#------------------------------------------------------------------------------ #$Date: 2021-02-24 04:01:52 +0200 (Wed, 24 Feb 2021) $ #$Revision: 262173 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/06/1560601.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1560601 loop_ _publ_author_name 'Liu, Tiantian' 'Chen, Xiaojie' 'Zhao, Juan' 'Wei, Weichun' 'Mao, Zhu' 'Wu, William' 'Jiao, Shibo' 'Liu, Yang' 'Yang, Zhiyong' 'Chi, Zhenguo' _publ_section_title ; Hybridized Local and Charge-Transfer Excited State Fluorophores Enabling Organic Light-Emitting Diodes with Record High Efficiencies Close to 20% ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC00272D _journal_year 2021 _chemical_formula_moiety 'C58 H58 N4 S, C6 H14' _chemical_formula_sum 'C64 H72 N4 S' _chemical_formula_weight 929.31 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_date 2019-12-03 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2020-08-04 deposited with the CCDC. 2021-02-23 downloaded from the CCDC. ; _cell_angle_alpha 114.757(4) _cell_angle_beta 104.294(4) _cell_angle_gamma 93.279(5) _cell_formula_units_Z 2 _cell_length_a 12.0410(11) _cell_length_b 15.9608(15) _cell_length_c 16.4529(14) _cell_measurement_reflns_used 9960 _cell_measurement_temperature 207(2) _cell_measurement_theta_max 52.615 _cell_measurement_theta_min 2.696 _cell_volume 2735.8(4) _computing_cell_refinement 'SAINT V8.40A (?, 2016)' _computing_data_reduction 'SAINT V8.40A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XS (Sheldrick, 2008)' _diffrn_ambient_temperature 207.0 _diffrn_measured_fraction_theta_full 0.961 _diffrn_measured_fraction_theta_max 0.961 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0967 _diffrn_reflns_av_unetI/netI 0.1068 _diffrn_reflns_Laue_measured_fraction_full 0.961 _diffrn_reflns_Laue_measured_fraction_max 0.961 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 41322 _diffrn_reflns_point_group_measured_fraction_full 0.961 _diffrn_reflns_point_group_measured_fraction_max 0.961 _diffrn_reflns_theta_full 25.023 _diffrn_reflns_theta_max 25.023 _diffrn_reflns_theta_min 1.428 _exptl_absorpt_coefficient_mu 0.102 _exptl_absorpt_correction_T_max 0.7392 _exptl_absorpt_correction_T_min 0.6144 _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.128 _exptl_crystal_description needle _exptl_crystal_F_000 1000 _exptl_crystal_size_max 0.43 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.02 _refine_diff_density_max 2.473 _refine_diff_density_min -0.451 _refine_diff_density_rms 0.093 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 636 _refine_ls_number_reflns 9284 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.041 _refine_ls_R_factor_all 0.1862 _refine_ls_R_factor_gt 0.1335 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1617P)^2^+7.7825P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3389 _refine_ls_wR_factor_ref 0.3664 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5992 _reflns_number_total 9284 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; p-1.res created by SHELXL-2014/7 TITL p-1_a.res in P-1 REM Old TITL p-1 in P-1 #2 REM SHELXT solution in P-1 REM R1 0.276, Rweak 0.100, Alpha 0.132, Orientation as input REM Formula found by SHELXT: C61 N4 S CELL 0.71073 12.041 15.9608 16.4529 114.757 104.294 93.279 ZERR 2 0.0011 0.0015 0.0014 0.004 0.004 0.005 LATT 1 SFAC C H N S UNIT 128 144 8 2 L.S. 10 PLAN 20 TEMP -66.15 BOND $H list 4 fmap 2 53 ACTA REM REM REM WGHT 0.161700 7.782500 FVAR 0.27083 S001 4 0.922005 0.402467 0.125780 11.00000 0.05784 0.11633 = 0.04692 0.02550 0.01118 0.03039 N002 3 0.248946 0.312740 -0.161935 11.00000 0.03484 0.06635 = 0.03275 0.01631 0.00436 0.01239 N003 3 1.217004 0.697236 0.675229 11.00000 0.04738 0.05547 = 0.02972 0.01217 0.00357 0.00938 C004 1 0.721724 0.559861 0.340793 11.00000 0.04068 0.05189 = 0.04239 0.01461 0.00024 0.00928 AFIX 43 H004 2 0.707861 0.597025 0.397862 11.00000 -1.20000 AFIX 0 C005 1 0.254493 0.263240 -0.253289 11.00000 0.03937 0.05429 = 0.03683 0.01667 0.01061 0.01507 C006 1 0.636304 0.464273 0.170720 11.00000 0.03956 0.04576 = 0.04036 0.02156 0.00314 0.01112 C007 1 0.751760 0.450093 0.169412 11.00000 0.04551 0.05435 = 0.03651 0.02039 0.00240 0.01124 C008 1 0.847277 0.490481 0.252941 11.00000 0.03865 0.05742 = 0.04326 0.02322 0.00593 0.01529 C009 1 1.120502 0.662543 0.593366 11.00000 0.04357 0.04512 = 0.02809 0.01267 0.00158 0.00944 C00A 1 0.625535 0.519307 0.257325 11.00000 0.04072 0.05565 = 0.05194 0.02453 0.00972 0.01100 AFIX 43 H00A 2 0.551123 0.530893 0.261945 11.00000 -1.20000 AFIX 0 C00B 1 0.353665 0.438712 -0.007099 11.00000 0.03782 0.05464 = 0.04045 0.02099 0.00648 0.01357 AFIX 43 H00B 2 0.296502 0.475008 -0.013873 11.00000 -1.20000 AFIX 0 C00C 1 0.931891 0.588996 0.428833 11.00000 0.04221 0.04426 = 0.03180 0.01529 0.00386 0.00833 C00D 1 1.330630 0.679715 0.679193 11.00000 0.04570 0.04767 = 0.03428 0.01699 0.00844 0.01119 C00E 1 0.833542 0.547133 0.341631 11.00000 0.04146 0.05006 = 0.03967 0.02232 0.00189 0.00732 C00F 1 0.920493 0.589496 0.511093 11.00000 0.03932 0.04798 = 0.03981 0.01745 0.00939 0.01096 AFIX 43 H00F 2 0.847883 0.565133 0.511639 11.00000 -1.20000 AFIX 0 C00G 1 0.344161 0.349447 -0.078017 11.00000 0.03538 0.05529 = 0.03719 0.01676 0.00433 0.00890 C00H 1 0.447251 0.474083 0.073413 11.00000 0.03903 0.04976 = 0.04019 0.01633 0.00770 0.01210 AFIX 43 H00H 2 0.451489 0.533952 0.121553 11.00000 -1.20000 AFIX 0 N00I 3 0.951039 0.467862 0.237138 11.00000 0.06188 0.08932 = 0.04899 0.02747 0.00753 0.02020 C00J 1 0.131648 0.315523 -0.166566 11.00000 0.03793 0.05313 = 0.04029 0.01772 0.00985 0.01441 C00K 1 0.430114 0.297701 -0.067350 11.00000 0.04294 0.04659 = 0.04458 0.01661 0.00387 0.00990 AFIX 43 H00K 2 0.423417 0.236832 -0.114718 11.00000 -1.20000 AFIX 0 C00L 1 0.063707 0.267031 -0.261223 11.00000 0.03722 0.04661 = 0.03469 0.01688 0.01044 0.01355 C00M 1 0.535702 0.423775 0.085565 11.00000 0.03695 0.05397 = 0.03819 0.02341 0.00411 0.00576 N00N 3 0.784255 0.398337 0.090542 11.00000 0.05267 0.08911 = 0.04717 0.02264 0.00571 0.02221 C00O 1 1.013413 0.624964 0.591922 11.00000 0.05288 0.04800 = 0.03091 0.01417 0.01313 0.01398 AFIX 43 H00O 2 1.003783 0.623546 0.646343 11.00000 -1.20000 AFIX 0 C00P 1 1.217434 0.757469 0.766149 11.00000 0.04946 0.04818 = 0.03494 0.01613 0.01059 0.01293 C00Q 1 1.041191 0.627202 0.431632 11.00000 0.04823 0.05811 = 0.03713 0.02361 0.00661 0.00889 AFIX 43 H00Q 2 1.051695 0.627480 0.376993 11.00000 -1.20000 AFIX 0 C00R 1 0.525386 0.334034 0.011654 11.00000 0.04040 0.04673 = 0.04222 0.01663 0.00378 0.01255 AFIX 43 H00R 2 0.584254 0.298613 0.016391 11.00000 -1.20000 AFIX 0 C00S 1 0.141747 0.234719 -0.316008 11.00000 0.03782 0.04694 = 0.03546 0.01626 0.00466 0.01011 C00T 1 -0.057883 0.257712 -0.285377 11.00000 0.04051 0.04428 = 0.03897 0.01544 0.00534 0.01191 AFIX 43 H00T 2 -0.103045 0.224514 -0.348557 11.00000 -1.20000 AFIX 0 C00U 1 1.402607 0.728207 0.772726 11.00000 0.04841 0.04757 = 0.02632 0.01485 0.00108 0.00586 C00V 1 0.124186 0.185202 -0.412531 11.00000 0.04391 0.05013 = 0.03450 0.01137 0.00628 0.01332 AFIX 43 H00V 2 0.048165 0.165954 -0.454179 11.00000 -1.20000 AFIX 0 C00W 1 1.133472 0.664311 0.512465 11.00000 0.04459 0.05420 = 0.04316 0.02118 0.00553 0.00088 AFIX 43 H00W 2 1.205497 0.690936 0.513011 11.00000 -1.20000 AFIX 0 C00X 1 1.330244 0.777616 0.827319 11.00000 0.04788 0.04480 = 0.03419 0.01633 0.00427 0.00848 C00Y 1 1.519201 0.718490 0.794508 11.00000 0.04705 0.04996 = 0.03867 0.02132 0.00113 0.00315 AFIX 43 H00Y 2 1.566984 0.750361 0.857014 11.00000 -1.20000 AFIX 0 C00Z 1 0.350993 0.245050 -0.287018 11.00000 0.03402 0.06210 = 0.04762 0.01704 0.00679 0.01114 AFIX 43 H00Z 2 0.427353 0.265771 -0.245852 11.00000 -1.20000 AFIX 0 C010 1 1.352586 0.838777 0.922318 11.00000 0.05834 0.04380 = 0.03438 0.01119 0.00611 0.00753 AFIX 43 H010 2 1.428529 0.853661 0.963283 11.00000 -1.20000 AFIX 0 C011 1 -0.111947 0.297499 -0.216037 11.00000 0.04510 0.04938 = 0.04942 0.02032 0.01450 0.01514 C012 1 0.330185 0.195732 -0.382626 11.00000 0.04509 0.06280 = 0.05063 0.01876 0.01910 0.01650 AFIX 43 H012 2 0.394455 0.182514 -0.405663 11.00000 -1.20000 AFIX 0 C013 1 0.218487 0.164302 -0.447205 11.00000 0.05306 0.06000 = 0.04371 0.01965 0.01703 0.02003 C014 1 1.565876 0.662488 0.725350 11.00000 0.05034 0.05280 = 0.04913 0.02281 0.01333 0.00953 C015 1 0.078531 0.353913 -0.096540 11.00000 0.04437 0.07424 = 0.03710 0.01520 0.01081 0.01523 AFIX 43 H015 2 0.122944 0.385561 -0.033052 11.00000 -1.20000 AFIX 0 C016 1 -0.040772 0.344289 -0.122755 11.00000 0.05157 0.07052 = 0.04812 0.02158 0.02161 0.01967 AFIX 43 H016 2 -0.076750 0.370582 -0.075436 11.00000 -1.20000 AFIX 0 C017 1 1.152949 0.855427 0.892643 11.00000 0.06647 0.05464 = 0.05113 0.01460 0.01850 0.01425 AFIX 43 H017 2 1.092339 0.881462 0.915303 11.00000 -1.20000 AFIX 0 C018 1 1.127827 0.797570 0.798422 11.00000 0.05407 0.05486 = 0.04345 0.01242 0.00835 0.01419 AFIX 43 H018 2 1.052683 0.785495 0.757180 11.00000 -1.20000 AFIX 0 C019 1 1.374873 0.622377 0.609060 11.00000 0.05534 0.05656 = 0.03501 0.01419 0.00593 0.00946 AFIX 43 H019 2 1.327338 0.589066 0.546594 11.00000 -1.20000 AFIX 0 C01A 1 0.195575 0.108019 -0.553014 11.00000 0.07637 0.06934 = 0.04544 0.01954 0.02569 0.02565 C01B 1 1.490527 0.616009 0.634117 11.00000 0.05489 0.05762 = 0.04677 0.01836 0.01728 0.01185 AFIX 43 H01B 2 1.520876 0.577793 0.586618 11.00000 -1.20000 AFIX 0 C01C 1 -0.243680 0.288899 -0.244580 11.00000 0.04144 0.06092 = 0.06738 0.01941 0.01632 0.01672 C01D 1 1.264166 0.877836 0.956992 11.00000 0.07408 0.04876 = 0.03905 0.01471 0.01279 0.00874 C01E 1 0.125924 0.156656 -0.604966 11.00000 0.10121 0.08810 = 0.04555 0.02729 0.02529 0.03246 AFIX 137 H01A 2 0.049750 0.158406 -0.595113 11.00000 -1.50000 H01C 2 0.116779 0.122385 -0.671469 11.00000 -1.50000 H01D 2 0.166817 0.220199 -0.581450 11.00000 -1.50000 AFIX 0 C01F 1 1.695199 0.654838 0.749946 11.00000 0.04914 0.06139 = 0.06529 0.02826 0.01938 0.01008 C01G 1 1.290827 0.944108 1.061059 11.00000 0.10498 0.06094 = 0.04181 0.00931 0.02559 0.01061 C01H 1 -0.303430 0.183707 -0.296103 11.00000 0.05185 0.07881 = 0.07841 0.01250 0.01610 0.00089 AFIX 137 H01E 2 -0.282191 0.152430 -0.353327 11.00000 -1.50000 H01F 2 -0.387371 0.179159 -0.311381 11.00000 -1.50000 H01G 2 -0.277957 0.153990 -0.255702 11.00000 -1.50000 AFIX 0 C01I 1 0.122484 0.009311 -0.585977 11.00000 0.09100 0.06377 = 0.05904 0.01346 0.01206 0.01430 AFIX 137 H01H 2 0.165696 -0.022983 -0.553749 11.00000 -1.50000 H01I 2 0.107178 -0.027079 -0.653097 11.00000 -1.50000 H01J 2 0.049196 0.016709 -0.571549 11.00000 -1.50000 AFIX 0 C01J 1 0.307516 0.092458 -0.579562 11.00000 0.09187 0.13029 = 0.05812 0.00863 0.03615 0.03143 AFIX 137 H01K 2 0.353283 0.152449 -0.562905 11.00000 -1.50000 H01L 2 0.288775 0.053313 -0.646572 11.00000 -1.50000 H01M 2 0.351973 0.061674 -0.546162 11.00000 -1.50000 AFIX 0 C01K 1 -0.289266 0.333566 -0.161259 11.00000 0.05294 0.10024 = 0.10701 -0.00283 0.03357 0.01546 AFIX 137 H01N 2 -0.262732 0.307030 -0.118105 11.00000 -1.50000 H01O 2 -0.373799 0.321603 -0.182559 11.00000 -1.50000 H01P 2 -0.260509 0.400719 -0.129665 11.00000 -1.50000 AFIX 0 C01L 1 -0.281507 0.332248 -0.311550 11.00000 0.05194 0.16229 = 0.18423 0.12677 0.02578 0.04169 AFIX 137 H01Q 2 -0.248801 0.398757 -0.279672 11.00000 -1.50000 H01R 2 -0.365891 0.323641 -0.331918 11.00000 -1.50000 H01S 2 -0.253882 0.301912 -0.365645 11.00000 -1.50000 AFIX 0 C01M 1 1.379990 1.031940 1.086549 11.00000 0.15975 0.06633 = 0.06420 0.00337 0.01814 -0.01497 AFIX 137 H01T 2 1.448869 1.012483 1.068949 11.00000 -1.50000 H01U 2 1.401651 1.072092 1.153540 11.00000 -1.50000 H01V 2 1.345197 1.066161 1.053095 11.00000 -1.50000 AFIX 0 C01N 1 1.729743 0.637073 0.831524 11.00000 0.06922 0.49188 = 0.15809 0.22224 0.05468 0.13245 AFIX 137 H01W 2 1.731284 0.692996 0.887191 11.00000 -1.50000 H01X 2 1.806708 0.620681 0.838190 11.00000 -1.50000 H01Y 2 1.674297 0.585683 0.823648 11.00000 -1.50000 AFIX 0 C01O 1 1.355517 0.900544 1.120290 11.00000 0.24852 0.12365 = 0.05236 0.03811 0.04702 0.05949 AFIX 137 H01Z 2 1.305210 0.845429 1.110670 11.00000 -1.50000 H 2 1.378169 0.945707 1.185952 11.00000 -1.50000 HA 2 1.424597 0.882598 1.102177 11.00000 -1.50000 AFIX 0 C01P 1 1.767669 0.740621 0.764967 11.00000 0.07596 0.15595 = 0.40418 0.17285 0.09275 0.03144 AFIX 137 H01 2 1.755088 0.794393 0.816131 11.00000 -1.50000 HB 2 1.746438 0.748782 0.708251 11.00000 -1.50000 HC 2 1.849194 0.735167 0.780409 11.00000 -1.50000 AFIX 0 C01Q 1 1.720745 0.571855 0.668905 11.00000 0.07919 0.13970 = 0.13899 0.02314 0.01264 0.05778 AFIX 137 H0AA 2 1.671467 0.514195 0.654530 11.00000 -1.50000 HD 2 1.801949 0.566515 0.687605 11.00000 -1.50000 HE 2 1.704827 0.582860 0.613803 11.00000 -1.50000 AFIX 0 C01R 1 1.185907 0.978386 1.087970 11.00000 0.12059 0.26921 = 0.07330 -0.04816 0.04781 0.01891 AFIX 137 H1AA 2 1.146335 1.003438 1.046554 11.00000 -1.50000 HF 2 1.210111 1.027225 1.152181 11.00000 -1.50000 HG 2 1.133332 0.926693 1.082603 11.00000 -1.50000 AFIX 0 C2 1 0.798848 0.977407 0.234688 11.00000 0.22431 0.12885 = 0.17927 0.07738 0.07405 -0.01995 AFIX 23 H2A 2 0.852795 1.035367 0.254193 11.00000 -1.20000 H2B 2 0.838050 0.947999 0.272731 11.00000 -1.20000 AFIX 0 C3 1 0.708672 1.009862 0.273477 11.00000 0.17181 0.16792 = 0.19456 0.09161 0.06144 -0.01693 AFIX 23 H3A 2 0.669959 1.041473 0.237614 11.00000 -1.20000 H3B 2 0.653292 0.952724 0.254163 11.00000 -1.20000 AFIX 0 C4 1 0.805744 0.920869 0.146720 11.00000 0.22683 0.16627 = 0.19712 0.07877 0.07537 -0.04831 AFIX 23 H4A 2 0.759767 0.859788 0.128754 11.00000 -1.20000 H4B 2 0.760913 0.945611 0.106138 11.00000 -1.20000 AFIX 0 C5 1 0.900045 0.900362 0.116746 11.00000 0.26383 0.22236 = 0.24464 0.15843 0.13633 0.08401 AFIX 137 H5A 2 0.875584 0.866092 0.048860 11.00000 -1.50000 H5B 2 0.939270 0.862198 0.143406 11.00000 -1.50000 H5C 2 0.953021 0.958066 0.136441 11.00000 -1.50000 AFIX 0 C6 1 0.617261 1.095515 0.396419 11.00000 0.24102 0.20056 = 0.14613 0.00189 0.07674 -0.02727 AFIX 137 H6A 2 0.586105 1.138300 0.372630 11.00000 -1.50000 H6B 2 0.644377 1.127568 0.464409 11.00000 -1.50000 H6C 2 0.556759 1.041979 0.375952 11.00000 -1.50000 AFIX 0 C7 1 0.710791 1.064649 0.362025 11.00000 0.30463 0.19886 = 0.18816 0.04116 0.13411 0.03433 AFIX 23 H7A 2 0.766274 1.121993 0.382188 11.00000 -1.20000 H7B 2 0.747991 1.032990 0.398377 11.00000 -1.20000 AFIX 0 HKLF 4 REM p-1_a.res in P-1 REM R1 = 0.1335 for 5992 Fo > 4sig(Fo) and 0.1862 for all 9284 data REM 636 parameters refined using 0 restraints END WGHT 0.1617 7.7826 REM Highest difference peak 2.473, deepest hole -0.451, 1-sigma level 0.093 Q1 1 0.5519 0.6155 0.4051 11.00000 0.05 2.47 Q2 1 0.6854 0.6174 0.4370 11.00000 0.05 0.86 Q3 1 0.5203 0.5567 0.2959 11.00000 0.05 0.83 Q4 1 1.7536 0.7241 0.8603 11.00000 0.05 0.55 Q5 1 1.7052 0.5615 0.7358 11.00000 0.05 0.54 Q6 1 1.1821 0.8798 1.0908 11.00000 0.05 0.42 Q7 1 1.7429 0.6975 0.6979 11.00000 0.05 0.39 Q8 1 1.2629 1.0360 1.0739 11.00000 0.05 0.34 Q9 1 0.2127 0.0604 -0.7335 11.00000 0.05 0.31 Q10 1 1.5627 0.5870 0.4794 11.00000 0.05 0.30 Q11 1 -0.2471 0.4072 -0.2156 11.00000 0.05 0.30 Q12 1 0.0318 0.3828 0.0412 11.00000 0.05 0.29 Q13 1 0.2120 0.0331 -0.5767 11.00000 0.05 0.29 Q14 1 1.8427 0.6799 0.8599 11.00000 0.05 0.28 Q15 1 -0.2992 0.2409 -0.3462 11.00000 0.05 0.28 Q16 1 -0.4765 0.3379 -0.4577 11.00000 0.05 0.28 Q17 1 -0.0730 0.4380 0.0204 11.00000 0.05 0.27 Q18 1 -0.0824 0.3797 -0.0225 11.00000 0.05 0.26 Q19 1 0.3209 0.2232 -0.5670 11.00000 0.05 0.25 Q20 1 0.9010 0.3571 0.0213 11.00000 0.05 0.25 REM The information below was added by Olex2. REM REM R1 = 0.1335 for 5992 Fo > 4sig(Fo) and 0.1862 for all 41322 data REM n/a parameters refined using n/a restraints REM Highest difference peak 2.47, deepest hole -0.45 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1862 REM R1_gt = 0.1335 REM wR_ref = 0.3664 REM GOOF = 1.041 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 41322 REM Reflections_gt = 5992 REM Parameters = n/a REM Hole = -0.45 REM Peak = 2.47 REM Flack = n/a ; _cod_data_source_file d1sc00272d2.cif _cod_data_source_block p-1 _cod_database_code 1560601 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C3(H3A,H3B), C4(H4A,H4B), C7(H7A,H7B) 2.b Aromatic/amide H refined with riding coordinates: C004(H004), C00A(H00A), C00B(H00B), C00F(H00F), C00H(H00H), C00K(H00K), C00O(H00O), C00Q(H00Q), C00R(H00R), C00T(H00T), C00V(H00V), C00W(H00W), C00Y(H00Y), C00Z(H00Z), C010(H010), C012(H012), C015(H015), C016(H016), C017(H017), C018(H018), C019(H019), C01B(H01B) 2.c Idealised Me refined as rotating group: C01E(H01A,H01C,H01D), C01H(H01E,H01F,H01G), C01I(H01H,H01I,H01J), C01J(H01K, H01L,H01M), C01K(H01N,H01O,H01P), C01L(H01Q,H01R,H01S), C01M(H01T,H01U,H01V), C01N(H01W,H01X,H01Y), C01O(H01Z,H,HA), C01P(H01,HB,HC), C01Q(H0AA,HD,HE), C01R(H1AA,HF,HG), C5(H5A,H5B,H5C), C6(H6A,H6B,H6C) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S001 S 0.92201(16) 0.40247(16) 0.12578(12) 0.0779(6) Uani 1 1 d . . . . . N002 N 0.2489(4) 0.3127(3) -0.1619(3) 0.0478(11) Uani 1 1 d . . . . . N003 N 1.2170(4) 0.6972(3) 0.6752(3) 0.0483(11) Uani 1 1 d . . . . . C004 C 0.7217(5) 0.5599(4) 0.3408(4) 0.0497(14) Uani 1 1 d . . . . . H004 H 0.7079 0.5970 0.3979 0.060 Uiso 1 1 calc R . . . . C005 C 0.2545(5) 0.2632(4) -0.2533(4) 0.0447(13) Uani 1 1 d . . . . . C006 C 0.6363(4) 0.4643(4) 0.1707(4) 0.0427(13) Uani 1 1 d . . . . . C007 C 0.7518(5) 0.4501(4) 0.1694(4) 0.0473(13) Uani 1 1 d . . . . . C008 C 0.8473(5) 0.4905(4) 0.2529(4) 0.0472(13) Uani 1 1 d . . . . . C009 C 1.1205(5) 0.6625(4) 0.5934(3) 0.0420(13) Uani 1 1 d . . . . . C00A C 0.6255(5) 0.5193(4) 0.2573(4) 0.0500(14) Uani 1 1 d . . . . . H00A H 0.5511 0.5309 0.2619 0.060 Uiso 1 1 calc R . . . . C00B C 0.3537(4) 0.4387(4) -0.0071(4) 0.0452(13) Uani 1 1 d . . . . . H00B H 0.2965 0.4750 -0.0139 0.054 Uiso 1 1 calc R . . . . C00C C 0.9319(5) 0.5890(4) 0.4288(3) 0.0415(12) Uani 1 1 d . . . . . C00D C 1.3306(5) 0.6797(4) 0.6792(4) 0.0436(13) Uani 1 1 d . . . . . C00E C 0.8335(5) 0.5471(4) 0.3416(4) 0.0450(13) Uani 1 1 d . . . . . C00F C 0.9205(5) 0.5895(4) 0.5111(4) 0.0435(13) Uani 1 1 d . . . . . H00F H 0.8479 0.5651 0.5116 0.052 Uiso 1 1 calc R . . . . C00G C 0.3442(4) 0.3494(4) -0.0780(4) 0.0453(13) Uani 1 1 d . . . . . C00H C 0.4473(4) 0.4741(4) 0.0734(4) 0.0450(13) Uani 1 1 d . . . . . H00H H 0.4515 0.5340 0.1216 0.054 Uiso 1 1 calc R . . . . N00I N 0.9510(5) 0.4679(4) 0.2371(4) 0.0695(15) Uani 1 1 d . . . . . C00J C 0.1316(5) 0.3155(4) -0.1666(4) 0.0450(13) Uani 1 1 d . . . . . C00K C 0.4301(5) 0.2977(4) -0.0674(4) 0.0478(13) Uani 1 1 d . . . . . H00K H 0.4234 0.2368 -0.1147 0.057 Uiso 1 1 calc R . . . . C00L C 0.0637(4) 0.2670(4) -0.2612(3) 0.0398(12) Uani 1 1 d . . . . . C00M C 0.5357(4) 0.4238(4) 0.0856(4) 0.0436(13) Uani 1 1 d . . . . . N00N N 0.7843(4) 0.3983(4) 0.0905(4) 0.0672(15) Uani 1 1 d . . . . . C00O C 1.0134(5) 0.6250(4) 0.5919(4) 0.0449(13) Uani 1 1 d . . . . . H00O H 1.0038 0.6235 0.6463 0.054 Uiso 1 1 calc R . . . . C00P C 1.2174(5) 0.7575(4) 0.7661(4) 0.0453(13) Uani 1 1 d . . . . . C00Q C 1.0412(5) 0.6272(4) 0.4316(4) 0.0483(14) Uani 1 1 d . . . . . H00Q H 1.0517 0.6275 0.3770 0.058 Uiso 1 1 calc R . . . . C00R C 0.5254(5) 0.3340(4) 0.0117(4) 0.0458(13) Uani 1 1 d . . . . . H00R H 0.5843 0.2986 0.0164 0.055 Uiso 1 1 calc R . . . . C00S C 0.1417(4) 0.2347(4) -0.3160(3) 0.0420(12) Uani 1 1 d . . . . . C00T C -0.0579(5) 0.2577(4) -0.2854(4) 0.0435(13) Uani 1 1 d . . . . . H00T H -0.1030 0.2245 -0.3486 0.052 Uiso 1 1 calc R . . . . C00U C 1.4026(5) 0.7282(4) 0.7727(3) 0.0435(13) Uani 1 1 d . . . . . C00V C 0.1242(5) 0.1852(4) -0.4125(4) 0.0464(13) Uani 1 1 d . . . . . H00V H 0.0482 0.1660 -0.4542 0.056 Uiso 1 1 calc R . . . . C00W C 1.1335(5) 0.6643(4) 0.5125(4) 0.0494(14) Uani 1 1 d . . . . . H00W H 1.2055 0.6909 0.5130 0.059 Uiso 1 1 calc R . . . . C00X C 1.3302(5) 0.7776(4) 0.8273(4) 0.0444(13) Uani 1 1 d . . . . . C00Y C 1.5192(5) 0.7185(4) 0.7945(4) 0.0473(13) Uani 1 1 d . . . . . H00Y H 1.5670 0.7504 0.8570 0.057 Uiso 1 1 calc R . . . . C00Z C 0.3510(5) 0.2451(4) -0.2870(4) 0.0516(14) Uani 1 1 d . . . . . H00Z H 0.4274 0.2658 -0.2459 0.062 Uiso 1 1 calc R . . . . C010 C 1.3526(5) 0.8388(4) 0.9223(4) 0.0494(14) Uani 1 1 d . . . . . H010 H 1.4285 0.8537 0.9633 0.059 Uiso 1 1 calc R . . . . C011 C -0.1119(5) 0.2975(4) -0.2160(4) 0.0482(13) Uani 1 1 d . . . . . C012 C 0.3302(5) 0.1957(4) -0.3826(4) 0.0540(15) Uani 1 1 d . . . . . H012 H 0.3945 0.1825 -0.4057 0.065 Uiso 1 1 calc R . . . . C013 C 0.2185(5) 0.1643(4) -0.4472(4) 0.0526(15) Uani 1 1 d . . . . . C014 C 1.5659(5) 0.6625(4) 0.7254(4) 0.0511(14) Uani 1 1 d . . . . . C015 C 0.0785(5) 0.3539(4) -0.0965(4) 0.0555(15) Uani 1 1 d . . . . . H015 H 0.1229 0.3856 -0.0331 0.067 Uiso 1 1 calc R . . . . C016 C -0.0408(5) 0.3443(4) -0.1228(4) 0.0568(15) Uani 1 1 d . . . . . H016 H -0.0767 0.3706 -0.0754 0.068 Uiso 1 1 calc R . . . . C017 C 1.1529(6) 0.8554(4) 0.8926(4) 0.0604(16) Uani 1 1 d . . . . . H017 H 1.0923 0.8815 0.9153 0.072 Uiso 1 1 calc R . . . . C018 C 1.1278(5) 0.7976(4) 0.7984(4) 0.0553(15) Uani 1 1 d . . . . . H018 H 1.0527 0.7855 0.7572 0.066 Uiso 1 1 calc R . . . . C019 C 1.3749(5) 0.6224(4) 0.6091(4) 0.0528(15) Uani 1 1 d . . . . . H019 H 1.3273 0.5891 0.5466 0.063 Uiso 1 1 calc R . . . . C01A C 0.1956(6) 0.1080(5) -0.5530(4) 0.0639(17) Uani 1 1 d . . . . . C01B C 1.4905(5) 0.6160(4) 0.6341(4) 0.0544(15) Uani 1 1 d . . . . . H01B H 1.5209 0.5778 0.5866 0.065 Uiso 1 1 calc R . . . . C01C C -0.2437(5) 0.2889(4) -0.2446(5) 0.0596(16) Uani 1 1 d . . . . . C01D C 1.2642(6) 0.8778(4) 0.9570(4) 0.0567(16) Uani 1 1 d . . . . . C01E C 0.1259(7) 0.1567(5) -0.6050(5) 0.078(2) Uani 1 1 d . . . . . H01A H 0.0497 0.1584 -0.5951 0.117 Uiso 1 1 calc GR . . . . H01C H 0.1168 0.1224 -0.6715 0.117 Uiso 1 1 calc GR . . . . H01D H 0.1668 0.2202 -0.5815 0.117 Uiso 1 1 calc GR . . . . C01F C 1.6952(5) 0.6548(4) 0.7499(4) 0.0582(15) Uani 1 1 d . . . . . C01G C 1.2908(7) 0.9441(5) 1.0611(4) 0.074(2) Uani 1 1 d . . . . . C01H C -0.3034(6) 0.1837(5) -0.2961(5) 0.079(2) Uani 1 1 d . . . . . H01E H -0.2822 0.1524 -0.3533 0.119 Uiso 1 1 calc GR . . . . H01F H -0.3874 0.1792 -0.3114 0.119 Uiso 1 1 calc GR . . . . H01G H -0.2780 0.1540 -0.2557 0.119 Uiso 1 1 calc GR . . . . C01I C 0.1225(7) 0.0093(5) -0.5860(5) 0.078(2) Uani 1 1 d . . . . . H01H H 0.1657 -0.0230 -0.5537 0.118 Uiso 1 1 calc GR . . . . H01I H 0.1072 -0.0271 -0.6531 0.118 Uiso 1 1 calc GR . . . . H01J H 0.0492 0.0167 -0.5715 0.118 Uiso 1 1 calc GR . . . . C01J C 0.3075(7) 0.0925(7) -0.5796(5) 0.102(3) Uani 1 1 d . . . . . H01K H 0.3533 0.1524 -0.5629 0.153 Uiso 1 1 calc GR . . . . H01L H 0.2888 0.0533 -0.6466 0.153 Uiso 1 1 calc GR . . . . H01M H 0.3520 0.0617 -0.5462 0.153 Uiso 1 1 calc GR . . . . C01K C -0.2893(6) 0.3336(6) -0.1613(6) 0.102(3) Uani 1 1 d . . . . . H01N H -0.2627 0.3070 -0.1181 0.154 Uiso 1 1 calc GR . . . . H01O H -0.3738 0.3216 -0.1826 0.154 Uiso 1 1 calc GR . . . . H01P H -0.2605 0.4007 -0.1297 0.154 Uiso 1 1 calc GR . . . . C01L C -0.2815(7) 0.3322(8) -0.3115(8) 0.116(4) Uani 1 1 d . . . . . H01Q H -0.2488 0.3988 -0.2797 0.174 Uiso 1 1 calc GR . . . . H01R H -0.3659 0.3236 -0.3319 0.174 Uiso 1 1 calc GR . . . . H01S H -0.2539 0.3019 -0.3656 0.174 Uiso 1 1 calc GR . . . . C01M C 1.3800(9) 1.0319(6) 1.0865(6) 0.111(3) Uani 1 1 d . . . . . H01T H 1.4489 1.0125 1.0689 0.166 Uiso 1 1 calc GR . . . . H01U H 1.4017 1.0721 1.1535 0.166 Uiso 1 1 calc GR . . . . H01V H 1.3452 1.0662 1.0531 0.166 Uiso 1 1 calc GR . . . . C01N C 1.7297(8) 0.6371(14) 0.8315(9) 0.204(9) Uani 1 1 d . . . . . H01W H 1.7313 0.6930 0.8872 0.306 Uiso 1 1 calc GR . . . . H01X H 1.8067 0.6207 0.8382 0.306 Uiso 1 1 calc GR . . . . H01Y H 1.6743 0.5857 0.8236 0.306 Uiso 1 1 calc GR . . . . C01O C 1.3555(12) 0.9005(7) 1.1203(6) 0.140(5) Uani 1 1 d . . . . . H01Z H 1.3052 0.8454 1.1107 0.211 Uiso 1 1 calc GR . . . . H H 1.3782 0.9457 1.1860 0.211 Uiso 1 1 calc GR . . . . HA H 1.4246 0.8826 1.1022 0.211 Uiso 1 1 calc GR . . . . C01P C 1.7677(9) 0.7406(9) 0.7650(13) 0.190(7) Uani 1 1 d . . . . . H01 H 1.7551 0.7944 0.8161 0.285 Uiso 1 1 calc GR . . . . HB H 1.7464 0.7488 0.7083 0.285 Uiso 1 1 calc GR . . . . HC H 1.8492 0.7352 0.7804 0.285 Uiso 1 1 calc GR . . . . C01Q C 1.7207(8) 0.5719(8) 0.6689(8) 0.136(4) Uani 1 1 d . . . . . H0AA H 1.6715 0.5142 0.6545 0.204 Uiso 1 1 calc GR . . . . HD H 1.8019 0.5665 0.6876 0.204 Uiso 1 1 calc GR . . . . HE H 1.7048 0.5829 0.6138 0.204 Uiso 1 1 calc GR . . . . C01R C 1.1859(10) 0.9784(11) 1.0880(7) 0.196(8) Uani 1 1 d . . . . . H1AA H 1.1463 1.0034 1.0466 0.295 Uiso 1 1 calc GR . . . . HF H 1.2101 1.0272 1.1522 0.295 Uiso 1 1 calc GR . . . . HG H 1.1333 0.9267 1.0826 0.295 Uiso 1 1 calc GR . . . . C2 C 0.7988(17) 0.9774(11) 0.2347(13) 0.174(6) Uani 1 1 d . . . . . H2A H 0.8528 1.0354 0.2542 0.209 Uiso 1 1 calc R . . . . H2B H 0.8380 0.9480 0.2727 0.209 Uiso 1 1 calc R . . . . C3 C 0.7087(15) 1.0099(12) 0.2735(14) 0.175(6) Uani 1 1 d . . . . . H3A H 0.6700 1.0415 0.2376 0.210 Uiso 1 1 calc R . . . . H3B H 0.6533 0.9527 0.2542 0.210 Uiso 1 1 calc R . . . . C4 C 0.8057(18) 0.9209(14) 0.1467(15) 0.199(8) Uani 1 1 d . . . . . H4A H 0.7598 0.8598 0.1288 0.239 Uiso 1 1 calc R . . . . H4B H 0.7609 0.9456 0.1061 0.239 Uiso 1 1 calc R . . . . C5 C 0.9000(18) 0.9004(13) 0.1167(14) 0.210(8) Uani 1 1 d . . . . . H5A H 0.8756 0.8661 0.0489 0.315 Uiso 1 1 calc GR . . . . H5B H 0.9393 0.8622 0.1434 0.315 Uiso 1 1 calc GR . . . . H5C H 0.9530 0.9581 0.1364 0.315 Uiso 1 1 calc GR . . . . C6 C 0.6173(17) 1.0955(13) 0.3964(11) 0.222(9) Uani 1 1 d . . . . . H6A H 0.5861 1.1383 0.3726 0.334 Uiso 1 1 calc GR . . . . H6B H 0.6444 1.1276 0.4644 0.334 Uiso 1 1 calc GR . . . . H6C H 0.5568 1.0420 0.3760 0.334 Uiso 1 1 calc GR . . . . C7 C 0.711(2) 1.0646(14) 0.3620(15) 0.235(10) Uani 1 1 d . . . . . H7A H 0.7663 1.1220 0.3822 0.282 Uiso 1 1 calc R . . . . H7B H 0.7480 1.0330 0.3984 0.282 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S001 0.0578(11) 0.1163(16) 0.0469(10) 0.0255(10) 0.0112(8) 0.0304(10) N002 0.035(3) 0.066(3) 0.033(2) 0.016(2) 0.0044(19) 0.012(2) N003 0.047(3) 0.055(3) 0.030(2) 0.012(2) 0.004(2) 0.009(2) C004 0.041(3) 0.052(3) 0.042(3) 0.015(3) 0.000(2) 0.009(3) C005 0.039(3) 0.054(3) 0.037(3) 0.017(2) 0.011(2) 0.015(3) C006 0.040(3) 0.046(3) 0.040(3) 0.022(2) 0.003(2) 0.011(2) C007 0.046(3) 0.054(3) 0.037(3) 0.020(3) 0.002(2) 0.011(3) C008 0.039(3) 0.057(3) 0.043(3) 0.023(3) 0.006(2) 0.015(3) C009 0.044(3) 0.045(3) 0.028(3) 0.013(2) 0.002(2) 0.009(2) C00A 0.041(3) 0.056(3) 0.052(4) 0.025(3) 0.010(3) 0.011(3) C00B 0.038(3) 0.055(3) 0.040(3) 0.021(3) 0.006(2) 0.014(3) C00C 0.042(3) 0.044(3) 0.032(3) 0.015(2) 0.004(2) 0.008(2) C00D 0.046(3) 0.048(3) 0.034(3) 0.017(2) 0.008(2) 0.011(3) C00E 0.041(3) 0.050(3) 0.040(3) 0.022(3) 0.002(2) 0.007(2) C00F 0.039(3) 0.048(3) 0.040(3) 0.017(2) 0.009(2) 0.011(2) C00G 0.035(3) 0.055(3) 0.037(3) 0.017(3) 0.004(2) 0.009(2) C00H 0.039(3) 0.050(3) 0.040(3) 0.016(2) 0.008(2) 0.012(2) N00I 0.062(4) 0.089(4) 0.049(3) 0.027(3) 0.008(3) 0.020(3) C00J 0.038(3) 0.053(3) 0.040(3) 0.018(3) 0.010(2) 0.014(2) C00K 0.043(3) 0.047(3) 0.045(3) 0.017(3) 0.004(3) 0.010(3) C00L 0.037(3) 0.047(3) 0.035(3) 0.017(2) 0.010(2) 0.014(2) C00M 0.037(3) 0.054(3) 0.038(3) 0.023(3) 0.004(2) 0.006(2) N00N 0.053(3) 0.089(4) 0.047(3) 0.023(3) 0.006(2) 0.022(3) C00O 0.053(4) 0.048(3) 0.031(3) 0.014(2) 0.013(2) 0.014(3) C00P 0.049(3) 0.048(3) 0.035(3) 0.016(2) 0.011(2) 0.013(3) C00Q 0.048(3) 0.058(3) 0.037(3) 0.024(3) 0.007(3) 0.009(3) C00R 0.040(3) 0.047(3) 0.042(3) 0.017(3) 0.004(2) 0.013(2) C00S 0.038(3) 0.047(3) 0.035(3) 0.016(2) 0.005(2) 0.010(2) C00T 0.041(3) 0.044(3) 0.039(3) 0.015(2) 0.005(2) 0.012(2) C00U 0.048(3) 0.048(3) 0.026(3) 0.015(2) 0.001(2) 0.006(2) C00V 0.044(3) 0.050(3) 0.034(3) 0.011(2) 0.006(2) 0.013(3) C00W 0.045(3) 0.054(3) 0.043(3) 0.021(3) 0.006(3) 0.001(3) C00X 0.048(3) 0.045(3) 0.034(3) 0.016(2) 0.004(2) 0.008(2) C00Y 0.047(3) 0.050(3) 0.039(3) 0.021(3) 0.001(2) 0.003(3) C00Z 0.034(3) 0.062(4) 0.048(3) 0.017(3) 0.007(2) 0.011(3) C010 0.058(4) 0.044(3) 0.034(3) 0.011(2) 0.006(3) 0.008(3) C011 0.045(3) 0.049(3) 0.049(3) 0.020(3) 0.014(3) 0.015(3) C012 0.045(3) 0.063(4) 0.051(4) 0.019(3) 0.019(3) 0.017(3) C013 0.053(4) 0.060(4) 0.044(3) 0.020(3) 0.017(3) 0.020(3) C014 0.050(4) 0.053(3) 0.049(3) 0.023(3) 0.013(3) 0.010(3) C015 0.044(4) 0.074(4) 0.037(3) 0.015(3) 0.011(3) 0.015(3) C016 0.052(4) 0.071(4) 0.048(3) 0.022(3) 0.022(3) 0.020(3) C017 0.066(4) 0.055(4) 0.051(4) 0.015(3) 0.019(3) 0.014(3) C018 0.054(4) 0.055(3) 0.043(3) 0.012(3) 0.008(3) 0.014(3) C019 0.055(4) 0.057(3) 0.035(3) 0.014(3) 0.006(3) 0.009(3) C01A 0.076(5) 0.069(4) 0.045(3) 0.020(3) 0.026(3) 0.026(4) C01B 0.055(4) 0.058(4) 0.047(3) 0.018(3) 0.017(3) 0.012(3) C01C 0.041(3) 0.061(4) 0.067(4) 0.019(3) 0.016(3) 0.017(3) C01D 0.074(4) 0.049(3) 0.039(3) 0.015(3) 0.013(3) 0.009(3) C01E 0.101(6) 0.088(5) 0.046(4) 0.027(4) 0.025(4) 0.032(4) C01F 0.049(4) 0.061(4) 0.065(4) 0.028(3) 0.019(3) 0.010(3) C01G 0.105(6) 0.061(4) 0.042(4) 0.009(3) 0.026(4) 0.011(4) C01H 0.052(4) 0.079(5) 0.078(5) 0.013(4) 0.016(3) 0.001(4) C01I 0.091(5) 0.064(4) 0.059(4) 0.013(3) 0.012(4) 0.014(4) C01J 0.092(6) 0.130(7) 0.058(5) 0.009(5) 0.036(4) 0.031(5) C01K 0.053(5) 0.100(6) 0.107(7) -0.003(5) 0.034(4) 0.015(4) C01L 0.052(5) 0.162(9) 0.184(10) 0.127(9) 0.026(5) 0.042(5) C01M 0.160(9) 0.066(5) 0.064(5) 0.003(4) 0.018(5) -0.015(5) C01N 0.069(6) 0.49(3) 0.158(10) 0.222(15) 0.055(7) 0.132(11) C01O 0.249(14) 0.124(8) 0.052(5) 0.038(5) 0.047(7) 0.059(9) C01P 0.076(7) 0.156(11) 0.40(2) 0.173(14) 0.093(11) 0.031(7) C01Q 0.079(6) 0.140(9) 0.139(9) 0.023(7) 0.013(6) 0.058(6) C01R 0.121(9) 0.269(17) 0.073(6) -0.048(8) 0.048(6) 0.019(10) C2 0.224(19) 0.129(12) 0.179(16) 0.077(11) 0.074(15) -0.020(12) C3 0.172(15) 0.168(15) 0.195(17) 0.092(13) 0.061(13) -0.017(12) C4 0.23(2) 0.166(15) 0.197(19) 0.079(14) 0.075(16) -0.048(14) C5 0.26(2) 0.222(19) 0.24(2) 0.158(17) 0.136(19) 0.084(17) C6 0.24(2) 0.201(17) 0.146(13) 0.002(12) 0.077(14) -0.027(15) C7 0.30(3) 0.199(19) 0.188(19) 0.041(15) 0.13(2) 0.034(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N00N S001 N00I 101.3(3) . . ? C005 N002 C00G 126.5(4) . . ? C005 N002 C00J 107.9(4) . . ? C00J N002 C00G 125.5(4) . . ? C00D N003 C009 126.0(4) . . ? C00P N003 C009 126.3(5) . . ? C00P N003 C00D 107.7(4) . . ? C00A C004 H004 118.5 . . ? C00E C004 H004 118.5 . . ? C00E C004 C00A 123.0(5) . . ? N002 C005 C00S 109.3(4) . . ? N002 C005 C00Z 130.4(5) . . ? C00S C005 C00Z 120.2(5) . . ? C007 C006 C00M 122.8(5) . . ? C00A C006 C007 115.1(5) . . ? C00A C006 C00M 122.1(5) . . ? C008 C007 C006 121.5(5) . . ? N00N C007 C006 125.6(5) . . ? N00N C007 C008 112.9(5) . . ? C00E C008 C007 122.2(5) . . ? N00I C008 C007 112.6(5) . . ? N00I C008 C00E 125.2(5) . . ? C00O C009 N003 120.9(5) . . ? C00O C009 C00W 119.2(5) . . ? C00W C009 N003 119.9(5) . . ? C004 C00A H00A 118.4 . . ? C006 C00A C004 123.1(5) . . ? C006 C00A H00A 118.4 . . ? C00G C00B H00B 120.1 . . ? C00H C00B H00B 120.1 . . ? C00H C00B C00G 119.9(5) . . ? C00F C00C C00E 121.1(5) . . ? C00F C00C C00Q 117.3(5) . . ? C00Q C00C C00E 121.6(5) . . ? N003 C00D C00U 109.1(4) . . ? C019 C00D N003 130.3(5) . . ? C019 C00D C00U 120.5(5) . . ? C004 C00E C008 115.1(5) . . ? C004 C00E C00C 122.2(5) . . ? C008 C00E C00C 122.7(5) . . ? C00C C00F H00F 119.3 . . ? C00O C00F C00C 121.4(5) . . ? C00O C00F H00F 119.3 . . ? C00B C00G N002 120.4(5) . . ? C00K C00G N002 120.4(5) . . ? C00K C00G C00B 119.2(5) . . ? C00B C00H H00H 119.0 . . ? C00B C00H C00M 122.1(5) . . ? C00M C00H H00H 119.0 . . ? C008 N00I S001 106.6(4) . . ? N002 C00J C00L 108.5(4) . . ? C015 C00J N002 131.2(5) . . ? C015 C00J C00L 120.2(5) . . ? C00G C00K H00K 119.5 . . ? C00R C00K C00G 121.0(5) . . ? C00R C00K H00K 119.5 . . ? C00J C00L C00S 107.4(4) . . ? C00T C00L C00J 120.2(5) . . ? C00T C00L C00S 132.4(5) . . ? C00H C00M C006 121.0(5) . . ? C00H C00M C00R 117.0(5) . . ? C00R C00M C006 122.0(5) . . ? C007 N00N S001 106.5(4) . . ? C009 C00O H00O 119.8 . . ? C00F C00O C009 120.4(5) . . ? C00F C00O H00O 119.8 . . ? N003 C00P C00X 109.0(5) . . ? C018 C00P N003 129.9(5) . . ? C018 C00P C00X 121.1(5) . . ? C00C C00Q H00Q 119.3 . . ? C00W C00Q C00C 121.5(5) . . ? C00W C00Q H00Q 119.3 . . ? C00K C00R C00M 120.8(5) . . ? C00K C00R H00R 119.6 . . ? C00M C00R H00R 119.6 . . ? C005 C00S C00L 107.0(4) . . ? C00V C00S C005 120.3(5) . . ? C00V C00S C00L 132.7(5) . . ? C00L C00T H00T 119.9 . . ? C011 C00T C00L 120.1(5) . . ? C011 C00T H00T 119.9 . . ? C00D C00U C00X 106.6(5) . . ? C00Y C00U C00D 119.5(5) . . ? C00Y C00U C00X 133.9(5) . . ? C00S C00V H00V 119.8 . . ? C013 C00V C00S 120.4(5) . . ? C013 C00V H00V 119.8 . . ? C009 C00W H00W 119.9 . . ? C00Q C00W C009 120.1(5) . . ? C00Q C00W H00W 119.9 . . ? C00P C00X C00U 107.6(4) . . ? C010 C00X C00P 119.3(5) . . ? C010 C00X C00U 133.1(5) . . ? C00U C00Y H00Y 119.4 . . ? C014 C00Y C00U 121.1(5) . . ? C014 C00Y H00Y 119.4 . . ? C005 C00Z H00Z 121.1 . . ? C012 C00Z C005 117.8(5) . . ? C012 C00Z H00Z 121.1 . . ? C00X C010 H010 119.6 . . ? C01D C010 C00X 120.9(5) . . ? C01D C010 H010 119.6 . . ? C00T C011 C016 117.6(5) . . ? C00T C011 C01C 119.0(5) . . ? C016 C011 C01C 123.4(5) . . ? C00Z C012 H012 118.2 . . ? C00Z C012 C013 123.5(5) . . ? C013 C012 H012 118.2 . . ? C00V C013 C012 117.8(5) . . ? C00V C013 C01A 118.8(5) . . ? C012 C013 C01A 123.4(5) . . ? C00Y C014 C01B 116.9(5) . . ? C00Y C014 C01F 120.5(5) . . ? C01B C014 C01F 122.6(5) . . ? C00J C015 H015 121.0 . . ? C016 C015 C00J 118.1(5) . . ? C016 C015 H015 121.0 . . ? C011 C016 H016 118.1 . . ? C015 C016 C011 123.7(5) . . ? C015 C016 H016 118.1 . . ? C018 C017 H017 118.2 . . ? C018 C017 C01D 123.6(6) . . ? C01D C017 H017 118.2 . . ? C00P C018 H018 121.2 . . ? C017 C018 C00P 117.7(6) . . ? C017 C018 H018 121.2 . . ? C00D C019 H019 121.2 . . ? C01B C019 C00D 117.7(5) . . ? C01B C019 H019 121.2 . . ? C013 C01A C01I 108.7(5) . . ? C01E C01A C013 110.6(5) . . ? C01E C01A C01I 108.2(6) . . ? C01J C01A C013 112.3(6) . . ? C01J C01A C01E 109.6(6) . . ? C01J C01A C01I 107.4(6) . . ? C014 C01B H01B 117.8 . . ? C019 C01B C014 124.3(5) . . ? C019 C01B H01B 117.8 . . ? C011 C01C C01H 110.2(5) . . ? C011 C01C C01L 110.0(6) . . ? C01K C01C C011 112.6(5) . . ? C01K C01C C01H 105.8(6) . . ? C01K C01C C01L 110.0(7) . . ? C01L C01C C01H 108.0(6) . . ? C010 C01D C017 117.4(5) . . ? C010 C01D C01G 119.8(6) . . ? C017 C01D C01G 122.7(6) . . ? C01A C01E H01A 109.5 . . ? C01A C01E H01C 109.5 . . ? C01A C01E H01D 109.5 . . ? H01A C01E H01C 109.5 . . ? H01A C01E H01D 109.5 . . ? H01C C01E H01D 109.5 . . ? C014 C01F C01Q 111.2(6) . . ? C01N C01F C014 111.4(6) . . ? C01N C01F C01P 111.0(11) . . ? C01N C01F C01Q 106.2(9) . . ? C01P C01F C014 110.0(6) . . ? C01P C01F C01Q 106.9(9) . . ? C01D C01G C01M 109.2(6) . . ? C01O C01G C01D 110.5(6) . . ? C01O C01G C01M 103.2(8) . . ? C01R C01G C01D 113.4(7) . . ? C01R C01G C01M 107.0(9) . . ? C01R C01G C01O 112.9(9) . . ? C01C C01H H01E 109.5 . . ? C01C C01H H01F 109.5 . . ? C01C C01H H01G 109.5 . . ? H01E C01H H01F 109.5 . . ? H01E C01H H01G 109.5 . . ? H01F C01H H01G 109.5 . . ? C01A C01I H01H 109.5 . . ? C01A C01I H01I 109.5 . . ? C01A C01I H01J 109.5 . . ? H01H C01I H01I 109.5 . . ? H01H C01I H01J 109.5 . . ? H01I C01I H01J 109.5 . . ? C01A C01J H01K 109.5 . . ? C01A C01J H01L 109.5 . . ? C01A C01J H01M 109.5 . . ? H01K C01J H01L 109.5 . . ? H01K C01J H01M 109.5 . . ? H01L C01J H01M 109.5 . . ? C01C C01K H01N 109.5 . . ? C01C C01K H01O 109.5 . . ? C01C C01K H01P 109.5 . . ? H01N C01K H01O 109.5 . . ? H01N C01K H01P 109.5 . . ? H01O C01K H01P 109.5 . . ? C01C C01L H01Q 109.5 . . ? C01C C01L H01R 109.5 . . ? C01C C01L H01S 109.5 . . ? H01Q C01L H01R 109.5 . . ? H01Q C01L H01S 109.5 . . ? H01R C01L H01S 109.5 . . ? C01G C01M H01T 109.5 . . ? C01G C01M H01U 109.5 . . ? C01G C01M H01V 109.5 . . ? H01T C01M H01U 109.5 . . ? H01T C01M H01V 109.5 . . ? H01U C01M H01V 109.5 . . ? C01F C01N H01W 109.5 . . ? C01F C01N H01X 109.5 . . ? C01F C01N H01Y 109.5 . . ? H01W C01N H01X 109.5 . . ? H01W C01N H01Y 109.5 . . ? H01X C01N H01Y 109.5 . . ? C01G C01O H01Z 109.5 . . ? C01G C01O H 109.5 . . ? C01G C01O HA 109.5 . . ? H01Z C01O H 109.5 . . ? H01Z C01O HA 109.5 . . ? H C01O HA 109.5 . . ? C01F C01P H01 109.5 . . ? C01F C01P HB 109.5 . . ? C01F C01P HC 109.5 . . ? H01 C01P HB 109.5 . . ? H01 C01P HC 109.5 . . ? HB C01P HC 109.5 . . ? C01F C01Q H0AA 109.5 . . ? C01F C01Q HD 109.5 . . ? C01F C01Q HE 109.5 . . ? H0AA C01Q HD 109.5 . . ? H0AA C01Q HE 109.5 . . ? HD C01Q HE 109.5 . . ? C01G C01R H1AA 109.5 . . ? C01G C01R HF 109.5 . . ? C01G C01R HG 109.5 . . ? H1AA C01R HF 109.5 . . ? H1AA C01R HG 109.5 . . ? HF C01R HG 109.5 . . ? H2A C2 H2B 105.2 . . ? C3 C2 H2A 103.2 . . ? C3 C2 H2B 103.2 . . ? C4 C2 H2A 103.2 . . ? C4 C2 H2B 103.2 . . ? C4 C2 C3 136(2) . . ? C2 C3 H3A 104.5 . . ? C2 C3 H3B 104.5 . . ? H3A C3 H3B 105.6 . . ? C7 C3 C2 131(2) . . ? C7 C3 H3A 104.5 . . ? C7 C3 H3B 104.5 . . ? C2 C4 H4A 104.8 . . ? C2 C4 H4B 104.8 . . ? H4A C4 H4B 105.8 . . ? C5 C4 C2 130(2) . . ? C5 C4 H4A 104.8 . . ? C5 C4 H4B 104.8 . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C7 C6 H6A 109.5 . . ? C7 C6 H6B 109.5 . . ? C7 C6 H6C 109.5 . . ? C3 C7 C6 129(2) . . ? C3 C7 H7A 105.2 . . ? C3 C7 H7B 105.2 . . ? C6 C7 H7A 105.2 . . ? C6 C7 H7B 105.2 . . ? H7A C7 H7B 105.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S001 N00I 1.615(5) . ? S001 N00N 1.604(5) . ? N002 C005 1.396(7) . ? N002 C00G 1.424(6) . ? N002 C00J 1.400(7) . ? N003 C009 1.414(6) . ? N003 C00D 1.403(7) . ? N003 C00P 1.398(7) . ? C004 H004 0.9400 . ? C004 C00A 1.425(7) . ? C004 C00E 1.371(8) . ? C005 C00S 1.400(7) . ? C005 C00Z 1.402(8) . ? C006 C007 1.425(8) . ? C006 C00A 1.369(8) . ? C006 C00M 1.470(7) . ? C007 C008 1.421(7) . ? C007 N00N 1.382(7) . ? C008 C00E 1.416(8) . ? C008 N00I 1.376(8) . ? C009 C00O 1.381(8) . ? C009 C00W 1.389(8) . ? C00A H00A 0.9400 . ? C00B H00B 0.9400 . ? C00B C00G 1.388(7) . ? C00B C00H 1.381(7) . ? C00C C00E 1.475(7) . ? C00C C00F 1.390(7) . ? C00C C00Q 1.400(8) . ? C00D C00U 1.409(7) . ? C00D C019 1.388(8) . ? C00F H00F 0.9400 . ? C00F C00O 1.380(7) . ? C00G C00K 1.383(7) . ? C00H H00H 0.9400 . ? C00H C00M 1.395(7) . ? C00J C00L 1.408(7) . ? C00J C015 1.389(8) . ? C00K H00K 0.9400 . ? C00K C00R 1.378(7) . ? C00L C00S 1.430(7) . ? C00L C00T 1.401(7) . ? C00M C00R 1.411(7) . ? C00O H00O 0.9400 . ? C00P C00X 1.402(7) . ? C00P C018 1.390(8) . ? C00Q H00Q 0.9400 . ? C00Q C00W 1.375(7) . ? C00R H00R 0.9400 . ? C00S C00V 1.398(7) . ? C00T H00T 0.9400 . ? C00T C011 1.391(8) . ? C00U C00X 1.435(8) . ? C00U C00Y 1.395(8) . ? C00V H00V 0.9400 . ? C00V C013 1.389(8) . ? C00W H00W 0.9400 . ? C00X C010 1.397(7) . ? C00Y H00Y 0.9400 . ? C00Y C014 1.390(8) . ? C00Z H00Z 0.9400 . ? C00Z C012 1.379(8) . ? C010 H010 0.9400 . ? C010 C01D 1.388(8) . ? C011 C016 1.402(8) . ? C011 C01C 1.519(8) . ? C012 H012 0.9400 . ? C012 C013 1.400(8) . ? C013 C01A 1.529(8) . ? C014 C01B 1.394(8) . ? C014 C01F 1.535(8) . ? C015 H015 0.9400 . ? C015 C016 1.374(8) . ? C016 H016 0.9400 . ? C017 H017 0.9400 . ? C017 C018 1.373(8) . ? C017 C01D 1.404(9) . ? C018 H018 0.9400 . ? C019 H019 0.9400 . ? C019 C01B 1.374(8) . ? C01A C01E 1.521(9) . ? C01A C01I 1.562(10) . ? C01A C01J 1.519(10) . ? C01B H01B 0.9400 . ? C01C C01H 1.557(9) . ? C01C C01K 1.512(10) . ? C01C C01L 1.525(10) . ? C01D C01G 1.525(8) . ? C01E H01A 0.9700 . ? C01E H01C 0.9700 . ? C01E H01D 0.9700 . ? C01F C01N 1.453(11) . ? C01F C01P 1.473(12) . ? C01F C01Q 1.548(11) . ? C01G C01M 1.551(11) . ? C01G C01O 1.515(12) . ? C01G C01R 1.498(13) . ? C01H H01E 0.9700 . ? C01H H01F 0.9700 . ? C01H H01G 0.9700 . ? C01I H01H 0.9700 . ? C01I H01I 0.9700 . ? C01I H01J 0.9700 . ? C01J H01K 0.9700 . ? C01J H01L 0.9700 . ? C01J H01M 0.9700 . ? C01K H01N 0.9700 . ? C01K H01O 0.9700 . ? C01K H01P 0.9700 . ? C01L H01Q 0.9700 . ? C01L H01R 0.9700 . ? C01L H01S 0.9700 . ? C01M H01T 0.9700 . ? C01M H01U 0.9700 . ? C01M H01V 0.9700 . ? C01N H01W 0.9700 . ? C01N H01X 0.9700 . ? C01N H01Y 0.9700 . ? C01O H01Z 0.9700 . ? C01O H 0.9700 . ? C01O HA 0.9700 . ? C01P H01 0.9700 . ? C01P HB 0.9700 . ? C01P HC 0.9700 . ? C01Q H0AA 0.9700 . ? C01Q HD 0.9700 . ? C01Q HE 0.9700 . ? C01R H1AA 0.9700 . ? C01R HF 0.9700 . ? C01R HG 0.9700 . ? C2 H2A 0.9800 . ? C2 H2B 0.9800 . ? C2 C3 1.41(2) . ? C2 C4 1.37(2) . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 C7 1.34(2) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 C5 1.35(2) . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C5 H5C 0.9700 . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 H6C 0.9700 . ? C6 C7 1.41(2) . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -1 0 0 50.79 5.3 -1 0 0 53.09 5.4 -1 0 0 57.39 5.3 1 0 0 52.69 5.3 1 0 0 50.59 5.3 1 0 0 51.09 5.4 1 0 0 41.3 5.2 1 0 0 48.8 5.4 1 0 0 53.59 5.2 -2 0 0 1612.24 163.58 2 0 0 1563.04 163.18 -3 0 0 56.79 5 -3 0 0 45.3 5 -3 0 0 48.1 5.4 -3 0 0 45.2 5 -3 0 0 48.1 5.5 -3 0 0 45.2 5.6 3 0 0 46.9 5.8 3 0 0 40 5.1 3 0 0 45.8 5.4 3 0 0 54.99 5 3 0 0 50.89 5.9 3 0 0 53.19 5.4 3 0 0 51.99 5 -4 0 0 35.5 4.2 -4 0 0 30.6 3.3 -4 0 0 34.7 4.1 4 0 0 37.2 3.9 4 0 0 30.5 3.5 4 0 0 33.1 3.3 4 0 0 35.8 4.6 4 0 0 32.1 3.6 4 0 0 34.1 4.6 4 0 0 26.8 3.9 -5 0 0 268.57 27.1 -5 0 0 258.57 27.3 -5 0 0 273.67 27.3 5 0 0 264.47 27.5 5 0 0 262.27 27.3 5 0 0 239.98 27.1 5 0 0 282.97 27.2 5 0 0 243.78 27.3 5 0 0 287.37 27.6 -6 0 0 44.2 5 -6 0 0 36.2 5.2 -6 0 0 47.5 5 -6 0 0 50.49 4.7 6 0 0 44.7 4.7 6 0 0 44 5.4 6 0 0 45 6.1 6 0 0 45.3 4.9 6 0 0 40.3 5.4 6 0 0 45.2 6 6 0 0 47.9 5 6 0 0 46.7 4.7 -7 0 0 18.5 3.1 -7 0 0 19 2 -7 0 0 22.3 2.8 7 0 0 17.3 3.6 7 0 0 17.9 2 7 0 0 25.2 4.1 7 0 0 15.7 3 7 0 0 18.4 3.2 -8 0 0 1.5 0.3 8 0 0 1.8 0.5 8 0 0 2 3 8 0 0 2.6 2.7 8 0 0 1.7 1.3 -9 0 0 0.2 0.3 9 0 0 1 2.7 9 0 0 0.7 3.3 9 0 0 -0.6 0.7 9 0 0 0 1.4 -10 0 0 27.2 3.1 -10 0 0 31.7 3.1 10 0 0 31.6 3.9 10 0 0 30.6 5.6 10 0 0 30.2 3.9 10 0 0 31.4 5.8 -11 0 0 0.3 0.4 -11 0 0 -0.5 0.8 11 0 0 -0.5 3.4 11 0 0 -0.2 1.2 11 0 0 2.5 4.6 11 0 0 2.9 3.3 -12 0 0 2.6 1.1 12 0 0 7.4 5.7 12 0 0 1.9 1.9 13 0 0 -4.8 9.8 13 -1 0 10.3 7.7 12 -1 0 6.8 4.4 12 -1 0 8.4 5.5 12 -1 0 7 6.8 11 -1 0 52.29 8.8 11 -1 0 51.59 7.9 11 -1 0 55.69 6 -11 1 0 47.2 4.8 -11 1 0 38.5 4.9 10 -1 0 15.5 2.8 10 -1 0 32 5.6 10 -1 0 27.3 5.1 10 -1 0 20 2.9 -10 1 0 18.7 2 9 -1 0 5.6 3.4 9 -1 0 8.3 1.7 9 -1 0 5.4 3.4 9 -1 0 7.1 1 -9 1 0 9.1 1 8 -1 0 1.1 1.4 8 -1 0 2.2 2.8 8 -1 0 0.4 2.5 8 -1 0 0.6 0.4 -8 1 0 1.2 0.3 7 -1 0 20.1 2.6 7 -1 0 20.3 4.1 7 -1 0 21.2 2.2 7 -1 0 20.5 3.7 7 -1 0 21.5 2.5 7 -1 0 20.3 3.2 7 -1 0 18 3.1 -7 1 0 18.9 2.8 -7 1 0 21.7 2.2 6 -1 0 4.9 1.5 6 -1 0 3 1.3 6 -1 0 5.8 1 6 -1 0 4.3 0.7 6 -1 0 3 2.2 6 -1 0 2.9 2 -6 1 0 6 1.1 -6 1 0 5.4 1.3 5 -1 0 28.5 3.3 5 -1 0 35.5 3.4 5 -1 0 33.5 4 5 -1 0 33.5 3.7 5 -1 0 32.8 4.7 5 -1 0 34.8 4.6 5 -1 0 33.5 4 -5 1 0 32.4 3.9 -5 1 0 31.6 3.3 4 -1 0 199.28 21.3 4 -1 0 217.88 21.6 4 -1 0 182.28 21.5 4 -1 0 205.28 21.7 4 -1 0 249.97 21.8 -4 1 0 188.08 21.5 -4 1 0 214.68 21.3 -4 1 0 210.88 21.5 -4 1 0 216.58 21.5 3 -1 0 54.39 5.5 3 -1 0 48.9 5.5 3 -1 0 46.1 5.6 3 -1 0 49.4 5.7 3 -1 0 55.69 5.8 3 -1 0 53.19 6.1 3 -1 0 59.79 6.1 3 -1 0 47 5.5 3 -1 0 54.99 5.5 -3 1 0 55.89 5.7 -3 1 0 53.29 5.8 -3 1 0 54.69 5.5 -3 1 0 63.59 5.6 -3 1 0 57.19 5.5 2 -1 0 612.04 56.69 -2 1 0 469.85 56.29 1 -1 0 23.9 2.3 1 -1 0 19.5 2.2 1 -1 0 19.8 2.2 1 -1 0 25.1 2.3 1 -1 0 23.4 2.3 1 -1 0 25.5 2.3 1 -1 0 18.8 2.3 1 -1 0 21.1 2.2 -1 1 0 17.5 2.2 -1 1 0 22.3 2.2 -1 1 0 20.7 2.2 -1 1 0 25.9 2.3 -1 1 0 23.3 2.2 -1 1 0 17.4 2.2 -1 1 0 25 2.3 0 -1 0 831.02 83.19 0 1 0 786.82 83.19 -1 -1 0 3.2 0.3 -1 -1 0 4.1 0.8 -1 -1 0 2.8 0.3 -1 -1 0 3.3 0.7 -1 -1 0 3.2 0.9 1 1 0 2.9 0.3 1 1 0 2.9 1 1 1 0 3 1 1 1 0 2.5 0.3 1 1 0 2.3 0.7 -2 -1 0 641.64 74.29 2 1 0 787.32 74.69 -3 -1 0 6 1.3 -3 -1 0 5.8 1.9 -3 -1 0 6.7 1.8 -3 -1 0 6.2 0.6 3 1 0 5.6 1.8 3 1 0 6.2 1.5 3 1 0 5.1 2.1 3 1 0 5.5 1 3 1 0 5.9 1.4 -4 -1 0 3.2 1.7 -4 -1 0 3.2 1.2 -4 -1 0 3.2 1.7 -4 -1 0 1.9 1.1 -4 -1 0 2.8 0.4 4 1 0 2.9 1.4 4 1 0 2.4 2 4 1 0 4.6 0.7 4 1 0 4.4 0.5 4 1 0 1.1 1.3 4 1 0 3.1 0.7 -5 -1 0 38.8 5.8 -5 -1 0 53.19 4.8 -5 -1 0 38.2 5.6 -5 -1 0 34.6 5.7 5 1 0 36.6 5.4 5 1 0 40.4 6.1 5 1 0 52.89 5 5 1 0 47.8 4.8 5 1 0 44.8 6.2 5 1 0 53.79 4.8 -6 -1 0 102.39 10.5 -6 -1 0 88.29 10.7 -6 -1 0 104.39 10.4 -6 -1 0 85.99 10.8 6 1 0 103.99 11.1 6 1 0 97.59 10.7 6 1 0 114.09 11.3 6 1 0 94.39 10.7 -7 -1 0 24.5 3.6 -7 -1 0 26.7 2.6 7 1 0 27.6 4.5 7 1 0 23.5 3.9 7 1 0 24.9 3.2 7 1 0 24.1 4.7 -8 -1 0 1.6 0.4 8 1 0 2.6 1.2 8 1 0 0.4 0.9 8 1 0 1.5 3.1 8 1 0 2.3 3 -9 -1 0 4.1 0.7 9 1 0 6.4 1.5 9 1 0 2.9 2.8 9 1 0 4.1 3.6 9 1 0 9.4 1.7 -10 -1 0 16.9 2 -10 -1 0 20.7 2 10 1 0 17.2 5 10 1 0 20.9 6.6 10 1 0 15 3.1 10 1 0 19.1 2.9 -11 -1 0 1.6 0.9 -11 -1 0 0.9 0.6 11 1 0 -1 4.1 11 1 0 1.4 1 11 1 0 4.7 5.9 11 1 0 3 4 -12 -1 0 3.8 2.3 12 1 0 10 5.7 13 1 0 5.9 7.3 -13 2 0 17.5 2.6 12 -2 0 10 2.2 12 -2 0 13.4 5 12 -2 0 5.6 5.2 12 -2 0 10.7 7.7 -12 2 0 4.4 1.4 11 -2 0 101.79 10.7 11 -2 0 94.89 10.7 11 -2 0 117.49 12.5 -11 2 0 91.89 10.1 10 -2 0 15.2 4.3 10 -2 0 11.9 1.4 10 -2 0 12.5 4 -10 2 0 10.9 1.3 9 -2 0 26 4.3 9 -2 0 25.7 4.4 9 -2 0 21.4 2.2 -9 2 0 18.4 2.1 8 -2 0 63.99 7.3 8 -2 0 69.99 8.4 8 -2 0 68.69 6.9 8 -2 0 72.89 8.5 -8 2 0 66.19 6.9 7 -2 0 -0.6 2.3 7 -2 0 0.7 0.5 7 -2 0 0 0.7 7 -2 0 -0.6 1.3 7 -2 0 -0.5 2.1 7 -2 0 0.3 0.4 -7 2 0 0.5 0.3 6 -2 0 199.48 19.7 6 -2 0 185.68 19.3 6 -2 0 177.08 19.4 6 -2 0 171.78 19.3 6 -2 0 200.18 19 6 -2 0 182.98 19.7 5 -2 0 58.39 6.1 5 -2 0 46 6.1 5 -2 0 51.09 6.6 5 -2 0 56.19 5.7 5 -2 0 63.19 5.7 5 -2 0 49.8 6.6 -5 2 0 57.69 5.7 4 -2 0 14.2 2.1 4 -2 0 16.4 1.8 4 -2 0 18.6 1.8 4 -2 0 19.6 1.8 4 -2 0 14.5 2.3 4 -2 0 14.5 3.1 4 -2 0 16.2 3.1 4 -2 0 12.5 2.4 4 -2 0 20 1.8 -4 2 0 13.6 2 -4 2 0 16.2 2.1 -4 2 0 18 1.8 3 -2 0 81.29 9 3 -2 0 91.59 8.9 3 -2 0 79.79 8.7 3 -2 0 94.29 9 3 -2 0 79.89 8.9 3 -2 0 87.99 8.9 -3 2 0 89.09 8.8 -3 2 0 73.59 8.7 -3 2 0 88.99 8.8 -3 2 0 93.29 9 -3 2 0 83.89 8.7 2 -2 0 743.53 74.69 -2 2 0 689.93 74.89 1 -2 0 9.3 1.4 1 -2 0 9.6 1 1 -2 0 9 1 1 -2 0 8 1.4 1 -2 0 6.5 1.4 1 -2 0 11 1.1 1 -2 0 8.6 1.2 1 -2 0 9.1 1 -1 2 0 10.3 1.1 -1 2 0 9 1 -1 2 0 9.1 1.2 -1 2 0 7.9 1.3 -1 2 0 9 1 -1 2 0 9.6 1 -1 2 0 10.9 1 0 -2 0 136.49 14 0 2 0 133.89 14 0 2 0 137.19 14 -1 -2 0 14.8 2.7 -1 -2 0 13.6 2.4 -1 -2 0 15.9 2.3 -1 -2 0 18.1 1.8 -1 -2 0 16.5 1.7 -1 -2 0 14.8 1.7 -1 -2 0 16 2.2 -1 -2 0 16.8 1.7 1 2 0 16.1 2.9 1 2 0 16.5 2.3 1 2 0 14.8 1.7 1 2 0 16.8 1.7 1 2 0 14.8 2.2 1 2 0 19.3 1.7 1 2 0 13.1 2.4 -2 -2 0 369.76 42.1 2 2 0 411.46 42.9 2 2 0 416.56 42.5 -3 -2 0 18.3 2.9 -3 -2 0 15.7 2.6 -3 -2 0 19.1 1.8 -3 -2 0 13.1 2.5 -3 -2 0 15.4 1.6 -3 -2 0 15.4 1.6 3 2 0 12.2 2.7 3 2 0 12.5 2.5 3 2 0 14.9 1.6 3 2 0 14.9 1.8 3 2 0 15.2 1.8 3 2 0 11.1 2.8 -4 -2 0 0.8 0.5 -4 -2 0 0 1.7 -4 -2 0 0.8 1.2 -4 -2 0 1.8 1.9 -4 -2 0 1.9 1.4 -4 -2 0 1.5 0.3 4 2 0 0.5 1.5 4 2 0 1.1 2.3 4 2 0 1.3 0.5 4 2 0 1 1.4 4 2 0 1.7 3.1 4 2 0 1.9 0.3 -5 -2 0 0.7 0.3 -5 -2 0 0.8 1.1 -5 -2 0 -1.1 2.1 -5 -2 0 -0.2 2.9 5 2 0 0.3 0.7 5 2 0 0.3 0.4 5 2 0 0 2.1 5 2 0 0.1 2.3 5 2 0 0.2 0.7 5 2 0 0.7 1.6 -6 -2 0 17.4 1.6 -6 -2 0 14 2.7 -6 -2 0 12.7 2.3 6 2 0 9.1 2.3 6 2 0 14 3.3 6 2 0 17.2 3.4 6 2 0 12.6 2.1 6 2 0 13.1 1.9 6 2 0 11.8 2.5 -7 -2 0 0.5 0.3 -7 -2 0 0.9 0.3 -7 -2 0 0.8 1.1 7 2 0 0.7 1.1 7 2 0 0.3 2.1 7 2 0 0.6 0.8 7 2 0 -0.3 2.7 -8 -2 0 1.4 0.3 -8 -2 0 1.6 0.3 8 2 0 0.3 2.3 8 2 0 0.2 2.8 8 2 0 1.1 1.3 8 2 0 0.9 1 -9 -2 0 45.1 4.2 -9 -2 0 38 4.2 9 2 0 45.4 7.5 9 2 0 39.2 4.7 9 2 0 39.9 7.6 -10 -2 0 0.9 0.4 -10 -2 0 0 0.4 10 2 0 0.4 1.7 10 2 0 0.9 5.8 10 2 0 -2.3 5.8 10 2 0 4.8 1.7 -11 -2 0 -0.6 0.7 -11 -2 0 0.9 0.6 11 2 0 1.6 4.1 11 2 0 2.3 5.3 11 2 0 3.7 5.3 11 2 0 1.6 1.2 12 2 0 8.1 6.4 13 2 0 7.3 8.1 13 -3 0 19.4 7 -13 3 0 27.8 3.3 12 -3 0 6.2 4.3 12 -3 0 2.6 1.1 12 -3 0 5.2 5.5 11 -3 0 1.7 1.2 11 -3 0 1.8 3.8 11 -3 0 1.7 0.9 11 -3 0 2.6 2.1 11 -3 0 -0.2 4 -11 3 0 1.9 0.5 10 -3 0 9.8 2 10 -3 0 11.1 3.9 10 -3 0 8.7 3.9 10 -3 0 8 1.1 -10 3 0 8.1 1 9 -3 0 28.7 5.1 9 -3 0 22.6 2.4 9 -3 0 27.9 5.2 9 -3 0 20.5 3 -9 3 0 22.9 2.4 8 -3 0 4.1 2.5 8 -3 0 4.3 2.7 8 -3 0 2.7 1.5 8 -3 0 4 0.6 8 -3 0 1.9 1.6 -8 3 0 3.1 0.5 7 -3 0 2.8 1.3 7 -3 0 4.8 1.4 7 -3 0 4.7 0.7 7 -3 0 5.8 1.2 7 -3 0 2.9 2.3 7 -3 0 5.4 2.4 -7 3 0 4.8 0.6 6 -3 0 93.09 10.1 6 -3 0 96.59 10.1 6 -3 0 105.29 10.6 6 -3 0 92.89 10.5 6 -3 0 101.69 10 6 -3 0 91.09 9.7 6 -3 0 97.79 9.7 -6 3 0 99.59 9.7 -6 3 0 81.19 10 5 -3 0 165.28 16.2 5 -3 0 158.48 16 5 -3 0 152.48 15.9 5 -3 0 147.89 15.9 5 -3 0 154.68 15.7 5 -3 0 172.38 16.2 -5 3 0 129.29 15.9 4 -3 0 167.48 17.8 4 -3 0 174.98 17.8 4 -3 0 182.08 17.9 4 -3 0 170.48 17.8 4 -3 0 174.88 17.6 -4 3 0 165.78 17.8 3 -3 0 14.3 2.1 3 -3 0 12.9 2.2 3 -3 0 10.9 1.6 3 -3 0 15.5 1.9 3 -3 0 16.1 1.4 3 -3 0 12.7 1.4 3 -3 0 15.4 1.4 3 -3 0 13.2 1.4 3 -3 0 13.8 1.8 3 -3 0 11.6 1.4 -3 3 0 13 1.4 -3 3 0 11.3 1.6 -3 3 0 12.4 1.4 2 -3 0 41.1 4.4 2 -3 0 36.2 4.1 2 -3 0 41.4 4.1 2 -3 0 39.5 4.4 2 -3 0 40.5 4.4 2 -3 0 41.8 4.3 -2 3 0 36.4 4.2 -2 3 0 40.8 4.1 -2 3 0 37.9 4.2 -2 3 0 42.1 4.1 -2 3 0 40.2 4.1 -2 3 0 40.8 4.1 -2 3 0 39.7 4.3 1 -3 0 9.7 1.8 1 -3 0 12.3 2 1 -3 0 11.1 2 1 -3 0 12.7 1.3 1 -3 0 11.7 1.9 1 -3 0 11.4 1.5 1 -3 0 14.5 1.3 1 -3 0 13.7 1.3 -1 3 0 10.3 1.8 -1 3 0 9.6 1.7 -1 3 0 12.6 1.5 -1 3 0 10.7 1.7 -1 3 0 12.1 1.3 -1 3 0 11.2 1.3 0 -3 0 814.82 88.59 0 3 0 887.11 89.09 -1 -3 0 4.8 1.6 -1 -3 0 4 1 -1 -3 0 6.2 0.7 -1 -3 0 7.5 1.5 -1 -3 0 7.1 2 -1 -3 0 5.4 0.6 -1 -3 0 6.9 0.6 1 3 0 6.1 0.8 1 3 0 4 1.3 1 3 0 3.7 1.4 1 3 0 6.4 0.9 1 3 0 5.2 1.9 1 3 0 4.7 1.2 -2 -3 0 1.6 0.6 -2 -3 0 0.9 1.3 -2 -3 0 1.1 1.8 -2 -3 0 2.2 1.9 -2 -3 0 0.9 0.2 2 3 0 1 1.8 2 3 0 0.9 1.8 2 3 0 0 0.5 2 3 0 1.7 0.5 2 3 0 0.6 1.1 2 3 0 -0.4 1.3 -3 -3 0 20.4 3 -3 -3 0 13 2.7 -3 -3 0 11 1.2 -3 -3 0 11.1 1.2 -3 -3 0 13.6 2.4 -3 -3 0 9.4 1.4 3 3 0 13.9 2.8 3 3 0 12 1.2 3 3 0 15 2.9 3 3 0 13.9 2.6 3 3 0 10.6 1.8 -4 -3 0 80.59 9.5 -4 -3 0 86.59 8.5 -4 -3 0 81.59 8.7 -4 -3 0 90.49 8.9 -4 -3 0 82.39 9.5 4 3 0 80.59 9.4 4 3 0 81.79 8.5 4 3 0 82.89 9.1 4 3 0 80.39 9 4 3 0 76.09 8.5 4 3 0 89.59 9.6 -5 -3 0 0.6 1.9 -5 -3 0 -0.9 2.1 -5 -3 0 1.1 0.3 -5 -3 0 1.2 0.3 -5 -3 0 0.4 1.6 5 3 0 1.4 0.8 5 3 0 1.8 1.8 5 3 0 2.8 2.6 5 3 0 0.8 1.5 5 3 0 1.3 0.3 5 3 0 0.3 2 -6 -3 0 34.1 4 -6 -3 0 32.5 3.3 -6 -3 0 34.9 4.2 -6 -3 0 35.1 3.3 6 3 0 29.4 4.4 6 3 0 32.4 5.3 6 3 0 27 5.1 6 3 0 33 5.5 6 3 0 27.7 3.5 6 3 0 29.4 3.7 -7 -3 0 1.2 0.3 -7 -3 0 2.3 0.3 -7 -3 0 -0.2 1.2 7 3 0 2.9 2.9 7 3 0 0.4 2.9 7 3 0 1 1.1 7 3 0 0.8 0.9 -8 -3 0 1 0.4 -8 -3 0 1.7 0.4 8 3 0 1.8 1.4 8 3 0 0.2 3.1 8 3 0 1.9 3.4 8 3 0 1 1 -9 -3 0 32.7 3.4 -9 -3 0 30.8 3.4 9 3 0 34.2 6.1 9 3 0 33.2 6.1 9 3 0 35.3 4 -10 -3 0 1.4 0.4 -10 -3 0 1.7 0.4 10 3 0 1.9 3.8 10 3 0 0.4 1.1 10 3 0 -1.1 4.4 11 3 0 3.6 6.6 11 3 0 8.9 5.3 11 3 0 5.4 1.6 11 3 0 -0.4 4.8 12 3 0 2.4 7.3 13 3 0 12.1 8.3 13 -4 0 1.9 5.9 12 -4 0 4.1 3.9 12 -4 0 5.2 4.1 12 -4 0 3.4 2.3 11 -4 0 37.3 7.1 11 -4 0 37.1 6.7 11 -4 0 31 4 -11 4 0 30.8 3.3 10 -4 0 14 2.5 10 -4 0 19.2 4.3 10 -4 0 17.6 1.9 10 -4 0 21.4 4.4 -10 4 0 17.1 1.8 9 -4 0 0.6 0.8 9 -4 0 1.1 2.7 9 -4 0 0 2.6 9 -4 0 1.9 0.6 -9 4 0 0.9 0.4 8 -4 0 1.7 1.5 8 -4 0 -0.9 2.3 8 -4 0 0.2 0.9 8 -4 0 0.8 0.4 8 -4 0 1.2 2.3 -8 4 0 0.4 0.3 7 -4 0 5.6 1.4 7 -4 0 3.4 1.4 7 -4 0 5.5 1.1 7 -4 0 5.9 2.3 7 -4 0 4.3 0.7 7 -4 0 5 2.3 -7 4 0 4.6 0.6 6 -4 0 11.4 2.3 6 -4 0 7.2 0.8 6 -4 0 10.7 2.2 6 -4 0 9.5 1.7 6 -4 0 7.8 1.4 6 -4 0 7.7 0.9 6 -4 0 9.9 1.8 -6 4 0 7.2 0.8 -6 4 0 5.7 1.2 5 -4 0 151.28 17.7 5 -4 0 184.68 18.1 5 -4 0 193.38 18.2 5 -4 0 174.88 17.9 5 -4 0 171.08 18 5 -4 0 173.28 17.7 5 -4 0 179.38 17.9 -5 4 0 164.78 18 -5 4 0 173.08 17.7 4 -4 0 40.3 4.5 4 -4 0 42.4 4.4 4 -4 0 41.1 4.8 4 -4 0 45.5 5 4 -4 0 47.7 5 4 -4 0 47 4.7 4 -4 0 40.9 4.5 4 -4 0 45.2 4.5 -4 4 0 41.6 4.5 -4 4 0 45.4 4.7 -4 4 0 43.1 4.4 3 -4 0 16.6 2 3 -4 0 15.2 1.8 3 -4 0 14.6 1.6 3 -4 0 13.1 1.6 3 -4 0 15.5 1.6 3 -4 0 15.7 2.3 3 -4 0 15.9 2.4 3 -4 0 14.6 1.6 3 -4 0 15.2 2.2 -3 4 0 15.8 2 -3 4 0 15.3 1.6 -3 4 0 16.2 1.6 2 -4 0 79.39 8.2 2 -4 0 80.49 8.2 2 -4 0 82.79 8.3 2 -4 0 77.29 8.2 -2 4 0 76.89 8.2 -2 4 0 71.69 8.1 1 -4 0 288.47 28.3 1 -4 0 273.67 28.3 -1 4 0 228.98 28.2 -1 4 0 267.57 28.2 -1 4 0 271.07 28.3 -1 4 0 274.47 28 -1 4 0 268.57 28.2 -1 4 0 325.27 28.2 0 -4 0 80.19 8.3 0 -4 0 86.49 8.7 0 -4 0 90.59 8.4 0 -4 0 72.59 8.7 0 -4 0 74.49 8.8 0 4 0 79.49 8.9 0 4 0 90.69 8.4 0 4 0 77.59 8.6 0 4 0 83.69 8.3 0 4 0 76.29 8.6 0 4 0 66.59 8.6 0 4 0 84.79 8.3 -1 -4 0 1.1 1.8 -1 -4 0 1.8 0.3 -1 -4 0 0.9 1.3 1 4 0 2.2 0.3 1 4 0 1.9 0.5 1 4 0 0.5 1.7 1 4 0 0.4 1 1 4 0 1 0.7 1 4 0 0.6 1.2 -2 -4 0 29.3 3.2 -2 -4 0 26.7 3.4 -2 -4 0 37.1 3.2 -2 -4 0 26.4 4.3 -2 -4 0 27 4.6 2 4 0 34.3 3.2 2 4 0 27.5 4.5 2 4 0 32.2 3.3 2 4 0 30.4 4.7 2 4 0 30.8 4.2 2 4 0 28.2 3.9 -3 -4 0 55.99 6.5 -3 -4 0 53.09 5.4 -3 -4 0 52.09 5.2 -3 -4 0 54.89 5.9 -3 -4 0 47.5 6.4 3 4 0 51.89 5.9 3 4 0 47.9 5.2 3 4 0 55.69 6.2 3 4 0 47.3 5.9 3 4 0 47.5 5.4 -4 -4 0 0.4 0.2 -4 -4 0 0.2 0.3 -4 -4 0 0.1 1.1 -4 -4 0 -0.7 2.1 -4 -4 0 -0.9 2.2 -4 -4 0 0 0.5 4 4 0 -1.5 2.1 4 4 0 -0.5 0.4 4 4 0 -0.1 1.4 4 4 0 -1.1 2.3 4 4 0 -0.5 1.4 4 4 0 0.4 0.7 -5 -4 0 7 1.6 -5 -4 0 5.4 1.2 -5 -4 0 6.8 0.7 -5 -4 0 6.7 1.8 -5 -4 0 6 2.5 -5 -4 0 5.7 0.7 5 4 0 5.9 2.3 5 4 0 5.5 0.7 5 4 0 4.7 1 5 4 0 6 1.2 5 4 0 5.7 2.8 5 4 0 5.4 1.8 5 4 0 3.5 1.7 -6 -4 0 5.6 0.7 -6 -4 0 4.8 0.7 -6 -4 0 6.9 1.8 6 4 0 4.8 1.2 6 4 0 4 2 6 4 0 7.2 3.3 6 4 0 8.1 1.2 -7 -4 0 -0.4 1.4 -7 -4 0 0.5 0.3 -7 -4 0 0.5 0.3 7 4 0 0 0.7 7 4 0 -0.3 2.9 7 4 0 0.1 1.2 7 4 0 -1.8 2.3 -8 -4 0 10.1 1.2 -8 -4 0 10.2 1.2 8 4 0 16.2 4.4 8 4 0 16.5 2.1 8 4 0 12.5 2.3 8 4 0 12.5 3.7 -9 -4 0 0.3 0.4 -9 -4 0 0.4 0.3 9 4 0 -0.7 3.9 9 4 0 -2 3.5 9 4 0 0.6 1.1 9 4 0 -0.5 1.6 -10 -4 0 3.6 0.6 -10 -4 0 2.8 0.6 10 4 0 3.5 1.3 10 4 0 6.9 5.1 10 4 0 5.2 4.2 11 4 0 2.2 1.7 11 4 0 0.7 5.9 12 -5 0 4.9 3.4 12 -5 0 4.8 1.4 11 -5 0 5 3.9 11 -5 0 1.5 1 11 -5 0 0.7 3.5 11 -5 0 3.4 0.9 -11 5 0 3.7 0.5 10 -5 0 2.3 1.1 10 -5 0 1.1 3.4 10 -5 0 2.2 0.7 10 -5 0 3.1 3.2 -10 5 0 2 0.4 9 -5 0 21.3 2.3 9 -5 0 19.2 2.8 9 -5 0 24.5 4.2 9 -5 0 25.2 4.9 -9 5 0 21.4 2.2 8 -5 0 0.8 2.2 8 -5 0 1.9 2.4 8 -5 0 0.8 0.8 8 -5 0 0.4 0.4 -8 5 0 0.4 0.3 7 -5 0 9.6 2.5 7 -5 0 9.1 1.6 7 -5 0 10 1.7 7 -5 0 7.5 1.7 7 -5 0 10.3 1.2 -7 5 0 9.7 1 6 -5 0 1.8 0.3 6 -5 0 3.2 0.6 6 -5 0 1.2 1.1 6 -5 0 0.3 1.7 6 -5 0 3.9 0.5 6 -5 0 0.3 0.9 6 -5 0 1.2 1.7 6 -5 0 1.9 0.7 -6 5 0 2.1 0.4 -6 5 0 1.2 1 -6 5 0 2.8 0.6 5 -5 0 113.79 12 5 -5 0 118.89 12 5 -5 0 107.79 11.6 5 -5 0 112.09 11.9 5 -5 0 115.09 11.6 5 -5 0 109.69 11.8 -5 5 0 117.19 11.6 -5 5 0 114.49 11.6 4 -5 0 3.7 0.6 4 -5 0 4.2 0.5 4 -5 0 3.7 1.4 4 -5 0 4.1 0.6 4 -5 0 4 0.6 4 -5 0 2.5 1.3 4 -5 0 3.4 1.2 4 -5 0 2.4 0.7 -4 5 0 3.8 0.5 -4 5 0 4.3 0.6 -4 5 0 3.6 0.8 3 -5 0 59.39 5.6 3 -5 0 60.79 5.6 3 -5 0 46.1 6 3 -5 0 49.8 6.1 3 -5 0 46 5.9 3 -5 0 47.6 6 3 -5 0 56.49 5.6 3 -5 0 53.09 5.6 -3 5 0 63.39 5.9 -3 5 0 55.89 5.6 2 -5 0 38.1 4.6 2 -5 0 38.3 4.1 2 -5 0 34.2 4.5 2 -5 0 37.5 4.5 2 -5 0 35.6 4.4 -2 5 0 44.3 4 -2 5 0 45.7 3.9 -2 5 0 34.2 4.4 -2 5 0 35.1 4.1 -2 5 0 34.6 4.2 1 -5 0 398.26 40.1 -1 5 0 353.56 39.9 -1 5 0 412.06 40 -1 5 0 436.96 40.1 -1 5 0 349.87 39.9 0 -5 0 4.7 0.6 0 -5 0 4.8 1.4 0 -5 0 4.1 1.4 0 -5 0 3.5 0.5 0 -5 0 4 0.4 0 -5 0 3.4 1.4 0 -5 0 2.8 1.8 0 -5 0 3.3 0.9 0 5 0 3.7 0.5 0 5 0 3 1.2 0 5 0 2.5 1.7 0 5 0 4.2 0.8 0 5 0 2.9 1.2 0 5 0 3.4 1.8 0 5 0 4.6 0.6 -1 -5 0 4.1 1.9 -1 -5 0 3.2 0.4 -1 -5 0 3.2 1.5 -1 -5 0 2.3 1.5 -1 -5 0 2.5 0.3 -1 -5 0 3.7 1.3 -1 -5 0 1.8 0.7 1 5 0 2.4 1.8 1 5 0 3.3 0.4 1 5 0 3.3 1.5 1 5 0 3.1 0.5 1 5 0 2.5 1.3 1 5 0 3.6 0.8 1 5 0 2.6 2.6 -2 -5 0 59.59 6.3 -2 -5 0 73.19 7 -2 -5 0 60.19 7.5 -2 -5 0 64.09 7.2 2 5 0 60.69 6.9 2 5 0 55.19 6.8 2 5 0 57.19 6.4 2 5 0 66.09 7.5 2 5 0 56.49 6.3 2 5 0 62.79 7.1 2 5 0 68.49 6.5 -3 -5 0 3.5 0.4 -3 -5 0 1.6 1.1 -3 -5 0 2.2 0.7 -3 -5 0 3.2 0.5 -3 -5 0 1.9 2.1 -3 -5 0 4.9 2.2 3 5 0 4.1 0.7 3 5 0 4.7 2.6 3 5 0 2.6 1.4 3 5 0 4 1.8 3 5 0 2.7 0.5 3 5 0 3.2 0.7 3 5 0 3.3 1.4 -4 -5 0 2.6 1.3 -4 -5 0 7.7 2 -4 -5 0 7.8 0.8 -4 -5 0 5.5 1.1 -4 -5 0 6.4 0.6 -4 -5 0 7.8 2.7 -4 -5 0 5.2 2.7 4 5 0 5.4 0.9 4 5 0 3.8 1.8 4 5 0 6.3 1.1 4 5 0 8.9 3.2 4 5 0 5.5 0.7 4 5 0 3.1 1.6 4 5 0 3.7 2.5 -5 -5 0 4.2 1.4 -5 -5 0 5.7 0.6 -5 -5 0 3.9 0.6 -5 -5 0 4.3 1.8 -5 -5 0 5.1 1.2 5 5 0 3.1 0.7 5 5 0 4.7 1.9 5 5 0 3.2 2.7 5 5 0 6.5 2.6 5 5 0 6.6 1 5 5 0 4 2 -6 -5 0 12.8 1.5 -6 -5 0 14.8 1.5 -6 -5 0 15.5 3.1 6 5 0 16.5 4.2 6 5 0 10.2 3.5 6 5 0 15.2 2 -7 -5 0 22.2 2.3 -7 -5 0 21 2.3 7 5 0 25.7 5 7 5 0 26 4.7 7 5 0 21.2 2.8 -8 -5 0 25.4 2.3 -8 -5 0 19.5 2.2 8 5 0 19.6 2.9 8 5 0 24.2 5.2 8 5 0 17.6 4.6 -9 -5 0 7.9 1 -9 -5 0 7.2 0.9 9 5 0 10.3 4.5 9 5 0 13.7 2.8 9 5 0 5.8 8.2 10 5 0 23.3 7.8 10 5 0 15.8 6.3 10 5 0 19.1 4.4 10 5 0 11.9 2.7 11 5 0 74.09 11.5 12 5 0 0.5 7.7 13 -6 0 -2 6.6 12 -6 0 12.3 2.3 12 -6 0 10.2 3.3 11 -6 0 12.8 2.4 11 -6 0 11.8 1.6 11 -6 0 8.4 5 11 -6 0 17.4 4.8 -11 6 0 8.8 1.4 10 -6 0 2.7 5.4 10 -6 0 0.8 1.1 10 -6 0 0.7 0.6 10 -6 0 1.7 3.1 -10 6 0 0.6 0.4 9 -6 0 23.6 4 9 -6 0 21.6 4.3 9 -6 0 16.2 1.8 9 -6 0 16.1 2.5 -9 6 0 15.4 1.8 8 -6 0 16.4 3.2 8 -6 0 18.9 3.2 8 -6 0 11.5 1.9 8 -6 0 11.9 1.4 -8 6 0 10.6 1.3 7 -6 0 26.7 3.9 7 -6 0 30.3 3.3 7 -6 0 36.6 4.8 7 -6 0 33.3 3.7 7 -6 0 30.7 3.9 -7 6 0 31.9 3.2 6 -6 0 66.99 6.4 6 -6 0 55.69 6.3 6 -6 0 52.09 6.6 6 -6 0 63.79 6.8 6 -6 0 63.89 6.8 6 -6 0 64.89 7.1 6 -6 0 65.29 7.2 6 -6 0 65.59 6.4 -6 6 0 63.19 6.4 -6 6 0 61.89 6.3 5 -6 0 18.2 1.9 5 -6 0 19.4 1.9 5 -6 0 18.6 2 5 -6 0 17.5 2.6 5 -6 0 15.5 2.3 5 -6 0 18.3 2.9 5 -6 0 17.3 2 5 -6 0 19.1 2.5 5 -6 0 16.9 2.9 -5 6 0 17.4 2.5 -5 6 0 20.8 2 -5 6 0 16.8 1.9 4 -6 0 53.59 6.1 4 -6 0 61.39 6.6 4 -6 0 61.39 6.7 4 -6 0 61.49 6.5 4 -6 0 59.29 6.1 4 -6 0 66.39 6.1 4 -6 0 55.89 6.5 4 -6 0 56.59 6.1 -4 6 0 62.79 6.1 -4 6 0 63.79 6.1 -4 6 0 53.09 6.4 3 -6 0 24.3 2.5 3 -6 0 26.4 3.4 3 -6 0 25.9 2.5 3 -6 0 25.5 3.1 3 -6 0 27.6 2.5 3 -6 0 23 3.2 3 -6 0 24.8 3.4 3 -6 0 19.5 2.7 -3 6 0 20 2.8 -3 6 0 27.5 2.6 -3 6 0 22.7 2.8 -3 6 0 24 2.5 -3 6 0 24.3 2.8 2 -6 0 23.7 3.2 2 -6 0 24.8 3.4 2 -6 0 28 2.5 2 -6 0 23.9 2.5 2 -6 0 25.8 4.4 2 -6 0 24.4 3.4 2 -6 0 23.2 2.8 2 -6 0 25.4 2.5 -2 6 0 24 2.5 -2 6 0 21.1 2.7 -2 6 0 22.4 2.8 -2 6 0 22 3 -2 6 0 21.8 2.7 -2 6 0 26.2 2.6 -2 6 0 23.9 3.2 1 -6 0 3.8 0.4 1 -6 0 3.2 0.5 1 -6 0 3.4 1.6 1 -6 0 4 1.6 1 -6 0 2.5 1.6 1 -6 0 3.8 0.4 1 -6 0 1.6 1.5 -1 6 0 2.8 1.3 -1 6 0 4.4 0.6 -1 6 0 2.1 1.5 -1 6 0 1.4 1 0 -6 0 14.3 2.7 0 -6 0 12.7 2.5 0 -6 0 12.6 1.3 0 -6 0 10.8 1.3 0 -6 0 14.7 1.4 0 -6 0 10.5 1.6 0 -6 0 9.9 2.4 0 -6 0 14.4 2.3 0 6 0 11.4 2.4 0 6 0 14.7 1.8 0 6 0 13.2 1.4 0 6 0 10.4 2 0 6 0 15 1.4 0 6 0 10.8 2.3 -1 -6 0 1.1 1.8 -1 -6 0 0.9 1.6 -1 -6 0 2.7 2.1 -1 -6 0 1.9 0.2 -1 -6 0 0.8 0.7 -1 -6 0 2 1.7 -1 -6 0 1.5 0.3 -1 -6 0 1.8 0.4 1 6 0 0.7 1.2 1 6 0 1 0.3 1 6 0 0.9 1.8 1 6 0 -0.3 1.4 1 6 0 1.4 0.5 1 6 0 1.2 1.1 1 6 0 0.9 0.5 -2 -6 0 0.9 0.2 -2 -6 0 -0.8 1.9 -2 -6 0 -0.4 1.3 -2 -6 0 0.6 1.7 -2 -6 0 0 1.5 -2 -6 0 0.6 0.5 2 6 0 0.4 0.4 2 6 0 1.5 0.5 2 6 0 0 1.2 2 6 0 0.7 1.4 2 6 0 0.2 1.7 2 6 0 1.9 2.1 -3 -6 0 -1.4 1.5 -3 -6 0 0.3 0.5 -3 -6 0 -0.7 2 -3 -6 0 1.1 1.7 -3 -6 0 1 1.3 -3 -6 0 1.3 0.3 -3 -6 0 0.4 0.2 3 6 0 0.7 1.2 3 6 0 0.7 0.3 3 6 0 0.6 0.5 3 6 0 -0.4 1.4 3 6 0 0.6 1.9 3 6 0 0.5 0.6 3 6 0 1.4 2.6 -4 -6 0 34.3 4.3 -4 -6 0 27.5 3.4 -4 -6 0 32.7 5.3 -4 -6 0 33.8 3.3 -4 -6 0 37.4 4.8 4 6 0 37.5 3.7 4 6 0 28 3.3 4 6 0 40.1 5.8 4 6 0 33.6 5.1 4 6 0 33.2 5.2 -5 -6 0 -0.3 1.4 -5 -6 0 2.5 1.9 -5 -6 0 3 0.5 -5 -6 0 2.4 0.4 5 6 0 1.5 2.6 5 6 0 2.4 0.9 5 6 0 2.2 3.1 -6 -6 0 12.7 1.5 -6 -6 0 14 1.4 -6 -6 0 16.7 3 6 6 0 13.4 2 6 6 0 21.1 4.5 6 6 0 19.1 4.3 -7 -6 0 75.89 8 -7 -6 0 70.89 8 7 6 0 85.79 11 7 6 0 76.19 8.2 7 6 0 84.19 10.4 7 6 0 88.19 8.6 -8 -6 0 14 1.4 -8 -6 0 10.4 1.3 8 6 0 15.9 2.5 8 6 0 12.8 2.4 8 6 0 8.5 5 8 6 0 23.3 5.7 -9 -6 0 6.2 1 9 6 0 3.4 7.9 9 6 0 10.1 2.1 9 6 0 10 5.6 9 6 0 15.8 2.9 10 6 0 19.8 8.3 10 6 0 -0.2 5.1 11 6 0 -0.7 7.4 13 -7 0 3.5 2.1 13 -7 0 1.2 3.9 12 -7 0 3.6 2.1 12 -7 0 3.8 2.6 11 -7 0 3.5 4.6 11 -7 0 1.2 1.1 11 -7 0 1.8 3.6 11 -7 0 0.5 1.1 10 -7 0 0.2 3.1 10 -7 0 0.9 1.1 10 -7 0 -0.5 3.7 10 -7 0 0.3 0.7 -10 7 0 0 0.4 9 -7 0 5.5 1.5 9 -7 0 11.4 3.3 9 -7 0 6.9 3 9 -7 0 6.2 1 -9 7 0 7 0.8 8 -7 0 0.6 0.8 8 -7 0 1 2.2 8 -7 0 0.5 2.1 8 -7 0 0.6 0.5 -8 7 0 0.5 0.3 7 -7 0 30.9 3.9 7 -7 0 28.8 3.2 7 -7 0 34.5 4.9 7 -7 0 34.9 3.3 7 -7 0 29.1 4.6 -7 7 0 29 3.2 6 -7 0 31.8 4.1 6 -7 0 32.2 4.9 6 -7 0 30.8 3.5 6 -7 0 31.1 3.8 6 -7 0 36.3 4.5 6 -7 0 34.1 3.5 6 -7 0 33.2 4.1 -6 7 0 36.8 3.5 -6 7 0 36.1 3.5 5 -7 0 15.7 2.5 5 -7 0 14.4 2.1 5 -7 0 16.5 2.8 5 -7 0 16.8 1.7 5 -7 0 15.4 1.8 5 -7 0 16.6 2.9 5 -7 0 17.6 1.7 5 -7 0 14.4 1.8 5 -7 0 14.5 2.5 -5 7 0 17.7 1.7 -5 7 0 11.9 2.4 -5 7 0 16.6 1.7 4 -7 0 3 0.5 4 -7 0 1.2 1.2 4 -7 0 0.7 1.4 4 -7 0 2.5 1.3 4 -7 0 2.2 1.6 4 -7 0 3.7 0.5 4 -7 0 4.9 0.6 4 -7 0 1.6 0.8 4 -7 0 5.2 0.6 -4 7 0 3.3 0.4 -4 7 0 2.6 1.1 -4 7 0 4.7 0.7 3 -7 0 27 2.5 3 -7 0 24.7 2.4 3 -7 0 25.7 2.5 3 -7 0 19.4 3.3 3 -7 0 20.9 3.5 3 -7 0 19.6 3.1 3 -7 0 16 3.4 -3 7 0 27.9 2.5 -3 7 0 18.9 2.7 -3 7 0 21.5 2.8 -3 7 0 24.6 2.4 -3 7 0 19.2 2.8 2 -7 0 32.3 4.6 2 -7 0 43.5 3.7 2 -7 0 37.2 4.6 2 -7 0 39.5 3.7 2 -7 0 34.8 4 2 -7 0 35.4 4.4 2 -7 0 34.7 4.5 -2 7 0 34.1 4.1 -2 7 0 35.8 3.8 -2 7 0 29.9 4.1 -2 7 0 34.4 4.3 -2 7 0 31.2 4 -2 7 0 38.5 3.7 1 -7 0 0.7 1.5 1 -7 0 4.3 0.4 1 -7 0 6.3 1 1 -7 0 2.9 0.5 1 -7 0 4 0.4 1 -7 0 1.8 1.3 1 -7 0 1.1 1.6 1 -7 0 1.7 1.5 -1 7 0 0.9 1.1 -1 7 0 0.3 1.5 -1 7 0 5.5 0.9 -1 7 0 1.5 1.1 -1 7 0 3.1 0.5 -1 7 0 0.5 1.1 0 -7 0 20.6 2.8 0 -7 0 28.7 3.7 0 -7 0 30.2 3.8 0 -7 0 26.8 2.5 0 -7 0 20.2 3.9 0 7 0 22.6 3.2 0 7 0 26.7 3.8 0 7 0 25.1 2.5 0 7 0 22.2 2.5 0 7 0 21.2 3.2 -1 -7 0 0.1 2.1 -1 -7 0 1.1 2.5 -1 -7 0 0.3 0.5 -1 -7 0 0.2 1.5 -1 -7 0 1.4 0.4 -1 -7 0 1.4 0.2 -1 -7 0 1 1.3 -1 -7 0 1.6 0.3 1 7 0 -0.2 1.2 1 7 0 -0.2 1.7 1 7 0 1.2 1.3 1 7 0 1.3 0.3 1 7 0 1 0.4 1 7 0 0 1.1 -2 -7 0 0.8 1.6 -2 -7 0 -0.1 1.6 -2 -7 0 0.2 2.2 -2 -7 0 2.1 1.9 -2 -7 0 -0.6 0.6 2 7 0 0.1 1.2 2 7 0 -0.7 2.2 2 7 0 0.3 0.5 2 7 0 1.2 1.8 2 7 0 1 0.3 2 7 0 0.6 0.5 -3 -7 0 87.09 8.8 -3 -7 0 98.59 9.8 -3 -7 0 97.89 9.1 -3 -7 0 67.39 12.2 -3 -7 0 82.99 8.8 3 7 0 74.29 8.8 3 7 0 76.99 9.8 3 7 0 85.09 8.9 3 7 0 106.69 10.5 -4 -7 0 60.69 7.5 -4 -7 0 68.09 6.7 -4 -7 0 64.29 7.9 -4 -7 0 63.89 7 4 7 0 65.29 6.8 4 7 0 64.99 7.9 4 7 0 68.29 8.8 -5 -7 0 0.6 0.7 -5 -7 0 -0.1 1.4 -5 -7 0 1 0.2 -5 -7 0 1.8 0.4 -5 -7 0 2.2 2.3 5 7 0 3.3 3.1 5 7 0 2.1 0.9 -6 -7 0 89.89 9.7 -6 -7 0 77.09 8.4 6 7 0 81.49 8.5 6 7 0 81.59 10.8 6 7 0 86.09 11.1 -7 -7 0 1.2 0.4 -7 -7 0 0.6 0.2 7 7 0 3.3 1.3 7 7 0 3.3 4.6 7 7 0 0.5 0.9 7 7 0 -1.3 3.7 -8 -7 0 0.8 0.4 8 7 0 -0.5 2 8 7 0 4.2 7.4 8 7 0 0.2 1.5 9 7 0 -2 5.8 9 7 0 -2.6 3.6 9 7 0 0 1.4 10 7 0 2.2 5.3 13 -8 0 2.7 2.7 13 -8 0 -4.3 3.2 12 -8 0 2 2.9 11 -8 0 0.2 1 11 -8 0 1.8 3.7 11 -8 0 4.1 1.4 10 -8 0 0.6 3 10 -8 0 0.7 0.9 10 -8 0 0.1 3.2 -10 8 0 0.2 0.4 9 -8 0 1.2 2.7 9 -8 0 2.9 2.8 9 -8 0 2.5 0.6 9 -8 0 2.2 1 -9 8 0 1.6 0.5 8 -8 0 -0.5 2.4 8 -8 0 0.9 0.5 8 -8 0 1.5 0.9 8 -8 0 1.1 2.7 -8 8 0 0.6 0.3 7 -8 0 11.9 1.9 7 -8 0 20.5 3.8 7 -8 0 18.6 2.1 7 -8 0 15.7 2.4 7 -8 0 19.4 3 -7 8 0 16.4 1.8 -7 8 0 17.6 1.7 6 -8 0 0.1 1.6 6 -8 0 0.2 1.5 6 -8 0 0.7 0.7 6 -8 0 0.1 1.2 6 -8 0 0.7 0.5 6 -8 0 0.4 0.5 -6 8 0 0.5 0.6 -6 8 0 0.2 0.3 5 -8 0 69.29 8 5 -8 0 68.49 7.3 5 -8 0 78.39 7.6 5 -8 0 77.09 7.4 5 -8 0 69.29 8 5 -8 0 73.59 7.4 5 -8 0 69.29 7.4 -5 8 0 66.09 7.3 4 -8 0 14.8 1.8 4 -8 0 15 1.7 4 -8 0 16.4 2.8 4 -8 0 19.7 2.2 4 -8 0 20.1 3.1 4 -8 0 15.7 1.8 4 -8 0 18.8 2.9 4 -8 0 18.5 2.9 -4 8 0 18.3 1.8 -4 8 0 14.6 1.9 3 -8 0 0.6 0.6 3 -8 0 0.4 1.4 3 -8 0 0.5 0.3 3 -8 0 1.3 0.2 3 -8 0 0.2 1.5 3 -8 0 0.7 1.2 3 -8 0 1.5 0.5 3 -8 0 -0.5 1.4 -3 8 0 1.2 1 -3 8 0 0.7 0.8 2 -8 0 102.79 11.1 2 -8 0 95.89 11.2 2 -8 0 113.29 10.5 2 -8 0 105.19 11.1 2 -8 0 111.29 11.2 2 -8 0 102.59 10.5 2 -8 0 90.79 10.7 -2 8 0 94.79 10.8 -2 8 0 110.59 10.9 -2 8 0 99.69 10.7 -2 8 0 112.19 10.5 -2 8 0 94.99 10.8 -2 8 0 99.99 10.6 1 -8 0 18.4 3.4 1 -8 0 20.5 2 1 -8 0 20.4 2 1 -8 0 21.4 3.4 1 -8 0 16.1 3.1 1 -8 0 19.7 3.4 1 -8 0 19.2 2.1 -1 8 0 14.9 3.5 -1 8 0 21.9 2.2 -1 8 0 17.5 2.8 -1 8 0 18.9 2 -1 8 0 19.9 2.8 -1 8 0 18.1 3.2 0 -8 0 3.4 0.8 0 -8 0 2.3 1.7 0 -8 0 4.1 0.4 0 -8 0 1.8 1.8 0 -8 0 3.7 0.4 0 -8 0 5 2 0 -8 0 3.8 0.6 0 8 0 2.1 1.7 0 8 0 3.4 0.6 0 8 0 5.1 1.5 0 8 0 2.1 0.8 -1 -8 0 24.3 2.6 -1 -8 0 22.7 3 -1 -8 0 25.2 4 -1 -8 0 29.4 2.7 -1 -8 0 28.2 4 -1 -8 0 32.3 4.2 -1 -8 0 27.2 4.7 1 8 0 26 3.7 1 8 0 24.4 2.6 1 8 0 23.1 2.7 1 8 0 28.3 4.2 -2 -8 0 12.7 2.5 -2 -8 0 6 2.9 -2 -8 0 13.8 1.4 -2 -8 0 11.3 1.2 -2 -8 0 16.3 2.9 -2 -8 0 10 3.5 -2 -8 0 12 1.3 2 8 0 13.3 2.6 2 8 0 13.6 1.4 2 8 0 14.7 3.2 2 8 0 10.4 1.3 -3 -8 0 -0.2 0.3 -3 -8 0 0.1 0.5 -3 -8 0 1.2 1.8 -3 -8 0 0.1 0.6 -3 -8 0 1.3 2 -3 -8 0 0 0.1 3 8 0 0.4 0.5 3 8 0 0.5 2.7 3 8 0 0.5 0.5 3 8 0 -0.2 1.6 -4 -8 0 6.7 0.7 -4 -8 0 5.2 2.3 -4 -8 0 5.8 1.2 -4 -8 0 3.4 2.6 -4 -8 0 5.4 0.6 4 8 0 3.6 3.5 4 8 0 5.9 2.7 4 8 0 5.1 1.1 -5 -8 0 2.7 1.2 -5 -8 0 5.1 0.6 -5 -8 0 4.6 0.5 5 8 0 6.4 3.8 5 8 0 6.3 1.1 5 8 0 -0.2 2.7 -6 -8 0 2.2 0.8 -6 -8 0 2.2 2.5 6 8 0 -0.3 3.4 6 8 0 2.4 1.1 6 8 0 1.2 4.2 -7 -8 0 2 0.4 7 8 0 2 4.9 7 8 0 0.9 1.4 7 8 0 0.5 1 8 8 0 2.7 5.6 8 8 0 4.3 2.2 8 8 0 2.1 1.9 9 8 0 17.4 4.8 9 8 0 8.4 3.1 10 8 0 10.4 8 11 -9 0 1.1 1.7 10 -9 0 2.1 3 10 -9 0 -0.2 0.9 10 -9 0 1.8 0.9 9 -9 0 0.4 0.6 9 -9 0 0.3 1 -9 9 0 0.5 0.4 8 -9 0 17.2 1.9 8 -9 0 11.4 2.5 8 -9 0 22.2 3.5 8 -9 0 23.4 4 -8 9 0 16.4 1.7 7 -9 0 8 1.3 7 -9 0 14.8 2.8 7 -9 0 11.1 1.8 7 -9 0 12.9 2.9 7 -9 0 10.6 1.3 -7 9 0 9 1.3 -7 9 0 11 1.1 6 -9 0 6.2 1.5 6 -9 0 8.3 1.1 6 -9 0 8.4 2.2 6 -9 0 11.4 2.3 -6 9 0 7.7 1 -6 9 0 6.8 0.8 5 -9 0 25.4 3.7 5 -9 0 19.5 2.4 5 -9 0 24.1 3.8 5 -9 0 22.9 2.4 5 -9 0 22.8 2.4 -5 9 0 23.6 2.4 -5 9 0 23.3 2.3 4 -9 0 22.9 2 4 -9 0 18.7 3.2 4 -9 0 17.9 2 4 -9 0 17.4 3.4 4 -9 0 18.8 3 4 -9 0 17 2 4 -9 0 17.6 1.9 4 -9 0 16.1 2.3 -4 9 0 19.6 2 3 -9 0 -0.1 0.5 3 -9 0 0.4 1.3 3 -9 0 0.8 2.1 3 -9 0 1.1 0.2 3 -9 0 -0.4 1.7 3 -9 0 0.4 0.3 3 -9 0 1.4 1.8 3 -9 0 0.7 0.4 -3 9 0 1.1 0.7 -3 9 0 1.5 0.4 2 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3.1 3 5 9 0 3.7 4.3 5 9 0 -0.2 0.8 -6 -9 0 16.8 1.7 6 9 0 17.6 5.5 6 9 0 15.9 2.1 7 9 0 9.6 5.7 7 9 0 7.7 1.7 7 9 0 6.7 1.5 8 9 0 4.1 1.7 8 9 0 5 3.1 -9 -9 0 0.3 2.1 9 9 0 2.3 3.8 -10 -9 0 0.1 2.2 12 -10 0 1.6 1.7 12 -10 0 2.8 2.5 11 -10 0 3.2 2.2 10 -10 0 9 1.9 10 -10 0 7.9 1.7 10 -10 0 15.3 4.3 9 -10 0 7.3 1.3 9 -10 0 9.3 3.4 9 -10 0 8.8 1.9 9 -10 0 8.5 3.6 8 -10 0 6 1.1 8 -10 0 8.8 2 8 -10 0 8.5 2.9 -8 10 0 7 0.8 7 -10 0 6 1.1 7 -10 0 5.7 1 7 -10 0 9 2.9 7 -10 0 9.7 2.7 7 -10 0 4 1.2 -7 10 0 7.6 0.8 -7 10 0 6.2 1 6 -10 0 4.7 0.7 6 -10 0 3 2 6 -10 0 4.8 1.2 6 -10 0 4.8 2.2 6 -10 0 4.4 0.7 6 -10 0 2.6 0.6 -6 10 0 3.2 0.8 -6 10 0 3.2 0.5 5 -10 0 10.1 2.5 5 -10 0 10.5 1.1 5 -10 0 9.4 1.7 5 -10 0 8.8 1.1 5 -10 0 11.4 2.5 5 -10 0 8.7 1.1 -5 10 0 8.9 1.2 -5 10 0 8 1 4 -10 0 0.8 0.7 4 -10 0 1.4 0.4 4 -10 0 1.4 0.5 4 -10 0 1 1.7 4 -10 0 2.1 0.5 4 -10 0 2.1 1.9 -4 10 0 2.5 0.7 -4 10 0 1.7 0.3 3 -10 0 3.9 0.7 3 -10 0 4.2 0.5 3 -10 0 3.6 0.4 3 -10 0 3.7 1.9 3 -10 0 2.2 0.7 3 -10 0 4.2 2 -3 10 0 3.5 0.5 -3 10 0 5.5 0.8 2 -10 0 0.2 1.8 2 -10 0 1.1 0.3 2 -10 0 1.3 0.6 2 -10 0 -0.1 1.8 2 -10 0 0.9 0.4 2 -10 0 1.4 0.3 -2 10 0 1.7 0.3 -2 10 0 1.5 0.8 1 -10 0 2.7 1.9 1 -10 0 3.3 0.4 1 -10 0 4.1 1 1 -10 0 2.7 0.6 1 -10 0 3.5 0.5 1 -10 0 3.9 2.4 -1 10 0 4.1 1 -1 10 0 2.4 0.5 -1 10 0 -0.6 2 0 -10 0 1.3 0.3 0 -10 0 1.7 2.2 0 -10 0 2.5 0.9 0 -10 0 2 0.4 0 -10 0 1.4 0.5 0 -10 0 2.5 2.2 0 10 0 0.2 1.6 0 10 0 0.9 0.9 0 10 0 1.9 0.3 -1 -10 0 4.6 0.8 -1 -10 0 3.9 0.5 -1 -10 0 4 2.9 -1 -10 0 4.4 0.5 -1 -10 0 4.9 1.2 -1 -10 0 6.8 2.6 1 10 0 0.1 2.8 -2 -10 0 2.4 0.3 -2 -10 0 0.6 0.7 -2 -10 0 1.5 0.5 -2 -10 0 2.4 2.4 -2 -10 0 2.8 4.2 2 10 0 -1 2.1 2 10 0 2.1 0.5 -3 -10 0 19.5 1.9 -3 -10 0 17 3.7 -3 -10 0 14.8 4.5 -3 -10 0 18 2 3 10 0 15.6 4 3 10 0 18 2 -4 -10 0 3.4 0.5 -4 -10 0 3.3 0.6 -4 -10 0 5.9 3.3 4 10 0 2.6 3.8 4 10 0 3.5 0.7 -5 -10 0 -0.1 0.3 -5 -10 0 -0.2 0.5 -5 -10 0 -1.4 3.3 5 10 0 0.1 0.8 -6 -10 0 12.3 2 6 10 0 17.4 2 -7 -10 0 1.4 1.1 7 10 0 3 2.1 7 10 0 -0.3 1.1 -8 -10 0 6.8 2.2 8 10 0 3 1.7 8 10 0 5 3.9 -9 -10 0 4.6 2.2 9 10 0 0.6 1.4 12 -11 0 1.2 1.3 12 -11 0 0.7 2.7 11 -11 0 2.4 2.3 10 -11 0 2.4 1.7 9 -11 0 0.7 3.4 9 -11 0 3.6 4.1 9 -11 0 1 1.4 9 -11 0 1.6 1.2 8 -11 0 2.3 2.8 8 -11 0 5.8 3.6 8 -11 0 0.4 0.8 7 -11 0 6.5 0.9 7 -11 0 5.1 0.9 7 -11 0 2.4 2.5 -7 11 0 4.2 1 -7 11 0 4 0.7 6 -11 0 3.4 2.3 6 -11 0 5 0.8 6 -11 0 1.6 0.9 6 -11 0 2.6 0.6 6 -11 0 2.6 2.3 6 -11 0 2.6 0.6 -6 11 0 3.7 1.1 -6 11 0 2.8 0.5 5 -11 0 7.4 1 5 -11 0 8.5 1 5 -11 0 5.8 1.6 5 -11 0 7.2 1 5 -11 0 7.8 2.7 -5 11 0 8.3 0.9 4 -11 0 3.4 2 4 -11 0 2.1 0.5 4 -11 0 0.4 2.2 4 -11 0 1.1 0.7 4 -11 0 1.9 0.5 4 -11 0 1.9 0.6 -4 11 0 3.1 0.4 -4 11 0 2.3 0.8 3 -11 0 17 2 3 -11 0 24.3 4 3 -11 0 20.1 3.8 3 -11 0 16.8 2 3 -11 0 21.8 2.4 -3 11 0 16.3 2.1 -3 11 0 19.3 1.9 2 -11 0 0.8 2 2 -11 0 0.5 0.3 2 -11 0 0.6 0.7 2 -11 0 0.5 0.5 2 -11 0 1.5 1.9 2 -11 0 0.4 0.3 -2 11 0 1.5 1.2 1 -11 0 17.1 3.4 1 -11 0 15 3.1 1 -11 0 14.8 1.8 1 -11 0 20.1 2.4 1 -11 0 16.7 1.7 -1 11 0 15.3 1.9 -1 11 0 15.6 1.7 0 -11 0 1.2 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2 3 2.8 9 -5 2 1.5 1.1 -10 5 -2 9.8 1.1 10 -5 2 17.4 3.8 10 -5 2 13.6 3.4 10 -5 2 13.1 2 10 -5 2 9.5 1.3 10 -5 2 6 2.4 -11 5 -2 0.5 0.4 11 -5 2 2.3 3.2 11 -5 2 0.2 2.1 11 -5 2 1.6 1 -12 5 -2 -0.5 0.5 12 -5 2 1.8 4.3 13 -5 2 2.7 5.8 13 4 -2 12.2 9 11 4 -2 1.1 4.8 11 4 -2 0.2 1.2 11 4 -2 3.8 5.8 11 4 -2 0.3 4.1 -11 -4 2 0.2 0.7 10 4 -2 24.9 10.3 10 4 -2 11.7 2.7 10 4 -2 16.2 2.3 10 4 -2 18.5 6.4 -10 -4 2 9.4 1.2 9 4 -2 1.7 1.3 9 4 -2 3.9 1.6 9 4 -2 3.5 4.1 9 4 -2 4.5 3.6 -9 -4 2 3.3 0.5 -9 -4 2 2.8 0.5 8 4 -2 13 4 8 4 -2 12.5 2.4 8 4 -2 14.8 2.2 8 4 -2 18.6 4.5 -8 -4 2 13.2 1.5 -8 -4 2 14.2 1.5 7 4 -2 97.39 10.5 7 4 -2 93.39 9.2 7 4 -2 114.39 11.9 7 4 -2 72.79 8.9 -7 -4 2 92.09 8.8 -7 -4 2 81.59 9.4 -7 -4 2 76.29 8.8 6 4 -2 -0.4 0.9 6 4 -2 -1.3 2.6 6 4 -2 1.4 2.5 6 4 -2 1.6 0.3 6 4 -2 1 1.6 6 4 -2 1 2.2 6 4 -2 0.7 0.8 -6 -4 2 1.5 0.3 -6 -4 2 1 1.3 -6 -4 2 1.6 0.3 5 4 -2 41.7 4.2 5 4 -2 39.6 5.2 5 4 -2 36.4 4.4 5 4 -2 35.2 5.3 5 4 -2 45.3 6.3 -5 -4 2 43.1 4.2 -5 -4 2 42.5 4.9 -5 -4 2 45.7 4.2 -5 -4 2 39.5 6.2 -5 -4 2 39.1 6 -5 -4 2 43 5 4 4 -2 37.1 3.4 4 4 -2 30.6 5.3 4 4 -2 30.6 3.2 4 4 -2 28.7 4.2 4 4 -2 25.9 5.4 4 4 -2 29.7 4.5 -4 -4 2 23.2 4.7 -4 -4 2 30.1 4 -4 -4 2 24.5 4.8 -4 -4 2 30.5 4 -4 -4 2 33.8 3.3 -4 -4 2 28.5 3.1 -4 -4 2 29.4 3.1 3 4 -2 29.4 4.8 3 4 -2 27.8 2.8 3 4 -2 25.9 2.8 3 4 -2 26.3 4.2 3 4 -2 24.2 3.7 3 4 -2 27 3.6 -3 -4 2 25.9 2.8 -3 -4 2 31.2 3.8 -3 -4 2 26.8 2.8 -3 -4 2 29.7 4.8 -3 -4 2 28.4 3.6 -3 -4 2 26.5 2.9 2 4 -2 888.71 95.59 1 4 -2 2.4 1.7 1 4 -2 0.8 0.2 1 4 -2 0.7 1.2 1 4 -2 1.4 1.1 1 4 -2 1.4 0.5 -1 -4 2 2 1.6 -1 -4 2 1.7 1.7 -1 -4 2 1.3 1.1 -1 -4 2 1 1.2 -1 -4 2 2.2 0.3 -1 -4 2 0.4 0.4 0 4 -2 9999 1022 -1 4 -2 1042.2 108.49 -2 4 -2 14.9 1.4 -2 4 -2 15.3 1.5 -2 4 -2 13.6 1.4 2 -4 2 14.1 1.5 2 -4 2 13.4 1.5 2 -4 2 11.8 1.5 -3 4 -2 55.89 6 -3 4 -2 56.49 6.2 -3 4 -2 59.39 6 3 -4 2 55.89 6 3 -4 2 67.29 6 3 -4 2 56.29 6.1 -4 4 -2 38.1 4.6 -4 4 -2 45 4.4 -4 4 -2 38.6 4.3 4 -4 2 41.7 4.5 4 -4 2 45.7 4.7 4 -4 2 40.2 4.4 4 -4 2 45.2 4.4 4 -4 2 46.7 4.6 -5 4 -2 2.1 0.3 -5 4 -2 1.4 0.7 5 -4 2 1.8 1 5 -4 2 1.5 0.7 5 -4 2 1.6 0.4 5 -4 2 0.8 1 5 -4 2 1.4 1.3 5 -4 2 0.9 1.4 -6 4 -2 36.1 3.5 6 -4 2 31.5 3.9 6 -4 2 32.5 3.8 6 -4 2 27.5 4.5 6 -4 2 32.3 4.7 6 -4 2 30.3 3.9 6 -4 2 38.8 3.5 -7 4 -2 46.8 4.2 7 -4 2 41.6 4.3 7 -4 2 36.1 4.8 7 -4 2 36.6 4.7 7 -4 2 40.5 4.6 7 -4 2 42.5 5.5 -8 4 -2 11.1 1.3 8 -4 2 10.7 1.4 8 -4 2 14.6 3 8 -4 2 16.3 3.3 8 -4 2 11.6 1.9 -9 4 -2 6 0.8 9 -4 2 5.7 0.9 9 -4 2 5.3 3.1 9 -4 2 9.2 3.1 -10 4 -2 48.2 4.8 10 -4 2 48.8 7.2 10 -4 2 43.7 4.9 10 -4 2 48.2 5.4 10 -4 2 49 9.5 -11 4 -2 21.5 2.2 11 -4 2 17.5 3.5 11 -4 2 19.9 2.5 11 -4 2 32.2 7.4 -12 4 -2 2.7 0.6 12 -4 2 6.1 3.9 -13 4 -2 1.4 1.8 13 -4 2 8.2 5.4 13 3 -2 1.4 8.5 -12 -3 2 1.8 1.5 11 3 -2 36.6 7 11 3 -2 54.69 8.8 11 3 -2 29.7 4.2 -11 -3 2 31.8 3.4 10 3 -2 5.8 6.3 10 3 -2 2.5 3.8 10 3 -2 2.1 1.7 10 3 -2 3.7 1.2 -10 -3 2 4 0.6 -10 -3 2 3.8 0.6 9 3 -2 9.4 2.2 9 3 -2 11.7 5 9 3 -2 9.3 3.6 -9 -3 2 8.6 1 -9 -3 2 9.2 1 8 3 -2 5.1 3 8 3 -2 8.1 3.9 8 3 -2 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7.7 5 6 -3 68.59 6.9 5 6 -3 64.89 6.8 5 6 -3 59.29 8 5 6 -3 70.49 8.2 -5 -6 3 66.49 7.6 -5 -6 3 66.59 6.8 -5 -6 3 65.69 7 -5 -6 3 66.49 7.6 -5 -6 3 63.19 8.6 -5 -6 3 62.69 6.8 4 6 -3 0.1 0.3 4 6 -3 0.3 4.9 4 6 -3 -0.1 0.4 4 6 -3 0.8 1.3 4 6 -3 -0.1 0.5 4 6 -3 1 1.6 4 6 -3 -0.5 1.9 -4 -6 3 0 0.2 -4 -6 3 -1.9 2.1 -4 -6 3 0 0.5 -4 -6 3 -0.3 1.3 -4 -6 3 0.3 0.2 -4 -6 3 -1.5 2.3 -4 -6 3 0 1.4 3 6 -3 16.9 1.9 3 6 -3 15.2 3.2 3 6 -3 15.9 1.9 3 6 -3 20.4 3 3 6 -3 23.1 3.6 3 6 -3 16.9 3.1 -3 -6 3 21.5 1.9 -3 -6 3 17.2 2.1 -3 -6 3 20.3 3.1 -3 -6 3 19.6 1.9 -3 -6 3 16 3.2 -3 -6 3 20.6 3.4 -3 -6 3 16.5 1.9 2 6 -3 102.29 10.4 2 6 -3 94.49 10.7 2 6 -3 102.69 11.1 2 6 -3 98.29 10.7 2 6 -3 108.09 10.8 -2 -6 3 104.39 11.1 -2 -6 3 110.89 10.8 -2 -6 3 103.59 10.7 -2 -6 3 114.99 12 -2 -6 3 80.19 10.3 -2 -6 3 94.89 10.2 1 6 -3 126.49 12.8 1 6 -3 119.29 12.6 1 6 -3 126.49 12.7 1 6 -3 112.59 12.6 -1 -6 3 118.39 12.6 -1 -6 3 120.09 12.7 -1 -6 3 123.09 13 -1 -6 3 117.89 12.8 0 6 -3 8.6 1.7 0 6 -3 12.6 1.2 0 6 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6 -3 0 0.4 9 -6 3 0.2 2.6 9 -6 3 0.5 0.6 9 -6 3 0.8 0.9 9 -6 3 1.7 1.2 9 -6 3 -0.1 2.3 -10 6 -3 112.39 12.9 10 -6 3 134.69 14.1 10 -6 3 138.29 13.3 10 -6 3 123.39 13.1 -11 6 -3 -0.1 0.4 11 -6 3 1.2 1 11 -6 3 0.4 2 11 -6 3 1.5 1.2 11 -6 3 0.1 2.7 12 -6 3 2.4 2 12 -6 3 1.2 2.9 13 -6 3 7.9 4.4 13 5 -3 3.2 7.9 12 5 -3 6.1 7.1 -12 -5 3 1.2 1 11 5 -3 4.7 6.2 11 5 -3 6.2 4.7 -11 -5 3 2 0.8 10 5 -3 4.3 5.8 10 5 -3 -1.7 2 10 5 -3 -4.3 6.2 10 5 -3 0.5 2 -10 -5 3 0 0.4 9 5 -3 0 4.3 9 5 -3 3.3 3.8 9 5 -3 5.5 1.5 9 5 -3 1 1.3 -9 -5 3 2.3 0.4 8 5 -3 14.8 4.1 8 5 -3 16.3 2.5 8 5 -3 12.8 2.1 8 5 -3 11.9 4.5 -8 -5 3 12.4 1.5 -8 -5 3 15.6 1.6 7 5 -3 6.3 1.3 7 5 -3 3.4 0.6 7 5 -3 2.7 3.5 7 5 -3 6.7 1.1 7 5 -3 2 2.8 -7 -5 3 3.8 1.7 -7 -5 3 5.5 0.6 -7 -5 3 3.5 0.6 6 5 -3 5.9 3.3 6 5 -3 5.1 0.7 6 5 -3 8 1.1 6 5 -3 5 3 6 5 -3 9.2 2.6 -6 -5 3 4.5 0.7 -6 -5 3 6.5 1.8 -6 -5 3 6.2 1.5 -6 -5 3 6.4 0.7 5 5 -3 1.1 0.3 5 5 -3 0.7 0.6 5 5 -3 -3.2 2.7 5 5 -3 -0.2 1.4 5 5 -3 -0.5 2.1 5 5 -3 0.2 0.6 -5 -5 3 0.8 2.1 -5 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109.29 11.3 2 -5 3 118.79 11.3 -3 5 -3 3.4 0.7 -3 5 -3 2 0.3 3 -5 3 2.5 0.7 3 -5 3 1.4 0.4 -4 5 -3 18.2 1.9 -4 5 -3 17.9 2.3 -4 5 -3 19.1 2 4 -5 3 20.4 2.1 4 -5 3 20.3 2.2 4 -5 3 18 2.1 -5 5 -3 5.5 0.6 5 -5 3 7.5 1.1 5 -5 3 5 1 5 -5 3 6.3 1.4 5 -5 3 4.6 1 5 -5 3 5.8 1.4 5 -5 3 4.4 0.8 -6 5 -3 28.8 3.1 6 -5 3 30.2 4.1 6 -5 3 32.1 3.5 6 -5 3 36 4 6 -5 3 30.7 3.4 6 -5 3 30.6 3.2 6 -5 3 27 3.4 -7 5 -3 10.8 1.2 7 -5 3 14 2.6 7 -5 3 10.7 1.7 7 -5 3 10.7 2 7 -5 3 12.3 2.3 7 -5 3 11.2 2.4 7 -5 3 11.6 1.3 -8 5 -3 3.3 0.5 8 -5 3 3.4 2.2 8 -5 3 5.2 2.4 8 -5 3 3.1 0.6 8 -5 3 3.8 1 -9 5 -3 1.4 0.4 9 -5 3 3.1 1.4 9 -5 3 2.2 2.6 9 -5 3 3.3 0.7 9 -5 3 2.8 3 9 -5 3 1.5 0.9 -10 5 -3 56.89 5.8 10 -5 3 50.19 5.9 10 -5 3 57.09 7.6 10 -5 3 65.79 6.3 -11 5 -3 2.3 0.5 11 -5 3 3.5 2.4 11 -5 3 3.9 1.2 11 -5 3 3.7 3.2 11 -5 3 6.9 3.4 11 -5 3 0.6 1 -12 5 -3 2.3 0.5 12 -5 3 0.6 4.1 13 -5 3 5.8 5.2 13 4 -3 8.1 8.7 12 4 -3 2.6 6.9 -12 -4 3 1.9 1.2 11 4 -3 18.1 10.2 11 4 -3 17.7 5.4 11 4 -3 23.3 4.7 -11 -4 3 8.5 1.3 10 4 -3 22.6 9.9 10 4 -3 16 2.7 10 4 -3 11.6 5.1 10 4 -3 15.3 2.4 -10 -4 3 11.3 1.4 9 4 -3 7.2 1.7 9 4 -3 11 1.8 9 4 -3 6.9 3.7 -9 -4 3 7.2 0.8 -9 -4 3 4.6 0.7 8 4 -3 19.2 1.9 8 4 -3 21.9 4.9 8 4 -3 34 5.5 8 4 -3 22.3 2.5 8 4 -3 20.2 2.9 -8 -4 3 14.8 1.9 -8 -4 3 17.5 1.9 7 4 -3 4.2 3.2 7 4 -3 4.1 1.2 7 4 -3 3.1 0.5 7 4 -3 4.3 3.6 -7 -4 3 3.1 0.5 -7 -4 3 2.3 1.8 -7 -4 3 2.6 0.4 6 4 -3 11.7 2.2 6 4 -3 16.9 3.8 6 4 -3 12.4 3.5 6 4 -3 15.6 3 6 4 -3 16.4 1.6 6 4 -3 13.5 2.1 6 4 -3 16.3 3.1 -6 -4 3 18.6 1.6 -6 -4 3 18.7 3.4 -6 -4 3 15.4 1.7 -6 -4 3 15.1 2.7 5 4 -3 19.7 3.4 5 4 -3 23.3 4.4 5 4 -3 18.8 3.9 5 4 -3 17.7 3.4 -5 -4 3 24.6 5.1 -5 -4 3 24.7 2.1 -5 -4 3 19.4 3.2 -5 -4 3 18.8 2.2 -5 -4 3 14.3 3.4 -5 -4 3 19.2 3.2 4 4 -3 29.7 4.7 4 4 -3 36 5.9 4 4 -3 28.7 4.6 4 4 -3 42.4 4 4 4 -3 34.5 5.1 -4 -4 3 27.3 5.5 -4 -4 3 34 4.6 -4 -4 3 32 4.7 -4 -4 3 29.6 5.5 -4 -4 3 45 3.8 -4 -4 3 40.9 3.8 3 4 -3 7.4 1.6 3 4 -3 7.1 2.1 3 4 -3 11.1 2.7 3 4 -3 6.5 0.8 3 4 -3 8.4 1.7 -3 -4 3 11.4 2 -3 -4 3 8.3 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4.9 1.8 0 -6 4 6.6 1.1 0 -6 4 6.5 0.9 0 -6 4 5.2 1.5 0 -6 4 4.6 1.4 -1 6 -4 156.78 16.7 -1 6 -4 145.19 16.6 -1 6 -4 180.08 16.6 1 -6 4 157.18 16.9 1 -6 4 165.28 16.8 1 -6 4 162.28 16.8 1 -6 4 168.68 16.7 -2 6 -4 137.29 14.2 2 -6 4 131.79 14.3 2 -6 4 147.79 14.3 2 -6 4 139.79 14.4 2 -6 4 137.39 14.3 -3 6 -4 1.5 0.5 -3 6 -4 0.4 0.5 -3 6 -4 1.1 0.2 3 -6 4 1.7 0.6 3 -6 4 0.4 0.5 3 -6 4 1.9 0.5 4 -6 4 118.69 13.7 4 -6 4 147.19 13.6 -5 6 -4 32.2 3.3 5 -6 4 31.8 3.3 -6 6 -4 33.7 3.2 6 -6 4 29.6 4 6 -6 4 29 3.6 6 -6 4 31.1 3.3 -7 6 -4 0.2 0.3 7 -6 4 0.2 1.5 7 -6 4 0.3 0.6 7 -6 4 0.3 0.7 7 -6 4 0.1 1.1 7 -6 4 0.2 0.9 7 -6 4 0.2 1.7 -8 6 -4 8.7 1 8 -6 4 12.7 1.8 8 -6 4 8.4 2 8 -6 4 8.4 1.2 8 -6 4 10 2.4 -9 6 -4 61.19 6.6 9 -6 4 72.99 6.9 9 -6 4 55.49 6.9 9 -6 4 63.09 6.7 9 -6 4 70.09 7.8 9 -6 4 70.89 7.4 -10 6 -4 0.7 0.4 10 -6 4 0 0.8 10 -6 4 0.2 2.4 10 -6 4 0.4 1.6 10 -6 4 1.6 0.9 -11 6 -4 -0.1 0.4 11 -6 4 -0.1 1.9 11 -6 4 0.6 1.2 11 -6 4 1.1 1.3 -12 6 -4 0.9 0.6 12 -6 4 2.1 4.4 13 5 -4 10.1 8.2 -12 -5 4 -0.1 1.4 11 5 -4 13.6 4 11 5 -4 15 6.5 -11 -5 4 8.7 1.3 10 5 -4 34.8 6.3 10 5 -4 31.7 3.9 10 5 -4 25.9 3.5 10 5 -4 38.7 9.7 -10 -5 4 22.2 2.7 9 5 -4 10.2 2 9 5 -4 5.4 4.7 9 5 -4 14.5 5 -9 -5 4 9.8 1.1 8 5 -4 6.2 4.4 8 5 -4 6.7 1.3 8 5 -4 3.8 0.6 8 5 -4 2.9 4.2 8 5 -4 6.5 1.5 -8 -5 4 1 1.6 7 5 -4 62.09 8.4 7 5 -4 62.59 6.1 7 5 -4 55.79 6.6 7 5 -4 66.69 8.8 -7 -5 4 61.79 6.1 -7 -5 4 62.89 7 -7 -5 4 53.39 6.1 6 5 -4 6.8 2.7 6 5 -4 7.9 3 6 5 -4 4.2 0.6 6 5 -4 6.6 2 6 5 -4 5.1 3.3 -6 -5 4 5.6 1.7 -6 -5 4 3.9 0.6 -6 -5 4 4.6 0.6 -6 -5 4 5.5 1.9 5 5 -4 4.6 2.9 5 5 -4 2.7 1.8 5 5 -4 2.6 1.3 5 5 -4 2.4 2.2 -5 -5 4 2.3 0.3 -5 -5 4 4.3 2.8 -5 -5 4 3.2 1.7 -5 -5 4 -0.4 2.1 -5 -5 4 2.3 1.4 -5 -5 4 2.2 0.3 4 5 -4 1.7 2 4 5 -4 1.1 1.5 4 5 -4 1.6 1.1 4 5 -4 0.3 2.4 4 5 -4 3 0.7 -4 -5 4 1.6 0.6 -4 -5 4 0.2 2.2 -4 -5 4 1.6 1.4 -4 -5 4 1.3 0.3 -4 -5 4 1.5 2.2 -4 -5 4 1.7 0.3 3 5 -4 1.3 0.5 3 5 -4 0.8 2.2 3 5 -4 2.1 0.3 3 5 -4 1.3 2.4 3 5 -4 1.7 1.1 3 5 -4 1.5 1.3 -3 -5 4 2.5 2 -3 -5 4 1.5 2.5 -3 -5 4 1 0.2 -3 -5 4 0.3 0.4 -3 -5 4 2 0.2 -3 -5 4 2.2 1.5 -3 -5 4 1.9 1.3 2 5 -4 8.6 1 2 5 -4 9 2 2 5 -4 8 1.4 2 5 -4 10.2 1.8 2 5 -4 10.4 2.5 2 5 -4 8.1 0.9 -2 -5 4 8.9 1 -2 -5 4 7.3 1.5 -2 -5 4 9.3 2.3 -2 -5 4 10.4 3 -2 -5 4 10.5 1.2 -2 -5 4 9.6 1 -2 -5 4 8.2 2.4 1 5 -4 25.5 3.4 1 5 -4 26.9 3.4 1 5 -4 32.7 4 1 5 -4 26.5 3.2 -1 -5 4 28.2 3.5 -1 -5 4 30.3 3.5 -1 -5 4 26.5 3.9 -1 -5 4 25.4 4.1 -1 5 -4 25 3.2 -1 5 -4 29.3 3.2 -1 5 -4 28.8 3.2 1 -5 4 29.9 3.2 1 -5 4 33.4 3.4 1 -5 4 34 3.2 1 -5 4 35.6 3.6 1 -5 4 36.9 3.5 1 -5 4 34.3 3.8 -2 5 -4 12.3 1.2 -2 5 -4 12.7 1.3 -2 5 -4 12.8 1.5 2 -5 4 13.2 1.4 2 -5 4 10.1 1.4 2 -5 4 12.1 1.3 2 -5 4 10.6 1.5 2 -5 4 12 1.4 2 -5 4 11.6 1.8 -3 5 -4 2.4 0.6 -3 5 -4 3.2 0.5 3 -5 4 4.2 0.6 3 -5 4 4 0.6 -4 5 -4 2.3 0.4 -4 5 -4 3.1 0.4 4 -5 4 2.4 0.5 4 -5 4 4.2 0.6 4 -5 4 2.6 0.6 -5 5 -4 0.7 0.3 5 -5 4 1.7 0.8 5 -5 4 0.9 0.5 5 -5 4 1.4 1 5 -5 4 1.4 1.1 5 -5 4 0.9 0.4 5 -5 4 1.2 0.8 6 -5 4 3 0.7 6 -5 4 4.9 1 6 -5 4 3.7 1.6 6 -5 4 2.2 0.6 6 -5 4 2.6 1.4 6 -5 4 4.5 0.7 6 -5 4 3.5 1 6 -5 4 2.7 1.1 -7 5 -4 0.9 0.3 7 -5 4 0.2 0.6 7 -5 4 -0.3 1.8 7 -5 4 0.8 1.6 7 -5 4 1.6 1.7 7 -5 4 0.3 0.5 7 -5 4 0.6 1 7 -5 4 0.2 1 -8 5 -4 18.2 2 8 -5 4 18.5 2.1 8 -5 4 18.4 3.5 8 -5 4 19 2.5 8 -5 4 28.1 3.2 8 -5 4 19.7 3.7 -9 5 -4 46.9 5 9 -5 4 55.19 5.4 9 -5 4 46.2 5 9 -5 4 41.3 5.3 9 -5 4 51.39 6.3 9 -5 4 57.29 6.5 -10 5 -4 0.4 0.4 10 -5 4 -0.5 0.7 10 -5 4 0.1 0.9 10 -5 4 -1.8 2.4 10 -5 4 2.1 2.6 10 -5 4 0.3 1.4 -11 5 -4 0.1 0.4 11 -5 4 -0.1 2 11 -5 4 -0.3 1.3 11 -5 4 5.9 3 12 -5 4 5.6 4.1 13 4 -4 11.5 8.5 12 4 -4 2.2 5.9 -12 -4 4 2.8 1.5 11 4 -4 11 6.5 11 4 -4 6.3 5.3 11 4 -4 15.7 4.5 10 4 -4 25.3 6.4 10 4 -4 17.9 3.2 10 4 -4 33 6.3 -10 -4 4 20.8 2.2 9 4 -4 3.8 4.6 9 4 -4 3.1 2.8 9 4 -4 6.6 4.3 -9 -4 4 3.9 0.6 8 4 -4 3.1 3.7 8 4 -4 2.2 0.4 8 4 -4 0.7 4.4 8 4 -4 2.1 1.2 -8 -4 4 2.4 0.4 -8 -4 4 2.4 0.4 7 4 -4 62.59 7.9 7 4 -4 63.99 8.3 -7 -4 4 55.59 5.9 -7 -4 4 65.89 7.4 -7 -4 4 53.49 5.9 6 4 -4 12 2.5 6 4 -4 10.1 1.7 6 4 -4 8.1 2.6 6 4 -4 12.3 1.9 6 4 -4 8.2 1.8 6 4 -4 9.8 3.2 -6 -4 4 10.6 1.2 -6 -4 4 12.6 2.5 -6 -4 4 13.6 1.2 -6 -4 4 16.8 3.3 -6 -4 4 7.9 2 5 4 -4 9.7 3.2 5 4 -4 8.8 2.1 5 4 -4 10.2 1.1 5 4 -4 6.4 2.6 -5 -4 4 8.3 2.8 -5 -4 4 12.2 2.2 -5 -4 4 8.5 2 -5 -4 4 10.6 1.1 -5 -4 4 7.4 2.7 4 4 -4 1.4 1.5 4 4 -4 1.1 1.3 4 4 -4 1.8 0.6 4 4 -4 1.2 2.5 4 4 -4 2.9 2.7 -4 -4 4 1.5 1.6 -4 -4 4 0.2 1.9 -4 -4 4 1.4 0.2 -4 -4 4 1.7 1.3 -4 -4 4 2 0.3 -4 -4 4 3.4 2.4 3 4 -4 55.19 6.3 3 4 -4 59.59 6.9 3 4 -4 57.49 5.9 3 4 -4 60.69 7.2 3 4 -4 54.09 6.5 -3 -4 4 49.3 7 -3 -4 4 53.49 5.9 -3 -4 4 56.29 6.5 -3 -4 4 62.19 5.9 -3 -4 4 60.69 5.9 -3 -4 4 57.79 7.1 -3 -4 4 59.49 6.5 2 4 -4 96.19 10.4 2 4 -4 100.49 10.1 2 4 -4 77.99 10.7 2 4 -4 92.79 10.6 2 4 -4 93.09 9.8 -2 -4 4 101.69 10.2 -2 -4 4 100.89 10.6 -2 -4 4 91.79 10.5 -2 -4 4 103.09 10.2 1 4 -4 446.06 42.2 1 4 -4 403.86 42.1 1 4 -4 402.46 42.1 -1 -4 4 406.66 42.4 -1 -4 4 394.66 42.3 -1 4 -4 28.9 2.9 1 -4 4 25.7 3.4 1 -4 4 27.8 3 1 -4 4 25.9 3.3 1 -4 4 28.2 2.9 1 -4 4 27.2 2.9 1 -4 4 31.4 2.9 1 -4 4 23.3 3.1 1 -4 4 27.4 2.9 1 -4 4 30.1 2.9 -2 4 -4 13.8 1.4 -2 4 -4 12.9 1.6 -2 4 -4 12.1 1.4 2 -4 4 15.7 1.8 2 -4 4 11.3 1.5 2 -4 4 16.7 1.7 2 -4 4 14 1.5 2 -4 4 14.7 1.5 -3 4 -4 6.1 0.6 -3 4 -4 5.1 0.6 3 -4 4 4 0.8 3 -4 4 5.9 0.8 3 -4 4 6.7 0.7 3 -4 4 5.4 1 3 -4 4 6 1.1 3 -4 4 6.4 1.2 -4 4 -4 19.7 2.3 -4 4 -4 24.4 2.7 4 -4 4 23.4 2.9 4 -4 4 19.8 2.6 4 -4 4 20.4 2.6 4 -4 4 25.5 2.8 4 -4 4 25.8 2.5 -5 4 -4 9.8 1 5 -4 4 8.3 1.1 5 -4 4 8.8 1.7 5 -4 4 11.4 1.9 5 -4 4 11.7 1.4 5 -4 4 12.5 2.2 5 -4 4 9.1 1.6 5 -4 4 9.2 1.3 -6 4 -4 47.5 4.8 6 -4 4 41.5 5.2 6 -4 4 51.29 5.1 6 -4 4 46.1 5.4 6 -4 4 47 5 6 -4 4 44.3 5.6 6 -4 4 47.3 4.9 6 -4 4 51.29 5.6 -7 4 -4 8.2 0.9 7 -4 4 8.1 1.4 7 -4 4 8.2 1.1 7 -4 4 8.3 1.4 7 -4 4 11.5 2.3 7 -4 4 9.9 2.3 7 -4 4 8.8 1.4 7 -4 4 7.2 1.8 -8 4 -4 94.29 10 8 -4 4 108.89 10.9 8 -4 4 90.29 10 8 -4 4 97.29 10.2 8 -4 4 104.09 10.9 -9 4 -4 12.9 1.3 9 -4 4 13.2 3.3 9 -4 4 16.9 2.2 9 -4 4 10.6 1.4 9 -4 4 14.7 3.1 9 -4 4 8.8 1.9 -10 4 -4 0.2 0.4 10 -4 4 0 0.6 10 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4 0.7 1 -8 10 4.5 1.4 -2 8 -10 2.9 0.4 2 -8 10 3.5 1.4 2 -8 10 2.4 1 2 -8 10 2.6 0.5 2 -8 10 3.6 1.3 2 -8 10 2.5 0.6 2 -8 10 1.3 1.9 -3 8 -10 3.3 0.5 3 -8 10 2.4 0.6 3 -8 10 3.3 1.2 3 -8 10 3.4 1.3 3 -8 10 3.9 1.7 3 -8 10 2.6 0.6 -4 8 -10 2.9 0.5 4 -8 10 3.4 1.2 4 -8 10 4.1 1.3 4 -8 10 3.8 0.8 4 -8 10 5.4 0.7 -5 8 -10 9.2 0.9 5 -8 10 6.6 1.1 5 -8 10 9.5 1.7 5 -8 10 7.4 1.2 -6 8 -10 74.19 7 6 -8 10 63.89 7.1 6 -8 10 66.49 7.1 -7 8 -10 2 0.6 7 -8 10 0.6 0.6 7 -8 10 0.2 0.8 -8 8 -10 0.4 0.9 8 -8 10 0 0.8 8 -8 10 0.3 0.7 -9 8 -10 1.3 1.1 9 -8 10 -0.5 0.9 -10 8 -10 3.1 1.3 10 -8 10 2.1 1.4 -12 -7 10 0.1 0.5 -12 -7 10 1.9 1.2 -11 -7 10 0.4 0.7 -11 -7 10 1 1.5 10 7 -10 1.8 0.5 -10 -7 10 3.4 0.6 -10 -7 10 4.4 0.6 -9 -7 10 1 0.4 -9 -7 10 1.2 0.5 8 7 -10 0.6 5.3 8 7 -10 1.9 0.5 -8 -7 10 1.9 0.5 -8 -7 10 0.9 2.7 -8 -7 10 1.3 0.4 7 7 -10 3.8 0.7 7 7 -10 5.7 6.6 -7 -7 10 6.1 2.8 -7 -7 10 8.9 3.9 -7 -7 10 4.1 0.6 6 7 -10 5.3 0.7 6 7 -10 1.5 3.2 -6 -7 10 2.7 2.5 -6 -7 10 4.9 2.8 -6 -7 10 4.2 0.6 -6 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