#------------------------------------------------------------------------------ #$Date: 2021-07-31 04:49:09 +0300 (Sat, 31 Jul 2021) $ #$Revision: 267840 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/42/1564271.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564271 loop_ _publ_author_name 'Speelman, Amy L.' 'Tran, Ba' 'Erickson, Jeremy D.' 'Vasiliu, Monica' 'Dixon, David A.' 'Bullock, R. Morris' _publ_section_title ; Accelerating the Insertion Reactions of (NHC)Cu-H via Remote Ligand Functionalization ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC01911B _journal_year 2021 _chemical_formula_moiety 'C83 H67 Cu N2, 2(C4 H8 O)' _chemical_formula_sum 'C91 H83 Cu N2 O2' _chemical_formula_weight 1300.13 _chemical_properties_physical Air-sensitive,Moisture-sensitive _space_group_crystal_system monoclinic _space_group_IT_number 9 _space_group_name_Hall 'C -2yc' _space_group_name_H-M_alt 'C 1 c 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2020-08-04 _audit_creation_method ; Olex2 1.3 (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6143) ; _audit_update_record ; 2020-12-14 deposited with the CCDC. 2021-07-23 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 113.26(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 23.946(5) _cell_length_b 12.861(3) _cell_length_c 24.517(5) _cell_measurement_reflns_used 9617 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 32.49 _cell_measurement_theta_min 2.20 _cell_volume 6937(3) _computing_cell_refinement 'SAINT V8.40A (Bruker, 2019)' _computing_data_reduction 'SAINT V8.40A (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0624 _diffrn_reflns_av_unetI/netI 0.0709 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 36 _diffrn_reflns_limit_h_min -36 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_number 104060 _diffrn_reflns_point_group_measured_fraction_full 0.990 _diffrn_reflns_point_group_measured_fraction_max 0.964 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 32.633 _diffrn_reflns_theta_min 1.876 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.368 _exptl_absorpt_correction_T_max 0.8255 _exptl_absorpt_correction_T_min 0.6945 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.1158 before and 0.0793 after correction. The Ratio of minimum to maximum transmission is 0.8609. The \l/2 correction factor is 0.00150. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.245 _exptl_crystal_description block _exptl_crystal_F_000 2752 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.29 _exptl_crystal_size_min 0.188 _refine_diff_density_max 1.151 _refine_diff_density_min -1.207 _refine_diff_density_rms 0.080 _refine_ls_abs_structure_details ; Flack x determined using 8081 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.037(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.049 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 867 _refine_ls_number_reflns 24502 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.049 _refine_ls_R_factor_all 0.0798 _refine_ls_R_factor_gt 0.0613 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0762P)^2^+9.5991P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1537 _refine_ls_wR_factor_ref 0.1696 _reflns_Friedel_coverage 0.939 _reflns_Friedel_fraction_full 0.980 _reflns_Friedel_fraction_max 0.934 _reflns_number_gt 20150 _reflns_number_total 24502 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; jdebt08_a.res created by SHELXL-2014/7 TITL JDEBT08_a.res in Cc REM Old TITL JDEBT08 in Cc REM SHELXT solution in Cc REM R1 0.092, Rweak 0.017, Alpha 0.004, Orientation as input REM Flack x = 0.089 ( 0.004 ) from Parsons' quotients REM Formula found by SHELXT: C86 N7 O2 Cu CELL 0.71073 23.946 12.861 24.517 90 113.26 90 ZERR 4 0.0048 0.0026 0.0049 0 0.03 0 LATT -7 SYMM +X,-Y,0.5+Z SFAC C H Cu N O UNIT 364 332 4 8 8 L.S. 64 PLAN 7 SIZE 0.188 0.29 0.3 CONF BOND $H LIST 4 MORE -1 fmap 2 acta OMIT -2 0 0 OMIT 0 0 -2 REM REM REM WGHT 0.076200 9.599100 FVAR 0.13850 CU1 3 0.542139 0.345698 0.531040 11.00000 0.02206 0.02362 = 0.02237 0.00217 0.00821 0.00175 N1 4 0.437544 0.453285 0.448489 11.00000 0.02045 0.02672 = 0.01806 0.00077 0.00905 0.00067 N2 4 0.507310 0.565504 0.489701 11.00000 0.02028 0.02196 = 0.01662 0.00023 0.00788 0.00118 C1 1 0.496250 0.461913 0.487662 11.00000 0.02104 0.02174 = 0.01542 0.00362 0.00979 0.00324 C2 1 0.413102 0.550041 0.426353 11.00000 0.02207 0.02906 = 0.02156 0.00270 0.00682 0.00377 AFIX 43 H2 2 0.374038 0.563469 0.398614 11.00000 -1.20000 AFIX 0 C3 1 0.456903 0.620121 0.452853 11.00000 0.02506 0.02815 = 0.02170 0.00372 0.00907 0.00310 AFIX 43 H3 2 0.453908 0.691795 0.447451 11.00000 -1.20000 AFIX 0 C4 1 0.404360 0.357531 0.428838 11.00000 0.02088 0.03107 = 0.01525 -0.00041 0.01074 -0.00101 C5 1 0.406955 0.307171 0.379210 11.00000 0.02090 0.02823 = 0.01843 -0.00039 0.00993 -0.00009 C6 1 0.370970 0.219734 0.357440 11.00000 0.02794 0.03169 = 0.02052 -0.00505 0.01230 -0.00443 AFIX 43 H6 2 0.372124 0.185643 0.324448 11.00000 -1.20000 AFIX 0 C7 1 0.333134 0.181917 0.383965 11.00000 0.02667 0.03386 = 0.02381 -0.00713 0.01246 -0.00702 C8 1 0.333944 0.231056 0.434895 11.00000 0.02611 0.03850 = 0.02143 -0.00701 0.01356 -0.00841 AFIX 43 H8 2 0.310462 0.203896 0.453979 11.00000 -1.20000 AFIX 0 C9 1 0.368780 0.319582 0.458202 11.00000 0.02055 0.03421 = 0.01814 -0.00395 0.01015 -0.00312 C10 1 0.449427 0.346507 0.350927 11.00000 0.01984 0.02838 = 0.01612 -0.00008 0.00942 -0.00110 AFIX 13 H10 2 0.483231 0.381346 0.382504 11.00000 -1.20000 AFIX 0 C11 1 0.476914 0.255555 0.330210 11.00000 0.02660 0.03119 = 0.02204 0.00427 0.01532 0.00300 C12 1 0.519074 0.192342 0.372842 11.00000 0.03168 0.04167 = 0.02651 0.00931 0.01611 0.00743 AFIX 43 H12 2 0.530643 0.206940 0.412976 11.00000 -1.20000 AFIX 0 C13 1 0.543878 0.107223 0.355254 11.00000 0.04349 0.04519 = 0.04722 0.02016 0.03052 0.01805 AFIX 43 H13 2 0.571717 0.064659 0.383777 11.00000 -1.20000 AFIX 0 C14 1 0.527471 0.085662 0.295946 11.00000 0.05570 0.03471 = 0.05313 0.00927 0.04151 0.01225 AFIX 43 H14 2 0.544612 0.029259 0.284477 11.00000 -1.20000 AFIX 0 C15 1 0.485497 0.147928 0.253464 11.00000 0.04907 0.03785 = 0.03432 -0.00110 0.02915 0.00515 AFIX 43 H15 2 0.474277 0.133064 0.213404 11.00000 -1.20000 AFIX 0 C16 1 0.460040 0.232433 0.270276 11.00000 0.03246 0.03537 = 0.02322 0.00032 0.01555 0.00352 AFIX 43 H16 2 0.431627 0.273804 0.241487 11.00000 -1.20000 AFIX 0 C17 1 0.420656 0.427438 0.302083 11.00000 0.02506 0.02815 = 0.01874 -0.00165 0.01082 0.00122 C18 1 0.458864 0.495513 0.288763 11.00000 0.03018 0.03475 = 0.02723 0.00141 0.01379 -0.00315 AFIX 43 H18 2 0.500575 0.492551 0.310816 11.00000 -1.20000 AFIX 0 C19 1 0.435771 0.567399 0.243290 11.00000 0.04274 0.03581 = 0.03340 0.00768 0.02050 0.00162 AFIX 43 H19 2 0.461919 0.611910 0.234851 11.00000 -1.20000 AFIX 0 C20 1 0.373777 0.572977 0.210412 11.00000 0.04764 0.03798 = 0.03187 0.01482 0.01849 0.01319 AFIX 43 H20 2 0.358140 0.621454 0.179981 11.00000 -1.20000 AFIX 0 C21 1 0.335056 0.506095 0.222971 11.00000 0.03601 0.04873 = 0.03374 0.01211 0.01253 0.00983 AFIX 43 H21 2 0.293375 0.509582 0.200837 11.00000 -1.20000 AFIX 0 C22 1 0.358414 0.433539 0.268723 11.00000 0.02707 0.03806 = 0.03015 0.00467 0.01321 0.00277 AFIX 43 H22 2 0.332176 0.388943 0.276969 11.00000 -1.20000 AFIX 0 C23 1 0.292719 0.089102 0.358569 11.00000 0.04152 0.04550 = 0.03489 -0.01400 0.02183 -0.01776 AFIX 137 H23A 2 0.282233 0.057866 0.388820 11.00000 -1.50000 H23B 2 0.313823 0.039305 0.344522 11.00000 -1.50000 H23C 2 0.256368 0.111038 0.326194 11.00000 -1.50000 AFIX 0 C24 1 0.367074 0.373176 0.512945 11.00000 0.02191 0.03383 = 0.02021 -0.00597 0.01211 -0.00423 AFIX 13 H24 2 0.402292 0.419747 0.528032 11.00000 -1.20000 AFIX 0 C25 1 0.375147 0.293190 0.561959 11.00000 0.02456 0.03625 = 0.01905 -0.00596 0.01042 0.00016 C26 1 0.433432 0.264592 0.601007 11.00000 0.02510 0.06175 = 0.02404 -0.00663 0.00980 0.00504 AFIX 43 H26 2 0.467011 0.296630 0.598193 11.00000 -1.20000 AFIX 0 C27 1 0.442091 0.188962 0.644048 11.00000 0.04159 0.06232 = 0.02994 0.00276 0.01111 0.01802 AFIX 43 H27 2 0.481335 0.170654 0.669509 11.00000 -1.20000 AFIX 0 C28 1 0.392802 0.140538 0.649401 11.00000 0.06493 0.04216 = 0.03369 0.00407 0.01864 0.00858 AFIX 43 H28 2 0.398683 0.090240 0.678407 11.00000 -1.20000 AFIX 0 C29 1 0.334820 0.168102 0.611013 11.00000 0.05026 0.03626 = 0.03096 -0.00176 0.01815 -0.00706 AFIX 43 H29 2 0.301398 0.135946 0.614089 11.00000 -1.20000 AFIX 0 C30 1 0.326015 0.243874 0.567630 11.00000 0.02982 0.03109 = 0.02247 -0.00199 0.01084 -0.00413 AFIX 43 H30 2 0.286695 0.261662 0.542123 11.00000 -1.20000 AFIX 0 C31 1 0.310602 0.440749 0.498886 11.00000 0.02586 0.03004 = 0.02517 -0.00133 0.01513 -0.00274 C32 1 0.266265 0.452832 0.442060 11.00000 0.03677 0.05213 = 0.02903 -0.00251 0.01639 0.00579 AFIX 43 H32 2 0.270425 0.418943 0.410364 11.00000 -1.20000 AFIX 0 C33 1 0.215504 0.515273 0.431950 11.00000 0.03984 0.05262 = 0.03656 0.00776 0.01593 0.01308 AFIX 43 H33 2 0.185772 0.522078 0.393755 11.00000 -1.20000 AFIX 0 C34 1 0.209389 0.567068 0.478729 11.00000 0.04558 0.03655 = 0.04533 0.00830 0.02566 0.00973 AFIX 43 H34 2 0.175363 0.608182 0.472052 11.00000 -1.20000 AFIX 0 C35 1 0.253680 0.557742 0.535173 11.00000 0.04960 0.03435 = 0.04621 -0.00513 0.02762 0.00467 AFIX 43 H35 2 0.249835 0.593073 0.566607 11.00000 -1.20000 AFIX 0 C36 1 0.304008 0.495571 0.545027 11.00000 0.03417 0.03384 = 0.03112 -0.00612 0.01409 0.00190 AFIX 43 H36 2 0.333987 0.490318 0.583192 11.00000 -1.20000 AFIX 0 C37 1 0.562451 0.619316 0.525735 11.00000 0.02244 0.01933 = 0.01737 -0.00046 0.00892 -0.00176 C38 1 0.602968 0.649472 0.500172 11.00000 0.02354 0.02190 = 0.01666 0.00146 0.01046 0.00126 C39 1 0.649092 0.718621 0.531654 11.00000 0.02413 0.02762 = 0.02186 -0.00064 0.01299 -0.00266 AFIX 43 H39 2 0.675438 0.741653 0.514721 11.00000 -1.20000 AFIX 0 C40 1 0.656949 0.754409 0.587934 11.00000 0.02338 0.02846 = 0.02216 -0.00347 0.01179 -0.00501 C41 1 0.618700 0.715744 0.613771 11.00000 0.02640 0.02866 = 0.01746 -0.00347 0.01133 -0.00452 AFIX 43 H41 2 0.625925 0.733976 0.652688 11.00000 -1.20000 AFIX 0 C42 1 0.569790 0.650314 0.582736 11.00000 0.02367 0.02471 = 0.01631 -0.00093 0.01083 -0.00236 C43 1 0.598991 0.602236 0.441658 11.00000 0.02229 0.02462 = 0.01616 -0.00057 0.01107 -0.00021 AFIX 13 H43 2 0.559323 0.567790 0.424287 11.00000 -1.20000 AFIX 0 C44 1 0.599477 0.683804 0.396425 11.00000 0.02672 0.02222 = 0.01898 -0.00032 0.01208 -0.00028 C45 1 0.544966 0.732253 0.361982 11.00000 0.02932 0.03830 = 0.02843 0.00774 0.01497 0.00409 AFIX 43 H45 2 0.510179 0.716932 0.368561 11.00000 -1.20000 AFIX 0 C46 1 0.541427 0.803300 0.317806 11.00000 0.03562 0.04452 = 0.03345 0.01577 0.01552 0.00946 AFIX 43 H46 2 0.504431 0.834292 0.295018 11.00000 -1.20000 AFIX 0 C47 1 0.593069 0.827923 0.307741 11.00000 0.04690 0.03016 = 0.02646 0.00680 0.02132 0.00381 AFIX 43 H47 2 0.590834 0.874844 0.278086 11.00000 -1.20000 AFIX 0 C48 1 0.647900 0.781731 0.342416 11.00000 0.03841 0.03043 = 0.03255 0.00061 0.02213 -0.00405 AFIX 43 H48 2 0.682800 0.798171 0.336287 11.00000 -1.20000 AFIX 0 C49 1 0.650995 0.710763 0.386425 11.00000 0.02734 0.03454 = 0.02797 0.00450 0.01441 -0.00093 AFIX 43 H49 2 0.688183 0.680777 0.409594 11.00000 -1.20000 AFIX 0 C50 1 0.646554 0.516789 0.452585 11.00000 0.02399 0.02653 = 0.01653 0.00166 0.01103 0.00185 C51 1 0.627772 0.417278 0.431712 11.00000 0.03152 0.02673 = 0.02526 0.00021 0.01322 0.00242 AFIX 43 H51 2 0.586454 0.403715 0.412076 11.00000 -1.20000 AFIX 0 C52 1 0.669300 0.337113 0.439443 11.00000 0.03903 0.02823 = 0.03295 0.00200 0.01131 0.00838 AFIX 43 H52 2 0.655520 0.270791 0.425432 11.00000 -1.20000 AFIX 0 C53 1 0.731108 0.355891 0.467958 11.00000 0.03613 0.04065 = 0.03352 0.00658 0.01537 0.01479 AFIX 43 H53 2 0.759073 0.302737 0.473109 11.00000 -1.20000 AFIX 0 C54 1 0.750509 0.455189 0.488652 11.00000 0.02783 0.04713 = 0.03248 0.00594 0.01284 0.00714 AFIX 43 H54 2 0.791909 0.468916 0.507267 11.00000 -1.20000 AFIX 0 C55 1 0.708943 0.534623 0.481977 11.00000 0.02592 0.03295 = 0.02688 0.00088 0.01095 0.00165 AFIX 43 H55 2 0.722787 0.600287 0.497221 11.00000 -1.20000 AFIX 0 C56 1 0.705234 0.833195 0.620442 11.00000 0.02776 0.04040 = 0.02546 -0.01065 0.01387 -0.01211 AFIX 137 H56A 2 0.688787 0.883905 0.638752 11.00000 -1.50000 H56B 2 0.718638 0.867128 0.592875 11.00000 -1.50000 H56C 2 0.739036 0.798741 0.650408 11.00000 -1.50000 AFIX 0 C57 1 0.525254 0.616880 0.609461 11.00000 0.02716 0.02683 = 0.01907 -0.00129 0.01352 -0.00474 AFIX 13 H57 2 0.503784 0.555938 0.586874 11.00000 -1.20000 AFIX 0 C58 1 0.558046 0.581237 0.673583 11.00000 0.02725 0.02986 = 0.02267 0.00362 0.01570 0.00118 C59 1 0.574311 0.477224 0.684887 11.00000 0.04373 0.03160 = 0.03378 0.00123 0.02380 -0.00014 AFIX 43 H59 2 0.563648 0.430210 0.653587 11.00000 -1.20000 AFIX 0 C60 1 0.606504 0.442993 0.742855 11.00000 0.05120 0.04139 = 0.04292 0.01552 0.02806 0.01586 AFIX 43 H60 2 0.617240 0.373311 0.750152 11.00000 -1.20000 AFIX 0 C61 1 0.622520 0.512837 0.789635 11.00000 0.03792 0.05271 = 0.03266 0.01717 0.02040 0.01182 AFIX 43 H61 2 0.644672 0.490208 0.828227 11.00000 -1.20000 AFIX 0 C62 1 0.605594 0.616188 0.778995 11.00000 0.03491 0.04517 = 0.02189 0.00493 0.01286 0.00027 AFIX 43 H62 2 0.616271 0.662888 0.810445 11.00000 -1.20000 AFIX 0 C63 1 0.572518 0.650342 0.721105 11.00000 0.03151 0.03033 = 0.01932 0.00293 0.01177 0.00107 AFIX 43 H63 2 0.560081 0.719332 0.714161 11.00000 -1.20000 AFIX 0 C64 1 0.476907 0.698348 0.603003 11.00000 0.02197 0.03430 = 0.01714 -0.00014 0.00856 -0.00188 C65 1 0.428573 0.669231 0.618338 11.00000 0.02650 0.04729 = 0.03069 0.00460 0.01519 -0.00404 AFIX 43 H65 2 0.426775 0.601846 0.631313 11.00000 -1.20000 AFIX 0 C66 1 0.383463 0.739882 0.614348 11.00000 0.02401 0.06063 = 0.03813 0.00456 0.01626 0.00120 AFIX 43 H66 2 0.351403 0.719277 0.624219 11.00000 -1.20000 AFIX 0 C67 1 0.385683 0.841049 0.595769 11.00000 0.02988 0.05691 = 0.03292 0.01039 0.01332 0.01169 AFIX 43 H67 2 0.355992 0.888837 0.594349 11.00000 -1.20000 AFIX 0 C68 1 0.432772 0.870453 0.579254 11.00000 0.03232 0.04709 = 0.03174 0.01269 0.01443 0.00978 AFIX 43 H68 2 0.434212 0.937755 0.565998 11.00000 -1.20000 AFIX 0 C69 1 0.477794 0.798858 0.582612 11.00000 0.02896 0.03967 = 0.02644 0.00677 0.01499 0.00251 AFIX 43 H69 2 0.508836 0.818708 0.571036 11.00000 -1.20000 AFIX 0 C70 1 0.572173 0.218200 0.573087 11.00000 0.02595 0.02642 = 0.02774 0.00563 0.01291 0.00377 C71 1 0.549910 0.123310 0.535814 11.00000 0.03424 0.02486 = 0.02756 0.00675 0.01851 0.00557 C72 1 0.488510 0.105676 0.503951 11.00000 0.03484 0.03456 = 0.02654 0.00119 0.01332 -0.00395 AFIX 43 H72 2 0.460329 0.152914 0.506697 11.00000 -1.20000 AFIX 0 C73 1 0.468210 0.018353 0.467831 11.00000 0.04803 0.04151 = 0.02907 -0.00074 0.01360 -0.01300 AFIX 43 H73 2 0.426737 0.007304 0.447324 11.00000 -1.20000 AFIX 0 C74 1 0.509555 -0.052362 0.462254 11.00000 0.06767 0.03105 = 0.02851 -0.00248 0.02013 -0.00626 AFIX 43 H74 2 0.495972 -0.110535 0.438064 11.00000 -1.20000 AFIX 0 C75 1 0.570751 -0.035316 0.492905 11.00000 0.06455 0.03174 = 0.03153 0.00271 0.02720 0.00982 AFIX 43 H75 2 0.598720 -0.081456 0.488753 11.00000 -1.20000 AFIX 0 C76 1 0.591021 0.050092 0.529917 11.00000 0.04001 0.03632 = 0.03022 0.00513 0.01993 0.00973 AFIX 43 H76 2 0.632519 0.059343 0.551284 11.00000 -1.20000 AFIX 0 C77 1 0.608593 0.210807 0.631640 11.00000 0.02537 0.02723 = 0.03100 0.00165 0.01215 0.00140 AFIX 43 H77 2 0.624676 0.273236 0.650418 11.00000 -1.20000 AFIX 0 C78 1 0.626271 0.117147 0.669766 11.00000 0.02868 0.02948 = 0.02315 0.00103 0.01459 0.00411 C79 1 0.587477 0.032155 0.661642 11.00000 0.03467 0.02811 = 0.02465 -0.00067 0.01541 0.00013 AFIX 43 H79 2 0.549804 0.031847 0.629904 11.00000 -1.20000 AFIX 0 C80 1 0.604519 -0.052377 0.700554 11.00000 0.04515 0.03096 = 0.03001 0.00102 0.02422 0.00053 AFIX 43 H80 2 0.578108 -0.108335 0.694317 11.00000 -1.20000 AFIX 0 C81 1 0.660211 -0.053906 0.748272 11.00000 0.04656 0.03685 = 0.03021 0.00973 0.02368 0.01383 AFIX 43 H81 2 0.671485 -0.110596 0.773886 11.00000 -1.20000 AFIX 0 C82 1 0.698887 0.030292 0.757283 11.00000 0.03414 0.04627 = 0.02627 0.00810 0.01346 0.01102 AFIX 43 H82 2 0.736360 0.030218 0.789294 11.00000 -1.20000 AFIX 0 C83 1 0.682203 0.114963 0.718900 11.00000 0.02618 0.03923 = 0.02854 0.00479 0.01219 0.00544 AFIX 43 H83 2 0.708571 0.171159 0.725903 11.00000 -1.20000 AFIX 0 O1 5 0.791930 0.482230 0.710803 11.00000 0.07169 0.10293 = 0.06959 0.00148 0.01454 -0.00425 C84 1 0.730823 0.510661 0.685471 11.00000 0.06054 0.10439 = 0.05102 0.01002 0.01610 0.01430 AFIX 23 H84A 2 0.727379 0.585409 0.679865 11.00000 -1.20000 H84B 2 0.711034 0.491205 0.711688 11.00000 -1.20000 AFIX 0 C85 1 0.700073 0.456203 0.625970 11.00000 0.03869 0.07096 = 0.04826 0.02669 0.01780 0.00558 AFIX 23 H85A 2 0.698120 0.501540 0.593646 11.00000 -1.20000 H85B 2 0.659176 0.434845 0.619845 11.00000 -1.20000 AFIX 0 C86 1 0.740244 0.361611 0.629906 11.00000 0.04449 0.08858 = 0.05660 0.02587 0.03146 0.01511 AFIX 23 H86A 2 0.758274 0.365534 0.600814 11.00000 -1.20000 H86B 2 0.717425 0.297359 0.624275 11.00000 -1.20000 AFIX 0 C87 1 0.788865 0.370181 0.693537 11.00000 0.05873 0.11670 = 0.05468 0.03342 0.01488 0.03189 AFIX 23 H87A 2 0.777828 0.327595 0.720397 11.00000 -1.20000 H87B 2 0.827960 0.346924 0.694985 11.00000 -1.20000 AFIX 0 O2 5 0.379116 0.800726 0.376899 11.00000 0.05612 0.08429 = 0.05312 0.01559 0.01484 0.00914 C88 1 0.333000 0.798685 0.398982 11.00000 0.05263 0.06063 = 0.06766 -0.01327 0.01844 0.00927 AFIX 23 H88A 2 0.327296 0.867428 0.412233 11.00000 -1.20000 H88B 2 0.343771 0.751149 0.432293 11.00000 -1.20000 AFIX 0 C89 1 0.276875 0.763707 0.349996 11.00000 0.05794 0.15528 = 0.07426 -0.04804 0.01657 -0.00723 AFIX 23 H89A 2 0.262594 0.699355 0.360661 11.00000 -1.20000 H89B 2 0.245265 0.815778 0.341633 11.00000 -1.20000 AFIX 0 C90 1 0.291077 0.747991 0.298630 11.00000 0.08774 0.15517 = 0.05166 -0.02153 0.01823 -0.04404 AFIX 23 H90A 2 0.261193 0.781845 0.264063 11.00000 -1.20000 H90B 2 0.291869 0.674427 0.290238 11.00000 -1.20000 AFIX 0 C91 1 0.353213 0.795991 0.314514 11.00000 0.10589 0.08263 = 0.06116 -0.00397 0.03982 0.00501 AFIX 23 H91A 2 0.377819 0.753358 0.299970 11.00000 -1.20000 H91B 2 0.349698 0.865026 0.297540 11.00000 -1.20000 AFIX 0 HKLF 4 REM JDEBT08_a.res in Cc REM R1 = 0.0613 for 20150 Fo > 4sig(Fo) and 0.0798 for all 24502 data REM 867 parameters refined using 2 restraints END WGHT 0.0761 9.6035 REM Highest difference peak 1.151, deepest hole -1.207, 1-sigma level 0.080 Q1 1 0.7583 0.3876 0.7175 11.00000 0.05 1.15 Q2 1 0.5387 0.4356 0.5285 11.00000 0.05 0.74 Q3 1 0.5605 0.3801 0.5198 11.00000 0.05 0.65 Q4 1 0.5441 0.2564 0.5332 11.00000 0.05 0.64 Q5 1 0.5438 -0.0312 0.5288 11.00000 0.05 0.57 Q6 1 0.5622 0.3147 0.5197 11.00000 0.05 0.53 Q7 1 0.3205 0.8164 0.2749 11.00000 0.05 0.51 REM The information below was added by Olex2. REM REM R1 = 0.0613 for 20150 Fo > 4sig(Fo) and 0.0798 for all 106383 data REM 867 parameters refined using n/a restraints REM Highest difference peak 1.15, deepest hole -1.21 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0798 REM R1_gt = 0.0613 REM wR_ref = 0.1696 REM GOOF = 1.049 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 106383 REM Reflections_gt = 20150 REM Parameters = 867 REM Hole = -1.21 REM Peak = 1.15 REM Flack = 0.037(4) ; _cod_data_source_file d1sc01911b3.cif _cod_data_source_block jdebt08_a _cod_database_code 1564271 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.934 _shelx_estimated_absorpt_t_min 0.898 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C10(H10), C24(H24), C43(H43), C57(H57) 2.b Secondary CH2 refined with riding coordinates: C84(H84A,H84B), C85(H85A,H85B), C86(H86A,H86B), C87(H87A,H87B), C88(H88A, H88B), C89(H89A,H89B), C90(H90A,H90B), C91(H91A,H91B) 2.c Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C6(H6), C8(H8), C12(H12), C13(H13), C14(H14), C15(H15), C16(H16), C18(H18), C19(H19), C20(H20), C21(H21), C22(H22), C26(H26), C27(H27), C28(H28), C29(H29), C30(H30), C32(H32), C33(H33), C34(H34), C35(H35), C36(H36), C39(H39), C41(H41), C45(H45), C46(H46), C47(H47), C48(H48), C49(H49), C51(H51), C52(H52), C53(H53), C54(H54), C55(H55), C59(H59), C60(H60), C61(H61), C62(H62), C63(H63), C65(H65), C66(H66), C67(H67), C68(H68), C69(H69), C72(H72), C73(H73), C74(H74), C75(H75), C76(H76), C77(H77), C79(H79), C80(H80), C81(H81), C82(H82), C83(H83) 2.d Idealised Me refined as rotating group: C23(H23A,H23B,H23C), C56(H56A,H56B,H56C) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.54214(2) 0.34570(3) 0.53104(2) 0.02286(9) Uani 1 1 d . . . . . N1 N 0.43754(13) 0.4533(2) 0.44849(12) 0.0213(5) Uani 1 1 d . . . . . N2 N 0.50731(12) 0.5655(2) 0.48970(12) 0.0194(5) Uani 1 1 d . . . . . C1 C 0.49625(14) 0.4619(2) 0.48766(13) 0.0186(5) Uani 1 1 d . . . . . C2 C 0.41310(16) 0.5500(3) 0.42635(15) 0.0248(6) Uani 1 1 d . . . . . H2 H 0.3740 0.5635 0.3986 0.030 Uiso 1 1 calc R U . . . C3 C 0.45690(16) 0.6201(3) 0.45285(15) 0.0250(6) Uani 1 1 d . . . . . H3 H 0.4539 0.6918 0.4475 0.030 Uiso 1 1 calc R U . . . C4 C 0.40436(15) 0.3575(3) 0.42884(13) 0.0213(6) Uani 1 1 d . . . . . C5 C 0.40696(15) 0.3072(3) 0.37921(14) 0.0218(6) Uani 1 1 d . . . . . C6 C 0.37097(16) 0.2197(3) 0.35744(15) 0.0259(6) Uani 1 1 d . . . . . H6 H 0.3721 0.1856 0.3244 0.031 Uiso 1 1 calc R U . . . C7 C 0.33313(17) 0.1819(3) 0.38396(16) 0.0273(6) Uani 1 1 d . . . . . C8 C 0.33394(17) 0.2311(3) 0.43489(15) 0.0274(7) Uani 1 1 d . . . . . H8 H 0.3105 0.2039 0.4540 0.033 Uiso 1 1 calc R U . . . C9 C 0.36878(15) 0.3196(3) 0.45820(14) 0.0235(6) Uani 1 1 d . . . . . C10 C 0.44943(15) 0.3465(3) 0.35093(14) 0.0207(5) Uani 1 1 d . . . . . H10 H 0.4832 0.3813 0.3825 0.025 Uiso 1 1 calc R U . . . C11 C 0.47691(16) 0.2556(3) 0.33021(15) 0.0248(6) Uani 1 1 d . . . . . C12 C 0.51907(19) 0.1923(3) 0.37284(17) 0.0318(8) Uani 1 1 d . . . . . H12 H 0.5306 0.2069 0.4130 0.038 Uiso 1 1 calc R U . . . C13 C 0.5439(2) 0.1072(4) 0.3553(2) 0.0414(10) Uani 1 1 d . . . . . H13 H 0.5717 0.0647 0.3838 0.050 Uiso 1 1 calc R U . . . C14 C 0.5275(2) 0.0857(3) 0.2959(2) 0.0416(10) Uani 1 1 d . . . . . H14 H 0.5446 0.0293 0.2845 0.050 Uiso 1 1 calc R U . . . C15 C 0.4855(2) 0.1479(3) 0.2535(2) 0.0365(9) Uani 1 1 d . . . . . H15 H 0.4743 0.1331 0.2134 0.044 Uiso 1 1 calc R U . . . C16 C 0.46004(18) 0.2324(3) 0.27028(16) 0.0289(7) Uani 1 1 d . . . . . H16 H 0.4316 0.2738 0.2415 0.035 Uiso 1 1 calc R U . . . C17 C 0.42066(16) 0.4274(3) 0.30208(14) 0.0233(6) Uani 1 1 d . . . . . C18 C 0.45886(18) 0.4955(3) 0.28876(17) 0.0300(7) Uani 1 1 d . . . . . H18 H 0.5006 0.4926 0.3108 0.036 Uiso 1 1 calc R U . . . C19 C 0.4358(2) 0.5674(3) 0.24329(19) 0.0356(8) Uani 1 1 d . . . . . H19 H 0.4619 0.6119 0.2349 0.043 Uiso 1 1 calc R U . . . C20 C 0.3738(2) 0.5730(4) 0.21041(19) 0.0383(9) Uani 1 1 d . . . . . H20 H 0.3581 0.6215 0.1800 0.046 Uiso 1 1 calc R U . . . C21 C 0.3351(2) 0.5061(4) 0.2230(2) 0.0399(9) Uani 1 1 d . . . . . H21 H 0.2934 0.5096 0.2008 0.048 Uiso 1 1 calc R U . . . C22 C 0.35841(18) 0.4335(3) 0.26872(18) 0.0312(7) Uani 1 1 d . . . . . H22 H 0.3322 0.3889 0.2770 0.037 Uiso 1 1 calc R U . . . C23 C 0.2927(2) 0.0891(4) 0.3586(2) 0.0385(9) Uani 1 1 d . . . . . H23A H 0.2822 0.0579 0.3888 0.058 Uiso 1 1 calc R U . . . H23B H 0.3138 0.0393 0.3445 0.058 Uiso 1 1 calc R U . . . H23C H 0.2564 0.1110 0.3262 0.058 Uiso 1 1 calc R U . . . C24 C 0.36707(15) 0.3732(3) 0.51294(15) 0.0241(6) Uani 1 1 d . . . . . H24 H 0.4023 0.4197 0.5280 0.029 Uiso 1 1 calc R U . . . C25 C 0.37515(16) 0.2932(3) 0.56196(15) 0.0261(6) Uani 1 1 d . . . . . C26 C 0.43343(18) 0.2646(4) 0.60101(17) 0.0369(9) Uani 1 1 d . . . . . H26 H 0.4670 0.2966 0.5982 0.044 Uiso 1 1 calc R U . . . C27 C 0.4421(2) 0.1890(5) 0.6440(2) 0.0456(11) Uani 1 1 d . . . . . H27 H 0.4813 0.1707 0.6695 0.055 Uiso 1 1 calc R U . . . C28 C 0.3928(3) 0.1405(4) 0.6494(2) 0.0472(11) Uani 1 1 d . . . . . H28 H 0.3987 0.0902 0.6784 0.057 Uiso 1 1 calc R U . . . C29 C 0.3348(2) 0.1681(3) 0.6110(2) 0.0385(9) Uani 1 1 d . . . . . H29 H 0.3014 0.1359 0.6141 0.046 Uiso 1 1 calc R U . . . C30 C 0.32602(18) 0.2439(3) 0.56763(16) 0.0276(7) Uani 1 1 d . . . . . H30 H 0.2867 0.2617 0.5421 0.033 Uiso 1 1 calc R U . . . C31 C 0.31060(16) 0.4407(3) 0.49889(16) 0.0254(6) Uani 1 1 d . . . . . C32 C 0.2663(2) 0.4528(4) 0.44206(19) 0.0383(9) Uani 1 1 d . . . . . H32 H 0.2704 0.4189 0.4104 0.046 Uiso 1 1 calc R U . . . C33 C 0.2155(2) 0.5153(4) 0.4320(2) 0.0427(10) Uani 1 1 d . . . . . H33 H 0.1858 0.5221 0.3938 0.051 Uiso 1 1 calc R U . . . C34 C 0.2094(2) 0.5671(4) 0.4787(2) 0.0401(9) Uani 1 1 d . . . . . H34 H 0.1754 0.6082 0.4721 0.048 Uiso 1 1 calc R U . . . C35 C 0.2537(2) 0.5577(4) 0.5352(2) 0.0407(9) Uani 1 1 d . . . . . H35 H 0.2498 0.5931 0.5666 0.049 Uiso 1 1 calc R U . . . C36 C 0.30401(19) 0.4956(3) 0.54503(18) 0.0327(8) Uani 1 1 d . . . . . H36 H 0.3340 0.4903 0.5832 0.039 Uiso 1 1 calc R U . . . C37 C 0.56245(15) 0.6193(2) 0.52574(14) 0.0194(5) Uani 1 1 d . . . . . C38 C 0.60297(15) 0.6495(2) 0.50017(13) 0.0199(5) Uani 1 1 d . . . . . C39 C 0.64909(16) 0.7186(3) 0.53165(15) 0.0233(6) Uani 1 1 d . . . . . H39 H 0.6754 0.7417 0.5147 0.028 Uiso 1 1 calc R U . . . C40 C 0.65695(16) 0.7544(3) 0.58793(15) 0.0238(6) Uani 1 1 d . . . . . C41 C 0.61870(16) 0.7157(3) 0.61377(14) 0.0233(6) Uani 1 1 d . . . . . H41 H 0.6259 0.7340 0.6527 0.028 Uiso 1 1 calc R U . . . C42 C 0.56979(15) 0.6503(2) 0.58274(14) 0.0206(5) Uani 1 1 d . . . . . C43 C 0.59899(15) 0.6022(3) 0.44166(13) 0.0199(5) Uani 1 1 d . . . . . H43 H 0.5593 0.5678 0.4243 0.024 Uiso 1 1 calc R U . . . C44 C 0.59948(15) 0.6838(3) 0.39642(14) 0.0217(6) Uani 1 1 d . . . . . C45 C 0.54497(18) 0.7323(3) 0.36198(17) 0.0309(7) Uani 1 1 d . . . . . H45 H 0.5102 0.7169 0.3686 0.037 Uiso 1 1 calc R U . . . C46 C 0.5414(2) 0.8033(4) 0.3178(2) 0.0373(9) Uani 1 1 d . . . . . H46 H 0.5044 0.8343 0.2950 0.045 Uiso 1 1 calc R U . . . C47 C 0.5931(2) 0.8279(3) 0.30774(19) 0.0324(8) Uani 1 1 d . . . . . H47 H 0.5908 0.8748 0.2781 0.039 Uiso 1 1 calc R U . . . C48 C 0.64790(19) 0.7817(3) 0.34242(17) 0.0313(7) Uani 1 1 d . . . . . H48 H 0.6828 0.7982 0.3363 0.038 Uiso 1 1 calc R U . . . C49 C 0.65099(17) 0.7108(3) 0.38642(17) 0.0289(7) Uani 1 1 d . . . . . H49 H 0.6882 0.6808 0.4096 0.035 Uiso 1 1 calc R U . . . C50 C 0.64655(15) 0.5168(3) 0.45258(14) 0.0214(6) Uani 1 1 d . . . . . C51 C 0.62777(18) 0.4173(3) 0.43171(16) 0.0272(6) Uani 1 1 d . . . . . H51 H 0.5865 0.4037 0.4121 0.033 Uiso 1 1 calc R U . . . C52 C 0.6693(2) 0.3371(3) 0.43944(19) 0.0343(8) Uani 1 1 d . . . . . H52 H 0.6555 0.2708 0.4254 0.041 Uiso 1 1 calc R U . . . C53 C 0.7311(2) 0.3559(3) 0.4680(2) 0.0363(9) Uani 1 1 d . . . . . H53 H 0.7591 0.3027 0.4731 0.044 Uiso 1 1 calc R U . . . C54 C 0.75051(19) 0.4552(4) 0.48865(19) 0.0355(8) Uani 1 1 d . . . . . H54 H 0.7919 0.4689 0.5073 0.043 Uiso 1 1 calc R U . . . C55 C 0.70894(17) 0.5346(3) 0.48198(16) 0.0284(7) Uani 1 1 d . . . . . H55 H 0.7228 0.6003 0.4972 0.034 Uiso 1 1 calc R U . . . C56 C 0.70523(18) 0.8332(3) 0.62044(17) 0.0302(7) Uani 1 1 d . . . . . H56A H 0.6888 0.8839 0.6388 0.045 Uiso 1 1 calc R U . . . H56B H 0.7186 0.8671 0.5929 0.045 Uiso 1 1 calc R U . . . H56C H 0.7390 0.7987 0.6504 0.045 Uiso 1 1 calc R U . . . C57 C 0.52525(16) 0.6169(3) 0.60946(14) 0.0230(6) Uani 1 1 d . . . . . H57 H 0.5038 0.5559 0.5869 0.028 Uiso 1 1 calc R U . . . C58 C 0.55805(16) 0.5812(3) 0.67358(15) 0.0248(6) Uani 1 1 d . . . . . C59 C 0.5743(2) 0.4772(3) 0.68489(19) 0.0337(8) Uani 1 1 d . . . . . H59 H 0.5636 0.4302 0.6536 0.040 Uiso 1 1 calc R U . . . C60 C 0.6065(2) 0.4430(4) 0.7429(2) 0.0422(10) Uani 1 1 d . . . . . H60 H 0.6172 0.3733 0.7502 0.051 Uiso 1 1 calc R U . . . C61 C 0.6225(2) 0.5128(4) 0.7896(2) 0.0391(10) Uani 1 1 d . . . . . H61 H 0.6447 0.4902 0.8282 0.047 Uiso 1 1 calc R U . . . C62 C 0.60559(19) 0.6162(4) 0.77900(17) 0.0335(8) Uani 1 1 d . . . . . H62 H 0.6163 0.6629 0.8104 0.040 Uiso 1 1 calc R U . . . C63 C 0.57252(18) 0.6503(3) 0.72110(15) 0.0265(6) Uani 1 1 d . . . . . H63 H 0.5601 0.7193 0.7142 0.032 Uiso 1 1 calc R U . . . C64 C 0.47691(15) 0.6983(3) 0.60300(14) 0.0242(6) Uani 1 1 d . . . . . C65 C 0.42857(18) 0.6692(4) 0.61834(18) 0.0336(8) Uani 1 1 d . . . . . H65 H 0.4268 0.6018 0.6313 0.040 Uiso 1 1 calc R U . . . C66 C 0.38346(19) 0.7399(4) 0.6143(2) 0.0397(9) Uani 1 1 d . . . . . H66 H 0.3514 0.7193 0.6242 0.048 Uiso 1 1 calc R U . . . C67 C 0.3857(2) 0.8410(4) 0.5958(2) 0.0396(9) Uani 1 1 d . . . . . H67 H 0.3560 0.8888 0.5943 0.048 Uiso 1 1 calc R U . . . C68 C 0.4328(2) 0.8705(4) 0.57925(19) 0.0365(8) Uani 1 1 d . . . . . H68 H 0.4342 0.9378 0.5660 0.044 Uiso 1 1 calc R U . . . C69 C 0.47779(18) 0.7989(3) 0.58261(17) 0.0304(7) Uani 1 1 d . . . . . H69 H 0.5088 0.8187 0.5710 0.037 Uiso 1 1 calc R U . . . C70 C 0.57217(17) 0.2182(3) 0.57309(16) 0.0260(6) Uani 1 1 d . . . . . C71 C 0.54991(18) 0.1233(3) 0.53581(17) 0.0269(7) Uani 1 1 d . . . . . C72 C 0.48851(19) 0.1057(3) 0.50395(17) 0.0316(7) Uani 1 1 d . . . . . H72 H 0.4603 0.1529 0.5067 0.038 Uiso 1 1 calc R U . . . C73 C 0.4682(2) 0.0184(4) 0.46783(19) 0.0400(9) Uani 1 1 d . . . . . H73 H 0.4267 0.0073 0.4473 0.048 Uiso 1 1 calc R U . . . C74 C 0.5096(3) -0.0524(3) 0.46225(19) 0.0421(10) Uani 1 1 d . . . . . H74 H 0.4960 -0.1105 0.4381 0.050 Uiso 1 1 calc R U . . . C75 C 0.5708(3) -0.0353(3) 0.49290(19) 0.0400(10) Uani 1 1 d . . . . . H75 H 0.5987 -0.0815 0.4888 0.048 Uiso 1 1 calc R U . . . C76 C 0.5910(2) 0.0501(3) 0.52992(18) 0.0336(8) Uani 1 1 d . . . . . H76 H 0.6325 0.0593 0.5513 0.040 Uiso 1 1 calc R U . . . C77 C 0.60859(17) 0.2108(3) 0.63164(17) 0.0275(6) Uani 1 1 d . . . . . H77 H 0.6247 0.2732 0.6504 0.033 Uiso 1 1 calc R U . . . C78 C 0.62627(16) 0.1171(3) 0.66977(15) 0.0257(6) Uani 1 1 d . . . . . C79 C 0.58748(18) 0.0322(3) 0.66164(16) 0.0280(7) Uani 1 1 d . . . . . H79 H 0.5498 0.0318 0.6299 0.034 Uiso 1 1 calc R U . . . C80 C 0.6045(2) -0.0524(3) 0.70055(18) 0.0324(8) Uani 1 1 d . . . . . H80 H 0.5781 -0.1083 0.6943 0.039 Uiso 1 1 calc R U . . . C81 C 0.6602(2) -0.0539(3) 0.74827(18) 0.0352(8) Uani 1 1 d . . . . . H81 H 0.6715 -0.1106 0.7739 0.042 Uiso 1 1 calc R U . . . C82 C 0.6989(2) 0.0303(4) 0.75728(18) 0.0351(8) Uani 1 1 d . . . . . H82 H 0.7364 0.0302 0.7893 0.042 Uiso 1 1 calc R U . . . C83 C 0.68220(17) 0.1150(3) 0.71890(17) 0.0309(7) Uani 1 1 d . . . . . H83 H 0.7086 0.1712 0.7259 0.037 Uiso 1 1 calc R U . . . O1 O 0.7919(3) 0.4822(5) 0.7108(3) 0.0856(16) Uani 1 1 d . . . . . C84 C 0.7308(3) 0.5107(7) 0.6855(3) 0.074(2) Uani 1 1 d . . . . . H84A H 0.7274 0.5854 0.6799 0.089 Uiso 1 1 calc R U . . . H84B H 0.7110 0.4912 0.7117 0.089 Uiso 1 1 calc R U . . . C85 C 0.7001(2) 0.4562(5) 0.6260(2) 0.0524(13) Uani 1 1 d . . . . . H85A H 0.6981 0.5015 0.5936 0.063 Uiso 1 1 calc R U . . . H85B H 0.6592 0.4348 0.6198 0.063 Uiso 1 1 calc R U . . . C86 C 0.7402(3) 0.3616(6) 0.6299(3) 0.0596(16) Uani 1 1 d . . . . . H86A H 0.7583 0.3655 0.6008 0.072 Uiso 1 1 calc R U . . . H86B H 0.7174 0.2974 0.6243 0.072 Uiso 1 1 calc R U . . . C87 C 0.7889(3) 0.3702(8) 0.6935(3) 0.079(2) Uani 1 1 d . . . . . H87A H 0.7778 0.3276 0.7204 0.095 Uiso 1 1 calc R U . . . H87B H 0.8280 0.3469 0.6950 0.095 Uiso 1 1 calc R U . . . O2 O 0.3791(2) 0.8007(4) 0.3769(2) 0.0666(12) Uani 1 1 d . . . . . C88 C 0.3330(3) 0.7987(5) 0.3990(3) 0.0620(16) Uani 1 1 d . . . . . H88A H 0.3273 0.8674 0.4122 0.074 Uiso 1 1 calc R U . . . H88B H 0.3438 0.7511 0.4323 0.074 Uiso 1 1 calc R U . . . C89 C 0.2769(4) 0.7637(10) 0.3500(4) 0.099(3) Uani 1 1 d . . . . . H89A H 0.2626 0.6994 0.3607 0.119 Uiso 1 1 calc R U . . . H89B H 0.2453 0.8158 0.3416 0.119 Uiso 1 1 calc R U . . . C90 C 0.2911(5) 0.7480(10) 0.2986(4) 0.101(3) Uani 1 1 d . . . . . H90A H 0.2612 0.7818 0.2641 0.121 Uiso 1 1 calc R U . . . H90B H 0.2919 0.6744 0.2902 0.121 Uiso 1 1 calc R U . . . C91 C 0.3532(4) 0.7960(7) 0.3145(4) 0.081(2) Uani 1 1 d . . . . . H91A H 0.3778 0.7534 0.3000 0.097 Uiso 1 1 calc R U . . . H91B H 0.3497 0.8650 0.2975 0.097 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.02206(17) 0.02362(17) 0.02237(17) 0.00217(15) 0.00821(13) 0.00175(15) N1 0.0205(12) 0.0267(13) 0.0181(11) 0.0008(9) 0.0091(10) 0.0007(10) N2 0.0203(12) 0.0220(11) 0.0166(10) 0.0002(9) 0.0079(9) 0.0012(9) C1 0.0210(13) 0.0217(13) 0.0154(11) 0.0036(10) 0.0098(10) 0.0032(10) C2 0.0221(14) 0.0291(16) 0.0216(14) 0.0027(12) 0.0068(12) 0.0038(12) C3 0.0251(15) 0.0281(15) 0.0217(14) 0.0037(12) 0.0091(12) 0.0031(12) C4 0.0209(14) 0.0311(15) 0.0153(12) -0.0004(11) 0.0107(11) -0.0010(11) C5 0.0209(13) 0.0282(15) 0.0184(12) -0.0004(11) 0.0099(11) -0.0001(11) C6 0.0279(16) 0.0317(16) 0.0205(13) -0.0050(12) 0.0123(12) -0.0044(12) C7 0.0267(16) 0.0339(17) 0.0238(15) -0.0071(13) 0.0125(13) -0.0070(13) C8 0.0261(16) 0.0385(18) 0.0214(14) -0.0070(13) 0.0136(12) -0.0084(13) C9 0.0206(14) 0.0342(16) 0.0181(13) -0.0039(12) 0.0102(11) -0.0031(12) C10 0.0198(13) 0.0284(15) 0.0161(12) -0.0001(10) 0.0094(11) -0.0011(11) C11 0.0266(16) 0.0312(16) 0.0220(14) 0.0043(12) 0.0153(12) 0.0030(12) C12 0.0317(18) 0.042(2) 0.0265(16) 0.0093(14) 0.0161(14) 0.0074(15) C13 0.043(2) 0.045(2) 0.047(2) 0.0202(19) 0.031(2) 0.0180(19) C14 0.056(3) 0.035(2) 0.053(3) 0.0093(18) 0.042(2) 0.0123(18) C15 0.049(3) 0.038(2) 0.034(2) -0.0011(15) 0.029(2) 0.0051(17) C16 0.0325(18) 0.0354(18) 0.0232(15) 0.0003(13) 0.0156(14) 0.0035(14) C17 0.0251(15) 0.0281(15) 0.0187(13) -0.0017(11) 0.0108(12) 0.0012(12) C18 0.0302(17) 0.0347(18) 0.0272(16) 0.0014(14) 0.0138(14) -0.0032(14) C19 0.043(2) 0.0358(19) 0.0334(19) 0.0077(15) 0.0205(17) 0.0016(16) C20 0.048(2) 0.038(2) 0.0319(19) 0.0148(16) 0.0185(18) 0.0132(17) C21 0.036(2) 0.049(2) 0.0337(19) 0.0121(18) 0.0125(17) 0.0098(18) C22 0.0271(17) 0.0381(19) 0.0301(17) 0.0047(15) 0.0132(14) 0.0028(14) C23 0.042(2) 0.046(2) 0.0349(19) -0.0140(17) 0.0218(18) -0.0178(18) C24 0.0219(14) 0.0338(16) 0.0202(13) -0.0060(12) 0.0121(12) -0.0042(12) C25 0.0246(15) 0.0363(17) 0.0190(13) -0.0060(12) 0.0104(12) 0.0002(13) C26 0.0251(17) 0.062(3) 0.0240(16) -0.0066(17) 0.0098(14) 0.0050(17) C27 0.042(2) 0.062(3) 0.0299(19) 0.0028(19) 0.0111(18) 0.018(2) C28 0.065(3) 0.042(2) 0.034(2) 0.0041(18) 0.019(2) 0.009(2) C29 0.050(3) 0.036(2) 0.0310(19) -0.0018(15) 0.0181(18) -0.0071(17) C30 0.0298(17) 0.0311(16) 0.0225(15) -0.0020(12) 0.0108(13) -0.0041(13) C31 0.0259(15) 0.0300(16) 0.0252(15) -0.0013(12) 0.0151(13) -0.0027(12) C32 0.037(2) 0.052(2) 0.0290(18) -0.0025(17) 0.0164(16) 0.0058(18) C33 0.040(2) 0.053(3) 0.037(2) 0.0078(19) 0.0159(18) 0.0131(19) C34 0.046(2) 0.037(2) 0.045(2) 0.0083(18) 0.026(2) 0.0097(17) C35 0.050(2) 0.034(2) 0.046(2) -0.0051(17) 0.028(2) 0.0047(18) C36 0.0342(19) 0.0338(18) 0.0311(18) -0.0061(14) 0.0141(15) 0.0019(15) C37 0.0224(13) 0.0193(12) 0.0174(12) -0.0005(10) 0.0089(11) -0.0018(10) C38 0.0235(14) 0.0219(13) 0.0167(12) 0.0015(10) 0.0105(11) 0.0013(10) C39 0.0241(14) 0.0276(15) 0.0219(13) -0.0006(11) 0.0130(12) -0.0027(11) C40 0.0234(14) 0.0285(15) 0.0222(13) -0.0035(12) 0.0118(12) -0.0050(11) C41 0.0264(15) 0.0287(15) 0.0175(13) -0.0035(11) 0.0113(12) -0.0045(12) C42 0.0237(14) 0.0247(14) 0.0163(12) -0.0009(10) 0.0108(11) -0.0024(11) C43 0.0223(13) 0.0246(13) 0.0162(12) -0.0006(10) 0.0111(11) -0.0002(11) C44 0.0267(15) 0.0222(13) 0.0190(13) -0.0003(10) 0.0121(12) -0.0003(11) C45 0.0293(17) 0.0383(19) 0.0284(16) 0.0077(14) 0.0150(14) 0.0041(14) C46 0.036(2) 0.045(2) 0.0335(19) 0.0158(17) 0.0155(16) 0.0095(17) C47 0.047(2) 0.0302(17) 0.0265(17) 0.0068(14) 0.0213(17) 0.0038(16) C48 0.038(2) 0.0304(17) 0.0326(18) 0.0006(14) 0.0221(16) -0.0040(14) C49 0.0273(16) 0.0345(17) 0.0280(16) 0.0045(13) 0.0144(14) -0.0009(13) C50 0.0240(14) 0.0265(14) 0.0165(12) 0.0017(11) 0.0110(11) 0.0019(11) C51 0.0315(17) 0.0267(15) 0.0253(15) 0.0002(12) 0.0132(13) 0.0024(13) C52 0.039(2) 0.0282(17) 0.0329(19) 0.0020(14) 0.0113(16) 0.0084(15) C53 0.036(2) 0.041(2) 0.0335(19) 0.0066(16) 0.0154(17) 0.0148(16) C54 0.0278(18) 0.047(2) 0.0325(19) 0.0059(17) 0.0128(16) 0.0071(16) C55 0.0259(16) 0.0330(17) 0.0269(16) 0.0009(13) 0.0110(13) 0.0017(13) C56 0.0278(17) 0.0404(19) 0.0255(15) -0.0106(14) 0.0139(14) -0.0121(14) C57 0.0272(15) 0.0268(15) 0.0191(13) -0.0013(11) 0.0135(12) -0.0047(12) C58 0.0272(15) 0.0299(16) 0.0227(14) 0.0036(12) 0.0157(13) 0.0012(12) C59 0.044(2) 0.0316(18) 0.0338(18) 0.0012(14) 0.0238(17) -0.0001(15) C60 0.051(3) 0.041(2) 0.043(2) 0.0155(19) 0.028(2) 0.0159(19) C61 0.038(2) 0.053(3) 0.0327(19) 0.0172(18) 0.0204(17) 0.0118(18) C62 0.0349(19) 0.045(2) 0.0219(15) 0.0049(15) 0.0129(14) 0.0003(16) C63 0.0315(17) 0.0303(17) 0.0193(14) 0.0029(12) 0.0118(13) 0.0011(13) C64 0.0220(14) 0.0343(17) 0.0171(12) -0.0001(12) 0.0086(11) -0.0019(12) C65 0.0265(17) 0.047(2) 0.0307(18) 0.0046(16) 0.0152(15) -0.0040(15) C66 0.0240(17) 0.061(3) 0.038(2) 0.0046(19) 0.0163(16) 0.0012(17) C67 0.0299(19) 0.057(3) 0.0329(19) 0.0104(18) 0.0133(16) 0.0117(17) C68 0.0323(19) 0.047(2) 0.0317(18) 0.0127(16) 0.0144(16) 0.0098(17) C69 0.0290(17) 0.0397(19) 0.0264(16) 0.0068(14) 0.0150(14) 0.0025(14) C70 0.0259(15) 0.0264(15) 0.0277(15) 0.0056(12) 0.0129(13) 0.0038(12) C71 0.0342(19) 0.0249(13) 0.0276(16) 0.0067(13) 0.0185(15) 0.0056(13) C72 0.0348(19) 0.0346(18) 0.0265(16) 0.0012(14) 0.0133(15) -0.0039(15) C73 0.048(2) 0.042(2) 0.0291(19) -0.0007(16) 0.0136(18) -0.0130(18) C74 0.068(3) 0.0310(19) 0.0285(18) -0.0025(15) 0.020(2) -0.0063(19) C75 0.065(3) 0.0317(19) 0.0315(19) 0.0027(15) 0.027(2) 0.0098(19) C76 0.040(2) 0.0363(19) 0.0302(17) 0.0051(15) 0.0199(16) 0.0097(16) C77 0.0254(16) 0.0272(15) 0.0310(17) 0.0016(13) 0.0122(14) 0.0014(12) C78 0.0287(16) 0.0295(16) 0.0232(14) 0.0010(12) 0.0146(13) 0.0041(12) C79 0.0347(18) 0.0281(16) 0.0247(15) -0.0007(12) 0.0154(14) 0.0001(13) C80 0.045(2) 0.0310(17) 0.0300(17) 0.0010(14) 0.0242(17) 0.0005(15) C81 0.047(2) 0.037(2) 0.0302(18) 0.0097(15) 0.0237(17) 0.0138(17) C82 0.0341(19) 0.046(2) 0.0263(17) 0.0081(15) 0.0135(15) 0.0110(16) C83 0.0262(17) 0.0392(19) 0.0285(16) 0.0048(14) 0.0122(14) 0.0054(14) O1 0.072(3) 0.103(4) 0.070(3) 0.001(3) 0.015(3) -0.004(3) C84 0.061(4) 0.104(6) 0.051(3) 0.010(4) 0.016(3) 0.014(4) C85 0.039(2) 0.071(4) 0.048(3) 0.027(3) 0.018(2) 0.006(2) C86 0.044(3) 0.089(4) 0.057(3) 0.026(3) 0.031(3) 0.015(3) C87 0.059(4) 0.117(7) 0.055(4) 0.033(4) 0.015(3) 0.032(4) O2 0.056(2) 0.084(3) 0.053(2) 0.016(2) 0.015(2) 0.009(2) C88 0.053(3) 0.061(4) 0.068(4) -0.013(3) 0.018(3) 0.009(3) C89 0.058(4) 0.155(9) 0.074(5) -0.048(6) 0.017(4) -0.007(5) C90 0.088(6) 0.155(9) 0.052(4) -0.022(5) 0.018(4) -0.044(6) C91 0.106(6) 0.083(5) 0.061(4) -0.004(4) 0.040(4) 0.005(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u -2 0 0 -0.88 0.87 -4 0 0 574.29 55.44 -4 0 0 643.45 55.45 -4 0 0 601.3 55.45 -4 0 0 555.4 55.44 -4 0 0 521.74 55.43 4 0 0 662.79 55.45 4 0 0 584.09 55.44 -6 0 0 212.83 20.07 -6 0 0 211.43 20.08 -6 0 0 195.23 20.07 -6 0 0 216.97 20.06 -6 0 0 220.57 20.06 -6 0 0 185.22 20.06 -6 0 0 206.76 20.05 -6 0 0 196.7 20.05 -6 0 0 185.66 20.06 6 0 0 240.66 20.08 6 0 0 241.56 20.07 6 0 0 246.85 20.06 6 0 0 217.21 20.06 -8 0 0 76.38 7.57 -8 0 0 71.1 7.57 -8 0 0 79.25 7.56 -8 0 0 77.36 7.56 -8 0 0 69.61 7.55 -8 0 0 77.33 7.58 8 0 0 95.07 7.58 8 0 0 96.16 7.56 -10 0 0 102.05 9.4 -10 0 0 98.59 9.39 -10 0 0 88.43 9.37 -10 0 0 102.88 9.42 -10 0 0 88.96 9.38 10 0 0 106.18 9.42 10 0 0 108.77 9.38 10 0 0 106.3 9.4 10 0 0 95.91 9.38 -12 0 0 248.65 22.67 -12 0 0 253.87 22.72 -12 0 0 228.04 22.66 -12 0 0 250.5 22.66 12 0 0 203.8 22.67 12 0 0 255.36 22.71 12 0 0 249.67 22.66 -14 0 0 24.3 2.18 -14 0 0 23.64 2.18 -14 0 0 20.14 2.26 -14 0 0 24.2 2.26 -14 0 0 21.4 2.12 14 0 0 19.4 2.27 14 0 0 20.59 2.14 -16 0 0 57.9 5.64 -16 0 0 62.76 5.73 -16 0 0 57.2 5.64 -16 0 0 59.22 5.73 16 0 0 59.77 5.74 16 0 0 57.88 5.61 -18 0 0 237.16 22.24 -18 0 0 225.08 22.14 -18 0 0 240.24 22.27 -18 0 0 226.74 22.19 -18 0 0 243.67 22.2 18 0 0 237.83 22.17 18 0 0 241.63 22.28 -20 0 0 27.96 2.84 -20 0 0 28.3 3.03 -20 0 0 29.98 2.92 -20 0 0 30.89 3.05 -20 0 0 28.05 2.91 20 0 0 33.34 2.88 20 0 0 27.82 3.06 -22 0 0 16.64 1.98 -22 0 0 18.92 1.98 -22 0 0 16.24 1.79 -22 0 0 15.18 1.76 -22 0 0 16.73 1.67 22 0 0 18.04 2.02 -24 0 0 43.71 4.09 -24 0 0 45.71 3.98 -24 0 0 40.76 4.34 24 0 0 34.23 3.89 -26 0 0 1.55 1.69 -30 0 0 31.91 3.44 -32 0 0 0.72 1.51 32 0 0 0.13 2.64 33 -1 0 0.32 0.97 -33 1 0 0.13 0.99 -33 1 0 0.22 1.09 -29 1 0 12.58 1.82 27 -1 0 0.85 0.99 -27 1 0 5.04 1.22 25 -1 0 3.16 0.6 -25 1 0 2.84 1.82 -25 1 0 6.38 1.06 -25 1 0 3.92 1.35 23 -1 0 3.05 1.92 -23 1 0 6.71 0.98 -23 1 0 6.48 0.95 -23 1 0 9.55 1.26 -23 1 0 7.37 1.26 21 -1 0 53.48 5.54 -21 1 0 54.84 5.4 -21 1 0 59.41 5.49 -21 1 0 52.26 5.5 -21 1 0 60.45 5.4 19 -1 0 6.46 0.93 19 -1 0 6.39 1.2 -19 1 0 7.74 0.95 -19 1 0 9.57 1.16 -19 1 0 8.78 1.1 -19 1 0 7.25 0.82 -19 1 0 7.45 0.94 17 -1 0 54.54 4.52 -17 1 0 46.96 4.5 -17 1 0 48.41 4.68 -17 1 0 43.17 4.47 -17 1 0 43.6 4.56 15 -1 0 10.69 1.27 -15 1 0 8.74 0.94 -15 1 0 6.08 0.84 -15 1 0 8.32 0.95 -15 1 0 3.92 1.17 -15 1 0 7.57 0.95 13 -1 0 4.94 0.75 13 -1 0 4.84 0.55 13 -1 0 5.03 0.9 -13 1 0 2.64 0.82 -13 1 0 3.04 0.63 -13 1 0 2.93 0.8 -13 1 0 3.99 0.64 -13 1 0 3.34 0.55 11 -1 0 138.68 14.93 11 -1 0 172.37 15 11 -1 0 169.19 14.95 11 -1 0 167.14 14.96 -11 1 0 171.07 14.95 -11 1 0 143.39 14.97 -11 1 0 158.35 14.95 -11 1 0 175.78 14.93 -11 1 0 137.18 14.92 -11 1 0 157.62 14.94 9 -1 0 185.67 16.28 9 -1 0 178.86 16.25 9 -1 0 176.76 16.25 9 -1 0 174.84 16.23 9 -1 0 160.12 16.24 -9 1 0 175.02 16.26 -9 1 0 159.52 16.23 -9 1 0 168.13 16.25 -9 1 0 169.21 16.24 -9 1 0 172.56 16.24 -9 1 0 179.5 16.23 -9 1 0 174.87 16.26 7 -1 0 21.4 1.87 7 -1 0 23.18 1.88 7 -1 0 22.37 1.88 -7 1 0 17.22 1.87 -7 1 0 19.26 1.88 -7 1 0 17.98 1.87 -7 1 0 16.69 1.86 -7 1 0 18.26 1.86 -7 1 0 19.03 1.85 -7 1 0 17.38 1.87 5 -1 0 370.21 33.02 5 -1 0 329.93 33.02 5 -1 0 368.94 33 5 -1 0 395.58 33.04 5 -1 0 393.85 33.02 -5 1 0 344.87 33 -5 1 0 341.39 33.02 -5 1 0 344.26 33.02 -5 1 0 308.81 33.01 -5 1 0 361.43 33.03 -5 1 0 348.31 33.02 -5 1 0 315.53 33.02 3 -1 0 59.94 6.48 3 -1 0 69.11 6.48 3 -1 0 66.96 6.5 3 -1 0 64.83 6.48 -3 1 0 72.44 6.48 -3 1 0 65.73 6.48 -3 1 0 72.83 6.5 -3 1 0 77.27 6.48 -3 -1 0 77.19 6.41 -3 -1 0 69.79 6.37 -3 -1 0 75.1 6.39 -3 -1 0 74.77 6.38 -3 -1 0 71.26 6.37 -3 -1 0 68.54 6.37 -3 -1 0 70.53 6.37 3 1 0 65.36 6.37 3 1 0 63.14 6.37 3 1 0 61.5 6.39 3 1 0 60.41 6.36 3 1 0 62.98 6.38 3 1 0 64.28 6.37 3 1 0 60.82 6.37 -5 -1 0 333.2 32.51 -5 -1 0 349.43 32.52 -5 -1 0 354.8 32.52 -5 -1 0 324.49 32.51 -5 -1 0 311.39 32.51 -5 -1 0 338.65 32.52 -5 -1 0 334.67 32.54 5 1 0 335.49 32.51 5 1 0 379.41 32.53 5 1 0 381.03 32.53 5 1 0 347.68 32.52 5 1 0 368.9 32.54 -7 -1 0 16.69 1.84 -7 -1 0 18.11 1.84 -7 -1 0 17.69 1.88 -7 -1 0 16.36 1.82 -7 -1 0 20.08 1.85 -7 -1 0 19.3 1.86 -7 -1 0 17.26 1.85 7 1 0 21.53 1.85 7 1 0 20.92 1.84 7 1 0 23.41 1.89 -9 -1 0 166.07 16.02 -9 -1 0 180.84 16.05 -9 -1 0 159.41 16.04 -9 -1 0 186.1 16.05 -9 -1 0 175 16.08 -9 -1 0 179.31 16.06 9 1 0 163.68 16.02 9 1 0 168.17 16.05 9 1 0 161.72 16.07 9 1 0 157.65 16.03 9 1 0 181.5 16.07 -11 -1 0 144.32 15.23 -11 -1 0 160.27 15.21 -11 -1 0 175.4 15.31 -11 -1 0 165 15.25 -11 -1 0 182.09 15.26 11 1 0 148.04 15.27 11 1 0 165.4 15.25 11 1 0 144.89 15.22 11 1 0 175.03 15.24 -13 -1 0 2.68 0.56 -13 -1 0 1.97 0.39 -13 -1 0 2.25 0.58 -13 -1 0 2 0.4 -13 -1 0 2.89 0.76 13 1 0 1.23 0.46 13 1 0 4.23 0.75 -15 -1 0 6.38 1.12 -15 -1 0 6.58 1.01 -15 -1 0 6.2 0.98 -15 -1 0 6.44 1.18 -15 -1 0 7.43 0.87 15 1 0 11.17 1.21 15 1 0 9.5 0.94 15 1 0 9.59 0.88 -17 -1 0 49.29 4.86 -17 -1 0 47.37 4.97 -17 -1 0 45.68 4.85 -17 -1 0 48.04 4.95 17 1 0 58.57 4.98 17 1 0 53.16 4.78 -19 -1 0 7.95 1.26 -19 -1 0 8.45 1.15 -19 -1 0 7.26 0.83 -19 -1 0 8.9 1.22 19 1 0 2.65 1.56 -21 -1 0 55.07 5.37 -21 -1 0 53.01 5.29 -21 -1 0 59.07 5.5 -21 -1 0 56.49 5.47 21 1 0 56.18 5.48 -23 -1 0 5.11 1.7 -23 -1 0 3.32 0.81 23 1 0 3.08 0.76 -25 -1 0 2.94 1.68 -27 -1 0 1.49 1.66 -29 -1 0 11.93 1.81 -31 -1 0 8.97 1.6 -31 -1 0 0.9 2.31 -33 -1 0 0 1.55 -33 -1 0 -0.43 0.94 33 1 0 0.57 2.53 32 -2 0 0.83 2.67 -32 2 0 4.71 1.15 -30 2 0 -36.97 35.81 -28 2 0 159.54 41.53 26 -2 0 -0.2 1.89 -26 2 0 1.06 0.94 24 -2 0 5.35 1.04 -24 2 0 7.78 1.34 -24 2 0 8.71 0.98 -24 2 0 7.64 0.96 -24 2 0 5.06 1.35 22 -2 0 13.34 1.83 22 -2 0 15.46 1.59 -22 2 0 12.45 1.53 -22 2 0 15.01 1.78 -22 2 0 15.16 1.53 -22 2 0 14.37 1.69 20 -2 0 49.41 4.97 20 -2 0 42.65 5.06 -20 2 0 54.6 5.02 -20 2 0 54.93 4.93 -20 2 0 50.9 4.94 -20 2 0 56.33 5.07 18 -2 0 68.07 6.54 18 -2 0 69.93 6.45 -18 2 0 66.63 6.41 -18 2 0 68.45 6.51 -18 2 0 66.09 6.4 -18 2 0 66.56 6.47 16 -2 0 40.63 4.18 16 -2 0 38.71 3.97 -16 2 0 38.31 3.93 -16 2 0 45.08 4.04 -16 2 0 42.69 3.97 -16 2 0 42.85 4 14 -2 0 120.85 10.41 14 -2 0 97.61 10.33 14 -2 0 111.11 10.32 -14 2 0 96.19 10.3 -14 2 0 125.07 10.37 -14 2 0 116.3 10.3 -14 2 0 114.72 10.33 -14 2 0 95.01 10.29 12 -2 0 63.85 5.99 12 -2 0 64.89 6 12 -2 0 62.89 5.95 12 -2 0 65.38 6.04 12 -2 0 68 6.01 -12 2 0 56.5 5.98 -12 2 0 67.14 6.03 -12 2 0 61.94 5.96 -12 2 0 59.98 6 -12 2 0 62.52 5.96 10 -2 0 323.28 30.09 10 -2 0 323.51 30.13 10 -2 0 338.09 30.14 10 -2 0 355.26 30.14 -10 2 0 330.32 30.1 -10 2 0 278.85 30.12 -10 2 0 347.59 30.15 -10 2 0 307.5 30.13 -10 2 0 293.55 30.13 -10 2 0 314.16 30.13 8 -2 0 91.39 9.66 8 -2 0 103.31 9.67 8 -2 0 97.28 9.66 8 -2 0 105.59 9.68 -8 2 0 111.31 9.67 -8 2 0 101.53 9.66 -8 2 0 106.1 9.63 -8 2 0 102.65 9.66 -8 2 0 101.09 9.67 -8 2 0 107.36 9.67 -8 2 0 99.16 9.66 6 -2 0 230.63 21.12 6 -2 0 229.95 21.12 6 -2 0 210.86 21.11 6 -2 0 219.38 21.11 -6 2 0 226.79 21.11 -6 2 0 242.66 21.12 -6 2 0 212.99 21.12 -6 2 0 226.46 21.11 4 -2 0 524.35 52.2 4 -2 0 601.98 52.2 4 -2 0 561.23 52.19 -4 2 0 536.82 52.2 -4 2 0 577.59 52.18 -4 2 0 567.09 52.19 -4 2 0 527.28 52.19 -4 2 0 559.16 52.19 2 -2 0 675.96 62.79 2 -2 0 630.84 62.79 2 -2 0 646.64 62.8 -2 2 0 691.67 62.81 -2 2 0 684.45 62.79 -2 2 0 676.33 62.81 -2 2 0 669.03 62.81 -2 2 0 687.12 62.8 0 -2 0 50.36 4.6 0 -2 0 48.31 4.61 0 -2 0 51.35 4.63 0 -2 0 49.68 4.6 0 -2 0 46.47 4.6 0 -2 0 49.31 4.63 0 2 0 50.07 4.62 0 2 0 49.1 4.6 0 2 0 48.22 4.63 0 2 0 50.36 4.61 0 2 0 49.59 4.62 0 2 0 44.44 4.63 -2 -2 0 684.34 60.27 2 2 0 570.52 60.36 2 2 0 673.07 60.29 -4 -2 0 554.65 51.36 -4 -2 0 511.38 51.33 -4 -2 0 535.87 51.33 -4 -2 0 552.92 51.31 -4 -2 0 560.62 51.34 -4 -2 0 539.87 51.33 -4 -2 0 530.76 51.32 4 2 0 597.75 51.34 4 2 0 547.95 51.36 4 2 0 568.53 51.33 4 2 0 520.7 51.34 4 2 0 552.36 51.33 -6 -2 0 239.64 20.78 -6 -2 0 224.87 20.77 -6 -2 0 220.47 20.76 -6 -2 0 223.86 20.76 -6 -2 0 236.56 20.81 -6 -2 0 239.54 20.78 -6 -2 0 218.71 20.76 6 2 0 201.48 20.79 6 2 0 199.28 20.75 6 2 0 229.38 20.77 6 2 0 204.45 20.76 6 2 0 221.91 20.77 6 2 0 217.82 20.77 -8 -2 0 110.14 9.54 -8 -2 0 99.84 9.52 -8 -2 0 104.33 9.53 -8 -2 0 103.76 9.51 -8 -2 0 105.46 9.53 -8 -2 0 107.88 9.58 8 2 0 87.91 9.5 8 2 0 101.86 9.53 8 2 0 96.16 9.56 8 2 0 93.48 9.52 -10 -2 0 276.99 29.56 -10 -2 0 327.55 29.56 -10 -2 0 332.32 29.61 -10 -2 0 303.25 29.53 10 2 0 351.92 29.59 10 2 0 289.63 29.62 10 2 0 321.73 29.55 10 2 0 317.14 29.53 -12 -2 0 59.63 5.65 -12 -2 0 58.08 5.6 -12 -2 0 57.97 5.64 -12 -2 0 59.68 5.73 12 2 0 62.62 5.67 12 2 0 63.18 5.64 12 2 0 54.18 5.61 -14 -2 0 115.48 10.64 -14 -2 0 120.17 10.56 -14 -2 0 109.01 10.5 -14 -2 0 110.41 10.55 14 2 0 111.22 10.55 14 2 0 105.06 10.58 14 2 0 110.32 10.52 -16 -2 0 19.67 2.47 -16 -2 0 27.67 2.46 -16 -2 0 22.32 2.61 16 2 0 21.98 2.29 -18 -2 0 59.08 6.31 -18 -2 0 65.46 6.39 -18 -2 0 68.46 6.43 18 2 0 67.06 6.37 18 2 0 70.3 6.28 -20 -2 0 52.41 4.71 -20 -2 0 49.57 4.62 -20 -2 0 40.95 4.52 -20 -2 0 56.96 4.77 20 2 0 41.08 4.68 20 2 0 47.55 4.55 -22 -2 0 13 2.31 -22 -2 0 14.24 1.55 -22 -2 0 14.66 1.71 -22 -2 0 11.34 1.35 22 2 0 15.25 1.74 -24 -2 0 2.98 2.05 -24 -2 0 8.03 1.35 -24 -2 0 7.88 1.51 24 2 0 4.57 1.88 -26 -2 0 1.09 1.66 -26 -2 0 0.3 1.67 -26 -2 0 2.3 1.24 26 2 0 -2.64 1.65 -28 -2 0 15.39 1.88 28 2 0 8.68 2.3 -30 -2 0 9.42 1.69 30 2 0 3.05 2.31 -32 -2 0 3.82 1.59 -32 -2 0 -0.72 2.28 32 2 0 0.76 2.43 -29 3 0 9.62 1.41 -27 3 0 10.52 1.16 -27 3 0 6.84 1.54 25 -3 0 0.52 0.54 -25 3 0 5.03 1.79 -25 3 0 1.85 1.16 -25 3 0 1.68 0.48 23 -3 0 14.95 2.23 23 -3 0 18.52 2.03 -23 3 0 20.45 1.92 -23 3 0 17.34 1.92 -23 3 0 19.41 2.07 -23 3 0 22.18 2.21 21 -3 0 29.48 3.04 21 -3 0 33.66 2.88 -21 3 0 26.84 2.86 -21 3 0 28.46 2.76 -21 3 0 25.5 2.94 -21 3 0 26.62 2.76 19 -3 0 0.03 0.39 19 -3 0 0.66 0.51 -19 3 0 0.26 0.29 -19 3 0 0.3 0.54 -19 3 0 0.18 0.48 -19 3 0 0.14 0.29 17 -3 0 132.1 12.75 17 -3 0 135.56 12.74 17 -3 0 124.78 12.81 -17 3 0 134.17 12.68 -17 3 0 136.13 12.75 -17 3 0 146.79 12.79 15 -3 0 78.84 8.06 15 -3 0 96.01 8.06 -15 3 0 80.12 8.04 -15 3 0 76.74 7.95 -15 3 0 89.27 7.95 13 -3 0 89.15 8.71 13 -3 0 82.96 8.64 13 -3 0 87.35 8.66 13 -3 0 85.97 8.63 -13 3 0 99.96 8.59 -13 3 0 99.28 8.58 11 -3 0 88.2 9.03 -11 3 0 102.35 9.02 -11 3 0 101 9.04 -11 3 0 90.26 9.01 9 -3 0 44.94 4.15 9 -3 0 48.65 4.19 9 -3 0 45.71 4.16 9 -3 0 46.33 4.16 -9 3 0 37.88 4.13 -9 3 0 38.3 4.16 -9 3 0 43.8 4.15 7 -3 0 367.21 33.44 7 -3 0 388.75 33.46 7 -3 0 350.63 33.45 7 -3 0 400.01 33.47 -7 3 0 365.07 33.44 -7 3 0 327.66 33.44 -7 3 0 355.78 33.45 -7 3 0 329.67 33.45 -7 3 0 324.85 33.44 5 -3 0 362.96 32.84 5 -3 0 377.14 32.86 5 -3 0 397.81 32.86 5 -3 0 400.1 32.86 -5 3 0 345.48 32.83 -5 3 0 319.46 32.85 -5 3 0 332.26 32.83 -5 3 0 308.91 32.84 -5 3 0 320.3 32.85 -5 3 0 339.43 32.84 3 -3 0 512.39 48.3 3 -3 0 501.09 48.24 3 -3 0 508.85 48.22 3 -3 0 547.1 48.26 3 -3 0 479.02 48.22 3 -3 0 529.37 48.25 -3 3 0 506.83 48.24 -3 3 0 521.78 48.25 -3 3 0 519.38 48.25 -3 3 0 514.25 48.26 -3 3 0 518.85 48.22 -3 3 0 511 48.22 -3 3 0 535.49 48.23 -3 3 0 497.78 48.26 -3 3 0 509.37 48.22 -3 3 0 521.74 48.25 1 -3 0 769.54 68.78 1 -3 0 743.59 68.67 1 -3 0 792.43 68.7 1 -3 0 796.98 68.83 1 -3 0 704.43 68.68 -1 3 0 687.98 68.67 -1 3 0 704.61 68.75 -1 3 0 681.56 68.68 -1 3 0 735.96 68.7 -1 3 0 717.29 68.68 -1 -3 0 665.96 67.79 -1 -3 0 724.34 67.91 -1 -3 0 697.78 67.8 -1 -3 0 702.6 67.8 1 3 0 788.23 67.81 1 3 0 764.15 67.87 -3 -3 0 503.6 48.27 -3 -3 0 518.08 48.27 -3 -3 0 531.04 48.31 -3 -3 0 486.13 48.28 -3 -3 0 543.99 48.28 -3 -3 0 491.04 48.25 -3 -3 0 522.14 48.25 3 3 0 494.72 48.29 3 3 0 561.84 48.27 3 3 0 521.6 48.27 3 3 0 504.39 48.29 3 3 0 513.54 48.27 3 3 0 508.32 48.25 3 3 0 507.71 48.3 -5 -3 0 340.05 33.29 -5 -3 0 317.56 33.25 -5 -3 0 315.62 33.24 -5 -3 0 331.48 33.24 -5 -3 0 334.84 33.25 -5 -3 0 330.41 33.23 -5 -3 0 352.6 33.22 5 3 0 382.32 33.23 5 3 0 365.1 33.28 5 3 0 397.72 33.25 5 3 0 364.07 33.22 5 3 0 381.76 33.24 5 3 0 372.03 33.25 5 3 0 362.32 33.26 5 3 0 371.07 33.23 -7 -3 0 359 32.74 -7 -3 0 322.92 32.67 -7 -3 0 327.58 32.68 -7 -3 0 333.71 32.67 -7 -3 0 335.04 32.69 -7 -3 0 321.18 32.68 7 3 0 387.63 32.69 7 3 0 352.82 32.67 7 3 0 353.95 32.68 7 3 0 382.35 32.68 7 3 0 338.1 32.72 7 3 0 367.46 32.67 -9 -3 0 41.41 4.13 -9 -3 0 43.34 4.2 -9 -3 0 38.48 4.11 -9 -3 0 45.06 4.14 -9 -3 0 42.33 4.11 9 3 0 44.55 4.12 9 3 0 47.56 4.13 9 3 0 43.99 4.1 -11 -3 0 104.35 10.74 11 3 0 114.89 10.7 11 3 0 127.96 10.77 11 3 0 108.32 10.74 -13 -3 0 61.59 7.19 13 3 0 82.29 6.96 -15 -3 0 89.47 8.57 15 3 0 90.28 8.47 15 3 0 88.31 8.53 -17 -3 0 111.08 11.26 -17 -3 0 136 11.38 -17 -3 0 122.7 11.39 17 3 0 107.69 11.28 17 3 0 121.67 11.26 17 3 0 116.42 11.22 -19 -3 0 -0.49 0.26 -19 -3 0 0.68 0.5 -19 -3 0 0.62 0.79 -19 -3 0 0.58 0.43 19 3 0 0.33 0.98 19 3 0 -0.43 0.45 19 3 0 -0.01 0.34 -21 -3 0 25.87 2.91 -21 -3 0 24.69 2.96 -21 -3 0 31.06 3.1 -21 -3 0 22.87 2.92 21 3 0 28.93 3 21 3 0 34.05 2.82 21 3 0 31.62 2.92 -23 -3 0 19.74 1.93 -23 -3 0 17.01 1.99 -23 -3 0 16.66 2.61 23 3 0 13.36 2.01 -25 -3 0 2.75 1.86 -25 -3 0 4.56 1.43 -25 -3 0 1.65 0.75 25 3 0 0.04 1.72 -29 -3 0 5.8 1.72 -31 -3 0 16.29 2.17 31 3 0 7.58 2.78 -32 4 0 4.13 0.79 -30 4 0 3.55 0.99 -28 4 0 4.6 1.01 26 -4 0 3.17 0.7 -26 4 0 2.56 1.31 -26 4 0 2.66 0.84 24 -4 0 5.4 2.15 -24 4 0 4.8 1.76 22 -4 0 36 4.44 22 -4 0 44.59 4.34 -22 4 0 49.16 4.22 -22 4 0 43.97 4.32 -22 4 0 40.88 4.22 -22 4 0 48.23 4.42 20 -4 0 26.25 2.69 20 -4 0 23.45 2.86 20 -4 0 26.78 2.74 -20 4 0 29.6 2.6 -20 4 0 26.71 2.71 -20 4 0 25.49 2.6 -20 4 0 28.46 2.81 18 -4 0 3.5 0.71 18 -4 0 3.07 1.2 -18 4 0 3.56 0.72 -18 4 0 3.4 0.54 -18 4 0 2.62 0.64 -18 4 0 3.47 0.5 16 -4 0 132.85 12.22 16 -4 0 138.41 12.18 16 -4 0 134.03 12.21 -16 4 0 130.03 12.17 -16 4 0 121.97 12.15 -16 4 0 124.41 12.07 -16 4 0 119.75 12.07 14 -4 0 97.58 9.31 14 -4 0 100.26 9.31 14 -4 0 95.33 9.33 14 -4 0 100.9 9.37 -14 4 0 102.48 9.32 -14 4 0 91.54 9.22 -14 4 0 98.35 9.28 12 -4 0 47.81 4.86 12 -4 0 55.06 4.83 12 -4 0 52.11 4.91 12 -4 0 52.18 4.84 -12 4 0 44.72 4.8 10 -4 0 21.89 2.19 10 -4 0 21.5 2.21 10 -4 0 22.39 2.23 10 -4 0 20.61 2.2 -10 4 0 24.31 2.18 8 -4 0 103.31 9.68 8 -4 0 99.71 9.68 8 -4 0 102.06 9.68 8 -4 0 96.96 9.66 -8 4 0 111.38 9.65 -8 4 0 108.67 9.65 -8 4 0 94.11 9.71 6 -4 0 737.33 68.97 6 -4 0 775.73 68.97 6 -4 0 722.31 68.95 6 -4 0 804.63 68.97 -6 4 0 738.5 68.93 -6 4 0 687.79 68.95 -6 4 0 700.81 68.97 -6 4 0 724.38 68.93 -6 4 0 730.06 68.95 4 -4 0 174.08 15.7 4 -4 0 177.88 15.71 4 -4 0 159.73 15.69 4 -4 0 172.44 15.74 4 -4 0 156.47 15.66 -4 4 0 167.24 15.66 -4 4 0 171.25 15.71 -4 4 0 159.54 15.7 -4 4 0 165.56 15.71 -4 4 0 171.84 15.67 -4 4 0 173.73 15.68 -4 4 0 164.63 15.72 -4 4 0 162.2 15.69 -4 4 0 171.71 15.69 -4 4 0 157.57 15.67 2 -4 0 640.16 59.91 2 -4 0 625.88 59.86 2 -4 0 672.68 59.86 2 -4 0 646.65 59.89 2 -4 0 603.84 59.83 2 -4 0 603.57 59.84 2 -4 0 680.75 59.91 -2 4 0 642.44 59.87 -2 4 0 636.55 59.86 -2 4 0 624.86 59.83 -2 4 0 627.76 59.89 -2 4 0 650.73 59.88 -2 4 0 668.18 59.83 -2 4 0 618.38 59.85 0 -4 0 0.28 0.32 0 -4 0 0.26 0.18 0 -4 0 0.24 0.52 0 -4 0 0.46 0.17 0 -4 0 0.16 0.45 0 -4 0 0.57 0.45 0 -4 0 0.51 0.16 0 4 0 0.91 0.37 0 4 0 -0.1 0.43 0 4 0 0.55 0.18 0 4 0 0.41 0.18 0 4 0 0.12 0.48 -2 -4 0 634.68 60.14 -2 -4 0 621.78 60.12 -2 -4 0 668.43 60.22 -2 -4 0 699.42 60.13 -2 -4 0 638.58 60.14 -2 -4 0 615.85 60.13 2 4 0 660.9 60.13 2 4 0 635.44 60.14 2 4 0 650.28 60.15 2 4 0 614.21 60.14 2 4 0 605.12 60.17 2 4 0 639.57 60.14 2 4 0 657.95 60.17 -4 -4 0 159.3 15.62 -4 -4 0 171.74 15.67 -4 -4 0 169.92 15.6 -4 -4 0 158.72 15.6 -4 -4 0 171.42 15.62 4 4 0 170.32 15.62 4 4 0 175.46 15.62 4 4 0 162.51 15.62 4 4 0 159.56 15.59 4 4 0 153.1 15.65 4 4 0 170.87 15.6 4 4 0 170.92 15.63 -6 -4 0 742.32 66.82 -6 -4 0 648.97 66.85 -6 -4 0 695.41 66.85 -6 -4 0 637.21 66.83 -6 -4 0 716.84 66.91 -6 -4 0 761.62 66.86 6 4 0 743.49 66.84 6 4 0 734.93 66.83 6 4 0 692.42 66.82 6 4 0 737.08 66.85 6 4 0 715.57 66.85 6 4 0 733.35 66.85 -8 -4 0 110.28 9.77 -8 -4 0 101.89 9.75 -8 -4 0 104.29 9.83 8 4 0 100.08 9.74 8 4 0 103.23 9.75 8 4 0 105.56 9.76 8 4 0 105.16 9.74 8 4 0 97.65 9.74 -10 -4 0 19.77 2.18 -10 -4 0 22.32 2 10 4 0 18.58 2.11 10 4 0 19.74 1.98 -12 -4 0 37.54 4.6 -12 -4 0 46.69 4.3 12 4 0 44.37 4.31 12 4 0 46.23 4.28 -14 -4 0 73.78 7.86 -14 -4 0 94.29 7.83 14 4 0 77.28 7.81 14 4 0 75.58 7.76 14 4 0 88.17 7.79 -16 -4 0 120.54 11.33 16 4 0 127.98 11.34 16 4 0 103.38 11.26 16 4 0 125.35 11.29 -18 -4 0 2.75 0.67 -18 -4 0 -0.04 1.67 -18 -4 0 4.13 1.34 18 4 0 6.02 0.82 18 4 0 5.16 0.68 18 4 0 5.28 0.9 -20 -4 0 25.33 2.64 -20 -4 0 22.88 2.59 -20 -4 0 27.6 2.82 20 4 0 23.79 2.65 20 4 0 25.07 2.49 20 4 0 26.39 2.58 -22 -4 0 38.77 4.01 -22 -4 0 40.89 4.09 -22 -4 0 46.22 4.22 22 4 0 42.24 3.9 22 4 0 33.96 4.04 -24 -4 0 0.08 1.56 -32 -4 0 8.29 2.04 -32 -4 0 2.74 1.05 32 4 0 2.08 0.95 -31 5 0 -1.37 0.88 27 -5 0 5.91 1.65 25 -5 0 0.75 1.55 25 -5 0 3.6 1.95 -25 5 0 3.58 1.74 23 -5 0 1.09 1.9 23 -5 0 2.03 0.61 -23 5 0 3.74 1.53 21 -5 0 23.32 2.33 21 -5 0 22.57 2.39 21 -5 0 21.11 2.55 -21 5 0 20.66 2.3 -21 5 0 24.09 2.42 19 -5 0 1.58 0.61 19 -5 0 1.29 0.5 19 -5 0 0.42 0.58 -19 5 0 0.43 0.51 -19 5 0 0.98 0.51 17 -5 0 15.7 1.64 17 -5 0 15.29 1.61 -17 5 0 10.56 1.96 -17 5 0 14.04 1.55 15 -5 0 22.53 2.06 15 -5 0 17.11 2.14 -15 5 0 18.57 1.95 13 -5 0 9.8 1.69 13 -5 0 11.08 1.63 13 -5 0 10.89 1.83 13 -5 0 15.9 1.51 -13 5 0 14 1.4 -13 5 0 15.35 1.45 11 -5 0 24.24 2.53 11 -5 0 28.36 2.58 11 -5 0 25.26 2.51 11 -5 0 25.05 2.55 -11 5 0 24.98 2.5 -11 5 0 25.54 2.49 9 -5 0 116.65 10.61 9 -5 0 106.21 10.6 9 -5 0 106.91 10.57 9 -5 0 108.1 10.61 -9 5 0 116.63 10.56 -9 5 0 117.61 10.56 7 -5 0 37.3 3.65 7 -5 0 36.76 3.68 7 -5 0 39.54 3.68 7 -5 0 37.06 3.68 -7 5 0 40.1 3.67 -7 5 0 38.83 3.62 -7 5 0 38.18 3.59 -7 5 0 38.25 3.63 -7 5 0 36.15 3.66 5 -5 0 193.02 19.58 5 -5 0 202.97 19.62 5 -5 0 203.22 19.65 5 -5 0 190.06 19.58 5 -5 0 217.73 19.64 5 -5 0 220.37 19.65 -5 5 0 199.43 19.64 -5 5 0 211.59 19.62 -5 5 0 206.94 19.63 -5 5 0 223.11 19.65 -5 5 0 206.04 19.59 -5 5 0 209.32 19.59 -5 5 0 220.77 19.61 -5 5 0 221.27 19.6 3 -5 0 2.07 0.34 3 -5 0 2.49 0.45 3 -5 0 1.98 0.36 3 -5 0 1.54 0.43 3 -5 0 2.24 0.47 3 -5 0 2.48 0.55 3 -5 0 2.11 0.61 -3 5 0 1.7 0.46 -3 5 0 1.9 0.59 -3 5 0 2.51 0.43 -3 5 0 2.28 0.43 -3 5 0 1.85 0.35 -3 5 0 1.97 0.38 1 -5 0 94.49 8.74 1 -5 0 101.79 8.79 1 -5 0 93.58 8.82 1 -5 0 97.61 8.78 1 -5 0 94.02 8.76 1 -5 0 77.71 8.79 1 -5 0 101.45 8.76 -1 5 0 87.04 8.75 -1 5 0 89.5 8.75 -1 5 0 86.78 8.76 -1 5 0 98.08 8.76 -1 5 0 88.39 8.8 -1 5 0 90.41 8.74 -1 5 0 100.2 8.79 -1 -5 0 84.44 9.02 -1 -5 0 81.63 8.98 -1 -5 0 90.67 9.01 -1 -5 0 94.28 9.07 -1 -5 0 102.95 9.01 1 5 0 95.61 9 1 5 0 103.02 9.03 1 5 0 93.31 8.98 1 5 0 99.99 9.02 1 5 0 100.57 9.01 1 5 0 103.81 9.01 -3 -5 0 1.5 0.46 -3 -5 0 1.72 0.33 -3 -5 0 2.29 0.37 -3 -5 0 1.76 0.49 3 5 0 1.53 0.44 3 5 0 2.29 0.62 3 5 0 1.67 0.57 3 5 0 2.35 0.49 3 5 0 1.67 0.6 3 5 0 2.47 0.57 -5 -5 0 193.06 19.61 -5 -5 0 210.15 19.61 -5 -5 0 201.32 19.7 -5 -5 0 229.12 19.65 5 5 0 219.25 19.64 5 5 0 210.12 19.61 5 5 0 191.75 19.6 5 5 0 208.64 19.64 5 5 0 217.86 19.64 -7 -5 0 41.24 3.61 -7 -5 0 35.94 3.68 -7 -5 0 39.25 3.54 7 5 0 37.64 3.59 7 5 0 35.78 3.54 7 5 0 38.9 3.58 7 5 0 32.52 3.53 7 5 0 36.59 3.58 7 5 0 38.62 3.56 -9 -5 0 92.65 10.33 -9 -5 0 115.53 10.24 9 5 0 108.28 10.18 9 5 0 114.45 10.21 9 5 0 108.14 10.19 9 5 0 107.54 10.18 -11 -5 0 22.01 2.23 11 5 0 19.65 2.13 11 5 0 21.12 2.13 -13 -5 0 9.77 1.78 -13 -5 0 14.3 1.48 -13 -5 0 13.57 1.46 13 5 0 12.18 1.4 13 5 0 10.47 1.34 13 5 0 11.75 1.38 -15 -5 0 16.59 1.69 -15 -5 0 12.78 2.15 -15 -5 0 10.38 1.74 15 5 0 13.71 1.5 15 5 0 12.28 1.47 15 5 0 7.87 1.41 -17 -5 0 13.06 1.7 -17 -5 0 6.8 1.98 -17 -5 0 14.3 1.65 17 5 0 14.78 1.61 17 5 0 10.95 1.5 17 5 0 11 1.41 -19 -5 0 1.29 0.53 -19 -5 0 0.24 1.91 -19 -5 0 1.1 0.55 19 5 0 1.06 0.4 19 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25.55 3.01 16 -6 0 21.05 3.02 16 -6 0 25.62 2.97 -16 6 0 30.42 2.98 -16 6 0 31.95 2.9 -16 6 0 34.5 2.96 14 -6 0 29.77 3.45 14 -6 0 32.24 3.38 14 -6 0 29.55 3.52 -14 6 0 38.91 3.37 -14 6 0 34.92 3.32 12 -6 0 53.75 4.97 12 -6 0 52.32 4.92 12 -6 0 54.79 4.99 12 -6 0 53.42 4.96 -12 6 0 45.52 4.89 -12 6 0 48.44 4.89 10 -6 0 10.23 1.19 10 -6 0 11.46 1.26 10 -6 0 9.06 1.27 10 -6 0 10.45 1.26 -10 6 0 11.55 1.16 -10 6 0 12.77 1.15 -10 6 0 9.74 1.27 8 -6 0 103.14 8.38 8 -6 0 105.09 8.38 -8 6 0 76.87 8.34 -8 6 0 84.39 8.27 -8 6 0 83.08 8.35 -8 6 0 86.69 8.31 -8 6 0 79.52 8.28 6 -6 0 152.93 14.23 6 -6 0 137.86 14.13 6 -6 0 159.5 14.13 6 -6 0 159.72 14.19 6 -6 0 168.2 14.21 6 -6 0 158.93 14.23 -6 6 0 147.86 14.15 -6 6 0 139.82 14.21 -6 6 0 143.32 14.14 -6 6 0 130.17 14.2 -6 6 0 159.34 14.15 -6 6 0 151.44 14.17 4 -6 0 28.33 3.03 4 -6 0 27.14 2.94 4 -6 0 29.39 2.94 4 -6 0 28.81 3.01 4 -6 0 29.49 2.99 -4 6 0 32.91 2.98 -4 6 0 32.6 2.96 -4 6 0 33.3 2.96 -4 6 0 32.29 2.96 -4 6 0 32.94 3.09 -4 6 0 32.63 3.02 2 -6 0 23.87 2.5 2 -6 0 27.42 2.41 2 -6 0 21.5 2.41 2 -6 0 23.6 2.44 2 -6 0 24.19 2.51 2 -6 0 20.33 2.47 -2 6 0 28.65 2.47 -2 6 0 28.15 2.53 -2 6 0 25.73 2.43 -2 6 0 25.01 2.42 -2 6 0 26.84 2.42 0 -6 0 99.26 9.6 0 -6 0 98.91 9.69 0 -6 0 107.44 9.62 0 -6 0 104.37 9.65 0 -6 0 94.97 9.66 0 6 0 104.75 9.61 0 6 0 102.07 9.65 0 6 0 102.68 9.63 0 6 0 97.34 9.59 0 6 0 108.09 9.67 -2 -6 0 25.55 2.52 -2 -6 0 26.28 2.51 -2 -6 0 25.03 2.61 -2 -6 0 25.58 2.51 2 6 0 23.64 2.56 2 6 0 25.5 2.51 2 6 0 27.18 2.6 2 6 0 28.3 2.59 -4 -6 0 32.28 2.93 -4 -6 0 32.51 2.96 -4 -6 0 31.82 3.06 4 6 0 30.37 2.91 4 6 0 30.3 3.01 4 6 0 29.21 2.95 4 6 0 30.04 2.96 4 6 0 27.19 2.91 -6 -6 0 170.5 14.97 -6 -6 0 147.41 15.04 -6 -6 0 156.71 14.93 6 6 0 143.25 14.92 6 6 0 161.54 14.96 6 6 0 167.27 14.97 6 6 0 162.74 14.96 6 6 0 161.64 14.93 -8 -6 0 84.29 9.02 -8 -6 0 80.93 8.88 8 6 0 91.27 8.88 8 6 0 100.41 8.91 8 6 0 98.64 8.93 8 6 0 95.14 8.89 8 6 0 103.99 8.95 8 6 0 101.47 8.94 -10 -6 0 2.5 1.55 -10 -6 0 10.38 1.18 10 6 0 5.15 1.05 10 6 0 8.13 0.94 10 6 0 7.47 1.06 -12 -6 0 34.65 4.14 -12 -6 0 44.36 4.17 12 6 0 43.67 4.1 12 6 0 41.37 4.12 12 6 0 47.64 4.12 -14 -6 0 33.7 3.37 14 6 0 32.87 3.29 14 6 0 32.93 3.3 -16 -6 0 20.35 1.97 -16 -6 0 16.95 2.24 -16 -6 0 11.44 2.62 16 6 0 19.92 2.07 16 6 0 16.14 2 -18 -6 0 2.01 1.9 -18 -6 0 2.27 0.64 -18 -6 0 2.05 1.29 18 6 0 4.26 0.86 18 6 0 3.72 1.27 18 6 0 4.73 1.11 -20 -6 0 24.03 2.96 -20 -6 0 34.94 3.28 20 6 0 26.45 2.99 20 6 0 29.31 2.94 20 6 0 31.38 2.87 -22 -6 0 20.56 3.08 -22 -6 0 19.82 2.18 -22 -6 0 19.88 2.21 22 6 0 17.23 2.05 22 6 0 20.41 2.3 -24 -6 0 13.44 1.89 -24 -6 0 12.88 2.06 -24 -6 0 14.14 2.56 24 6 0 9.25 1.64 24 6 0 10.65 1.46 24 6 0 13.37 1.83 -26 -6 0 2.32 2.06 -26 -6 0 3.19 1.36 -26 -6 0 2.1 1.6 26 6 0 0.38 1.46 26 6 0 2.14 0.72 -28 -6 0 6.07 1.65 -28 -6 0 2.08 1.71 -28 -6 0 5.19 1.49 28 6 0 1.23 1.59 -30 -6 0 9.17 2.96 -30 -6 0 15.95 2.63 -30 -6 0 21.49 2.52 30 6 0 16.73 2.53 31 -7 0 2.14 0.82 -31 7 0 3.41 1.06 -31 7 0 1.75 0.96 29 -7 0 13.68 2.33 -29 7 0 21.11 2.53 -29 7 0 18.68 2.62 27 -7 0 3.72 1.59 27 -7 0 3.9 2.37 -27 7 0 5.51 1.66 -27 7 0 4.09 1.79 25 -7 0 23.29 3.34 25 -7 0 27.8 2.69 -25 7 0 18.73 2.93 23 -7 0 11.96 2.16 23 -7 0 16.91 1.9 23 -7 0 13.97 1.95 -23 7 0 19.44 2.01 -23 7 0 18.55 1.91 21 -7 0 9.37 1.32 21 -7 0 10.1 1.34 21 -7 0 9.85 1.44 21 -7 0 8.14 1.64 -21 7 0 9.63 1.36 -21 7 0 9.61 1.32 19 -7 0 3.05 1.62 19 -7 0 3 1.42 19 -7 0 2.32 1.35 19 -7 0 3.63 0.81 -19 7 0 2.68 0.64 -19 7 0 4.79 0.79 -19 7 0 2.07 1.38 17 -7 0 1.17 1.37 17 -7 0 1.09 1.08 17 -7 0 0.45 1.62 17 -7 0 0.81 1.21 -17 7 0 2.51 1.22 -17 7 0 3.97 0.88 -17 7 0 3.3 1.24 15 -7 0 76.24 7.92 15 -7 0 77.01 7.73 15 -7 0 77.96 7.87 -15 7 0 74.75 7.68 -15 7 0 84.08 7.75 -15 7 0 91.16 7.73 13 -7 0 14.6 2.32 13 -7 0 14.5 2.39 13 -7 0 23.32 2.5 -13 7 0 21.46 2.11 11 -7 0 59.46 5.96 11 -7 0 63.25 5.96 11 -7 0 63.73 5.92 11 -7 0 63.21 5.97 -11 7 0 59.61 5.88 -11 7 0 61.53 5.95 -11 7 0 62.23 5.89 9 -7 0 101.27 9.38 9 -7 0 100.33 9.33 9 -7 0 99.05 9.37 9 -7 0 105.96 9.37 -9 7 0 97.78 9.31 -9 7 0 93.47 9.28 -9 7 0 95.19 9.36 -9 7 0 95.84 9.26 -7 7 0 9.36 1.16 -7 7 0 9.6 1.02 -7 7 0 9.69 1.06 -7 7 0 10.26 1.01 5 -7 0 298.64 29.28 5 -7 0 325.82 29.22 5 -7 0 309.72 29.24 5 -7 0 311.79 29.27 -5 7 0 317.55 29.26 -5 7 0 308.95 29.21 -5 7 0 326.38 29.21 -5 7 0 291.72 29.2 3 -7 0 161.04 16.2 3 -7 0 178.77 16.17 3 -7 0 173.34 16.25 3 -7 0 182.66 16.17 3 -7 0 186.28 16.23 -3 7 0 164.66 16.18 -3 7 0 155.98 16.17 -3 7 0 164.71 16.17 -3 7 0 180.1 16.18 -3 7 0 173.87 16.22 1 -7 0 173.62 16.72 1 -7 0 169.72 16.64 1 -7 0 182.64 16.74 1 -7 0 189.83 16.66 1 -7 0 185.33 16.69 -1 7 0 181.71 16.66 -1 7 0 172.32 16.64 -1 7 0 166.8 16.66 -1 7 0 185.35 16.71 -1 7 0 164.45 16.64 -1 7 0 177.56 16.71 -1 -7 0 161.98 16.92 -1 -7 0 179.98 16.89 -1 -7 0 170.27 16.87 -1 -7 0 168.06 16.94 1 7 0 195.6 16.86 1 7 0 184.71 16.93 1 7 0 171.2 16.87 1 7 0 188.67 16.9 1 7 0 193.59 16.88 -3 -7 0 166.54 16.36 -3 -7 0 170.21 16.36 -3 -7 0 167.54 16.31 -3 -7 0 166.23 16.45 -3 -7 0 155.95 16.31 3 7 0 182.97 16.33 3 7 0 186.22 16.37 3 7 0 183.61 16.39 3 7 0 186.63 16.38 -5 -7 0 302.59 28.79 -5 -7 0 299.67 28.7 -5 -7 0 305.64 28.68 5 7 0 324.48 28.72 5 7 0 305.94 28.7 5 7 0 284.45 28.66 5 7 0 316.1 28.71 7 7 0 13.85 1.49 7 7 0 16.38 1.6 7 7 0 13.75 1.5 7 7 0 17.15 1.61 7 7 0 14.9 1.59 7 7 0 16.46 1.53 -9 -7 0 90.45 8.84 -9 -7 0 89.5 8.77 -9 -7 0 88.12 8.95 -9 -7 0 80.55 8.79 9 7 0 104.76 8.85 9 7 0 90.83 8.76 9 7 0 95.32 8.78 9 7 0 103.55 8.83 9 7 0 92.83 8.83 9 7 0 95.42 8.79 -11 -7 0 43.16 4.25 -11 -7 0 45.89 4.27 11 7 0 39.93 4.24 -13 -7 0 15.8 2.84 -13 -7 0 20.3 2.34 13 7 0 16.04 2.22 13 7 0 24.04 2.18 13 7 0 24.28 2.24 -15 -7 0 78.53 7.83 -15 -7 0 74.09 8.12 15 7 0 81.43 7.76 15 7 0 86.97 7.75 -17 -7 0 2.39 0.62 -17 -7 0 5.61 1.3 -17 -7 0 -0.7 1.9 17 7 0 0.49 0.81 17 7 0 1.38 1.01 17 7 0 1.1 1.15 -19 -7 0 1.9 0.65 -19 -7 0 1.55 0.65 -19 -7 0 2.48 1.12 19 7 0 0.65 0.85 19 7 0 5.34 0.82 -21 -7 0 6.93 1.25 -21 -7 0 5.15 1.37 -21 -7 0 5.22 0.99 21 7 0 7.93 1.11 21 7 0 5.88 1.19 21 7 0 8.21 0.95 -23 -7 0 15.15 2.28 -23 -7 0 18.13 2.88 -23 -7 0 15.46 2.18 23 7 0 11.03 2.12 -25 -7 0 32.15 3.14 -25 -7 0 25.58 3.25 25 7 0 22.49 3.1 -27 -7 0 2.48 2.19 -27 -7 0 2.99 1.85 -27 -7 0 5.19 1.63 -29 -7 0 15.25 2.17 -29 -7 0 7.69 2.81 -29 -7 0 10.99 2.42 -31 -7 0 1.34 2.37 -31 -7 0 1.26 2.02 -30 8 0 5.04 1.93 -26 8 0 1.97 1.61 24 -8 0 -0.17 2.43 24 -8 0 1.58 1.36 24 -8 0 0.43 0.7 -24 8 0 0.01 1.55 -24 8 0 1.57 1.73 22 -8 0 1.47 0.79 22 -8 0 -0.33 0.69 22 -8 0 -0.09 0.63 22 -8 0 -0.24 0.77 -22 8 0 0.55 0.61 -22 8 0 0.37 1.25 20 -8 0 9.63 1.64 20 -8 0 10.28 1.7 20 -8 0 8.33 1.45 20 -8 0 8.16 1.78 -20 8 0 10.78 1.31 -20 8 0 9.57 1.34 18 -8 0 27.01 2.98 18 -8 0 26.94 3.02 18 -8 0 24.18 2.89 18 -8 0 26.66 2.87 -18 8 0 25.8 2.66 -18 8 0 27.43 2.73 -18 8 0 27.83 2.89 16 -8 0 1.33 1.15 16 -8 0 1.1 1.69 -16 8 0 2.39 0.98 -16 8 0 4 1.61 -16 8 0 5.64 0.84 14 -8 0 14.06 1.73 14 -8 0 9.07 2.04 14 -8 0 17.25 1.97 -14 8 0 12.35 1.69 -14 8 0 9.08 1.91 12 -8 0 107.91 10.66 12 -8 0 113.91 10.61 12 -8 0 113.03 10.66 12 -8 0 107.86 10.65 -12 8 0 113.04 10.58 -12 8 0 112.26 10.56 -12 8 0 109.57 10.65 -12 8 0 116.22 10.53 10 -8 0 47.68 4.75 10 -8 0 48.28 4.7 10 -8 0 47.66 4.75 10 -8 0 49.05 4.74 -10 8 0 47.21 4.63 -10 8 0 49.81 4.75 -10 8 0 48.84 4.61 -10 8 0 50.55 4.67 8 -8 0 37.03 3.49 8 -8 0 34.3 3.51 8 -8 0 35.59 3.45 8 -8 0 35.54 3.5 -8 8 0 36.14 3.49 -8 8 0 34.38 3.41 -8 8 0 32.85 3.36 -8 8 0 36.89 3.38 6 -8 0 15.13 1.76 6 -8 0 15.65 1.72 6 -8 0 14.97 1.67 -6 8 0 15.75 1.62 -6 8 0 17.68 1.62 -6 8 0 16.37 1.61 -6 8 0 15.66 1.72 4 -8 0 15.69 1.63 4 -8 0 11.4 1.58 4 -8 0 15.98 1.61 4 -8 0 14.15 1.66 -4 8 0 16.95 1.64 -4 8 0 15.82 1.53 -4 8 0 16.19 1.54 -4 8 0 14.79 1.54 2 -8 0 16.71 1.9 2 -8 0 18.78 1.83 2 -8 0 19.06 1.82 2 -8 0 17.27 1.84 -2 8 0 18.29 1.84 -2 8 0 16.69 1.87 -2 8 0 16.67 1.85 -2 8 0 16.82 1.74 -2 8 0 16.12 1.76 -2 8 0 18.29 1.74 0 -8 0 7.69 1.23 0 -8 0 9.91 1.13 0 -8 0 11 1.09 0 -8 0 9.11 1.27 0 8 0 10.3 1.1 0 8 0 9.83 1.03 0 8 0 8.92 1.16 0 8 0 6.1 1.23 0 8 0 11.42 1.16 -2 -8 0 16.69 1.96 -2 -8 0 18.96 2.03 -2 -8 0 18.5 1.86 -2 -8 0 17.61 1.86 2 8 0 17.62 1.93 2 8 0 19.02 1.88 2 8 0 18.62 1.81 2 8 0 18.9 1.9 -4 -8 0 14.22 1.49 -4 -8 0 13.89 1.49 -4 -8 0 15.15 1.8 -4 -8 0 15.85 1.62 -4 -8 0 16.15 1.58 4 8 0 15.96 1.65 4 8 0 16.28 1.62 4 8 0 16.05 1.54 4 8 0 15.15 1.62 -6 -8 0 15.04 1.61 -6 -8 0 15.63 1.84 -6 -8 0 14.39 1.66 -6 -8 0 15.49 1.56 6 8 0 16.44 1.66 6 8 0 16.61 1.66 6 8 0 16.28 1.69 6 8 0 15.36 1.58 -8 -8 0 30.37 3.32 -8 -8 0 33.8 3.5 -8 -8 0 34.57 3.26 -8 -8 0 36.68 3.32 8 8 0 33.51 3.26 8 8 0 32.58 3.23 8 8 0 33.32 3.32 8 8 0 32.52 3.31 8 8 0 36.61 3.33 -10 -8 0 44.61 4.54 -10 -8 0 47.46 4.62 -10 -8 0 40.54 4.46 -10 -8 0 48.29 4.34 10 8 0 42.33 4.47 10 8 0 46.4 4.37 10 8 0 47.71 4.42 -12 -8 0 103.98 9.59 -12 -8 0 101.28 9.74 12 8 0 100.96 9.52 12 8 0 96.2 9.58 -14 -8 0 14.52 1.84 14 8 0 13.93 1.76 14 8 0 16.12 1.75 -16 -8 0 2.21 0.61 -16 -8 0 1.84 0.56 16 8 0 2.06 0.46 -18 -8 0 17.69 2.31 -18 -8 0 22.61 2.36 -18 -8 0 23.21 2.67 18 8 0 20.37 2.28 18 8 0 22.57 2.27 18 8 0 22.41 2.25 -20 -8 0 8.99 1.77 -20 -8 0 9.26 1.32 -20 -8 0 7.31 1.34 20 8 0 9.14 1.1 20 8 0 5.79 1.21 20 8 0 8.76 1.19 -22 -8 0 -0.18 1.11 -22 -8 0 0.3 0.7 -22 -8 0 -0.36 0.64 22 8 0 0.29 0.45 22 8 0 -0.04 1.3 22 8 0 0.18 0.51 29 -9 0 10.29 2.2 -29 9 0 7.26 2.34 -29 9 0 9.72 2.11 -29 9 0 16.09 2.06 27 -9 0 6.8 2.19 -27 9 0 1.41 1.7 -27 9 0 3.38 2.01 -27 9 0 5.06 1.77 -27 9 0 7.17 1.68 25 -9 0 1.03 1.58 25 -9 0 1.36 0.78 -25 9 0 0.2 0.67 -25 9 0 2.22 1.71 -25 9 0 -0.02 1.88 -25 9 0 1.29 1.44 23 -9 0 27.98 3.2 23 -9 0 25.32 3 23 -9 0 24.41 2.89 -23 9 0 30.55 3.44 -23 9 0 28.57 3.21 -23 9 0 30.29 3.04 21 -9 0 15.51 1.97 21 -9 0 16.46 2.14 21 -9 0 18.46 2.28 21 -9 0 17.22 2.04 -21 9 0 17.53 1.98 -21 9 0 20.65 2.58 19 -9 0 5.87 1.71 19 -9 0 4.22 1.45 19 -9 0 6.28 1.98 -19 9 0 7.86 1.04 -19 9 0 7.87 1.15 -19 9 0 6.79 1.45 -19 9 0 7.02 1.85 17 -9 0 36.42 3.69 -17 9 0 35.06 3.58 -17 9 0 39.04 3.93 -17 9 0 36.54 3.68 -15 9 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8.45 1 9 0 88.15 8.53 1 9 0 81.75 8.56 1 9 0 88.47 8.47 -3 -9 0 37.53 3.26 -3 -9 0 39.31 3.45 -3 -9 0 33.74 3.35 -3 -9 0 35.8 3.25 3 9 0 29.98 3.29 3 9 0 30.25 3.18 3 9 0 30.86 3.24 3 9 0 28.65 3.26 -5 -9 0 19.63 1.93 -5 -9 0 19.26 1.8 -5 -9 0 18.92 1.88 -5 -9 0 18.2 1.79 -5 -9 0 17.96 2.04 -5 -9 0 19.2 2.14 5 9 0 16.15 1.91 5 9 0 18.1 1.96 5 9 0 17.12 1.83 5 9 0 18.3 1.93 -7 -9 0 100.77 10.39 -7 -9 0 108.46 10.44 -7 -9 0 106.47 10.58 7 9 0 116.76 10.45 7 9 0 117.97 10.46 7 9 0 111.7 10.39 7 9 0 108.12 10.44 -9 -9 0 33.87 3.68 -9 -9 0 37.34 3.74 -9 -9 0 39.47 3.87 -9 -9 0 38.67 3.98 9 9 0 43.51 3.86 9 9 0 39.79 3.77 9 9 0 37.62 3.68 9 9 0 38.1 3.76 -11 -9 0 23.54 2.96 -11 -9 0 24.25 2.42 -11 -9 0 23.5 2.52 11 9 0 21.34 2.5 11 9 0 23.73 2.45 11 9 0 21.56 2.3 -13 -9 0 4 1.23 -13 -9 0 10.32 1.78 -13 -9 0 3.76 1.04 13 9 0 2.38 0.84 13 9 0 3.88 1.07 13 9 0 4.29 1.07 -15 -9 0 44.72 5.51 -15 -9 0 50.48 5.18 -15 -9 0 46.22 5.21 15 9 0 51.24 5.09 15 9 0 59.79 5.14 15 9 0 58.67 5.16 -17 -9 0 33.51 3.9 -17 -9 0 27.07 3.28 -17 -9 0 26.42 3.24 17 9 0 32.38 3.2 17 9 0 37.46 3.2 17 9 0 34.74 3.24 -19 -9 0 5.02 1.32 -19 -9 0 3 0.78 -19 -9 0 6.61 1.14 19 9 0 4.09 0.78 19 9 0 3.07 0.66 19 9 0 4.43 0.81 -21 -9 0 13.48 1.66 -21 -9 0 5.96 2.18 -21 -9 0 12.92 2.11 21 9 0 9.75 1.6 21 9 0 16.18 1.9 21 9 0 12.03 2 -23 -9 0 6.86 2.37 23 9 0 15.13 2.13 23 9 0 12.47 1.69 -25 -9 0 0.02 1.7 -25 -9 0 0.43 2.31 -25 -9 0 0.37 1.79 25 9 0 2.51 1.26 25 9 0 0.71 1.52 -27 -9 0 2.49 2.8 28 -10 0 2.61 1.94 28 -10 0 2.35 1.91 -28 10 0 3.29 1.58 -28 10 0 2.54 1.76 -28 10 0 3.43 1.29 -28 10 0 1.88 1.66 26 -10 0 21 2.83 -26 10 0 13.94 2.45 -26 10 0 13.26 2.18 -26 10 0 10.25 2.46 -26 10 0 18.41 2.34 24 -10 0 5.84 1.27 24 -10 0 5.02 1.12 24 -10 0 6.18 1.96 -24 10 0 10.33 1.69 -24 10 0 5.89 1.79 -24 10 0 7.82 1.4 22 -10 0 14.48 1.75 22 -10 0 10.05 1.64 22 -10 0 10.49 1.79 22 -10 0 8.93 1.94 -22 10 0 15.19 1.62 -22 10 0 11.91 2.27 20 -10 0 19.63 2.31 20 -10 0 21.63 2.31 20 -10 0 24.32 2.53 20 -10 0 19.45 2.73 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36.08 3.29 -5 11 0 34.45 3.48 -5 11 0 35.27 3.43 3 -11 0 12.97 1.87 3 -11 0 14.58 1.47 3 -11 0 10.01 1.43 -3 11 0 9.09 1.51 -3 11 0 9.31 1.95 -3 11 0 11.51 1.92 1 -11 0 7.24 1.51 1 -11 0 1.7 1.05 -1 11 0 1.64 1.62 -1 11 0 3.03 1.05 -1 11 0 1.3 1.25 -1 11 0 2.16 1.5 -1 -11 0 2.57 1.13 -1 -11 0 2.61 1.39 1 11 0 1.22 1.6 1 11 0 5.97 0.95 1 11 0 1.04 1.29 -3 -11 0 7.33 2.55 -3 -11 0 17.18 1.93 -3 -11 0 18.02 1.72 -3 -11 0 15.99 2.05 3 11 0 16.85 1.62 3 11 0 15.23 1.58 3 11 0 13.58 1.71 3 11 0 14.97 1.77 3 11 0 14.53 1.84 -5 -11 0 37.54 3.54 -5 -11 0 34.78 3.61 -5 -11 0 32.03 3.34 -5 -11 0 31.35 3.18 -5 -11 0 37.39 3.35 5 11 0 30.63 3.35 5 11 0 32.47 3.41 5 11 0 30.22 3.34 5 11 0 36 3.26 -7 -11 0 22.79 2.55 -7 -11 0 18.89 2.06 -7 -11 0 20.48 2.16 -7 -11 0 21.44 2.23 -7 -11 0 21.14 2.39 7 11 0 19.05 2.25 7 11 0 22.08 2.11 7 11 0 21.75 2.28 7 11 0 20.81 2.23 -9 -11 0 13.35 1.6 -9 -11 0 12.75 1.88 -9 -11 0 12.31 1.64 -9 -11 0 12.76 1.55 -9 -11 0 15.78 1.72 9 11 0 12.54 1.56 9 11 0 10.52 1.39 9 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1.23 0.38 13 3 -10 39.76 4.11 13 3 -10 40.59 4.13 -13 -3 10 45.49 4.16 -13 -3 10 45.52 4.12 11 3 -10 101.61 8.59 11 3 -10 91.1 8.55 11 3 -10 102.59 8.62 -11 -3 10 87.39 8.61 -11 -3 10 83.65 8.56 -11 -3 10 86.84 8.6 -11 -3 10 83.49 8.53 9 3 -10 306.61 28.86 9 3 -10 323.68 28.85 9 3 -10 308.27 28.88 -9 -3 10 292.84 28.86 -9 -3 10 312.65 28.88 -9 -3 10 287.62 28.84 -9 -3 10 321.53 28.89 7 3 -10 11.87 1.34 7 3 -10 11.02 1.3 -7 -3 10 14.18 1.31 -7 -3 10 15.12 1.37 -7 -3 10 14.04 1.42 5 3 -10 139.7 14 5 3 -10 138.48 14.02 5 3 -10 137.41 13.96 5 3 -10 133.34 13.99 -5 -3 10 158.64 14.01 -5 -3 10 169.56 14.01 -5 -3 10 163.43 13.97 3 3 -10 26.83 2.19 3 3 -10 25.38 2.25 -3 -3 10 21.08 2.24 -3 -3 10 20.95 2.19 -3 -3 10 21.29 2.26 -3 -3 10 22.3 2.24 -3 -3 10 21.66 2.25 1 3 -10 279.85 26.05 1 3 -10 286.29 26.05 -1 -3 10 278.88 26.05 -1 -3 10 276.17 26.07 -1 -3 10 270.19 26.07 -1 -3 10 273.96 26.07 -1 3 -10 229.24 20.98 -1 3 -10 224.03 20.98 1 -3 10 217.93 21 1 -3 10 216.91 20.98 1 -3 10 233.6 21 1 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52.87 5.38 -5 3 -14 52.35 5.35 5 -3 14 61.85 5.48 -7 3 -14 90.83 8.15 -7 3 -14 91.4 8.01 7 -3 14 75.67 7.97 7 -3 14 85.98 8.07 7 -3 14 79.22 8.05 -9 3 -14 41.97 4.15 -9 3 -14 43.41 4.23 -9 3 -14 45.94 4.21 -9 3 -14 43.16 4.37 9 -3 14 38.35 4.19 9 -3 14 51.77 4.43 9 -3 14 44.69 4.3 -11 3 -14 64.47 6.21 -11 3 -14 63.86 6.04 -11 3 -14 63.39 6.02 11 -3 14 70.93 6.14 11 -3 14 63.06 6.13 11 -3 14 55.6 5.96 -13 3 -14 35.85 3.76 -13 3 -14 38.26 3.57 -13 3 -14 35.56 3.53 13 -3 14 37.87 3.67 13 -3 14 33.35 3.69 -15 3 -14 29.11 2.75 -15 3 -14 27.06 2.8 -15 3 -14 27.42 3.05 15 -3 14 24.72 2.95 15 -3 14 29.81 2.93 17 -3 14 3.86 0.87 -19 3 -14 10.45 2.42 -21 3 -14 5.13 2.38 -23 3 -14 7.8 2.48 -23 3 -14 10.02 1.21 23 -3 14 9.69 2.43 -25 3 -14 0.53 0.86 -25 3 -14 2.8 2.55 25 -3 14 3.21 2.52 -36 -2 14 -0.42 1.57 -36 -2 14 0.14 1.68 -34 -2 14 -2.05 1.69 32 2 -14 2.53 1.86 32 2 -14 0.68 1.28 -32 -2 14 0.57 0.73 30 2 -14 12.34 1.43 30 2 -14 11.04 2.06 -30 -2 14 9.6 1.56 28 2 -14 0.72 0.55 28 2 -14 1.09 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90.26 9.01 9 -3 0 44.94 4.15 9 -3 0 48.65 4.19 9 -3 0 45.71 4.16 9 -3 0 46.33 4.16 -9 3 0 37.88 4.13 -9 3 0 38.3 4.16 -9 3 0 43.8 4.15 7 -3 0 367.21 33.44 7 -3 0 388.75 33.46 7 -3 0 350.63 33.45 7 -3 0 400.01 33.47 -7 3 0 365.07 33.44 -7 3 0 327.66 33.44 -7 3 0 355.78 33.45 -7 3 0 329.67 33.45 -7 3 0 324.85 33.44 5 -3 0 362.96 32.84 5 -3 0 377.14 32.86 5 -3 0 397.81 32.86 5 -3 0 400.1 32.86 -5 3 0 345.48 32.83 -5 3 0 319.46 32.85 -5 3 0 332.26 32.83 -5 3 0 308.91 32.84 -5 3 0 320.3 32.85 -5 3 0 339.43 32.84 3 -3 0 512.39 48.3 3 -3 0 501.09 48.24 3 -3 0 508.85 48.22 3 -3 0 547.1 48.26 3 -3 0 479.02 48.22 3 -3 0 529.37 48.25 -3 3 0 506.83 48.24 -3 3 0 521.78 48.25 -3 3 0 519.38 48.25 -3 3 0 514.25 48.26 -3 3 0 518.85 48.22 -3 3 0 511 48.22 -3 3 0 535.49 48.23 -3 3 0 497.78 48.26 -3 3 0 509.37 48.22 -3 3 0 521.74 48.25 1 -3 0 769.54 68.78 1 -3 0 743.59 68.67 1 -3 0 792.43 68.7 1 -3 0 796.98 68.83 1 -3 0 704.43 68.68 -1 3 0 687.98 68.67 -1 3 0 704.61 68.75 -1 3 0 681.56 68.68 -1 3 0 735.96 68.7 -1 3 0 717.29 68.68 -1 -3 0 665.96 67.79 -1 -3 0 724.34 67.91 -1 -3 0 697.78 67.8 -1 -3 0 702.6 67.8 1 3 0 788.23 67.81 1 3 0 764.15 67.87 -3 -3 0 503.6 48.27 -3 -3 0 518.08 48.27 -3 -3 0 531.04 48.31 -3 -3 0 486.13 48.28 -3 -3 0 543.99 48.28 -3 -3 0 491.04 48.25 -3 -3 0 522.14 48.25 3 3 0 494.72 48.29 3 3 0 561.84 48.27 3 3 0 521.6 48.27 3 3 0 504.39 48.29 3 3 0 513.54 48.27 3 3 0 508.32 48.25 3 3 0 507.71 48.3 -5 -3 0 340.05 33.29 -5 -3 0 317.56 33.25 -5 -3 0 315.62 33.24 -5 -3 0 331.48 33.24 -5 -3 0 334.84 33.25 -5 -3 0 330.41 33.23 -5 -3 0 352.6 33.22 5 3 0 382.32 33.23 5 3 0 365.1 33.28 5 3 0 397.72 33.25 5 3 0 364.07 33.22 5 3 0 381.76 33.24 5 3 0 372.03 33.25 5 3 0 362.32 33.26 5 3 0 371.07 33.23 -7 -3 0 359 32.74 -7 -3 0 322.92 32.67 -7 -3 0 327.58 32.68 -7 -3 0 333.71 32.67 -7 -3 0 335.04 32.69 -7 -3 0 321.18 32.68 7 3 0 387.63 32.69 7 3 0 352.82 32.67 7 3 0 353.95 32.68 7 3 0 382.35 32.68 7 3 0 338.1 32.72 7 3 0 367.46 32.67 -9 -3 0 41.41 4.13 -9 -3 0 43.34 4.2 -9 -3 0 38.48 4.11 -9 -3 0 45.06 4.14 -9 -3 0 42.33 4.11 9 3 0 44.55 4.12 9 3 0 47.56 4.13 9 3 0 43.99 4.1 -11 -3 0 104.35 10.74 11 3 0 114.89 10.7 11 3 0 127.96 10.77 11 3 0 108.32 10.74 -13 -3 0 61.59 7.19 13 3 0 82.29 6.96 -15 -3 0 89.47 8.57 15 3 0 90.28 8.47 15 3 0 88.31 8.53 -17 -3 0 111.08 11.26 -17 -3 0 136 11.38 -17 -3 0 122.7 11.39 17 3 0 107.69 11.28 17 3 0 121.67 11.26 17 3 0 116.42 11.22 -19 -3 0 -0.49 0.26 -19 -3 0 0.68 0.5 -19 -3 0 0.62 0.79 -19 -3 0 0.58 0.43 19 3 0 0.33 0.98 19 3 0 -0.43 0.45 19 3 0 -0.01 0.34 -21 -3 0 25.87 2.91 -21 -3 0 24.69 2.96 -21 -3 0 31.06 3.1 -21 -3 0 22.87 2.92 21 3 0 28.93 3 21 3 0 34.05 2.82 21 3 0 31.62 2.92 -23 -3 0 19.74 1.93 -23 -3 0 17.01 1.99 -23 -3 0 16.66 2.61 23 3 0 13.36 2.01 -25 -3 0 2.75 1.86 -25 -3 0 4.56 1.43 -25 -3 0 1.65 0.75 25 3 0 0.04 1.72 -29 -3 0 5.8 1.72 -31 -3 0 16.29 2.17 31 3 0 7.58 2.78 -32 4 0 4.13 0.79 -30 4 0 3.55 0.99 -28 4 0 4.6 1.01 26 -4 0 3.17 0.7 -26 4 0 2.56 1.31 -26 4 0 2.66 0.84 24 -4 0 5.4 2.15 -24 4 0 4.8 1.76 22 -4 0 36 4.44 22 -4 0 44.59 4.34 -22 4 0 49.16 4.22 -22 4 0 43.97 4.32 -22 4 0 40.88 4.22 -22 4 0 48.23 4.42 20 -4 0 26.25 2.69 20 -4 0 23.45 2.86 20 -4 0 26.78 2.74 -20 4 0 29.6 2.6 -20 4 0 26.71 2.71 -20 4 0 25.49 2.6 -20 4 0 28.46 2.81 18 -4 0 3.5 0.71 18 -4 0 3.07 1.2 -18 4 0 3.56 0.72 -18 4 0 3.4 0.54 -18 4 0 2.62 0.64 -18 4 0 3.47 0.5 16 -4 0 132.85 12.22 16 -4 0 138.41 12.18 16 -4 0 134.03 12.21 -16 4 0 130.03 12.17 -16 4 0 121.97 12.15 -16 4 0 124.41 12.07 -16 4 0 119.75 12.07 14 -4 0 97.58 9.31 14 -4 0 100.26 9.31 14 -4 0 95.33 9.33 14 -4 0 100.9 9.37 -14 4 0 102.48 9.32 -14 4 0 91.54 9.22 -14 4 0 98.35 9.28 12 -4 0 47.81 4.86 12 -4 0 55.06 4.83 12 -4 0 52.11 4.91 12 -4 0 52.18 4.84 -12 4 0 44.72 4.8 10 -4 0 21.89 2.19 10 -4 0 21.5 2.21 10 -4 0 22.39 2.23 10 -4 0 20.61 2.2 -10 4 0 24.31 2.18 8 -4 0 103.31 9.68 8 -4 0 99.71 9.68 8 -4 0 102.06 9.68 8 -4 0 96.96 9.66 -8 4 0 111.38 9.65 -8 4 0 108.67 9.65 -8 4 0 94.11 9.71 6 -4 0 737.33 68.97 6 -4 0 775.73 68.97 6 -4 0 722.31 68.95 6 -4 0 804.63 68.97 -6 4 0 738.5 68.93 -6 4 0 687.79 68.95 -6 4 0 700.81 68.97 -6 4 0 724.38 68.93 -6 4 0 730.06 68.95 4 -4 0 174.08 15.7 4 -4 0 177.88 15.71 4 -4 0 159.73 15.69 4 -4 0 172.44 15.74 4 -4 0 156.47 15.66 -4 4 0 167.24 15.66 -4 4 0 171.25 15.71 -4 4 0 159.54 15.7 -4 4 0 165.56 15.71 -4 4 0 171.84 15.67 -4 4 0 173.73 15.68 -4 4 0 164.63 15.72 -4 4 0 162.2 15.69 -4 4 0 171.71 15.69 -4 4 0 157.57 15.67 2 -4 0 640.16 59.91 2 -4 0 625.88 59.86 2 -4 0 672.68 59.86 2 -4 0 646.65 59.89 2 -4 0 603.84 59.83 2 -4 0 603.57 59.84 2 -4 0 680.75 59.91 -2 4 0 642.44 59.87 -2 4 0 636.55 59.86 -2 4 0 624.86 59.83 -2 4 0 627.76 59.89 -2 4 0 650.73 59.88 -2 4 0 668.18 59.83 -2 4 0 618.38 59.85 0 -4 0 0.28 0.32 0 -4 0 0.26 0.18 0 -4 0 0.24 0.52 0 -4 0 0.46 0.17 0 -4 0 0.16 0.45 0 -4 0 0.57 0.45 0 -4 0 0.51 0.16 0 4 0 0.91 0.37 0 4 0 -0.1 0.43 0 4 0 0.55 0.18 0 4 0 0.41 0.18 0 4 0 0.12 0.48 -2 -4 0 634.68 60.14 -2 -4 0 621.78 60.12 -2 -4 0 668.43 60.22 -2 -4 0 699.42 60.13 -2 -4 0 638.58 60.14 -2 -4 0 615.85 60.13 2 4 0 660.9 60.13 2 4 0 635.44 60.14 2 4 0 650.28 60.15 2 4 0 614.21 60.14 2 4 0 605.12 60.17 2 4 0 639.57 60.14 2 4 0 657.95 60.17 -4 -4 0 159.3 15.62 -4 -4 0 171.74 15.67 -4 -4 0 169.92 15.6 -4 -4 0 158.72 15.6 -4 -4 0 171.42 15.62 4 4 0 170.32 15.62 4 4 0 175.46 15.62 4 4 0 162.51 15.62 4 4 0 159.56 15.59 4 4 0 153.1 15.65 4 4 0 170.87 15.6 4 4 0 170.92 15.63 -6 -4 0 742.32 66.82 -6 -4 0 648.97 66.85 -6 -4 0 695.41 66.85 -6 -4 0 637.21 66.83 -6 -4 0 716.84 66.91 -6 -4 0 761.62 66.86 6 4 0 743.49 66.84 6 4 0 734.93 66.83 6 4 0 692.42 66.82 6 4 0 737.08 66.85 6 4 0 715.57 66.85 6 4 0 733.35 66.85 -8 -4 0 110.28 9.77 -8 -4 0 101.89 9.75 -8 -4 0 104.29 9.83 8 4 0 100.08 9.74 8 4 0 103.23 9.75 8 4 0 105.56 9.76 8 4 0 105.16 9.74 8 4 0 97.65 9.74 -10 -4 0 19.77 2.18 -10 -4 0 22.32 2 10 4 0 18.58 2.11 10 4 0 19.74 1.98 -12 -4 0 37.54 4.6 -12 -4 0 46.69 4.3 12 4 0 44.37 4.31 12 4 0 46.23 4.28 -14 -4 0 73.78 7.86 -14 -4 0 94.29 7.83 14 4 0 77.28 7.81 14 4 0 75.58 7.76 14 4 0 88.17 7.79 -16 -4 0 120.54 11.33 16 4 0 127.98 11.34 16 4 0 103.38 11.26 16 4 0 125.35 11.29 -18 -4 0 2.75 0.67 -18 -4 0 -0.04 1.67 -18 -4 0 4.13 1.34 18 4 0 6.02 0.82 18 4 0 5.16 0.68 18 4 0 5.28 0.9 -20 -4 0 25.33 2.64 -20 -4 0 22.88 2.59 -20 -4 0 27.6 2.82 20 4 0 23.79 2.65 20 4 0 25.07 2.49 20 4 0 26.39 2.58 -22 -4 0 38.77 4.01 -22 -4 0 40.89 4.09 -22 -4 0 46.22 4.22 22 4 0 42.24 3.9 22 4 0 33.96 4.04 -24 -4 0 0.08 1.56 -32 -4 0 8.29 2.04 -32 -4 0 2.74 1.05 32 4 0 2.08 0.95 -31 5 0 -1.37 0.88 27 -5 0 5.91 1.65 25 -5 0 0.75 1.55 25 -5 0 3.6 1.95 -25 5 0 3.58 1.74 23 -5 0 1.09 1.9 23 -5 0 2.03 0.61 -23 5 0 3.74 1.53 21 -5 0 23.32 2.33 21 -5 0 22.57 2.39 21 -5 0 21.11 2.55 -21 5 0 20.66 2.3 -21 5 0 24.09 2.42 19 -5 0 1.58 0.61 19 -5 0 1.29 0.5 19 -5 0 0.42 0.58 -19 5 0 0.43 0.51 -19 5 0 0.98 0.51 17 -5 0 15.7 1.64 17 -5 0 15.29 1.61 -17 5 0 10.56 1.96 -17 5 0 14.04 1.55 15 -5 0 22.53 2.06 15 -5 0 17.11 2.14 -15 5 0 18.57 1.95 13 -5 0 9.8 1.69 13 -5 0 11.08 1.63 13 -5 0 10.89 1.83 13 -5 0 15.9 1.51 -13 5 0 14 1.4 -13 5 0 15.35 1.45 11 -5 0 24.24 2.53 11 -5 0 28.36 2.58 11 -5 0 25.26 2.51 11 -5 0 25.05 2.55 -11 5 0 24.98 2.5 -11 5 0 25.54 2.49 9 -5 0 116.65 10.61 9 -5 0 106.21 10.6 9 -5 0 106.91 10.57 9 -5 0 108.1 10.61 -9 5 0 116.63 10.56 -9 5 0 117.61 10.56 7 -5 0 37.3 3.65 7 -5 0 36.76 3.68 7 -5 0 39.54 3.68 7 -5 0 37.06 3.68 -7 5 0 40.1 3.67 -7 5 0 38.83 3.62 -7 5 0 38.18 3.59 -7 5 0 38.25 3.63 -7 5 0 36.15 3.66 5 -5 0 193.02 19.58 5 -5 0 202.97 19.62 5 -5 0 203.22 19.65 5 -5 0 190.06 19.58 5 -5 0 217.73 19.64 5 -5 0 220.37 19.65 -5 5 0 199.43 19.64 -5 5 0 211.59 19.62 -5 5 0 206.94 19.63 -5 5 0 223.11 19.65 -5 5 0 206.04 19.59 -5 5 0 209.32 19.59 -5 5 0 220.77 19.61 -5 5 0 221.27 19.6 3 -5 0 2.07 0.34 3 -5 0 2.49 0.45 3 -5 0 1.98 0.36 3 -5 0 1.54 0.43 3 -5 0 2.24 0.47 3 -5 0 2.48 0.55 3 -5 0 2.11 0.61 -3 5 0 1.7 0.46 -3 5 0 1.9 0.59 -3 5 0 2.51 0.43 -3 5 0 2.28 0.43 -3 5 0 1.85 0.35 -3 5 0 1.97 0.38 1 -5 0 94.49 8.74 1 -5 0 101.79 8.79 1 -5 0 93.58 8.82 1 -5 0 97.61 8.78 1 -5 0 94.02 8.76 1 -5 0 77.71 8.79 1 -5 0 101.45 8.76 -1 5 0 87.04 8.75 -1 5 0 89.5 8.75 -1 5 0 86.78 8.76 -1 5 0 98.08 8.76 -1 5 0 88.39 8.8 -1 5 0 90.41 8.74 -1 5 0 100.2 8.79 -1 -5 0 84.44 9.02 -1 -5 0 81.63 8.98 -1 -5 0 90.67 9.01 -1 -5 0 94.28 9.07 -1 -5 0 102.95 9.01 1 5 0 95.61 9 1 5 0 103.02 9.03 1 5 0 93.31 8.98 1 5 0 99.99 9.02 1 5 0 100.57 9.01 1 5 0 103.81 9.01 -3 -5 0 1.5 0.46 -3 -5 0 1.72 0.33 -3 -5 0 2.29 0.37 -3 -5 0 1.76 0.49 3 5 0 1.53 0.44 3 5 0 2.29 0.62 3 5 0 1.67 0.57 3 5 0 2.35 0.49 3 5 0 1.67 0.6 3 5 0 2.47 0.57 -5 -5 0 193.06 19.61 -5 -5 0 210.15 19.61 -5 -5 0 201.32 19.7 -5 -5 0 229.12 19.65 5 5 0 219.25 19.64 5 5 0 210.12 19.61 5 5 0 191.75 19.6 5 5 0 208.64 19.64 5 5 0 217.86 19.64 -7 -5 0 41.24 3.61 -7 -5 0 35.94 3.68 -7 -5 0 39.25 3.54 7 5 0 37.64 3.59 7 5 0 35.78 3.54 7 5 0 38.9 3.58 7 5 0 32.52 3.53 7 5 0 36.59 3.58 7 5 0 38.62 3.56 -9 -5 0 92.65 10.33 -9 -5 0 115.53 10.24 9 5 0 108.28 10.18 9 5 0 114.45 10.21 9 5 0 108.14 10.19 9 5 0 107.54 10.18 -11 -5 0 22.01 2.23 11 5 0 19.65 2.13 11 5 0 21.12 2.13 -13 -5 0 9.77 1.78 -13 -5 0 14.3 1.48 -13 -5 0 13.57 1.46 13 5 0 12.18 1.4 13 5 0 10.47 1.34 13 5 0 11.75 1.38 -15 -5 0 16.59 1.69 -15 -5 0 12.78 2.15 -15 -5 0 10.38 1.74 15 5 0 13.71 1.5 15 5 0 12.28 1.47 15 5 0 7.87 1.41 -17 -5 0 13.06 1.7 -17 -5 0 6.8 1.98 -17 -5 0 14.3 1.65 17 5 0 14.78 1.61 17 5 0 10.95 1.5 17 5 0 11 1.41 -19 -5 0 1.29 0.53 -19 -5 0 0.24 1.91 -19 -5 0 1.1 0.55 19 5 0 1.06 0.4 19 5 0 1.59 0.5 19 5 0 0.83 0.48 -21 -5 0 23.21 2.44 -21 -5 0 29.15 2.76 -21 -5 0 21.16 2.51 21 5 0 25.25 2.59 21 5 0 22.78 2.31 21 5 0 19.1 2.48 -23 -5 0 7.2 1.63 -23 -5 0 4.96 2.31 -23 -5 0 2.23 1.07 23 5 0 6.02 1.43 23 5 0 5.06 0.77 23 5 0 3.06 1.6 -25 -5 0 1.43 1.64 -25 -5 0 0.56 2.03 25 5 0 1.8 0.63 -27 -5 0 1.22 2 27 5 0 2.7 1.54 -29 -5 0 6.73 1.75 -31 -5 0 0.86 1.89 -31 -5 0 0.85 2.25 31 5 0 3.69 2.2 30 -6 0 6.83 2.16 30 -6 0 12.16 1.79 28 -6 0 5.42 2.08 28 -6 0 1.98 1.46 -28 6 0 4.5 1.62 -28 6 0 1.87 1.64 26 -6 0 1.22 1.66 26 -6 0 3.36 2.09 -26 6 0 7.18 1.54 -26 6 0 4.99 1.68 24 -6 0 19.78 1.96 24 -6 0 13.77 1.99 24 -6 0 19.01 2.68 -24 6 0 16.5 2.19 -24 6 0 17.31 2.4 22 -6 0 18.09 2.48 22 -6 0 21.88 2.22 22 -6 0 19.92 2.29 -22 6 0 22.09 2.31 20 -6 0 32.75 3.33 20 -6 0 30.53 3.48 20 -6 0 33.6 3.33 20 -6 0 31.64 3.37 -20 6 0 36.33 3.37 -20 6 0 33.22 3.31 -20 6 0 33.38 3.36 18 -6 0 3.81 1.32 18 -6 0 2.9 0.71 18 -6 0 3.98 1.19 -18 6 0 2.5 0.9 -18 6 0 0.94 1.19 -18 6 0 4.4 0.71 16 -6 0 25.55 3.01 16 -6 0 21.05 3.02 16 -6 0 25.62 2.97 -16 6 0 30.42 2.98 -16 6 0 31.95 2.9 -16 6 0 34.5 2.96 14 -6 0 29.77 3.45 14 -6 0 32.24 3.38 14 -6 0 29.55 3.52 -14 6 0 38.91 3.37 -14 6 0 34.92 3.32 12 -6 0 53.75 4.97 12 -6 0 52.32 4.92 12 -6 0 54.79 4.99 12 -6 0 53.42 4.96 -12 6 0 45.52 4.89 -12 6 0 48.44 4.89 10 -6 0 10.23 1.19 10 -6 0 11.46 1.26 10 -6 0 9.06 1.27 10 -6 0 10.45 1.26 -10 6 0 11.55 1.16 -10 6 0 12.77 1.15 -10 6 0 9.74 1.27 8 -6 0 103.14 8.38 8 -6 0 105.09 8.38 -8 6 0 76.87 8.34 -8 6 0 84.39 8.27 -8 6 0 83.08 8.35 -8 6 0 86.69 8.31 -8 6 0 79.52 8.28 6 -6 0 152.93 14.23 6 -6 0 137.86 14.13 6 -6 0 159.5 14.13 6 -6 0 159.72 14.19 6 -6 0 168.2 14.21 6 -6 0 158.93 14.23 -6 6 0 147.86 14.15 -6 6 0 139.82 14.21 -6 6 0 143.32 14.14 -6 6 0 130.17 14.2 -6 6 0 159.34 14.15 -6 6 0 151.44 14.17 4 -6 0 28.33 3.03 4 -6 0 27.14 2.94 4 -6 0 29.39 2.94 4 -6 0 28.81 3.01 4 -6 0 29.49 2.99 -4 6 0 32.91 2.98 -4 6 0 32.6 2.96 -4 6 0 33.3 2.96 -4 6 0 32.29 2.96 -4 6 0 32.94 3.09 -4 6 0 32.63 3.02 2 -6 0 23.87 2.5 2 -6 0 27.42 2.41 2 -6 0 21.5 2.41 2 -6 0 23.6 2.44 2 -6 0 24.19 2.51 2 -6 0 20.33 2.47 -2 6 0 28.65 2.47 -2 6 0 28.15 2.53 -2 6 0 25.73 2.43 -2 6 0 25.01 2.42 -2 6 0 26.84 2.42 0 -6 0 99.26 9.6 0 -6 0 98.91 9.69 0 -6 0 107.44 9.62 0 -6 0 104.37 9.65 0 -6 0 94.97 9.66 0 6 0 104.75 9.61 0 6 0 102.07 9.65 0 6 0 102.68 9.63 0 6 0 97.34 9.59 0 6 0 108.09 9.67 -2 -6 0 25.55 2.52 -2 -6 0 26.28 2.51 -2 -6 0 25.03 2.61 -2 -6 0 25.58 2.51 2 6 0 23.64 2.56 2 6 0 25.5 2.51 2 6 0 27.18 2.6 2 6 0 28.3 2.59 -4 -6 0 32.28 2.93 -4 -6 0 32.51 2.96 -4 -6 0 31.82 3.06 4 6 0 30.37 2.91 4 6 0 30.3 3.01 4 6 0 29.21 2.95 4 6 0 30.04 2.96 4 6 0 27.19 2.91 -6 -6 0 170.5 14.97 -6 -6 0 147.41 15.04 -6 -6 0 156.71 14.93 6 6 0 143.25 14.92 6 6 0 161.54 14.96 6 6 0 167.27 14.97 6 6 0 162.74 14.96 6 6 0 161.64 14.93 -8 -6 0 84.29 9.02 -8 -6 0 80.93 8.88 8 6 0 91.27 8.88 8 6 0 100.41 8.91 8 6 0 98.64 8.93 8 6 0 95.14 8.89 8 6 0 103.99 8.95 8 6 0 101.47 8.94 -10 -6 0 2.5 1.55 -10 -6 0 10.38 1.18 10 6 0 5.15 1.05 10 6 0 8.13 0.94 10 6 0 7.47 1.06 -12 -6 0 34.65 4.14 -12 -6 0 44.36 4.17 12 6 0 43.67 4.1 12 6 0 41.37 4.12 12 6 0 47.64 4.12 -14 -6 0 33.7 3.37 14 6 0 32.87 3.29 14 6 0 32.93 3.3 -16 -6 0 20.35 1.97 -16 -6 0 16.95 2.24 -16 -6 0 11.44 2.62 16 6 0 19.92 2.07 16 6 0 16.14 2 -18 -6 0 2.01 1.9 -18 -6 0 2.27 0.64 -18 -6 0 2.05 1.29 18 6 0 4.26 0.86 18 6 0 3.72 1.27 18 6 0 4.73 1.11 -20 -6 0 24.03 2.96 -20 -6 0 34.94 3.28 20 6 0 26.45 2.99 20 6 0 29.31 2.94 20 6 0 31.38 2.87 -22 -6 0 20.56 3.08 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1.17 1.37 17 -7 0 1.09 1.08 17 -7 0 0.45 1.62 17 -7 0 0.81 1.21 -17 7 0 2.51 1.22 -17 7 0 3.97 0.88 -17 7 0 3.3 1.24 15 -7 0 76.24 7.92 15 -7 0 77.01 7.73 15 -7 0 77.96 7.87 -15 7 0 74.75 7.68 -15 7 0 84.08 7.75 -15 7 0 91.16 7.73 13 -7 0 14.6 2.32 13 -7 0 14.5 2.39 13 -7 0 23.32 2.5 -13 7 0 21.46 2.11 11 -7 0 59.46 5.96 11 -7 0 63.25 5.96 11 -7 0 63.73 5.92 11 -7 0 63.21 5.97 -11 7 0 59.61 5.88 -11 7 0 61.53 5.95 -11 7 0 62.23 5.89 9 -7 0 101.27 9.38 9 -7 0 100.33 9.33 9 -7 0 99.05 9.37 9 -7 0 105.96 9.37 -9 7 0 97.78 9.31 -9 7 0 93.47 9.28 -9 7 0 95.19 9.36 -9 7 0 95.84 9.26 -7 7 0 9.36 1.16 -7 7 0 9.6 1.02 -7 7 0 9.69 1.06 -7 7 0 10.26 1.01 5 -7 0 298.64 29.28 5 -7 0 325.82 29.22 5 -7 0 309.72 29.24 5 -7 0 311.79 29.27 -5 7 0 317.55 29.26 -5 7 0 308.95 29.21 -5 7 0 326.38 29.21 -5 7 0 291.72 29.2 3 -7 0 161.04 16.2 3 -7 0 178.77 16.17 3 -7 0 173.34 16.25 3 -7 0 182.66 16.17 3 -7 0 186.28 16.23 -3 7 0 164.66 16.18 -3 7 0 155.98 16.17 -3 7 0 164.71 16.17 -3 7 0 180.1 16.18 -3 7 0 173.87 16.22 1 -7 0 173.62 16.72 1 -7 0 169.72 16.64 1 -7 0 182.64 16.74 1 -7 0 189.83 16.66 1 -7 0 185.33 16.69 -1 7 0 181.71 16.66 -1 7 0 172.32 16.64 -1 7 0 166.8 16.66 -1 7 0 185.35 16.71 -1 7 0 164.45 16.64 -1 7 0 177.56 16.71 -1 -7 0 161.98 16.92 -1 -7 0 179.98 16.89 -1 -7 0 170.27 16.87 -1 -7 0 168.06 16.94 1 7 0 195.6 16.86 1 7 0 184.71 16.93 1 7 0 171.2 16.87 1 7 0 188.67 16.9 1 7 0 193.59 16.88 -3 -7 0 166.54 16.36 -3 -7 0 170.21 16.36 -3 -7 0 167.54 16.31 -3 -7 0 166.23 16.45 -3 -7 0 155.95 16.31 3 7 0 182.97 16.33 3 7 0 186.22 16.37 3 7 0 183.61 16.39 3 7 0 186.63 16.38 -5 -7 0 302.59 28.79 -5 -7 0 299.67 28.7 -5 -7 0 305.64 28.68 5 7 0 324.48 28.72 5 7 0 305.94 28.7 5 7 0 284.45 28.66 5 7 0 316.1 28.71 7 7 0 13.85 1.49 7 7 0 16.38 1.6 7 7 0 13.75 1.5 7 7 0 17.15 1.61 7 7 0 14.9 1.59 7 7 0 16.46 1.53 -9 -7 0 90.45 8.84 -9 -7 0 89.5 8.77 -9 -7 0 88.12 8.95 -9 -7 0 80.55 8.79 9 7 0 104.76 8.85 9 7 0 90.83 8.76 9 7 0 95.32 8.78 9 7 0 103.55 8.83 9 7 0 92.83 8.83 9 7 0 95.42 8.79 -11 -7 0 43.16 4.25 -11 -7 0 45.89 4.27 11 7 0 39.93 4.24 -13 -7 0 15.8 2.84 -13 -7 0 20.3 2.34 13 7 0 16.04 2.22 13 7 0 24.04 2.18 13 7 0 24.28 2.24 -15 -7 0 78.53 7.83 -15 -7 0 74.09 8.12 15 7 0 81.43 7.76 15 7 0 86.97 7.75 -17 -7 0 2.39 0.62 -17 -7 0 5.61 1.3 -17 -7 0 -0.7 1.9 17 7 0 0.49 0.81 17 7 0 1.38 1.01 17 7 0 1.1 1.15 -19 -7 0 1.9 0.65 -19 -7 0 1.55 0.65 -19 -7 0 2.48 1.12 19 7 0 0.65 0.85 19 7 0 5.34 0.82 -21 -7 0 6.93 1.25 -21 -7 0 5.15 1.37 -21 -7 0 5.22 0.99 21 7 0 7.93 1.11 21 7 0 5.88 1.19 21 7 0 8.21 0.95 -23 -7 0 15.15 2.28 -23 -7 0 18.13 2.88 -23 -7 0 15.46 2.18 23 7 0 11.03 2.12 -25 -7 0 32.15 3.14 -25 -7 0 25.58 3.25 25 7 0 22.49 3.1 -27 -7 0 2.48 2.19 -27 -7 0 2.99 1.85 -27 -7 0 5.19 1.63 -29 -7 0 15.25 2.17 -29 -7 0 7.69 2.81 -29 -7 0 10.99 2.42 -31 -7 0 1.34 2.37 -31 -7 0 1.26 2.02 -30 8 0 5.04 1.93 -26 8 0 1.97 1.61 24 -8 0 -0.17 2.43 24 -8 0 1.58 1.36 24 -8 0 0.43 0.7 -24 8 0 0.01 1.55 -24 8 0 1.57 1.73 22 -8 0 1.47 0.79 22 -8 0 -0.33 0.69 22 -8 0 -0.09 0.63 22 -8 0 -0.24 0.77 -22 8 0 0.55 0.61 -22 8 0 0.37 1.25 20 -8 0 9.63 1.64 20 -8 0 10.28 1.7 20 -8 0 8.33 1.45 20 -8 0 8.16 1.78 -20 8 0 10.78 1.31 -20 8 0 9.57 1.34 18 -8 0 27.01 2.98 18 -8 0 26.94 3.02 18 -8 0 24.18 2.89 18 -8 0 26.66 2.87 -18 8 0 25.8 2.66 -18 8 0 27.43 2.73 -18 8 0 27.83 2.89 16 -8 0 1.33 1.15 16 -8 0 1.1 1.69 -16 8 0 2.39 0.98 -16 8 0 4 1.61 -16 8 0 5.64 0.84 14 -8 0 14.06 1.73 14 -8 0 9.07 2.04 14 -8 0 17.25 1.97 -14 8 0 12.35 1.69 -14 8 0 9.08 1.91 12 -8 0 107.91 10.66 12 -8 0 113.91 10.61 12 -8 0 113.03 10.66 12 -8 0 107.86 10.65 -12 8 0 113.04 10.58 -12 8 0 112.26 10.56 -12 8 0 109.57 10.65 -12 8 0 116.22 10.53 10 -8 0 47.68 4.75 10 -8 0 48.28 4.7 10 -8 0 47.66 4.75 10 -8 0 49.05 4.74 -10 8 0 47.21 4.63 -10 8 0 49.81 4.75 -10 8 0 48.84 4.61 -10 8 0 50.55 4.67 8 -8 0 37.03 3.49 8 -8 0 34.3 3.51 8 -8 0 35.59 3.45 8 -8 0 35.54 3.5 -8 8 0 36.14 3.49 -8 8 0 34.38 3.41 -8 8 0 32.85 3.36 -8 8 0 36.89 3.38 6 -8 0 15.13 1.76 6 -8 0 15.65 1.72 6 -8 0 14.97 1.67 -6 8 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0.67 -25 9 0 2.22 1.71 -25 9 0 -0.02 1.88 -25 9 0 1.29 1.44 23 -9 0 27.98 3.2 23 -9 0 25.32 3 23 -9 0 24.41 2.89 -23 9 0 30.55 3.44 -23 9 0 28.57 3.21 -23 9 0 30.29 3.04 21 -9 0 15.51 1.97 21 -9 0 16.46 2.14 21 -9 0 18.46 2.28 21 -9 0 17.22 2.04 -21 9 0 17.53 1.98 -21 9 0 20.65 2.58 19 -9 0 5.87 1.71 19 -9 0 4.22 1.45 19 -9 0 6.28 1.98 -19 9 0 7.86 1.04 -19 9 0 7.87 1.15 -19 9 0 6.79 1.45 -19 9 0 7.02 1.85 17 -9 0 36.42 3.69 -17 9 0 35.06 3.58 -17 9 0 39.04 3.93 -17 9 0 36.54 3.68 -15 9 0 59.42 5.48 -15 9 0 52.73 5.48 13 -9 0 1.71 1.28 13 -9 0 1.74 0.66 -13 9 0 6.14 1.1 -13 9 0 2.93 0.79 -13 9 0 5.66 0.95 11 -9 0 27.14 2.81 11 -9 0 23.35 2.8 11 -9 0 27.98 2.74 -11 9 0 25.06 2.76 -11 9 0 27.07 2.64 -11 9 0 29.52 2.83 -11 9 0 28.07 2.61 9 -9 0 37.53 3.83 9 -9 0 42.96 3.79 9 -9 0 39.37 3.84 -9 9 0 33.32 3.65 -9 9 0 37.91 3.72 -9 9 0 38.08 3.81 -9 9 0 40.8 3.68 7 -9 0 105.09 10.72 7 -9 0 109.79 10.85 7 -9 0 120.75 10.82 7 -9 0 114.41 10.87 -7 9 0 116.61 10.85 -7 9 0 121.48 10.76 -7 9 0 107.37 10.76 -7 9 0 117.93 10.77 5 -9 0 14.54 1.99 5 -9 0 16.24 1.9 5 -9 0 15.81 1.79 5 -9 0 16.41 1.94 -5 9 0 21.64 1.97 -5 9 0 19.62 1.84 -5 9 0 21.82 1.86 -5 9 0 19.85 1.84 3 -9 0 25.39 3.13 3 -9 0 28.82 3.09 3 -9 0 30.27 3.09 -3 9 0 33.85 3.03 -3 9 0 36.53 3.12 -3 9 0 30.96 3 1 -9 0 85.14 7.63 1 -9 0 74.76 7.61 -1 9 0 63.75 7.73 -1 9 0 86.89 7.59 -1 9 0 88.86 7.66 -1 9 0 76.89 7.65 -1 9 0 79.32 7.59 -1 -9 0 91.58 8.56 -1 -9 0 91.85 8.49 -1 -9 0 92.64 8.59 -1 -9 0 96.36 8.47 1 9 0 82.11 8.45 1 9 0 88.15 8.53 1 9 0 81.75 8.56 1 9 0 88.47 8.47 -3 -9 0 37.53 3.26 -3 -9 0 39.31 3.45 -3 -9 0 33.74 3.35 -3 -9 0 35.8 3.25 3 9 0 29.98 3.29 3 9 0 30.25 3.18 3 9 0 30.86 3.24 3 9 0 28.65 3.26 -5 -9 0 19.63 1.93 -5 -9 0 19.26 1.8 -5 -9 0 18.92 1.88 -5 -9 0 18.2 1.79 -5 -9 0 17.96 2.04 -5 -9 0 19.2 2.14 5 9 0 16.15 1.91 5 9 0 18.1 1.96 5 9 0 17.12 1.83 5 9 0 18.3 1.93 -7 -9 0 100.77 10.39 -7 -9 0 108.46 10.44 -7 -9 0 106.47 10.58 7 9 0 116.76 10.45 7 9 0 117.97 10.46 7 9 0 111.7 10.39 7 9 0 108.12 10.44 -9 -9 0 33.87 3.68 -9 -9 0 37.34 3.74 -9 -9 0 39.47 3.87 -9 -9 0 38.67 3.98 9 9 0 43.51 3.86 9 9 0 39.79 3.77 9 9 0 37.62 3.68 9 9 0 38.1 3.76 -11 -9 0 23.54 2.96 -11 -9 0 24.25 2.42 -11 -9 0 23.5 2.52 11 9 0 21.34 2.5 11 9 0 23.73 2.45 11 9 0 21.56 2.3 -13 -9 0 4 1.23 -13 -9 0 10.32 1.78 -13 -9 0 3.76 1.04 13 9 0 2.38 0.84 13 9 0 3.88 1.07 13 9 0 4.29 1.07 -15 -9 0 44.72 5.51 -15 -9 0 50.48 5.18 -15 -9 0 46.22 5.21 15 9 0 51.24 5.09 15 9 0 59.79 5.14 15 9 0 58.67 5.16 -17 -9 0 33.51 3.9 -17 -9 0 27.07 3.28 -17 -9 0 26.42 3.24 17 9 0 32.38 3.2 17 9 0 37.46 3.2 17 9 0 34.74 3.24 -19 -9 0 5.02 1.32 -19 -9 0 3 0.78 -19 -9 0 6.61 1.14 19 9 0 4.09 0.78 19 9 0 3.07 0.66 19 9 0 4.43 0.81 -21 -9 0 13.48 1.66 -21 -9 0 5.96 2.18 -21 -9 0 12.92 2.11 21 9 0 9.75 1.6 21 9 0 16.18 1.9 21 9 0 12.03 2 -23 -9 0 6.86 2.37 23 9 0 15.13 2.13 23 9 0 12.47 1.69 -25 -9 0 0.02 1.7 -25 -9 0 0.43 2.31 -25 -9 0 0.37 1.79 25 9 0 2.51 1.26 25 9 0 0.71 1.52 -27 -9 0 2.49 2.8 28 -10 0 2.61 1.94 28 -10 0 2.35 1.91 -28 10 0 3.29 1.58 -28 10 0 2.54 1.76 -28 10 0 3.43 1.29 -28 10 0 1.88 1.66 26 -10 0 21 2.83 -26 10 0 13.94 2.45 -26 10 0 13.26 2.18 -26 10 0 10.25 2.46 -26 10 0 18.41 2.34 24 -10 0 5.84 1.27 24 -10 0 5.02 1.12 24 -10 0 6.18 1.96 -24 10 0 10.33 1.69 -24 10 0 5.89 1.79 -24 10 0 7.82 1.4 22 -10 0 14.48 1.75 22 -10 0 10.05 1.64 22 -10 0 10.49 1.79 22 -10 0 8.93 1.94 -22 10 0 15.19 1.62 -22 10 0 11.91 2.27 20 -10 0 19.63 2.31 20 -10 0 21.63 2.31 20 -10 0 24.32 2.53 20 -10 0 19.45 2.73 -20 10 0 19.3 2.66 -20 10 0 18.85 2.15 -20 10 0 19.14 2.42 18 -10 0 30.85 3.79 -18 10 0 34.34 3.52 -18 10 0 37.12 3.59 -18 10 0 34.71 3.78 16 -10 0 6.57 1.61 -16 10 0 4.07 1.02 -16 10 0 4.9 1.43 -16 10 0 3.93 1.15 14 -10 0 4.57 1.56 14 -10 0 1.58 1.38 -14 10 0 4.64 1.08 -14 10 0 2.25 0.82 -14 10 0 6.31 1.47 12 -10 0 1.93 1.59 12 -10 0 3.54 1.38 -12 10 0 5.99 0.8 -12 10 0 4.77 1.08 -12 10 0 3.28 1.54 10 -10 0 9.64 1.45 10 -10 0 9.45 1.47 10 -10 0 11.47 1.35 -10 10 0 11.64 1.19 -10 10 0 11.76 1.47 -10 10 0 10.39 1.13 -10 10 0 10.53 1.39 8 -10 0 60.4 5.52 8 -10 0 56.25 5.58 8 -10 0 60.65 5.61 -8 10 0 56.7 5.56 -8 10 0 54.33 5.45 -8 10 0 54.5 5.43 6 -10 0 98.32 9.26 6 -10 0 94.01 9.13 6 -10 0 103.09 9.29 6 -10 0 105.77 9.21 -6 10 0 87.22 9.14 -6 10 0 94.62 9.23 -6 10 0 92.35 9.26 -6 10 0 100.14 9.15 -6 10 0 95.31 9.14 4 -10 0 24.46 2.89 4 -10 0 25.63 2.76 4 -10 0 25.08 2.95 4 -10 0 28.46 2.88 -4 10 0 26.65 2.95 -4 10 0 35.66 2.98 -4 10 0 34.07 2.81 2 -10 0 9.38 1.95 2 -10 0 9.32 2.14 -2 10 0 9.67 2.02 -2 10 0 10.81 1.71 0 -10 0 131.83 13 0 10 0 130.12 13.03 0 10 0 143.96 13.01 0 10 0 133.14 12.96 0 10 0 144.08 12.92 -2 -10 0 24.86 2.66 -2 -10 0 27.34 2.79 -2 -10 0 24.78 2.64 2 10 0 29.5 2.58 2 10 0 24.34 2.64 2 10 0 26.93 2.73 2 10 0 25.18 2.56 2 10 0 27.67 2.7 -4 -10 0 34.03 3.26 -4 -10 0 33.74 3.04 -4 -10 0 33.41 3.02 -4 -10 0 35.12 3.19 4 10 0 27.91 2.95 4 10 0 27.29 3.07 4 10 0 25.97 3.04 4 10 0 27.05 3.01 -6 -10 0 92.61 9.03 -6 -10 0 91.45 9.22 -6 -10 0 85.09 8.96 -6 -10 0 91.57 9.05 -6 -10 0 94.84 9.14 6 10 0 96.08 9.07 6 10 0 102.94 9.07 6 10 0 101.13 9 6 10 0 101.09 9.09 -8 -10 0 49.14 4.89 -8 -10 0 49.76 5.19 -8 -10 0 50.02 4.98 -8 -10 0 49.18 4.92 8 10 0 56.18 5.01 8 10 0 53.93 4.91 8 10 0 50.27 4.87 8 10 0 53.74 5 8 10 0 49.02 4.98 -10 -10 0 12.54 2.06 -10 -10 0 9.72 1.32 -10 -10 0 8.06 1.61 10 10 0 9.17 1.18 10 10 0 11.01 1.59 10 10 0 9 1.33 10 10 0 11.33 1.55 12 10 0 2.55 1.1 12 10 0 -0.15 0.71 12 10 0 2.14 1.11 -14 -10 0 3.42 1.86 14 10 0 5.14 1.21 14 10 0 3.75 1.17 -16 -10 0 2.14 1.55 -16 -10 0 3.83 1.39 -16 -10 0 2.22 2.05 16 10 0 5.25 1.11 16 10 0 8.13 1.24 16 10 0 4.03 0.79 -18 -10 0 23.36 2.99 -18 -10 0 26.45 2.99 -18 -10 0 33.45 3.85 18 10 0 30.19 2.95 18 10 0 27.03 2.88 18 10 0 32.37 2.92 -20 -10 0 16.04 2.14 -20 -10 0 15.23 2.15 20 10 0 17.26 2.04 20 10 0 21.71 1.99 20 10 0 19.16 2.06 -22 -10 0 11.59 2.18 -22 -10 0 5.93 1.76 22 10 0 9.23 1.75 22 10 0 10.41 1.62 22 10 0 11.38 1.81 -24 -10 0 5.3 1.82 -24 -10 0 1.71 2.78 -24 -10 0 1.96 1.06 24 10 0 5.34 1.55 24 10 0 5.74 1.27 24 10 0 8.07 1.58 -26 -10 0 11.55 2.19 -26 -10 0 10.55 2.48 -26 -10 0 11.32 2.27 26 10 0 13.33 2.06 26 10 0 18.99 2.09 -28 -10 0 1.93 1.84 -28 -10 0 3.99 2.36 28 10 0 4.26 1.57 27 -11 0 -1.64 1.94 -27 11 0 2.36 1.7 -27 11 0 0.59 1.49 -27 11 0 0.25 1.6 -27 11 0 2.11 1.54 25 -11 0 -0.16 2.26 -25 11 0 0.38 1.56 -25 11 0 0.7 1.9 -25 11 0 4.7 1.83 -25 11 0 2.83 1.55 23 -11 0 2.52 0.99 23 -11 0 5.23 1.23 23 -11 0 2.79 1.07 -23 11 0 7.69 1.38 -23 11 0 4.52 1.59 21 -11 0 2.6 1.04 21 -11 0 2.02 2.04 21 -11 0 2.05 0.97 21 -11 0 2.27 0.99 -21 11 0 1.31 1.83 -21 11 0 6.59 1.03 -21 11 0 4.3 1.81 19 -11 0 1.9 1.8 -19 11 0 5.17 1.36 -19 11 0 1.98 1.21 -19 11 0 7.17 1.65 -19 11 0 6.07 1.24 17 -11 0 -0.06 1.47 -17 11 0 -0.19 1.37 -17 11 0 0.34 1.03 -17 11 0 1.93 0.95 15 -11 0 1.76 1.27 15 -11 0 2.6 1.46 -15 11 0 2.16 1.33 -15 11 0 2.08 1 -15 11 0 3.33 0.78 13 -11 0 -1.18 1.51 13 -11 0 -0.03 1.44 -13 11 0 0.14 1.4 -13 11 0 0.28 0.95 -13 11 0 -0.64 0.67 11 -11 0 13.82 2.24 11 -11 0 14.95 2.24 11 -11 0 15.35 1.81 -11 11 0 16.2 1.73 -11 11 0 17.52 1.94 -11 11 0 15.86 1.9 9 -11 0 12.4 1.79 9 -11 0 13.76 1.67 9 -11 0 12.64 1.75 -9 11 0 14.39 1.52 -9 11 0 16.36 1.77 -9 11 0 13.91 1.79 -9 11 0 15.01 1.56 7 -11 0 23.24 2.48 7 -11 0 22.69 2.52 7 -11 0 24 2.42 -7 11 0 24.1 2.32 -7 11 0 20.78 2.51 -7 11 0 21.15 2.3 -7 11 0 23.45 2.48 -7 11 0 24.15 2.33 5 -11 0 34.09 3.49 5 -11 0 31.54 3.42 5 -11 0 29 3.24 5 -11 0 35.71 3.39 -5 11 0 28.8 3.37 -5 11 0 39.16 3.33 -5 11 0 36.08 3.29 -5 11 0 34.45 3.48 -5 11 0 35.27 3.43 3 -11 0 12.97 1.87 3 -11 0 14.58 1.47 3 -11 0 10.01 1.43 -3 11 0 9.09 1.51 -3 11 0 9.31 1.95 -3 11 0 11.51 1.92 1 -11 0 7.24 1.51 1 -11 0 1.7 1.05 -1 11 0 1.64 1.62 -1 11 0 3.03 1.05 -1 11 0 1.3 1.25 -1 11 0 2.16 1.5 -1 -11 0 2.57 1.13 -1 -11 0 2.61 1.39 1 11 0 1.22 1.6 1 11 0 5.97 0.95 1 11 0 1.04 1.29 -3 -11 0 7.33 2.55 -3 -11 0 17.18 1.93 -3 -11 0 18.02 1.72 -3 -11 0 15.99 2.05 3 11 0 16.85 1.62 3 11 0 15.23 1.58 3 11 0 13.58 1.71 3 11 0 14.97 1.77 3 11 0 14.53 1.84 -5 -11 0 37.54 3.54 -5 -11 0 34.78 3.61 -5 -11 0 32.03 3.34 -5 -11 0 31.35 3.18 -5 -11 0 37.39 3.35 5 11 0 30.63 3.35 5 11 0 32.47 3.41 5 11 0 30.22 3.34 5 11 0 36 3.26 -7 -11 0 22.79 2.55 -7 -11 0 18.89 2.06 -7 -11 0 20.48 2.16 -7 -11 0 21.44 2.23 -7 -11 0 21.14 2.39 7 11 0 19.05 2.25 7 11 0 22.08 2.11 7 11 0 21.75 2.28 7 11 0 20.81 2.23 -9 -11 0 13.35 1.6 -9 -11 0 12.75 1.88 -9 -11 0 12.31 1.64 -9 -11 0 12.76 1.55 -9 -11 0 15.78 1.72 9 11 0 12.54 1.56 9 11 0 10.52 1.39 9 11 0 13.05 1.53 9 11 0 11.78 1.39 11 11 0 11.98 1.79 15 11 0 1.21 1.25 15 11 0 4.48 1.3 -17 -11 0 1.24 0.66 -17 -11 0 0.61 1.45 -17 -11 0 2.97 2.27 17 11 0 1.49 0.62 17 11 0 0.07 1.27 17 11 0 -0.03 0.41 -19 -11 0 1.16 2.72 -19 -11 0 2.44 0.75 -19 -11 0 1.95 0.79 19 11 0 3.13 0.59 19 11 0 1.67 0.62 19 11 0 4.31 0.8 -21 -11 0 4.24 0.91 -21 -11 0 1.39 0.76 -21 -11 0 1.38 1.35 21 11 0 2.67 1.59 21 11 0 1.7 0.57 21 11 0 1.77 0.63 -23 -11 0 4.03 1.9 23 11 0 3.53 1.5 25 11 0 0.39 0.86 26 -12 0 0.26 0.93 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0 13.89 1.53 -6 12 0 15.64 1.58 -6 12 0 16.77 1.76 -6 12 0 14.47 1.79 -6 12 0 14.55 1.53 4 -12 0 2.53 1.6 4 -12 0 2.92 1.94 -4 12 0 2.78 1.8 -4 12 0 4.86 1.39 -4 12 0 8.86 1.16 -4 12 0 4.93 1.26 -4 12 0 4.02 1.71 2 -12 0 0.83 1.64 2 -12 0 1.62 1.06 2 -12 0 1.42 1.44 -2 12 0 0.86 1.54 -2 12 0 1.37 1.64 -2 12 0 3.57 1 0 -12 0 2.51 1.12 0 -12 0 0.79 1.73 0 -12 0 1.69 1.44 0 -12 0 1.4 1.46 0 12 0 0.94 1.27 0 12 0 1.07 1.58 -2 -12 0 2.64 1.51 -2 -12 0 1.74 1.23 -2 -12 0 0.53 1.95 2 12 0 0.56 1.48 2 12 0 0.22 1.45 2 12 0 1.95 1.04 2 12 0 -0.25 1.61 -4 -12 0 13.84 1.96 -4 -12 0 13.09 1.78 -4 -12 0 13.04 1.57 -4 -12 0 12.43 1.56 4 12 0 14.46 1.42 4 12 0 8.46 1.58 4 12 0 13.59 1.36 4 12 0 13.8 1.68 4 12 0 11.36 1.56 -6 -12 0 15.93 1.65 -6 -12 0 12.42 1.32 -6 -12 0 17.02 1.89 -6 -12 0 16.92 1.58 -6 -12 0 15.93 2.02 6 12 0 11.95 1.39 6 12 0 12.33 1.46 6 12 0 12.2 1.69 6 12 0 12.43 1.64 6 12 0 11.09 1.61 -8 -12 0 25.88 2.63 -8 -12 0 24.4 2.73 -8 -12 0 28.82 3.03 -8 -12 0 28.04 2.82 -8 -12 0 28.17 3.17 8 12 0 24.96 2.6 8 12 0 27.83 2.85 8 12 0 27.2 2.81 8 12 0 29 2.69 10 12 0 8.15 1.08 10 12 0 11.93 1.81 -16 -12 0 14.48 2.92 16 12 0 13.33 1.68 16 12 0 12.18 1.61 -18 -12 0 1.59 0.77 -18 -12 0 0.21 0.69 -18 -12 0 1.31 2.8 -18 -12 0 0.92 1.85 18 12 0 2.19 0.52 18 12 0 2.52 0.73 18 12 0 1.08 1.52 -20 -12 0 2.29 1.44 -20 -12 0 3.91 0.99 -20 -12 0 3.32 0.84 20 12 0 3.33 0.64 20 12 0 4.03 0.86 20 12 0 1.93 0.67 -22 -12 0 -0.5 3.04 -22 -12 0 1.76 0.81 -22 -12 0 0.57 0.81 -22 -12 0 -0.77 1.1 22 12 0 1.72 0.59 -26 -12 0 -0.76 2.13 23 -13 0 8.37 1.4 23 -13 0 5.42 1.22 -23 13 0 11 2.32 -23 13 0 2.17 1.06 21 -13 0 20.98 2.97 21 -13 0 28.35 3.65 -21 13 0 28.35 2.77 -21 13 0 27.41 2.88 -21 13 0 31.26 3.51 -21 13 0 29.5 3.55 19 -13 0 6.66 2.1 -19 13 0 4.94 1.01 -19 13 0 5.42 1.04 -19 13 0 2.94 1.99 -19 13 0 2.57 2.07 17 -13 0 12.77 2.11 -17 13 0 7.62 2.36 -17 13 0 15.84 1.89 15 -13 0 11.99 2.1 -15 13 0 8.23 2.05 13 -13 0 12.51 2.14 -13 13 0 11.62 2.21 11 -13 0 24.58 2.64 -11 13 0 23.31 2.65 -11 13 0 17.22 3.11 -11 13 0 23.4 2.52 9 -13 0 56.2 6.02 9 -13 0 66.56 6.08 -9 13 0 57.32 6.04 -9 13 0 63.82 5.86 -9 13 0 59.73 6 7 -13 0 34.33 3.19 7 -13 0 26.25 3.05 -7 13 0 28.55 3.05 -7 13 0 29.49 2.89 -7 13 0 28.85 2.87 -7 13 0 24.1 3.09 5 -13 0 17.87 2.73 5 -13 0 27.61 2.51 5 -13 0 17.6 2.13 -5 13 0 19.93 2.25 -5 13 0 23.11 2.17 -5 13 0 10.88 2.79 3 -13 0 58.43 5.41 -3 13 0 46.3 5.38 -3 13 0 61.89 5.2 -3 13 0 44.77 5.46 1 -13 0 75.49 6.44 -1 13 0 55.08 6.49 -1 13 0 61.96 6.42 -1 -13 0 99.33 8.84 1 13 0 84.17 8.84 1 13 0 89.79 8.9 -3 -13 0 68.22 6.06 -3 -13 0 60.66 5.75 -3 -13 0 45.48 6.22 -3 -13 0 59.42 5.79 3 13 0 69.83 5.69 3 13 0 54.87 5.94 3 13 0 47.09 5.99 -5 -13 0 23.47 2.65 -5 -13 0 20.64 2.39 -5 -13 0 23.72 2.79 -5 -13 0 19.09 2.39 5 13 0 24.75 2.29 5 13 0 22.25 2.23 5 13 0 23.16 2.46 5 13 0 22.52 2.55 -7 -13 0 28.07 3.13 -7 -13 0 26.64 2.96 -7 -13 0 23.88 2.75 -7 -13 0 27.6 2.72 7 13 0 23.58 2.81 7 13 0 24.29 2.77 7 13 0 28.47 2.64 -9 -13 0 74.84 6.18 -9 -13 0 66.01 6.16 -9 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306.91 27.15 -1 -5 9 291.38 27.14 -1 -5 9 308.15 27.13 1 -5 9 16.39 1.73 1 -5 9 18.9 1.75 1 -5 9 17.35 1.82 1 -5 9 18.25 1.82 1 -5 9 18.72 1.82 1 -5 9 16.69 1.73 -3 5 -9 40.83 3.54 -3 5 -9 41.1 3.54 3 -5 9 34.44 3.61 3 -5 9 34.52 3.62 3 -5 9 36.12 3.58 3 -5 9 34.44 3.62 -5 5 -9 37.43 3.84 -5 5 -9 35.07 3.78 5 -5 9 41.27 3.89 5 -5 9 41.82 3.89 5 -5 9 42.15 3.9 5 -5 9 44.75 3.94 -7 5 -9 125.98 12.9 -7 5 -9 149.35 12.94 -7 5 -9 121.59 12.89 7 -5 9 134.78 13.03 7 -5 9 143.02 13.01 7 -5 9 147.01 13.03 7 -5 9 141.41 12.99 -9 5 -9 150.11 13.91 -9 5 -9 135.56 13.84 -9 5 -9 146.12 13.82 9 -5 9 157.88 13.93 9 -5 9 146.09 13.87 9 -5 9 145.17 13.92 -11 5 -9 84.38 8.59 -11 5 -9 81.62 8.58 -11 5 -9 83.92 8.69 -11 5 -9 97.94 8.59 11 -5 9 97.45 8.69 11 -5 9 89.81 8.72 11 -5 9 102.84 8.74 -13 5 -9 56.12 5.41 -13 5 -9 56.33 5.56 13 -5 9 55.07 5.52 13 -5 9 56.41 5.55 13 -5 9 60.43 5.53 -15 5 -9 6.34 1.19 -15 5 -9 6.23 0.9 15 -5 9 8.3 1.17 15 -5 9 9.38 1.19 15 -5 9 7.61 1.16 15 -5 9 7.85 1.29 -17 5 -9 26.46 2.56 -17 5 -9 22.46 2.25 -17 5 -9 19.1 2.22 17 -5 9 26.53 2.52 17 -5 9 24.36 2.59 17 -5 9 25.33 2.47 -19 5 -9 3.56 0.93 19 -5 9 0.76 0.89 -21 5 -9 3.36 1.63 -23 5 -9 23.33 2.95 -25 5 -9 9.87 2.17 -27 5 -9 19.88 2.61 -30 -4 9 5.53 1.64 28 4 -9 2.47 1.16 28 4 -9 -0.92 2.07 -28 -4 9 2.28 0.74 -28 -4 9 0.04 2.04 -28 -4 9 3.71 1.12 26 4 -9 0.52 0.6 26 4 -9 -1.17 0.63 -26 -4 9 -1.57 0.82 -26 -4 9 0.76 0.74 -26 -4 9 0.29 0.56 24 4 -9 11.54 1.69 24 4 -9 10.54 1.63 24 4 -9 11.46 1.56 24 4 -9 13.18 1.34 -24 -4 9 11.83 1.54 -24 -4 9 13.16 1.73 -24 -4 9 15.08 1.75 22 4 -9 101.08 8.51 22 4 -9 78.33 8.37 22 4 -9 93.96 8.39 -22 -4 9 84.33 8.5 -22 -4 9 80.71 8.42 20 4 -9 41.18 4.06 -20 -4 9 38.14 4.16 -20 -4 9 40.52 3.97 -20 -4 9 38.11 4.1 18 4 -9 67.06 6.59 18 4 -9 65.89 6.58 -18 -4 9 70.8 6.59 -18 -4 9 69.77 6.67 16 4 -9 84.25 9.02 16 4 -9 91.67 9.01 -16 -4 9 100.25 9.04 -16 -4 9 103.82 9.1 14 4 -9 25.65 2.85 14 4 -9 27.93 2.88 -14 -4 9 30.51 2.98 -14 -4 9 33.32 2.92 -14 -4 9 29.83 2.89 12 4 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12.07 -6 -6 14 133.25 12.02 -6 -6 14 128.88 12.02 4 6 -14 111.39 9.71 4 6 -14 100.02 9.6 -4 -6 14 101.33 9.69 -4 -6 14 102.45 9.6 -4 -6 14 107.03 9.65 -4 -6 14 97.45 9.69 -4 -6 14 93.89 9.65 2 6 -14 22.71 2.12 2 6 -14 23.75 2.18 2 6 -14 20.67 2.05 -2 -6 14 19.78 2.14 -2 -6 14 18.86 2.08 -2 -6 14 21.95 2.13 -2 -6 14 21.47 2.19 -2 -6 14 20.99 2.23 -2 -6 14 22.05 2.1 0 6 -14 126.56 12.12 0 6 -14 121.78 12.08 0 -6 14 128.81 12.11 0 -6 14 130.65 12.16 0 -6 14 128.01 12.15 0 -6 14 127.99 12.09 0 -6 14 133.7 12.09 2 -6 14 11.68 1.5 2 -6 14 13.67 1.48 2 -6 14 13.5 1.61 2 -6 14 12 1.33 -4 6 -14 143.51 14.15 4 -6 14 157.49 14.24 -8 6 -14 0.47 0.7 8 -6 14 0.54 1.4 -10 6 -14 31.85 3.04 -10 6 -14 31.52 3.28 -10 6 -14 28.4 2.99 10 -6 14 33.05 3.22 10 -6 14 31.85 3.21 -12 6 -14 25.81 2.84 -12 6 -14 25.14 2.56 -12 6 -14 25.23 2.55 12 -6 14 27.95 2.81 12 -6 14 26.53 2.77 12 -6 14 26.16 2.77 -14 6 -14 16.3 2.01 -14 6 -14 16.12 1.64 14 -6 14 16.63 1.96 14 -6 14 14.66 1.98 -16 6 -14 6.61 1.4 16 -6 14 8.98 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27.29 2.59 -7 5 -14 27.22 3.06 7 -5 14 29.59 2.85 7 -5 14 23.1 2.9 -9 5 -14 68.52 6.31 -9 5 -14 61.72 6.09 9 -5 14 64.53 6.23 9 -5 14 62.63 6.21 -11 5 -14 -0.33 0.38 -11 5 -14 -0.41 0.29 -11 5 -14 -0.27 0.3 -11 5 -14 -0.47 0.72 11 -5 14 0.2 0.48 11 -5 14 -0.62 0.66 -13 5 -14 -0.04 0.28 -13 5 -14 -0.11 0.28 -13 5 -14 -0.11 0.77 -13 5 -14 0.23 0.38 13 -5 14 -0.32 0.55 13 -5 14 0.41 0.75 -15 5 -14 8.45 1.4 15 -5 14 3.22 1.97 15 -5 14 7.72 1.28 -17 5 -14 0.59 1.88 -19 5 -14 0.33 1.78 -21 5 -14 0.24 1.77 32 4 -14 7.82 1.7 -32 -4 14 3.7 1.75 -32 -4 14 4.5 1.2 30 4 -14 0.13 0.73 30 4 -14 0.79 0.47 -30 -4 14 0.22 0.92 -30 -4 14 0.38 0.7 28 4 -14 4.92 0.94 28 4 -14 7.18 1.46 -28 -4 14 4.23 1.07 -28 -4 14 4.85 0.96 26 4 -14 8.42 1.64 -26 -4 14 6.36 1.25 -26 -4 14 8.7 1.5 -24 -4 14 43.36 4.75 -24 -4 14 43.87 4.47 -22 -4 14 27.18 2.9 -22 -4 14 22.73 3.14 20 4 -14 8.7 1.68 -20 -4 14 13.73 1.74 -20 -4 14 12.65 1.85 18 4 -14 21.55 2.24 -18 -4 14 20.67 2.21 -18 -4 14 20.74 2.26 16 4 -14 1.25 0.5 16 4 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8.2 1.76 -13 -3 35 6.22 1.32 -13 -3 35 8.47 1.25 -13 -3 35 6.79 1.09 -13 -3 35 9.22 1.6 11 3 -35 -0.79 1.17 11 3 -35 0.34 1.68 -11 -3 35 6.8 2.02 -11 -3 35 11.5 2.2 -11 -3 35 0.67 0.89 9 3 -35 14.53 2.35 -9 -3 35 17.13 2.48 -9 -3 35 15.17 2.27 7 3 -35 1.83 2.53 -7 -3 35 5.73 1.62 -7 -3 35 6.01 1.65 5 3 -35 6.95 1.7 5 3 -35 8.21 2.55 -5 -3 35 4.62 1.67 24 2 -35 4.59 1.89 24 2 -35 3.77 1.71 -24 -2 35 1.36 1.96 -24 -2 35 2.59 1.98 22 2 -35 5.78 1.53 22 2 -35 4.65 1.72 -22 -2 35 5.09 1.85 -22 -2 35 4.9 1.81 20 2 -35 0.06 1.6 20 2 -35 0.21 1.29 -20 -2 35 1.77 1.66 -20 -2 35 0.44 0.99 18 2 -35 7.58 2.02 18 2 -35 0.33 1.97 -18 -2 35 1.8 1.35 -18 -2 35 1.74 1.42 16 2 -35 1.38 2.11 16 2 -35 6.2 2.21 -16 -2 35 2.8 0.95 -16 -2 35 1.65 1.53 -16 -2 35 1.31 0.98 14 2 -35 2.73 1.24 14 2 -35 2.75 1.02 -14 -2 35 1.99 1.68 -14 -2 35 2.95 0.99 -14 -2 35 2.48 1.01 -14 -2 35 2.9 0.87 12 2 -35 0.52 0.82 -12 -2 35 0.74 0.87 -12 -2 35 -2.45 1.3 -12 -2 35 1.58 0.79 -12 -2 35 1.15 0.9 -10 -2 35 -0.88 1.35 -10 -2 35 -1.73 1.13 -10 -2 35 -0.66 1.82 8 2 -35 10.6 2.35 -8 -2 35 3.1 1.14 -8 -2 35 4.41 1.46 6 2 -35 7.87 2.35 6 2 -35 3.81 1.65 -6 -2 35 10.39 1.83 4 2 -35 31.48 3.65 4 2 -35 30.85 4.2 -4 -2 35 37.88 3.95 23 1 -35 8.72 1.92 23 1 -35 11.32 2.43 -23 -1 35 10.41 2.24 -23 -1 35 9.69 2.15 21 1 -35 2.52 1.53 21 1 -35 1.99 1.09 -21 -1 35 -0.34 1.35 19 1 -35 1.68 1.78 -19 -1 35 2.69 1.46 -19 -1 35 5.74 1.87 17 1 -35 14.28 2.59 -17 -1 35 18.08 2.2 -17 -1 35 10.98 2.1 -17 -1 35 15.42 2.09 -17 -1 35 13.34 2.19 15 1 -35 20.93 2.63 15 1 -35 23.53 3.24 -15 -1 35 22.7 2.69 -15 -1 35 20.49 2.62 -15 -1 35 20.09 2.34 13 1 -35 9.87 2.16 -13 -1 35 7.66 1.24 -13 -1 35 5.8 1.25 -13 -1 35 6.17 1.3 11 1 -35 18.03 2.86 11 1 -35 22.25 2.7 -11 -1 35 18.99 2.86 -11 -1 35 12.29 2.29 -11 -1 35 17.4 2.26 -11 -1 35 18.95 2.18 9 1 -35 3.62 2.01 9 1 -35 2.28 1.63 -9 -1 35 0.03 1.23 7 1 -35 0.44 1.88 7 1 -35 3.16 1.49 -7 -1 35 0.89 0.93 5 1 -35 17.76 3.05 -5 -1 35 19.99 2.27 3 1 -35 21.33 3.52 -3 -1 35 17.75 2.46 -3 -1 35 26.51 3.06 24 0 -35 1.04 1.05 -24 0 35 1.28 2.11 -24 0 35 0.82 1.9 22 0 -35 -0.62 1.73 22 0 -35 -1.5 2.24 -22 0 35 -0.48 2.01 -22 0 35 0.83 1.7 20 0 -35 0.54 0.99 20 0 -35 2.61 1.85 -20 0 35 0.55 1.76 18 0 -35 3.05 2.07 18 0 -35 -0.33 0.92 -18 0 35 2.29 1.55 -18 0 35 0.8 1.92 -18 0 35 1.31 0.98 16 0 -35 0.38 1.08 16 0 -35 -1.02 0.89 -16 0 35 1.62 1.02 -16 0 35 0.35 0.79 -16 0 35 3.86 1.76 -16 0 35 -0.43 0.64 14 0 -35 1.1 0.92 14 0 -35 0.8 1.14 -14 0 35 0.34 0.79 -14 0 35 0.75 0.99 -14 0 35 0.08 0.79 12 0 -35 -2.02 1.86 12 0 -35 -1.59 2.39 -12 0 35 -0.05 0.79 -12 0 35 -0.34 0.74 -12 0 35 1.27 2.22 10 0 -35 -0.28 2.24 10 0 -35 -0.22 1.77 -10 0 35 0.96 2.13 -10 0 35 0.86 1.84 8 0 -35 -0.24 1.52 6 0 -35 0.56 1.57 4 0 -35 0.75 2.67 -4 0 35 -2.03 1.35 19 -1 -35 0.48 0.98 -19 1 35 2.16 1.69 -19 1 35 3.21 2.19 17 -1 -35 13.19 2.21 17 -1 -35 18.41 2.25 -17 1 35 19.69 3.01 -17 1 35 15.56 2.18 -17 1 35 15.2 1.91 15 -1 -35 20.79 2.59 15 -1 -35 22.79 2.61 -15 1 35 17.44 2.57 -15 1 35 19.53 2.3 -15 1 35 20.42 2.57 -15 1 35 20.43 2.27 13 -1 -35 9.8 1.61 13 -1 -35 8.79 1.72 -13 1 35 10.2 2.07 -13 1 35 5.5 1.3 -13 1 35 7.02 1.43 11 -1 -35 17.74 2.49 -11 1 35 16.37 2.45 -11 1 35 19.91 2.92 9 -1 -35 5.61 1.6 7 -1 -35 2.11 3.21 5 -1 -35 17.25 3.28 3 -1 -35 20.46 2.66 3 -1 -35 19.49 2.82 -3 1 35 23 2.58 -3 1 35 18.55 2.56 -24 2 35 -0.23 1.93 -24 2 35 -0.46 2.24 -22 2 35 5.79 2.03 -22 2 35 8.51 2.12 20 -2 -35 3.12 1.84 -20 2 35 -0.43 1.62 18 -2 -35 5.41 2.05 -18 2 35 2.27 0.91 -18 2 35 -0.27 0.87 -18 2 35 6.13 1.63 16 -2 -35 3.87 1.27 -16 2 35 2.41 0.98 -16 2 35 4.35 1.16 -16 2 35 3.41 0.96 -16 2 35 2.55 0.91 14 -2 -35 3.13 1.05 14 -2 -35 2.12 2.36 -14 2 35 1.34 0.79 -14 2 35 3.57 1.11 -14 2 35 2.49 0.88 -14 2 35 3.81 0.98 12 -2 -35 0.53 2.3 -12 2 35 0.3 1.74 -12 2 35 2 0.92 -12 2 35 2.61 1.04 10 -2 -35 0.41 2.31 -10 2 35 0.62 1.49 8 -2 -35 5.95 2.36 -8 2 35 4.37 1.49 6 -2 -35 12.23 2.79 4 -2 -35 38.78 4.59 -4 2 35 34.09 3.83 -4 2 35 32.07 4.22 -23 3 35 0.57 1.61 -23 3 35 -0.4 1.81 -23 3 35 0.11 1.79 -21 3 35 0.51 1.63 19 -3 -35 9.19 2.06 -19 3 35 4.39 1.14 17 -3 -35 7.16 2.19 -17 3 35 3.28 1.05 -17 3 35 1.84 2.45 -15 3 35 0.81 1.03 -15 3 35 0.33 0.72 -15 3 35 1.05 0.9 -15 3 35 0.86 0.88 13 -3 -35 7.94 2.36 -13 3 35 7.08 1.26 -13 3 35 6.35 1.38 -13 3 35 6.45 1.24 -13 3 35 9.62 1.68 11 -3 -35 -0.52 2.2 -11 3 35 -0.06 1.67 -11 3 35 3.06 2.15 -11 3 35 2.61 1.92 9 -3 -35 10.7 2.09 -9 3 35 6.46 1.81 -9 3 35 10.94 2.26 7 -3 -35 2.08 1.69 -7 3 35 1.83 1.13 -7 3 35 3.78 1.59 5 -3 -35 3.79 2.41 -5 3 35 2.95 2.15 -5 3 35 0.9 1.55 -18 4 35 -0.76 0.79 16 -4 -35 7.98 2.28 -16 4 35 2.6 1.14 -16 4 35 2.93 0.97 -16 4 35 3.43 1 -16 4 35 2.45 0.99 14 -4 -35 17.41 2.69 -14 4 35 12.03 1.73 -14 4 35 12.13 2.01 -14 4 35 14.34 2.1 -14 4 35 11.73 1.79 12 -4 -35 8.5 2.3 -12 4 35 7.27 2.41 -12 4 35 9.02 2.13 -12 4 35 8.96 2.49 10 -4 -35 0.53 2.02 -10 4 35 0.29 1.7 -10 4 35 0.32 2.09 8 -4 -35 0.19 2.02 -8 4 35 -0.86 1.78 6 -4 -35 1.46 2.22 6 -4 -35 0.11 1.54 -6 4 35 -0.33 1.98 -6 4 35 -0.29 1.24 19 -5 -35 15.29 1.99 -19 5 35 11.64 2.19 17 -5 -35 3.21 1.17 -17 5 35 0.2 0.85 -17 5 35 -0.83 0.98 -17 5 35 1.15 0.88 15 -5 -35 14.33 2.23 -15 5 35 14.41 1.96 -15 5 35 15.67 2.18 -15 5 35 17.14 2.25 -15 5 35 13.27 1.92 13 -5 -35 22.18 3.25 -13 5 35 17.43 2.43 -13 5 35 17.74 2.12 -13 5 35 15.97 2.16 -13 5 35 16.72 2.37 11 -5 -35 17.49 3.08 -11 5 35 17.05 2.86 -11 5 35 14.69 2.1 -11 5 35 18.27 2.78 9 -5 -35 12.94 2.89 7 -5 -35 0.71 2.45 18 -6 -35 1.02 1.06 16 -6 -35 0.84 1.03 -16 6 35 1.65 1.1 -16 6 35 0.49 0.91 -16 6 35 0.93 0.87 14 -6 -35 -0.11 1.16 -14 6 35 -0.05 1 -14 6 35 -0.4 0.89 -14 6 35 0.79 0.98 -14 6 35 0.76 0.91 12 -6 -35 4.34 1.44 -12 6 35 2.19 0.94 -12 6 35 4.66 2.31 -12 6 35 4.27 2.31 -12 6 35 4.87 1.11 10 -6 -35 16.58 3.09 18 4 -36 -1.29 1.07 18 4 -36 2.11 2.13 -18 -4 36 -0.57 2.13 16 4 -36 0.78 1.21 16 4 -36 1.22 0.99 -16 -4 36 0.7 0.86 -16 -4 36 -0.32 0.9 -16 -4 36 0.14 0.95 14 4 -36 3.22 1.34 14 4 -36 3.93 1.11 -14 -4 36 4.46 1.12 -14 -4 36 5.26 1.19 -14 -4 36 5.94 1.21 12 4 -36 4.46 2.01 12 4 -36 1.64 1.29 -12 -4 36 2.76 1.12 -12 -4 36 3.52 1 -12 -4 36 3.89 1.07 10 4 -36 3.07 1.33 10 4 -36 2.25 1.95 -10 -4 36 -0.87 1.57 -10 -4 36 1.8 0.92 -10 -4 36 0.46 0.87 19 3 -36 -0.01 2.11 19 3 -36 -0.94 1.95 -19 -3 36 4.39 2.13 -19 -3 36 2.44 2.07 17 3 -36 8.13 2.3 17 3 -36 10.47 1.8 -17 -3 36 5.24 1.33 -17 -3 36 11.79 2.55 15 3 -36 3.93 1.18 15 3 -36 8.7 1.72 -15 -3 36 6.65 1.32 -15 -3 36 6.01 1.23 -15 -3 36 2.79 1.16 13 3 -36 2.62 1.3 13 3 -36 -1.38 1.7 -13 -3 36 3.93 1.02 -13 -3 36 3.21 1.03 -13 -3 36 2.98 1.04 11 3 -36 0.05 1.17 11 3 -36 -0.85 1.75 -11 -3 36 -0.07 1.94 -11 -3 36 0.21 0.88 -11 -3 36 -1.9 1.99 9 3 -36 1.84 1.32 -9 -3 36 -0.67 0.82 -9 -3 36 1.16 0.98 -9 -3 36 0.74 0.66 -9 -3 36 2 0.94 20 2 -36 0.24 1.71 20 2 -36 1.28 1.84 -20 -2 36 -0.74 1.26 -20 -2 36 -0.85 0.99 18 2 -36 2.84 2.15 18 2 -36 1.62 1.97 -18 -2 36 0.36 1.42 -18 -2 36 0.54 1.32 16 2 -36 1.17 0.92 16 2 -36 1.32 2.21 -16 -2 36 0.45 0.85 -16 -2 36 2.74 1.59 -16 -2 36 2.73 1.07 14 2 -36 9.62 1.77 14 2 -36 8.44 1.63 -14 -2 36 6.6 1.19 -14 -2 36 6.95 1.37 -14 -2 36 5.67 1.28 12 2 -36 8.73 2.24 -12 -2 36 6.05 1.49 -12 -2 36 4.69 1.19 -12 -2 36 6.11 2.24 -10 -2 36 -0.41 1.31 8 2 -36 11.93 2.58 8 2 -36 10.85 1.96 21 1 -36 0.9 1.48 21 1 -36 1.62 1.62 -21 -1 36 1.89 1.61 19 1 -36 3.81 1.89 -19 -1 36 1.66 1.85 -19 -1 36 0.59 1.46 17 1 -36 -1.96 2.06 17 1 -36 0.92 1.01 -17 -1 36 -0.07 1.67 -17 -1 36 -0.14 0.79 -17 -1 36 -0.27 0.91 15 1 -36 3.22 1.24 15 1 -36 2.14 1.05 -15 -1 36 2.54 0.83 -15 -1 36 3.04 1.01 -15 -1 36 5.21 1.12 13 1 -36 3.88 1.95 -13 -1 36 1.56 0.78 -13 -1 36 1.21 0.92 -13 -1 36 2.71 1.01 11 1 -36 10.58 2.21 11 1 -36 13.47 2.49 -11 -1 36 13.11 2.43 -11 -1 36 7.69 1.8 -11 -1 36 8.04 1.86 9 1 -36 9.04 1.97 9 1 -36 7.6 2.33 7 1 -36 3.39 1.99 -7 -1 36 0.08 1.08 22 0 -36 4.41 1.91 22 0 -36 1.98 1.57 -22 0 36 2.34 1.76 -22 0 36 5.38 2.31 20 0 -36 55.89 5.62 20 0 -36 58.35 5.86 -20 0 36 51.06 5.7 -20 0 36 47.6 5.39 -20 0 36 51.23 5.77 18 0 -36 43.85 4.65 18 0 -36 50.77 4.75 -18 0 36 44.96 4.72 -18 0 36 41.9 5.02 -18 0 36 40.07 4.42 16 0 -36 18.12 2.38 16 0 -36 21.68 2.42 -16 0 36 15.92 2.07 -16 0 36 17.43 2.39 -16 0 36 13.77 2.32 14 0 -36 19.14 3.05 14 0 -36 18.51 2.31 -14 0 36 16.08 2.03 -14 0 36 16.19 2.31 -14 0 36 16.07 2.35 12 0 -36 13.99 2.63 12 0 -36 17.93 3 -12 0 36 16.79 2.81 -12 0 36 18.73 2.95 -12 0 36 16.62 1.95 10 0 -36 0.87 2.23 8 0 -36 0.52 1.52 6 0 -36 3.38 2.47 21 -1 -36 -0.18 1 -21 1 36 3.44 2.08 19 -1 -36 0.48 1.07 -19 1 36 -0.14 2.36 17 -1 -36 0.02 0.93 17 -1 -36 -0.38 1.09 -17 1 36 0.36 0.94 -17 1 36 -0.7 0.77 -17 1 36 -1.1 0.76 15 -1 -36 3.78 1.13 15 -1 -36 3.56 1.33 -15 1 36 2.22 0.99 -15 1 36 4.93 1.03 -15 1 36 4.48 1.18 13 -1 -36 1.75 1.23 -13 1 36 1 0.96 -13 1 36 0.66 0.85 -13 1 36 -0.23 0.81 11 -1 -36 12.43 2.12 -11 1 36 11.62 2.03 9 -1 -36 17.28 3.07 7 -1 -36 5.53 1.57 20 -2 -36 1.11 2.04 -20 2 36 0.41 1.6 18 -2 -36 1.69 1.13 -18 2 36 2.55 1.09 -18 2 36 0.37 0.86 -18 2 36 6.18 1.26 -18 2 36 0.77 0.86 16 -2 -36 3.48 1.1 16 -2 -36 3.61 1.25 -16 2 36 2.18 0.94 -16 2 36 1.12 0.93 -16 2 36 1.06 0.84 -16 2 36 1.34 1.06 14 -2 -36 9.87 1.65 14 -2 -36 12.02 2.56 -14 2 36 6.99 1.42 -14 2 36 8.07 1.41 -14 2 36 8.61 1.56 12 -2 -36 5.48 2.47 -12 2 36 4.8 1.18 -12 2 36 8.56 2.29 -12 2 36 1.97 1.78 10 -2 -36 0.85 2.37 -10 2 36 0.57 1.48 8 -2 -36 12.87 2.66 -8 2 36 8.29 1.73 19 -3 -36 0.23 2.03 -19 3 36 1.11 1.18 17 -3 -36 8.48 2.35 -17 3 36 7.16 1.99 -17 3 36 7.5 1.47 -17 3 36 6.97 1.37 15 -3 -36 6.74 2.38 -15 3 36 6.06 1.23 -15 3 36 6.55 1.2 -15 3 36 5.61 1.19 -15 3 36 4.69 1.3 13 -3 -36 2.26 2.23 -13 3 36 3.08 1.9 -13 3 36 6.07 2.34 -13 3 36 2.76 1.04 11 -3 -36 0.01 1.98 -11 3 36 0.82 1.56 -11 3 36 0.79 2 -11 3 36 -1.26 1.86 9 -3 -36 2.07 1.7 -9 3 36 0.47 1.35 -9 3 36 2.88 1.79 -18 4 36 -0.7 0.79 -18 4 36 1.04 1.06 16 -4 -36 2.5 2.11 -16 4 36 1.93 0.93 -16 4 36 0.85 0.86 -16 4 36 1.95 1.11 -16 4 36 2.12 0.9 14 -4 -36 6.19 2.36 -14 4 36 4.79 1.21 -14 4 36 4.7 1.25 -14 4 36 4.75 1.17 -14 4 36 3.02 1.12 12 -4 -36 5.19 2.07 -12 4 36 2.9 1.95 -12 4 36 4.88 2.19 -12 4 36 3.9 2.32 10 -4 -36 2.05 2.05 -10 4 36 1.07 1.62 -10 4 36 0.6 1.9 -14 -2 37 0.84 0.75 15 1 -37 1.58 1.21 15 1 -37 1.61 0.96 -15 -1 37 0.45 0.94 -15 -1 37 -0.79 1.78 -15 -1 37 0.95 0.89 13 1 -37 8.04 1.53 -13 -1 37 5.2 1.23 -13 -1 37 6.09 1.32 -13 -1 37 5.37 1.04 16 0 -37 0.85 1.19 16 0 -37 -0.11 0.95 -16 0 37 0.06 0.83 -16 0 37 0.27 0.97 -16 0 37 0.54 0.79 14 0 -37 0.88 2.06 14 0 -37 0.67 2.39 -14 0 37 -0.51 0.78 -14 0 37 2.04 2.35 -14 0 37 -0.07 0.75 12 0 -37 0.82 2.34 -12 0 37 -0.82 0.69 -12 0 37 1.01 2.29 -12 0 37 1.75 2.04 15 -1 -37 2.6 1.26 15 -1 -37 1.76 1.01 -15 1 37 1.25 0.93 -15 1 37 0.15 0.98 -15 1 37 -1.29 0.75 13 -1 -37 6.81 1.57 -13 1 37 4.97 1.05 -13 1 37 4.27 1.15 -13 1 37 6.01 1.33 ; ; loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 3.00 -1.00 0.00 0.1290 -3.00 1.00 0.00 0.1150 0.00 -1.00 3.00 0.1430 1.00 0.00 -2.00 0.1090 0.00 0.00 -1.00 0.0760 2.00 -1.00 -1.00 0.1560 0.00 0.00 1.00 0.1340 2.00 0.00 3.00 0.1450 2.00 -2.00 -1.00 0.1700 0.00 -1.00 -1.00 0.1470 -2.00 -3.00 -3.00 0.1480 0.00 -3.00 -2.00 0.1570 -3.00 -1.00 -2.00 0.1290 -1.00 0.00 0.00 0.0810 1.00 0.00 0.00 0.1230 -3.00 0.00 2.00 0.0700 -1.00 2.00 -3.00 0.1130 3.00 2.00 0.00 0.0500 3.00 0.00 -1.00 0.0940 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Cu1 C70 168.14(14) . . ? C1 N1 C2 111.2(3) . . ? C1 N1 C4 125.9(3) . . ? C2 N1 C4 122.8(3) . . ? C1 N2 C3 111.6(3) . . ? C1 N2 C37 127.8(3) . . ? C3 N2 C37 120.6(3) . . ? N1 C1 Cu1 122.5(2) . . ? N2 C1 Cu1 133.4(2) . . ? N2 C1 N1 103.8(3) . . ? N1 C2 H2 126.7 . . ? C3 C2 N1 106.5(3) . . ? C3 C2 H2 126.7 . . ? N2 C3 H3 126.6 . . ? C2 C3 N2 106.8(3) . . ? C2 C3 H3 126.6 . . ? C5 C4 N1 118.5(3) . . ? C5 C4 C9 121.9(3) . . ? C9 C4 N1 119.5(3) . . ? C4 C5 C10 120.5(3) . . ? C6 C5 C4 118.3(3) . . ? C6 C5 C10 121.2(3) . . ? C5 C6 H6 119.3 . . ? C5 C6 C7 121.5(3) . . ? C7 C6 H6 119.3 . . ? C6 C7 C23 120.8(3) . . ? C8 C7 C6 118.6(3) . . ? C8 C7 C23 120.6(3) . . ? C7 C8 H8 118.9 . . ? C7 C8 C9 122.2(3) . . ? C9 C8 H8 118.9 . . ? C4 C9 C24 121.9(3) . . ? C8 C9 C4 117.4(3) . . ? C8 C9 C24 120.7(3) . . ? C5 C10 H10 106.5 . . ? C5 C10 C17 114.0(3) . . ? C11 C10 C5 110.5(3) . . ? C11 C10 H10 106.5 . . ? C11 C10 C17 112.4(3) . . ? C17 C10 H10 106.5 . . ? C12 C11 C10 118.6(3) . . ? C12 C11 C16 119.3(3) . . ? C16 C11 C10 122.1(3) . . ? C11 C12 H12 120.1 . . ? C11 C12 C13 119.9(4) . . ? C13 C12 H12 120.1 . . ? C12 C13 H13 119.8 . . ? C14 C13 C12 120.4(4) . . ? C14 C13 H13 119.8 . . ? C13 C14 H14 120.0 . . ? C13 C14 C15 119.9(4) . . ? C15 C14 H14 120.0 . . ? C14 C15 H15 119.8 . . ? C14 C15 C16 120.3(4) . . ? C16 C15 H15 119.8 . . ? C11 C16 H16 119.9 . . ? C15 C16 C11 120.2(4) . . ? C15 C16 H16 119.9 . . ? C18 C17 C10 118.4(3) . . ? C22 C17 C10 123.1(3) . . ? C22 C17 C18 118.5(3) . . ? C17 C18 H18 119.4 . . ? C19 C18 C17 121.2(4) . . ? C19 C18 H18 119.4 . . ? C18 C19 H19 120.0 . . ? C20 C19 C18 120.0(4) . . ? C20 C19 H19 120.0 . . ? C19 C20 H20 120.1 . . ? C19 C20 C21 119.8(4) . . ? C21 C20 H20 120.1 . . ? C20 C21 H21 119.9 . . ? C20 C21 C22 120.2(4) . . ? C22 C21 H21 119.9 . . ? C17 C22 C21 120.5(4) . . ? C17 C22 H22 119.8 . . ? C21 C22 H22 119.8 . . ? C7 C23 H23A 109.5 . . ? C7 C23 H23B 109.5 . . ? C7 C23 H23C 109.5 . . ? H23A C23 H23B 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C9 C24 H24 106.9 . . ? C9 C24 C25 110.3(3) . . ? C9 C24 C31 112.8(3) . . ? C25 C24 H24 106.9 . . ? C31 C24 H24 106.9 . . ? C31 C24 C25 112.6(3) . . ? C26 C25 C24 119.8(3) . . ? C30 C25 C24 122.3(3) . . ? C30 C25 C26 117.9(4) . . ? C25 C26 H26 119.5 . . ? C27 C26 C25 121.0(4) . . ? C27 C26 H26 119.5 . . ? C26 C27 H27 119.7 . . ? C28 C27 C26 120.6(4) . . ? C28 C27 H27 119.7 . . ? C27 C28 H28 120.5 . . ? C29 C28 C27 119.0(5) . . ? C29 C28 H28 120.5 . . ? C28 C29 H29 119.8 . . ? C28 C29 C30 120.5(5) . . ? C30 C29 H29 119.8 . . ? C25 C30 C29 121.0(4) . . ? C25 C30 H30 119.5 . . ? C29 C30 H30 119.5 . . ? C32 C31 C24 123.3(3) . . ? C32 C31 C36 118.1(4) . . ? C36 C31 C24 118.6(3) . . ? C31 C32 H32 119.6 . . ? C31 C32 C33 120.7(4) . . ? C33 C32 H32 119.6 . . ? C32 C33 H33 120.0 . . ? C34 C33 C32 120.0(4) . . ? C34 C33 H33 120.0 . . ? C33 C34 H34 120.0 . . ? C35 C34 C33 120.0(4) . . ? C35 C34 H34 120.0 . . ? C34 C35 H35 120.1 . . ? C34 C35 C36 119.8(4) . . ? C36 C35 H35 120.1 . . ? C31 C36 H36 119.3 . . ? C35 C36 C31 121.3(4) . . ? C35 C36 H36 119.3 . . ? C38 C37 N2 119.1(3) . . ? C42 C37 N2 118.2(3) . . ? C42 C37 C38 122.2(3) . . ? C37 C38 C43 120.9(3) . . ? C39 C38 C37 117.8(3) . . ? C39 C38 C43 121.2(3) . . ? C38 C39 H39 119.1 . . ? C38 C39 C40 121.8(3) . . ? C40 C39 H39 119.1 . . ? C39 C40 C56 121.4(3) . . ? C41 C40 C39 118.4(3) . . ? C41 C40 C56 120.3(3) . . ? C40 C41 H41 119.1 . . ? C40 C41 C42 121.8(3) . . ? C42 C41 H41 119.1 . . ? C37 C42 C41 117.6(3) . . ? C37 C42 C57 121.3(3) . . ? C41 C42 C57 121.1(3) . . ? C38 C43 H43 106.2 . . ? C38 C43 C44 113.1(3) . . ? C38 C43 C50 110.9(3) . . ? C44 C43 H43 106.2 . . ? C50 C43 H43 106.2 . . ? C50 C43 C44 113.7(3) . . ? C45 C44 C43 118.2(3) . . ? C45 C44 C49 117.7(3) . . ? C49 C44 C43 124.0(3) . . ? C44 C45 H45 119.3 . . ? C44 C45 C46 121.3(4) . . ? C46 C45 H45 119.3 . . ? C45 C46 H46 119.9 . . ? C47 C46 C45 120.1(4) . . ? C47 C46 H46 119.9 . . ? C46 C47 H47 120.4 . . ? C48 C47 C46 119.2(4) . . ? C48 C47 H47 120.4 . . ? C47 C48 H48 119.9 . . ? C47 C48 C49 120.3(4) . . ? C49 C48 H48 119.9 . . ? C44 C49 H49 119.4 . . ? C48 C49 C44 121.3(4) . . ? C48 C49 H49 119.3 . . ? C51 C50 C43 119.3(3) . . ? C51 C50 C55 117.8(3) . . ? C55 C50 C43 122.9(3) . . ? C50 C51 H51 119.2 . . ? C50 C51 C52 121.6(4) . . ? C52 C51 H51 119.2 . . ? C51 C52 H52 119.9 . . ? C53 C52 C51 120.2(4) . . ? C53 C52 H52 119.9 . . ? C52 C53 H53 120.6 . . ? C54 C53 C52 118.8(4) . . ? C54 C53 H53 120.6 . . ? C53 C54 H54 119.6 . . ? C53 C54 C55 120.9(4) . . ? C55 C54 H54 119.6 . . ? C50 C55 H55 119.7 . . ? C54 C55 C50 120.7(4) . . ? C54 C55 H55 119.7 . . ? C40 C56 H56A 109.5 . . ? C40 C56 H56B 109.5 . . ? C40 C56 H56C 109.5 . . ? H56A C56 H56B 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? C42 C57 H57 106.5 . . ? C42 C57 C58 111.5(3) . . ? C42 C57 C64 113.3(3) . . ? C58 C57 H57 106.5 . . ? C64 C57 H57 106.5 . . ? C64 C57 C58 112.0(3) . . ? C59 C58 C57 119.0(3) . . ? C59 C58 C63 119.2(3) . . ? C63 C58 C57 121.8(3) . . ? C58 C59 H59 119.8 . . ? C58 C59 C60 120.4(4) . . ? C60 C59 H59 119.8 . . ? C59 C60 H60 120.0 . . ? C61 C60 C59 120.0(4) . . ? C61 C60 H60 120.0 . . ? C60 C61 H61 119.9 . . ? C62 C61 C60 120.1(4) . . ? C62 C61 H61 119.9 . . ? C61 C62 H62 120.0 . . ? C61 C62 C63 120.0(4) . . ? C63 C62 H62 120.0 . . ? C58 C63 H63 119.9 . . ? C62 C63 C58 120.2(4) . . ? C62 C63 H63 119.9 . . ? C65 C64 C57 117.6(3) . . ? C69 C64 C57 124.0(3) . . ? C69 C64 C65 118.5(4) . . ? C64 C65 H65 119.7 . . ? C66 C65 C64 120.6(4) . . ? C66 C65 H65 119.7 . . ? C65 C66 H66 119.7 . . ? C65 C66 C67 120.6(4) . . ? C67 C66 H66 119.7 . . ? C66 C67 H67 120.3 . . ? C66 C67 C68 119.4(4) . . ? C68 C67 H67 120.3 . . ? C67 C68 H68 120.0 . . ? C67 C68 C69 119.9(4) . . ? C69 C68 H68 120.0 . . ? C64 C69 C68 120.9(4) . . ? C64 C69 H69 119.5 . . ? C68 C69 H69 119.5 . . ? C71 C70 Cu1 113.7(3) . . ? C77 C70 Cu1 125.2(3) . . ? C77 C70 C71 121.0(3) . . ? C72 C71 C70 121.5(3) . . ? C72 C71 C76 117.5(4) . . ? C76 C71 C70 120.9(4) . . ? C71 C72 H72 119.4 . . ? C71 C72 C73 121.1(4) . . ? C73 C72 H72 119.4 . . ? C72 C73 H73 119.8 . . ? C74 C73 C72 120.4(4) . . ? C74 C73 H73 119.8 . . ? C73 C74 H74 120.4 . . ? C75 C74 C73 119.2(4) . . ? C75 C74 H74 120.4 . . ? C74 C75 H75 119.8 . . ? C74 C75 C76 120.4(4) . . ? C76 C75 H75 119.8 . . ? C71 C76 H76 119.4 . . ? C75 C76 C71 121.2(4) . . ? C75 C76 H76 119.4 . . ? C70 C77 H77 115.5 . . ? C70 C77 C78 129.0(4) . . ? C78 C77 H77 115.5 . . ? C79 C78 C77 122.6(3) . . ? C79 C78 C83 117.5(3) . . ? C83 C78 C77 119.7(4) . . ? C78 C79 H79 119.6 . . ? C78 C79 C80 120.9(4) . . ? C80 C79 H79 119.6 . . ? C79 C80 H80 119.6 . . ? C81 C80 C79 120.8(4) . . ? C81 C80 H80 119.6 . . ? C80 C81 H81 120.5 . . ? C80 C81 C82 119.0(4) . . ? C82 C81 H81 120.5 . . ? C81 C82 H82 119.7 . . ? C81 C82 C83 120.6(4) . . ? C83 C82 H82 119.7 . . ? C78 C83 H83 119.4 . . ? C82 C83 C78 121.2(4) . . ? C82 C83 H83 119.4 . . ? C84 O1 C87 101.6(6) . . ? O1 C84 H84A 109.8 . . ? O1 C84 H84B 109.8 . . ? O1 C84 C85 109.4(6) . . ? H84A C84 H84B 108.2 . . ? C85 C84 H84A 109.8 . . ? C85 C84 H84B 109.8 . . ? C84 C85 H85A 110.8 . . ? C84 C85 H85B 110.8 . . ? C84 C85 C86 104.6(5) . . ? H85A C85 H85B 108.9 . . ? C86 C85 H85A 110.8 . . ? C86 C85 H85B 110.8 . . ? C85 C86 H86A 111.3 . . ? C85 C86 H86B 111.3 . . ? C85 C86 C87 102.2(6) . . ? H86A C86 H86B 109.2 . . ? C87 C86 H86A 111.3 . . ? C87 C86 H86B 111.3 . . ? O1 C87 C86 106.8(6) . . ? O1 C87 H87A 110.4 . . ? O1 C87 H87B 110.4 . . ? C86 C87 H87A 110.4 . . ? C86 C87 H87B 110.4 . . ? H87A C87 H87B 108.6 . . ? C91 O2 C88 109.9(6) . . ? O2 C88 H88A 110.3 . . ? O2 C88 H88B 110.3 . . ? O2 C88 C89 107.0(6) . . ? H88A C88 H88B 108.6 . . ? C89 C88 H88A 110.3 . . ? C89 C88 H88B 110.3 . . ? C88 C89 H89A 110.2 . . ? C88 C89 H89B 110.2 . . ? H89A C89 H89B 108.5 . . ? C90 C89 C88 107.5(7) . . ? C90 C89 H89A 110.2 . . ? C90 C89 H89B 110.2 . . ? C89 C90 H90A 110.7 . . ? C89 C90 H90B 110.7 . . ? C89 C90 C91 105.4(7) . . ? H90A C90 H90B 108.8 . . ? C91 C90 H90A 110.7 . . ? C91 C90 H90B 110.7 . . ? O2 C91 C90 105.3(7) . . ? O2 C91 H91A 110.7 . . ? O2 C91 H91B 110.7 . . ? C90 C91 H91A 110.7 . . ? C90 C91 H91B 110.7 . . ? H91A C91 H91B 108.8 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 C1 1.910(3) . ? Cu1 C70 1.919(4) . ? N1 C1 1.358(4) . ? N1 C2 1.391(4) . ? N1 C4 1.441(4) . ? N2 C1 1.355(4) . ? N2 C3 1.380(4) . ? N2 C37 1.443(4) . ? C2 H2 0.9300 . ? C2 C3 1.340(5) . ? C3 H3 0.9300 . ? C4 C5 1.401(4) . ? C4 C9 1.402(4) . ? C5 C6 1.389(5) . ? C5 C10 1.526(4) . ? C6 H6 0.9300 . ? C6 C7 1.395(5) . ? C7 C8 1.393(5) . ? C7 C23 1.508(5) . ? C8 H8 0.9300 . ? C8 C9 1.394(5) . ? C9 C24 1.524(4) . ? C10 H10 0.9800 . ? C10 C11 1.524(5) . ? C10 C17 1.530(5) . ? C11 C12 1.393(5) . ? C11 C16 1.394(5) . ? C12 H12 0.9300 . ? C12 C13 1.393(6) . ? C13 H13 0.9300 . ? C13 C14 1.376(7) . ? C14 H14 0.9300 . ? C14 C15 1.382(7) . ? C15 H15 0.9300 . ? C15 C16 1.386(6) . ? C16 H16 0.9300 . ? C17 C18 1.395(5) . ? C17 C22 1.391(5) . ? C18 H18 0.9300 . ? C18 C19 1.384(6) . ? C19 H19 0.9300 . ? C19 C20 1.383(7) . ? C20 H20 0.9300 . ? C20 C21 1.386(7) . ? C21 H21 0.9300 . ? C21 C22 1.395(6) . ? C22 H22 0.9300 . ? C23 H23A 0.9600 . ? C23 H23B 0.9600 . ? C23 H23C 0.9600 . ? C24 H24 0.9800 . ? C24 C25 1.535(5) . ? C24 C31 1.528(5) . ? C25 C26 1.394(5) . ? C25 C30 1.391(5) . ? C26 H26 0.9300 . ? C26 C27 1.389(7) . ? C27 H27 0.9300 . ? C27 C28 1.386(8) . ? C28 H28 0.9300 . ? C28 C29 1.381(8) . ? C29 H29 0.9300 . ? C29 C30 1.396(6) . ? C30 H30 0.9300 . ? C31 C32 1.387(6) . ? C31 C36 1.394(5) . ? C32 H32 0.9300 . ? C32 C33 1.395(6) . ? C33 H33 0.9300 . ? C33 C34 1.383(7) . ? C34 H34 0.9300 . ? C34 C35 1.377(7) . ? C35 H35 0.9300 . ? C35 C36 1.386(6) . ? C36 H36 0.9300 . ? C37 C38 1.402(4) . ? C37 C42 1.396(4) . ? C38 C39 1.390(5) . ? C38 C43 1.526(4) . ? C39 H39 0.9300 . ? C39 C40 1.395(5) . ? C40 C41 1.395(4) . ? C40 C56 1.507(5) . ? C41 H41 0.9300 . ? C41 C42 1.398(5) . ? C42 C57 1.518(4) . ? C43 H43 0.9800 . ? C43 C44 1.530(4) . ? C43 C50 1.528(5) . ? C44 C45 1.391(5) . ? C44 C49 1.393(5) . ? C45 H45 0.9300 . ? C45 C46 1.394(5) . ? C46 H46 0.9300 . ? C46 C47 1.390(6) . ? C47 H47 0.9300 . ? C47 C48 1.385(6) . ? C48 H48 0.9300 . ? C48 C49 1.393(5) . ? C49 H49 0.9300 . ? C50 C51 1.386(5) . ? C50 C55 1.398(5) . ? C51 H51 0.9300 . ? C51 C52 1.392(5) . ? C52 H52 0.9300 . ? C52 C53 1.386(7) . ? C53 H53 0.9300 . ? C53 C54 1.385(7) . ? C54 H54 0.9300 . ? C54 C55 1.390(6) . ? C55 H55 0.9300 . ? C56 H56A 0.9600 . ? C56 H56B 0.9600 . ? C56 H56C 0.9600 . ? C57 H57 0.9800 . ? C57 C58 1.524(5) . ? C57 C64 1.523(5) . ? C58 C59 1.390(5) . ? C58 C63 1.396(5) . ? C59 H59 0.9300 . ? C59 C60 1.394(6) . ? C60 H60 0.9300 . ? C60 C61 1.386(7) . ? C61 H61 0.9300 . ? C61 C62 1.384(7) . ? C62 H62 0.9300 . ? C62 C63 1.395(5) . ? C63 H63 0.9300 . ? C64 C65 1.402(5) . ? C64 C69 1.389(5) . ? C65 H65 0.9300 . ? C65 C66 1.385(6) . ? C66 H66 0.9300 . ? C66 C67 1.386(7) . ? C67 H67 0.9300 . ? C67 C68 1.392(6) . ? C68 H68 0.9300 . ? C68 C69 1.395(6) . ? C69 H69 0.9300 . ? C70 C71 1.491(5) . ? C70 C77 1.357(5) . ? C71 C72 1.384(6) . ? C71 C76 1.410(5) . ? C72 H72 0.9300 . ? C72 C73 1.393(6) . ? C73 H73 0.9300 . ? C73 C74 1.390(7) . ? C74 H74 0.9300 . ? C74 C75 1.375(8) . ? C75 H75 0.9300 . ? C75 C76 1.385(6) . ? C76 H76 0.9300 . ? C77 H77 0.9300 . ? C77 C78 1.480(5) . ? C78 C79 1.397(5) . ? C78 C83 1.404(5) . ? C79 H79 0.9300 . ? C79 C80 1.397(5) . ? C80 H80 0.9300 . ? C80 C81 1.384(6) . ? C81 H81 0.9300 . ? C81 C82 1.385(7) . ? C82 H82 0.9300 . ? C82 C83 1.391(6) . ? C83 H83 0.9300 . ? O1 C84 1.394(9) . ? O1 C87 1.496(11) . ? C84 H84A 0.9700 . ? C84 H84B 0.9700 . ? C84 C85 1.521(10) . ? C85 H85A 0.9700 . ? C85 H85B 0.9700 . ? C85 C86 1.530(9) . ? C86 H86A 0.9700 . ? C86 H86B 0.9700 . ? C86 C87 1.538(10) . ? C87 H87A 0.9700 . ? C87 H87B 0.9700 . ? O2 C88 1.409(8) . ? O2 C91 1.407(9) . ? C88 H88A 0.9700 . ? C88 H88B 0.9700 . ? C88 C89 1.475(10) . ? C89 H89A 0.9700 . ? C89 H89B 0.9700 . ? C89 C90 1.442(12) . ? C90 H90A 0.9700 . ? C90 H90B 0.9700 . ? C90 C91 1.513(13) . ? C91 H91A 0.9700 . ? C91 H91B 0.9700 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 C70 C71 C72 -53.6(4) . . . . ? Cu1 C70 C71 C76 123.8(3) . . . . ? Cu1 C70 C77 C78 169.7(3) . . . . ? N1 C2 C3 N2 1.0(4) . . . . ? N1 C4 C5 C6 -174.7(3) . . . . ? N1 C4 C5 C10 6.6(5) . . . . ? N1 C4 C9 C8 175.3(3) . . . . ? N1 C4 C9 C24 -3.8(5) . . . . ? N2 C37 C38 C39 167.4(3) . . . . ? N2 C37 C38 C43 -16.6(4) . . . . ? N2 C37 C42 C41 -170.5(3) . . . . ? N2 C37 C42 C57 7.7(5) . . . . ? C1 N1 C2 C3 -1.0(4) . . . . ? C1 N1 C4 C5 -88.7(4) . . . . ? C1 N1 C4 C9 93.7(4) . . . . ? C1 N2 C3 C2 -0.7(4) . . . . ? C1 N2 C37 C38 99.8(4) . . . . ? C1 N2 C37 C42 -87.8(4) . . . . ? C2 N1 C1 Cu1 175.4(2) . . . . ? C2 N1 C1 N2 0.6(3) . . . . ? C2 N1 C4 C5 87.8(4) . . . . ? C2 N1 C4 C9 -89.8(4) . . . . ? C3 N2 C1 Cu1 -173.9(2) . . . . ? C3 N2 C1 N1 0.0(3) . . . . ? C3 N2 C37 C38 -82.3(4) . . . . ? C3 N2 C37 C42 90.1(4) . . . . ? C4 N1 C1 Cu1 -7.8(4) . . . . ? C4 N1 C1 N2 177.4(3) . . . . ? C4 N1 C2 C3 -177.9(3) . . . . ? C4 C5 C6 C7 -0.2(5) . . . . ? C4 C5 C10 C11 142.4(3) . . . . ? C4 C5 C10 C17 -89.9(4) . . . . ? C4 C9 C24 C25 -132.4(3) . . . . ? C4 C9 C24 C31 100.6(4) . . . . ? C5 C4 C9 C8 -2.2(5) . . . . ? C5 C4 C9 C24 178.7(3) . . . . ? C5 C6 C7 C8 -2.8(6) . . . . ? C5 C6 C7 C23 177.9(4) . . . . ? C5 C10 C11 C12 -69.6(4) . . . . ? C5 C10 C11 C16 108.7(4) . . . . ? C5 C10 C17 C18 156.6(3) . . . . ? C5 C10 C17 C22 -26.1(5) . . . . ? C6 C5 C10 C11 -36.2(4) . . . . ? C6 C5 C10 C17 91.5(4) . . . . ? C6 C7 C8 C9 3.4(6) . . . . ? C7 C8 C9 C4 -1.0(6) . . . . ? C7 C8 C9 C24 178.1(4) . . . . ? C8 C9 C24 C25 48.5(4) . . . . ? C8 C9 C24 C31 -78.4(4) . . . . ? C9 C4 C5 C6 2.8(5) . . . . ? C9 C4 C5 C10 -175.8(3) . . . . ? C9 C24 C25 C26 86.1(4) . . . . ? C9 C24 C25 C30 -91.0(4) . . . . ? C9 C24 C31 C32 -0.9(5) . . . . ? C9 C24 C31 C36 -178.9(3) . . . . ? C10 C5 C6 C7 178.4(3) . . . . ? C10 C11 C12 C13 178.5(4) . . . . ? C10 C11 C16 C15 -179.0(4) . . . . ? C10 C17 C18 C19 177.1(4) . . . . ? C10 C17 C22 C21 -177.1(4) . . . . ? C11 C10 C17 C18 -76.7(4) . . . . ? C11 C10 C17 C22 100.6(4) . . . . ? C11 C12 C13 C14 0.7(7) . . . . ? C12 C11 C16 C15 -0.6(6) . . . . ? C12 C13 C14 C15 -0.9(7) . . . . ? C13 C14 C15 C16 0.4(7) . . . . ? C14 C15 C16 C11 0.4(7) . . . . ? C16 C11 C12 C13 0.1(6) . . . . ? C17 C10 C11 C12 161.8(3) . . . . ? C17 C10 C11 C16 -19.9(5) . . . . ? C17 C18 C19 C20 0.4(6) . . . . ? C18 C17 C22 C21 0.1(6) . . . . ? C18 C19 C20 C21 -0.3(7) . . . . ? C19 C20 C21 C22 0.2(7) . . . . ? C20 C21 C22 C17 -0.1(7) . . . . ? C22 C17 C18 C19 -0.3(6) . . . . ? C23 C7 C8 C9 -177.3(4) . . . . ? C24 C25 C26 C27 -177.1(4) . . . . ? C24 C25 C30 C29 177.2(3) . . . . ? C24 C31 C32 C33 179.7(4) . . . . ? C24 C31 C36 C35 -179.7(4) . . . . ? C25 C24 C31 C32 -126.6(4) . . . . ? C25 C24 C31 C36 55.4(4) . . . . ? C25 C26 C27 C28 -0.4(7) . . . . ? C26 C25 C30 C29 -0.1(6) . . . . ? C26 C27 C28 C29 0.4(8) . . . . ? C27 C28 C29 C30 -0.2(7) . . . . ? C28 C29 C30 C25 0.1(6) . . . . ? C30 C25 C26 C27 0.2(6) . . . . ? C31 C24 C25 C26 -146.8(3) . . . . ? C31 C24 C25 C30 36.0(5) . . . . ? C31 C32 C33 C34 0.9(8) . . . . ? C32 C31 C36 C35 2.2(6) . . . . ? C32 C33 C34 C35 0.6(8) . . . . ? C33 C34 C35 C36 -0.6(7) . . . . ? C34 C35 C36 C31 -0.8(7) . . . . ? C36 C31 C32 C33 -2.2(7) . . . . ? C37 N2 C1 Cu1 4.2(5) . . . . ? C37 N2 C1 N1 178.1(3) . . . . ? C37 N2 C3 C2 -178.9(3) . . . . ? C37 C38 C39 C40 2.5(5) . . . . ? C37 C38 C43 C44 130.9(3) . . . . ? C37 C38 C43 C50 -100.0(3) . . . . ? C37 C42 C57 C58 135.4(3) . . . . ? C37 C42 C57 C64 -97.1(4) . . . . ? C38 C37 C42 C41 1.6(5) . . . . ? C38 C37 C42 C57 179.9(3) . . . . ? C38 C39 C40 C41 2.7(5) . . . . ? C38 C39 C40 C56 -177.1(3) . . . . ? C38 C43 C44 C45 -83.0(4) . . . . ? C38 C43 C44 C49 98.7(4) . . . . ? C38 C43 C50 C51 122.0(3) . . . . ? C38 C43 C50 C55 -59.3(4) . . . . ? C39 C38 C43 C44 -53.2(4) . . . . ? C39 C38 C43 C50 75.9(4) . . . . ? C39 C40 C41 C42 -6.0(5) . . . . ? C40 C41 C42 C37 3.9(5) . . . . ? C40 C41 C42 C57 -174.4(3) . . . . ? C41 C42 C57 C58 -46.4(4) . . . . ? C41 C42 C57 C64 81.1(4) . . . . ? C42 C37 C38 C39 -4.7(5) . . . . ? C42 C37 C38 C43 171.3(3) . . . . ? C42 C57 C58 C59 -89.4(4) . . . . ? C42 C57 C58 C63 90.1(4) . . . . ? C42 C57 C64 C65 170.9(3) . . . . ? C42 C57 C64 C69 -8.7(5) . . . . ? C43 C38 C39 C40 -173.5(3) . . . . ? C43 C44 C45 C46 -176.6(4) . . . . ? C43 C44 C49 C48 176.6(3) . . . . ? C43 C50 C51 C52 178.7(3) . . . . ? C43 C50 C55 C54 -177.3(3) . . . . ? C44 C43 C50 C51 -109.3(3) . . . . ? C44 C43 C50 C55 69.5(4) . . . . ? C44 C45 C46 C47 -0.6(7) . . . . ? C45 C44 C49 C48 -1.7(6) . . . . ? C45 C46 C47 C48 -0.5(7) . . . . ? C46 C47 C48 C49 0.6(6) . . . . ? C47 C48 C49 C44 0.5(6) . . . . ? C49 C44 C45 C46 1.7(6) . . . . ? C50 C43 C44 C45 149.4(3) . . . . ? C50 C43 C44 C49 -28.9(5) . . . . ? C50 C51 C52 C53 -0.8(6) . . . . ? C51 C50 C55 C54 1.4(5) . . . . ? C51 C52 C53 C54 0.3(6) . . . . ? C52 C53 C54 C55 1.1(6) . . . . ? C53 C54 C55 C50 -1.9(6) . . . . ? C55 C50 C51 C52 -0.1(5) . . . . ? C56 C40 C41 C42 173.8(3) . . . . ? C57 C58 C59 C60 177.4(4) . . . . ? C57 C58 C63 C62 -176.4(3) . . . . ? C57 C64 C65 C66 179.1(4) . . . . ? C57 C64 C69 C68 -178.3(4) . . . . ? C58 C57 C64 C65 -61.9(4) . . . . ? C58 C57 C64 C69 118.5(4) . . . . ? C58 C59 C60 C61 0.0(7) . . . . ? C59 C58 C63 C62 3.2(6) . . . . ? C59 C60 C61 C62 1.2(7) . . . . ? C60 C61 C62 C63 -0.2(6) . . . . ? C61 C62 C63 C58 -2.0(6) . . . . ? C63 C58 C59 C60 -2.1(6) . . . . ? C64 C57 C58 C59 142.4(3) . . . . ? C64 C57 C58 C63 -38.0(4) . . . . ? C64 C65 C66 C67 -0.8(7) . . . . ? C65 C64 C69 C68 2.1(6) . . . . ? C65 C66 C67 C68 2.0(7) . . . . ? C66 C67 C68 C69 -1.2(7) . . . . ? C67 C68 C69 C64 -0.8(7) . . . . ? C69 C64 C65 C66 -1.3(6) . . . . ? C70 C71 C72 C73 178.0(4) . . . . ? C70 C71 C76 C75 -176.5(4) . . . . ? C70 C77 C78 C79 -33.2(6) . . . . ? C70 C77 C78 C83 151.6(4) . . . . ? C71 C70 C77 C78 -8.0(6) . . . . ? C71 C72 C73 C74 -1.1(6) . . . . ? C72 C71 C76 C75 1.0(6) . . . . ? C72 C73 C74 C75 0.2(6) . . . . ? C73 C74 C75 C76 1.4(6) . . . . ? C74 C75 C76 C71 -2.0(6) . . . . ? C76 C71 C72 C73 0.5(6) . . . . ? C77 C70 C71 C72 124.3(4) . . . . ? C77 C70 C71 C76 -58.3(5) . . . . ? C77 C78 C79 C80 -176.4(3) . . . . ? C77 C78 C83 C82 176.8(3) . . . . ? C78 C79 C80 C81 0.2(6) . . . . ? C79 C78 C83 C82 1.4(5) . . . . ? C79 C80 C81 C82 0.5(6) . . . . ? C80 C81 C82 C83 -0.2(6) . . . . ? C81 C82 C83 C78 -0.7(6) . . . . ? C83 C78 C79 C80 -1.1(5) . . . . ? O1 C84 C85 C86 22.5(8) . . . . ? C84 O1 C87 C86 38.7(7) . . . . ? C84 C85 C86 C87 2.4(7) . . . . ? C85 C86 C87 O1 -24.7(7) . . . . ? C87 O1 C84 C85 -37.5(8) . . . . ? O2 C88 C89 C90 -1.4(12) . . . . ? C88 O2 C91 C90 -22.3(9) . . . . ? C88 C89 C90 C91 -11.6(13) . . . . ? C89 C90 C91 O2 20.6(12) . . . . ? C91 O2 C88 C89 15.2(9) . . . . ?