#------------------------------------------------------------------------------ #$Date: 2021-02-23 12:37:02 +0200 (Tue, 23 Feb 2021) $ #$Revision: 262161 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/05/1560597.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1560597 loop_ _publ_author_name 'Novikov, S.A.' 'Grigoriev, M.S.' 'Serezhkina, L.B.' 'Serezhkin, V.N.' _publ_section_title ; Potassium and magnesium succinatouranilates -- Synthesis and crystal structure ; _journal_name_full 'Journal of Solid State Chemistry' _journal_page_first 178 _journal_page_last 182 _journal_paper_doi 10.1016/j.jssc.2017.02.010 _journal_volume 248 _journal_year 2017 _chemical_formula_sum 'C12 H12 K2 O16 U2' _chemical_formula_weight 966.48 _space_group_crystal_system tetragonal _space_group_IT_number 88 _space_group_name_Hall '-I 4ad' _space_group_name_H-M_alt 'I 41/a :2' _atom_sites_solution_hydrogens geom _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 9.9637(3) _cell_length_b 9.9637(3) _cell_length_c 40.898(3) _cell_measurement_reflns_used 19040 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.997 _cell_measurement_theta_min 4.090 _cell_volume 4060.2(3) _computing_structure_refinement 'SHELXL-2014 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker KAPPA APEX II' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0555 _diffrn_reflns_av_unetI/netI 0.0364 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 56 _diffrn_reflns_limit_l_min -57 _diffrn_reflns_number 19040 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.997 _diffrn_reflns_theta_min 4.090 _exptl_absorpt_coefficient_mu 16.426 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Bruker, 2008)' _exptl_crystal_density_diffrn 3.162 _exptl_crystal_description fragment _exptl_crystal_F_000 3472 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.040 _exptl_transmission_factor_max 0.559 _exptl_transmission_factor_min 0.339 _refine_diff_density_max 0.951 _refine_diff_density_min -0.668 _refine_diff_density_rms 0.175 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 146 _refine_ls_number_reflns 2954 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.042 _refine_ls_R_factor_all 0.0377 _refine_ls_R_factor_gt 0.0239 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0100P)^2^+19.4912P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0415 _refine_ls_wR_factor_ref 0.0442 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2416 _reflns_number_total 2954 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file JSSC-2017-248-178-1.cif _cod_data_source_block s155 _cod_original_cell_volume 4060.1(4) _cod_original_sg_symbol_H-M 'I 41/a' _cod_database_code 1560597 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.243 _shelx_estimated_absorpt_t_max 0.559 _shelxl_version_number 2014-3 _shelx_res_file ; TITL s155 in I4(1)/a CELL 0.71073 9.9637 9.9637 40.8977 90.000 90.000 90.000 ZERR 8.00 0.0003 0.0003 0.0034 0.000 0.000 0.000 LATT 2 SYMM 0.5-X, -Y, 0.5+Z SYMM 0.75-Y, 0.25+X, 0.25+Z SYMM 0.75+Y, 0.75-X, 0.75+Z SFAC C H O K U UNIT 96 96 128 16 16 TEMP -173 SIZE 0.12 0.10 0.04 L.S. 8 BOND $H FMAP 2 PLAN 20 SHEL 5 0.5 OMIT -2 60 OMIT 2 2 10 OMIT 2 3 7 OMIT 1 3 6 ACTA CONF WGHT 0.010000 19.491199 FVAR 0.09357 U1 5 0.318592 0.463210 0.429335 11.00000 0.00822 0.01063 = 0.01082 0.00017 -0.00021 -0.00012 K1 4 0.000000 0.250000 0.389991 10.50000 0.01140 0.01027 = 0.02114 0.00000 0.00000 0.00284 K2 4 0.500000 0.750000 0.491632 10.50000 0.01363 0.02070 = 0.01627 0.00000 0.00000 0.00179 O1 3 0.297189 0.620322 0.449451 11.00000 0.02317 0.01075 = 0.01568 -0.00173 0.00027 0.00620 O2 3 0.341997 0.305892 0.410572 11.00000 0.02171 0.01076 = 0.01591 0.00000 -0.00119 0.00044 O11 3 0.324082 0.565431 0.375671 11.00000 0.00692 0.01462 = 0.01363 0.00327 -0.00395 -0.00185 O12 3 0.126227 0.504439 0.392202 11.00000 0.00934 0.01603 = 0.01709 0.00158 0.00064 -0.00208 O13 3 0.310928 0.282885 0.290310 11.00000 0.02253 0.01077 = 0.01450 0.00023 0.00418 0.00022 O14 3 0.202766 0.292109 0.336600 11.00000 0.02004 0.01121 = 0.01689 0.00220 0.00337 0.00339 O21 3 0.099703 0.375073 0.450881 11.00000 0.01015 0.02930 = 0.01374 0.00603 -0.00164 -0.00429 O22 3 0.277984 0.344040 0.481002 11.00000 0.00944 0.02194 = 0.01279 0.00224 -0.00207 0.00045 C11 1 0.202157 0.544148 0.369283 11.00000 0.01507 0.00303 = 0.01623 -0.00087 -0.00138 0.00133 C12 1 0.151520 0.566125 0.335170 11.00000 0.01181 0.01292 = 0.01479 0.00014 -0.00522 0.00146 AFIX 23 H12A 2 0.145260 0.663694 0.330855 11.00000 -1.20000 H12B 2 0.060327 0.527569 0.333132 11.00000 -1.20000 AFIX 0 C13 1 0.243878 0.501319 0.309701 11.00000 0.01509 0.01358 = 0.01050 0.00091 -0.00229 -0.00194 AFIX 23 H13A 2 0.210768 0.524617 0.287595 11.00000 -1.20000 H13B 2 0.334994 0.539759 0.312047 11.00000 -1.20000 AFIX 0 C14 1 0.253078 0.351560 0.312432 11.00000 0.01353 0.01309 = 0.01614 -0.00260 -0.00364 -0.00321 C21 1 0.153246 0.324595 0.475994 11.00000 0.01271 0.01791 = 0.01419 -0.00154 0.00135 0.00187 C22 1 0.075601 0.240086 0.499764 11.00000 0.01047 0.01975 = 0.01361 0.00218 -0.00005 0.00047 AFIX 23 H22A 2 0.109520 0.258950 0.522048 11.00000 -1.20000 H22B 2 0.094518 0.144527 0.494994 11.00000 -1.20000 AFIX 0 HKLF 4 REM s155 in I4(1)/a REM R1 = 0.0239 for 2416 Fo > 4sig(Fo) and 0.0377 for all 2954 data REM 146 parameters refined using 0 restraints END WGHT 0.0100 19.4821 REM Highest difference peak 0.951, deepest hole -0.668, 1-sigma level 0.175 Q1 1 0.4019 0.3178 0.3937 11.00000 0.05 0.95 Q2 1 0.0979 0.2767 0.4846 11.00000 0.05 0.65 Q3 1 0.3257 0.5627 0.4417 11.00000 0.05 0.65 Q4 1 0.0000 0.2500 0.5378 10.50000 0.05 0.64 Q5 1 0.1735 0.6476 0.4386 11.00000 0.05 0.62 Q6 1 0.0852 0.5290 0.3856 11.00000 0.05 0.61 Q7 1 0.3260 0.4029 0.4524 11.00000 0.05 0.61 Q8 1 0.2089 0.5531 0.3190 11.00000 0.05 0.61 Q9 1 0.3616 0.5456 0.4035 11.00000 0.05 0.61 Q10 1 0.0319 0.2249 0.3799 11.00000 0.05 0.60 Q11 1 0.2678 0.4159 0.4238 11.00000 0.05 0.60 Q12 1 0.1799 0.5427 0.3540 11.00000 0.05 0.59 Q13 1 0.2213 0.2838 0.4394 11.00000 0.05 0.59 Q14 1 0.1259 0.5261 0.4031 11.00000 0.05 0.59 Q15 1 0.0491 0.5315 0.3251 11.00000 0.05 0.58 Q16 1 0.3260 0.3918 0.4718 11.00000 0.05 0.57 Q17 1 0.1371 0.6275 0.2869 11.00000 0.05 0.57 Q18 1 0.0000 0.2500 0.4212 10.50000 0.05 0.56 Q19 1 0.1934 0.3631 0.3310 11.00000 0.05 0.56 Q20 1 0.0397 0.3505 0.4468 11.00000 0.05 0.56 ; _shelx_res_checksum 35596 _shelx_hkl_file ; 1 -1 0 -12.018 3.119 1 1 1 0 -12.229 2.373 1 1 1 0 -10.276 3.565 1 -1 1 0 -9.3213 2.7722 1 -1 1 0 -10.504 2.680 1 -1 -1 0 -9.6636 2.7110 2 -1 -1 0 -9.1300 2.8162 1 0 2 0 8997.69 311.87 1 -2 0 0 9194.57 311.72 1 0 -2 0 9325.84 313.30 1 -2 0 0 8912.51 318.36 3 2 0 0 9286.82 312.72 1 0 2 0 9036.90 313.08 1 -2 -2 0 7368.80 250.54 1 2 2 0 7471.07 250.96 1 2 2 0 7617.41 252.78 1 2 -2 0 7491.37 252.07 1 -2 2 0 7195.16 251.03 1 -2 -2 0 6662.56 298.02 2 3 1 0 -20.981 9.895 1 -3 -1 0 -8.0252 14.0908 3 -3 -1 0 -6.0757 6.2338 1 1 -3 0 6.9487 10.6658 1 -1 3 0 11.5159 7.8210 1 -1 -3 0 -0.5439 8.4008 1 3 -1 0 -10.915 8.125 1 1 3 0 5.64046 8.72880 1 -3 1 0 2.4576 11.0964 3 -3 1 0 -0.3807 6.9706 1 -3 3 0 2.93446 8.83281 1 -3 -3 0 -2.8045 7.5323 1 3 -3 0 -1.0120 10.4249 1 3 3 0 2.7235 12.1360 1 -4 -2 0 197.331 15.743 1 -2 4 0 214.183 16.370 1 2 -4 0 245.497 19.500 1 -4 0 0 1537.90 65.40 3 4 0 0 1610.19 60.81 1 0 4 0 1487.83 58.88 1 -4 0 0 1640.67 58.58 1 0 -4 0 1508.64 61.13 1 -2 -4 0 32.6989 9.6342 1 -4 2 0 51.3178 14.5848 3 -4 2 0 53.9074 10.6355 1 -2 -4 0 27.1120 12.8248 2 2 4 0 41.6036 11.6939 1 4 -2 0 37.2423 11.8632 1 -4 -4 0 18.5610 9.2900 1 4 -4 0 34.4280 12.6259 1 4 4 0 10.2267 15.3620 1 -4 4 0 24.5425 10.8165 1 -5 -3 0 8.49067 8.99613 1 3 -5 0 -2.8907 13.2913 1 -3 5 0 -2.1482 10.8334 1 5 3 0 15.1798 14.3062 1 1 -5 0 -8.2330 13.5400 1 -5 -1 0 12.9319 9.1582 1 -1 5 0 -7.6706 10.2169 1 5 1 0 -4.2212 11.3735 1 -5 -1 0 -7.1893 17.1046 3 -5 1 0 -5.2206 8.9822 1 5 -1 0 -8.3733 10.9136 1 -1 -5 0 -3.4986 11.0046 1 -5 1 0 -4.1667 15.3103 3 1 5 0 10.0480 11.4795 1 -3 -5 0 8.94004 9.43779 1 -5 3 0 21.1039 11.0107 1 -5 3 0 9.5018 15.8326 3 3 5 0 23.7496 14.4822 1 5 -3 0 8.2630 12.1283 1 -3 -5 0 6.1499 14.9771 2 -5 -5 0 9.7943 10.7792 1 5 -5 0 16.5802 15.2704 1 5 5 0 34.3247 20.2636 1 -5 5 0 33.8354 13.8077 1 4 -6 0 3258.05 123.76 1 -6 -4 0 3189.99 117.46 1 -4 6 0 3205.64 120.20 1 6 4 0 3220.35 125.71 1 6 2 0 1176.19 53.60 1 2 -6 0 1181.06 53.37 1 -6 -2 0 1088.12 47.57 1 -2 6 0 1202.05 50.93 1 -6 0 0 1646.49 64.83 1 0 -6 0 1625.24 68.42 1 -6 0 0 1713.93 74.06 3 0 6 0 1653.51 67.03 1 6 0 0 1750.85 68.68 1 6 -2 0 408.617 28.839 1 -6 2 0 408.516 24.823 1 -2 -6 0 364.711 24.330 1 2 6 0 355.981 27.393 1 -6 2 0 410.803 32.502 3 -6 4 0 132.522 24.062 3 -6 4 0 112.600 18.244 1 6 -4 0 129.164 20.902 1 -4 -6 0 120.398 18.608 2 4 6 0 111.173 22.620 1 -4 -6 0 124.836 15.277 1 6 6 0 -6.0705 22.6564 1 -6 6 0 71.3218 18.9310 1 6 -6 0 45.8522 21.0349 1 -5 7 0 -6.6339 16.7548 1 5 -7 0 12.5033 19.6616 1 7 5 0 7.9149 21.5046 1 7 3 0 4.2858 17.6890 1 3 -7 0 -23.892 17.752 1 -7 -3 0 -9.9418 11.3348 1 -3 7 0 19.4514 15.6619 1 -7 -1 0 -8.6267 23.1455 3 7 1 0 -9.3230 14.6306 1 -1 7 0 18.9115 14.7788 1 -7 -1 0 1.8618 10.6150 1 1 -7 0 2.0272 17.1944 1 1 7 0 -11.142 14.903 1 -1 -7 0 -0.9558 13.4110 1 7 -1 0 2.4442 14.7925 1 -7 1 0 -7.8486 19.4590 3 -7 1 0 25.9264 12.5687 1 -7 3 0 16.6091 21.7997 3 3 7 0 3.9950 17.6675 1 -3 -7 0 -17.794 20.420 2 -3 -7 0 0.6042 12.0626 1 7 -3 0 13.9776 16.7995 1 -7 3 0 14.9364 13.3944 1 -7 5 0 31.5136 23.9721 3 -7 5 0 10.7982 15.4948 1 7 -5 0 -37.922 17.407 1 5 7 0 14.6161 23.0724 1 -7 7 0 -5.3079 17.9423 1 7 -7 0 21.2241 20.8076 1 7 7 0 -27.572 23.814 1 -7 7 0 -2.2983 24.6561 3 6 -8 0 370.620 36.284 1 8 6 0 438.549 41.514 1 4 -8 0 2007.23 87.11 1 8 4 0 1998.94 88.14 1 -4 8 0 2046.88 84.88 1 -2 8 0 5498.79 202.48 1 -8 -2 0 5674.98 198.82 1 2 -8 0 5476.04 205.39 1 8 2 0 5594.93 204.81 1 -8 0 0 1114.00 50.49 1 8 0 0 1092.33 54.11 1 0 8 0 1121.30 54.17 1 0 -8 0 1149.91 54.26 1 -8 0 0 1170.74 63.11 3 8 -2 0 210.362 25.238 1 -8 2 0 220.720 22.201 1 -8 2 0 197.807 30.196 3 2 8 0 220.513 26.664 1 8 -4 0 1076.72 55.17 1 -8 4 0 1117.15 65.37 3 4 8 0 1148.99 59.79 1 -8 4 0 1071.24 52.21 1 6 8 0 887.945 57.138 1 -8 6 0 882.459 48.289 1 8 -6 0 762.097 50.501 1 -8 6 0 875.740 59.581 3 -8 8 0 688.292 46.415 1 8 8 0 707.962 57.158 1 -8 8 0 628.479 56.616 3 9 7 0 -42.659 26.040 1 -7 9 0 -1.3052 22.9118 1 9 5 0 -25.821 22.247 1 -5 9 0 19.2555 21.0319 1 9 3 0 -13.914 20.081 1 -3 9 0 -43.057 17.434 1 -9 -1 0 -31.648 25.384 3 -1 9 0 -0.4253 18.5123 1 -9 -1 0 -15.634 13.685 1 9 1 0 30.7829 20.5187 1 -9 1 0 -3.1820 13.6605 1 -9 1 0 22.2331 27.7658 3 9 -1 0 9.3792 19.4670 1 1 9 0 -2.6127 18.1822 1 -9 3 0 27.0741 28.5142 3 9 -3 0 -16.060 19.518 1 3 9 0 22.9635 22.2118 1 -9 3 0 5.0094 16.9713 1 9 -5 0 -51.787 19.891 1 -9 5 0 -27.043 18.672 1 5 9 0 -26.213 25.094 1 -9 5 0 2.2705 30.3473 3 -9 7 0 -13.496 31.868 3 9 -7 0 -27.900 24.064 1 -9 7 0 14.4434 20.6767 1 7 9 0 24.4238 32.0020 1 9 9 0 -4.9830 33.0439 1 -9 9 0 4.2859 37.8763 3 -9 9 0 -20.306 25.088 1 -8 10 0 -9.9730 37.7106 3 -8 10 0 -1.5681 25.5595 1 10 8 0 -23.173 30.415 1 10 6 0 135.374 33.167 1 -6 10 0 134.141 29.547 1 10 4 0 2449.92 107.52 1 -4 10 0 2501.62 104.87 1 -2 10 0 1376.41 67.66 1 10 2 0 1394.19 67.83 1 -10 0 0 1568.95 83.28 3 0 10 0 1569.76 74.17 1 10 0 0 1593.96 73.96 1 2 10 0 224.691 31.592 1 10 -2 0 207.027 30.150 1 -10 2 0 199.902 25.305 1 -10 2 0 187.222 37.991 3 -10 4 0 707.837 59.835 3 10 -4 0 668.517 46.443 1 4 10 0 639.881 52.668 1 -10 4 0 728.523 44.608 1 6 10 0 2823.89 128.62 1 -10 6 0 2879.39 131.04 3 10 -6 0 2818.38 122.50 1 -10 6 0 2910.95 118.18 1 -10 8 0 373.984 39.733 1 8 10 0 445.684 53.569 1 -10 8 0 291.465 50.534 3 11 7 0 -17.115 30.858 1 -7 11 0 -11.769 27.821 1 11 5 0 0.6546 27.4412 1 -5 11 0 -53.354 23.490 1 -3 11 0 -0.3236 24.2744 1 11 3 0 -16.959 24.179 1 -1 11 0 -31.338 22.516 1 -11 -1 0 28.7484 36.2919 3 11 1 0 -11.024 23.886 1 1 11 0 -11.121 23.981 1 11 -1 0 -15.650 23.420 1 -11 1 0 -11.954 33.780 3 -11 3 0 115.666 38.900 3 11 -3 0 -3.7833 23.4587 1 3 11 0 -16.014 25.552 1 11 -5 0 -52.319 25.044 1 -11 5 0 1.6783 35.8943 3 5 11 0 7.3645 32.8469 1 7 11 0 31.3451 39.8769 1 -11 7 0 -0.9657 40.8369 3 -6 12 0 108.883 33.433 1 12 6 0 112.478 35.909 1 -4 12 0 81.0504 30.7782 1 12 4 0 70.7922 31.1036 1 -2 12 0 676.572 51.526 1 12 2 0 689.945 52.029 1 -12 0 0 42.1639 40.1823 3 0 12 0 2.2373 26.5038 1 12 0 0 2.6453 26.7383 1 2 12 0 -9.2032 27.7459 1 12 -2 0 21.8356 25.1833 1 -12 2 0 28.4689 39.2986 3 4 12 0 1602.12 86.02 1 12 -4 0 1447.43 77.88 1 -12 4 0 1380.90 86.56 3 6 12 0 1255.62 83.96 1 -12 6 0 1196.37 85.73 3 -5 13 0 16.1837 30.9895 1 13 5 0 29.1021 29.7391 1 -3 13 0 -8.4918 29.2404 1 13 3 0 0.6339 30.0099 1 13 1 0 32.9797 30.4073 1 -1 13 0 1.5218 30.2172 1 1 13 0 -22.178 29.865 1 -13 1 0 47.1865 46.9163 3 13 -1 0 -15.711 28.012 1 3 13 0 -66.736 30.321 1 13 -3 0 26.3909 32.2311 1 -13 3 0 -69.621 40.711 3 13 -5 0 -1.6953 32.4039 1 -13 5 0 45.0632 47.0345 3 5 13 0 -47.649 37.720 1 0 14 0 0.8286 33.1270 1 14 0 0 52.2044 33.5913 1 0 1 -1 0.20107 1.99737 1 -1 0 -1 -1.7229 2.1007 1 1 0 -1 2.15020 1.84213 1 0 -1 -1 -1.9168 1.8349 1 -1 0 -1 0.90226 1.66198 1 0 1 -1 -0.9960 1.1848 1 1 0 -1 -0.4898 1.2842 1 -1 0 -1 2.84298 3.21645 3 0 -1 -1 0.74360 3.05780 1 0 1 1 -0.1391 2.6011 1 1 0 1 -0.1311 1.4710 1 -1 0 1 -1.6131 1.4130 1 1 0 1 -0.2935 2.2111 1 0 -1 1 -1.7971 1.3910 1 -1 0 1 5.89016 2.28408 1 0 1 1 -0.7991 1.7891 1 -1 0 1 -1.6259 2.8666 3 0 -1 1 -1.3838 2.1066 1 -1 2 -1 1450.98 54.48 1 2 1 -1 1542.14 54.45 1 2 1 -1 1483.07 56.35 1 1 -2 -1 1607.92 56.18 1 -2 -1 -1 1570.33 54.75 1 2 1 1 1491.74 56.87 1 -1 2 1 1499.91 54.65 1 1 -2 1 1539.41 55.88 1 -2 -1 1 1411.21 53.93 1 1 2 -1 178.078 12.668 1 -1 -2 -1 168.142 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11.3102 1 -3 4 -1 81.3098 12.2270 1 3 -4 -1 97.9278 14.6194 1 -4 -3 1 105.535 11.264 1 4 3 1 86.2927 17.5608 1 3 -4 1 105.127 15.377 1 -3 4 1 94.8636 12.4227 1 1 -4 -1 55.0275 13.4570 1 -4 -1 -1 32.5089 17.7103 3 4 1 -1 33.1326 12.4007 1 -4 -1 -1 60.7467 9.3978 1 -4 -1 1 46.4682 15.7645 3 -1 4 1 51.1259 10.2806 1 1 -4 1 65.1093 13.0446 1 4 1 1 30.7865 11.8073 1 -4 -1 1 55.1335 8.9527 1 -4 1 -1 404.465 21.473 1 -1 -4 -1 415.375 24.403 1 -4 1 -1 401.134 29.480 3 4 -1 -1 423.559 24.491 1 1 4 -1 413.739 22.555 1 1 4 1 377.143 23.575 1 -4 1 1 436.486 22.418 1 -4 1 1 412.378 28.924 3 4 -1 1 408.160 23.438 1 -1 -4 1 453.943 23.719 1 -3 -4 -1 543.812 26.077 1 3 4 -1 569.668 30.660 1 -3 -4 -1 481.355 29.125 2 4 -3 -1 526.976 28.314 1 -4 3 -1 491.592 33.646 3 -4 3 -1 497.662 27.290 1 -4 3 1 540.974 27.928 1 3 4 1 572.580 31.529 1 4 -3 1 577.355 29.801 1 -3 -4 1 515.766 25.030 1 -3 -4 1 530.071 32.330 2 5 4 -1 1071.12 52.90 1 -4 5 -1 1139.47 48.28 1 -5 -4 -1 1056.34 45.27 1 4 -5 -1 1080.94 50.51 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414.564 43.024 1 -7 8 -7 398.684 35.052 1 -7 8 -7 414.639 44.801 3 8 7 -7 480.245 43.102 1 -7 8 7 417.981 36.581 1 8 7 7 357.586 43.932 1 5 -8 -7 898.868 57.447 1 8 5 -7 1012.67 53.67 1 -5 8 -7 1049.89 50.54 1 8 5 7 991.894 59.185 1 -5 8 7 971.925 51.540 1 -3 8 -7 22.1363 16.2183 1 -8 -3 -7 31.3080 16.3125 1 3 -8 -7 -12.361 22.871 1 8 3 -7 60.7916 19.3684 1 8 3 7 31.8827 20.4541 1 -3 8 7 32.9270 19.1572 1 -8 -1 -7 298.246 39.745 3 -1 8 -7 229.252 23.715 1 8 1 -7 229.423 25.063 1 1 -8 -7 256.178 32.353 1 -8 -1 -7 240.740 23.927 1 -1 8 7 231.038 26.174 1 -8 -1 7 220.016 32.672 3 8 1 7 209.712 26.873 1 8 -1 -7 1348.69 60.81 1 -1 -8 -7 1292.29 63.89 1 -8 1 -7 1268.14 69.58 3 -8 1 -7 1305.66 57.61 1 1 8 -7 1333.62 59.26 1 8 -1 7 1338.96 63.10 1 1 8 7 1268.16 60.26 1 -8 1 7 1278.67 55.71 1 -8 1 7 1238.33 66.88 3 -8 3 -7 250.712 25.649 1 8 -3 -7 231.953 26.749 1 -8 3 -7 235.924 32.997 3 3 8 -7 315.219 29.904 1 -3 -8 -7 216.042 25.358 1 8 -3 7 245.338 29.308 1 -8 3 7 237.260 23.314 1 -3 -8 7 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10.2979 17.6872 1 -7 5 12 -15.834 16.061 1 7 7 -12 4.7803 21.6839 1 -7 7 -12 -2.0042 18.1537 1 7 -7 -12 36.4718 23.7279 1 -7 7 -12 30.3295 27.0664 3 -7 7 12 6.4321 18.9325 1 7 7 12 0.6809 26.3196 1 -6 8 -12 476.422 44.215 3 -6 8 -12 378.339 33.261 1 6 -8 -12 419.813 40.605 1 8 6 -12 393.865 35.668 1 8 6 12 374.112 41.430 1 -6 8 12 442.442 37.844 1 -4 8 -12 985.675 48.226 1 4 -8 -12 901.429 57.063 1 8 4 -12 1001.55 49.90 1 -8 -4 -12 847.544 47.817 1 8 4 12 912.335 54.736 1 -4 8 12 965.648 51.384 1 -8 -2 -12 1427.05 63.90 1 -2 8 -12 1473.54 63.47 1 8 2 -12 1470.19 64.45 1 2 -8 -12 1518.19 73.65 1 -2 8 12 1476.23 68.13 1 8 2 12 1472.44 70.16 1 -8 0 -12 522.222 33.501 1 0 -8 -12 524.932 43.252 1 8 0 -12 507.242 33.851 1 -8 0 -12 606.431 50.971 3 0 8 -12 502.394 32.646 1 -8 0 12 552.162 41.107 3 8 0 12 579.821 40.375 1 0 8 12 491.861 37.507 1 -8 2 -12 19.7928 16.9103 1 2 8 -12 8.6658 18.1759 1 -8 2 -12 19.6510 27.6981 3 -2 -8 -12 -1.9453 21.9975 1 8 -2 -12 23.4644 17.8852 1 8 -2 12 38.6980 20.4998 1 -8 2 12 -2.0330 20.6362 3 2 8 12 12.6384 19.9744 1 -2 -8 12 3.0622 23.6062 2 8 -4 -12 244.276 28.345 1 -8 4 -12 193.187 24.200 1 4 8 -12 186.917 29.469 1 -8 4 -12 154.990 32.140 3 -4 -8 -12 184.610 26.623 1 -4 -8 12 222.904 35.843 2 -8 4 12 195.473 30.370 3 8 -4 12 222.590 28.275 1 4 8 12 218.766 31.328 1 -8 4 12 201.781 23.756 1 6 8 -12 254.635 35.370 1 -8 6 -12 291.442 30.849 1 -8 6 -12 278.203 39.060 3 8 -6 -12 349.089 35.204 1 -8 6 12 300.184 30.858 1 -8 6 12 347.463 40.516 3 6 8 12 262.993 36.029 1 8 -8 -12 12.1756 25.4775 1 -8 8 -12 50.1265 32.0794 3 -8 8 -12 61.8013 25.4588 1 8 8 -12 -33.836 23.890 1 -8 8 12 26.6662 23.4255 1 -8 8 12 38.4120 35.7061 3 8 8 12 -15.783 28.831 1 -7 9 -12 74.4662 33.6087 3 -7 9 -12 69.4864 23.7822 1 7 -9 -12 47.2761 31.6748 1 9 7 -12 107.561 28.343 1 9 7 12 103.028 31.707 1 -7 9 12 96.6779 28.3384 1 -5 9 -12 968.719 51.070 1 5 -9 -12 933.054 61.247 1 9 5 -12 874.820 50.495 1 -5 9 12 878.128 52.937 1 9 5 12 847.314 56.941 1 -9 -3 -12 2063.66 85.96 1 3 -9 -12 2041.83 95.28 1 -3 9 -12 2050.89 85.75 1 9 3 -12 2027.31 85.70 1 9 3 12 2077.75 91.66 1 -3 9 12 1984.10 88.10 1 1 -9 -12 2107.33 95.44 1 -9 -1 -12 2080.55 86.44 1 -1 9 -12 2113.14 86.66 1 -9 -1 -12 2130.12 102.66 3 9 1 -12 1947.30 86.66 1 -9 -1 12 2124.50 93.85 3 -1 9 12 2140.72 90.53 1 9 1 12 2202.61 92.87 1 1 9 -12 340.823 30.651 1 -9 1 -12 347.465 29.041 1 -9 1 -12 343.712 43.280 3 -1 -9 -12 312.910 36.818 1 9 -1 -12 244.899 27.987 1 -9 1 12 288.442 34.433 3 9 -1 12 364.322 34.803 1 1 9 12 225.003 29.718 1 -9 3 -12 214.051 38.455 3 9 -3 -12 193.670 27.313 1 -9 3 -12 180.638 25.166 1 3 9 -12 287.578 31.942 1 3 9 12 184.849 31.669 1 -3 -9 12 282.918 38.359 2 -9 3 12 257.544 34.611 3 9 -3 12 260.435 30.964 1 5 9 -12 595.610 49.513 1 -9 5 -12 697.761 55.910 3 9 -5 -12 676.569 45.892 1 -9 5 -12 541.828 41.201 1 5 9 12 655.738 51.773 1 -5 -9 12 587.610 51.701 2 -9 5 12 580.122 50.769 3 7 9 -12 561.816 49.103 1 9 -7 -12 486.830 45.736 1 -9 7 -12 547.362 54.084 3 -9 7 -12 552.104 41.637 1 -9 7 12 510.272 52.153 3 7 9 12 572.222 52.957 1 9 9 -12 145.123 33.073 1 -9 9 -12 103.426 29.568 1 9 -9 -12 37.8441 33.7173 1 -9 9 -12 87.1529 36.8102 3 -9 9 12 108.420 42.408 3 9 9 12 104.843 38.059 1 -8 10 -12 47.9406 27.5924 1 -8 10 -12 -12.940 35.421 3 10 8 -12 -5.0736 25.6045 1 10 8 12 2.4205 30.1649 1 -6 10 -12 224.370 31.368 1 10 6 -12 211.868 32.127 1 10 6 12 170.189 37.148 1 -6 10 12 196.461 33.194 1 4 -10 -12 598.121 54.111 1 -4 10 -12 512.238 41.257 1 10 4 -12 466.026 39.213 1 -4 10 12 578.503 42.454 1 10 4 12 495.464 47.420 1 -10 -2 -12 421.993 34.805 1 2 -10 -12 548.354 49.407 1 10 2 -12 597.994 40.031 1 -2 10 -12 550.184 40.441 1 10 2 12 486.010 44.437 1 -2 10 12 588.763 42.006 1 10 0 -12 185.179 27.082 1 -10 0 -12 227.016 44.651 3 0 10 -12 176.344 27.333 1 -10 0 -12 205.070 26.916 1 0 10 12 191.989 31.032 1 10 0 12 190.611 29.736 1 -10 0 12 231.528 35.623 3 2 10 -12 34.9316 25.5257 1 -10 2 -12 68.0552 22.0537 1 10 -2 -12 32.4758 21.8644 1 -10 2 -12 7.0636 30.7496 3 10 -2 12 48.7481 25.5685 1 2 10 12 1.5179 23.7371 1 -2 -10 12 44.3267 30.5302 2 -10 2 12 55.5219 28.6621 3 -10 4 -12 279.065 31.827 1 -10 4 -12 252.905 44.099 3 4 10 -12 209.988 37.331 1 10 -4 -12 230.171 32.865 1 -10 4 12 202.271 38.853 3 4 10 12 268.398 37.972 1 10 -4 12 216.058 33.073 1 -4 -10 12 272.507 41.987 2 6 10 -12 415.612 48.759 1 10 -6 -12 515.497 47.398 1 -10 6 -12 446.250 53.859 3 -10 6 -12 524.854 44.319 1 6 10 12 587.453 52.414 1 -10 6 12 682.922 57.871 3 10 -8 -12 274.913 42.743 1 -10 8 -12 260.172 35.741 1 -10 8 -12 278.332 48.556 3 8 10 -12 265.755 42.119 1 -10 8 12 281.444 49.707 3 8 10 12 274.191 46.400 1 -7 11 -12 99.1116 32.2530 1 -7 11 -12 14.8578 37.7033 3 11 7 -12 75.5261 30.5712 1 -7 11 12 126.086 33.776 1 11 7 12 51.3716 35.2683 1 -5 11 -12 271.461 36.089 1 11 5 -12 341.200 36.811 1 11 5 12 332.899 43.608 1 -5 11 12 347.819 39.220 1 -3 11 -12 600.242 44.208 1 11 3 -12 544.480 41.640 1 -3 11 12 594.285 45.491 1 11 3 12 521.610 47.495 1 -1 11 -12 754.788 49.682 1 11 1 -12 806.606 49.544 1 -1 11 12 739.443 52.307 1 11 1 12 836.334 52.410 1 1 11 -12 105.632 30.665 1 -11 1 -12 74.8232 23.8243 1 -11 1 -12 164.734 45.746 3 11 -1 -12 127.875 25.916 1 11 -1 12 72.3479 28.7172 1 -1 -11 12 111.142 36.166 2 1 11 12 82.2963 29.1159 1 -11 1 12 56.8052 32.8748 3 -11 3 -12 403.938 53.078 3 11 -3 -12 430.646 41.720 1 -11 3 -12 429.625 37.847 1 3 11 -12 432.754 45.581 1 3 11 12 415.963 45.199 1 11 -3 12 425.173 43.132 1 -11 3 12 416.849 46.250 3 -11 5 -12 1062.70 63.79 1 5 11 -12 1280.15 75.03 1 11 -5 -12 1267.70 68.34 1 -11 5 -12 1174.63 82.71 3 5 11 12 1191.21 74.23 1 -11 5 12 1352.62 81.20 3 11 -7 -12 1065.00 66.89 1 7 11 -12 911.159 71.641 1 -11 7 -12 1039.75 77.66 3 -11 7 -12 1070.68 62.15 1 -11 7 12 1122.32 77.46 3 7 11 12 1092.05 74.97 1 12 6 -12 -60.322 23.480 1 -6 12 -12 32.0390 29.6674 1 -6 12 12 -6.2676 28.5923 1 12 6 12 -34.071 31.833 1 12 4 -12 67.8501 27.1011 1 -4 12 -12 82.0120 29.4790 1 -4 12 12 75.8545 30.1338 1 12 4 12 3.0802 30.8543 1 12 2 -12 131.121 29.751 1 -2 12 -12 84.0400 29.4066 1 -2 12 12 119.563 33.327 1 12 2 12 190.218 36.630 1 0 12 -12 37.7271 29.8831 1 -12 0 -12 16.3891 42.1186 3 12 0 -12 7.3176 25.0756 1 0 12 12 -3.7128 28.1774 1 12 0 12 28.5876 26.9294 1 -12 0 12 -30.036 33.928 3 -12 2 -12 25.6439 24.5214 1 2 12 -12 50.9299 33.9926 1 -12 2 -12 14.9793 41.7092 3 12 -2 -12 -2.1723 25.7793 1 12 -2 12 56.4872 29.1396 1 -12 2 12 63.3905 37.4383 3 2 12 12 19.0514 28.2632 1 -12 4 -12 476.613 43.173 1 12 -4 -12 562.567 48.487 1 -12 4 -12 483.170 61.822 3 4 12 -12 429.864 53.718 1 -12 4 12 450.171 53.807 3 4 12 12 465.863 52.399 1 -12 6 -12 403.376 43.650 1 6 12 -12 349.465 50.973 1 -12 6 -12 372.457 59.193 3 12 -6 -12 409.114 48.485 1 6 12 12 465.068 54.597 1 -12 6 12 305.791 50.421 3 -3 13 -12 -1.3628 31.0338 1 13 3 -12 34.0362 27.3391 1 13 3 12 53.8575 34.1318 1 -3 13 12 46.2166 30.8529 1 13 1 -12 66.9127 29.2354 1 -1 13 -12 -0.7686 31.7402 1 13 1 12 22.4908 31.2364 1 -1 13 12 72.1453 33.4810 1 1 13 -12 26.6098 35.2703 1 -13 1 -12 58.2346 47.4881 3 13 -1 -12 13.3195 25.2419 1 13 -1 12 -50.229 29.049 1 -13 1 12 -13.437 37.975 3 1 13 12 -24.572 30.078 1 13 -3 -12 176.874 37.076 1 -13 3 -12 97.4969 49.3041 3 3 13 -12 278.379 47.842 1 -13 3 12 236.104 48.314 3 3 13 12 183.947 42.048 1 -1 0 -13 850.912 39.248 3 1 0 -13 989.921 35.677 1 0 1 -13 860.707 34.800 3 -1 0 -13 926.281 37.879 1 -1 0 -13 941.337 38.984 1 0 -1 -13 894.924 39.833 1 0 -1 -13 933.466 38.907 1 0 1 -13 890.432 34.789 1 0 1 -13 955.341 34.200 1 1 0 -13 911.005 34.955 1 1 0 13 966.581 36.649 1 0 1 13 809.416 46.306 2 0 1 13 905.623 36.527 1 -1 0 13 965.063 33.957 1 0 -1 13 914.219 48.447 2 1 0 13 910.685 45.684 2 -1 0 13 951.404 48.920 2 -2 -1 -13 3548.70 122.55 1 -1 2 -13 3270.70 118.25 1 -1 2 -13 3381.64 118.21 1 2 1 -13 3115.98 116.72 1 1 -2 -13 3463.58 122.96 1 2 1 13 3464.16 142.51 2 -1 2 13 3529.46 120.46 1 1 -2 13 3466.19 117.55 1 2 1 13 3366.87 122.29 1 2 -1 -13 585.752 26.425 1 -1 -2 -13 567.550 31.132 1 -2 1 -13 556.104 25.714 1 -2 1 -13 571.446 29.920 3 -2 1 -13 571.233 27.269 1 2 -1 -13 611.727 25.570 1 1 2 13 594.844 28.094 1 -1 -2 13 607.574 39.001 2 -2 1 13 554.331 24.741 1 2 -1 13 580.496 25.849 1 2 -3 -13 183.487 18.507 1 -2 3 -13 179.045 13.573 1 -3 -2 -13 195.397 18.596 1 3 2 -13 182.430 11.345 1 -2 3 -13 165.505 13.146 1 3 2 -13 140.257 11.410 1 -2 3 13 157.804 15.428 1 3 2 13 188.600 19.815 1 3 2 13 175.489 13.870 2 -3 -2 13 151.981 22.084 2 0 3 -13 367.359 17.149 1 0 3 -13 369.414 16.145 1 3 0 -13 381.504 18.183 1 0 -3 -13 361.233 27.037 1 3 0 -13 357.561 18.583 1 -3 0 -13 369.757 21.865 1 -3 0 -13 393.621 27.377 3 0 3 13 379.986 21.824 1 -3 0 13 397.928 21.226 3 -3 0 13 367.555 17.227 1 3 0 13 366.840 23.729 1 2 3 -13 3869.95 135.67 1 -3 2 -13 3936.55 139.51 1 3 -2 -13 3846.02 140.37 1 -2 -3 -13 3986.42 143.98 1 2 3 -13 4068.92 135.29 1 -3 2 -13 3834.43 143.99 3 2 3 13 4076.86 142.58 1 3 -2 13 3832.31 139.53 1 -2 -3 13 4113.79 171.54 2 -3 2 13 3785.07 139.13 1 4 3 -13 2086.33 72.34 1 3 -4 -13 1994.94 78.90 1 -3 4 -13 1924.19 74.58 1 4 3 -13 2024.23 74.47 1 -4 -3 -13 1948.40 77.65 1 4 3 13 1987.81 80.73 1 3 -4 13 1864.77 74.22 1 -3 4 13 1995.19 76.42 1 4 1 -13 5434.92 183.86 1 4 1 -13 5338.79 184.71 1 -4 -1 -13 5246.41 196.27 3 -1 4 -13 5317.45 183.98 1 -4 -1 -13 5231.60 187.60 1 1 -4 -13 5346.67 191.95 1 -1 4 -13 5424.10 184.52 1 -4 -1 13 5064.62 188.65 3 -1 4 13 5559.91 188.37 1 4 1 13 4988.72 188.87 1 -4 1 -13 1247.52 56.87 3 -4 1 -13 1231.05 50.42 1 4 -1 -13 1254.67 49.34 1 -1 -4 -13 1215.19 56.12 1 1 4 -13 1325.27 48.18 1 -1 -4 13 1151.67 63.64 2 4 -1 13 1206.34 50.91 1 1 4 13 1258.41 51.91 1 -4 1 13 1179.52 51.41 3 -4 1 13 1254.31 48.04 1 -4 3 -13 23.8787 11.0019 1 3 4 -13 19.8179 11.5472 1 -3 -4 -13 7.5106 13.9808 1 -4 3 -13 29.1715 14.7596 3 4 -3 -13 13.0588 11.7940 1 3 4 -13 8.20747 8.63395 1 4 -3 13 18.2617 11.2297 1 -3 -4 13 6.8716 19.8332 2 3 4 13 5.5945 13.8648 1 -4 3 13 23.6756 11.4154 1 5 4 -13 1014.60 46.66 1 -5 -4 -13 1021.19 47.67 1 -4 5 -13 996.391 45.409 1 5 4 -13 1047.78 42.95 1 -4 5 -13 1046.08 50.53 3 4 -5 -13 918.614 48.519 1 4 -5 13 1000.80 45.71 1 5 4 13 911.179 51.882 1 -4 5 13 1015.53 46.48 1 2 -5 -13 39.6933 18.3791 1 5 2 -13 74.5991 10.4778 1 -5 -2 -13 44.5781 13.5690 1 -2 5 -13 60.1609 11.3550 1 5 2 -13 63.6660 12.4924 1 5 2 13 54.9236 16.4069 1 -2 5 13 40.8564 14.9446 1 0 5 -13 60.0052 9.8051 1 -5 0 -13 51.4980 12.2895 1 -5 0 -13 30.3820 19.2754 3 5 0 -13 40.1136 10.9954 1 0 -5 -13 101.369 20.414 1 0 5 -13 48.1320 10.9469 1 -5 0 13 64.0589 15.1279 3 5 0 13 62.0037 14.9230 1 -5 0 13 46.0992 8.5713 1 0 5 13 52.0307 14.1629 1 2 5 -13 -0.7976 12.0033 1 -5 2 -13 23.5231 15.8703 3 5 -2 -13 6.1308 11.6398 1 -5 2 -13 17.2018 12.1345 1 -2 -5 -13 25.8901 17.9411 1 2 5 -13 -1.1729 9.8916 1 -5 2 13 13.3801 13.2910 3 -2 -5 13 10.7526 19.5506 2 2 5 13 -11.145 13.385 1 -5 2 13 6.1972 10.0146 1 5 -2 13 24.5739 13.8594 1 4 5 -13 273.000 24.058 1 -5 4 -13 336.931 29.318 3 -4 -5 -13 295.403 26.554 1 5 -4 -13 331.813 27.366 1 -5 4 -13 257.147 22.794 1 4 5 -13 288.566 21.374 1 4 5 13 295.201 28.148 1 -4 -5 13 247.187 32.238 2 5 -4 13 268.922 23.656 1 -5 4 13 330.083 23.469 1 6 5 -13 15.1474 17.3518 1 -6 -5 -13 -5.7986 16.5177 1 5 -6 -13 14.9678 19.1718 1 -5 6 -13 15.8040 15.4173 1 -5 6 -13 17.1917 20.7545 3 -5 6 13 -5.2590 16.5246 1 6 5 13 2.9572 22.2713 1 -3 6 -13 1351.09 55.05 1 3 -6 -13 1315.81 63.40 1 6 3 -13 1299.22 55.24 1 -6 -3 -13 1273.33 57.90 1 -3 6 13 1312.31 58.47 1 6 3 13 1212.22 61.27 1 3 -6 13 1310.29 54.88 1 -1 6 -13 1946.95 76.77 1 6 1 -13 1980.42 78.18 1 1 -6 -13 2053.34 88.57 1 -6 -1 -13 2002.64 79.84 1 -6 -1 -13 2131.75 94.02 3 -1 6 -13 2027.06 77.66 1 6 1 13 1981.90 83.75 1 -6 -1 13 2025.24 83.12 3 -1 6 13 2134.47 83.02 1 1 -6 13 2121.21 75.97 1 6 -1 -13 1449.79 59.86 1 -6 1 -13 1411.53 68.29 3 1 6 -13 1454.80 57.11 1 -1 -6 -13 1466.43 69.09 1 -6 1 -13 1396.57 60.38 1 1 6 -13 1335.56 58.85 1 6 -1 13 1474.41 62.34 1 -6 1 13 1551.07 57.77 1 1 6 13 1442.57 62.86 1 -6 1 13 1409.33 63.12 3 3 6 -13 78.3988 18.0309 1 3 6 -13 71.1291 18.0931 1 -6 3 -13 75.6583 20.7987 3 -3 -6 -13 126.162 23.104 1 -6 3 -13 103.423 18.118 1 6 -3 -13 91.3830 17.1650 1 -3 -6 13 107.957 27.124 2 -6 3 13 63.1907 19.3721 3 6 -3 13 107.762 19.234 1 3 6 13 69.0511 19.3053 1 6 -5 -13 826.075 43.334 1 -5 -6 -13 670.879 40.022 1 5 6 -13 620.010 43.110 1 -6 5 -13 617.135 39.132 1 -6 5 -13 769.374 49.490 3 -5 -6 13 793.864 54.690 2 5 6 13 731.524 46.977 1 6 -5 13 735.889 40.374 1 -6 5 13 699.601 38.705 1 -7 -6 -13 1745.05 75.29 1 -6 7 -13 1771.80 83.12 3 7 6 -13 1661.78 75.87 1 6 -7 -13 1851.10 82.01 1 -6 7 -13 1642.57 74.41 1 -6 7 13 1646.64 74.89 1 7 6 13 1716.05 80.93 1 4 -7 -13 576.868 43.457 1 -7 -4 -13 485.288 33.992 1 -4 7 -13 531.422 33.887 1 7 4 -13 559.364 35.346 1 -4 7 13 561.700 35.740 1 7 4 13 635.082 43.123 1 2 -7 -13 531.629 41.060 1 -2 7 -13 515.311 31.595 1 -7 -2 -13 515.302 32.559 1 7 2 -13 562.496 33.452 1 7 2 13 504.558 38.373 1 -2 7 13 582.169 37.551 1 0 -7 -13 300.769 32.993 1 7 0 -13 327.345 24.923 1 -7 0 -13 286.912 24.967 1 0 7 -13 333.570 24.477 1 -7 0 -13 273.275 35.869 3 0 7 13 250.267 27.171 1 -7 0 13 304.173 21.097 1 -7 0 13 347.294 29.579 3 7 0 13 280.613 27.757 1 7 -2 -13 371.877 28.703 1 -7 2 -13 355.480 26.912 1 -7 2 -13 337.413 36.324 3 2 7 -13 360.704 28.046 1 -2 -7 -13 323.556 34.467 1 7 -2 13 386.387 31.642 1 -7 2 13 320.995 30.175 3 -2 -7 13 423.810 39.663 2 2 7 13 320.289 30.020 1 -7 2 13 299.967 24.153 1 -7 4 -13 884.297 43.995 1 4 7 -13 708.618 46.293 1 -7 4 -13 808.025 50.323 3 -4 -7 -13 813.384 45.902 1 7 -4 -13 780.467 43.576 1 7 -4 13 811.395 44.631 1 -7 4 13 740.412 41.526 1 -4 -7 13 735.740 54.831 2 4 7 13 825.954 47.095 1 -7 4 13 806.088 50.735 3 7 -6 -13 100.333 24.396 1 -7 6 -13 192.300 23.888 1 -7 6 -13 111.996 28.926 3 6 7 -13 139.043 27.623 1 -6 -7 -13 151.688 24.479 1 -7 6 13 129.962 23.947 1 6 7 13 181.435 31.605 1 -7 6 13 161.986 31.689 3 8 7 -13 244.025 31.945 1 -7 8 -13 212.510 29.409 1 7 -8 -13 244.428 35.347 1 -7 8 -13 258.988 38.339 3 -7 8 13 208.092 30.366 1 8 7 13 223.370 37.601 1 -8 -5 -13 48.7170 19.5799 1 -5 8 -13 42.4828 19.2974 1 8 5 -13 15.6556 19.7400 1 5 -8 -13 30.1912 26.5562 1 8 5 13 46.4222 24.5461 1 -5 8 13 57.2213 22.2847 1 -3 8 -13 -22.700 14.028 1 -8 -3 -13 -39.544 13.886 1 3 -8 -13 7.2889 24.7733 1 8 3 -13 14.0109 16.1261 1 8 3 13 -3.9199 21.3688 1 -3 8 13 4.6349 17.6007 1 -1 8 -13 338.874 28.047 1 -8 -1 -13 416.289 30.818 1 8 1 -13 376.230 29.106 1 -8 -1 -13 382.851 43.988 3 1 -8 -13 367.510 39.704 1 8 1 13 307.972 31.847 1 -1 8 13 392.681 34.048 1 -8 -1 13 394.496 35.256 3 -1 -8 -13 91.5449 26.5054 1 1 8 -13 113.978 19.155 1 -8 1 -13 125.009 20.029 1 8 -1 -13 112.780 20.476 1 -8 1 -13 108.823 31.573 3 -8 1 13 109.572 23.982 3 1 8 13 121.159 22.925 1 8 -1 13 111.414 24.351 1 -8 3 -13 43.2955 26.9955 3 -8 3 -13 16.8244 16.5156 1 3 8 -13 37.3691 20.4456 1 -3 -8 -13 68.1589 21.3268 1 8 -3 -13 36.7857 18.8796 1 -3 -8 13 37.8187 27.6572 2 3 8 13 51.1446 21.5925 1 -8 3 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46.003 1 -8 7 -15 543.035 51.350 3 7 8 15 645.679 52.154 1 -8 7 15 543.025 50.470 3 -8 9 -15 1022.23 59.95 1 -8 9 -15 922.309 68.481 3 9 8 -15 949.412 58.123 1 8 -9 -15 1079.95 69.50 1 9 8 15 921.759 63.790 1 -8 9 15 1136.68 74.86 3 6 -9 -15 328.245 40.983 1 9 6 -15 368.113 33.549 1 -6 9 -15 456.959 46.408 3 -6 9 -15 406.272 36.647 1 9 6 15 312.037 40.734 1 -6 9 15 355.132 36.223 1 -4 9 -15 183.214 25.841 1 4 -9 -15 175.071 36.008 1 -9 -4 -15 268.365 29.239 1 9 4 -15 246.272 27.342 1 9 4 15 210.390 31.478 1 -4 9 15 232.165 31.479 1 2 -9 -15 400.350 44.697 1 9 2 -15 464.305 35.126 1 -9 -2 -15 444.943 35.723 1 -2 9 -15 464.144 35.092 1 -2 9 15 503.969 38.614 1 9 2 15 501.998 41.393 1 -9 0 -15 353.347 31.466 1 0 -9 -15 374.872 43.180 1 -9 0 -15 423.387 48.807 3 9 0 -15 422.982 32.671 1 0 9 -15 401.708 32.578 1 -9 0 15 455.009 38.673 3 0 9 15 338.218 35.811 1 9 0 15 507.342 38.506 1 2 9 -15 1305.14 66.53 1 9 -2 -15 1444.81 66.71 1 -9 2 -15 1386.54 66.26 1 -9 2 -15 1393.80 81.71 3 -2 -9 -15 1516.90 73.56 1 -2 -9 15 1447.52 81.24 2 9 -2 15 1478.76 68.44 1 -9 2 15 1468.72 72.02 3 2 9 15 1402.18 69.19 1 -9 4 -15 425.369 47.477 3 9 -4 -15 516.433 39.947 1 4 9 -15 476.423 42.445 1 -9 4 -15 445.341 35.263 1 -9 4 15 497.985 43.419 3 -4 -9 15 513.708 50.028 2 4 9 15 461.054 42.134 1 -9 6 -15 469.986 49.638 3 -9 6 -15 452.761 38.742 1 9 -6 -15 463.815 43.160 1 6 9 -15 422.432 43.035 1 -9 6 15 475.385 46.920 3 6 9 15 460.179 46.177 1 -9 8 -15 45.1857 26.3770 1 8 9 -15 33.3615 28.4783 1 -9 8 -15 7.0258 32.0934 3 9 -8 -15 -7.7173 29.2205 1 8 9 15 2.1548 31.9266 1 -9 8 15 11.5167 35.0331 3 -9 10 -15 16.6789 28.4913 1 10 9 -15 28.9021 27.9466 1 -9 10 -15 -14.903 37.802 3 10 9 15 19.3115 32.3846 1 -9 10 15 15.5853 41.5221 3 -7 10 -15 6.2658 32.4407 3 -7 10 -15 33.5707 26.2404 1 7 -10 -15 59.3556 32.9339 1 10 7 -15 9.4016 24.8146 1 10 7 15 57.6369 32.2216 1 10 5 -15 679.507 44.188 1 5 -10 -15 668.989 59.828 1 -5 10 15 702.283 50.208 1 10 5 15 695.808 53.662 1 -10 -3 -15 87.9904 23.2631 1 10 3 -15 99.8719 22.4663 1 -3 10 -15 23.0174 21.2825 1 3 -10 -15 77.7831 30.1992 1 10 3 15 60.7607 25.8077 1 -3 10 15 41.4239 24.4573 1 -1 10 -15 12.1822 21.0917 1 -10 -1 -15 -20.424 16.350 1 10 1 -15 -9.7994 18.6309 1 1 -10 -15 -28.821 27.758 1 10 1 15 -6.3985 23.9642 1 -1 10 15 21.5647 22.5871 1 1 10 -15 367.539 36.422 1 -10 1 -15 387.624 50.210 3 10 -1 -15 381.211 34.911 1 -10 1 -15 449.864 36.834 1 10 -1 15 391.491 37.665 1 -10 1 15 366.652 38.757 3 -1 -10 15 414.014 46.455 2 1 10 15 377.623 38.370 1 10 -3 -15 24.1646 23.3860 1 3 10 -15 52.6393 28.3325 1 -10 3 -15 28.5938 21.8773 1 -10 3 -15 45.8966 34.7747 3 -10 3 15 14.6070 27.2585 3 10 -3 15 -6.1475 22.7329 1 -3 -10 15 61.8143 31.7960 2 3 10 15 21.8963 25.1392 1 -10 5 -15 3.2164 32.8629 3 -10 5 -15 -8.6316 21.7036 1 10 -5 -15 -7.3860 23.9512 1 5 10 -15 21.4622 30.8797 1 -10 5 15 27.2862 33.0437 3 5 10 15 3.1171 28.2257 1 -10 7 -15 401.427 53.559 3 10 -7 -15 420.796 46.973 1 -10 7 -15 489.763 43.688 1 7 10 -15 451.217 48.128 1 7 10 15 414.810 50.813 1 -10 7 15 401.463 52.739 3 9 10 -15 202.140 37.249 1 10 -9 -15 151.537 41.157 1 -10 9 -15 207.754 49.845 3 -10 9 -15 207.485 36.902 1 -10 9 15 240.125 50.571 3 9 10 15 251.484 45.979 1 11 6 -15 59.4090 25.9951 1 -6 11 -15 88.8223 30.1532 1 -6 11 -15 87.9678 38.2090 3 -6 11 15 61.2329 29.2207 1 11 6 15 77.5891 34.8118 1 -4 11 -15 132.846 30.157 1 11 4 -15 149.207 28.973 1 -4 11 15 183.948 32.780 1 11 4 15 162.224 34.797 1 -2 11 -15 287.557 34.920 1 11 2 -15 231.802 31.214 1 -2 11 15 225.308 35.027 1 11 2 15 210.321 35.096 1 11 0 -15 1192.69 63.19 1 -11 0 -15 1315.89 87.45 3 -11 0 -15 1228.69 63.12 1 0 11 -15 1212.32 64.97 1 11 0 15 1313.78 69.44 1 -11 0 15 1224.89 71.07 3 0 11 15 1189.55 66.79 1 11 -2 -15 610.788 45.344 1 -11 2 -15 552.202 59.729 3 -11 2 -15 639.058 44.237 1 2 11 -15 523.501 48.274 1 -11 2 15 572.818 51.694 3 -2 -11 15 643.169 58.082 2 11 -2 15 560.174 48.192 1 2 11 15 552.320 49.666 1 -11 4 -15 523.716 59.037 3 4 11 -15 543.550 52.210 1 11 -4 -15 579.218 48.255 1 -11 4 -15 518.971 44.166 1 -11 4 15 423.220 48.145 3 4 11 15 551.564 51.570 1 6 11 -15 -25.825 32.546 1 -11 6 -15 -34.333 38.332 3 11 -6 -15 -12.110 25.844 1 -11 6 -15 -35.056 24.338 1 6 11 15 -28.893 28.740 1 -11 6 15 30.0799 35.1711 3 12 5 -15 438.758 41.882 1 -5 12 15 360.654 45.689 1 12 5 15 439.539 48.012 1 -3 12 -15 667.807 51.565 1 12 3 -15 718.324 48.991 1 -3 12 15 701.299 54.758 1 12 3 15 670.409 52.391 1 12 1 -15 29.9551 24.5953 1 -1 12 -15 29.8310 29.4847 1 12 1 15 18.8391 29.6629 1 -1 12 15 30.9724 28.0287 1 -12 1 -15 -12.326 21.687 1 12 -1 -15 -2.2779 24.8601 1 1 12 -15 54.2450 30.6178 1 -12 1 -15 -72.436 39.736 3 -12 1 15 3.9177 32.0656 3 1 12 15 -28.292 29.174 1 -1 -12 15 88.2515 36.1312 2 12 -1 15 23.9284 28.3130 1 -12 3 -15 377.014 39.444 1 -12 3 -15 376.449 57.433 3 12 -3 -15 344.494 41.580 1 3 12 -15 344.705 47.667 1 -12 3 15 356.163 46.443 3 3 12 15 371.368 46.841 1 -12 5 -15 138.610 47.609 3 -12 5 -15 115.793 31.408 1 5 12 -15 155.156 42.503 1 12 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274.783 29.094 2 3 3 16 200.698 20.458 1 3 -3 16 215.622 16.770 1 -3 3 16 199.612 17.216 1 -4 -2 -16 21.9176 12.7386 1 2 -4 -16 19.9867 16.1422 1 -2 4 -16 20.3765 9.2158 1 4 2 -16 30.5867 8.6964 1 4 2 -16 22.2697 7.2316 1 -2 4 -16 22.1369 8.8848 1 -2 4 16 32.2469 12.7292 1 4 2 16 20.0468 13.6033 1 2 -4 16 22.2124 8.3979 1 4 0 -16 477.310 24.298 1 -4 0 -16 493.715 28.158 1 4 0 -16 499.349 23.795 1 0 -4 -16 505.778 33.747 1 0 4 -16 512.232 22.258 1 -4 0 -16 476.927 36.817 3 0 4 -16 460.321 21.454 1 -4 0 16 513.779 22.154 1 0 4 16 512.489 29.100 1 4 0 16 522.737 29.317 1 -4 0 16 459.200 25.765 3 -4 2 -16 59.4524 12.5681 1 2 4 -16 68.2045 8.6319 1 -4 2 -16 65.6286 17.1534 3 4 -2 -16 67.6160 12.8837 1 2 4 -16 61.1927 9.6402 1 -2 -4 -16 73.1118 18.6534 1 -4 2 16 54.2179 13.2492 3 -4 2 16 66.7826 11.8013 1 4 -2 16 33.6730 11.8381 1 2 4 16 66.4018 15.3463 1 -2 -4 16 60.6720 21.9973 2 -4 4 -16 -2.6893 14.5487 3 -4 -4 -16 24.3880 16.9344 1 4 -4 -16 20.6305 14.6152 1 4 4 -16 -2.8280 8.6985 1 4 4 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19.6197 3 -5 3 -16 11.7886 13.2375 1 3 5 -16 41.8287 12.4389 1 3 5 -16 26.3541 13.5219 1 -5 3 16 2.7986 11.6825 1 -3 -5 16 28.6808 24.3261 2 -5 3 16 40.0437 16.9962 3 5 -3 16 44.7303 13.9825 1 3 5 16 2.1482 15.1974 1 5 5 -16 133.508 20.208 1 -5 5 -16 166.470 25.203 3 -5 5 -16 148.194 19.697 1 5 -5 -16 113.548 21.758 1 -5 -5 -16 143.407 22.335 1 5 5 16 104.111 25.312 1 -5 5 16 110.987 18.522 1 -5 -5 16 214.896 32.816 2 5 -5 16 119.716 18.282 1 4 -6 -16 601.490 39.632 1 -4 6 -16 558.303 32.679 1 6 4 -16 559.051 31.720 1 -6 -4 -16 511.089 34.796 1 -4 6 16 474.062 34.904 1 6 4 16 562.773 38.354 1 6 2 -16 712.958 35.384 1 -2 6 -16 758.336 35.034 1 2 -6 -16 708.911 45.147 1 -6 -2 -16 750.508 40.317 1 -2 6 16 734.874 40.913 1 6 2 16 697.304 40.592 1 0 6 -16 337.659 23.026 1 0 6 -16 352.998 22.076 1 -6 0 -16 343.424 36.179 3 0 -6 -16 315.970 34.517 1 6 0 -16 355.575 24.855 1 -6 0 -16 382.622 27.613 1 -6 0 16 307.402 25.954 3 6 0 16 354.582 29.528 1 0 6 16 340.123 28.762 1 -2 -6 -16 26.9862 22.2737 1 2 6 -16 42.9925 13.4645 1 6 -2 -16 37.8880 14.7963 1 -6 2 -16 10.7159 13.2924 1 2 6 -16 30.5139 13.9838 1 -6 2 -16 32.1191 22.2061 3 6 -2 16 8.4506 14.2410 1 -2 -6 16 14.9799 23.2998 2 2 6 16 36.3935 19.0611 1 -6 2 16 -3.3489 16.0675 3 -6 2 16 38.1350 13.2948 1 4 6 -16 28.9835 18.6810 1 6 -4 -16 5.7391 17.2802 1 -6 4 -16 9.2341 21.3058 3 -4 -6 -16 -2.2022 20.4284 1 -6 4 -16 -24.306 14.267 1 4 6 16 -2.3398 20.1340 1 6 -4 16 -7.5033 14.9080 1 -6 4 16 -5.3088 14.3159 1 -4 -6 16 -10.034 25.177 2 -6 4 16 11.2487 18.4089 3 6 -6 -16 8.2601 20.7320 1 -6 -6 -16 15.7256 18.0501 1 -6 6 -16 51.1724 17.9957 1 6 6 -16 4.8090 17.3497 1 -6 6 -16 35.6779 23.3668 3 -6 6 16 3.4572 17.2011 1 6 6 16 -6.7130 21.4741 1 -5 7 -16 590.863 47.701 3 5 -7 -16 606.901 46.102 1 7 5 -16 765.287 40.548 1 -5 7 -16 682.550 39.390 1 -7 -5 -16 691.432 42.754 1 7 5 16 720.906 47.287 1 -5 7 16 626.935 39.896 1 -3 7 -16 1124.95 51.11 1 7 3 -16 1150.17 51.10 1 3 -7 -16 1090.29 62.18 1 -7 -3 -16 1145.41 55.43 1 7 3 16 1071.18 56.49 1 -3 7 16 1195.38 56.43 1 -7 -1 -16 930.518 47.117 1 7 1 -16 1026.51 45.56 1 -7 -1 -16 981.347 64.920 3 1 -7 -16 933.136 58.551 1 -1 7 -16 954.828 44.057 1 7 1 16 974.445 50.078 1 -1 7 16 959.969 50.073 1 -7 -1 16 972.697 50.397 3 -1 -7 -16 712.745 49.719 1 -7 1 -16 609.687 48.248 3 7 -1 -16 686.477 36.178 1 1 7 -16 607.732 33.296 1 -7 1 -16 681.969 37.976 1 1 7 16 622.919 38.966 1 -7 1 16 613.517 39.791 3 -1 -7 16 605.696 50.200 2 7 -1 16 607.672 40.019 1 -7 3 -16 26.6849 16.9330 1 3 7 -16 -6.4066 17.2551 1 -7 3 -16 14.6381 23.8084 3 -3 -7 -16 12.0004 20.7668 1 7 -3 -16 -39.144 15.305 1 7 -3 16 13.7486 17.1704 1 -7 3 16 3.6089 18.7455 3 3 7 16 15.9390 18.8343 1 -7 3 16 -4.1826 13.5721 1 -3 -7 16 13.3204 25.8046 2 -7 5 -16 96.2937 27.6147 3 -7 5 -16 126.616 20.673 1 -5 -7 -16 94.4079 22.5294 1 7 -5 -16 108.244 24.316 1 5 7 -16 98.3180 23.6328 1 -5 -7 16 57.9720 29.7268 2 -7 5 16 87.0070 25.0360 3 5 7 16 111.053 24.865 1 -7 5 16 120.357 19.678 1 7 -7 -16 15.5288 23.0372 1 -7 7 -16 1.0901 20.1483 1 -7 7 -16 3.0495 26.3424 3 7 7 -16 18.2891 21.6241 1 -7 7 16 -8.2818 20.1475 1 7 7 16 0.3395 26.9729 1 -6 8 -16 92.9490 29.5520 3 6 -8 -16 60.1613 29.3832 1 8 6 -16 106.479 23.087 1 -6 8 -16 98.0739 23.7759 1 -6 8 16 60.8513 23.9153 1 8 6 16 103.347 27.983 1 4 -8 -16 1053.91 62.47 1 8 4 -16 1113.05 51.30 1 -4 8 -16 893.656 49.539 1 -8 -4 -16 1045.17 54.05 1 -4 8 16 1108.98 56.11 1 8 4 16 981.468 57.550 1 -8 -2 -16 2005.48 83.06 1 2 -8 -16 1962.21 92.48 1 -2 8 -16 1917.02 79.23 1 8 2 -16 1966.42 80.32 1 -2 8 16 1956.83 84.60 1 8 2 16 1989.65 85.44 1 -8 0 -16 401.883 44.554 3 -8 0 -16 325.626 29.100 1 8 0 -16 385.342 28.994 1 0 8 -16 433.339 29.606 1 0 -8 -16 401.471 41.077 1 0 8 16 366.067 33.125 1 -8 0 16 374.316 33.415 3 8 0 16 367.503 33.446 1 -2 -8 -16 72.2315 27.4277 1 8 -2 -16 61.6743 18.9819 1 -8 2 -16 44.8502 27.9981 3 -8 2 -16 49.7977 17.8259 1 2 8 -16 80.6900 20.9871 1 -8 2 16 55.3904 21.5577 3 8 -2 16 81.1932 22.1423 1 -2 -8 16 74.5494 28.7089 2 2 8 16 78.0208 23.2179 1 -8 4 -16 285.708 35.491 3 -8 4 -16 261.780 27.359 1 -4 -8 -16 257.165 33.441 1 4 8 -16 238.577 30.449 1 8 -4 -16 255.361 29.588 1 -8 4 16 234.168 31.819 3 4 8 16 221.988 30.353 1 -4 -8 16 263.882 38.107 2 8 -6 -16 213.750 32.039 1 6 8 -16 144.760 30.872 1 -8 6 -16 171.701 26.714 1 -8 6 -16 147.833 34.459 3 6 8 16 206.007 33.179 1 -8 6 16 157.526 32.854 3 -8 8 -16 136.700 37.124 3 8 8 -16 156.210 29.309 1 8 -8 -16 226.001 37.394 1 -8 8 -16 105.500 26.601 1 8 8 16 184.330 37.305 1 -8 8 16 231.442 40.910 3 -7 9 -16 5.4884 31.0454 3 -7 9 -16 29.1392 24.0059 1 7 -9 -16 -52.245 25.172 1 9 7 -16 51.4529 24.1255 1 9 7 16 36.4145 27.7110 1 9 5 -16 906.765 50.340 1 5 -9 -16 956.042 60.495 1 -5 9 -16 919.026 50.798 1 9 5 16 894.840 58.151 1 -5 9 16 851.335 53.950 1 3 -9 -16 1659.58 87.86 1 -9 -3 -16 1816.11 78.45 1 9 3 -16 1693.88 75.89 1 9 3 16 1765.01 83.02 1 -3 9 16 1824.19 80.46 1 -9 -1 -16 1489.72 66.31 1 9 1 -16 1411.96 63.59 1 -1 9 -16 1361.41 62.98 1 1 -9 -16 1333.19 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40.579 1 11 0 -19 -10.398 20.883 1 -11 0 -19 -76.585 37.320 3 0 11 -19 9.1193 25.5841 1 -11 0 -19 0.8855 22.1945 1 11 0 19 15.5462 25.4229 1 0 11 19 -5.9110 26.4746 1 0 -11 19 25.8987 37.7584 2 -11 0 19 -56.577 25.657 3 -11 2 -19 132.674 28.426 1 2 11 -19 107.833 32.612 1 11 -2 -19 144.593 28.554 1 -11 2 -19 114.179 43.876 3 -2 -11 19 93.9111 36.9592 2 -11 2 19 142.290 33.572 3 2 11 19 118.521 31.783 1 4 11 -19 43.8276 33.4041 1 11 -4 -19 28.6293 27.5644 1 -11 4 -19 22.9664 25.8490 1 -11 4 -19 21.9611 38.7092 3 4 11 19 -22.429 26.688 1 -11 4 19 7.2769 30.4380 3 -4 -11 19 12.9527 36.4254 2 11 -6 -19 40.7421 31.1378 1 -11 6 -19 -22.369 26.048 1 -11 6 -19 32.7368 41.6991 3 6 11 -19 -13.163 30.242 1 -11 6 19 24.5627 33.0802 3 6 11 19 -5.5987 32.3018 1 -5 12 -19 -20.558 27.214 1 12 5 -19 -27.390 23.730 1 12 5 19 27.8274 32.0736 1 -3 12 -19 147.114 32.591 1 12 3 -19 130.799 28.071 1 -3 12 19 68.8700 32.7253 1 12 3 19 108.694 31.130 1 12 1 -19 331.251 37.216 1 -1 12 -19 304.993 40.704 1 -1 12 19 285.728 39.985 1 12 1 19 351.763 42.373 1 -12 1 -19 555.586 68.367 3 12 -1 -19 640.082 48.959 1 1 12 -19 521.576 51.907 1 -12 1 -19 615.782 45.136 1 1 12 19 626.865 53.175 1 -1 -12 19 652.781 62.674 2 -12 1 19 553.997 51.930 3 -12 3 -19 309.700 38.975 1 3 12 -19 240.142 43.195 1 -12 3 -19 327.444 56.387 3 12 -3 -19 317.936 40.726 1 -12 3 19 354.159 44.919 3 3 12 19 354.845 46.610 1 5 12 -19 24.2371 36.2808 1 -12 5 -19 11.3118 43.4067 3 12 -5 -19 4.7176 30.8374 1 -12 5 -19 3.5287 25.1163 1 5 12 19 34.3255 34.3404 1 -12 5 19 25.2465 35.7682 3 -2 13 -19 343.200 46.397 1 13 2 -19 357.426 39.974 1 -2 13 19 348.305 46.217 1 13 0 -19 -20.156 25.519 1 0 13 -19 -65.400 32.108 1 0 -13 19 32.1620 42.6231 2 0 13 19 -8.0748 31.7808 1 2 13 -19 19.5045 37.6856 1 13 -2 -19 77.8690 32.2911 1 -13 2 -19 56.6677 51.4345 3 2 13 19 55.8226 36.5931 1 0 0 -20 4455.66 152.85 1 0 0 -20 4431.70 152.84 1 0 0 20 3669.87 182.45 2 0 0 20 4544.96 148.72 1 1 -1 -20 2016.91 73.28 1 -1 1 -20 1684.78 71.67 3 1 1 -20 1895.99 69.43 1 -1 1 -20 1897.18 71.08 1 -1 1 -20 1861.90 71.29 1 1 -1 -20 1921.66 73.26 1 1 1 -20 1887.80 68.52 1 -1 -1 -20 1850.93 74.83 1 1 -1 20 1941.37 88.50 2 1 1 20 1991.68 71.28 1 1 1 20 1930.60 86.85 2 -1 -1 20 1855.08 90.17 2 0 -2 -20 4974.97 181.19 1 2 0 -20 4981.56 175.10 1 -2 0 -20 5083.13 178.98 1 0 2 -20 5265.94 173.73 1 0 2 -20 4966.43 176.45 3 0 2 -20 4858.32 173.90 1 2 0 -20 5108.54 175.60 1 2 0 20 4723.87 211.86 2 2 0 20 5377.47 177.02 1 0 2 20 4755.44 176.84 1 0 -2 20 5211.47 215.43 2 -2 2 -20 1249.71 50.61 1 -2 -2 -20 1190.68 56.06 1 -2 2 -20 1307.61 54.02 3 -2 2 -20 1283.93 51.50 1 2 -2 -20 1307.60 54.61 1 -2 -2 20 1287.54 67.02 2 -2 2 20 1375.67 51.25 1 2 -2 20 1274.40 48.31 1 2 2 20 1286.18 60.88 2 2 2 20 1321.82 53.85 1 -1 3 -20 118.960 11.500 1 -1 3 -20 124.194 13.553 3 3 1 -20 144.818 10.379 1 3 1 -20 136.509 10.292 1 1 -3 -20 104.419 19.911 1 -1 3 -20 109.574 11.145 1 -3 -1 -20 123.905 17.938 1 3 1 20 124.282 15.732 1 -1 3 20 151.095 15.993 1 3 1 20 174.246 18.745 2 -3 1 -20 368.084 27.994 3 -3 1 -20 354.076 23.079 1 3 -1 -20 372.010 22.455 1 -1 -3 -20 359.480 29.879 1 -3 1 20 379.348 19.726 3 -3 1 20 412.922 19.834 1 -1 -3 20 327.945 33.296 2 1 3 20 393.836 25.359 1 3 -1 20 392.271 22.111 1 -3 -3 -20 -7.1996 17.8161 1 3 3 -20 21.3234 5.0372 1 3 3 -20 15.5204 6.1526 1 3 -3 -20 15.6879 14.3064 1 -3 3 -20 18.1159 14.3368 3 -3 3 -20 2.5881 10.4616 1 -3 -3 20 14.6272 22.1668 2 3 -3 20 -2.0013 2.8897 1 3 3 20 16.3580 15.0996 1 -3 3 20 -8.7741 10.5549 1 -2 4 -20 56.4598 10.6393 1 4 2 -20 22.9655 8.2865 1 2 -4 -20 58.4074 18.1605 1 -4 -2 -20 57.8297 16.4386 1 -2 4 -20 35.7520 13.5896 3 -2 4 -20 38.8249 10.6719 1 4 2 -20 43.5268 7.8627 1 4 2 20 42.9778 14.5276 2 -2 4 20 37.8734 13.4003 1 4 2 20 56.5818 15.9653 1 0 -4 -20 155.701 24.648 1 -4 0 -20 178.413 23.933 3 4 0 -20 134.912 13.246 1 0 4 -20 152.802 11.869 1 4 0 -20 159.593 13.307 1 0 4 -20 151.666 10.781 1 -4 0 -20 160.393 17.942 1 4 0 20 145.773 17.445 1 0 -4 20 157.118 26.523 2 -4 0 20 148.996 13.734 3 0 4 20 136.142 17.637 1 -2 -4 -20 448.093 34.593 1 -4 2 -20 423.576 26.829 1 -4 2 -20 481.522 36.437 3 4 -2 -20 450.463 27.187 1 2 4 20 444.453 30.523 1 -2 -4 20 454.713 41.832 2 -4 2 20 441.441 26.733 3 -4 2 20 442.233 24.905 1 4 -2 20 464.727 25.626 1 -4 4 -20 87.6549 15.9834 1 -4 -4 -20 151.551 25.385 1 -4 4 -20 109.945 20.380 3 4 4 -20 97.7422 13.3374 1 4 -4 -20 102.982 20.349 1 4 4 -20 129.607 11.993 1 4 -4 20 110.613 13.906 1 -4 4 20 153.835 18.391 1 -4 -4 20 111.601 29.614 2 4 4 20 124.453 21.079 1 -3 5 -20 290.901 26.147 3 -5 -3 -20 335.468 29.393 1 3 -5 -20 313.120 31.173 1 5 3 -20 370.511 20.514 1 -3 5 -20 306.027 22.897 1 5 3 -20 285.236 20.760 1 -3 5 20 338.533 25.904 1 5 3 20 338.777 23.052 2 5 3 20 303.396 27.822 1 -1 5 -20 95.5413 11.8296 1 5 1 -20 142.361 12.726 1 -1 5 -20 123.976 12.938 1 5 1 -20 89.0330 12.5906 1 -5 -1 -20 93.8046 17.5546 1 1 -5 -20 106.707 25.136 1 -1 5 20 74.1759 16.7412 1 5 1 20 114.584 17.793 1 -5 1 -20 11.7566 12.7763 1 5 -1 -20 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47.47 1 6 2 20 1157.66 53.21 1 -2 6 20 1121.03 53.45 1 0 6 -20 423.622 24.032 1 -6 0 -20 494.790 41.908 3 6 0 -20 418.186 26.838 1 -6 0 -20 462.577 31.516 1 0 -6 -20 407.841 38.046 1 6 0 20 394.171 31.209 1 -6 0 20 431.626 29.510 3 0 6 20 462.782 33.096 1 2 6 -20 285.525 22.340 1 6 -2 -20 304.693 25.266 1 -2 -6 -20 311.722 35.778 1 -6 2 -20 236.354 24.449 1 -6 2 -20 281.249 32.230 3 2 6 -20 285.827 20.881 1 -2 -6 20 286.027 37.051 2 2 6 20 304.133 28.542 1 6 -2 20 245.730 24.749 1 -6 2 20 324.858 25.262 3 -6 4 -20 16.1934 22.0958 3 -4 -6 -20 60.0903 25.0855 1 4 6 -20 18.3754 16.5753 1 -6 4 -20 40.7558 17.1938 1 6 -4 -20 49.9594 18.8405 1 -6 4 20 31.8135 19.1818 3 -4 -6 20 -0.8194 26.1862 2 4 6 20 4.4800 19.1943 1 -6 6 -20 80.5453 26.1972 3 6 6 -20 87.6110 19.2797 1 6 -6 -20 31.2060 23.5391 1 -6 6 -20 64.9339 19.7776 1 -6 -6 -20 64.4604 24.0894 1 6 6 20 77.2317 25.3259 1 7 5 -20 373.556 27.641 1 5 -7 -20 427.207 38.798 1 -5 7 -20 368.974 36.027 3 -5 7 -20 333.737 29.821 1 -7 -5 -20 461.453 37.810 1 -5 7 20 341.781 32.344 1 7 5 20 305.388 33.298 1 3 -7 -20 873.778 55.418 1 -7 -3 -20 891.387 49.184 1 7 3 -20 833.202 41.729 1 -3 7 -20 863.865 42.340 1 7 3 20 860.638 48.966 1 -3 7 20 896.053 48.838 1 1 -7 -20 636.698 47.326 1 -1 7 -20 763.600 35.932 1 7 1 -20 734.100 37.056 1 -7 -1 -20 680.910 41.442 1 -1 7 20 629.089 42.175 1 7 1 20 687.290 40.405 1 7 -1 -20 255.635 24.016 1 1 7 -20 271.497 22.146 1 -7 1 -20 244.433 25.622 1 -7 1 -20 264.870 36.372 3 -1 -7 -20 236.654 35.686 1 1 7 20 346.135 31.780 1 7 -1 20 272.475 27.296 1 -1 -7 20 280.237 36.927 2 -7 1 20 302.403 26.770 3 3 7 -20 -2.1083 17.4007 1 -3 -7 -20 -24.515 23.076 1 -7 3 -20 15.0316 24.5970 3 7 -3 -20 5.0236 16.4067 1 -7 3 -20 -0.3994 16.2146 1 -7 3 20 3.4265 17.8783 3 3 7 20 -3.0292 18.5267 1 7 -3 20 4.3356 15.7257 1 -3 -7 20 -29.103 24.023 2 -7 5 -20 46.9773 19.6272 1 7 -5 -20 43.0451 21.8800 1 5 7 -20 4.2554 19.6260 1 -7 5 -20 19.3921 24.9698 3 -5 -7 -20 -6.1428 22.6206 1 -5 -7 20 -2.8532 29.4358 2 -7 5 20 29.1037 23.1530 3 5 7 20 18.3081 21.0657 1 -7 7 -20 -0.2076 19.9807 1 7 -7 -20 -8.6643 24.9530 1 -7 7 -20 -6.9329 27.3874 3 -7 -7 -20 18.2083 23.9857 1 7 7 -20 -2.4576 18.8098 1 7 7 20 72.5938 27.6358 1 6 -8 -20 269.902 37.037 1 -6 8 -20 269.757 30.956 1 8 6 -20 277.379 27.549 1 -8 -6 -20 335.044 36.059 1 -6 8 -20 260.274 36.714 3 8 6 20 236.254 33.516 1 4 -8 -20 1928.22 95.99 1 8 4 -20 1886.27 81.96 1 -8 -4 -20 2020.28 88.51 1 -4 8 -20 2075.09 85.06 1 8 4 20 2081.54 90.12 1 -4 8 20 2324.06 91.26 1 8 2 -20 2253.23 89.06 1 2 -8 -20 2241.95 101.68 1 -2 8 -20 2200.60 88.85 1 -8 -2 -20 2237.78 93.98 1 8 2 20 2234.58 94.51 1 -2 8 20 2340.73 95.34 1 -8 0 -20 2020.47 84.44 1 0 -8 -20 1982.90 93.40 1 8 0 -20 1873.05 81.00 1 -8 0 -20 2038.72 100.20 3 0 8 -20 2034.77 80.31 1 -8 0 20 2184.32 85.07 3 8 0 20 1941.16 86.26 1 0 8 20 1992.61 87.06 1 8 -2 -20 73.2197 19.8372 1 -2 -8 -20 114.371 31.546 1 2 8 -20 97.9049 21.9855 1 -8 2 -20 97.1396 20.8729 1 -8 2 -20 125.620 30.438 3 -8 2 20 69.7165 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41.284 1 -3 9 20 782.011 49.302 1 9 3 20 698.300 48.527 1 9 1 -20 581.572 36.280 1 1 -9 -20 508.030 50.355 1 -1 9 -20 513.515 36.717 1 -9 -1 -20 618.970 41.084 1 9 1 20 538.486 39.565 1 -1 9 20 552.195 44.495 1 -9 1 -20 43.5157 20.0691 1 -1 -9 -20 62.4603 32.1033 1 -9 1 -20 54.0270 34.2289 3 1 9 -20 69.0534 22.4326 1 9 -1 -20 70.4011 20.3477 1 -9 1 20 85.7909 24.2329 3 1 9 20 77.7196 25.6372 1 9 -1 20 64.6552 22.1884 1 -1 -9 20 60.7070 31.3143 2 3 9 -20 101.960 27.590 1 9 -3 -20 163.031 26.587 1 -3 -9 -20 183.467 32.630 1 -9 3 -20 112.282 35.178 3 -9 3 -20 145.569 24.153 1 -3 -9 20 117.944 34.086 2 -9 3 20 160.749 28.883 3 3 9 20 140.803 30.622 1 -9 5 -20 274.415 42.508 3 9 -5 -20 281.825 35.120 1 -9 5 -20 212.830 29.716 1 5 9 -20 248.004 33.145 1 5 9 20 339.928 39.548 1 -5 -9 20 279.503 41.977 2 -9 5 20 232.586 35.490 3 9 -7 -20 183.698 36.035 1 -9 7 -20 157.659 31.196 1 7 9 -20 218.364 30.956 1 -9 7 -20 194.835 40.839 3 7 9 20 188.497 38.391 1 -9 7 20 201.746 37.832 3 -9 9 -20 12.5436 29.2134 1 9 9 -20 23.1714 25.7215 1 -9 9 -20 99.3038 40.4619 3 9 -9 -20 12.7702 33.6866 1 9 9 20 -7.1610 30.8639 1 -9 9 20 12.2653 39.1672 3 -8 10 -20 36.6363 28.6183 1 -8 10 -20 7.4895 35.6195 3 8 -10 -20 29.8953 36.9904 1 10 8 -20 17.3533 25.3101 1 10 8 20 9.1357 31.9030 1 -6 10 -20 254.466 41.282 3 -6 10 -20 223.578 33.483 1 6 -10 -20 250.288 43.001 1 10 6 -20 295.115 31.887 1 10 6 20 311.893 40.774 1 10 4 -20 1157.03 59.34 1 4 -10 -20 1312.05 75.57 1 -4 10 -20 1236.27 62.80 1 -4 10 20 1244.43 68.34 1 10 4 20 1270.27 69.57 1 2 -10 -20 1847.03 94.42 1 -10 -2 -20 1948.58 85.18 1 10 2 -20 1879.44 80.97 1 10 2 20 1882.58 87.04 1 -2 10 20 1886.67 88.36 1 0 10 -20 459.795 39.169 1 -10 0 -20 442.157 37.906 1 -10 0 -20 504.436 56.939 3 0 -10 -20 481.607 51.615 1 10 0 -20 482.275 36.566 1 10 0 20 465.501 41.548 1 0 -10 20 461.331 52.070 2 -10 0 20 483.671 41.052 3 0 10 20 396.698 40.302 1 2 10 -20 19.8551 25.5845 1 -10 2 -20 67.6890 33.7861 3 -10 2 -20 -7.2008 19.6740 1 10 -2 -20 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34.361 1 -2 1 -23 742.677 35.073 1 1 2 -23 717.730 29.070 1 -1 -2 -23 660.840 40.050 1 -2 1 -23 703.484 37.068 3 -2 1 -23 744.028 37.128 1 2 -1 -23 670.482 34.087 1 1 2 -23 733.921 29.185 1 1 2 23 726.037 33.964 1 -2 1 23 710.060 30.383 1 1 2 23 718.893 42.836 2 -1 -2 23 817.819 48.456 2 2 -1 23 722.473 45.303 2 2 -1 23 599.660 28.895 1 -2 3 -23 295.422 22.089 3 -2 3 -23 310.576 20.969 1 -2 3 -23 299.537 20.888 1 -3 -2 -23 287.876 28.680 1 2 -3 -23 301.895 26.133 1 3 2 -23 287.975 14.816 1 3 2 -23 312.041 14.984 1 -3 -2 23 311.998 33.990 2 3 2 23 307.994 23.855 1 -2 3 23 320.137 21.869 1 3 2 23 312.552 26.718 2 0 3 -23 291.217 19.747 3 0 3 -23 337.452 17.424 1 3 0 -23 361.266 20.713 1 0 -3 -23 356.283 30.550 1 3 0 -23 384.958 21.087 1 0 3 -23 336.083 17.670 1 -3 0 -23 343.712 26.307 1 0 -3 23 361.352 34.713 2 3 0 23 330.853 29.988 2 3 0 23 388.489 23.464 1 0 3 23 363.427 24.292 1 -2 -3 -23 1168.45 56.77 1 3 -2 -23 1155.63 50.51 1 -3 2 -23 1215.05 49.62 1 -3 2 -23 1147.13 52.85 3 2 3 23 1175.42 51.69 1 -3 2 23 1140.53 46.94 1 -2 -3 23 1115.50 66.34 2 -3 4 -23 2572.75 101.87 3 -4 -3 -23 2566.35 106.47 1 4 3 -23 2659.31 92.80 1 3 -4 -23 2563.93 104.16 1 -3 4 -23 2385.97 97.36 1 4 3 -23 2588.02 92.79 1 4 3 23 2608.27 102.34 1 -3 4 23 2616.38 99.58 1 -4 -3 23 3028.31 128.54 2 4 3 23 2721.59 112.81 2 1 -4 -23 1886.18 80.28 1 4 1 -23 1855.36 67.39 1 -4 -1 -23 1760.71 75.24 1 -1 4 -23 1848.38 67.52 1 -1 4 -23 1851.56 71.28 3 4 1 -23 1739.79 67.04 1 4 1 23 1874.21 73.18 1 -1 4 23 1767.68 72.74 1 4 1 23 1838.79 85.40 2 4 -1 -23 2398.33 90.49 1 -1 -4 -23 2313.16 99.92 1 1 4 -23 2599.81 85.04 1 4 -1 -23 2327.70 90.71 1 -4 1 -23 2421.99 100.44 3 1 4 -23 2380.10 84.70 1 -4 1 -23 2437.93 94.15 1 1 4 23 2515.27 94.86 1 -4 1 23 2431.35 89.28 3 -1 -4 23 2587.14 117.33 2 4 -1 23 2379.65 91.36 1 -4 3 -23 66.3784 15.2525 1 4 -3 -23 67.6861 17.0712 1 -3 -4 -23 41.0963 21.9832 1 -4 3 -23 76.8766 19.0999 3 -4 3 23 61.9019 14.4058 1 4 -3 23 65.2779 12.1080 1 -3 -4 23 43.0608 26.5525 2 3 4 23 45.3931 18.1792 1 4 -5 -23 112.208 22.961 1 -4 5 -23 155.185 24.125 3 -5 -4 -23 188.203 26.849 1 -4 5 -23 137.237 19.633 1 5 4 -23 142.525 14.472 1 5 4 23 122.870 22.027 1 -4 5 23 143.437 20.725 1 -2 5 -23 135.626 19.052 3 5 2 -23 123.466 13.303 1 2 -5 -23 140.610 26.296 1 -5 -2 -23 147.342 24.031 1 -2 5 -23 136.500 15.493 1 5 2 23 150.293 20.355 2 -2 5 23 133.769 19.912 1 5 2 23 141.029 20.803 1 0 5 -23 152.750 12.682 1 -5 0 -23 143.889 28.167 3 -5 0 -23 148.862 21.466 1 0 5 -23 136.212 11.669 1 0 -5 -23 171.505 29.244 1 5 0 -23 144.658 15.370 1 0 5 23 116.586 18.720 1 -5 0 23 140.343 15.374 3 5 0 23 161.391 19.298 1 0 -5 23 188.232 30.873 2 -5 2 -23 201.580 22.544 1 2 5 -23 233.962 16.100 1 -2 -5 -23 176.854 29.810 1 2 5 -23 231.383 15.530 1 -5 2 -23 244.885 28.600 3 5 -2 -23 206.026 21.737 1 -2 -5 23 216.399 33.877 2 5 -2 23 243.846 21.114 1 2 5 23 236.952 24.556 1 -5 2 23 237.915 19.805 3 -5 4 -23 39.0702 21.5717 3 -4 -5 -23 69.1308 25.7610 1 5 -4 -23 39.1574 19.1843 1 -5 4 -23 10.4073 14.8126 1 4 5 -23 32.6801 12.5899 1 4 5 23 4.6745 17.5966 1 -4 -5 23 35.6013 26.5174 2 -5 6 -23 388.205 29.527 1 -6 -5 -23 375.933 38.310 1 5 -6 -23 331.325 35.593 1 6 5 -23 360.801 25.074 1 -5 6 -23 304.008 33.050 3 6 5 23 388.934 35.451 1 -6 -3 -23 564.321 38.718 1 3 -6 -23 560.691 44.196 1 -3 6 -23 546.930 39.855 3 -3 6 -23 577.776 32.983 1 6 3 -23 563.845 28.801 1 -3 6 23 590.939 35.665 1 6 3 23 542.487 37.430 1 -6 -1 -23 2045.97 86.58 1 -1 6 -23 2078.39 78.12 1 1 -6 -23 2118.02 93.33 1 6 1 -23 2089.30 79.00 1 6 1 23 1957.17 83.33 1 -1 6 23 2117.84 85.51 1 6 -1 -23 351.401 26.579 1 -6 1 -23 361.854 37.277 3 1 6 -23 335.379 21.380 1 -1 -6 -23 372.461 40.050 1 -6 1 -23 300.782 28.813 1 -6 1 23 352.630 27.606 3 6 -1 23 359.884 27.971 1 1 6 23 346.651 30.443 1 -1 -6 23 375.134 40.802 2 -6 3 -23 73.8865 18.5290 1 -3 -6 -23 78.1529 26.3825 1 -6 3 -23 104.064 26.473 3 3 6 -23 77.7607 16.0998 1 6 -3 -23 69.6472 18.5654 1 3 6 23 75.8591 22.2590 1 -3 -6 23 107.181 30.046 2 -6 3 23 63.7442 18.0120 3 -5 -6 -23 1036.04 59.19 1 -6 5 -23 923.193 56.457 3 -6 5 -23 986.378 49.110 1 5 6 -23 935.915 44.291 1 6 -5 -23 1022.46 53.81 1 5 6 23 876.494 52.033 1 -5 -6 23 908.770 64.772 2 6 -7 -23 1029.94 62.05 1 -7 -6 -23 1247.17 63.41 1 -6 7 -23 1201.29 66.96 3 -6 7 -23 1017.04 55.86 1 7 6 23 1182.71 63.09 1 -4 7 -23 1138.59 53.95 1 7 4 -23 1175.09 51.36 1 4 -7 -23 1118.69 63.42 1 -7 -4 -23 1166.00 60.59 1 -4 7 -23 1188.93 60.76 3 7 4 23 1263.97 60.77 1 -4 7 23 1165.14 58.55 1 -7 -2 -23 36.2012 19.4743 1 -2 7 -23 50.3261 15.3511 1 2 -7 -23 29.0298 26.2846 1 7 2 -23 33.9366 13.8209 1 -2 7 23 13.5840 17.8781 1 7 2 23 14.5432 18.4542 1 0 7 -23 36.4666 13.7310 1 -7 0 -23 48.0564 19.6589 1 7 0 -23 27.7466 14.5664 1 -7 0 -23 3.6211 27.5010 3 0 -7 -23 25.1897 26.3091 1 -7 0 23 75.7314 17.4219 3 0 -7 23 34.8401 28.9049 2 7 0 23 41.4268 18.3695 1 0 7 23 58.1768 21.5804 1 -7 2 -23 760.705 55.959 3 2 7 -23 813.006 39.662 1 7 -2 -23 807.613 43.003 1 -7 2 -23 777.932 44.272 1 -2 -7 -23 704.759 51.738 1 2 7 23 792.205 47.671 1 -7 2 23 810.047 41.782 3 -2 -7 23 751.932 57.404 2 7 -4 -23 78.3419 21.9483 1 -7 4 -23 109.847 22.124 1 4 7 -23 130.217 20.798 1 -4 -7 -23 70.3741 28.2246 1 -7 4 -23 115.376 29.222 3 4 7 23 57.2885 22.6679 1 -7 4 23 69.5282 21.0708 3 -4 -7 23 109.590 32.781 2 -7 6 -23 50.4768 28.1844 3 7 -6 -23 41.7213 25.0836 1 -7 6 -23 31.4376 21.0775 1 -6 -7 -23 66.1751 26.0912 1 6 7 -23 90.0008 19.7448 1 6 7 23 50.0569 24.3434 1 -7 6 23 29.2685 24.3636 3 -7 8 -23 38.0202 23.1305 1 8 7 -23 11.7098 18.8552 1 7 -8 -23 14.0365 27.7935 1 -7 8 -23 -15.760 28.188 3 8 7 23 19.3078 26.7694 1 -5 8 -23 49.4771 20.9207 1 5 -8 -23 50.9657 28.8686 1 8 5 -23 78.6101 18.6866 1 -5 8 -23 106.119 27.880 3 -8 -5 -23 78.2877 26.4354 1 8 5 23 72.9755 26.0541 1 8 3 -23 232.931 22.593 1 -8 -3 -23 198.644 28.797 1 -3 8 -23 227.526 24.909 1 3 -8 -23 222.691 37.110 1 8 3 23 214.533 29.279 1 -3 8 23 271.724 30.629 1 8 1 -23 259.225 24.668 1 1 -8 -23 260.967 36.713 1 -1 8 -23 282.338 24.583 1 -8 -1 -23 239.441 28.944 1 -1 8 23 280.969 30.345 1 8 1 23 266.196 29.414 1 -8 1 -23 210.024 26.450 1 8 -1 -23 191.973 23.511 1 -8 1 -23 247.439 38.947 3 -1 -8 -23 181.828 35.768 1 1 8 -23 185.887 22.780 1 -8 1 23 238.472 25.736 3 1 8 23 205.095 29.351 1 8 -1 23 192.045 24.864 1 -1 -8 23 209.737 37.360 2 8 -3 -23 68.6752 21.1357 1 -8 3 -23 98.2737 21.9115 1 3 8 -23 39.4234 21.7317 1 -3 -8 -23 63.7196 28.7222 1 -8 3 -23 64.3270 30.5631 3 -8 3 23 91.8679 22.4586 3 -3 -8 23 127.043 32.619 2 3 8 23 48.7163 25.1137 1 -5 -8 -23 365.873 41.811 1 -8 5 -23 365.070 43.257 3 -8 5 -23 312.157 33.464 1 8 -5 -23 323.675 35.746 1 5 8 -23 344.282 31.199 1 -8 5 23 353.830 35.158 3 -5 -8 23 308.384 44.349 2 5 8 23 347.173 38.515 1 7 8 -23 1234.61 58.55 1 -8 7 -23 1218.43 74.53 3 8 -7 -23 1069.58 66.31 1 -8 7 -23 1221.61 64.24 1 -8 7 23 1238.16 70.16 3 7 8 23 1258.46 70.65 1 8 -9 -23 358.711 46.941 1 -8 9 -23 377.053 42.158 1 -8 9 -23 481.367 53.305 3 9 8 -23 360.828 34.229 1 -8 9 23 390.244 50.505 3 9 8 23 342.069 41.886 1 -6 9 -23 1264.96 73.26 3 6 -9 -23 1333.28 77.28 1 9 6 -23 1283.67 59.52 1 -6 9 -23 1208.80 64.57 1 9 6 23 1176.39 66.48 1 -4 9 -23 104.780 23.901 1 9 4 -23 122.728 21.021 1 -4 9 -23 163.959 31.027 3 4 -9 -23 141.076 34.881 1 -9 -4 -23 109.489 27.873 1 9 4 23 80.4117 25.4685 1 9 2 -23 20.8267 17.6346 1 -9 -2 -23 16.0403 20.7626 1 2 -9 -23 13.7552 30.6093 1 -2 9 -23 43.0047 19.7751 1 -2 9 23 64.5107 25.3273 1 9 2 23 47.5549 21.4558 1 9 0 -23 911.177 50.531 1 0 9 -23 1002.87 51.30 1 -9 0 -23 1059.45 74.03 3 0 -9 -23 1042.53 65.57 1 -9 0 -23 955.171 54.111 1 -9 0 23 1226.66 56.00 3 0 9 23 1088.86 59.68 1 9 0 23 976.125 54.720 1 0 -9 23 1125.91 75.13 2 -9 2 -23 897.991 52.314 1 9 -2 -23 904.465 50.382 1 -2 -9 -23 874.686 63.776 1 2 9 -23 957.755 53.085 1 -9 2 -23 964.663 68.998 3 -2 -9 23 960.947 68.976 2 2 9 23 941.217 56.661 1 -9 2 23 898.029 51.382 3 9 -4 -23 910.659 55.437 1 -9 4 -23 1035.46 55.87 1 -4 -9 -23 942.213 62.109 1 -9 4 -23 1001.39 69.65 3 4 9 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-10 1 -23 61.1936 37.6469 3 10 -1 -23 70.8437 22.7334 1 -10 1 -23 53.3378 24.9451 1 1 10 -23 75.6317 27.1593 1 -1 -10 -23 73.2941 35.2080 1 1 10 23 56.9569 27.8337 1 -1 -10 23 48.4767 34.9121 2 3 10 -23 43.2507 27.5775 1 -10 3 -23 10.6991 23.7155 1 -10 3 -23 -24.370 34.660 3 10 -3 -23 49.6894 23.9958 1 -3 -10 23 87.4986 34.9256 2 -10 3 23 42.3415 25.8307 3 3 10 23 43.2937 28.8247 1 10 -5 -23 127.511 31.229 1 5 10 -23 131.724 30.849 1 -10 5 -23 94.0887 40.9161 3 -10 5 -23 126.814 28.112 1 -10 5 23 81.1484 30.9073 3 -5 -10 23 124.562 40.355 2 5 10 23 131.243 33.981 1 -10 7 -23 46.5504 30.2767 1 10 -7 -23 134.001 35.542 1 -10 7 -23 42.5711 40.7465 3 7 10 -23 103.764 28.860 1 -10 7 23 94.8338 35.1429 3 7 10 23 71.0040 34.4324 1 -6 11 -23 36.9657 28.6276 1 -6 11 -23 89.1774 37.1466 3 6 -11 -23 84.3254 40.7666 1 11 6 -23 62.5303 23.6145 1 11 6 23 -15.359 26.855 1 4 -11 -23 46.2947 38.6095 1 -4 11 -23 29.4747 26.5260 1 11 4 -23 17.2215 21.9190 1 11 4 23 9.6551 28.2587 1 11 2 -23 339.463 34.126 1 -11 -2 -23 325.497 38.224 1 -2 11 -23 253.238 35.650 1 2 -11 -23 345.969 49.446 1 -2 11 23 332.962 40.050 1 -11 0 -23 650.721 46.601 1 11 0 -23 596.682 43.290 1 0 11 -23 645.677 48.806 1 0 -11 23 691.660 66.604 2 0 11 23 632.994 49.204 1 2 11 -23 1276.29 72.13 1 -11 2 -23 1369.39 69.18 1 -11 2 -23 1416.96 87.06 3 11 -2 -23 1418.78 69.95 1 2 11 23 1341.55 75.60 1 -2 -11 23 1219.58 86.67 2 -11 4 -23 314.964 38.992 1 -11 4 -23 327.091 54.205 3 4 11 -23 329.608 41.754 1 11 -4 -23 350.301 40.730 1 -4 -11 23 361.949 48.779 2 4 11 23 375.829 46.012 1 11 -6 -23 -38.725 26.189 1 -11 6 -23 28.6224 28.9911 1 -11 6 -23 27.7811 42.7024 3 6 11 -23 68.5181 31.1927 1 6 11 23 15.6044 30.8617 1 -11 6 23 39.9256 34.0049 3 -3 12 -23 340.094 42.679 1 12 3 -23 380.027 36.912 1 -1 12 -23 512.493 49.547 1 -12 -1 -23 472.623 46.087 1 12 1 -23 520.342 43.397 1 -1 12 23 531.947 52.444 1 1 -12 23 596.046 67.996 2 -12 1 -23 20.9673 24.7812 1 1 12 -23 42.7495 33.5416 1 12 -1 -23 8.0703 25.3504 1 -12 1 -23 45.0727 47.5324 3 1 12 23 9.6143 31.0523 1 -1 -12 23 2.8429 37.5241 2 -12 3 -23 10.0160 28.0587 1 12 -3 -23 44.4261 29.2319 1 -12 3 -23 64.7911 45.8840 3 3 12 -23 47.5274 33.8893 1 3 12 23 9.7094 32.0898 1 -3 -12 23 -9.2574 37.0709 2 0 0 -24 317.848 23.814 1 0 0 -24 314.649 24.368 1 0 0 24 312.741 29.378 2 1 -1 -24 4095.81 146.79 1 1 -1 -24 3873.92 146.16 1 1 1 -24 4017.91 142.84 1 -1 1 -24 4003.75 145.33 1 -1 1 -24 4147.31 145.30 1 -1 -1 -24 4082.70 148.60 1 1 1 -24 4032.28 142.60 1 -1 1 24 4292.56 142.07 1 1 1 24 3943.42 143.18 1 1 1 24 4012.44 173.39 2 1 -1 24 4017.62 175.78 2 -1 -1 24 3845.94 176.29 2 0 -2 -24 496.385 33.540 1 0 2 -24 504.831 25.641 1 0 2 -24 492.794 24.972 3 -2 0 -24 506.842 31.137 1 2 0 -24 567.224 27.067 1 0 2 -24 567.506 25.647 1 2 0 -24 548.213 27.744 1 2 0 24 500.240 25.443 1 0 2 24 504.855 27.560 1 0 -2 24 489.029 38.495 2 2 0 24 478.940 36.513 2 -2 2 -24 399.162 23.489 1 2 2 -24 348.639 16.122 1 2 -2 -24 321.829 25.789 1 2 2 -24 358.354 18.359 1 -2 2 -24 366.961 24.422 1 -2 -2 -24 364.051 30.808 1 -2 2 -24 404.348 28.754 3 2 -2 24 312.387 33.520 2 2 2 24 422.738 30.933 2 2 2 24 381.849 24.848 1 -2 2 24 334.024 20.782 1 -2 -2 24 326.892 33.409 2 -1 3 -24 1030.31 41.28 1 -1 3 -24 1045.34 44.00 3 -1 3 -24 955.763 40.866 1 1 -3 -24 992.332 51.188 1 3 1 -24 1025.28 39.57 1 -3 -1 -24 1046.84 49.91 1 3 1 24 1007.01 44.39 1 3 1 24 1002.98 53.68 2 -1 3 24 1014.66 44.55 1 1 -3 24 1004.00 60.91 2 -3 1 -24 1917.51 81.08 3 -1 -3 -24 1931.14 82.33 1 3 -1 -24 2014.43 75.05 1 1 3 -24 1901.80 70.27 3 -3 1 -24 1983.83 76.78 1 3 -1 -24 2025.19 75.02 1 -3 1 24 1892.23 70.79 3 -1 -3 24 1899.48 94.66 2 3 -1 24 1984.90 73.32 1 1 3 24 1954.58 76.63 1 -3 -3 -24 139.054 24.673 1 -3 3 -24 151.684 20.163 3 3 -3 -24 167.322 21.321 1 -3 3 -24 175.160 18.133 1 3 3 24 148.781 19.991 1 -3 3 24 169.736 17.649 1 -3 -3 24 139.095 27.508 2 4 2 -24 34.7341 8.4502 1 4 2 -24 48.5365 8.9699 1 -2 4 -24 17.2650 11.5498 1 -4 -2 -24 28.0619 19.3711 1 2 -4 -24 11.0993 19.5351 1 -2 4 -24 43.1550 14.0562 3 -2 4 24 29.1830 15.2362 1 4 2 24 45.3524 16.7191 2 4 2 24 58.4085 16.0165 1 -4 0 -24 110.148 23.174 3 0 4 -24 86.2242 9.2793 1 0 -4 -24 84.1785 21.9064 1 4 0 -24 73.6068 12.1302 1 0 4 -24 86.1988 9.6466 1 -4 0 -24 34.5478 17.0215 1 4 0 -24 91.4514 12.0325 1 -4 0 24 97.1878 10.1744 3 4 0 24 77.0575 15.5302 1 0 4 24 80.6669 16.9668 1 0 -4 24 110.475 26.795 2 -4 2 -24 16.5305 13.6208 1 4 -2 -24 -0.8173 13.1027 1 -4 2 -24 -13.044 17.888 3 -2 -4 -24 15.8405 22.7530 1 -4 2 24 -4.6286 4.7843 1 -4 2 24 21.7986 11.2683 3 4 -2 24 -11.762 10.178 1 -2 -4 24 10.3414 24.4868 2 2 4 24 1.8903 15.4404 1 4 4 -24 41.0923 9.0927 1 4 4 -24 43.2610 9.5611 1 -4 4 -24 32.9396 15.0682 1 4 -4 -24 53.2667 19.3694 1 -4 4 -24 26.5554 18.1960 3 -4 -4 -24 71.3437 24.9870 1 4 4 24 29.0419 18.4650 1 -4 -4 24 29.4018 29.1115 2 -4 4 24 22.5523 14.4504 1 3 -5 -24 386.467 35.591 1 -3 5 -24 439.485 31.231 3 -5 -3 -24 480.056 38.120 1 5 3 -24 397.470 21.691 1 -3 5 -24 372.827 25.505 1 -3 5 24 403.264 29.316 1 5 3 24 393.355 29.436 1 5 1 -24 146.573 14.168 1 -1 5 -24 126.500 13.945 1 1 -5 -24 136.986 25.669 1 -5 -1 -24 154.360 23.424 1 5 1 24 127.019 19.090 1 -1 5 24 125.668 20.172 1 -1 -5 -24 38.9218 24.9796 1 5 -1 -24 -1.4067 11.9548 1 -5 1 -24 -25.420 19.962 3 -5 1 -24 42.0880 16.4359 1 1 5 -24 9.37076 7.27997 1 1 5 -24 1.31870 7.47233 1 1 5 24 4.5339 16.9631 1 5 -1 24 16.7927 13.1963 1 -5 1 24 33.4260 12.1600 3 -1 -5 24 45.0015 26.0954 2 -5 3 -24 7.4540 19.9042 3 -3 -5 -24 2.0037 21.9814 1 3 5 -24 5.1813 10.9940 1 3 5 -24 18.4041 11.0705 1 -5 3 -24 -1.3213 14.9469 1 5 -3 -24 2.5562 15.0661 1 -5 3 24 24.3466 15.3529 3 3 5 24 -15.071 15.894 1 -3 -5 24 30.2199 27.0743 2 -5 5 -24 113.183 19.933 1 5 -5 -24 125.096 23.156 1 -5 -5 -24 116.741 25.768 1 5 5 -24 85.4623 13.3393 1 -5 5 -24 161.191 25.626 3 -5 -5 24 118.247 32.053 2 5 5 24 113.214 24.300 1 -4 6 -24 179.674 25.976 3 6 4 -24 147.936 16.334 1 -6 -4 -24 186.808 29.879 1 4 -6 -24 186.706 29.570 1 -4 6 -24 156.131 21.306 1 -4 6 24 178.145 23.841 1 6 4 24 188.006 24.706 1 6 2 -24 15.9631 11.3676 1 -6 -2 -24 18.2389 19.9235 1 -2 6 -24 -10.903 12.785 1 2 -6 -24 50.7582 25.6070 1 6 2 24 9.4624 16.9432 1 -2 6 24 8.5718 15.8059 1 -6 0 -24 42.5940 26.4253 3 0 6 -24 34.3407 11.5084 1 6 0 -24 62.4114 14.5594 1 -6 0 -24 56.2350 19.9556 1 0 -6 -24 25.7227 25.6476 1 6 0 24 20.1349 16.1593 1 -6 0 24 43.8912 14.2308 3 0 6 24 49.1943 19.6245 1 0 -6 24 20.9047 28.4615 2 -6 2 -24 13.7315 23.4053 3 -2 -6 -24 9.5594 24.1398 1 2 6 -24 1.1656 12.2997 1 6 -2 -24 -4.9993 15.0355 1 -6 2 -24 -18.323 14.373 1 -2 -6 24 8.9628 26.3797 2 2 6 24 -4.1297 16.6605 1 -6 2 24 13.4416 14.3062 3 4 6 -24 -11.051 13.316 1 -6 4 -24 -1.3699 16.2309 1 6 -4 -24 -12.323 17.287 1 -4 -6 -24 -11.569 22.701 1 -6 4 -24 -16.401 20.592 3 4 6 24 -7.0837 19.9450 1 -4 -6 24 -10.093 26.187 2 -6 4 24 -7.2378 16.1507 3 -6 6 -24 -28.299 21.940 3 -6 6 -24 -31.000 16.953 1 6 -6 -24 12.9494 23.2813 1 -6 -6 -24 46.7639 25.9385 1 6 6 -24 9.1502 14.0335 1 6 6 24 15.6538 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79.93 1 -1 -5 -26 1748.09 86.14 1 -5 1 -26 1988.58 88.99 3 1 5 -26 1955.46 69.25 1 5 -1 -26 1859.37 75.99 1 1 5 -26 1882.57 69.28 1 5 -1 26 2095.97 77.24 1 -1 -5 26 2056.52 100.91 2 1 5 26 1970.58 80.70 1 -5 1 26 1992.74 73.94 3 -3 -5 -26 2716.05 115.95 1 5 -3 -26 2672.39 107.07 1 -5 3 -26 2807.93 106.92 1 -5 3 -26 2773.22 113.51 3 -3 -5 26 2796.53 132.39 2 3 5 26 2743.31 109.02 1 -5 3 26 2722.84 103.83 3 -5 -5 -26 1626.44 80.39 1 -5 5 -26 1714.01 70.99 1 5 -5 -26 1609.98 75.89 1 5 5 -26 1699.01 62.95 1 -5 5 -26 1636.45 76.30 3 -5 -5 26 1579.14 91.72 2 5 5 26 1679.77 74.15 1 6 4 -26 173.477 16.281 1 -4 6 -26 179.307 22.422 1 4 -6 -26 172.159 29.734 1 -6 -4 -26 232.998 32.410 1 -4 6 -26 158.833 25.266 3 6 4 26 148.243 24.388 1 -2 6 -26 19.1063 13.8609 1 -2 6 -26 36.3725 16.9285 3 6 2 -26 32.2347 11.7923 1 2 -6 -26 14.6090 22.8536 1 -6 -2 -26 -3.7689 20.4734 1 -2 6 26 29.9246 16.5044 1 6 2 26 23.1764 16.9946 1 6 2 26 3.6806 16.5065 2 0 -6 -26 177.909 31.793 1 6 0 -26 133.740 17.312 1 -6 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64.75 1 3 0 27 1588.83 79.84 2 0 -3 27 1604.67 84.25 2 3 0 27 1669.95 63.13 1 -3 2 -27 935.516 51.041 3 3 -2 -27 1022.82 47.77 1 -3 2 -27 1003.20 47.38 1 -2 -3 -27 1013.72 55.39 1 -2 -3 27 1005.89 62.66 2 2 3 27 1087.91 47.76 1 -3 4 -27 70.1271 19.1616 3 4 3 -27 70.8480 8.9393 1 -4 -3 -27 29.8214 24.0924 1 -3 4 -27 83.7899 16.4295 1 4 3 -27 45.0562 8.0478 1 3 -4 -27 72.8875 21.7152 1 4 3 27 48.9860 17.6097 2 4 3 27 77.4109 18.1794 1 -4 -3 27 38.9259 30.4771 2 4 1 -27 453.577 22.774 1 1 -4 -27 370.012 35.419 1 4 1 -27 399.586 22.310 1 -1 4 -27 404.492 27.769 3 -4 -1 -27 453.696 35.015 1 -1 4 -27 403.339 23.517 1 1 -4 27 425.506 41.999 2 4 1 27 396.634 35.268 2 4 1 27 437.212 28.443 1 -1 4 27 351.585 27.857 1 -1 -4 -27 97.0107 25.8870 1 1 4 -27 86.7308 8.0286 1 -4 1 -27 41.2747 20.7066 3 4 -1 -27 89.1954 15.7364 1 1 4 -27 74.2975 10.2706 3 1 4 -27 72.5313 7.9643 1 -4 1 -27 40.3880 17.6684 1 -1 -4 27 61.5034 24.7063 2 1 4 27 83.3243 17.8278 1 -4 1 27 84.8647 10.4856 3 -3 -4 -27 466.379 41.277 1 -4 3 -27 426.822 34.207 3 -4 3 -27 376.865 29.016 1 4 -3 -27 472.470 32.313 1 3 4 27 446.722 32.326 1 -3 -4 27 418.060 40.906 2 -4 5 -27 1547.48 63.04 1 5 4 -27 1485.16 55.33 1 -4 5 -27 1499.70 68.90 3 -5 -4 -27 1432.87 72.77 1 4 -5 -27 1403.01 69.72 1 5 4 27 1388.46 65.05 1 2 -5 -27 1735.91 81.13 1 -2 5 -27 1771.95 74.55 3 5 2 -27 1752.47 67.38 1 -5 -2 -27 1749.18 81.23 1 -2 5 -27 1822.73 70.49 1 -2 5 27 1811.79 74.76 1 5 2 27 1832.34 74.63 1 5 2 27 1917.07 84.75 2 0 5 -27 1817.09 65.03 1 0 -5 -27 1713.14 80.58 1 5 0 -27 1777.43 68.46 1 -5 0 -27 1782.65 75.74 1 0 -5 27 1628.22 92.71 2 0 5 27 1834.64 74.47 1 5 0 27 1677.30 70.84 1 -2 -5 -27 353.830 37.929 1 5 -2 -27 371.160 28.553 1 -5 2 -27 398.562 30.896 1 -5 2 -27 398.106 37.169 3 -5 2 27 445.750 25.874 3 -2 -5 27 456.234 43.585 2 2 5 27 376.119 31.884 1 -4 -5 -27 96.2400 29.2239 1 -5 4 -27 76.8236 23.9717 3 4 5 -27 73.0580 9.8772 1 5 -4 -27 102.133 21.639 1 -5 4 -27 87.8918 19.6224 1 4 5 27 88.9704 21.1232 1 -4 -5 27 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35.8805 2 5 -2 49 69.5440 35.6696 2 -5 4 -49 46.7629 31.1569 1 5 -4 -49 -19.616 28.646 1 -4 -5 -49 -8.2721 34.2538 1 5 -4 49 2.1003 37.4574 2 3 -6 -49 184.999 40.047 1 -3 6 -49 119.974 28.338 1 -6 -3 -49 149.509 42.365 1 3 -6 49 104.906 44.389 2 6 1 -49 488.424 36.336 1 -1 6 -49 475.169 33.679 1 -6 -1 -49 609.033 58.090 1 1 -6 49 487.828 57.772 2 -6 1 -49 371.521 46.419 1 6 -1 -49 321.805 34.608 1 -1 -6 -49 326.589 47.641 1 -1 -6 49 312.512 48.007 2 -3 -6 -49 5.9623 33.2624 1 -6 3 -49 -43.825 31.137 1 6 -3 -49 18.0325 27.8691 1 -3 -6 49 27.5726 34.7327 2 6 -3 49 -17.828 35.774 2 2 -7 -49 64.5688 37.2429 1 -7 -2 -49 -33.407 35.785 1 7 2 -49 94.0513 20.7872 1 -2 7 -49 86.6589 22.9358 1 2 -7 49 54.6338 42.3642 2 7 0 -49 -9.1777 22.0989 1 0 -7 -49 -56.798 33.623 1 -7 0 -49 -23.456 33.972 1 0 -7 49 25.7522 38.4686 2 7 -2 -49 122.195 30.457 1 -7 2 -49 170.470 40.190 1 -2 -7 -49 159.946 44.256 1 -2 -7 49 112.227 41.378 2 0 0 -50 13.8038 24.1880 1 -1 -1 -50 7.8993 26.4797 1 1 -1 -50 4.8331 24.8411 1 1 1 -50 30.4987 22.5082 1 -1 1 -50 -15.677 23.055 1 1 -1 50 2.1484 29.5188 2 2 0 -50 40.7559 23.7897 1 0 2 -50 -2.0888 21.5694 1 0 -2 -50 16.1940 25.8350 1 -2 0 -50 34.7490 28.6288 1 2 0 50 16.8150 29.3755 2 0 -2 50 17.6280 30.5652 2 2 -2 -50 229.539 33.969 1 -2 -2 -50 153.840 34.823 1 2 2 -50 171.831 24.382 1 -2 2 -50 190.588 33.039 1 2 -2 50 193.357 38.501 2 -3 -1 -50 -3.6949 28.7492 1 3 1 -50 -15.348 21.096 1 1 -3 -50 -16.396 26.126 1 -1 3 -50 24.7059 22.9880 1 1 -3 50 27.6516 32.9385 2 -3 1 -50 16.6006 28.0235 1 3 -1 -50 -10.983 23.018 1 -1 -3 -50 8.1237 30.4857 1 1 3 -50 13.7474 18.8485 1 -1 -3 50 14.2611 32.5220 2 3 -1 50 -0.5754 28.4883 2 3 3 -50 37.1366 16.0842 1 3 -3 -50 31.0629 27.5553 1 -3 -3 -50 -6.2384 31.2213 1 -3 3 -50 73.9680 29.1446 1 3 -3 50 13.2347 33.6947 2 -4 -2 -50 101.989 35.555 1 2 -4 -50 105.883 34.264 1 4 2 -50 57.5895 20.6320 1 -2 4 -50 112.038 27.269 1 2 -4 50 84.6067 37.8102 2 0 4 -50 257.401 26.415 1 -4 0 -50 245.549 41.076 1 0 -4 -50 332.729 43.325 1 4 0 -50 228.219 29.717 1 0 -4 50 245.268 42.786 2 -2 -4 -50 1043.08 69.95 1 4 -2 -50 1054.16 60.52 1 -4 2 -50 1090.22 64.17 1 4 -2 50 1235.70 76.06 2 -2 -4 50 911.255 71.817 2 -4 -4 -50 838.960 64.110 1 -4 4 -50 781.512 56.335 1 4 -4 -50 830.223 57.520 1 4 -4 50 902.621 70.067 2 -3 5 -50 -0.8049 25.1025 1 -5 -3 -50 41.6963 36.1968 1 3 -5 -50 6.5676 29.9923 1 3 -5 50 24.0074 37.3942 2 -5 -1 -50 1.5092 33.5240 1 5 1 -50 8.0054 20.9267 1 -1 5 -50 46.6647 20.4209 1 1 -5 -50 16.4690 31.2083 1 1 -5 50 12.1994 35.4947 2 -1 -5 -50 73.7814 34.4930 1 -5 1 -50 100.136 36.236 1 5 -1 -50 61.5925 25.9892 1 5 -1 50 64.3501 33.6393 2 -1 -5 50 40.4991 34.9632 2 -3 -5 -50 2.5408 34.5472 1 -5 3 -50 58.8673 32.7694 1 5 -3 -50 -15.446 26.980 1 -3 -5 50 64.3098 37.4238 2 5 -3 50 20.8240 35.2303 2 -6 -2 -50 34.4094 37.5222 1 -2 6 -50 47.6256 22.9258 1 6 2 -50 7.9013 18.7962 1 2 -6 -50 32.0536 34.8927 1 2 -6 50 -0.4652 36.8569 2 0 -6 -50 427.258 52.070 1 -6 0 -50 508.639 55.394 1 6 0 -50 511.494 39.275 1 0 -6 50 476.858 56.671 2 -2 -6 -50 1315.24 81.24 1 -6 2 -50 1425.36 79.33 1 6 -2 -50 1237.70 68.36 1 6 -2 50 1303.05 84.60 2 0 -1 -51 -2.0109 26.5441 1 0 1 -51 -11.831 22.843 1 -1 0 -51 15.7252 25.9590 1 1 0 -51 27.9537 24.4907 1 0 -1 51 -12.680 29.937 2 -2 -1 -51 393.006 43.295 1 -1 2 -51 353.415 36.201 1 1 -2 -51 403.596 40.627 1 2 1 -51 405.761 34.472 1 1 -2 51 445.105 47.580 2 -1 -2 -51 163.226 34.878 1 -2 1 -51 110.151 32.318 1 2 -1 -51 126.066 29.425 1 1 2 -51 143.237 24.773 1 -1 -2 51 157.390 38.677 2 2 -1 51 140.046 34.276 2 2 -3 -51 44.3320 29.1449 1 -2 3 -51 -3.4326 24.0157 1 3 2 -51 -15.061 18.275 1 -3 -2 -51 33.1759 30.4137 1 2 -3 51 13.7467 33.0634 2 0 -3 -51 100.988 31.204 1 3 0 -51 52.1317 24.8115 1 0 3 -51 24.5395 21.8794 1 -3 0 -51 114.127 32.062 1 0 -3 51 98.5520 34.8911 2 3 0 51 50.0911 31.2804 2 -3 2 -51 142.824 32.773 1 -2 -3 -51 132.799 35.989 1 2 3 -51 141.259 21.127 1 3 -2 -51 171.839 32.241 1 -2 -3 51 146.316 39.444 2 3 -2 51 230.738 40.517 2 -3 4 -51 517.898 43.152 1 3 -4 -51 404.246 46.606 1 -4 -3 -51 409.721 49.776 1 3 -4 51 453.255 54.252 2 4 1 -51 710.365 43.127 1 -4 -1 -51 632.202 55.954 1 -1 4 -51 630.294 42.519 1 1 -4 51 691.823 61.152 2 -1 -4 -51 308.156 43.771 1 1 4 -51 300.715 25.154 1 -4 1 -51 337.330 42.701 1 4 -1 -51 378.133 36.908 1 -1 -4 51 278.473 44.665 2 4 -1 51 322.440 43.817 2 -3 -4 -51 34.3677 34.0335 1 -4 3 -51 7.6067 28.1188 1 4 -3 -51 51.4162 29.3333 1 4 -3 51 24.3647 34.0061 2 -5 -4 -51 11.4755 36.4293 1 -4 5 -51 26.1571 28.7960 1 4 -5 -51 20.9318 32.1612 1 4 -5 51 52.6764 40.0150 2 5 2 -51 0.3063 19.3755 1 2 -5 -51 88.0695 34.1703 1 -2 5 -51 32.6264 23.6117 1 -5 -2 -51 51.5368 36.7891 1 2 -5 51 9.3999 35.9808 2 0 5 -51 -5.0537 16.1174 1 0 -5 -51 19.3646 32.2643 1 -5 0 -51 -41.480 31.946 1 5 0 -51 -23.634 21.597 1 0 -5 51 40.0815 35.9824 2 5 -2 -51 22.7311 27.9171 1 -2 -5 -51 28.2565 35.8394 1 -5 2 -51 88.1727 35.4632 1 5 -2 51 40.6055 35.2094 2 -2 -5 51 27.7213 35.2943 2 -4 -5 -51 25.8170 37.3639 1 -5 4 -51 129.976 34.722 1 5 -4 -51 102.280 33.308 1 5 -4 51 60.6738 39.6138 2 -1 6 -51 568.285 36.015 1 6 1 -51 527.873 38.305 1 -6 -1 -51 506.860 55.322 1 1 -6 51 564.840 61.045 2 6 -1 -51 201.980 30.859 1 -6 1 -51 209.979 40.630 1 -1 -6 -51 195.153 42.256 1 -1 -6 51 251.652 44.679 2 0 0 -52 659.287 47.891 1 1 -1 -52 1458.74 72.74 1 -1 -1 -52 1541.49 75.82 1 1 1 -52 1414.37 68.24 1 -1 1 -52 1443.99 71.51 1 1 -1 52 1321.97 84.08 2 2 0 -52 191.750 29.639 1 0 -2 -52 193.579 34.263 1 -2 0 -52 221.695 35.506 1 0 2 -52 147.485 27.373 1 0 -2 52 129.267 36.335 2 2 0 52 156.525 36.563 2 2 -2 -52 111.024 31.178 1 2 2 -52 186.108 25.529 1 -2 2 -52 235.446 34.108 1 -2 -2 -52 148.975 36.129 1 2 -2 52 162.124 38.797 2 -1 3 -52 362.821 35.073 1 -3 -1 -52 364.740 43.376 1 3 1 -52 332.841 32.662 1 1 -3 52 379.314 46.883 2 1 3 -52 299.052 27.636 1 3 -1 -52 294.295 35.296 1 -1 -3 -52 324.068 42.964 1 -3 1 -52 331.462 40.115 1 3 -1 52 275.059 40.782 2 -1 -3 52 318.218 45.523 2 -3 -3 -52 54.6346 32.7138 1 -3 3 -52 34.6685 28.6756 1 3 -3 -52 41.4077 29.6125 1 3 -3 52 65.4230 36.3722 2 -2 4 -52 36.7192 25.0074 1 4 2 -52 7.8346 19.3286 1 2 -4 -52 -27.565 28.983 1 -4 -2 -52 -11.984 31.149 1 2 -4 52 -2.5894 34.4502 2 0 -4 -52 21.4172 30.4998 1 4 0 -52 -8.1273 23.3793 1 0 4 -52 10.4565 19.1724 1 -4 0 -52 28.7044 32.2468 1 0 -4 52 17.3267 34.4655 2 -4 2 -52 -2.2841 28.6208 1 -2 -4 -52 -28.019 30.075 1 4 -2 -52 -5.5997 25.8762 1 4 -2 52 -8.7144 33.6420 2 -2 -4 52 -10.356 33.030 2 -4 4 -52 -4.1739 29.1752 1 4 -4 -52 -20.043 29.574 1 -4 -4 -52 27.7026 36.3572 1 4 -4 52 29.7839 36.9288 2 -5 -3 -52 133.553 41.296 1 3 -5 -52 158.626 38.029 1 -3 5 -52 149.222 30.723 1 3 -5 52 118.942 41.261 2 -5 -1 -52 -40.652 31.028 1 1 -5 -52 8.6897 30.9927 1 -1 5 -52 27.9043 21.1778 1 5 1 -52 25.2996 21.7940 1 1 -5 52 -6.0051 36.3276 2 -1 -5 -52 63.8770 33.9268 1 5 -1 -52 9.3953 24.4914 1 -5 1 -52 13.2738 32.1185 1 -1 -5 52 -3.2135 34.4944 2 -3 -5 -52 -4.2577 34.8888 1 5 -3 -52 -19.106 27.074 1 -5 3 -52 -3.0646 30.8927 1 5 -3 52 19.5126 35.8426 2 -3 -5 52 -1.2600 36.3866 2 0 -6 -52 161.310 40.709 1 6 0 -52 130.439 27.281 1 -6 0 -52 185.300 40.755 1 0 -6 52 82.7879 40.4780 2 0 1 -53 90.0744 26.5980 1 0 -1 -53 39.9444 29.0147 1 -1 0 -53 119.597 29.819 1 1 0 -53 90.2624 27.6290 1 1 -2 -53 245.889 36.781 1 -2 -1 -53 284.192 39.342 1 2 1 -53 305.891 31.758 1 -1 2 -53 264.965 33.332 1 1 -2 53 306.752 43.776 2 -2 1 -53 262.182 35.668 1 -1 -2 -53 193.315 37.112 1 2 -1 -53 205.182 32.815 1 1 2 -53 264.195 28.910 1 2 -1 53 216.869 39.692 2 3 2 -53 574.053 38.132 1 2 -3 -53 529.166 49.229 1 -3 -2 -53 582.496 53.353 1 -2 3 -53 704.896 45.984 1 2 -3 53 573.275 58.295 2 0 -3 -53 60.9112 32.0637 1 3 0 -53 53.3941 24.9121 1 0 3 -53 45.4137 23.2247 1 -3 0 -53 86.6710 32.3406 1 0 -3 53 82.2237 37.0637 2 3 0 53 95.3739 33.9350 2 3 -2 -53 5.1798 25.9717 1 2 3 -53 36.0881 18.2912 1 -3 2 -53 -55.895 25.589 1 -2 -3 -53 37.0123 33.4599 1 3 -2 53 -12.830 32.451 2 3 -4 -53 289.648 41.664 1 -3 4 -53 269.313 35.559 1 -4 -3 -53 313.524 45.758 1 3 -4 53 233.468 45.421 2 4 1 -53 222.423 28.314 1 -4 -1 -53 298.091 41.948 1 -1 4 -53 208.910 28.474 1 1 -4 -53 232.066 40.096 1 1 -4 53 201.574 44.569 2 -4 1 -53 474.533 49.112 1 4 -1 -53 501.725 42.194 1 -1 -4 -53 495.452 51.190 1 -1 -4 53 403.698 52.029 2 4 -1 53 471.420 50.412 2 -4 3 -53 60.8768 30.7937 1 4 -3 -53 43.9993 29.7818 1 -3 -4 -53 40.6154 35.5266 1 4 -3 53 90.2048 37.8119 2 -2 5 -53 275.164 31.771 1 2 -5 -53 226.915 41.177 1 -5 -2 -53 294.269 45.788 1 2 -5 53 220.727 47.117 2 0 -5 -53 382.601 48.520 1 5 0 -53 343.193 35.089 1 -5 0 -53 451.733 49.318 1 0 -5 53 441.779 53.045 2 -5 2 -53 -3.4898 32.0291 1 -2 -5 -53 0.5608 34.1397 1 5 -2 -53 38.1632 27.9428 1 5 -2 53 -15.894 32.446 2 -2 -5 53 -29.463 35.224 2 0 0 -54 9.2706 26.4576 1 1 1 -54 -16.575 23.641 1 1 -1 -54 30.8141 25.8887 1 -1 1 -54 26.1123 26.9658 1 -1 -1 -54 6.2083 28.2898 1 1 -1 54 -43.492 31.733 2 -2 0 -54 18.5231 27.5627 1 0 -2 -54 48.5510 30.3269 1 0 2 -54 0.8534 23.1896 1 2 0 -54 19.2037 24.5047 1 0 -2 54 -24.451 31.262 2 2 0 54 -49.297 28.720 2 -2 2 -54 27.0896 26.6278 1 2 -2 -54 57.6489 28.9952 1 -2 -2 -54 63.3211 34.3021 1 2 2 -54 85.2205 22.3017 1 2 -2 54 60.5628 34.4298 2 1 -3 -54 21.9950 30.6398 1 3 1 -54 -3.5015 22.2808 1 -1 3 -54 50.5863 24.3854 1 -3 -1 -54 -13.344 31.058 1 1 -3 54 -0.3082 32.2628 2 -1 -3 -54 282.694 41.182 1 3 -1 -54 270.495 35.136 1 1 3 -54 244.799 26.676 1 -3 1 -54 303.775 40.661 1 -1 -3 54 268.348 44.998 2 3 -1 54 238.962 41.556 2 3 -3 -54 389.187 43.422 1 -3 -3 -54 326.640 45.611 1 -3 3 -54 405.529 41.273 1 3 -3 54 457.745 52.073 2 -2 4 -54 20.7341 25.1033 1 2 -4 -54 66.2652 32.9808 1 -4 -2 -54 -11.235 32.486 1 4 2 -54 25.8765 20.0938 1 2 -4 54 39.4589 38.1078 2 -4 0 -54 30.4461 33.0330 1 0 -4 -54 55.5535 32.3241 1 0 4 -54 31.5405 19.9504 1 4 0 -54 23.1043 24.9139 1 0 -4 54 -31.167 32.413 2 -4 2 -54 206.440 37.076 1 -2 -4 -54 173.197 39.599 1 4 -2 -54 168.776 33.711 1 -2 -4 54 215.549 44.512 2 4 -2 54 132.631 39.134 2 0 -1 -55 54.7144 30.3909 1 1 0 -55 43.0791 26.6142 1 0 1 -55 13.9731 25.2547 1 -1 0 -55 21.5538 28.7799 1 2 1 -55 24.6230 23.5775 1 -2 -1 -55 45.4460 29.9340 1 -1 2 -55 30.3092 26.1144 1 1 -2 -55 31.9561 28.7640 1 1 -2 55 -41.739 31.687 2 2 -1 -55 154.916 31.234 1 -2 1 -55 187.909 34.106 1 -1 -2 -55 134.446 35.142 1 1 2 -55 178.181 26.398 1 2 -1 55 171.617 39.991 2 -2 3 -55 346.625 36.160 1 -3 -2 -55 292.025 44.301 1 2 -3 -55 301.630 40.435 1 3 2 -55 275.183 28.496 1 2 -3 55 300.178 45.756 2 0 3 -55 509.013 38.168 1 3 0 -55 500.429 41.016 1 0 -3 -55 523.737 50.487 1 -3 0 -55 553.688 50.228 1 0 -3 55 543.386 56.859 2 -2 -3 -55 127.810 37.136 1 3 -2 -55 88.0968 30.4550 1 -3 2 -55 124.258 33.209 1 3 -2 55 133.575 37.891 2 4 1 -55 33.2579 23.0108 1 1 -4 -55 35.6990 32.2840 1 -1 4 -55 107.972 25.049 1 -4 -1 -55 39.7535 32.6633 1 1 -4 55 67.7198 36.8842 2 -1 -4 -55 0.8356 31.6832 1 4 -1 -55 52.7322 26.6574 1 -4 1 -55 15.5065 31.9565 1 -1 -4 55 17.7250 35.6533 2 0 0 -56 1689.86 81.25 1 1 1 -56 78.9059 26.8129 1 -1 -1 -56 105.146 32.517 1 1 -1 -56 37.3120 29.0091 1 -1 1 -56 91.3710 30.0590 1 2 0 -56 860.673 52.783 1 0 2 -56 835.979 49.534 1 0 -2 -56 901.660 59.327 1 -2 0 -56 786.386 57.482 1 0 -2 56 799.237 67.074 2 -2 -2 -56 384.711 45.476 1 -2 2 -56 381.494 39.900 1 2 2 -56 328.519 30.930 1 2 -2 -56 382.375 41.133 1 2 -2 56 406.765 49.527 2 1 -3 -56 63.7382 32.2002 1 -3 -1 -56 -47.180 28.818 1 3 1 -56 84.9068 25.2505 1 -1 3 -56 56.2032 24.9601 1 1 -3 56 41.5212 35.0865 2 -3 1 -56 -20.968 27.710 1 -1 -3 -56 33.0224 31.1548 1 1 3 -56 4.7644 19.6576 1 3 -1 -56 -39.721 24.571 1 3 -1 56 -0.4835 32.5204 2 -1 -3 56 20.8264 36.6281 2 0 1 -57 108.135 28.552 1 0 -1 -57 89.1248 31.9229 1 1 0 -57 63.7832 29.1497 1 -1 0 -57 8.1718 28.5872 1 1 -2 -57 132.505 34.715 1 -1 2 -57 162.715 31.384 1 2 1 -57 210.352 29.534 1 -2 -1 -57 163.321 37.341 1 1 -2 57 246.567 44.454 2 -2 1 -57 20.3139 29.5234 1 -1 -2 -57 62.7176 32.6809 1 1 2 -57 7.0306 22.7875 1 2 -1 -57 20.7188 26.0949 1 2 -1 57 -47.453 30.510 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 49415 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group U1 U 0.31859(2) 0.46321(2) 0.42934(2) 0.00989(4) Uani 1 1 d . . . . . K1 K 0.0000 0.2500 0.38999(3) 0.0143(3) Uani 1 2 d S T P . . K2 K 0.5000 0.7500 0.49163(3) 0.0169(3) Uani 1 2 d S T P . . O1 O 0.2972(3) 0.6203(3) 0.44945(7) 0.0165(7) Uani 1 1 d . . . . . O2 O 0.3420(3) 0.3059(3) 0.41057(7) 0.0161(7) Uani 1 1 d . . . . . O11 O 0.3241(3) 0.5654(3) 0.37567(7) 0.0117(6) Uani 1 1 d . . . . . O12 O 0.1262(3) 0.5044(3) 0.39220(7) 0.0142(6) Uani 1 1 d . . . . . O13 O 0.3109(3) 0.2829(3) 0.29031(7) 0.0159(6) Uani 1 1 d . . . . . O14 O 0.2028(3) 0.2921(3) 0.33660(7) 0.0160(7) Uani 1 1 d . . . . . O21 O 0.0997(3) 0.3751(3) 0.45088(7) 0.0177(7) Uani 1 1 d . . . . . O22 O 0.2780(3) 0.3440(3) 0.48100(7) 0.0147(6) Uani 1 1 d . . . . . C11 C 0.2022(4) 0.5441(4) 0.36928(10) 0.0114(8) Uani 1 1 d . . . . . C12 C 0.1515(4) 0.5661(4) 0.33517(10) 0.0132(9) Uani 1 1 d . . . . . H12A H 0.1453 0.6637 0.3309 0.016 Uiso 1 1 calc R U . . . H12B H 0.0603 0.5276 0.3331 0.016 Uiso 1 1 calc R U . . . C13 C 0.2439(4) 0.5013(4) 0.30970(10) 0.0131(9) Uani 1 1 d . . . . . H13A H 0.2108 0.5246 0.2876 0.016 Uiso 1 1 calc R U . . . H13B H 0.3350 0.5398 0.3120 0.016 Uiso 1 1 calc R U . . . C14 C 0.2531(4) 0.3516(4) 0.31243(10) 0.0143(9) Uani 1 1 d . . . . . C21 C 0.1532(4) 0.3246(4) 0.47599(11) 0.0149(9) Uani 1 1 d . . . . . C22 C 0.0756(4) 0.2401(5) 0.49976(11) 0.0146(9) Uani 1 1 d . . . . . H22A H 0.1095 0.2590 0.5220 0.018 Uiso 1 1 calc R U . . . H22B H 0.0945 0.1445 0.4950 0.018 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 U1 0.00822(8) 0.01063(8) 0.01082(7) 0.00017(6) -0.00021(6) -0.00012(6) K1 0.0114(6) 0.0103(6) 0.0211(7) 0.000 0.000 0.0028(5) K2 0.0136(6) 0.0207(7) 0.0163(7) 0.000 0.000 0.0018(5) O1 0.0232(17) 0.0107(14) 0.0157(15) -0.0017(12) 0.0003(13) 0.0062(13) O2 0.0217(17) 0.0108(15) 0.0159(16) 0.0000(12) -0.0012(13) 0.0004(13) O11 0.0069(14) 0.0146(15) 0.0136(14) 0.0033(12) -0.0040(11) -0.0018(12) O12 0.0093(15) 0.0160(16) 0.0171(16) 0.0016(12) 0.0006(12) -0.0021(12) O13 0.0225(17) 0.0108(15) 0.0145(15) 0.0002(12) 0.0042(13) 0.0002(13) O14 0.0200(17) 0.0112(15) 0.0169(16) 0.0022(12) 0.0034(13) 0.0034(13) O21 0.0101(15) 0.0293(19) 0.0137(15) 0.0060(13) -0.0016(12) -0.0043(13) O22 0.0094(15) 0.0219(17) 0.0128(15) 0.0022(13) -0.0021(12) 0.0004(12) C11 0.015(2) 0.0030(18) 0.016(2) -0.0009(15) -0.0014(16) 0.0013(16) C12 0.012(2) 0.013(2) 0.015(2) 0.0001(16) -0.0052(16) 0.0015(15) C13 0.015(2) 0.014(2) 0.010(2) 0.0009(15) -0.0023(15) -0.0019(19) C14 0.014(2) 0.013(2) 0.016(2) -0.0026(16) -0.0036(16) -0.0032(17) C21 0.013(2) 0.018(2) 0.014(2) -0.0015(17) 0.0014(16) 0.0019(17) C22 0.010(2) 0.020(2) 0.014(2) 0.0022(18) 0.0000(15) 0.0005(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O2 U1 O1 178.22(14) . . O2 U1 O11 88.65(12) . . O1 U1 O11 92.96(12) . . O2 U1 O22 88.08(12) . . O1 U1 O22 90.45(12) . . O11 U1 O22 170.70(10) . . O2 U1 O14 93.86(13) . 11_666 O1 U1 O14 86.09(13) . 11_666 O11 U1 O14 66.24(10) . 11_666 O22 U1 O14 122.67(10) . 11_666 O2 U1 O12 89.02(12) . . O1 U1 O12 92.56(12) . . O11 U1 O12 52.58(9) . . O22 U1 O12 118.65(10) . . O14 U1 O12 118.67(10) 11_666 . O2 U1 O13 91.02(13) . 11_666 O1 U1 O13 87.54(13) . 11_666 O11 U1 O13 118.36(10) . 11_666 O22 U1 O13 70.41(10) . 11_666 O14 U1 O13 52.29(10) 11_666 11_666 O12 U1 O13 170.94(10) . 11_666 O2 U1 O21 87.51(13) . . O1 U1 O21 92.37(13) . . O11 U1 O21 119.02(9) . . O22 U1 O21 52.14(10) . . O14 U1 O21 174.62(10) 11_666 . O12 U1 O21 66.51(10) . . O13 U1 O21 122.54(10) 11_666 . O2 U1 C11 85.98(13) . . O1 U1 C11 95.81(13) . . O11 U1 C11 26.29(11) . . O22 U1 C11 144.63(11) . . O14 U1 C11 92.52(11) 11_666 . O12 U1 C11 26.56(11) . . O13 U1 C11 144.44(11) 11_666 . O21 U1 C11 92.76(11) . . O2 U1 C14 91.45(13) . 11_666 O1 U1 C14 87.73(14) . 11_666 O11 U1 C14 92.01(11) . 11_666 O22 U1 C14 96.77(11) . 11_666 O14 U1 C14 25.98(11) 11_666 11_666 O12 U1 C14 144.57(11) . 11_666 O13 U1 C14 26.37(11) 11_666 11_666 O21 U1 C14 148.90(11) . 11_666 C11 U1 C14 118.19(12) . 11_666 O2 U1 C21 86.42(13) . . O1 U1 C21 92.70(13) . . O11 U1 C21 144.80(11) . . O22 U1 C21 26.19(11) . . O14 U1 C21 148.85(11) 11_666 . O12 U1 C21 92.47(11) . . O13 U1 C21 96.57(11) 11_666 . O21 U1 C21 25.99(11) . . C11 U1 C21 118.52(12) . . C14 U1 C21 122.92(12) 11_666 . O2 U1 K1 58.40(10) . . O1 U1 K1 122.55(11) . . O11 U1 K1 83.16(7) . . O22 U1 K1 87.71(7) . . O14 U1 K1 139.71(7) 11_666 . O12 U1 K1 41.85(7) . . O13 U1 K1 143.47(7) 11_666 . O21 U1 K1 44.91(7) . . C11 U1 K1 59.72(8) . . C14 U1 K1 149.45(8) 11_666 . C21 U1 K1 64.69(9) . . O11 K1 O11 151.70(14) 16_656 11_566 O11 K1 O12 107.16(9) 16_656 . O11 K1 O12 73.77(9) 11_566 . O11 K1 O12 73.78(9) 16_656 6_454 O11 K1 O12 107.16(9) 11_566 6_454 O12 K1 O12 176.34(13) . 6_454 O11 K1 O21 104.60(9) 16_656 . O11 K1 O21 99.19(9) 11_566 . O12 K1 O21 56.39(9) . . O12 K1 O21 119.98(9) 6_454 . O11 K1 O21 99.19(9) 16_656 6_454 O11 K1 O21 104.60(9) 11_566 6_454 O12 K1 O21 119.98(9) . 6_454 O12 K1 O21 56.39(9) 6_454 6_454 O21 K1 O21 65.24(12) . 6_454 O11 K1 O14 101.59(9) 16_656 6_454 O11 K1 O14 56.20(8) 11_566 6_454 O12 K1 O14 116.55(9) . 6_454 O12 K1 O14 66.39(9) 6_454 6_454 O21 K1 O14 153.77(8) . 6_454 O21 K1 O14 109.11(9) 6_454 6_454 O11 K1 O14 56.20(8) 16_656 . O11 K1 O14 101.59(9) 11_566 . O12 K1 O14 66.39(9) . . O12 K1 O14 116.55(9) 6_454 . O21 K1 O14 109.11(9) . . O21 K1 O14 153.77(8) 6_454 . O14 K1 O14 86.76(13) 6_454 . O11 K1 U1 84.27(7) 16_656 . O11 K1 U1 106.83(6) 11_566 . O12 K1 U1 35.76(6) . . O12 K1 U1 141.88(7) 6_454 . O21 K1 U1 36.83(6) . . O21 K1 U1 98.42(7) 6_454 . O14 K1 U1 150.32(7) 6_454 . O14 K1 U1 72.28(6) . . O11 K1 U1 106.83(6) 16_656 6_454 O11 K1 U1 84.28(7) 11_566 6_454 O12 K1 U1 141.88(7) . 6_454 O12 K1 U1 35.75(6) 6_454 6_454 O21 K1 U1 98.42(7) . 6_454 O21 K1 U1 36.83(6) 6_454 6_454 O14 K1 U1 72.28(6) 6_454 6_454 O14 K1 U1 150.32(7) . 6_454 U1 K1 U1 134.31(4) . 6_454 O11 K1 U1 124.85(8) 16_656 11_566 O11 K1 U1 27.67(6) 11_566 11_566 O12 K1 U1 86.64(6) . 11_566 O12 K1 U1 95.72(6) 6_454 11_566 O21 K1 U1 125.88(6) . 11_566 O21 K1 U1 119.75(6) 6_454 11_566 O14 K1 U1 32.30(6) 6_454 11_566 O14 K1 U1 84.91(6) . 11_566 U1 K1 U1 122.375(10) . 11_566 U1 K1 U1 87.906(7) 6_454 11_566 O11 K1 U1 27.67(6) 16_656 16_656 O11 K1 U1 124.85(8) 11_566 16_656 O12 K1 U1 95.72(6) . 16_656 O12 K1 U1 86.64(6) 6_454 16_656 O21 K1 U1 119.75(6) . 16_656 O21 K1 U1 125.88(6) 6_454 16_656 O14 K1 U1 84.91(6) 6_454 16_656 O14 K1 U1 32.30(6) . 16_656 U1 K1 U1 87.905(7) . 16_656 U1 K1 U1 122.375(10) 6_454 16_656 U1 K1 U1 100.04(3) 11_566 16_656 O22 K2 O22 130.04(14) 9_666 14_556 O22 K2 O13 80.66(10) 9_666 8_454 O22 K2 O13 63.46(9) 14_556 8_454 O22 K2 O13 63.46(9) 9_666 3 O22 K2 O13 80.66(10) 14_556 3 O13 K2 O13 87.69(14) 8_454 3 O22 K2 O1 131.52(9) 9_666 . O22 K2 O1 80.23(9) 14_556 . O13 K2 O1 143.20(9) 8_454 . O13 K2 O1 92.38(9) 3 . O22 K2 O1 80.23(9) 9_666 6_564 O22 K2 O1 131.52(9) 14_556 6_564 O13 K2 O1 92.38(9) 8_454 6_564 O13 K2 O1 143.20(9) 3 6_564 O1 K2 O1 108.55(13) . 6_564 O22 K2 O13 76.00(8) 9_666 11_666 O22 K2 O13 124.65(9) 14_556 11_666 O13 K2 O13 153.29(9) 8_454 11_666 O13 K2 O13 70.40(10) 3 11_666 O1 K2 O13 55.91(8) . 11_666 O1 K2 O13 96.25(8) 6_564 11_666 O22 K2 O13 124.65(8) 9_666 16_666 O22 K2 O13 76.00(8) 14_556 16_666 O13 K2 O13 70.40(10) 8_454 16_666 O13 K2 O13 153.29(9) 3 16_666 O1 K2 O13 96.25(8) . 16_666 O1 K2 O13 55.91(8) 6_564 16_666 O13 K2 O13 134.50(11) 11_666 16_666 O22 K2 C14 76.76(10) 9_666 11_666 O22 K2 C14 139.65(10) 14_556 11_666 O13 K2 C14 155.81(10) 8_454 11_666 O13 K2 C14 89.90(10) 3 11_666 O1 K2 C14 60.94(9) . 11_666 O1 K2 C14 75.44(10) 6_564 11_666 O13 K2 C14 21.21(8) 11_666 11_666 O13 K2 C14 116.36(10) 16_666 11_666 O22 K2 C14 139.65(10) 9_666 16_666 O22 K2 C14 76.76(10) 14_556 16_666 O13 K2 C14 89.90(10) 8_454 16_666 O13 K2 C14 155.81(10) 3 16_666 O1 K2 C14 75.44(10) . 16_666 O1 K2 C14 60.94(9) 6_564 16_666 O13 K2 C14 116.36(10) 11_666 16_666 O13 K2 C14 21.21(8) 16_666 16_666 C14 K2 C14 101.72(15) 11_666 16_666 O22 K2 U1 97.84(7) 9_666 6_564 O22 K2 U1 111.83(7) 14_556 6_564 O13 K2 U1 85.57(7) 8_454 6_564 O13 K2 U1 160.97(6) 3 6_564 O1 K2 U1 103.64(7) . 6_564 O1 K2 U1 20.19(6) 6_564 6_564 O13 K2 U1 110.17(6) 11_666 6_564 O13 K2 U1 35.87(5) 16_666 6_564 C14 K2 U1 89.01(8) 11_666 6_564 C14 K2 U1 42.07(7) 16_666 6_564 O22 K2 U1 111.83(7) 9_666 . O22 K2 U1 97.84(7) 14_556 . O13 K2 U1 160.97(6) 8_454 . O13 K2 U1 85.57(7) 3 . O1 K2 U1 20.19(6) . . O1 K2 U1 103.64(7) 6_564 . O13 K2 U1 35.87(5) 11_666 . O13 K2 U1 110.17(6) 16_666 . C14 K2 U1 42.07(7) 11_666 . C14 K2 U1 89.01(8) 16_666 . U1 K2 U1 106.00(3) 6_564 . U1 O1 K2 124.90(14) . . C11 O11 U1 95.5(2) . . C11 O11 K1 135.4(3) . 11_666 U1 O11 K1 122.16(11) . 11_666 C11 O12 U1 92.5(2) . . C11 O12 K1 121.4(3) . . U1 O12 K1 102.39(10) . . C14 O13 U1 93.6(3) . 16_656 C14 O13 K2 152.4(3) . 7_544 U1 O13 K2 108.95(11) 16_656 7_544 C14 O13 K2 84.9(2) . 11_566 U1 O13 K2 91.21(9) 16_656 11_566 K2 O13 K2 109.60(10) 7_544 11_566 C14 O14 U1 94.7(3) . 16_656 C14 O14 K1 154.9(3) . . U1 O14 K1 107.11(10) 16_656 . C21 O21 U1 93.3(3) . . C21 O21 K1 131.3(3) . . U1 O21 K1 98.26(10) . . C21 O22 U1 95.5(3) . . C21 O22 K2 145.9(3) . 9_666 U1 O22 K2 113.36(11) . 9_666 O11 C11 O12 118.3(4) . . O11 C11 C12 119.5(4) . . O12 C11 C12 122.2(4) . . O11 C11 U1 58.2(2) . . O12 C11 U1 61.0(2) . . C12 C11 U1 170.3(3) . . C11 C12 C13 111.6(3) . . C11 C12 H12A 109.3 . . C13 C12 H12A 109.3 . . C11 C12 H12B 109.3 . . C13 C12 H12B 109.3 . . H12A C12 H12B 108.0 . . C14 C13 C12 113.9(4) . . C14 C13 H13A 108.8 . . C12 C13 H13A 108.8 . . C14 C13 H13B 108.8 . . C12 C13 H13B 108.8 . . H13A C13 H13B 107.7 . . O14 C14 O13 119.1(4) . . O14 C14 C13 120.2(4) . . O13 C14 C13 120.7(4) . . O14 C14 U1 59.3(2) . 16_656 O13 C14 U1 60.0(2) . 16_656 C13 C14 U1 175.9(3) . 16_656 O14 C14 K2 94.2(3) . 11_566 O13 C14 K2 73.9(2) . 11_566 C13 C14 K2 101.3(3) . 11_566 U1 C14 K2 82.76(10) 16_656 11_566 O21 C21 O22 118.8(4) . . O21 C21 C22 122.2(4) . . O22 C21 C22 118.9(4) . . O21 C21 U1 60.7(2) . . O22 C21 U1 58.3(2) . . C22 C21 U1 174.2(3) . . C21 C22 C22 116.0(4) . 6_454 C21 C22 H22A 108.3 . . C22 C22 H22A 108.3 6_454 . C21 C22 H22B 108.3 . . C22 C22 H22B 108.3 6_454 . H22A C22 H22B 107.4 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 U1 O2 1.761(3) . U1 O1 1.781(3) . U1 O11 2.420(3) . U1 O22 2.457(3) . U1 O14 2.467(3) 11_666 U1 O12 2.480(3) . U1 O13 2.481(3) 11_666 U1 O21 2.511(3) . U1 C11 2.833(4) . U1 C14 2.859(4) 11_666 U1 C21 2.875(4) . U1 K1 4.1447(6) . K1 O11 2.620(3) 16_656 K1 O11 2.620(3) 11_566 K1 O12 2.831(3) . K1 O12 2.831(3) 6_454 K1 O21 2.957(3) . K1 O21 2.957(3) 6_454 K1 O14 3.004(3) 6_454 K1 O14 3.004(3) . K1 U1 4.1447(6) 6_454 K1 U1 4.4126(9) 11_566 K1 U1 4.4126(9) 16_656 K2 O22 2.650(3) 9_666 K2 O22 2.650(3) 14_556 K2 O13 2.760(3) 8_454 K2 O13 2.760(3) 3 K2 O1 2.954(3) . K2 O1 2.955(3) 6_564 K2 O13 3.378(3) 11_666 K2 O13 3.378(3) 16_666 K2 C14 3.503(4) 11_666 K2 C14 3.503(4) 16_666 K2 U1 4.2336(9) 6_564 O11 C11 1.261(5) . O11 K1 2.620(3) 11_666 O12 C11 1.268(5) . O13 C14 1.272(5) . O13 U1 2.482(3) 16_656 O13 K2 2.760(3) 7_544 O13 K2 3.378(3) 11_566 O14 C14 1.257(5) . O14 U1 2.467(3) 16_656 O21 C21 1.262(5) . O22 C21 1.274(5) . O22 K2 2.650(3) 9_666 C11 C12 1.500(6) . C12 C13 1.533(6) . C12 H12A 0.9900 . C12 H12B 0.9900 . C13 C14 1.499(6) . C13 H13A 0.9900 . C13 H13B 0.9900 . C14 U1 2.859(4) 16_656 C14 K2 3.503(4) 11_566 C21 C22 1.501(6) . C22 C22 1.519(8) 6_454 C22 H22A 0.9900 . C22 H22B 0.9900 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 O11 U1 O1 K2 -111.52(16) . . . . O22 U1 O1 K2 77.14(16) . . . . O14 U1 O1 K2 -45.59(16) 11_666 . . . O12 U1 O1 K2 -164.16(16) . . . . O13 U1 O1 K2 6.77(16) 11_666 . . . O21 U1 O1 K2 129.25(16) . . . . C11 U1 O1 K2 -137.73(16) . . . . C14 U1 O1 K2 -19.62(17) 11_666 . . . C21 U1 O1 K2 103.24(17) . . . . K1 U1 O1 K2 164.70(9) . . . . U1 O11 C11 O12 10.9(4) . . . . K1 O11 C11 O12 -138.3(3) 11_666 . . . U1 O11 C11 C12 -169.0(3) . . . . K1 O11 C11 C12 41.8(6) 11_666 . . . K1 O11 C11 U1 -149.2(4) 11_666 . . . U1 O12 C11 O11 -10.6(4) . . . . K1 O12 C11 O11 -116.8(3) . . . . U1 O12 C11 C12 169.3(3) . . . . K1 O12 C11 C12 63.2(5) . . . . K1 O12 C11 U1 -106.1(2) . . . . O11 C11 C12 C13 47.3(5) . . . . O12 C11 C12 C13 -132.6(4) . . . . C11 C12 C13 C14 63.1(5) . . . . U1 O14 C14 O13 5.2(4) 16_656 . . . K1 O14 C14 O13 -145.7(5) . . . . U1 O14 C14 C13 -175.3(3) 16_656 . . . K1 O14 C14 C13 33.9(9) . . . . K1 O14 C14 U1 -150.8(7) . . . 16_656 U1 O14 C14 K2 79.02(13) 16_656 . . 11_566 K1 O14 C14 K2 -71.8(6) . . . 11_566 U1 O13 C14 O14 -5.1(4) 16_656 . . . K2 O13 C14 O14 -150.4(4) 7_544 . . . K2 O13 C14 O14 85.8(4) 11_566 . . . U1 O13 C14 C13 175.3(3) 16_656 . . . K2 O13 C14 C13 30.0(8) 7_544 . . . K2 O13 C14 C13 -93.8(4) 11_566 . . . K2 O13 C14 U1 -145.3(6) 7_544 . . 16_656 K2 O13 C14 U1 90.89(9) 11_566 . . 16_656 U1 O13 C14 K2 -90.89(9) 16_656 . . 11_566 K2 O13 C14 K2 123.8(6) 7_544 . . 11_566 C12 C13 C14 O14 -9.2(6) . . . . C12 C13 C14 O13 170.3(4) . . . . C12 C13 C14 K2 92.5(3) . . . 11_566 U1 O21 C21 O22 4.5(4) . . . . K1 O21 C21 O22 108.5(4) . . . . U1 O21 C21 C22 -174.2(4) . . . . K1 O21 C21 C22 -70.2(5) . . . . K1 O21 C21 U1 104.0(3) . . . . U1 O22 C21 O21 -4.6(4) . . . . K2 O22 C21 O21 -153.1(3) 9_666 . . . U1 O22 C21 C22 174.1(3) . . . . K2 O22 C21 C22 25.6(7) 9_666 . . . K2 O22 C21 U1 -148.5(5) 9_666 . . . O21 C21 C22 C22 -22.2(6) . . . 6_454 O22 C21 C22 C22 159.2(4) . . . 6_454