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Information card for entry 1557919
Preview
| Coordinates | 1557919.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | 1,4,8,11-Tetraazatricyclo[6.6.2.2(4,1)]octadecane |
|---|---|
| Formula | C14 H33 Cl3 N4 O2 Zn |
| Calculated formula | C14 Cl3 N4 O Ow Zn |
| Title of publication | An Inert Proton Coordinated Inside a Nearly Tetrahedral Tetraamine Cavity. Synthesis and X-Ray Crystal Structure of the Aquatrichlorozincate(II) Salt of the Inside Monoprotonated Amine 1,4,8,11-Tetraazatricyclo[6.6.2.2(4,1)]octadecane |
| Authors of publication | Springborg, Johan; Olsen, Carl Erik; Sotofte, Inger |
| Journal of publication | Acta Chemica Scandinavica |
| Year of publication | 1995 |
| Journal volume | 49 |
| Pages of publication | 555 - 563 |
| a | 11.505 ± 0.004 Å |
| b | 8.186 ± 0.004 Å |
| c | 11.185 ± 0.006 Å |
| α | 90° |
| β | 105.87 ± 0.03° |
| γ | 90° |
| Cell volume | 1013.3 ± 0.8 Å3 |
| Ambient diffraction temperature | 120 K |
| Number of distinct elements | 6 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for significantly intense reflections | 0.0448 |
| Weighted residual factors for all reflections included in the refinement | 0.1032 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 251187 (current) | 2020-04-27 | cif/ Adding structures of 1557919 via cif-deposit CGI script. |
1557919.cif |
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