#------------------------------------------------------------------------------ #$Date: 2021-03-17 02:48:37 +0200 (Wed, 17 Mar 2021) $ #$Revision: 263068 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/10/1561044.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1561044 loop_ _publ_author_name 'Karmakar, Ananta' 'Nimje, Roshan Y.' 'Silamkoti, Arundutt' 'Pitchai, Manivel' 'Basha, Mushkin' 'Singarayer, Christuraj' 'Ramasamy, Duraisamy' 'Babu, G. T. Venkatesh' 'Samikannu, Ramesh' 'Subramaniam, Srinath' 'Anjanappa, Prakash' 'Vetrichelvan, Muthalagu' 'Kumar, Hemantha' 'Dikundwar, Amol G.' 'Gupta, Anuradha' 'Gupta, Arun Kumar' 'Rampulla, Richard' 'Dhar, T. G. Murali' 'Mathur, Arvind' _publ_section_title ; Practical Synthesis of (3aR, 9bR)-8-Fluoro-7-(perfluoropropan-2-yl)-9b-(phenylsulfonyl)-2,3,3a,4,5,9b-hexahydro-1H-benzo[e]indole: An Advanced Intermediate to Access the ROR\gt Inverse Agonist BMT-362265 ; _journal_name_full 'Organic Process Research & Development' _journal_paper_doi 10.1021/acs.oprd.1c00019 _journal_year 2021 _chemical_absolute_configuration ad _chemical_formula_moiety 'C44 H50 F2 N2 O6 S4' _chemical_formula_sum 'C44 H50 F2 N2 O6 S4' _chemical_formula_weight 869.10 _chemical_name_common compound-31 _chemical_name_systematic ; (3aR,3'aR,9bR,9'bR)-3-((R)-tert-butylsulfinyl)- 3'-(tert-butylsulfinyl)-8,8'-difluoro-9b,9'b-bis(phenylsulfonyl) -2,2',3,3a,3',3'a,4,4',5,5',9b,9'b-dodecahydro-1H,1'H-7,7'-bibenzo[e]indole ; _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _audit_creation_date 2020-11-03 _audit_creation_method ; Olex2 1.3 (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.7957(5) _cell_length_b 14.9403(8) _cell_length_c 30.1708(15) _cell_measurement_reflns_used 9773 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 28.42 _cell_measurement_theta_min 2.44 _cell_volume 4415.5(4) _computing_cell_refinement 'SAINT V8.40A (Bruker, 2019)' _computing_data_reduction 'SAINT V8.40A (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2016/6 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_detector 'Bruker PHOTON II detector' _diffrn_detector_area_resol_mean 7.4 _diffrn_detector_type 'CPAD area detector' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker SMART APEX' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0833 _diffrn_reflns_av_unetI/netI 0.0795 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 40 _diffrn_reflns_limit_l_min -41 _diffrn_reflns_number 58552 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.922 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.415 _diffrn_reflns_theta_min 1.521 _diffrn_source 'fine focus sealed X-ray tube' _diffrn_source_current 35.0 _diffrn_source_power 1.75 _diffrn_source_type 'sealed tube' _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.272 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.6903 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1472 before and 0.0807 after correction. The Ratio of minimum to maximum transmission is 0.9252. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.307 _exptl_crystal_description plate _exptl_crystal_F_000 1832 _exptl_crystal_recrystallization_method 'The material was recrystallised from a mixture of methanol and THF by slow evaporation' _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.283 _refine_diff_density_min -0.316 _refine_diff_density_rms 0.045 _refine_ls_abs_structure_details ; Flack x determined using 2869 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.03(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.999 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 529 _refine_ls_number_reflns 12304 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.999 _refine_ls_R_factor_all 0.0852 _refine_ls_R_factor_gt 0.0460 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0420P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0946 _refine_ls_wR_factor_ref 0.1062 _reflns_Friedel_coverage 0.752 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.882 _reflns_number_gt 8256 _reflns_number_total 12304 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file op1c00019_si_002.cif _cod_data_source_block compound-31 _cod_database_code 1561044 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.973 _shelx_estimated_absorpt_t_min 0.935 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C24(H24), C8(H8) 2.b Secondary CH2 refined with riding coordinates: C25(H25A,H25B), C27(H27A,H27B), C10(H10A,H10B), C26(H26A,H26B), C5(H5A,H5B), C9(H9A,H9B), C6(H6A,H6B), C28(H28A,H28B) 2.c Aromatic/amide H refined with riding coordinates: C18(H18), C21(H21), C16(H16), C38(H38), C34(H34), C13(H13), C40(H40), C44(H44), C36(H36), C35(H35), C37(H37), C43(H43), C41(H41), C42(H42) 2.d Idealised Me refined as rotating group: C32(H32A,H32B,H32C), C30(H30A,H30B,H30C), C2(H2A,H2B,H2C), C31(H31A,H31B, H31C), C4(H4A,H4B,H4C), C3(H3A,H3B,H3C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL new_a.res in P2(1)2(1)2(1) compound-31.res created by SHELXL-2016/6 at 12:41:55 on 03-Nov-2020 REM Old TITL new in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.119, Rweak 0.026, Alpha 0.001, Orientation as input REM Flack x = 0.003 ( 0.035 ) from Parsons' quotients REM Formula found by SHELXT: C43 F2 N5 O6 S4 CELL 0.71073 9.7957 14.9403 30.1708 90 90 90 ZERR 4 0.0005 0.0008 0.0015 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H F N O S UNIT 176 200 8 8 24 16 L.S. 10 PLAN 10 SIZE 0.1 0.15 0.25 TEMP 23(2) CONF BOND $H MORE -1 ABIN fmap 2 acta REM REM REM WGHT 0.042000 FVAR 0.34174 S2 6 0.850358 0.718890 0.354753 11.00000 0.04868 0.02465 = 0.03791 0.00035 0.00331 -0.00363 S3 6 0.108846 0.286308 0.558213 11.00000 0.03913 0.03003 = 0.04036 0.00056 0.00360 -0.00578 S4 6 -0.119118 0.491744 0.649868 11.00000 0.03762 0.04816 = 0.03736 0.00129 0.00510 0.00870 S1 6 1.170118 0.565008 0.284721 11.00000 0.03480 0.05950 = 0.04294 -0.00506 0.00803 -0.00428 F1 3 0.338981 0.609611 0.381539 11.00000 0.03184 0.08230 = 0.07722 0.03105 0.00998 0.01159 F2 3 0.256403 0.412968 0.395850 11.00000 0.05962 0.08486 = 0.03425 -0.00755 0.00491 -0.01830 O2 5 0.976470 0.748439 0.335104 11.00000 0.06249 0.04215 = 0.05704 0.00169 0.01415 -0.02344 O4 5 0.126729 0.239616 0.517089 11.00000 0.06371 0.03636 = 0.04852 -0.01142 -0.00367 -0.00486 O3 5 0.732037 0.774356 0.350579 11.00000 0.07188 0.02977 = 0.05865 0.00043 -0.00037 0.01227 N2 4 -0.078451 0.483874 0.595367 11.00000 0.02618 0.04376 = 0.03523 -0.00601 0.00212 0.00423 O5 5 0.002687 0.256407 0.587826 11.00000 0.04626 0.05370 = 0.06117 0.01325 0.01471 -0.01303 O1 5 1.206110 0.649531 0.261165 11.00000 0.05264 0.06358 = 0.08163 -0.00558 0.02397 -0.01613 C24 1 0.068157 0.459319 0.589452 11.00000 0.02893 0.03399 = 0.03335 -0.00235 -0.00059 0.00255 AFIX 13 H24 2 0.096513 0.420477 0.613954 11.00000 -1.20000 AFIX 0 O6 5 -0.206562 0.413793 0.662667 11.00000 0.07157 0.05001 = 0.06650 0.01142 0.02751 0.00361 N1 4 0.997572 0.555595 0.286231 11.00000 0.03265 0.03943 = 0.03635 -0.00217 0.00489 0.00137 C12 1 0.697296 0.568653 0.360420 11.00000 0.03002 0.02759 = 0.03137 0.00310 0.00356 -0.00462 C11 1 0.723430 0.503119 0.392458 11.00000 0.03566 0.02699 = 0.03835 0.00513 0.00456 -0.00037 C23 1 0.073929 0.405237 0.545233 11.00000 0.02637 0.02826 = 0.03376 -0.00089 -0.00111 -0.00228 C33 1 0.265788 0.284988 0.586929 11.00000 0.04224 0.02599 = 0.04194 -0.00028 0.00464 0.00601 C19 1 0.292124 0.488210 0.526529 11.00000 0.03054 0.03394 = 0.03777 -0.00110 0.00001 -0.00443 C18 1 0.390706 0.512105 0.495159 11.00000 0.02911 0.03991 = 0.04553 0.00031 0.00087 -0.00980 AFIX 43 H18 2 0.465123 0.546001 0.504359 11.00000 -1.20000 AFIX 0 C17 1 0.382333 0.487505 0.451029 11.00000 0.03211 0.03981 = 0.03667 0.00645 0.00560 -0.00473 C25 1 0.156466 0.542696 0.589234 11.00000 0.03621 0.03937 = 0.03956 -0.00654 -0.00193 -0.00165 AFIX 23 H25A 2 0.116263 0.587172 0.569787 11.00000 -1.20000 H25B 2 0.160271 0.567657 0.618888 11.00000 -1.20000 AFIX 0 C45 1 0.812298 0.606648 0.332438 11.00000 0.03505 0.02372 = 0.03116 0.00050 0.00253 -0.00002 C39 1 0.881411 0.701192 0.412184 11.00000 0.05986 0.03089 = 0.03789 -0.00459 0.00161 -0.00520 C27 1 -0.074280 0.408712 0.527024 11.00000 0.02805 0.04462 = 0.04228 -0.00503 -0.00181 -0.00370 AFIX 23 H27A 2 -0.083877 0.456566 0.505520 11.00000 -1.20000 H27B 2 -0.098177 0.352511 0.512920 11.00000 -1.20000 AFIX 0 C8 1 0.946644 0.552136 0.332722 11.00000 0.03204 0.03268 = 0.03145 -0.00147 0.00558 -0.00037 AFIX 13 H8 2 1.012688 0.582173 0.352062 11.00000 -1.20000 AFIX 0 C20 1 0.180817 0.436883 0.512630 11.00000 0.02869 0.03017 = 0.03331 0.00130 0.00135 -0.00272 C15 1 0.489472 0.513431 0.418835 11.00000 0.03780 0.03715 = 0.03699 0.00216 0.00540 -0.00557 C22 1 0.269262 0.437849 0.438989 11.00000 0.04045 0.04597 = 0.02850 -0.00145 0.00186 -0.00426 C21 1 0.170032 0.412290 0.468381 11.00000 0.03341 0.03627 = 0.03457 -0.00109 0.00000 -0.00887 AFIX 43 H21 2 0.095856 0.378654 0.458752 11.00000 -1.20000 AFIX 0 C10 1 0.862495 0.459731 0.394569 11.00000 0.03885 0.03451 = 0.04900 0.01540 0.00494 0.00305 AFIX 23 H10A 2 0.920833 0.493218 0.414566 11.00000 -1.20000 H10B 2 0.853884 0.399263 0.405937 11.00000 -1.20000 AFIX 0 C16 1 0.620233 0.477722 0.421224 11.00000 0.04183 0.03423 = 0.03798 0.00829 0.00023 -0.00169 AFIX 43 H16 2 0.639153 0.435256 0.442908 11.00000 -1.20000 AFIX 0 C26 1 0.299616 0.521069 0.573602 11.00000 0.03301 0.04416 = 0.04213 -0.00625 -0.00186 -0.00825 AFIX 23 H26A 2 0.356457 0.574134 0.575201 11.00000 -1.20000 H26B 2 0.339553 0.475356 0.592392 11.00000 -1.20000 AFIX 0 C29 1 -0.233569 0.589243 0.650623 11.00000 0.03915 0.04100 = 0.04502 -0.00459 0.00659 0.00995 C38 1 0.265482 0.279110 0.632957 11.00000 0.06079 0.04036 = 0.04268 0.00198 -0.00040 0.00969 AFIX 43 H38 2 0.183924 0.274891 0.648597 11.00000 -1.20000 AFIX 0 C14 1 0.466403 0.574728 0.385068 11.00000 0.03072 0.04741 = 0.04504 0.00814 0.00246 0.00003 C34 1 0.386556 0.289448 0.563236 11.00000 0.04601 0.02960 = 0.05203 -0.00315 0.00603 0.00197 AFIX 43 H34 2 0.385028 0.292275 0.532447 11.00000 -1.20000 AFIX 0 C13 1 0.566098 0.602606 0.356004 11.00000 0.04106 0.03923 = 0.03942 0.00838 0.00150 0.00164 AFIX 43 H13 2 0.545831 0.643572 0.333748 11.00000 -1.20000 AFIX 0 C5 1 0.915251 0.617820 0.259105 11.00000 0.04618 0.04357 = 0.02916 0.00041 0.00311 0.00164 AFIX 23 H5A 2 0.906037 0.596115 0.228953 11.00000 -1.20000 H5B 2 0.955836 0.677030 0.258536 11.00000 -1.20000 AFIX 0 C9 1 0.925803 0.457385 0.349053 11.00000 0.04338 0.03096 = 0.05102 0.00525 0.00972 0.00734 AFIX 23 H9A 2 0.866535 0.425237 0.328807 11.00000 -1.20000 H9B 2 1.012804 0.426471 0.350238 11.00000 -1.20000 AFIX 0 C6 1 0.778269 0.619024 0.282605 11.00000 0.03879 0.04012 = 0.03450 0.00337 -0.00191 -0.00034 AFIX 23 H6A 2 0.720549 0.570733 0.272087 11.00000 -1.20000 H6B 2 0.731755 0.675463 0.277658 11.00000 -1.20000 AFIX 0 C28 1 -0.164802 0.425652 0.566993 11.00000 0.02718 0.05962 = 0.05440 -0.01313 0.00350 -0.00315 AFIX 23 H28A 2 -0.248496 0.455823 0.558505 11.00000 -1.20000 H28B 2 -0.187386 0.370172 0.581996 11.00000 -1.20000 AFIX 0 C40 1 1.011578 0.683312 0.427274 11.00000 0.06265 0.05828 = 0.04915 -0.00496 -0.00458 -0.00583 AFIX 43 H40 2 1.084983 0.684081 0.407729 11.00000 -1.20000 AFIX 0 C44 1 0.771107 0.702435 0.441333 11.00000 0.07550 0.05918 = 0.04518 -0.00756 0.00834 0.00210 AFIX 43 H44 2 0.683555 0.715749 0.431400 11.00000 -1.20000 AFIX 0 C36 1 0.510015 0.285212 0.631438 11.00000 0.05227 0.04786 = 0.08920 -0.01598 -0.02199 0.00780 AFIX 43 H36 2 0.592807 0.285948 0.646520 11.00000 -1.20000 AFIX 0 C1 1 1.218197 0.474059 0.246509 11.00000 0.05141 0.06681 = 0.04660 0.00086 0.01767 0.01640 C35 1 0.508560 0.289662 0.585566 11.00000 0.04289 0.03987 = 0.07745 -0.00989 0.00251 -0.00011 AFIX 43 H35 2 0.590232 0.292791 0.569926 11.00000 -1.20000 AFIX 0 C37 1 0.389424 0.279700 0.654854 11.00000 0.08219 0.04664 = 0.05172 -0.00637 -0.02223 0.01456 AFIX 43 H37 2 0.391498 0.276352 0.685627 11.00000 -1.20000 AFIX 0 C32 1 -0.270512 0.599231 0.699583 11.00000 0.05719 0.06233 = 0.04987 -0.00827 0.01690 0.00626 AFIX 137 H32A 2 -0.318753 0.546882 0.709337 11.00000 -1.50000 H32B 2 -0.327375 0.650980 0.703443 11.00000 -1.50000 H32C 2 -0.188617 0.606104 0.716725 11.00000 -1.50000 AFIX 0 C30 1 -0.359358 0.572208 0.622208 11.00000 0.05308 0.07725 = 0.07152 -0.02221 -0.01239 0.02687 AFIX 137 H30A 2 -0.335291 0.576901 0.591451 11.00000 -1.50000 H30B 2 -0.428254 0.615719 0.629126 11.00000 -1.50000 H30C 2 -0.393845 0.513263 0.628130 11.00000 -1.50000 AFIX 0 C2 1 1.164336 0.492256 0.200339 11.00000 0.10383 0.06764 = 0.04750 -0.01067 0.01322 0.01314 AFIX 137 H2A 2 1.066467 0.495197 0.201130 11.00000 -1.50000 H2B 2 1.192244 0.444948 0.180806 11.00000 -1.50000 H2C 2 1.200149 0.548160 0.189809 11.00000 -1.50000 AFIX 0 C43 1 0.795473 0.683406 0.485200 11.00000 0.11238 0.10063 = 0.04127 -0.00321 0.01712 0.01753 AFIX 43 H43 2 0.723032 0.683494 0.505124 11.00000 -1.20000 AFIX 0 C31 1 -0.152433 0.669345 0.635254 11.00000 0.09601 0.04433 = 0.07246 -0.00019 0.02646 0.00577 AFIX 137 H31A 2 -0.070308 0.674065 0.652460 11.00000 -1.50000 H31B 2 -0.205993 0.722620 0.639005 11.00000 -1.50000 H31C 2 -0.129399 0.662289 0.604525 11.00000 -1.50000 AFIX 0 C41 1 1.032277 0.664225 0.471669 11.00000 0.08933 0.08607 = 0.05950 -0.00482 -0.02908 0.00604 AFIX 43 H41 2 1.119419 0.651361 0.482114 11.00000 -1.20000 AFIX 0 C42 1 0.923175 0.664472 0.500059 11.00000 0.13605 0.10750 = 0.04165 -0.00153 -0.00673 0.03205 AFIX 43 H42 2 0.936680 0.651514 0.529888 11.00000 -1.20000 AFIX 0 C4 1 1.163600 0.386420 0.265032 11.00000 0.09981 0.04977 = 0.08543 0.00095 0.02649 0.02233 AFIX 137 H4A 2 1.197390 0.377984 0.294606 11.00000 -1.50000 H4B 2 1.193297 0.337736 0.246639 11.00000 -1.50000 H4C 2 1.065649 0.388215 0.265544 11.00000 -1.50000 AFIX 0 C3 1 1.374316 0.475196 0.247708 11.00000 0.05705 0.13353 = 0.11081 -0.01741 0.02528 0.02487 AFIX 137 H3A 2 1.406947 0.530536 0.235493 11.00000 -1.50000 H3B 2 1.409075 0.426089 0.230569 11.00000 -1.50000 H3C 2 1.404895 0.469677 0.277815 11.00000 -1.50000 AFIX 0 HKLF 4 REM new_a.res in P2(1)2(1)2(1) REM R1 = 0.0460 for 8256 Fo > 4sig(Fo) and 0.0852 for all 12304 data REM 529 parameters refined using 0 restraints END WGHT 0.0420 0.0000 REM Highest difference peak 0.283, deepest hole -0.316, 1-sigma level 0.045 Q1 1 0.8680 0.7171 0.3853 11.00000 0.05 0.28 Q2 1 0.8190 0.6597 0.3444 11.00000 0.05 0.23 Q3 1 0.1989 0.4194 0.4931 11.00000 0.05 0.21 Q4 1 -0.1030 0.4806 0.6188 11.00000 0.05 0.20 Q5 1 0.2446 0.4618 0.5219 11.00000 0.05 0.20 Q6 1 0.9778 0.7411 0.3022 11.00000 0.05 0.19 Q7 1 1.0404 0.6914 0.4908 11.00000 0.05 0.18 Q8 1 -0.1617 0.4188 0.6434 11.00000 0.05 0.17 Q9 1 0.0597 0.4349 0.5632 11.00000 0.05 0.17 Q10 1 1.1585 0.5688 0.1758 11.00000 0.05 0.17 ; _shelx_res_checksum 26109 _shelx_hkl_file ; 1 0 0 -0.10 0.40 1 0 0 0.80 0.60 1 0 0 1.50 0.60 -1 0 0 1.10 0.60 -1 0 0 0.10 0.60 -1 0 0 0.50 0.60 -2 0 0 1595.94 139.99 -2 0 0 1653.83 139.99 -2 0 0 1632.64 139.99 2 0 0 1678.33 139.99 2 0 0 1724.13 139.99 2 0 0 1591.74 139.89 3 0 0 1.00 1.30 -3 0 0 0.30 1.50 3 0 0 0.30 1.30 3 0 0 -0.10 1.20 -3 0 0 1.20 1.30 -3 0 0 -1.70 1.20 3 0 0 -0.30 1.10 4 0 0 633.54 55.09 4 0 0 629.84 55.09 4 0 0 658.43 55.19 -4 0 0 621.14 55.29 -4 0 0 611.04 55.19 -4 0 0 666.13 55.39 5 0 0 -1.10 1.80 -5 0 0 -3.70 1.70 5 0 0 -0.10 1.80 -5 0 0 1.30 2.20 -6 0 0 58.69 8.00 6 0 0 58.09 7.70 -6 0 0 62.69 8.40 6 0 0 71.19 7.90 -7 0 0 -0.80 3.00 7 0 0 2.30 2.50 -7 0 0 -3.90 2.40 -8 0 0 214.78 20.70 -8 0 0 210.28 20.40 8 0 0 186.28 19.90 -9 0 0 -1.00 4.10 -9 0 0 -2.90 3.60 9 0 0 -0.70 3.40 -10 0 0 23.50 7.00 10 0 0 13.40 5.50 -11 0 0 2.00 4.90 11 0 0 -2.50 5.00 12 0 0 13.80 7.60 -12 0 0 5.50 6.20 -13 0 0 -0.40 6.80 0 -1 0 0.20 0.10 0 -1 0 -0.10 0.40 0 1 0 0.30 0.30 0 -1 0 0.50 0.30 0 1 0 0.00 0.20 0 1 0 0.40 0.20 1 -1 0 192.48 16.70 -1 1 0 171.88 17.00 1 -1 0 190.88 16.60 1 -1 0 189.18 17.00 1 1 0 197.28 16.70 -1 1 0 187.78 16.60 -1 -1 0 219.28 16.80 -1 -1 0 190.78 16.70 -1 1 0 194.28 16.70 2 -1 0 1733.63 144.19 -2 1 0 1731.03 144.19 -2 1 0 1727.53 144.19 -2 1 0 1708.33 144.59 2 1 0 1715.23 143.79 -2 -1 0 1716.83 144.29 2 1 0 1487.95 144.09 2 -1 0 1731.83 144.19 2 1 0 1744.83 144.19 2 -1 0 1674.03 144.59 -2 -1 0 1692.13 144.29 -2 -1 0 1687.63 143.89 3 1 0 609.54 51.09 -3 -1 0 591.84 50.79 3 -1 0 581.44 50.89 3 1 0 570.34 50.59 3 -1 0 567.04 51.39 -3 1 0 593.84 51.49 3 -1 0 612.14 51.09 3 1 0 591.54 51.09 3 -1 0 599.34 50.99 -3 -1 0 614.34 51.19 -3 1 0 582.14 50.99 -3 -1 0 588.24 51.09 -4 -1 0 78.99 9.90 4 -1 0 111.09 10.20 4 1 0 111.09 9.60 4 1 0 106.69 10.10 -4 -1 0 94.39 10.10 -4 1 0 97.49 10.60 -4 1 0 102.39 10.10 4 -1 0 101.79 9.90 4 -1 0 105.39 10.50 -4 -1 0 103.69 9.90 5 1 0 115.89 11.30 5 1 0 124.19 12.00 -5 1 0 131.09 12.90 -5 -1 0 113.19 11.80 5 -1 0 114.39 12.00 -5 1 0 120.29 12.00 5 -1 0 122.29 12.30 -5 -1 0 130.39 12.40 -6 -1 0 104.99 12.00 -6 -1 0 112.29 11.90 -6 1 0 107.49 11.90 6 1 0 119.09 11.20 6 1 0 120.49 12.00 -6 1 0 118.59 12.80 6 -1 0 125.59 12.10 -7 1 0 251.77 24.80 -7 1 0 262.07 25.50 -7 -1 0 242.98 24.90 7 1 0 277.87 23.80 -7 -1 0 274.47 24.70 7 -1 0 268.87 24.70 7 1 0 254.27 24.50 8 1 0 104.59 12.50 -8 1 0 103.39 13.00 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1603.84 146.19 -2 2 0 1810.92 146.69 2 -2 0 1689.83 147.39 -2 -2 0 1942.51 146.89 3 2 0 43.60 4.80 3 2 0 24.60 4.10 3 -2 0 40.40 4.20 -3 2 0 30.30 5.40 -3 2 0 34.70 4.50 -3 2 0 44.60 4.80 3 -2 0 40.30 5.70 -3 -2 0 37.90 4.80 3 -2 0 43.90 4.80 -3 -2 0 41.40 4.90 -4 -2 0 462.35 38.80 4 -2 0 433.66 38.30 4 -2 0 492.65 38.90 -4 -2 0 427.76 38.00 4 -2 0 438.86 39.30 4 2 0 433.16 37.60 -4 2 0 427.06 38.50 4 2 0 418.66 38.50 -4 2 0 435.66 39.40 -4 2 0 438.66 38.50 -5 2 0 214.38 20.80 -5 -2 0 213.78 19.30 -5 -2 0 200.48 20.00 5 2 0 219.28 18.70 5 2 0 209.88 19.80 -5 2 0 211.88 19.80 5 -2 0 216.58 19.90 6 2 0 2.00 1.50 6 -2 0 7.00 3.00 -6 2 0 0.40 3.10 -6 -2 0 1.50 2.60 6 2 0 4.20 2.60 -6 2 0 2.10 2.30 -6 -2 0 6.30 2.40 -7 -2 0 12.40 4.20 -7 2 0 9.80 3.90 7 2 0 20.40 4.60 7 -2 0 16.40 4.30 -7 -2 0 11.20 3.50 -7 2 0 1.20 3.80 7 2 0 17.90 2.80 -8 2 0 228.68 23.60 -8 -2 0 229.18 23.10 -8 2 0 217.58 22.30 8 -2 0 225.58 22.20 -8 -2 0 220.78 21.70 8 2 0 261.07 22.70 9 2 0 75.69 9.60 9 -2 0 44.70 7.80 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26.60 -3 -3 0 271.97 25.80 3 3 0 323.77 26.80 -4 3 0 119.69 11.60 4 3 0 123.59 10.60 -4 -3 0 136.49 12.10 -4 3 0 108.09 11.50 4 -3 0 112.19 11.30 -4 3 0 129.99 13.20 4 3 0 112.69 11.70 -4 -3 0 123.59 10.80 -5 3 0 34.40 5.40 5 3 0 40.30 4.00 -5 3 0 32.70 6.80 5 -3 0 51.29 6.30 -5 3 0 33.90 5.30 -5 -3 0 44.60 4.60 5 3 0 45.80 6.00 -5 -3 0 41.20 5.90 -6 3 0 135.59 14.60 6 3 0 136.39 12.90 -6 -3 0 124.69 11.80 6 -3 0 107.19 12.60 -6 -3 0 131.99 13.30 6 3 0 119.39 11.20 -6 3 0 145.69 13.10 -7 3 0 256.07 24.20 -7 -3 0 246.18 24.60 7 3 0 260.37 24.40 -7 -3 0 263.67 23.30 -7 3 0 247.98 25.80 7 -3 0 272.47 24.40 7 3 0 253.57 22.40 -8 3 0 58.29 10.30 8 3 0 68.69 9.30 8 -3 0 53.89 8.60 -8 -3 0 42.60 6.80 -8 3 0 57.09 8.70 -8 -3 0 88.99 10.70 -9 3 0 7.00 6.00 -9 3 0 -1.70 4.00 -9 -3 0 5.30 4.50 9 -3 0 4.70 4.00 9 3 0 0.90 3.80 10 -3 0 1.60 4.70 -10 -3 0 2.30 4.10 10 3 0 12.10 5.30 -10 3 0 3.70 6.00 -10 3 0 7.40 5.30 -11 3 0 23.80 7.20 11 -3 0 12.20 6.10 11 3 0 16.60 6.50 -11 -3 0 20.70 7.10 12 3 0 3.50 6.20 -12 3 0 -1.20 6.30 -12 -3 0 0.60 6.80 -13 3 0 1.60 6.80 13 -3 0 -4.10 6.70 0 4 0 9999.00 737.53 0 -4 0 8559.64 738.43 0 4 0 7720.83 737.73 0 -4 0 8369.06 737.43 0 4 0 9396.66 738.63 0 -4 0 8217.48 737.73 -1 4 0 4337.77 346.57 1 -4 0 4205.38 346.27 -1 4 0 3514.05 347.27 -1 -4 0 3596.24 346.67 1 -4 0 4356.06 346.47 1 -4 0 4453.95 347.67 -1 -4 0 3975.60 346.37 1 4 0 4408.86 346.27 -1 4 0 3763.52 346.37 1 4 0 4228.28 346.67 -2 -4 0 1138.19 91.39 -2 -4 0 1093.89 91.19 2 -4 0 959.40 92.49 2 -4 0 1114.19 91.39 2 4 0 1164.48 91.69 -2 4 0 1171.88 91.39 -2 4 0 1021.60 92.69 -2 -4 0 926.01 91.39 -2 4 0 1057.19 91.29 2 -4 0 1026.30 91.29 3 -4 0 519.25 41.00 3 4 0 466.45 40.60 3 4 0 475.95 41.40 3 -4 0 474.75 41.10 -3 -4 0 427.66 40.60 3 -4 0 481.25 41.10 -3 -4 0 462.15 40.30 -3 -4 0 482.45 41.40 -3 4 0 480.45 42.70 -3 4 0 481.45 41.10 -4 -4 0 420.86 35.80 -4 4 0 412.46 36.90 -4 -4 0 455.15 37.30 4 -4 0 450.05 36.80 4 -4 0 431.36 36.60 4 4 0 417.86 37.10 4 4 0 366.56 35.80 -4 4 0 443.36 38.70 -5 -4 0 74.99 8.20 5 -4 0 53.49 6.70 -5 4 0 54.49 6.90 -5 4 0 65.39 9.50 -5 4 0 49.00 6.70 5 4 0 59.99 7.40 5 4 0 47.70 5.00 -5 -4 0 57.79 5.30 -6 4 0 5.60 2.70 6 -4 0 7.90 2.90 -6 4 0 7.20 3.90 -6 4 0 6.20 2.70 -6 -4 0 -1.90 2.50 6 -4 0 1.80 2.80 6 4 0 4.30 1.20 6 4 0 2.70 2.90 -6 -4 0 3.40 1.50 7 -4 0 18.30 4.70 7 -4 0 16.00 4.50 -7 4 0 22.30 6.50 -7 -4 0 13.70 2.80 -7 -4 0 20.40 5.50 7 4 0 16.10 2.30 -7 4 0 23.60 4.80 7 4 0 30.70 5.30 -8 -4 0 665.63 58.69 8 4 0 676.33 57.99 -8 4 0 638.04 59.89 -8 4 0 674.33 58.09 8 -4 0 604.54 57.79 9 4 0 1.90 4.30 -9 4 0 6.90 6.30 9 -4 0 5.60 4.00 9 -4 0 -2.10 3.40 -9 4 0 1.40 4.10 -9 -4 0 3.70 4.30 10 -4 0 72.79 10.40 -10 4 0 73.49 10.90 10 -4 0 60.19 10.10 -10 -4 0 52.09 10.30 10 4 0 61.09 10.10 -10 4 0 54.89 11.90 11 4 0 11.60 6.10 -11 4 0 8.40 5.90 -11 -4 0 15.80 6.40 11 -4 0 0.60 8.10 -11 4 0 11.40 7.90 11 -4 0 8.50 6.40 11 -4 0 11.60 6.30 -12 4 0 48.60 10.50 12 4 0 41.90 9.70 -12 -4 0 40.70 10.50 12 -4 0 66.69 11.80 13 4 0 5.10 9.10 -13 4 0 3.50 7.60 13 -4 0 0.90 7.50 0 5 0 1.60 1.60 0 -5 0 -2.90 2.30 0 -5 0 2.10 1.50 0 5 0 0.60 2.60 0 5 0 1.90 1.10 0 -5 0 2.30 1.30 1 -5 0 86.69 8.80 1 5 0 87.89 9.50 -1 -5 0 96.49 9.10 -1 -5 0 109.59 9.80 1 -5 0 106.09 8.60 -1 -5 0 107.59 9.70 1 5 0 85.39 8.50 -1 5 0 84.29 10.70 -1 5 0 91.19 8.90 -1 5 0 72.19 8.50 -1 -5 0 103.19 8.70 1 5 0 90.79 9.10 2 -5 0 346.87 32.60 -2 -5 0 342.47 32.70 -2 -5 0 408.66 33.00 2 5 0 368.76 32.90 2 -5 0 360.86 32.50 -2 5 0 364.96 32.70 -2 -5 0 366.26 32.60 -2 5 0 423.66 32.70 -2 5 0 405.46 34.50 3 -5 0 125.49 12.00 -3 5 0 136.39 14.00 3 -5 0 116.39 11.40 3 -5 0 122.59 11.40 3 5 0 114.79 11.80 -3 -5 0 110.99 11.20 -3 5 0 120.19 11.40 -3 -5 0 121.79 10.80 -3 -5 0 126.99 11.70 -4 -5 0 507.45 41.80 -4 -5 0 466.55 42.10 4 5 0 507.05 43.30 -4 5 0 483.75 42.90 -4 -5 0 472.85 43.20 -4 5 0 510.05 45.10 4 -5 0 487.95 42.80 -5 -5 0 405.96 38.80 -5 5 0 417.86 40.40 5 5 0 443.96 38.70 -5 5 0 454.85 38.60 5 -5 0 436.46 38.30 -6 -5 0 60.39 8.70 -6 5 0 74.39 11.20 6 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6 0 158.48 15.80 -2 -6 0 137.89 13.80 2 -6 0 150.88 13.70 -2 6 0 154.18 13.80 -2 -6 0 158.48 14.30 -2 -6 0 139.89 13.60 2 -6 0 138.19 13.40 2 6 0 142.69 14.00 -3 -6 0 121.79 12.30 -3 6 0 135.59 12.30 -3 6 0 133.59 14.60 -3 -6 0 120.39 11.70 3 -6 0 122.39 12.10 -3 -6 0 137.29 12.50 3 6 0 139.89 12.90 -4 -6 0 221.68 19.50 -4 -6 0 216.58 18.90 -4 6 0 243.08 22.90 4 6 0 215.08 20.50 4 -6 0 204.88 19.90 -4 6 0 218.48 20.00 -4 -6 0 220.68 20.40 -5 6 0 125.39 12.70 -5 6 0 118.59 16.10 5 -6 0 123.49 12.60 -5 -6 0 132.09 13.30 5 6 0 124.29 12.90 6 -6 0 182.98 17.70 -6 6 0 188.58 18.00 -6 -6 0 214.48 18.90 6 6 0 169.58 18.10 -6 6 0 166.28 21.50 -7 6 0 277.27 27.60 7 6 0 260.27 25.10 -7 6 0 266.47 24.70 -7 -6 0 258.27 25.20 7 -6 0 240.38 24.40 -8 6 0 45.50 7.70 8 -6 0 35.00 7.50 -8 -6 0 55.99 9.10 -8 6 0 58.99 11.90 8 6 0 51.29 8.30 8 -6 0 53.49 8.20 -9 6 0 47.00 11.30 9 -6 0 39.60 7.70 9 6 0 45.20 8.40 9 -6 0 35.50 7.90 -9 -6 0 40.80 8.90 10 -6 0 87.59 12.70 10 -6 0 103.49 13.30 -10 6 0 84.99 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16.90 6 -10 0 171.98 16.50 -7 -10 0 0.30 4.90 7 10 0 -3.50 4.40 7 -10 0 -1.90 3.50 -7 10 0 -0.50 3.20 -7 10 0 -3.20 6.40 -8 10 0 60.39 9.70 -8 -10 0 48.20 9.70 8 -10 0 49.00 8.60 8 10 0 58.59 10.10 -8 10 0 66.89 14.10 -9 10 0 0.70 4.70 -9 10 0 8.00 9.70 9 -10 0 -0.10 5.10 -9 -10 0 -0.70 5.20 9 10 0 1.90 5.40 10 -10 0 28.50 7.70 10 -10 0 27.30 12.80 -10 -10 0 21.20 8.30 10 10 0 15.50 8.50 -10 10 0 36.60 13.90 -11 10 0 -5.50 12.10 11 10 0 9.50 8.00 11 -10 0 -0.40 6.60 -11 -10 0 3.00 7.90 11 -10 0 7.00 10.40 12 -10 0 1.90 8.50 12 -10 0 6.50 14.50 0 11 0 2.40 4.80 0 -11 0 -2.10 3.40 0 11 0 -0.40 2.70 0 -11 0 -2.80 2.00 -1 -11 0 171.78 18.50 -1 11 0 196.68 23.80 1 -11 0 242.98 18.70 -1 11 0 204.18 19.60 1 -11 0 196.48 21.90 -1 -11 0 196.48 20.80 1 11 0 186.58 19.50 -2 -11 0 299.97 24.00 -2 11 0 231.68 26.60 2 11 0 255.97 24.40 -2 11 0 261.37 24.20 -2 -11 0 189.18 24.20 2 -11 0 273.47 23.20 3 -11 0 34.50 5.20 -3 11 0 33.20 5.80 -3 -11 0 33.50 6.00 3 11 0 20.10 5.50 -3 11 0 34.80 8.90 -3 -11 0 31.10 6.00 -4 -11 0 233.08 22.90 4 11 0 220.18 23.40 -4 -11 0 241.98 22.00 -4 11 0 225.68 22.50 4 -11 0 230.78 21.90 -4 11 0 302.17 27.60 5 -11 0 33.60 6.00 -5 -11 0 36.00 5.00 -5 11 0 56.79 7.70 -5 11 0 36.90 11.10 -5 -11 0 29.10 6.60 5 11 0 38.00 7.40 -6 11 0 0.20 6.40 -6 11 0 1.10 3.50 6 -11 0 -3.30 3.00 6 11 0 -5.40 4.30 -6 -11 0 2.80 4.20 -7 11 0 85.89 11.80 -7 11 0 89.19 17.20 7 -11 0 97.19 11.60 -7 -11 0 73.89 12.00 7 11 0 86.79 13.10 -8 11 0 -3.00 4.30 8 -11 0 -5.60 3.80 -8 11 0 -3.20 7.00 -8 -11 0 4.00 6.40 8 11 0 -9.20 5.50 9 -11 0 2.70 5.20 9 -11 0 2.80 8.90 -9 11 0 11.00 9.80 -9 -11 0 2.00 7.00 9 11 0 -7.80 6.20 10 -11 0 11.20 12.60 -10 11 0 10.30 12.60 -10 -11 0 6.80 6.80 10 -11 0 7.60 6.70 10 11 0 6.30 8.50 -11 11 0 2.50 13.20 11 11 0 -8.60 8.60 11 -11 0 2.70 7.60 11 -11 0 11.00 12.60 0 -12 0 -6.70 4.40 0 12 0 -3.90 2.80 0 -12 0 0.50 2.40 1 12 0 165.08 17.00 -1 -12 0 135.59 18.50 1 -12 0 176.48 20.50 1 -12 0 181.18 15.70 -1 12 0 118.79 19.00 -1 -12 0 169.08 16.10 -1 12 0 161.18 16.90 -2 -12 0 2.20 4.20 -2 12 0 -7.60 4.30 2 12 0 -3.80 3.60 -2 12 0 3.60 3.50 2 -12 0 14.10 6.50 -2 -12 0 -3.40 2.80 2 -12 0 -1.10 2.60 3 12 0 57.49 9.40 3 -12 0 65.29 8.20 3 -12 0 62.09 12.40 -3 12 0 63.39 9.30 -3 -12 0 90.09 10.30 -3 -12 0 65.79 9.30 -3 12 0 74.59 13.60 -4 12 0 79.09 14.10 4 -12 0 80.29 8.90 -4 -12 0 57.79 9.40 4 12 0 54.09 9.40 -4 12 0 74.39 9.80 -4 -12 0 66.19 8.70 -5 12 0 8.50 7.60 -5 12 0 6.50 3.90 -5 -12 0 1.90 4.80 5 12 0 9.50 5.20 5 -12 0 6.30 3.60 6 -12 0 11.40 4.30 -6 12 0 3.90 7.50 -6 -12 0 4.70 5.00 -6 12 0 9.40 4.50 6 12 0 11.30 5.20 7 -12 0 6.60 4.40 7 12 0 1.20 5.20 -7 -12 0 11.20 5.90 7 -12 0 -0.30 7.10 -7 12 0 3.50 5.00 -7 12 0 9.80 9.80 8 12 0 16.50 6.80 -8 -12 0 11.90 7.60 8 -12 0 2.20 8.60 -8 12 0 13.40 6.00 -8 12 0 16.30 10.90 8 -12 0 5.40 5.50 -9 12 0 21.00 12.40 9 -12 0 16.10 12.50 9 -12 0 15.60 6.30 9 12 0 8.30 7.10 -9 -12 0 2.40 7.40 -10 -12 0 4.10 7.80 10 -12 0 9.30 13.30 10 -12 0 -1.30 6.30 -10 12 0 0.60 12.80 10 12 0 10.40 8.30 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164.78 19.00 -7 9 7 162.88 17.90 7 9 7 161.88 18.10 7 -9 -7 174.58 16.90 -7 9 -7 173.38 23.90 7 -9 -7 173.58 22.00 -7 -9 7 175.78 18.30 -7 9 -7 155.98 16.50 -8 9 7 6.20 5.20 8 9 -7 15.70 6.30 -8 -9 -7 3.00 5.50 8 -9 7 -0.80 4.50 -8 9 -7 13.60 9.20 -8 -9 7 2.70 4.90 8 9 7 1.40 4.50 8 -9 -7 10.90 7.70 8 -9 -7 5.20 4.20 -9 9 7 12.50 7.10 -9 -9 -7 14.20 7.30 9 9 -7 9.60 6.70 9 -9 7 6.40 6.00 9 -9 -7 13.20 5.40 9 9 7 6.30 5.70 -9 9 -7 -7.40 8.10 -9 -9 7 18.40 7.10 9 -9 -7 7.60 8.10 10 -9 7 2.50 5.90 -10 -9 -7 -4.80 7.10 10 9 -7 -7.60 6.30 -10 9 7 3.80 6.40 -10 9 -7 -0.60 10.40 10 -9 -7 12.10 7.80 10 -9 -7 1.20 7.90 -10 -9 7 -1.30 5.50 10 9 7 -2.20 5.60 10 -9 -7 -0.50 5.10 -11 -9 -7 7.20 7.40 11 -9 7 6.40 7.90 11 9 -7 9.40 8.70 -11 9 -7 -8.30 8.90 11 9 7 6.80 7.90 11 -9 -7 7.70 10.30 11 -9 -7 6.80 8.80 -11 -9 7 11.00 7.20 -12 9 -7 6.20 14.20 12 -9 -7 25.80 21.60 0 10 7 32.60 6.00 0 10 -7 37.60 7.80 0 -10 -7 36.10 4.60 0 10 -7 34.90 5.70 0 -10 -7 25.90 6.20 0 -10 7 19.10 4.40 1 -10 7 283.87 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5.10 -6 -10 12 4.10 4.40 6 -10 -12 19.50 7.70 7 10 -12 14.90 6.00 -7 10 12 20.20 7.50 -7 -10 -12 20.30 7.00 7 -10 12 14.80 5.80 7 10 12 11.90 5.30 -7 10 -12 18.40 9.40 -7 -10 12 8.90 5.20 7 -10 -12 12.10 8.10 8 -10 12 32.90 7.60 -8 10 12 15.80 7.40 8 10 -12 27.80 7.60 -8 -10 -12 30.70 8.60 8 10 12 39.10 8.40 -8 10 -12 31.10 11.80 8 -10 -12 50.09 11.20 -8 -10 12 26.80 7.80 -9 -10 -12 22.20 8.30 -9 10 12 4.70 7.40 9 10 -12 14.60 7.10 9 -10 12 15.90 6.80 -9 10 -12 -5.50 8.10 9 -10 -12 6.20 9.40 -9 -10 12 0.40 5.90 9 10 12 2.00 5.90 10 10 -12 6.00 8.20 10 -10 12 8.40 7.70 -10 10 12 2.90 7.10 -10 -10 -12 14.80 9.80 -10 -10 12 15.10 7.80 10 -10 -12 -1.20 9.10 10 -10 -12 21.80 10.60 10 10 12 13.00 8.00 -10 10 -12 21.40 13.20 11 -10 -12 21.50 13.30 11 -10 -12 16.70 10.80 0 -11 -12 78.29 11.70 0 11 -12 68.49 9.60 0 11 12 80.19 10.90 0 -11 12 73.19 9.20 0 -11 -12 86.49 8.70 0 11 -12 87.69 13.60 -1 -11 -12 149.99 15.50 1 11 -12 119.19 16.90 -1 -11 -12 145.29 13.50 -1 11 12 120.49 15.10 1 11 -12 108.69 14.40 1 -11 12 145.29 13.80 -1 -11 12 122.69 13.40 1 -11 -12 143.39 12.90 1 -11 -12 136.09 16.90 -1 11 -12 132.49 13.70 -1 11 -12 134.09 18.90 1 11 12 124.69 15.30 2 11 -12 37.90 6.60 -2 -11 -12 38.70 6.10 2 11 -12 30.40 7.80 2 -11 12 21.30 5.10 -2 11 12 31.90 6.50 -2 -11 -12 40.30 7.30 2 -11 -12 33.20 8.50 -2 11 -12 29.70 5.30 -2 11 -12 18.50 8.70 2 11 12 21.70 6.10 -2 -11 12 36.30 6.10 2 -11 -12 43.10 4.80 -3 -11 -12 127.69 12.50 -3 11 12 84.19 12.70 3 11 -12 108.39 13.30 3 -11 12 98.39 12.00 3 11 -12 92.09 13.40 -3 -11 -12 118.59 12.70 3 -11 -12 119.69 10.40 3 -11 -12 121.49 16.10 -3 11 -12 93.69 11.20 -3 -11 12 92.69 12.40 3 11 12 111.39 13.60 -3 11 -12 123.19 18.30 -4 -11 -12 -2.30 2.70 -4 -11 -12 2.30 4.10 4 11 -12 3.00 3.90 4 11 -12 0.50 4.10 -4 11 12 1.80 4.20 4 -11 12 -0.40 3.10 4 -11 -12 -0.50 5.40 -4 11 -12 -7.30 6.10 4 11 12 -2.90 4.00 -4 11 -12 1.30 2.40 4 -11 -12 -3.10 1.80 -4 -11 12 -1.30 3.30 5 11 -12 32.50 7.80 5 -11 12 32.10 6.40 -5 -11 -12 20.60 6.30 -5 11 12 24.50 6.70 -5 -11 -12 18.50 4.90 5 11 12 22.20 6.30 -5 -11 12 28.80 6.60 -5 11 -12 14.60 9.70 5 -11 -12 20.00 8.50 6 11 -12 -4.90 3.70 -6 11 12 6.60 5.50 -6 -11 -12 7.60 3.50 -6 -11 -12 3.30 5.00 6 -11 12 13.40 5.00 -6 -11 12 4.30 4.50 -6 11 -12 21.40 10.40 6 -11 -12 4.90 6.70 6 11 12 4.50 4.70 7 -11 12 7.60 5.60 -7 -11 -12 9.90 5.90 -7 11 12 11.70 6.70 7 11 -12 20.70 7.00 7 11 12 3.20 4.70 -7 11 -12 13.10 9.70 -7 -11 12 3.10 5.40 7 -11 -12 3.70 8.10 -8 -11 -12 10.10 7.00 8 11 -12 10.20 7.10 8 -11 12 8.90 5.50 -8 11 12 -3.10 5.10 -8 -11 12 11.90 6.20 -8 11 -12 15.10 10.00 8 11 12 9.50 5.90 8 -11 -12 5.10 7.70 9 -11 12 25.90 8.60 9 11 -12 28.50 9.20 -9 -11 -12 23.10 9.20 -9 11 12 39.10 10.30 9 11 12 20.40 7.10 -9 -11 12 11.20 7.20 -9 11 -12 26.30 12.70 9 -11 -12 12.60 11.20 10 -11 12 13.30 9.20 -10 11 12 18.80 10.10 -10 -11 -12 14.20 9.30 10 -11 -12 9.00 11.20 -10 -11 12 -1.70 7.40 -10 11 -12 2.10 12.10 10 11 12 4.30 8.10 -11 11 12 2.90 9.40 11 -11 -12 12.50 14.60 0 -12 -12 -0.60 2.60 0 12 -12 -4.10 5.50 0 12 12 -1.00 3.80 0 -12 12 7.00 3.80 0 -12 -12 -5.20 4.40 0 12 -12 6.20 3.80 1 -12 12 207.68 19.90 -1 12 12 195.78 20.70 -1 -12 -12 208.48 19.60 1 12 -12 212.18 22.80 -1 -12 -12 219.68 21.90 1 12 -12 190.28 20.40 1 -12 -12 180.58 21.70 -1 12 -12 216.18 20.10 1 -12 -12 210.28 19.00 1 12 12 192.08 20.80 -1 12 -12 182.38 24.30 -1 -12 12 221.48 20.10 2 -12 12 10.50 4.00 -2 12 12 9.10 4.40 -2 -12 -12 11.10 4.30 2 12 -12 11.70 5.00 -2 -12 -12 2.40 4.60 2 12 -12 6.10 5.80 -2 12 -12 -3.40 5.60 2 -12 -12 12.60 3.00 -2 -12 12 7.20 4.20 2 -12 -12 4.30 5.20 -2 12 -12 11.90 3.90 2 12 12 6.70 4.60 -3 12 12 38.60 7.60 3 12 -12 34.90 8.20 3 -12 12 30.80 6.00 -3 -12 -12 29.80 6.50 -3 -12 -12 35.60 6.70 3 12 -12 36.70 7.20 -3 -12 12 37.30 7.00 -3 12 -12 39.00 10.70 3 -12 -12 32.30 8.80 -3 12 -12 37.60 6.20 3 12 12 46.60 8.10 3 -12 -12 42.70 5.20 -4 12 12 10.10 4.80 4 12 -12 14.10 5.00 -4 -12 -12 10.20 5.00 -4 -12 -12 5.00 4.20 4 -12 12 10.30 4.50 -4 -12 12 13.10 5.20 4 12 12 6.40 5.00 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6.70 0 -13 12 43.00 7.10 0 13 -12 47.80 10.70 0 -13 -12 30.50 8.60 0 13 12 38.10 7.80 0 13 -12 36.30 7.20 -1 -13 -12 53.09 7.70 1 -13 12 63.09 8.20 1 13 -12 38.60 10.30 -1 13 12 42.70 8.60 1 13 -12 70.09 9.30 -1 -13 -12 50.59 9.60 1 -13 -12 37.00 9.50 1 -13 -12 61.09 7.10 -1 13 -12 55.39 12.70 -1 13 -12 42.70 7.70 -1 -13 12 62.79 8.50 1 13 12 46.00 8.70 -2 13 12 -1.10 3.60 2 -13 12 8.80 4.00 2 13 -12 3.10 5.90 2 13 -12 9.90 5.30 -2 -13 -12 2.20 3.80 -2 -13 -12 3.60 4.90 -2 13 -12 -8.10 5.70 2 13 12 1.20 5.20 2 -13 -12 6.90 2.90 -2 13 -12 2.30 3.60 2 -13 -12 3.90 5.90 -2 -13 12 -9.60 2.80 3 13 -12 12.00 6.40 -3 -13 -12 9.70 4.80 -3 13 12 18.20 5.70 3 13 -12 12.70 5.50 -3 -13 -12 9.00 4.80 3 -13 12 15.00 5.00 3 13 12 14.70 5.70 -3 -13 12 3.80 4.70 3 -13 -12 20.40 7.70 -3 13 -12 5.20 3.60 -3 13 -12 30.70 10.30 4 13 -12 13.30 5.70 -4 -13 -12 4.90 4.30 -4 -13 -12 6.90 5.20 4 -13 12 3.30 4.20 -4 13 12 3.60 5.40 4 13 12 9.60 6.00 4 -13 -12 10.40 6.70 -4 13 -12 3.00 8.00 -4 -13 12 9.70 4.90 -4 13 -12 11.60 4.20 -5 13 12 -2.30 4.80 5 13 -12 8.10 5.30 5 -13 12 11.70 4.70 -5 -13 -12 6.70 4.10 -5 -13 -12 0.70 5.50 -5 13 -12 6.20 9.30 -5 -13 12 8.90 5.60 5 -13 -12 7.40 7.70 5 13 12 13.70 6.60 -6 -13 -12 38.00 9.20 -6 13 12 65.59 11.70 6 13 -12 48.70 10.00 6 -13 12 36.80 8.00 -6 -13 12 62.69 10.40 -6 13 -12 70.29 16.50 6 -13 -12 47.20 13.20 6 13 12 59.69 10.60 -7 -13 -12 8.00 6.70 -7 13 12 2.90 6.50 7 13 -12 1.20 6.20 7 -13 12 1.90 5.40 7 13 12 0.00 5.90 7 -13 -12 11.30 9.40 -7 13 -12 -6.90 9.90 -7 -13 12 4.90 6.60 -8 13 12 30.60 9.80 8 -13 12 18.70 8.20 8 13 -12 12.60 8.00 -8 -13 -12 28.30 8.70 -8 -13 12 16.00 8.80 8 13 12 34.30 8.90 8 -13 -12 42.90 13.60 -8 13 -12 -1.60 10.90 9 -13 12 2.80 7.70 -9 -13 -12 -8.90 8.00 -9 13 12 5.60 7.60 9 -13 -12 1.90 12.10 9 13 12 13.90 8.40 -10 13 12 6.30 12.40 10 13 12 23.70 13.20 0 14 -12 60.39 9.10 0 -14 12 49.50 8.20 0 14 -12 57.39 13.00 0 -14 -12 56.49 11.50 0 -14 -12 73.29 8.50 0 14 12 62.29 10.40 1 -14 12 13.10 4.80 -1 -14 -12 19.20 7.30 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8.40 6 -14 12 42.00 7.80 -6 14 12 33.70 9.00 6 14 -12 10.00 6.70 -6 14 -12 21.50 12.30 -6 -14 12 17.70 7.60 6 -14 -12 38.00 12.30 6 14 12 23.00 8.50 7 14 -12 7.30 6.60 7 -14 12 5.50 5.40 -7 14 12 5.30 8.00 -7 -14 -12 3.20 6.90 7 14 12 -10.10 7.00 -7 14 -12 3.00 11.30 7 -14 -12 -6.60 8.20 -7 -14 12 0.90 6.10 -8 -14 -12 -1.20 7.60 8 14 -12 3.80 7.90 8 -14 12 0.90 6.30 -8 14 12 -14.10 7.00 8 14 12 -6.10 6.50 8 -14 -12 6.30 11.40 -8 14 -12 21.60 13.90 -8 -14 12 1.60 7.10 -9 -14 -12 0.50 10.60 -9 14 12 27.50 10.20 9 14 12 8.30 8.30 0 -15 -12 1.80 5.90 0 15 -12 3.20 7.80 0 -15 12 5.90 4.10 0 15 -12 7.50 4.80 0 15 12 -5.50 4.90 -1 -15 -12 63.39 9.00 -1 15 12 66.69 11.00 -1 -15 -12 47.90 10.40 1 15 -12 60.59 13.20 1 15 -12 67.59 10.20 1 -15 12 41.20 8.10 1 15 12 65.69 11.50 -1 15 -12 62.29 9.90 -1 -15 12 65.59 10.00 1 -15 -12 46.30 11.70 -1 15 -12 75.99 15.10 2 15 -12 69.39 13.10 -2 15 12 51.89 10.30 -2 -15 -12 74.39 10.10 -2 -15 -12 64.79 11.20 2 -15 12 56.19 9.30 2 15 -12 60.69 10.40 2 -15 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5.00 9.70 -8 -15 -12 11.70 7.90 8 15 12 1.30 8.20 0 16 -12 -8.70 4.50 0 -16 -12 7.80 6.80 0 16 -12 0.20 8.50 0 16 12 0.00 5.30 0 -16 12 1.30 4.70 1 -16 12 153.08 15.70 1 16 -12 135.59 20.90 -1 -16 -12 147.29 19.60 -1 16 12 109.19 17.10 1 16 -12 167.28 18.40 1 -16 -12 124.89 19.30 -1 16 -12 107.99 20.40 -1 -16 12 168.48 16.70 -1 16 -12 136.49 16.80 1 16 12 154.08 18.70 2 16 -12 27.50 7.80 2 -16 12 33.30 6.80 -2 -16 -12 26.20 8.60 -2 16 12 39.90 8.80 -2 -16 -12 41.40 8.50 2 16 12 42.40 9.50 -2 -16 12 29.80 8.00 -2 16 -12 37.40 8.30 2 -16 -12 24.10 10.00 -2 16 -12 45.00 13.90 -3 -16 -12 19.50 7.40 3 -16 12 31.40 7.30 3 16 -12 30.80 8.60 -3 -16 -12 35.10 8.70 -3 16 12 55.89 10.10 -3 16 -12 24.60 12.60 3 -16 -12 56.99 12.90 3 16 12 25.40 9.00 -3 -16 12 25.00 7.20 4 16 -12 7.30 6.40 -4 16 12 5.00 5.50 -4 -16 -12 -3.00 6.20 4 -16 12 2.40 4.50 -4 -16 12 2.90 5.10 4 -16 -12 10.90 9.80 4 16 12 -10.20 5.80 -4 16 -12 14.40 11.60 5 16 -12 12.40 8.00 5 -16 12 5.10 5.30 -5 16 12 30.50 8.70 -5 -16 -12 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9 9 -15 2.70 5.90 -9 9 15 9.20 8.60 9 -9 15 7.10 7.20 -9 -9 -15 7.20 7.00 -9 9 -15 6.70 10.70 9 -9 -15 2.90 7.90 9 9 15 12.90 6.50 -9 -9 15 1.80 5.90 10 9 -15 8.60 7.80 -10 9 15 21.10 9.40 10 -9 15 15.10 8.60 -10 -9 -15 2.40 8.20 10 -9 -15 6.40 9.20 10 -9 -15 21.60 10.80 -10 -9 15 4.30 7.70 -10 9 -15 11.60 12.90 -11 9 -15 32.50 26.80 11 -9 -15 25.90 13.60 11 -9 -15 19.20 13.00 0 -10 -15 4.80 4.70 0 -10 15 -0.10 3.00 0 10 -15 3.70 2.90 0 -10 -15 -0.20 2.20 0 10 15 -3.30 3.30 0 10 -15 0.90 5.10 1 10 -15 1.70 5.30 -1 -10 -15 5.50 2.90 -1 -10 -15 2.20 3.60 -1 10 15 1.70 3.50 1 10 -15 5.80 3.40 1 -10 15 5.40 3.40 1 -10 -15 4.30 2.10 -1 -10 15 12.20 3.90 1 10 15 -6.20 2.80 -1 10 -15 5.70 3.00 1 -10 -15 9.60 6.00 -1 10 -15 5.20 5.50 2 -10 15 21.80 4.60 2 10 -15 28.20 7.60 2 10 -15 32.80 6.10 -2 10 15 11.20 4.80 -2 -10 -15 11.00 4.10 -2 -10 -15 16.30 4.90 -2 -10 15 19.80 4.70 -2 10 -15 36.40 4.80 -2 10 -15 43.20 10.50 2 -10 -15 21.90 6.60 2 -10 -15 14.60 2.90 2 10 15 16.90 5.60 3 -10 15 34.90 6.30 -3 10 15 47.30 7.90 -3 -10 -15 36.30 6.50 -3 -10 -15 31.80 6.70 3 10 -15 54.69 8.10 3 10 -15 50.69 8.80 -3 10 -15 45.40 6.10 -3 -10 15 43.90 7.30 3 10 15 55.29 8.10 3 -10 -15 43.60 9.10 -3 10 -15 43.50 11.80 -4 10 15 4.40 4.10 -4 -10 -15 6.90 4.00 4 10 -15 4.00 4.40 -4 -10 -15 3.30 3.30 4 10 -15 5.80 4.50 4 -10 15 2.50 3.70 -4 -10 15 4.60 4.10 4 -10 -15 2.00 4.90 4 10 15 1.50 3.90 -4 10 -15 9.80 8.10 5 10 -15 1.80 4.20 5 -10 15 -0.10 4.20 -5 -10 -15 4.80 4.50 -5 -10 -15 3.40 3.40 -5 10 15 5.60 4.90 -5 -10 15 -1.10 3.80 -5 10 -15 16.90 9.90 5 10 15 13.70 5.30 5 -10 -15 4.20 5.70 -6 10 15 2.00 4.60 6 -10 15 5.80 4.80 6 10 -15 -1.90 3.90 -6 -10 -15 5.70 5.20 -6 -10 -15 11.30 4.20 6 10 15 7.20 4.90 6 -10 -15 9.60 7.60 -6 -10 15 -0.40 3.80 -6 10 -15 -0.20 7.00 -7 -10 -15 5.70 5.30 -7 10 15 1.80 5.00 7 10 -15 1.40 4.70 7 -10 15 8.10 5.10 -7 -10 15 6.60 5.20 7 10 15 13.90 6.00 7 -10 -15 6.40 7.10 -7 10 -15 17.70 9.20 8 10 -15 47.20 9.50 -8 -10 -15 47.30 10.20 -8 10 15 33.60 10.10 8 -10 15 45.70 8.90 8 10 15 59.59 10.00 -8 10 -15 55.89 14.50 8 -10 -15 40.60 10.90 -8 -10 15 36.40 8.60 -9 10 15 16.30 9.40 9 -10 15 17.70 7.50 9 10 -15 21.00 7.80 -9 -10 -15 6.10 7.90 9 -10 -15 18.70 9.10 -9 -10 15 7.60 7.30 -9 10 -15 20.30 12.10 9 10 15 17.60 7.40 -10 -10 -15 -4.20 8.10 -10 10 15 -1.60 9.00 10 -10 15 14.70 9.00 10 -10 -15 3.90 9.70 -10 -10 15 6.60 8.50 10 -10 -15 13.30 11.20 -10 10 -15 11.20 12.80 11 -10 -15 3.10 13.00 0 11 -15 7.00 6.90 0 11 -15 3.20 3.10 0 -11 15 6.20 3.40 0 -11 -15 7.50 5.20 0 11 15 -1.20 3.30 0 -11 -15 5.20 2.90 -1 11 15 142.99 15.80 -1 -11 -15 166.68 16.70 -1 -11 -15 140.39 14.20 1 -11 15 148.99 14.80 1 11 -15 156.18 19.30 1 11 -15 121.49 15.60 -1 11 -15 142.49 14.40 -1 -11 15 138.89 14.20 1 -11 -15 131.49 13.00 1 -11 -15 147.59 17.70 -1 11 -15 131.79 18.90 1 11 15 145.39 15.50 2 11 -15 107.79 13.10 -2 -11 -15 87.09 12.70 -2 -11 -15 119.99 12.50 -2 11 15 107.19 13.80 2 11 -15 110.89 15.40 2 -11 15 118.89 12.20 -2 11 -15 122.99 18.10 2 11 15 109.39 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15 30.00 6.30 2 12 15 28.70 7.00 -3 -12 -15 25.50 6.20 -3 12 15 20.20 6.60 -3 -12 -15 29.00 6.20 3 12 -15 20.90 6.30 3 -12 15 14.20 4.90 3 12 -15 30.60 7.90 3 -12 -15 45.20 10.10 -3 12 -15 26.70 5.40 -3 -12 15 21.10 5.90 -3 12 -15 41.70 11.20 3 12 15 38.90 8.00 4 12 -15 1.70 4.10 4 -12 15 1.70 4.10 -4 -12 -15 -0.60 3.60 -4 12 15 -3.10 4.10 -4 -12 -15 2.60 4.70 4 12 15 -4.70 4.00 4 -12 -15 3.50 6.50 -4 -12 15 5.80 4.20 -4 12 -15 8.30 8.60 -5 -12 -15 31.60 7.50 -5 -12 -15 34.80 6.50 5 12 -15 23.70 7.00 5 -12 15 26.10 6.40 -5 12 15 31.70 8.20 -5 -12 15 32.00 7.30 5 -12 -15 30.20 10.00 -5 12 -15 38.50 13.40 5 12 15 38.40 8.10 6 -12 15 67.99 10.50 -6 -12 -15 72.99 11.40 6 12 -15 63.59 11.50 -6 12 15 64.29 12.00 6 -12 -15 84.19 14.70 -6 -12 15 74.19 11.70 -6 12 -15 68.99 16.40 6 12 15 60.49 11.20 7 -12 15 12.50 6.20 -7 12 15 9.70 6.90 -7 -12 -15 4.50 6.40 7 12 -15 9.30 6.50 -7 12 -15 10.50 11.60 -7 -12 15 3.40 6.50 7 12 15 13.50 7.20 7 -12 -15 16.80 9.80 8 12 -15 10.10 7.30 -8 -12 -15 27.80 9.10 8 -12 15 16.40 7.20 -8 12 15 6.80 7.20 8 -12 -15 13.20 10.80 -8 12 -15 19.80 13.20 8 12 15 9.80 7.40 -8 -12 15 12.80 7.30 -9 -12 -15 38.90 11.00 9 -12 15 37.70 11.30 -9 12 15 21.70 10.80 9 -12 -15 50.09 14.50 -9 -12 15 20.40 8.40 -9 12 -15 29.90 16.40 9 12 15 29.50 9.90 0 13 15 121.69 15.90 0 13 -15 108.29 18.00 0 13 -15 147.39 14.60 0 -13 15 123.89 14.50 0 -13 -15 116.19 16.80 1 -13 15 25.50 6.10 1 13 -15 24.10 6.70 -1 13 15 19.20 6.50 -1 -13 -15 31.40 7.90 1 13 -15 23.00 9.10 -1 -13 -15 22.40 5.20 -1 13 -15 31.30 6.00 1 -13 -15 24.80 7.90 -1 13 -15 20.70 9.10 -1 -13 15 20.70 5.40 1 13 15 23.80 6.60 2 13 -15 48.90 10.90 -2 -13 -15 34.80 7.90 -2 -13 -15 41.20 7.20 2 -13 15 50.99 7.80 -2 13 15 36.00 8.20 2 13 -15 43.20 8.50 -2 -13 15 47.30 8.10 -2 13 -15 38.70 11.30 -2 13 -15 39.90 6.90 2 -13 -15 39.60 9.50 2 13 15 38.60 8.30 3 -13 15 23.90 5.80 3 13 -15 27.60 9.40 -3 -13 -15 35.80 7.50 -3 -13 -15 31.60 7.00 3 13 -15 48.80 8.40 -3 13 15 20.60 7.00 3 -13 -15 33.90 10.10 3 13 15 36.60 8.10 -3 13 -15 39.80 12.50 -3 -13 15 26.70 6.50 -4 13 15 11.00 5.90 4 13 -15 10.20 6.00 -4 -13 -15 12.30 4.90 -4 -13 -15 1.40 5.20 4 -13 15 19.20 5.80 4 13 15 3.80 6.10 -4 -13 15 12.60 5.40 4 -13 -15 8.40 7.10 -4 13 -15 35.20 12.60 -5 -13 -15 25.70 7.30 5 13 -15 25.00 7.30 5 -13 15 14.00 5.20 -5 13 15 14.00 6.60 -5 -13 -15 17.10 5.60 5 -13 -15 17.90 8.70 -5 -13 15 23.90 6.90 5 13 15 23.60 7.20 -5 13 -15 12.20 10.00 6 13 -15 12.90 7.00 -6 13 15 30.40 8.90 -6 -13 -15 25.50 7.80 6 -13 15 23.80 7.00 6 13 15 41.40 9.70 -6 13 -15 20.80 12.30 -6 -13 15 15.70 6.70 6 -13 -15 14.20 9.50 7 13 -15 35.50 9.60 -7 -13 -15 39.60 9.70 7 -13 15 12.40 6.80 -7 13 15 30.20 9.90 7 -13 -15 22.00 10.50 -7 13 -15 27.20 13.90 -7 -13 15 15.80 7.60 7 13 15 28.90 9.00 8 13 -15 -1.80 7.70 -8 -13 -15 7.90 8.20 -8 13 15 15.40 9.40 8 -13 15 5.60 6.10 -8 -13 15 1.90 5.70 8 -13 -15 -1.70 8.60 -8 13 -15 -4.20 11.50 8 13 15 3.10 6.60 -9 -13 -15 10.60 10.00 -9 13 15 19.70 10.70 9 13 15 25.20 9.60 0 -14 -15 -2.50 5.30 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78.09 12.50 3 15 -15 96.09 12.90 -3 -15 15 70.69 11.30 3 -15 -15 55.79 13.40 -3 15 -15 65.59 15.90 3 15 15 75.69 12.30 -4 15 15 12.50 6.80 4 15 -15 -1.30 6.00 4 -15 15 0.60 5.00 -4 -15 -15 2.90 5.10 -4 -15 -15 10.20 7.80 -4 15 -15 10.50 11.60 4 -15 -15 11.10 9.00 4 15 15 -0.10 6.80 -4 -15 15 3.40 5.30 -5 15 15 13.90 8.00 5 15 -15 13.40 7.40 5 -15 15 20.80 6.80 -5 -15 -15 7.30 7.40 -5 15 -15 18.60 13.50 5 15 15 28.30 9.80 -5 -15 15 24.40 8.70 5 -15 -15 5.90 8.60 -6 -15 -15 1.60 7.40 6 15 -15 -0.70 7.70 6 -15 15 2.10 5.50 -6 15 15 11.70 7.80 -6 -15 15 0.90 6.80 6 -15 -15 0.90 9.00 -6 15 -15 -2.50 11.60 6 15 15 14.40 9.10 7 -15 15 -3.00 9.70 -7 -15 -15 1.30 8.60 -7 15 15 4.20 8.00 7 15 15 1.20 7.30 -8 -15 -15 4.90 9.90 0 16 15 18.30 7.40 0 16 -15 20.50 10.60 0 -16 15 27.40 6.90 0 -16 -15 11.70 9.50 0 16 -15 26.60 7.30 1 16 -15 27.80 11.30 1 16 -15 30.40 7.80 -1 16 15 15.80 7.30 1 -16 15 25.80 6.40 -1 -16 -15 15.40 7.50 1 -16 -15 18.60 9.80 -1 16 -15 11.80 10.70 1 16 15 28.00 8.40 -1 16 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113.39 11.60 2 0 -22 111.69 10.90 2 0 -22 80.29 12.90 3 0 22 156.38 12.40 3 0 -22 108.99 11.70 3 0 -22 92.29 14.20 -3 0 -22 108.79 14.60 -3 0 -22 121.19 11.80 3 0 22 124.29 12.70 -3 0 22 137.89 11.90 3 0 -22 123.99 12.90 4 0 22 20.10 3.30 -4 0 22 19.10 3.70 4 0 -22 19.90 4.50 4 0 -22 7.00 5.10 -4 0 -22 17.00 6.00 4 0 22 25.00 5.00 5 0 -22 194.28 20.60 5 0 22 255.57 21.60 -5 0 22 209.58 20.20 5 0 -22 236.48 23.60 -5 0 -22 209.48 22.60 -6 0 -22 7.80 5.80 6 0 22 7.00 4.10 6 0 -22 15.30 4.50 -6 0 22 6.30 3.30 6 0 -22 4.60 5.20 -7 0 22 82.99 10.80 7 0 -22 67.89 13.10 7 0 22 100.29 12.70 -7 0 -22 115.19 15.80 7 0 -22 90.89 11.10 8 0 -22 7.20 6.20 -8 0 -22 -6.60 5.40 8 0 22 6.40 5.10 9 0 22 3.80 5.10 9 0 -22 -2.30 6.10 -9 0 -22 -8.30 6.50 10 0 22 3.00 5.40 10 0 -22 -7.60 6.80 -10 0 -22 4.90 9.80 0 1 -22 145.99 15.40 0 1 -22 142.69 15.00 0 -1 22 160.18 13.80 0 -1 -22 157.38 15.40 0 1 22 130.69 13.30 0 1 22 169.58 15.40 -1 1 22 8.60 1.80 1 -1 22 9.10 2.70 -1 1 22 6.50 2.20 1 1 -22 8.00 3.70 1 1 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28.10 9.00 8 2 22 24.60 7.50 -8 -2 22 41.90 7.60 -9 -2 -22 19.60 7.10 9 2 -22 10.70 7.60 9 -2 22 24.70 7.40 -9 -2 -22 17.90 9.20 9 -2 -22 9.80 7.80 9 2 22 19.80 7.40 -9 -2 22 15.20 6.10 -9 2 -22 11.20 9.20 -10 -2 -22 8.60 6.90 -10 -2 -22 -0.10 9.00 10 2 -22 0.90 7.30 10 -2 22 -3.30 5.50 10 2 22 6.50 6.30 10 -2 -22 1.60 7.60 -10 2 -22 0.60 9.70 11 2 22 14.90 13.60 -11 2 -22 26.00 15.60 0 3 22 118.49 13.10 0 3 22 131.59 10.80 0 -3 -22 121.29 13.10 0 3 22 110.89 11.10 0 3 -22 119.19 12.60 0 3 -22 115.29 14.20 0 -3 22 117.69 11.80 1 3 -22 135.89 14.50 -1 3 22 133.99 14.40 1 3 -22 137.59 14.00 -1 3 22 132.99 11.50 -1 -3 -22 129.09 14.10 -1 3 22 126.89 11.40 1 -3 22 136.79 13.00 1 3 22 138.69 13.90 1 3 22 132.69 12.70 -1 -3 22 140.09 12.80 1 -3 -22 146.69 14.40 -1 3 -22 114.49 15.20 -1 3 -22 137.79 13.20 1 3 22 124.29 12.30 2 -3 22 6.60 2.80 2 3 -22 5.50 3.90 2 3 -22 3.20 3.70 -2 -3 -22 -0.80 3.10 -2 3 22 7.90 4.60 -2 3 -22 4.90 4.50 2 -3 -22 5.00 3.70 -2 3 -22 1.90 1.80 2 3 22 3.50 2.80 -2 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17.00 5.00 5 9 -22 10.70 6.20 -5 -9 -22 15.30 5.40 -5 -9 -22 18.30 6.10 5 -9 22 15.80 6.00 -5 9 22 19.00 7.40 5 9 22 22.70 6.40 -5 9 -22 17.50 10.10 -5 -9 22 16.80 5.70 5 -9 -22 15.60 8.10 -6 9 22 34.10 9.70 -6 -9 -22 62.59 10.30 6 -9 22 48.10 9.10 6 9 -22 62.09 10.90 -6 -9 -22 52.09 9.50 -6 9 -22 62.69 16.30 -6 -9 22 58.09 9.60 6 9 22 52.59 9.30 6 -9 -22 58.89 12.20 7 -9 22 -2.10 5.50 -7 -9 -22 8.40 5.80 7 9 -22 1.50 5.80 -7 -9 -22 11.00 7.10 -7 9 22 0.70 6.40 7 -9 -22 12.20 8.40 -7 9 -22 19.90 11.80 7 9 22 2.40 5.60 -7 -9 22 6.10 5.70 -8 -9 -22 32.40 9.30 8 -9 22 27.70 7.90 -8 9 22 38.40 11.10 8 9 -22 35.60 9.60 -8 9 -22 9.70 11.20 -8 -9 22 29.10 7.90 8 -9 -22 17.60 8.40 -9 -9 -22 3.20 8.50 -9 9 22 4.10 8.70 9 -9 -22 16.90 12.80 -9 -9 22 6.70 6.80 -9 9 -22 14.90 13.50 9 -9 -22 -8.70 8.30 -10 -9 -22 13.20 12.20 10 -9 -22 31.80 13.20 0 -10 -22 4.20 5.30 0 -10 22 1.20 3.70 0 10 -22 6.20 3.80 0 10 22 10.60 5.60 0 10 -22 -4.60 6.10 -1 10 22 9.70 5.20 1 10 -22 9.40 6.80 1 -10 22 1.10 3.30 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22 19.60 5.50 -1 -12 -22 25.10 7.70 -1 12 22 29.80 7.90 1 -12 22 16.40 5.70 1 12 -22 37.70 7.80 1 12 -22 44.20 11.60 1 -12 -22 21.30 7.10 -1 -12 22 20.20 5.40 1 12 22 15.20 6.20 -1 12 -22 41.80 11.90 2 -12 22 14.70 4.70 2 12 -22 13.80 8.70 -2 -12 -22 7.80 5.20 -2 12 22 24.20 7.20 2 12 -22 6.90 4.90 2 -12 -22 26.70 8.70 -2 -12 22 10.60 5.20 -2 12 -22 34.60 12.00 2 12 22 7.20 5.40 -3 12 22 58.09 10.20 3 -12 22 27.10 6.50 3 12 -22 31.80 8.00 -3 -12 -22 57.09 9.30 -3 -12 22 46.10 8.60 -3 12 -22 38.00 13.50 3 -12 -22 43.20 10.70 3 12 22 65.09 10.50 4 12 -22 28.10 7.90 4 -12 22 27.00 6.60 -4 -12 -22 19.80 6.80 -4 12 22 32.20 9.60 -4 12 -22 23.00 12.10 -4 -12 22 24.90 7.10 4 -12 -22 21.10 9.60 4 12 22 31.70 8.40 5 -12 22 14.40 5.70 -5 12 22 24.70 8.50 5 12 -22 12.50 6.70 -5 -12 -22 2.70 5.30 5 -12 -22 4.00 7.50 5 12 22 7.40 7.10 -5 -12 22 7.80 5.80 -5 12 -22 -0.10 10.40 6 12 -22 4.20 7.30 -6 12 22 -8.80 5.50 -6 -12 -22 -2.90 5.00 6 -12 22 3.70 5.20 6 12 22 3.20 6.80 6 -12 -22 -6.40 7.90 -6 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14 22 -4.10 7.10 -4 -14 22 4.60 6.10 -4 14 -22 15.30 14.60 5 -14 22 13.50 6.80 -5 14 22 35.30 11.00 5 14 -22 15.30 8.60 -5 -14 -22 21.10 7.70 5 -14 -22 14.60 10.10 -5 14 -22 31.60 14.70 -5 -14 22 7.40 6.80 5 14 22 42.10 10.40 6 14 -22 5.80 8.70 6 14 22 -2.50 6.90 7 14 22 14.40 9.80 0 -15 22 15.40 6.20 0 -15 -22 15.70 7.50 0 15 22 13.30 7.50 0 15 -22 13.90 12.00 1 -15 22 54.99 9.90 1 15 -22 64.19 10.80 -1 15 22 70.49 12.40 1 15 -22 66.49 16.30 -1 -15 -22 41.10 10.80 1 15 22 51.79 10.70 -1 15 -22 46.50 15.60 1 -15 -22 55.79 12.30 -1 -15 22 59.79 10.40 -2 -15 -22 2.90 6.60 2 -15 22 5.00 6.20 -2 15 22 10.10 7.30 2 15 -22 16.20 7.40 -2 -15 22 14.80 6.00 2 -15 -22 4.80 9.00 -2 15 -22 20.10 13.70 2 15 22 9.20 7.30 -3 15 22 18.50 8.40 -3 -15 -22 11.10 7.50 3 -15 22 5.00 5.90 3 15 -22 3.00 7.40 3 15 22 9.40 8.70 -3 -15 22 7.50 6.20 3 -15 -22 5.20 9.80 -3 15 -22 0.30 11.80 -4 -15 -22 26.40 8.60 -4 15 22 23.00 10.20 4 15 -22 13.10 9.50 4 -15 22 14.00 8.30 -4 15 -22 16.60 14.60 -4 -15 22 22.90 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4 -23 18.10 9.80 9 -4 23 6.90 6.20 -9 -4 -23 4.10 8.00 -9 -4 -23 6.40 6.80 9 4 -23 9.70 7.60 9 -4 -23 5.60 8.10 -9 -4 23 15.00 7.10 9 -4 -23 2.40 7.30 -9 4 -23 21.60 11.40 -10 -4 -23 -5.50 5.90 10 4 -23 3.90 7.80 10 -4 23 7.50 6.30 10 4 23 -7.30 5.50 10 -4 -23 2.40 8.10 -10 4 -23 -15.70 10.20 -11 4 -23 2.80 14.20 0 -5 -23 101.99 13.30 0 -5 23 117.19 11.30 0 5 -23 121.39 15.00 0 5 23 119.19 13.70 0 5 -23 101.49 11.60 1 5 -23 64.39 10.50 1 -5 23 73.79 9.30 -1 5 23 90.09 11.30 -1 -5 -23 99.19 11.60 1 5 -23 75.89 9.80 -1 5 -23 88.69 12.80 1 5 23 89.59 11.00 -1 -5 23 92.79 9.50 -1 5 -23 86.09 9.30 1 -5 -23 88.29 11.40 1 5 23 83.79 8.50 2 5 -23 164.78 16.10 -2 -5 -23 122.09 15.20 2 -5 23 155.38 14.80 2 5 -23 155.98 16.30 -2 5 23 147.49 17.40 2 -5 -23 159.98 16.50 -2 5 -23 149.59 14.30 2 5 23 160.88 16.00 -2 -5 23 151.28 15.00 2 5 23 162.98 14.60 -2 5 -23 148.89 19.40 -3 5 23 34.50 7.70 3 5 -23 25.20 6.50 -3 -5 -23 27.10 6.20 3 5 -23 26.20 6.20 3 -5 23 29.10 5.70 3 -5 -23 32.50 6.80 3 5 23 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5.80 2.70 2 -2 -28 0.00 4.20 -2 -2 28 8.10 2.80 -2 2 -28 -1.80 5.00 -3 2 28 12.90 5.80 -3 -2 -28 6.10 5.10 3 2 -28 7.30 5.40 3 2 -28 7.70 5.30 3 -2 28 5.90 3.60 3 2 28 2.70 3.10 -3 -2 28 5.40 2.70 3 -2 -28 -2.80 3.70 3 -2 -28 5.80 5.50 -3 2 -28 1.60 5.40 3 2 28 7.10 3.90 4 2 -28 17.50 6.50 -4 2 28 7.30 6.30 4 -2 28 15.80 4.80 4 2 -28 13.80 6.00 -4 -2 -28 12.90 6.40 -4 -2 28 17.70 4.20 4 -2 -28 9.40 6.50 4 -2 -28 13.70 5.40 -4 2 -28 21.70 7.60 4 2 28 20.90 5.10 -5 -2 -28 38.50 9.10 5 2 -28 21.80 6.80 5 -2 28 38.20 7.00 5 2 -28 28.40 8.20 5 2 28 29.80 6.50 5 -2 -28 25.50 7.70 -5 2 -28 27.70 9.30 5 -2 -28 23.60 6.70 6 2 -28 5.70 5.70 6 2 -28 0.50 5.00 6 -2 28 -1.70 4.90 -6 -2 -28 2.80 6.20 -6 2 -28 -10.70 6.70 6 -2 -28 11.10 5.50 6 -2 -28 11.40 6.60 6 2 28 5.00 4.90 7 2 -28 3.30 6.80 7 -2 28 3.30 5.90 -7 -2 -28 0.60 7.50 -7 2 -28 -0.30 8.60 7 2 28 2.80 5.40 7 -2 -28 0.90 6.40 7 -2 -28 -0.60 5.40 8 2 -28 33.60 10.50 -8 -2 -28 28.40 10.90 8 -2 28 6.80 7.20 8 2 28 13.30 7.10 8 -2 -28 17.30 9.20 -8 2 -28 21.50 11.90 -9 -2 -28 5.40 11.00 9 -2 28 13.70 8.30 9 2 -28 -3.50 8.40 9 2 28 9.70 8.00 -9 2 -28 5.60 12.90 -10 -2 -28 35.90 15.80 0 3 -28 0.90 4.20 0 3 -28 0.90 3.90 0 -3 28 3.30 3.00 0 -3 -28 -1.40 4.30 0 3 28 -1.30 3.80 1 -3 28 7.10 3.10 1 3 -28 6.90 4.60 1 3 -28 10.80 5.50 -1 3 28 5.20 4.70 -1 -3 -28 4.70 4.60 -1 3 -28 12.10 4.10 -1 -3 28 14.40 3.40 1 3 28 11.80 5.30 1 -3 -28 14.50 5.10 -1 3 -28 8.80 6.20 2 -3 28 9.70 3.50 -2 3 28 20.70 7.00 2 3 -28 4.30 4.60 -2 -3 -28 3.80 4.60 2 3 -28 13.40 6.00 2 -3 -28 10.60 5.00 2 3 28 13.70 3.50 -2 3 -28 14.90 6.30 2 3 28 19.90 5.60 -2 -3 28 13.60 3.50 3 3 -28 13.80 6.00 3 3 -28 10.10 4.90 -3 3 28 9.80 6.30 3 -3 28 6.10 4.10 -3 -3 -28 7.10 4.80 3 -3 -28 3.80 4.50 -3 -3 28 5.40 3.10 -3 3 -28 -1.30 5.10 3 3 28 10.50 3.50 3 3 28 4.90 4.30 -4 -3 -28 70.29 11.20 4 -3 28 49.90 9.00 4 3 -28 80.59 11.90 4 3 -28 79.49 10.90 -4 3 28 78.39 12.70 -4 3 -28 61.09 12.20 4 3 28 65.29 8.90 -4 -3 28 68.79 8.60 4 -3 -28 56.59 11.30 4 -3 -28 61.69 10.30 5 3 -28 13.30 5.60 -5 3 28 10.10 6.50 -5 -3 -28 9.50 5.90 5 -3 28 8.50 5.00 5 3 -28 9.20 6.50 -5 -3 28 3.40 4.30 5 -3 -28 8.50 5.90 5 -3 -28 12.30 6.80 5 3 28 1.90 4.60 -5 3 -28 14.60 8.90 6 3 -28 -7.80 5.60 -6 -3 -28 -3.60 5.90 6 -3 28 -5.00 4.50 6 3 28 4.50 4.70 6 -3 -28 5.10 5.30 -6 3 -28 -0.20 8.40 6 -3 -28 -1.60 5.60 -7 -3 -28 1.40 6.50 7 3 -28 3.60 7.10 7 -3 28 14.80 6.60 7 -3 -28 13.10 6.50 7 3 28 2.90 5.60 7 -3 -28 20.00 8.90 -7 3 -28 3.60 7.90 8 -3 28 37.30 9.40 -8 -3 -28 46.30 11.40 8 3 -28 28.30 10.10 8 -3 -28 47.80 10.00 8 -3 -28 26.30 10.60 -8 3 -28 66.49 15.70 8 3 28 39.60 9.50 -9 -3 -28 15.20 11.20 9 -3 28 19.20 9.10 -9 3 -28 -7.30 12.10 9 3 28 1.70 7.00 0 4 28 10.50 5.60 0 -4 28 16.20 4.00 0 -4 -28 17.30 5.80 0 4 -28 19.70 7.10 0 4 -28 8.00 3.90 -1 4 28 35.70 8.30 -1 -4 -28 34.80 7.80 1 4 -28 37.40 8.70 1 -4 28 34.60 5.60 1 4 -28 38.90 7.30 1 -4 -28 40.10 7.80 1 4 28 29.00 7.10 -1 4 -28 24.50 8.30 -1 -4 28 31.00 5.40 -1 4 -28 41.00 5.90 2 -4 28 118.09 12.20 2 4 -28 108.69 14.50 2 4 -28 132.39 14.70 -2 -4 -28 87.39 13.60 -2 4 28 116.39 15.90 -2 4 -28 102.19 15.30 2 -4 -28 98.89 13.30 -2 -4 28 113.39 11.10 2 4 28 96.69 13.30 3 4 -28 8.60 5.40 -3 4 28 14.80 7.20 3 -4 28 10.80 4.10 3 4 -28 14.80 6.10 -3 -4 -28 4.80 5.00 3 -4 -28 18.90 6.40 -3 -4 28 11.60 3.80 3 4 28 13.70 4.80 -3 4 -28 10.40 6.90 3 4 28 11.40 4.20 4 -4 28 -0.30 3.70 4 4 -28 0.70 4.60 -4 -4 -28 1.50 4.30 4 4 -28 -0.90 4.30 -4 4 28 6.30 6.70 4 -4 -28 13.20 5.60 -4 4 -28 10.70 8.30 4 4 28 4.90 3.90 -4 -4 28 3.60 3.40 -5 4 28 30.90 9.00 5 4 -28 8.40 6.70 -5 -4 -28 19.00 6.50 5 -4 28 12.50 5.40 5 4 -28 17.40 6.00 5 -4 -28 18.60 8.30 -5 -4 28 15.90 4.90 -5 4 -28 16.90 8.60 5 4 28 21.20 5.30 5 -4 -28 13.20 6.50 6 -4 28 2.00 4.70 -6 -4 -28 3.70 6.40 6 4 -28 8.70 6.10 -6 4 28 0.90 6.40 6 4 28 3.10 4.90 -6 4 -28 6.10 9.10 6 -4 -28 -2.10 6.10 6 -4 -28 5.20 6.20 7 4 -28 10.30 7.10 7 -4 28 19.30 6.80 -7 -4 -28 5.70 7.40 -7 4 -28 -6.10 8.50 7 -4 -28 11.50 9.00 7 4 28 20.20 6.90 7 -4 -28 25.50 8.00 8 4 -28 -0.70 7.10 8 -4 28 -3.80 5.70 -8 -4 -28 -0.30 8.80 8 4 28 -1.10 5.90 8 -4 -28 2.90 6.60 8 -4 -28 -10.80 7.10 -8 4 -28 15.90 12.10 -9 -4 -28 9.90 10.70 9 -4 28 2.70 8.40 -9 4 -28 -7.70 12.60 9 4 28 2.80 7.40 0 -5 -28 84.39 12.00 0 5 -28 68.29 13.00 0 5 28 111.59 13.50 0 5 -28 81.69 10.70 0 -5 28 100.39 10.70 1 -5 28 79.49 9.50 -1 5 28 85.09 12.50 1 5 -28 58.29 9.50 -1 -5 -28 91.89 11.70 1 5 -28 64.19 11.50 -1 -5 28 79.79 9.10 1 5 28 78.59 11.20 -1 5 -28 91.59 13.90 1 -5 -28 55.99 10.10 2 5 -28 25.90 7.50 -2 5 28 14.10 6.90 2 5 -28 26.60 6.50 2 -5 28 32.30 5.60 -2 -5 -28 26.10 6.60 -2 -5 28 28.80 5.30 -2 5 -28 34.70 9.80 2 5 28 31.00 7.10 2 -5 -28 29.20 7.60 -3 5 28 26.60 7.60 3 5 -28 21.10 6.90 -3 -5 -28 21.60 6.40 3 -5 28 13.90 4.90 3 5 -28 25.50 7.10 3 5 28 18.70 5.90 3 -5 -28 23.70 6.70 -3 -5 28 34.60 5.70 -3 5 -28 23.90 9.50 -4 5 28 4.60 6.80 -4 -5 -28 5.60 4.80 4 -5 28 -2.60 3.90 4 5 -28 6.10 5.30 4 5 -28 1.70 4.80 4 5 28 12.80 4.80 -4 5 -28 6.20 7.80 4 -5 -28 1.40 4.90 -4 -5 28 1.90 3.60 5 5 -28 21.80 7.10 -5 -5 -28 20.90 6.80 5 5 -28 28.10 8.60 5 -5 28 32.80 7.00 -5 5 28 26.80 8.80 5 5 28 27.70 6.30 -5 -5 28 29.30 6.60 5 -5 -28 41.00 8.70 -5 5 -28 35.50 11.50 -6 5 28 4.50 6.60 6 -5 28 1.20 5.00 6 5 -28 6.00 6.40 -6 -5 -28 -1.50 5.80 6 5 28 3.30 4.50 6 -5 -28 1.90 5.40 6 -5 -28 4.80 6.90 -6 -5 28 2.70 4.30 -6 5 -28 9.70 9.30 -7 5 28 7.50 8.40 -7 -5 -28 14.80 7.60 7 -5 28 19.60 6.80 7 5 -28 10.80 7.50 7 -5 -28 19.70 9.80 7 -5 -28 11.90 6.80 7 5 28 19.80 7.10 -7 5 -28 23.90 11.80 8 -5 28 -0.90 5.50 8 5 -28 4.20 7.90 -8 -5 -28 -3.20 8.10 8 -5 -28 1.40 7.80 8 -5 -28 2.50 6.80 8 5 28 4.20 6.80 -8 5 -28 4.20 11.80 -9 -5 -28 10.10 8.60 -9 -5 -28 17.30 11.50 9 5 28 17.60 9.10 0 -6 28 3.50 3.50 0 6 28 -1.20 4.90 0 6 -28 0.10 3.10 0 -6 -28 7.70 5.20 0 6 -28 4.50 6.20 1 6 -28 55.99 10.60 1 6 -28 44.60 7.90 -1 -6 -28 53.49 9.00 -1 6 28 37.60 9.20 1 -6 28 53.69 7.60 -1 6 -28 50.89 10.90 1 6 28 36.20 7.90 1 -6 -28 38.90 8.30 -1 -6 28 49.50 6.90 -2 6 28 50.89 10.00 2 6 -28 51.29 8.70 2 6 -28 48.10 9.90 -2 -6 -28 34.50 8.00 2 -6 28 53.79 7.40 2 -6 -28 42.20 8.40 -2 -6 28 45.90 6.80 2 6 28 47.20 8.60 -2 6 -28 46.40 11.00 -3 6 28 -1.00 4.90 3 6 -28 -2.30 4.50 3 6 -28 6.20 5.90 3 -6 28 -2.20 3.20 -3 -6 -28 6.30 4.80 -3 -6 28 3.10 3.60 3 6 28 7.90 4.80 3 -6 -28 -3.10 5.00 -3 6 -28 -3.60 7.00 4 6 -28 13.50 6.20 -4 -6 -28 -2.60 4.30 -4 6 28 6.90 6.50 4 6 -28 0.00 5.20 4 -6 28 0.00 4.20 -4 6 -28 15.70 9.30 4 6 28 5.50 4.60 -4 -6 28 0.00 3.40 4 -6 -28 11.20 5.90 5 -6 28 15.20 5.80 5 6 -28 2.40 5.60 -5 6 28 3.00 6.50 -5 -6 -28 7.80 6.20 -5 6 -28 14.40 10.20 5 -6 -28 13.00 7.00 -5 -6 28 14.80 5.30 -6 6 28 26.80 9.20 6 6 -28 18.90 8.20 6 -6 28 9.60 6.60 -6 -6 -28 26.00 8.50 6 -6 -28 27.10 8.30 -6 6 -28 17.70 9.80 -6 -6 28 22.90 6.60 6 6 28 16.60 7.50 -7 -6 -28 9.70 6.90 7 6 -28 12.80 7.70 -7 6 28 19.30 9.00 -7 -6 -28 26.30 8.90 7 -6 28 18.40 6.70 7 -6 -28 19.40 10.40 -7 6 -28 13.70 11.40 7 -6 -28 39.40 9.20 7 6 28 18.20 6.90 -7 -6 28 22.60 7.20 -8 -6 -28 13.60 7.50 8 6 -28 5.90 7.50 -8 -6 -28 8.50 8.70 8 -6 28 12.60 7.20 -8 6 28 11.50 9.60 8 6 28 26.30 7.70 8 -6 -28 1.80 7.80 8 -6 -28 -4.30 9.70 -8 6 -28 10.60 12.60 -9 -6 -28 9.20 8.50 9 6 28 12.10 7.70 0 7 28 5.10 5.10 0 7 -28 2.30 6.20 0 -7 -28 5.60 4.40 0 -7 28 12.00 4.50 0 7 -28 4.60 3.80 -1 7 28 0.60 4.70 1 -7 28 2.60 3.30 1 7 -28 3.80 6.20 -1 -7 -28 -2.80 4.30 1 7 -28 0.20 4.20 1 7 28 7.40 5.30 -1 -7 28 8.30 3.90 -1 7 -28 -6.40 7.10 1 -7 -28 6.40 4.90 -2 7 28 17.20 6.70 2 -7 28 17.80 4.90 2 7 -28 17.50 7.60 2 7 -28 19.30 6.20 -2 -7 -28 23.70 6.90 -2 7 -28 12.70 8.50 2 -7 -28 13.50 6.20 2 7 28 22.40 6.20 -2 -7 28 14.10 4.50 -3 7 28 28.90 8.50 3 7 -28 18.20 6.80 3 -7 28 24.80 6.30 3 7 -28 35.10 8.80 -3 -7 -28 29.70 7.20 3 7 28 32.60 7.50 -3 7 -28 40.30 11.60 -3 -7 28 32.30 6.50 3 -7 -28 28.30 7.50 -4 -7 -28 78.79 11.70 4 -7 28 84.49 10.90 4 7 -28 53.09 10.80 -4 7 28 88.19 13.80 4 7 -28 75.99 12.50 4 7 28 90.29 11.80 -4 -7 28 77.09 10.60 4 -7 -28 71.19 12.40 -4 7 -28 80.09 17.30 5 -7 28 1.10 5.00 -5 -7 -28 4.80 6.00 5 7 -28 2.30 5.90 -5 7 28 16.10 8.10 -5 -7 28 3.50 4.80 -5 7 -28 12.60 9.60 5 -7 -28 4.20 6.40 -6 7 28 0.30 6.50 6 7 -28 -3.20 6.30 -6 -7 -28 3.70 6.30 6 -7 28 4.30 6.00 -6 -7 28 6.30 5.00 6 -7 -28 -5.90 5.80 -6 7 -28 1.60 9.00 -7 7 28 -11.10 6.20 7 7 -28 -2.40 5.90 7 -7 28 7.70 6.60 -7 -7 -28 6.40 6.40 7 -7 -28 -1.90 6.20 -7 7 -28 -5.50 11.00 -7 -7 28 2.00 5.40 7 -7 -28 3.00 8.50 8 -7 28 1.00 5.90 8 7 -28 4.60 8.30 -8 -7 -28 10.00 9.10 -8 7 -28 4.50 16.50 8 -7 -28 -3.20 8.10 -9 -7 -28 2.20 14.80 9 -7 -28 12.90 10.10 0 -8 28 3.90 4.10 0 8 28 7.30 5.80 0 8 -28 1.90 8.10 0 -8 -28 2.80 5.30 1 -8 28 31.40 6.10 1 8 -28 29.80 6.70 -1 8 28 31.60 8.20 -1 -8 -28 29.60 7.50 1 8 -28 33.00 10.30 -1 -8 28 33.10 6.30 1 8 28 23.70 7.30 1 -8 -28 22.90 7.50 -1 8 -28 28.00 11.30 -2 8 28 4.50 6.40 2 8 -28 1.80 4.60 2 -8 28 4.90 4.10 2 8 -28 5.00 8.90 -2 -8 -28 4.80 5.30 -2 -8 28 8.70 4.30 2 -8 -28 1.70 5.00 -2 8 -28 2.00 9.50 2 8 28 7.20 5.40 3 8 -28 55.59 12.80 3 8 -28 31.50 8.30 3 -8 28 60.59 8.70 -3 8 28 51.29 11.60 -3 -8 -28 43.60 8.60 -3 -8 28 54.19 8.80 3 -8 -28 49.10 10.60 3 8 28 72.09 10.40 -3 8 -28 53.19 13.60 -4 8 28 4.30 6.70 4 -8 28 0.40 4.20 4 8 -28 1.90 4.90 -4 -8 -28 7.90 5.00 4 -8 -28 13.10 6.10 4 8 28 -3.70 4.90 -4 -8 28 6.70 4.40 -4 8 -28 0.60 8.60 5 8 -28 2.80 6.40 -5 8 28 5.40 7.40 -5 -8 -28 3.70 6.30 5 -8 28 8.10 5.70 5 -8 -28 7.90 7.40 -5 8 -28 16.80 10.60 -5 -8 28 3.80 4.90 -6 8 28 62.59 13.00 6 8 -28 39.30 10.40 -6 -8 -28 44.40 9.80 6 -8 28 47.70 9.60 -6 8 -28 55.29 16.20 -6 -8 28 47.50 9.40 6 -8 -28 48.60 12.00 -7 8 28 -2.00 7.60 7 -8 28 6.10 6.60 -7 -8 -28 2.10 7.30 7 8 -28 8.30 8.30 7 -8 -28 -1.20 7.50 -7 -8 28 -3.00 6.30 -7 8 -28 -2.90 11.40 -8 -8 -28 -1.60 8.90 8 -8 -28 -11.70 7.70 -8 -8 28 6.90 7.40 9 -8 -28 3.90 13.30 0 -9 -28 4.40 5.60 0 9 -28 12.90 9.70 0 -9 28 7.10 4.40 0 9 28 4.70 6.00 1 9 -28 53.59 12.80 1 9 -28 29.20 7.00 -1 9 28 60.39 10.70 -1 -9 -28 57.19 10.00 1 -9 28 44.20 7.40 1 9 28 39.00 9.10 1 -9 -28 51.49 9.90 -1 -9 28 51.99 8.30 -1 9 -28 62.99 14.30 2 -9 28 5.30 4.90 2 9 -28 11.70 5.70 2 9 -28 7.90 9.10 -2 9 28 3.60 6.20 -2 -9 -28 -0.70 4.70 2 -9 -28 7.90 5.70 2 9 28 4.40 5.30 -2 9 -28 -5.20 7.90 -2 -9 28 0.60 3.90 3 9 -28 5.80 8.80 -3 9 28 13.60 8.00 -3 -9 -28 16.80 6.50 3 -9 28 2.40 4.00 3 9 -28 4.50 5.40 -3 -9 28 -0.50 3.70 3 9 28 14.40 6.30 3 -9 -28 19.50 7.70 -3 9 -28 10.10 9.30 -4 9 28 5.70 7.00 4 9 -28 10.70 6.60 -4 -9 -28 7.10 6.50 4 -9 28 10.80 5.80 -4 -9 28 3.90 4.60 -4 9 -28 13.60 10.20 4 9 28 9.50 6.50 4 -9 -28 0.60 5.90 -5 -9 -28 20.30 6.80 5 -9 28 3.00 5.40 5 9 -28 14.30 7.60 -5 9 28 13.40 8.30 5 9 28 17.70 8.30 -5 9 -28 35.40 12.50 5 -9 -28 11.30 8.60 -5 -9 28 2.40 5.40 6 9 -28 9.70 8.60 6 -9 28 1.00 5.10 -6 9 28 12.20 8.50 -6 -9 -28 3.90 6.40 -6 -9 28 0.30 5.70 -6 9 -28 -2.90 11.80 6 -9 -28 -6.10 8.20 7 9 -28 3.60 8.90 -7 -9 -28 4.20 7.40 7 -9 28 -6.60 5.20 -7 -9 28 13.60 7.20 7 -9 -28 0.00 8.70 8 -9 -28 -4.30 10.20 -8 -9 28 10.50 8.30 0 -10 -28 -3.00 5.10 0 10 28 -2.50 5.30 0 10 -28 3.30 8.80 0 -10 28 1.60 4.20 1 -10 28 27.20 6.10 -1 10 28 28.50 8.40 -1 -10 -28 24.70 7.70 1 10 -28 36.70 11.70 1 10 28 32.10 8.40 -1 -10 28 31.60 6.80 -1 10 -28 27.70 11.80 1 -10 -28 20.80 7.80 2 10 -28 20.20 6.90 2 10 -28 26.70 11.50 -2 10 28 29.40 8.60 2 -10 28 28.70 6.30 -2 -10 -28 19.80 6.80 2 10 28 45.70 9.50 -2 -10 28 26.40 6.60 -2 10 -28 33.90 13.80 2 -10 -28 44.50 9.80 3 10 -28 -4.70 4.80 -3 10 28 -6.50 5.70 -3 -10 -28 -4.40 5.00 3 -10 28 -2.40 3.60 3 10 28 -4.90 5.60 3 -10 -28 6.70 6.30 -3 -10 28 -3.70 4.40 -3 10 -28 -5.30 9.50 -4 10 28 -0.30 7.40 4 -10 28 0.50 4.50 -4 -10 -28 11.20 6.40 4 10 -28 4.70 6.50 4 10 28 -0.60 6.30 -4 -10 28 7.10 5.20 4 -10 -28 -8.70 6.90 -4 10 -28 23.00 13.00 -5 -10 -28 15.80 7.30 5 10 -28 19.40 8.40 5 -10 28 10.80 5.80 -5 10 28 5.00 8.60 5 10 28 11.10 7.60 -5 -10 28 16.70 6.60 5 -10 -28 9.00 7.90 -5 10 -28 5.90 12.20 6 -10 28 13.80 6.60 -6 -10 -28 15.10 7.80 -6 10 28 22.00 10.30 6 10 -28 9.00 7.30 -6 -10 28 15.50 7.50 -6 10 -28 10.70 15.90 6 -10 -28 22.30 10.00 -7 -10 -28 20.10 8.40 7 10 -28 -4.20 10.30 7 -10 -28 1.90 11.20 -7 -10 28 4.90 8.00 -8 -10 28 16.00 10.20 0 -11 -28 1.20 5.50 0 11 -28 7.00 10.20 0 11 28 4.30 6.60 0 -11 28 4.40 5.10 -1 -11 -28 16.30 7.40 1 11 -28 19.10 10.50 1 -11 28 17.30 6.40 -1 11 28 26.30 8.20 -1 -11 28 23.10 6.60 1 11 28 25.60 8.00 1 -11 -28 17.10 7.10 -1 11 -28 21.60 11.40 -2 11 28 13.10 7.70 2 11 -28 2.50 5.40 2 11 -28 18.50 9.90 2 -11 28 4.10 4.30 -2 -11 -28 -0.20 5.90 2 -11 -28 6.30 6.40 2 11 28 15.50 6.90 -2 -11 28 6.50 5.20 -2 11 -28 -4.40 9.90 -3 -11 -28 -3.70 6.00 3 11 -28 -8.50 5.20 3 -11 28 6.10 5.50 -3 11 28 -6.90 5.30 3 11 28 -6.40 5.90 -3 -11 28 -4.70 4.90 -3 11 -28 2.70 8.80 3 -11 -28 -1.80 6.40 -4 -11 -28 36.40 9.50 -4 11 28 37.00 11.30 4 11 -28 41.50 9.60 4 -11 28 37.10 8.40 -4 -11 28 38.40 8.80 4 -11 -28 45.20 11.70 -4 11 -28 32.50 14.30 4 11 28 25.70 8.90 5 -11 28 4.00 5.90 5 11 -28 4.20 6.40 -5 11 28 -4.80 6.40 -5 -11 -28 0.70 6.50 -5 11 -28 2.80 13.90 5 11 28 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-2.9904 0.0018 0 4 9 2.3066 -0.0182 0 4 10 -4.5743 -0.0044 0 4 11 -0.0237 0.0114 0 4 12 11.4674 0.0053 0 4 13 -0.1024 0.0001 0 4 14 -11.3642 -0.0030 0 4 15 -0.6752 -0.0013 0 4 16 5.4904 0.0019 0 4 17 0.6789 -0.0058 0 4 18 1.3430 -0.0020 0 4 19 0.1348 0.0117 0 4 20 -5.5071 0.0003 0 4 21 -0.7890 -0.0111 0 4 22 6.0645 0.0016 0 4 23 1.0536 0.0045 0 4 24 -4.1918 -0.0010 0 4 25 -1.3786 0.0030 0 4 26 1.9820 0.0005 0 4 27 1.6014 -0.0053 0 4 28 -0.8920 -0.0024 0 4 29 -1.0587 0.0021 0 4 30 0.9331 0.0036 0 4 31 -0.1489 0.0002 0 4 32 -1.4267 -0.0007 0 4 33 1.1444 0.0028 0 4 34 1.9482 -0.0032 0 4 35 -1.5378 -0.0079 0 4 36 -2.1759 0.0036 0 4 37 1.7310 0.0085 0 4 38 1.6716 0.0002 0 4 39 -1.9276 -0.0021 0 5 1 -0.0056 -6.8773 0 5 2 -0.0104 0.8659 0 5 3 -0.0002 14.0974 0 5 4 0.0027 -1.0375 0 5 5 0.0086 -8.2019 0 5 6 0.0062 0.7603 0 5 7 -0.0096 -5.4690 0 5 8 -0.0021 -1.1860 0 5 9 0.0047 15.9531 0 5 10 -0.0113 2.9740 0 5 11 -0.0018 -16.9199 0 5 12 0.0163 -4.9874 0 5 13 0.0027 10.3635 0 5 14 -0.0067 5.3236 0 5 15 -0.0027 -2.5574 0 5 16 -0.0051 -3.6883 0 5 17 -0.0008 -1.5565 0 5 18 0.0064 1.7079 0 5 19 0.0070 0.9527 0 5 20 0.0001 -0.8076 0 5 21 -0.0123 2.0594 0 5 22 -0.0034 0.8773 0 5 23 0.0119 -4.2495 0 5 24 -0.0009 -1.1467 0 5 25 -0.0057 4.0916 0 5 26 0.0076 1.2415 0 5 27 0.0005 -2.4276 0 5 28 -0.0096 -1.0894 0 5 29 -0.0015 0.7257 0 5 30 0.0051 0.6715 0 5 31 0.0043 0.5054 0 5 32 0.0019 -0.1588 0 5 33 -0.0030 -1.2570 0 5 34 -0.0058 -0.2524 0 5 35 -0.0016 1.1749 0 5 36 0.0039 0.6581 0 5 37 0.0054 -0.1820 0 5 38 0.0018 -1.1417 0 5 39 -0.0081 -0.8093 0 6 0 -27.1279 -0.0025 0 6 1 -7.7099 -0.0016 0 6 2 20.6088 0.0014 0 6 3 7.5060 0.0036 0 6 4 -6.6937 0.0005 0 6 5 -6.2882 -0.0039 0 6 6 -3.5394 -0.0021 0 6 7 3.7525 -0.0003 0 6 8 4.2048 0.0024 0 6 9 -0.9605 0.0049 0 6 10 1.7925 -0.0006 0 6 11 -0.4470 -0.0044 0 6 12 -7.6618 -0.0019 0 6 13 -0.0141 0.0016 0 6 14 8.7660 0.0028 0 6 15 1.1701 -0.0031 0 6 16 -4.8051 -0.0021 0 6 17 -1.5175 0.0072 0 6 18 -1.1676 0.0018 0 6 19 0.6035 -0.0070 0 6 20 5.2332 -0.0035 0 6 21 0.8902 0.0019 0 6 22 -5.5035 0.0059 0 6 23 -1.8788 0.0028 0 6 24 3.2716 -0.0059 0 6 25 1.7210 -0.0046 0 6 26 -1.1232 0.0025 0 6 27 -0.8461 0.0050 0 6 28 0.2797 0.0010 0 6 29 0.3595 -0.0045 0 6 30 -0.2288 -0.0014 0 6 31 -0.6030 0.0028 0 6 32 0.2102 0.0006 0 6 33 0.6335 -0.0017 0 6 34 -0.0285 -0.0018 0 6 35 0.2652 0.0022 0 6 36 -0.3120 0.0032 0 6 37 -1.2956 -0.0011 0 6 38 0.7914 -0.0019 0 6 39 1.2788 -0.0040 0 7 1 -0.0079 5.0146 0 7 2 0.0065 -1.2158 0 7 3 0.0068 -10.3437 0 7 4 -0.0082 1.1537 0 7 5 -0.0006 6.1226 0 7 6 0.0074 -0.4942 0 7 7 -0.0013 3.7137 0 7 8 -0.0072 0.8736 0 7 9 -0.0030 -11.4576 0 7 10 0.0075 -2.5652 0 7 11 0.0082 12.6497 0 7 12 -0.0049 4.2463 0 7 13 -0.0078 -8.1933 0 7 14 -0.0004 -4.6679 0 7 15 0.0011 2.0551 0 7 16 0.0034 3.6315 0 7 17 0.0062 1.8181 0 7 18 -0.0020 -1.7192 0 7 19 -0.0076 -1.7083 0 7 20 0.0005 0.0009 0 7 21 0.0037 -1.1139 0 7 22 -0.0014 0.4059 0 7 23 -0.0012 3.7064 0 7 24 0.0018 0.4851 0 7 25 0.0040 -3.9737 0 7 26 0.0006 -1.1453 0 7 27 -0.0077 2.1231 0 7 28 -0.0033 0.3331 0 7 29 0.0065 0.0356 0 7 30 0.0051 1.1607 0 7 31 -0.0017 -0.9308 0 7 32 -0.0071 -1.6837 0 7 33 -0.0005 0.4899 0 7 34 0.0080 1.1272 0 7 35 -0.0009 0.1702 0 7 36 -0.0052 -0.7830 0 7 37 0.0004 -0.1665 0 7 38 0.0002 1.1158 0 8 0 15.2910 -0.0111 0 8 1 4.1688 -0.0006 0 8 2 -11.3349 0.0160 0 8 3 -5.3421 -0.0046 0 8 4 2.7211 -0.0158 0 8 5 5.5657 0.0054 0 8 6 3.8679 0.0067 0 8 7 -3.7639 -0.0015 0 8 8 -4.3670 0.0053 0 8 9 1.3043 -0.0012 0 8 10 0.0897 -0.0114 0 8 11 0.1405 -0.0017 0 8 12 4.5225 0.0093 0 8 13 -0.3826 0.0072 0 8 14 -5.9158 -0.0045 0 8 15 0.0321 -0.0084 0 8 16 3.5807 0.0042 0 8 17 0.4107 0.0047 0 8 18 0.4948 -0.0086 0 8 19 -0.3681 -0.0021 0 8 20 -3.6846 0.0091 0 8 21 -0.5334 0.0037 0 8 22 4.3163 -0.0001 0 8 23 1.5760 -0.0054 0 8 24 -2.4419 -0.0107 0 8 25 -1.5166 0.0033 0 8 26 -0.2431 0.0118 0 8 27 0.3698 0.0008 0 8 28 1.6265 -0.0045 0 8 29 0.4631 -0.0032 0 8 30 -1.1101 0.0001 0 8 31 -0.1437 0.0029 0 8 32 0.1887 -0.0023 0 8 33 -0.5808 -0.0021 0 8 34 -0.5068 0.0037 0 8 35 0.6860 0.0032 0 8 36 1.7228 0.0011 0 8 37 -0.2334 -0.0064 0 8 38 -2.1777 -0.0071 0 9 1 0.0024 -2.5391 0 9 2 0.0034 1.9797 0 9 3 -0.0014 5.4271 0 9 4 -0.0115 -2.3229 0 9 5 -0.0019 -3.5353 0 9 6 0.0177 1.5585 0 9 7 0.0040 -2.0084 0 9 8 -0.0174 -1.3078 0 9 9 -0.0032 7.1041 0 9 10 0.0103 1.9801 0 9 11 0.0012 -8.1871 0 9 12 -0.0026 -2.7289 0 9 13 -0.0006 5.2532 0 9 14 0.0001 2.8840 0 9 15 0.0022 -1.2654 0 9 16 -0.0003 -2.3470 0 9 17 -0.0032 -1.0043 0 9 18 -0.0036 1.2095 0 9 19 -0.0003 0.9032 0 9 20 0.0113 0.0891 0 9 21 0.0070 0.6717 0 9 22 -0.0144 -0.7100 0 9 23 -0.0098 -2.3324 0 9 24 0.0091 0.2802 0 9 25 0.0061 2.6803 0 9 26 -0.0020 0.5139 0 9 27 -0.0028 -1.1766 0 9 28 -0.0003 -0.7085 0 9 29 0.0048 -0.9716 0 9 30 0.0005 0.1636 0 9 31 -0.0071 1.8201 0 9 32 -0.0033 0.4631 0 9 33 0.0030 -0.9756 0 9 34 0.0063 -0.6012 0 9 35 0.0041 -0.0613 0 9 36 -0.0035 0.3185 0 9 37 -0.0064 0.0938 0 9 38 -0.0037 -0.0697 0 10 0 -7.0064 -0.0133 0 10 1 -2.7617 0.0014 0 10 2 5.2305 0.0116 0 10 3 3.4164 -0.0014 0 10 4 -1.0394 -0.0074 0 10 5 -3.7358 -0.0011 0 10 6 -2.6769 0.0028 0 10 7 3.0020 0.0037 0 10 8 3.0808 0.0025 0 10 9 -1.5290 -0.0039 0 10 10 -0.1247 -0.0081 0 10 11 0.1912 0.0034 0 10 12 -3.1204 0.0120 0 10 13 0.4072 -0.0046 0 10 14 3.6920 -0.0129 0 10 15 -0.3000 0.0054 0 10 16 -1.5960 0.0120 0 10 17 0.0438 -0.0023 0 10 18 -1.0712 -0.0095 0 10 19 -0.2422 -0.0025 0 10 20 2.6752 0.0055 0 10 21 0.9742 0.0038 0 10 22 -2.8288 -0.0018 0 10 23 -1.7025 -0.0023 0 10 24 1.7668 -0.0010 0 10 25 1.8147 0.0032 0 10 26 -0.2101 0.0051 0 10 27 -1.1884 -0.0054 0 10 28 -0.7339 -0.0095 0 10 29 0.2592 0.0027 0 10 30 0.5986 0.0091 0 10 31 0.3614 0.0036 0 10 32 -0.1774 -0.0018 0 10 33 -0.4161 -0.0049 0 10 34 0.4208 -0.0067 0 10 35 0.2290 -0.0004 0 10 36 -1.1101 0.0096 0 10 37 -0.2572 0.0029 0 11 1 -0.0015 1.5688 0 11 2 0.0003 -1.2767 0 11 3 -0.0017 -3.5131 0 11 4 -0.0057 1.8225 0 11 5 0.0060 2.5702 0 11 6 0.0086 -1.4784 0 11 7 -0.0060 0.9379 0 11 8 -0.0070 0.8695 0 11 9 0.0020 -4.3453 0 11 10 0.0036 -1.0342 0 11 11 0.0012 4.9322 0 11 12 -0.0018 2.1979 0 11 13 -0.0020 -2.7265 0 11 14 0.0012 -3.2539 0 11 15 0.0026 0.1565 0 11 16 0.0007 2.9430 0 11 17 -0.0039 0.8664 0 11 18 -0.0035 -1.3331 0 11 19 0.0047 -0.4546 0 11 20 0.0049 -0.3114 0 11 21 -0.0054 -0.3639 0 11 22 -0.0053 0.9227 0 11 23 0.0057 0.9041 0 11 24 0.0062 -0.4569 0 11 25 -0.0039 -0.8427 0 11 26 -0.0057 -0.4516 0 11 27 0.0006 0.1146 0 11 28 0.0023 1.1585 0 11 29 -0.0002 0.7935 0 11 30 0.0002 -1.3798 0 11 31 0.0036 -1.1078 0 11 32 0.0012 1.2619 0 11 33 -0.0046 0.6510 0 11 34 -0.0016 -1.1081 0 11 35 -0.0019 -0.0650 0 11 36 -0.0045 0.9485 0 12 0 4.4253 -0.0007 0 12 1 0.9457 0.0011 0 12 2 -3.1554 0.0048 0 12 3 -1.8911 0.0000 0 12 4 0.1584 -0.0060 0 12 5 2.9615 -0.0004 0 12 6 2.4607 0.0018 0 12 7 -2.8640 0.0013 0 12 8 -2.8256 0.0031 0 12 9 1.1117 -0.0034 0 12 10 1.0276 -0.0034 0 12 11 0.9758 0.0058 0 12 12 0.9399 0.0006 0 12 13 -1.4929 -0.0069 0 12 14 -1.3266 0.0006 0 12 15 0.2373 0.0055 0 12 16 0.2380 0.0008 0 12 17 1.0920 -0.0031 0 12 18 1.1020 -0.0026 0 12 19 -1.0337 0.0017 0 12 20 -1.9002 0.0031 0 12 21 -0.1530 -0.0012 0 12 22 2.0683 -0.0020 0 12 23 1.2567 -0.0001 0 12 24 -1.6453 -0.0009 0 12 25 -1.5452 0.0009 0 12 26 0.7696 0.0027 0 12 27 1.1334 -0.0003 0 12 28 0.0351 -0.0001 0 12 29 -0.4993 0.0001 0 12 30 -0.2569 -0.0040 0 12 31 0.0192 -0.0020 0 12 32 0.0761 0.0014 0 12 33 0.2134 0.0037 0 12 34 -0.1360 0.0083 0 13 1 0.0024 -1.0305 0 13 2 -0.0014 1.7028 0 13 3 -0.0032 2.3710 0 13 4 0.0004 -2.1153 0 13 5 0.0026 -2.0331 0 13 6 0.0015 0.9206 0 13 7 -0.0027 0.2352 0 13 8 -0.0020 0.6100 0 13 9 0.0041 1.6834 0 13 10 0.0008 -0.5495 0 13 11 -0.0048 -2.3760 0 13 12 0.0004 -1.4045 0 13 13 0.0028 1.6766 0 13 14 -0.0003 3.2982 0 13 15 0.0004 -0.5177 0 13 16 -0.0009 -3.1985 0 13 17 -0.0025 -0.2219 0 13 18 0.0018 1.3871 0 13 19 0.0035 0.3968 0 13 20 -0.0005 0.3741 0 13 21 -0.0036 -0.2108 0 13 22 -0.0025 -1.0386 0 13 23 0.0029 -0.1975 0 13 24 0.0037 0.8974 0 13 25 -0.0030 0.5352 0 13 26 -0.0010 -0.5155 0 13 27 0.0051 -0.3191 0 13 28 -0.0021 0.0294 0 13 29 -0.0064 -0.4614 0 13 30 0.0013 0.5075 0 13 31 0.0028 1.0519 0 13 32 0.0025 -0.8044 0 13 33 0.0029 -0.8285 0 13 34 -0.0045 0.6524 0 14 0 -2.4264 0.0005 0 14 1 0.5337 0.0046 0 14 2 1.7462 0.0003 0 14 3 0.5652 -0.0037 0 14 4 -0.1200 -0.0004 0 14 5 -1.8364 0.0016 0 14 6 -1.4898 -0.0005 0 14 7 1.9004 -0.0011 0 14 8 2.1351 0.0008 0 14 9 -0.3576 0.0022 0 14 10 -1.5464 0.0004 0 14 11 -1.3090 -0.0025 0 14 12 0.3670 -0.0024 0 14 13 1.2094 0.0009 0 14 14 0.4031 0.0041 0 14 15 0.5731 0.0016 0 14 16 -0.2971 -0.0045 0 14 17 -2.0776 -0.0034 0 14 18 -0.3537 0.0028 0 14 19 1.9990 0.0031 0 14 20 0.9418 -0.0007 0 14 21 -1.0166 -0.0013 0 14 22 -1.0680 0.0001 0 14 23 0.3279 0.0003 0 14 24 0.5790 -0.0009 0 14 25 -0.0233 -0.0011 0 14 26 0.3739 0.0013 0 14 27 -0.3893 0.0005 0 14 28 -1.2080 -0.0022 0 14 29 0.7510 0.0039 0 14 30 1.3249 0.0051 0 14 31 -0.5319 -0.0084 0 14 32 -0.8144 -0.0079 0 15 1 0.0005 0.7566 0 15 2 -0.0010 -1.1699 0 15 3 -0.0005 -1.6367 0 15 4 -0.0016 1.3735 0 15 5 0.0001 1.2904 0 15 6 0.0018 -0.2866 0 15 7 -0.0006 0.0196 0 15 8 0.0002 -1.1869 0 15 9 0.0020 -1.4375 0 15 10 -0.0020 1.3851 0 15 11 -0.0031 2.1060 0 15 12 0.0023 0.1492 0 15 13 0.0027 -1.6531 0 15 14 -0.0017 -1.7823 0 15 15 -0.0014 0.4476 0 15 16 0.0009 1.7176 0 15 17 0.0002 0.6257 0 15 18 -0.0009 -0.2587 0 15 19 -0.0004 -0.8719 0 15 20 0.0012 -0.8742 0 15 21 0.0026 0.3523 0 15 22 0.0004 0.9940 0 15 23 -0.0052 0.2598 0 15 24 -0.0041 -0.9045 0 15 25 0.0058 -0.3423 0 15 26 0.0062 1.0982 0 15 27 -0.0043 -0.1425 0 15 28 -0.0037 -0.9852 0 15 29 0.0026 0.6937 0 16 0 2.3217 -0.0006 0 16 1 -0.8648 0.0007 0 16 2 -1.4657 0.0014 0 16 3 -0.2629 0.0000 0 16 4 -0.2851 -0.0010 0 16 5 1.5760 0.0006 0 16 6 1.4872 -0.0001 0 16 7 -1.7589 -0.0013 0 16 8 -1.5158 0.0012 0 16 9 0.3850 0.0009 0 16 10 0.7260 -0.0020 0 16 11 1.2535 0.0000 0 16 12 0.3131 0.0021 0 16 13 -1.3456 -0.0006 0 16 14 -1.1091 -0.0014 0 16 15 -0.2170 0.0001 0 16 16 1.1341 0.0010 0 16 17 1.6409 0.0018 0 16 18 -0.2384 -0.0010 0 16 19 -1.5592 -0.0042 0 16 20 -0.8209 0.0003 0 16 21 0.6062 0.0044 0 16 22 0.9482 0.0015 0 16 23 -0.1083 -0.0018 0 16 24 -0.0012 -0.0018 0 16 25 0.1992 -0.0008 0 17 1 0.0001 -0.7671 0 17 2 0.0015 2.1440 0 17 3 0.0005 1.5730 0 17 4 -0.0028 -2.5121 0 17 5 -0.0014 -1.1638 0 17 6 0.0028 0.9961 0 17 7 0.0022 0.3516 0 17 8 -0.0017 0.8393 0 17 9 -0.0019 0.0870 0 17 10 0.0003 -1.3028 0 17 11 0.0001 -0.2403 0 17 12 -0.0001 0.2817 0 17 13 0.0015 0.2717 0 17 14 0.0012 0.7898 0 17 15 -0.0002 0.1671 0 17 16 -0.0016 -0.6967 0 17 17 -0.0036 -1.0722 0 17 18 -0.0004 -0.2191 0 17 19 0.0058 1.4833 0 17 20 0.0036 0.7665 0 17 21 -0.0047 -0.6709 0 17 22 -0.0054 -0.4904 0 18 0 0.0425 -0.0053 0 18 1 1.7264 -0.0014 0 18 2 -0.2904 0.0056 0 18 3 -0.2344 0.0021 0 18 4 0.6634 -0.0031 0 18 5 -1.0316 -0.0020 0 18 6 -0.6801 -0.0004 0 18 7 0.7899 0.0013 0 18 8 0.4824 0.0024 0 18 9 0.3223 -0.0012 0 18 10 -0.4194 -0.0027 0 18 11 -0.7543 0.0024 0 18 12 0.2914 0.0036 0 18 13 -0.0005 -0.0045 0 18 14 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2.3489 11 10 2 0.1727 -0.9818 11 10 3 -0.3265 -1.4352 11 10 4 0.0113 0.3479 11 10 5 0.1467 0.4541 11 10 6 -0.1558 0.2297 11 10 7 0.3042 0.0397 11 10 8 -0.1595 -0.4344 11 10 9 -0.5915 -0.1832 11 10 10 0.5340 0.1527 11 10 11 0.3791 0.1646 11 10 12 -0.2712 0.4244 11 10 13 0.1454 0.0144 11 10 14 -0.4693 -0.7666 11 10 15 -0.5731 -0.1601 11 10 16 0.7965 0.4498 11 11 0 0.0223 0.4592 11 11 1 0.5031 -0.6457 11 11 2 0.5111 -0.5533 11 11 3 -1.1226 0.3814 11 11 4 -0.5605 0.6429 11 11 5 1.0595 -0.3270 11 11 6 0.2832 -0.4818 11 11 7 -0.6614 0.4704 11 11 8 -0.1705 0.1566 11 11 9 0.3151 -0.2643 11 11 10 0.3397 0.0509 11 11 11 -0.1875 -0.3453 11 11 12 -0.4823 -0.1209 11 12 0 0.0081 -1.5283 11 12 1 0.0285 -0.0784 11 12 10 -0.5244 -0.3074 12 0 0 0.1081 0.0347 12 0 1 0.0148 -0.3477 12 0 2 0.0632 -0.0110 12 0 3 -0.0257 0.8200 12 0 4 -0.4369 -0.0252 12 0 5 0.0078 -0.7632 12 0 6 0.7422 0.0233 12 0 7 0.0128 0.3636 12 0 8 -0.8305 0.0120 12 0 9 -0.0085 -0.2413 12 0 10 0.7562 -0.0306 12 0 11 -0.0124 0.6031 12 0 12 -0.7007 0.0097 12 0 13 0.0200 -0.8032 12 0 14 0.8228 0.0184 12 0 15 -0.0054 0.2645 12 0 16 -1.0418 -0.0167 12 1 0 -1.2926 -0.0097 12 1 1 -0.3347 -0.1457 12 1 2 0.8673 0.5600 12 1 3 0.0968 0.3938 12 1 4 -0.0423 -0.5363 12 1 5 -0.1588 -0.4089 12 1 6 -0.3955 0.0433 12 1 7 0.5457 0.1268 12 1 8 0.2058 0.3427 12 1 9 -0.7281 0.2990 12 1 10 -0.0171 -0.2812 12 1 11 0.4806 -0.5080 12 1 12 0.4501 -0.0238 12 1 13 -0.0977 0.2474 12 1 14 -1.1342 0.1881 12 1 15 -0.1907 0.2677 12 1 16 1.1259 -0.0850 12 2 0 0.6461 -0.0113 12 2 1 1.3650 0.2381 12 2 2 -0.3995 -0.0118 12 2 3 -0.5269 -0.1228 12 2 4 0.0392 0.1962 12 2 5 -0.3805 -0.7236 12 2 6 -0.1227 -0.1585 12 2 7 0.7051 1.1541 12 2 8 0.6334 -0.3206 12 2 9 -0.5236 -0.3341 12 2 10 -0.9982 0.8100 12 2 11 0.3540 -1.0583 12 2 12 0.8892 -0.9650 12 2 13 -0.4907 1.7097 12 2 14 -0.6264 1.0185 12 2 15 0.7681 -1.2270 12 2 16 0.5619 -1.1237 12 2 17 -0.8358 0.3236 12 3 0 0.2499 -0.0080 12 3 1 0.7464 -0.3420 12 3 2 0.0052 -0.5732 12 3 3 -1.0014 0.5636 12 3 4 -0.0066 0.7083 12 3 5 1.1855 -0.1297 12 3 6 -1.0338 -0.3579 12 3 7 -0.9048 -0.2926 12 3 8 2.3136 -0.1343 12 3 9 0.2517 0.0928 12 3 10 -2.4770 0.3879 12 3 11 0.1627 0.4278 12 3 12 1.5332 -0.2865 12 3 13 -0.0613 -0.5403 12 3 14 -0.6170 0.0603 12 3 15 -0.0390 0.1413 12 3 16 0.3883 -0.0636 12 3 17 -0.3217 0.2179 12 3 18 -0.6133 0.3447 12 4 0 -1.3043 0.0016 12 4 1 -0.7089 0.3873 12 4 2 0.9327 0.1950 12 4 3 0.5028 -1.2320 12 4 4 -0.2622 0.1972 12 4 5 -0.0942 1.6952 12 4 6 0.0264 -0.8002 12 4 7 -0.3766 -1.0299 12 4 8 -0.2856 0.8345 12 4 9 0.6481 -0.3524 12 4 10 0.4885 -0.3189 12 4 11 -0.6356 1.1664 12 4 12 -0.3175 0.0467 12 4 13 0.5975 -1.0709 12 4 14 0.0136 -0.4025 12 4 15 -0.7405 0.8885 12 4 16 0.1386 0.8201 12 4 17 0.7823 -1.0482 12 4 18 -0.2201 -0.6244 12 4 19 -0.3292 1.0863 12 4 20 0.4123 -0.0455 12 5 0 0.7358 -0.0036 12 5 1 -0.7109 0.0518 12 5 2 -0.3037 -0.3781 12 5 3 0.7917 0.0097 12 5 4 -0.8069 0.5970 12 5 5 -0.4570 -0.1968 12 5 6 1.9094 -0.7318 12 5 7 -0.0574 0.2288 12 5 8 -2.1532 0.8850 12 5 9 -0.0957 0.0103 12 5 10 1.5708 -0.8816 12 5 11 0.8871 -0.2947 12 5 12 -1.1343 0.5337 12 5 13 -1.2543 0.3727 12 5 14 1.3285 -0.1127 12 5 15 0.6779 -0.2174 12 5 16 -1.4769 0.1059 12 5 17 0.1090 -0.0345 12 5 18 0.9480 -0.4605 12 5 19 -0.2641 0.2005 12 6 0 -0.5941 0.0005 12 6 1 -0.2366 -0.4591 12 6 2 0.5087 0.5751 12 6 3 0.2367 1.0497 12 6 4 -0.2411 -0.8318 12 6 5 -0.2984 -1.0167 12 6 6 -0.1337 0.3032 12 6 7 0.3042 0.6442 12 6 8 0.4129 0.7070 12 6 9 -0.1009 -0.4286 12 6 10 -0.4272 -0.9925 12 6 11 -0.0890 0.4663 12 6 12 0.1611 0.1093 12 6 13 -0.1056 -0.3868 12 6 14 0.2671 0.7794 12 6 15 0.5264 -0.0514 12 6 16 -0.6090 -0.5512 12 6 17 -0.5610 0.5428 12 7 0 0.3748 0.0040 12 7 1 0.9571 0.3308 12 7 2 -0.3663 0.3614 12 7 3 -0.4667 -0.9374 12 7 4 0.2422 -0.6899 12 7 5 -0.1252 1.2244 12 7 6 -0.0673 1.0258 12 7 7 0.1272 -1.1304 12 7 8 0.2242 -1.2026 12 7 9 0.6688 0.7056 12 7 10 -0.8103 0.8760 12 7 11 -1.4014 -0.1433 12 7 12 1.3064 -0.1485 12 7 13 1.1463 -0.1882 12 7 14 -1.2487 -0.3331 12 7 15 -0.2715 0.0049 12 8 0 1.7302 0.0087 12 8 1 0.0548 -0.2631 12 8 2 -1.4609 -0.3316 12 8 3 -0.1131 0.5648 12 8 4 0.8267 0.4238 12 8 5 0.2328 -0.2677 12 8 6 -0.1320 -0.2967 12 8 7 -0.2281 -0.5742 12 8 8 -0.4465 0.1942 12 8 9 -0.0324 1.2165 12 8 10 0.6819 -0.2872 12 8 11 0.2824 -1.0355 12 8 12 -0.3274 0.3915 12 9 0 -1.6597 0.0008 12 9 1 0.0793 -0.4817 12 9 2 1.3419 -0.1433 12 9 3 0.1821 1.1892 12 9 4 -0.6181 0.2865 12 9 5 -0.5881 -1.3500 12 9 6 0.0242 -0.4514 12 9 7 0.7845 1.1812 12 9 8 0.0316 0.5616 12 9 9 -0.4883 -0.7999 12 9 10 0.2488 -0.4356 12 9 11 -0.0796 0.2511 12 10 0 -2.0536 0.0093 12 10 1 0.6851 0.1517 12 10 2 1.6029 -0.3606 12 10 3 -0.2651 -0.3028 12 10 4 -0.6809 0.4811 12 10 5 -0.2346 0.2439 12 10 6 -0.0488 -0.2230 12 10 7 0.5154 -0.1682 12 10 8 0.4441 -0.1914 13 0 1 0.0204 0.0606 13 0 2 -0.2278 -0.0088 13 0 3 0.0097 -0.7256 13 0 4 0.3909 0.0151 13 0 5 -0.0261 1.0627 13 0 6 -0.4897 -0.0164 13 0 7 0.0057 -0.5365 13 0 8 0.6821 0.0136 13 0 9 0.0222 -0.1803 13 0 10 -0.9932 -0.0106 13 0 11 -0.0202 0.1757 13 0 12 1.0061 0.0091 13 0 13 -0.0052 0.5217 13 1 0 -0.0126 -0.4271 13 1 1 -0.2666 0.1708 13 1 2 -0.4369 0.1638 13 1 3 0.4633 0.0992 13 1 4 0.1447 0.1731 13 1 5 -0.0662 -0.2423 13 1 6 0.6005 -0.0611 13 1 7 -0.4712 0.0531 13 1 8 -0.9347 -0.3531 13 1 9 0.5544 0.0884 13 1 10 0.5912 0.5614 13 1 11 -0.1543 0.3222 13 1 12 -0.0754 -0.3774 13 1 13 -0.2459 -1.0324 13 1 14 -0.1579 -0.0342 13 2 0 -0.0056 1.2046 13 2 1 -0.1644 -0.4298 13 2 2 0.1795 -0.7564 13 2 3 0.1838 0.5412 13 2 4 0.3048 -0.0944 13 2 5 0.1604 -0.4905 13 2 6 -0.8959 0.4591 13 2 7 -0.3270 0.2812 13 2 8 0.5660 -0.1284 13 2 9 0.0305 -0.2587 13 2 10 0.6425 -0.2954 13 2 11 0.4880 0.5460 13 2 12 -1.5548 0.2576 13 2 13 -0.9501 -0.8503 13 2 14 1.3803 0.1199 13 2 15 1.1816 0.9092 13 3 0 0.0100 0.5418 13 3 1 0.3625 0.4854 13 3 2 -0.1935 -0.4936 13 3 3 -0.7182 -0.7119 13 3 4 0.3689 0.3918 13 3 6 -0.4192 -0.2635 13 3 7 0.2010 1.3634 13 3 8 0.3448 0.0998 13 3 9 -0.4493 -2.4567 13 3 10 -0.3387 -0.0088 13 3 11 0.3396 2.1552 13 4 0 -0.0140 -0.7484 13 4 1 0.0772 0.9646 13 4 2 0.6246 0.4856 13 4 3 -0.3843 -0.7848 13 4 4 -1.4760 0.0114 13 4 5 0.7821 0.4661 13 4 6 1.8280 -0.2853 13 4 7 -0.7927 -0.1798 13 4 8 -1.0052 0.2857 13 4 9 0.3010 0.0879 13 4 10 -0.3683 -0.2441 13 4 11 0.1129 -0.1344 13 5 0 -0.0170 -1.0496 13 5 1 -0.0670 -0.6963 13 5 2 -0.0652 1.0025 13 5 3 -0.0317 0.2675 13 5 4 0.0059 -0.6033 13 5 5 0.4870 0.6466 13 5 6 0.1764 -0.2176 13 5 7 -0.9402 -1.6300 13 5 9 1.0634 2.0247 13 5 10 0.3496 -0.3461 13 6 0 0.0225 -0.0132 13 6 1 -0.3816 0.4810 13 6 2 -0.3429 0.2519 13 6 3 1.0521 -0.2933 13 6 4 0.5526 -0.6501 13 6 5 -1.2062 0.0271 13 6 6 -0.6139 0.6817 13 7 0 0.0225 0.6420 13 7 1 0.1133 -0.6698 13 7 2 0.4147 -0.4690 13 7 3 -0.0965 0.4970 13 7 4 -0.7833 -0.0079 13 7 5 -0.3575 -0.1901 0 0 0 0.0 0.0 ; _shelx_fab_checksum 696 _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems' _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a Hampton Cryo loop using Paratone Oil' _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S2 S 0.85036(8) 0.71889(5) 0.35475(3) 0.03708(19) Uani 1 1 d . . . . . S3 S 0.10885(8) 0.28631(5) 0.55821(3) 0.03651(18) Uani 1 1 d . . . . . S4 S -0.11912(8) 0.49174(6) 0.64987(3) 0.0410(2) Uani 1 1 d . . . . . S1 S 1.17012(9) 0.56501(7) 0.28472(3) 0.0457(2) Uani 1 1 d . . . . . F1 F 0.3390(2) 0.60961(15) 0.38154(7) 0.0638(6) Uani 1 1 d . . . . . F2 F 0.2564(2) 0.41297(16) 0.39585(6) 0.0596(6) Uani 1 1 d . . . . . O2 O 0.9765(3) 0.74844(16) 0.33510(8) 0.0539(7) Uani 1 1 d . . . . . O4 O 0.1267(3) 0.23962(14) 0.51709(7) 0.0495(6) Uani 1 1 d . . . . . O3 O 0.7320(3) 0.77436(15) 0.35058(8) 0.0534(6) Uani 1 1 d . . . . . N2 N -0.0785(2) 0.48387(18) 0.59537(8) 0.0351(6) Uani 1 1 d . . . . . O5 O 0.0027(2) 0.25641(17) 0.58783(8) 0.0537(7) Uani 1 1 d . . . . . O1 O 1.2061(3) 0.64953(19) 0.26116(10) 0.0660(8) Uani 1 1 d . . . . . C24 C 0.0682(3) 0.4593(2) 0.58945(10) 0.0321(7) Uani 1 1 d . . . . . H24 H 0.096513 0.420477 0.613954 0.039 Uiso 1 1 calc R U . . . O6 O -0.2066(3) 0.41379(17) 0.66267(9) 0.0627(7) Uani 1 1 d . . . . . N1 N 0.9976(2) 0.55559(18) 0.28623(8) 0.0361(6) Uani 1 1 d . . . . . C12 C 0.6973(3) 0.56865(19) 0.36042(9) 0.0297(6) Uani 1 1 d . . . . . C11 C 0.7234(3) 0.5031(2) 0.39246(10) 0.0337(7) Uani 1 1 d . . . . . C23 C 0.0739(3) 0.40524(19) 0.54523(9) 0.0295(6) Uani 1 1 d . . . . . C33 C 0.2658(3) 0.2850(2) 0.58693(10) 0.0367(7) Uani 1 1 d . . . . . C19 C 0.2921(3) 0.4882(2) 0.52653(10) 0.0341(7) Uani 1 1 d . . . . . C18 C 0.3907(3) 0.5121(2) 0.49516(10) 0.0382(7) Uani 1 1 d . . . . . H18 H 0.465123 0.546001 0.504359 0.046 Uiso 1 1 calc R U . . . C17 C 0.3823(3) 0.4875(2) 0.45103(10) 0.0362(7) Uani 1 1 d . . . . . C25 C 0.1565(3) 0.5427(2) 0.58923(11) 0.0384(7) Uani 1 1 d . . . . . H25A H 0.116263 0.587172 0.569787 0.046 Uiso 1 1 calc R U . . . H25B H 0.160271 0.567657 0.618888 0.046 Uiso 1 1 calc R U . . . C45 C 0.8123(3) 0.60665(18) 0.33244(9) 0.0300(6) Uani 1 1 d . . . . . C39 C 0.8814(4) 0.7012(2) 0.41218(10) 0.0429(8) Uani 1 1 d . . . . . C27 C -0.0743(3) 0.4087(2) 0.52702(10) 0.0383(7) Uani 1 1 d . . . . . H27A H -0.083877 0.456566 0.505520 0.046 Uiso 1 1 calc R U . . . H27B H -0.098177 0.352511 0.512920 0.046 Uiso 1 1 calc R U . . . C8 C 0.9466(3) 0.5521(2) 0.33272(9) 0.0321(7) Uani 1 1 d . . . . . H8 H 1.012688 0.582173 0.352062 0.038 Uiso 1 1 calc R U . . . C20 C 0.1808(3) 0.43688(19) 0.51263(9) 0.0307(6) Uani 1 1 d . . . . . C15 C 0.4895(3) 0.5134(2) 0.41884(10) 0.0373(7) Uani 1 1 d . . . . . C22 C 0.2693(3) 0.4378(2) 0.43899(10) 0.0383(7) Uani 1 1 d . . . . . C21 C 0.1700(3) 0.4123(2) 0.46838(10) 0.0347(7) Uani 1 1 d . . . . . H21 H 0.095856 0.378654 0.458752 0.042 Uiso 1 1 calc R U . . . C10 C 0.8625(3) 0.4597(2) 0.39457(10) 0.0408(8) Uani 1 1 d . . . . . H10A H 0.920833 0.493218 0.414566 0.049 Uiso 1 1 calc R U . . . H10B H 0.853884 0.399263 0.405937 0.049 Uiso 1 1 calc R U . . . C16 C 0.6202(3) 0.4777(2) 0.42122(10) 0.0380(7) Uani 1 1 d . . . . . H16 H 0.639153 0.435256 0.442908 0.046 Uiso 1 1 calc R U . . . C26 C 0.2996(3) 0.5211(2) 0.57360(10) 0.0398(8) Uani 1 1 d . . . . . H26A H 0.356457 0.574134 0.575201 0.048 Uiso 1 1 calc R U . . . H26B H 0.339553 0.475356 0.592392 0.048 Uiso 1 1 calc R U . . . C29 C -0.2336(3) 0.5892(2) 0.65062(11) 0.0417(8) Uani 1 1 d . . . . . C38 C 0.2655(4) 0.2791(2) 0.63296(11) 0.0479(9) Uani 1 1 d . . . . . H38 H 0.183924 0.274891 0.648597 0.058 Uiso 1 1 calc R U . . . C14 C 0.4664(3) 0.5747(2) 0.38507(11) 0.0411(8) Uani 1 1 d . . . . . C34 C 0.3866(3) 0.2894(2) 0.56324(11) 0.0425(8) Uani 1 1 d . . . . . H34 H 0.385028 0.292275 0.532447 0.051 Uiso 1 1 calc R U . . . C13 C 0.5661(3) 0.6026(2) 0.35600(10) 0.0399(8) Uani 1 1 d . . . . . H13 H 0.545831 0.643572 0.333748 0.048 Uiso 1 1 calc R U . . . C5 C 0.9153(3) 0.6178(2) 0.25910(10) 0.0396(8) Uani 1 1 d . . . . . H5A H 0.906037 0.596115 0.228953 0.048 Uiso 1 1 calc R U . . . H5B H 0.955836 0.677030 0.258536 0.048 Uiso 1 1 calc R U . . . C9 C 0.9258(3) 0.4574(2) 0.34905(11) 0.0418(8) Uani 1 1 d . . . . . H9A H 0.866535 0.425237 0.328807 0.050 Uiso 1 1 calc R U . . . H9B H 1.012804 0.426471 0.350238 0.050 Uiso 1 1 calc R U . . . C6 C 0.7783(3) 0.6190(2) 0.28260(10) 0.0378(7) Uani 1 1 d . . . . . H6A H 0.720549 0.570733 0.272087 0.045 Uiso 1 1 calc R U . . . H6B H 0.731755 0.675463 0.277658 0.045 Uiso 1 1 calc R U . . . C28 C -0.1648(3) 0.4257(3) 0.56699(11) 0.0471(8) Uani 1 1 d . . . . . H28A H -0.248496 0.455823 0.558505 0.056 Uiso 1 1 calc R U . . . H28B H -0.187386 0.370172 0.581996 0.056 Uiso 1 1 calc R U . . . C40 C 1.0116(4) 0.6833(3) 0.42727(12) 0.0567(10) Uani 1 1 d . . . . . H40 H 1.084983 0.684081 0.407729 0.068 Uiso 1 1 calc R U . . . C44 C 0.7711(5) 0.7024(3) 0.44133(12) 0.0600(10) Uani 1 1 d . . . . . H44 H 0.683555 0.715749 0.431400 0.072 Uiso 1 1 calc R U . . . C36 C 0.5100(4) 0.2852(3) 0.63144(15) 0.0631(11) Uani 1 1 d . . . . . H36 H 0.592807 0.285948 0.646520 0.076 Uiso 1 1 calc R U . . . C1 C 1.2182(4) 0.4741(3) 0.24651(12) 0.0549(10) Uani 1 1 d . . . . . C35 C 0.5086(4) 0.2897(2) 0.58557(14) 0.0534(9) Uani 1 1 d . . . . . H35 H 0.590232 0.292791 0.569926 0.064 Uiso 1 1 calc R U . . . C37 C 0.3894(5) 0.2797(2) 0.65485(13) 0.0602(11) Uani 1 1 d . . . . . H37 H 0.391498 0.276352 0.685627 0.072 Uiso 1 1 calc R U . . . C32 C -0.2705(4) 0.5992(3) 0.69958(11) 0.0565(10) Uani 1 1 d . . . . . H32A H -0.318753 0.546882 0.709337 0.085 Uiso 1 1 calc R U . . . H32B H -0.327375 0.650980 0.703443 0.085 Uiso 1 1 calc R U . . . H32C H -0.188617 0.606104 0.716725 0.085 Uiso 1 1 calc R U . . . C30 C -0.3594(4) 0.5722(3) 0.62221(14) 0.0673(12) Uani 1 1 d . . . . . H30A H -0.335291 0.576901 0.591451 0.101 Uiso 1 1 calc R U . . . H30B H -0.428254 0.615719 0.629126 0.101 Uiso 1 1 calc R U . . . H30C H -0.393845 0.513263 0.628130 0.101 Uiso 1 1 calc R U . . . C2 C 1.1643(5) 0.4923(3) 0.20034(12) 0.0730(12) Uani 1 1 d . . . . . H2A H 1.066467 0.495197 0.201130 0.109 Uiso 1 1 calc R U . . . H2B H 1.192244 0.444948 0.180806 0.109 Uiso 1 1 calc R U . . . H2C H 1.200149 0.548160 0.189809 0.109 Uiso 1 1 calc R U . . . C43 C 0.7955(6) 0.6834(4) 0.48520(13) 0.0848(16) Uani 1 1 d . . . . . H43 H 0.723032 0.683494 0.505124 0.102 Uiso 1 1 calc R U . . . C31 C -0.1524(5) 0.6693(3) 0.63525(14) 0.0709(13) Uani 1 1 d . . . . . H31A H -0.070308 0.674065 0.652460 0.106 Uiso 1 1 calc R U . . . H31B H -0.205993 0.722620 0.639005 0.106 Uiso 1 1 calc R U . . . H31C H -0.129399 0.662289 0.604525 0.106 Uiso 1 1 calc R U . . . C41 C 1.0323(5) 0.6642(3) 0.47167(15) 0.0783(14) Uani 1 1 d . . . . . H41 H 1.119419 0.651361 0.482114 0.094 Uiso 1 1 calc R U . . . C42 C 0.9232(7) 0.6645(4) 0.50006(15) 0.0951(18) Uani 1 1 d . . . . . H42 H 0.936680 0.651514 0.529888 0.114 Uiso 1 1 calc R U . . . C4 C 1.1636(5) 0.3864(3) 0.26503(15) 0.0783(14) Uani 1 1 d . . . . . H4A H 1.197390 0.377984 0.294606 0.118 Uiso 1 1 calc R U . . . H4B H 1.193297 0.337736 0.246639 0.118 Uiso 1 1 calc R U . . . H4C H 1.065649 0.388215 0.265544 0.118 Uiso 1 1 calc R U . . . C3 C 1.3743(5) 0.4752(4) 0.24771(18) 0.1005(18) Uani 1 1 d . . . . . H3A H 1.406947 0.530536 0.235493 0.151 Uiso 1 1 calc R U . . . H3B H 1.409075 0.426089 0.230569 0.151 Uiso 1 1 calc R U . . . H3C H 1.404895 0.469677 0.277815 0.151 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S2 0.0487(5) 0.0246(3) 0.0379(4) 0.0004(3) 0.0033(4) -0.0036(4) S3 0.0391(4) 0.0300(4) 0.0404(4) 0.0006(3) 0.0036(4) -0.0058(4) S4 0.0376(4) 0.0482(5) 0.0374(4) 0.0013(4) 0.0051(4) 0.0087(4) S1 0.0348(4) 0.0595(5) 0.0429(5) -0.0051(4) 0.0080(4) -0.0043(4) F1 0.0318(11) 0.0823(16) 0.0772(15) 0.0311(12) 0.0100(10) 0.0116(11) F2 0.0596(13) 0.0849(16) 0.0342(10) -0.0076(11) 0.0049(10) -0.0183(12) O2 0.0625(16) 0.0422(13) 0.0570(15) 0.0017(12) 0.0141(13) -0.0234(12) O4 0.0637(17) 0.0364(12) 0.0485(14) -0.0114(10) -0.0037(12) -0.0049(11) O3 0.0719(17) 0.0298(11) 0.0586(15) 0.0004(11) -0.0004(13) 0.0123(12) N2 0.0262(13) 0.0438(15) 0.0352(14) -0.0060(12) 0.0021(11) 0.0042(12) O5 0.0463(15) 0.0537(15) 0.0612(16) 0.0133(13) 0.0147(12) -0.0130(12) O1 0.0526(17) 0.0636(18) 0.0816(19) -0.0056(15) 0.0240(14) -0.0161(14) C24 0.0289(15) 0.0340(16) 0.0333(16) -0.0023(13) -0.0006(13) 0.0025(13) O6 0.0716(18) 0.0500(15) 0.0665(17) 0.0114(13) 0.0275(14) 0.0036(14) N1 0.0326(13) 0.0394(14) 0.0363(14) -0.0022(12) 0.0049(12) 0.0014(12) C12 0.0300(15) 0.0276(14) 0.0314(15) 0.0031(12) 0.0036(12) -0.0046(12) C11 0.0357(17) 0.0270(14) 0.0384(17) 0.0051(13) 0.0046(14) -0.0004(13) C23 0.0264(15) 0.0283(14) 0.0338(16) -0.0009(12) -0.0011(12) -0.0023(12) C33 0.0422(18) 0.0260(14) 0.0419(17) -0.0003(14) 0.0046(14) 0.0060(15) C19 0.0305(16) 0.0339(16) 0.0378(16) -0.0011(14) 0.0000(13) -0.0044(13) C18 0.0291(16) 0.0399(17) 0.0455(19) 0.0003(15) 0.0009(14) -0.0098(15) C17 0.0321(16) 0.0398(16) 0.0367(17) 0.0064(14) 0.0056(14) -0.0047(14) C25 0.0362(17) 0.0394(17) 0.0396(17) -0.0065(14) -0.0019(14) -0.0017(14) C45 0.0351(17) 0.0237(14) 0.0312(15) 0.0005(12) 0.0025(13) 0.0000(12) C39 0.060(2) 0.0309(16) 0.0379(17) -0.0046(14) 0.0016(17) -0.0052(16) C27 0.0281(16) 0.0446(19) 0.0423(18) -0.0050(15) -0.0018(14) -0.0037(14) C8 0.0320(16) 0.0327(16) 0.0315(16) -0.0015(13) 0.0056(13) -0.0004(13) C20 0.0287(15) 0.0302(14) 0.0333(16) 0.0013(13) 0.0014(12) -0.0027(13) C15 0.0378(18) 0.0372(17) 0.0370(17) 0.0022(14) 0.0054(14) -0.0056(15) C22 0.0405(18) 0.0460(18) 0.0285(16) -0.0015(14) 0.0019(14) -0.0043(15) C21 0.0334(16) 0.0363(16) 0.0346(16) -0.0011(13) 0.0000(14) -0.0089(14) C10 0.0389(18) 0.0345(16) 0.0490(19) 0.0154(14) 0.0049(15) 0.0030(14) C16 0.0418(18) 0.0342(16) 0.0380(17) 0.0083(13) 0.0002(14) -0.0017(15) C26 0.0330(17) 0.0442(18) 0.0421(18) -0.0062(15) -0.0019(14) -0.0083(14) C29 0.0391(18) 0.0410(17) 0.0450(18) -0.0046(15) 0.0066(16) 0.0099(15) C38 0.061(2) 0.0404(18) 0.0427(19) 0.0020(16) -0.0004(17) 0.0097(18) C14 0.0307(18) 0.0474(19) 0.0450(19) 0.0081(16) 0.0025(14) 0.0000(15) C34 0.0460(19) 0.0296(15) 0.0520(19) -0.0032(15) 0.0060(17) 0.0020(16) C13 0.0411(18) 0.0392(17) 0.0394(18) 0.0084(15) 0.0015(15) 0.0016(14) C5 0.046(2) 0.0436(18) 0.0292(16) 0.0004(14) 0.0031(15) 0.0016(16) C9 0.0434(19) 0.0310(16) 0.051(2) 0.0053(15) 0.0097(16) 0.0073(14) C6 0.0388(17) 0.0401(17) 0.0345(16) 0.0034(14) -0.0019(15) -0.0003(14) C28 0.0272(16) 0.060(2) 0.054(2) -0.0131(18) 0.0035(15) -0.0032(16) C40 0.063(3) 0.058(2) 0.049(2) -0.0050(19) -0.0046(19) -0.006(2) C44 0.075(3) 0.059(3) 0.045(2) -0.0076(19) 0.008(2) 0.002(2) C36 0.052(2) 0.048(2) 0.089(3) -0.016(2) -0.022(2) 0.008(2) C1 0.051(2) 0.067(3) 0.047(2) 0.0009(19) 0.0177(18) 0.016(2) C35 0.043(2) 0.0399(19) 0.077(3) -0.010(2) 0.0025(19) -0.0001(18) C37 0.082(3) 0.047(2) 0.052(2) -0.0064(18) -0.022(2) 0.015(2) C32 0.057(2) 0.062(2) 0.050(2) -0.0083(19) 0.0169(19) 0.006(2) C30 0.053(2) 0.077(3) 0.072(3) -0.022(2) -0.012(2) 0.027(2) C2 0.104(3) 0.068(3) 0.048(2) -0.011(2) 0.013(2) 0.013(3) C43 0.112(4) 0.101(4) 0.041(2) -0.003(2) 0.017(3) 0.018(3) C31 0.096(3) 0.044(2) 0.072(3) 0.000(2) 0.026(3) 0.006(2) C41 0.089(4) 0.086(4) 0.060(3) -0.005(3) -0.029(3) 0.006(3) C42 0.136(5) 0.107(4) 0.042(3) -0.002(3) -0.007(3) 0.032(4) C4 0.100(4) 0.050(2) 0.085(3) 0.001(2) 0.026(3) 0.022(3) C3 0.057(3) 0.134(5) 0.111(4) -0.017(4) 0.025(3) 0.025(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 S2 C45 107.57(14) . . ? O2 S2 C39 107.45(16) . . ? O3 S2 O2 118.78(15) . . ? O3 S2 C45 109.31(14) . . ? O3 S2 C39 108.09(16) . . ? C39 S2 C45 104.77(13) . . ? O4 S3 O5 118.26(15) . . ? O4 S3 C23 107.84(14) . . ? O4 S3 C33 108.23(15) . . ? O5 S3 C23 107.17(14) . . ? O5 S3 C33 108.70(15) . . ? C33 S3 C23 105.99(14) . . ? N2 S4 C29 102.13(14) . . ? O6 S4 N2 109.31(14) . . ? O6 S4 C29 105.33(15) . . ? O1 S1 N1 108.57(15) . . ? O1 S1 C1 105.41(16) . . ? N1 S1 C1 102.14(16) . . ? C24 N2 S4 111.03(19) . . ? C28 N2 S4 117.8(2) . . ? C28 N2 C24 109.6(2) . . ? N2 C24 H24 109.1 . . ? N2 C24 C23 105.3(2) . . ? N2 C24 C25 110.3(2) . . ? C23 C24 H24 109.1 . . ? C25 C24 H24 109.1 . . ? C25 C24 C23 113.6(2) . . ? C8 N1 S1 111.2(2) . . ? C5 N1 S1 118.5(2) . . ? C5 N1 C8 111.1(2) . . ? C11 C12 C45 120.7(3) . . ? C13 C12 C11 119.4(3) . . ? C13 C12 C45 119.8(3) . . ? C12 C11 C10 119.6(3) . . ? C16 C11 C12 119.4(3) . . ? C16 C11 C10 121.0(3) . . ? C24 C23 S3 108.83(19) . . ? C27 C23 S3 106.2(2) . . ? C27 C23 C24 104.5(2) . . ? C20 C23 S3 108.0(2) . . ? C20 C23 C24 114.8(2) . . ? C20 C23 C27 114.0(2) . . ? C38 C33 S3 119.3(3) . . ? C34 C33 S3 119.4(2) . . ? C34 C33 C38 121.4(3) . . ? C18 C19 C26 121.5(3) . . ? C20 C19 C18 118.4(3) . . ? C20 C19 C26 120.0(3) . . ? C19 C18 H18 118.6 . . ? C17 C18 C19 122.9(3) . . ? C17 C18 H18 118.6 . . ? C18 C17 C15 121.3(3) . . ? C22 C17 C18 116.3(3) . . ? C22 C17 C15 122.4(3) . . ? C24 C25 H25A 109.5 . . ? C24 C25 H25B 109.5 . . ? H25A C25 H25B 108.1 . . ? C26 C25 C24 110.7(3) . . ? C26 C25 H25A 109.5 . . ? C26 C25 H25B 109.5 . . ? C12 C45 S2 106.67(19) . . ? C12 C45 C8 115.5(2) . . ? C12 C45 C6 115.1(2) . . ? C8 C45 S2 107.7(2) . . ? C8 C45 C6 104.5(2) . . ? C6 C45 S2 106.79(19) . . ? C40 C39 S2 120.5(3) . . ? C40 C39 C44 120.7(3) . . ? C44 C39 S2 118.7(3) . . ? C23 C27 H27A 110.6 . . ? C23 C27 H27B 110.6 . . ? H27A C27 H27B 108.7 . . ? C28 C27 C23 105.7(2) . . ? C28 C27 H27A 110.6 . . ? C28 C27 H27B 110.6 . . ? N1 C8 C45 105.1(2) . . ? N1 C8 H8 108.9 . . ? N1 C8 C9 112.6(2) . . ? C45 C8 H8 108.9 . . ? C9 C8 C45 112.3(2) . . ? C9 C8 H8 108.9 . . ? C19 C20 C23 121.1(3) . . ? C21 C20 C23 119.3(3) . . ? C21 C20 C19 119.5(3) . . ? C16 C15 C17 121.2(3) . . ? C14 C15 C17 122.6(3) . . ? C14 C15 C16 116.2(3) . . ? F2 C22 C17 118.2(3) . . ? F2 C22 C21 118.5(3) . . ? C21 C22 C17 123.2(3) . . ? C20 C21 H21 120.2 . . ? C22 C21 C20 119.6(3) . . ? C22 C21 H21 120.2 . . ? C11 C10 H10A 109.7 . . ? C11 C10 H10B 109.7 . . ? H10A C10 H10B 108.2 . . ? C9 C10 C11 110.0(3) . . ? C9 C10 H10A 109.7 . . ? C9 C10 H10B 109.7 . . ? C11 C16 C15 122.3(3) . . ? C11 C16 H16 118.8 . . ? C15 C16 H16 118.8 . . ? C19 C26 C25 108.6(2) . . ? C19 C26 H26A 110.0 . . ? C19 C26 H26B 110.0 . . ? C25 C26 H26A 110.0 . . ? C25 C26 H26B 110.0 . . ? H26A C26 H26B 108.4 . . ? C32 C29 S4 103.5(2) . . ? C30 C29 S4 110.7(2) . . ? C30 C29 C32 111.7(3) . . ? C31 C29 S4 107.7(2) . . ? C31 C29 C32 110.1(3) . . ? C31 C29 C30 112.7(3) . . ? C33 C38 H38 120.8 . . ? C37 C38 C33 118.3(4) . . ? C37 C38 H38 120.8 . . ? F1 C14 C15 117.4(3) . . ? F1 C14 C13 119.1(3) . . ? C13 C14 C15 123.5(3) . . ? C33 C34 H34 120.3 . . ? C35 C34 C33 119.4(3) . . ? C35 C34 H34 120.3 . . ? C12 C13 H13 120.5 . . ? C14 C13 C12 119.0(3) . . ? C14 C13 H13 120.5 . . ? N1 C5 H5A 111.1 . . ? N1 C5 H5B 111.1 . . ? N1 C5 C6 103.4(2) . . ? H5A C5 H5B 109.1 . . ? C6 C5 H5A 111.1 . . ? C6 C5 H5B 111.1 . . ? C8 C9 H9A 109.8 . . ? C8 C9 H9B 109.8 . . ? C10 C9 C8 109.3(2) . . ? C10 C9 H9A 109.8 . . ? C10 C9 H9B 109.8 . . ? H9A C9 H9B 108.3 . . ? C45 C6 H6A 110.7 . . ? C45 C6 H6B 110.7 . . ? C5 C6 C45 105.2(2) . . ? C5 C6 H6A 110.7 . . ? C5 C6 H6B 110.7 . . ? H6A C6 H6B 108.8 . . ? N2 C28 C27 102.9(2) . . ? N2 C28 H28A 111.2 . . ? N2 C28 H28B 111.2 . . ? C27 C28 H28A 111.2 . . ? C27 C28 H28B 111.2 . . ? H28A C28 H28B 109.1 . . ? C39 C40 H40 120.2 . . ? C39 C40 C41 119.6(4) . . ? C41 C40 H40 120.2 . . ? C39 C44 H44 121.0 . . ? C43 C44 C39 118.1(4) . . ? C43 C44 H44 121.0 . . ? C35 C36 H36 119.8 . . ? C37 C36 H36 119.8 . . ? C37 C36 C35 120.4(4) . . ? C2 C1 S1 110.7(3) . . ? C2 C1 C4 111.7(4) . . ? C2 C1 C3 111.6(4) . . ? C4 C1 S1 108.4(2) . . ? C4 C1 C3 110.6(4) . . ? C3 C1 S1 103.4(3) . . ? C34 C35 C36 120.0(4) . . ? C34 C35 H35 120.0 . . ? C36 C35 H35 120.0 . . ? C38 C37 H37 119.7 . . ? C36 C37 C38 120.5(4) . . ? C36 C37 H37 119.7 . . ? C29 C32 H32A 109.5 . . ? C29 C32 H32B 109.5 . . ? C29 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C29 C30 H30A 109.5 . . ? C29 C30 H30B 109.5 . . ? C29 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C1 C2 H2A 109.5 . . ? C1 C2 H2B 109.5 . . ? C1 C2 H2C 109.5 . . ? H2A C2 H2B 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? C44 C43 H43 119.3 . . ? C42 C43 C44 121.4(5) . . ? C42 C43 H43 119.3 . . ? C29 C31 H31A 109.5 . . ? C29 C31 H31B 109.5 . . ? C29 C31 H31C 109.5 . . ? H31A C31 H31B 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C40 C41 H41 120.3 . . ? C42 C41 C40 119.4(4) . . ? C42 C41 H41 120.3 . . ? C43 C42 C41 120.8(4) . . ? C43 C42 H42 119.6 . . ? C41 C42 H42 119.6 . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4B 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C1 C3 H3A 109.5 . . ? C1 C3 H3B 109.5 . . ? C1 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S2 O2 1.440(2) . ? S2 O3 1.430(2) . ? S2 C45 1.845(3) . ? S2 C39 1.779(3) . ? S3 O4 1.434(2) . ? S3 O5 1.442(2) . ? S3 C23 1.851(3) . ? S3 C33 1.765(3) . ? S4 N2 1.696(2) . ? S4 O6 1.496(3) . ? S4 C29 1.838(3) . ? S1 O1 1.491(3) . ? S1 N1 1.697(3) . ? S1 C1 1.843(4) . ? F1 C14 1.357(4) . ? F2 C22 1.359(3) . ? N2 C24 1.493(4) . ? N2 C28 1.485(4) . ? C24 H24 0.9800 . ? C24 C23 1.561(4) . ? C24 C25 1.517(4) . ? N1 C8 1.490(4) . ? N1 C5 1.478(4) . ? C12 C11 1.399(4) . ? C12 C45 1.518(4) . ? C12 C13 1.388(4) . ? C11 C10 1.510(4) . ? C11 C16 1.385(4) . ? C23 C27 1.553(4) . ? C23 C20 1.512(4) . ? C33 C38 1.391(4) . ? C33 C34 1.384(4) . ? C19 C18 1.398(4) . ? C19 C20 1.397(4) . ? C19 C26 1.504(4) . ? C18 H18 0.9300 . ? C18 C17 1.384(4) . ? C17 C15 1.482(4) . ? C17 C22 1.382(4) . ? C25 H25A 0.9700 . ? C25 H25B 0.9700 . ? C25 C26 1.514(4) . ? C45 C8 1.548(4) . ? C45 C6 1.551(4) . ? C39 C40 1.380(5) . ? C39 C44 1.393(5) . ? C27 H27A 0.9700 . ? C27 H27B 0.9700 . ? C27 C28 1.518(4) . ? C8 H8 0.9800 . ? C8 C9 1.513(4) . ? C20 C21 1.389(4) . ? C15 C16 1.389(4) . ? C15 C14 1.388(4) . ? C22 C21 1.370(4) . ? C21 H21 0.9300 . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C10 C9 1.507(4) . ? C16 H16 0.9300 . ? C26 H26A 0.9700 . ? C26 H26B 0.9700 . ? C29 C32 1.528(5) . ? C29 C30 1.523(5) . ? C29 C31 1.510(5) . ? C38 H38 0.9300 . ? C38 C37 1.382(5) . ? C14 C13 1.377(4) . ? C34 H34 0.9300 . ? C34 C35 1.372(5) . ? C13 H13 0.9300 . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C5 C6 1.518(4) . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C28 H28A 0.9700 . ? C28 H28B 0.9700 . ? C40 H40 0.9300 . ? C40 C41 1.384(6) . ? C44 H44 0.9300 . ? C44 C43 1.375(6) . ? C36 H36 0.9300 . ? C36 C35 1.386(5) . ? C36 C37 1.379(6) . ? C1 C2 1.514(5) . ? C1 C4 1.521(6) . ? C1 C3 1.530(6) . ? C35 H35 0.9300 . ? C37 H37 0.9300 . ? C32 H32A 0.9600 . ? C32 H32B 0.9600 . ? C32 H32C 0.9600 . ? C30 H30A 0.9600 . ? C30 H30B 0.9600 . ? C30 H30C 0.9600 . ? C2 H2A 0.9600 . ? C2 H2B 0.9600 . ? C2 H2C 0.9600 . ? C43 H43 0.9300 . ? C43 C42 1.359(7) . ? C31 H31A 0.9600 . ? C31 H31B 0.9600 . ? C31 H31C 0.9600 . ? C41 H41 0.9300 . ? C41 C42 1.370(7) . ? C42 H42 0.9300 . ? C4 H4A 0.9600 . ? C4 H4B 0.9600 . ? C4 H4C 0.9600 . ? C3 H3A 0.9600 . ? C3 H3B 0.9600 . ? C3 H3C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S2 C45 C8 N1 -100.3(2) . . . . ? S2 C45 C8 C9 136.9(2) . . . . ? S2 C45 C6 C5 85.5(3) . . . . ? S2 C39 C40 C41 -176.0(3) . . . . ? S2 C39 C44 C43 176.2(3) . . . . ? S3 C23 C27 C28 91.5(3) . . . . ? S3 C23 C20 C19 -101.3(3) . . . . ? S3 C23 C20 C21 76.9(3) . . . . ? S3 C33 C38 C37 -178.9(3) . . . . ? S3 C33 C34 C35 179.1(3) . . . . ? S4 N2 C24 C23 149.84(19) . . . . ? S4 N2 C24 C25 -87.2(3) . . . . ? S4 N2 C28 C27 -160.9(2) . . . . ? S1 N1 C8 C45 142.0(2) . . . . ? S1 N1 C8 C9 -95.4(3) . . . . ? S1 N1 C5 C6 -156.1(2) . . . . ? F1 C14 C13 C12 178.3(3) . . . . ? F2 C22 C21 C20 -180.0(3) . . . . ? O2 S2 C45 C12 168.20(19) . . . . ? O2 S2 C45 C8 43.6(2) . . . . ? O2 S2 C45 C6 -68.2(2) . . . . ? O2 S2 C39 C40 -24.1(3) . . . . ? O2 S2 C39 C44 158.3(3) . . . . ? O4 S3 C23 C24 -174.54(19) . . . . ? O4 S3 C23 C27 73.4(2) . . . . ? O4 S3 C23 C20 -49.3(2) . . . . ? O4 S3 C33 C38 -145.2(3) . . . . ? O4 S3 C33 C34 34.6(3) . . . . ? O3 S2 C45 C12 -61.6(2) . . . . ? O3 S2 C45 C8 173.81(18) . . . . ? O3 S2 C45 C6 62.0(2) . . . . ? O3 S2 C39 C40 -153.4(3) . . . . ? O3 S2 C39 C44 29.0(3) . . . . ? N2 S4 C29 C32 -179.1(2) . . . . ? N2 S4 C29 C30 61.1(3) . . . . ? N2 S4 C29 C31 -62.5(3) . . . . ? N2 C24 C23 S3 -109.4(2) . . . . ? N2 C24 C23 C27 3.8(3) . . . . ? N2 C24 C23 C20 129.4(3) . . . . ? N2 C24 C25 C26 -167.9(2) . . . . ? O5 S3 C23 C24 57.1(2) . . . . ? O5 S3 C23 C27 -54.9(2) . . . . ? O5 S3 C23 C20 -177.63(19) . . . . ? O5 S3 C33 C38 -15.5(3) . . . . ? O5 S3 C33 C34 164.2(3) . . . . ? O1 S1 N1 C8 -120.0(2) . . . . ? O1 S1 N1 C5 10.5(3) . . . . ? O1 S1 C1 C2 -48.1(3) . . . . ? O1 S1 C1 C4 -171.0(3) . . . . ? O1 S1 C1 C3 71.6(3) . . . . ? C24 N2 C28 C27 -32.7(3) . . . . ? C24 C23 C27 C28 -23.5(3) . . . . ? C24 C23 C20 C19 20.4(4) . . . . ? C24 C23 C20 C21 -161.5(3) . . . . ? C24 C25 C26 C19 62.8(3) . . . . ? O6 S4 N2 C24 -108.0(2) . . . . ? O6 S4 N2 C28 19.5(3) . . . . ? O6 S4 C29 C32 66.7(3) . . . . ? O6 S4 C29 C30 -53.1(3) . . . . ? O6 S4 C29 C31 -176.7(3) . . . . ? N1 S1 C1 C2 65.3(3) . . . . ? N1 S1 C1 C4 -57.6(3) . . . . ? N1 S1 C1 C3 -175.0(3) . . . . ? N1 C8 C9 C10 -174.9(3) . . . . ? N1 C5 C6 C45 32.8(3) . . . . ? C12 C11 C10 C9 -30.0(4) . . . . ? C12 C11 C16 C15 1.7(5) . . . . ? C12 C45 C8 N1 140.6(2) . . . . ? C12 C45 C8 C9 17.8(4) . . . . ? C12 C45 C6 C5 -156.3(3) . . . . ? C11 C12 C45 S2 -104.1(3) . . . . ? C11 C12 C45 C8 15.6(4) . . . . ? C11 C12 C45 C6 137.7(3) . . . . ? C11 C12 C13 C14 3.8(5) . . . . ? C11 C10 C9 C8 62.7(4) . . . . ? C23 S3 C33 C38 99.4(3) . . . . ? C23 S3 C33 C34 -80.9(3) . . . . ? C23 C24 C25 C26 -49.9(3) . . . . ? C23 C27 C28 N2 34.1(3) . . . . ? C23 C20 C21 C22 -177.5(3) . . . . ? C33 S3 C23 C24 -58.8(2) . . . . ? C33 S3 C23 C27 -170.88(19) . . . . ? C33 S3 C23 C20 66.4(2) . . . . ? C33 C38 C37 C36 -0.5(5) . . . . ? C33 C34 C35 C36 0.2(5) . . . . ? C19 C18 C17 C15 -179.5(3) . . . . ? C19 C18 C17 C22 0.5(5) . . . . ? C19 C20 C21 C22 0.7(4) . . . . ? C18 C19 C20 C23 177.2(3) . . . . ? C18 C19 C20 C21 -0.9(4) . . . . ? C18 C19 C26 C25 141.1(3) . . . . ? C18 C17 C15 C16 68.1(4) . . . . ? C18 C17 C15 C14 -111.2(4) . . . . ? C18 C17 C22 F2 179.4(3) . . . . ? C18 C17 C22 C21 -0.8(5) . . . . ? C17 C15 C16 C11 -177.8(3) . . . . ? C17 C15 C14 F1 -1.6(5) . . . . ? C17 C15 C14 C13 177.1(3) . . . . ? C17 C22 C21 C20 0.3(5) . . . . ? C25 C24 C23 S3 129.8(2) . . . . ? C25 C24 C23 C27 -117.1(3) . . . . ? C25 C24 C23 C20 8.6(4) . . . . ? C45 S2 C39 C40 90.1(3) . . . . ? C45 S2 C39 C44 -87.5(3) . . . . ? C45 C12 C11 C10 -9.3(4) . . . . ? C45 C12 C11 C16 172.0(3) . . . . ? C45 C12 C13 C14 -172.6(3) . . . . ? C45 C8 C9 C10 -56.5(4) . . . . ? C39 S2 C45 C12 54.1(2) . . . . ? C39 S2 C45 C8 -70.6(2) . . . . ? C39 S2 C45 C6 177.6(2) . . . . ? C39 C40 C41 C42 -0.8(7) . . . . ? C39 C44 C43 C42 0.4(7) . . . . ? C27 C23 C20 C19 140.9(3) . . . . ? C27 C23 C20 C21 -41.0(4) . . . . ? C8 N1 C5 C6 -25.5(3) . . . . ? C8 C45 C6 C5 -28.5(3) . . . . ? C20 C23 C27 C28 -149.6(3) . . . . ? C20 C19 C18 C17 0.3(5) . . . . ? C20 C19 C26 C25 -35.1(4) . . . . ? C15 C17 C22 F2 -0.6(5) . . . . ? C15 C17 C22 C21 179.2(3) . . . . ? C15 C14 C13 C12 -0.4(5) . . . . ? C22 C17 C15 C16 -111.8(4) . . . . ? C22 C17 C15 C14 68.8(4) . . . . ? C10 C11 C16 C15 -177.0(3) . . . . ? C16 C11 C10 C9 148.7(3) . . . . ? C16 C15 C14 F1 179.0(3) . . . . ? C16 C15 C14 C13 -2.3(5) . . . . ? C26 C19 C18 C17 -176.0(3) . . . . ? C26 C19 C20 C23 -6.4(4) . . . . ? C26 C19 C20 C21 175.4(3) . . . . ? C29 S4 N2 C24 140.8(2) . . . . ? C29 S4 N2 C28 -91.7(3) . . . . ? C38 C33 C34 C35 -1.2(5) . . . . ? C14 C15 C16 C11 1.6(5) . . . . ? C34 C33 C38 C37 1.3(5) . . . . ? C13 C12 C11 C10 174.3(3) . . . . ? C13 C12 C11 C16 -4.4(5) . . . . ? C13 C12 C45 S2 72.3(3) . . . . ? C13 C12 C45 C8 -168.0(3) . . . . ? C13 C12 C45 C6 -45.9(4) . . . . ? C5 N1 C8 C45 7.7(3) . . . . ? C5 N1 C8 C9 130.3(3) . . . . ? C6 C45 C8 N1 13.0(3) . . . . ? C6 C45 C8 C9 -109.8(3) . . . . ? C28 N2 C24 C23 18.1(3) . . . . ? C28 N2 C24 C25 141.1(3) . . . . ? C40 C39 C44 C43 -1.4(6) . . . . ? C40 C41 C42 C43 -0.2(8) . . . . ? C44 C39 C40 C41 1.6(6) . . . . ? C44 C43 C42 C41 0.3(8) . . . . ? C1 S1 N1 C8 128.9(2) . . . . ? C1 S1 N1 C5 -100.5(2) . . . . ? C35 C36 C37 C38 -0.4(6) . . . . ? C37 C36 C35 C34 0.6(6) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.013 0.212 0.711 90.6 19.0 ? 2 -0.013 0.712 0.789 90.6 19.1 ? 3 0.487 0.788 0.211 90.6 19.0 ? 4 0.513 0.288 0.289 90.6 19.0 ?