#------------------------------------------------------------------------------ #$Date: 2020-05-05 22:59:05 +0300 (Tue, 05 May 2020) $ #$Revision: 251751 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/80/1558004.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1558004 loop_ _publ_author_name 'Lykova, Inna' 'Varlamov, Dmitry' 'Chukanov, Nikita' 'Pekov, Igor' 'Belakovskiy, Dmitry' 'Ivanov, Oleg' 'Zubkova, Natalia' 'Britvin, Sergey' _publ_section_title ; Chromium Members of the Pumpellyite Group: Shuiskite-(Cr), Ca2CrCr2[SiO4][Si2O6(OH)](OH)2O, a New Mineral, and Shuiskite-(Mg), a New Species Name for Shuiskite ; _journal_issue 5 _journal_name_full Minerals _journal_page_first 390 _journal_paper_doi 10.3390/min10050390 _journal_volume 10 _journal_year 2020 _chemical_formula_sum 'Al0.6 Ca2 Cr1.92 H3.48 Mg0.48 O14 Si3' _chemical_formula_weight 519.63 _chemical_name_common shuiskite-(Cr) _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_Hall '-C 2y' _space_group_name_H-M_alt 'C 1 2/m 1' _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 97.833(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 19.2436(6) _cell_length_b 5.9999(2) _cell_length_c 8.8316(3) _cell_measurement_reflns_used 4699 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 34.6290 _cell_measurement_theta_min 2.9260 _cell_volume 1010.18(6) _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.960 _diffrn_measurement_device_type 'Xcalibur S' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0000 _diffrn_reflns_av_unetI/netI 0.0286 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.960 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 3579 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.960 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 34.792 _diffrn_reflns_theta_min 2.938 _exptl_absorpt_coefficient_mu 3.618 _exptl_absorpt_correction_T_max 0.845 _exptl_absorpt_correction_T_min 0.495 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour grey-green _exptl_crystal_density_diffrn 3.417 _exptl_crystal_description needle _exptl_crystal_F_000 1028 _exptl_crystal_size_max 0.377 _exptl_crystal_size_mid 0.053 _exptl_crystal_size_min 0.049 _refine_diff_density_max 1.342 _refine_diff_density_min -1.706 _refine_diff_density_rms 0.285 _refine_ls_extinction_coef 0.0012(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.076 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 127 _refine_ls_number_reflns 3579 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.076 _refine_ls_R_factor_all 0.0644 _refine_ls_R_factor_gt 0.0469 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0434P)^2^+5.7592P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1033 _refine_ls_wR_factor_ref 0.1088 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2793 _reflns_number_total 3579 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file minerals-782521-supplementary.cif _cod_data_source_block 6133 _cod_original_cell_volume 1010.17(6) _cod_original_sg_symbol_H-M 'C 2/m' _cod_original_formula_sum 'Al0.60 H3.48 Ca2 Cr1.92 Mg0.48 O14 Si3' _cod_database_code 1558004 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL saran-6133-full_hklf5 in C2/m 6133.res created by SHELXL-2018/3 at 15:40:05 on 23-Oct-2019 REM C2/m (#12 in standard setting) CELL 0.71073 19.243617 5.999870 8.831574 90.0000 97.8328 90.0000 ZERR 4.00 0.000640 0.000218 0.000331 0.0000 0.0031 0.0000 LATT 7 SYMM -x, y,-z SFAC O Mg Al Si Ca Cr H UNIT 56.00 1.92 2.40 12.00 8.00 7.68 13.92 L.S. 14 BOND FMAP 2 PLAN 20 acta omit 2 0 -4 omit -1 -1 0 WGHT 0.043400 5.759200 EXTI 0.001205 BASF 0.07519 FVAR 2.01561 0.48426 0.69964 0.51579 0.30047 MOLE 1 CA1 5 0.339452 0.500000 0.251774 10.50000 0.00603 0.01121 = 0.00820 0.00000 0.00250 0.00000 CA2 5 0.154857 0.500000 0.188083 10.50000 0.00632 0.00719 = 0.01909 0.00000 -0.00036 0.00000 sump 1.0 0.001 1.0 2 1.0 4 exyz Cr1 Mg1 eadp Cr1 Mg1 CR1 6 0.250000 0.250000 0.500000 40.50000 0.00510 0.00507 = 0.00628 0.00066 0.00163 0.00048 MG1 2 0.250000 0.250000 0.500000 20.50000 0.00510 0.00507 = 0.00628 0.00066 0.00163 0.00048 sump 1.0 0.001 1.0 3 1.0 5 exyz Cr2 Al2 eadp Cr2 Al2 CR2 6 0.495320 0.247299 0.253944 31.00000 0.00410 0.00472 = 0.00505 0.00038 0.00116 0.00036 AL2 3 0.495320 0.247299 0.253944 51.00000 0.00410 0.00472 = 0.00505 0.00038 0.00116 0.00036 SI1 4 0.091592 0.000000 0.051279 10.50000 0.00456 0.00589 = 0.00451 0.00000 0.00095 0.00000 SI2 4 0.248117 0.000000 0.165225 10.50000 0.00551 0.00607 = 0.00627 0.00000 -0.00016 0.00000 SI3 4 0.401947 0.000000 0.465346 10.50000 0.00376 0.00578 = 0.00510 0.00000 0.00113 0.00000 O1 1 0.073861 0.223043 0.137280 11.00000 0.00834 0.00751 = 0.00983 -0.00116 0.00372 -0.00050 O2 1 0.246429 0.229259 0.265693 11.00000 0.00851 0.00721 = 0.00821 -0.00046 0.00071 -0.00022 O3 1 0.414677 0.220866 0.367075 11.00000 0.00765 0.00714 = 0.01019 0.00186 0.00317 0.00049 O4 1 0.444340 0.500000 0.130275 10.50000 0.00647 0.00721 = 0.00538 0.00000 -0.00021 0.00000 O5 1 0.456707 0.000000 0.126489 10.50000 0.00796 0.00988 = 0.00796 0.00000 0.00149 0.00000 O6 1 0.045067 0.500000 0.370892 10.50000 0.00833 0.00738 = 0.00610 0.00000 -0.00019 0.00000 O7 1 0.034501 0.000000 0.373727 10.50000 0.01462 0.00900 = 0.00752 0.00000 0.00026 0.00000 O8 1 0.176856 0.000000 0.034904 10.50000 0.00457 0.01131 = 0.00944 0.00000 0.00265 0.00000 O9 1 0.176534 0.500000 0.475084 10.50000 0.00416 0.01393 = 0.00986 0.00000 0.00443 0.00000 O10 1 0.313266 0.000000 0.066473 10.50000 0.00691 0.01928 = 0.01126 0.00000 0.00289 0.00000 O11 1 0.184165 0.000000 0.497098 10.50000 0.00553 0.00956 = 0.00806 0.00000 0.00131 0.00000 MOLE 2 HKLF 5 REM saran-6133-full_hklf5 in C2/m REM wR2 = 0.1088, GooF = S = 1.076, Restrained GooF = 1.076 for all data REM R1 = 0.0469 for 2793 Fo > 4sig(Fo) and 0.0644 for all 3579 data REM 127 parameters refined using 2 restraints END WGHT 0.0641 2.0972 REM Highest difference peak 1.342, deepest hole -1.706, 1-sigma level 0.285 Q1 1 0.0967 0.5000 0.1014 10.50000 0.05 1.34 Q2 1 0.1333 0.0000 -0.0225 10.50000 0.05 1.30 Q3 1 0.0460 0.0000 0.4665 10.50000 0.05 1.26 Q4 1 0.3966 0.0000 0.2466 10.50000 0.05 1.25 Q5 1 0.1896 0.0000 0.1325 10.50000 0.05 1.20 Q6 1 0.2200 0.0000 0.0875 10.50000 0.05 1.20 Q7 1 -0.0102 0.0000 0.2782 10.50000 0.05 1.17 Q8 1 0.1602 0.0000 0.5574 10.50000 0.05 1.16 Q9 1 0.3436 0.0000 0.0019 10.50000 0.05 1.14 Q10 1 0.2320 0.0000 0.5430 10.50000 0.05 1.14 Q11 1 0.1935 0.0000 -0.0969 10.50000 0.05 1.13 Q12 1 0.0591 0.0000 0.4294 10.50000 0.05 1.12 Q13 1 0.1592 0.5000 0.3652 10.50000 0.05 1.07 Q14 1 0.3184 0.0000 0.2764 10.50000 0.05 1.04 Q15 1 0.4389 0.0000 0.0685 10.50000 0.05 1.04 Q16 1 0.2252 0.0000 0.4369 10.50000 0.05 1.04 Q17 1 0.4022 0.5000 0.3763 10.50000 0.05 1.03 Q18 1 0.2735 0.0000 0.3362 10.50000 0.05 0.99 Q19 1 0.1815 0.5000 0.5328 10.50000 0.05 0.99 Q20 1 0.3789 0.0000 0.4147 10.50000 0.05 0.99 ; _shelx_res_checksum 99028 _shelx_hkl_file ; 0 0 -2 47711.3 311.555 1 2 0 -3 90943.8 563.021 -2 0 0 -3 90943.8 563.021 1 0 0 4 89885.9 577.368 1 0 0 5 13781.9 223.358 1 4 0 -6 1764.85 196.117 -2 0 0 -6 1764.85 196.117 1 -4 0 7 8175.96 215.281 -2 0 0 7 8175.96 215.281 1 0 0 -8 90640.8 764.001 1 0 0 -9 55689.5 672.206 1 -6 0 10 45934.1 1311.47 -2 0 0 10 45934.1 1311.47 1 0 0 -11 1119.21 372.706 1 0 0 -12 6649.91 475.159 1 8 0 -13 6719.73 691.568 -2 0 0 -13 6719.73 691.568 1 0 -2 0 53205.9 394.739 -2 0 2 0 53205.9 394.739 1 0 -2 -1 37910.2 200.082 1 0 2 -2 89167.7 270.179 1 -2 -2 3 19783.8 141.965 -2 0 2 3 19783.8 141.965 1 0 -2 -4 28652.8 622.879 1 2 -2 -4 28639.8 219.316 -2 0 2 -4 28639.8 219.316 1 0 2 -5 20846.7 150.015 1 0 -2 -6 24843.0 639.001 1 -4 2 6 33731.8 322.940 -2 0 -2 6 33731.8 322.940 1 -4 2 7 3346.24 153.931 -2 0 -2 7 3346.24 153.931 1 0 2 -8 66329.9 409.936 1 0 2 -9 302.142 162.957 1 6 -2 -10 804.715 175.746 -2 0 2 -10 804.715 175.746 1 0 2 -11 503.005 196.390 1 0 -2 12 16221.5 377.721 1 8 2 -13 5368.78 475.261 -2 0 -2 -13 5368.78 475.261 1 0 -4 0 933532. 8959.51 -2 0 4 0 933532. 8959.51 1 0 -4 1 1264.26 61.0850 1 0 -4 2 14661.7 202.145 1 2 -4 -3 41736.9 452.372 -2 0 4 -3 41736.9 452.372 1 2 4 -4 61228.9 401.241 -2 0 -4 -4 61228.9 401.241 1 0 -4 -5 6153.26 153.691 1 0 -4 -6 1597.00 324.255 1 4 4 -6 1632.11 208.854 -2 0 -4 -6 1632.11 208.854 1 4 -4 -7 4361.16 247.661 -2 0 4 -7 4361.16 247.661 1 0 4 8 50575.3 574.394 1 0 4 -9 31353.1 452.763 1 6 -4 -10 28138.2 643.423 -2 0 4 -10 28138.2 643.423 1 0 -4 11 603.190 217.795 1 0 4 12 5805.13 301.355 1 0 6 0 17239.9 392.097 -2 0 -6 0 17239.9 392.097 1 0 -6 1 10885.3 221.163 1 0 6 -2 10395.3 200.190 1 2 6 -3 4524.33 166.807 -2 0 -6 -3 4524.33 166.807 1 -2 -6 4 13082.7 285.511 -2 0 6 4 13082.7 285.511 1 0 6 -5 7488.44 188.846 1 4 6 -6 12761.6 318.233 -2 0 -6 -6 12761.6 318.233 1 4 -6 -7 822.514 223.040 -2 0 6 -7 822.514 223.040 1 0 -6 8 24472.7 433.081 1 0 6 -9 316.987 198.428 1 6 -6 -10 1102.13 299.311 -2 0 6 -10 1102.13 299.311 1 0 -8 0 176159. 1347.69 -2 0 8 0 176159. 1347.69 1 0 -8 1 140.004 148.169 1 0 -8 -2 4584.97 218.221 1 2 8 -3 13797.0 492.635 -2 0 -8 -3 13797.0 492.635 1 2 -8 -4 23516.1 550.196 -2 0 8 -4 23516.1 550.196 1 0 -8 -5 1097.99 179.591 1 -4 8 6 1230.21 268.332 -2 0 -8 6 1230.21 268.332 1 4 -8 -7 1462.77 553.260 -2 0 8 -7 1462.77 553.260 1 -7 -1 14 1053.67 729.194 -2 -1 1 14 1053.67 729.194 1 7 1 -13 3961.43 446.016 -2 1 -1 -13 3961.43 446.016 1 1 -1 -12 450.682 248.289 1 -1 -1 11 7103.92 292.821 1 5 -1 -10 5731.17 320.340 -2 1 1 -10 5731.17 320.340 1 -1 -1 9 938.168 159.165 1 -1 -1 8 8299.46 176.020 1 3 1 -7 14496.2 264.469 -2 1 -1 -7 14496.2 264.469 1 1 -1 -6 4679.04 246.345 1 3 -1 -6 6821.36 176.603 -2 1 1 -6 6821.36 176.603 1 -1 1 5 612.617 55.6727 1 -1 1 4 24897.1 373.004 1 1 -1 -4 21327.2 258.930 -2 1 1 -4 21327.2 258.930 1 1 -1 -3 126000. 575.011 1 -1 1 3 138715. 468.192 -2 -1 -1 3 138715. 468.192 1 -1 -1 2 5245.90 58.7587 1 1 -1 -1 5982.18 53.0356 1 1 1 0 640.326 32.1622 -2 -1 -1 0 640.326 32.1622 1 1 -1 1 36083.3 136.147 1 1 -1 2 7772.24 76.3162 1 3 -1 -3 12675.0 121.540 -2 -1 1 -3 12675.0 121.540 1 1 -1 4 3341.06 81.1589 1 3 1 -4 4363.91 200.057 -2 -1 -1 -4 4363.91 200.057 1 -1 -1 -5 834.215 49.5389 1 -1 -1 -6 8501.63 352.709 1 5 1 -6 5772.22 131.846 -2 -1 -1 -6 5772.22 131.846 1 -5 1 7 9757.26 196.728 -2 1 -1 7 9757.26 196.728 1 -1 -1 -8 223.990 91.4891 1 -1 -1 -9 4752.05 214.171 1 7 -1 -10 1486.59 226.001 -2 -1 1 -10 1486.59 226.001 1 -1 1 -11 4634.46 264.340 1 1 1 12 4138.71 306.113 1 9 -1 -13 231.398 260.528 -2 -1 1 -13 231.398 260.528 1 -1 -3 12 667.734 199.832 1 -1 3 11 2680.64 249.254 1 -5 3 10 2936.09 317.063 -2 -1 -3 10 2936.09 317.063 1 1 -3 -9 3263.65 215.151 1 -1 3 8 7232.40 192.505 1 -3 -3 7 7233.03 269.251 -2 -1 3 7 7233.03 269.251 1 1 -3 -6 7254.48 443.735 1 3 3 -6 5905.99 205.397 -2 1 -3 -6 5905.99 205.397 1 -1 -3 5 208.489 58.9052 1 1 -3 -4 10609.3 490.231 1 -1 -3 4 11421.2 154.285 -2 -1 3 4 11421.2 154.285 1 1 3 -3 125916. 493.773 -2 1 -3 -3 125916. 493.773 1 -1 -3 2 1573.60 72.4293 1 1 -3 -1 5740.32 93.0943 1 1 3 0 190.768 57.0087 -2 -1 -3 0 190.768 57.0087 1 1 3 1 26793.1 167.280 1 -1 -3 -2 5803.34 114.302 1 3 3 -3 767.120 99.5917 -2 -1 -3 -3 767.120 99.5917 1 -1 -3 -4 463.282 79.6749 1 3 -3 -4 391.987 150.552 -2 -1 3 -4 391.987 150.552 1 1 3 5 280.706 86.7698 1 -5 3 6 7569.26 190.744 -2 1 -3 6 7569.26 190.744 1 -5 3 7 20613.3 354.087 -2 1 -3 7 20613.3 354.087 1 1 -3 8 345.067 152.717 1 -1 -3 -9 1811.35 168.708 1 7 3 -10 2673.94 316.052 -2 -1 -3 -10 2673.94 316.052 1 1 -3 11 1604.92 238.260 1 -1 -3 -12 4922.73 235.005 1 9 -3 -13 62.3910 517.793 -2 -1 3 -13 62.3910 517.793 1 1 5 -11 7605.05 360.958 1 5 -5 -10 3581.85 398.362 -2 1 5 -10 3581.85 398.362 1 -1 5 9-22.2746 270.510 1 1 5 -8 4286.30 284.488 1 -3 5 7 9386.48 463.946 -2 -1 -5 7 9386.48 463.946 1 -3 -5 6 3650.86 226.877 -2 -1 5 6 3650.86 226.877 1 -1 5 5 1414.72 130.648 1 1 5 -4 3831.68 167.988 -2 1 -5 -4 3831.68 167.988 1 -1 -5 3 29340.2 340.330 -2 -1 5 3 29340.2 340.330 1 -1 -5 2 787.319 83.7151 1 1 -5 -1 12239.0 163.800 1 1 5 0 598.083 85.6159 -2 -1 -5 0 598.083 85.6159 1 1 -5 1 9153.45 179.746 1 -1 5 -2 624.588 91.0290 1 3 -5 -3 5620.27 196.418 -2 -1 5 -3 5620.27 196.418 1 -3 -5 4 1247.03 149.373 -2 1 5 4 1247.03 149.373 1 1 5 5 566.625 103.080 1 5 -5 -6 1131.79 174.268 -2 -1 5 -6 1131.79 174.268 1 5 -5 -7 1184.77 203.624 -2 -1 5 -7 1184.77 203.624 1 -1 5 -8 625.399 187.843 1 -1 5 -9 3968.84 238.508 1 -7 -5 10 648.715 249.105 -2 1 5 10 648.715 249.105 1 1 5 11 4586.53 321.926 1 1 7 -9 2135.41 283.247 1 -1 7 8 2874.75 240.649 1 3 7 -7 2151.68 290.533 -2 1 -7 -7 2151.68 290.533 1 -3 -7 6 3356.46 262.583 -2 -1 7 6 3356.46 262.583 1 -1 7 5 135.095 144.985 1 -1 -7 4 2693.91 235.702 -2 -1 7 4 2693.91 235.702 1 1 -7 -3 38761.6 665.369 -2 1 7 -3 38761.6 665.369 1 -1 7 2 282.590 137.186 1 1 -7 -1 2048.92 138.605 1 1 -7 0 236.225 121.556 -2 -1 7 0 236.225 121.556 1 -1 7 -1 9636.10 207.172 1 1 -7 2 1546.21 172.850 1 -3 -7 3 348.228 176.913 -2 1 7 3 348.228 176.913 1 -3 -7 4 149.661 187.533 -2 1 7 4 149.661 187.533 1 -1 7 -5 330.622 139.219 1 -1 -7 -6 2729.41 567.119 1 -5 -7 6 3682.63 274.992 -2 1 7 6 3682.63 274.992 1 5 -7 -7 11259.4 408.942 -2 -1 7 -7 11259.4 408.942 1 1 7 8 619.569 210.566 1 -1 7 -9 221.217 358.550 1 -1 -9 4 1743.33 917.276 -2 -1 9 4 1743.33 917.276 1 -1 9 3 6088.42 420.899 -2 -1 -9 3 6088.42 420.899 1 -1 -9 2 365.146 217.346 1 1 9 -1 3702.09 272.102 1 -1 -9 0 598.649 270.810 -2 1 9 0 598.649 270.810 1 -1 9 -1 2503.81 263.585 1 -1 9 -2 459.456 226.840 1 -3 -9 3 1426.93 356.787 -2 1 9 3 1426.93 356.787 1 -3 -9 4 458.052 680.663 -2 1 9 4 458.052 680.663 1 -6 0 13 303.420 462.747 -2 -2 0 13 303.420 462.747 1 2 0 -12 4512.77 433.663 1 -2 0 11 4717.28 419.705 1 -4 0 10 18272.0 864.234 -2 -2 0 10 18272.0 864.234 1 2 0 -9 212.213 279.872 1 -2 0 8 54114.7 771.512 1 2 0 -7 54053.6 469.457 -2 2 0 -7 54053.6 469.457 1 2 0 -6 14829.1 246.575 1 2 0 -6 14712.2 477.234 -2 2 0 -6 14712.2 477.234 1 2 0 -5 435.102 54.5248 1 2 0 -4 69179.5 359.155 1 0 0 -4 64140.1 1056.99 -2 2 0 -4 64140.1 1056.99 1 2 0 -3 90952.9 897.496 1 0 0 -3 98601.5 786.554 -2 2 0 -3 98601.5 786.554 1 -2 0 2 2255.05 155.028 1 -2 0 1 3399.08 84.9948 1 2 0 1 10445.9 107.873 1 2 0 2 212029. 705.032 1 4 0 -3 20387.1 176.551 -2 -2 0 -3 20387.1 176.551 1 2 0 4 27173.3 236.285 1 4 0 -4 32228.5 461.163 -2 -2 0 -4 32228.5 461.163 1 -2 0 -5 21126.2 220.654 1 -6 0 6 124081. 675.777 -2 2 0 6 124081. 675.777 1 6 0 -7 5728.84 231.070 -2 -2 0 -7 5728.84 231.070 1 -2 0 -8 3037.34 154.605 1 -2 0 -9 36628.4 577.708 1 -8 0 10 27365.1 825.357 -2 2 0 10 27365.1 825.357 1 -2 0 -11 264.094 339.042 1 2 0 12 4907.32 318.683 1 10 0 -13 4623.58 475.429 -2 -2 0 -13 4623.58 475.429 1 -6 2 13 3100.56 421.825 -2 -2 -2 13 3100.56 421.825 1 2 -2 -12 7270.68 308.616 1 -2 -2 11 694.141 196.389 1 -4 -2 10 10562.4 385.026 -2 -2 2 10 10562.4 385.026 1 2 -2 -9 4374.41 191.997 1 -2 -2 8 122.528 92.6222 1 2 -2 -7 1248.83 124.187 -2 2 2 -7 1248.83 124.187 1 2 -2 -6 150961. 1071.97 1 -2 2 6 152825. 668.219 -2 -2 -2 6 152825. 668.219 1 2 -2 -5 30116.0 168.431 1 2 -2 -4 11106.1 234.536 1 0 2 4 13300.7 153.648 -2 -2 -2 4 13300.7 153.648 1 0 2 -3 12121.3 126.764 -2 2 -2 -3 12121.3 126.764 1 2 2 -2 47110.3 183.372 1 -2 2 1 25421.3 116.888 1 -2 2 0 49134.7 205.635 -2 2 -2 0 49134.7 205.635 1 -2 2 -1 31612.8 146.376 1 2 2 2 174690. 320.471 1 4 2 -3 1163.70 69.1377 -2 -2 -2 -3 1163.70 69.1377 1 -2 2 -4 24586.7 313.156 1 4 2 -4 33603.1 250.392 -2 -2 -2 -4 33603.1 250.392 1 2 -2 5 2526.51 68.1946 1 -2 2 -6 12987.4 281.382 1 -6 2 6 14429.8 196.370 -2 2 -2 6 14429.8 196.370 1 -6 -2 7 35313.2 382.645 -2 2 2 7 35313.2 382.645 1 -2 -2 -8 4427.06 134.770 1 -2 -2 -9 8486.56 228.055 1 -8 2 10 32889.4 735.050 -2 2 -2 10 32889.4 735.050 1 -2 2 -11 9198.48 320.487 1 -2 2 -12 28425.4 426.024 1 10 -2 -13 519.359 248.411 -2 -2 2 -13 519.359 248.411 1 2 4 -12 3135.63 311.759 1 2 -4 -11 3714.60 361.309 1 -4 4 10 11920.4 632.407 -2 -2 -4 10 11920.4 632.407 1 2 -4 -9 130.904 165.536 1 -2 -4 8 29305.3 336.429 1 2 -4 -7 29443.0 578.062 -2 2 4 -7 29443.0 578.062 1 -2 4 6 8316.41 221.535 -2 -2 -4 6 8316.41 221.535 1 -2 -4 5 817.195 99.7656 1 0 4 -4 8996.65 180.932 -2 2 -4 -4 8996.65 180.932 1 0 -4 3 45821.6 333.383 -2 -2 4 3 45821.6 333.383 1 2 4 -2 3005.90 73.8783 1 -2 4 1 1307.03 63.5033 1 2 -4 0 2258.35 103.611 -2 -2 4 0 2258.35 103.611 1 -2 -4 -1 2903.79 90.1077 1 -2 -4 -2 60961.8 311.476 1 4 -4 -3 9900.87 217.014 -2 -2 4 -3 9900.87 217.014 1 -4 4 4 6933.74 206.021 -2 2 -4 4 6933.74 206.021 1 2 4 5 10247.1 181.772 1 6 -4 -6 92203.3 614.503 -2 -2 4 -6 92203.3 614.503 1 6 4 -7 3149.77 238.301 -2 -2 -4 -7 3149.77 238.301 1 2 4 8 1764.86 166.486 1 2 4 9 23147.3 419.837 1 -8 4 10 18002.8 486.401 -2 2 -4 10 18002.8 486.401 1 2 -4 11 540.988 197.408 1 2 -4 12 3768.16 236.152 1 4 -6 -10 6205.16 425.408 -2 2 6 -10 6205.16 425.408 1 2 -6 -9 2994.05 325.470 1 2 6 -8 445.513 243.131 1 2 -6 -7 235.294 250.238 -2 2 6 -7 235.294 250.238 1 -2 -6 6 53829.3 617.256 -2 -2 6 6 53829.3 617.256 1 -2 6 5 9296.76 232.564 1 0 -6 -4 5771.82 220.753 -2 2 6 -4 5771.82 220.753 1 0 -6 -3 2006.85 155.370 -2 2 6 -3 2006.85 155.370 1 -2 6 2 50766.8 374.126 1 -2 6 1 5258.94 178.801 1 -2 6 0 11985.7 309.418 -2 2 -6 0 11985.7 309.418 1 2 -6 1 8650.24 198.323 1 -2 6 -2 36012.3 306.278 1 4 -6 -3 564.221 119.918 -2 -2 6 -3 564.221 119.918 1 -2 6 -4 10891.4 537.774 1 -4 -6 4 11719.7 272.927 -2 2 6 4 11719.7 272.927 1 -2 -6 -5 759.176 112.640 1 -6 -6 6 2479.91 214.221 -2 2 6 6 2479.91 214.221 1 6 -6 -7 16315.6 444.646 -2 -2 6 -7 16315.6 444.646 1 2 6 8 2073.90 204.344 1 2 -6 9 5080.96 260.800 1 -8 6 10 16729.1 588.693 -2 2 -6 10 16729.1 588.693 1 -2 -8 7 10092.0 647.115 -2 -2 8 7 10092.0 647.115 1 2 -8 -6 2600.34 594.328 1 2 -8 -6 2873.67 355.201 -2 2 8 -6 2873.67 355.201 1 -2 8 5 1183.00 186.718 1 0 8 -4 2195.33 283.905 -2 2 -8 -4 2195.33 283.905 1 0 -8 3 15225.1 491.131 -2 -2 8 3 15225.1 491.131 1 2 8 -2 1809.24 212.129 1 2 8 -1 606.487 172.473 1 -2 8 0 600.783 208.215 -2 2 -8 0 600.783 208.215 1 2 8 1 475.672 189.942 1 2 -8 2 13191.8 357.345 1 4 8 -3 3183.97 332.899 -2 -2 -8 -3 3183.97 332.899 1 4 -8 -4 1574.78 296.385 -2 -2 8 -4 1574.78 296.385 1 2 -8 5 2477.16 223.296 1 -2 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89.0389 1 3 -1 6 12134.3 229.887 1 7 1 -6 12940.5 244.983 -2 -3 -1 -6 12940.5 244.983 1 7 -1 -7 5686.76 186.281 -2 -3 1 -7 5686.76 186.281 1 -3 1 -8 3254.89 108.497 1 -3 -1 -9 2181.05 148.427 1 9 1 -10 3857.62 253.193 -2 -3 -1 -10 3857.62 253.193 1 3 -1 11 348.175 153.387 1 -3 -1 -12 183.852 138.465 1 11 -1 -13 3770.20 409.887 -2 -3 1 -13 3770.20 409.887 1 -3 3 12 4459.62 318.141 1 3 3 -11 8147.57 323.178 1 -3 3 10 2971.72 317.408 -2 -3 -3 10 2971.72 317.408 1 3 3 -9 587.622 169.453 1 -3 -3 8 27780.2 308.549 1 1 -3 -7 740.256 138.461 -2 3 3 -7 740.256 138.461 1 3 3 -6 1718.28 212.680 1 -1 -3 6 2658.10 148.248 -2 -3 3 6 2658.10 148.248 1 -3 3 5 66059.4 277.531 1 1 -3 4 243.081 82.6007 -2 -3 3 4 243.081 82.6007 1 1 -3 3 4405.17 119.658 -2 -3 3 3 4405.17 119.658 1 3 3 -2 3546.71 62.2836 1 3 -3 -1 10848.8 86.8617 1 3 3 0 330.632 49.1555 -2 -3 -3 0 330.632 49.1555 1 -3 3 -1 6635.07 75.4744 1 3 -3 2 7110.31 92.4368 1 -5 3 3 19407.6 198.024 -2 3 -3 3 19407.6 198.024 1 -3 3 -4 16957.1 590.291 1 -5 3 4 19044.9 191.596 -2 3 -3 4 19044.9 191.596 1 3 -3 5 23086.8 186.693 1 -7 -3 6 8889.62 157.126 -2 3 3 6 8889.62 157.126 1 -7 -3 7 3986.93 251.098 -2 3 3 7 3986.93 251.098 1 3 3 8 2776.90 168.209 1 3 -3 9 460.392 148.950 1 -9 -3 10 3865.59 240.116 -2 3 3 10 3865.59 240.116 1 -3 3 -11 314.027 181.256 1 -3 3 -12 257.694 162.030 1 -3 5 11 5050.35 416.333 1 3 5 -10 4831.34 512.107 -2 3 -5 -10 4831.34 512.107 1 3 -5 -9 3794.99 320.996 1 -3 -5 8 26474.2 405.670 1 -1 5 7 936.233 197.443 -2 -3 -5 7 936.233 197.443 1 3 -5 -6 5626.02 597.024 1 -1 -5 6 6836.54 250.053 -2 -3 5 6 6836.54 250.053 1 -3 -5 5 9514.40 195.865 1 -1 -5 -4 1814.64 151.656 -2 3 5 -4 1814.64 151.656 1 1 -5 3 1655.30 116.955 -2 -3 5 3 1655.30 116.955 1 -3 5 2 402.251 79.2570 1 -3 5 1 662.172 72.0416 1 -3 5 0 161.321 70.4507 -2 3 -5 0 161.321 70.4507 1 -3 5 -1 623.377 94.3675 1 -3 5 -2 4834.66 126.580 1 -5 5 3 35012.1 390.872 -2 3 -5 3 35012.1 390.872 1 -3 5 -4 15806.1 621.981 1 -5 5 4 14259.9 271.949 -2 3 -5 4 14259.9 271.949 1 -3 5 -5 604.091 101.444 1 7 -5 -6 5909.33 207.332 -2 -3 5 -6 5909.33 207.332 1 7 -5 -7 2805.81 214.903 -2 -3 5 -7 2805.81 214.903 1 3 5 8 1651.28 167.127 1 3 5 9 2606.28 219.963 1 9 -5 -10 2426.40 261.297 -2 -3 5 -10 2426.40 261.297 1 3 5 11-37.3899 253.333 1 -3 7 9 363.688 311.863 1 3 -7 -8 9408.80 383.623 1 1 -7 -7 437.801 269.641 -2 3 7 -7 437.801 269.641 1 1 -7 -6 1262.44 238.853 -2 3 7 -6 1262.44 238.853 1 -3 -7 5 28791.0 398.020 1 -1 7 -4 678.030 208.617 -2 3 -7 -4 678.030 208.617 1 1 7 3 2023.31 249.382 -2 -3 -7 3 2023.31 249.382 1 -3 7 2 1630.58 156.552 1 -3 -7 1 2668.32 157.732 1 -3 -7 0 372.243 135.969 -2 3 7 0 372.243 135.969 1 -3 7 -1 2248.13 147.367 1 -3 7 -2 1247.40 148.841 1 5 7 -3 4809.83 238.693 -2 -3 -7 -3 4809.83 238.693 1 -5 -7 4 5751.55 270.972 -2 3 7 4 5751.55 270.972 1 3 7 5 9778.72 242.306 1 7 -7 -6 3883.96 272.267 -2 -3 7 -6 3883.96 272.267 1 -7 -7 7 1556.74 258.136 -2 3 7 7 1556.74 258.136 1 3 7 8 1517.93 217.482 1 -3 7 -9 161.528 456.871 1 1 -9 4 1461.05 644.346 -2 -3 9 4 1461.05 644.346 1 1 9 3 1051.06 302.304 -2 -3 -9 3 1051.06 302.304 1 3 -9 -2 122.053 243.032 1 -3 9 1 283.847 243.590 1 3 9 0 343.870 254.345 -2 -3 -9 0 343.870 254.345 1 -3 -9 -1 165.853 217.807 1 3 -9 2 1501.03 211.018 1 -5 -9 3 11664.8 855.464 -2 3 9 3 11664.8 855.464 1 -5 -9 4 3303.98 985.475 -2 3 9 4 3303.98 985.475 1 -4 0 13 6205.29 673.755 -2 -4 0 13 6205.29 673.755 1 4 0 -12 17553.9 628.664 1 4 0 -11 8680.89 487.817 1 2 0 -10 2106.24 439.024 -2 4 0 -10 2106.24 439.024 1 4 0 -9 12075.1 485.383 1 4 0 -8 96308.8 1007.87 1 0 0 -7 2997.99 405.638 -2 4 0 -7 2997.99 405.638 1 0 0 -6 1114.52 282.934 -2 4 0 -6 1114.52 282.934 1 4 0 -5 7705.28 266.619 1 -2 0 -4 135201. 963.939 -2 4 0 -4 135201. 963.939 1 2 0 3 5132.77 246.439 -2 -4 0 3 5132.77 246.439 1 -4 0 2 63874.5 310.799 1 4 0 -1 15909.9 135.557 1 -4 0 0 79689.9 372.167 -2 4 0 0 79689.9 372.167 1 4 0 1 9282.76 163.901 1 4 0 2 96624.9 350.232 1 6 0 -3 2241.98 118.529 -2 -4 0 -3 2241.98 118.529 1 -4 0 -4 3646.94 168.835 1 -6 0 4 10450.6 327.690 -2 4 0 4 10450.6 327.690 1 -4 0 -5 34593.2 236.939 1 4 0 6 18865.8 267.111 1 8 0 -6 17786.8 295.876 -2 -4 0 -6 17786.8 295.876 1 8 0 -7 24631.0 467.322 -2 -4 0 -7 24631.0 467.322 1 -4 0 -8 28459.7 410.970 1 -4 0 -9 10773.0 360.916 1 10 0 -10 5239.64 355.983 -2 -4 0 -10 5239.64 355.983 1 -4 0 -11 7522.03 307.341 1 -4 0 -12 40070.5 708.763 1 12 0 -13 739.089 358.656 -2 -4 0 -13 739.089 358.656 1 4 2 -13 10198.3 518.650 -2 4 -2 -13 10198.3 518.650 1 -4 -2 12 10218.4 345.775 1 -4 -2 11 10525.6 360.715 1 2 2 -10 2301.58 385.500 -2 4 -2 -10 2301.58 385.500 1 -4 2 9 10236.2 209.577 1 4 2 -8 20586.9 238.205 1 0 2 7 5741.59 217.701 -2 -4 -2 7 5741.59 217.701 1 4 -2 -6 140913. 981.416 1 0 -2 6 150826. 618.170 -2 -4 2 6 150826. 618.170 1 -4 2 5 72315.5 257.105 1 4 -2 -4 139503. 792.977 1 2 2 4 141664. 499.344 -2 -4 -2 4 141664. 499.344 1 -2 -2 -3 691.710 75.8305 -2 4 2 -3 691.710 75.8305 1 -4 -2 2 10382.0 95.4591 1 4 -2 -1 22699.7 117.885 1 -4 2 0 249739. 588.761 -2 4 -2 0 249739. 588.761 1 -4 2 -1 5150.97 55.1842 1 4 2 2 167180. 302.481 1 6 2 -3 27986.9 196.225 -2 -4 -2 -3 27986.9 196.225 1 -4 2 -4 500487. 3051.40 1 6 -2 -4 504273. 924.218 -2 -4 2 -4 504273. 924.218 1 4 -2 5 1117.73 60.6381 1 8 2 -6 1544.88 100.927 -2 -4 -2 -6 1544.88 100.927 1 -8 2 7 40488.9 425.424 -2 4 -2 7 40488.9 425.424 1 4 -2 8 25394.4 243.204 1 -4 -2 -9 2794.38 139.101 1 10 -2 -10 17727.0 422.578 -2 -4 2 -10 17727.0 422.578 1 -4 -2 -11 7500.25 277.373 1 -4 2 -12 13742.5 327.521 1 -12 2 13 10342.1 625.677 -2 4 -2 13 10342.1 625.677 1 4 4 -12 13793.1 441.507 1 4 4 -11 5908.85 386.403 1 2 4 -10 2020.81 411.817 -2 4 -4 -10 2020.81 411.817 1 -4 4 9 6212.69 321.904 1 4 4 -8 62579.4 542.411 1 0 -4 -7 1945.86 169.027 -2 4 4 -7 1945.86 169.027 1 0 4 -6 488.650 151.778 -2 4 -4 -6 488.650 151.778 1 -4 -4 5 2720.22 108.883 1 2 -4 4 56350.9 369.593 -2 -4 4 4 56350.9 369.593 1 2 -4 3 2979.81 119.366 -2 -4 4 3 2979.81 119.366 1 4 -4 -2 27823.1 142.768 1 -4 -4 1 6799.36 105.789 1 4 -4 0 26489.5 199.308 -2 -4 4 0 26489.5 199.308 1 4 4 1 3756.76 69.8301 1 4 -4 2 23011.5 160.283 1 -6 4 3 1869.56 101.394 -2 4 -4 3 1869.56 101.394 1 4 4 4 295.315 163.454 1 6 4 -4 2761.38 122.967 -2 -4 -4 -4 2761.38 122.967 1 -4 4 -5 16770.0 181.540 1 4 4 6 10117.5 625.893 1 8 -4 -6 10183.3 234.532 -2 -4 4 -6 10183.3 234.532 1 8 -4 -7 13551.0 375.805 -2 -4 4 -7 13551.0 375.805 1 -4 4 -8 19598.1 292.070 1 4 -4 9 7105.39 254.986 1 10 4 -10 3515.71 277.793 -2 -4 -4 -10 3515.71 277.793 1 -4 4 -11 4815.60 258.929 1 -4 4 -12 25923.5 612.855 1 -2 -6 10 2264.90 475.116 -2 -4 6 10 2264.90 475.116 1 -4 6 9 6434.67 369.605 1 -4 6 8 8786.47 346.570 1 0 6 -7 1592.95 278.448 -2 4 -6 -7 1592.95 278.448 1 0 6 -6 40114.0 536.867 -2 4 -6 -6 40114.0 536.867 1 -4 6 5 19657.8 320.183 1 2 6 4 37590.2 491.735 -2 -4 -6 4 37590.2 491.735 1 2 -6 3 388.510 143.793 -2 -4 6 3 388.510 143.793 1 4 6 -2 124.071 111.543 1 -4 6 1 7608.72 178.696 1 4 6 0 74425.9 726.315 -2 -4 -6 0 74425.9 726.315 1 -4 -6 -1 2209.71 125.574 1 4 -6 2 19610.3 231.018 1 6 -6 -3 6919.15 219.320 -2 -4 6 -3 6919.15 219.320 1 -4 6 -4 158032. 2111.71 1 6 -6 -4 144650. 822.495 -2 -4 6 -4 144650. 822.495 1 4 -6 5 238.066 110.706 1 8 6 -6 1265.09 198.599 -2 -4 -6 -6 1265.09 198.599 1 8 -6 -7 19434.9 473.542 -2 -4 6 -7 19434.9 473.542 1 4 6 8 15074.5 359.140 1 4 6 9 1109.72 218.255 1 -10 6 10 8903.59 539.823 -2 4 -6 10 8903.59 539.823 1 0 -8 -7 1642.57 486.419 -2 4 8 -7 1642.57 486.419 1 0 8 -6 580.873 273.569 -2 4 -8 -6 580.873 273.569 1 -4 -8 5 501.898 187.091 1 -2 -8 -4 16414.5 459.972 -2 4 8 -4 16414.5 459.972 1 2 -8 3 890.431 263.987 -2 -4 8 3 890.431 263.987 1 4 8 -2 9700.58 317.015 1 4 8 -1 2038.76 195.201 1 4 8 0 7253.52 334.922 -2 -4 -8 0 7253.52 334.922 1 4 -8 1 746.594 194.719 1 4 8 2 2458.49 255.488 1 -6 -8 3 700.131 299.000 -2 4 8 3 700.131 299.000 1 -6 -8 4 700.996 266.705 -2 4 8 4 700.996 266.705 1 4 8 5 4866.83 256.642 1 -8 -8 6 4528.38 358.971 -2 4 8 6 4528.38 358.971 1 -8 -8 7 5323.24 1041.17 -2 4 8 7 5323.24 1041.17 1 -3 -1 14 1500.67 738.817 -2 -5 1 14 1500.67 738.817 1 -3 1 13 8348.73 541.340 -2 -5 -1 13 8348.73 541.340 1 5 1 -12 1365.95 264.294 1 5 -1 -11 326.503 215.082 1 -1 1 10 5074.70 354.197 -2 -5 -1 10 5074.70 354.197 1 5 -1 -9 5870.96 211.670 1 5 -1 -8 13350.1 243.401 1 1 1 7 4111.76 255.374 -2 -5 -1 7 4111.76 255.374 1 1 -1 6 2996.93 223.798 -2 -5 1 6 2996.93 223.798 1 -5 1 5 261.391 106.414 1 -3 -1 -4 10145.0 200.589 -2 5 1 -4 10145.0 200.589 1 3 1 3 36903.9 231.811 -2 -5 -1 3 36903.9 231.811 1 -5 1 2 14689.2 91.8765 1 5 -1 -1 10888.4 79.6458 1 -5 1 0 851.458 45.1176 -2 5 -1 0 851.458 45.1176 1 5 -1 1 249501. 636.967 1 -5 1 -2 13807.4 106.161 1 -7 1 3 10589.8 152.705 -2 5 -1 3 10589.8 152.705 1 5 1 4 51695.5 806.843 1 -7 1 4 53406.2 306.046 -2 5 -1 4 53406.2 306.046 1 5 -1 5 390.632 58.8413 1 5 1 6 666.056 231.135 1 -9 1 6 872.053 105.335 -2 5 -1 6 872.053 105.335 1 -9 -1 7 1081.54 115.496 -2 5 1 7 1081.54 115.496 1 5 1 8 1895.25 90.8020 1 5 1 9 465.843 100.213 1 -11 1 10 6020.22 239.833 -2 5 -1 10 6020.22 239.833 1 -5 -1 -11 8772.88 266.442 1 -5 1 -12 182.064 167.820 1 -13 -1 13 1557.37 304.394 -2 5 1 13 1557.37 304.394 1 5 -3 -12 1471.75 280.848 1 5 3 -11 428.293 286.421 1 1 -3 -10 3172.81 325.862 -2 5 3 -10 3172.81 325.862 1 5 3 -9 994.481 145.915 1 -5 -3 8 7762.20 195.303 1 -1 -3 -7 11857.7 283.953 -2 5 3 -7 11857.7 283.953 1 5 -3 -6 2434.45 225.932 1 1 -3 6 3809.99 141.980 -2 -5 3 6 3809.99 141.980 1 5 -3 -5 577.306 58.6198 1 5 3 -4 3122.19 178.900 1 3 3 4 5040.92 137.351 -2 -5 -3 4 5040.92 137.351 1 3 3 3 38713.2 312.260 -2 -5 -3 3 38713.2 312.260 1 -5 3 2 7725.04 87.8880 1 5 -3 -1 2526.56 61.9220 1 5 3 0 727.562 47.9166 -2 -5 -3 0 727.562 47.9166 1 -5 -3 -1 73171.3 213.331 1 -5 -3 -2 11583.7 112.445 1 7 -3 -3 461.441 62.4560 -2 -5 3 -3 461.441 62.4560 1 5 3 4 41377.5 357.481 1 -7 3 4 43982.0 271.249 -2 5 -3 4 43982.0 271.249 1 -5 -3 -5 2008.02 74.9955 1 5 3 6 305.955 281.397 1 9 -3 -6 545.479 96.5800 -2 -5 3 -6 545.479 96.5800 1 -9 -3 7 733.967 137.732 -2 5 3 7 733.967 137.732 1 5 -3 8 2354.31 134.968 1 5 -3 9 2119.95 186.530 1 11 -3 -10 2593.30 267.482 -2 -5 3 -10 2593.30 267.482 1 -5 3 -11 3743.29 236.115 1 -5 3 -12 19.2728 170.314 1 -5 5 11 451.879 328.326 1 -1 -5 10 2336.78 341.763 -2 -5 5 10 2336.78 341.763 1 -5 -5 9 4745.58 328.470 1 5 5 -8 8328.39 271.327 1 -1 -5 -7 341.803 174.114 -2 5 5 -7 341.803 174.114 1 1 5 6 1341.88 188.096 -2 -5 -5 6 1341.88 188.096 1 -5 -5 5 262.005 90.3572 1 -3 -5 -4 5056.55 159.734 -2 5 5 -4 5056.55 159.734 1 3 -5 3 10865.3 238.910 -2 -5 5 3 10865.3 238.910 1 -5 5 2 8203.23 145.403 1 5 -5 -1 4571.43 117.120 1 -5 5 0 240.832 75.2497 -2 5 -5 0 240.832 75.2497 1 -5 -5 -1 123269. 411.169 1 5 -5 2 5046.19 122.684 1 7 -5 -3 4713.58 162.758 -2 -5 5 -3 4713.58 162.758 1 -5 5 -4 15668.3 666.796 1 -7 -5 4 15415.5 251.180 -2 5 5 4 15415.5 251.180 1 -5 5 -5 227.104 102.514 1 9 5 -6 742.449 169.421 -2 -5 -5 -6 742.449 169.421 1 9 -5 -7 993.708 207.916 -2 -5 5 -7 993.708 207.916 1 5 5 8 80.3409 155.106 1 -5 -5 -9 45.3960 196.003 1 -11 -5 10 5016.92 324.548 -2 5 5 10 5016.92 324.548 1 5 -5 11 7286.78 422.425 1 5 7 -9 339.273 471.245 1 5 -7 -8 2465.94 248.388 1 1 -7 7 7702.34 432.663 -2 -5 7 7 7702.34 432.663 1 -1 7 -6 1456.40 270.599 -2 5 -7 -6 1456.40 270.599 1 -5 7 5 252.043 150.104 1 3 -7 4 1413.43 246.837 -2 -5 7 4 1413.43 246.837 1 -3 -7 -3 11636.5 418.736 -2 5 7 -3 11636.5 418.736 1 5 -7 -2 2156.85 171.254 1 -5 7 1 416.178 166.615 1 5 7 0 702.938 147.748 -2 -5 -7 0 702.938 147.748 1 -5 -7 -1 15591.3 311.663 1 5 -7 2 4497.45 221.190 1 7 7 -3 559.129 203.776 -2 -5 -7 -3 559.129 203.776 1 -5 7 -4 15391.8 751.302 1 7 -7 -4 15697.5 439.346 -2 -5 7 -4 15697.5 439.346 1 -5 -7 -5 1350.75 187.753 1 -9 -7 6 979.591 228.924 -2 5 7 6 979.591 228.924 1 9 -7 -7 557.450 249.977 -2 -5 7 -7 557.450 249.977 1 5 -7 8 1564.67 227.183 1 -3 -9 -4 2465.48 711.840 -2 5 9 -4 2465.48 711.840 1 -3 -9 -3 3648.03 475.926 -2 5 9 -3 3648.03 475.926 1 5 -9 -2 3387.78 266.391 1 -5 -9 1 2639.16 270.528 1 5 -9 0 369.618 267.860 -2 -5 9 0 369.618 267.860 1 -5 9 -1 38693.8 555.811 1 5 9 2 1343.77 224.163 1 -2 0 13 1002.93 487.863 -2 -6 0 13 1002.93 487.863 1 6 0 -12 14903.9 611.115 1 -6 0 11 8641.88 498.876 1 0 0 -10 13360.6 784.517 -2 6 0 -10 13360.6 784.517 1 -6 0 9 14629.5 531.291 1 6 0 -8 1513.91 278.032 1 -2 0 -7 883.402 341.418 -2 6 0 -7 883.402 341.418 1 2 0 6 91318.2 1033.97 -2 -6 0 6 91318.2 1033.97 1 -6 0 5 9811.61 296.978 1 4 0 4 98437.9 843.948 -2 -6 0 4 98437.9 843.948 1 4 0 3 15377.0 354.897 -2 -6 0 3 15377.0 354.897 1 6 0 -2 337820. 1049.55 1 6 0 -1 4695.81 102.489 1 6 0 0 351.871 90.1043 -2 -6 0 0 351.871 90.1043 1 6 0 1 9730.59 144.718 1 6 0 2 17144.2 135.767 1 8 0 -3 2525.71 146.967 -2 -6 0 -3 2525.71 146.967 1 -6 0 -4 112468. 1342.21 1 8 0 -4 112995. 717.738 -2 -6 0 -4 112995. 717.738 1 -6 0 -5 13632.4 213.172 1 6 0 6 77259.1 789.472 1 10 0 -6 69631.9 576.561 -2 -6 0 -6 69631.9 576.561 1 -10 0 7 925.046 154.730 -2 6 0 7 925.046 154.730 1 6 0 8 10374.5 265.037 1 -6 0 -9 167.071 142.323 1 -12 0 10 911.292 217.569 -2 6 0 10 911.292 217.569 1 6 0 11 1166.26 214.960 1 6 0 12 14532.6 403.760 1 14 0 -13 1954.79 466.052 -2 -6 0 -13 1954.79 466.052 1 2 2 -13 1342.73 352.537 -2 6 -2 -13 1342.73 352.537 1 -6 -2 12 204.384 223.995 1 -6 -2 11 1107.13 257.303 1 0 2 10 9464.79 541.787 -2 -6 -2 10 9464.79 541.787 1 -6 2 9 1322.83 150.314 1 6 2 -8 1200.91 129.383 1 2 2 7 23747.3 436.824 -2 -6 -2 7 23747.3 436.824 1 2 2 6 33035.9 349.694 -2 -6 -2 6 33035.9 349.694 1 -6 -2 5 1712.01 73.1216 1 -6 2 4 1203.49 268.957 1 4 -2 4 43020.7 314.987 -2 -6 2 4 43020.7 314.987 1 4 -2 3 21232.0 184.724 -2 -6 2 3 21232.0 184.724 1 6 2 -2 15507.8 117.976 1 -6 2 1 22336.2 136.775 1 -6 -2 0 49980.2 204.554 -2 6 2 0 49980.2 204.554 1 -6 -2 -1 15624.1 98.6240 1 6 2 2 104472. 265.700 1 -8 -2 3 1850.84 78.0791 -2 6 2 3 1850.84 78.0791 1 -8 2 4 25150.5 196.139 -2 6 -2 4 25150.5 196.139 1 -6 2 -5 10741.8 124.783 1 -10 2 6 18305.4 204.964 -2 6 -2 6 18305.4 204.964 1 -10 2 7 10769.1 207.922 -2 6 -2 7 10769.1 207.922 1 6 2 8 10043.3 165.033 1 6 2 9 8849.64 184.457 1 -12 -2 10 36464.1 689.181 -2 6 2 10 36464.1 689.181 1 -6 2 -11 810.941 186.479 1 -6 -2 -12 281.187 169.445 1 -6 4 12 9224.07 397.243 1 6 4 -11 6745.49 408.155 1 0 4 10 10768.5 526.631 -2 -6 -4 10 10768.5 526.631 1 6 4 -9 8831.52 293.794 1 -6 -4 8 2522.22 186.784 1 -2 4 -7 903.053 187.838 -2 6 -4 -7 903.053 187.838 1 2 4 6 58301.3 484.763 -2 -6 -4 6 58301.3 484.763 1 -6 4 5 6298.27 130.909 1 4 -4 4 32061.9 278.549 -2 -6 4 4 32061.9 278.549 1 4 4 3 10291.1 163.980 -2 -6 -4 3 10291.1 163.980 1 -6 4 2 177624. 411.854 1 -6 -4 1 964.521 62.3589 1 -6 -4 0 1436.31 69.3988 -2 6 4 0 1436.31 69.3988 1 6 4 1 6192.40 84.2150 1 6 -4 2 29065.1 185.040 1 8 -4 -3 1982.20 106.195 -2 -6 4 -3 1982.20 106.195 1 8 4 -4 43440.1 310.295 -2 -6 -4 -4 43440.1 310.295 1 6 -4 5 7002.86 130.290 1 -10 4 6 40641.6 350.735 -2 6 -4 6 40641.6 350.735 1 -10 -4 7 623.415 145.801 -2 6 4 7 623.415 145.801 1 6 -4 8 8284.15 229.123 1 -6 4 -9 125.205 158.709 1 -12 4 10 995.047 245.063 -2 6 -4 10 995.047 245.063 1 -6 4 -11 1204.13 207.750 1 -6 4 -12 7965.08 799.771 1 0 6 -10 8111.06 627.406 -2 6 -6 -10 8111.06 627.406 1 -6 6 9 1587.85 300.807 1 6 -6 -8 144.947 173.373 1 -2 6 -7 10446.4 402.665 -2 6 -6 -7 10446.4 402.665 1 6 -6 -6 10005.4 759.347 1 2 -6 6 9898.82 389.674 -2 -6 6 6 9898.82 389.674 1 6 -6 -5 1461.25 144.410 1 -4 6 -4 11313.4 286.368 -2 6 -6 -4 11313.4 286.368 1 4 -6 3 6270.17 231.084 -2 -6 6 3 6270.17 231.084 1 -6 6 2 1055.68 123.384 1 6 -6 -1 3993.35 142.810 1 -6 -6 0-21.5929 117.427 -2 6 6 0-21.5929 117.427 1 -6 6 -1 5777.24 139.004 1 -6 6 -2 22876.6 253.005 1 -8 -6 3 1086.45 136.437 -2 6 6 3 1086.45 136.437 1 -6 6 -4 7.18349 226.174 1 8 -6 -4 7944.83 245.460 -2 -6 6 -4 7944.83 245.460 1 -6 -6 -5 3158.91 165.190 1 -10 6 6 8719.68 315.358 -2 6 -6 6 8719.68 315.358 1 -10 6 7 4432.47 307.367 -2 6 -6 7 4432.47 307.367 1 6 -6 8 2167.73 201.956 1 -6 -6 -9 4737.25 283.951 1 -2 -8 -7 927.443 795.419 -2 6 8 -7 927.443 795.419 1 6 -8 -6 18018.0 1105.02 1 2 -8 6 20366.8 658.029 -2 -6 8 6 20366.8 658.029 1 -6 8 5 2805.55 240.035 1 4 8 4 7468.74 365.505 -2 -6 -8 4 7468.74 365.505 1 -4 8 -3 3470.25 327.522 -2 6 -8 -3 3470.25 327.522 1 6 -8 -2 58815.2 650.745 1 6 8 -1 200.129 195.926 1 6 -8 0 3028.10 224.250 -2 -6 8 0 3028.10 224.250 1 -6 8 -1 1979.01 202.705 1 6 8 2 13087.3 389.668 1 8 -8 -3 915.287 300.741 -2 -6 8 -3 915.287 300.741 1 8 8 -4 9521.49 457.653 -2 -6 -8 -4 9521.49 457.653 1 6 8 5 1540.62 211.546 1 -10 8 6 15381.4 564.671 -2 6 -8 6 15381.4 564.671 1 -1 1 13 792.870 327.559 -2 -7 -1 13 792.870 327.559 1 -7 -1 12 1911.59 236.463 1 -7 -1 11 4408.28 270.142 1 1 1 10 3889.84 241.316 -2 -7 -1 10 3889.84 241.316 1 -7 -1 9 1948.40 172.763 1 -7 -1 8 11571.6 238.089 1 3 1 7 6300.39 343.234 -2 -7 -1 7 6300.39 343.234 1 3 1 6 4087.98 244.514 -2 -7 -1 6 4087.98 244.514 1 -7 1 5 13085.5 223.976 1 -7 -1 4 43011.1 468.894 1 -5 1 -4 46940.5 347.869 -2 7 -1 -4 46940.5 347.869 1 -5 -1 -3 28371.5 244.101 -2 7 1 -3 28371.5 244.101 1 -7 -1 2 1688.63 49.2156 1 7 -1 -1 127083. 239.117 1 7 -1 0 2100.87 56.6763 -2 -7 1 0 2100.87 56.6763 1 7 -1 1 7414.48 82.5480 1 7 -1 2 457.065 45.5932 1 -9 1 3 2059.51 94.9807 -2 7 -1 3 2059.51 94.9807 1 -7 1 -4 9429.52 451.822 1 9 -1 -4 9767.98 167.233 -2 -7 1 -4 9767.98 167.233 1 -7 1 -5 363.826 63.1143 1 -11 1 6 11610.6 185.588 -2 7 -1 6 11610.6 185.588 1 11 1 -7 10059.9 256.028 -2 -7 -1 -7 10059.9 256.028 1 -7 1 -8 8065.50 155.420 1 -7 1 -9 10149.6 184.873 1 -13 1 10 15685.3 382.025 -2 7 -1 10 15685.3 382.025 1 -7 1 -11 368.627 152.281 1 7 -1 12 82.4095 165.830 1 -15 1 13 7229.72 981.601 -2 7 -1 13 7229.72 981.601 1 -7 -3 12 3540.52 311.719 1 -7 3 11 1001.89 288.378 1 -1 3 -10 896.860 345.836 -2 7 -3 -10 896.860 345.836 1 -7 -3 9 386.101 153.104 1 7 3 -8 10988.4 234.231 1 3 3 7 2397.10 182.607 -2 -7 -3 7 2397.10 182.607 1 3 -3 6 3736.67 148.459 -2 -7 3 6 3736.67 148.459 1 -7 -3 5 14320.2 192.557 1 -5 3 -4 38711.8 308.103 -2 7 -3 -4 38711.8 308.103 1 5 -3 3 2765.36 103.210 -2 -7 3 3 2765.36 103.210 1 -7 3 2 7720.41 99.2907 1 -7 -3 1 31178.8 151.986 1 -7 -3 0 734.635 50.1520 -2 7 3 0 734.635 50.1520 1 7 3 1 4612.25 71.5030 1 7 3 2 1039.85 59.0945 1 9 -3 -3 290.534 70.5664 -2 -7 3 -3 290.534 70.5664 1 -9 -3 4 7100.22 142.372 -2 7 3 4 7100.22 142.372 1 7 3 5 321.031 64.0313 1 -11 -3 6 9221.73 193.600 -2 7 3 6 9221.73 193.600 1 -11 -3 7 19071.4 335.041 -2 7 3 7 19071.4 335.041 1 7 -3 8 6769.45 176.520 1 7 3 9 5472.35 190.762 1 13 3 -10 11453.7 432.504 -2 -7 -3 -10 11453.7 432.504 1 7 -3 11 981.068 198.051 1 7 -3 12 48.2235 208.136 1 7 -5 -11 4589.58 402.905 1 1 5 10 3530.30 401.590 -2 -7 -5 10 3530.30 401.590 1 -7 5 9 1702.53 229.536 1 -7 5 8 3704.76 205.209 1 3 -5 7 5351.88 300.372 -2 -7 5 7 5351.88 300.372 1 3 5 6 1669.84 195.462 -2 -7 -5 6 1669.84 195.462 1 -7 -5 5 4099.13 143.637 1 5 -5 4 12449.6 216.755 -2 -7 5 4 12449.6 216.755 1 5 5 3 9936.15 235.918 -2 -7 -5 3 9936.15 235.918 1 -7 5 2 352.610 82.9911 1 7 5 -1 66727.2 309.564 1 7 -5 0 2283.50 122.545 -2 -7 5 0 2283.50 122.545 1 7 5 1 2999.63 102.688 1 7 -5 2 702.991 83.8711 1 -9 5 3 3287.68 146.805 -2 7 -5 3 3287.68 146.805 1 -7 5 -4 3320.09 370.666 1 -9 5 4 3779.89 177.872 -2 7 -5 4 3779.89 177.872 1 7 -5 5 563.421 92.4760 1 -11 -5 6 4301.46 205.187 -2 7 5 6 4301.46 205.187 1 -11 -5 7 1931.49 254.468 -2 7 5 7 1931.49 254.468 1 -7 5 -8 4029.54 226.412 1 -7 5 -9 6923.56 266.557 1 13 5 -10 10706.9 511.072 -2 -7 -5 -10 10706.9 511.072 1 -7 5 -11 401.863 396.179 1 -7 7 9 418.386 572.185 1 -7 7 8 7564.80 316.690 1 -3 7 -7 843.232 277.073 -2 7 -7 -7 843.232 277.073 1 7 -7 -6 1601.24 518.101 1 3 -7 6 1918.74 310.530 -2 -7 7 6 1918.74 310.530 1 -7 7 5 8533.66 260.898 1 -5 7 -4 13855.5 407.214 -2 7 -7 -4 13855.5 407.214 1 5 -7 3 287.573 229.929 -2 -7 7 3 287.573 229.929 1 -7 7 2 4446.20 191.922 1 7 -7 -1 7696.30 229.741 1 -7 -7 0 426.240 172.059 -2 7 7 0 426.240 172.059 1 -7 7 -1 1170.77 157.928 1 -7 7 -2 785.149 177.213 1 9 -7 -3 398.032 203.043 -2 -7 7 -3 398.032 203.043 1 -7 7 -4 938.372 303.679 1 9 7 -4 1801.08 303.270 -2 -7 -7 -4 1801.08 303.270 1 7 7 5 299.266 156.299 1 -11 -7 6 3778.48 276.280 -2 7 7 6 3778.48 276.280 1 11 7 -7 11254.2 483.748 -2 -7 -7 -7 11254.2 483.748 1 7 7 8 3462.34 285.754 1 -5 -9 -3 4843.96 905.461 -2 7 9 -3 4843.96 905.461 1 -7 -9 2 262.405 244.366 1 -7 9 1 24415.0 536.629 1 7 9 0 1208.49 272.054 -2 -7 -9 0 1208.49 272.054 1 7 9 1 1339.14 291.091 1 -7 9 -2 1031.81 331.052 1 0 0 13 5684.02 665.546 -2 -8 0 13 5684.02 665.546 1 -8 0 12 50337.5 981.805 1 8 0 -11 41398.8 877.391 1 2 0 10 24333.6 1010.94 -2 -8 0 10 24333.6 1010.94 1 -8 0 9 24615.7 641.522 1 8 0 -8 475.610 250.671 1 4 0 7 35384.1 905.937 -2 -8 0 7 35384.1 905.937 1 4 0 6 1603.24 303.169 -2 -8 0 6 1603.24 303.169 1 -8 0 5 37671.8 540.474 1 6 0 4 47708.2 616.267 -2 -8 0 4 47708.2 616.267 1 6 0 3 8366.57 235.453 -2 -8 0 3 8366.57 235.453 1 -8 0 2 328431. 952.526 1 -8 0 1 34343.0 261.456 1 8 0 0 13615.8 248.578 -2 -8 0 0 13615.8 248.578 1 8 0 1 9184.05 89.0507 1 8 0 2 8731.08 128.869 1 10 0 -3 50574.0 327.037 -2 -8 0 -3 50574.0 327.037 1 10 0 -4 234193. 1151.42 -2 -8 0 -4 234193. 1151.42 1 -8 0 -5 14019.7 236.188 1 12 0 -6 22623.2 303.761 -2 -8 0 -6 22623.2 303.761 1 -12 0 7 14713.1 373.621 -2 8 0 7 14713.1 373.621 1 -8 0 -8 42256.2 492.357 1 -8 0 -9 932.391 174.507 1 14 0 -10 1655.30 269.638 -2 -8 0 -10 1655.30 269.638 1 8 0 11 4975.32 259.870 1 8 0 12 15959.3 475.584 1 0 2 13 17234.2 632.242 -2 -8 -2 13 17234.2 632.242 1 -8 -2 12 7992.20 328.953 1 -8 -2 11 11679.6 378.523 1 2 2 10 3103.94 247.160 -2 -8 -2 10 3103.94 247.160 1 -8 -2 9 4341.46 176.428 1 -8 -2 8 93315.6 485.488 1 4 2 7 35382.2 493.297 -2 -8 -2 7 35382.2 493.297 1 4 2 6 16360.0 254.598 -2 -8 -2 6 16360.0 254.598 1 -8 -2 5 25048.3 199.997 1 6 2 4 329540. 772.542 -2 -8 -2 4 329540. 772.542 1 6 2 3 420.966 68.3034 -2 -8 -2 3 420.966 68.3034 1 8 -2 -2 1374.28 60.5304 1 8 2 -1 29858.6 165.529 1 -8 2 0 184097. 495.390 -2 8 -2 0 184097. 495.390 1 -8 2 -1 5427.18 70.5448 1 -8 -2 -2 4742.42 73.4055 1 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2 -3 3 1 917.555 46.4163 2 3 3 1 553.859 42.0671 2 -3 -3 -2 602.372 50.5559 2 -3 -3 -4 1261.08 131.714 2 3 3 5 1929.43 73.8235 2 -3 -3 -6 792.474 148.812 2 3 3 8 239.788 130.480 2 3 3 9 159.426 153.748 2 3 3 11 80.8141 266.415 2 3 3 12 267.929 244.331 2 -3 5 11 356.879 307.684 2 -3 5 9 548.892 257.125 2 -3 5 8 1743.17 230.321 2 -3 5 5 909.208 116.364 2 3 -5 -2 146.727 86.2636 2 -3 5 1 181.167 105.236 2 3 5 1 137.502 81.3939 2 -3 -5 -2 548.363 76.9933 2 3 5 5 126.103 91.3557 2 -3 5 -8 37.5105 155.876 2 3 5 9 218.275 205.839 2 3 5 11 16.6675 294.734 2 3 -7 -9-37.6599 336.362 2 -3 7 8 822.507 213.823 2 -3 7 5 2168.16 163.183 2 -3 -7 2 131.707 112.208 2 -3 7 1 307.611 114.307 2 3 7 1 336.728 136.499 2 -3 -7 -2 114.202 139.575 2 3 7 5 999.802 163.183 2 -3 7 -6 259.725 462.497 2 3 7 8 70.3456 213.055 2 3 -7 9 237.644 569.203 2 3 -9 -2 20.2993 199.707 2 3 9 -1 123.320 213.161 2 -3 9 -1 319.532 236.616 2 3 -9 2 247.393 212.268 2 -4 0 12 1484.31 359.558 2 -4 0 11 731.985 349.364 2 -4 0 9 878.354 296.510 2 -4 0 8 5974.37 262.180 2 -4 0 6 89.7046 146.571 2 -4 0 5 565.222 75.5072 2 4 0 -4 11307.9 260.534 2 -4 0 2 5170.72 106.288 2 4 0 -1 1573.41 56.2159 2 4 0 1 855.467 62.7638 2 4 0 2 6715.67 145.718 2 4 0 5 3954.37 201.267 2 4 0 8 1975.69 284.925 2 4 0 9 1171.17 323.811 2 4 0 11 883.118 371.400 2 4 0 12 3617.84 415.568 2 -4 2 12 932.334 227.960 2 -4 2 11 664.548 243.600 2 -4 2 9 1032.95 172.202 2 -4 2 8 1333.18 111.778 2 4 2 -6 11875.0 472.025 2 -4 2 5 6382.41 94.1048 2 -4 2 4 11143.0 268.898 2 -4 2 2 820.089 38.8732 2 -4 2 1 1975.19 41.1123 2 4 2 1 409.522 40.1835 2 4 2 2 13138.0 111.734 2 4 -2 4 36609.5 869.804 2 4 2 5 189.137 70.6090 2 4 2 8 1634.05 137.711 2 4 2 9 371.389 138.491 2 4 2 11 818.875 202.368 2 4 2 12 1271.53 228.310 2 -4 4 12 1160.71 264.291 2 -4 4 11 720.984 287.789 2 -4 4 9 609.064 162.617 2 -4 4 8 4425.34 202.011 2 4 4 -6 43.0200 270.237 2 -4 4 5 255.204 96.5629 2 -4 4 2 2235.51 76.8759 2 4 4 -1 632.770 49.9027 2 -4 -4 -1 350.743 48.4823 2 4 4 2 1972.95 57.1037 2 -4 4 -5 1098.73 86.5395 2 4 4 8 1309.53 153.253 2 4 4 9 617.076 191.584 2 4 4 11 317.008 274.228 2 -4 6 9 612.707 232.158 2 -4 6 8 726.685 203.239 2 -4 6 5 1911.29 122.840 2 4 -6 -4 3367.72 322.696 2 4 -6 -2 82.9653 94.4746 2 -4 6 1 655.549 126.403 2 -4 -6 -1 219.965 110.420 2 -4 -6 -2 1624.10 124.121 2 4 6 5 76.5178 107.812 2 4 6 8 1151.16 189.931 2 4 6 9 214.528 223.990 2 -4 -8 5 225.970 168.735 2 4 -8 -2 750.265 216.311 2 4 -8 -1 177.554 195.070 2 -4 -8 -1 181.264 180.378 2 4 -8 2 485.110 207.033 2 4 -8 5 618.303 196.984 2 -4 8 -6 281.915 489.913 2 -5 1 12 124.736 241.879 2 -5 1 11 314.440 227.092 2 -5 1 9 323.426 148.025 2 -5 1 8 874.727 117.107 2 5 1 -6 182.896 117.273 2 -5 1 5 67.5439 45.3508 2 -5 1 4 653.736 62.1089 2 -5 -1 3 2675.92 210.779 2 -5 -1 2 1197.00 47.8354 2 -5 -1 1 823.065 43.8882 2 5 1 1 20551.3 92.8177 2 5 1 2 1085.73 46.1342 2 5 1 4 2820.41 162.120 2 5 1 5 148.573 86.9474 2 5 1 8 367.935 131.746 2 5 1 9 196.453 147.194 2 5 1 11 793.212 192.536 2 5 1 12 20.4683 215.599 2 -5 3 12 437.345 251.427 2 -5 3 11 227.008 198.658 2 -5 3 9 134.641 156.764 2 5 3 -8 666.388 127.439 2 -5 3 5 76.2487 67.3236 2 5 -3 -4 140.040 273.324 2 -5 3 2 605.165 52.9156 2 -5 3 1 203.906 42.1827 2 5 3 1 5932.62 77.9731 2 5 3 2 924.677 54.6732 2 5 3 5 139.757 83.8526 2 5 3 8 98.2246 118.590 2 5 3 9 379.804 163.012 2 5 3 11 389.227 217.381 2 5 3 12 10.2662 250.089 2 -5 5 11-40.4942 277.403 2 -5 5 9 499.105 250.879 2 5 5 -8 507.530 219.842 2 -5 5 5 61.7267 86.4659 2 5 -5 -4 327.598 170.431 2 -5 5 2 588.694 81.2426 2 -5 5 1 520.653 89.1004 2 -5 -5 -1 9404.64 140.599 2 -5 5 -2 522.396 81.1097 2 5 5 5 105.091 81.8474 2 -5 5 -8 96.1838 162.755 2 -5 5 -9-34.8270 206.028 2 5 5 11 333.316 389.654 2 5 -7 -9 330.701 369.897 2 -5 7 8 352.712 197.527 2 5 7 -6 109.025 468.331 2 -5 7 5 191.872 141.478 2 5 -7 -2 201.335 130.022 2 -5 7 1 133.297 124.865 2 -5 -7 -1 1199.06 177.972 2 -5 -7 -2 471.914 152.510 2 5 -7 5 14.6757 161.986 2 -5 7 -6 156.306 429.125 2 5 7 8 225.235 219.014 2 -5 -9 2 310.059 196.685 2 -5 -9 1 508.492 267.659 2 -5 9 -1 3374.00 279.498 2 5 -9 2 80.1243 236.474 2 -6 0 12 1177.83 340.595 2 -6 0 11 1031.29 333.867 2 -6 0 9 1220.27 208.010 2 -6 0 8 173.046 155.987 2 -6 0 5 769.992 59.8936 2 -6 0 4 7959.57 177.857 2 -6 0 2 27208.1 220.786 2 -6 0 1 419.963 76.2283 2 6 0 1 836.170 71.8507 2 6 0 2 1218.03 82.6047 2 6 0 5 1499.24 176.962 2 6 0 8 981.521 254.983 2 6 0 9 375.484 282.676 2 6 0 11 325.968 364.174 2 6 0 12 1295.05 224.836 2 -6 2 12 411.208 244.922 2 -6 2 11 124.733 183.746 2 -6 2 9 246.596 130.558 2 -6 2 8 163.124 97.0128 2 -6 2 6 2448.24 146.063 2 -6 2 5 183.461 54.4496 2 6 -2 -4 181.091 191.337 2 -6 -2 2 1345.25 47.7750 2 -6 2 1 1741.12 45.4745 2 6 2 1 1299.16 55.3243 2 6 2 2 8100.01 94.9291 2 6 2 5 1037.63 81.8779 2 6 2 8 758.120 124.335 2 6 2 9 875.006 153.002 2 6 2 11 11.0948 192.394 2 6 2 12 226.820 229.964 2 -6 4 12 1069.00 260.163 2 -6 4 11 368.851 284.496 2 -6 4 9 880.946 166.871 2 -6 4 8 532.560 169.709 2 6 4 -5 866.541 110.723 2 6 -4 -4 3010.13 290.955 2 -6 4 2 14895.9 132.847 2 6 4 -1 161.932 52.7364 2 -6 -4 -1 455.353 46.3762 2 6 4 2 2609.40 76.2594 2 -6 4 -5 672.137 75.8674 2 6 4 8 735.685 153.661 2 6 4 9-42.3127 195.671 2 6 4 11 349.439 232.688 2 -6 6 9 71.7052 197.391 2 -6 6 8-37.4007 181.136 2 -6 6 5 130.460 96.8796 2 6 -6 -4 701.900 252.498 2 6 -6 -2 193.707 89.3894 2 -6 6 1 327.980 103.436 2 -6 -6 -1 525.061 128.309 2 -6 -6 -2 1783.63 147.926 2 6 6 5 436.802 114.820 2 6 6 8 195.383 178.712 2 6 6 9 520.345 213.595 2 6 8 -6 1909.52 581.955 2 6 8 -5 95.8442 187.239 2 -6 -8 2 5597.74 290.088 2 -6 -8 1 81.7940 163.688 2 -6 8 -1 174.427 210.303 2 6 -8 2 1288.09 222.878 2 6 -8 5 375.214 202.199 2 -6 8 -6 1344.70 507.312 2 -7 1 12 300.873 236.548 2 -7 1 11 158.154 191.710 2 -7 1 9 294.251 138.160 2 -7 -1 8 634.795 93.2905 2 -7 1 6 216.212 72.8394 2 -7 -1 5 907.472 68.3353 2 -7 -1 4 3479.65 262.792 2 -7 -1 2 197.191 41.1679 2 -7 1 1 9519.07 91.2097 2 7 1 1 621.504 40.9697 2 7 1 2 72.3513 45.1809 2 7 1 5 21.4289 65.1013 2 7 1 8 691.470 137.326 2 7 1 9 892.959 162.942 2 7 1 11 102.340 188.902 2 7 1 12 116.753 185.002 2 -7 3 12 308.227 185.891 2 -7 3 11 369.677 199.886 2 -7 3 9 200.247 142.973 2 7 3 -8 799.984 146.406 2 -7 3 5 1236.10 69.7000 2 -7 -3 4 2869.53 359.751 2 -7 -3 2 698.999 48.0932 2 -7 -3 1 2523.61 59.6613 2 -7 -3 -1 401.283 48.1810 2 7 3 2 102.447 55.4850 2 7 3 5 128.216 80.4361 2 7 3 8 514.758 122.738 2 7 3 9 481.645 188.405 2 7 3 11 202.686 219.930 2 7 3 12 5.34860 286.709 2 -7 5 11 697.882 273.530 2 -7 5 9 7.92071 199.062 2 7 5 -8 245.794 168.717 2 -7 5 5 415.315 102.778 2 7 -5 -4 1032.72 229.702 2 7 5 -2 43.6532 77.1282 2 7 5 -1 5212.90 119.685 2 -7 -5 -1 381.141 75.7298 2 -7 -5 -2 199.600 78.0725 2 7 5 5 148.420 83.2479 2 7 5 8 378.621 146.276 2 -7 5 -9 372.185 185.366 2 -7 5 -11 281.118 587.502 2 7 -7 -9-4.30099 478.639 2 -7 7 8 550.434 203.340 2 -7 -7 5 493.738 139.872 2 7 -7 -4 1272.73 302.488 2 -7 -7 2 411.104 156.030 2 -7 -7 1 718.616 163.338 2 -7 -7 -1 181.797 155.737 2 -7 -7 -2 63.3655 141.228 2 -7 7 -5 160.656 159.893 2 -7 7 -6 263.507 431.612 2 7 7 8 354.808 241.921 2 -7 -9 2-196.489 261.240 2 -7 -9 1 1801.15 267.312 2 -7 9 -1 176.084 259.677 2 -7 9 -2-303.257 356.405 2 -8 0 12 3103.84 374.408 2 -8 0 11 2741.62 376.312 2 -8 0 9 1654.29 214.490 2 -8 0 8 170.166 136.036 2 -8 0 6 15.4796 38.4845 2 -8 0 5 3803.73 101.285 2 8 0 -4 3674.18 293.569 2 -8 0 2 30509.6 191.808 2 -8 0 1 2982.22 84.1097 2 8 0 1 706.386 60.1229 2 8 0 2 530.728 77.7336 2 8 0 5 945.809 183.039 2 8 0 8 3024.04 315.765 2 8 0 9 292.682 298.220 2 8 0 11 460.730 303.524 2 8 0 12 1126.78 238.068 2 -8 2 12 1015.82 195.359 2 -8 2 11 916.021 215.163 2 -8 -2 9 511.929 128.806 2 -8 2 8 5891.03 157.355 2 -8 -2 5 2773.86 73.2919 2 -8 2 2 125.310 41.6150 2 -8 2 1 2326.04 55.1003 2 8 2 1 436.397 59.0518 2 8 2 2 389.870 55.9129 2 8 2 5 4778.27 88.0539 2 8 2 8 2114.72 143.741 2 8 2 9 665.230 149.430 2 8 2 11 98.3785 185.593 2 8 2 12 1223.90 224.912 2 -8 4 12 2513.51 249.909 2 -8 4 11 1983.47 217.727 2 -8 4 9 1655.56 207.191 2 8 4 -8 102.567 139.068 2 -8 -4 6 47.6051 308.472 2 8 4 -5 2212.16 90.3689 2 -8 4 2 7880.04 106.465 2 -8 -4 1 1334.41 65.9801 2 -8 -4 -1 261.070 58.6692 2 8 4 2 549.179 67.6473 2 8 4 5 617.061 72.3952 2 8 4 8 2185.96 145.572 2 8 4 9 90.4368 171.924 2 8 4 11 354.696 221.505 2 -8 6 9 233.610 209.680 2 -8 6 8 3278.12 226.710 2 -8 6 5 588.161 129.816 2 8 -6 -4 9146.81 551.536 2 -8 -6 2 91.0310 102.447 2 -8 -6 1 796.707 110.865 2 -8 -6 -1 232.093 129.119 2 -8 -6 -2 314.250 136.386 2 8 6 5 1486.23 134.528 2 8 6 8 1299.33 198.943 2 8 6 9 373.056 214.045 2 -8 -8 5 591.062 194.611 2 -8 -8 2 1616.87 200.273 2 8 8 -1 278.088 175.733 2 -8 8 -1 170.554 212.985 2 8 -8 2 401.525 222.631 2 8 -8 5 295.669 207.549 2 -8 8 -6 83.4435 469.601 2 -9 1 12 204.430 146.054 2 -9 1 11 85.4374 187.779 2 -9 1 9 416.152 114.986 2 -9 -1 8 358.952 80.3916 2 -9 -1 6 98.6297 219.087 2 -9 -1 5 726.296 68.1327 2 9 -1 -4 1984.64 295.191 2 -9 1 2 107.463 46.1645 2 -9 1 1 97.0319 48.2173 2 9 1 1 1180.66 47.8436 2 9 1 2 137.688 46.7279 2 9 1 5 4392.53 97.1961 2 9 1 8 1485.37 156.758 2 9 1 9 109.854 164.813 2 9 1 11 269.039 211.763 2 9 1 12 156.235 188.259 2 -9 3 12 64.6430 164.985 2 -9 3 11 77.0584 176.378 2 -9 -3 9 127.744 165.573 2 -9 3 8 288.045 135.026 2 -9 -3 6 273.207 288.934 2 -9 -3 5 2031.03 74.7568 2 -9 3 2 147.323 54.9578 2 -9 -3 1 220.244 53.5035 2 -9 -3 -1 849.571 70.7389 2 9 3 2 67.0194 62.4998 2 9 3 5 7099.39 112.847 2 9 3 8 892.727 131.110 2 9 3 9 265.219 168.989 2 9 3 11 285.818 190.434 2 9 3 12 137.468 240.242 2 -9 5 11 146.785 250.637 2 9 5 -9 407.518 202.933 2 9 5 -8 131.540 153.591 2 -9 5 5 201.681 97.3681 2 9 -5 -4 1292.62 263.329 2 -9 -5 2 121.922 80.5117 2 -9 -5 1 66.7609 80.5295 2 9 5 1 778.235 97.2005 2 9 5 2 127.033 81.8711 2 9 5 5 1343.28 102.626 2 9 5 8 1082.49 159.843 2 9 5 9 31.5349 175.617 2 9 -7 -9-145.034 485.869 2 -9 -7 8 214.944 203.283 2 -9 -7 5 975.618 180.535 2 9 -7 -4 871.144 280.831 2 -9 -7 2 87.8403 143.983 2 -9 -7 1 201.837 148.695 2 -9 -7 -1 409.251 171.777 2 -9 -7 -2 145.708 156.743 2 9 -7 5 2676.07 197.736 2 9 -7 8 59.0576 368.407 2 -9 -9 1 172.046 516.326 2 9 -9 1 519.863 443.450 2 10 0 -12 85.8192 236.652 2 10 0 -11-120.795 206.261 2 10 0 -9 217.518 141.681 2 10 0 -8 189.817 138.552 2 -10 0 6 2324.30 206.582 2 -10 0 5 618.447 106.033 2 -10 0 2 1196.37 75.1567 2 -10 0 1 142.449 91.2217 2 10 0 1 33.0130 126.368 2 10 0 2 3816.75 118.589 2 10 0 5 170.582 139.214 2 10 0 8 21.4997 254.478 2 10 0 9 409.387 333.344 2 10 0 11 247.751 205.800 2 10 0 12 85.0239 204.763 2 -10 2 12 969.560 174.976 2 -10 2 11 2344.85 222.201 2 -10 -2 9 145.911 109.411 2 -10 -2 8 967.090 107.135 2 -10 -2 5 3698.30 83.6360 2 -10 2 2 24601.8 138.359 2 -10 -2 1 192.420 50.1502 2 -10 -2 -1 4009.74 86.7760 2 10 2 2 15147.6 140.017 2 10 2 5 4457.14 85.6518 2 10 2 8 1028.20 124.272 2 10 2 9 555.214 149.231 2 10 2 11 102.886 175.786 2 10 2 12 319.417 249.064 2 -10 4 12 259.195 213.307 2 -10 4 11 237.075 199.294 2 -10 -4 9 111.191 182.350 2 -10 -4 8 92.2247 151.063 2 -10 -4 5 462.765 80.0447 2 -10 -4 2 237.990 73.6070 2 -10 -4 1 102.455 76.1116 2 -10 -4 -1 62.9352 70.7576 2 -10 -4 -2 1460.11 80.2072 2 10 4 5 28.6575 71.6323 2 10 4 8 113.875 131.070 2 10 4 9 380.174 164.333 2 10 4 11-248.622 359.556 2 -10 -6 9 89.7973 207.603 2 -10 -6 8 396.750 178.111 2 -10 6 5 688.169 137.981 2 10 -6 -4 218.930 252.576 2 -10 -6 2 7408.26 181.676 2 -10 -6 1 248.244 117.013 2 -10 -6 -1 1577.33 155.249 2 -10 -6 -2 7382.60 196.298 2 10 6 5 1316.74 137.147 2 10 6 8 555.781 192.441 2 10 6 9-171.987 516.360 2 -10 -8 5 443.239 194.802 2 -10 -8 2 228.919 180.307 2 -10 -8 1 182.207 186.573 2 -10 -8 -1 206.634 204.054 2 10 -8 2 106.476 198.743 2 -10 8 -5-12.3921 295.826 2 -11 1 12 213.731 153.157 2 -11 1 11 257.285 180.809 2 -11 1 9 71.1616 106.446 2 -11 -1 8 417.194 87.7474 2 -11 -1 5 1779.24 82.7599 2 -11 1 2 36.1267 48.7275 2 -11 -1 1 5384.56 84.3436 2 11 -1 1 116.156 36.1884 2 11 1 2 59.8101 52.3435 2 11 1 5 410.581 70.5965 2 11 1 8 229.205 120.595 2 11 1 9 633.626 146.032 2 11 1 11 419.035 179.634 2 11 1 12 78.3089 288.692 2 -11 3 12 112.102 167.177 2 -11 3 11 256.477 187.304 2 -11 -3 9 19.8792 152.031 2 -11 -3 8 141.773 117.384 2 -11 -3 5 1523.44 74.6550 2 -11 3 2 85.1830 56.6647 2 -11 -3 1 4613.81 101.764 2 -11 -3 -1 550.083 80.4390 2 11 3 2 45.4423 68.8732 2 11 3 5 163.148 71.3620 2 11 3 8 291.717 122.853 2 11 3 9 953.214 162.553 2 11 3 11 354.453 208.066 2 -11 5 11 256.231 288.371 2 -11 -5 9 55.8746 193.372 2 -11 -5 8 588.196 175.153 2 11 5 -5 1274.00 105.732 2 -11 -5 2 34.5291 103.499 2 -11 -5 1 1756.95 123.518 2 11 5 1 430.054 99.3633 2 11 5 2 153.257 91.4023 2 11 5 5 352.654 97.4583 2 11 5 8 127.699 164.964 2 11 5 9 319.637 195.426 2 -11 7 8 59.3746 216.054 2 -11 -7 5 392.440 152.942 2 11 -7 -4 166.540 287.230 2 -11 -7 2 216.692 143.217 2 -11 -7 1 1431.75 190.383 2 -11 7 -1 464.383 194.285 2 -11 -7 -2 227.375 162.007 2 -11 7 -5 65.0937 145.288 2 11 -9 -1 1091.39 437.477 2 -12 0 12 1734.13 220.879 2 12 0 -11 199.219 204.294 2 12 0 -9 2245.68 201.439 2 12 0 -8 2569.51 193.259 2 -12 0 5 534.025 125.607 2 -12 0 2 4640.94 83.2199 2 12 0 -1 2289.45 149.258 2 12 0 1 727.204 97.7600 2 12 0 2 1438.11 83.6626 2 12 0 5 377.217 149.083 2 12 0 8 755.480 184.855 2 12 0 9 1857.17 260.675 2 12 0 11 338.527 262.927 2 -12 2 12 239.470 164.856 2 -12 2 11 229.925 178.831 2 -12 2 9 1370.86 125.438 2 -12 -2 8 3382.46 128.899 2 -12 -2 6 360.643 293.132 2 -12 -2 5 3142.99 86.8099 2 -12 2 2 1316.11 62.5006 2 -12 -2 1 5071.43 97.7106 2 12 -2 1 492.495 72.3977 2 12 2 2 681.627 69.9423 2 12 2 5 468.938 70.4752 2 12 2 8 7666.87 194.477 2 12 2 9 1010.28 164.442 2 12 2 11 251.094 206.000 2 12 -4 -12 1167.63 311.347 2 -12 4 11 221.902 191.764 2 -12 -4 9 1189.50 189.252 2 -12 -4 8 1639.94 151.468 2 -12 4 5 347.228 82.1710 2 -12 -4 2 1800.50 94.8671 2 -12 -4 1 821.930 88.2769 2 -12 -4 -1 395.261 81.1428 2 -12 -4 -2 1029.08 82.3163 2 12 4 5 189.525 83.8547 2 12 4 8 512.682 147.116 2 12 4 9 1375.53 223.918 2 -12 6 9 430.336 229.945 2 -12 6 8 1262.45 197.993 2 -12 6 5 1824.92 147.022 2 12 -6 -4 142.310 252.081 2 12 6 -2 475.441 120.819 2 12 6 -1 1501.88 148.365 2 12 6 1 430.914 158.220 2 12 6 2 181.425 132.292 2 12 -6 5 341.214 123.618 2 12 -6 8 3806.20 382.097 2 -12 -8 5 399.167 241.912 2 12 -8 -4 4248.11 527.394 2 -12 -8 2 681.489 214.733 2 -12 8 1 225.702 188.386 2 -12 -8 -1 243.412 226.543 2 12 -8 2 501.119 234.939 2 -13 1 12 37.8256 174.886 2 -13 1 11 79.4594 168.243 2 -13 1 9 268.798 103.568 2 -13 -1 8 623.336 105.444 2 -13 1 5 426.661 78.2510 2 -13 1 2 457.649 56.9053 2 -13 -1 1 1061.96 70.0790 2 13 1 1 241.149 56.0614 2 13 1 2 261.340 51.7152 2 13 1 5 745.329 65.7719 2 13 1 8 148.219 144.036 2 13 1 9 325.493 173.213 2 13 1 11 151.716 202.105 2 -13 3 12 56.3026 170.645 2 -13 3 11 72.3472 181.438 2 -13 -3 9 208.416 138.124 2 -13 -3 8 668.098 127.972 2 -13 3 5 256.797 58.9599 2 -13 -3 2 624.662 62.8273 2 -13 -3 1 146.539 77.1261 2 13 -3 1 192.515 81.0997 2 13 -3 2 519.577 72.8057 2 13 3 5 231.608 81.2601 2 -13 3 -6 1103.95 321.237 2 13 -3 8 8.07538 151.209 2 13 -3 9 137.714 198.525 2 -13 -3 -11 65.3198 487.067 2 13 -5 -11-320.968 410.356 2 -13 5 9 195.620 196.493 2 13 5 -8 249.163 184.237 2 -13 5 5 279.271 108.966 2 -13 -5 2 170.969 109.576 2 -13 -5 1 864.587 127.710 2 -13 -5 -1 200.209 118.471 2 13 5 2 59.4163 86.7492 2 13 5 5 492.390 115.333 2 13 -5 8 353.728 188.683 2 13 -5 9 207.986 237.388 2 -13 7 8 109.687 347.711 2 -13 -7 5 126.882 157.981 2 13 -7 -4-22.1861 308.243 2 -13 -7 2 399.923 157.204 2 13 7 -1 127.433 177.969 2 -13 7 -1 181.397 179.484 2 -13 -7 -2 317.617 196.395 2 13 -7 5 232.324 199.617 2 -14 0 12 89.3124 215.102 2 -14 0 11 886.268 221.403 2 14 0 -9 152.781 179.607 2 14 0 -8 765.070 178.621 2 -14 0 5 60.1781 128.557 2 14 0 -2 779.224 70.4648 2 14 0 -1 848.038 114.854 2 14 0 1 2708.94 133.633 2 14 0 2 16604.6 259.559 2 14 0 5 2915.72 195.361 2 14 0 8 109.415 258.456 2 14 0 9 3727.09 404.034 2 14 0 11 839.389 289.969 2 -14 2 12 64.3525 166.943 2 -14 2 11 118.904 179.175 2 -14 2 9 160.485 130.803 2 -14 -2 8 271.788 97.6974 2 -14 2 5 453.278 62.8963 2 -14 -2 2 2990.57 88.9499 2 -14 -2 1 219.536 70.2933 2 14 -2 1 1784.24 83.4359 2 14 -2 2 127.183 67.7852 2 14 -2 5 83.8549 96.3774 2 14 2 8 951.370 161.969 2 14 2 9 241.607 174.527 2 14 2 11 119.638 435.960 2 -14 4 11 422.305 219.868 2 -14 4 9 227.598 160.689 2 -14 4 8 494.683 146.585 2 -14 4 5 58.7028 88.0101 2 -14 -4 2 714.706 91.9831 2 -14 -4 1 386.998 88.8973 2 -14 -4 -1 1339.67 100.610 2 -14 -4 -2 11567.7 163.197 2 14 -4 5 2578.57 133.988 2 14 -4 8 91.6657 168.909 2 14 -4 9 3218.50 298.529 2 -14 6 9 75.2478 225.023 2 -14 6 8 94.3455 199.047 2 14 6 -5 48.1587 135.278 2 14 6 -2 1804.17 145.932 2 14 6 -1 331.179 142.493 2 14 6 1 636.472 151.406 2 14 6 2 121.330 153.094 2 -14 6 -5-20.8298 170.462 2 14 8 -5 11.5039 282.105 2 14 -8 -4 431.348 399.255 2 14 8 -2 811.170 193.841 2 -14 -8 1 7.75831 206.605 2 -14 -8 -1 303.276 279.118 2 -14 8 -2 4408.28 614.456 2 -15 1 12 669.859 170.308 2 -15 1 11 454.903 150.774 2 -15 1 9 684.822 115.111 2 -15 1 8 340.783 106.361 2 -15 1 5 94.2947 74.6161 2 -15 -1 2 257.925 66.2607 2 -15 -1 1 3468.18 131.907 2 15 1 1 327.832 86.9188 2 15 -1 2 1794.87 92.8139 2 15 1 5 260.818 91.0391 2 15 1 8 257.577 149.230 2 15 1 9 213.477 174.728 2 15 1 11-83.4955 502.244 2 -15 3 12 172.487 280.348 2 -15 3 11 386.239 191.105 2 -15 3 9 297.442 143.766 2 -15 3 8 378.460 130.076 2 -15 3 5 166.996 75.9789 2 -15 -3 2 212.441 60.7391 2 -15 -3 1 3546.89 103.110 2 15 -3 1 316.678 107.851 2 15 -3 2 1163.81 101.972 2 15 -3 5 636.401 101.600 2 15 -3 8 34.7124 158.600 2 15 -3 9 194.019 207.371 2 15 5 -9 574.395 213.848 2 -15 5 8 181.951 168.456 2 -15 5 5 54.5101 112.835 2 -15 -5 2 94.8386 113.191 2 -15 -5 1 1333.82 140.516 2 15 -5 1 67.1985 146.881 2 15 -5 2 1374.94 124.168 2 15 -5 5 146.518 134.916 2 15 -5 8 124.509 212.147 2 -15 -7 5 228.223 151.518 2 15 -7 -4 293.419 314.904 2 15 7 -2 96.8231 178.504 2 15 7 -1 1395.15 221.445 2 15 7 1 220.297 214.759 2 15 7 2 176.841 215.627 2 -15 7 -5 8.24733 446.157 2 -16 0 12 1237.83 239.222 2 -16 0 11 349.792 200.524 2 -16 0 9 1305.11 196.903 2 16 0 -8 1960.06 207.814 2 -16 0 5 4330.64 156.407 2 16 0 -4 860.922 189.230 2 16 0 -2 732.005 118.110 2 16 0 -1 512.246 119.036 2 16 0 1 121.131 106.453 2 16 0 2 2027.63 118.041 2 16 0 5 1265.52 169.269 2 16 0 8 1947.39 309.617 2 16 0 9 665.164 295.439 2 -16 2 12-17.1847 175.492 2 -16 2 11 432.907 189.190 2 -16 2 9 888.645 144.357 2 -16 2 8 1881.91 125.221 2 -16 2 5 2192.67 87.9836 2 -16 -2 2 1400.05 99.3212 2 -16 -2 1 2152.47 125.683 2 -16 -2 -1 338.444 98.9303 2 16 -2 2 1504.98 107.542 2 16 -2 5 98.9401 104.370 2 16 -2 8 893.939 185.739 2 16 -2 9 191.422 199.665 2 -16 4 11 78.7363 275.214 2 16 4 -9 638.942 169.075 2 16 4 -8 1221.41 164.553 2 -16 4 5 2054.36 114.778 2 -16 -4 2 240.885 92.0314 2 -16 -4 1 438.568 105.222 2 16 -4 1 141.365 116.224 2 16 -4 2 1009.24 114.085 2 16 -4 5 369.868 111.156 2 16 -4 8 1622.31 214.953 2 -16 -4 -9 402.831 421.669 2 -16 6 9 380.834 362.864 2 -16 6 8 689.507 216.561 2 16 6 -5 761.643 145.672 2 16 6 -2 928.158 169.206 2 16 6 -1 1165.17 196.731 2 16 6 1-22.3910 158.448 2 16 6 2 610.582 192.778 2 -16 6 -5 462.526 196.738 2 -17 -1 12 228.624 226.572 2 -17 1 11 503.086 160.444 2 17 -1 -9 182.003 124.915 2 -17 1 8 310.159 120.518 2 17 1 -6 1265.06 271.255 2 -17 -1 5 16.0102 99.5213 2 -17 -1 2 245.793 84.2439 2 17 -1 -1 1759.76 125.866 2 17 -1 1 2213.48 105.808 2 17 -1 2 852.449 87.6281 2 17 -1 5 389.647 118.119 2 17 1 8 334.230 167.673 2 17 1 9 193.714 188.060 2 -17 3 11 604.988 228.962 2 -17 3 9 134.373 169.848 2 -17 3 8 323.217 141.544 2 -17 -3 5 92.3768 84.1675 2 -17 -3 2 115.373 89.3122 2 -17 -3 1 720.786 108.871 2 -17 -3 -1 775.882 122.245 2 17 -3 2 609.006 105.294 2 17 -3 5 296.553 105.643 2 17 -3 8 345.179 185.914 2 17 -3 9 217.598 220.876 2 -17 -5 9 226.732 275.302 2 -17 -5 8 442.021 247.747 2 -17 -5 5-11.6911 173.224 2 -17 -5 2 157.635 151.737 2 -17 -5 1 1107.08 172.361 2 17 -5 1 1727.72 168.091 2 17 -5 2 685.810 143.008 2 17 -5 5 301.975 146.509 2 17 7 -5 349.167 206.921 2 17 7 -2 204.532 214.411 2 17 7 -1 102.093 242.915 2 17 7 1 210.397 220.041 2 17 7 2 165.135 198.311 2 18 0 -12 105.193 440.208 2 18 0 -11 725.533 242.840 2 18 0 -9 3076.13 279.562 2 18 0 -8 293.371 183.360 2 18 0 -5 92.3927 160.146 2 18 0 -2 5156.83 186.041 2 18 0 -1 259.676 140.339 2 18 0 1 545.402 127.275 2 18 0 2 2258.52 184.639 2 18 0 5 231.233 178.170 2 18 0 8 702.030 223.793 2 18 0 9 446.502 256.926 2 18 -2 -11 362.097 215.679 2 18 -2 -9 1220.05 197.993 2 -18 -2 8 181.986 149.169 2 -18 -2 5 634.417 91.5590 2 -18 -2 2 86.3366 91.1029 2 -18 -2 1 721.046 115.544 2 18 -2 1 1010.51 120.251 2 18 -2 2 1344.93 114.711 2 18 -2 5 3954.11 168.457 2 18 -2 8 390.737 190.409 2 18 -2 9 793.612 241.465 2 -18 -4 9 1952.67 237.714 2 -18 -4 8 127.692 189.269 2 -18 -4 5 104.452 122.220 2 -18 -4 2 3108.72 143.979 2 -18 -4 1 215.684 119.945 2 18 -4 1 446.711 123.635 2 18 -4 2 1395.45 130.477 2 18 -4 5 70.8297 121.504 2 -18 -4 -8 969.541 381.137 2 -18 -6 5 561.867 192.067 2 -18 -6 2 257.835 178.319 2 -18 -6 1 142.023 199.804 2 -18 6 -1 678.757 176.207 2 18 6 2 605.264 201.498 2 18 -6 5 1213.84 235.676 2 -19 -1 12 210.559 527.736 2 19 -1 -11 197.506 190.110 2 19 -1 -9 177.143 139.486 2 19 -1 -8 227.848 150.518 2 -19 -1 5 718.252 117.088 2 19 -1 -2 621.022 110.534 2 19 -1 -1 334.830 112.359 2 19 -1 1 867.913 126.330 2 19 -1 2-51.6526 100.174 2 19 -1 5 124.388 135.819 2 19 -1 8 314.346 187.342 2 19 -1 9 607.807 223.254 2 -19 3 11-1169.83 568.582 2 19 -3 -9 240.354 223.430 2 -19 -3 8 381.476 187.094 2 -19 -3 5 1065.48 112.587 2 -19 -3 2 1384.14 111.715 2 -19 -3 1 171.673 112.511 2 19 -3 1 737.141 123.986 2 19 -3 2-99.7316 117.378 2 19 -3 5 68.0028 113.132 2 19 -3 8 428.217 213.264 2 -19 -5 9 280.387 422.292 2 -19 -5 8-155.696 265.811 2 -19 -5 5 670.148 184.247 2 -19 -5 2 122.593 167.588 2 -19 -5 1 213.036 163.559 2 19 -5 1 290.385 161.589 2 -19 -5 -2 87.9433 163.721 2 19 -5 5 183.207 182.255 2 19 -7 -5 569.408 418.639 2 19 7 -2 817.650 235.654 2 19 7 -1 85.7344 251.712 2 19 7 1-23.5603 314.894 2 19 7 2-165.370 412.292 2 20 0 -11 1398.69 277.446 2 20 0 -9 3629.49 297.832 2 20 0 -8 124.061 195.827 2 20 0 -5 3737.45 238.655 2 20 0 -2 1091.13 222.583 2 20 0 -1 1760.92 192.513 2 20 0 1 666.335 150.422 2 20 0 2 948.526 138.352 2 -20 0 -5 1747.33 309.846 2 20 0 8 889.021 247.239 2 -20 2 11 138.574 558.759 2 20 -2 -9 77.8571 181.575 2 -20 -2 8 1624.28 183.231 2 -20 -2 5 1566.51 114.690 2 -20 -2 2 298.550 99.5920 2 -20 -2 1 1090.29 130.470 2 20 -2 1 506.996 115.190 2 20 -2 2 472.050 113.706 2 20 -2 5 337.464 155.264 2 20 -2 8 1007.91 209.977 2 -20 -4 9 2331.70 265.403 2 -20 -4 8-5.42798 203.423 2 -20 4 5 2244.51 163.756 2 -20 -4 2 734.629 126.520 2 -20 -4 1 1388.94 158.148 2 20 -4 1 408.180 140.322 2 20 -4 2 611.886 133.619 2 20 -4 5 539.429 142.166 2 -20 -6 5 638.372 201.159 2 -20 -6 2 191.451 186.888 2 -20 -6 1 596.181 213.524 2 20 6 1 460.376 186.141 2 20 6 2 187.684 186.598 2 21 -1 -11 190.558 489.497 2 21 -1 -9 373.357 163.572 2 21 -1 -8 368.791 162.679 2 21 -1 -5-1.84894 123.893 2 21 -1 -2-178.701 142.384 2 21 -1 -1 243.733 118.517 2 21 -1 1 1366.49 144.958 2 21 -1 2 361.273 115.739 2 21 1 5 394.770 176.836 2 21 -1 8 137.151 246.536 2 21 -3 -9 116.943 233.587 2 -21 -3 8 354.170 190.251 2 -21 -3 5 458.802 136.832 2 -21 -3 2 76.6847 119.376 2 -21 -3 1 126.808 121.481 2 21 -3 1 1301.32 152.532 2 21 -3 2 289.455 118.096 2 21 -3 5 263.772 152.476 2 -21 -5 8 106.686 381.989 2 -21 -5 5-153.659 185.527 2 -21 -5 2 212.605 178.605 2 -21 -5 1 400.307 183.052 2 21 -5 1 571.284 176.647 2 -21 -5 -2 144.384 149.680 2 21 -5 5 390.535 232.910 2 22 0 -11-400.196 550.625 2 22 0 -9 54.2711 233.523 2 22 0 -8 65.7199 208.291 2 22 0 -5 833.395 208.165 2 22 0 -2 486.880 223.065 2 22 0 -1 319.729 242.663 2 22 0 1 265.493 192.686 2 22 0 2 645.650 196.325 2 22 0 5 493.462 220.909 2 22 -2 -9 34.9133 195.046 2 22 -2 -8 82.5262 173.791 2 -22 -2 5 1096.91 115.207 2 22 -2 -2 11439.3 273.826 2 22 -2 -1 326.228 137.273 2 22 -2 1 1230.09 151.354 2 22 -2 2 2890.32 169.067 2 22 2 5 1403.96 211.363 2 -22 -4 9 283.787 404.470 2 -22 -4 8 270.370 217.589 2 -22 -4 5 795.412 160.910 2 -22 -4 2 517.364 148.777 2 -22 -4 1 203.574 153.173 2 22 -4 1 21.9566 156.071 2 22 -4 2 306.696 137.930 2 22 -4 5 363.644 169.670 2 22 -4 6 2408.55 658.654 2 -22 6 5 408.533 496.752 2 -22 -6 2 5288.66 278.044 2 -22 6 1 148.409 227.685 2 22 6 1 735.267 262.807 2 22 6 2 2097.45 285.492 2 23 -1 -9 175.802 173.789 2 23 -1 -8 1157.37 182.217 2 23 -1 -5 2960.34 191.041 2 23 -1 -2 88.9195 154.597 2 23 -1 -1 918.791 163.101 2 23 -1 1 225.721 140.436 2 23 -1 2 243.871 124.353 2 23 1 5 788.917 186.326 2 -23 3 9-19.9834 411.924 2 -23 -3 8 388.599 211.587 2 -23 -3 5 3174.24 176.586 2 -23 -3 2 58.7596 148.508 2 -23 -3 1 671.658 159.297 2 23 -3 1 130.954 157.053 2 23 -3 2-2.01174 136.563 2 23 3 5 663.461 200.086 2 23 3 6 224.421 424.358 2 -23 -5 5 2876.33 228.731 2 -23 -5 2 207.416 188.438 2 -23 -5 1 414.511 212.944 2 23 -5 1 379.074 201.291 2 23 -5 2 307.819 176.499 2 24 0 -9 984.193 260.202 2 24 0 -8 1960.37 265.089 2 24 0 -5 64.2853 211.704 2 24 0 -2 1400.39 267.268 2 24 0 -1 1867.11 324.157 2 24 0 1 1044.87 231.255 2 24 0 2 752.533 223.837 2 24 0 5 507.749 227.547 2 24 2 -9 1773.85 272.576 2 24 -2 -8 264.104 188.016 2 -24 -2 5 3576.60 209.882 2 24 -2 -2 190.890 168.832 2 24 -2 -1 2252.46 203.309 2 24 -2 1 326.573 146.630 2 24 -2 2 26.0194 141.785 2 24 2 5 297.728 198.526 2 24 2 6 693.806 308.083 2 -24 -4 5 234.126 152.413 2 -24 -4 2 1134.78 166.270 2 -24 -4 1 1102.53 202.134 2 24 -4 1 521.480 194.036 2 24 -4 2 672.990 162.432 2 25 1 -9-228.126 360.353 2 25 -1 -8 579.188 193.495 2 25 -1 -5 163.749 157.158 2 25 -1 -2 324.656 176.556 2 25 -1 -1 241.341 209.039 2 25 -1 1 1095.43 188.022 2 25 -1 2 559.739 151.113 2 25 -1 5 406.181 167.288 2 -25 3 8 444.452 579.857 2 -25 -3 5 324.867 152.156 2 25 -3 -2 506.092 174.338 2 25 -3 -1 210.333 189.113 2 25 -3 1 865.336 182.250 2 25 -3 2 566.156 158.237 2 -25 -3 -5 117.828 429.406 2 -25 5 4 70.9247 549.921 2 25 -5 -2 107.037 330.450 2 25 -5 -1 56.2342 289.830 2 25 -5 1 437.096 352.391 2 -25 -5 -2 162.434 572.469 2 26 0 -9 52.2213 463.586 2 26 0 -8-98.8843 240.581 2 26 0 -5 285.405 212.882 2 26 0 -2 2453.02 337.488 2 26 0 -1 694.764 328.839 2 26 0 1 1450.27 337.221 2 26 0 2 2600.08 281.399 2 26 0 5 1684.83 359.696 2 26 2 -8 402.628 474.889 2 26 -2 -5-59.4235 182.308 2 26 -2 -2 153.137 168.773 2 26 -2 -1 142.593 173.655 2 26 -2 1 701.275 181.443 2 26 -2 2 59.5044 152.936 2 -26 -4 5-87.6399 263.488 2 26 -4 -2 1978.65 198.999 2 26 -4 -1 273.812 216.411 2 26 -4 1 1074.85 244.798 2 26 -4 2 2421.07 234.707 2 27 1 -8 389.824 459.705 2 27 -1 -5 261.637 167.914 2 27 -1 -2-31.0676 186.324 2 27 -1 -1 2847.80 272.066 2 27 -1 1 721.198 239.139 2 27 -1 2 317.500 210.612 2 27 -3 -5 143.855 175.224 2 27 -3 -2 166.353 216.733 2 27 -3 -1 2171.27 238.328 2 27 -3 1 260.994 220.554 2 27 -3 2 155.462 224.420 2 -27 -3 -3 2272.14 602.544 2 28 0 -5 2021.71 279.405 2 28 0 -2 410.754 286.374 2 28 0 -1 1127.41 342.493 2 28 0 1 315.413 333.393 2 28 0 2 451.415 302.213 2 28 -2 -5 1245.39 208.065 2 28 -2 -2 13.8733 191.149 2 28 -2 -1 477.976 215.228 2 28 2 1 659.106 296.832 2 -28 -2 -2 1025.27 343.611 2 -28 -4 2-417.745 582.784 2 -28 -4 1 1095.13 680.934 2 29 -1 -5 425.884 280.058 2 -29 -1 4 711.393 330.278 2 29 -1 -2 171.588 209.260 2 29 -1 -1 569.227 246.975 2 30 0 -1-44.6621 513.802 2 ; _shelx_hkl_checksum 2440 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ca1 Ca 0.33945(4) 0.500000 0.25177(10) 0.00834(17) Uani 1 2 d S T P . . Ca2 Ca 0.15486(5) 0.500000 0.18808(11) 0.01106(18) Uani 1 2 d S T P . . Cr1 Cr 0.250000 0.250000 0.500000 0.0054(3) Uani 0.516(8) 2 d S . P . . Mg1 Mg 0.250000 0.250000 0.500000 0.0054(3) Uani 0.484(9) 2 d S . P . . Cr2 Cr 0.49532(3) 0.24730(9) 0.25394(6) 0.00457(16) Uani 0.700(7) 1 d . . P . . Al2 Al 0.49532(3) 0.24730(9) 0.25394(6) 0.00457(16) Uani 0.300(8) 1 d . . P . . Si1 Si 0.09159(6) 0.000000 0.05128(13) 0.0050(2) Uani 1 2 d S T P . . Si2 Si 0.24812(6) 0.000000 0.16523(13) 0.0060(2) Uani 1 2 d S T P . . Si3 Si 0.40195(6) 0.000000 0.46535(13) 0.0048(2) Uani 1 2 d S T P . . O1 O 0.07386(11) 0.2230(4) 0.1373(2) 0.0083(4) Uani 1 1 d . . . . . O2 O 0.24643(11) 0.2293(4) 0.2657(2) 0.0080(4) Uani 1 1 d . . . . . O3 O 0.41468(11) 0.2209(4) 0.3671(3) 0.0081(4) Uani 1 1 d . . . . . O4 O 0.44434(16) 0.500000 0.1303(3) 0.0064(5) Uani 1 2 d S T P . . O5 O 0.45671(16) 0.000000 0.1265(4) 0.0086(5) Uani 1 2 d S T P . . O6 O 0.04507(16) 0.500000 0.3709(3) 0.0074(5) Uani 1 2 d S T P . . O7 O 0.03450(18) 0.000000 0.3737(4) 0.0105(6) Uani 1 2 d S T P . . O8 O 0.17686(15) 0.000000 0.0349(4) 0.0083(5) Uani 1 2 d S T P . . O9 O 0.17653(16) 0.500000 0.4751(4) 0.0090(5) Uani 1 2 d S T P . . O10 O 0.31327(17) 0.000000 0.0665(4) 0.0123(6) Uani 1 2 d S T P . . O11 O 0.18416(16) 0.000000 0.4971(3) 0.0077(5) Uani 1 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ca1 0.0060(3) 0.0112(4) 0.0082(3) 0.000 0.0025(3) 0.000 Ca2 0.0063(3) 0.0072(3) 0.0191(4) 0.000 -0.0004(3) 0.000 Cr1 0.0051(4) 0.0051(4) 0.0063(4) 0.0007(3) 0.0016(3) 0.0005(3) Mg1 0.0051(4) 0.0051(4) 0.0063(4) 0.0007(3) 0.0016(3) 0.0005(3) Cr2 0.0041(2) 0.0047(2) 0.0050(2) 0.00038(17) 0.00116(16) 0.00036(17) Al2 0.0041(2) 0.0047(2) 0.0050(2) 0.00038(17) 0.00116(16) 0.00036(17) Si1 0.0046(4) 0.0059(5) 0.0045(4) 0.000 0.0009(3) 0.000 Si2 0.0055(5) 0.0061(5) 0.0063(4) 0.000 -0.0002(4) 0.000 Si3 0.0038(4) 0.0058(5) 0.0051(4) 0.000 0.0011(3) 0.000 O1 0.0083(9) 0.0075(9) 0.0098(9) -0.0012(7) 0.0037(7) -0.0005(7) O2 0.0085(9) 0.0072(9) 0.0082(9) -0.0005(7) 0.0007(7) -0.0002(7) O3 0.0077(9) 0.0071(9) 0.0102(9) 0.0019(7) 0.0032(7) 0.0005(7) O4 0.0065(12) 0.0072(12) 0.0054(11) 0.000 -0.0002(9) 0.000 O5 0.0080(13) 0.0099(13) 0.0080(13) 0.000 0.0015(10) 0.000 O6 0.0083(13) 0.0074(12) 0.0061(12) 0.000 -0.0002(10) 0.000 O7 0.0146(14) 0.0090(13) 0.0075(13) 0.000 0.0003(11) 0.000 O8 0.0046(12) 0.0113(13) 0.0094(13) 0.000 0.0027(10) 0.000 O9 0.0042(12) 0.0139(14) 0.0099(13) 0.000 0.0044(10) 0.000 O10 0.0069(13) 0.0193(16) 0.0113(14) 0.000 0.0029(11) 0.000 O11 0.0055(12) 0.0096(13) 0.0081(13) 0.000 0.0013(10) 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O11 Ca1 O3 77.04(8) 7_556 . ? O11 Ca1 O3 77.04(8) 7_556 6_565 ? O3 Ca1 O3 90.77(11) . 6_565 ? O11 Ca1 O4 135.16(11) 7_556 . ? O3 Ca1 O4 71.92(7) . . ? O3 Ca1 O4 71.92(7) 6_565 . ? O11 Ca1 O2 73.19(8) 7_556 . ? O3 Ca1 O2 85.20(7) . . ? O3 Ca1 O2 150.11(8) 6_565 . ? O4 Ca1 O2 133.53(6) . . ? O11 Ca1 O2 73.19(8) 7_556 6_565 ? O3 Ca1 O2 150.11(8) . 6_565 ? O3 Ca1 O2 85.20(7) 6_565 6_565 ? O4 Ca1 O2 133.53(6) . 6_565 ? O2 Ca1 O2 83.78(10) . 6_565 ? O11 Ca1 O8 161.71(11) 7_556 7 ? O3 Ca1 O8 114.95(7) . 7 ? O3 Ca1 O8 114.95(7) 6_565 7 ? O4 Ca1 O8 63.13(10) . 7 ? O2 Ca1 O8 93.40(8) . 7 ? O2 Ca1 O8 93.40(8) 6_565 7 ? O11 Ca1 Si1 166.47(9) 7_556 7 ? O3 Ca1 Si1 93.57(6) . 7 ? O3 Ca1 Si1 93.57(6) 6_565 7 ? O4 Ca1 Si1 31.31(7) . 7 ? O2 Ca1 Si1 116.21(6) . 7 ? O2 Ca1 Si1 116.21(6) 6_565 7 ? O8 Ca1 Si1 31.83(7) 7 7 ? O11 Ca1 Cr1 35.34(5) 7_556 4_556 ? O3 Ca1 Cr1 112.28(6) . 4_556 ? O3 Ca1 Cr1 74.74(6) 6_565 4_556 ? O4 Ca1 Cr1 146.47(5) . 4_556 ? O2 Ca1 Cr1 79.47(6) . 4_556 ? O2 Ca1 Cr1 38.24(5) 6_565 4_556 ? O8 Ca1 Cr1 131.37(6) 7 4_556 ? Si1 Ca1 Cr1 151.372(14) 7 4_556 ? O11 Ca1 Cr1 35.34(5) 7_556 . ? O3 Ca1 Cr1 74.73(6) . . ? O3 Ca1 Cr1 112.28(6) 6_565 . ? O4 Ca1 Cr1 146.47(5) . . ? O2 Ca1 Cr1 38.24(5) . . ? O2 Ca1 Cr1 79.47(6) 6_565 . ? O8 Ca1 Cr1 131.37(6) 7 . ? Si1 Ca1 Cr1 151.372(14) 7 . ? Cr1 Ca1 Cr1 53.652(13) 4_556 . ? O1 Ca2 O1 93.54(11) . 6_565 ? O1 Ca2 O10 94.04(8) . 7 ? O1 Ca2 O10 94.04(8) 6_565 7 ? O1 Ca2 O2 91.05(7) . . ? O1 Ca2 O2 173.80(9) 6_565 . ? O10 Ca2 O2 89.78(8) 7 . ? O1 Ca2 O2 173.80(9) . 6_565 ? O1 Ca2 O2 91.05(7) 6_565 6_565 ? O10 Ca2 O2 89.78(8) 7 6_565 ? O2 Ca2 O2 84.08(11) . 6_565 ? O1 Ca2 O9 102.33(8) . . ? O1 Ca2 O9 102.33(8) 6_565 . ? O10 Ca2 O9 155.92(11) 7 . ? O2 Ca2 O9 72.58(7) . . ? O2 Ca2 O9 72.58(7) 6_565 . ? O1 Ca2 O6 64.45(7) . . ? O1 Ca2 O6 64.45(7) 6_565 . ? O10 Ca2 O6 146.88(11) 7 . ? O2 Ca2 O6 114.15(7) . . ? O2 Ca2 O6 114.15(7) 6_565 . ? O9 Ca2 O6 57.20(9) . . ? O1 Ca2 Si3 83.21(6) . 7_556 ? O1 Ca2 Si3 83.21(6) 6_565 7_556 ? O10 Ca2 Si3 175.97(9) 7 7_556 ? O2 Ca2 Si3 93.22(6) . 7_556 ? O2 Ca2 Si3 93.22(6) 6_565 7_556 ? O9 Ca2 Si3 28.11(7) . 7_556 ? O6 Ca2 Si3 29.09(6) . 7_556 ? O1 Ca2 Si1 23.71(6) . . ? O1 Ca2 Si1 111.79(7) 6_565 . ? O10 Ca2 Si1 78.03(4) 7 . ? O2 Ca2 Si1 73.77(5) . . ? O2 Ca2 Si1 154.58(6) 6_565 . ? O9 Ca2 Si1 111.16(3) . . ? O6 Ca2 Si1 86.77(4) . . ? Si3 Ca2 Si1 100.21(3) 7_556 . ? O1 Ca2 Si1 111.79(7) . 1_565 ? O1 Ca2 Si1 23.71(6) 6_565 1_565 ? O10 Ca2 Si1 78.03(4) 7 1_565 ? O2 Ca2 Si1 154.58(6) . 1_565 ? O2 Ca2 Si1 73.77(5) 6_565 1_565 ? O9 Ca2 Si1 111.16(3) . 1_565 ? O6 Ca2 Si1 86.77(4) . 1_565 ? Si3 Ca2 Si1 100.21(3) 7_556 1_565 ? Si1 Ca2 Si1 124.03(4) . 1_565 ? O1 Ca2 Cr1 138.65(7) . 4_556 ? O1 Ca2 Cr1 96.59(6) 6_565 4_556 ? O10 Ca2 Cr1 124.90(7) 7 4_556 ? O2 Ca2 Cr1 77.21(6) . 4_556 ? O2 Ca2 Cr1 36.32(5) 6_565 4_556 ? O9 Ca2 Cr1 36.32(5) . 4_556 ? O6 Ca2 Cr1 84.28(6) . 4_556 ? Si3 Ca2 Cr1 58.54(2) 7_556 4_556 ? Si1 Ca2 Cr1 142.78(3) . 4_556 ? Si1 Ca2 Cr1 91.467(19) 1_565 4_556 ? O11 Cr1 O11 180.0 7_556 . ? O11 Cr1 O9 97.08(9) 7_556 7_556 ? O11 Cr1 O9 82.92(9) . 7_556 ? O11 Cr1 O9 82.92(9) 7_556 . ? O11 Cr1 O9 97.08(9) . . ? O9 Cr1 O9 180.0 7_556 . ? O11 Cr1 O2 90.44(11) 7_556 7_556 ? O11 Cr1 O2 89.57(11) . 7_556 ? O9 Cr1 O2 90.47(11) 7_556 7_556 ? O9 Cr1 O2 89.53(11) . 7_556 ? O11 Cr1 O2 89.56(11) 7_556 . ? O11 Cr1 O2 90.44(11) . . ? O9 Cr1 O2 89.53(11) 7_556 . ? O9 Cr1 O2 90.47(11) . . ? O2 Cr1 O2 180.00(12) 7_556 . ? O11 Cr1 Ca1 43.26(9) 7_556 . ? O11 Cr1 Ca1 136.73(9) . . ? O9 Cr1 Ca1 89.40(8) 7_556 . ? O9 Cr1 Ca1 90.61(8) . . ? O2 Cr1 Ca1 133.18(6) 7_556 . ? O2 Cr1 Ca1 46.82(6) . . ? O11 Cr1 Ca1 136.74(9) 7_556 7_556 ? O11 Cr1 Ca1 43.27(9) . 7_556 ? O9 Cr1 Ca1 90.60(8) 7_556 7_556 ? O9 Cr1 Ca1 89.39(8) . 7_556 ? O2 Cr1 Ca1 46.82(6) 7_556 7_556 ? O2 Cr1 Ca1 133.18(6) . 7_556 ? Ca1 Cr1 Ca1 180.0 . 7_556 ? O11 Cr1 Ca2 87.09(8) 7_556 . ? O11 Cr1 Ca2 92.91(8) . . ? O9 Cr1 Ca2 133.53(9) 7_556 . ? O9 Cr1 Ca2 46.47(9) . . ? O2 Cr1 Ca2 135.90(6) 7_556 . ? O2 Cr1 Ca2 44.10(6) . . ? Ca1 Cr1 Ca2 62.72(2) . . ? Ca1 Cr1 Ca2 117.28(2) 7_556 . ? O11 Cr1 Ca2 92.91(8) 7_556 7_556 ? O11 Cr1 Ca2 87.10(8) . 7_556 ? O9 Cr1 Ca2 46.47(9) 7_556 7_556 ? O9 Cr1 Ca2 133.53(9) . 7_556 ? O2 Cr1 Ca2 44.10(6) 7_556 7_556 ? O2 Cr1 Ca2 135.90(6) . 7_556 ? Ca1 Cr1 Ca2 117.28(2) . 7_556 ? Ca1 Cr1 Ca2 62.72(2) 7_556 7_556 ? Ca2 Cr1 Ca2 180.0 . 7_556 ? O7 Cr2 O5 177.73(12) 3 . ? O7 Cr2 O1 86.86(12) 3 8 ? O5 Cr2 O1 91.51(11) . 8 ? O7 Cr2 O3 93.50(12) 3 . ? O5 Cr2 O3 88.10(11) . . ? O1 Cr2 O3 178.55(9) 8 . ? O7 Cr2 O6 100.19(10) 3 3_545 ? O5 Cr2 O6 81.36(10) . 3_545 ? O1 Cr2 O6 89.40(11) 8 3_545 ? O3 Cr2 O6 91.92(11) . 3_545 ? O7 Cr2 O4 80.45(10) 3 . ? O5 Cr2 O4 97.99(10) . . ? O1 Cr2 O4 90.01(11) 8 . ? O3 Cr2 O4 88.66(11) . . ? O6 Cr2 O4 179.11(11) 3_545 . ? O7 Cr2 Cr2 141.35(8) 3 6 ? O5 Cr2 Cr2 40.37(7) . 6 ? O1 Cr2 Cr2 95.23(7) 8 6 ? O3 Cr2 Cr2 85.37(6) . 6 ? O6 Cr2 Cr2 41.42(7) 3_545 6 ? O4 Cr2 Cr2 138.00(6) . 6 ? O7 Cr2 Ca1 86.03(9) 3 . ? O5 Cr2 Ca1 94.04(9) . . ? O1 Cr2 Ca1 135.38(7) 8 . ? O3 Cr2 Ca1 43.29(6) . . ? O6 Cr2 Ca1 135.21(9) 3_545 . ? O4 Cr2 Ca1 45.37(9) . . ? Cr2 Cr2 Ca1 116.837(11) 6 . ? O7 Cr2 Ca2 97.83(10) 3 3_545 ? O5 Cr2 Ca2 81.74(9) . 3_545 ? O1 Cr2 Ca2 36.57(7) 8 3_545 ? O3 Cr2 Ca2 144.66(7) . 3_545 ? O6 Cr2 Ca2 53.19(9) 3_545 3_545 ? O4 Cr2 Ca2 126.15(9) . 3_545 ? Cr2 Cr2 Ca2 65.133(11) 6 3_545 ? Ca1 Cr2 Ca2 170.15(3) . 3_545 ? O1 Si1 O1 113.70(17) . 6 ? O1 Si1 O4 111.83(10) . 7 ? O1 Si1 O4 111.83(10) 6 7 ? O1 Si1 O8 108.52(10) . . ? O1 Si1 O8 108.52(10) 6 . ? O4 Si1 O8 101.65(16) 7 . ? O1 Si1 Ca1 123.13(8) . 7 ? O1 Si1 Ca1 123.13(8) 6 7 ? O4 Si1 Ca1 49.12(11) 7 7 ? O8 Si1 Ca1 52.53(11) . 7 ? O1 Si1 Ca2 131.28(10) . 1_545 ? O1 Si1 Ca2 35.02(8) 6 1_545 ? O4 Si1 Ca2 115.22(3) 7 1_545 ? O8 Si1 Ca2 73.83(5) . 1_545 ? Ca1 Si1 Ca2 97.49(3) 7 1_545 ? O1 Si1 Ca2 35.02(8) . . ? O1 Si1 Ca2 131.28(10) 6 . ? O4 Si1 Ca2 115.22(3) 7 . ? O8 Si1 Ca2 73.83(5) . . ? Ca1 Si1 Ca2 97.49(3) 7 . ? Ca2 Si1 Ca2 124.03(4) 1_545 . ? O10 Si2 O2 111.39(10) . 6 ? O10 Si2 O2 111.39(10) . . ? O2 Si2 O2 114.06(17) 6 . ? O10 Si2 O8 104.62(17) . . ? O2 Si2 O8 107.38(10) 6 . ? O2 Si2 O8 107.38(10) . . ? O10 Si2 Ca1 73.51(6) . . ? O2 Si2 Ca1 130.22(9) 6 . ? O2 Si2 Ca1 37.90(8) . . ? O8 Si2 Ca1 119.43(3) . . ? O10 Si2 Ca1 73.51(6) . 1_545 ? O2 Si2 Ca1 37.91(8) 6 1_545 ? O2 Si2 Ca1 130.23(9) . 1_545 ? O8 Si2 Ca1 119.43(3) . 1_545 ? Ca1 Si2 Ca1 117.55(4) . 1_545 ? O10 Si2 Ca2 117.97(4) . . ? O2 Si2 Ca2 129.56(9) 6 . ? O2 Si2 Ca2 37.36(8) . . ? O8 Si2 Ca2 70.19(5) . . ? Ca1 Si2 Ca2 60.153(18) . . ? Ca1 Si2 Ca2 164.09(4) 1_545 . ? O10 Si2 Ca2 117.97(4) . 1_545 ? O2 Si2 Ca2 37.36(8) 6 1_545 ? O2 Si2 Ca2 129.56(9) . 1_545 ? O8 Si2 Ca2 70.19(5) . 1_545 ? Ca1 Si2 Ca2 164.09(4) . 1_545 ? Ca1 Si2 Ca2 60.154(18) 1_545 1_545 ? Ca2 Si2 Ca2 117.15(4) . 1_545 ? O3 Si3 O3 109.68(17) . 6 ? O3 Si3 O6 110.39(11) . 7_556 ? O3 Si3 O6 110.39(10) 6 7_556 ? O3 Si3 O9 112.26(10) . 7_556 ? O3 Si3 O9 112.26(10) 6 7_556 ? O6 Si3 O9 101.63(17) 7_556 7_556 ? O3 Si3 Ca2 125.08(8) . 7_556 ? O3 Si3 Ca2 125.08(8) 6 7_556 ? O6 Si3 Ca2 56.34(11) 7_556 7_556 ? O9 Si3 Ca2 45.29(12) 7_556 7_556 ? Si1 O1 Cr2 123.96(13) . 8_455 ? Si1 O1 Ca2 121.27(12) . . ? Cr2 O1 Ca2 112.81(10) 8_455 . ? Si2 O2 Cr1 126.33(13) . . ? Si2 O2 Ca2 118.43(11) . . ? Cr1 O2 Ca2 99.58(9) . . ? Si2 O2 Ca1 117.64(12) . . ? Cr1 O2 Ca1 94.94(8) . . ? Ca2 O2 Ca1 92.85(8) . . ? Si3 O3 Cr2 121.75(13) . . ? Si3 O3 Ca1 133.21(13) . . ? Cr2 O3 Ca1 101.81(9) . . ? Si1 O4 Cr2 128.66(8) 7 . ? Si1 O4 Cr2 128.66(8) 7 6_565 ? Cr2 O4 Cr2 96.01(13) . 6_565 ? Si1 O4 Ca1 99.57(14) 7 . ? Cr2 O4 Ca1 97.61(10) . . ? Cr2 O4 Ca1 97.61(10) 6_565 . ? Cr2 O5 Cr2 99.26(14) . 6 ? Si3 O6 Cr2 130.84(7) 7_556 8_455 ? Si3 O6 Cr2 130.84(7) 7_556 3_455 ? Cr2 O6 Cr2 97.16(13) 8_455 3_455 ? Si3 O6 Ca2 94.58(13) 7_556 . ? Cr2 O6 Ca2 92.75(10) 8_455 . ? Cr2 O6 Ca2 92.75(10) 3_455 . ? Cr2 O7 Cr2 102.70(15) 3_445 8_455 ? Si2 O8 Si1 131.9(2) . . ? Si2 O8 Ca1 132.48(16) . 7 ? Si1 O8 Ca1 95.64(14) . 7 ? Si3 O9 Cr1 127.38(9) 7_556 4_556 ? Si3 O9 Cr1 127.38(9) 7_556 . ? Cr1 O9 Cr1 93.91(12) 4_556 . ? Si3 O9 Ca2 106.60(16) 7_556 . ? Cr1 O9 Ca2 97.20(10) 4_556 . ? Cr1 O9 Ca2 97.20(10) . . ? Si2 O10 Ca2 144.63(19) . 7 ? Cr1 O11 Cr1 99.77(14) . 4_546 ? Cr1 O11 Ca1 101.39(11) . 7_556 ? Cr1 O11 Ca1 101.39(11) 4_546 7_556 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ca1 O11 2.324(3) 7_556 ? Ca1 O3 2.353(2) . ? Ca1 O3 2.353(2) 6_565 ? Ca1 O4 2.412(3) . ? Ca1 O2 2.433(2) . ? Ca1 O2 2.433(2) 6_565 ? Ca1 O8 2.508(3) 7 ? Ca1 Si1 3.1452(14) 7 ? Ca1 Cr1 3.3238(8) 4_556 ? Ca1 Cr1 3.3238(8) . ? Ca2 O1 2.281(2) . ? Ca2 O1 2.281(2) 6_565 ? Ca2 O10 2.410(3) 7 ? Ca2 O2 2.426(2) . ? Ca2 O2 2.426(2) 6_565 ? Ca2 O9 2.512(3) . ? Ca2 O6 2.828(3) . ? Ca2 Si3 3.3875(15) 7_556 ? Ca2 Si1 3.3971(7) . ? Ca2 Si1 3.3972(7) 1_565 ? Ca2 Cr1 3.4374(9) 4_556 ? Cr1 O11 1.961(2) 7_556 ? Cr1 O11 1.9613(19) . ? Cr1 O9 2.052(2) 7_556 ? Cr1 O9 2.052(2) . ? Cr1 O2 2.065(2) 7_556 ? Cr1 O2 2.065(2) . ? Cr2 O7 1.941(2) 3 ? Cr2 O5 1.947(2) . ? Cr2 O1 1.950(2) 8 ? Cr2 O3 1.963(2) . ? Cr2 O6 1.979(2) 3_545 ? Cr2 O4 2.040(2) . ? Cr2 Cr2 2.9675(11) 6 ? Si1 O1 1.598(2) . ? Si1 O1 1.598(2) 6 ? Si1 O4 1.657(3) 7 ? Si1 O8 1.667(3) . ? Si2 O10 1.622(3) . ? Si2 O2 1.640(2) 6 ? Si2 O2 1.640(2) . ? Si2 O8 1.666(3) . ? Si3 O3 1.621(2) . ? Si3 O3 1.621(2) 6 ? Si3 O6 1.652(3) 7_556 ? Si3 O9 1.666(3) 7_556 ?