#------------------------------------------------------------------------------ #$Date: 2020-04-23 23:23:41 +0300 (Thu, 23 Apr 2020) $ #$Revision: 251097 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/78/1557882.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557882 loop_ _publ_author_name 'Sun, Changli' 'Liu, Zhiyong' 'Zhu, Xiangcheng' 'Fan, Zhiying' 'Huang, Xuanmei' 'Wu, Qiaoling' 'Zheng, Xiaohong' 'Qin, Xiangjing' 'Zhang, Tianyu' 'Zhang, Hua' 'Ju, Jianhua' 'Ma, Junying' _publ_section_title ; Antitubercular Ilamycins from Marine-Derived Streptomyces atratus SCSIO ZH16 \DilaR ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.0c00151 _journal_year 2020 _chemical_absolute_configuration rm _chemical_formula_moiety 'C54 H75 N9 O13' _chemical_formula_sum 'C54 H75 N9 O13' _chemical_formula_weight 1058.23 _space_group_crystal_system orthorhombic _space_group_IT_number 18 _space_group_name_Hall 'P 2 2ab' _space_group_name_H-M_alt 'P 21 21 2' _atom_sites_solution_hydrogens mixed _audit_creation_date 2020-02-08 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 31.3214(9) _cell_length_b 17.9026(7) _cell_length_c 12.6750(6) _cell_measurement_reflns_used 10911 _cell_measurement_temperature 100(6) _cell_measurement_theta_max 72.0380 _cell_measurement_theta_min 3.7450 _cell_volume 7107.3(5) _computing_cell_refinement 'CrysAlisPro 1.171.39.33c (Rigaku OD, 2017)' _computing_data_collection 'CrysAlisPro 1.171.39.33c (Rigaku OD, 2017)' _computing_data_reduction 'CrysAlisPro 1.171.39.33c (Rigaku OD, 2017)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(6) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 105.00 135.00 0.30 6.59 -- 45.70 82.00 -90.00 100 2 \w 87.00 135.00 0.30 6.59 -- 45.70 82.00 90.00 160 3 \w 100.00 134.20 0.30 6.59 -- 45.70 57.00 -60.00 114 4 \w 23.00 92.30 0.30 6.59 -- 45.70 57.00 -60.00 231 5 \w 85.00 126.10 0.30 6.59 -- 45.70 77.00 0.00 137 6 \w 87.00 121.20 0.30 6.59 -- 45.70 82.00 60.00 114 7 \w 84.00 130.20 0.30 6.59 -- 45.70 77.00-120.00 154 8 \w 18.00 125.40 0.30 26.35 -- 100.10 -82.00 -30.00 358 9 \w 76.00 170.20 0.30 26.35 -- 100.10 61.00 -30.00 314 10 \w 36.00 79.20 0.30 26.35 -- 100.10 -61.00 0.00 144 11 \w 87.00 175.20 0.30 26.35 -- 100.10 61.00 150.00 294 12 \w 73.00 186.40 0.30 26.35 -- 100.10 61.00 -90.00 378 13 \w 105.00 131.10 0.30 26.35 -- 100.10 -61.00 0.00 87 14 \w 72.00 181.20 0.30 26.35 -- 100.10 61.00-150.00 364 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC12 (RINC): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0268071000 _diffrn_orient_matrix_UB_12 0.0456464000 _diffrn_orient_matrix_UB_13 -0.0789746000 _diffrn_orient_matrix_UB_21 -0.0412609000 _diffrn_orient_matrix_UB_22 -0.0301204000 _diffrn_orient_matrix_UB_23 0.0508640000 _diffrn_orient_matrix_UB_31 -0.0002723000 _diffrn_orient_matrix_UB_32 0.0665882000 _diffrn_orient_matrix_UB_33 0.0768027000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0651 _diffrn_reflns_av_unetI/netI 0.0677 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -37 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 34009 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_theta_full 67.080 _diffrn_reflns_theta_max 67.080 _diffrn_reflns_theta_min 3.487 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.586 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.09811 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.33c (Rigaku Oxford Diffraction, 2017) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 0.989 _exptl_crystal_description plate _exptl_crystal_F_000 2264 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _platon_squeeze_details ; TITL sunchangliP 21 21 2llecR = 0.18 CELL 31.3214 17.9026 12.6750 90.00 90.00 90.00 SPGR P21212 # Solvent Accessible Volume = 1995 # Electrons Found in S.A.V. = 603 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others Q101 0.263 0.440 0.187 ! 7.27 eA-3 C102 0.121 0.471 0.421 ! 6.90 eA-3 C103 0.555 0.528 0.397 ! 5.67 eA-3 C104 0.013 0.965 0.738 ! 4.72 eA-3 C105 0.757 0.059 0.927 ! 4.71 eA-3 C106 0.500 0.501 0.563 ! 3.75 eA-3 Q107 0.032 0.050 0.533 ! 3.43 eA-3 Q108 0.936 0.375 0.921 ! 3.14 eA-3 C109 0.542 0.096 0.513 ! 3.12 eA-3 C110 0.100 0.467 0.158 ! 2.62 eA-3 C111 1.000 0.997 0.593 ! 2.59 eA-3 C112 0.012 0.640 0.291 ! 2.25 eA-3 C113 0.469 0.895 0.082 ! 2.04 eA-3 C114 0.857 0.464 0.921 ! 1.79 eA-3 C115 0.866 0.484 0.887 ! 1.75 eA-3 C116 0.383 0.031 0.011 ! 1.71 eA-3 C117 0.861 0.503 0.127 ! 1.60 eA-3 C118 0.031 1.001 0.656 ! 1.56 eA-3 C119 1.000 0.497 0.611 ! 1.54 eA-3 C120 0.018 0.578 0.064 ! 1.42 eA-3 C121 0.940 0.562 0.101 ! 1.32 eA-3 C122 0.516 0.060 0.760 ! 1.31 eA-3 C123 0.024 0.425 0.142 ! 1.30 eA-3 Q124 0.970 0.658 0.612 ! 1.29 eA-3 C125 0.523 0.098 0.776 ! 1.28 eA-3 C126 0.416 0.996 0.313 ! 1.22 eA-3 C127 0.984 0.402 0.985 ! 1.20 eA-3 C128 0.466 0.903 0.854 ! 1.16 eA-3 C129 0.446 0.984 0.258 ! 1.11 eA-3 C130 0.950 0.585 0.595 ! 1.09 eA-3 C131 0.443 0.950 0.299 ! 1.08 eA-3 C132 0.111 0.567 0.794 ! 1.03 eA-3 C133 0.071 0.437 0.599 ! 0.97 eA-3 C134 0.541 0.065 0.375 ! 0.94 eA-3 C135 0.397 0.980 0.919 ! 0.82 eA-3 C136 0.526 0.079 0.982 ! 0.82 eA-3 C137 0.056 0.520 0.638 ! 0.81 eA-3 Q138 0.482 0.863 0.317 ! 0.76 eA-3 C139 0.468 0.961 0.456 ! 0.75 eA-3 C140 0.440 0.923 0.196 ! 0.75 eA-3 C141 0.530 0.050 0.204 ! 0.75 eA-3 C142 0.502 0.059 0.157 ! 0.74 eA-3 C143 0.086 0.464 0.842 ! 0.73 eA-3 C144 0.406 0.019 0.228 ! 0.72 eA-3 C145 0.096 0.543 0.899 ! 0.70 eA-3 C146 0.252 0.875 0.981 ! 0.68 eA-3 Q147 0.046 0.917 0.665 ! 0.68 eA-3 Q148 0.930 0.359 0.024 ! 0.68 eA-3 C149 0.961 0.493 0.656 ! 0.66 eA-3 C150 0.344 1.003 0.962 ! 0.66 eA-3 C151 0.506 0.965 0.708 ! 0.66 eA-3 Q152 0.385 0.047 0.716 ! 0.66 eA-3 C153 0.008 0.435 0.626 ! 0.64 eA-3 C154 0.491 0.969 0.147 ! 0.64 eA-3 Q155 0.310 0.145 0.064 ! 0.62 eA-3 Q156 0.420 0.073 0.196 ! 0.60 eA-3 Q157 0.233 0.513 0.116 ! 0.60 eA-3 Q158 0.947 0.425 0.846 ! 0.59 eA-3 Q159 0.600 0.828 0.124 ! 0.59 eA-3 C160 0.242 0.532 0.086 ! 0.58 eA-3 C161 0.137 0.541 0.081 ! 0.58 eA-3 C162 0.031 0.550 0.587 ! 0.57 eA-3 C163 0.133 0.641 0.890 ! 0.57 eA-3 C164 0.460 0.891 0.947 ! 0.57 eA-3 C165 0.011 0.513 0.078 ! 0.56 eA-3 Q166 0.623 0.016 0.454 ! 0.56 eA-3 Q167 0.470 0.186 0.802 ! 0.55 eA-3 Q168 0.107 0.486 0.622 ! 0.54 eA-3 C169 0.919 0.485 0.851 ! 0.53 eA-3 C170 0.032 0.518 0.561 ! 0.52 eA-3 C171 0.414 0.997 0.449 ! 0.52 eA-3 C172 0.482 0.985 0.052 ! 0.52 eA-3 C173 0.916 0.567 0.851 ! 0.52 eA-3 Q174 0.384 0.012 0.468 ! 0.51 eA-3 Q175 0.615 0.036 0.422 ! 0.50 eA-3 ; _refine_diff_density_max 0.438 _refine_diff_density_min -0.267 _refine_diff_density_rms 0.045 _refine_ls_abs_structure_details ; Flack x determined using 3186 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.83(11) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.026 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 697 _refine_ls_number_reflns 12559 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.026 _refine_ls_R_factor_all 0.0796 _refine_ls_R_factor_gt 0.0576 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1089P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1587 _refine_ls_wR_factor_ref 0.1727 _reflns_Friedel_coverage 0.794 _reflns_Friedel_fraction_full 0.975 _reflns_Friedel_fraction_max 0.975 _reflns_number_gt 9247 _reflns_number_total 12559 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL sunchangli_il-5b_collect_a.res in P2(1)2(1)2 sunchangli_il-5b_collect_sq.res created by SHELXL-2016/6 at 09:45:03 on 08-Feb-2020 REM Old TITL sunchangli_il-5B_collect in P2(1)2(1)2 REM SHELXT solution in P2(1)2(1)2 REM R1 0.192, Rweak 0.039, Alpha 0.005, Orientation as input REM Flack x = 0.444 ( 0.114 ) from Parsons' quotients REM Formula found by SHELXT: C123 N20 O26 CELL 1.54184 31.3214 17.9026 12.675 90 90 90 ZERR 4 0.0009 0.0007 0.0006 0 0 0 LATT -1 SYMM -X,-Y,+Z SYMM 0.5-X,0.5+Y,-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 216 300 36 52 L.S. 5 0 170 PLAN 35 SIZE 0.05 0.1 0.1 TEMP -173(6) BOND $H MORE -1 CONF ABIN fmap 2 acta SHEL 999 0.837 REM REM REM WGHT 0.108900 FVAR 0.34193 O56 4 -0.720450 -0.714220 -0.487799 11.00000 0.03456 0.04333 = 0.06340 0.00902 -0.00046 0.00185 O61 4 -0.644335 -0.583568 -0.514937 11.00000 0.04161 0.03311 = 0.07787 -0.00428 0.00305 -0.00209 O57 4 -0.780070 -0.851171 -0.592989 11.00000 0.03384 0.03621 = 0.06194 0.00162 0.00117 -0.00177 O60 4 -0.908505 -0.870015 -0.569804 11.00000 0.03807 0.06321 = 0.05530 0.00320 0.00066 0.00067 O46 4 -0.793693 -0.346111 -0.237859 11.00000 0.06992 0.04991 = 0.07538 -0.00961 -0.00242 0.00465 N25 3 -0.962818 -0.897363 -0.893897 11.00000 0.03033 0.06265 = 0.05800 0.00092 -0.00020 -0.00419 O47 4 -0.738938 -0.438741 -0.158818 11.00000 0.06941 0.05719 = 0.06762 -0.00520 -0.00996 0.00132 AFIX 7 H47 2 -0.751687 -0.395670 -0.162821 11.00000 -1.20000 AFIX 0 N2 3 -0.827815 -0.944366 -0.583857 11.00000 0.02939 0.04070 = 0.05644 0.00639 0.00087 -0.00366 AFIX 43 H2 2 -0.835088 -0.986839 -0.553884 11.00000 -1.20000 AFIX 0 O59 4 -0.712057 -0.970927 -0.302995 11.00000 0.05086 0.03934 = 0.09518 0.01708 -0.01675 -0.00772 N11 3 -0.610960 -0.694098 -0.492944 11.00000 0.03160 0.03625 = 0.07414 -0.00165 -0.00233 -0.00273 O58 4 -0.841620 -0.623639 -0.730319 11.00000 0.05783 0.03593 = 0.10175 0.00644 -0.02608 -0.00194 N14 3 -0.706437 -0.650658 -0.636832 11.00000 0.03621 0.03937 = 0.06652 0.00256 0.00148 0.00184 AFIX 43 H14 2 -0.715843 -0.619245 -0.684909 11.00000 -1.20000 AFIX 0 N5 3 -0.738075 -0.888462 -0.420256 11.00000 0.03303 0.04257 = 0.06949 0.00847 -0.00644 -0.00507 AFIX 43 H5 2 -0.733599 -0.846983 -0.455831 11.00000 -1.20000 AFIX 0 N44 3 -0.804761 -0.391814 -0.305302 11.00000 0.04732 0.05064 = 0.07181 -0.00328 -0.00254 0.00229 N8 3 -0.656351 -0.809810 -0.396412 11.00000 0.03009 0.03725 = 0.06820 0.00362 -0.00263 -0.00010 AFIX 43 H8 2 -0.670493 -0.770308 -0.418458 11.00000 -1.20000 AFIX 0 N20 3 -0.881673 -0.785993 -0.686008 11.00000 0.03694 0.03839 = 0.07278 0.00125 -0.00559 -0.00101 O45 4 -0.831042 -0.375954 -0.373672 11.00000 0.07842 0.04692 = 0.09936 -0.00324 -0.02279 0.01503 N17 3 -0.799553 -0.702786 -0.638495 11.00000 0.03872 0.03055 = 0.07679 0.00052 -0.01531 -0.00344 AFIX 43 H17 2 -0.791416 -0.749601 -0.631892 11.00000 -1.20000 AFIX 0 O55 4 -0.597358 -0.881834 -0.413442 11.00000 0.04692 0.04770 = 0.13783 0.02089 0.01433 0.01408 C3 1 -0.795067 -0.906866 -0.546484 11.00000 0.03009 0.03132 = 0.06436 -0.00164 0.00292 0.00357 C23 1 -0.907726 -0.953434 -0.806490 11.00000 0.04089 0.04108 = 0.05193 -0.00211 -0.00141 -0.01156 C12 1 -0.638870 -0.648675 -0.544910 11.00000 0.02815 0.03348 = 0.06209 0.00774 0.00281 -0.00211 C2AA 1 -0.776395 -0.932272 -0.442615 11.00000 0.03358 0.03916 = 0.06709 0.00813 -0.00284 -0.00025 AFIX 13 H2AA 2 -0.768164 -0.986059 -0.448889 11.00000 -1.20000 AFIX 0 C24 1 -0.947819 -0.920795 -0.798832 11.00000 0.03523 0.06088 = 0.05373 -0.00083 -0.00076 -0.01096 AFIX 43 H24 2 -0.963048 -0.915441 -0.734455 11.00000 -1.20000 AFIX 0 C26 1 -0.932072 -0.914646 -0.969684 11.00000 0.03866 0.04723 = 0.05429 -0.00295 -0.00063 -0.01300 C21 1 -0.881964 -0.854279 -0.639867 11.00000 0.03032 0.04212 = 0.05753 0.00368 -0.00394 -0.00252 C15 1 -0.732462 -0.672731 -0.560647 11.00000 0.03374 0.03548 = 0.05968 0.00341 -0.00200 -0.00485 C41 1 -0.754262 -0.485279 -0.233663 11.00000 0.04513 0.04822 = 0.06615 -0.00767 -0.00198 -0.00217 C22 1 -0.880949 -0.980588 -0.719222 11.00000 0.03733 0.03937 = 0.05828 -0.00313 0.00110 -0.00800 AFIX 23 H22A 2 -0.862619 -1.021832 -0.744823 11.00000 -1.20000 H22B 2 -0.899472 -1.000551 -0.662562 11.00000 -1.20000 AFIX 0 C13 1 -0.662731 -0.677190 -0.642689 11.00000 0.03578 0.04426 = 0.05915 -0.00196 -0.00104 0.00771 AFIX 13 H13 2 -0.662604 -0.733048 -0.642732 11.00000 -1.20000 AFIX 0 C19 1 -0.849259 -0.758855 -0.759400 11.00000 0.04574 0.03430 = 0.07061 0.00205 -0.01014 -0.01198 AFIX 13 H19 2 -0.826410 -0.797666 -0.765021 11.00000 -1.20000 AFIX 0 C31 1 -0.897424 -0.948847 -0.916502 11.00000 0.03137 0.04330 = 0.05697 0.00293 0.00021 -0.00785 C16 1 -0.779062 -0.647702 -0.570231 11.00000 0.03347 0.03215 = 0.07000 -0.00068 -0.00883 -0.00303 AFIX 13 H16 2 -0.780380 -0.597286 -0.604042 11.00000 -1.20000 AFIX 0 C27 1 -0.932051 -0.905900 -1.078949 11.00000 0.05093 0.05739 = 0.05082 0.00841 -0.00216 -0.02062 AFIX 43 H27 2 -0.955439 -0.883449 -1.114612 11.00000 -1.20000 AFIX 0 C32 1 -1.003048 -0.855559 -0.914087 11.00000 0.03627 0.06188 = 0.07856 0.01263 -0.00688 -0.00668 C6 1 -0.709793 -0.909290 -0.347922 11.00000 0.03525 0.03875 = 0.07746 0.00515 -0.00463 0.00316 C30 1 -0.861889 -0.973253 -0.975188 11.00000 0.04576 0.05512 = 0.06324 -0.00323 -0.00136 -0.01103 AFIX 43 H30 2 -0.838246 -0.995993 -0.940946 11.00000 -1.20000 AFIX 0 C29 1 -0.861942 -0.963744 -1.081874 11.00000 0.05654 0.07342 = 0.05837 -0.01080 0.01087 -0.01079 AFIX 43 H29 2 -0.837896 -0.979591 -1.121697 11.00000 -1.20000 AFIX 0 C38 1 -0.784406 -0.588324 -0.385236 11.00000 0.03338 0.04295 = 0.06049 0.00140 0.00522 -0.00006 C18 1 -0.829439 -0.687968 -0.709650 11.00000 0.04476 0.03549 = 0.07674 0.00268 -0.00976 -0.00261 C7 1 -0.674564 -0.855626 -0.313753 11.00000 0.03603 0.04218 = 0.06803 0.00477 -0.00615 -0.00071 AFIX 13 H7 2 -0.650877 -0.886575 -0.283963 11.00000 -1.20000 AFIX 0 C66 1 -0.809875 -0.924362 -0.353201 11.00000 0.04367 0.05723 = 0.05729 0.00393 -0.00208 -0.01032 AFIX 23 H66A 2 -0.835256 -0.954637 -0.371593 11.00000 -1.20000 H66B 2 -0.797682 -0.945105 -0.287364 11.00000 -1.20000 AFIX 0 C39 1 -0.752718 -0.607600 -0.312051 11.00000 0.04421 0.04498 = 0.07652 0.00211 -0.01011 0.00518 AFIX 43 H39 2 -0.741194 -0.656682 -0.312908 11.00000 -1.20000 AFIX 0 C43 1 -0.800911 -0.517110 -0.381867 11.00000 0.03637 0.04363 = 0.06128 0.00045 -0.00287 0.00132 AFIX 43 H43 2 -0.822412 -0.502783 -0.430706 11.00000 -1.20000 AFIX 0 C42 1 -0.786204 -0.465426 -0.306746 11.00000 0.04232 0.04172 = 0.06674 -0.00108 0.00092 0.00114 C65 1 -0.590469 -0.664345 -0.399545 11.00000 0.04601 0.04593 = 0.06588 0.00311 -0.01219 -0.00584 AFIX 137 H65A 2 -0.611245 -0.635519 -0.358503 11.00000 -1.50000 H65B 2 -0.566773 -0.631804 -0.420445 11.00000 -1.50000 H65C 2 -0.579521 -0.705578 -0.356482 11.00000 -1.50000 AFIX 0 C37 1 -0.801229 -0.645317 -0.463074 11.00000 0.03222 0.03425 = 0.07610 -0.00135 -0.00167 -0.00353 AFIX 23 H37A 2 -0.831939 -0.635221 -0.474831 11.00000 -1.20000 H37B 2 -0.798937 -0.695408 -0.430470 11.00000 -1.20000 AFIX 0 C9 1 -0.618143 -0.826129 -0.440687 11.00000 0.03309 0.04176 = 0.08365 -0.00336 -0.00378 0.00475 C40 1 -0.737856 -0.556679 -0.238574 11.00000 0.04722 0.04959 = 0.07090 0.00030 -0.00781 0.00494 AFIX 43 H40 2 -0.716008 -0.571136 -0.190763 11.00000 -1.20000 AFIX 0 O52 4 -0.567429 -0.795400 -0.753534 11.00000 0.09107 0.09618 = 0.12276 -0.00729 0.01395 -0.02049 AFIX 83 H52 2 -0.570670 -0.841389 -0.743115 11.00000 -1.50000 AFIX 0 C33 1 -1.029042 -0.900157 -0.992704 11.00000 0.03827 0.05558 = 0.09151 0.01554 -0.01472 -0.00927 AFIX 43 H33 2 -1.029368 -0.952759 -0.982857 11.00000 -1.20000 AFIX 0 C70 1 -0.692053 -0.806835 -0.222917 11.00000 0.05157 0.04520 = 0.07392 0.00473 -0.00476 0.00084 AFIX 23 H70A 2 -0.715133 -0.774768 -0.251138 11.00000 -1.20000 H70B 2 -0.704880 -0.840058 -0.169121 11.00000 -1.20000 AFIX 0 C68 1 -0.862275 -0.819808 -0.349074 11.00000 0.05302 0.08068 = 0.06263 0.00458 0.00260 -0.01528 AFIX 43 H68 2 -0.882300 -0.852929 -0.380385 11.00000 -1.20000 AFIX 0 C1AA 1 -0.852347 -0.917362 -0.673607 11.00000 0.03939 0.04138 = 0.04905 -0.00350 -0.00279 -0.00474 AFIX 13 H1AA 2 -0.832449 -0.898979 -0.729578 11.00000 -1.20000 AFIX 0 C75 1 -0.641193 -0.648984 -0.741992 11.00000 0.05214 0.08982 = 0.05957 0.01336 0.00590 0.01193 AFIX 137 H75A 2 -0.637740 -0.594665 -0.737653 11.00000 -1.50000 H75B 2 -0.658801 -0.661488 -0.803414 11.00000 -1.50000 H75C 2 -0.613101 -0.672551 -0.749155 11.00000 -1.50000 AFIX 0 C67 1 -0.823888 -0.845394 -0.332857 11.00000 0.04847 0.06369 = 0.07717 0.00852 0.00994 -0.01292 AFIX 43 H67 2 -0.803182 -0.811545 -0.306137 11.00000 -1.20000 AFIX 0 C10 1 -0.600672 -0.771778 -0.521545 11.00000 0.03759 0.03542 = 0.07854 -0.00155 -0.00344 0.00154 AFIX 13 H10 2 -0.614518 -0.782915 -0.590872 11.00000 -1.20000 AFIX 0 C28 1 -0.896404 -0.931367 -1.133715 11.00000 0.06499 0.07661 = 0.05583 -0.00428 0.00771 -0.02723 AFIX 43 H28 2 -0.895597 -0.926512 -1.208324 11.00000 -1.20000 AFIX 0 C71 1 -0.659394 -0.757536 -0.169556 11.00000 0.09323 0.06940 = 0.06949 -0.00687 -0.00012 -0.03109 AFIX 13 H71 2 -0.649432 -0.719990 -0.222528 11.00000 -1.20000 AFIX 0 C48 1 -0.551992 -0.782615 -0.534467 11.00000 0.03877 0.05623 = 0.08843 -0.00624 -0.00275 0.00963 AFIX 23 H48A 2 -0.538092 -0.770622 -0.466393 11.00000 -1.20000 H48B 2 -0.546458 -0.836022 -0.549411 11.00000 -1.20000 AFIX 0 C63 1 -0.833495 -0.721479 -0.949716 11.00000 0.09893 0.06410 = 0.08126 0.01917 -0.01693 -0.03076 AFIX 13 H63 2 -0.822117 -0.671708 -0.927534 11.00000 -1.20000 AFIX 0 C62 1 -0.866871 -0.744328 -0.869766 11.00000 0.07085 0.05004 = 0.07447 0.01273 -0.02120 -0.02651 AFIX 23 H62A 2 -0.881225 -0.790204 -0.895142 11.00000 -1.20000 H62B 2 -0.888707 -0.704468 -0.865336 11.00000 -1.20000 AFIX 0 C74 1 -0.915428 -0.734032 -0.653480 11.00000 0.04616 0.04552 = 0.08977 -0.00143 -0.00940 0.00438 AFIX 137 H74A 2 -0.910391 -0.718118 -0.580556 11.00000 -1.50000 H74B 2 -0.943206 -0.758998 -0.658221 11.00000 -1.50000 H74C 2 -0.915229 -0.690277 -0.699938 11.00000 -1.50000 AFIX 0 C34 1 -1.050787 -0.875014 -1.071472 11.00000 0.07797 0.07743 = 0.11163 0.02820 -0.04334 -0.02039 AFIX 93 H34A 2 -1.051646 -0.822873 -1.085231 11.00000 -1.20000 H34B 2 -1.065946 -0.908636 -1.115735 11.00000 -1.20000 AFIX 0 C69 1 -0.877917 -0.741343 -0.322223 11.00000 0.05162 0.08075 = 0.07805 0.00034 0.01383 0.00348 AFIX 137 H69A 2 -0.900513 -0.744450 -0.268921 11.00000 -1.50000 H69B 2 -0.889179 -0.717454 -0.385981 11.00000 -1.50000 H69C 2 -0.854105 -0.711740 -0.294525 11.00000 -1.50000 AFIX 0 C73 1 -0.680622 -0.714530 -0.078179 11.00000 0.13032 0.07535 = 0.08376 -0.00761 -0.00397 0.00159 AFIX 137 H73A 2 -0.687981 -0.749472 -0.021508 11.00000 -1.50000 H73B 2 -0.706606 -0.690000 -0.103769 11.00000 -1.50000 H73C 2 -0.660776 -0.676778 -0.051169 11.00000 -1.50000 AFIX 0 O54 4 -0.487388 -0.664146 -0.495618 11.00000 0.06999 0.17651 = 0.14507 -0.01699 -0.01051 -0.02096 AFIX 147 H54 2 -0.462744 -0.650289 -0.478291 11.00000 -1.50000 AFIX 0 C49 1 -0.531035 -0.736602 -0.619675 11.00000 0.05365 0.12000 = 0.07625 0.00370 0.00469 0.00914 AFIX 13 H49 2 -0.547867 -0.689485 -0.627772 11.00000 -1.20000 AFIX 0 C36 1 -0.992833 -0.776470 -0.950394 11.00000 0.05663 0.04407 = 0.10300 0.00336 -0.01593 -0.00602 AFIX 137 H36A 2 -0.972457 -0.753624 -0.901388 11.00000 -1.50000 H36B 2 -1.019120 -0.746801 -0.951906 11.00000 -1.50000 H36C 2 -0.980348 -0.778087 -1.021252 11.00000 -1.50000 AFIX 0 C50 1 -0.531834 -0.776004 -0.721752 11.00000 0.07153 0.10830 = 0.13334 0.00885 -0.01128 0.03016 C64 1 -0.796543 -0.773791 -0.956397 11.00000 0.14791 0.07438 = 0.10518 0.01599 0.03635 -0.01797 AFIX 137 H64A 2 -0.782849 -0.777675 -0.887094 11.00000 -1.20000 H64B 2 -0.775885 -0.754880 -1.007960 11.00000 -1.20000 H64C 2 -0.806610 -0.823196 -0.978527 11.00000 -1.20000 AFIX 0 C35 1 -1.028377 -0.852329 -0.811806 11.00000 0.04204 0.10144 = 0.09054 0.01906 0.00719 0.01384 AFIX 137 H35A 2 -1.010370 -0.831774 -0.755635 11.00000 -1.50000 H35B 2 -1.037616 -0.902784 -0.792362 11.00000 -1.50000 H35C 2 -1.053464 -0.820347 -0.821521 11.00000 -1.50000 AFIX 0 O51 4 -0.498074 -0.786498 -0.771537 11.00000 0.09275 0.21835 = 0.13574 -0.00361 0.02272 0.04069 C72 1 -0.621546 -0.798671 -0.131642 11.00000 0.07705 0.10837 = 0.11301 -0.01164 -0.02355 -0.01502 AFIX 137 H72A 2 -0.605054 -0.816764 -0.192174 11.00000 -1.50000 H72B 2 -0.630727 -0.841225 -0.088622 11.00000 -1.50000 H72C 2 -0.603726 -0.765336 -0.088956 11.00000 -1.50000 AFIX 0 C53 1 -0.484640 -0.714593 -0.588565 11.00000 0.04980 0.22427 = 0.09856 0.02379 0.00501 -0.01035 AFIX 23 H53A 2 -0.467904 -0.759766 -0.570696 11.00000 -1.20000 H53B 2 -0.470415 -0.688772 -0.648020 11.00000 -1.20000 AFIX 0 C3AA 1 -0.853657 -0.711684 -1.058000 11.00000 0.18505 0.15004 = 0.09502 0.04535 -0.03443 -0.05935 AFIX 137 H3AA 2 -0.857954 -0.760770 -1.090534 11.00000 -1.50000 H3AB 2 -0.834764 -0.681577 -1.102609 11.00000 -1.50000 H3AC 2 -0.881245 -0.686392 -1.050629 11.00000 -1.50000 AFIX 0 HKLF 4 REM sunchangli_il-5b_collect_a.res in P2(1)2(1)2 REM R1 = 0.0576 for 9247 Fo > 4sig(Fo) and 0.0796 for all 12559 data REM 697 parameters refined using 0 restraints END WGHT 0.1089 0.0000 REM Highest difference peak 0.438, deepest hole -0.267, 1-sigma level 0.045 Q1 1 -0.5765 -0.8641 -0.7039 11.00000 0.05 0.44 Q2 1 -0.4726 -0.5762 -0.5340 11.00000 0.05 0.39 Q3 1 -0.5348 -0.7865 -0.8205 11.00000 0.05 0.35 Q4 1 -0.7340 -1.0366 -0.2613 11.00000 0.05 0.22 Q5 1 -0.4904 -0.7675 -0.6607 11.00000 0.05 0.22 Q6 1 -0.6403 -0.5777 -0.7214 11.00000 0.05 0.20 Q7 1 -0.8457 -0.8111 -0.2599 11.00000 0.05 0.18 Q8 1 -0.6401 -0.8414 -0.0746 11.00000 0.05 0.18 Q9 1 -0.8391 -0.5625 -0.7421 11.00000 0.05 0.17 Q10 1 -0.5005 -0.5956 -0.4801 11.00000 0.05 0.17 Q11 1 -0.4670 -0.8111 -0.6242 11.00000 0.05 0.17 Q12 1 -0.7413 -0.5698 -0.7366 11.00000 0.05 0.17 Q13 1 -0.6092 -0.9628 -0.4153 11.00000 0.05 0.17 Q14 1 -0.7624 -0.5607 -0.2324 11.00000 0.05 0.16 Q15 1 -0.8220 -0.3047 -0.3934 11.00000 0.05 0.16 Q16 1 -0.7344 -0.5585 -0.8096 11.00000 0.05 0.16 Q17 1 -0.8257 -0.7766 -1.0047 11.00000 0.05 0.16 Q18 1 -0.7227 -0.5391 -0.4040 11.00000 0.05 0.16 Q19 1 -0.8932 -0.7157 -0.8300 11.00000 0.05 0.15 Q20 1 -0.6665 -0.7540 -0.6429 11.00000 0.05 0.15 Q21 1 -0.9098 -0.9128 -1.3059 11.00000 0.05 0.15 Q22 1 -0.8432 -0.6400 -0.9204 11.00000 0.05 0.15 Q23 1 -0.8465 -0.8457 -0.4568 11.00000 0.05 0.15 Q24 1 -0.8885 -0.6785 -1.0369 11.00000 0.05 0.15 Q25 1 -0.8167 -0.9332 -1.1262 11.00000 0.05 0.15 Q26 1 -0.7401 -0.5947 -0.5337 11.00000 0.05 0.15 Q27 1 -0.8417 -0.8549 -0.3869 11.00000 0.05 0.15 Q28 1 -0.8814 -0.5262 -0.5625 11.00000 0.05 0.15 Q29 1 -0.5545 -0.5221 -0.6145 11.00000 0.05 0.15 Q30 1 -0.8150 -0.9087 -1.1216 11.00000 0.05 0.15 Q31 1 -0.7961 -0.8441 -0.7040 11.00000 0.05 0.15 Q32 1 -0.9729 -0.7426 -0.7017 11.00000 0.05 0.15 Q33 1 -0.6146 -0.6560 -0.2890 11.00000 0.05 0.15 Q34 1 -0.6500 -0.6867 -0.0344 11.00000 0.05 0.14 Q35 1 -0.7137 -0.6814 -0.2599 11.00000 0.05 0.14 REM The information below was added by Olex2. REM REM R1 = 0.0576 for 9247 Fo > 4sig(Fo) and 0.0796 for all 35433 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.44, deepest hole -0.27 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0796 REM R1_gt = 0.0576 REM wR_ref = 0.1727 REM GOOF = 1.026 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 35433 REM Reflections_gt = 9247 REM Parameters = n/a REM Hole = -0.27 REM Peak = 0.44 REM Flack = 0.83(11) ; _cod_data_source_file np0c00151_si_003.cif _cod_data_source_block sunchangli_il-5b_collect_sq _cod_database_code 1557882 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.971 _shelx_estimated_absorpt_t_min 0.944 _reflns_odcompleteness_completeness 99.90 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, H47 of O47, {H64A,H64B,H64C} of C64, All C(H,H) groups, All N(H) groups At 1.5 times of: H54 of O54, {H36A,H36B,H36C} of C36, {H35A,H35B,H35C} of C35, {H72A,H72B, H72C} of C72, {H3AA,H3AB,H3AC} of C3AA, {H65A,H65B,H65C} of C65, H52 of O52, {H74A,H74B,H74C} of C74, {H69A,H69B,H69C} of C69, {H73A,H73B,H73C} of C73, {H75A,H75B,H75C} of C75 2.a Rotating group: O47(H47) 2.b Ternary CH refined with riding coordinates: C2AA(H2AA), C13(H13), C19(H19), C16(H16), C7(H7), C1AA(H1AA), C10(H10), C71(H71), C63(H63), C49(H49) 2.c Secondary CH2 refined with riding coordinates: C22(H22A,H22B), C66(H66A,H66B), C37(H37A,H37B), C70(H70A,H70B), C48(H48A, H48B), C62(H62A,H62B), C53(H53A,H53B) 2.d Aromatic/amide H refined with riding coordinates: N2(H2), N14(H14), N5(H5), N8(H8), N17(H17), C24(H24), C27(H27), C30(H30), C29(H29), C39(H39), C43(H43), C40(H40), C33(H33), C68(H68), C67(H67), C28(H28) 2.e Tetrahedral OH refined with riding coordinates: O52(H52) 2.f X=CH2 refined with riding coordinates: C34(H34A,H34B) 2.g Idealised Me refined as rotating group: C65(H65A,H65B,H65C), C75(H75A,H75B,H75C), C74(H74A,H74B,H74C), C69(H69A,H69B, H69C), C73(H73A,H73B,H73C), C36(H36A,H36B,H36C), C64(H64A,H64B,H64C), C35(H35A, H35B,H35C), C72(H72A,H72B,H72C), C3AA(H3AA,H3AB,H3AC) 2.h Idealised tetrahedral OH refined as rotating group: O54(H54) ; _shelx_fab_file ; 4 0 0 113.43 0.01 6 0 0 -21.73 0.15 8 0 0 90.66 -3.98 10 0 0 -38.00 -3.82 12 0 0 -0.36 -1.16 14 0 0 -21.91 0.16 16 0 0 25.33 0.30 18 0 0 3.76 0.15 20 0 0 5.56 0.36 22 0 0 -5.01 0.71 24 0 0 3.55 0.38 26 0 0 -1.80 -0.39 28 0 0 -3.79 -0.15 30 0 0 0.38 -0.12 32 0 0 1.73 0.44 34 0 0 2.18 -0.26 36 0 0 -0.89 0.06 38 0 0 -1.33 -0.04 2 1 0 -2.70 -1.93 3 1 0 7.14 -0.37 4 1 0 -21.92 -0.75 5 1 0 77.07 0.54 6 1 0 -4.22 3.30 7 1 0 -36.85 3.07 8 1 0 -14.73 4.98 9 1 0 -2.17 6.54 10 1 0 -5.31 1.79 11 1 0 -1.69 3.17 12 1 0 -12.72 -0.13 13 1 0 35.09 1.31 14 1 0 9.84 0.72 15 1 0 -10.28 0.29 16 1 0 2.96 0.34 17 1 0 10.24 0.54 18 1 0 9.61 0.29 19 1 0 1.30 -0.01 20 1 0 3.86 -0.34 21 1 0 16.60 -0.15 22 1 0 8.32 -0.25 23 1 0 -1.58 0.03 24 1 0 2.12 -0.30 25 1 0 0.37 0.15 26 1 0 4.04 0.00 27 1 0 -4.89 0.55 28 1 0 0.09 0.00 29 1 0 2.43 0.33 30 1 0 2.13 -0.36 31 1 0 -6.04 -0.22 32 1 0 -0.43 0.25 33 1 0 0.63 -0.17 34 1 0 0.51 0.24 35 1 0 -0.79 -0.15 36 1 0 -1.22 0.20 37 1 0 2.34 0.09 38 1 0 -0.07 0.11 0 2 0 363.74 -0.77 1 2 0 57.61 0.86 2 2 0 114.14 -0.03 3 2 0 -8.04 1.45 4 2 0 26.14 0.03 5 2 0 69.92 -0.12 6 2 0 -20.97 0.12 7 2 0 -18.17 -4.53 8 2 0 70.48 -2.62 9 2 0 38.93 -2.63 10 2 0 -13.20 -2.02 11 2 0 -5.54 0.36 12 2 0 -2.21 0.24 13 2 0 11.03 0.64 14 2 0 -10.84 0.24 15 2 0 -20.53 -0.09 16 2 0 21.93 -0.26 17 2 0 -0.28 -0.18 18 2 0 10.41 -0.27 19 2 0 -8.42 -0.22 20 2 0 6.81 0.28 21 2 0 -0.32 0.09 22 2 0 -1.03 0.45 23 2 0 -2.32 -0.05 24 2 0 3.13 0.12 25 2 0 2.39 0.03 26 2 0 -0.31 -0.35 27 2 0 0.24 -0.26 28 2 0 -3.56 -0.45 29 2 0 -1.33 -0.12 30 2 0 -1.00 -0.07 31 2 0 -0.07 -0.66 32 2 0 1.46 0.41 33 2 0 -0.50 -0.23 34 2 0 2.73 0.10 35 2 0 2.14 -0.22 36 2 0 0.07 0.08 37 2 0 0.19 0.27 38 2 0 -0.85 0.04 1 3 0 4.68 0.54 2 3 0 -31.09 -1.53 3 3 0 115.90 -0.04 4 3 0 -48.88 -2.90 5 3 0 98.10 0.21 6 3 0 -2.57 2.32 7 3 0 -17.44 1.32 8 3 0 -23.02 5.24 9 3 0 -24.25 2.09 10 3 0 -5.61 2.48 11 3 0 -3.80 0.47 12 3 0 -22.96 -0.30 13 3 0 15.51 -0.43 14 3 0 19.35 -0.56 15 3 0 -5.12 0.32 16 3 0 0.40 0.03 17 3 0 1.62 0.14 18 3 0 15.05 0.59 19 3 0 -0.61 -0.25 20 3 0 3.62 0.09 21 3 0 8.18 -0.12 22 3 0 15.08 0.17 23 3 0 -1.40 0.13 24 3 0 3.11 -0.02 25 3 0 -3.98 0.12 26 3 0 6.35 0.17 27 3 0 -3.21 0.27 28 3 0 0.20 -0.07 29 3 0 0.31 0.29 30 3 0 3.58 -0.03 31 3 0 -2.40 -0.22 32 3 0 -2.26 0.12 33 3 0 -1.10 -0.30 34 3 0 0.41 -0.16 35 3 0 -0.27 -0.20 36 3 0 -1.16 -0.40 37 3 0 0.97 -0.05 38 3 0 0.19 -0.20 0 4 0 38.62 -0.32 1 4 0 74.62 -0.46 2 4 0 -11.61 0.56 3 4 0 15.94 2.49 4 4 0 -76.96 0.35 5 4 0 69.83 1.70 6 4 0 -1.94 0.64 7 4 0 -26.86 -4.10 8 4 0 35.16 -0.56 9 4 0 30.48 -3.74 10 4 0 15.55 0.21 11 4 0 -10.92 0.00 12 4 0 -8.82 1.09 13 4 0 9.35 2.45 14 4 0 4.33 -0.20 15 4 0 -18.01 1.23 16 4 0 10.58 -0.43 17 4 0 9.98 -0.04 18 4 0 15.69 0.27 19 4 0 1.33 -0.55 20 4 0 4.64 0.35 21 4 0 7.56 -0.14 22 4 0 1.87 0.26 23 4 0 3.81 -0.28 24 4 0 1.13 -0.08 25 4 0 7.20 -0.36 26 4 0 0.70 -0.11 27 4 0 1.95 -0.24 28 4 0 -4.25 -0.27 29 4 0 -0.87 -0.01 30 4 0 -0.77 -0.12 31 4 0 -0.47 -0.48 32 4 0 0.69 0.06 33 4 0 0.06 -0.18 34 4 0 1.57 0.15 35 4 0 1.09 0.40 36 4 0 1.13 0.09 37 4 0 -0.22 0.80 1 5 0 75.52 -0.59 2 5 0 -38.28 -3.19 3 5 0 116.38 -0.89 4 5 0 -38.56 -6.10 5 5 0 67.35 -0.21 6 5 0 11.27 -0.94 7 5 0 -3.59 0.85 8 5 0 -2.49 4.81 9 5 0 -26.83 1.59 10 5 0 2.74 2.76 11 5 0 5.00 0.37 12 5 0 -20.76 -0.44 13 5 0 0.84 1.16 14 5 0 14.40 -1.79 15 5 0 5.16 1.65 16 5 0 -10.67 0.21 17 5 0 -1.56 0.40 18 5 0 4.14 0.85 19 5 0 5.44 -0.38 20 5 0 -2.36 0.48 21 5 0 3.76 -0.17 22 5 0 11.61 -0.02 23 5 0 2.60 0.38 24 5 0 1.86 0.22 25 5 0 -3.97 0.12 26 5 0 4.83 0.37 27 5 0 0.30 0.08 28 5 0 -1.53 -0.11 29 5 0 -1.50 0.30 30 5 0 1.68 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5 12 0.37 0.54 23 6 12 -0.85 -1.09 24 6 12 -0.31 0.67 22 7 12 0.45 1.15 23 7 12 0.04 0.02 21 8 12 -1.00 0.57 22 8 12 -0.21 -0.29 20 9 12 0.05 -0.02 21 9 12 -1.42 0.96 18 10 12 -0.42 0.87 19 10 12 0.95 0.20 16 11 12 -0.17 0.19 17 11 12 -1.26 -0.84 13 12 12 0.60 -0.52 14 12 12 -1.51 -0.96 15 12 12 -0.17 0.05 11 13 12 0.37 1.42 12 13 12 -1.02 0.46 13 13 12 0.38 0.72 0 14 12 -0.83 0.15 1 14 12 0.64 0.78 2 14 12 0.36 -0.22 3 14 12 0.07 0.97 4 14 12 1.31 0.64 5 14 12 1.42 1.29 6 14 12 -0.64 1.95 7 14 12 -2.05 -1.21 8 14 12 -0.40 0.94 9 14 12 1.12 0.05 0 15 12 -0.07 -0.47 1 15 12 0.71 -0.16 15 0 13 0.69 -5.07 22 0 13 -0.31 -0.05 23 0 13 0.05 -0.56 22 1 13 -1.19 0.94 23 1 13 0.86 0.09 22 2 13 0.09 -0.01 21 3 13 0.50 -1.11 22 3 13 -1.37 0.35 21 4 13 1.60 -0.17 22 4 13 0.62 -0.17 20 5 13 -0.46 -0.58 21 5 13 1.34 -0.65 19 6 13 -0.54 0.56 20 6 13 0.02 0.53 18 7 13 0.72 -0.99 19 7 13 0.20 -0.89 17 8 13 0.54 -0.18 18 8 13 0.55 -0.65 15 9 13 -0.17 -0.07 16 9 13 -1.24 0.18 17 9 13 1.46 1.43 13 10 13 -0.35 0.28 14 10 13 -0.54 0.43 15 10 13 1.17 -1.14 10 11 13 1.48 -0.64 11 11 13 -1.41 -0.73 12 11 13 -0.60 -1.34 0 12 13 -1.39 -0.07 1 12 13 -0.51 0.28 2 12 13 -1.35 -0.30 3 12 13 -0.66 -1.40 4 12 13 -0.50 -1.50 5 12 13 0.17 -0.63 6 12 13 -0.66 -1.21 7 12 13 -0.28 -0.75 8 12 13 0.33 -0.95 9 12 13 -0.54 0.39 0 13 13 -0.06 -1.79 1 13 13 0.04 -0.52 2 13 13 0.50 -0.65 3 13 13 -1.12 0.41 4 13 13 -0.09 0.40 18 0 14 0.54 -0.13 19 0 14 0.07 -0.34 18 1 14 0.11 -0.57 19 1 14 -0.48 0.26 17 2 14 -0.94 0.18 18 2 14 -0.03 0.34 17 3 14 -0.48 -0.94 18 3 14 -0.17 -0.85 16 4 14 0.08 0.86 17 4 14 -0.23 -0.41 15 5 14 0.32 -0.51 16 5 14 0.18 0.19 17 5 14 -0.18 -0.66 14 6 14 -0.59 -0.18 15 6 14 -1.52 1.56 16 6 14 -0.59 0.56 13 7 14 1.19 0.09 14 7 14 0.33 -0.53 11 8 14 -0.07 0.65 12 8 14 1.13 2.42 13 8 14 0.68 0.44 6 9 14 1.94 -0.13 7 9 14 0.24 0.77 9 9 14 1.90 1.54 10 9 14 0.40 0.90 11 9 14 -1.25 -1.25 0 10 14 0.24 -0.14 1 10 14 0.99 -0.96 2 10 14 0.76 -0.02 3 10 14 0.13 0.03 4 10 14 1.46 0.15 5 10 14 -1.17 0.49 6 10 14 0.32 -1.00 7 10 14 -0.92 0.35 8 10 14 -1.30 -0.38 0 11 14 0.08 1.58 1 11 14 0.55 0.22 8 0 15 -2.05 -0.41 9 0 15 -0.08 0.61 10 0 15 -0.70 -0.07 11 0 15 -0.12 2.07 12 0 15 -1.45 0.03 13 0 15 -0.04 0.56 9 1 15 1.28 0.21 10 1 15 -0.20 -2.36 12 1 15 -0.46 -1.29 13 1 15 0.68 -0.06 9 2 15 0.00 1.07 12 2 15 -1.40 -0.24 13 2 15 -0.50 0.09 11 3 15 0.63 -1.05 12 3 15 -0.09 -1.18 10 4 15 -1.11 0.66 11 4 15 -1.11 1.49 12 4 15 -0.12 0.11 8 5 15 0.29 -1.57 9 5 15 -0.02 -0.30 10 5 15 0.64 -1.43 5 6 15 0.06 -1.00 6 6 15 0.46 0.10 7 6 15 0.06 1.00 8 6 15 0.63 -0.48 9 6 15 -0.12 0.61 0 7 15 0.18 -0.95 1 7 15 0.02 -0.69 2 7 15 0.39 0.80 3 7 15 0.33 -0.01 4 7 15 1.71 0.30 5 7 15 0.03 0.03 6 7 15 -0.28 0.90 0 0 16 -0.19 0.09 1 0 16 0.02 -1.92 2 0 16 -1.91 0.13 0 1 16 -0.12 1.61 1 1 16 0.94 -0.27 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 230318) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material ; _platon_squeeze_void_probe_radius 1.20 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 5.891 _oxdiff_exptl_absorpt_empirical_full_min 0.319 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O56 O -0.72045(8) -0.71422(17) -0.4878(2) 0.0471(7) Uani 1 1 d . . . . . O61 O -0.64434(9) -0.58357(17) -0.5149(3) 0.0509(7) Uani 1 1 d . . . . . O57 O -0.78007(8) -0.85117(16) -0.5930(2) 0.0440(7) Uani 1 1 d . . . . . O60 O -0.90851(9) -0.87001(19) -0.5698(2) 0.0522(8) Uani 1 1 d . . . . . O46 O -0.79369(11) -0.3461(2) -0.2379(3) 0.0651(9) Uani 1 1 d . . . . . N25 N -0.96282(10) -0.8974(2) -0.8939(3) 0.0503(9) Uani 1 1 d . . . . . O47 O -0.73894(11) -0.4387(2) -0.1588(3) 0.0647(9) Uani 1 1 d . . . . . H47 H -0.751687 -0.395670 -0.162821 0.078 Uiso 1 1 d GR . . . . N2 N -0.82782(9) -0.9444(2) -0.5839(3) 0.0422(8) Uani 1 1 d . . . . . H2 H -0.835088 -0.986839 -0.553884 0.051 Uiso 1 1 calc R . . . . O59 O -0.71206(10) -0.97093(18) -0.3030(3) 0.0618(9) Uani 1 1 d . . . . . N11 N -0.61096(10) -0.6941(2) -0.4929(3) 0.0473(9) Uani 1 1 d . . . . . O58 O -0.84162(10) -0.62364(19) -0.7303(3) 0.0652(9) Uani 1 1 d . . . . . N14 N -0.70644(10) -0.6507(2) -0.6368(3) 0.0474(8) Uani 1 1 d . . . . . H14 H -0.715843 -0.619245 -0.684909 0.057 Uiso 1 1 calc R . . . . N5 N -0.73808(10) -0.8885(2) -0.4203(3) 0.0484(9) Uani 1 1 d . . . . . H5 H -0.733599 -0.846983 -0.455831 0.058 Uiso 1 1 calc R . . . . N44 N -0.80476(12) -0.3918(2) -0.3053(4) 0.0566(10) Uani 1 1 d . . . . . N8 N -0.65635(9) -0.8098(2) -0.3964(3) 0.0452(8) Uani 1 1 d . . . . . H8 H -0.670493 -0.770308 -0.418458 0.054 Uiso 1 1 calc R . . . . N20 N -0.88167(10) -0.7860(2) -0.6860(3) 0.0494(9) Uani 1 1 d . . . . . O45 O -0.83104(12) -0.3760(2) -0.3737(3) 0.0749(11) Uani 1 1 d . . . . . N17 N -0.79955(10) -0.7028(2) -0.6385(3) 0.0487(9) Uani 1 1 d . . . . . H17 H -0.791416 -0.749601 -0.631892 0.058 Uiso 1 1 calc R . . . . O55 O -0.59736(10) -0.8818(2) -0.4134(4) 0.0775(12) Uani 1 1 d . . . . . C3 C -0.79507(11) -0.9069(2) -0.5465(4) 0.0419(10) Uani 1 1 d . . . . . C23 C -0.90773(12) -0.9534(2) -0.8065(4) 0.0446(10) Uani 1 1 d . . . . . C12 C -0.63887(11) -0.6487(2) -0.5449(3) 0.0412(9) Uani 1 1 d . . . . . C2AA C -0.77640(12) -0.9323(3) -0.4426(4) 0.0466(10) Uani 1 1 d . . . . . H2AA H -0.768164 -0.986059 -0.448889 0.056 Uiso 1 1 calc R . . . . C24 C -0.94782(12) -0.9208(3) -0.7988(4) 0.0499(11) Uani 1 1 d . . . . . H24 H -0.963048 -0.915441 -0.734455 0.060 Uiso 1 1 calc R . . . . C26 C -0.93207(12) -0.9146(3) -0.9697(4) 0.0467(10) Uani 1 1 d . . . . . C21 C -0.88196(11) -0.8543(2) -0.6399(4) 0.0433(10) Uani 1 1 d . . . . . C15 C -0.73246(12) -0.6727(2) -0.5606(4) 0.0430(10) Uani 1 1 d . . . . . C41 C -0.75426(14) -0.4853(3) -0.2337(4) 0.0532(11) Uani 1 1 d . . . . . C22 C -0.88095(12) -0.9806(3) -0.7192(4) 0.0450(10) Uani 1 1 d . . . . . H22A H -0.862619 -1.021832 -0.744823 0.054 Uiso 1 1 calc R . . . . H22B H -0.899472 -1.000551 -0.662562 0.054 Uiso 1 1 calc R . . . . C13 C -0.66273(12) -0.6772(3) -0.6427(4) 0.0464(10) Uani 1 1 d . . . . . H13 H -0.662604 -0.733048 -0.642732 0.056 Uiso 1 1 calc R . . . . C19 C -0.84926(13) -0.7589(3) -0.7594(4) 0.0502(11) Uani 1 1 d . . . . . H19 H -0.826410 -0.797666 -0.765021 0.060 Uiso 1 1 calc R . . . . C31 C -0.89742(11) -0.9488(2) -0.9165(4) 0.0439(10) Uani 1 1 d . . . . . C16 C -0.77906(12) -0.6477(2) -0.5702(4) 0.0452(10) Uani 1 1 d . . . . . H16 H -0.780380 -0.597286 -0.604042 0.054 Uiso 1 1 calc R . . . . C27 C -0.93205(14) -0.9059(3) -1.0789(4) 0.0530(12) Uani 1 1 d . . . . . H27 H -0.955439 -0.883449 -1.114612 0.064 Uiso 1 1 calc R . . . . C32 C -1.00305(13) -0.8556(3) -0.9141(4) 0.0589(12) Uani 1 1 d . . . . . C6 C -0.70979(12) -0.9093(3) -0.3479(4) 0.0505(11) Uani 1 1 d . . . . . C30 C -0.86189(14) -0.9733(3) -0.9752(4) 0.0547(11) Uani 1 1 d . . . . . H30 H -0.838246 -0.995993 -0.940946 0.066 Uiso 1 1 calc R . . . . C29 C -0.86194(16) -0.9637(3) -1.0819(4) 0.0628(13) Uani 1 1 d . . . . . H29 H -0.837896 -0.979591 -1.121697 0.075 Uiso 1 1 calc R . . . . C38 C -0.78441(12) -0.5883(2) -0.3852(4) 0.0456(10) Uani 1 1 d . . . . . C18 C -0.82944(13) -0.6880(3) -0.7096(4) 0.0523(11) Uani 1 1 d . . . . . C7 C -0.67456(12) -0.8556(3) -0.3138(4) 0.0487(10) Uani 1 1 d . . . . . H7 H -0.650877 -0.886575 -0.283963 0.058 Uiso 1 1 calc R . . . . C66 C -0.80988(13) -0.9244(3) -0.3532(4) 0.0527(11) Uani 1 1 d . . . . . H66A H -0.835256 -0.954637 -0.371593 0.063 Uiso 1 1 calc R . . . . H66B H -0.797682 -0.945105 -0.287364 0.063 Uiso 1 1 calc R . . . . C39 C -0.75272(13) -0.6076(3) -0.3121(4) 0.0552(12) Uani 1 1 d . . . . . H39 H -0.741194 -0.656682 -0.312908 0.066 Uiso 1 1 calc R . . . . C43 C -0.80091(12) -0.5171(3) -0.3819(4) 0.0471(10) Uani 1 1 d . . . . . H43 H -0.822412 -0.502783 -0.430706 0.057 Uiso 1 1 calc R . . . . C42 C -0.78620(13) -0.4654(3) -0.3067(4) 0.0503(11) Uani 1 1 d . . . . . C65 C -0.59047(14) -0.6643(3) -0.3995(4) 0.0526(11) Uani 1 1 d . . . . . H65A H -0.611245 -0.635519 -0.358503 0.079 Uiso 1 1 calc GR . . . . H65B H -0.566773 -0.631804 -0.420445 0.079 Uiso 1 1 calc GR . . . . H65C H -0.579521 -0.705578 -0.356482 0.079 Uiso 1 1 calc GR . . . . C37 C -0.80123(12) -0.6453(2) -0.4631(4) 0.0475(10) Uani 1 1 d . . . . . H37A H -0.831939 -0.635221 -0.474831 0.057 Uiso 1 1 calc R . . . . H37B H -0.798937 -0.695408 -0.430470 0.057 Uiso 1 1 calc R . . . . C9 C -0.61814(12) -0.8261(3) -0.4407(4) 0.0528(12) Uani 1 1 d . . . . . C40 C -0.73786(14) -0.5567(3) -0.2386(4) 0.0559(12) Uani 1 1 d . . . . . H40 H -0.716008 -0.571136 -0.190763 0.067 Uiso 1 1 calc R . . . . O52 O -0.56743(16) -0.7954(3) -0.7535(4) 0.1033(15) Uani 1 1 d . . . . . H52 H -0.570670 -0.841389 -0.743115 0.155 Uiso 1 1 calc R . . . . C33 C -1.02904(13) -0.9002(3) -0.9927(5) 0.0618(13) Uani 1 1 d . . . . . H33 H -1.029368 -0.952759 -0.982857 0.074 Uiso 1 1 calc R . . . . C70 C -0.69205(15) -0.8068(3) -0.2229(4) 0.0569(12) Uani 1 1 d . . . . . H70A H -0.715133 -0.774768 -0.251138 0.068 Uiso 1 1 calc R . . . . H70B H -0.704880 -0.840058 -0.169121 0.068 Uiso 1 1 calc R . . . . C68 C -0.86228(16) -0.8198(3) -0.3491(4) 0.0654(14) Uani 1 1 d . . . . . H68 H -0.882300 -0.852929 -0.380385 0.079 Uiso 1 1 calc R . . . . C1AA C -0.85235(12) -0.9174(2) -0.6736(3) 0.0433(9) Uani 1 1 d . . . . . H1AA H -0.832449 -0.898979 -0.729578 0.052 Uiso 1 1 calc R . . . . C75 C -0.64119(16) -0.6490(4) -0.7420(4) 0.0672(14) Uani 1 1 d . . . . . H75A H -0.637740 -0.594665 -0.737653 0.101 Uiso 1 1 calc GR . . . . H75B H -0.658801 -0.661488 -0.803414 0.101 Uiso 1 1 calc GR . . . . H75C H -0.613101 -0.672551 -0.749155 0.101 Uiso 1 1 calc GR . . . . C67 C -0.82389(15) -0.8454(3) -0.3329(4) 0.0631(13) Uani 1 1 d . . . . . H67 H -0.803182 -0.811545 -0.306137 0.076 Uiso 1 1 calc R . . . . C10 C -0.60067(12) -0.7718(2) -0.5215(4) 0.0505(11) Uani 1 1 d . . . . . H10 H -0.614518 -0.782915 -0.590872 0.061 Uiso 1 1 calc R . . . . C28 C -0.89640(16) -0.9314(3) -1.1337(4) 0.0658(14) Uani 1 1 d . . . . . H28 H -0.895597 -0.926512 -1.208324 0.079 Uiso 1 1 calc R . . . . C71 C -0.6594(2) -0.7575(4) -0.1696(5) 0.0774(17) Uani 1 1 d . . . . . H71 H -0.649432 -0.719990 -0.222528 0.093 Uiso 1 1 calc R . . . . C48 C -0.55199(13) -0.7826(3) -0.5345(5) 0.0611(13) Uani 1 1 d . . . . . H48A H -0.538092 -0.770622 -0.466393 0.073 Uiso 1 1 calc R . . . . H48B H -0.546458 -0.836022 -0.549411 0.073 Uiso 1 1 calc R . . . . C63 C -0.8335(2) -0.7215(4) -0.9497(5) 0.0814(18) Uani 1 1 d . . . . . H63 H -0.822117 -0.671708 -0.927534 0.098 Uiso 1 1 calc R . . . . C62 C -0.86687(17) -0.7443(3) -0.8698(4) 0.0651(14) Uani 1 1 d . . . . . H62A H -0.881225 -0.790204 -0.895142 0.078 Uiso 1 1 calc R . . . . H62B H -0.888707 -0.704468 -0.865336 0.078 Uiso 1 1 calc R . . . . C74 C -0.91543(14) -0.7340(3) -0.6535(5) 0.0605(13) Uani 1 1 d . . . . . H74A H -0.910391 -0.718118 -0.580556 0.091 Uiso 1 1 calc GR . . . . H74B H -0.943206 -0.758998 -0.658221 0.091 Uiso 1 1 calc GR . . . . H74C H -0.915229 -0.690277 -0.699938 0.091 Uiso 1 1 calc GR . . . . C34 C -1.05079(19) -0.8750(4) -1.0715(6) 0.089(2) Uani 1 1 d . . . . . H34A H -1.051646 -0.822873 -1.085231 0.107 Uiso 1 1 calc R . . . . H34B H -1.065946 -0.908636 -1.115735 0.107 Uiso 1 1 calc R . . . . C69 C -0.87792(16) -0.7413(4) -0.3222(5) 0.0701(15) Uani 1 1 d . . . . . H69A H -0.900513 -0.744450 -0.268921 0.105 Uiso 1 1 calc GR . . . . H69B H -0.889179 -0.717454 -0.385981 0.105 Uiso 1 1 calc GR . . . . H69C H -0.854105 -0.711740 -0.294525 0.105 Uiso 1 1 calc GR . . . . C73 C -0.6806(3) -0.7145(4) -0.0782(6) 0.096(2) Uani 1 1 d . . . . . H73A H -0.687981 -0.749472 -0.021508 0.145 Uiso 1 1 calc GR . . . . H73B H -0.706606 -0.690000 -0.103769 0.145 Uiso 1 1 calc GR . . . . H73C H -0.660776 -0.676778 -0.051169 0.145 Uiso 1 1 calc GR . . . . O54 O -0.48739(15) -0.6641(4) -0.4956(6) 0.131(2) Uani 1 1 d . . . . . H54 H -0.462744 -0.650289 -0.478291 0.196 Uiso 1 1 calc GR . . . . C49 C -0.53103(17) -0.7366(5) -0.6197(5) 0.0833(19) Uani 1 1 d . . . . . H49 H -0.547867 -0.689485 -0.627772 0.100 Uiso 1 1 calc R . . . . C36 C -0.99283(16) -0.7765(3) -0.9504(5) 0.0679(14) Uani 1 1 d . . . . . H36A H -0.972457 -0.753624 -0.901388 0.102 Uiso 1 1 calc GR . . . . H36B H -1.019120 -0.746801 -0.951906 0.102 Uiso 1 1 calc GR . . . . H36C H -0.980348 -0.778087 -1.021252 0.102 Uiso 1 1 calc GR . . . . C50 C -0.5318(2) -0.7760(5) -0.7218(7) 0.104(2) Uani 1 1 d . . . . . C64 C -0.7965(3) -0.7738(4) -0.9564(7) 0.109(3) Uani 1 1 d . . . . . H64A H -0.782849 -0.777675 -0.887094 0.131 Uiso 1 1 calc GR . . . . H64B H -0.775885 -0.754880 -1.007960 0.131 Uiso 1 1 calc GR . . . . H64C H -0.806610 -0.823196 -0.978527 0.131 Uiso 1 1 calc GR . . . . C35 C -1.02838(15) -0.8523(4) -0.8118(5) 0.0780(17) Uani 1 1 d . . . . . H35A H -1.010370 -0.831774 -0.755635 0.117 Uiso 1 1 calc GR . . . . H35B H -1.037616 -0.902784 -0.792362 0.117 Uiso 1 1 calc GR . . . . H35C H -1.053464 -0.820347 -0.821521 0.117 Uiso 1 1 calc GR . . . . O51 O -0.49807(19) -0.7865(5) -0.7715(5) 0.149(3) Uani 1 1 d . . . . . C72 C -0.6215(2) -0.7987(5) -0.1316(7) 0.099(2) Uani 1 1 d . . . . . H72A H -0.605054 -0.816764 -0.192174 0.149 Uiso 1 1 calc GR . . . . H72B H -0.630727 -0.841225 -0.088622 0.149 Uiso 1 1 calc GR . . . . H72C H -0.603726 -0.765336 -0.088956 0.149 Uiso 1 1 calc GR . . . . C53 C -0.48464(19) -0.7146(7) -0.5886(7) 0.124(4) Uani 1 1 d . . . . . H53A H -0.467904 -0.759766 -0.570696 0.149 Uiso 1 1 calc R . . . . H53B H -0.470415 -0.688772 -0.648020 0.149 Uiso 1 1 calc R . . . . C3AA C -0.8537(4) -0.7117(7) -1.0580(7) 0.143(4) Uani 1 1 d . . . . . H3AA H -0.857954 -0.760770 -1.090534 0.215 Uiso 1 1 calc GR . . . . H3AB H -0.834764 -0.681577 -1.102609 0.215 Uiso 1 1 calc GR . . . . H3AC H -0.881245 -0.686392 -1.050629 0.215 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O56 0.0346(12) 0.0433(17) 0.0634(19) 0.0090(16) -0.0005(13) 0.0018(12) O61 0.0416(14) 0.0331(17) 0.078(2) -0.0043(15) 0.0030(14) -0.0021(12) O57 0.0338(12) 0.0362(16) 0.0619(17) 0.0016(14) 0.0012(12) -0.0018(11) O60 0.0381(13) 0.063(2) 0.0553(18) 0.0032(16) 0.0007(13) 0.0007(13) O46 0.070(2) 0.050(2) 0.075(2) -0.0096(19) -0.0024(18) 0.0046(16) N25 0.0303(15) 0.063(3) 0.058(2) 0.001(2) -0.0002(15) -0.0042(16) O47 0.069(2) 0.057(2) 0.068(2) -0.0052(19) -0.0100(17) 0.0013(17) N2 0.0294(14) 0.041(2) 0.056(2) 0.0064(17) 0.0009(14) -0.0037(13) O59 0.0509(16) 0.0393(19) 0.095(2) 0.0171(18) -0.0168(16) -0.0077(14) N11 0.0316(14) 0.0362(19) 0.074(2) -0.0016(19) -0.0023(16) -0.0027(14) O58 0.0578(17) 0.0359(18) 0.102(3) 0.0064(18) -0.0261(18) -0.0019(15) N14 0.0362(16) 0.039(2) 0.067(2) 0.0026(18) 0.0015(16) 0.0018(14) N5 0.0330(15) 0.043(2) 0.069(2) 0.0085(19) -0.0064(16) -0.0051(14) N44 0.0473(19) 0.051(2) 0.072(3) -0.003(2) -0.0025(19) 0.0023(18) N8 0.0301(14) 0.037(2) 0.068(2) 0.0036(17) -0.0026(15) -0.0001(13) N20 0.0369(16) 0.038(2) 0.073(2) 0.0012(19) -0.0056(16) -0.0010(15) O45 0.078(2) 0.047(2) 0.099(3) -0.003(2) -0.023(2) 0.0150(18) N17 0.0387(16) 0.0305(19) 0.077(2) 0.0005(18) -0.0153(17) -0.0034(14) O55 0.0469(16) 0.048(2) 0.138(3) 0.021(2) 0.014(2) 0.0141(16) C3 0.0301(16) 0.031(2) 0.064(3) -0.002(2) 0.0029(17) 0.0036(15) C23 0.0409(19) 0.041(2) 0.052(2) -0.002(2) -0.0014(18) -0.0116(18) C12 0.0282(16) 0.033(2) 0.062(3) 0.008(2) 0.0028(16) -0.0021(16) C2AA 0.0336(17) 0.039(2) 0.067(3) 0.008(2) -0.0028(18) -0.0002(17) C24 0.0352(18) 0.061(3) 0.054(3) -0.001(2) -0.0008(18) -0.0110(19) C26 0.0387(19) 0.047(3) 0.054(3) -0.003(2) -0.0006(18) -0.0130(18) C21 0.0303(17) 0.042(2) 0.058(2) 0.004(2) -0.0039(17) -0.0025(16) C15 0.0337(18) 0.035(2) 0.060(3) 0.003(2) -0.0020(18) -0.0048(16) C41 0.045(2) 0.048(3) 0.066(3) -0.008(2) -0.002(2) -0.002(2) C22 0.0373(18) 0.039(2) 0.058(3) -0.003(2) 0.0011(18) -0.0080(17) C13 0.0358(18) 0.044(3) 0.059(3) -0.002(2) -0.0010(18) 0.0077(17) C19 0.046(2) 0.034(2) 0.071(3) 0.002(2) -0.010(2) -0.0120(18) C31 0.0314(17) 0.043(2) 0.057(3) 0.003(2) 0.0002(17) -0.0079(16) C16 0.0335(17) 0.032(2) 0.070(3) -0.001(2) -0.0088(18) -0.0030(16) C27 0.051(2) 0.057(3) 0.051(3) 0.008(2) -0.0022(19) -0.021(2) C32 0.0363(19) 0.062(3) 0.079(3) 0.013(3) -0.007(2) -0.007(2) C6 0.0352(19) 0.039(3) 0.077(3) 0.005(2) -0.0046(19) 0.0032(17) C30 0.046(2) 0.055(3) 0.063(3) -0.003(2) -0.001(2) -0.011(2) C29 0.057(3) 0.073(4) 0.058(3) -0.011(3) 0.011(2) -0.011(2) C38 0.0334(17) 0.043(3) 0.060(3) 0.001(2) 0.0052(17) -0.0001(17) C18 0.045(2) 0.035(3) 0.077(3) 0.003(2) -0.010(2) -0.0026(18) C7 0.0360(18) 0.042(2) 0.068(3) 0.005(2) -0.0061(19) -0.0007(18) C66 0.044(2) 0.057(3) 0.057(3) 0.004(2) -0.0021(19) -0.010(2) C39 0.044(2) 0.045(3) 0.077(3) 0.002(2) -0.010(2) 0.0052(19) C43 0.0364(18) 0.044(3) 0.061(3) 0.000(2) -0.0029(18) 0.0013(18) C42 0.042(2) 0.042(3) 0.067(3) -0.001(2) 0.001(2) 0.0011(18) C65 0.046(2) 0.046(3) 0.066(3) 0.003(2) -0.012(2) -0.0058(19) C37 0.0322(17) 0.034(2) 0.076(3) -0.001(2) -0.0017(19) -0.0035(16) C9 0.0331(18) 0.042(3) 0.084(3) -0.003(2) -0.004(2) 0.0048(18) C40 0.047(2) 0.050(3) 0.071(3) 0.000(2) -0.008(2) 0.005(2) O52 0.091(3) 0.096(4) 0.123(4) -0.007(3) 0.014(3) -0.020(3) C33 0.038(2) 0.056(3) 0.092(4) 0.016(3) -0.015(2) -0.009(2) C70 0.052(2) 0.045(3) 0.074(3) 0.005(2) -0.005(2) 0.001(2) C68 0.053(3) 0.081(4) 0.063(3) 0.005(3) 0.003(2) -0.015(3) C1AA 0.0394(18) 0.041(2) 0.049(2) -0.003(2) -0.0028(17) -0.0047(17) C75 0.052(2) 0.090(4) 0.060(3) 0.013(3) 0.006(2) 0.012(3) C67 0.048(2) 0.064(3) 0.077(3) 0.009(3) 0.010(2) -0.013(2) C10 0.0376(19) 0.035(2) 0.079(3) -0.002(2) -0.003(2) 0.0015(17) C28 0.065(3) 0.077(4) 0.056(3) -0.004(3) 0.008(2) -0.027(3) C71 0.093(4) 0.069(4) 0.069(3) -0.007(3) 0.000(3) -0.031(3) C48 0.039(2) 0.056(3) 0.088(4) -0.006(3) -0.003(2) 0.010(2) C63 0.099(4) 0.064(4) 0.081(4) 0.019(3) -0.017(3) -0.031(3) C62 0.071(3) 0.050(3) 0.074(3) 0.013(3) -0.021(3) -0.027(2) C74 0.046(2) 0.046(3) 0.090(4) -0.001(3) -0.009(2) 0.004(2) C34 0.078(4) 0.077(4) 0.112(5) 0.028(4) -0.043(4) -0.020(3) C69 0.052(3) 0.081(4) 0.078(4) 0.000(3) 0.014(2) 0.003(3) C73 0.130(6) 0.075(5) 0.084(4) -0.008(4) -0.004(4) 0.002(4) O54 0.070(3) 0.177(6) 0.145(5) -0.017(5) -0.011(3) -0.021(3) C49 0.054(3) 0.120(6) 0.076(4) 0.004(4) 0.005(3) 0.009(3) C36 0.057(3) 0.044(3) 0.103(4) 0.003(3) -0.016(3) -0.006(2) C50 0.072(4) 0.108(6) 0.133(7) 0.009(5) -0.011(4) 0.030(4) C64 0.148(7) 0.074(5) 0.105(5) 0.016(4) 0.036(5) -0.018(5) C35 0.042(2) 0.101(5) 0.091(4) 0.019(4) 0.007(3) 0.014(3) O51 0.093(3) 0.218(8) 0.136(5) -0.004(5) 0.023(4) 0.041(4) C72 0.077(4) 0.108(6) 0.113(5) -0.012(5) -0.024(4) -0.015(4) C53 0.050(3) 0.224(11) 0.099(5) 0.024(7) 0.005(3) -0.010(4) C3AA 0.185(9) 0.150(9) 0.095(6) 0.045(6) -0.034(6) -0.059(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C24 N25 C26 107.7(4) . . ? C24 N25 C32 126.9(4) . . ? C26 N25 C32 125.3(4) . . ? C41 O47 H47 110.0 . . ? C3 N2 H2 119.2 . . ? C3 N2 C1AA 121.6(4) . . ? C1AA N2 H2 119.2 . . ? C12 N11 C65 117.4(4) . . ? C12 N11 C10 125.8(4) . . ? C65 N11 C10 116.8(4) . . ? C15 N14 H14 119.3 . . ? C15 N14 C13 121.4(4) . . ? C13 N14 H14 119.3 . . ? C2AA N5 H5 119.0 . . ? C6 N5 H5 119.0 . . ? C6 N5 C2AA 122.1(4) . . ? O46 N44 C42 120.2(4) . . ? O45 N44 O46 121.6(4) . . ? O45 N44 C42 118.2(4) . . ? C7 N8 H8 119.1 . . ? C9 N8 H8 119.1 . . ? C9 N8 C7 121.7(4) . . ? C21 N20 C19 125.4(4) . . ? C21 N20 C74 116.5(4) . . ? C19 N20 C74 118.0(4) . . ? C16 N17 H17 117.4 . . ? C18 N17 H17 117.4 . . ? C18 N17 C16 125.3(4) . . ? O57 C3 N2 122.1(4) . . ? O57 C3 C2AA 120.4(4) . . ? N2 C3 C2AA 117.5(4) . . ? C24 C23 C22 127.0(4) . . ? C24 C23 C31 104.3(4) . . ? C31 C23 C22 128.5(4) . . ? O61 C12 N11 120.1(4) . . ? O61 C12 C13 119.6(4) . . ? N11 C12 C13 120.3(4) . . ? N5 C2AA C3 109.0(4) . . ? N5 C2AA H2AA 108.7 . . ? N5 C2AA C66 111.4(4) . . ? C3 C2AA H2AA 108.7 . . ? C3 C2AA C66 110.3(3) . . ? C66 C2AA H2AA 108.7 . . ? N25 C24 C23 112.4(4) . . ? N25 C24 H24 123.8 . . ? C23 C24 H24 123.8 . . ? N25 C26 C31 107.3(4) . . ? C27 C26 N25 131.3(4) . . ? C27 C26 C31 121.4(4) . . ? O60 C21 N20 121.0(4) . . ? O60 C21 C1AA 116.0(4) . . ? N20 C21 C1AA 122.9(4) . . ? O56 C15 N14 122.3(3) . . ? O56 C15 C16 121.5(4) . . ? N14 C15 C16 116.2(4) . . ? O47 C41 C42 123.9(4) . . ? O47 C41 C40 118.1(4) . . ? C40 C41 C42 117.9(4) . . ? C23 C22 H22A 109.3 . . ? C23 C22 H22B 109.3 . . ? C23 C22 C1AA 111.6(4) . . ? H22A C22 H22B 108.0 . . ? C1AA C22 H22A 109.3 . . ? C1AA C22 H22B 109.3 . . ? N14 C13 C12 108.0(3) . . ? N14 C13 H13 109.3 . . ? N14 C13 C75 110.7(4) . . ? C12 C13 H13 109.3 . . ? C75 C13 C12 110.1(4) . . ? C75 C13 H13 109.3 . . ? N20 C19 H19 108.2 . . ? N20 C19 C18 107.0(4) . . ? N20 C19 C62 112.9(3) . . ? C18 C19 H19 108.2 . . ? C62 C19 H19 108.2 . . ? C62 C19 C18 112.3(4) . . ? C26 C31 C23 108.4(4) . . ? C30 C31 C23 132.4(4) . . ? C30 C31 C26 119.2(4) . . ? N17 C16 C15 105.6(3) . . ? N17 C16 H16 109.7 . . ? N17 C16 C37 110.3(3) . . ? C15 C16 H16 109.7 . . ? C37 C16 C15 111.8(4) . . ? C37 C16 H16 109.7 . . ? C26 C27 H27 121.3 . . ? C28 C27 C26 117.3(5) . . ? C28 C27 H27 121.3 . . ? N25 C32 C33 107.7(4) . . ? N25 C32 C36 110.0(4) . . ? N25 C32 C35 108.3(4) . . ? C33 C32 C36 113.8(4) . . ? C33 C32 C35 107.5(4) . . ? C35 C32 C36 109.4(5) . . ? O59 C6 N5 121.8(4) . . ? O59 C6 C7 118.0(4) . . ? N5 C6 C7 120.1(4) . . ? C31 C30 H30 120.5 . . ? C29 C30 C31 119.0(5) . . ? C29 C30 H30 120.5 . . ? C30 C29 H29 119.3 . . ? C30 C29 C28 121.5(5) . . ? C28 C29 H29 119.3 . . ? C39 C38 C37 120.8(4) . . ? C43 C38 C39 118.3(4) . . ? C43 C38 C37 120.9(4) . . ? O58 C18 N17 123.1(4) . . ? O58 C18 C19 123.5(4) . . ? N17 C18 C19 113.3(4) . . ? N8 C7 C6 115.9(4) . . ? N8 C7 H7 107.1 . . ? N8 C7 C70 111.0(4) . . ? C6 C7 H7 107.1 . . ? C6 C7 C70 108.1(4) . . ? C70 C7 H7 107.1 . . ? C2AA C66 H66A 108.7 . . ? C2AA C66 H66B 108.7 . . ? H66A C66 H66B 107.6 . . ? C67 C66 C2AA 114.1(4) . . ? C67 C66 H66A 108.7 . . ? C67 C66 H66B 108.7 . . ? C38 C39 H39 119.3 . . ? C40 C39 C38 121.4(4) . . ? C40 C39 H39 119.3 . . ? C38 C43 H43 119.7 . . ? C38 C43 C42 120.5(4) . . ? C42 C43 H43 119.7 . . ? C41 C42 N44 120.6(4) . . ? C43 C42 N44 118.6(4) . . ? C43 C42 C41 120.8(4) . . ? N11 C65 H65A 109.5 . . ? N11 C65 H65B 109.5 . . ? N11 C65 H65C 109.5 . . ? H65A C65 H65B 109.5 . . ? H65A C65 H65C 109.5 . . ? H65B C65 H65C 109.5 . . ? C16 C37 H37A 108.3 . . ? C16 C37 H37B 108.3 . . ? C38 C37 C16 116.1(3) . . ? C38 C37 H37A 108.3 . . ? C38 C37 H37B 108.3 . . ? H37A C37 H37B 107.4 . . ? N8 C9 C10 117.5(4) . . ? O55 C9 N8 121.5(5) . . ? O55 C9 C10 121.0(4) . . ? C41 C40 C39 121.0(4) . . ? C41 C40 H40 119.5 . . ? C39 C40 H40 119.5 . . ? C50 O52 H52 109.5 . . ? C32 C33 H33 116.2 . . ? C34 C33 C32 127.5(5) . . ? C34 C33 H33 116.2 . . ? C7 C70 H70A 108.5 . . ? C7 C70 H70B 108.5 . . ? H70A C70 H70B 107.5 . . ? C71 C70 C7 115.1(4) . . ? C71 C70 H70A 108.5 . . ? C71 C70 H70B 108.5 . . ? C67 C68 H68 117.1 . . ? C67 C68 C69 125.8(5) . . ? C69 C68 H68 117.1 . . ? N2 C1AA C21 110.4(3) . . ? N2 C1AA C22 110.7(4) . . ? N2 C1AA H1AA 109.6 . . ? C21 C1AA C22 107.1(3) . . ? C21 C1AA H1AA 109.6 . . ? C22 C1AA H1AA 109.6 . . ? C13 C75 H75A 109.5 . . ? C13 C75 H75B 109.5 . . ? C13 C75 H75C 109.5 . . ? H75A C75 H75B 109.5 . . ? H75A C75 H75C 109.5 . . ? H75B C75 H75C 109.5 . . ? C66 C67 H67 117.5 . . ? C68 C67 C66 125.0(5) . . ? C68 C67 H67 117.5 . . ? N11 C10 C9 111.1(4) . . ? N11 C10 H10 108.0 . . ? N11 C10 C48 111.1(4) . . ? C9 C10 H10 108.0 . . ? C9 C10 C48 110.3(4) . . ? C48 C10 H10 108.0 . . ? C27 C28 H28 119.2 . . ? C29 C28 C27 121.6(5) . . ? C29 C28 H28 119.2 . . ? C70 C71 H71 107.7 . . ? C70 C71 C73 109.6(5) . . ? C73 C71 H71 107.7 . . ? C72 C71 C70 113.5(5) . . ? C72 C71 H71 107.7 . . ? C72 C71 C73 110.5(6) . . ? C10 C48 H48A 108.3 . . ? C10 C48 H48B 108.3 . . ? H48A C48 H48B 107.4 . . ? C49 C48 C10 115.9(5) . . ? C49 C48 H48A 108.3 . . ? C49 C48 H48B 108.3 . . ? C62 C63 H63 107.4 . . ? C62 C63 C3AA 110.4(6) . . ? C64 C63 H63 107.4 . . ? C64 C63 C62 113.9(5) . . ? C64 C63 C3AA 110.1(8) . . ? C3AA C63 H63 107.4 . . ? C19 C62 H62A 108.7 . . ? C19 C62 H62B 108.7 . . ? C63 C62 C19 114.2(4) . . ? C63 C62 H62A 108.7 . . ? C63 C62 H62B 108.7 . . ? H62A C62 H62B 107.6 . . ? N20 C74 H74A 109.5 . . ? N20 C74 H74B 109.5 . . ? N20 C74 H74C 109.5 . . ? H74A C74 H74B 109.5 . . ? H74A C74 H74C 109.5 . . ? H74B C74 H74C 109.5 . . ? C33 C34 H34A 120.0 . . ? C33 C34 H34B 120.0 . . ? H34A C34 H34B 120.0 . . ? C68 C69 H69A 109.5 . . ? C68 C69 H69B 109.5 . . ? C68 C69 H69C 109.5 . . ? H69A C69 H69B 109.5 . . ? H69A C69 H69C 109.5 . . ? H69B C69 H69C 109.5 . . ? C71 C73 H73A 109.5 . . ? C71 C73 H73B 109.5 . . ? C71 C73 H73C 109.5 . . ? H73A C73 H73B 109.5 . . ? H73A C73 H73C 109.5 . . ? H73B C73 H73C 109.5 . . ? C53 O54 H54 109.5 . . ? C48 C49 H49 107.7 . . ? C48 C49 C53 111.3(6) . . ? C50 C49 C48 111.1(7) . . ? C50 C49 H49 107.7 . . ? C50 C49 C53 111.1(6) . . ? C53 C49 H49 107.7 . . ? C32 C36 H36A 109.5 . . ? C32 C36 H36B 109.5 . . ? C32 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? O52 C50 C49 115.9(7) . . ? O52 C50 O51 124.0(9) . . ? O51 C50 C49 120.2(7) . . ? C63 C64 H64A 109.5 . . ? C63 C64 H64B 109.5 . . ? C63 C64 H64C 109.5 . . ? H64A C64 H64B 109.5 . . ? H64A C64 H64C 109.5 . . ? H64B C64 H64C 109.5 . . ? C32 C35 H35A 109.5 . . ? C32 C35 H35B 109.5 . . ? C32 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C71 C72 H72A 109.5 . . ? C71 C72 H72B 109.5 . . ? C71 C72 H72C 109.5 . . ? H72A C72 H72B 109.5 . . ? H72A C72 H72C 109.5 . . ? H72B C72 H72C 109.5 . . ? O54 C53 C49 107.5(6) . . ? O54 C53 H53A 110.2 . . ? O54 C53 H53B 110.2 . . ? C49 C53 H53A 110.2 . . ? C49 C53 H53B 110.2 . . ? H53A C53 H53B 108.5 . . ? C63 C3AA H3AA 109.5 . . ? C63 C3AA H3AB 109.5 . . ? C63 C3AA H3AC 109.5 . . ? H3AA C3AA H3AB 109.5 . . ? H3AA C3AA H3AC 109.5 . . ? H3AB C3AA H3AC 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O56 C15 1.243(5) . ? O61 C12 1.238(5) . ? O57 C3 1.250(5) . ? O60 C21 1.249(5) . ? O46 N44 1.233(5) . ? N25 C24 1.360(6) . ? N25 C26 1.395(6) . ? N25 C32 1.488(6) . ? O47 H47 0.8698 . ? O47 C41 1.351(6) . ? N2 H2 0.8800 . ? N2 C3 1.314(5) . ? N2 C1AA 1.455(6) . ? O59 C6 1.244(5) . ? N11 C12 1.364(5) . ? N11 C65 1.448(6) . ? N11 C10 1.473(6) . ? O58 C18 1.241(6) . ? N14 H14 0.8800 . ? N14 C15 1.324(6) . ? N14 C13 1.451(5) . ? N5 H5 0.8800 . ? N5 C2AA 1.462(5) . ? N5 C6 1.328(6) . ? N44 O45 1.228(5) . ? N44 C42 1.440(6) . ? N8 H8 0.8800 . ? N8 C7 1.448(6) . ? N8 C9 1.354(5) . ? N20 C21 1.355(6) . ? N20 C19 1.460(6) . ? N20 C74 1.467(6) . ? N17 H17 0.8800 . ? N17 C16 1.461(6) . ? N17 C18 1.327(6) . ? O55 C9 1.240(6) . ? C3 C2AA 1.511(6) . ? C23 C24 1.388(6) . ? C23 C22 1.471(6) . ? C23 C31 1.434(6) . ? C12 C13 1.535(6) . ? C2AA H2AA 1.0000 . ? C2AA C66 1.551(6) . ? C24 H24 0.9500 . ? C26 C31 1.417(6) . ? C26 C27 1.394(7) . ? C21 C1AA 1.523(6) . ? C15 C16 1.532(5) . ? C41 C42 1.409(7) . ? C41 C40 1.379(7) . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C22 C1AA 1.555(6) . ? C13 H13 1.0000 . ? C13 C75 1.515(7) . ? C19 H19 1.0000 . ? C19 C18 1.547(6) . ? C19 C62 1.526(7) . ? C31 C30 1.408(6) . ? C16 H16 1.0000 . ? C16 C37 1.526(7) . ? C27 H27 0.9500 . ? C27 C28 1.392(7) . ? C32 C33 1.514(7) . ? C32 C36 1.523(7) . ? C32 C35 1.521(8) . ? C6 C7 1.526(6) . ? C30 H30 0.9500 . ? C30 C29 1.363(7) . ? C29 H29 0.9500 . ? C29 C28 1.390(8) . ? C38 C39 1.402(6) . ? C38 C43 1.376(6) . ? C38 C37 1.514(6) . ? C7 H7 1.0000 . ? C7 C70 1.546(7) . ? C66 H66A 0.9900 . ? C66 H66B 0.9900 . ? C66 C67 1.503(8) . ? C39 H39 0.9500 . ? C39 C40 1.384(7) . ? C43 H43 0.9500 . ? C43 C42 1.405(7) . ? C65 H65A 0.9800 . ? C65 H65B 0.9800 . ? C65 H65C 0.9800 . ? C37 H37A 0.9900 . ? C37 H37B 0.9900 . ? C9 C10 1.515(7) . ? C40 H40 0.9500 . ? O52 H52 0.8400 . ? O52 C50 1.235(9) . ? C33 H33 0.9500 . ? C33 C34 1.290(8) . ? C70 H70A 0.9900 . ? C70 H70B 0.9900 . ? C70 C71 1.511(7) . ? C68 H68 0.9500 . ? C68 C67 1.303(7) . ? C68 C69 1.526(9) . ? C1AA H1AA 1.0000 . ? C75 H75A 0.9800 . ? C75 H75B 0.9800 . ? C75 H75C 0.9800 . ? C67 H67 0.9500 . ? C10 H10 1.0000 . ? C10 C48 1.546(6) . ? C28 H28 0.9500 . ? C71 H71 1.0000 . ? C71 C73 1.542(10) . ? C71 C72 1.476(10) . ? C48 H48A 0.9900 . ? C48 H48B 0.9900 . ? C48 C49 1.509(9) . ? C63 H63 1.0000 . ? C63 C62 1.512(9) . ? C63 C64 1.491(11) . ? C63 C3AA 1.521(10) . ? C62 H62A 0.9900 . ? C62 H62B 0.9900 . ? C74 H74A 0.9800 . ? C74 H74B 0.9800 . ? C74 H74C 0.9800 . ? C34 H34A 0.9500 . ? C34 H34B 0.9500 . ? C69 H69A 0.9800 . ? C69 H69B 0.9800 . ? C69 H69C 0.9800 . ? C73 H73A 0.9800 . ? C73 H73B 0.9800 . ? C73 H73C 0.9800 . ? O54 H54 0.8400 . ? O54 C53 1.487(12) . ? C49 H49 1.0000 . ? C49 C50 1.474(12) . ? C49 C53 1.556(9) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C50 O51 1.246(9) . ? C64 H64A 0.9800 . ? C64 H64B 0.9800 . ? C64 H64C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C72 H72A 0.9800 . ? C72 H72B 0.9800 . ? C72 H72C 0.9800 . ? C53 H53A 0.9900 . ? C53 H53B 0.9900 . ? C3AA H3AA 0.9800 . ? C3AA H3AB 0.9800 . ? C3AA H3AC 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O56 C15 C16 N17 -92.1(5) . . . . ? O56 C15 C16 C37 27.8(6) . . . . ? O61 C12 C13 N14 -42.8(5) . . . . ? O61 C12 C13 C75 78.2(5) . . . . ? O57 C3 C2AA N5 -7.0(5) . . . . ? O57 C3 C2AA C66 115.7(4) . . . . ? O60 C21 C1AA N2 -59.2(4) . . . . ? O60 C21 C1AA C22 61.4(5) . . . . ? O46 N44 C42 C41 -2.1(7) . . . . ? O46 N44 C42 C43 177.3(4) . . . . ? N25 C26 C31 C23 0.9(5) . . . . ? N25 C26 C31 C30 179.0(4) . . . . ? N25 C26 C27 C28 -177.9(5) . . . . ? N25 C32 C33 C34 -139.1(6) . . . . ? O47 C41 C42 N44 0.1(7) . . . . ? O47 C41 C42 C43 -179.4(4) . . . . ? O47 C41 C40 C39 178.8(4) . . . . ? N2 C3 C2AA N5 174.5(4) . . . . ? N2 C3 C2AA C66 -62.9(5) . . . . ? O59 C6 C7 N8 145.1(4) . . . . ? O59 C6 C7 C70 -89.6(5) . . . . ? N11 C12 C13 N14 139.0(4) . . . . ? N11 C12 C13 C75 -100.1(5) . . . . ? N11 C10 C48 C49 -61.4(6) . . . . ? N14 C15 C16 N17 84.8(5) . . . . ? N14 C15 C16 C37 -155.3(4) . . . . ? N5 C2AA C66 C67 58.2(5) . . . . ? N5 C6 C7 N8 -37.9(6) . . . . ? N5 C6 C7 C70 87.4(5) . . . . ? N8 C7 C70 C71 -59.8(5) . . . . ? N8 C9 C10 N11 36.5(5) . . . . ? N8 C9 C10 C48 160.2(4) . . . . ? N20 C21 C1AA N2 124.4(4) . . . . ? N20 C21 C1AA C22 -115.1(4) . . . . ? N20 C19 C18 O58 -94.9(6) . . . . ? N20 C19 C18 N17 81.8(5) . . . . ? N20 C19 C62 C63 -175.8(5) . . . . ? O45 N44 C42 C41 176.6(4) . . . . ? O45 N44 C42 C43 -4.0(6) . . . . ? N17 C16 C37 C38 -177.7(3) . . . . ? O55 C9 C10 N11 -140.8(5) . . . . ? O55 C9 C10 C48 -17.1(7) . . . . ? C3 N2 C1AA C21 -76.4(4) . . . . ? C3 N2 C1AA C22 165.2(4) . . . . ? C3 C2AA C66 C67 -63.0(5) . . . . ? C23 C22 C1AA N2 177.0(3) . . . . ? C23 C22 C1AA C21 56.6(5) . . . . ? C23 C31 C30 C29 177.0(5) . . . . ? C12 N11 C10 C9 -110.7(5) . . . . ? C12 N11 C10 C48 126.0(4) . . . . ? C2AA N5 C6 O59 7.5(7) . . . . ? C2AA N5 C6 C7 -169.4(4) . . . . ? C2AA C66 C67 C68 114.2(6) . . . . ? C24 N25 C26 C31 -0.7(5) . . . . ? C24 N25 C26 C27 176.8(5) . . . . ? C24 N25 C32 C33 -123.8(5) . . . . ? C24 N25 C32 C36 111.6(5) . . . . ? C24 N25 C32 C35 -7.9(7) . . . . ? C24 C23 C22 C1AA -87.5(5) . . . . ? C24 C23 C31 C26 -0.8(5) . . . . ? C24 C23 C31 C30 -178.5(5) . . . . ? C26 N25 C24 C23 0.2(5) . . . . ? C26 N25 C32 C33 61.2(6) . . . . ? C26 N25 C32 C36 -63.3(6) . . . . ? C26 N25 C32 C35 177.2(5) . . . . ? C26 C31 C30 C29 -0.5(7) . . . . ? C26 C27 C28 C29 -0.5(7) . . . . ? C21 N20 C19 C18 -120.7(4) . . . . ? C21 N20 C19 C62 115.3(5) . . . . ? C15 N14 C13 C12 -64.4(5) . . . . ? C15 N14 C13 C75 175.0(4) . . . . ? C15 C16 C37 C38 65.2(5) . . . . ? C22 C23 C24 N25 175.9(4) . . . . ? C22 C23 C31 C26 -176.2(4) . . . . ? C22 C23 C31 C30 6.1(8) . . . . ? C13 N14 C15 O56 3.4(6) . . . . ? C13 N14 C15 C16 -173.4(4) . . . . ? C19 N20 C21 O60 172.5(4) . . . . ? C19 N20 C21 C1AA -11.2(6) . . . . ? C31 C23 C24 N25 0.4(5) . . . . ? C31 C23 C22 C1AA 87.0(5) . . . . ? C31 C26 C27 C28 -0.7(7) . . . . ? C31 C30 C29 C28 -0.7(8) . . . . ? C16 N17 C18 O58 4.4(8) . . . . ? C16 N17 C18 C19 -172.4(4) . . . . ? C27 C26 C31 C23 -176.9(4) . . . . ? C27 C26 C31 C30 1.2(6) . . . . ? C32 N25 C24 C23 -175.5(4) . . . . ? C32 N25 C26 C31 175.1(4) . . . . ? C32 N25 C26 C27 -7.4(8) . . . . ? C6 N5 C2AA C3 -164.3(4) . . . . ? C6 N5 C2AA C66 73.7(5) . . . . ? C6 C7 C70 C71 172.1(4) . . . . ? C30 C29 C28 C27 1.2(8) . . . . ? C38 C39 C40 C41 1.1(8) . . . . ? C38 C43 C42 N44 -179.3(4) . . . . ? C38 C43 C42 C41 0.2(7) . . . . ? C18 N17 C16 C15 -143.2(4) . . . . ? C18 N17 C16 C37 95.9(5) . . . . ? C18 C19 C62 C63 63.1(6) . . . . ? C7 N8 C9 O55 1.2(7) . . . . ? C7 N8 C9 C10 -176.1(4) . . . . ? C7 C70 C71 C73 -177.8(5) . . . . ? C7 C70 C71 C72 -53.6(7) . . . . ? C39 C38 C43 C42 0.0(6) . . . . ? C39 C38 C37 C16 -92.6(5) . . . . ? C43 C38 C39 C40 -0.6(7) . . . . ? C43 C38 C37 C16 89.9(5) . . . . ? C42 C41 C40 C39 -0.9(7) . . . . ? C65 N11 C12 O61 3.5(6) . . . . ? C65 N11 C12 C13 -178.3(4) . . . . ? C65 N11 C10 C9 67.4(5) . . . . ? C65 N11 C10 C48 -55.9(5) . . . . ? C37 C38 C39 C40 -178.2(4) . . . . ? C37 C38 C43 C42 177.6(4) . . . . ? C9 N8 C7 C6 -101.8(5) . . . . ? C9 N8 C7 C70 134.4(4) . . . . ? C9 C10 C48 C49 174.8(5) . . . . ? C40 C41 C42 N44 179.7(4) . . . . ? C40 C41 C42 C43 0.3(7) . . . . ? C1AA N2 C3 O57 -8.7(6) . . . . ? C1AA N2 C3 C2AA 169.8(4) . . . . ? C10 N11 C12 O61 -178.5(4) . . . . ? C10 N11 C12 C13 -0.2(6) . . . . ? C10 C48 C49 C50 -88.6(6) . . . . ? C10 C48 C49 C53 147.1(6) . . . . ? C48 C49 C50 O52 56.0(9) . . . . ? C48 C49 C50 O51 -125.5(8) . . . . ? C48 C49 C53 O54 -65.4(9) . . . . ? C62 C19 C18 O58 29.5(7) . . . . ? C62 C19 C18 N17 -153.8(4) . . . . ? C74 N20 C21 O60 -3.3(6) . . . . ? C74 N20 C21 C1AA 173.0(4) . . . . ? C74 N20 C19 C18 55.2(5) . . . . ? C74 N20 C19 C62 -68.8(5) . . . . ? C69 C68 C67 C66 175.7(5) . . . . ? C36 C32 C33 C34 -16.9(8) . . . . ? C50 C49 C53 O54 170.3(7) . . . . ? C64 C63 C62 C19 53.0(8) . . . . ? C35 C32 C33 C34 104.4(7) . . . . ? C53 C49 C50 O52 -179.6(8) . . . . ? C53 C49 C50 O51 -1.1(12) . . . . ? C3AA C63 C62 C19 177.4(7) . . . . ? loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.500 -0.002 868 259 ' ' 2 0.500 1.000 -0.012 867 257 ' ' 3 0.500 0.500 0.388 131 44 ' ' 4 0.000 1.000 0.612 131 45 ' ' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 1 9999 517.94 0 0 2 368.49 17.74 0 0 2 315.7 17.7 0 0 3 1635.84 75.28 0 0 3 1336.39 75.18 0 0 4 413.28 23.95 0 0 4 549.47 24.13 0 0 5 93.66 5.79 0 0 6 1131.41 59.1 0 0 7 199.96 11.27 0 0 8 118.78 6.53 0 0 9 0.04 3.51 0 0 9 1.73 1.87 0 0 10 -1.9 3.36 0 0 10 0.95 2.2 0 0 11 0.37 2.41 0 0 11 -0.93 2.87 0 0 12 11.46 2.76 0 0 12 23.14 2.77 0 0 13 2.3 2.27 0 0 14 6.65 1.89 0 0 -15 1.08 2.32 0 -1 1 271.28 13.98 0 1 -1 256.19 14.18 0 1 2 901.73 46.18 0 -1 2 886.58 46.13 0 1 2 881.69 46.13 0 1 3 507.74 25.81 0 -1 3 457.68 25.85 0 1 3 504.71 25.74 0 1 4 126.47 6.19 0 1 4 118.08 6 0 -1 4 106.33 6.3 0 -1 5 121.6 7.35 0 1 5 146.58 7.29 0 1 -5 135.32 10.15 0 1 5 144.33 7.04 0 -1 6 384.97 20.71 0 -1 7 10.01 3.39 0 -1 8 25.4 2.26 0 -1 8 25.66 3.91 0 1 8 26.45 2.13 0 -1 8 24.2 3.6 0 1 9 2.27 1.79 0 -1 9 1.24 1.93 0 1 9 -1.62 3.62 0 -1 9 -0.51 3.43 0 1 10 21.98 2.44 0 -1 10 19.72 2.48 0 1 11 62.36 5.04 0 1 11 82.88 4.79 0 -1 11 85.04 4.87 0 -1 11 64.16 5.14 0 1 12 15.47 2.75 0 1 12 26.09 2.7 0 -1 12 23.49 2.88 0 -1 12 21.23 2.99 0 -1 13 18.32 2.56 0 1 13 17.7 2.43 0 -1 14 14.28 2.07 0 1 14 16.53 1.99 0 1 -15 -0.7 2.5 0 -1 -15 -2.27 2.18 0 -2 0 8.88 0.79 0 2 -1 1372.96 77.54 0 -2 1 1547.63 77.41 0 -2 1 1493.82 77.29 0 -2 2 90.49 4.85 0 2 -2 85.37 6.84 0 2 -3 36.54 6.04 0 -2 4 188.16 9.86 0 2 -4 186.63 11.46 0 -2 4 175.34 10.07 0 2 -5 112.36 9.12 0 -2 5 117.61 6.19 0 -2 5 106.56 6.71 0 -2 6 77.58 5.78 0 -2 6 77.43 5.18 0 -2 7 468.23 25.29 0 -2 7 476.6 25.07 0 2 8 150.66 8.7 0 -2 8 184.89 9.4 0 -2 8 177.32 9.29 0 -2 8 165.15 9.66 0 -2 9 11.42 3.56 0 2 9 7.06 1.85 0 -2 9 1.68 3.29 0 2 10 59.62 5.05 0 -2 10 38.94 4.95 0 -2 11 34.45 3.61 0 2 11 31.94 2.96 0 2 11 26.15 3.41 0 2 12 0.39 2.24 0 -2 12 1.52 2.77 0 2 12 -2.82 2.29 0 -2 13 2.01 2.27 0 2 13 1.6 2.11 0 2 13 1.65 1.89 0 2 14 -0.43 1.71 0 -2 14 1.59 1.81 0 2 -14 0.23 4.33 0 -2 15 -0.61 1.27 0 -2 -15 0.32 1.84 0 2 -15 0.67 2.62 0 -3 0 1.34 1.14 0 3 0 0.22 2.47 0 -3 1 487.67 26.2 0 -3 1 581.71 26.41 0 -3 2 1134.35 61.72 0 -3 2 1224.96 61.5 0 3 -2 1063.43 61.95 0 -3 3 232.1 12.26 0 3 -3 240.14 13.78 0 3 -4 109.01 8.57 0 -3 5 220.2 13.54 0 -3 5 255.88 13.14 0 -3 6 47.33 4.9 0 -3 6 50.15 4.11 0 -3 7 0.71 3.57 0 -3 7 -0.78 2.68 0 3 -8 20.21 7.55 0 3 8 22.41 2.09 0 -3 8 19.24 3.84 0 -3 8 24.74 3.22 0 -3 8 23.65 2.28 0 -3 9 16.12 3.88 0 -3 9 16.82 3.36 0 3 9 18.24 2.08 0 -3 9 16.87 2.34 0 -3 9 15.58 3.01 0 3 10 14.19 3.59 0 -3 10 15.59 2.5 0 3 10 14.7 2.28 0 -3 10 14.43 3.37 0 3 11 18.47 3.15 0 -3 11 24.84 3.53 0 3 11 28.87 2.67 0 3 12 33.61 2.96 0 3 13 25.03 2.48 0 3 -14 3.42 4.43 0 3 -15 -1.68 2.68 0 4 0 617.64 33.5 0 -4 0 640.42 33.09 0 -4 1 2503.69 115.22 0 -4 -1 2043.14 115.11 0 4 -2 251.73 15.28 0 -4 2 279.27 14.44 0 -4 2 276.63 14.82 0 -4 3 6.27 1.05 0 -4 3 6.14 2.42 0 4 -3 7.21 4.05 0 4 -4 361.35 20.24 0 -4 5 11.4 3.08 0 4 -5 13.73 6.96 0 -4 6 187 9.93 0 4 -6 165.14 12.69 0 -4 6 159.98 10.51 0 -4 7 9.01 3.08 0 -4 7 5.67 2.76 0 -4 7 4.51 3.58 0 4 -7 9.32 7.18 0 -4 8 48.95 3.98 0 4 -8 44.4 7.91 0 -4 8 52.11 3.25 0 4 8 42.38 3.03 0 -4 8 43.88 4.7 0 -4 9 83.5 6.38 0 4 9 77.75 4.81 0 -4 9 84.5 5.02 0 -4 9 75.66 5.54 0 -4 10 0.81 2.37 0 -4 10 4.49 3.86 0 4 10 1.97 1.97 0 -4 10 0.09 3.28 0 -4 11 52.08 3.75 0 4 11 45.04 3.44 0 -4 11 47.38 4.28 0 4 12 8.16 2.15 0 -4 12 8.07 2.61 0 4 -13 1.29 6.33 0 -4 13 6.86 2.2 0 -4 14 0.29 1.68 0 4 -14 0.78 4.59 0 4 -15 -1.52 2.68 0 -4 15 -0.37 1.13 0 -5 0 -0.12 1.66 0 5 0 -0.19 3.33 0 -5 1 4.04 1.9 0 -5 -1 6.99 1.55 0 5 -2 584.26 31.64 0 -5 2 592.52 30.85 0 -5 2 601.86 31.22 0 -5 3 451.79 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13.86 7.25 0 -6 8 19.8 4.47 0 -6 8 23.31 4.11 0 6 8 15.03 1.81 0 -6 8 20.5 3.01 0 -6 8 19.84 2.35 0 -6 9 -3.06 4.13 0 -6 9 2.6 2.96 0 -6 9 3.27 5.03 0 -6 9 1.26 2.25 0 6 9 1.01 1.71 0 -6 10 -0.6 2.8 0 -6 10 4.26 2.52 0 -6 10 -2.05 4.09 0 6 10 5.69 1.88 0 -6 11 1.7 2.36 0 -6 12 -1.89 2.31 0 6 -12 5.88 7.33 0 -6 13 1.16 1.95 0 6 -13 10.78 6.22 0 -6 14 1.16 1.51 0 -6 15 0.88 0.86 0 7 0 -0.78 4.81 0 -7 0 -0.22 2.29 0 -7 -1 34.31 3.04 0 -7 1 30.86 1.89 0 -7 1 36.06 3.48 0 -7 -2 21.83 2.77 0 7 -2 21.6 5.75 0 -7 2 22.3 1.64 0 -7 2 16.75 3.82 0 -7 3 596.09 28.69 0 7 -3 571.23 30.23 0 -7 3 526.87 29.42 0 7 -4 145.33 10.79 0 7 -5 330.07 19.52 0 -7 6 132.17 8.58 0 -7 6 127.12 7.56 0 -7 6 129.35 8.05 0 7 -6 125.67 10.29 0 -7 7 203.79 10.65 0 -7 7 185.47 10.38 0 7 -7 205.13 13.33 0 -7 7 172.76 9.86 0 -7 8 4.91 4.41 0 7 -8 6.54 7.22 0 -7 8 0.95 2.12 0 -7 8 3.98 2.9 0 -7 9 0.96 4.17 0 -7 9 3.13 2.33 0 -7 9 1.33 5.12 0 -7 9 3.96 3.01 0 -7 10 8.89 2.57 0 -7 10 7.25 2.92 0 -7 10 5.35 4.1 0 -7 10 4.86 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9.39 0 -9 -3 37.78 3.8 0 -9 3 38.57 5.15 0 9 -3 40.71 7.23 0 9 -4 281.61 17.41 0 9 -5 125.99 9.75 0 9 -5 117.23 6.84 0 9 -6 176.56 10.13 0 9 -6 184.63 13 0 -9 6 194.4 11.33 0 -9 6 180.91 10.74 0 -9 6 180.67 9.8 0 -9 7 169.3 9.19 0 -9 7 151.12 9.66 0 -9 7 185.08 10.22 0 -9 7 164.65 10.67 0 9 -7 165.19 12.97 0 9 -7 173.76 9.82 0 -9 8 152.11 10.6 0 9 -8 178.71 10.13 0 -9 8 149.11 9.66 0 -9 8 172.15 9.24 0 -9 8 182.2 10.38 0 9 -8 158.76 13.69 0 -9 9 27.82 2.81 0 9 -9 27 5.34 0 -9 9 19.22 3.33 0 -9 9 15.82 5.48 0 -9 10 0.45 2.35 0 -9 10 1.43 5.36 0 9 -10 -1.82 5.73 0 9 -11 3.76 5.9 0 -9 11 9.45 2.21 0 -9 11 2.08 5.56 0 9 -12 -0.49 5.55 0 -9 12 1.25 1.86 0 -9 13 5.65 1.5 0 9 -13 6.37 4.8 0 9 -14 7.97 3.25 0 -10 0 13.27 3.83 0 -10 1 1.24 3.86 0 -10 -1 0.04 3.39 0 -10 2 177.82 10.94 0 -10 -2 175.87 10.31 0 10 -3 81.22 8.48 0 -10 3 75.47 6.7 0 10 -4 93.5 8.55 0 10 4 69.27 5.24 0 10 -5 128.87 7.18 0 10 5 114.95 7.65 0 -10 6 42.47 5.21 0 10 -6 35.43 3.57 0 -10 6 41.41 3.82 0 10 -6 39.93 7.58 0 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28.93 6.14 0 16 -1 27.52 6.41 0 16 -2 107.17 8.88 0 16 2 108.1 8.44 0 16 3 50.72 6.2 0 16 4 36.54 5.44 0 16 -4 42.59 6.85 0 16 5 38.59 5.27 0 16 -5 50.39 7.19 0 16 -6 16.32 6.56 0 -16 7 11.66 5.07 0 16 -7 9.58 6.43 0 -16 8 5.18 4.8 0 16 -8 -2.36 6.53 0 -16 9 3.12 4.21 0 16 -9 -1.77 5.95 0 -16 10 -0.38 3.76 0 17 0 -4.21 5.85 0 17 1 -0.41 5.68 0 17 -1 -2.04 5.96 0 17 2 1.16 5.45 0 17 -2 7.74 6.34 0 -17 3 2.44 7.42 0 17 3 3.08 5.23 0 17 4 15.09 5.04 0 17 -4 6.59 6.32 0 -17 4 8.45 6.52 0 -17 5 5.51 5.83 0 17 5 9.38 4.6 0 17 -5 9.25 6.16 0 17 -6 -0.83 6.04 0 17 -7 5.68 5.83 0 -17 7 3.97 4.66 0 -17 8 -1.01 4.42 0 17 -8 1.46 5.75 0 17 -9 -1.8 5.05 0 -17 9 -2.51 3.71 0 18 0 39.51 6.18 0 18 -1 20.08 5.91 0 18 1 17.07 5.58 0 -18 2 5.37 7.52 0 18 -2 9.72 5.84 0 18 2 17.98 5.21 0 -18 3 1.15 6.97 0 18 3 22.39 5.08 0 18 -4 6.66 5.71 0 18 4 0.88 4.33 0 -18 4 -0.17 6.14 0 18 5 -0.09 3.89 0 -18 5 -0.72 5.61 0 18 -5 3.49 5.54 0 18 -6 14.14 5.56 0 18 -7 -0.23 5.18 0 -18 8 10.27 3.93 0 18 -8 5.57 4.79 0 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7.8 4 7 -7 0.39 7.7 -4 7 7 2.63 3.96 -4 7 7 1.53 2.21 4 -7 7 1.74 1.66 4 -7 7 6.32 3.42 4 -7 7 2.71 4.03 4 -7 7 2.91 2.28 4 -7 6 7.75 3.5 4 7 -6 9.62 7.33 -4 7 6 4.8 3.17 4 -7 6 6.28 3.71 4 -7 6 5.42 2.31 4 -7 5 88.7 5.47 4 -7 5 96.22 6.43 4 7 -5 89.78 9.03 4 -7 4 296.6 16.22 4 7 -4 285.55 18.08 4 7 -2 195.03 13.33 -4 -7 -2 217.05 11.86 -4 -7 -1 174.12 9.51 4 -7 1 152.64 9.29 4 7 -1 165.91 10.76 -4 -7 0 56.93 4.29 4 -7 0 50.46 3.85 4 7 0 45.74 6.26 4 -7 -1 122.54 7.32 -4 -7 1 149.52 7.96 -4 -7 2 215.96 11.69 -4 7 -2 210.6 12.74 -4 -7 2 196.66 10.75 -4 7 -3 13.36 6.12 -4 -7 3 17.13 4.41 -4 -7 3 15.05 2.07 -4 -7 4 277.35 14.83 -4 7 -4 279.84 16.39 -4 -7 5 93.46 5.58 -4 7 -5 96.88 7.79 -4 7 -6 2.63 4.94 -4 -7 6 5.35 2.6 -4 7 -6 6.81 2.9 -4 -7 6 5.46 2 -4 -7 7 5.08 4.03 -4 -7 7 3.6 2.81 -4 7 -7 -0.02 3.32 -4 7 -7 -0.08 5.04 -4 -7 7 0.65 2.11 -4 -7 7 7.33 3.25 -4 -7 7 1.07 4.6 -4 -7 8 50 3.85 -4 -7 8 47.05 4.53 -4 -7 8 55.09 4.38 -4 -7 8 52.5 5.77 -4 -7 8 59.22 5.33 -4 7 -8 55.04 5.2 -4 -7 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4.09 4 -9 9 11.93 2.24 4 9 -9 25.3 10.39 4 9 -9 17.69 5.19 4 -9 9 10.61 5.76 4 -9 8 5.3 3.98 4 -9 8 0.62 4.97 -4 9 8 14.81 6.82 4 9 -8 5.74 8.96 4 -9 7 25.18 4.37 4 -9 7 31.01 4.76 -4 9 7 19.4 4.16 4 9 -7 32.58 8.55 4 -9 6 138.93 7.98 4 -9 6 131.19 8.1 4 9 -6 115.31 7.18 4 9 -6 128.41 10.97 -4 9 6 110.77 7.66 4 -9 5 68.32 4.4 -4 9 5 60.2 5.16 4 -9 5 74.17 5.59 4 9 -5 69.64 8.39 4 -9 4 3.83 3.96 -4 9 4 0.69 3.38 -4 -9 -4 1.71 2.87 4 -9 4 -0.82 4.01 -4 -9 -3 181.57 10.52 -4 -9 -2 636.46 33.24 4 9 -2 594.76 34.41 4 -9 1 139.1 8.91 4 9 -1 158.42 11.32 -4 -9 -1 145.14 8.74 -4 -9 0 30.84 4.22 4 -9 0 38.26 3.98 4 9 0 40.51 6.81 -4 -9 1 139.04 8.91 -4 -9 2 616.81 33.03 -4 -9 3 194.82 11.71 -4 9 -3 190.17 12.53 -4 9 -4 3.52 5.7 -4 -9 4 4.73 4.13 -4 -9 5 71.23 4.52 -4 9 -5 82.56 7.95 -4 -9 5 74.14 6.67 -4 9 -5 71.59 4.74 -4 -9 6 111.31 6.62 -4 9 -6 131.35 9.86 -4 9 -6 119.58 6.97 -4 -9 7 29.95 3.07 -4 9 -7 28.79 3.97 -4 -9 7 39.02 5.04 -4 9 -7 35.34 6.95 -4 -9 8 6.19 4.64 -4 -9 8 4.84 4.74 -4 -9 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44.11 7.41 -4 -10 -2 51.36 4.63 -4 -10 -1 49.48 4.47 4 10 -1 51.19 7.19 -4 -10 0 14.48 3.53 -4 -10 1 47.75 4.96 -4 -10 2 54 5.36 -4 -10 3 204.33 12.34 -4 -10 4 34.52 5.12 -4 10 -4 37.76 3.04 -4 10 -4 39.76 6.33 -4 -10 5 8.6 4.67 -4 -10 5 11.03 2.28 -4 10 -5 12.4 6.12 -4 10 -5 12.14 2.62 -4 -10 6 7.92 2.35 -4 10 -6 9.25 6.29 -4 10 -6 8.49 2.96 -4 -10 7 78.32 7.21 -4 10 -7 60 8.3 -4 10 -7 68.35 5.31 -4 -10 7 81.7 6.44 -4 -10 7 67.28 4.7 -4 -10 8 1.81 2.67 -4 10 -8 6.59 3.97 -4 -10 8 3 3.3 -4 -10 8 1.38 4.74 -4 10 -9 43.8 5.11 -4 -10 9 33.02 3.98 -4 -10 9 42.8 3.51 -4 -10 9 45.19 5.47 -4 -10 10 4.26 2.41 -4 -10 10 0.12 4.84 -4 10 -10 5.31 4.73 -4 -10 11 6.75 2.18 -4 10 -11 10.37 4.86 -4 10 -12 -0.05 4.31 -4 -10 12 2.36 1.74 -4 10 -13 3 3.47 -4 -10 13 0.01 1.27 4 11 -13 -1.83 2.99 4 11 -12 5.85 4.07 4 -11 11 -0.57 5.59 4 11 -11 19.63 4.45 4 11 -10 15.57 4.17 4 -11 10 1.45 5.51 4 -11 9 3.79 5.66 4 11 -9 4.91 3.71 -4 11 8 50.46 7.34 4 -11 8 48.25 5.46 4 -11 8 55.18 6.34 4 11 -8 48.86 4.45 4 11 -8 59.18 10.7 4 11 -7 27.58 8.98 4 -11 7 22.29 4.59 4 -11 7 26.25 5.44 -4 11 7 20.9 4.66 4 -11 6 3.5 4.2 4 11 -6 -1.38 7.67 -4 11 6 2.98 4.6 -4 11 5 24.47 4.68 4 11 -5 26.49 7.58 4 -11 5 32.7 4.8 4 -11 5 33.15 5.14 4 -11 4 33.78 5.41 4 -11 4 42.11 4.94 -4 11 4 40.61 4.79 -4 -11 -4 45.72 4.59 -4 11 3 7.43 3.91 4 -11 3 6.57 4.3 -4 -11 -3 7.5 3.25 4 11 -3 7.3 6.73 -4 11 2 96.25 6.8 4 11 -2 98.26 9.43 -4 -11 -2 106.56 6.92 -4 11 1 75.64 5.89 4 11 -1 79.54 8.14 -4 -11 -1 84.32 6.14 -4 -11 0 29.7 4.28 4 11 1 77.56 5.74 -4 11 -1 74.37 5.94 -4 -11 1 81.44 6.35 -4 11 -2 87.79 6.8 -4 -11 2 92 7.15 4 11 2 104.45 6.46 -4 11 -3 5.33 2.07 -4 -11 3 6.86 4.18 4 11 3 6.98 3.21 -4 -11 4 44.46 5.72 -4 11 -4 38 3.13 -4 11 -5 22.18 2.89 -4 11 -6 -0.64 2.9 -4 -11 6 -0.1 2.45 -4 -11 7 24.68 3.88 -4 -11 7 27.24 5.76 -4 -11 7 25.25 3.07 -4 11 -7 27.25 3.78 -4 -11 7 27.67 5.45 -4 -11 8 41.33 4.45 -4 -11 8 47.5 5.97 -4 11 -8 58.34 4.93 -4 -11 8 49.32 3.87 -4 -11 8 57.83 5.86 -4 -11 9 7.3 2.5 -4 -11 9 8.4 4.94 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2.72 -4 -12 4 24.42 5.67 -4 12 -5 55.54 4.09 -4 12 -6 118.57 7.07 -4 -12 7 3.01 3.23 -4 12 -7 4.1 3.13 -4 -12 7 -1.35 2.56 -4 -12 7 1.56 4.96 -4 -12 7 5.58 5.18 -4 -12 8 15.32 2.68 -4 12 -8 15.05 3.54 -4 -12 8 18.79 5.14 -4 -12 9 1.34 4.8 -4 -12 9 0.6 2.23 -4 12 -9 1.25 3.64 -4 12 -10 6.34 3.81 -4 -12 10 5.08 2.05 -4 -12 10 1.84 4.58 -4 12 -11 14.4 3.83 -4 -12 11 10.15 1.75 -4 12 -12 0.29 3.31 4 -13 11 -0.02 4.83 4 -13 10 3.46 5.29 4 -13 9 1.01 5.3 -4 13 8 -3.04 6.95 4 -13 8 5.32 5.51 4 -13 7 -0.7 4.1 4 13 -7 10.26 8.56 4 -13 7 0.03 5.36 -4 13 7 -1.04 4.61 4 13 -6 -5.81 8.17 4 -13 6 3.82 4.34 -4 13 6 0.5 5.07 4 13 -5 51.86 9.06 -4 13 5 52.26 6.05 4 -13 5 51.19 6.57 4 -13 4 17.98 6.13 -4 13 4 35.34 5.41 4 13 -3 9.69 7.2 -4 13 3 -3.07 4.93 -4 13 2 88.72 7.11 -4 13 1 3.07 4.8 -4 -13 -1 0.33 4.24 4 13 -1 3.9 4.95 -4 -13 0 70.64 6.62 4 13 0 66.27 6.31 -4 13 -1 4.82 5.01 4 13 1 0.17 4.44 -4 -13 1 3.4 4.8 -4 13 -2 90.71 7.17 -4 -13 2 85.34 7.61 4 13 2 86.48 6.64 -4 13 -3 2.02 5.28 -4 -13 3 2.22 5.03 4 13 3 5.62 4.13 -4 -13 4 31.88 6.13 -4 13 -4 31.46 5.86 -4 13 -4 25.49 2.84 -4 13 -5 55.54 6.62 -4 13 -5 44.42 3.74 -4 -13 6 5.29 5.71 -4 -13 6 8.52 5.39 -4 13 -6 2.66 5.96 -4 13 -6 3.55 2.76 -4 -13 7 -1.28 5.26 -4 13 -7 0.31 6.08 -4 13 -7 6.02 2.95 -4 -13 7 0.71 4.63 -4 13 -8 8.8 3.26 -4 13 -8 8.03 6.03 -4 -13 8 10.27 4.92 -4 13 -9 4.4 3.31 -4 -13 9 7.51 4.69 -4 -13 10 6.03 4.42 -4 13 -10 5.34 3.34 -4 13 -11 -1.37 3.17 -4 13 -12 0.1 2.64 4 14 -11 -1.52 7.17 4 -14 10 6.71 4.97 4 -14 9 0.93 5.27 -4 14 8 3.47 7.25 4 -14 8 0.54 5.44 -4 14 7 12.17 4.81 4 14 -6 20.25 8.28 -4 14 6 28.43 5.58 4 -14 6 31.82 6 -4 14 5 83.63 7.28 4 14 -5 82.2 10.29 4 -14 5 80.63 7.96 -4 14 4 18.73 5.65 4 -14 4 16.03 6.69 -4 14 3 96.23 7.26 4 -14 3 49.11 8.17 -4 14 2 152.95 10.13 4 14 -1 108.23 8.18 -4 14 1 104.53 8.17 4 14 0 87.21 7.57 -4 -14 0 104.09 8.33 -4 -14 1 100.87 8.75 4 14 1 105.34 7.85 -4 -14 2 147.6 10.85 4 14 2 144.5 9.52 -4 14 -2 158.55 10.16 4 14 3 112 7.47 -4 14 -3 94.37 8.25 -4 -14 3 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7.53 3.17 5 -5 11 12.72 2.42 5 -5 10 180.31 8.23 5 5 -10 232.77 19.3 5 -5 9 -2.29 5.52 5 -5 9 5.62 1.98 5 5 -9 16.33 12.5 -5 5 9 5.9 7.56 5 -5 8 -1.21 4.63 5 5 -8 5.84 11.03 5 -5 8 3.93 1.68 -5 5 8 -7.61 8.1 5 -5 7 4.14 4.05 5 -5 7 8.37 2.07 -5 5 7 6.03 5.3 5 -5 7 9.52 3.43 5 -5 7 8.15 1.62 -5 5 7 4.88 2.3 5 5 -7 -0.41 9.54 -5 5 7 8.03 1.72 5 -5 6 81.89 5.87 5 -5 6 81.6 5.06 5 -5 5 385.27 21.43 5 -5 5 402.14 21.09 5 5 -4 45.04 14.1 5 -5 4 40 4.17 5 -5 4 37.77 3.02 5 5 -3 407.11 23.07 5 -5 3 385.27 19.78 5 -5 3 364.19 19.43 5 5 -2 1108.56 61.6 5 -5 2 1194.67 60.9 5 5 -2 1141.7 62.2 5 -5 1 433.73 22.76 5 5 -1 432.7 23.53 -5 -5 0 859.58 43.52 5 5 0 783.57 43.84 5 5 1 485.43 25.99 -5 5 -2 1208.28 63.34 -5 -5 3 390.87 20.69 -5 -5 3 374.03 20.18 -5 5 -3 410.42 20.98 -5 5 -4 44.09 5.16 -5 -5 4 42 3.31 -5 -5 4 38.95 5.08 -5 -5 5 368.77 21.69 -5 -5 5 394.67 20.82 -5 5 -5 407.68 21.67 -5 5 -6 89.67 6.83 -5 -5 6 82.35 5.24 -5 -5 7 3.59 4.27 5 5 7 3.38 1.48 -5 -5 7 6.59 3.29 -5 -5 7 6.5 2.04 -5 -5 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139.82 16.26 5 -6 4 103.31 6.22 5 -6 4 123.3 7.11 5 -6 3 148.96 8 5 6 -3 167.27 15.72 5 -6 2 82.99 5.36 5 6 -2 86.79 12.1 5 6 -2 88.57 7.26 -5 -6 -1 184.88 10.01 5 6 -1 168.27 11.06 -5 -6 0 77.15 4.91 5 6 0 66.97 5.97 5 -6 -1 148.5 8.31 5 6 1 165.32 9.73 -5 -6 1 174.7 8.91 -5 -6 2 74.91 5.5 -5 6 -2 80.4 6.23 -5 -6 3 141.93 7.94 -5 6 -3 154.15 9.64 -5 6 -4 112.68 8.63 -5 -6 4 118.21 6.62 -5 -6 4 108.29 7.88 -5 6 -5 66.32 6.21 -5 -6 5 68.45 6.36 -5 -6 5 59.32 4.16 -5 6 -6 301.24 16.25 -5 6 -6 297.47 14.89 -5 -6 6 287.71 14.88 -5 -6 6 251.47 14.62 -5 -6 7 18.62 3.12 -5 -6 7 15.82 3.51 -5 -6 7 17.64 4.67 -5 6 -7 25.24 3.64 -5 -6 7 16.24 2.4 -5 -6 8 35.52 3.22 -5 -6 8 35.8 4.15 -5 -6 8 37.25 5.23 -5 -6 8 31.66 3.76 -5 -6 9 88.2 5.5 -5 -6 9 88.62 6.25 -5 -6 9 86.58 5.91 -5 -6 9 81.74 6.91 -5 -6 10 25.95 3.19 -5 -6 10 21.4 3.76 -5 -6 10 26.09 4.61 -5 -6 10 18.16 3.72 -5 -6 11 5.07 2.8 -5 6 -11 9.41 5.9 -5 -6 11 4.35 3.34 -5 6 -12 19.01 5.78 -5 -6 12 16.33 2.72 -5 6 -13 3.16 4.5 -5 -6 13 6.82 2.11 -5 6 -14 0.53 3.24 -5 -6 14 0.24 1.48 5 7 -14 -4.53 4.91 5 7 -13 -0.04 7.21 5 -7 13 0.47 1.62 5 -7 12 11.14 2.03 5 7 -12 18.79 8.38 5 -7 11 0.03 6.81 5 -7 11 12.4 2.22 5 7 -10 44.98 12.68 5 -7 10 34.9 2.83 -5 7 9 -2.21 9.89 5 -7 9 -2.25 3.8 5 7 -9 1.03 11.28 5 -7 9 2.4 5.41 5 -7 9 2.2 2.01 5 -7 8 1 1.83 5 -7 8 3.29 3.74 5 -7 8 3.1 2.26 5 7 -8 -0.51 9.96 -5 7 8 -9.46 7.84 5 -7 8 2.38 4.92 5 -7 7 89.61 5.92 5 -7 7 78.25 4.97 -5 7 7 77.13 4.83 5 7 -7 92.3 10.49 5 -7 7 82.19 4.51 -5 7 7 69.55 6.02 -5 7 6 17.96 2.27 5 -7 6 9.75 3.72 5 -7 6 10.36 2.19 5 -7 6 13.91 3.47 -5 7 6 9.83 3.3 5 7 -6 19.17 7.95 5 -7 5 8.67 3.3 5 -7 5 7.97 2.19 5 7 -5 8.06 7.29 5 -7 4 222.87 12.22 5 -7 4 241.12 12.86 5 -7 3 34.47 4.27 5 7 -3 30.65 7.34 -5 -7 -2 151.1 8.8 5 7 -2 141.92 10.65 -5 -7 -1 825.52 42.77 5 7 -1 785.54 43.59 5 7 0 335.67 18.01 -5 -7 0 341.49 17.01 5 -7 0 290.71 16.61 -5 -7 1 719.07 36.92 5 -7 -1 678.18 36.56 5 7 1 772.6 37.71 -5 -7 2 143.93 8.01 -5 -7 2 158.66 9.23 -5 -7 3 33.76 2.87 -5 -7 3 35.09 5.22 -5 7 -3 41.28 6.38 -5 7 -4 261.8 13.65 -5 -7 4 206.28 11.68 -5 7 -5 11.29 5.04 -5 -7 5 8.28 2.03 -5 -7 6 11.06 2.23 -5 7 -6 14.29 2.96 -5 -7 6 12.89 2.77 -5 7 -6 13.71 4.88 -5 -7 6 10.95 2.12 -5 -7 7 96.1 5.85 -5 7 -7 96.28 6.19 -5 -7 7 98.35 7.35 -5 7 -7 96.71 8.15 -5 -7 7 84.16 5.55 -5 -7 7 101.32 6.6 -5 -7 8 0.97 2.52 -5 7 -8 -0.02 4.1 -5 -7 8 1.37 4.53 -5 -7 8 -0.53 3.31 -5 -7 8 2.14 3.07 -5 -7 9 4.09 2.71 -5 7 -9 8.13 5.01 -5 -7 9 1.67 3.38 -5 -7 9 5.34 4.46 -5 -7 9 4.71 3.39 -5 -7 10 30.71 4.79 -5 -7 10 32.98 3.94 -5 -7 10 33.31 3.38 -5 -7 10 25.14 3.93 -5 -7 11 9.81 2.8 -5 -7 12 13.35 2.52 -5 -7 13 -0.14 1.92 -5 7 -13 8.89 4.43 -5 -7 14 1.94 1.37 -5 7 -14 6.63 3.06 5 8 -14 0.92 4.19 5 8 -13 15.82 6.44 5 -8 13 16.35 1.73 5 -8 12 1.94 1.74 5 8 -12 2.63 7.41 5 -8 11 5.47 2.05 5 -8 11 0.19 6.46 5 8 -11 12.18 7.4 5 -8 10 -0.09 2.11 5 8 -10 6.04 11.8 5 -8 10 -1.85 6.22 5 -8 9 30.8 2.69 5 -8 9 31.02 4.52 -5 8 9 45.75 11.12 5 8 -9 35.27 11.35 5 8 -8 40.6 10.3 -5 8 8 33.33 7.71 5 -8 8 30.64 4.51 5 -8 8 32.38 2.6 -5 8 7 92.72 5.52 5 -8 7 82.01 6.71 5 -8 7 99.5 6.61 5 -8 7 88.35 5.61 5 8 -7 105.94 10.81 -5 8 7 86.81 6.46 5 -8 6 92.47 6.42 -5 8 6 87.56 5.44 5 -8 6 111.1 6.5 5 -8 6 90.48 5.5 -5 8 6 84.25 6.2 5 8 -6 101.08 9.68 5 8 -5 57.43 7.42 5 -8 5 60.4 4.94 5 -8 5 56.11 3.69 -5 8 5 41.02 4.54 5 -8 4 28.36 4.01 5 -8 4 21.94 2.54 5 8 -3 11.95 6.5 5 -8 3 4.77 3.74 -5 -8 -2 627.79 33.81 5 8 -2 666.19 35.01 -5 -8 -1 494.77 26.19 5 8 -1 472.53 27.24 -5 -8 0 311.07 16.57 5 -8 0 292.14 16.26 5 8 0 315.29 18.15 -5 -8 1 464.27 24.94 -5 -8 2 634.22 32.38 -5 -8 2 597.54 31.68 -5 8 -3 6.87 5.35 -5 -8 3 4.81 4.51 -5 -8 3 5.5 1.83 -5 8 -4 21.46 5.23 -5 -8 4 26.32 5.16 -5 -8 4 27.27 2.49 -5 8 -5 59.32 6.34 -5 -8 5 57.69 3.75 -5 8 -5 56.52 3.96 -5 -8 5 50.85 3.76 -5 8 -6 101.94 5.78 -5 8 -6 95.13 7.94 -5 -8 6 92.94 5.36 -5 -8 7 110.95 8.03 -5 8 -7 113.28 6.62 -5 -8 7 96.27 7.04 -5 -8 7 93.8 6.23 -5 -8 7 95.92 5.92 -5 8 -7 94.64 8.76 -5 -8 8 33.57 3.41 -5 -8 8 34.41 4.24 -5 -8 8 30.76 5.32 -5 8 -8 40.26 4.72 -5 -8 8 31.55 3.8 -5 -8 8 47.32 5.11 -5 -8 9 26.39 3.98 -5 -8 9 31.51 3.4 -5 -8 9 30.18 5.08 -5 8 -9 39.16 5.18 -5 8 -10 9.95 5.3 -5 -8 10 4.35 3.95 -5 -8 10 -0.13 2.76 -5 -8 10 1.69 3.06 -5 -8 11 6.68 2.63 -5 8 -11 7.46 5.52 -5 -8 12 -0.48 2.14 -5 -8 13 14.1 1.99 -5 -8 14 0.79 1.12 5 -9 12 21.27 2.04 5 9 -12 26.01 6.35 5 -9 11 7.48 1.94 5 -9 11 2.58 6.3 5 9 -11 11.24 6.51 5 9 -10 -2.31 5.92 5 -9 10 2.04 2 5 -9 10 -0.09 6.11 -5 9 9 38.97 11.33 5 9 -9 52.13 12.12 5 -9 9 47.8 5 5 9 -9 52.82 5.84 -5 9 8 21.99 7.31 5 -9 8 18.76 5.43 5 -9 8 23.84 4.43 5 9 -8 24.92 9.94 5 9 -7 15.1 8.37 -5 9 7 12.09 4.18 5 -9 7 11.27 3.93 5 -9 7 13.06 4.57 5 -9 6 13.95 4.28 5 -9 6 10 3.68 5 9 -6 14.72 7.44 -5 9 6 7.59 3.96 -5 9 5 62.94 5.24 5 9 -5 78.44 8.52 5 -9 5 70.02 5.44 -5 9 4 148.68 9.68 5 -9 4 182.06 10.11 -5 -9 -4 171.89 10.03 5 -9 4 180.99 9.95 5 9 -3 156.37 11.92 -5 -9 -3 181.36 10 5 -9 3 157.99 10.06 -5 -9 -2 423.08 22.63 5 9 -2 404.09 23.83 5 9 -1 259.35 15.92 -5 -9 -1 249.63 14.2 -5 -9 0 2.66 3.72 5 9 0 3.98 6.41 -5 -9 1 242.75 13.85 -5 -9 2 382.4 21.62 -5 -9 2 400.53 20.88 -5 -9 3 149.67 9.71 -5 -9 4 154.92 10.51 -5 9 -4 169.68 9.16 -5 9 -4 164.06 11.18 -5 9 -5 73.07 4.79 -5 -9 5 71.71 6.6 -5 -9 5 75.54 4.62 -5 9 -5 73.83 7.5 -5 -9 6 9.73 2.38 -5 9 -6 9.3 5.78 -5 9 -6 10.69 3 -5 9 -7 15.47 6.04 -5 9 -7 15.49 3.64 -5 -9 7 17.56 2.79 -5 -9 7 19.17 4.64 -5 -9 8 32.74 5.4 -5 9 -8 27.88 4.35 -5 -9 8 26.15 3.23 -5 -9 8 24.65 3.92 -5 -9 8 31.43 4.98 -5 -9 9 52.3 5.79 -5 9 -9 49.87 5.49 -5 -9 9 45.26 4.61 -5 -9 9 53.95 5.66 -5 -9 9 50.35 4.06 -5 -9 10 -0.16 2.68 -5 9 -10 0.36 5.04 -5 -9 11 9.19 2.5 -5 9 -11 12.22 5.21 -5 -9 12 26.31 2.58 -5 9 -12 29.37 5.07 -5 -9 13 2.64 1.55 -5 9 -13 -4.14 3.84 -5 -9 14 1.03 0.93 -5 9 -14 2.59 2.46 5 10 -13 5.36 4.07 5 10 -12 15.72 5.18 5 10 -11 0.56 5.07 5 -10 11 -1.81 5.98 5 -10 10 0.29 6.14 5 10 -10 19.53 5.12 5 10 -9 67.18 12.35 5 10 -9 71.45 5.68 -5 10 9 56.96 11.48 5 -10 9 57.86 5.45 5 -10 8 174.17 10.65 5 10 -8 194.69 10.11 -5 10 8 150.38 11.77 5 -10 8 129.77 10.8 5 10 -8 206.43 16 5 10 -7 30.66 9.54 -5 10 7 18.22 4.63 5 -10 7 25.95 4.5 5 -10 7 30.83 5.17 5 10 -6 217.36 14.76 -5 10 6 188.16 11.4 5 -10 6 194.26 11.63 5 -10 5 2.83 4.27 -5 10 5 0.21 3.84 5 10 -5 2.04 6.52 5 -10 5 2.3 3.8 -5 -10 -5 -0.38 3.04 5 -10 4 8 4.36 5 -10 4 9.42 3.67 -5 -10 -4 8.6 3.03 -5 10 4 9.44 3.7 5 -10 3 3.53 3.71 -5 10 3 7.48 3.52 -5 -10 -3 8.1 3.52 5 10 -3 0.55 6.19 5 -10 2 32.08 4.25 5 10 -2 28.48 6.76 -5 10 2 29.83 4.03 -5 -10 -2 29.86 3.72 5 10 -1 91.8 8.79 -5 -10 -1 102.72 6.9 5 10 0 51.07 7.26 -5 -10 0 47.43 4.83 -5 -10 1 87.56 6.64 -5 10 -2 36.79 4.38 -5 -10 2 37.14 4.97 -5 10 -3 9.57 2.12 -5 -10 3 11.3 4.55 -5 -10 4 10.07 2.22 -5 10 -4 11.19 2.31 -5 -10 4 7.77 4.57 -5 -10 5 3.39 2.29 -5 10 -5 3 2.57 -5 -10 5 -1.37 4.74 -5 -10 6 194.79 10.96 -5 10 -6 212.8 11.19 -5 10 -6 183.46 13.58 -5 -10 7 33.63 3.36 -5 10 -7 36.13 4.12 -5 -10 7 35.51 5.24 -5 -10 8 224.02 11.66 -5 10 -8 202.17 11.26 -5 -10 8 192.07 10.77 -5 -10 8 169.1 11.26 -5 -10 9 72 6.15 -5 -10 9 64.3 4.53 -5 10 -9 71.43 5.88 -5 -10 9 61.1 6.13 -5 -10 9 54.95 5 -5 10 -10 20.98 4.92 -5 -10 10 19.72 2.81 -5 10 -11 2.76 4.75 -5 -10 11 3.02 2.2 -5 -10 12 14 2 -5 10 -12 16.96 4.36 -5 10 -13 5.23 3.43 -5 -10 13 4.34 1.33 5 11 -12 4.16 3.77 5 11 -11 18.12 4.28 5 -11 11 -0.37 5.67 5 11 -10 5.53 4.04 5 -11 10 -3.76 5.77 -5 11 9 61.18 11.78 5 11 -9 77.13 5.3 -5 11 8 69.36 8.41 5 -11 8 77.49 7.33 5 -11 8 88.45 6.76 -5 11 7 147.44 10.09 5 11 -7 170.43 14.5 5 -11 7 148.61 10.29 -5 11 6 2.84 4.67 5 11 -6 8.03 7.68 5 -11 6 6.89 4.05 -5 11 5 30.17 4.98 5 -11 5 36.14 4.85 5 -11 5 51.44 5.29 5 11 -5 42.42 8.2 5 -11 4 25.7 5.11 -5 11 4 35.43 4.69 -5 -11 -4 36.51 4.39 5 -11 4 37.96 4.82 5 -11 3 24.89 4.21 -5 11 3 19.2 4.19 -5 -11 -3 17.12 3.71 5 11 -3 20.03 6.85 -5 11 2 66.4 5.49 5 11 -2 73.87 8.59 -5 -11 -2 69.01 5.54 -5 -11 -1 22.46 3.86 5 11 -1 24.56 6.81 -5 11 0 50.19 5.01 -5 -11 0 57.33 5.32 -5 -11 1 20.54 4.63 -5 11 -1 29.8 4.3 5 11 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39.99 4.43 7 -7 8 36.53 2.71 -7 7 8 38.72 3.51 7 7 -8 47.38 11.99 7 -7 8 6.34 5.47 -7 7 7 4.9 5.08 -7 7 7 2.04 1.76 7 -7 7 2.71 4.38 -7 7 7 2.8 2.51 7 7 -7 -2.26 8.69 7 -7 7 1.47 3.2 7 -7 6 14.1 3.24 -7 7 6 12.35 2.5 7 -7 6 10.07 1.99 -7 7 6 13.79 3.49 7 -7 6 12.48 3.89 7 7 -6 8.42 8.12 -7 7 5 36.73 4.14 7 7 -5 52.72 14.47 7 -7 5 40.25 3.92 7 -7 4 218.8 12.38 7 7 -4 215.27 14.67 7 7 -3 534.97 29.59 7 -7 3 471.76 25.02 7 7 -3 443.52 26.43 7 7 -2 62.42 13.83 -7 -7 -2 69.83 5.15 7 7 -2 51.27 7.57 7 -7 2 58.41 4.71 7 -7 1 1426.94 77.95 -7 -7 -1 1655.73 78.33 7 7 -1 1507.16 78.98 7 7 0 487.19 28.16 -7 -7 0 527.86 27.42 7 7 1 1452.16 77.91 -7 -7 1 1501.4 77.48 -7 -7 3 460.14 24.26 -7 -7 4 241.92 13.77 -7 -7 4 230.6 12.67 -7 7 -5 36.62 3.29 -7 -7 5 37.99 3.09 -7 -7 5 32.43 5.23 -7 -7 6 11.1 2.34 -7 7 -6 5.04 4.25 -7 7 -6 11.42 2.89 -7 -7 6 11.03 2.2 -7 -7 6 12.5 2.65 -7 -7 7 0.18 2.69 -7 -7 7 0.11 2.41 -7 7 -7 7.34 3.32 -7 -7 8 44.67 4.55 -7 -7 8 35.47 3.54 -7 -7 8 38.13 5.53 -7 -7 8 35.47 3.78 -7 -7 9 35.61 3.67 -7 -7 9 38.51 4.02 -7 -7 9 43.87 5.49 -7 -7 9 42.99 4.53 -7 -7 10 7.3 3.06 -7 -7 10 7.51 4.17 -7 -7 10 5.33 3.33 -7 -7 10 6.86 3.36 -7 -7 11 14.67 2.93 -7 7 -11 21.15 5.31 -7 7 -12 2.3 4.78 -7 -7 12 5.65 2.41 -7 7 -13 1.59 3.83 -7 -7 13 0.89 1.88 -7 -7 14 1.41 1.29 -7 7 -14 2.33 2.6 7 8 -14 0.56 4.07 7 -8 13 1.95 1.24 7 8 -13 -5.6 6.36 7 -8 12 6.32 1.73 7 8 -12 0.99 7.61 7 -8 11 37.34 2.73 7 -8 11 1.02 6.96 -7 8 10 6.92 9.28 7 -8 10 -4.5 6.94 7 8 -9 76.9 13.65 -7 8 9 40.66 11.68 -7 8 8 9.32 8.71 7 -8 8 7.58 5.47 -7 8 8 23.81 3.18 7 -8 8 24.33 4.1 7 8 -8 33.46 11.03 7 -8 7 20.42 5.01 -7 8 7 38.96 5.11 7 8 -7 43.41 10.07 -7 8 7 34.73 3.27 7 -8 7 38.46 4.35 7 -8 6 32.64 3.76 7 8 -6 25.25 7.91 -7 8 6 24.5 4.11 -7 8 6 24.27 2.83 -7 8 5 0.74 2.15 -7 8 5 1.8 3.53 7 -8 5 1.74 2.98 7 -8 5 3.95 3.64 7 8 -4 152.02 11.32 7 -8 4 156.22 9.07 -7 -8 -3 188.45 10.28 7 -8 3 165.9 9.94 7 8 -3 167.58 12.12 7 -8 2 888.29 47.4 -7 -8 -2 940.28 47.71 7 8 -2 889.9 48.56 -7 -8 -1 211.1 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81.28 6.98 -7 9 7 94.75 5.66 7 -9 7 87.21 6.6 7 -9 6 137.83 8.72 7 9 -6 154.99 12.15 -7 9 6 140.44 8.79 -7 9 6 136.91 7.85 -7 9 5 181.61 11.22 7 -9 5 185.99 11.18 -7 9 5 183.97 10.53 7 -9 4 181.9 9.39 -7 9 4 145.03 9.29 7 -9 4 165.04 9.37 -7 -9 -4 157.2 9.64 -7 9 4 151.03 8.68 7 9 -4 167.73 11.82 -7 9 3 43.04 4.47 7 9 -3 54.17 6.95 -7 -9 -3 56.29 4.84 7 -9 3 54.05 4.52 7 9 -2 14.45 6.33 7 -9 2 12.52 3.11 -7 -9 -2 20.48 3.95 7 9 -1 301.99 19 -7 -9 -1 330.35 17.71 7 9 0 61.89 7.24 -7 -9 0 66.72 5.46 -7 -9 1 305.9 17.07 -7 -9 2 15.81 2.04 -7 -9 2 19.51 4.39 -7 -9 3 58.68 3.85 -7 -9 3 61.91 5.59 -7 -9 4 139.54 10.13 -7 9 -4 158.52 8.65 -7 -9 4 163.88 8.73 -7 -9 4 151.28 8.64 -7 -9 5 189.37 10.76 -7 9 -5 207.88 10.87 -7 -9 6 147.53 8.46 -7 9 -6 153.23 8.64 -7 -9 7 82.06 5.72 -7 9 -7 100.52 6.2 -7 -9 7 100 7.04 -7 -9 8 15.19 3.07 -7 -9 8 13.44 3.83 -7 -9 8 11.44 4.62 -7 -9 8 14.53 5.07 -7 9 -8 19.26 4.14 -7 -9 9 1.15 3.33 -7 -9 9 3.47 4.53 -7 9 -9 2.13 4.48 -7 -9 9 4.34 2.93 -7 -9 10 5.45 2.77 -7 9 -10 6.06 4.86 -7 -9 11 1.57 2.48 -7 9 -11 8.89 4.78 -7 -9 12 0.33 1.94 -7 -9 13 3.58 1.53 7 10 -13 3.48 3.5 7 10 -12 5.78 4.55 7 10 -11 2.9 4.88 -7 10 10 1.4 9.7 7 10 -10 9.57 4.75 7 -10 10 1.72 6.26 -7 10 9 35.77 12.33 7 10 -9 57.75 5.07 7 -10 8 53.36 5.16 7 -10 8 34.71 6.36 -7 10 8 52.14 8.75 7 10 -8 58.13 11.61 -7 10 7 26.84 5.21 7 10 -7 40.72 9.86 7 -10 7 28.48 4.4 -7 10 7 30.73 3.31 7 -10 6 119.48 8.16 -7 10 6 134.94 8.5 7 10 -6 138.35 11.86 -7 -10 -6 107.54 8.44 -7 10 6 128.99 7.3 -7 10 5 36.78 4.99 7 -10 5 42.67 4.46 -7 -10 -5 35.82 4.46 -7 10 5 42.52 3.38 7 -10 4 38.25 4.12 7 -10 4 39.81 4.74 7 10 -4 41.43 7.17 -7 -10 -4 39.66 4.44 -7 10 4 35.2 4.58 -7 10 4 37.52 3.19 -7 -10 -3 7.4 3.77 -7 10 3 6.86 1.93 -7 10 3 8.43 3.72 7 10 -3 10.1 6.34 7 -10 3 7.47 3.97 7 -10 3 6.09 3.24 7 10 -2 20.33 6.31 -7 -10 -2 17.32 3.63 7 -10 2 6.81 4.26 7 10 -1 29.76 6.09 -7 -10 -1 32.91 4.23 -7 10 1 31.99 4.01 -7 10 0 279.37 15.85 -7 -10 0 305.09 16.32 7 10 0 305.69 17.81 -7 10 -1 33.82 4.09 -7 -10 1 36.86 4.56 -7 10 -2 18.37 3.65 -7 10 -2 17.99 2.29 -7 -10 2 16.16 4.01 -7 -10 3 6.59 2.23 -7 10 -3 4.94 3.61 -7 -10 3 2.64 4.33 -7 10 -3 8.61 2.2 -7 10 -4 40.51 3.26 -7 10 -4 39.74 4.47 -7 -10 4 40.13 5.49 -7 -10 4 36.22 3.25 -7 10 -5 38.71 3.49 -7 -10 5 40.48 3.42 -7 -10 5 45.98 5.9 -7 -10 6 122.78 7.27 -7 10 -6 127.32 7.5 -7 -10 7 30.7 3.47 -7 10 -7 34.9 4.07 -7 -10 7 35.73 5.29 -7 -10 8 63.96 6.49 -7 -10 8 50.66 5.13 -7 -10 8 62.67 5.95 -7 10 -8 60.42 5.27 -7 -10 8 60.62 4.49 -7 10 -9 73.5 5.71 -7 -10 9 57.68 4.53 -7 -10 10 7.25 2.64 -7 10 -10 12.44 4.6 -7 -10 11 -0.54 2.22 -7 10 -11 -1.57 4.24 -7 -10 12 6.53 1.87 -7 10 -12 8.71 3.88 -7 10 -13 2.53 3.02 -7 -10 13 1.41 1.28 -7 11 10 16.36 9.42 7 -11 10 -3.51 6.13 7 -11 9 3.79 5.82 -7 11 9 3.77 11.93 7 -11 8 19.88 5.93 7 -11 8 22.1 4.1 7 11 -8 24.54 10.01 -7 11 8 20.21 8.29 -7 11 7 63.2 6.21 7 -11 7 53.42 5.55 -7 11 6 104.71 7.85 7 -11 6 90.5 7.3 7 11 -6 88.12 11.03 7 -11 5 44.04 4.76 -7 -11 -5 42.11 4.98 7 -11 5 55.85 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1805.53 89.75 -8 4 0 1713.82 89.47 8 4 0 1696.06 90.56 8 4 1 517.18 29.3 -8 -4 1 588.98 29.27 8 4 1 558.19 30.49 -8 -4 2 111.59 6.65 -8 -4 3 25.48 3.59 -8 -4 3 32.25 2.83 -8 -4 4 41.54 3.51 -8 -4 4 35.86 4.82 -8 -4 5 101.8 7.44 -8 -4 5 100.55 6.24 -8 -4 6 218.68 12.1 -8 -4 7 12.07 2.33 -8 4 -7 16.15 3.09 -8 -4 7 19.64 4.59 -8 -4 7 14.38 1.96 8 4 7 14.37 1.7 -8 -4 7 11.77 2.6 -8 -4 7 14.46 3.64 -8 -4 8 10.76 4.28 8 4 8 8.36 1.71 -8 -4 8 9.47 2.54 -8 4 -8 10.05 3.6 -8 -4 8 11.76 3.53 -8 -4 8 6.73 4.13 -8 -4 9 16.29 4.29 8 4 9 15.92 2.13 -8 -4 9 21.9 3.84 -8 -4 9 18.87 4.3 -8 -4 9 19.12 3.02 -8 4 -9 16.83 4.31 -8 -4 10 96.35 5.76 -8 -4 10 81.41 6.37 -8 -4 10 74.91 6.76 -8 4 -10 102.51 7.05 -8 -4 10 91.06 6.47 -8 4 -11 7.07 4.91 -8 -4 11 13.72 2.98 -8 -4 12 2.51 2.63 -8 4 -12 -4.52 4.41 -8 -4 13 8.15 2.27 -8 4 -13 2.82 3.78 -8 4 -14 -0.17 2.62 -8 -4 14 -0.97 1.62 -8 -4 15 0.46 0.95 8 5 -14 4.54 6.52 -8 5 13 0.84 2.2 8 -5 13 1.62 1.64 -8 5 12 -0.92 3.56 8 -5 12 -0.26 1.97 8 -5 12 2.09 6.7 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8 -6 2 2384.64 124.04 8 6 -2 2557.61 125.76 8 6 -2 2302.78 124.96 8 -6 1 120.65 7.31 8 6 -1 131.49 14.42 8 6 -1 134.27 9.57 -8 -6 -1 157.44 7.96 8 6 0 41.74 5.87 8 6 0 37.97 11.34 8 6 1 130.12 8.65 -8 -6 2 2383.43 124.09 -8 -6 3 439.06 23.5 -8 -6 3 457.42 24.06 -8 -6 4 572.67 30.63 -8 -6 4 566.36 29.92 -8 -6 5 6.53 4.57 -8 -6 5 7.84 2.18 -8 -6 6 109.83 6.13 -8 -6 6 95.42 5.79 -8 -6 6 90.99 6.1 -8 -6 7 21.09 3.3 -8 -6 7 23.04 2.88 -8 -6 7 27.47 2.82 -8 -6 8 32.31 3.79 -8 -6 8 33.79 3.44 -8 -6 8 38.02 5.33 -8 6 -8 37.37 4.32 -8 -6 9 79.47 5.21 -8 -6 9 63.93 5.35 -8 -6 9 80.23 6.72 -8 6 -9 83.86 6.29 -8 -6 10 16.73 4.39 -8 -6 10 16.26 3.5 -8 6 -10 16.39 4.98 -8 6 -11 32.33 5.28 -8 -6 11 25.61 3.58 -8 6 -12 2.5 4.45 -8 6 -13 8.52 3.74 -8 6 -14 1.46 2.5 8 7 -14 8.3 5.05 8 7 -13 15.01 7.82 8 -7 12 6.9 1.81 -8 7 12 4 3.14 -8 7 11 29.1 10.21 8 -7 11 8.74 2.03 -8 7 10 3.62 9.3 8 -7 10 -0.06 1.98 8 7 -10 -13.02 14.88 8 -7 10 1.97 6.75 8 -7 9 10.32 2.07 8 7 -9 11.24 13.83 8 -7 9 3.08 6.15 8 -7 8 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9 11.25 3.32 -8 -7 10 0.34 3.34 -8 -7 10 -0.1 2.97 -8 -7 10 -1.95 4.01 -8 -7 10 -2.68 3.21 -8 7 -10 -1.01 4.78 -8 -7 11 7.38 2.84 -8 7 -11 7.16 5.02 -8 -7 12 8.34 2.44 -8 7 -12 9.28 4.55 -8 -7 13 6.89 1.88 -8 7 -13 11.12 3.65 -8 -7 14 1.45 1.29 -8 7 -14 -1.15 2.36 8 8 -13 13.79 6.35 8 -8 12 2.79 1.59 8 8 -12 3.71 7.28 8 -8 11 4.57 6.62 -8 8 11 7 9.9 8 -8 11 3.59 1.84 8 -8 10 -1.19 6.87 -8 8 10 11.72 9.61 -8 8 9 -10.3 12.23 8 8 -9 15.81 12.79 8 -8 9 0.72 6.14 -8 8 8 103.26 5.46 8 8 -8 115.12 13.99 8 -8 7 19.08 3.7 -8 8 7 17.97 5.42 8 8 -7 22.42 9.73 -8 8 7 18.81 3.03 8 -8 7 6.15 4.78 -8 8 6 30.17 3.1 -8 8 6 28.12 4.3 8 8 -6 37.33 8.3 8 -8 6 32.31 3.86 -8 8 5 129.05 8.49 8 -8 5 137.26 8.37 -8 8 5 133.64 7.81 8 -8 4 10.61 3.54 8 8 -4 9.59 5.9 -8 8 4 9.76 3.42 8 -8 4 10.82 2.98 8 8 -3 187.28 12.8 8 -8 3 187.3 10.81 -8 -8 -3 203.32 11.33 8 -8 2 235.46 13.85 8 8 -2 254.75 15.61 8 8 -1 54.57 7.06 -8 -8 -1 52.86 5.13 8 8 0 40.41 6.44 -8 -8 0 36.51 4.36 -8 -8 1 49.08 4.8 8 8 1 52.83 6.12 -8 -8 2 261.16 14.75 -8 -8 3 183.51 10.09 -8 -8 4 12 2.14 -8 8 -4 11.15 2.35 -8 -8 5 102.87 6.94 -8 -8 5 119.86 7.04 -8 -8 5 138.11 8.93 -8 8 -5 152.05 7.21 -8 -8 5 129 7.22 -8 -8 6 27.56 2.99 -8 8 -6 33.51 3.39 -8 -8 6 26.14 2.84 -8 -8 6 26.38 2.98 -8 -8 6 27.21 5.29 -8 -8 7 15.54 2.95 -8 8 -7 16.64 3.6 -8 -8 7 18.29 2.96 -8 -8 8 93.98 6.24 -8 -8 8 105.96 8.06 -8 8 -8 113.39 6.93 -8 -8 8 96.55 6.35 -8 -8 8 99.17 6.98 -8 -8 9 6.09 3.22 -8 -8 9 10.93 4.7 -8 -8 9 5.46 3.64 -8 -8 9 7.15 3.07 -8 -8 10 33.79 3.6 -8 -8 11 2.79 2.63 -8 8 -12 12.99 4.33 -8 -8 12 1.45 2.22 -8 -8 13 4.52 1.73 -8 8 -13 7.04 3.35 -8 -8 14 1.97 1.06 -8 8 -14 2.56 2.23 8 9 -13 13.7 4.78 8 9 -12 5.35 5.81 -8 9 11 -0.89 9.64 8 -9 11 -2.54 6.34 8 9 -11 5.91 5.98 -8 9 10 8.21 9.7 8 9 -10 5.17 5.67 8 -9 10 -1.64 6.39 -8 9 9 11.21 12.57 8 9 -9 7.92 11.83 8 -9 9 -0.06 6.03 -8 9 8 93.82 10.23 -8 9 8 70.82 4.77 8 9 -8 92.63 12.41 8 9 -7 11.67 9.31 -8 9 7 11.9 5.14 8 -9 7 13.75 3.81 -8 9 7 11.3 2.96 8 -9 6 1.54 3.4 -8 9 6 1.3 4.29 8 9 -6 -2.46 7.63 -8 9 6 -1.12 2.67 -8 9 5 104.05 7.22 8 -9 5 96.21 6.92 -8 9 5 103.96 6.28 8 -9 4 22.49 3.78 8 -9 4 16.69 3.15 -8 9 4 14.8 3.76 8 9 -4 11.45 6.02 -8 -9 -4 14.84 3.87 -8 9 4 16.75 2.53 8 -9 3 57.65 4.4 -8 9 3 61.2 4.8 -8 -9 -3 61.09 4.95 8 9 -3 66.51 7.57 8 -9 3 43.78 4.93 8 9 -2 9.38 6.08 -8 -9 -2 12.25 3.81 -8 -9 -1 70.77 5.52 8 9 -1 59.42 7.01 8 9 0 30.46 6.22 -8 -9 0 29.66 4 -8 -9 1 64.28 5.29 -8 -9 2 11.38 1.88 -8 -9 2 17.5 3.93 -8 -9 3 64.67 5.93 -8 9 -3 66.48 4.19 -8 -9 3 62.25 4.11 -8 -9 4 18.37 2.51 -8 9 -4 19.27 2.53 -8 9 -4 16.32 3.44 -8 -9 4 15.59 2.26 -8 -9 5 86.89 5.8 -8 -9 5 93.16 5.82 -8 9 -6 0.61 3.03 -8 -9 6 1.7 2.6 -8 9 -7 13.69 3.61 -8 -9 7 11.31 2.91 -8 -9 7 17.64 4.9 -8 -9 8 74.77 5.09 -8 -9 8 71.49 5.88 -8 -9 8 71.98 7.1 -8 9 -8 74.32 5.85 -8 -9 9 6.66 3.52 -8 -9 9 10.87 4.71 -8 9 -9 11.59 4.46 -8 -9 9 11.83 3.09 -8 -9 10 3 2.81 -8 9 -10 9.24 4.72 -8 -9 11 2.32 2.41 -8 -9 12 6.39 2.01 -8 -9 13 11.12 1.68 -8 9 -14 2.32 1.83 8 10 -12 0.6 4.22 8 -10 11 -0.29 6.22 8 10 -11 36.61 5 -8 10 10 7.14 9.67 8 -10 10 1.7 6.48 8 10 -10 5.03 4.57 8 -10 9 2.99 5.7 -8 10 9 4.89 12.75 -8 10 8 15.72 9.13 8 10 -8 21.1 10.5 -8 10 8 21.82 3.24 8 -10 8 21.43 6.04 8 -10 7 45.85 4.87 -8 10 7 47.29 5.99 8 10 -7 52.36 9.99 -8 10 7 46.62 4.04 -8 10 6 25.36 5.2 8 -10 6 30.77 4.27 -8 10 6 35.66 3.45 -8 -10 -6 25.13 4.54 8 -10 6 39.02 5.21 -8 -10 -5 11.18 3.7 -8 10 5 6.13 4.64 8 -10 5 11.54 3.44 8 10 -5 10.08 7.06 -8 10 5 12.48 2.77 8 -10 5 14.67 4.33 8 -10 4 8.26 4.07 -8 -10 -4 5.74 3.47 -8 10 4 6.96 3.99 8 10 -4 11.8 6.34 8 -10 4 8.95 3.25 -8 10 4 9.56 2.56 8 10 -3 43.17 6.93 -8 10 3 40.06 4.49 -8 10 3 39.46 2.95 -8 -10 -3 53.95 4.81 -8 10 2 105.89 5.59 8 10 -2 101.73 8.8 -8 -10 -2 125.91 7.22 -8 10 1 204.87 12.25 -8 -10 -1 234 12.78 8 10 -1 241.3 14.48 8 10 0 256.21 14.44 -8 -10 0 234.29 12.8 -8 10 -1 214.39 12.77 -8 10 -1 238.9 12.27 -8 -10 1 216.19 13.27 -8 10 -2 97.93 6.8 -8 -10 2 103.02 7.52 -8 -10 2 112.96 6.07 -8 10 -2 101.63 6.09 -8 -10 2 106.38 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5.95 -10 9 4 7.51 2.58 10 -9 3 -1.71 3.46 -10 -9 -3 0.9 3.43 -10 9 3 1.69 2.07 10 9 -3 1.9 5.66 -10 9 2 299.1 17.61 -10 9 2 323.67 17.26 10 9 -2 338.25 19.22 10 9 -1 18.23 5.22 -10 9 1 17.45 3.44 -10 -9 -1 17.83 3.84 -10 -9 0 142.41 9.19 10 9 0 158.17 10.67 -10 9 -1 25.02 2.5 -10 -9 1 14.85 3.95 -10 -9 2 327.79 17.28 -10 9 -2 326.41 17.31 -10 -9 3 0.95 1.88 -10 9 -3 0.52 2.21 -10 -9 3 0.49 2.17 -10 9 -4 2.56 2.48 -10 -9 4 9.62 4.56 -10 -9 4 9.73 2.15 -10 -9 4 5.85 2.47 -10 -9 5 1.5 2.58 -10 -9 5 1.17 4.82 -10 9 -5 -0.72 2.65 -10 -9 5 3.79 2.17 -10 -9 6 29.98 3.42 -10 9 -6 33.37 3.59 -10 -9 6 31.24 3.14 -10 -9 6 31.1 5.74 -10 -9 7 18.75 3.29 -10 9 -7 23.85 3.75 -10 -9 8 61.6 4.87 -10 9 -8 65.96 5.42 -10 -9 8 71.28 7.09 -10 -9 8 69.09 5.73 -10 -9 9 7.34 3.53 -10 -9 9 8.49 3.19 -10 -9 9 6.69 4.47 -10 -9 10 12.13 3 -10 -9 11 2.67 2.49 -10 -9 12 4.46 2 -10 9 -12 5.06 3.58 -10 9 -13 4.83 2.71 -10 -9 13 5.73 1.48 -10 10 11 5.22 9.71 -10 10 10 9.43 10.42 10 -10 10 3.3 6.38 -10 10 9 7.9 13.74 10 -10 9 -1.93 6.23 10 10 -8 7.54 10.28 -10 10 8 6.07 3.22 -10 10 8 13.51 10.44 10 -10 7 3.97 5.54 -10 10 7 10.49 6.15 -10 -10 -7 6.09 4.42 -10 10 7 8.91 3.31 -10 -10 -6 23.89 4.9 -10 10 6 25.61 5.26 10 -10 6 24.06 3.93 10 10 -6 29.51 8.36 -10 10 6 31.53 3.67 10 -10 6 30.94 5.36 10 -10 5 8.53 3.36 -10 10 5 4.79 4.81 10 10 -5 11.15 7.36 10 -10 5 13.86 4.52 -10 10 5 9.52 3 -10 -10 -5 9.66 3.96 10 -10 4 194.66 10.79 -10 10 4 157.56 10.86 -10 -10 -4 195.42 11.31 -10 10 4 183.87 10.14 10 10 -4 178.75 13.1 10 10 -3 46.91 7.14 -10 10 3 39.65 3.3 -10 -10 -3 51.45 4.9 10 -10 3 46.02 4.65 10 10 -2 13.63 5.98 -10 10 2 13.81 3.82 -10 10 2 19.4 2.5 10 -10 2 11.6 3.89 -10 -10 -2 19.25 4.17 -10 10 1 45.52 4.63 -10 10 1 51.06 3.59 -10 -10 -1 61.03 4.97 10 10 -1 58.48 6.76 -10 10 0 115.23 5.94 -10 -10 0 103.63 7.21 10 10 0 107.09 8.72 -10 -10 1 57.21 3.72 -10 -10 1 56.8 5.49 -10 10 -1 58.17 4.65 -10 10 -1 54.64 3.81 -10 -10 2 16.44 2.17 -10 -10 2 18.96 2.41 -10 10 -2 17.82 2.56 -10 -10 2 17.86 4.31 -10 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3.34 -11 -6 10 12.56 3.53 -11 -6 10 9.93 3.19 -11 6 -10 11.44 4.26 -11 -6 11 3.39 2.91 -11 -6 11 7.19 2.87 -11 6 -11 4.56 4.12 -11 6 -12 12.58 3.76 -11 -6 12 5.57 2.48 -11 6 -13 1.06 2.85 -11 -6 13 2.04 1.82 -11 -6 14 2.04 1.27 -11 6 -14 0.86 1.86 -11 7 13 0.61 1.84 11 7 -13 9.77 6.85 -11 7 11 4.01 10.84 -11 7 10 10.23 10.48 11 -7 10 0.14 7.1 -11 7 9 63.81 11.81 11 7 -9 52.31 15.82 -11 7 8 3.22 2.43 -11 7 8 3.21 3.32 11 -7 8 -3.62 5.91 11 7 -8 -4.27 12.96 -11 7 8 -7.33 11.78 -11 7 7 58.2 8.42 11 -7 7 40.58 11.92 -11 7 7 54.4 4.37 -11 7 7 55.43 3.77 11 7 -6 136.67 12.01 -11 7 6 125.79 6.58 -11 7 6 124.67 7.94 -11 7 6 126.25 7.03 -11 7 5 18.04 1.94 -11 7 5 14 3.91 11 7 -5 17.31 7.29 -11 7 5 17.67 2.72 11 -7 5 21.98 3.98 11 7 -5 18.85 16.31 11 -7 4 256.85 12.04 11 7 -4 234.27 19.84 -11 7 4 194.43 11.6 11 7 -4 196.87 14.24 11 7 -3 353.76 22.34 11 7 -3 278.99 17.73 11 7 -2 32.4 6.36 -11 -7 -2 40.29 4.32 11 7 -1 21.34 5.19 11 7 -1 19.3 12.84 11 7 0 19.4 5.19 11 7 0 23.19 12.13 11 7 1 18.91 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36.01 8.14 -12 4 6 28.37 3.11 12 -4 5 357.01 22.61 12 4 -5 530.03 32.23 12 4 -4 61.26 21.81 -12 4 4 53.77 3.92 -12 4 3 575.3 30.16 12 4 -3 536.6 37.51 -12 4 2 20.38 2.56 12 4 -1 341.02 26.03 -12 4 1 409.07 21.33 12 4 0 97.43 7.05 -12 -4 0 111.06 6.4 -12 4 0 89.42 5.39 12 4 0 100.17 12.93 -12 -4 1 415.56 21.65 12 4 1 405.52 24.74 12 4 1 387.17 21.48 -12 -4 2 26.17 3.69 12 4 2 28.4 11.06 -12 -4 3 557.93 30.57 -12 -4 3 584.49 30.31 -12 -4 4 50.62 5.29 -12 -4 4 59.18 4.22 -12 -4 5 379.1 21.02 -12 -4 5 421.87 22.1 -12 -4 5 428.52 21.44 -12 -4 6 25.86 2.87 -12 4 -6 25.82 2.78 -12 -4 6 27.06 3.23 -12 -4 6 28.58 2.28 -12 -4 7 358.06 19.36 -12 4 -7 361.13 19.37 -12 -4 7 374.11 19.84 -12 -4 7 366.21 19.17 -12 -4 8 18.51 3.08 -12 -4 8 16.37 4.45 -12 -4 8 14.58 4.05 -12 4 -8 14.09 3.32 -12 -4 8 19.98 2.46 -12 -4 9 94.75 7.39 -12 -4 9 116.22 6.83 -12 4 -9 110.49 7.07 -12 -4 9 111.59 7.52 -12 -4 10 64.87 5.75 -12 -4 10 76.81 5.22 -12 4 -10 74.72 5.71 -12 -4 10 71.81 5.81 -12 -4 11 24.4 3.68 -12 4 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25.23 12 5 2 510.06 27.83 -12 -5 3 6.97 3.96 -12 -5 3 6.45 2.72 -12 -5 4 232.02 13.56 -12 -5 4 236.29 12.95 -12 -5 5 63.26 5.47 -12 5 -5 56.52 3.79 -12 -5 5 63.86 4.28 -12 5 -6 4.59 2.45 -12 -5 6 5.18 4.34 -12 -5 6 4.69 2.61 -12 -5 6 3.89 2.47 -12 -5 7 88.56 5.4 -12 5 -7 85.75 5.45 -12 -5 7 92.97 5.74 -12 -5 7 70.42 5.77 -12 -5 7 79.39 4.9 -12 -5 8 36.01 3.04 -12 -5 8 34.14 4.52 -12 -5 8 45.61 4.84 -12 -5 8 36.71 3.81 -12 -5 8 45.05 5.32 -12 5 -8 34.96 4.02 -12 5 -9 13.26 3.96 -12 -5 9 11.31 3.77 -12 -5 9 14.45 3.31 -12 -5 9 11.55 4 -12 -5 10 52.6 4.77 -12 -5 10 61.82 4.53 -12 -5 10 48.88 5 -12 5 -10 61.49 5.19 -12 -5 11 13.76 3.24 -12 -5 11 14.95 3.06 -12 5 -11 19.38 4.09 -12 -5 12 0.92 2.48 -12 -5 12 0.94 2.58 -12 5 -12 -3.1 3.44 -12 -5 13 -0.29 1.86 -12 5 -13 0.72 1.63 -12 5 -13 3.21 2.71 -12 -5 14 1.39 1.25 -12 5 -14 0.01 1.67 12 6 -14 2.99 4.69 -12 -6 -14 0.66 1.12 -12 6 13 -0.55 2.24 12 6 -13 6.12 8.37 -12 6 11 0.77 11.23 12 -6 11 3.49 1.75 12 -6 10 14.63 2.08 -12 6 10 12.61 10.45 -12 6 9 8.34 10.44 12 -6 9 -0.95 6.76 12 6 -9 -8.75 16.32 -12 6 8 36.79 11.87 -12 6 8 29.73 2.98 -12 6 8 25.67 3.77 12 6 -8 40.43 14.27 -12 6 7 4.38 9.18 -12 6 7 1.89 3.03 -12 6 7 0.21 2.19 12 -6 7 5.54 8.52 -12 6 6 5.62 5.54 12 -6 6 5.34 12.23 12 6 -6 -2.94 20.38 -12 6 6 8.16 2.75 -12 6 6 7.39 1.9 12 -6 6 -1.41 4.39 12 6 -6 8.96 10.15 12 -6 5 118.86 8.53 -12 6 5 140.91 7.86 -12 6 5 141.04 7.55 -12 6 4 21.2 3.72 -12 6 4 25.37 2.8 12 6 -4 24.05 7.7 12 6 -3 145.97 10.84 12 6 -3 182.14 17.41 12 6 -2 30.26 6.19 12 6 -1 37.49 13.34 12 6 -1 31.92 5.84 -12 -6 0 75.11 5.73 12 6 0 68.18 6.13 12 6 0 71.23 13.49 12 6 1 29.54 4.63 12 6 1 26.7 11.88 -12 -6 1 33.6 4.29 -12 -6 2 32.09 4.11 -12 -6 3 141.05 9.36 -12 -6 3 162.3 8.84 -12 6 -4 19.05 2.43 -12 -6 4 22.53 2.74 -12 -6 4 24.29 4.31 -12 -6 5 158 10.23 -12 6 -5 156.86 8.72 -12 -6 5 157.05 9.03 -12 -6 6 18.04 3.12 -12 6 -6 8.75 2.69 -12 -6 6 6.63 4.62 -12 -6 6 7.3 2.55 -12 -6 7 0.67 3.15 -12 6 -7 3.45 3.06 12 6 7 4.27 6.63 -12 -6 7 1.12 2.5 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7 3 260.89 15.02 -12 7 3 277.44 14.62 12 7 -3 287.23 16.92 -12 -7 -2 83.99 5.96 12 7 -2 69.63 7.3 12 7 -1 92.86 13.7 12 7 -1 88.16 7.55 12 7 0 700.11 39.95 12 7 0 710.09 38.03 -12 -7 1 85.19 6.33 12 7 1 98.44 7.02 -12 -7 2 77.57 6.02 -12 -7 3 284.45 15.93 -12 -7 3 300.89 16.88 -12 -7 3 331.78 16.28 -12 7 -4 8.21 2.3 -12 -7 4 8.15 2.2 -12 -7 4 4.11 2.27 -12 -7 4 6.13 4.02 -12 -7 5 12.53 2.71 -12 7 -5 9.99 2.56 -12 -7 5 14.05 4.73 -12 -7 5 11.54 2.51 -12 -7 6 24.02 3.11 -12 7 -6 30.6 3.31 -12 -7 6 26.41 3.21 -12 -7 6 31.22 5.22 -12 -7 7 21.08 3.12 -12 7 -7 24.93 3.54 -12 -7 7 22.96 3.19 -12 -7 8 2.22 4.05 -12 -7 8 9.35 5.25 -12 7 -8 1.41 3.56 -12 -7 8 2.45 2.94 -12 -7 9 35.04 3.78 -12 -7 9 38.33 4.67 -12 -7 9 35.29 5.26 -12 7 -9 45.66 4.6 -12 7 -10 22.89 4.28 -12 -7 10 17.69 3.2 -12 7 -11 5.29 3.91 -12 7 -12 -0.12 3.27 -12 7 -13 1.82 2.64 -12 -7 14 -0.23 0.97 12 8 -12 2.95 5.85 12 -8 12 3.29 5.96 -12 8 11 2.28 11.13 -12 8 10 7.47 10.84 12 -8 10 5.54 6.92 -12 8 9 13.38 12.84 12 8 -9 2.45 13.72 12 -8 9 1.25 6.74 -12 8 8 12.03 12.67 12 8 -8 6.55 11.64 -12 8 8 1.15 3.48 -12 8 8 1.94 2.43 12 -8 7 1.97 5.4 12 -8 7 8.78 12.54 -12 8 7 11.07 3.42 -12 8 7 5.79 8.2 -12 8 7 9.22 2.22 -12 8 6 -4.13 4.96 12 8 -6 -0.7 7.93 -12 8 6 -0.24 3.15 12 -8 6 -2.07 4.61 12 8 -6 12.91 19.32 -12 8 6 1.35 1.95 12 8 -5 11.06 6.71 12 -8 5 17.51 4.3 -12 8 5 12.74 2.93 12 8 -5 3.62 17.07 -12 8 4 93.3 7.05 12 -8 4 121.76 6.92 -12 8 4 102.6 6.29 12 8 -4 94.94 9.27 12 8 -4 123.87 16.91 -12 -8 -3 3.48 3.26 12 -8 3 7.62 3.5 -12 8 3 4.27 3.56 -12 8 3 4.7 2.19 12 8 -3 10.43 5.32 12 8 -3 0.42 13.04 -12 8 2 27.14 2.6 -12 -8 -2 26.73 4.09 12 8 -2 22.23 5.63 -12 8 2 20.27 3.66 -12 -8 -1 220.64 12.78 12 8 -1 217.32 13.53 12 8 0 4.73 4.87 -12 8 -1 217.11 11.43 12 8 1 192.04 12.76 -12 -8 2 26.26 2.53 -12 8 -2 25.56 2.57 -12 -8 2 22.57 4.07 -12 -8 3 8.05 2.3 -12 -8 3 7.47 2.27 -12 8 -3 7.49 2.29 -12 -8 3 5.75 3.67 -12 -8 4 100.88 6.03 -12 -8 4 92.78 5.82 -12 -8 4 102.96 7.46 -12 -8 5 14.19 2.89 -12 -8 5 16.12 4.86 -12 -8 5 11.88 2.4 -12 -8 6 1.03 2.95 -12 -8 6 1.8 4.93 -12 -8 6 1.3 2.46 -12 -8 7 9.11 2.85 -12 -8 7 7.6 3.2 -12 8 -7 15.41 3.41 -12 -8 7 9.26 2.62 -12 -8 8 2.25 2.86 -12 -8 8 0.69 3.24 -12 -8 8 6.01 5.17 -12 8 -8 0.72 3.68 -12 -8 9 7.79 2.9 -12 -8 9 9.37 3.39 -12 -8 9 7.03 4.52 -12 8 -9 4.36 3.99 -12 -8 10 12.59 3.21 -12 8 -10 11.67 4.17 -12 8 -11 1.45 3.82 -12 8 -12 -0.79 3.26 -12 8 -13 0.97 2.47 -12 9 11 -7.39 10.89 -12 9 10 7.28 10.7 12 -9 10 -3.01 6.64 -12 9 9 -0.58 13.47 12 -9 9 -0.03 6.5 -12 9 8 44.55 13.08 12 9 -8 68.07 12.39 -12 9 8 74.41 5.38 12 -9 7 8.79 5.66 -12 9 7 -1.4 8 12 -9 7 10.3 13.92 -12 9 7 10.77 3.44 -12 9 6 50.24 5.98 12 9 -6 43.78 8.92 -12 9 6 54.19 4.48 12 -9 6 49.56 5.92 12 9 -5 24.78 7.26 -12 9 5 30.25 3.59 12 -9 5 38.56 4.89 -12 -9 -4 21.04 4.36 12 9 -4 20.07 6.11 -12 9 4 25.1 3.15 12 -9 4 24.11 4.26 -12 9 3 92.54 7.15 -12 9 3 106.49 6.37 -12 -9 -3 110.39 7.5 12 9 -3 102.95 9.05 12 -9 2 23.99 6.38 -12 -9 -2 18.34 6.65 12 9 -2 12.46 7.63 -12 9 1 42.08 4.33 -12 9 1 51.74 3.59 -12 -9 -1 62.38 5.28 12 9 -1 54.78 6.35 12 9 0 -0.67 4.89 -12 9 0 2.66 3.12 -12 9 0 -1.24 2.23 -12 -9 0 1.68 3.69 -12 9 -1 49.63 4.1 -12 9 -1 48.12 3.53 12 9 1 52.96 5.52 -12 -9 2 11.94 2.19 -12 9 -2 7.18 2.97 -12 9 -2 10.47 2.34 -12 -9 3 105.39 6.22 -12 -9 3 104.14 7.51 -12 9 -3 108.15 6.23 -12 -9 3 104.88 6.4 -12 -9 4 21.42 2.95 -12 9 -4 24.51 2.92 -12 -9 4 21.47 4.99 -12 -9 4 22.05 2.7 -12 -9 5 30.79 3.46 -12 9 -5 31.4 3.36 -12 -9 5 27.12 2.95 -12 -9 5 28.31 5.51 -12 -9 6 45.63 4.28 -12 -9 6 54.69 4.06 -12 -9 6 46.75 6.52 -12 -9 7 9.1 3.3 -12 -9 8 62.05 4.91 -12 -9 8 69.13 6.92 -12 -9 9 8.13 3.25 -12 9 -10 -0.13 4.01 -12 -9 10 1.57 2.83 -12 -9 11 0.77 2.37 -12 9 -11 3.03 3.66 -12 -9 12 3.98 1.94 -12 9 -12 5.79 3.18 -12 9 -13 2.18 2.2 -12 -9 13 1.92 1.25 -12 10 11 9.33 10.08 -12 10 10 5.41 10.76 12 -10 10 0.79 6.41 -12 10 9 -2.67 13.8 -12 10 8 -6.03 12.66 12 10 -8 5.28 9.98 -12 10 8 3.21 3.42 -12 10 7 7.94 7.95 12 10 -7 11.01 8.9 -12 -10 -7 11.95 4.91 -12 10 7 15.47 3.67 12 -10 7 8.74 6.01 -12 10 6 63.14 6.59 12 -10 6 76.6 6.76 12 10 -6 61.92 9.62 -12 -10 -6 59.25 6.57 -12 10 6 74.63 5.32 -12 -10 -5 16.31 4.51 -12 10 5 26.92 5.42 12 10 -5 19.34 7.22 -12 10 5 27.04 3.71 12 -10 5 32.22 5.27 -12 -10 -4 10.19 4.18 12 10 -4 4.08 6.14 -12 10 4 5.7 3.09 12 -10 4 10.78 4.54 12 10 -3 45.96 7 -12 10 3 42.48 5.02 -12 10 3 46.5 3.62 -12 -10 -3 44.27 5.25 12 -10 3 39.49 4.86 12 10 -2 31.38 6.2 -12 10 2 31.8 3.03 -12 10 2 26.69 4.23 12 -10 2 20.09 4.23 -12 -10 -2 34.57 4.76 -12 10 1 167.53 8.68 -12 -10 -1 162.41 9.85 12 10 -1 156.98 11.12 12 10 0 25.88 5.55 -12 10 0 33.06 2.95 -12 10 0 23.42 3.73 -12 -10 0 26.37 4.33 -12 10 -1 167.96 9.79 -12 10 -1 174.64 9.4 -12 -10 1 160.04 10.57 -12 -10 2 35.19 3.07 -12 10 -2 35.79 3.2 -12 10 -2 32.45 3.79 -12 -10 2 31.86 2.94 -12 10 -3 40.88 3.96 -12 -10 3 38.3 3.4 -12 10 -3 37.02 3.42 -12 -10 3 36.52 3.22 -12 -10 4 6.35 2.88 -12 10 -4 6.72 2.84 -12 -10 4 12.38 4.8 -12 -10 4 8.81 2.39 -12 -10 5 24.91 3.45 -12 10 -5 27.92 3.41 -12 -10 5 23.92 5.71 -12 -10 6 62.63 5.08 -12 -10 6 65.81 7.19 -12 10 -6 80.68 5.2 -12 -10 7 10.74 3.32 -12 10 -7 11.98 3.67 -12 -10 8 2.73 3.16 -12 -10 8 5.5 3.63 -12 -10 8 2.41 5.12 -12 10 -8 1.24 3.73 -12 -10 9 -2.47 3.05 -12 -10 10 6.14 2.66 -12 -10 11 3.68 2.12 -12 -10 12 1.64 1.6 -12 10 -12 0.01 2.86 -12 -10 13 0.38 0.97 -12 10 -13 0.53 1.88 12 -11 12 -0.78 4.67 -12 11 11 2.31 9.27 -12 11 10 4.31 10.18 12 -11 10 2.13 6.16 -12 11 9 8.23 13.56 -12 11 8 13.39 12.44 -12 11 8 1.8 3.3 12 -11 8 0.03 6.27 -12 -11 -7 37.35 5.93 -12 11 7 61.8 8.57 12 11 -7 69.21 10.34 -12 11 7 63.08 4.74 12 -11 7 47.9 6.99 -12 11 6 29.17 6.06 12 -11 6 36.03 6.09 12 11 -6 26.52 8.27 -12 11 6 31.17 3.95 -12 -11 -6 16.74 5.06 -12 11 5 55.66 6.67 12 11 -5 53.03 8.54 -12 -11 -5 51.35 6.17 -12 11 5 57.94 4.96 -12 -11 -4 95.06 8.08 -12 11 4 100.88 6.71 12 11 -4 94.18 9.73 -12 11 3 92.16 7.24 -12 11 3 94.81 6 -12 -11 -3 108.87 7.76 12 11 -3 91.93 9.03 12 -11 3 97.83 7.26 12 11 -2 42.55 6.92 -12 11 2 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11 6.71 11.05 13 -4 10 20.92 2.27 -13 4 10 23.31 9.49 13 4 -10 42.31 28.4 13 -4 9 95.03 5.35 -13 4 9 92.94 5.91 -13 4 8 95.95 6.47 -13 4 8 100.14 6.04 13 -4 8 102.74 5.65 13 4 -7 34.94 29.89 13 -4 7 19.9 1.95 -13 4 7 15.73 2.39 13 -4 7 19.21 5.98 -13 4 7 14.18 3.26 -13 4 7 16.2 9.81 13 -4 6 150.27 11.67 -13 4 6 159.1 8.68 13 -4 5 219.41 13.54 -13 4 5 204.71 9.09 -13 4 5 198.41 10.56 13 4 -4 337.9 27.64 -13 4 4 277.09 15.11 -13 4 3 105.98 6.23 13 4 -2 51.3 18.15 -13 4 2 34.01 2.9 13 4 -1 41.79 14.92 -13 4 1 48.41 3.42 13 4 0 -4.89 11.92 -13 -4 0 5.52 3.14 13 4 0 2.67 4.45 -13 4 0 1.69 1.8 -13 -4 1 56.97 4.86 13 4 1 54.97 12.46 13 4 1 45.23 4.45 -13 -4 2 36.1 4.19 13 4 2 30.71 11.54 -13 -4 3 109.32 7.39 -13 -4 3 116.01 6.96 -13 -4 4 291.14 16.12 -13 -4 4 284.66 15.61 -13 -4 5 218.79 12.5 -13 -4 5 249.3 13.69 -13 4 -5 230.77 12.4 -13 -4 5 249.83 12.93 -13 -4 6 150.51 8.75 -13 -4 6 144.29 10.07 -13 4 -6 157.36 8.65 -13 -4 6 149.81 9.11 -13 -4 6 161.77 8.45 -13 -4 7 15.32 2.96 -13 4 -7 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141.54 7.83 13 5 -1 869.89 51.54 13 5 -1 933.76 53.13 -13 -5 -1 1050.85 51.14 -13 -5 0 119.29 7.35 13 5 0 99.78 7.81 13 5 0 114.58 13.71 13 5 1 951.26 49.34 -13 -5 1 918.11 47.4 13 5 1 868.96 47.41 -13 -5 2 128.15 8.31 13 5 2 159.39 13.23 -13 -5 3 42.7 3.6 -13 -5 3 36.77 4.52 -13 -5 4 141.68 8.17 -13 -5 4 154.31 9.34 -13 -5 4 150.51 8.53 -13 -5 5 131.8 7.89 -13 -5 5 140.49 9.26 -13 5 -5 143.86 7.79 -13 -5 5 142.02 8.26 -13 -5 6 41.05 3.69 -13 5 -6 45.69 3.59 -13 -5 6 48.17 3.96 -13 -5 6 39.52 5.36 -13 -5 7 8.54 3.44 -13 -5 7 7.43 2.03 -13 -5 7 7.8 3.01 -13 5 -7 9.12 2.95 -13 -5 7 8.88 2.86 -13 -5 8 37.29 4.8 -13 -5 8 34.29 3.04 -13 -5 8 34.86 4.26 -13 -5 8 37.24 3.82 -13 -5 8 37.31 5.24 -13 5 -8 39.43 3.99 -13 -5 9 68.96 5.72 -13 -5 9 86.07 5.52 -13 5 -9 80.9 5.74 -13 -5 9 78.78 6.2 -13 -5 10 20.23 3.66 -13 -5 10 25.18 3.52 -13 5 -10 27.79 4.07 -13 -5 11 30.82 3.56 -13 -5 11 34.88 3.5 -13 5 -11 31.36 4.15 -13 -5 12 7.61 2.46 -13 -5 12 8.01 2.47 -13 5 -12 8.83 3.27 -13 5 -13 6.67 1.63 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115.32 6.16 -13 7 5 10.32 4.23 13 7 -5 12.95 7.85 13 -7 5 9.99 5.24 13 7 -5 5.94 17.83 -13 7 4 23.59 2.17 -13 7 4 22.7 4.06 -13 7 4 26.24 2.95 13 7 -4 20.74 6.49 13 -7 4 28.64 4.06 13 7 -4 26.05 14.82 -13 7 3 20.25 3.75 -13 7 3 23.31 2.61 13 7 -3 27.4 6.13 13 7 -3 35.34 13.55 13 7 -2 181.84 16.54 13 7 -2 180.41 11.89 13 7 -1 53.04 6.13 13 7 -1 57.74 13.31 13 7 0 18 4.55 13 7 0 10.21 11.91 -13 -7 0 17.21 3.93 -13 -7 1 58.12 5.21 -13 -7 2 175.1 9.67 -13 -7 2 192.61 10.71 -13 -7 3 21.26 4.17 -13 -7 3 24.08 2.62 -13 -7 3 22.21 2.84 -13 7 -3 23.77 2.55 -13 -7 4 21.93 2.75 -13 7 -4 23.09 2.63 -13 -7 4 25.94 4.32 -13 -7 4 19.15 2.67 -13 7 -5 5.69 2.51 -13 -7 5 11.92 4.08 -13 -7 5 10.94 2.61 -13 -7 6 118.97 8.95 -13 7 -6 125.4 7.13 -13 -7 6 113.88 7.38 -13 -7 7 17.81 3.09 -13 7 -7 22.48 3.5 -13 -7 7 18.87 3.21 -13 -7 8 -0.91 3 -13 -7 8 -0.78 4.98 -13 7 -8 -0.04 3.49 -13 -7 8 -1.31 4.1 -13 -7 9 25.08 3.32 -13 -7 9 22.7 4.82 -13 7 -9 28.4 4.14 -13 -7 9 19.62 4.18 -13 -7 10 1.16 2.82 -13 7 -10 0.08 3.8 -13 -7 11 7.05 2.74 -13 7 -11 1.45 3.62 -13 -7 12 2.62 2.2 -13 7 -12 2.7 3.07 -13 -7 13 5.47 1.61 -13 7 -13 2.76 2.41 -13 8 11 9.43 11.07 -13 8 10 8.21 10.94 -13 8 9 50.34 12.98 -13 8 8 49.53 13.95 -13 8 8 57.65 4.91 -13 8 8 57.37 4.05 13 -8 7 1.7 11.4 13 8 -7 3.51 9.37 -13 8 7 10.17 9.16 -13 8 7 2.45 3.48 13 -8 7 -3.15 5.69 -13 8 7 8.42 2.33 -13 8 6 3.57 5.56 13 8 -6 12.64 8.29 -13 8 6 13.31 3.44 13 -8 6 6.05 4.87 13 8 -6 2.03 20.4 -13 8 6 11.02 2.14 -13 8 5 119.16 6.99 13 -8 5 103.82 7.77 13 8 -5 112.43 10.54 13 8 -4 37.79 15.26 -13 8 4 24.35 4.42 13 8 -4 29.25 6.5 -13 8 4 26.43 3.21 13 -8 4 33.84 4.39 -13 8 3 27.11 4.27 -13 8 3 36.71 3.18 13 8 -3 36.5 5.99 -13 -8 -3 42.81 4.8 13 -8 3 51.18 4.3 13 8 -3 46.23 14.17 13 8 -2 49.62 5.96 -13 8 2 50.18 3.37 -13 -8 -2 52.83 4.7 -13 8 1 176.81 10.62 -13 8 1 194.15 10.28 13 8 -1 208.83 16.86 13 8 -1 200.33 12.15 13 8 0 26.44 5.23 -13 8 0 32.31 2.77 -13 8 -1 212.91 11.42 -13 -8 1 207.82 12.31 -13 -8 2 57.99 3.77 -13 8 -2 56.31 3.86 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5.64 3.9 -13 9 3 46.71 5.13 -13 9 3 56.41 4.1 13 9 -3 49.85 6.77 -13 -9 -3 61.94 5.56 -13 9 2 62.03 4.25 -13 -9 -2 74.99 5.79 -13 9 2 53.92 5.06 13 9 -2 59.64 6.84 -13 9 1 70.65 5.54 -13 9 1 86.84 4.94 -13 -9 -1 73.2 6.16 13 9 -1 77.88 7.21 -13 9 0 329.93 19.18 -13 9 0 376.12 18.97 13 9 0 364.31 20.67 -13 9 -1 75.44 5.28 -13 9 -1 80.64 4.9 -13 9 -2 63.67 4.21 -13 -9 2 61.43 4.16 -13 -9 2 61.53 5.59 -13 -9 3 59.38 5.62 -13 9 -3 56.31 3.95 -13 -9 3 47.06 4.02 -13 -9 3 57.07 4 -13 -9 4 3.57 2.77 -13 -9 4 3.03 2.29 -13 9 -4 3.06 2.62 -13 -9 4 2.3 4.42 -13 -9 5 48.9 4.16 -13 -9 5 47.38 3.99 -13 -9 5 47.92 6.24 -13 -9 6 32.01 3.87 -13 -9 6 35.67 3.5 -13 -9 6 44.08 6.03 -13 -9 7 13.12 3.36 -13 -9 8 24.78 5.4 -13 9 -8 24.19 4.03 -13 -9 8 19.93 3.65 -13 -9 9 11.78 3.32 -13 9 -9 12.48 4.02 -13 -9 10 -0.96 2.85 -13 9 -10 -0.61 3.74 -13 -9 11 3.28 2.44 -13 9 -11 1.08 3.47 -13 9 -12 -1.36 2.88 -13 -9 12 -0.95 1.84 -13 9 -13 -0.54 1.93 -13 -9 13 0.61 1.17 -13 10 11 9.64 10.38 -13 10 10 0.37 10.78 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8 5.43 10.51 -14 5 8 2.47 2.68 14 5 -8 -14.89 37.86 -14 5 8 4.74 3.56 14 -5 7 -1.28 6.19 -14 5 7 12.93 11.06 -14 5 7 -1.09 2.33 -14 5 7 1.86 3.31 14 5 -7 17.7 30.3 14 5 -6 31.64 22.6 14 -5 6 20.15 8.59 -14 5 6 17.98 3.12 14 -5 6 -2.64 5.04 -14 5 6 12.01 2.26 14 -5 5 77.51 10.84 -14 5 5 94.17 4.61 -14 5 5 67.23 6.77 -14 5 4 156.11 10.49 14 5 -4 201.02 19.43 14 -5 4 224.48 10.66 -14 5 4 179.4 9.81 -14 5 3 16.24 2.25 -14 5 2 155.07 8.56 14 5 -2 155 16.11 -14 -5 -1 10.96 3.69 14 5 -1 11.41 4.64 14 5 -1 8.12 11.92 14 5 0 114.44 13.55 -14 -5 0 126.3 7.66 14 5 0 108.79 7.99 14 5 1 -3.49 11.14 -14 -5 1 16.48 3.63 -14 -5 2 135.44 8.3 14 5 2 149.29 13.68 -14 -5 3 17.78 3.01 -14 -5 3 13.93 3.83 -14 -5 4 189.3 10.42 -14 -5 4 193.96 11.46 -14 5 -4 190.17 10.31 -14 -5 4 194.73 10.8 -14 -5 5 87.61 5.57 -14 -5 5 85.25 6.68 -14 5 -5 92.07 5.36 -14 -5 5 89.37 5.93 -14 -5 6 15.02 2.92 -14 5 -6 15.14 2.55 -14 -5 6 16.3 4.75 -14 -5 6 14.01 2.85 -14 -5 6 10.86 1.89 -14 -5 7 3.41 3.36 -14 -5 7 0.69 3.06 -14 5 -7 1.61 2.8 -14 -5 7 1.12 2.87 -14 -5 7 0.61 2.04 -14 -5 8 2.52 4.02 -14 -5 8 3.12 3.23 -14 -5 8 0.47 3.66 -14 5 -8 1.73 3.2 -14 -5 8 2.19 2.21 -14 -5 9 12.22 3.67 -14 5 -9 16.9 3.6 -14 -5 9 11.19 3.41 -14 -5 9 10.43 3.88 -14 -5 10 1.97 3.09 -14 -5 10 1.89 3.22 -14 5 -10 1 3.49 -14 -5 11 -0.1 2.87 -14 -5 11 -2.15 2.85 -14 5 -11 2.84 3.33 -14 5 -12 0.43 1.86 -14 -5 12 2.29 2.34 -14 -5 12 -0.38 2.38 -14 5 -12 2.26 2.97 -14 -5 13 2.16 1.69 -14 5 -13 1.52 1.39 -14 5 -13 2.45 2.23 -14 -5 14 0.32 1.03 -14 6 13 2.8 2.13 -14 -6 -13 0.42 1.73 14 6 -13 3.09 6.82 -14 6 11 0.61 11.56 -14 6 10 70.17 11.78 -14 6 9 24.16 10.86 14 6 -9 42.85 17.47 -14 6 9 31.06 3.4 -14 6 8 34.11 12.51 -14 6 8 36.3 4.3 -14 6 8 37.52 3.45 -14 6 7 68.21 11.76 14 -6 7 43.44 8.08 14 -6 7 -3.83 6.63 -14 6 7 62.15 4.71 14 6 -7 58.69 12.93 -14 6 7 61.35 3.89 14 6 -7 123.47 30.03 14 -6 6 131.3 13.05 -14 6 6 135.8 7.07 -14 6 6 133.63 6.58 14 6 -6 127.66 13.27 -14 6 5 45.99 5.85 14 6 -5 62.45 9.46 -14 6 5 61.52 4.46 14 -6 5 53.11 5.65 -14 6 5 66.28 3.89 14 6 -4 85.43 15.69 14 6 -4 74.41 8.56 14 -6 4 89.4 5.53 -14 6 4 67.65 4.07 14 6 -3 26.91 5.79 -14 6 3 19.25 3.7 14 6 -2 76.31 7.35 14 6 -2 89.16 13.48 -14 -6 -1 32.67 4.16 14 6 -1 29.17 5.38 14 6 -1 29.17 11.97 -14 -6 0 68.21 5.41 14 6 0 53.97 5.52 14 6 0 65.77 12.14 14 6 1 30.98 11.4 -14 -6 1 26.49 4.05 -14 -6 2 78.49 5.79 -14 -6 3 29.52 2.75 -14 -6 3 24.17 3.97 -14 6 -3 25.43 2.54 -14 -6 3 30.47 3.12 -14 -6 4 59.16 4.36 -14 -6 4 73.43 5.89 -14 6 -4 67.28 4.26 -14 -6 4 71.99 4.8 -14 -6 5 68.18 4.77 -14 -6 5 66.21 6.19 -14 6 -5 71.75 4.48 -14 -6 5 68.62 4.92 -14 -6 6 121.14 7.69 -14 -6 6 128.53 7.76 -14 -6 6 136.26 9.49 -14 6 -6 138.92 7.63 -14 -6 6 140.9 8.07 -14 -6 7 45.95 4.22 -14 -6 7 52.87 4.27 -14 6 -7 57.46 4.06 -14 -6 7 46.22 4.35 -14 -6 8 28.54 3.67 -14 -6 8 34.38 3.8 -14 -6 8 30.52 5.5 -14 6 -8 32.63 3.88 -14 -6 8 36.38 4.79 -14 -6 9 31.45 3.74 -14 -6 9 38.52 3.99 -14 6 -9 34.73 4.23 -14 -6 9 40.23 4.6 -14 -6 10 109.55 6.82 -14 6 -10 107.94 7.07 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30.92 4.14 -14 -7 2 88.77 5.26 -14 7 -2 88.13 5.25 -14 -7 2 92.96 6.59 -14 -7 3 292.45 16.69 -14 7 -3 290.47 15.7 -14 -7 3 308.19 16.09 -14 7 -4 8.95 2.45 -14 -7 4 10.55 4.12 -14 7 -5 4.78 2.62 -14 -7 5 4.98 4.3 -14 -7 5 5.3 2.66 -14 -7 6 75.07 7.17 -14 7 -6 78.51 5.15 -14 -7 6 78.97 5.46 -14 -7 7 2.82 2.79 -14 7 -7 7.14 3.14 -14 -7 7 4.08 2.78 -14 -7 8 10.07 3.02 -14 -7 8 11.18 4.2 -14 -7 8 6.18 5.19 -14 7 -8 8.64 3.45 -14 -7 9 53.07 4.56 -14 -7 9 67.29 4.95 -14 7 -9 68.27 5.17 -14 -7 9 67.85 5.6 -14 -7 10 4.32 2.72 -14 -7 10 4.19 3.19 -14 7 -10 2.84 3.68 -14 -7 11 5.69 2.65 -14 7 -11 7.72 3.44 -14 -7 12 4.58 2.14 -14 7 -12 0.38 2.9 -14 -7 13 10.93 1.62 -14 7 -13 8.81 2.2 -14 -8 -12 1.17 1.8 -14 8 11 -0.04 10.97 -14 8 10 13.1 11.21 -14 8 9 12.47 12.51 -14 8 8 -0.03 14.29 -14 8 8 4.29 3.72 -14 8 8 2.6 2.53 -14 8 7 5.3 10.98 14 -8 7 6.96 10.35 14 8 -7 19.18 9.93 -14 8 7 18.23 2.62 -14 8 7 18.27 3.79 14 -8 7 -4.56 6.09 14 8 -6 27.65 8.39 14 -8 6 18.62 5.59 -14 8 6 29.18 3.84 -14 8 6 25.35 2.61 14 8 -6 37.65 21.71 -14 8 5 19.22 4.61 14 8 -5 19.88 18.38 14 8 -5 21.4 7.22 -14 8 5 19.25 3.43 14 -8 5 26.19 4.82 -14 8 4 6.09 4.15 14 8 -4 12.31 6.25 -14 8 4 8.86 2.96 14 -8 4 8.88 4.07 14 8 -4 3.89 15.58 -14 8 3 112.91 8.93 -14 8 3 139.9 8.3 -14 -8 -3 176.13 9.68 14 8 -3 134.84 10.71 14 -8 3 194.58 9 -14 8 2 58.16 5.06 14 8 -2 63.23 6.54 -14 8 2 72.71 4.36 -14 -8 -2 59.61 5.71 -14 8 1 70.26 5.18 -14 8 1 76.41 4.6 14 8 -1 69.12 6.74 14 8 -1 68.94 13.12 14 8 0 3.32 3.88 -14 8 0 9.52 3 -14 8 0 8.18 2.29 -14 -8 0 9.35 3.68 -14 8 -1 72.48 4.58 -14 -8 1 77.39 5.91 -14 -8 2 68.35 4.37 -14 -8 2 67.6 5.78 -14 -8 3 156.05 8.64 -14 -8 3 149.41 9.76 -14 -8 3 155.43 8.94 -14 -8 4 9.69 2.39 -14 -8 4 8.61 2.71 -14 -8 4 10.05 4.09 -14 -8 5 19.22 3.37 -14 8 -5 20.35 2.98 -14 -8 5 15.82 4.78 -14 -8 5 17.28 2.96 -14 8 -6 27.81 3.47 -14 -8 6 25.69 3.58 -14 -8 6 23.41 5.53 -14 -8 6 24.76 3.26 -14 8 -7 20.3 3.59 -14 -8 7 15.17 3.03 -14 -8 8 2.09 2.74 -14 -8 8 2.47 4.99 -14 8 -8 2.32 3.51 -14 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26.64 4.53 -14 -9 3 79.26 4.95 -14 -9 3 69.92 6.34 -14 9 -3 78.4 4.89 -14 -9 3 67.85 4.97 -14 -9 4 104.64 6.5 -14 -9 4 105.22 8.07 -14 -9 4 108.09 6.64 -14 -9 5 115.99 8.79 -14 -9 5 112.13 6.82 -14 -9 5 102.69 6.76 -14 -9 6 59.6 4.7 -14 -9 6 62.1 6.91 -14 -9 6 50 4.41 -14 -9 7 23.62 3.87 -14 9 -7 39.42 4.03 -14 -9 8 4.46 3.41 -14 -9 8 2.1 4.89 -14 9 -8 5.95 3.73 -14 -9 8 3.34 3.86 -14 9 -9 6.97 3.76 -14 -9 9 7.71 3.28 -14 -9 10 2.42 2.86 -14 9 -10 4.16 3.68 -14 -9 11 11.13 2.41 -14 9 -11 8.34 3.3 -14 -9 12 3.46 1.73 -14 9 -12 0.11 2.59 -14 9 -13 4.08 1.73 -14 10 11 0.52 10.16 -14 10 10 14.83 10.87 -14 10 9 20.59 13.24 -14 10 8 -8.95 14.42 -14 10 8 -1.09 3.49 14 -10 8 -0.51 6.57 -14 -10 -7 16.35 5.25 -14 10 7 35.32 10.36 14 10 -7 24.45 8.88 14 -10 7 10.29 12.34 -14 10 7 33.02 4.08 14 -10 7 8 6.32 -14 10 6 58.82 7.13 14 10 -6 56.89 9.05 -14 -10 -6 48.89 6.38 -14 10 6 61.32 5.05 14 -10 6 56.32 6.64 14 10 -5 60.29 8.47 -14 -10 -5 58.15 6.55 -14 10 5 72.89 5.42 14 -10 5 83.18 6.75 -14 10 4 154.28 11.19 -14 -10 -4 175.99 11.82 -14 10 4 183.4 10.56 14 10 -4 162.2 13.06 -14 10 3 7.91 4.55 14 10 -3 6.4 6.06 -14 10 3 8.47 3.05 14 -10 3 13.31 4.69 -14 -10 -3 9.79 4.41 14 10 -2 27.77 6.18 -14 10 2 28.09 4.7 -14 10 2 42.91 3.69 -14 -10 -2 41.93 5.29 14 10 -1 35.56 6.11 -14 10 1 38.39 3.47 -14 10 1 33.57 4.45 -14 -10 -1 37.49 4.87 -14 10 0 11.1 3.66 -14 10 0 14.12 2.83 -14 -10 0 14.5 4.06 -14 10 -1 35.71 4.11 -14 -10 1 38.34 3.3 -14 10 -1 37.93 3.43 -14 -10 2 31.3 3.17 -14 10 -2 32.49 3.31 -14 10 -2 29.52 3.78 -14 -10 2 27.84 2.98 -14 -10 3 10.44 2.91 -14 10 -3 10.92 2.84 -14 -10 3 4.64 4.51 -14 -10 3 8.26 2.45 -14 -10 4 170.25 9.73 -14 -10 4 166.79 11.3 -14 10 -4 183.73 9.67 -14 -10 4 157.96 9.81 -14 -10 5 67.69 5.09 -14 -10 5 68.11 7.15 -14 10 -5 78.91 5 -14 -10 5 56.95 4.73 -14 -10 6 43.8 4.28 -14 -10 6 44.74 6.42 -14 -10 7 23.93 3.73 -14 -10 8 1.99 3.31 -14 -10 9 21.44 3.42 -14 -10 10 23.91 2.98 -14 10 -10 24 3.79 -14 10 -11 1.84 3.01 -14 -10 11 2.08 2.07 -14 10 -12 -0.01 2.4 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11.55 -15 6 5 12.35 2.08 15 6 -5 17.51 8.54 15 6 -4 40.62 15.63 -15 6 4 24.07 4.36 -15 6 4 29.65 2.55 15 -6 4 45.44 4.59 15 6 -4 32.45 6.82 15 6 -3 63.08 6.86 -15 6 3 60.66 5.11 -15 6 3 75.89 4.45 -15 6 3 62.68 3.97 15 6 -2 108.55 14.12 -15 6 2 108.76 6.22 15 6 -2 93.45 8.3 -15 -6 -2 114.74 7.3 -15 -6 -1 23.24 3.83 15 6 -1 15.11 11.41 15 6 -1 18.19 4.68 15 6 0 33.87 4.62 -15 -6 0 37.01 4.2 15 6 0 32.56 11.83 15 6 1 28.49 11.19 -15 -6 1 17.69 3.78 -15 6 -2 101.46 5.71 -15 -6 2 91.62 6.76 -15 -6 3 71.95 4.78 -15 -6 3 76.53 5.84 -15 6 -3 75.93 4.67 -15 -6 4 30.25 3.22 -15 6 -4 37.32 3 -15 -6 4 35.83 3.48 -15 -6 4 36.94 4.46 -15 -6 5 12.03 2.98 -15 6 -5 9.74 1.55 -15 6 -5 13.74 2.52 -15 -6 5 11.58 4.21 -15 -6 5 12.46 2.87 -15 6 -6 17.6 1.89 -15 -6 6 14.14 3.31 -15 6 -6 17.16 2.84 -15 -6 6 10.2 4.87 -15 -6 6 15.22 3.16 -15 -6 7 0.54 3.05 -15 -6 7 1.41 3.25 -15 6 -7 4.28 2.9 -15 -6 7 1.59 2.91 -15 -6 8 9.63 3.19 -15 -6 8 11.6 3.42 -15 -6 8 14.08 4.28 -15 6 -8 13.64 3.26 -15 -6 8 8.57 3.09 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36.99 16.07 -15 7 3 15.52 3.93 -15 7 3 23.64 2.74 15 7 -3 24.01 5.74 -15 7 3 20.37 2.1 15 -7 3 31.27 4.24 -15 7 2 223.41 12.78 15 7 -2 263.95 18.54 15 7 -2 241.78 14.23 -15 -7 -1 78.82 5.93 15 7 -1 62.98 6.24 15 7 -1 60.71 13.04 -15 -7 0 264.07 14.56 15 7 0 241.66 14.69 15 7 0 255.49 18.63 -15 7 -1 66.12 4.22 -15 -7 1 64.92 5.33 -15 7 -2 263.2 13.7 -15 -7 2 235.33 14.53 -15 -7 3 18.37 4.17 -15 -7 3 23.5 3.04 -15 7 -3 23.79 2.58 -15 7 -4 34.71 3.04 -15 -7 4 30.15 3.25 -15 -7 4 32.59 4.75 -15 7 -5 20.43 2.86 -15 -7 5 19.5 4.55 -15 -7 5 14.15 2.94 -15 7 -6 42.4 3.66 -15 -7 6 33.67 3.77 -15 -7 6 35.82 5.6 -15 -7 7 3.82 2.83 -15 -7 7 8.31 3.51 -15 7 -7 6.98 3.17 -15 -7 7 4.23 2.92 -15 -7 8 34.12 3.64 -15 -7 8 36.37 4.14 -15 -7 8 44.7 4.92 -15 7 -8 38.05 4.14 -15 -7 8 41.46 5.91 -15 -7 9 5.93 2.75 -15 -7 9 6.87 3.4 -15 7 -9 8.43 3.55 -15 -7 10 1.01 2.52 -15 -7 10 1.61 3.16 -15 7 -10 -1.89 3.5 -15 -7 11 5.22 2.62 -15 7 -11 9.16 3.3 -15 -7 12 7.11 1.99 -15 7 -12 0.89 2.74 -15 -7 13 1.06 1.34 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81.23 6.56 -15 -8 3 39.75 5.03 -15 8 -3 43.89 3.47 -15 -8 3 45.61 3.63 -15 -8 3 43.98 3.71 -15 -8 4 73.08 6.52 -15 -8 4 74.45 4.99 -15 8 -4 74.17 4.79 -15 -8 4 66.14 4.97 -15 8 -5 18.64 3.05 -15 -8 5 11.55 4.74 -15 -8 5 17.19 2.93 -15 8 -6 13.83 3.11 -15 -8 6 11.29 5.26 -15 -8 6 8.07 2.92 -15 8 -7 17.12 3.46 -15 -8 7 12.01 2.98 -15 -8 8 4.49 3.95 -15 -8 8 1.42 2.72 -15 -8 8 5.98 4.88 -15 8 -8 7.28 3.55 -15 -8 9 9.36 2.69 -15 8 -9 10.86 3.78 -15 8 -10 49.89 4.64 -15 8 -11 17.69 3.35 -15 -8 12 9.35 1.95 -15 8 -12 6.15 2.65 -15 -8 13 0.31 1.16 -15 8 -13 1.85 1.69 -15 9 12 -1.6 2.35 -15 9 11 -9.95 10.7 -15 9 10 3.45 11.46 -15 9 9 17.84 12.8 -15 9 8 64.72 15.23 -15 9 8 79.25 5.12 -15 9 7 13.98 11.77 15 -9 7 -4.2 10.05 -15 9 7 11.58 2.38 15 9 -7 6.76 8.73 -15 9 7 9.25 3.85 15 -9 7 1.36 6.35 15 -9 6 22.95 15.51 15 9 -6 58.37 9.2 -15 9 6 71.9 5.12 -15 -9 -6 52.01 6.4 15 -9 6 40.78 6.78 -15 9 5 66.54 6.89 15 9 -5 85 9.23 -15 -9 -5 76.35 7.19 -15 9 5 85.51 5.91 15 -9 5 97.15 7.07 -15 -9 -4 19.57 4.54 15 9 -4 6.29 16.07 -15 9 4 17.18 4.85 15 9 -4 17.73 6.07 -15 9 4 20.2 3.66 15 -9 4 21.38 4.9 -15 9 3 63.96 5.96 -15 9 3 66.17 4.8 -15 -9 -3 67.12 6.37 15 9 -3 57.73 7.13 -15 9 2 83.13 6.69 -15 9 2 110.77 6.07 -15 -9 -2 97 7.24 15 9 -2 90.18 8.09 -15 9 1 92.98 6.79 -15 9 1 114.23 6.31 15 9 -1 100.9 8.26 -15 9 0 452.3 25.08 -15 9 0 485.63 24.88 -15 9 -1 102.78 6.59 -15 9 -1 110.73 6.28 -15 -9 1 95.87 7.32 -15 -9 2 106.42 6.17 -15 9 -2 109.09 6.2 -15 -9 2 93.92 7.43 -15 -9 2 96.46 6.31 -15 -9 3 74.49 4.99 -15 -9 3 75.54 6.38 -15 -9 3 72.29 5.04 -15 -9 4 16.81 3.29 -15 -9 4 11.39 4.72 -15 -9 4 16.84 2.86 -15 -9 5 82.54 5.7 -15 -9 5 88.85 7.57 -15 -9 5 78.05 5.61 -15 -9 6 57.64 4.87 -15 -9 6 56.55 6.95 -15 9 -6 67.77 4.79 -15 -9 6 56.81 4.66 -15 -9 7 9.4 3.58 -15 9 -7 6.81 3.49 -15 -9 7 7.09 2.63 -15 -9 8 59.79 4.97 -15 9 -8 65.07 5.1 -15 -9 9 16.53 3.46 -15 9 -9 22.42 3.93 -15 9 -10 12.61 3.63 -15 9 -11 0.66 2.96 -15 9 -12 2.15 2.41 -15 10 11 10.36 9.95 -15 10 10 5.41 10.77 15 -10 9 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5.69 15 -11 3 79.27 6.83 -15 11 2 127.5 9.19 -15 11 2 154.23 8.48 -15 -11 -2 150.77 9.87 15 11 -2 129.97 10.78 -15 11 1 114.23 6.59 -15 -11 -1 105.1 7.87 -15 11 0 4.63 4.1 -15 11 0 -0.71 3.07 -15 -11 0 3.89 4.18 -15 11 -1 98.16 6.95 -15 -11 1 103.93 6.32 -15 11 -1 106.1 6.46 -15 11 -2 134.09 8.46 -15 -11 2 140.66 8.07 -15 11 -2 139.5 8.06 -15 -11 2 133.5 8.21 -15 -11 3 69.82 5.24 -15 -11 3 74.95 7.04 -15 11 -3 80.46 5.17 -15 -11 3 69.29 5 -15 -11 4 11.09 3.55 -15 11 -4 10.45 3.27 -15 -11 4 9.93 5.15 -15 -11 5 18.72 3.67 -15 11 -5 19.1 3.52 -15 -11 5 10.22 5.34 -15 -11 6 12.69 3.57 -15 11 -6 10.59 3.49 -15 -11 6 9.65 5.2 -15 -11 7 7.78 3.39 -15 -11 8 22.77 3.36 -15 -11 9 1.42 2.7 -15 -11 10 9.41 2.33 -15 -11 11 0.6 1.64 -15 11 -11 1.44 2.66 -15 -11 12 3.31 1.09 -15 11 -12 1.16 1.87 -15 12 11 3.65 7.85 -15 12 10 7.48 9.67 -15 12 9 6.07 12.04 -15 12 8 6.85 14.34 -15 12 8 4.7 3.18 15 -12 8 -5.23 6.67 -15 12 7 9.44 11.64 -15 12 7 1.98 3.49 15 -12 7 6.65 6.8 15 -12 6 153.59 9.74 -15 12 6 115.44 7.93 -15 -12 -5 62.44 7.23 -15 12 5 76.63 5.86 -15 12 4 52.13 6.72 15 12 -4 42.96 7.59 15 -12 4 76.07 7.1 -15 -12 -4 50.66 6.33 -15 12 4 66.41 5.37 15 -12 3 47.15 6.57 15 12 -3 34.43 7.07 -15 12 3 42.23 6.13 -15 12 3 46.4 4.31 -15 12 3 45.44 4.82 -15 -12 -3 32.49 5.51 15 12 -2 6.96 5.81 -15 12 2 10.49 5.07 -15 12 2 11.34 3.53 -15 -12 -2 15.04 4.63 -15 12 1 167.65 11.14 -15 12 1 199.94 10.52 -15 -12 -1 172.48 11.59 -15 12 0 52.71 5.84 -15 12 0 66.12 4.83 -15 -12 0 53.69 6.12 -15 -12 0 63.06 4.58 -15 12 -1 161.95 10.77 -15 -12 1 194.21 10.26 -15 12 -1 194.23 10.34 -15 -12 1 152.9 11.54 -15 -12 2 10.87 3.3 -15 12 -2 9.57 4.1 -15 12 -2 12.85 3.36 -15 -12 3 42.14 4.26 -15 12 -3 45.74 4.13 -15 -12 4 48.22 4.63 -15 12 -4 53.51 4.5 -15 -12 4 44.89 6.16 -15 -12 5 60.94 5 -15 12 -5 69.11 4.96 -15 -12 6 93.8 6.39 -15 12 -6 101.28 6.43 -15 -12 7 2.69 3.07 -15 12 -7 6.44 3.51 -15 -12 8 8.64 2.84 -15 12 -8 -0.21 3.42 -15 -12 9 4.01 2.47 -15 12 -9 4.26 3.24 -15 -12 10 10.49 2.07 -15 -12 11 3.93 1.36 -15 13 10 -8.99 8.67 -15 13 9 9.36 10.51 -15 13 8 10.56 13.32 -15 13 8 12.86 3 -15 13 7 46.24 11.9 -15 13 7 39.35 4.06 15 -13 7 39.66 7.26 15 -13 6 33.56 6.8 -15 13 6 28.43 4.13 -15 13 5 36.61 4.53 15 -13 5 42.68 6.91 15 13 -4 33.99 7.11 -15 13 4 31.78 6.5 -15 -13 -4 23.81 5.34 -15 13 4 39.24 4.6 15 13 -3 9.57 5.93 -15 13 3 5.69 5.78 -15 13 3 6.91 4.07 -15 -13 -3 5.07 4.45 -15 13 2 24.72 5.67 -15 13 2 24.07 3.78 -15 -13 -2 21.34 4.82 -15 13 1 6.41 5.1 -15 13 1 9.89 3.61 -15 -13 -1 5.89 4.88 -15 -13 0 15.04 5.04 -15 13 0 18.88 4.97 -15 13 0 17.54 3.6 -15 13 -1 7.76 4.58 -15 13 -1 6.4 3.38 -15 -13 1 5.87 4.68 -15 -13 2 23.47 3.66 -15 13 -2 30.81 3.73 -15 13 -2 22.76 4.66 -15 -13 2 32.54 5.56 -15 -13 3 2.9 3.4 -15 13 -3 2 4 -15 13 -3 4.84 3.22 -15 -13 3 5.29 5.11 -15 -13 4 34.82 4.05 -15 13 -4 33.84 3.9 -15 -13 5 25.9 3.72 -15 13 -5 34.05 3.83 -15 -13 6 21.7 3.53 -15 13 -6 25.39 3.64 -15 -13 7 31.86 3.46 -15 13 -7 34.69 3.82 -15 -13 8 13.24 2.63 -15 13 -8 14.72 3.25 -15 -13 9 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3.74 1.48 -36 -3 -4 3.58 1.3 -36 3 3 14.13 1.85 -36 -3 -3 15.24 1.68 -36 3 2 0.69 1.75 -36 -3 -2 1.9 1.55 -36 3 1 1.13 1.85 -36 -3 -1 2.22 1.54 -36 -3 0 3.82 1.62 -36 3 0 3.69 1.78 -36 -3 1 0.23 1.57 -36 3 -1 1.52 1.7 -36 -3 2 1.14 1.45 -36 3 -2 0.97 1.67 -36 -3 3 13.28 1.59 -36 3 -3 15.93 1.75 -36 -3 4 2.29 1.13 -36 3 -4 3.41 1.37 -36 3 -5 2.66 1.13 -36 4 4 3.7 1.36 -36 -4 -4 4.41 1.22 -36 4 3 4.22 1.5 -36 -4 -3 3.42 1.31 -36 4 2 5.11 1.67 -36 -4 -2 7.09 1.44 -36 4 1 4.96 1.75 -36 -4 -1 2.91 1.42 -36 -4 0 0.76 1.41 -36 4 0 0.71 1.66 -36 -4 1 4.26 1.4 -36 4 -1 4.26 1.65 -36 -4 2 5.68 1.35 -36 4 -2 6.22 1.63 -36 -4 3 2.33 1.14 -36 4 -3 2.83 1.45 -36 4 -4 5.99 1.29 -36 5 4 9.96 1.31 -36 5 3 4.11 1.36 -36 5 2 5.72 1.51 -36 -5 -2 5.69 1.27 -36 -5 -1 13.69 1.49 -36 5 1 14.59 1.73 -36 5 0 29.62 2.28 -36 5 -1 12.79 1.7 -36 5 -2 6.93 1.47 -36 5 -3 3.11 1.28 -36 6 2 2.28 1.25 -36 6 1 1.31 1.3 -36 6 0 15.29 1.61 -36 6 -1 2.59 1.3 -36 6 -2 2.9 1.2 -37 0 0 0.64 1.54 -37 0 -1 16.54 1.82 -37 0 1 15.41 1.85 -37 0 2 25.28 2.18 -37 0 -2 31.66 2.19 -37 0 3 1.96 1.38 -37 0 -3 3.74 1.36 -37 0 4 5.73 1.23 -37 0 -4 6.87 1.28 -37 1 4 3.63 1.2 -37 -1 -4 4.13 1.18 -37 1 3 3.92 1.4 -37 -1 -3 2.58 1.33 -37 1 2 18.84 1.85 -37 -1 -2 17.07 1.76 -37 -1 -1 11.17 1.63 -37 -1 0 3.22 1.54 -37 -1 1 8.72 1.56 -37 -1 2 17.94 1.78 -37 -1 3 3.19 1.3 -37 -2 -4 4.85 1.14 -37 -2 -3 10.43 1.41 -37 -2 -2 5.56 1.4 -37 2 1 7.84 1.61 -37 -2 -1 6.01 1.46 -37 -2 0 11.04 1.61 -37 2 0 10.67 1.7 -37 -2 1 4.62 1.43 -37 2 -1 4.74 1.55 -37 -2 2 3.71 1.33 -37 2 -2 5.21 1.47 -37 -2 3 6.19 1.25 -37 2 -3 8.03 1.41 -37 2 -4 3.98 1.16 -37 3 4 10.58 1.27 -37 3 3 0.33 1.31 -37 -3 -3 0.35 1.15 -37 3 2 8.34 1.53 -37 -3 -2 8.54 1.36 -37 3 1 -1.01 1.5 -37 -3 -1 -0.11 1.32 -37 -3 0 1.93 1.32 -37 3 0 3.83 1.54 -37 -3 1 1.05 1.26 -37 3 -1 0.76 1.45 -37 -3 2 9.62 1.31 -37 3 -2 9.9 1.52 -37 3 -3 -0.37 1.2 -37 4 3 8.56 1.29 -37 4 2 4.28 1.33 -37 4 1 7.52 1.43 -37 -4 -1 5.43 1.23 -37 -4 0 4.12 1.16 -37 4 0 4.64 1.45 -37 4 -1 7.49 1.48 -37 4 -2 4.85 1.31 -37 4 -3 8.19 1.22 -37 5 2 9.32 1.28 -37 5 1 3.83 1.21 -37 5 0 6.59 1.3 -37 5 -1 4.54 1.24 -38 0 0 42.15 2.64 -38 0 1 37.64 2.45 -38 0 -1 39.69 2.47 -38 0 2 2.58 1.14 -38 0 -2 2.44 1.17 -38 0 -3 2.23 1.05 -38 1 3 4.01 1.07 -38 1 2 16.02 1.52 -38 -1 -2 17.54 1.5 -38 1 1 10.35 1.36 -38 -1 -1 5.75 1.3 -38 -1 0 0.86 1.23 -38 -1 1 6 1.25 -38 -1 2 15.1 1.42 -38 -2 -2 2.07 1.06 -38 2 1 4.05 1.24 -38 -2 -1 -0.69 1.11 -38 -2 0 0.55 1.14 -38 2 0 -1.48 1.26 -38 -2 1 0.44 1.07 -38 2 -1 0.42 1.22 -38 2 -2 0.44 1.13 -38 3 2 3.32 1.11 -38 3 1 3.7 1.16 -38 3 0 -0.3 1.16 -38 3 -1 2.95 1.16 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 2 0 0 2.822 1 1 0 2.843