#------------------------------------------------------------------------------
#$Date: 2020-09-26 08:29:00 +0300 (Sat, 26 Sep 2020) $
#$Revision: 256801 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/55/92/1559211.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_1559211
loop_
_publ_author_name
'Mizuhata, Yoshiyuki'
'Iwai, Kento'
'Tokitoh, Norihiro'
_publ_section_title
;
2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
;
_journal_coeditor_code IS4044
_journal_issue 9
_journal_name_full IUCrData
_journal_page_first x201299
_journal_paper_doi 10.1107/S2414314620012997
_journal_volume 5
_journal_year 2020
_chemical_formula_iupac 'C26 H48 N4 Si3'
_chemical_formula_moiety 'C26 H48 N4 Si3'
_chemical_formula_sum 'C26 H48 N4 Si3'
_chemical_formula_weight 500.95
_chemical_name_systematic
;
2,2-Bis[3,5-bis(dimethylamino)phenyl]-1,1,1,3,3,3-hexamethyltrisilane
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2ybc'
_space_group_name_H-M_alt 'P 1 21/c 1'
_symmetry_cell_setting monoclinic
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary dual
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL-2018/1
_cell_angle_alpha 90
_cell_angle_beta 97.371(2)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 20.6543(3)
_cell_length_b 8.36500(10)
_cell_length_c 17.5215(3)
_cell_measurement_reflns_used 24488
_cell_measurement_temperature 103(2)
_cell_measurement_theta_max 30.3000
_cell_measurement_theta_min 1.7700
_cell_volume 3002.23(8)
_computing_cell_refinement
;
CrysAlisPro (Rigaku OD, 2018)
;
_computing_data_collection
;
CrystalClear (Rigaku, 1999)
;
_computing_data_reduction
;
CrysAlisPro (Rigaku OD, 2018)
;
_computing_molecular_graphics
;
Yadokari-XG (Kabuto et al., 2009)
Mercury (Macrae et al., 2020)
;
_computing_publication_material
;
Yadokari-XG
;
_computing_structure_refinement
;
SHELXL2018/1 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 103(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type 'Rigaku Saturn'
_diffrn_measurement_method '\w scans'
_diffrn_radiation_monochromator graphite
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0293
_diffrn_reflns_av_unetI/netI 0.0176
_diffrn_reflns_limit_h_max 25
_diffrn_reflns_limit_h_min -25
_diffrn_reflns_limit_k_max 10
_diffrn_reflns_limit_k_min -10
_diffrn_reflns_limit_l_max 21
_diffrn_reflns_limit_l_min -21
_diffrn_reflns_number 33409
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 25.499
_diffrn_reflns_theta_min 1.988
_diffrn_source 'fine-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu 0.178
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_T_min 0.97740
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro (Rigaku OD, 2018)
;
_exptl_crystal_colour colorless
_exptl_crystal_density_diffrn 1.108
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description prism
_exptl_crystal_F_000 1096
_exptl_crystal_size_max 0.20
_exptl_crystal_size_mid 0.20
_exptl_crystal_size_min 0.20
_refine_diff_density_max 0.384
_refine_diff_density_min -0.182
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.038
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 312
_refine_ls_number_reflns 5581
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.038
_refine_ls_R_factor_all 0.0397
_refine_ls_R_factor_gt 0.0325
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0427P)^2^+1.4907P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0817
_refine_ls_wR_factor_ref 0.0863
_reflns_number_gt 4877
_reflns_number_total 5581
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file is4044sup1.cif
_cod_data_source_block I
_cod_original_sg_symbol_H-M 'P 21/c'
_cod_database_code 1559211
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.965
_shelx_estimated_absorpt_t_max 0.965
_shelx_hkl_file
;
-2 0 0 186.92 2.15
2 0 0 209.08 2.20
-2 0 0 214.26 2.32
2 0 0 208.36 2.25
-3 0 0 360.22 3.57
-3 0 0 360.71 3.71
-3 0 0 354.07 3.67
3 0 0 374.39 3.72
3 0 0 350.76 3.46
-4 0 0 102.94 2.32
4 0 0 107.51 2.33
-4 0 0 100.68 2.20
5 0 0 529.86 5.71
-5 0 0 521.66 5.50
-5 0 0 531.42 5.79
6 0 0 4.43 0.83
-6 0 0 5.55 0.95
-6 0 0 5.32 0.83
-7 0 0 0.78 0.73
-7 0 0 0.49 0.29
-7 0 0 -0.45 0.65
7 0 0 0.98 0.29
7 0 0 0.65 0.71
8 0 0 88.37 1.42
-8 0 0 81.22 2.99
-8 0 0 87.18 1.43
8 0 0 89.07 3.06
-8 0 0 85.34 2.88
-9 0 0 10.67 1.29
9 0 0 8.38 1.32
-9 0 0 9.44 1.34
9 0 0 7.80 0.53
-9 0 0 11.07 0.63
10 0 0 197.46 5.14
-10 0 0 210.90 2.33
10 0 0 193.68 2.21
-10 0 0 201.01 5.12
-10 0 0 195.65 4.85
11 0 0 -0.07 0.32
-11 0 0 -0.52 0.41
-11 0 0 1.17 1.05
-11 0 0 1.50 0.88
11 0 0 1.30 0.96
-12 0 0 239.04 2.47
-12 0 0 243.28 5.92
-12 0 0 242.77 6.22
12 0 0 241.99 6.20
-13 0 0 461.00 8.96
-13 0 0 435.23 8.27
-13 0 0 427.52 3.07
13 0 0 443.04 8.72
14 0 0 19.24 2.16
-14 0 0 17.48 2.00
-14 0 0 15.52 1.98
-15 0 0 15.77 2.04
15 0 0 14.33 2.04
-15 0 0 18.09 2.05
16 0 0 592.56 11.34
-16 0 0 565.79 10.75
-17 0 0 148.82 6.11
-17 0 0 150.58 5.84
17 0 0 141.94 5.91
-18 0 0 353.30 9.64
-18 0 0 354.77 9.03
18 0 0 364.08 9.74
19 0 0 449.55 11.10
-19 0 0 464.96 10.79
-19 0 0 463.61 11.34
20 0 0 167.98 7.17
-20 0 0 163.30 6.72
-20 0 0 155.69 6.92
-21 0 0 56.84 4.22
21 0 0 64.32 4.81
-21 0 0 57.00 4.62
-22 0 0 8.58 2.59
-22 0 0 13.23 2.58
22 0 0 9.06 2.19
23 0 0 2.96 2.07
-23 0 0 2.54 2.34
-23 0 0 4.24 2.67
-24 0 0 37.72 4.32
-24 0 0 35.22 4.05
24 0 0 37.44 4.45
-25 0 0 92.15 6.47
-25 0 0 88.35 6.04
25 0 0 93.31 6.53
-26 0 0 44.53 4.60
26 0 0 55.83 5.34
-26 0 0 55.29 5.62
27 0 0 5.37 3.46
-27 0 0 13.22 3.30
-27 0 0 3.67 3.23
-28 0 0 13.91 3.87
0 -1 0 0.40 0.34
0 1 0 0.26 0.36
0 1 0 1.21 0.35
0 -1 0 0.48 0.33
0 1 0 0.07 0.32
1 -1 0 2025.24 8.08
-1 -1 0 2016.10 7.89
-1 1 0 2051.29 8.09
1 -1 0 2028.22 8.18
1 1 0 2135.24 7.80
-1 1 0 2024.43 8.15
-1 -1 0 2053.24 8.01
-1 1 0 2101.67 8.31
1 1 0 2021.21 8.00
1 -1 0 2025.92 8.17
1 1 0 2022.75 7.48
1 1 0 2104.45 8.03
-2 -1 0 1149.19 6.30
-2 -1 0 1208.14 6.85
2 -1 0 1150.50 6.25
-2 1 0 1134.45 6.74
-2 -1 0 1178.19 6.53
2 1 0 1165.06 6.03
2 1 0 1143.96 6.26
-2 -1 0 1151.53 6.03
-2 1 0 1176.39 6.23
2 1 0 1128.14 6.47
-3 -1 0 790.03 4.98
3 1 0 808.61 5.15
3 1 0 816.59 5.91
-3 1 0 801.33 4.35
3 -1 0 822.36 6.43
-3 1 0 819.00 6.48
3 -1 0 832.75 4.41
3 -1 0 825.15 5.38
-3 1 0 819.87 5.39
3 1 0 817.13 6.04
-3 -1 0 804.32 6.43
-4 1 0 40.62 1.25
4 1 0 39.97 1.58
4 1 0 38.14 1.18
4 1 0 38.64 1.52
4 -1 0 41.44 1.26
-4 -1 0 38.42 1.64
4 -1 0 38.39 1.61
-4 -1 0 39.87 1.21
-4 1 0 38.42 1.64
4 -1 0 41.70 1.32
5 -1 0 74.34 1.73
-5 1 0 72.25 1.84
5 -1 0 74.31 2.40
-5 -1 0 69.99 2.38
-5 1 0 75.64 2.42
5 1 0 75.82 2.27
-5 -1 0 74.63 1.61
5 1 0 72.65 1.60
-5 -1 0 69.76 2.24
6 -1 0 151.66 2.48
-6 -1 0 141.19 3.50
-6 -1 0 146.93 3.58
6 -1 0 159.20 3.72
-6 -1 0 147.39 2.24
-6 1 0 147.17 2.90
-6 1 0 149.78 3.63
6 1 0 152.26 3.43
-7 -1 0 88.53 3.00
-7 -1 0 85.97 1.76
-7 -1 0 82.83 2.86
7 1 0 95.16 2.97
-7 -1 0 83.29 1.78
-7 1 0 88.56 2.50
-7 1 0 86.18 3.00
7 -1 0 86.86 1.93
7 -1 0 88.25 3.01
-8 1 0 220.04 4.22
-8 1 0 215.22 4.95
-8 -1 0 224.48 4.82
8 -1 0 230.66 5.09
-8 -1 0 220.21 2.81
-8 -1 0 216.48 2.84
8 -1 0 225.41 3.13
8 1 0 219.15 4.72
-8 -1 0 214.94 4.92
9 -1 0 2.84 1.13
9 -1 0 0.38 0.46
-9 1 0 1.48 0.89
-9 -1 0 0.47 0.85
-9 -1 0 0.18 0.43
9 1 0 -0.48 0.93
-9 -1 0 1.26 0.98
-9 1 0 1.90 0.97
-10 -1 0 16.67 1.75
10 1 0 15.07 1.62
10 -1 0 15.62 0.93
10 -1 0 12.82 1.57
-10 1 0 14.40 1.37
-10 -1 0 15.61 1.71
-10 -1 0 15.18 0.85
-10 1 0 15.30 1.67
11 -1 0 38.99 2.64
-11 -1 0 32.92 2.37
-11 -1 0 35.34 1.20
11 1 0 33.06 2.27
-11 -1 0 36.66 2.44
-11 1 0 40.05 2.61
-11 1 0 32.23 2.01
11 -1 0 35.19 1.32
-12 1 0 136.29 4.25
-12 -1 0 132.41 2.18
-12 -1 0 130.02 4.67
-12 -1 0 132.03 2.18
12 -1 0 127.14 4.65
12 -1 0 117.58 2.34
-12 1 0 130.79 4.74
-12 -1 0 139.29 4.77
12 1 0 141.34 4.73
13 -1 0 128.64 2.45
-13 -1 0 130.28 2.13
13 -1 0 134.90 5.07
-13 1 0 138.33 4.51
-13 1 0 138.53 5.09
13 1 0 136.74 4.90
-13 -1 0 131.62 4.90
-13 -1 0 134.36 2.13
-13 -1 0 136.44 4.99
-14 1 0 70.52 3.41
14 -1 0 71.74 1.83
-14 1 0 74.17 3.94
14 -1 0 66.28 3.71
-14 -1 0 71.96 1.51
14 1 0 70.44 3.75
-14 -1 0 72.19 3.81
-14 -1 0 70.41 3.84
15 1 0 195.99 6.39
-15 -1 0 185.02 6.22
-15 -1 0 190.38 6.32
-15 1 0 186.65 5.68
-15 1 0 185.50 6.34
15 -1 0 172.11 6.14
-16 -1 0 103.55 4.91
16 1 0 90.25 4.58
16 -1 0 92.41 4.80
-16 1 0 92.61 4.73
-16 -1 0 94.08 4.68
-16 1 0 94.68 4.32
-17 -1 0 142.44 5.90
17 1 0 145.32 5.93
-17 -1 0 144.39 5.92
-17 1 0 152.16 5.62
17 -1 0 130.05 5.80
-17 1 0 148.89 6.17
18 -1 0 -1.85 1.80
-18 -1 0 1.87 1.65
18 1 0 2.87 1.66
-18 1 0 4.75 1.96
-18 1 0 4.92 1.75
-18 -1 0 5.38 1.74
-19 -1 0 688.50 13.59
-19 1 0 695.55 13.95
19 1 0 661.11 13.43
-19 -1 0 665.60 13.67
19 -1 0 661.38 13.69
-19 1 0 693.02 12.64
-20 -1 0 79.64 5.09
20 -1 0 78.29 5.14
-20 1 0 71.79 4.98
20 1 0 73.45 5.03
-20 1 0 64.48 4.21
-20 -1 0 70.58 4.60
-21 -1 0 25.82 3.28
-21 1 0 22.50 3.21
21 1 0 19.76 3.14
-21 1 0 29.35 3.29
21 -1 0 30.51 3.51
-21 -1 0 25.88 3.43
-22 -1 0 66.74 5.03
22 -1 0 58.87 4.87
-22 -1 0 62.85 4.79
-22 1 0 63.18 4.97
-22 1 0 77.21 4.93
22 1 0 64.94 4.97
-23 -1 0 18.03 3.13
-23 1 0 22.44 3.21
-23 -1 0 15.92 3.25
23 1 0 12.73 2.83
-23 1 0 17.95 3.27
23 -1 0 16.30 3.37
-24 -1 0 9.46 2.79
24 1 0 6.48 2.53
24 -1 0 11.09 3.18
-24 -1 0 8.60 2.80
-24 1 0 9.09 3.00
-24 1 0 4.69 2.28
-25 1 0 4.61 2.38
-25 -1 0 5.01 2.48
25 -1 0 4.40 2.65
25 1 0 6.11 3.15
-25 1 0 6.18 3.21
-26 -1 0 21.73 3.88
26 1 0 19.73 3.78
-26 1 0 13.22 3.15
26 -1 0 26.39 4.27
26 1 0 21.75 3.90
-27 -1 0 -3.61 2.98
27 1 0 3.64 3.00
27 1 0 1.33 2.81
27 -1 0 1.04 2.92
-27 1 0 -0.52 3.09
-28 -1 0 -2.36 3.18
0 -2 0 1201.61 8.78
0 2 0 1232.49 8.34
0 -2 0 1211.45 6.56
0 2 0 1167.37 8.45
-1 2 0 2835.71 12.78
1 2 0 2782.61 12.33
1 2 0 2746.58 12.75
1 -2 0 2785.78 8.82
-1 2 0 2763.63 12.99
-1 -2 0 2671.25 13.00
1 -2 0 2763.70 13.28
-1 -2 0 2704.34 11.00
-2 2 0 1318.13 9.24
-2 -2 0 1326.30 9.21
2 2 0 1331.51 8.68
-2 2 0 1308.75 9.36
-2 -2 0 1326.79 8.53
2 -2 0 1338.26 9.44
2 -2 0 1326.93 5.52
-2 2 0 1317.67 5.48
2 2 0 1315.64 9.09
-3 2 0 3946.58 17.08
-3 -2 0 3947.06 15.97
-3 2 0 4030.06 9.57
-3 2 0 3988.93 17.07
3 -2 0 3967.44 16.44
-3 2 0 4033.11 9.61
-3 -2 0 3962.13 16.19
3 2 0 4020.76 16.42
4 -2 0 2468.55 13.02
4 2 0 2451.91 12.96
4 2 0 2407.48 13.35
-4 2 0 2404.62 8.22
-4 -2 0 2432.54 13.73
-4 2 0 2458.18 13.99
-4 -2 0 2403.07 12.42
-4 2 0 2430.76 14.24
4 -2 0 2452.53 8.39
5 2 0 187.69 3.85
-5 -2 0 176.38 3.37
5 -2 0 183.59 4.11
-5 2 0 177.87 4.10
5 -2 0 188.46 2.65
5 -2 0 179.15 3.56
-5 -2 0 176.58 4.03
5 2 0 186.07 3.95
-5 2 0 183.96 2.61
-6 -2 0 12.63 1.37
6 2 0 13.68 1.33
6 -2 0 10.70 1.24
-6 2 0 14.18 0.95
6 2 0 12.76 1.25
6 -2 0 14.24 1.17
-6 -2 0 13.13 1.08
-6 2 0 11.53 1.28
7 2 0 2836.88 16.94
7 -2 0 2833.73 17.77
-7 2 0 2773.10 17.70
-7 -2 0 2773.97 13.32
-7 2 0 2819.90 12.51
7 2 0 2780.79 16.51
-7 -2 0 2769.96 17.61
8 2 0 318.84 6.02
-8 2 0 323.66 4.69
-8 -2 0 316.50 6.46
8 -2 0 320.44 6.45
-8 2 0 328.88 6.50
8 -2 0 331.40 4.94
-8 -2 0 331.90 4.65
8 2 0 327.17 6.03
-9 2 0 11.37 1.12
9 -2 0 13.45 1.74
9 -2 0 11.26 1.13
-9 -2 0 11.08 1.06
-9 2 0 9.11 1.38
9 2 0 11.51 1.41
9 2 0 10.16 1.33
-9 -2 0 9.18 1.47
-10 -2 0 4.53 0.79
-10 2 0 3.95 1.11
10 -2 0 4.37 0.85
-10 2 0 4.85 0.95
10 2 0 2.48 1.03
10 -2 0 4.41 1.34
-10 -2 0 4.68 1.20
10 2 0 4.16 1.14
11 -2 0 131.23 3.22
11 -2 0 145.30 4.94
-11 2 0 135.95 4.79
11 2 0 138.28 4.55
-11 -2 0 142.98 3.08
-11 2 0 137.85 3.82
-11 -2 0 141.09 4.88
11 2 0 146.48 4.72
12 2 0 316.88 7.23
12 2 0 334.89 7.40
12 -2 0 328.71 5.07
12 -2 0 321.55 7.56
-12 2 0 306.91 7.51
-12 -2 0 304.06 7.43
-12 -2 0 324.07 4.56
-12 2 0 332.73 6.17
-13 2 0 2.99 1.03
-13 -2 0 0.64 1.11
13 -2 0 0.33 0.64
13 2 0 1.32 1.25
13 -2 0 2.32 1.34
13 2 0 -0.01 1.00
-13 -2 0 0.90 0.65
-13 2 0 3.40 1.35
-14 -2 0 304.99 8.03
14 2 0 312.72 7.79
14 -2 0 314.74 4.91
14 2 0 308.02 7.73
-14 2 0 313.16 8.17
-14 -2 0 308.48 4.33
-14 2 0 308.46 6.61
14 -2 0 299.82 7.95
-15 -2 0 155.27 6.07
15 -2 0 156.88 5.95
15 2 0 151.35 5.69
15 2 0 159.69 5.82
-15 2 0 155.92 5.99
-15 2 0 160.65 5.04
15 -2 0 151.67 3.41
16 -2 0 334.37 9.02
16 2 0 351.32 8.87
16 2 0 348.65 8.80
-16 -2 0 337.34 9.01
-16 2 0 337.49 7.57
-16 2 0 348.77 9.16
-17 -2 0 155.64 6.49
-17 2 0 171.36 5.67
17 2 0 158.17 6.23
17 -2 0 168.87 6.75
17 2 0 164.76 6.34
-17 2 0 164.86 6.64
18 2 0 199.93 7.24
-18 2 0 206.85 6.44
-18 2 0 216.40 7.78
18 2 0 222.06 7.69
-18 -2 0 222.01 7.86
18 -2 0 216.84 7.82
-19 -2 0 5.43 1.94
-19 2 0 2.06 1.46
19 -2 0 5.88 2.05
-19 2 0 3.52 1.80
19 2 0 4.02 1.82
19 2 0 6.24 1.97
-20 2 0 62.64 4.69
20 -2 0 71.17 5.06
-20 -2 0 63.73 4.73
20 2 0 66.75 4.83
-20 2 0 68.69 4.21
20 2 0 61.57 4.61
-21 -2 0 77.49 5.33
21 2 0 74.39 5.15
21 2 0 76.68 5.16
-21 2 0 76.76 4.54
21 -2 0 66.91 5.05
-21 2 0 72.82 5.24
22 2 0 21.72 3.33
-22 -2 0 23.26 3.31
22 -2 0 23.80 3.50
22 2 0 22.14 3.35
-22 2 0 27.93 3.87
-22 2 0 27.18 3.11
-23 2 0 66.80 5.51
23 2 0 64.76 5.19
23 -2 0 73.51 5.65
23 2 0 64.08 5.20
-23 -2 0 81.27 5.88
-24 2 0 -1.84 2.44
24 -2 0 0.04 2.32
24 2 0 3.94 2.64
-24 -2 0 -4.12 2.77
24 2 0 -0.80 2.08
25 2 0 11.15 2.97
25 2 0 10.23 3.03
-25 2 0 8.91 3.10
25 -2 0 10.29 3.01
-25 -2 0 5.69 2.88
-26 -2 0 47.91 5.19
-26 2 0 45.47 5.26
26 2 0 43.98 4.99
26 -2 0 41.15 4.98
26 2 0 40.42 4.91
-27 -2 0 15.15 3.97
-27 2 0 22.23 4.61
27 2 0 17.66 3.95
27 -2 0 12.68 4.02
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-9 -1 -9 159.16 4.08
9 1 9 157.80 5.74
9 -1 9 153.55 5.38
-9 1 -9 161.25 4.85
9 -1 9 157.47 5.47
-10 -1 -9 146.01 4.20
-10 -1 -9 141.41 5.81
-10 1 -9 143.48 5.67
10 -1 9 155.30 5.42
10 1 9 145.90 5.66
10 1 9 147.69 5.31
-10 1 -9 150.66 4.91
10 -1 9 154.04 5.63
11 -1 9 0.13 1.37
-11 -1 -9 0.88 1.43
-11 1 -9 0.14 1.40
-11 -1 -9 -1.30 1.07
11 1 9 -0.49 1.21
11 -1 9 1.26 1.28
-11 1 -9 0.99 1.16
11 1 9 -0.51 1.35
12 -1 9 7.34 1.86
-12 -1 -9 5.35 1.76
-12 1 -9 6.88 1.80
-12 -1 -9 7.69 1.52
12 1 9 6.60 1.55
12 -1 9 9.78 1.78
-12 1 -9 7.66 1.62
12 1 9 8.70 2.06
-13 -1 -9 34.03 3.30
-13 1 -9 27.87 2.96
-13 1 -9 32.09 2.92
13 1 9 29.55 2.71
-13 -1 -9 31.80 2.52
13 1 9 32.75 3.15
13 -1 9 28.57 3.07
13 -1 9 33.37 2.93
-14 -1 -9 39.81 3.67
14 1 9 38.42 3.08
-14 1 -9 37.31 3.47
-14 -1 -9 41.78 2.96
14 1 9 30.82 3.38
14 -1 9 37.00 3.00
-14 1 -9 39.52 3.21
14 -1 9 41.09 3.67
-15 -1 -9 147.20 6.84
-15 1 -9 161.18 6.90
15 -1 9 165.73 6.04
15 1 9 158.28 5.89
-15 -1 -9 174.11 5.98
15 1 9 166.80 7.15
-15 1 -9 156.31 6.03
15 -1 9 157.82 6.91
-16 -1 -9 169.26 7.46
-16 1 -9 201.17 7.87
-16 1 -9 192.82 6.96
16 1 9 183.63 6.39
-16 -1 -9 182.04 6.34
16 -1 9 183.96 6.36
16 1 9 193.11 7.87
16 -1 9 196.09 7.84
-17 -1 -9 62.94 4.91
-17 1 -9 72.38 4.96
-17 -1 -9 67.63 4.23
17 1 9 69.25 4.96
17 -1 9 60.07 4.63
-17 1 -9 63.37 4.35
-18 1 -9 74.46 4.84
-18 -1 -9 66.54 5.16
-18 1 -9 74.74 5.10
-18 -1 -9 66.55 4.34
18 1 9 67.52 5.14
18 -1 9 79.04 5.47
-19 -1 -9 33.62 4.00
-19 1 -9 29.23 3.66
19 1 9 39.54 4.36
19 -1 9 34.46 4.10
-19 1 -9 29.31 3.44
-20 1 -9 1.65 2.01
20 -1 9 1.10 2.42
-20 -1 -9 2.11 2.43
-20 1 -9 4.72 2.60
20 1 9 5.34 2.65
21 -1 9 0.89 2.38
-21 -1 -9 0.26 2.34
-21 1 -9 2.75 2.41
-21 1 -9 1.03 2.24
21 1 9 0.14 2.56
22 -1 9 20.19 3.76
-22 -1 -9 18.55 3.54
-22 1 -9 17.79 3.48
-22 1 -9 18.79 3.31
22 1 9 14.56 3.57
23 -1 9 8.72 3.42
-23 -1 -9 5.84 2.87
-23 1 -9 9.21 3.36
23 1 9 1.03 2.64
-23 1 -9 7.04 3.05
-24 -1 -9 1.06 2.83
-24 1 -9 -0.73 3.22
-25 1 -9 11.49 4.00
-27 -2 9 26.21 4.56
-26 -2 9 6.87 3.01
26 2 -9 12.42 3.86
-26 2 9 5.34 3.49
26 -2 -9 6.23 3.04
-25 -2 9 -1.16 2.81
25 2 -9 1.05 2.89
-25 2 9 3.24 2.65
25 -2 -9 3.79 2.80
-24 -2 9 1.03 2.60
24 2 -9 6.36 2.86
-24 2 9 2.75 2.63
24 -2 -9 6.19 2.70
23 -2 -9 -2.77 2.27
-23 -2 9 -2.16 2.45
23 2 -9 3.55 2.59
-23 2 9 -0.23 2.49
-22 -2 9 9.85 2.82
22 -2 -9 5.06 2.36
22 2 -9 6.28 2.61
-22 2 9 9.05 2.55
-21 -2 9 7.66 2.43
21 -2 -9 6.44 2.28
21 2 -9 3.92 2.26
-21 2 9 4.42 2.35
-20 -2 9 29.71 3.43
20 2 -9 32.61 3.93
-20 2 9 38.60 3.94
20 -2 -9 32.42 3.45
-19 2 9 0.67 1.79
-19 -2 9 5.47 2.12
19 2 -9 1.34 1.92
19 -2 -9 2.20 1.93
-18 -2 9 -0.19 1.76
18 2 -9 3.72 2.09
18 -2 -9 -0.83 1.69
-18 2 9 3.46 2.03
17 -2 -9 3.18 1.74
-17 2 9 4.02 1.55
-17 -2 9 3.72 1.76
17 2 -9 4.53 2.14
-17 2 9 4.41 1.65
-16 2 9 0.07 1.21
-16 -2 9 0.36 1.58
-16 2 9 1.02 1.61
16 -2 -9 2.09 1.57
16 2 -9 1.14 1.52
-15 2 9 108.23 4.17
-15 -2 9 116.63 5.56
15 2 -9 118.80 5.63
15 -2 -9 106.56 4.91
-15 2 9 106.10 5.08
-14 2 9 80.17 3.53
-14 -2 9 91.09 4.88
14 -2 -9 78.97 3.09
14 2 -9 79.32 4.57
-14 2 9 81.75 4.27
14 -2 -9 79.27 4.15
14 2 -9 79.49 3.14
-13 -2 9 189.69 6.72
-13 -2 9 179.11 4.33
13 2 -9 191.75 6.66
13 2 -9 178.35 4.29
13 -2 -9 178.63 5.96
13 -2 -9 173.65 4.59
-13 2 9 176.96 5.89
-13 2 9 185.14 5.11
-12 -2 9 19.74 2.42
12 -2 -9 19.22 2.10
12 2 -9 17.51 2.24
-12 2 9 18.86 2.09
-12 -2 9 13.27 1.43
12 2 -9 15.27 1.32
12 -2 -9 15.29 1.56
-12 2 9 14.78 1.62
-11 -2 9 45.86 3.31
11 2 -9 49.61 3.40
-11 2 9 49.38 2.92
-11 -2 9 46.83 2.45
11 2 -9 45.59 1.85
11 -2 -9 51.10 3.06
11 -2 -9 45.13 2.54
-11 2 9 46.13 2.50
-10 2 9 0.65 0.85
10 2 -9 0.21 0.54
-10 -2 9 1.36 1.14
-10 -2 9 1.91 0.93
10 2 -9 -0.47 1.14
-10 2 9 -0.58 0.97
-10 2 9 2.10 1.05
10 -2 -9 0.73 0.85
-9 -2 9 56.46 3.45
9 2 -9 61.85 3.41
-9 2 9 55.99 3.03
-9 2 9 61.70 2.96
-9 -2 9 58.79 2.80
9 2 -9 49.02 1.43
9 2 -9 53.88 1.45
9 -2 -9 59.26 2.88
-9 2 9 57.64 2.63
-8 -2 9 13.05 1.75
8 2 -9 13.55 1.73
8 -2 -9 12.99 1.39
-8 2 9 14.07 1.50
-8 2 9 14.35 1.70
-8 -2 9 12.24 1.45
8 -2 -9 14.72 1.62
7 2 -9 59.55 3.17
7 -2 -9 54.45 2.50
-7 2 9 57.06 2.51
-7 2 9 57.45 2.89
-7 -2 9 58.88 2.87
-7 -2 9 56.71 3.37
6 2 -9 128.85 4.42
-6 -2 9 129.49 4.22
6 -2 -9 138.44 3.93
-6 2 9 135.31 4.33
-6 2 9 132.25 3.47
-6 2 9 139.88 4.48
-6 -2 9 136.52 4.94
5 2 -9 38.76 2.41
-5 2 9 41.77 2.50
5 -2 -9 41.67 2.19
-5 2 9 43.85 1.89
-5 -2 9 42.60 2.56
-5 2 9 41.84 2.49
-5 -2 9 42.75 2.84
-4 -2 9 -0.37 1.05
4 2 -9 -0.55 0.87
-4 2 9 2.09 1.16
4 -2 -9 1.83 0.92
-4 2 9 1.13 0.66
-4 -2 9 0.34 0.84
-4 2 9 1.63 0.88
3 2 -9 32.98 2.23
3 -2 -9 33.87 2.08
-3 2 9 35.76 1.36
-3 2 9 38.85 2.55
-3 -2 9 35.76 2.42
-3 2 9 35.33 2.29
-3 -2 9 39.22 2.60
-2 -2 9 33.89 0.93
2 2 -9 30.55 2.07
2 -2 -9 32.45 2.12
2 -2 -9 31.44 1.01
2 2 -9 30.37 2.39
-2 2 9 27.57 2.27
-2 -2 9 29.46 2.25
2 -2 -9 27.66 0.98
-2 2 9 28.71 2.12
-1 2 9 4.56 1.14
1 2 -9 5.76 1.12
-1 -2 9 5.08 0.64
1 -2 -9 5.22 1.13
1 2 -9 6.90 1.45
-1 2 9 4.86 1.25
-1 -2 9 4.64 1.22
0 2 -9 32.92 2.16
0 2 9 37.13 2.42
0 -2 -9 31.34 2.14
0 2 -9 34.09 2.54
0 2 9 38.93 2.62
0 -2 9 33.06 1.44
0 -2 9 32.76 2.44
1 2 9 38.11 2.45
-1 -2 -9 37.42 2.46
-1 2 -9 39.02 2.68
1 2 9 37.33 2.64
1 -2 9 34.64 2.53
1 -2 9 38.90 1.71
-1 2 -9 40.77 2.30
2 2 9 25.03 2.06
-2 -2 -9 25.38 2.08
2 -2 9 22.79 2.12
-2 2 -9 27.52 2.29
2 2 9 24.03 2.23
2 -2 9 22.00 1.54
-2 2 -9 23.65 1.82
3 -2 9 4.09 0.99
-3 -2 -9 4.66 1.22
3 2 9 2.20 1.00
-3 2 -9 2.20 1.10
3 2 9 2.01 0.98
3 -2 9 2.49 0.90
-3 2 -9 0.97 0.83
4 2 9 90.61 3.90
-4 -2 -9 88.48 3.89
-4 2 -9 83.70 3.88
4 2 9 83.21 3.96
4 -2 9 91.70 4.05
-4 2 -9 87.41 3.41
4 -2 9 92.01 3.26
5 2 9 384.17 3.36
5 2 9 388.91 8.14
-5 -2 -9 384.67 8.19
-5 2 -9 384.84 8.33
5 2 9 337.56 7.73
5 -2 9 391.24 8.27
-5 2 -9 385.95 7.25
5 -2 9 382.57 6.95
6 -2 9 59.06 2.99
-6 -2 -9 59.89 3.51
6 2 9 59.79 3.37
6 2 9 59.20 1.71
-6 2 -9 58.16 3.39
6 2 9 64.17 3.58
6 -2 9 57.83 3.37
-6 2 -9 57.75 3.02
-7 -2 -9 184.93 6.09
7 2 9 171.75 5.81
-7 2 -9 172.57 5.83
7 2 9 173.97 3.28
7 2 9 178.79 5.79
7 -2 9 185.19 5.91
-7 2 -9 194.17 5.47
7 -2 9 176.93 5.26
-8 -2 -9 0.86 1.20
8 -2 9 -1.12 1.14
-8 2 -9 0.32 1.22
8 2 9 1.40 0.72
8 2 9 1.99 1.24
8 2 9 1.89 1.23
8 -2 9 0.63 1.11
-8 2 -9 0.93 1.02
9 2 9 1.63 1.24
-9 -2 -9 1.37 1.26
9 -2 9 2.76 1.44
-9 2 -9 -0.01 1.26
9 2 9 1.04 0.75
9 2 9 2.51 1.23
9 -2 9 -0.67 1.41
-9 2 -9 1.45 1.16
10 -2 9 198.92 6.35
-10 -2 -9 209.90 7.02
-10 2 -9 204.91 6.72
10 2 9 213.19 7.05
10 2 9 208.47 4.73
10 2 9 200.10 6.41
10 -2 9 211.70 6.59
-10 2 -9 202.21 6.17
11 -2 9 3.69 1.44
-11 -2 -9 1.14 1.38
11 -2 9 1.82 1.48
-11 2 -9 2.89 1.47
11 2 9 2.21 1.07
11 2 9 0.20 1.39
11 2 9 2.05 1.47
-11 2 -9 4.27 1.50
-12 -2 -9 5.99 1.88
12 -2 9 4.73 1.55
-12 2 -9 10.49 2.06
12 2 9 5.68 1.64
12 -2 9 4.85 1.52
12 2 9 3.43 1.61
-12 2 -9 7.92 1.79
-13 -2 -9 29.13 3.13
-13 2 -9 28.70 3.06
13 2 9 30.57 3.20
13 2 9 24.72 2.64
13 -2 9 31.12 2.83
-13 2 -9 28.39 2.72
13 -2 9 27.06 2.90
-14 -2 -9 4.11 2.02
14 -2 9 3.37 1.72
-14 2 -9 -0.52 1.76
14 2 9 0.01 1.35
14 -2 9 -1.06 1.43
-14 2 -9 0.09 1.57
14 2 9 0.65 1.87
-15 -2 -9 30.02 3.45
-15 2 -9 30.96 3.17
15 2 9 27.96 2.84
15 2 9 33.91 3.59
15 -2 9 27.54 2.79
-15 2 -9 29.20 3.04
15 -2 9 28.98 3.25
-16 -2 -9 4.81 2.30
16 -2 9 5.94 2.17
-16 2 -9 6.64 2.27
16 -2 9 4.84 1.65
-16 2 -9 3.20 1.71
16 2 9 -0.48 1.86
-17 -2 -9 1.44 2.07
17 -2 9 0.72 1.96
-17 2 -9 0.81 1.84
-17 2 -9 5.06 2.13
17 2 9 0.58 1.94
-18 -2 -9 21.24 3.41
18 -2 9 17.79 3.05
-18 2 -9 18.42 3.06
18 2 9 22.16 3.69
-18 2 -9 17.93 2.97
-19 -2 -9 74.58 5.60
-19 2 -9 68.31 5.10
19 2 9 68.11 5.40
-19 2 -9 67.19 4.99
19 -2 9 68.97 5.49
-20 -2 -9 35.87 4.54
20 -2 9 26.70 3.89
-20 2 -9 34.19 3.90
-20 2 -9 31.26 3.81
20 2 9 34.22 4.35
21 -2 9 8.81 3.13
-21 -2 -9 -0.50 2.56
-21 2 -9 1.80 2.55
-21 2 -9 2.50 2.71
21 2 9 3.11 2.69
22 -2 9 2.73 2.68
-22 -2 -9 1.89 2.65
-22 2 -9 0.73 2.52
-22 2 -9 1.58 2.73
22 2 9 -2.56 2.83
23 -2 9 2.13 2.87
-23 -2 -9 1.60 2.85
-23 2 -9 2.50 3.03
-23 2 -9 1.44 2.72
23 2 9 -2.26 3.12
-24 2 -9 -3.63 3.20
-24 2 -9 -0.97 3.03
-25 2 -9 1.92 3.23
-25 2 -9 -4.16 3.16
27 -3 -9 5.91 3.65
-26 3 9 9.52 3.61
26 -3 -9 11.51 3.52
-25 -3 9 -1.23 2.72
25 -3 -9 -0.38 2.69
25 3 -9 5.77 3.36
-25 3 9 -2.38 3.28
-24 -3 9 2.36 2.51
24 -3 -9 -0.11 2.70
-24 3 9 -1.24 2.93
24 3 -9 -2.37 3.22
-23 -3 9 32.39 4.16
23 3 -9 29.14 4.26
-23 3 9 32.53 4.12
23 -3 -9 31.68 3.99
-22 -3 9 -1.72 2.53
22 -3 -9 -2.97 2.56
22 3 -9 1.79 2.40
-22 3 9 0.82 2.50
-21 -3 9 3.55 2.39
21 3 -9 0.27 2.09
-21 3 9 4.68 2.57
21 -3 -9 0.96 2.16
-20 -3 9 -1.50 2.33
20 3 -9 0.24 2.24
-20 3 9 1.08 1.97
20 -3 -9 3.93 2.33
19 -3 -9 -1.13 1.85
-19 -3 9 0.11 2.02
-19 3 9 5.34 2.51
19 3 -9 3.72 2.19
-18 -3 9 38.08 3.93
18 -3 -9 31.32 3.40
18 3 -9 34.83 3.82
-18 3 9 30.62 3.36
-17 -3 9 23.58 3.18
17 3 -9 27.01 3.32
17 -3 -9 27.19 3.11
-17 3 9 24.66 3.07
-16 -3 9 56.77 4.28
16 3 -9 66.98 4.65
-16 3 9 62.41 4.23
16 -3 -9 67.11 4.43
-15 -3 9 9.67 2.16
15 3 -9 9.34 2.28
15 -3 -9 10.40 2.12
-15 3 9 11.39 2.22
-14 -3 9 180.38 7.07
14 -3 -9 179.20 6.56
14 3 -9 173.20 6.81
-14 3 9 184.18 6.36
14 -3 -9 178.56 5.09
-13 -3 9 4.55 1.71
13 3 -9 2.10 1.60
13 -3 -9 5.06 1.69
-13 3 9 4.59 1.48
-13 -3 9 3.73 1.13
13 -3 -9 2.17 1.11
-12 -3 9 30.52 3.03
12 3 -9 32.67 3.02
-12 3 9 33.70 2.78
-12 -3 9 31.80 2.17
12 -3 -9 30.41 2.34
12 -3 -9 32.91 2.85
-12 3 9 32.72 1.98
-11 -3 9 2.08 1.38
11 3 -9 1.79 1.50
11 -3 -9 0.85 0.84
-11 3 9 0.61 1.36
-11 3 9 2.63 1.28
11 -3 -9 0.52 1.09
-11 -3 9 0.97 0.97
10 3 -9 62.68 3.83
-10 3 9 66.22 3.36
10 -3 -9 69.20 2.65
-10 -3 9 75.05 3.35
-10 3 9 61.79 3.61
-10 -3 9 65.74 4.02
10 -3 -9 56.67 3.09
-9 -3 9 185.07 6.42
9 3 -9 188.76 6.26
9 -3 -9 192.24 4.28
-9 3 9 196.18 6.04
-9 -3 9 197.68 5.35
-9 3 9 186.10 5.14
9 -3 -9 184.95 5.47
-8 -3 9 46.57 3.29
8 3 -9 51.02 3.31
8 -3 -9 50.30 2.26
-8 3 9 52.72 3.17
-8 -3 9 48.87 2.76
8 -3 -9 46.82 2.88
-8 3 9 48.70 2.63
7 3 -9 41.90 2.98
-7 -3 9 42.73 2.71
7 -3 -9 43.92 2.07
-7 3 9 45.72 2.95
-7 3 9 44.82 2.32
7 -3 -9 43.87 2.78
-7 -3 9 46.01 3.22
6 3 -9 46.89 3.01
6 -3 -9 48.98 2.21
-6 -3 9 50.35 2.92
-6 3 9 44.80 2.19
-6 3 9 49.95 2.98
6 -3 -9 43.74 2.84
-6 -3 9 43.16 3.10
5 3 -9 19.32 1.99
-5 3 9 20.26 1.40
5 -3 -9 20.24 1.54
-5 -3 9 23.53 2.07
-5 3 9 21.78 2.04
5 -3 -9 21.43 2.09
-5 -3 9 18.83 2.10
4 3 -9 149.85 4.98
4 -3 -9 148.15 3.90
-4 3 9 153.04 3.32
-4 -3 9 160.07 5.14
-4 3 9 139.45 4.87
4 -3 -9 149.18 5.01
-4 -3 9 156.77 5.46
3 3 -9 6.44 1.43
3 -3 -9 6.31 1.13
-3 3 9 8.78 0.86
-3 -3 9 8.66 1.49
3 -3 -9 11.17 1.70
-3 3 9 7.73 1.46
-3 -3 9 7.77 1.49
2 3 -9 40.80 2.70
2 -3 -9 38.83 2.20
-2 -3 9 40.57 0.96
-2 -3 9 41.51 2.77
-2 3 9 43.24 1.42
-2 -3 9 37.29 0.93
-2 3 9 48.71 3.04
2 -3 -9 42.15 2.86
-2 -3 9 48.03 3.04
1 3 -9 12.85 1.65
-1 3 9 10.15 1.58
1 -3 -9 8.65 0.66
1 -3 -9 11.12 1.40
1 3 -9 10.89 1.67
-1 3 9 10.61 0.66
-1 -3 9 10.46 1.72
-1 -3 9 10.80 0.78
1 -3 -9 10.85 1.68
0 3 -9 16.59 1.91
0 -3 -9 13.28 1.55
0 3 -9 15.12 1.90
0 -3 9 13.43 1.83
0 -3 -9 15.81 1.98
0 -3 9 16.27 1.09
0 3 9 16.72 1.94
1 3 9 352.44 7.71
1 -3 9 360.31 5.09
-1 -3 -9 348.41 6.91
1 -3 9 349.51 7.96
-1 3 -9 364.87 8.03
-1 -3 -9 354.49 7.99
-1 3 -9 348.81 7.41
-2 3 -9 2.38 1.12
2 3 9 3.29 1.28
-2 -3 -9 3.47 1.20
-2 3 -9 3.28 1.15
2 -3 9 2.28 0.80
2 -3 9 3.27 1.21
3 3 9 141.17 5.16
3 -3 9 143.55 3.79
-3 -3 -9 143.88 4.81
3 3 9 130.57 5.12
-3 3 -9 141.51 5.08
3 -3 9 139.70 5.20
-3 3 -9 139.17 4.72
4 -3 9 19.10 1.70
4 3 9 16.94 2.02
-4 -3 -9 16.18 1.91
4 3 9 16.64 0.70
-4 3 -9 17.16 2.00
4 -3 9 23.62 2.31
4 3 9 16.35 2.15
-4 3 -9 18.16 1.95
4 3 9 18.20 0.70
5 3 9 11.17 0.77
5 -3 9 12.94 1.54
-5 -3 -9 9.28 1.73
5 3 9 10.88 1.76
-5 3 -9 11.75 1.80
5 3 9 8.33 1.61
5 -3 9 12.43 1.85
-5 3 -9 11.51 1.64
6 -3 9 333.26 6.88
6 3 9 326.97 4.08
6 3 9 334.45 8.27
-6 -3 -9 328.67 8.00
-6 3 -9 316.81 7.77
6 3 9 341.42 8.20
6 -3 9 337.77 8.19
-6 3 -9 332.64 7.68
7 -3 9 25.96 2.27
7 3 9 28.77 1.48
7 3 9 28.30 2.70
-7 -3 -9 27.58 2.63
-7 3 -9 31.15 2.69
7 -3 9 27.55 2.59
-7 3 -9 31.16 2.65
8 -3 9 397.13 9.13
8 -3 9 412.43 8.41
-8 -3 -9 419.22 9.62
8 3 9 429.01 5.77
8 3 9 423.58 9.75
-8 3 -9 415.47 9.20
-8 3 -9 436.68 9.11
9 -3 9 34.88 2.76
-9 -3 -9 34.97 3.10
9 3 9 37.48 2.01
9 3 9 38.22 3.14
-9 3 -9 39.31 3.03
9 -3 9 36.84 3.07
-9 3 -9 37.33 3.01
-9 -3 -9 37.44 2.93
-10 -3 -9 -0.36 1.44
-10 3 -9 -1.00 1.57
10 3 9 -0.42 0.95
10 -3 9 1.18 1.30
10 3 9 1.26 1.49
10 -3 9 -0.80 1.37
-10 3 -9 2.04 1.52
-10 -3 -9 2.99 1.63
-11 -3 -9 6.61 1.98
-11 3 -9 7.14 1.97
11 -3 9 9.07 1.97
11 3 9 7.84 2.23
11 -3 9 7.81 1.94
-11 3 -9 8.81 2.03
-11 -3 -9 8.28 1.88
-12 -3 -9 -1.56 1.57
-12 3 -9 2.57 1.58
12 3 9 0.65 1.53
12 -3 9 0.40 1.51
12 -3 9 0.72 1.40
-12 3 -9 2.65 1.60
-12 -3 -9 1.62 1.46
-13 -3 -9 9.96 2.41
-13 3 -9 8.06 2.03
13 -3 9 9.79 2.10
13 3 9 12.38 2.48
13 -3 9 10.36 2.14
-13 3 -9 12.44 2.39
-13 -3 -9 7.29 1.68
14 -3 9 38.57 3.60
-14 -3 -9 40.63 3.84
-14 3 -9 36.89 3.33
14 3 9 38.51 3.79
-14 3 -9 37.04 3.38
14 -3 9 37.44 3.45
-14 -3 -9 38.10 3.20
-15 -3 -9 12.65 2.67
-15 3 -9 16.01 2.54
15 -3 9 17.25 2.70
15 -3 9 17.48 2.59
15 3 9 15.83 3.03
-15 3 -9 16.67 2.67
-15 -3 -9 17.97 2.35
16 -3 9 30.27 3.43
-16 -3 -9 32.24 3.85
-16 3 -9 27.61 3.25
16 3 9 32.47 3.83
16 -3 9 32.85 3.13
-16 3 -9 26.80 3.25
-16 -3 -9 27.44 2.91
-17 -3 -9 31.34 3.91
-17 3 -9 31.44 3.55
17 3 9 28.23 3.82
-17 3 -9 26.72 3.43
17 -3 9 33.63 3.88
-18 -3 -9 9.57 3.10
-18 3 -9 11.46 2.59
18 -3 9 11.43 2.92
18 3 9 14.12 3.06
-18 3 -9 6.89 2.39
-19 -3 -9 11.64 2.91
-19 3 -9 18.45 2.93
19 -3 9 19.31 3.55
19 3 9 16.32 3.43
-19 3 -9 14.41 3.22
-20 -3 -9 -0.41 2.40
-20 3 -9 -1.79 2.40
20 -3 9 1.32 2.58
-20 3 -9 1.51 2.38
20 3 9 4.32 2.79
-21 -3 -9 22.69 3.86
-21 3 -9 19.10 3.50
21 -3 9 21.08 3.80
-21 3 -9 19.45 3.57
21 3 9 15.68 3.83
-22 -3 -9 7.42 3.30
-22 3 -9 6.21 2.95
22 -3 9 4.80 3.09
-22 3 -9 9.94 3.38
22 3 9 5.66 3.62
23 -3 9 -3.16 3.02
-23 3 -9 0.41 3.13
-24 3 -9 4.71 3.50
-25 -4 9 -5.52 3.61
25 -4 -9 3.50 3.20
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-24 -4 9 9.65 3.47
24 4 -9 11.20 3.52
24 -4 -9 10.87 3.25
-24 4 9 13.17 3.54
-23 -4 9 16.14 3.79
23 4 -9 18.65 3.77
23 -4 -9 16.69 3.86
-23 4 9 21.21 3.95
-22 -4 9 7.77 2.91
22 4 -9 -1.25 2.39
-22 4 9 6.96 2.72
22 -4 -9 2.14 2.60
-21 -4 9 6.47 2.79
21 4 -9 15.41 3.48
-21 4 9 13.64 3.23
21 -4 -9 10.48 3.10
-20 -4 9 17.73 3.33
20 -4 -9 11.12 2.78
20 4 -9 9.61 3.04
-20 4 9 11.76 2.88
-19 -4 9 4.82 2.43
19 4 -9 2.67 2.19
19 -4 -9 6.91 2.35
-19 4 9 3.79 2.03
-18 -4 9 8.75 2.76
18 4 -9 11.10 2.87
-18 4 9 5.41 2.07
18 -4 -9 8.81 2.47
-17 -4 9 22.30 3.30
17 4 -9 22.17 3.28
-17 4 9 21.82 3.00
17 -4 -9 21.23 3.21
-16 -4 9 13.67 2.74
16 4 -9 9.40 2.39
16 -4 -9 11.94 2.47
-16 4 9 9.88 2.10
-15 -4 9 1.07 1.86
15 4 -9 2.86 1.91
15 -4 -9 1.89 1.78
-15 4 9 -2.26 1.49
14 4 -9 7.24 2.10
14 -4 -9 5.92 1.95
-14 -4 9 6.20 2.22
-14 4 9 5.96 1.62
14 -4 -9 3.38 1.36
-13 -4 9 1.00 1.48
-13 -4 9 4.66 1.49
13 4 -9 2.66 1.73
13 -4 -9 3.86 1.75
13 -4 -9 4.09 1.37
-13 4 9 3.27 1.56
-12 -4 9 0.10 1.39
12 4 -9 -0.60 1.47
-12 4 9 -1.12 1.54
-12 4 9 -0.40 1.47
-12 -4 9 1.26 1.27
12 -4 -9 2.34 1.40
-11 -4 9 1.91 1.48
11 4 -9 4.18 1.90
-11 4 9 6.32 1.88
-11 4 9 3.11 1.44
-11 -4 9 1.43 1.20
11 -4 -9 3.30 1.41
-10 -4 9 133.71 5.93
10 4 -9 133.94 5.75
-10 4 9 138.91 5.73
-10 4 9 133.77 4.90
10 -4 -9 122.72 4.88
-10 -4 9 137.15 4.92
-9 -4 9 124.35 5.56
9 4 -9 119.71 5.31
9 -4 -9 120.81 4.85
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-9 -4 9 115.48 4.54
-8 -4 9 0.91 1.20
8 4 -9 2.57 1.61
8 -4 -9 0.63 0.68
-8 -4 9 1.27 1.12
-8 4 9 -1.58 1.14
-8 4 9 -0.01 1.19
8 -4 -9 1.47 1.19
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-7 4 9 57.67 3.59
7 4 -9 55.78 3.66
7 -4 -9 52.44 2.02
-7 4 9 53.36 2.74
-7 -4 9 50.96 3.17
7 -4 -9 50.08 3.26
-6 -4 9 10.22 1.97
6 4 -9 10.24 1.98
6 -4 -9 8.18 0.97
-6 -4 9 9.69 1.61
-6 4 9 8.49 1.25
-6 4 9 6.34 1.44
6 -4 -9 8.82 1.62
5 4 -9 113.07 4.88
5 -4 -9 105.20 3.00
-5 -4 9 106.07 4.59
-5 4 9 102.59 4.58
-5 4 9 114.43 3.50
5 -4 -9 101.98 4.52
-5 -4 9 105.06 4.81
-4 -4 9 35.56 2.78
4 4 -9 36.94 2.87
4 -4 -9 33.69 1.86
-4 4 9 34.91 1.89
-4 4 9 36.81 2.97
4 -4 -9 32.52 2.69
-4 -4 9 38.48 3.04
-3 -4 9 2.97 1.35
3 4 -9 5.08 1.49
3 -4 -9 3.96 0.99
-3 -4 9 1.67 1.19
-3 4 9 2.25 0.79
-3 -4 9 3.20 0.44
3 -4 -9 3.41 1.34
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2 4 -9 157.35 5.58
-2 -4 9 159.58 5.62
-2 -4 9 160.41 2.60
2 -4 -9 159.83 4.25
-2 4 9 160.35 3.39
-2 4 9 163.71 5.70
2 -4 -9 172.60 5.90
-2 -4 9 154.59 5.58
1 4 -9 67.69 3.69
1 -4 -9 72.84 3.05
-1 -4 9 76.03 2.11
-1 4 9 76.74 2.20
-1 -4 9 74.48 4.00
-1 4 9 73.34 3.94
1 -4 -9 78.63 4.12
0 4 -9 32.31 2.65
0 -4 -9 39.23 2.44
0 -4 9 42.69 1.84
0 4 -9 35.46 2.82
0 -4 9 39.68 2.99
0 4 9 37.33 1.49
0 -4 -9 41.43 3.13
0 4 9 37.01 2.90
-1 -4 -9 37.71 2.50
1 -4 9 42.76 1.98
-1 4 -9 41.10 3.03
1 -4 9 43.09 3.24
1 4 9 40.76 1.47
-1 -4 -9 36.12 2.98
1 4 9 42.71 3.06
-1 4 -9 43.13 3.03
2 4 9 124.53 5.13
-2 -4 -9 123.59 4.44
2 -4 9 126.51 3.56
-2 -4 -9 120.10 5.14
-2 4 -9 123.51 4.94
2 -4 9 122.12 5.16
2 4 9 127.75 2.46
-2 4 -9 130.59 5.08
-3 4 -9 5.78 1.46
3 4 9 5.21 1.53
-3 -4 -9 5.17 1.42
-3 4 -9 8.04 1.72
3 -4 9 6.88 1.65
3 4 9 6.43 0.75
-3 -4 -9 6.23 1.63
3 -4 9 5.05 1.05
4 4 9 142.94 5.67
-4 -4 -9 140.11 5.02
4 -4 9 145.30 4.34
-4 4 -9 146.26 5.35
4 -4 9 136.69 5.50
-4 4 -9 147.99 5.55
-4 -4 -9 134.80 5.49
4 4 9 155.90 2.89
-5 -4 -9 3.25 1.29
5 4 9 4.76 1.59
5 -4 9 3.75 1.46
-5 4 -9 2.15 1.25
5 -4 9 3.07 1.20
-5 -4 -9 4.30 1.50
-5 4 -9 2.67 1.38
6 4 9 121.25 5.47
-6 -4 -9 122.29 5.00
6 -4 9 125.37 4.43
-6 4 -9 132.14 5.21
6 -4 9 120.96 5.32
-6 4 -9 121.13 5.11
-6 -4 -9 110.43 5.05
-7 -4 -9 -0.05 1.22
7 4 9 0.21 1.34
-7 4 -9 1.30 1.31
7 -4 9 0.16 1.32
7 -4 9 0.06 1.18
-7 4 -9 0.84 1.31
-7 -4 -9 1.23 1.29
-8 -4 -9 0.85 1.38
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-8 4 -9 1.56 1.30
8 -4 9 2.01 1.51
8 -4 9 -1.11 1.36
-8 4 -9 0.48 1.30
-8 -4 -9 1.57 1.37
9 -4 9 25.14 2.77
9 4 9 19.59 2.59
-9 -4 -9 21.79 2.59
9 -4 9 24.46 2.62
-9 4 -9 21.90 2.51
-9 4 -9 28.25 2.88
-9 -4 -9 26.14 2.73
-10 -4 -9 152.60 6.32
10 -4 9 161.94 5.99
10 4 9 162.00 6.71
-10 4 -9 159.67 6.04
10 -4 9 147.67 6.06
-10 4 -9 148.01 6.17
-10 -4 -9 156.55 6.17
-11 -4 -9 90.87 5.12
11 -4 9 81.00 4.49
11 4 9 91.40 5.28
-11 4 -9 95.66 4.82
11 -4 9 86.06 4.83
-11 4 -9 86.90 4.90
-11 -4 -9 95.92 5.08
-12 -4 -9 1.26 1.62
-12 4 -9 1.49 1.61
12 4 9 0.10 1.74
12 -4 9 4.11 2.02
12 -4 9 0.69 1.48
-12 4 -9 0.27 1.64
-12 -4 -9 1.30 1.51
13 -4 9 36.24 3.48
-13 -4 -9 43.32 3.95
13 4 9 47.62 4.13
-13 4 -9 27.33 2.96
13 -4 9 34.42 3.22
-13 4 -9 31.18 3.29
-13 -4 -9 36.83 3.37
-14 -4 -9 10.93 2.69
-14 4 -9 11.08 2.33
14 -4 9 13.82 2.53
14 4 9 12.43 2.72
14 -4 9 5.93 1.84
-14 4 -9 8.02 2.13
-14 -4 -9 13.19 2.46
15 -4 9 3.81 2.23
-15 -4 -9 2.63 2.08
-15 4 -9 1.95 1.99
15 4 9 -0.30 2.26
15 -4 9 2.85 1.81
-15 4 -9 1.95 1.76
-16 -4 -9 1.91 2.15
-16 4 -9 -0.12 1.96
16 4 9 2.56 2.06
16 -4 9 -0.38 1.98
16 -4 9 -0.59 1.74
-16 4 -9 0.81 1.95
-16 -4 -9 2.32 1.93
-17 -4 -9 10.08 2.83
-17 4 -9 14.25 3.01
17 -4 9 14.11 2.85
17 4 9 8.90 2.95
-17 4 -9 11.82 2.82
-18 -4 -9 8.57 2.89
-18 4 -9 9.62 2.67
18 -4 9 7.63 2.53
18 4 9 6.23 2.88
-18 4 -9 3.68 2.46
-19 -4 -9 -0.91 2.65
-19 4 -9 -0.24 2.21
19 -4 9 3.66 2.63
19 4 9 4.99 2.91
-19 4 -9 0.14 2.45
20 4 9 -0.71 2.80
-20 -4 -9 6.25 3.10
20 -4 9 0.40 2.66
-20 4 -9 -0.51 2.53
-21 -4 -9 1.05 3.03
21 -4 9 2.51 2.93
21 4 9 -0.40 2.88
-21 4 -9 4.68 3.30
22 -4 9 4.84 3.26
-22 4 -9 2.29 3.08
-23 4 -9 66.28 6.38
24 -5 -9 2.45 3.44
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-23 -5 9 2.81 2.78
23 5 -9 0.36 2.90
-23 5 9 1.85 2.85
23 -5 -9 7.18 3.31
-22 -5 9 11.50 3.51
22 5 -9 13.59 3.75
-22 5 9 11.29 3.12
22 -5 -9 2.93 2.67
-21 -5 9 65.12 5.82
21 -5 -9 49.07 5.13
21 5 -9 54.83 5.41
-21 5 9 51.60 5.08
-20 -5 9 3.09 2.64
20 5 -9 4.28 2.37
20 -5 -9 3.94 2.75
-20 5 9 3.48 2.45
-19 -5 9 12.35 3.37
19 5 -9 16.80 3.38
19 -5 -9 14.00 3.13
-19 5 9 17.78 3.20
-18 -5 9 5.34 2.75
18 -5 -9 -2.34 2.37
18 5 -9 -1.13 2.05
-18 5 9 0.86 2.01
-17 -5 9 41.20 4.33
17 5 -9 44.45 4.37
17 -5 -9 47.15 4.52
-17 5 9 45.90 4.07
-16 -5 9 -0.27 2.12
16 5 -9 -2.29 2.43
-16 5 9 1.32 1.87
16 -5 -9 1.02 1.86
-15 -5 9 11.94 2.68
15 5 -9 12.87 2.65
15 -5 -9 13.03 2.77
-15 5 9 15.37 2.44
-14 -5 9 9.38 2.67
14 -5 -9 6.04 2.26
14 5 -9 4.07 2.06
-14 5 9 4.51 1.95
14 -5 -9 2.25 1.56
-13 -5 9 22.75 3.13
13 5 -9 20.30 2.91
-13 -5 9 26.58 2.55
13 -5 -9 24.20 2.66
13 -5 -9 22.20 3.04
-13 5 9 20.24 2.51
-12 -5 9 45.72 4.00
12 5 -9 46.30 3.95
-12 5 9 54.43 4.18
-12 5 9 42.55 3.33
-12 -5 9 51.35 3.40
12 -5 -9 40.94 3.22
-11 -5 9 77.89 4.97
11 5 -9 81.48 5.02
-11 5 9 93.98 5.20
-11 5 9 84.77 4.30
-11 -5 9 84.29 4.27
11 -5 -9 82.62 4.44
-10 -5 9 22.32 2.79
10 5 -9 19.56 2.78
-10 5 9 20.89 2.77
-10 5 9 21.04 2.46
-10 -5 9 19.39 2.26
10 -5 -9 24.90 2.78
-9 -5 9 413.38 10.46
9 5 -9 424.88 10.61
-9 5 9 443.38 10.75
-9 5 9 415.39 8.60
-9 -5 9 414.70 9.28
9 -5 -9 419.43 9.62
-8 -5 9 -0.46 1.48
8 5 -9 -1.39 1.47
-8 -5 9 -0.82 1.42
-8 5 9 -2.22 1.56
-8 5 9 1.05 1.30
8 -5 -9 0.34 1.33
7 5 -9 52.67 3.85
-7 5 9 51.73 3.79
-7 -5 9 45.32 3.36
-7 5 9 49.41 2.92
7 -5 -9 47.22 3.49
-7 -5 9 41.38 3.41
6 5 -9 59.80 3.99
-6 5 9 58.82 3.85
-6 -5 9 56.41 3.65
-6 5 9 60.11 3.02
6 -5 -9 63.31 3.98
-6 -5 9 51.98 3.74
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5 5 -9 1.74 1.42
-5 -5 9 -0.95 1.26
-5 5 9 -0.22 0.95
-5 5 9 -1.27 1.52
5 -5 -9 -0.53 1.31
4 5 -9 29.77 2.94
-4 -5 9 30.12 2.90
-4 5 9 28.60 2.01
-4 5 9 28.29 2.84
4 -5 -9 30.18 2.80
-4 -5 9 30.66 2.87
3 5 -9 18.55 2.39
3 -5 -9 18.31 1.51
-3 -5 9 21.59 2.53
-3 5 9 19.58 1.67
-3 5 9 16.35 2.25
3 -5 -9 16.32 2.29
-3 -5 9 22.55 2.55
2 5 -9 162.48 6.20
2 -5 -9 150.94 4.08
-2 -5 9 140.78 5.76
-2 5 9 151.81 3.92
-2 5 9 151.41 5.94
2 -5 -9 159.10 6.12
-2 -5 9 153.01 5.86
1 5 -9 74.87 4.32
1 -5 -9 81.79 3.23
-1 -5 9 71.23 4.23
-1 5 9 75.01 2.71
-1 5 9 78.25 4.48
1 -5 -9 73.54 4.24
-1 -5 9 76.80 2.54
-1 -5 9 74.44 4.16
0 -5 -9 60.91 2.95
0 5 -9 56.83 3.55
0 -5 9 55.32 3.77
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0 -5 9 56.36 2.37
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0 -5 -9 65.63 4.09
0 5 -9 65.67 4.03
-1 -5 -9 67.44 3.23
-1 5 -9 66.70 3.82
1 -5 9 66.48 4.17
1 -5 9 70.37 2.80
1 5 9 73.99 2.57
-1 -5 -9 66.57 4.15
1 5 9 75.00 4.41
-1 5 -9 63.74 4.03
-2 -5 -9 26.51 2.22
-2 5 -9 25.75 2.50
2 -5 9 29.10 2.92
2 -5 9 29.17 2.07
-2 -5 -9 29.01 2.89
2 5 9 37.36 3.18
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-3 -5 -9 28.79 2.44
-3 5 -9 31.17 2.77
3 -5 9 31.72 2.23
3 -5 9 31.18 3.05
-3 -5 -9 28.87 2.94
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3 5 9 36.41 3.23
4 5 9 59.24 4.12
-4 -5 -9 51.50 3.24
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4 -5 9 56.08 3.02
4 -5 9 53.07 3.82
-4 -5 -9 56.49 3.86
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5 5 9 56.05 4.00
-5 -5 -9 53.46 3.40
-5 5 -9 60.44 3.67
-5 5 -9 56.30 3.91
5 -5 9 54.91 3.02
5 -5 9 48.85 3.73
-5 -5 -9 57.57 3.94
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6 -5 9 19.41 2.14
6 -5 9 19.83 2.61
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-6 -5 -9 14.57 2.32
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7 -5 9 7.51 2.00
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7 -5 9 10.47 2.09
-7 -5 -9 6.80 1.81
-7 5 -9 4.57 1.72
8 -5 9 13.57 2.08
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8 5 9 10.85 2.16
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8 -5 9 15.35 2.63
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-8 -5 -9 15.51 2.42
9 5 9 269.53 8.86
-9 -5 -9 266.18 8.43
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9 -5 9 261.30 7.55
9 -5 9 267.35 8.61
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-9 -5 -9 275.13 8.48
10 5 9 57.06 4.52
-10 -5 -9 59.62 4.36
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10 -5 9 60.90 4.04
10 -5 9 50.28 3.97
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-10 -5 -9 53.92 4.02
-11 -5 -9 -1.26 2.19
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-11 5 -9 2.94 1.83
11 -5 9 1.79 1.73
-11 5 -9 2.24 1.69
11 -5 9 -0.53 1.60
-11 -5 -9 5.79 1.92
-12 -5 -9 33.75 3.61
12 5 9 36.77 3.92
12 -5 9 30.73 3.27
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12 -5 9 32.30 3.35
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-12 -5 -9 35.72 3.41
-13 -5 -9 1.86 1.92
-13 5 -9 -1.92 2.08
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13 -5 9 1.45 2.15
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-13 -5 -9 0.92 1.73
-14 -5 -9 13.55 2.87
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14 5 9 11.19 2.76
14 -5 9 10.87 2.46
14 -5 9 17.65 2.89
-14 5 -9 13.58 2.91
-14 -5 -9 14.90 2.81
-15 -5 -9 38.36 4.19
15 -5 9 32.90 3.87
15 5 9 27.79 3.82
-15 5 -9 31.81 3.41
15 -5 9 30.58 3.50
-15 5 -9 31.65 3.97
-15 -5 -9 38.02 3.68
-16 -5 -9 12.08 3.18
16 5 9 10.10 2.85
16 -5 9 2.65 2.02
-16 5 -9 9.31 2.86
16 -5 9 7.38 2.38
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17 -5 9 -3.16 2.36
-17 5 -9 2.15 2.48
-18 -5 -9 3.90 2.57
18 5 9 8.08 3.07
18 -5 9 -1.36 2.82
-18 5 -9 4.49 2.61
-19 -5 -9 2.31 2.99
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19 -5 9 3.74 2.80
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20 5 9 16.21 3.96
20 -5 9 12.77 3.40
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21 -5 9 0.41 3.15
-21 5 -9 7.25 3.50
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22 -6 -9 42.64 5.24
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-21 -6 9 3.04 2.80
21 6 -9 6.23 3.12
21 -6 -9 3.07 2.79
-21 6 9 8.65 3.33
20 -6 -9 2.13 2.89
-20 -6 9 0.42 2.58
20 6 -9 2.67 2.96
-20 6 9 -0.23 2.54
-19 -6 9 3.56 2.84
19 -6 -9 5.99 2.69
19 6 -9 1.23 2.62
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-18 -6 9 5.84 2.86
18 6 -9 2.97 2.47
18 -6 -9 2.14 2.38
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-17 -6 9 24.45 3.84
17 6 -9 30.60 4.14
-17 6 9 24.28 3.37
17 -6 -9 23.29 3.68
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11 -2 -10 289.09 6.43
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-10 2 10 128.27 4.60
-10 -2 10 140.39 4.40
10 -2 -10 137.28 4.55
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9 2 -10 212.81 6.28
9 -2 -10 210.59 5.26
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-9 2 10 217.61 5.83
-9 -2 10 191.73 5.17
9 -2 -10 201.10 5.52
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8 2 -10 117.97 4.61
8 -2 -10 120.39 3.97
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7 2 -10 150.82 5.03
7 -2 -10 145.32 4.31
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6 2 -10 136.18 4.60
6 -2 -10 141.57 4.25
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5 -2 -10 172.45 4.67
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-5 2 10 179.15 5.01
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4 -2 -10 125.90 4.07
4 -2 -10 121.75 2.74
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3 -2 -10 120.82 2.30
3 -2 -10 118.90 4.02
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2 -2 -10 535.55 3.49
2 -2 -10 535.52 8.48
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1 -2 -10 41.76 2.59
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15 1 -11 15.27 2.43
-15 1 11 16.12 2.13
-14 -1 11 72.98 4.33
14 -1 -11 82.69 3.89
14 1 -11 82.69 4.62
-14 1 11 83.32 4.14
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-13 -1 11 1.60 1.33
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13 -1 -11 -0.29 1.23
-13 -1 11 0.06 0.93
13 -1 -11 1.06 1.03
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12 -1 -11 23.61 2.35
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-12 -1 11 25.10 2.01
12 -1 -11 23.50 2.12
-12 1 11 22.71 2.31
-12 -1 11 23.74 2.52
11 -1 -11 155.16 4.79
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11 -1 -11 145.22 5.04
-11 1 11 144.21 4.56
-11 -1 11 148.46 4.52
-11 1 11 137.79 4.90
-11 -1 11 140.32 5.49
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-10 -1 11 34.18 2.38
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-10 1 11 30.29 2.42
-10 -1 11 29.64 2.71
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9 -1 -11 120.85 4.14
-9 1 11 122.07 3.99
-9 1 11 121.46 4.31
-9 -1 11 121.60 4.22
9 1 -11 122.02 2.71
-9 1 11 132.00 4.67
-9 -1 11 124.92 5.09
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8 -1 -11 58.31 2.82
8 -1 -11 59.31 3.20
-8 1 11 65.60 3.21
-8 1 11 62.02 2.86
-8 -1 11 61.54 3.11
-8 -1 11 67.61 3.79
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7 -1 -11 134.58 3.90
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-7 -1 11 135.70 4.56
-7 1 11 133.45 4.56
-7 -1 11 143.78 5.30
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6 -1 -11 161.06 3.98
-6 -1 11 155.05 4.97
6 -1 -11 168.33 5.24
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-6 1 11 161.65 4.37
-6 -1 11 148.63 5.30
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5 -1 -11 17.48 1.88
-5 -1 11 15.61 0.94
-5 -1 11 16.96 1.91
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-5 1 11 17.36 1.64
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-4 -1 11 52.58 1.61
-4 -1 11 56.54 3.16
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3 -1 -11 11.64 0.92
3 -1 -11 11.36 1.58
3 1 -11 11.82 1.79
-3 1 11 8.37 1.58
-3 -1 11 10.06 1.61
-3 -1 11 12.30 1.01
-3 1 11 12.99 1.42
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2 -1 -11 247.77 3.23
-2 1 11 253.23 6.67
2 -1 -11 262.65 6.55
2 1 -11 253.06 6.85
-2 -1 11 256.80 6.70
-2 1 11 265.72 5.62
-2 -1 11 261.37 4.03
-1 1 11 135.30 4.14
1 1 -11 123.84 3.65
-1 -1 11 132.60 3.13
1 -1 -11 131.90 4.77
1 1 -11 123.37 4.89
-1 1 11 133.85 5.04
-1 -1 11 124.61 4.77
1 -1 -11 116.78 1.78
1 -1 -11 129.56 1.84
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0 -1 11 23.91 1.56
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0 1 -11 23.83 2.28
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-1 1 -11 2.86 0.83
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-1 -1 -11 2.81 1.14
-1 1 -11 2.77 1.24
1 -1 11 2.81 0.95
1 1 11 2.78 1.28
1 -1 11 1.70 1.15
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-2 -1 -11 10.39 1.71
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2 -1 11 10.60 1.68
2 -1 11 8.40 1.11
-2 1 -11 11.36 1.25
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-3 1 -11 5.51 1.42
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3 -1 11 5.01 1.43
3 -1 11 2.31 0.86
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-4 -1 -11 33.34 0.94
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-5 -1 -11 91.29 4.43
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-5 -1 -11 84.81 1.88
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-6 -1 -11 30.37 2.77
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-7 -1 -11 9.96 1.01
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-8 -1 -11 4.03 0.93
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-8 1 -11 6.07 1.33
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-9 -1 -11 79.30 4.57
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9 -1 11 78.23 4.16
-9 1 -11 79.18 3.58
-10 -1 -11 71.73 4.51
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10 -1 11 77.58 4.29
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-11 -1 -11 4.24 1.74
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-11 1 -11 3.29 1.55
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-12 -1 -11 49.92 4.10
-12 1 -11 60.78 4.35
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-12 1 -11 55.49 3.41
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-13 -1 -11 160.21 7.04
-13 1 -11 155.30 6.80
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-13 1 -11 147.82 5.57
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-14 -1 -11 6.56 2.29
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-15 -1 -11 -0.43 1.78
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-17 1 -11 25.72 3.10
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-18 -1 -11 16.68 3.17
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-19 -1 -11 16.00 3.55
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-20 -1 -11 31.27 4.27
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-21 -1 -11 -1.91 2.91
-21 1 -11 2.53 2.87
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-22 -1 -11 18.78 4.19
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22 -1 11 18.28 4.14
-23 1 -11 27.54 4.45
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-25 -2 11 4.39 3.08
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-23 -2 11 -1.29 2.51
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-23 2 11 4.22 2.80
-22 -2 11 11.22 3.17
22 -2 -11 8.16 2.68
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21 -2 -11 -3.40 2.40
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20 -2 -11 1.74 1.84
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19 -2 -11 11.17 2.48
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-17 -2 11 59.89 4.53
17 -2 -11 60.71 4.22
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-16 -2 11 51.46 4.21
16 -2 -11 60.79 3.93
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-15 2 11 53.39 3.73
15 -2 -11 49.64 3.50
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-12 -2 11 11.12 1.67
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-11 -2 11 93.99 3.79
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-8 2 11 0.56 0.91
-8 2 11 0.42 1.02
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-7 -2 11 97.03 4.05
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-5 -2 11 -0.43 1.03
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3 -2 -11 0.92 0.50
3 -2 -11 1.38 1.07
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-3 -2 11 -0.43 0.99
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2 -2 -11 47.99 2.85
-2 -2 11 52.63 3.24
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-2 2 11 52.01 3.30
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-1 -2 11 20.34 1.15
1 -2 -11 21.81 2.14
1 2 -11 21.25 2.30
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0 -2 -11 48.97 2.97
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1 -2 11 21.55 2.24
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2 -2 11 23.16 1.77
2 -2 11 26.67 2.50
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4 -2 11 15.94 1.66
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5 -2 11 72.30 3.28
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9 -2 11 25.81 2.60
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-10 -2 -11 11.72 2.05
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19 -3 -11 40.78 4.11
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14 -3 -11 44.86 2.96
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8 -3 -11 76.55 3.90
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7 -3 -11 16.65 2.15
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6 -3 -11 16.84 1.95
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-5 -3 11 103.47 4.51
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5 -3 -11 96.03 4.42
-5 -3 11 94.45 4.72
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4 -3 -11 85.93 3.51
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2 -2 -15 52.18 3.70
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1 -2 -15 6.39 1.78
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-5 -5 -15 8.54 2.48
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-9 -4 21 3.73 2.78
9 -4 -21 5.84 3.19
8 4 -21 15.49 3.61
-8 -4 21 18.46 3.82
8 -4 -21 23.99 4.08
7 4 -21 12.30 3.77
-7 -4 21 8.73 3.07
7 -4 -21 14.58 3.88
6 4 -21 8.59 3.70
-6 -4 21 9.34 3.21
6 -4 -21 5.42 2.96
5 4 -21 29.17 4.42
-5 -4 21 28.04 4.17
5 -4 -21 35.62 5.28
4 4 -21 66.83 6.01
-4 -4 21 58.11 5.51
4 -4 -21 63.29 5.86
3 4 -21 22.50 4.16
-3 -4 21 23.73 4.07
3 -4 -21 25.44 4.15
2 4 -21 15.35 3.68
-2 -4 21 8.78 2.87
2 -4 -21 16.23 3.71
1 4 -21 42.59 5.24
-1 -4 21 32.90 4.54
1 -4 -21 38.28 5.04
0 4 -21 3.37 3.04
0 -4 21 3.85 3.26
0 -4 -21 -0.59 2.87
-1 4 -21 4.44 3.01
1 -4 21 6.53 3.39
-1 -4 -21 -3.36 3.15
-2 -4 -21 0.77 2.94
-2 4 -21 2.52 2.76
2 -4 21 -0.15 2.66
-2 -4 -21 -0.33 2.86
-3 -4 -21 25.83 4.48
-3 4 -21 27.96 4.46
3 -4 21 24.75 4.17
-3 -4 -21 22.63 3.97
-4 -4 -21 10.44 3.68
-4 4 -21 10.22 3.77
5 4 21 21.66 3.80
-5 -4 -21 25.91 4.41
-6 -4 -21 53.56 5.63
6 4 21 57.56 5.53
7 4 21 3.06 3.32
-7 -4 -21 8.61 3.62
8 4 21 0.64 3.15
11 -5 -21 12.24 3.91
-10 -5 21 3.50 3.26
10 -5 -21 9.03 3.62
-9 -5 21 9.95 3.60
9 -5 -21 10.86 3.56
-8 -5 21 14.41 3.79
8 -5 -21 23.73 4.47
-7 -5 21 2.00 2.95
7 -5 -21 5.25 3.25
-6 -5 21 7.94 3.50
6 -5 -21 4.30 3.39
-5 -5 21 39.89 5.09
5 -5 -21 40.25 5.01
-4 -5 21 1.94 2.84
4 -5 -21 3.51 3.80
-3 -5 21 29.65 4.27
3 -5 -21 34.06 4.83
-2 -5 21 0.96 2.75
2 -5 -21 -1.26 3.16
1 5 21 8.06 3.29
2 5 21 -2.69 2.93
3 5 21 -0.05 2.88
4 5 21 5.00 3.43
5 5 21 97.26 7.13
-2 6 21 3.52 3.38
-1 6 21 8.67 3.61
0 6 21 10.92 3.82
14 0 -22 3.38 3.23
13 0 -22 68.14 6.02
12 0 -22 6.62 3.07
11 0 -22 249.92 10.42
10 0 -22 -0.04 2.81
-10 0 22 -1.20 2.54
9 0 -22 225.68 9.83
-9 0 22 218.13 9.37
8 0 -22 23.27 4.03
-8 0 22 29.74 4.20
7 0 -22 16.98 3.55
-7 0 22 13.69 3.37
6 0 -22 5.16 2.79
-6 0 22 7.37 2.86
5 0 -22 11.14 3.16
-5 0 22 10.61 3.30
4 0 -22 7.56 3.16
-4 0 22 7.16 3.02
3 0 -22 15.64 3.29
-3 0 22 25.12 4.15
2 0 -22 1.35 2.66
-2 0 22 2.69 2.54
1 0 -22 12.61 3.37
-1 0 22 13.81 3.39
0 0 -22 161.27 8.61
0 0 22 141.73 8.35
-1 0 -22 88.61 6.86
1 0 22 60.97 5.74
-2 0 -22 -0.48 2.59
2 0 22 -0.24 2.68
-3 0 -22 8.30 3.26
3 0 22 9.10 3.40
-4 0 -22 0.47 2.67
4 0 22 1.48 2.83
-5 0 -22 98.31 7.29
5 0 22 92.50 7.25
-6 0 -22 9.42 3.62
6 0 22 2.13 3.11
16 1 -22 1.93 3.49
15 1 -22 39.02 5.23
14 1 -22 26.16 4.62
13 1 -22 2.94 3.06
12 1 -22 46.92 5.37
11 -1 -22 10.41 3.36
11 1 -22 12.56 3.56
10 -1 -22 40.36 4.86
10 1 -22 33.14 4.40
-10 -1 22 31.39 4.32
-10 1 22 31.61 4.05
9 -1 -22 9.76 3.44
9 1 -22 7.38 2.84
-9 1 22 7.92 3.07
-9 -1 22 11.78 3.26
8 -1 -22 63.17 5.55
8 1 -22 75.88 6.18
-8 1 22 69.28 5.74
-8 -1 22 62.92 5.55
7 -1 -22 6.27 2.87
7 1 -22 10.77 3.75
-7 1 22 7.93 3.03
-7 -1 22 2.56 2.66
6 -1 -22 -1.53 2.53
6 1 -22 -1.14 2.68
-6 1 22 -5.31 2.88
-6 -1 22 4.29 2.99
5 -1 -22 5.05 2.94
5 1 -22 4.68 2.85
-5 1 22 3.94 2.85
-5 -1 22 1.48 2.76
4 -1 -22 0.30 2.72
4 1 -22 2.12 2.71
-4 1 22 7.04 2.87
-4 -1 22 4.64 3.08
3 -1 -22 1.43 2.81
3 1 -22 -2.13 2.86
-3 1 22 0.59 2.43
-3 -1 22 1.52 2.75
2 -1 -22 6.85 3.08
2 1 -22 7.10 3.01
-2 1 22 6.30 3.01
-2 -1 22 4.64 2.87
1 -1 -22 50.52 5.12
1 1 -22 53.10 5.33
-1 1 22 49.12 5.17
-1 -1 22 58.85 5.53
0 -1 -22 1.05 2.65
0 1 -22 -0.07 2.61
0 1 22 1.23 2.53
0 -1 22 1.74 3.02
-1 -1 -22 38.62 4.68
-1 1 -22 38.10 4.89
1 1 22 38.68 4.81
1 -1 22 33.83 4.55
-2 -1 -22 19.77 4.24
-2 1 -22 24.84 4.47
2 1 22 15.09 3.72
2 -1 22 18.12 3.76
-3 -1 -22 45.90 5.18
-3 1 -22 50.87 5.53
3 1 22 53.50 5.63
3 -1 22 53.55 5.59
-4 -1 -22 12.63 3.73
-4 1 -22 7.43 3.05
4 1 22 6.68 3.17
4 -1 22 6.07 3.16
-5 -1 -22 7.57 3.53
-5 1 -22 9.90 4.01
5 1 22 5.54 3.21
5 -1 22 10.96 4.07
-6 -1 -22 53.92 5.68
13 2 -22 57.24 6.08
12 2 -22 34.87 5.00
11 2 -22 3.93 3.59
10 2 -22 30.33 4.61
-10 2 22 28.73 4.14
-10 -2 22 22.69 3.89
9 2 -22 6.00 3.18
-9 2 22 -1.13 2.61
-9 -2 22 1.83 2.59
8 2 -22 84.53 6.66
-8 2 22 84.15 6.23
-8 -2 22 83.56 6.30
7 2 -22 31.22 4.73
7 -2 -22 32.60 4.17
-7 2 22 40.02 4.75
-7 -2 22 42.45 4.72
6 -2 -22 31.90 4.31
6 2 -22 30.89 4.34
-6 2 22 33.98 4.49
-6 -2 22 38.04 4.63
5 -2 -22 14.38 3.42
5 2 -22 14.03 3.38
-5 2 22 15.92 3.60
-5 -2 22 23.72 4.04
4 -2 -22 23.84 3.86
4 2 -22 22.33 4.09
-4 2 22 21.42 3.68
-4 -2 22 14.76 3.60
3 -2 -22 3.13 2.77
3 2 -22 4.33 2.80
-3 2 22 3.03 2.54
-3 -2 22 2.90 2.60
2 -2 -22 1.75 2.68
2 2 -22 -3.50 3.27
-2 2 22 -0.57 2.71
-2 -2 22 2.07 2.57
1 -2 -22 0.39 2.46
1 2 -22 -4.15 3.23
-1 2 22 -2.50 2.82
-1 -2 22 -2.38 2.78
0 -2 -22 0.51 2.84
0 2 -22 5.13 3.15
0 2 22 -3.52 3.11
0 -2 22 -0.92 2.57
-1 2 -22 32.66 4.84
-1 -2 -22 24.86 4.26
1 2 22 33.96 4.83
1 -2 22 28.75 4.23
-2 -2 -22 115.57 7.35
-2 2 -22 127.78 8.07
2 2 22 112.47 7.66
2 -2 22 110.50 7.60
-3 -2 -22 58.73 5.61
-3 2 -22 51.79 5.63
3 2 22 56.04 5.94
3 -2 22 46.71 5.41
-4 -2 -22 185.50 9.53
-4 2 -22 201.94 10.26
4 2 22 198.04 9.87
4 -2 22 172.87 9.49
-5 -2 -22 15.13 3.86
-6 -2 -22 8.27 3.44
11 -3 -22 -2.00 2.97
10 3 -22 54.11 5.85
-10 -3 22 56.68 5.49
10 -3 -22 58.14 5.59
9 3 -22 14.69 4.06
-9 -3 22 10.60 3.50
9 -3 -22 11.84 3.36
8 3 -22 12.41 3.67
-8 -3 22 7.95 3.24
8 -3 -22 4.01 2.91
7 3 -22 0.77 2.97
-7 -3 22 1.02 2.83
7 -3 -22 -3.05 2.78
6 3 -22 29.00 4.77
-6 -3 22 25.31 4.21
5 3 -22 -2.14 2.89
-5 3 22 0.78 2.82
-5 -3 22 -1.88 2.65
4 3 -22 6.14 3.10
-4 3 22 14.22 3.79
-4 -3 22 15.61 3.78
3 3 -22 31.80 4.84
-3 3 22 31.27 4.42
-3 -3 22 21.90 3.90
2 -3 -22 0.88 2.68
2 3 -22 -4.88 3.13
-2 3 22 6.71 3.29
-2 -3 22 0.78 2.64
1 -3 -22 1.28 2.68
1 3 -22 -1.95 3.18
-1 3 22 -1.27 3.04
-1 -3 22 1.99 2.94
0 -3 -22 3.97 2.74
0 3 -22 -4.08 3.17
0 3 22 -0.96 2.82
0 -3 22 3.04 3.10
-1 -3 -22 31.34 4.43
-1 3 -22 31.34 4.52
1 3 22 45.77 5.14
1 -3 22 41.47 5.13
-2 -3 -22 -0.37 3.10
-2 3 -22 2.71 3.20
2 3 22 4.84 3.20
2 -3 22 -2.87 3.16
-3 -3 -22 20.08 3.97
-4 -3 -22 142.76 8.30
-5 -3 -22 65.50 6.12
-10 -4 22 -0.72 2.87
10 -4 -22 9.35 3.94
-9 -4 22 39.01 4.98
9 -4 -22 37.37 4.98
-8 -4 22 42.36 5.11
8 -4 -22 36.95 5.06
-7 -4 22 20.49 3.75
7 -4 -22 24.06 4.43
-6 -4 22 2.85 3.27
6 -4 -22 1.21 2.90
-5 -4 22 16.01 3.87
5 -4 -22 17.29 3.98
-4 -4 22 6.42 3.33
4 -4 -22 13.32 3.73
-3 -4 22 4.43 3.16
3 -4 -22 6.49 3.30
-2 -4 22 81.26 6.63
-3 -4 -22 20.27 4.00
-4 -4 -22 4.61 3.64
-5 -4 -22 62.54 6.32
13 0 -23 6.56 3.68
12 0 -23 -1.65 3.12
11 0 -23 -3.26 3.41
10 0 -23 -0.02 3.09
-10 0 23 2.19 2.90
9 0 -23 0.09 2.86
-9 0 23 -4.78 3.14
8 0 -23 -1.92 3.14
-8 0 23 -0.47 2.80
7 0 -23 2.22 3.02
-7 0 23 -1.67 2.81
6 0 -23 -2.55 2.97
-6 0 23 0.37 2.63
5 0 -23 0.24 2.86
-5 0 23 -5.33 3.10
4 0 -23 0.19 3.03
-4 0 23 1.39 2.62
3 0 -23 -1.24 3.01
-3 0 23 3.49 2.87
2 0 -23 -0.42 2.75
-2 0 23 -6.10 3.35
1 0 -23 -1.29 2.97
-1 0 23 4.84 3.15
0 0 -23 -0.13 2.82
0 0 23 1.54 2.84
-1 0 -23 3.09 3.08
1 0 23 6.19 3.23
-2 0 -23 2.69 3.23
12 1 -23 0.23 3.15
11 1 -23 2.11 3.24
10 1 -23 2.32 3.37
-10 1 23 2.70 3.10
-10 -1 23 3.09 3.22
9 -1 -23 -4.19 3.16
9 1 -23 -3.08 3.01
-9 1 23 4.71 3.22
-9 -1 23 3.24 3.16
8 -1 -23 1.26 3.15
8 1 -23 -0.65 3.01
-8 1 23 4.08 3.13
-8 -1 23 -0.02 2.77
7 -1 -23 28.14 4.45
7 1 -23 23.03 4.01
-7 -1 23 34.85 4.84
-7 1 23 28.41 4.49
6 -1 -23 -2.48 3.09
6 1 -23 5.95 3.78
-6 1 23 0.73 2.77
-6 -1 23 -1.94 3.04
5 -1 -23 9.55 3.49
5 1 -23 15.04 4.02
-5 1 23 8.97 3.09
4 -1 -23 4.08 3.16
4 1 -23 -0.20 2.86
-4 1 23 3.86 2.75
-4 -1 23 1.01 2.72
3 -1 -23 7.34 3.26
3 1 -23 6.81 3.30
-3 1 23 7.03 3.21
-3 -1 23 7.73 3.08
2 -1 -23 14.33 3.74
2 1 -23 16.30 4.01
-2 -1 23 8.48 3.42
1 -1 -23 0.17 2.87
1 1 -23 10.28 3.75
-1 1 23 5.44 3.12
-1 -1 23 5.47 3.27
0 -1 -23 5.82 3.50
0 1 -23 12.81 3.95
0 1 23 4.73 3.10
0 -1 23 5.71 3.17
-1 -1 -23 38.91 4.93
-1 1 -23 33.42 5.03
1 1 23 42.53 5.36
-2 -1 -23 1.53 2.93
-3 -1 -23 -0.82 2.98
-10 2 23 2.85 3.17
-10 -2 23 0.92 3.08
-9 2 23 7.63 3.08
-9 -2 23 9.15 3.50
8 2 -23 7.46 3.73
-8 2 23 2.91 2.94
-8 -2 23 -0.88 2.89
7 2 -23 -2.36 2.88
-7 2 23 0.57 3.01
-7 -2 23 -1.10 2.96
6 2 -23 3.28 3.05
-6 2 23 13.77 3.78
-6 -2 23 5.63 3.21
5 -2 -23 8.93 3.51
5 2 -23 4.10 3.17
-5 2 23 9.97 3.75
-5 -2 23 6.40 3.17
4 -2 -23 9.20 3.43
4 2 -23 10.81 3.74
-4 2 23 14.07 3.69
-4 -2 23 14.85 3.89
3 -2 -23 9.36 3.46
3 2 -23 5.14 3.35
-3 2 23 1.78 2.92
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2 -2 -23 -1.52 2.96
2 2 -23 2.10 3.33
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1 -2 -23 12.55 3.73
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0 -2 -23 1.23 3.37
-1 -2 -23 -0.17 3.00
-2 -2 -23 22.53 4.05
-3 -2 -23 9.85 3.65
10 -3 -23 21.46 4.10
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9 -3 -23 -5.20 3.53
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8 -3 -23 1.30 3.08
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7 -3 -23 5.99 3.47
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6 -3 -23 2.18 3.27
-5 -3 23 28.63 4.63
1 -3 -23 7.81 3.17
0 -3 -23 34.69 4.81
-1 -3 -23 0.88 2.99
-2 -3 -23 2.73 3.76
-3 -3 -23 4.96 3.41
9 0 -24 22.55 4.72
-9 0 24 10.56 3.80
8 0 -24 18.69 4.42
-8 0 24 26.64 4.42
7 0 -24 32.79 5.07
-7 0 24 36.41 4.94
6 0 -24 5.86 3.28
-6 0 24 9.16 3.77
5 0 -24 6.44 3.75
4 0 -24 29.33 4.63
-10 1 24 1.81 3.24
-9 1 24 22.07 4.11
-9 -1 24 26.21 4.62
8 -1 -24 5.16 3.36
-8 1 24 4.82 3.36
-8 -1 24 3.73 3.03
7 -1 -24 13.50 4.03
-7 1 24 11.44 3.84
-7 -1 24 9.04 3.59
6 -1 -24 16.71 4.11
5 -1 -24 18.05 4.17
4 -1 -24 8.33 3.51
3 -1 -24 43.77 5.24
2 -1 -24 75.51 6.75
4 -2 -24 10.84 4.00
3 -2 -24 71.16 6.34
2 -2 -24 20.41 4.35
1 -2 -24 121.36 8.10
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)'
;
_shelx_hkl_checksum 95407
_shelx_res_file
;
TITL ki_a.res in P2(1)/c
ki_a.res
created by SHELXL-2018/1 at 15:18:03 on 15-Sep-2020
REM Yadorkari-X generated
CELL 0.71073 20.6543 8.3650 17.5215 90.0000 97.3710 90.0000
ZERR 4.0 0.0003 0.0001 0.0003 0.0000 0.0020 0.0000
LATT 1
SYMM -X, 1/2+Y, 1/2-Z
REM SPGR P21/c monoclinic
SFAC Si C H N
UNIT 12 104 192 16
SIZE 0.20 0.20 0.20
TEMP -170.0
L.S. 10
FMAP 2
PLAN -20
ACTA
CONF
LIST 4
WPDB -1
BOND $H
OMIT -10.000000 51.000000
WGHT 0.042700 1.490700
FVAR 0.35849
SI1 1 0.304251 0.263588 0.405775 11.00000 0.01653 0.02160 =
0.01500 0.00142 0.00150 -0.00027
SI2 1 0.250810 0.239227 0.279663 11.00000 0.01451 0.01279 =
0.01429 0.00109 0.00278 0.00137
SI3 1 0.207126 -0.018642 0.260006 11.00000 0.01862 0.01526 =
0.02462 -0.00247 0.00459 -0.00180
C1 2 0.321871 0.477370 0.432812 11.00000 0.03231 0.02919 =
0.03443 -0.01077 -0.00263 -0.00071
AFIX 137
H1 3 0.342782 0.529781 0.392332 11.00000 -1.50000
H2 3 0.351105 0.481717 0.481460 11.00000 -1.50000
H3 3 0.280943 0.532430 0.438785 11.00000 -1.50000
AFIX 0
C2 2 0.257453 0.172719 0.479827 11.00000 0.02621 0.05228 =
0.02299 0.01446 0.00385 0.00007
AFIX 137
H4 3 0.282593 0.183946 0.530913 11.00000 -1.50000
H5 3 0.249861 0.059114 0.468290 11.00000 -1.50000
H6 3 0.215449 0.227615 0.478973 11.00000 -1.50000
AFIX 0
C3 2 0.384136 0.157023 0.406270 11.00000 0.02158 0.03644 =
0.02412 0.00084 -0.00223 0.00644
AFIX 137
H7 3 0.409142 0.164627 0.457597 11.00000 -1.50000
H8 3 0.408976 0.206399 0.368441 11.00000 -1.50000
H9 3 0.376058 0.044327 0.393031 11.00000 -1.50000
AFIX 0
C4 2 0.178314 0.377866 0.261245 11.00000 0.01609 0.01210 =
0.01908 0.00033 0.00245 -0.00067
C5 2 0.152551 0.422322 0.186636 11.00000 0.01847 0.01608 =
0.01606 -0.00111 0.00553 0.00025
AFIX 43
H10 3 0.174097 0.391031 0.144264 11.00000 -1.20000
AFIX 0
C6 2 0.094892 0.513144 0.173950 11.00000 0.01744 0.01415 =
0.01735 0.00157 0.00165 -0.00125
C7 2 0.064162 0.559490 0.237370 11.00000 0.01609 0.01605 =
0.02053 0.00096 0.00308 0.00259
AFIX 43
H11 3 0.025674 0.622675 0.229263 11.00000 -1.20000
AFIX 0
C8 2 0.089131 0.514398 0.312443 11.00000 0.02131 0.01793 =
0.01836 -0.00054 0.00575 0.00180
C9 2 0.146866 0.424164 0.323411 11.00000 0.02150 0.01868 =
0.01421 0.00197 0.00217 0.00246
AFIX 43
H12 3 0.164780 0.394190 0.374040 11.00000 -1.20000
AFIX 0
N1 4 0.067465 0.554130 0.099548 11.00000 0.02106 0.02628 =
0.01597 0.00312 0.00226 0.00634
C10 2 0.108034 0.541219 0.037715 11.00000 0.02690 0.03130 =
0.01603 0.00213 0.00362 0.00487
AFIX 137
H13 3 0.120610 0.429339 0.031923 11.00000 -1.50000
H14 3 0.147335 0.606661 0.050088 11.00000 -1.50000
H15 3 0.083461 0.578969 -0.010478 11.00000 -1.50000
AFIX 0
C11 2 0.015747 0.671934 0.089584 11.00000 0.02078 0.03237 =
0.02211 0.00820 0.00169 0.00578
AFIX 137
H16 3 0.032046 0.773793 0.112060 11.00000 -1.50000
H17 3 -0.020940 0.635214 0.115365 11.00000 -1.50000
H18 3 0.001115 0.686560 0.034579 11.00000 -1.50000
AFIX 0
N2 4 0.057448 0.558618 0.374631 11.00000 0.03181 0.04397 =
0.01665 0.00123 0.00631 0.02086
C12 2 0.000444 0.658508 0.363424 11.00000 0.01974 0.02871 =
0.02339 -0.00348 0.00758 0.00366
AFIX 137
H19 3 -0.032513 0.609127 0.325453 11.00000 -1.50000
H20 3 0.012242 0.763704 0.344817 11.00000 -1.50000
H21 3 -0.017287 0.670837 0.412357 11.00000 -1.50000
AFIX 0
C13 2 0.088887 0.529950 0.451759 11.00000 0.02856 0.03077 =
0.01743 -0.00148 0.00648 0.00458
AFIX 137
H22 3 0.131207 0.584552 0.459169 11.00000 -1.50000
H23 3 0.095511 0.414821 0.459639 11.00000 -1.50000
H24 3 0.061305 0.570997 0.488874 11.00000 -1.50000
AFIX 0
C14 2 0.314250 0.284887 0.214104 11.00000 0.01619 0.01699 =
0.01201 -0.00090 0.00092 -0.00030
C15 2 0.358723 0.166509 0.199098 11.00000 0.02052 0.01391 =
0.01685 0.00116 0.00294 0.00029
AFIX 43
H25 3 0.353827 0.060958 0.217532 11.00000 -1.20000
AFIX 0
C16 2 0.410350 0.201378 0.157296 11.00000 0.01653 0.01863 =
0.01505 -0.00275 -0.00013 0.00193
C17 2 0.416191 0.356851 0.129253 11.00000 0.01465 0.02100 =
0.01450 -0.00089 0.00255 -0.00175
AFIX 43
H26 3 0.450754 0.381126 0.100236 11.00000 -1.20000
AFIX 0
C18 2 0.371913 0.477500 0.143229 11.00000 0.01789 0.01604 =
0.01426 -0.00095 0.00002 -0.00196
C19 2 0.321218 0.439368 0.186358 11.00000 0.01673 0.01498 =
0.01618 -0.00126 0.00201 0.00174
AFIX 43
H27 3 0.291203 0.520064 0.196795 11.00000 -1.20000
AFIX 0
N3 4 0.454543 0.079080 0.142899 11.00000 0.02090 0.02157 =
0.02349 0.00105 0.00806 0.00627
N4 4 0.379922 0.634826 0.118444 11.00000 0.02407 0.01674 =
0.02629 0.00406 0.00914 -0.00101
C20 2 0.476934 -0.023040 0.208562 11.00000 0.04001 0.03739 =
0.02981 0.00388 0.00423 0.02308
AFIX 137
H28 3 0.439219 -0.073086 0.227626 11.00000 -1.50000
H29 3 0.500814 0.041608 0.249542 11.00000 -1.50000
H30 3 0.505801 -0.106202 0.192602 11.00000 -1.50000
AFIX 0
C21 2 0.507220 0.122954 0.099492 11.00000 0.03173 0.03109 =
0.05151 0.00351 0.02284 0.01055
AFIX 137
H31 3 0.536208 0.199436 0.129305 11.00000 -1.50000
H32 3 0.488974 0.171889 0.050608 11.00000 -1.50000
H33 3 0.532024 0.027143 0.089272 11.00000 -1.50000
AFIX 0
C22 2 0.430187 0.668465 0.070038 11.00000 0.03356 0.02124 =
0.04243 0.00520 0.01759 -0.00475
AFIX 137
H34 3 0.419445 0.614702 0.020332 11.00000 -1.50000
H35 3 0.472326 0.629362 0.095198 11.00000 -1.50000
H36 3 0.432763 0.784068 0.061867 11.00000 -1.50000
AFIX 0
C23 2 0.322647 0.733925 0.100426 11.00000 0.03556 0.02190 =
0.05432 0.01566 0.01896 0.00695
AFIX 137
H37 3 0.294343 0.722489 0.140908 11.00000 -1.50000
H38 3 0.298835 0.700536 0.051007 11.00000 -1.50000
H39 3 0.335941 0.845920 0.097152 11.00000 -1.50000
AFIX 0
C24 2 0.180189 -0.050812 0.154714 11.00000 0.02740 0.03354 =
0.03148 -0.01304 0.00118 0.00032
AFIX 137
H40 3 0.146709 0.028127 0.136380 11.00000 -1.50000
H41 3 0.162104 -0.158697 0.146642 11.00000 -1.50000
H42 3 0.217687 -0.038664 0.126137 11.00000 -1.50000
AFIX 0
C25 2 0.133992 -0.028864 0.313122 11.00000 0.02779 0.03354 =
0.04049 -0.00693 0.01287 -0.01186
AFIX 137
H43 3 0.148027 -0.019567 0.368531 11.00000 -1.50000
H44 3 0.111634 -0.131258 0.302292 11.00000 -1.50000
H45 3 0.104091 0.058891 0.296305 11.00000 -1.50000
AFIX 0
C26 2 0.264370 -0.181320 0.299571 11.00000 0.03762 0.01689 =
0.04745 0.00391 0.00557 0.00129
AFIX 137
H46 3 0.242957 -0.285333 0.290345 11.00000 -1.50000
H47 3 0.276191 -0.165481 0.355026 11.00000 -1.50000
H48 3 0.303862 -0.178120 0.274009 11.00000 -1.50000
AFIX 0
HKLF 4 1 1 0 0 0 1 0 0 0 1
REM ki_a.res in P2(1)/c
REM R1 = 0.0325 for 4877 Fo > 4sig(Fo) and 0.0397 for all 5581 data
REM 312 parameters refined using 0 restraints
END
WGHT 0.0427 1.4907
REM Highest difference peak 0.384, deepest hole -0.182, 1-sigma level 0.044
Q1 1 0.1690 -0.0223 0.2921 11.00000 0.05 0.38
Q2 1 0.2136 0.3251 0.2689 11.00000 0.05 0.38
Q3 1 0.2901 0.2670 0.2470 11.00000 0.05 0.37
Q4 1 0.2783 0.2513 0.3415 11.00000 0.05 0.34
Q5 1 0.1910 -0.0298 0.2037 11.00000 0.05 0.31
Q6 1 0.0703 0.5194 0.3439 11.00000 0.05 0.29
Q7 1 0.2408 -0.1021 0.2807 11.00000 0.05 0.29
Q8 1 0.2784 0.2350 0.4481 11.00000 0.05 0.28
Q9 1 0.3500 0.2178 0.4075 11.00000 0.05 0.28
Q10 1 0.3811 0.1819 0.1672 11.00000 0.05 0.27
Q11 1 0.3192 0.3870 0.4066 11.00000 0.05 0.26
Q12 1 0.4173 0.2786 0.1532 11.00000 0.05 0.26
Q13 1 0.2339 0.1048 0.2700 11.00000 0.05 0.26
Q14 1 0.1113 0.4528 0.3166 11.00000 0.05 0.26
Q15 1 0.3441 0.2461 0.2159 11.00000 0.05 0.25
Q16 1 0.0734 0.5067 0.2025 11.00000 0.05 0.25
Q17 1 0.4294 0.1393 0.1506 11.00000 0.05 0.25
Q18 1 0.0880 0.5519 0.1407 11.00000 0.05 0.25
Q19 1 0.2803 0.6941 0.1005 11.00000 0.05 0.25
Q20 1 0.1192 0.4697 0.1796 11.00000 0.05 0.25
;
_shelx_res_checksum 42194
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Si Si1 0.30425(2) 0.26359(5) 0.40578(2) 0.01776(11) Uani d 1 . .
Si Si2 0.25081(2) 0.23923(4) 0.27966(2) 0.01378(10) Uani d 1 . .
Si Si3 0.20713(2) -0.01864(5) 0.26001(2) 0.01934(11) Uani d 1 . .
C C1 0.32187(9) 0.4774(2) 0.43281(10) 0.0326(4) Uani d 1 . .
H H1 0.342782 0.529781 0.392332 0.049 Uiso calc 1 . .
H H2 0.351105 0.481717 0.481460 0.049 Uiso calc 1 . .
H H3 0.280943 0.532430 0.438785 0.049 Uiso calc 1 . .
C C2 0.25745(8) 0.1727(2) 0.47983(9) 0.0338(4) Uani d 1 . .
H H4 0.282593 0.183946 0.530913 0.051 Uiso calc 1 . .
H H5 0.249861 0.059114 0.468290 0.051 Uiso calc 1 . .
H H6 0.215449 0.227615 0.478973 0.051 Uiso calc 1 . .
C C3 0.38414(7) 0.1570(2) 0.40627(9) 0.0278(4) Uani d 1 . .
H H7 0.409142 0.164627 0.457597 0.042 Uiso calc 1 . .
H H8 0.408976 0.206399 0.368441 0.042 Uiso calc 1 . .
H H9 0.376058 0.044327 0.393031 0.042 Uiso calc 1 . .
C C4 0.17831(7) 0.37787(16) 0.26124(8) 0.0157(3) Uani d 1 . .
C C5 0.15255(7) 0.42232(16) 0.18664(8) 0.0166(3) Uani d 1 . .
H H10 0.174097 0.391031 0.144264 0.020 Uiso calc 1 . .
C C6 0.09489(7) 0.51314(16) 0.17395(8) 0.0164(3) Uani d 1 . .
C C7 0.06416(7) 0.55949(17) 0.23737(8) 0.0175(3) Uani d 1 . .
H H11 0.025674 0.622675 0.229263 0.021 Uiso calc 1 . .
C C8 0.08913(7) 0.51440(17) 0.31244(8) 0.0189(3) Uani d 1 . .
C C9 0.14687(7) 0.42416(17) 0.32341(8) 0.0181(3) Uani d 1 . .
H H12 0.164780 0.394190 0.374040 0.022 Uiso calc 1 . .
N N1 0.06746(6) 0.55413(15) 0.09955(7) 0.0211(3) Uani d 1 . .
C C10 0.10803(8) 0.5412(2) 0.03772(8) 0.0247(3) Uani d 1 . .
H H13 0.120610 0.429339 0.031923 0.037 Uiso calc 1 . .
H H14 0.147335 0.606661 0.050088 0.037 Uiso calc 1 . .
H H15 0.083461 0.578969 -0.010478 0.037 Uiso calc 1 . .
C C11 0.01575(7) 0.6719(2) 0.08958(9) 0.0252(3) Uani d 1 . .
H H16 0.032046 0.773793 0.112060 0.038 Uiso calc 1 . .
H H17 -0.020940 0.635214 0.115365 0.038 Uiso calc 1 . .
H H18 0.001115 0.686560 0.034579 0.038 Uiso calc 1 . .
N N2 0.05745(7) 0.55862(18) 0.37463(7) 0.0305(3) Uani d 1 . .
C C12 0.00044(7) 0.65851(19) 0.36342(9) 0.0235(3) Uani d 1 . .
H H19 -0.032513 0.609127 0.325453 0.035 Uiso calc 1 . .
H H20 0.012242 0.763704 0.344817 0.035 Uiso calc 1 . .
H H21 -0.017287 0.670837 0.412357 0.035 Uiso calc 1 . .
C C13 0.08889(8) 0.5299(2) 0.45176(8) 0.0253(3) Uani d 1 . .
H H22 0.131207 0.584552 0.459169 0.038 Uiso calc 1 . .
H H23 0.095511 0.414821 0.459639 0.038 Uiso calc 1 . .
H H24 0.061305 0.570997 0.488874 0.038 Uiso calc 1 . .
C C14 0.31425(7) 0.28489(17) 0.21410(8) 0.0151(3) Uani d 1 . .
C C15 0.35872(7) 0.16651(17) 0.19910(8) 0.0170(3) Uani d 1 . .
H H25 0.353827 0.060958 0.217532 0.020 Uiso calc 1 . .
C C16 0.41035(7) 0.20138(17) 0.15730(8) 0.0169(3) Uani d 1 . .
C C17 0.41619(7) 0.35685(17) 0.12925(8) 0.0167(3) Uani d 1 . .
H H26 0.450754 0.381126 0.100236 0.020 Uiso calc 1 . .
C C18 0.37191(7) 0.47750(17) 0.14323(8) 0.0162(3) Uani d 1 . .
C C19 0.32122(7) 0.43937(17) 0.18636(8) 0.0160(3) Uani d 1 . .
H H27 0.291203 0.520064 0.196795 0.019 Uiso calc 1 . .
N N3 0.45454(6) 0.07908(15) 0.14290(7) 0.0215(3) Uani d 1 . .
N N4 0.37992(6) 0.63483(15) 0.11844(7) 0.0219(3) Uani d 1 . .
C C20 0.47693(9) -0.0230(2) 0.20856(10) 0.0358(4) Uani d 1 . .
H H28 0.439219 -0.073086 0.227626 0.054 Uiso calc 1 . .
H H29 0.500814 0.041608 0.249542 0.054 Uiso calc 1 . .
H H30 0.505801 -0.106202 0.192602 0.054 Uiso calc 1 . .
C C21 0.50722(8) 0.1230(2) 0.09949(11) 0.0366(4) Uani d 1 . .
H H31 0.536208 0.199436 0.129305 0.055 Uiso calc 1 . .
H H32 0.488974 0.171889 0.050608 0.055 Uiso calc 1 . .
H H33 0.532024 0.027143 0.089272 0.055 Uiso calc 1 . .
C C22 0.43019(8) 0.6685(2) 0.07004(10) 0.0313(4) Uani d 1 . .
H H34 0.419445 0.614702 0.020332 0.047 Uiso calc 1 . .
H H35 0.472326 0.629362 0.095198 0.047 Uiso calc 1 . .
H H36 0.432763 0.784068 0.061867 0.047 Uiso calc 1 . .
C C23 0.32265(9) 0.7339(2) 0.10043(12) 0.0361(4) Uani d 1 . .
H H37 0.294343 0.722489 0.140908 0.054 Uiso calc 1 . .
H H38 0.298835 0.700536 0.051007 0.054 Uiso calc 1 . .
H H39 0.335941 0.845920 0.097152 0.054 Uiso calc 1 . .
C C24 0.18019(8) -0.0508(2) 0.15471(10) 0.0310(4) Uani d 1 . .
H H40 0.146709 0.028127 0.136380 0.047 Uiso calc 1 . .
H H41 0.162104 -0.158697 0.146642 0.047 Uiso calc 1 . .
H H42 0.217687 -0.038664 0.126137 0.047 Uiso calc 1 . .
C C25 0.13399(8) -0.0289(2) 0.31312(10) 0.0332(4) Uani d 1 . .
H H43 0.148027 -0.019567 0.368531 0.050 Uiso calc 1 . .
H H44 0.111634 -0.131258 0.302292 0.050 Uiso calc 1 . .
H H45 0.104091 0.058891 0.296305 0.050 Uiso calc 1 . .
C C26 0.26437(9) -0.18132(19) 0.29957(11) 0.0340(4) Uani d 1 . .
H H46 0.242957 -0.285333 0.290345 0.051 Uiso calc 1 . .
H H47 0.276191 -0.165481 0.355026 0.051 Uiso calc 1 . .
H H48 0.303862 -0.178120 0.274009 0.051 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Si1 0.0165(2) 0.0216(2) 0.0150(2) -0.00027(16) 0.00150(15) 0.00142(15)
Si2 0.01451(19) 0.01279(19) 0.0143(2) 0.00137(14) 0.00278(15) 0.00109(14)
Si3 0.0186(2) 0.0153(2) 0.0246(2) -0.00180(15) 0.00459(16) -0.00247(16)
C1 0.0323(9) 0.0292(9) 0.0344(9) -0.0007(7) -0.0026(7) -0.0108(7)
C2 0.0262(9) 0.0523(11) 0.0230(8) 0.0001(8) 0.0038(7) 0.0145(8)
C3 0.0216(8) 0.0364(9) 0.0241(8) 0.0064(7) -0.0022(6) 0.0008(7)
C4 0.0161(7) 0.0121(7) 0.0191(7) -0.0007(5) 0.0024(5) 0.0003(5)
C5 0.0185(7) 0.0161(7) 0.0161(7) 0.0002(6) 0.0055(5) -0.0011(5)
C6 0.0174(7) 0.0141(7) 0.0174(7) -0.0013(5) 0.0017(5) 0.0016(5)
C7 0.0161(7) 0.0160(7) 0.0205(7) 0.0026(5) 0.0031(6) 0.0010(6)
C8 0.0213(7) 0.0179(7) 0.0184(7) 0.0018(6) 0.0058(6) -0.0005(6)
C9 0.0215(7) 0.0187(7) 0.0142(7) 0.0025(6) 0.0022(6) 0.0020(6)
N1 0.0211(6) 0.0263(7) 0.0160(6) 0.0063(5) 0.0023(5) 0.0031(5)
C10 0.0269(8) 0.0313(9) 0.0160(7) 0.0049(7) 0.0036(6) 0.0021(6)
C11 0.0208(8) 0.0324(9) 0.0221(8) 0.0058(7) 0.0017(6) 0.0082(7)
N2 0.0318(8) 0.0440(9) 0.0167(7) 0.0209(7) 0.0063(6) 0.0012(6)
C12 0.0197(7) 0.0287(8) 0.0234(8) 0.0037(6) 0.0076(6) -0.0035(6)
C13 0.0286(8) 0.0308(9) 0.0174(7) 0.0046(7) 0.0065(6) -0.0015(6)
C14 0.0162(7) 0.0170(7) 0.0120(6) -0.0003(5) 0.0009(5) -0.0009(5)
C15 0.0205(7) 0.0139(7) 0.0168(7) 0.0003(6) 0.0029(6) 0.0012(5)
C16 0.0165(7) 0.0186(7) 0.0151(7) 0.0019(6) -0.0001(5) -0.0027(6)
C17 0.0147(7) 0.0210(7) 0.0145(7) -0.0017(6) 0.0026(5) -0.0009(6)
C18 0.0179(7) 0.0160(7) 0.0143(7) -0.0020(6) 0.0000(5) -0.0009(5)
C19 0.0167(7) 0.0150(7) 0.0162(7) 0.0017(5) 0.0020(5) -0.0013(5)
N3 0.0209(6) 0.0216(6) 0.0235(7) 0.0063(5) 0.0081(5) 0.0010(5)
N4 0.0241(7) 0.0167(6) 0.0263(7) -0.0010(5) 0.0091(5) 0.0041(5)
C20 0.0400(10) 0.0374(10) 0.0298(9) 0.0231(8) 0.0042(7) 0.0039(8)
C21 0.0317(9) 0.0311(9) 0.0515(11) 0.0105(8) 0.0228(8) 0.0035(8)
C22 0.0336(9) 0.0212(8) 0.0424(10) -0.0047(7) 0.0176(8) 0.0052(7)
C23 0.0356(10) 0.0219(8) 0.0543(12) 0.0070(7) 0.0190(9) 0.0157(8)
C24 0.0274(9) 0.0335(9) 0.0315(9) 0.0003(7) 0.0012(7) -0.0130(7)
C25 0.0278(9) 0.0335(9) 0.0405(10) -0.0119(7) 0.0129(7) -0.0069(8)
C26 0.0376(10) 0.0169(8) 0.0474(11) 0.0013(7) 0.0056(8) 0.0039(7)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
C1 Si1 C3 . . 108.08(8) ?
C1 Si1 C2 . . 108.21(9) ?
C3 Si1 C2 . . 109.61(8) ?
C1 Si1 Si2 . . 111.92(6) ?
C3 Si1 Si2 . . 105.68(5) ?
C2 Si1 Si2 . . 113.20(6) ?
C4 Si2 C14 . . 111.62(6) ?
C4 Si2 Si3 . . 104.95(4) ?
C14 Si2 Si3 . . 112.35(5) ?
C4 Si2 Si1 . . 111.97(5) ?
C14 Si2 Si1 . . 106.00(4) ?
Si3 Si2 Si1 . . 110.08(2) ?
C25 Si3 C26 . . 107.05(8) ?
C25 Si3 C24 . . 108.98(8) ?
C26 Si3 C24 . . 110.64(8) ?
C25 Si3 Si2 . . 106.75(6) ?
C26 Si3 Si2 . . 113.60(6) ?
C24 Si3 Si2 . . 109.63(6) ?
Si1 C1 H1 . . 109.5 ?
Si1 C1 H2 . . 109.5 ?
H1 C1 H2 . . 109.5 ?
Si1 C1 H3 . . 109.5 ?
H1 C1 H3 . . 109.5 ?
H2 C1 H3 . . 109.5 ?
Si1 C2 H4 . . 109.5 ?
Si1 C2 H5 . . 109.5 ?
H4 C2 H5 . . 109.5 ?
Si1 C2 H6 . . 109.5 ?
H4 C2 H6 . . 109.5 ?
H5 C2 H6 . . 109.5 ?
Si1 C3 H7 . . 109.5 ?
Si1 C3 H8 . . 109.5 ?
H7 C3 H8 . . 109.5 ?
Si1 C3 H9 . . 109.5 ?
H7 C3 H9 . . 109.5 ?
H8 C3 H9 . . 109.5 ?
C9 C4 C5 . . 119.86(13) ?
C9 C4 Si2 . . 118.43(10) ?
C5 C4 Si2 . . 121.45(11) ?
C4 C5 C6 . . 120.33(13) ?
C4 C5 H10 . . 119.8 ?
C6 C5 H10 . . 119.8 ?
N1 C6 C7 . . 120.08(13) ?
N1 C6 C5 . . 120.96(13) ?
C7 C6 C5 . . 118.95(13) ?
C8 C7 C6 . . 121.30(13) ?
C8 C7 H11 . . 119.4 ?
C6 C7 H11 . . 119.4 ?
N2 C8 C7 . . 120.67(13) ?
N2 C8 C9 . . 120.83(13) ?
C7 C8 C9 . . 118.50(13) ?
C4 C9 C8 . . 121.05(13) ?
C4 C9 H12 . . 119.5 ?
C8 C9 H12 . . 119.5 ?
C6 N1 C11 . . 118.99(12) ?
C6 N1 C10 . . 118.25(12) ?
C11 N1 C10 . . 116.55(12) ?
N1 C10 H13 . . 109.5 ?
N1 C10 H14 . . 109.5 ?
H13 C10 H14 . . 109.5 ?
N1 C10 H15 . . 109.5 ?
H13 C10 H15 . . 109.5 ?
H14 C10 H15 . . 109.5 ?
N1 C11 H16 . . 109.5 ?
N1 C11 H17 . . 109.5 ?
H16 C11 H17 . . 109.5 ?
N1 C11 H18 . . 109.5 ?
H16 C11 H18 . . 109.5 ?
H17 C11 H18 . . 109.5 ?
C8 N2 C12 . . 120.48(12) ?
C8 N2 C13 . . 119.29(12) ?
C12 N2 C13 . . 119.17(12) ?
N2 C12 H19 . . 109.5 ?
N2 C12 H20 . . 109.5 ?
H19 C12 H20 . . 109.5 ?
N2 C12 H21 . . 109.5 ?
H19 C12 H21 . . 109.5 ?
H20 C12 H21 . . 109.5 ?
N2 C13 H22 . . 109.5 ?
N2 C13 H23 . . 109.5 ?
H22 C13 H23 . . 109.5 ?
N2 C13 H24 . . 109.5 ?
H22 C13 H24 . . 109.5 ?
H23 C13 H24 . . 109.5 ?
C19 C14 C15 . . 119.40(13) ?
C19 C14 Si2 . . 120.66(10) ?
C15 C14 Si2 . . 119.65(10) ?
C14 C15 C16 . . 120.91(13) ?
C14 C15 H25 . . 119.5 ?
C16 C15 H25 . . 119.5 ?
C15 C16 C17 . . 118.86(13) ?
C15 C16 N3 . . 119.66(13) ?
C17 C16 N3 . . 121.47(13) ?
C16 C17 C18 . . 121.24(13) ?
C16 C17 H26 . . 119.4 ?
C18 C17 H26 . . 119.4 ?
N4 C18 C19 . . 120.37(13) ?
N4 C18 C17 . . 121.00(13) ?
C19 C18 C17 . . 118.54(13) ?
C14 C19 C18 . . 121.03(13) ?
C14 C19 H27 . . 119.5 ?
C18 C19 H27 . . 119.5 ?
C16 N3 C21 . . 117.02(12) ?
C16 N3 C20 . . 115.40(12) ?
C21 N3 C20 . . 112.20(13) ?
C18 N4 C23 . . 118.68(12) ?
C18 N4 C22 . . 119.02(12) ?
C23 N4 C22 . . 112.84(13) ?
N3 C20 H28 . . 109.5 ?
N3 C20 H29 . . 109.5 ?
H28 C20 H29 . . 109.5 ?
N3 C20 H30 . . 109.5 ?
H28 C20 H30 . . 109.5 ?
H29 C20 H30 . . 109.5 ?
N3 C21 H31 . . 109.5 ?
N3 C21 H32 . . 109.5 ?
H31 C21 H32 . . 109.5 ?
N3 C21 H33 . . 109.5 ?
H31 C21 H33 . . 109.5 ?
H32 C21 H33 . . 109.5 ?
N4 C22 H34 . . 109.5 ?
N4 C22 H35 . . 109.5 ?
H34 C22 H35 . . 109.5 ?
N4 C22 H36 . . 109.5 ?
H34 C22 H36 . . 109.5 ?
H35 C22 H36 . . 109.5 ?
N4 C23 H37 . . 109.5 ?
N4 C23 H38 . . 109.5 ?
H37 C23 H38 . . 109.5 ?
N4 C23 H39 . . 109.5 ?
H37 C23 H39 . . 109.5 ?
H38 C23 H39 . . 109.5 ?
Si3 C24 H40 . . 109.5 ?
Si3 C24 H41 . . 109.5 ?
H40 C24 H41 . . 109.5 ?
Si3 C24 H42 . . 109.5 ?
H40 C24 H42 . . 109.5 ?
H41 C24 H42 . . 109.5 ?
Si3 C25 H43 . . 109.5 ?
Si3 C25 H44 . . 109.5 ?
H43 C25 H44 . . 109.5 ?
Si3 C25 H45 . . 109.5 ?
H43 C25 H45 . . 109.5 ?
H44 C25 H45 . . 109.5 ?
Si3 C26 H46 . . 109.5 ?
Si3 C26 H47 . . 109.5 ?
H46 C26 H47 . . 109.5 ?
Si3 C26 H48 . . 109.5 ?
H46 C26 H48 . . 109.5 ?
H47 C26 H48 . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Si1 C1 . 1.8737(17) ?
Si1 C3 . 1.8744(16) ?
Si1 C2 . 1.8755(16) ?
Si1 Si2 . 2.3488(5) ?
Si2 C4 . 1.8887(14) ?
Si2 C14 . 1.8890(14) ?
Si2 Si3 . 2.3465(5) ?
Si3 C25 . 1.8751(17) ?
Si3 C26 . 1.8762(17) ?
Si3 C24 . 1.8767(17) ?
C1 H1 . 0.9800 ?
C1 H2 . 0.9800 ?
C1 H3 . 0.9800 ?
C2 H4 . 0.9800 ?
C2 H5 . 0.9800 ?
C2 H6 . 0.9800 ?
C3 H7 . 0.9800 ?
C3 H8 . 0.9800 ?
C3 H9 . 0.9800 ?
C4 C9 . 1.393(2) ?
C4 C5 . 1.3971(19) ?
C5 C6 . 1.406(2) ?
C5 H10 . 0.9500 ?
C6 N1 . 1.3959(18) ?
C6 C7 . 1.403(2) ?
C7 C8 . 1.402(2) ?
C7 H11 . 0.9500 ?
C8 N2 . 1.3911(19) ?
C8 C9 . 1.404(2) ?
C9 H12 . 0.9500 ?
N1 C11 . 1.4473(19) ?
N1 C10 . 1.4562(19) ?
C10 H13 . 0.9800 ?
C10 H14 . 0.9800 ?
C10 H15 . 0.9800 ?
C11 H16 . 0.9800 ?
C11 H17 . 0.9800 ?
C11 H18 . 0.9800 ?
N2 C12 . 1.4365(19) ?
N2 C13 . 1.4423(19) ?
C12 H19 . 0.9800 ?
C12 H20 . 0.9800 ?
C12 H21 . 0.9800 ?
C13 H22 . 0.9800 ?
C13 H23 . 0.9800 ?
C13 H24 . 0.9800 ?
C14 C19 . 1.395(2) ?
C14 C15 . 1.398(2) ?
C15 C16 . 1.400(2) ?
C15 H25 . 0.9500 ?
C16 C17 . 1.401(2) ?
C16 N3 . 1.4151(18) ?
C17 C18 . 1.404(2) ?
C17 H26 . 0.9500 ?
C18 N4 . 1.4023(18) ?
C18 C19 . 1.404(2) ?
C19 H27 . 0.9500 ?
N3 C21 . 1.452(2) ?
N3 C20 . 1.460(2) ?
N4 C23 . 1.446(2) ?
N4 C22 . 1.4499(19) ?
C20 H28 . 0.9800 ?
C20 H29 . 0.9800 ?
C20 H30 . 0.9800 ?
C21 H31 . 0.9800 ?
C21 H32 . 0.9800 ?
C21 H33 . 0.9800 ?
C22 H34 . 0.9800 ?
C22 H35 . 0.9800 ?
C22 H36 . 0.9800 ?
C23 H37 . 0.9800 ?
C23 H38 . 0.9800 ?
C23 H39 . 0.9800 ?
C24 H40 . 0.9800 ?
C24 H41 . 0.9800 ?
C24 H42 . 0.9800 ?
C25 H43 . 0.9800 ?
C25 H44 . 0.9800 ?
C25 H45 . 0.9800 ?
C26 H46 . 0.9800 ?
C26 H47 . 0.9800 ?
C26 H48 . 0.9800 ?
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_site_symmetry_1
_geom_contact_site_symmetry_2
_geom_contact_publ_flag
H4 C18 ? 1_555 2_555 yes
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C2 H4 Cg 4_566 0.98 2.81 3.7869(17) 172 y
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C14 Si2 C4 C9 . . . . -145.45(11) ?
Si3 Si2 C4 C9 . . . . 92.60(11) ?
Si1 Si2 C4 C9 . . . . -26.80(12) ?
C14 Si2 C4 C5 . . . . 40.35(13) ?
Si3 Si2 C4 C5 . . . . -81.60(12) ?
Si1 Si2 C4 C5 . . . . 159.00(10) ?
C9 C4 C5 C6 . . . . -0.2(2) ?
Si2 C4 C5 C6 . . . . 173.90(10) ?
C4 C5 C6 N1 . . . . -177.96(13) ?
C4 C5 C6 C7 . . . . 0.6(2) ?
N1 C6 C7 C8 . . . . 177.34(13) ?
C5 C6 C7 C8 . . . . -1.3(2) ?
C6 C7 C8 N2 . . . . -178.75(14) ?
C6 C7 C8 C9 . . . . 1.4(2) ?
C5 C4 C9 C8 . . . . 0.4(2) ?
Si2 C4 C9 C8 . . . . -173.87(11) ?
N2 C8 C9 C4 . . . . 179.17(14) ?
C7 C8 C9 C4 . . . . -1.0(2) ?
C7 C6 N1 C11 . . . . 13.1(2) ?
C5 C6 N1 C11 . . . . -168.37(13) ?
C7 C6 N1 C10 . . . . 164.45(13) ?
C5 C6 N1 C10 . . . . -17.0(2) ?
C7 C8 N2 C12 . . . . -3.3(2) ?
C9 C8 N2 C12 . . . . 176.48(14) ?
C7 C8 N2 C13 . . . . -171.42(14) ?
C9 C8 N2 C13 . . . . 8.4(2) ?
C4 Si2 C14 C19 . . . . 28.69(13) ?
Si3 Si2 C14 C19 . . . . 146.27(10) ?
Si1 Si2 C14 C19 . . . . -93.46(11) ?
C4 Si2 C14 C15 . . . . -157.41(11) ?
Si3 Si2 C14 C15 . . . . -39.83(12) ?
Si1 Si2 C14 C15 . . . . 80.44(11) ?
C19 C14 C15 C16 . . . . 0.6(2) ?
Si2 C14 C15 C16 . . . . -173.39(10) ?
C14 C15 C16 C17 . . . . -1.2(2) ?
C14 C15 C16 N3 . . . . -179.91(12) ?
C15 C16 C17 C18 . . . . 0.8(2) ?
N3 C16 C17 C18 . . . . 179.53(12) ?
C16 C17 C18 N4 . . . . 176.69(13) ?
C16 C17 C18 C19 . . . . 0.1(2) ?
C15 C14 C19 C18 . . . . 0.4(2) ?
Si2 C14 C19 C18 . . . . 174.32(10) ?
N4 C18 C19 C14 . . . . -177.34(13) ?
C17 C18 C19 C14 . . . . -0.7(2) ?
C15 C16 N3 C21 . . . . -179.75(14) ?
C17 C16 N3 C21 . . . . 1.6(2) ?
C15 C16 N3 C20 . . . . -44.38(19) ?
C17 C16 N3 C20 . . . . 136.94(15) ?
C19 C18 N4 C23 . . . . -32.2(2) ?
C17 C18 N4 C23 . . . . 151.30(15) ?
C19 C18 N4 C22 . . . . -176.24(13) ?
C17 C18 N4 C22 . . . . 7.3(2) ?
_cod_database_fobs_code 1559211