2 15 98.24 16.54 8 -2 -16 20.59 8.32 8 -2 -16 23.96 5.60 8 2 16 23.59 6.86 8 2 16 14.33 5.70 8 -2 -17 22.42 8.64 8 -2 -17 19.74 5.10 8 2 17 25.47 7.18 8 2 17 29.70 8.73 8 -2 -18 30.03 9.08 8 -2 -18 22.50 4.97 8 2 18 36.10 7.84 8 2 18 45.77 9.81 8 -2 -19 2.02 2.62 8 2 19 5.88 1.76 8 -2 -20 12.48 6.10 8 2 20 12.86 4.32 8 -2 -21 15.75 6.16 8 2 21 19.92 5.24 8 -2 -22 23.71 6.80 8 2 22 32.74 6.38 8 -2 -23 53.01 8.02 8 -2 -23 49.66 7.14 8 2 23 60.16 7.97 8 -3 23 41.11 6.42 8 3 -23 27.77 5.43 8 3 -22 30.92 6.45 8 -3 22 32.16 6.29 8 -3 22 25.10 5.82 8 3 -21 71.25 10.25 8 -3 21 90.79 11.21 8 -3 21 57.09 9.35 8 3 -20 14.66 4.78 8 -3 20 22.56 6.14 8 3 -19 17.17 5.74 8 3 -19 14.93 5.35 8 -3 19 22.27 6.96 8 3 -18 2.70 3.47 8 3 -18 2.53 2.64 8 3 -18 6.21 3.63 8 -3 18 4.96 4.53 8 3 -17 104.22 14.24 8 3 -17 123.45 17.49 8 3 -17 106.13 16.71 8 3 -16 80.13 13.11 8 3 -16 95.08 15.22 8 -3 16 100.43 14.39 8 3 -16 78.70 14.53 8 3 -15 90.70 14.65 8 3 -15 111.05 17.09 8 -3 15 135.16 16.65 8 3 -15 87.19 15.46 8 3 -14 0.25 2.60 8 3 -14 -6.91 6.24 8 3 -14 1.45 3.70 8 -3 14 5.94 3.60 8 3 -13 22.94 7.89 8 3 -13 21.65 7.84 8 3 -13 12.32 6.92 8 -3 13 14.63 5.47 8 3 -12 42.78 10.43 8 3 -12 46.65 11.17 8 3 -12 36.49 9.38 8 -3 12 45.96 9.71 8 3 -11 194.83 22.99 8 3 -11 218.10 24.29 8 -3 11 187.29 18.79 8 3 -11 256.23 19.31 8 3 -11 167.91 22.31 8 3 -10 94.89 16.02 8 3 -10 93.03 15.34 8 -3 10 89.24 13.19 8 3 -10 124.27 14.18 8 3 -10 77.85 14.81 8 -3 10 102.14 18.66 8 -3 10 133.26 21.60 8 3 -9 98.95 16.59 8 3 -9 122.63 14.31 8 3 -9 80.30 15.15 8 -3 9 99.65 18.08 8 -3 9 124.68 19.85 8 3 -8 13.04 5.98 8 3 -8 20.15 6.20 8 3 -8 17.23 6.43 8 -3 8 17.81 7.72 8 -3 8 30.07 10.68 8 3 -7 174.78 22.05 8 3 -7 207.27 19.78 8 3 -7 161.98 22.04 8 -3 7 159.37 23.68 8 -3 7 219.66 25.47 8 3 -6 315.16 29.74 8 3 -6 380.15 21.87 8 3 -6 387.26 26.91 8 3 -6 299.57 29.77 8 -3 6 264.46 46.26 8 3 -6 273.50 50.81 8 -3 6 298.06 31.73 8 -3 6 400.02 33.71 8 -3 5 92.81 27.09 8 3 -5 103.77 17.25 8 3 -5 96.56 11.18 8 3 -5 125.71 15.51 8 3 -5 86.64 16.20 8 3 -5 91.46 28.81 8 -3 5 92.99 17.28 8 -3 5 97.50 16.83 8 3 -4 185.20 22.74 8 3 -4 165.75 14.87 8 3 -4 211.11 19.78 8 3 -4 175.51 22.80 8 -3 4 175.32 37.96 8 3 -4 161.25 39.52 8 -3 4 168.13 22.42 8 -3 4 213.06 23.80 8 -3 3 86.75 26.45 8 3 -3 101.56 17.02 8 3 -3 57.22 12.03 8 3 -3 90.62 11.57 8 3 -3 129.20 15.55 8 3 -3 98.54 16.94 8 3 -3 103.34 30.48 8 -3 3 76.32 15.41 8 -3 3 107.52 16.84 8 -3 2 148.85 21.92 8 -3 2 101.97 28.27 8 3 -2 112.30 19.06 8 3 -2 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12.55 8 4 0 79.49 16.33 8 4 0 67.06 13.70 8 4 0 76.93 26.25 8 -4 0 69.48 13.43 8 4 1 -1.41 2.39 8 -4 -1 17.75 14.44 8 -4 -1 3.35 3.81 8 -4 -1 -3.70 5.21 8 4 1 -7.22 3.71 8 4 1 3.53 2.97 8 4 1 12.26 7.20 8 4 1 6.00 3.77 8 4 1 2.27 4.39 8 -4 -1 -4.19 6.13 8 -4 -2 106.20 17.29 8 -4 -2 97.21 29.49 8 -4 -2 86.53 12.10 8 4 2 60.05 10.10 8 4 2 132.93 15.23 8 4 2 143.71 22.11 8 4 2 92.46 16.13 8 4 2 87.64 29.13 8 -4 -2 83.38 13.49 8 4 2 77.46 14.85 8 4 3 19.06 7.60 8 -4 -3 26.72 14.95 8 -4 -3 28.88 9.43 8 4 3 13.47 4.91 8 -4 -3 25.25 6.25 8 4 3 28.01 7.11 8 4 3 25.57 9.18 8 4 3 11.09 7.92 8 -4 -3 17.31 5.92 8 4 4 61.82 13.39 8 -4 -4 63.66 23.57 8 -4 -4 74.74 14.22 8 4 4 44.69 9.24 8 -4 -4 71.87 10.63 8 4 4 85.15 12.42 8 4 4 74.21 14.63 8 -4 -4 22.13 13.73 8 4 4 45.57 21.66 8 -4 -4 64.59 11.85 8 4 5 41.72 11.44 8 -4 -5 55.02 13.02 8 4 5 37.26 8.27 8 -4 -5 51.99 9.15 8 4 5 73.64 11.94 8 4 5 64.03 13.66 8 -4 -5 55.15 10.96 8 4 6 60.44 13.99 8 -4 -6 68.91 14.13 8 4 6 104.84 15.15 8 4 6 86.09 15.49 8 4 6 58.90 11.16 8 -4 -6 77.52 12.98 8 -4 -7 91.71 15.85 8 4 7 105.32 17.21 8 4 7 85.97 13.43 8 -4 -7 91.52 13.65 8 4 7 99.19 17.43 8 4 8 9.80 5.51 8 4 8 8.63 3.86 8 -4 -8 10.94 5.85 8 4 8 12.73 7.48 8 -4 -8 6.09 2.49 8 -4 -9 108.47 17.03 8 4 9 165.24 21.91 8 4 9 117.55 16.13 8 -4 -9 116.79 14.32 8 4 9 114.27 19.29 8 4 10 80.90 16.50 8 -4 -10 70.64 13.03 8 4 10 94.29 14.40 8 -4 -10 78.70 11.65 8 4 11 -0.78 4.91 8 4 11 -5.17 5.21 8 -4 -11 -0.79 4.54 8 -4 -11 2.80 2.83 8 4 12 32.00 10.47 8 4 12 38.34 9.08 8 -4 -12 31.64 8.83 8 -4 -12 33.15 6.94 8 4 13 69.91 15.00 8 4 13 41.50 9.41 8 -4 -13 36.23 9.06 8 -4 -13 41.53 8.49 8 4 14 -5.06 5.27 8 4 14 1.86 2.52 8 -4 -14 1.67 1.78 8 4 15 66.01 13.16 8 -4 -15 47.88 11.36 8 -4 -15 56.22 8.99 8 4 15 53.23 9.82 8 4 16 45.47 10.75 8 -4 -16 41.15 9.60 8 -4 -16 51.99 8.32 8 4 16 56.72 9.98 8 4 17 15.26 6.75 8 -4 -17 14.69 6.63 8 -4 -17 19.08 4.89 8 4 17 23.05 6.28 8 -4 -18 76.72 13.20 8 4 18 88.26 11.98 8 -4 -18 70.60 8.87 8 4 18 100.27 14.15 8 -4 -19 70.62 11.83 8 4 19 80.84 10.66 8 -4 -19 62.64 8.07 8 -4 -20 88.56 12.93 8 4 20 105.52 11.85 8 -4 -21 36.47 8.05 8 4 21 37.34 6.77 8 -4 -22 65.06 9.88 8 4 22 71.43 8.62 8 5 -22 26.83 5.06 8 -5 22 30.05 5.54 8 5 -21 53.34 7.78 8 -5 21 65.70 8.79 8 -5 21 39.74 7.06 8 5 -20 6.60 4.20 8 5 -20 1.46 1.77 8 -5 20 6.51 3.32 8 -5 20 3.50 2.89 8 5 -19 4.26 3.48 8 5 -19 4.30 4.06 8 -5 19 6.44 3.87 8 -5 19 0.76 2.00 8 5 -18 18.68 6.43 8 5 -18 4.93 4.71 8 -5 18 16.74 5.82 8 -5 18 9.92 4.08 8 5 -17 80.69 13.26 8 -5 17 92.27 13.17 8 5 -17 67.90 14.06 8 -5 17 68.42 11.10 8 5 -16 79.74 13.74 8 -5 16 86.45 13.22 8 5 -16 61.34 13.60 8 -5 16 66.66 11.36 8 5 -15 2.57 5.66 8 5 -15 1.28 3.14 8 -5 15 -1.17 3.06 8 -5 15 -1.69 3.81 8 5 -14 0.64 4.20 8 5 -14 -0.95 5.40 8 -5 14 7.51 3.04 8 -5 14 0.98 3.31 8 5 -13 2.99 4.30 8 5 -13 -0.30 3.08 8 -5 13 11.76 5.70 8 -5 13 12.70 4.82 8 5 -12 121.46 18.23 8 -5 12 125.88 15.54 8 5 -12 83.36 16.38 8 -5 12 131.98 18.69 8 5 -11 23.85 8.02 8 5 -11 19.65 6.44 8 -5 11 20.86 6.28 8 -5 11 21.10 7.96 8 5 -10 57.02 11.30 8 5 -10 57.64 12.52 8 5 -10 42.11 11.24 8 -5 10 74.60 14.97 8 5 -9 3.09 2.63 8 5 -9 -5.66 6.77 8 -5 9 3.42 3.18 8 5 -8 77.70 13.77 8 5 -8 71.96 15.06 8 -5 8 76.23 16.39 8 5 -7 250.14 25.52 8 5 -7 214.87 26.33 8 -5 7 302.18 30.56 8 5 -6 65.29 12.90 8 5 -6 38.43 11.35 8 -5 6 70.72 15.38 8 5 -5 105.88 17.93 8 5 -5 89.43 16.91 8 5 -5 77.96 13.69 8 -5 5 105.46 17.79 8 5 -4 19.81 8.60 8 5 -4 44.49 11.38 8 5 -4 42.95 11.55 8 5 -4 35.53 8.75 8 -5 4 43.08 11.63 8 5 -3 93.75 17.33 8 5 -3 80.83 13.96 8 -5 3 101.33 17.45 8 5 -3 80.49 15.35 8 5 -2 7.97 5.42 8 -5 2 5.82 2.82 8 5 -2 26.17 9.65 8 5 -2 12.83 5.28 8 -5 2 30.28 10.11 8 5 -1 4.68 3.09 8 -5 1 -7.42 4.12 8 5 -1 4.86 4.04 8 5 -1 8.60 3.26 8 -5 1 3.03 5.22 8 5 0 24.75 8.71 8 -5 0 13.91 4.40 8 5 0 23.90 9.22 8 5 0 22.93 8.38 8 -5 0 15.60 6.99 8 5 1 6.81 4.97 8 -5 -1 -2.52 3.14 8 5 1 1.93 3.30 8 5 1 7.89 4.07 8 -5 -1 2.55 3.12 8 5 2 25.62 8.78 8 -5 -2 26.86 9.22 8 -5 -2 20.82 5.81 8 5 2 20.95 6.11 8 5 2 46.04 12.98 8 5 2 31.00 8.77 8 -5 -2 33.16 8.03 8 -5 -3 71.37 14.55 8 5 3 68.75 14.29 8 -5 -3 56.87 9.95 8 5 3 46.14 9.11 8 5 3 79.13 14.18 8 -5 -3 63.51 11.80 8 5 4 38.89 10.62 8 -5 -4 49.73 11.59 8 -5 -4 31.45 7.75 8 5 4 35.32 8.41 8 5 4 46.83 11.64 8 -5 -4 44.53 10.54 8 -5 -5 92.80 15.95 8 5 5 106.84 16.16 8 5 5 67.74 11.45 8 -5 -5 102.21 14.98 8 5 5 76.23 15.62 8 5 6 45.31 12.28 8 -5 -6 63.10 12.76 8 5 6 46.85 9.92 8 5 6 61.83 13.08 8 -5 -6 61.28 11.88 8 -5 -7 232.93 24.18 8 5 7 284.33 28.50 8 5 7 208.78 21.28 8 -5 -7 244.42 22.59 8 5 7 214.78 26.15 8 -5 -8 89.94 15.86 8 5 8 144.21 20.14 8 5 8 88.02 14.23 8 -5 -8 109.69 14.78 8 5 8 105.85 19.37 8 5 9 4.09 5.00 8 5 9 1.23 2.30 8 -5 -9 8.34 7.02 8 5 9 7.85 6.85 8 -5 -9 1.11 2.52 8 5 10 62.04 14.75 8 5 10 59.33 11.35 8 -5 -10 48.01 10.79 8 -5 -10 57.93 10.31 8 5 11 7.71 5.51 8 5 11 17.99 6.30 8 -5 -11 12.14 6.49 8 -5 -11 11.99 4.97 8 -5 -12 118.15 16.49 8 5 12 125.23 16.21 8 -5 -12 149.70 15.92 8 5 12 157.06 21.99 8 5 13 5.71 5.11 8 5 13 3.59 2.61 8 -5 -13 4.24 4.19 8 -5 -13 14.03 5.27 8 5 14 12.18 7.61 8 5 14 5.62 4.11 8 -5 -14 3.59 3.74 8 -5 -14 5.90 4.64 8 5 15 -1.70 3.40 8 5 15 -4.06 4.17 8 -5 -15 5.95 4.18 8 -5 -15 6.36 4.49 8 -5 -16 87.78 13.23 8 5 16 95.73 12.88 8 -5 -16 76.00 10.00 8 5 16 109.36 15.98 8 -5 -17 84.46 13.33 8 5 17 86.02 11.84 8 -5 -17 75.48 9.46 8 5 17 99.17 14.46 8 -5 -18 14.78 5.83 8 -5 -18 12.33 4.09 8 5 18 12.05 4.95 8 -5 -19 1.71 3.08 8 -5 -19 5.15 2.72 8 5 19 1.35 2.16 8 -5 -20 1.69 2.81 8 5 20 4.49 2.84 8 -5 -21 67.89 9.75 8 5 21 73.60 8.98 8 5 22 24.48 4.86 8 6 -21 29.00 5.50 8 -6 21 32.92 5.98 8 6 -20 2.93 2.73 8 6 -20 6.71 3.37 8 6 -20 -0.97 1.76 8 -6 20 -4.96 3.42 8 -6 19 43.28 8.03 8 6 -19 39.47 8.15 8 6 -19 30.38 7.15 8 -6 19 39.19 7.59 8 6 -18 27.64 6.92 8 6 -18 26.79 7.37 8 -6 18 22.15 6.57 8 -6 18 29.68 7.25 8 6 -17 26.15 7.33 8 6 -17 12.78 4.80 8 -6 17 21.03 6.62 8 -6 17 14.65 5.29 8 6 -16 24.72 7.43 8 6 -16 8.93 4.31 8 -6 16 23.59 6.66 8 -6 16 19.54 5.67 8 6 -15 30.30 8.63 8 6 -15 27.65 8.96 8 -6 15 30.53 7.83 8 -6 15 29.03 7.40 8 6 -14 4.84 4.81 8 6 -14 3.49 3.20 8 -6 14 1.29 2.21 8 -6 14 0.87 3.50 8 6 -13 21.35 7.67 8 6 -13 4.64 3.79 8 -6 13 20.74 6.08 8 -6 13 15.00 6.61 8 6 -12 4.15 3.40 8 6 -12 -4.04 6.02 8 -6 12 8.08 4.15 8 -6 12 -0.30 3.32 8 6 -11 23.00 8.59 8 6 -11 8.57 3.99 8 -6 11 20.04 7.96 8 6 -10 88.67 15.18 8 -6 10 84.30 14.99 8 6 -9 26.21 8.08 8 6 -9 16.27 7.28 8 -6 9 28.14 8.71 8 6 -8 40.09 12.24 8 -6 8 78.89 14.41 8 6 -7 7.17 3.47 8 6 -7 0.94 5.09 8 -6 7 11.67 6.57 8 6 -6 24.98 8.87 8 6 -6 24.85 6.85 8 -6 6 47.31 12.85 8 6 -5 58.01 13.15 8 6 -5 75.09 16.18 8 6 -5 68.09 12.68 8 -6 5 87.38 15.27 8 6 -4 44.11 11.48 8 -6 4 35.31 7.87 8 6 -4 57.24 13.71 8 6 -4 55.13 10.99 8 -6 4 64.59 14.00 8 6 -3 15.85 7.13 8 -6 3 7.61 4.51 8 6 -3 23.27 8.60 8 6 -3 26.61 7.27 8 -6 3 27.45 9.43 8 -6 2 101.26 12.74 8 6 -2 155.04 23.48 8 6 -2 131.35 17.98 8 -6 2 152.77 20.32 8 6 -2 114.58 18.69 8 6 -1 3.98 3.14 8 -6 1 -2.78 3.63 8 6 -1 9.23 6.67 8 6 -1 7.33 4.64 8 -6 1 5.63 4.76 8 6 0 43.43 12.69 8 -6 0 25.90 6.77 8 6 0 58.98 14.30 8 6 0 52.08 11.11 8 -6 0 49.55 10.33 8 6 1 2.75 4.19 8 -6 -1 -1.22 2.55 8 6 1 7.53 4.18 8 6 1 4.01 3.21 8 -6 -1 10.84 5.55 8 -6 -2 95.93 12.13 8 6 2 155.88 23.13 8 6 2 136.70 19.07 8 6 2 98.43 13.66 8 -6 -2 134.45 18.24 8 6 2 106.62 17.48 8 6 3 16.48 7.33 8 -6 -3 19.10 5.66 8 6 3 17.49 6.33 8 6 3 40.81 10.66 8 -6 -3 20.02 6.06 8 6 4 43.98 11.51 8 6 4 42.98 9.44 8 6 4 61.11 12.03 8 -6 -4 52.89 10.06 8 6 5 76.09 15.65 8 6 5 61.25 11.02 8 6 5 112.53 16.69 8 -6 -5 93.54 14.59 8 6 6 48.13 12.61 8 -6 -6 50.69 11.35 8 6 6 39.92 8.87 8 6 6 65.22 13.67 8 -6 -6 49.12 10.64 8 6 7 8.50 4.37 8 -6 -7 16.95 6.41 8 6 7 13.40 5.70 8 6 7 14.75 7.46 8 -6 -7 18.91 6.57 8 -6 -8 88.58 14.16 8 6 8 129.09 19.23 8 6 8 84.08 13.68 8 -6 -8 96.51 13.37 8 6 8 89.50 17.93 8 6 9 35.43 11.40 8 6 9 27.22 7.69 8 -6 -9 26.46 8.57 8 -6 -9 31.10 7.66 8 -6 -10 64.12 12.35 8 6 10 80.10 13.51 8 -6 -10 62.50 10.40 8 6 10 85.77 17.84 8 6 11 22.31 8.60 8 6 11 23.45 7.40 8 -6 -11 15.59 6.61 8 -6 -11 20.89 5.84 8 6 12 6.52 5.93 8 6 12 5.20 3.75 8 -6 -12 6.26 3.70 8 -6 -12 4.02 3.23 8 6 13 20.84 8.24 8 6 13 23.94 6.75 8 -6 -13 23.85 7.29 8 -6 -13 31.88 7.19 8 6 14 1.33 2.17 8 -6 -14 -1.13 2.74 8 -6 -14 6.11 3.09 8 6 15 42.02 10.22 8 6 15 26.02 6.76 8 -6 -15 30.40 7.91 8 -6 -15 34.48 7.14 8 6 16 22.49 6.79 8 -6 -16 18.44 6.24 8 -6 -16 19.81 5.37 8 6 16 17.32 4.89 8 6 17 16.69 5.63 8 -6 -17 20.24 5.87 8 -6 -17 17.91 5.03 8 6 17 21.20 6.05 8 -6 -18 19.64 6.22 8 -6 -18 18.96 4.80 8 6 18 26.12 6.45 8 -6 -19 50.66 8.68 8 6 19 45.72 7.77 8 -6 -20 7.95 3.68 8 6 20 5.13 3.01 8 6 21 58.13 7.38 8 7 -20 -1.09 2.11 8 -7 20 -2.93 1.91 8 7 -19 13.01 4.16 8 7 -19 9.46 3.61 8 -7 19 13.83 3.78 8 7 -18 6.97 3.59 8 7 -18 5.41 3.26 8 7 -18 0.70 1.16 8 -7 18 1.23 2.29 8 7 -17 39.53 8.41 8 7 -17 36.66 8.90 8 7 -17 27.28 5.67 8 -7 17 40.94 7.84 8 7 -16 99.31 13.52 8 7 -16 101.56 15.60 8 7 -16 81.85 10.60 8 -7 16 94.20 12.13 8 7 -15 25.62 7.87 8 7 -15 23.45 8.11 8 7 -15 15.35 4.88 8 -7 15 16.53 5.76 8 -7 15 28.69 7.36 8 7 -14 28.47 8.31 8 7 -14 18.90 6.96 8 7 -14 19.89 4.33 8 -7 14 22.49 6.54 8 -7 14 24.02 7.12 8 7 -13 15.15 6.54 8 7 -13 13.53 5.20 8 7 -13 1.31 2.93 8 -7 13 18.95 5.94 8 7 -12 40.91 10.14 8 7 -12 45.13 12.10 8 7 -12 30.82 7.66 8 -7 12 51.93 10.54 8 7 -11 58.45 11.07 8 7 -11 45.29 12.05 8 7 -11 34.51 8.19 8 -7 11 57.19 11.91 8 7 -10 76.39 13.37 8 7 -10 51.57 12.20 8 7 -10 51.77 10.12 8 -7 10 81.71 13.99 8 7 -9 118.51 16.35 8 7 -9 104.37 18.57 8 7 -9 97.23 13.67 8 -7 9 130.63 17.65 8 7 -8 24.04 9.43 8 7 -8 26.57 7.52 8 -7 8 35.82 9.66 8 7 -7 55.39 13.88 8 7 -7 58.46 11.33 8 -7 7 85.19 15.04 8 7 -6 62.77 15.36 8 7 -6 71.81 12.57 8 -7 6 103.79 16.44 8 7 -5 6.69 5.19 8 7 -5 2.67 4.93 8 7 -5 11.82 5.07 8 -7 5 1.54 4.51 8 7 -4 23.52 9.10 8 7 -4 35.46 11.35 8 7 -4 31.43 7.89 8 -7 4 35.46 9.99 8 7 -3 15.28 7.76 8 7 -3 21.23 8.81 8 7 -3 28.21 8.12 8 -7 3 38.61 10.84 8 7 -2 100.93 19.24 8 7 -2 84.32 14.26 8 -7 2 99.04 15.97 8 7 -2 66.40 14.70 8 7 -1 130.53 21.83 8 7 -1 125.04 17.57 8 -7 1 132.06 17.46 8 7 -1 86.30 16.47 8 7 0 5.73 5.80 8 7 0 11.55 8.09 8 7 0 18.71 6.88 8 -7 0 5.94 5.34 8 7 1 136.45 21.26 8 7 1 146.44 18.88 8 -7 -1 134.04 17.62 8 7 1 88.04 17.15 8 7 2 65.80 15.14 8 7 2 130.26 20.90 8 7 2 108.38 15.99 8 -7 -2 99.40 14.86 8 7 3 27.11 9.58 8 7 3 40.06 9.03 8 7 3 47.43 10.93 8 -7 -3 41.46 10.37 8 7 4 18.50 7.96 8 7 4 21.32 7.09 8 7 4 37.66 9.88 8 -7 -4 27.73 7.92 8 7 5 7.69 4.19 8 7 5 5.57 3.78 8 -7 -5 -0.26 2.37 8 7 6 52.72 13.77 8 7 6 111.97 16.69 8 7 6 73.45 12.67 8 -7 -6 96.11 14.14 8 7 7 67.96 15.32 8 7 7 51.52 10.95 8 7 7 75.17 14.43 8 -7 -7 65.51 11.85 8 7 8 34.71 10.44 8 7 8 44.92 9.96 8 -7 -8 31.61 7.62 8 7 9 115.22 15.72 8 -7 -9 131.56 15.20 8 7 9 135.87 20.50 8 7 10 77.04 15.67 8 7 10 81.39 13.70 8 -7 -10 76.89 11.08 8 7 11 62.69 13.74 8 7 11 61.47 11.78 8 -7 -11 55.64 10.95 8 -7 -11 70.72 10.76 8 7 12 53.19 13.02 8 -7 -12 54.22 10.60 8 7 12 64.68 11.28 8 -7 -12 51.30 9.09 8 7 13 23.23 8.36 8 7 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140.47 17.10 8 8 4 106.76 18.99 8 8 5 52.08 12.94 8 8 5 43.20 9.37 8 8 5 65.43 12.51 8 -8 -5 74.76 12.31 8 8 6 1.62 3.24 8 8 6 -0.09 3.85 8 -8 -6 8.30 4.71 8 8 7 92.59 14.06 8 -8 -7 106.66 13.29 8 8 7 90.18 17.32 8 8 8 9.18 7.21 8 8 8 22.96 7.16 8 -8 -8 28.09 6.90 8 8 9 54.65 14.21 8 8 9 67.12 12.24 8 -8 -9 90.15 11.92 8 8 10 135.54 16.83 8 -8 -10 154.00 15.06 8 8 10 148.32 20.78 8 8 11 3.97 5.70 8 8 11 5.40 4.03 8 -8 -11 4.45 3.46 8 8 12 40.35 10.80 8 8 12 47.29 9.77 8 -8 -12 49.25 8.51 8 8 13 10.98 6.36 8 8 13 10.51 3.58 8 -8 -13 10.73 3.22 8 8 14 65.58 10.35 8 -8 -14 76.98 9.61 8 8 14 76.04 13.40 8 8 15 10.84 5.83 8 8 15 2.25 2.11 8 -8 -15 7.90 3.42 8 8 16 61.44 9.12 8 -8 -16 64.13 7.87 8 8 17 47.10 7.35 8 -8 -17 57.70 7.04 8 8 18 1.44 1.73 8 9 -17 19.71 4.99 8 -9 17 9.16 3.12 8 9 -16 0.29 1.44 8 9 -16 3.87 2.74 8 -9 16 4.09 2.76 8 9 -15 12.01 4.25 8 9 -15 10.18 3.55 8 -9 15 15.96 4.61 8 9 -14 18.17 5.05 8 9 -14 14.57 6.41 8 -9 14 14.34 4.83 8 9 -13 25.53 6.73 8 9 -13 31.48 8.35 8 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24.84 7.72 9 -6 -13 24.03 6.48 9 -6 -13 13.71 4.27 9 6 13 15.33 4.75 9 -6 -14 61.72 9.54 9 6 14 62.95 9.26 9 -6 -14 62.87 8.38 9 6 14 66.01 11.80 9 6 15 22.24 6.60 9 -6 -15 17.67 4.92 9 -6 -15 10.26 3.26 9 6 15 12.91 3.73 9 -6 -16 68.70 9.37 9 6 16 69.30 9.12 9 -6 -16 67.55 7.81 9 6 16 82.43 11.33 9 -6 -17 14.82 4.31 9 -6 -17 8.72 2.85 9 6 17 10.06 3.02 9 6 18 8.58 2.85 9 7 -17 6.57 3.21 9 -7 17 1.66 1.22 9 7 -16 17.09 5.06 9 7 -16 10.85 3.04 9 -7 16 12.41 3.84 9 7 -15 3.25 2.68 9 7 -15 3.21 3.29 9 7 -15 -0.76 1.64 9 -7 15 -0.56 2.00 9 7 -14 34.24 6.74 9 7 -14 52.60 10.05 9 7 -14 35.90 6.42 9 -7 14 45.21 7.87 9 7 -13 1.90 2.58 9 7 -13 3.50 2.51 9 -7 13 1.60 2.21 9 7 -12 164.88 19.81 9 7 -12 115.50 12.86 9 -7 12 148.24 14.91 9 7 -11 48.61 11.37 9 7 -11 41.07 8.06 9 -7 11 45.35 9.23 9 7 -10 39.86 10.77 9 7 -10 49.61 9.13 9 -7 10 58.54 10.54 9 7 -9 13.04 6.40 9 7 -9 5.17 3.09 9 -7 9 10.95 3.41 9 7 -8 11.86 5.62 9 7 -8 11.64 5.18 9 -7 8 15.12 5.92 9 7 -7 47.42 11.52 9 7 -7 46.77 9.58 9 -7 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10.58 4.82 9 10 -4 16.34 4.46 9 -10 4 21.32 5.65 9 10 -3 9.68 4.55 9 10 -3 15.41 4.45 9 -10 3 16.46 5.19 9 10 -2 11.98 4.88 9 10 -2 25.94 6.57 9 -10 2 21.90 5.56 9 10 -1 47.10 10.14 9 -10 1 56.42 8.16 9 10 0 -2.79 4.76 9 10 0 4.19 3.25 9 -10 0 9.02 5.04 9 10 1 37.40 9.26 9 10 1 29.72 6.79 9 10 2 7.87 4.47 9 10 2 12.57 4.31 9 -10 -2 11.93 4.36 9 10 3 6.07 4.64 9 10 3 9.84 4.26 9 -10 -3 15.64 4.56 9 10 4 14.00 6.17 9 10 4 7.08 3.38 9 -10 -4 17.26 4.86 9 10 5 26.41 7.55 9 10 5 25.00 5.99 9 -10 -5 41.22 6.54 9 10 6 14.73 5.68 9 10 6 11.62 4.04 9 -10 -6 22.13 4.80 9 10 7 8.65 4.32 9 10 7 10.88 4.11 9 -10 -7 8.73 3.27 9 10 8 46.59 8.91 9 10 8 37.04 6.41 9 -10 -8 41.13 5.98 9 10 9 81.87 9.41 9 -10 -9 100.85 8.71 9 10 9 83.86 11.38 9 10 10 3.68 3.03 9 10 10 -0.83 1.31 9 -10 -10 4.04 2.07 9 10 11 4.65 2.56 9 10 11 6.86 2.45 9 -10 -11 7.48 2.37 9 -11 7 11.24 3.03 9 -11 6 15.73 3.65 9 -11 5 13.37 3.39 9 11 -4 6.36 2.88 9 -11 4 16.21 3.95 9 11 -3 25.78 6.08 9 -11 3 53.98 6.75 9 11 -2 17.47 5.39 9 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12.74 10 0 4 64.17 14.52 10 0 4 96.28 12.93 10 0 -4 95.39 12.43 10 0 4 99.84 13.73 10 0 -4 59.49 10.70 10 0 4 87.41 14.61 10 0 -5 203.45 24.88 10 0 5 188.02 20.20 10 0 5 206.16 18.44 10 0 -5 191.10 17.47 10 0 5 193.87 18.87 10 0 -5 142.12 16.69 10 0 5 242.15 24.00 10 0 6 14.00 6.44 10 0 -6 18.79 7.70 10 0 6 18.78 5.20 10 0 -6 17.80 4.50 10 0 -6 16.06 5.57 10 0 -7 250.01 26.69 10 0 7 257.68 19.75 10 0 -7 237.69 18.28 10 0 7 247.47 25.58 10 0 -8 27.41 9.69 10 0 8 36.39 7.08 10 0 -8 31.21 5.84 10 0 -8 14.44 4.76 10 0 8 37.89 10.61 10 0 -9 -2.73 3.36 10 0 9 4.61 3.21 10 0 -9 0.34 2.29 10 0 -9 -3.76 4.75 10 0 9 2.34 3.75 10 0 -10 10.81 5.68 10 0 -10 8.69 2.86 10 0 10 11.33 5.33 10 0 -11 0.77 3.21 10 0 -11 4.74 2.89 10 0 11 3.21 4.64 10 0 -12 5.66 6.54 10 0 12 0.48 1.47 10 0 12 0.14 3.93 10 0 -13 86.79 14.09 10 0 13 65.68 8.78 10 0 -14 4.43 3.84 10 0 14 6.20 3.59 10 0 -15 33.80 8.79 10 0 15 22.67 5.04 10 0 -16 76.54 11.63 10 0 16 55.85 7.47 10 0 -17 111.69 12.80 10 0 17 89.46 8.71 10 0 -18 7.56 3.56 10 0 -18 4.38 2.41 10 1 -18 49.19 7.35 10 1 -18 27.31 5.24 10 1 -17 39.61 7.48 10 -1 17 25.15 4.70 10 1 -16 24.59 6.27 10 -1 16 9.31 3.03 10 1 -15 7.71 4.58 10 -1 15 3.44 2.00 10 1 -14 22.32 7.48 10 -1 14 12.24 3.83 10 1 -13 16.43 6.96 10 1 -12 69.95 13.18 10 1 -11 104.81 16.50 10 1 -11 113.52 10.98 10 1 -10 32.35 10.92 10 1 -10 27.65 5.59 10 -1 10 36.42 10.78 10 1 -9 7.01 5.75 10 1 -9 4.22 3.18 10 -1 9 3.25 2.37 10 1 -9 -0.53 3.08 10 -1 9 12.79 6.82 10 1 -8 66.39 13.69 10 1 -8 49.51 7.56 10 -1 8 54.00 8.62 10 1 -8 32.29 7.76 10 -1 8 59.49 12.86 10 1 -7 52.49 12.94 10 1 -7 32.76 6.80 10 -1 7 27.35 6.49 10 1 -7 17.40 6.83 10 -1 7 41.78 10.02 10 1 -6 21.90 5.55 10 -1 6 9.61 3.68 10 1 -6 10.90 4.61 10 -1 6 16.93 7.32 10 1 -5 55.57 12.97 10 -1 5 68.76 14.90 10 1 -5 56.33 9.38 10 -1 5 39.44 9.13 10 1 -5 35.00 8.40 10 -1 5 60.09 12.60 10 1 -4 18.71 9.77 10 -1 4 5.33 7.09 10 1 -4 9.64 4.13 10 -1 4 6.39 2.59 10 1 -4 3.82 3.79 10 -1 4 10.49 5.33 10 1 -3 219.99 27.08 10 1 -3 136.26 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1 4 11.92 4.14 10 -1 -4 5.58 2.38 10 1 4 15.60 7.57 10 -1 -4 17.26 6.79 10 1 5 52.83 11.50 10 -1 -5 58.37 15.88 10 1 5 27.71 8.29 10 1 5 49.83 8.60 10 -1 -5 35.52 7.39 10 1 5 59.66 11.85 10 -1 -5 41.93 9.15 10 1 6 19.51 7.92 10 -1 -6 32.69 10.24 10 1 6 22.07 5.53 10 -1 -6 19.48 4.88 10 1 6 33.72 8.65 10 -1 -6 20.88 6.27 10 1 7 42.29 11.01 10 -1 -7 52.55 15.93 10 1 7 43.63 7.99 10 -1 -7 38.94 8.02 10 -1 -7 31.26 8.36 10 1 8 53.20 11.64 10 -1 -8 47.92 11.86 10 1 8 57.42 8.76 10 -1 -8 38.01 6.55 10 -1 -8 20.03 5.95 10 1 9 -0.71 2.66 10 -1 -9 0.73 4.54 10 -1 -9 -2.51 2.94 10 -1 -9 -1.40 2.95 10 -1 -10 32.95 9.36 10 -1 -10 23.47 4.77 10 -1 -10 11.61 4.63 10 1 10 17.84 8.18 10 -1 -11 72.39 12.68 10 -1 -11 80.54 8.74 10 1 11 72.39 8.90 10 -1 -12 62.14 12.08 10 1 12 47.14 7.39 10 1 12 72.87 12.41 10 -1 -13 13.71 6.72 10 1 13 11.04 3.53 10 1 13 20.19 8.15 10 -1 -14 14.27 6.25 10 1 14 11.32 3.78 10 -1 -15 9.67 4.44 10 1 15 4.56 2.21 10 -1 -16 15.96 5.87 10 1 16 14.05 3.60 10 -1 -17 16.97 4.57 10 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5.83 10 2 -3 49.26 8.06 10 -2 3 24.50 8.81 10 2 -3 40.02 7.90 10 2 -3 24.90 7.70 10 -2 3 32.92 8.40 10 -2 3 42.50 10.61 10 2 -2 -0.33 2.25 10 -2 2 -7.26 6.31 10 2 -2 2.80 3.97 10 2 -2 -3.94 3.02 10 -2 2 -4.44 4.56 10 2 -1 87.79 10.80 10 -2 1 54.51 11.95 10 2 -1 103.81 13.35 10 2 -1 61.90 12.02 10 -2 1 59.36 9.30 10 2 -1 79.79 12.76 10 2 0 7.03 4.97 10 2 0 1.85 2.43 10 -2 0 -4.68 4.81 10 2 0 4.38 2.67 10 2 0 -2.43 2.72 10 -2 0 -1.20 2.57 10 2 1 63.61 9.84 10 -2 -1 66.48 11.41 10 2 1 83.63 11.51 10 2 1 61.42 12.12 10 -2 -1 46.32 8.68 10 2 1 67.38 11.76 10 2 2 -0.73 2.26 10 -2 -2 14.87 10.00 10 -2 -2 13.45 7.36 10 2 2 -2.12 2.39 10 2 2 1.00 2.06 10 2 2 5.42 4.94 10 2 3 45.81 9.98 10 -2 -3 55.04 14.28 10 -2 -3 31.08 8.69 10 2 3 33.87 7.24 10 2 3 51.88 9.11 10 2 3 50.03 11.02 10 2 4 -0.49 2.91 10 -2 -4 6.38 5.72 10 2 4 1.72 2.70 10 2 4 -2.33 3.67 10 2 5 -2.54 4.86 10 -2 -5 2.38 4.54 10 2 5 2.91 3.46 10 2 5 6.84 5.55 10 2 6 19.61 5.63 10 -2 -6 20.56 8.52 10 2 6 23.49 7.28 10 2 6 36.53 7.61 10 -2 -6 25.36 5.32 10 2 6 33.58 10.04 10 2 7 1.63 3.86 10 -2 -7 23.77 8.56 10 2 7 29.26 7.73 10 -2 -7 0.87 4.62 10 2 7 20.89 8.98 10 -2 -8 103.28 16.34 10 -2 -8 116.13 12.16 10 2 8 136.45 17.43 10 2 9 8.10 4.14 10 -2 -9 2.28 4.09 10 -2 -9 3.64 1.63 10 -2 -10 50.42 11.20 10 -2 -10 54.10 7.71 10 2 10 42.07 6.85 10 -2 -10 33.49 6.62 10 -2 -11 77.89 13.20 10 -2 -11 99.66 9.79 10 2 11 80.82 9.65 10 -2 -11 55.76 8.32 10 -2 -12 4.78 5.03 10 -2 -12 7.19 2.72 10 2 12 9.33 2.78 10 2 12 15.71 5.69 10 -2 -13 12.19 4.88 10 2 13 26.57 5.62 10 2 13 37.07 9.03 10 -2 -14 -0.74 2.29 10 2 14 0.14 1.08 10 -2 -15 41.25 8.34 10 2 15 44.58 6.70 10 -2 -15 22.15 4.78 10 -2 -16 20.05 6.20 10 -2 -16 12.88 3.45 10 2 16 25.80 4.86 10 -2 -17 19.37 5.34 10 2 17 18.97 3.87 10 -2 -18 22.32 5.24 10 2 18 21.94 3.95 10 3 -18 22.98 4.36 10 3 -17 9.19 3.15 10 3 -16 11.35 3.81 10 -3 16 4.04 2.10 10 3 -15 16.70 5.05 10 3 -15 10.69 3.47 10 -3 15 6.63 3.15 10 3 -14 19.57 5.25 10 -3 14 22.07 5.79 10 3 -13 -4.38 4.19 10 -3 13 3.46 2.01 10 3 -12 12.67 4.65 10 -3 12 8.01 3.54 10 3 -11 40.66 8.83 10 -3 11 32.31 8.15 10 3 -10 48.83 11.63 10 3 -10 51.93 10.79 10 3 -10 31.52 7.77 10 -3 10 15.49 6.38 10 3 -9 20.01 8.31 10 3 -9 13.14 6.89 10 3 -9 -2.74 4.15 10 -3 9 -1.18 2.58 10 3 -8 6.43 6.62 10 -3 8 -5.30 4.26 10 3 -8 4.30 4.49 10 3 -8 -3.10 5.47 10 -3 8 2.90 3.99 10 3 -7 66.95 13.46 10 -3 7 41.56 7.92 10 3 -7 38.74 8.70 10 -3 7 34.57 8.99 10 -3 6 102.00 15.07 10 3 -6 88.80 13.74 10 -3 6 89.55 14.37 10 -3 5 48.14 9.52 10 3 -5 46.67 10.24 10 -3 5 42.26 9.70 10 -3 4 -0.94 5.47 10 3 -4 6.99 2.85 10 -3 4 8.92 4.48 10 -3 3 16.07 5.55 10 3 -3 18.95 6.94 10 -3 3 7.98 2.61 10 3 -2 220.49 16.21 10 -3 2 255.91 21.82 10 3 -2 199.30 21.12 10 -3 2 207.70 20.59 10 3 -2 233.27 22.00 10 3 -1 82.85 10.45 10 -3 1 87.17 12.21 10 3 -1 67.05 13.12 10 -3 1 72.70 11.57 10 3 -1 84.75 13.68 10 3 0 6.72 4.31 10 3 0 3.73 2.82 10 -3 0 -1.59 4.25 10 3 0 3.40 3.90 10 3 0 -4.01 3.33 10 -3 0 -4.95 4.28 10 -3 -1 92.79 12.60 10 3 1 78.38 10.48 10 3 1 84.86 14.32 10 -3 -1 79.19 12.08 10 3 1 71.84 12.88 10 -3 -2 301.54 28.76 10 -3 -2 244.94 20.17 10 3 2 196.13 16.88 10 3 2 349.14 23.54 10 3 2 235.09 22.76 10 -3 -2 220.39 19.58 10 3 2 206.35 21.45 10 3 3 26.11 7.84 10 -3 -3 26.25 9.88 10 -3 -3 36.08 7.89 10 3 3 10.94 5.14 10 3 3 37.72 8.79 10 3 3 18.81 7.73 10 -3 -3 18.18 5.15 10 3 4 13.87 6.21 10 -3 -4 16.74 7.76 10 3 4 -1.11 3.02 10 3 4 4.19 3.19 10 -3 -4 12.66 4.74 10 -3 -5 85.70 14.61 10 3 5 52.91 8.78 10 3 5 77.54 13.60 10 -3 -5 63.84 9.62 10 3 5 74.62 13.26 10 -3 -6 134.55 17.56 10 3 6 100.93 12.43 10 3 6 149.41 18.52 10 -3 -6 111.08 12.35 10 3 6 123.46 16.66 10 3 7 45.65 10.12 10 -3 -7 43.03 11.47 10 3 7 30.22 7.20 10 3 7 49.87 11.02 10 -3 -7 40.32 8.10 10 3 8 -2.42 3.29 10 -3 -8 -0.68 2.59 10 3 8 -6.98 3.79 10 -3 -8 -4.03 3.89 10 -3 -8 4.16 2.99 10 3 9 -1.87 3.00 10 -3 -9 0.16 2.49 10 -3 -9 3.79 3.20 10 3 9 2.98 1.46 10 3 10 24.65 7.94 10 -3 -10 30.43 7.96 10 -3 -10 28.67 5.59 10 -3 -10 33.44 6.19 10 3 10 23.12 4.97 10 3 11 44.76 9.86 10 -3 -11 40.12 9.02 10 -3 -11 41.28 6.11 10 3 11 43.39 6.95 10 -3 -11 46.98 6.78 10 3 12 9.12 4.55 10 -3 -12 5.29 3.41 10 -3 -12 10.02 3.05 10 3 12 9.27 3.12 10 -3 -13 -3.40 3.47 10 -3 -13 -0.73 1.15 10 3 13 0.71 1.82 10 3 13 3.12 3.59 10 -3 -14 28.98 7.13 10 3 14 33.80 5.85 10 3 14 50.94 9.71 10 -3 -15 12.82 4.34 10 3 15 17.30 4.15 10 3 15 24.22 6.79 10 -3 -16 17.83 5.38 10 3 16 21.70 4.36 10 -3 -17 20.03 5.43 10 3 17 17.95 3.77 10 -3 -18 31.92 5.99 10 4 -17 23.60 4.29 10 4 -16 10.25 2.66 10 -4 16 11.68 3.39 10 4 -15 18.65 4.99 10 -4 15 16.87 4.37 10 4 -14 6.50 3.19 10 -4 14 12.46 4.01 10 4 -13 15.44 5.52 10 4 -13 11.75 4.50 10 -4 13 10.84 4.16 10 4 -12 45.32 9.94 10 4 -12 33.31 7.29 10 -4 12 37.50 7.75 10 4 -11 53.65 10.94 10 4 -11 48.91 9.06 10 -4 11 37.91 8.15 10 4 -10 84.80 14.00 10 4 -10 61.67 10.59 10 -4 10 49.11 9.69 10 4 -9 26.30 8.75 10 4 -9 15.44 5.51 10 -4 9 14.96 5.63 10 -4 8 16.75 5.85 10 -4 8 23.42 5.79 10 4 -8 10.86 4.00 10 -4 8 20.03 6.64 10 -4 7 -2.41 4.19 10 4 -7 5.87 6.12 10 4 -7 4.49 3.05 10 -4 7 2.39 4.44 10 -4 6 5.02 2.99 10 4 -6 -1.78 3.88 10 -4 6 2.41 2.37 10 -4 5 3.27 2.31 10 4 -5 4.75 2.58 10 -4 5 -1.61 5.21 10 -4 4 88.42 12.76 10 4 -4 80.31 13.40 10 -4 4 62.38 11.40 10 -4 3 0.06 3.07 10 -4 3 -5.60 6.04 10 -4 2 94.00 12.67 10 4 -2 109.97 15.84 10 -4 2 77.05 13.06 10 4 -2 83.05 13.45 10 4 -1 86.72 9.80 10 -4 1 59.38 10.42 10 4 -1 66.50 12.32 10 -4 1 57.16 11.46 10 4 -1 66.20 11.68 10 4 0 1.20 2.53 10 4 0 0.00 1.41 10 -4 0 -5.31 3.52 10 4 0 -0.11 4.57 10 -4 0 -6.98 5.23 10 4 1 50.10 10.52 10 -4 -1 77.56 10.67 10 4 1 56.78 8.20 10 4 1 62.65 12.11 10 -4 -1 53.32 9.82 10 -4 -2 121.93 13.55 10 4 2 99.48 10.99 10 4 2 116.29 15.87 10 -4 -2 94.75 13.13 10 4 2 91.98 14.48 10 4 3 5.35 4.81 10 -4 -3 7.68 6.06 10 4 3 7.33 3.85 10 4 3 2.29 2.66 10 -4 -3 2.25 2.60 10 -4 -4 98.28 15.41 10 4 4 77.47 9.94 10 4 4 91.26 14.70 10 -4 -4 86.59 12.29 10 4 4 72.46 13.01 10 4 5 9.63 5.06 10 -4 -5 15.98 6.44 10 4 5 5.57 3.22 10 4 5 4.34 3.86 10 -4 -5 8.84 4.84 10 4 6 13.11 6.66 10 -4 -6 8.72 5.53 10 4 6 -2.22 2.58 10 4 6 14.46 7.21 10 -4 -6 10.47 4.65 10 4 7 6.47 5.70 10 -4 -7 6.26 4.10 10 -4 -7 3.00 1.71 10 4 8 28.69 7.89 10 -4 -8 25.93 7.51 10 4 8 17.41 4.82 10 -4 -8 28.04 6.40 10 4 8 21.30 4.99 10 4 9 12.47 6.93 10 -4 -9 17.40 6.18 10 4 9 2.23 1.63 10 -4 -9 8.85 2.13 10 -4 -9 18.94 4.93 10 4 9 9.63 2.83 10 -4 -10 64.23 10.96 10 4 10 46.17 8.28 10 -4 -10 59.62 8.02 10 4 10 51.31 7.34 10 -4 -10 68.33 9.20 10 4 10 75.31 12.26 10 4 11 43.87 9.54 10 -4 -11 51.51 9.63 10 4 11 42.81 7.46 10 -4 -11 46.46 6.55 10 4 11 40.31 6.93 10 -4 -11 55.40 7.63 10 4 12 59.65 10.68 10 -4 -12 43.99 8.02 10 4 12 32.88 6.63 10 4 12 44.89 7.01 10 -4 -12 45.93 6.59 10 4 13 7.10 4.11 10 -4 -13 11.46 4.13 10 4 13 0.54 1.62 10 -4 -13 9.76 2.89 10 4 13 10.77 3.26 10 -4 -14 9.40 4.31 10 -4 -14 8.35 2.92 10 4 14 10.82 3.83 10 4 14 12.16 4.90 10 -4 -15 18.95 5.39 10 4 15 19.09 4.37 10 -4 -15 9.81 2.68 10 -4 -16 21.40 5.21 10 4 16 17.09 3.77 10 -4 -17 32.26 5.70 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18.87 7.52 10 -5 2 13.44 5.58 10 5 -1 50.95 10.71 10 -5 1 73.81 10.16 10 5 -1 85.58 13.92 10 -5 1 65.14 11.85 10 5 0 15.38 5.98 10 -5 0 21.89 5.86 10 5 0 17.54 7.90 10 -5 0 6.17 3.66 10 -5 -1 94.66 11.60 10 5 1 70.06 12.31 10 -5 -1 89.74 13.65 10 5 1 68.09 12.31 10 5 2 13.24 5.93 10 -5 -2 11.32 4.08 10 5 3 48.29 9.84 10 -5 -3 48.12 9.69 10 5 4 40.99 9.73 10 -5 -4 45.76 10.55 10 5 4 51.54 10.78 10 -5 -4 45.80 9.51 10 5 5 36.65 8.93 10 -5 -5 55.30 11.26 10 5 5 60.67 11.68 10 -5 -5 54.84 9.56 10 5 6 3.70 3.19 10 -5 -6 10.11 5.26 10 5 6 6.65 5.77 10 -5 -6 -2.70 2.73 10 5 7 13.44 6.19 10 -5 -7 11.95 4.70 10 -5 -7 9.71 4.61 10 5 7 1.65 1.39 10 -5 -8 86.93 12.37 10 5 8 54.28 7.83 10 -5 -8 82.54 10.76 10 5 8 97.01 14.41 10 -5 -9 109.01 13.42 10 5 9 69.55 8.75 10 -5 -9 109.03 11.71 10 5 9 109.73 15.19 10 -5 -10 93.87 12.21 10 -5 -10 84.92 9.76 10 5 10 62.84 8.43 10 -5 -10 98.89 10.65 10 5 10 93.77 13.82 10 5 11 15.08 5.68 10 -5 -11 17.54 5.42 10 -5 -11 8.79 3.06 10 -5 -11 18.21 5.10 10 5 11 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0 68.72 11.37 10 7 1 13.99 5.98 10 7 1 27.87 6.71 10 -7 -1 37.16 8.73 10 7 2 20.93 7.10 10 7 2 35.56 7.85 10 -7 -2 24.76 7.05 10 7 3 19.69 6.89 10 7 3 26.93 6.97 10 -7 -3 21.85 6.36 10 7 4 7.77 4.67 10 7 4 6.21 5.73 10 -7 -4 2.26 2.55 10 7 5 28.70 7.86 10 -7 -5 36.00 7.39 10 7 6 6.29 4.17 10 7 6 0.35 1.26 10 -7 -6 4.88 2.68 10 7 7 49.69 10.06 10 -7 -7 53.00 8.33 10 7 8 36.50 8.54 10 -7 -8 50.23 7.70 10 7 9 15.47 5.65 10 -7 -9 10.90 3.43 10 7 9 3.75 1.78 10 7 10 22.07 6.68 10 -7 -10 7.87 2.39 10 -7 -10 24.69 5.18 10 7 10 9.85 3.23 10 -7 -11 119.80 10.17 10 7 11 127.20 13.82 10 7 12 17.70 4.99 10 -7 -12 14.36 3.63 10 7 12 10.86 2.98 10 7 13 33.38 5.03 10 -7 -13 40.78 5.49 10 7 13 45.89 7.41 10 -8 12 -0.24 1.10 10 -8 11 29.84 4.93 10 8 -10 32.17 5.30 10 -8 10 34.51 5.71 10 8 -9 1.50 2.29 10 -8 9 -3.15 2.80 10 8 -8 18.95 4.55 10 -8 8 10.14 3.81 10 8 -7 143.28 12.36 10 -8 7 160.90 13.42 10 8 -6 5.15 2.70 10 -8 6 11.33 3.67 10 8 -5 6.56 2.48 10 -8 5 14.63 4.24 10 8 -4 8.67 4.37 10 -8 4 4.60 3.74 10 8 -3 45.15 7.99 10 -8 3 53.59 8.70 10 8 -2 33.93 7.97 10 8 -2 58.22 8.99 10 -8 2 60.59 9.67 10 8 -1 14.83 5.22 10 8 -1 26.32 5.84 10 -8 1 26.25 6.37 10 8 0 7.74 3.89 10 8 0 12.16 4.11 10 -8 0 11.65 4.82 10 8 1 18.33 5.93 10 8 1 31.93 6.69 10 -8 -1 34.93 7.21 10 8 2 69.98 10.18 10 -8 -2 64.28 9.31 10 8 3 22.65 7.00 10 -8 -3 45.96 7.79 10 8 4 -0.18 2.60 10 -8 -4 4.69 1.77 10 8 5 8.37 4.58 10 8 5 0.65 1.17 10 -8 -5 11.80 3.94 10 8 6 6.61 4.39 10 8 6 3.84 1.97 10 -8 -6 12.54 4.26 10 -8 -7 170.88 13.25 10 8 7 140.06 15.52 10 8 8 17.55 5.62 10 -8 -8 22.30 4.79 10 8 8 8.63 2.90 10 8 9 1.06 1.76 10 -8 -9 1.22 1.30 10 8 9 -1.47 2.43 10 8 10 29.88 6.34 10 -8 -10 39.11 5.55 10 8 10 21.71 4.15 10 8 11 28.84 5.84 10 -8 -11 31.80 4.70 10 8 11 17.91 3.52 10 -8 -12 1.38 1.40 10 -9 9 15.36 3.34 10 -9 8 32.72 5.15 10 -9 7 1.77 1.71 10 9 -6 22.38 4.55 10 -9 6 28.70 5.60 10 9 -5 46.89 6.93 10 -9 5 51.72 7.34 10 9 -4 170.95 12.56 10 -9 4 165.95 12.98 10 9 -3 32.07 6.25 10 -9 3 25.57 6.17 10 9 -2 9.41 3.90 10 9 -2 21.72 4.74 10 -9 2 20.30 5.15 10 9 -1 3.47 2.54 10 9 -1 18.36 4.80 10 -9 1 16.28 4.51 10 9 0 -1.58 2.49 10 -9 0 1.71 2.64 10 9 1 13.96 5.39 10 -9 -1 20.61 4.99 10 9 2 17.36 5.37 10 -9 -2 24.15 5.24 10 9 3 17.37 5.55 10 -9 -3 26.40 5.33 10 -9 -4 178.13 12.95 10 9 4 127.96 14.71 10 9 5 41.12 8.07 10 -9 -5 59.00 7.19 10 9 6 15.27 3.57 10 9 6 22.28 6.01 10 9 7 2.64 3.23 10 -9 -7 2.32 1.72 10 9 8 28.54 6.13 10 -9 -8 34.68 5.12 10 9 9 14.11 4.02 10 -9 -9 17.78 3.37 10 -10 5 9.16 2.87 10 -10 4 6.07 2.47 10 -10 3 11.15 2.79 10 -10 2 -2.45 1.72 10 -10 1 4.83 1.65 10 10 0 -1.25 1.67 10 -10 0 -4.07 2.13 10 10 1 3.91 2.43 10 -10 -1 4.52 2.06 10 10 2 2.63 1.54 10 -10 -2 2.93 1.72 10 10 3 9.45 3.61 10 -10 -3 14.07 3.21 10 10 4 2.10 2.32 10 -10 -4 2.03 1.49 10 10 5 8.25 3.28 10 -10 -5 5.91 2.03 11 0 0 4.57 3.57 11 0 0 -1.68 3.42 11 0 0 2.35 2.72 11 0 -1 25.18 7.72 11 0 1 18.89 6.07 11 0 1 4.99 3.32 11 0 -1 0.99 2.61 11 0 -1 6.24 3.83 11 0 1 9.61 4.54 11 0 2 6.28 3.87 11 0 -2 6.07 3.12 11 0 -2 13.78 4.88 11 0 2 2.11 1.78 11 0 3 14.80 6.99 11 0 3 4.77 3.69 11 0 -3 -1.34 2.95 11 0 -3 7.39 4.67 11 0 3 9.14 4.85 11 0 4 148.53 16.07 11 0 4 166.02 14.85 11 0 -4 153.97 13.95 11 0 -4 101.28 12.21 11 0 4 147.71 16.44 11 0 5 55.45 9.51 11 0 5 40.80 7.22 11 0 -5 38.89 6.93 11 0 -5 18.31 5.10 11 0 5 27.50 6.93 11 0 6 2.43 4.12 11 0 6 -0.61 1.87 11 0 -6 2.57 2.08 11 0 -6 1.14 2.73 11 0 6 1.71 3.32 11 0 7 0.48 2.76 11 0 7 5.08 3.62 11 0 -7 3.53 3.12 11 0 -7 1.02 3.25 11 0 7 2.34 3.38 11 0 -8 13.22 8.58 11 0 8 16.35 8.39 11 0 -8 12.55 4.11 11 0 -8 6.32 4.30 11 0 8 13.05 5.88 11 0 -9 54.53 11.68 11 0 9 32.40 7.14 11 0 -9 54.81 7.04 11 0 -9 22.60 5.07 11 0 -10 21.67 7.72 11 0 10 21.22 6.09 11 0 -10 3.69 3.22 11 0 11 50.36 8.48 11 0 -11 31.02 6.21 11 0 12 -0.42 1.63 11 0 -12 2.17 1.74 11 0 -13 2.75 2.26 11 0 13 1.14 2.06 11 0 -13 0.33 1.16 11 0 -14 17.34 5.69 11 0 14 27.94 5.88 11 0 -15 66.00 8.75 11 0 15 19.71 4.36 11 -1 15 6.82 2.78 11 -1 14 36.10 5.61 11 1 -14 39.45 6.00 11 -1 13 -2.95 2.27 11 1 -13 3.23 2.17 11 -1 12 3.37 2.97 11 1 -12 7.78 3.20 11 -1 11 15.60 5.67 11 1 -11 11.42 3.88 11 -1 10 37.66 6.76 11 1 -10 29.93 6.56 11 -1 9 1.74 4.05 11 1 -9 3.79 3.09 11 -1 8 66.59 10.53 11 1 -8 58.25 9.00 11 -1 7 4.78 2.85 11 1 -7 28.20 5.65 11 -1 7 19.55 4.72 11 1 -7 9.24 4.27 11 -1 6 24.62 6.32 11 1 -6 32.66 6.23 11 -1 6 29.84 6.13 11 1 -6 11.85 3.81 11 -1 5 53.20 9.76 11 1 -5 43.43 7.32 11 -1 5 39.67 7.24 11 1 -5 23.55 6.53 11 -1 4 66.03 12.51 11 1 -4 61.68 8.60 11 -1 4 55.06 8.77 11 1 -4 59.08 9.77 11 -1 3 41.58 9.20 11 1 -3 69.25 9.42 11 -1 3 60.18 9.17 11 1 -3 42.95 8.79 11 -1 2 56.60 9.89 11 1 -2 78.90 10.28 11 -1 2 63.76 9.13 11 1 -2 55.57 9.32 11 -1 1 57.24 9.38 11 1 -1 69.11 9.66 11 -1 1 50.99 8.30 11 1 -1 44.22 8.05 11 1 0 16.07 5.55 11 -1 0 11.11 5.26 11 1 0 13.15 4.76 11 -1 0 12.74 4.39 11 1 0 6.12 2.77 11 1 0 12.29 4.85 11 -1 -1 51.93 9.83 11 1 1 65.53 9.68 11 1 1 71.62 9.74 11 -1 -1 52.82 8.51 11 1 1 43.33 7.98 11 1 1 46.86 9.26 11 1 2 88.66 11.34 11 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11 -2 11 1.58 1.70 11 2 -11 0.26 1.64 11 -2 10 36.86 6.77 11 2 -10 27.77 6.45 11 -2 9 9.43 3.76 11 2 -9 15.18 4.88 11 -2 8 19.50 6.34 11 -2 8 35.56 6.03 11 2 -8 22.23 6.18 11 -2 7 22.99 6.85 11 -2 7 36.28 6.30 11 2 -7 31.37 7.55 11 -2 6 10.24 4.83 11 -2 6 19.45 4.92 11 2 -6 13.70 5.34 11 -2 5 28.54 6.67 11 -2 5 22.47 5.13 11 2 -5 23.40 6.87 11 -2 4 126.81 15.13 11 -2 4 151.40 14.67 11 2 -4 113.34 13.40 11 -2 3 8.35 5.58 11 -2 3 1.86 2.23 11 2 -3 12.42 5.24 11 -2 2 27.04 6.93 11 2 -2 40.13 7.92 11 -2 2 20.82 5.29 11 2 -2 16.61 6.14 11 -2 1 135.82 13.59 11 2 -1 154.06 14.44 11 -2 1 126.16 14.04 11 2 -1 97.69 12.72 11 2 0 50.55 7.68 11 -2 0 38.56 7.57 11 2 0 45.66 8.62 11 -2 0 23.14 5.53 11 2 0 19.35 5.70 11 2 0 20.57 6.16 11 -2 -1 155.95 15.07 11 2 1 119.65 11.41 11 2 1 181.69 15.59 11 -2 -1 137.35 14.38 11 2 1 102.50 12.85 11 2 1 107.97 13.58 11 2 2 12.27 5.01 11 2 2 15.96 4.91 11 -2 -2 9.71 2.89 11 2 2 10.60 4.58 11 2 3 5.68 3.15 11 2 3 9.89 5.17 11 -2 -3 5.39 3.06 11 2 3 5.68 3.21 11 2 4 146.97 13.97 11 -2 -4 151.03 14.23 11 2 4 146.96 14.90 11 2 4 134.47 15.10 11 2 5 27.39 6.83 11 2 5 30.23 6.24 11 -2 -5 27.17 6.15 11 2 6 15.40 5.59 11 -2 -6 21.87 5.39 11 2 6 7.65 3.86 11 -2 -7 61.16 11.43 11 2 7 34.14 7.45 11 -2 -7 41.53 6.63 11 2 7 40.48 8.31 11 -2 -8 51.07 9.93 11 2 8 26.37 6.99 11 -2 -8 41.41 6.38 11 2 8 34.39 7.65 11 -2 -9 23.04 7.04 11 2 9 18.19 5.12 11 -2 -9 26.26 4.83 11 2 9 28.81 7.04 11 -2 -10 30.57 7.87 11 2 10 48.77 7.92 11 -2 -10 41.98 5.61 11 2 10 48.93 8.77 11 -2 -11 1.86 3.57 11 2 11 2.67 2.50 11 2 11 9.15 4.75 11 -2 -12 9.23 4.54 11 2 12 13.94 3.78 11 2 12 15.05 5.36 11 -2 -13 15.69 4.78 11 2 13 7.53 3.04 11 -2 -14 18.33 5.41 11 -3 14 -0.39 1.05 11 3 -14 6.19 2.66 11 -3 13 25.22 4.19 11 3 -13 36.78 6.17 11 -3 12 3.35 1.87 11 3 -12 5.67 2.73 11 -3 11 48.56 6.67 11 3 -11 63.32 9.08 11 -3 10 22.77 4.82 11 3 -10 37.95 7.46 11 -3 9 54.60 8.05 11 3 -9 66.47 9.96 11 -3 8 8.22 3.47 11 -3 8 10.55 3.12 11 3 -8 6.11 3.52 11 -3 7 51.42 7.85 11 -3 7 40.54 6.52 11 3 -7 48.68 9.20 11 -3 7 29.78 6.26 11 -3 6 3.35 2.86 11 -3 6 6.82 3.06 11 3 -6 3.85 3.24 11 -3 6 3.48 1.45 11 -3 5 21.59 6.50 11 -3 5 38.47 7.32 11 3 -5 24.44 6.52 11 -3 5 21.74 5.65 11 -3 4 -0.51 2.75 11 -3 4 -2.47 3.97 11 3 -4 1.22 3.34 11 -3 4 -0.33 2.71 11 -3 3 11.93 4.40 11 -3 3 1.13 3.05 11 3 -3 10.52 5.69 11 -3 3 9.62 3.41 11 -3 2 28.88 7.76 11 -3 2 27.72 5.99 11 3 -2 25.67 7.71 11 -3 2 26.05 5.84 11 -3 1 51.78 9.56 11 -3 1 49.38 8.98 11 3 -1 38.77 8.67 11 -3 1 33.94 7.03 11 3 0 30.80 7.21 11 -3 0 43.06 9.09 11 -3 0 34.95 7.25 11 3 0 24.43 6.54 11 3 1 36.61 7.81 11 -3 -1 48.87 8.68 11 3 1 41.38 8.05 11 3 2 26.48 6.76 11 3 2 36.95 6.24 11 -3 -2 30.60 6.46 11 3 2 24.54 6.60 11 3 3 6.23 3.69 11 3 3 16.99 4.25 11 -3 -3 7.46 3.17 11 3 3 4.99 2.97 11 3 4 1.00 1.67 11 3 4 0.49 1.90 11 -3 -4 -5.48 3.83 11 3 4 2.59 3.60 11 3 5 29.25 6.87 11 3 5 43.15 6.83 11 -3 -5 38.03 6.93 11 3 6 2.77 2.57 11 3 6 -0.58 1.62 11 -3 -6 -1.56 2.67 11 3 7 35.68 7.70 11 3 7 34.11 6.74 11 -3 -7 44.25 6.89 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10.49 4.43 11 -4 2 24.69 5.61 11 -4 2 14.88 5.24 11 4 -2 19.05 5.80 11 -4 2 21.55 6.08 11 -4 1 70.33 10.30 11 4 -1 68.09 10.43 11 -4 1 63.19 9.51 11 4 0 7.49 3.51 11 -4 0 10.72 4.30 11 4 0 13.95 5.61 11 -4 0 15.23 5.73 11 4 1 388.96 16.83 11 -4 -1 432.00 21.80 11 -4 -1 88.71 11.70 11 4 1 83.30 11.55 11 -4 -1 78.57 10.21 11 4 1 71.56 10.69 11 4 2 19.25 5.68 11 -4 -2 14.65 3.99 11 4 2 22.04 6.62 11 -4 -2 18.58 5.02 11 4 3 6.06 3.36 11 -4 -3 2.45 2.88 11 4 3 9.22 3.73 11 -4 -3 6.50 3.10 11 4 4 24.44 6.27 11 4 4 32.82 5.48 11 -4 -4 31.97 6.23 11 4 4 35.44 7.93 11 -4 -4 29.74 5.51 11 4 5 3.87 2.62 11 4 5 4.91 2.26 11 -4 -5 0.85 1.76 11 -4 -5 5.11 1.43 11 4 6 0.98 1.61 11 4 6 0.26 1.39 11 -4 -6 1.64 2.03 11 4 7 32.71 7.05 11 4 7 25.96 4.74 11 -4 -7 45.36 6.93 11 -4 -7 36.08 5.67 11 4 8 11.49 4.01 11 -4 -8 5.01 2.08 11 -4 -8 11.15 3.30 11 4 9 5.94 3.76 11 -4 -9 0.98 1.43 11 -4 -10 13.74 3.21 11 4 10 17.71 5.25 11 -4 -11 23.35 5.35 11 4 11 23.45 5.56 11 -4 -12 16.56 4.31 11 4 12 13.03 4.47 11 4 13 12.69 3.95 11 5 -12 21.17 4.37 11 5 -11 61.92 7.66 11 -5 10 16.90 3.29 11 -5 10 17.03 3.73 11 -5 9 20.38 3.73 11 5 -9 26.48 5.62 11 -5 9 14.82 3.72 11 -5 8 7.98 2.89 11 -5 8 13.60 3.59 11 -5 7 14.47 3.38 11 -5 7 13.24 3.25 11 -5 7 15.05 3.81 11 -5 6 18.75 3.95 11 -5 6 12.28 3.33 11 -5 5 2.30 1.88 11 -5 5 1.38 1.45 11 5 -5 6.37 3.74 11 -5 5 2.97 2.42 11 -5 4 19.90 4.26 11 -5 4 5.87 2.55 11 5 -4 14.46 5.36 11 -5 4 7.38 3.69 11 -5 3 59.78 7.30 11 -5 3 36.05 6.57 11 5 -3 45.84 8.32 11 -5 3 37.14 7.13 11 5 -2 35.75 7.45 11 -5 2 32.84 7.30 11 5 -1 51.95 8.94 11 -5 1 49.16 8.58 11 5 0 5.81 3.03 11 -5 0 6.44 3.88 11 5 1 34.25 7.23 11 5 1 58.59 9.55 11 -5 -1 53.30 8.76 11 5 2 28.51 6.89 11 -5 -2 27.32 6.23 11 5 3 22.06 5.94 11 -5 -3 34.20 6.33 11 5 4 12.17 4.14 11 -5 -4 9.88 3.12 11 -5 -4 9.66 3.27 11 5 5 -2.34 3.03 11 -5 -5 -5.35 3.60 11 -5 -5 1.56 2.12 11 5 6 18.17 5.39 11 -5 -6 23.19 5.00 11 -5 -6 16.11 4.04 11 5 7 12.22 3.94 11 -5 -7 17.13 4.18 11 -5 -7 14.09 3.51 11 5 8 8.26 3.93 11 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753.77 24.32 12 0 0 11.53 4.40 12 0 1 32.07 6.14 12 0 -1 29.89 5.89 12 0 2 37.13 6.76 12 0 -2 31.43 5.93 12 0 3 57.33 7.43 12 0 3 59.27 7.94 12 0 4 47.82 7.02 12 0 -4 77.05 8.37 12 0 5 9.06 3.33 12 0 -5 56.84 7.49 12 0 6 12.81 4.11 12 0 7 49.17 6.99 12 0 8 43.16 5.77 12 0 9 3.05 2.10 12 -1 9 4.95 1.79 12 -1 8 11.07 3.42 12 -1 7 36.67 5.86 12 -1 6 22.19 4.39 12 1 -6 11.42 2.84 12 -1 5 10.90 3.37 12 1 -5 3.11 2.25 12 -1 4 33.68 6.38 12 1 -4 16.26 3.67 12 -1 3 63.23 7.80 12 -1 3 52.61 7.10 12 -1 2 41.95 6.52 12 1 -2 15.58 3.48 12 -1 1 333.49 16.77 12 -1 1 4.92 2.68 12 -1 0 821.22 25.68 12 -1 0 30.66 5.54 12 1 1 482.99 19.16 12 -1 -1 9.11 3.38 12 1 2 252.79 14.22 12 -1 -2 51.29 7.02 12 1 3 113.43 9.69 12 -1 -3 52.04 6.79 12 1 4 60.03 7.16 12 -1 -4 51.65 6.78 12 1 5 15.42 3.77 12 -1 -5 14.04 3.57 12 1 6 21.10 4.22 12 -1 -6 46.46 6.05 12 1 7 54.99 6.58 12 1 8 5.34 2.46 12 1 9 12.85 3.14 12 -2 9 20.22 3.44 12 -2 8 17.53 3.44 12 -2 7 6.42 2.34 12 2 -7 -0.07 1.02 12 -2 6 2.14 1.80 12 2 -6 0.15 1.55 12 -2 5 22.74 4.24 12 -2 5 26.03 4.40 12 2 -5 11.72 3.30 12 -2 4 14.77 4.05 12 -2 4 7.86 2.78 12 -2 3 21.20 4.43 12 2 -3 10.27 3.32 12 -2 2 6.37 2.61 12 2 -2 3.75 2.80 12 -2 1 38.77 6.18 12 2 -1 22.16 4.61 12 -2 0 49.14 6.91 12 2 0 29.92 5.26 12 -2 -1 36.80 6.00 12 2 2 508.28 18.41 12 -2 -2 8.58 3.32 12 2 3 274.40 13.55 12 -2 -3 21.05 4.47 12 2 4 112.30 8.80 12 -2 -4 1.33 1.53 12 2 5 74.58 7.18 12 -2 -5 26.78 4.60 12 2 6 17.60 3.69 12 -2 -6 5.00 2.43 12 2 7 19.41 3.58 12 -2 -7 13.27 3.09 12 -3 7 4.56 1.75 12 3 -7 3.47 2.24 12 -3 6 13.97 3.07 12 3 -6 8.48 2.63 12 -3 5 3.72 1.90 12 3 -5 4.75 2.38 12 -3 4 9.69 2.84 12 3 -4 9.78 3.52 12 -3 3 27.18 4.66 12 3 -3 21.95 4.79 12 -3 2 12.75 3.44 12 3 -2 18.21 4.41 12 -3 1 24.55 4.95 12 3 -1 20.55 4.59 12 -3 0 27.47 5.15 12 3 0 25.99 5.11 12 -3 -1 26.42 4.94 12 -3 -2 23.42 4.60 12 -3 -3 45.47 6.28 12 3 3 26.49 5.57 12 -3 -4 17.70 3.86 12 3 4 13.33 3.84 12 -3 -5 7.05 2.49 12 3 5 5.47 2.78 12 -3 -6 13.94 3.03 12 3 6 18.18 4.43 12 4 -6 15.79 3.66 12 -4 5 186.13 8.87 12 4 -5 6.66 2.94 12 -4 4 26.75 4.22 12 4 -4 46.98 6.49 12 -4 3 10.55 2.76 12 4 -3 15.41 4.07 12 -4 2 8.02 2.51 12 4 -2 11.11 3.71 12 -4 1 17.60 3.97 12 4 -1 24.87 5.17 12 -4 0 8.29 2.65 12 4 0 16.66 4.36 12 -4 -1 25.37 4.57 12 -4 -2 7.00 2.37 12 -4 -3 15.39 3.48 12 -4 -4 58.15 6.55 12 -4 -5 8.51 2.45 12 5 -4 20.25 4.29 12 5 -3 3.47 2.53 12 -5 2 2.16 0.97 12 5 -2 9.29 3.05 12 -5 1 0.93 0.87 12 5 -1 4.70 2.01 12 -5 0 1.96 1.68 12 -5 -1 0.81 0.90 12 -5 -2 0.53 0.96 12 -5 -3 0.22 0.74 0 0 0 0.00 0.00 TITL exp_1494 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 10.203858 13.707818 24.744746 90.0000 90.0000 90.0000 ZERR 15.00 0.000238 0.000487 0.000662 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 165.00 150.00 15.00 15.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 3642 _shelx_fab_file ; -12 -5 -4 0.0097 -0.3461 -12 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8.8025 12 2 2 7.9024 -6.3563 12 2 3 -2.2023 0.1064 12 2 4 1.7206 0.2716 12 2 5 -0.5673 -2.0015 12 2 6 0.0360 0.2071 12 2 7 -2.6813 -0.8061 12 3 0 -1.1690 0.0017 12 3 1 4.8970 3.2544 12 3 2 -0.7615 -2.8831 12 3 3 4.0498 1.4391 12 3 4 1.2653 -0.8280 12 3 5 -1.0002 -0.8479 12 3 6 1.5768 -1.7191 12 4 0 0.0887 -0.0428 12 4 1 1.3185 3.4443 12 4 2 -0.1642 3.9987 12 4 3 1.4524 0.4465 12 4 4 1.3115 1.5628 12 4 5 0.3152 0.7920 12 5 0 -3.6587 -0.0135 12 5 1 -0.4949 0.0767 12 5 2 -1.6378 1.1942 12 5 3 -1.0881 0.7436 0 0 0 0.0 0.0 ; _shelx_fab_checksum 35521 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.1660(6) 0.5542(6) 0.7800(2) 0.0290(14) Uani 1 1 d . . . . . C2 C 0.0637(7) 0.5692(6) 0.8217(3) 0.0358(16) Uani 1 1 d . . . . . H2 H 0.076723 0.618593 0.846914 0.043 Uiso 1 1 calc R U . . . C3 C -0.0444(7) 0.5172(6) 0.8253(3) 0.0332(15) Uani 1 1 d . . . . . H3 H -0.102367 0.531088 0.853266 0.040 Uiso 1 1 calc R U . . . C4 C -0.0798(7) 0.4359(6) 0.7864(3) 0.0346(15) Uani 1 1 d . . . . . C5 C 0.0169(6) 0.4312(5) 0.7378(2) 0.0279(13) Uani 1 1 d . . . . . H5 H -0.011985 0.482342 0.712779 0.033 Uiso 1 1 calc R U . . . C6 C 0.0043(6) 0.3368(5) 0.7069(2) 0.0264(12) Uani 1 1 d . . . . . H6A H -0.087609 0.324618 0.699506 0.032 Uiso 1 1 calc R U . . . H6B H 0.036399 0.283793 0.729239 0.032 Uiso 1 1 calc R U . . . C7 C 0.0795(6) 0.3370(5) 0.6536(3) 0.0251(12) Uani 1 1 d . . . . . H7 H 0.077977 0.270666 0.638871 0.030 Uiso 1 1 calc R U . . . C8 C 0.2216(6) 0.3681(5) 0.6595(2) 0.0253(13) Uani 1 1 d . . . . . C9 C 0.2340(6) 0.4624(5) 0.6950(2) 0.0238(12) Uani 1 1 d . . . . . H9 H 0.184484 0.511995 0.675061 0.029 Uiso 1 1 calc R U . . . C10 C 0.1625(6) 0.4552(5) 0.7509(2) 0.0266(13) Uani 1 1 d . . . . . C11 C 0.3765(6) 0.5012(5) 0.6953(2) 0.0255(13) Uani 1 1 d . . . . . H11 H 0.409542 0.501020 0.732488 0.031 Uiso 1 1 calc R U . . . C12 C 0.4739(6) 0.4467(5) 0.6590(2) 0.0259(12) Uani 1 1 d . . . . . H12A H 0.498261 0.386362 0.676795 0.031 Uiso 1 1 calc R U . . . H12B H 0.552518 0.486013 0.655664 0.031 Uiso 1 1 calc R U . . . C13 C 0.4236(6) 0.4218(5) 0.6009(3) 0.0283(14) Uani 1 1 d . . . . . C14 C 0.2779(7) 0.3973(5) 0.6045(2) 0.0262(13) Uani 1 1 d . . . . . C15 C 0.1956(7) 0.4084(5) 0.5626(3) 0.0283(14) Uani 1 1 d . . . . . H15 H 0.230922 0.413436 0.528070 0.034 Uiso 1 1 calc R U . . . C16 C 0.0551(7) 0.4131(5) 0.5685(2) 0.0285(13) Uani 1 1 d . . . . . C17 C 0.5006(7) 0.3323(5) 0.5810(2) 0.0274(13) Uani 1 1 d . . . . . H17 H 0.480868 0.276792 0.604605 0.033 Uiso 1 1 calc R U . . . C18 C 0.4458(7) 0.5100(5) 0.5634(3) 0.0301(14) Uani 1 1 d . . . . . H18A H 0.537452 0.525520 0.562404 0.045 Uiso 1 1 calc R U . . . H18B H 0.397590 0.565017 0.576847 0.045 Uiso 1 1 calc R U . . . H18C H 0.416055 0.494321 0.527634 0.045 Uiso 1 1 calc R U . . . C19 C 0.2270(7) 0.3837(6) 0.7907(2) 0.0313(15) Uani 1 1 d . . . . . H19A H 0.320555 0.386976 0.786865 0.047 Uiso 1 1 calc R U . . . H19B H 0.197784 0.318571 0.783030 0.047 Uiso 1 1 calc R U . . . H19C H 0.203104 0.400853 0.826976 0.047 Uiso 1 1 calc R U . . . C20 C 0.6514(6) 0.3451(5) 0.5777(2) 0.0242(12) Uani 1 1 d . . . . . H20 H 0.676904 0.407689 0.593736 0.029 Uiso 1 1 calc R U . . . C21 C 0.7209(6) 0.2617(5) 0.6067(3) 0.0285(13) Uani 1 1 d . . . . . H21A H 0.693125 0.199273 0.592331 0.034 Uiso 1 1 calc R U . . . H21B H 0.815156 0.267372 0.602638 0.034 Uiso 1 1 calc R U . . . C22 C 0.6814(7) 0.3452(6) 0.5166(3) 0.0304(14) Uani 1 1 d . . . . . H22A H 0.713674 0.408576 0.505287 0.037 Uiso 1 1 calc R U . . . H22B H 0.746766 0.296304 0.507979 0.037 Uiso 1 1 calc R U . . . C23 C 0.5545(7) 0.3224(6) 0.4895(3) 0.0310(14) Uani 1 1 d . . . . . C28 C -0.2187(7) 0.4617(6) 0.7645(3) 0.0390(17) Uani 1 1 d . . . . . H28A H -0.246189 0.413211 0.738277 0.047 Uiso 1 1 calc R U . . . H28B H -0.281434 0.461767 0.793979 0.047 Uiso 1 1 calc R U . . . C29 C -0.0915(8) 0.3423(7) 0.8182(3) 0.0389(17) Uani 1 1 d . . . . . H29A H -0.133732 0.293665 0.796374 0.058 Uiso 1 1 calc R U . . . H29B H -0.142409 0.353808 0.850140 0.058 Uiso 1 1 calc R U . . . H29C H -0.005648 0.320013 0.828169 0.058 Uiso 1 1 calc R U . . . C30 C 0.2900(7) 0.2742(5) 0.6798(3) 0.0282(14) Uani 1 1 d . . . . . H30A H 0.235277 0.242523 0.706064 0.042 Uiso 1 1 calc R U . . . H30B H 0.372441 0.290763 0.696049 0.042 Uiso 1 1 calc R U . . . H30C H 0.304557 0.230922 0.649884 0.042 Uiso 1 1 calc R U . . . C31 C 0.4573(7) 0.6636(5) 0.6968(3) 0.0310(14) Uani 1 1 d . . . . . C32 C 0.4442(8) 0.7626(6) 0.6726(4) 0.047(2) Uani 1 1 d . . . . . H32A H 0.362558 0.767015 0.653552 0.071 Uiso 1 1 calc R U . . . H32B H 0.515332 0.773819 0.648016 0.071 Uiso 1 1 calc R U . . . H32C H 0.446368 0.810694 0.700815 0.071 Uiso 1 1 calc R U . . . O1 O 0.2491(5) 0.6137(4) 0.7727(2) 0.0340(11) Uani 1 1 d . . . . . O2 O -0.2148(5) 0.5546(5) 0.7401(2) 0.0443(13) Uani 1 1 d . . . . . H2A H -0.257747 0.593164 0.758165 0.066 Uiso 1 1 calc R U . . . O3 O 0.0025(4) 0.3998(4) 0.61785(17) 0.0280(9) Uani 1 1 d . . . . . O4 O -0.0199(5) 0.4389(4) 0.53240(19) 0.0349(11) Uani 1 1 d . . . . . O5 O 0.3717(5) 0.6006(4) 0.67583(18) 0.0289(10) Uani 1 1 d . . . . . O6 O 0.5392(5) 0.6412(4) 0.7295(2) 0.0387(12) Uani 1 1 d . . . . . O7 O 0.6842(5) 0.2706(4) 0.66260(19) 0.0320(11) Uani 1 1 d . . . . . H7A H 0.698094 0.218826 0.678164 0.048 Uiso 1 1 calc R U . . . O8 O 0.4578(5) 0.3092(4) 0.52630(18) 0.0305(10) Uani 1 1 d . . . . . O9 O 0.5312(5) 0.3176(4) 0.44198(19) 0.0392(12) Uani 1 1 d . . . . . Cl4 Cl -0.1593(2) 0.55471(17) 0.42720(7) 0.0453(5) Uani 1 1 d . . . . . Cl5 Cl 0.1233(2) 0.5681(2) 0.42956(8) 0.0551(6) Uani 1 1 d . . . . . Cl6 Cl -0.00316(18) 0.44271(14) 0.35147(7) 0.0394(4) Uani 1 1 d . . . . . C2S C -0.0105(8) 0.4917(6) 0.4174(3) 0.0372(16) Uani 1 1 d . . . . . H2S H -0.007007 0.437547 0.443205 0.045 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.030(3) 0.044(4) 0.013(3) -0.002(3) -0.008(2) 0.002(3) C2 0.036(4) 0.046(4) 0.026(3) -0.011(3) 0.001(3) 0.003(3) C3 0.036(3) 0.045(4) 0.018(3) -0.007(3) 0.002(3) -0.004(3) C4 0.034(3) 0.045(4) 0.025(3) -0.009(3) 0.005(3) -0.005(3) C5 0.031(3) 0.037(3) 0.016(3) 0.002(2) 0.002(2) -0.003(3) C6 0.024(3) 0.039(3) 0.017(3) -0.002(2) 0.004(2) -0.003(3) C7 0.026(3) 0.033(3) 0.016(3) -0.001(2) 0.000(2) 0.000(2) C8 0.029(3) 0.031(3) 0.015(3) -0.008(2) -0.002(2) 0.001(2) C9 0.029(3) 0.026(3) 0.016(3) -0.004(2) 0.001(2) 0.006(2) C10 0.031(3) 0.034(3) 0.015(3) 0.001(3) -0.001(2) 0.002(3) C11 0.029(3) 0.032(3) 0.015(3) -0.005(2) -0.003(2) 0.003(3) C12 0.027(3) 0.038(3) 0.013(3) -0.005(2) -0.004(2) 0.001(3) C13 0.026(3) 0.040(4) 0.020(3) -0.003(3) 0.000(2) -0.005(3) C14 0.037(3) 0.028(3) 0.013(3) -0.005(2) -0.004(2) -0.006(3) C15 0.033(3) 0.040(4) 0.012(3) -0.001(2) 0.000(2) 0.002(3) C16 0.034(3) 0.039(3) 0.013(3) -0.005(2) -0.005(2) -0.001(3) C17 0.030(3) 0.040(3) 0.013(3) 0.003(2) -0.003(2) 0.002(3) C18 0.033(3) 0.041(4) 0.017(3) -0.001(3) 0.003(3) 0.003(3) C19 0.035(3) 0.049(4) 0.011(3) 0.005(3) -0.001(2) 0.001(3) C20 0.024(3) 0.036(3) 0.013(3) -0.003(2) -0.002(2) 0.001(2) C21 0.024(3) 0.034(3) 0.028(3) 0.001(3) -0.003(2) -0.001(2) C22 0.030(3) 0.041(4) 0.021(3) 0.003(3) -0.001(2) 0.002(3) C23 0.031(3) 0.041(4) 0.021(3) -0.002(3) 0.003(3) 0.011(3) C28 0.032(3) 0.052(5) 0.033(4) -0.015(3) 0.002(3) -0.004(3) C29 0.044(4) 0.056(5) 0.017(3) -0.002(3) 0.004(3) 0.004(4) C30 0.031(3) 0.036(4) 0.017(3) -0.002(3) 0.005(2) 0.000(3) C31 0.025(3) 0.036(4) 0.032(3) -0.008(3) 0.002(3) 0.000(3) C32 0.034(4) 0.041(4) 0.066(6) 0.009(4) -0.003(4) -0.003(3) O1 0.035(3) 0.041(3) 0.026(2) -0.009(2) 0.0025(19) -0.003(2) O2 0.029(2) 0.059(4) 0.045(3) 0.002(3) 0.008(2) 0.006(2) O3 0.025(2) 0.042(2) 0.017(2) 0.0003(18) -0.0026(17) 0.003(2) O4 0.032(2) 0.053(3) 0.019(2) 0.002(2) -0.0032(18) 0.001(2) O5 0.026(2) 0.039(3) 0.021(2) -0.0024(19) -0.0032(18) -0.0012(19) O6 0.036(3) 0.047(3) 0.033(3) -0.007(2) -0.009(2) 0.001(2) O7 0.037(3) 0.040(3) 0.019(2) 0.0026(19) -0.0008(19) 0.002(2) O8 0.031(2) 0.046(3) 0.014(2) -0.0099(19) -0.0003(17) -0.001(2) O9 0.040(3) 0.062(3) 0.015(2) -0.010(2) 0.0010(19) 0.002(2) Cl4 0.0486(10) 0.0629(12) 0.0245(8) 0.0060(8) 0.0021(7) 0.0087(9) Cl5 0.0506(11) 0.0886(17) 0.0262(9) 0.0026(10) -0.0061(8) -0.0239(11) Cl6 0.0456(9) 0.0496(9) 0.0231(8) 0.0025(7) -0.0022(7) 0.0021(8) C2S 0.036(4) 0.055(4) 0.021(3) 0.011(3) -0.002(3) 0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 C10 115.6(6) . . ? O1 C1 C2 120.8(7) . . ? O1 C1 C10 123.4(6) . . ? C1 C2 H2 117.9 . . ? C3 C2 C1 124.2(7) . . ? C3 C2 H2 117.9 . . ? C2 C3 H3 118.2 . . ? C2 C3 C4 123.7(6) . . ? C4 C3 H3 118.2 . . ? C3 C4 C5 111.7(6) . . ? C3 C4 C28 105.7(6) . . ? C5 C4 C28 108.5(6) . . ? C29 C4 C3 108.2(6) . . ? C29 C4 C5 114.7(6) . . ? C29 C4 C28 107.6(6) . . ? C4 C5 H5 105.5 . . ? C6 C5 C4 111.9(5) . . ? C6 C5 H5 105.5 . . ? C6 C5 C10 111.6(5) . . ? C10 C5 C4 115.8(5) . . ? C10 C5 H5 105.5 . . ? C5 C6 H6A 108.9 . . ? C5 C6 H6B 108.9 . . ? C5 C6 C7 113.2(5) . . ? H6A C6 H6B 107.8 . . ? C7 C6 H6A 108.9 . . ? C7 C6 H6B 108.9 . . ? C6 C7 H7 108.2 . . ? C8 C7 C6 113.5(5) . . ? C8 C7 H7 108.2 . . ? O3 C7 C6 104.7(5) . . ? O3 C7 H7 108.2 . . ? O3 C7 C8 113.9(5) . . ? C7 C8 C9 111.2(5) . . ? C7 C8 C14 110.2(5) . . ? C7 C8 C30 103.2(5) . . ? C14 C8 C9 104.6(5) . . ? C14 C8 C30 109.7(5) . . ? C30 C8 C9 117.9(5) . . ? C8 C9 H9 104.4 . . ? C8 C9 C10 113.9(5) . . ? C10 C9 H9 104.4 . . ? C11 C9 C8 111.2(5) . . ? C11 C9 H9 104.4 . . ? C11 C9 C10 117.0(5) . . ? C1 C10 C5 107.9(5) . . ? C1 C10 C9 110.3(5) . . ? C1 C10 C19 104.7(5) . . ? C5 C10 C9 105.8(5) . . ? C19 C10 C5 114.1(6) . . ? C19 C10 C9 113.9(5) . . ? C9 C11 H11 109.1 . . ? C12 C11 C9 116.0(5) . . ? C12 C11 H11 109.1 . . ? O5 C11 C9 106.8(5) . . ? O5 C11 H11 109.1 . . ? O5 C11 C12 106.6(5) . . ? C11 C12 H12A 108.4 . . ? C11 C12 H12B 108.4 . . ? C11 C12 C13 115.6(5) . . ? H12A C12 H12B 107.4 . . ? C13 C12 H12A 108.4 . . ? C13 C12 H12B 108.4 . . ? C14 C13 C12 108.2(5) . . ? C14 C13 C17 110.0(6) . . ? C14 C13 C18 110.6(6) . . ? C17 C13 C12 107.5(5) . . ? C17 C13 C18 111.0(5) . . ? C18 C13 C12 109.5(6) . . ? C8 C14 C13 118.4(5) . . ? C15 C14 C8 118.8(6) . . ? C15 C14 C13 122.5(6) . . ? C14 C15 H15 118.4 . . ? C14 C15 C16 123.2(6) . . ? C16 C15 H15 118.4 . . ? O3 C16 C15 118.8(6) . . ? O4 C16 C15 123.9(6) . . ? O4 C16 O3 116.8(6) . . ? C13 C17 H17 108.9 . . ? C13 C17 C20 115.7(6) . . ? C20 C17 H17 108.9 . . ? O8 C17 C13 108.5(5) . . ? O8 C17 H17 108.9 . . ? O8 C17 C20 105.9(5) . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C10 C19 H19A 109.5 . . ? C10 C19 H19B 109.5 . . ? C10 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C17 C20 H20 110.0 . . ? C21 C20 C17 110.6(5) . . ? C21 C20 H20 110.0 . . ? C21 C20 C22 111.7(5) . . ? C22 C20 C17 104.4(5) . . ? C22 C20 H20 110.0 . . ? C20 C21 H21A 110.6 . . ? C20 C21 H21B 110.6 . . ? H21A C21 H21B 108.8 . . ? O7 C21 C20 105.5(5) . . ? O7 C21 H21A 110.6 . . ? O7 C21 H21B 110.6 . . ? C20 C22 H22A 110.6 . . ? C20 C22 H22B 110.6 . . ? H22A C22 H22B 108.8 . . ? C23 C22 C20 105.5(5) . . ? C23 C22 H22A 110.6 . . ? C23 C22 H22B 110.6 . . ? O8 C23 C22 111.0(6) . . ? O9 C23 C22 128.5(7) . . ? O9 C23 O8 120.4(7) . . ? C4 C28 H28A 109.9 . . ? C4 C28 H28B 109.9 . . ? H28A C28 H28B 108.3 . . ? O2 C28 C4 109.1(6) . . ? O2 C28 H28A 109.9 . . ? O2 C28 H28B 109.9 . . ? C4 C29 H29A 109.5 . . ? C4 C29 H29B 109.5 . . ? C4 C29 H29C 109.5 . . ? H29A C29 H29B 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C8 C30 H30A 109.5 . . ? C8 C30 H30B 109.5 . . ? C8 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? O5 C31 C32 112.0(6) . . ? O6 C31 C32 124.4(7) . . ? O6 C31 O5 123.5(7) . . ? C31 C32 H32A 109.5 . . ? C31 C32 H32B 109.5 . . ? C31 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C28 O2 H2A 109.5 . . ? C16 O3 C7 114.5(5) . . ? C31 O5 C11 117.3(5) . . ? C21 O7 H7A 109.5 . . ? C23 O8 C17 112.1(5) . . ? Cl4 C2S Cl6 110.5(4) . . ? Cl4 C2S H2S 108.2 . . ? Cl5 C2S Cl4 110.8(5) . . ? Cl5 C2S Cl6 110.7(4) . . ? Cl5 C2S H2S 108.2 . . ? Cl6 C2S H2S 108.2 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.481(10) . ? C1 C10 1.537(10) . ? C1 O1 1.191(9) . ? C2 H2 0.9300 . ? C2 C3 1.317(11) . ? C3 H3 0.9300 . ? C3 C4 1.517(10) . ? C4 C5 1.556(9) . ? C4 C28 1.558(11) . ? C4 C29 1.509(12) . ? C5 H5 0.9800 . ? C5 C6 1.509(9) . ? C5 C10 1.556(9) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 C7 1.525(8) . ? C7 H7 0.9800 . ? C7 C8 1.518(9) . ? C7 O3 1.463(8) . ? C8 C9 1.568(8) . ? C8 C14 1.530(9) . ? C8 C30 1.548(10) . ? C9 H9 0.9800 . ? C9 C10 1.568(8) . ? C9 C11 1.549(9) . ? C10 C19 1.537(9) . ? C11 H11 0.9800 . ? C11 C12 1.533(9) . ? C11 O5 1.447(8) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C12 C13 1.564(8) . ? C13 C14 1.527(9) . ? C13 C17 1.538(10) . ? C13 C18 1.540(10) . ? C14 C15 1.344(9) . ? C15 H15 0.9300 . ? C15 C16 1.442(10) . ? C16 O3 1.345(8) . ? C16 O4 1.229(8) . ? C17 H17 0.9800 . ? C17 C20 1.550(9) . ? C17 O8 1.457(7) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C20 H20 0.9800 . ? C20 C21 1.525(9) . ? C20 C22 1.543(9) . ? C21 H21A 0.9700 . ? C21 H21B 0.9700 . ? C21 O7 1.437(8) . ? C22 H22A 0.9700 . ? C22 H22B 0.9700 . ? C22 C23 1.491(10) . ? C23 O8 1.354(9) . ? C23 O9 1.203(9) . ? C28 H28A 0.9700 . ? C28 H28B 0.9700 . ? C28 O2 1.410(11) . ? C29 H29A 0.9600 . ? C29 H29B 0.9600 . ? C29 H29C 0.9600 . ? C30 H30A 0.9600 . ? C30 H30B 0.9600 . ? C30 H30C 0.9600 . ? C31 C32 1.489(11) . ? C31 O5 1.333(9) . ? C31 O6 1.204(9) . ? C32 H32A 0.9600 . ? C32 H32B 0.9600 . ? C32 H32C 0.9600 . ? O2 H2A 0.8200 . ? O7 H7A 0.8200 . ? Cl4 C2S 1.763(8) . ? Cl5 C2S 1.748(8) . ? Cl6 C2S 1.765(8) . ? C2S H2S 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 C2 C3 C4 -1.2(12) . . . . ? C2 C1 C10 C5 42.7(7) . . . . ? C2 C1 C10 C9 157.9(6) . . . . ? C2 C1 C10 C19 -79.2(7) . . . . ? C2 C3 C4 C5 -7.8(11) . . . . ? C2 C3 C4 C28 -125.6(8) . . . . ? C2 C3 C4 C29 119.4(8) . . . . ? C3 C4 C5 C6 165.5(6) . . . . ? C3 C4 C5 C10 36.1(9) . . . . ? C3 C4 C28 O2 57.7(7) . . . . ? C4 C5 C6 C7 169.8(6) . . . . ? C4 C5 C10 C1 -52.9(8) . . . . ? C4 C5 C10 C9 -171.0(6) . . . . ? C4 C5 C10 C19 62.9(8) . . . . ? C5 C4 C28 O2 -62.3(8) . . . . ? C5 C6 C7 C8 51.3(7) . . . . ? C5 C6 C7 O3 -73.5(6) . . . . ? C6 C5 C10 C1 177.5(5) . . . . ? C6 C5 C10 C9 59.5(6) . . . . ? C6 C5 C10 C19 -66.6(7) . . . . ? C6 C7 C8 C9 -46.8(7) . . . . ? C6 C7 C8 C14 -162.3(6) . . . . ? C6 C7 C8 C30 80.6(6) . . . . ? C6 C7 O3 C16 177.6(5) . . . . ? C7 C8 C9 C10 52.1(7) . . . . ? C7 C8 C9 C11 -173.1(5) . . . . ? C7 C8 C14 C13 -174.3(6) . . . . ? C7 C8 C14 C15 11.3(8) . . . . ? C8 C7 O3 C16 53.1(7) . . . . ? C8 C9 C10 C1 -173.5(5) . . . . ? C8 C9 C10 C5 -57.1(7) . . . . ? C8 C9 C10 C19 69.2(7) . . . . ? C8 C9 C11 C12 4.1(8) . . . . ? C8 C9 C11 O5 122.8(5) . . . . ? C8 C14 C15 C16 12.4(11) . . . . ? C9 C8 C14 C13 66.0(7) . . . . ? C9 C8 C14 C15 -108.4(7) . . . . ? C9 C11 C12 C13 44.6(8) . . . . ? C9 C11 O5 C31 146.2(5) . . . . ? C10 C1 C2 C3 -18.0(10) . . . . ? C10 C5 C6 C7 -58.6(7) . . . . ? C10 C9 C11 C12 137.3(6) . . . . ? C10 C9 C11 O5 -104.0(6) . . . . ? C11 C9 C10 C1 54.5(7) . . . . ? C11 C9 C10 C5 170.9(5) . . . . ? C11 C9 C10 C19 -62.8(8) . . . . ? C11 C12 C13 C14 -35.9(8) . . . . ? C11 C12 C13 C17 -154.6(6) . . . . ? C11 C12 C13 C18 84.7(7) . . . . ? C12 C11 O5 C31 -89.2(6) . . . . ? C12 C13 C14 C8 -19.8(8) . . . . ? C12 C13 C14 C15 154.3(7) . . . . ? C12 C13 C17 C20 -59.8(7) . . . . ? C12 C13 C17 O8 -178.5(5) . . . . ? C13 C14 C15 C16 -161.7(7) . . . . ? C13 C17 C20 C21 129.2(6) . . . . ? C13 C17 C20 C22 -110.5(6) . . . . ? C13 C17 O8 C23 114.3(6) . . . . ? C14 C8 C9 C10 171.1(5) . . . . ? C14 C8 C9 C11 -54.1(7) . . . . ? C14 C13 C17 C20 -177.4(5) . . . . ? C14 C13 C17 O8 63.9(6) . . . . ? C14 C15 C16 O3 -4.1(11) . . . . ? C14 C15 C16 O4 167.7(7) . . . . ? C15 C16 O3 C7 -28.9(9) . . . . ? C17 C13 C14 C8 97.3(7) . . . . ? C17 C13 C14 C15 -88.6(8) . . . . ? C17 C20 C21 O7 -64.1(6) . . . . ? C17 C20 C22 C23 -5.9(7) . . . . ? C18 C13 C14 C8 -139.7(6) . . . . ? C18 C13 C14 C15 34.4(9) . . . . ? C18 C13 C17 C20 59.9(7) . . . . ? C18 C13 C17 O8 -58.8(7) . . . . ? C20 C17 O8 C23 -10.5(7) . . . . ? C20 C22 C23 O8 -0.2(8) . . . . ? C20 C22 C23 O9 177.8(8) . . . . ? C21 C20 C22 C23 113.7(6) . . . . ? C22 C20 C21 O7 -179.9(5) . . . . ? C22 C23 O8 C17 6.8(8) . . . . ? C28 C4 C5 C6 -78.4(7) . . . . ? C28 C4 C5 C10 152.2(6) . . . . ? C29 C4 C5 C6 41.9(8) . . . . ? C29 C4 C5 C10 -87.5(8) . . . . ? C29 C4 C28 O2 173.1(6) . . . . ? C30 C8 C9 C10 -66.8(7) . . . . ? C30 C8 C9 C11 68.0(7) . . . . ? C30 C8 C14 C13 -61.4(8) . . . . ? C30 C8 C14 C15 124.3(7) . . . . ? C32 C31 O5 C11 178.8(6) . . . . ? O1 C1 C2 C3 166.4(8) . . . . ? O1 C1 C10 C5 -141.8(6) . . . . ? O1 C1 C10 C9 -26.6(8) . . . . ? O1 C1 C10 C19 96.3(7) . . . . ? O3 C7 C8 C9 72.9(7) . . . . ? O3 C7 C8 C14 -42.7(7) . . . . ? O3 C7 C8 C30 -159.7(5) . . . . ? O4 C16 O3 C7 158.7(6) . . . . ? O5 C11 C12 C13 -74.2(7) . . . . ? O6 C31 O5 C11 2.0(9) . . . . ? O8 C17 C20 C21 -110.7(6) . . . . ? O8 C17 C20 C22 9.6(7) . . . . ? O9 C23 O8 C17 -171.3(7) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.326 -0.250 0.500 369.5 173.3 ? 2 -0.386 0.250 1.000 369.5 173.7 ?