#------------------------------------------------------------------------------ #$Date: 2021-07-31 11:59:58 +0300 (Sat, 31 Jul 2021) $ #$Revision: 267860 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/42/1564295.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564295 loop_ _publ_author_name 'Soliman, Saied M.' 'Elsilk, Sobhy E.' 'El-Faham, Ayman' _publ_section_title ; Syntheses, structure, Hirshfeld analysis and antimicrobial activity of four new Co(II) complexes with s-triazine-based pincer ligand ; _journal_name_full 'Inorganica Chimica Acta' _journal_page_first 119753 _journal_paper_doi 10.1016/j.ica.2020.119753 _journal_volume 510 _journal_year 2020 _chemical_formula_sum 'C14 H25 Cl2 Co N7 O13' _chemical_formula_weight 629.24 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 78.9140(19) _cell_angle_beta 81.9100(18) _cell_angle_gamma 76.8150(19) _cell_formula_units_Z 2 _cell_length_a 8.0012(4) _cell_length_b 8.1605(4) _cell_length_c 20.4639(10) _cell_measurement_reflns_used 9896 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 36.25 _cell_measurement_theta_min 2.60 _cell_volume 1270.09(11) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Mercury 3.8' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2008)' _computing_structure_solution 'SHELXS-2013 (Sheldrick 2008)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0473 _diffrn_reflns_av_unetI/netI 0.0427 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 38461 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.605 _diffrn_reflns_theta_min 2.600 _exptl_absorpt_coefficient_mu 0.961 _exptl_absorpt_correction_T_max 0.7471 _exptl_absorpt_correction_T_min 0.6550 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Sheldrick, 2012)' _exptl_crystal_colour pink _exptl_crystal_density_diffrn 1.645 _exptl_crystal_description plate _exptl_crystal_F_000 646 _exptl_crystal_size_max 0.31 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.906 _refine_diff_density_min -0.539 _refine_diff_density_rms 0.075 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.018 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 375 _refine_ls_number_reflns 7787 _refine_ls_number_restraints 12 _refine_ls_restrained_S_all 1.018 _refine_ls_R_factor_all 0.0847 _refine_ls_R_factor_gt 0.0545 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0816P)^2^+0.7020P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1408 _refine_ls_wR_factor_ref 0.1547 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 5506 _reflns_number_total 7787 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file 2.cif _cod_data_source_block SA1CoClO4EA10T1RT_0m _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'Multi-Scan' was changed to 'multi-scan' in accordance with the built-in table derived from the CIF Core dictionary named 'cif_core.dic' version 2.4.5 last updated on 2014-11-21. Automatic conversion script Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius ; _cod_database_code 1564295 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; SA1CoClO4EA10T1RT_0m.res created by SHELXL-2014/7 TITL SA1CoClO4EA10T1RT_0m_a.res in P-1 CELL 0.71073 8.0012 8.1605 20.4639 78.914 81.910 76.815 ZERR 2.00 0.0004 0.0004 0.0010 0.0019 0.0018 0.0019 LATT 1 SFAC C H N CL CO O UNIT 28 50 14 4 2 26 LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP 20.000 ACTA L.S. 40 FMAP 2 PLAN -5 0 0.00 DFIX 0.75 0.01 O1 H1A O1 H1B DANG 1.34 0.02 H1A H1B DFIX 0.84 0.01 O3 H3A O3 H3B DANG 1.34 0.02 H3A H3B DFIX 0.84 0.01 O2 H2A O2 H2B DANG 1.34 0.02 H2A H2B DFIX 0.95 0.01 O13 H14 O13 H13 DANG 1.55 0.02 H13 H14 EADP O5A O5B EADP O7A O7B EADP O9A O9B HTAB BOND $H CONF WGHT 0.081600 0.702000 FVAR 0.36765 0.69593 CO1 5 0.400370 0.685223 0.704458 11.00000 0.03560 0.04000 = 0.02641 -0.01088 -0.00133 -0.00279 N1 3 0.316061 0.751212 0.796953 11.00000 0.03601 0.03795 = 0.02657 -0.00804 -0.00086 -0.00611 O1 6 0.659217 0.699514 0.700777 11.00000 0.04184 0.09469 = 0.04457 -0.00444 -0.00175 -0.01913 AFIX 148 H1A 2 0.684856 0.754035 0.668400 11.00000 -1.50000 AFIX 0 CL1 4 0.796574 0.344104 0.523972 11.00000 0.05109 0.06978 = 0.04568 -0.01506 -0.00341 -0.00737 CL2 4 -0.172810 0.730030 0.853362 11.00000 0.04846 0.07227 = 0.04254 -0.01495 -0.00270 -0.00072 N2 3 0.196612 0.964307 0.861922 11.00000 0.05271 0.04530 = 0.03202 -0.01383 0.00442 -0.00908 O2 6 0.467432 0.619798 0.612625 11.00000 0.06153 0.09304 = 0.04422 -0.03751 -0.00814 0.00859 AFIX 148 H2B 2 0.387412 0.587676 0.601168 11.00000 -1.50000 AFIX 0 O3 6 0.146525 0.660653 0.694983 11.00000 0.04582 0.06012 = 0.04416 -0.00757 -0.00803 -0.01559 AFIX 148 H3A 2 0.113210 0.721064 0.659725 11.00000 -1.50000 AFIX 0 C3 1 0.213378 0.838520 0.914451 11.00000 0.04176 0.05597 = 0.02928 -0.01419 0.00137 -0.01067 N3 3 0.280333 0.673471 0.913674 11.00000 0.03894 0.05398 = 0.02635 -0.00725 0.00072 -0.00856 H1B 2 0.686004 0.702208 0.734053 11.00000 0.09153 H13 2 0.783995 0.913171 0.586247 11.00000 0.07974 H14 2 0.949437 0.779253 0.572733 11.00000 0.52504 H3B 2 0.076305 0.694539 0.726476 11.00000 0.09033 C14 1 0.146999 0.765952 1.031168 11.00000 0.08638 0.09814 = 0.02790 -0.00736 0.00820 0.00589 AFIX 137 H14A 2 0.064235 0.700556 1.027318 11.00000 -1.50000 H14B 2 0.110597 0.822795 1.069272 11.00000 -1.50000 H14C 2 0.257487 0.691257 1.036679 11.00000 -1.50000 AFIX 0 N4 3 0.311209 0.961440 0.687496 11.00000 0.04779 0.04143 = 0.02826 -0.00980 0.00347 -0.01053 C4 1 0.429647 0.323256 0.885606 11.00000 0.04782 0.04579 = 0.04766 0.00535 -0.00596 -0.00708 O4 6 0.159985 0.890533 0.971657 11.00000 0.07725 0.07312 = 0.02902 -0.01855 0.00662 -0.00338 part 1 O5A 6 0.946180 0.209241 0.531239 21.00000 0.12487 0.13104 = 0.07765 -0.04408 -0.03243 0.06574 part 2 O5B 6 0.900052 0.208783 0.554188 -21.00000 0.12487 0.13104 = 0.07765 -0.04408 -0.03243 0.06574 part 0 C5 1 0.513160 0.205346 0.847238 11.00000 0.06000 0.04017 = 0.05977 0.00111 -0.01003 -0.00185 AFIX 43 H5 2 0.552026 0.089523 0.862152 11.00000 -1.20000 AFIX 0 N5 3 0.232359 1.023489 0.744902 11.00000 0.05050 0.03528 = 0.02835 -0.00800 0.00401 -0.00832 O6 6 0.799799 0.471033 0.561675 11.00000 0.07134 0.11392 = 0.09946 -0.05937 0.00207 -0.02431 C1 1 0.247314 0.911086 0.804817 11.00000 0.03592 0.03719 = 0.02992 -0.00900 0.00135 -0.00905 C2 1 0.328441 0.639847 0.852625 11.00000 0.02802 0.04144 = 0.03027 -0.00522 -0.00204 -0.00780 C6 1 0.530235 0.290152 0.780836 11.00000 0.04159 0.03964 = 0.04945 -0.00878 -0.00805 -0.00395 N6 3 0.459125 0.453719 0.777451 11.00000 0.03958 0.03865 = 0.03486 -0.00865 -0.00426 -0.00237 part 1 O7A 6 0.622317 0.306265 0.539095 21.00000 0.05941 0.12376 = 0.10614 -0.04341 0.01422 -0.03746 part 2 O7B 6 0.693026 0.241496 0.548679 -21.00000 0.05941 0.12376 = 0.10614 -0.04341 0.01422 -0.03746 part 0 N7 3 0.398175 0.474276 0.842249 11.00000 0.03789 0.04081 = 0.03120 -0.00346 -0.00205 -0.00521 C7 1 0.613306 0.219642 0.720367 11.00000 0.06409 0.05194 = 0.06557 -0.02494 -0.00547 0.00500 AFIX 137 H7A 2 0.535747 0.253723 0.686144 11.00000 -1.50000 H7B 2 0.641419 0.097339 0.730870 11.00000 -1.50000 H7C 2 0.716863 0.261933 0.704697 11.00000 -1.50000 AFIX 0 O8 6 0.805963 0.409554 0.454553 11.00000 0.10953 0.12182 = 0.05228 -0.00272 -0.01335 -0.04338 C8 1 0.371361 0.301110 0.958260 11.00000 0.09077 0.06921 = 0.04562 0.01319 0.00665 -0.00277 AFIX 137 H8A 2 0.249438 0.345599 0.964749 11.00000 -1.50000 H8B 2 0.431141 0.361431 0.980043 11.00000 -1.50000 H8C 2 0.395783 0.181970 0.977006 11.00000 -1.50000 AFIX 0 part 1 O9A 6 -0.340200 0.737654 0.850787 21.00000 0.05593 0.23157 = 0.17205 -0.03194 -0.02043 -0.06188 part 2 O9B 6 -0.274821 0.605718 0.845659 -21.00000 0.05593 0.23157 = 0.17205 -0.03194 -0.02043 -0.06188 part 0 C9 1 0.270811 1.088345 0.638151 11.00000 0.05142 0.04143 = 0.03426 -0.00280 -0.00164 -0.01631 H2A 2 0.564134 0.580546 0.595314 11.00000 0.08970 C11 1 0.140709 1.186916 0.729809 11.00000 0.05524 0.03397 = 0.04393 -0.00784 0.00086 -0.00771 C10 1 0.164700 1.230269 0.662501 11.00000 0.06348 0.03722 = 0.04467 0.00007 -0.00460 -0.00765 AFIX 43 H10 2 0.119424 1.334410 0.637186 11.00000 -1.20000 AFIX 0 O10 6 -0.175916 0.841452 0.898835 11.00000 0.15936 0.12918 = 0.09889 -0.06337 0.00870 -0.02046 O12 6 -0.104157 0.801324 0.790118 11.00000 0.12354 0.19180 = 0.06840 -0.00743 0.02020 -0.03448 C12 1 0.034572 1.285156 0.780313 11.00000 0.08166 0.04139 = 0.05769 -0.01427 0.00498 0.00153 AFIX 137 H12A 2 -0.031721 1.389032 0.758067 11.00000 -1.50000 H12B 2 0.108570 1.311771 0.808086 11.00000 -1.50000 H12C 2 -0.041936 1.218349 0.807524 11.00000 -1.50000 AFIX 0 O13 6 0.884478 0.846512 0.604442 11.00000 0.08932 0.10648 = 0.05574 -0.00607 0.00959 -0.01390 C13 1 0.336829 1.068295 0.567967 11.00000 0.07568 0.06623 = 0.03137 -0.00403 0.00307 -0.01536 AFIX 137 H13A 2 0.253818 1.030401 0.548035 11.00000 -1.50000 H13B 2 0.443536 0.985623 0.567500 11.00000 -1.50000 H13C 2 0.355804 1.175901 0.543003 11.00000 -1.50000 AFIX 0 O11 6 -0.051086 0.590413 0.877040 11.00000 0.13045 0.10757 = 0.22290 -0.00367 -0.07160 0.00538 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM SA1CoClO4EA10T1RT_0m_a.res in P-1 REM R1 = 0.0545 for 5506 Fo > 4sig(Fo) and 0.0847 for all 7787 data REM 375 parameters refined using 12 restraints END WGHT 0.0824 0.6324 REM Instructions for potential hydrogen bonds HTAB O1 O13 EQIV $1 -x+1, -y+1, -z+1 HTAB O2 O8_$1 EQIV $2 x-1, y, z HTAB O3 O13_$2 EQIV $3 x+1, y, z HTAB O1 Cl2_$3 HTAB O1 O9A_$3 HTAB O1 O9B_$3 HTAB O1 O12_$3 EQIV $4 x, y+1, z HTAB O13 O7B_$4 EQIV $5 -x+2, -y+1, -z+1 HTAB O13 Cl1_$5 HTAB O13 O5A_$5 HTAB O13 O8_$5 HTAB O3 O12 HTAB O2 Cl1 HTAB O2 O6 HTAB O2 O7A EQIV $6 -x+1, -y+2, -z+1 HTAB C10 O8_$6 EQIV $7 x-1, y+1, z HTAB C13 O5A_$7 HTAB C13 O7A_$4 REM Highest difference peak 0.906, deepest hole -0.539, 1-sigma level 0.075 Q1 1 -0.3299 0.8180 0.8843 11.00000 0.05 0.91 Q2 1 -0.2892 0.8420 0.7994 11.00000 0.05 0.54 Q3 1 -0.2121 0.5851 0.8225 11.00000 0.05 0.52 Q4 1 -0.0199 0.6706 0.8209 11.00000 0.05 0.52 Q5 1 -0.3344 0.8037 0.8191 11.00000 0.05 0.52 ; _shelx_res_checksum 77070 _shelx_hkl_file ; -1 0 0 146.89 3.50 -1 0 0 116.49 3.50 -1 0 0 143.19 3.50 1 0 0 136.09 3.90 1 0 0 132.79 3.50 -2 0 0 1220.98 52.99 2 0 0 937.91 44.90 -3 0 0 312.77 8.20 -3 0 0 303.67 8.00 -3 0 0 307.77 9.30 -3 0 0 299.57 8.10 3 0 0 296.47 8.10 3 0 0 304.07 9.30 3 0 0 305.37 8.00 3 0 0 308.87 8.10 -4 0 0 233.28 8.30 -4 0 0 250.77 6.70 -4 0 0 232.38 6.40 4 0 0 244.28 6.50 4 0 0 241.38 6.50 -5 0 0 218.48 6.20 -5 0 0 239.68 6.50 -5 0 0 216.98 8.30 5 0 0 223.68 6.20 5 0 0 221.28 6.20 5 0 0 222.78 8.20 -6 0 0 13.00 1.10 -6 0 0 15.50 1.70 -6 0 0 11.40 3.10 -6 0 0 15.40 1.00 6 0 0 13.00 1.00 6 0 0 11.70 1.20 6 0 0 10.20 2.80 -7 0 0 1.10 1.10 -7 0 0 1.50 0.60 -7 0 0 1.10 0.70 -7 0 0 1.60 0.80 7 0 0 0.80 0.70 7 0 0 0.60 0.90 7 0 0 -1.50 2.70 -8 0 0 7.40 0.90 -8 0 0 7.70 1.30 -8 0 0 5.80 1.20 -8 0 0 3.70 1.40 8 0 0 8.40 1.10 8 0 0 2.20 3.70 -9 0 0 5.60 0.90 -9 0 0 5.80 1.70 -9 0 0 6.00 1.40 9 0 0 5.50 1.60 9 0 0 0.90 5.20 9 0 0 7.30 1.30 -10 0 0 3.40 2.20 -10 0 0 4.00 1.50 -10 0 0 5.60 1.10 10 0 0 2.30 1.90 -11 0 0 1.00 1.20 -11 0 0 4.30 1.90 11 0 0 13.40 10.20 10 -1 0 0.50 7.50 -10 1 0 -1.10 2.30 -10 1 0 2.80 1.60 -10 1 0 3.00 1.20 9 -1 0 5.10 4.70 -9 1 0 10.70 1.60 -9 1 0 8.90 1.20 -9 1 0 9.40 2.00 8 -1 0 -3.60 3.00 8 -1 0 0.00 1.10 8 -1 0 1.90 0.90 -8 1 0 0.40 0.90 -8 1 0 -0.10 0.70 -8 1 0 -0.80 1.40 7 -1 0 24.40 4.40 7 -1 0 21.60 1.20 7 -1 0 22.40 1.90 -7 1 0 21.60 1.40 -7 1 0 21.80 1.70 -7 1 0 21.70 2.40 -7 1 0 21.60 1.50 6 -1 0 7.50 0.80 6 -1 0 4.50 2.30 6 -1 0 11.30 1.20 -6 1 0 8.70 1.30 -6 1 0 8.40 1.00 -6 1 0 3.80 3.20 -6 1 0 8.80 1.10 -6 1 0 9.20 1.20 5 -1 0 189.48 7.40 5 -1 0 188.48 5.20 5 -1 0 193.18 5.50 -5 1 0 201.18 5.90 -5 1 0 188.28 5.40 -5 1 0 192.48 5.40 -5 1 0 194.88 5.40 -5 1 0 182.28 7.70 4 -1 0 152.58 5.90 4 -1 0 158.38 4.40 4 -1 0 153.28 4.20 -4 1 0 151.88 4.40 -4 1 0 157.58 4.70 -4 1 0 152.08 6.30 -4 1 0 155.48 4.40 3 -1 0 5.70 0.40 3 -1 0 5.90 0.70 3 -1 0 4.00 1.30 3 -1 0 6.40 0.60 -3 1 0 6.90 0.80 -3 1 0 6.10 0.40 -3 1 0 5.50 0.60 2 -1 0 10.00 1.50 2 -1 0 12.10 0.80 2 -1 0 11.90 0.50 2 -1 0 12.60 0.60 -2 1 0 11.40 1.70 -2 1 0 11.10 0.80 -2 1 0 12.60 0.60 -2 1 0 13.10 0.40 1 -1 0 7.40 0.50 1 -1 0 6.40 0.80 1 -1 0 8.90 0.40 1 -1 0 9.10 0.50 -1 1 0 6.30 0.90 -1 1 0 8.00 0.40 -1 1 0 8.40 0.50 -1 1 0 8.30 0.50 0 1 0 136.39 3.30 0 1 0 108.39 3.20 -1 -1 0 1119.29 37.30 1 1 0 1059.39 37.00 -2 -1 0 1492.35 55.49 2 1 0 1345.57 54.49 -3 -1 0 4.50 0.40 -3 -1 0 5.70 0.60 -3 -1 0 4.40 1.40 3 1 0 5.00 0.60 3 1 0 4.20 1.40 3 1 0 4.50 0.40 3 1 0 4.10 0.70 -4 -1 0 31.90 1.50 -4 -1 0 37.30 1.20 -4 -1 0 36.50 1.40 4 1 0 34.40 1.50 4 1 0 39.10 1.50 4 1 0 39.70 3.70 -5 -1 0 7.30 2.20 -5 -1 0 6.10 0.80 -5 -1 0 6.80 0.80 -5 -1 0 6.40 0.60 5 1 0 5.30 2.20 5 1 0 7.10 0.80 -6 -1 0 24.40 3.90 -6 -1 0 32.30 1.60 -6 -1 0 35.10 1.80 6 1 0 32.30 4.30 6 1 0 34.40 1.60 6 1 0 34.40 1.70 -7 -1 0 25.40 1.90 -7 -1 0 27.70 1.30 -7 -1 0 28.20 1.60 7 1 0 26.90 1.70 7 1 0 26.20 1.70 7 1 0 22.50 4.80 -8 -1 0 5.10 1.30 -8 -1 0 5.30 1.20 -8 -1 0 6.70 1.00 -8 -1 0 4.80 0.80 8 1 0 0.80 3.00 8 1 0 6.80 1.30 -9 -1 0 1.80 1.20 -9 -1 0 4.30 1.20 -9 -1 0 2.00 0.70 -9 -1 0 0.90 1.40 9 1 0 1.20 1.50 9 1 0 4.10 1.40 9 1 0 -0.40 5.60 -10 -1 0 -0.20 0.70 -10 -1 0 1.00 1.40 10 1 0 -0.20 1.80 10 1 0 -4.00 6.70 -11 -1 0 7.30 1.20 -11 -1 0 10.30 2.10 11 1 0 3.50 2.70 11 1 0 19.90 11.30 10 -2 0 -1.80 8.20 -10 2 0 2.00 1.50 -10 2 0 1.30 1.40 9 -2 0 -3.00 6.10 -9 2 0 0.70 2.10 -9 2 0 0.70 1.30 -9 2 0 -0.30 1.00 8 -2 0 -1.10 3.50 -8 2 0 4.50 1.10 -8 2 0 3.60 1.20 -8 2 0 2.70 1.70 7 -2 0 19.10 1.80 7 -2 0 21.20 4.30 -7 2 0 18.50 1.50 -7 2 0 18.90 1.50 -7 2 0 18.70 2.50 6 -2 0 3.70 1.10 6 -2 0 0.10 2.30 -6 2 0 0.60 3.50 -6 2 0 2.80 0.70 -6 2 0 3.80 1.00 -6 2 0 3.30 0.90 -6 2 0 2.20 1.20 5 -2 0 36.20 3.50 5 -2 0 41.80 1.80 -5 2 0 42.80 1.90 -5 2 0 39.20 1.70 -5 2 0 39.60 2.30 -5 2 0 37.70 4.50 4 -2 0 53.29 1.90 4 -2 0 46.20 3.30 -4 2 0 48.20 2.30 -4 2 0 53.19 2.00 -4 2 0 53.09 1.90 -4 2 0 49.60 4.20 3 -2 0 9.10 1.00 -3 2 0 10.20 0.80 -3 2 0 10.00 0.80 -3 2 0 6.60 1.70 -3 2 0 8.90 1.00 2 -2 0 38.10 2.00 2 -2 0 41.20 1.30 2 -2 0 39.50 1.40 2 -2 0 39.60 1.60 -2 2 0 38.00 1.40 -2 2 0 37.90 1.40 -2 2 0 40.00 2.40 -2 2 0 37.10 1.60 -2 2 0 40.60 1.20 1 -2 0 411.56 11.10 1 -2 0 432.76 11.30 1 -2 0 425.36 11.40 1 -2 0 437.46 11.10 -1 2 0 428.46 11.10 -1 2 0 423.46 11.10 -1 2 0 406.96 11.10 -1 2 0 439.86 11.60 -1 2 0 430.76 11.30 0 2 0 2568.44 70.79 0 2 0 2616.04 73.19 -1 -2 0 427.86 11.10 1 2 0 430.06 11.10 1 2 0 427.56 11.10 -2 -2 0 36.90 1.70 -2 -2 0 36.60 1.10 -2 -2 0 36.70 1.20 2 2 0 37.30 1.10 2 2 0 39.80 2.00 2 2 0 38.10 1.30 -3 -2 0 18.10 0.90 -3 -2 0 21.10 1.70 -3 -2 0 20.80 0.70 3 2 0 18.20 1.10 3 2 0 18.70 0.90 3 2 0 19.90 0.70 3 2 0 21.70 2.30 -4 -2 0 727.43 20.00 -4 -2 0 722.13 18.80 4 2 0 717.63 18.60 4 2 0 740.23 19.10 4 2 0 682.43 20.20 4 2 0 756.12 18.90 -5 -2 0 0.80 1.60 -5 -2 0 0.60 0.50 -5 -2 0 0.40 0.30 5 2 0 2.70 2.20 5 2 0 0.90 0.60 5 2 0 -0.30 0.80 -6 -2 0 32.70 1.30 -6 -2 0 33.40 1.60 -6 -2 0 36.40 1.60 -6 -2 0 32.90 3.70 6 2 0 34.60 1.70 6 2 0 34.70 4.40 6 2 0 36.00 1.90 -7 -2 0 0.30 3.20 -7 -2 0 1.20 0.80 -7 -2 0 2.70 0.80 7 2 0 2.10 1.10 7 2 0 0.50 2.60 -8 -2 0 1.80 0.60 -8 -2 0 0.90 0.90 -8 -2 0 2.50 1.00 8 2 0 0.20 3.50 8 2 0 2.50 1.40 -9 -2 0 20.00 1.90 -9 -2 0 18.10 1.30 -9 -2 0 18.00 1.20 -9 -2 0 18.60 1.60 -9 -2 0 14.00 1.90 9 2 0 20.90 6.10 9 2 0 18.30 2.40 -10 -2 0 1.30 1.40 -10 -2 0 0.00 0.70 10 2 0 -5.40 7.30 10 2 0 -0.40 2.00 -11 -2 0 2.00 1.80 11 2 0 0.00 2.50 11 2 0 7.40 11.00 10 -3 0 7.70 9.80 -10 3 0 4.10 1.70 -10 3 0 1.50 1.90 9 -3 0 -3.40 8.20 -9 3 0 1.20 1.30 -9 3 0 0.80 1.50 8 -3 0 -2.90 3.90 -8 3 0 0.20 1.00 -8 3 0 5.20 2.10 -8 3 0 0.20 1.10 7 -3 0 10.20 3.40 -7 3 0 9.40 1.90 -7 3 0 13.40 1.50 -7 3 0 10.70 1.40 6 -3 0 10.00 1.50 6 -3 0 7.70 2.60 -6 3 0 7.00 1.40 -6 3 0 7.20 1.60 -6 3 0 8.20 1.10 5 -3 0 177.18 5.40 5 -3 0 182.98 7.10 -5 3 0 177.08 6.40 -5 3 0 172.58 8.20 -5 3 0 194.78 5.50 -5 3 0 179.38 5.30 4 -3 0 10.20 1.20 4 -3 0 10.50 2.00 -4 3 0 12.20 1.20 -4 3 0 10.00 2.50 -4 3 0 9.20 1.00 -4 3 0 11.70 1.50 3 -3 0 226.08 6.40 3 -3 0 232.38 7.40 -3 3 0 226.68 6.40 -3 3 0 236.78 8.00 -3 3 0 242.28 6.50 -3 3 0 230.38 6.80 -3 3 0 221.38 6.10 2 -3 0 453.05 12.10 2 -3 0 442.86 12.40 -2 3 0 467.45 11.80 -2 3 0 447.16 12.10 -2 3 0 445.26 11.70 -2 3 0 424.76 13.20 -2 3 0 435.56 11.80 1 -3 0 554.64 14.70 1 -3 0 534.95 14.40 1 -3 0 546.85 14.80 -1 3 0 567.74 14.70 -1 3 0 549.45 14.50 -1 3 0 581.94 15.00 -1 3 0 534.55 14.40 0 -3 0 838.12 21.50 0 -3 0 799.32 21.40 0 3 0 843.52 21.40 0 3 0 819.02 21.60 0 3 0 844.32 21.60 -1 -3 0 89.39 2.60 1 3 0 91.49 2.60 1 3 0 91.89 2.60 1 3 0 90.99 2.70 -2 -3 0 126.29 3.50 -2 -3 0 125.19 3.40 2 3 0 125.19 3.40 2 3 0 122.99 4.10 2 3 0 127.39 3.40 2 3 0 119.69 3.60 -3 -3 0 3.10 0.90 3 3 0 4.00 0.60 3 3 0 2.70 0.40 3 3 0 3.70 0.80 -4 -3 0 131.69 3.90 -4 -3 0 135.39 4.90 -4 -3 0 135.79 3.60 4 3 0 131.89 4.20 4 3 0 132.19 3.60 4 3 0 126.69 5.40 4 3 0 131.99 3.90 -5 -3 0 7.10 0.90 -5 -3 0 7.90 0.60 -5 -3 0 7.10 1.60 5 3 0 8.80 1.00 5 3 0 10.20 1.40 5 3 0 7.30 0.60 5 3 0 7.00 2.40 -6 -3 0 4.40 0.80 -6 -3 0 1.00 1.50 -6 -3 0 2.90 0.50 6 3 0 6.80 2.70 6 3 0 3.40 1.00 6 3 0 2.50 1.20 -7 -3 0 23.20 3.70 -7 -3 0 27.80 1.30 -7 -3 0 28.80 1.70 7 3 0 29.00 2.20 7 3 0 30.80 5.00 -8 -3 0 4.30 1.30 -8 -3 0 8.10 1.30 8 3 0 8.00 4.30 -9 -3 0 4.10 1.20 -9 -3 0 1.80 0.70 -9 -3 0 2.30 0.90 9 3 0 0.10 4.30 -10 -3 0 3.50 0.80 -10 -3 0 3.00 1.40 10 3 0 5.30 2.60 10 3 0 0.80 5.40 -11 -3 0 4.30 1.90 11 3 0 16.70 10.00 11 3 0 3.10 3.10 9 -4 0 -8.00 6.40 -9 4 0 -0.30 1.60 -9 4 0 -0.90 1.50 8 -4 0 10.60 5.70 -8 4 0 7.00 1.50 -8 4 0 10.80 1.70 7 -4 0 24.40 5.80 -7 4 0 12.80 2.10 -7 4 0 14.00 1.60 -7 4 0 17.90 1.90 6 -4 0 0.40 2.70 -6 4 0 1.20 0.90 -6 4 0 2.70 1.50 5 -4 0 -0.60 2.00 5 -4 0 -0.30 1.10 -5 4 0 0.10 1.30 -5 4 0 0.40 0.80 -5 4 0 1.30 1.90 4 -4 0 13.60 2.40 4 -4 0 17.20 1.60 -4 4 0 14.10 2.90 -4 4 0 15.70 1.60 -4 4 0 16.80 1.30 3 -4 0 35.60 2.40 3 -4 0 35.40 1.70 -3 4 0 38.40 3.50 -3 4 0 32.00 2.10 -3 4 0 35.60 1.70 -3 4 0 34.90 1.40 -3 4 0 35.40 1.80 2 -4 0 35.40 2.10 -2 4 0 37.20 1.90 -2 4 0 39.10 1.70 -2 4 0 36.00 2.00 -2 4 0 37.30 2.90 -2 4 0 37.80 1.70 1 -4 0 218.18 6.10 1 -4 0 209.98 6.40 -1 4 0 219.38 6.10 -1 4 0 216.78 6.20 -1 4 0 210.38 6.20 -1 4 0 232.58 6.80 -1 4 0 224.98 6.40 0 -4 0 13.60 0.90 0 4 0 11.80 1.50 0 4 0 13.50 1.20 0 4 0 10.50 1.10 0 4 0 13.00 1.00 -1 -4 0 86.69 2.60 1 4 0 89.39 2.60 1 4 0 80.89 2.70 1 4 0 83.79 2.80 1 4 0 85.99 2.80 -2 -4 0 13.40 0.80 2 4 0 15.40 0.80 2 4 0 14.20 0.80 2 4 0 10.80 0.90 2 4 0 15.50 1.40 -3 -4 0 195.88 5.50 -3 -4 0 196.68 5.40 3 4 0 205.18 5.60 3 4 0 189.98 6.40 3 4 0 202.48 6.00 3 4 0 200.98 5.30 -4 -4 0 109.19 3.40 -4 -4 0 108.49 4.20 -4 -4 0 109.89 3.10 4 4 0 109.89 3.40 4 4 0 110.79 3.10 4 4 0 111.19 3.90 4 4 0 108.69 5.00 -5 -4 0 1.20 0.60 -5 -4 0 1.20 0.40 -5 -4 0 -0.30 1.10 5 4 0 1.10 0.30 5 4 0 1.90 0.90 5 4 0 1.10 1.10 5 4 0 3.80 2.50 -6 -4 0 11.60 2.20 -6 -4 0 13.40 1.20 -6 -4 0 12.50 0.90 6 4 0 13.80 0.80 6 4 0 15.20 3.30 6 4 0 13.20 1.50 6 4 0 13.90 1.80 -7 -4 0 19.20 1.10 -7 -4 0 18.60 3.70 -7 -4 0 21.50 1.60 7 4 0 22.80 4.40 7 4 0 19.10 2.50 -8 -4 0 11.90 1.60 -8 -4 0 10.20 1.10 8 4 0 11.90 4.70 -9 -4 0 6.50 1.50 -9 -4 0 6.90 0.90 9 4 0 7.80 4.20 -10 -4 0 1.20 1.50 -10 -4 0 0.70 0.80 10 4 0 -1.10 5.30 10 4 0 -0.50 2.70 -11 -4 0 3.00 1.80 11 4 0 18.50 10.70 11 4 0 3.60 3.70 8 -5 0 3.90 5.40 -8 5 0 -0.60 1.40 -8 5 0 -0.40 1.60 7 -5 0 5.10 4.30 -7 5 0 3.20 1.30 6 -5 0 23.00 4.60 -6 5 0 26.40 1.90 -6 5 0 28.10 3.30 5 -5 0 32.60 2.30 5 -5 0 35.40 3.70 -5 5 0 35.80 2.00 -5 5 0 36.20 3.00 4 -5 0 2.20 1.60 -4 5 0 2.40 2.70 -4 5 0 2.20 1.20 -4 5 0 3.80 1.00 3 -5 0 1.90 1.40 -3 5 0 2.20 2.10 -3 5 0 2.90 1.00 -3 5 0 3.30 1.00 -3 5 0 3.20 1.30 -3 5 0 3.30 1.10 2 -5 0 -1.00 0.80 -2 5 0 -0.90 0.70 -2 5 0 0.30 0.80 -2 5 0 0.70 0.70 -2 5 0 0.10 1.20 -2 5 0 -0.60 1.60 1 -5 0 286.07 9.10 -1 5 0 310.77 8.80 -1 5 0 316.87 9.20 -1 5 0 303.97 8.50 0 -5 0 159.18 4.70 0 5 0 161.38 5.00 0 5 0 162.38 5.10 0 5 0 165.58 4.70 0 5 0 157.18 5.10 -1 -5 0 1.00 0.50 1 5 0 0.00 1.00 1 5 0 1.70 0.50 1 5 0 0.00 0.60 1 5 0 1.40 0.70 1 5 0 1.20 0.50 -2 -5 0 1.30 0.50 2 5 0 2.70 1.10 2 5 0 2.00 0.60 2 5 0 1.50 0.50 2 5 0 1.10 0.60 -3 -5 0 39.60 1.80 -3 -5 0 44.30 1.70 3 5 0 46.30 1.60 3 5 0 43.80 1.80 3 5 0 42.00 3.00 3 5 0 41.30 1.60 3 5 0 46.00 2.30 -4 -5 0 208.48 5.70 -4 -5 0 211.38 5.90 4 5 0 209.58 5.60 4 5 0 200.58 6.50 4 5 0 206.18 5.90 4 5 0 198.08 7.20 -5 -5 0 51.89 2.10 -5 -5 0 49.40 3.00 -5 -5 0 49.80 1.80 5 5 0 52.19 1.70 5 5 0 50.59 2.30 5 5 0 54.69 2.80 5 5 0 58.19 4.70 -6 -5 0 0.10 1.60 -6 -5 0 0.10 0.50 -6 -5 0 0.80 0.80 6 5 0 -0.20 0.40 6 5 0 3.70 3.00 -7 -5 0 5.10 1.10 -7 -5 0 3.80 0.70 7 5 0 3.30 0.60 7 5 0 7.50 3.70 -8 -5 0 4.80 0.70 -8 -5 0 4.90 1.40 8 5 0 8.00 4.60 -9 -5 0 6.70 0.70 -9 -5 0 6.40 1.40 9 5 0 4.40 4.50 10 5 0 -2.10 2.90 10 5 0 0.60 5.40 -11 -5 0 2.30 1.90 11 5 0 10.80 9.60 11 5 0 1.80 4.00 8 -6 0 10.30 8.10 -8 6 0 1.90 1.70 -8 6 0 0.50 2.00 -7 6 0 9.00 1.80 6 -6 0 14.60 4.80 -6 6 0 8.60 1.60 -6 6 0 13.70 3.50 5 -6 0 22.50 3.80 -5 6 0 17.60 1.90 -5 6 0 17.50 2.50 4 -6 0 15.20 2.50 -4 6 0 13.00 1.10 -4 6 0 14.70 1.00 -4 6 0 15.50 4.10 -4 6 0 14.20 1.60 -4 6 0 16.60 2.10 3 -6 0 1.30 1.30 -3 6 0 1.20 1.00 -3 6 0 2.40 1.30 -3 6 0 3.00 2.50 -3 6 0 0.70 1.10 -3 6 0 1.10 1.40 2 -6 0 2.60 1.30 -2 6 0 2.10 1.40 -2 6 0 3.70 2.20 -2 6 0 3.00 1.20 -2 6 0 2.00 1.60 -2 6 0 1.00 1.10 1 -6 0 44.70 2.50 -1 6 0 41.80 2.20 -1 6 0 40.00 2.50 -1 6 0 42.20 2.70 -1 6 0 42.40 2.10 -1 6 0 44.50 3.10 0 -6 0 70.89 2.50 0 6 0 62.29 2.60 0 6 0 62.99 3.00 0 6 0 62.89 2.50 0 6 0 71.39 3.20 0 6 0 61.49 2.30 0 6 0 65.49 2.90 -1 -6 0 5.60 0.80 1 6 0 5.00 1.00 1 6 0 6.20 0.90 1 6 0 7.00 1.20 1 6 0 7.80 1.00 1 6 0 7.10 1.70 -2 -6 0 5.10 0.80 2 6 0 4.30 1.80 2 6 0 5.70 0.80 2 6 0 4.80 0.90 2 6 0 5.20 0.90 2 6 0 6.80 1.50 2 6 0 5.70 1.00 -3 -6 0 8.20 1.00 3 6 0 9.30 1.30 3 6 0 12.80 2.20 3 6 0 13.90 2.00 3 6 0 9.00 1.20 3 6 0 9.00 1.10 -4 -6 0 9.40 1.00 -4 -6 0 11.40 1.10 4 6 0 15.30 2.90 4 6 0 8.90 1.00 -5 -6 0 21.20 1.40 -5 -6 0 20.70 1.20 5 6 0 21.90 1.20 5 6 0 30.60 4.50 -6 -6 0 19.80 1.80 -6 -6 0 27.50 1.70 6 6 0 34.60 5.50 6 6 0 22.90 1.40 -7 -6 0 19.50 1.70 -7 -6 0 17.80 1.20 7 6 0 15.60 1.10 7 6 0 20.20 4.50 -8 -6 0 2.50 1.30 -8 -6 0 2.30 0.70 8 6 0 4.70 4.40 -9 -6 0 1.10 1.30 9 6 0 0.60 3.10 9 6 0 6.70 5.40 -10 -6 0 4.20 1.80 10 6 0 6.10 3.70 10 6 0 5.90 5.30 -7 7 0 2.10 1.80 6 -7 0 7.00 4.30 -6 7 0 7.70 1.80 5 -7 0 3.50 3.10 -5 7 0 3.20 1.50 -5 7 0 5.00 2.40 4 -7 0 4.40 2.30 -4 7 0 4.60 1.00 -4 7 0 5.90 1.20 -4 7 0 5.80 1.50 -4 7 0 5.80 2.00 3 -7 0 0.30 1.50 -3 7 0 5.60 3.40 -3 7 0 3.00 1.50 -3 7 0 1.30 1.30 -3 7 0 1.20 1.60 -3 7 0 1.00 1.20 2 -7 0 9.90 2.10 -2 7 0 11.40 2.20 -2 7 0 10.80 1.70 -2 7 0 13.50 2.90 -2 7 0 9.00 1.80 -2 7 0 14.10 1.80 -1 7 0 14.70 1.80 -1 7 0 13.90 1.90 -1 7 0 15.60 1.90 -1 7 0 17.90 2.40 0 7 0 1.60 1.20 0 7 0 2.40 1.40 0 7 0 2.10 1.10 0 7 0 2.40 1.30 0 7 0 6.20 1.90 -1 -7 0 14.50 1.30 1 7 0 17.10 1.90 1 7 0 15.50 2.00 1 7 0 18.50 2.60 1 7 0 16.80 1.70 1 7 0 16.00 1.80 -2 -7 0 0.80 0.70 2 7 0 2.20 1.00 2 7 0 3.20 1.50 2 7 0 1.90 1.00 2 7 0 -0.50 1.60 2 7 0 1.30 0.90 2 7 0 1.30 1.60 2 7 0 1.70 0.90 -3 -7 0 1.00 0.70 3 7 0 1.30 0.80 3 7 0 1.60 1.00 3 7 0 1.30 0.90 3 7 0 2.30 1.50 3 7 0 0.50 2.00 -4 -7 0 14.40 1.20 4 7 0 16.40 2.80 4 7 0 14.30 1.00 4 7 0 13.80 1.30 4 7 0 14.90 1.40 4 7 0 17.60 3.10 -5 -7 0 1.40 0.70 5 7 0 2.00 0.80 5 7 0 4.00 2.80 -6 -7 0 6.20 1.20 -6 -7 0 5.60 0.80 6 7 0 4.00 0.90 6 7 0 8.80 3.80 -7 -7 0 1.90 1.10 -7 -7 0 2.50 0.80 7 7 0 3.10 3.90 7 7 0 0.60 2.80 7 7 0 2.00 0.80 -8 -7 0 7.00 0.90 -8 -7 0 7.50 1.50 8 7 0 5.60 3.30 8 7 0 10.90 5.20 -9 -7 0 2.00 2.00 9 7 0 2.00 3.60 9 7 0 4.40 5.20 -10 -7 0 -0.40 1.70 10 7 0 -0.80 4.20 10 7 0 4.10 8.20 6 -8 0 21.40 5.50 -6 8 0 14.40 2.30 5 -8 0 8.60 3.70 -5 8 0 1.90 1.80 4 -8 0 3.50 2.60 -4 8 0 3.50 1.70 -4 8 0 4.00 1.50 3 -8 0 2.80 2.00 -3 8 0 5.70 2.00 -3 8 0 2.70 1.60 -3 8 0 1.60 1.60 -3 8 0 2.60 1.90 2 -8 0 -0.10 1.40 -2 8 0 -2.00 2.10 -2 8 0 0.30 1.50 -2 8 0 -0.10 1.70 -2 8 0 0.20 1.70 -1 8 0 41.80 2.90 -1 8 0 43.30 2.90 -1 8 0 44.40 3.20 -1 8 0 44.10 3.70 0 8 0 32.70 2.50 0 8 0 35.20 3.70 0 8 0 29.00 2.70 0 8 0 36.70 3.20 1 8 0 4.00 1.50 1 8 0 2.10 1.20 1 8 0 5.00 2.30 -2 -8 0 21.10 1.70 2 8 0 24.80 2.30 2 8 0 26.00 2.30 2 8 0 24.30 3.40 2 8 0 24.50 2.70 2 8 0 26.90 2.30 -3 -8 0 -0.80 0.70 3 8 0 0.80 1.20 3 8 0 0.00 1.10 3 8 0 -0.40 1.00 3 8 0 -1.40 2.10 3 8 0 0.50 1.70 -4 -8 0 10.50 1.30 4 8 0 9.40 2.00 4 8 0 8.10 1.20 4 8 0 7.20 1.00 4 8 0 7.80 2.80 4 8 0 8.50 1.20 4 8 0 10.10 2.60 -5 -8 0 2.30 0.80 5 8 0 2.40 1.00 5 8 0 -0.20 2.20 5 8 0 5.30 3.20 -6 -8 0 3.00 0.90 6 8 0 -0.10 2.90 6 8 0 4.90 3.90 6 8 0 2.40 1.10 -7 -8 0 1.70 0.70 7 8 0 2.70 3.00 7 8 0 2.30 4.30 8 8 0 3.90 5.00 8 8 0 2.20 3.90 -9 -8 0 1.00 1.70 9 8 0 1.20 4.00 9 8 0 2.30 5.90 5 -9 0 6.60 4.10 -5 9 0 6.00 3.00 4 -9 0 11.00 3.30 -4 9 0 5.90 2.10 -3 9 0 6.70 2.10 -3 9 0 6.90 2.10 -2 9 0 3.70 2.60 -2 9 0 3.40 2.00 -1 9 0 5.40 2.10 -1 9 0 4.80 3.00 0 9 0 5.20 1.90 0 9 0 10.40 3.30 0 9 0 6.40 1.80 1 9 0 5.00 1.70 1 9 0 5.10 1.60 1 9 0 3.90 1.80 1 9 0 7.20 3.10 2 9 0 3.80 1.80 2 9 0 4.50 1.50 2 9 0 4.90 3.10 3 9 0 9.10 1.60 3 9 0 17.20 3.60 3 9 0 11.10 2.50 -4 -9 0 5.60 1.20 4 9 0 3.30 1.40 4 9 0 4.30 3.10 4 9 0 5.80 1.80 4 9 0 4.30 0.90 4 9 0 5.90 2.70 -5 -9 0 1.70 0.90 5 9 0 0.10 2.80 5 9 0 0.20 2.50 5 9 0 -2.30 3.50 -6 -9 0 12.70 1.50 6 9 0 6.00 3.20 6 9 0 8.70 4.60 7 9 0 15.10 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6.90 4.00 -6 7 3 3.30 1.40 5 -7 -3 8.50 3.30 -5 7 3 9.40 2.70 -5 7 3 8.60 1.50 4 -7 -3 9.30 2.70 -4 7 3 9.50 1.90 -4 7 3 9.40 1.40 3 -7 -3 -0.20 1.60 -3 7 3 0.80 1.30 -3 7 3 1.40 1.10 -3 7 3 1.50 0.90 -3 7 3 0.20 1.50 2 -7 -3 55.49 3.40 -2 7 3 51.39 2.50 -2 7 3 49.90 3.00 -2 7 3 50.39 2.40 -2 7 3 53.19 3.10 -1 7 3 32.70 2.50 -1 7 3 35.90 2.20 -1 7 3 33.80 2.60 -1 7 3 33.00 1.80 -1 7 3 36.40 2.10 -1 7 3 37.70 3.20 0 7 3 14.30 2.20 0 7 3 11.60 1.70 0 7 3 14.70 2.10 0 7 3 13.40 1.70 0 7 3 13.90 1.70 0 7 3 13.30 1.40 1 7 3 24.50 1.60 1 7 3 24.60 2.20 1 7 3 22.80 2.00 1 7 3 24.50 1.70 1 7 3 25.20 2.20 2 7 3 14.60 2.10 2 7 3 10.60 1.30 2 7 3 10.00 1.80 2 7 3 10.10 1.30 2 7 3 12.10 2.00 2 7 3 7.50 1.10 3 7 3 27.50 1.70 3 7 3 28.50 1.50 3 7 3 27.70 2.30 3 7 3 28.10 2.30 3 7 3 22.70 2.70 3 7 3 28.20 2.80 3 7 3 26.90 1.50 4 7 3 24.20 3.00 4 7 3 20.90 1.50 4 7 3 22.60 1.10 4 7 3 22.00 1.30 -5 -7 -3 33.70 1.80 5 7 3 36.00 4.10 5 7 3 32.80 1.50 -6 -7 -3 10.90 1.50 6 7 3 11.70 3.40 6 7 3 8.00 0.90 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31.90 1.90 2 7 -4 1.70 2.20 2 7 -4 0.60 1.10 -2 -7 4 -0.80 0.80 1 7 -4 103.19 4.10 1 7 -4 109.69 4.20 1 7 -4 114.89 5.20 -1 -7 4 115.89 3.90 0 7 -4 96.69 4.80 0 7 -4 93.99 3.80 0 7 -4 92.29 4.00 0 -7 4 99.19 3.60 0 -7 4 103.69 3.90 -1 7 -4 25.50 3.10 -1 7 -4 20.50 3.40 -1 7 -4 19.50 2.50 -1 7 -4 22.00 2.30 1 -7 4 19.70 2.10 1 -7 4 22.20 1.80 -2 7 -4 -0.80 2.90 -2 7 -4 3.80 1.80 -2 7 -4 3.10 2.10 -2 7 -4 3.10 1.50 2 -7 4 1.80 1.20 2 -7 4 1.70 1.10 2 -7 4 1.50 1.30 -3 7 -4 1.40 1.90 -3 7 -4 0.60 1.60 -3 7 -4 0.10 1.40 3 -7 4 1.00 1.40 -4 7 -4 1.70 1.40 -4 7 -4 1.40 1.50 -4 7 -4 1.30 2.10 4 -7 4 0.50 1.90 -5 7 -4 -0.60 1.50 -5 7 -4 0.70 1.10 5 -7 4 1.30 2.90 -6 7 -4 1.40 1.80 6 -7 4 9.30 4.90 -7 7 -4 3.30 2.10 7 -7 4 17.50 6.50 10 6 -4 22.10 9.50 10 6 -4 -1.20 4.90 9 6 -4 6.50 6.40 9 6 -4 4.00 3.50 -9 -6 4 0.60 1.50 -9 -6 4 1.90 0.90 8 6 -4 3.80 3.10 8 6 -4 4.40 4.90 -8 -6 4 3.80 0.90 -8 -6 4 5.00 1.30 7 6 -4 4.30 2.80 7 6 -4 3.10 3.40 7 6 -4 3.50 1.00 -7 -6 4 4.20 1.20 -7 -6 4 4.10 0.90 6 6 -4 0.20 0.80 6 6 -4 -0.20 2.80 6 6 -4 0.30 2.30 -6 -6 4 -0.40 0.70 -6 -6 4 1.40 1.70 5 6 -4 0.60 2.50 5 6 -4 1.10 0.80 5 6 -4 0.50 1.90 -5 -6 4 0.00 0.70 4 6 -4 58.89 3.70 4 6 -4 63.19 2.30 -4 -6 4 60.49 2.40 3 6 -4 27.60 1.70 3 6 -4 30.50 1.60 3 6 -4 30.10 3.00 3 6 -4 30.50 1.70 -3 -6 4 30.40 1.70 2 6 -4 2.10 0.90 2 6 -4 4.10 1.90 2 6 -4 0.40 0.80 2 6 -4 1.00 1.00 -2 -6 4 0.50 0.60 -2 -6 4 -0.30 0.60 1 6 -4 47.90 2.20 1 6 -4 51.29 3.40 1 6 -4 49.00 2.50 1 6 -4 46.60 2.10 -1 -6 4 51.09 2.30 -1 -6 4 49.70 2.10 0 6 -4 4.30 1.40 0 6 -4 6.40 2.10 0 6 -4 3.00 1.10 0 6 -4 3.90 0.90 0 -6 4 3.10 0.90 0 -6 4 4.40 0.90 -1 6 -4 206.28 7.00 -1 6 -4 205.28 7.10 -1 6 -4 207.28 6.40 1 -6 4 212.08 6.60 1 -6 4 210.78 6.30 -2 6 -4 59.29 3.40 -2 6 -4 56.19 2.70 -2 6 -4 50.49 4.30 2 -6 4 56.79 2.50 2 -6 4 54.29 2.90 2 -6 4 56.09 2.90 -3 6 -4 -0.80 1.30 -3 6 -4 -0.40 1.20 -3 6 -4 -0.20 1.20 -3 6 -4 -4.40 2.70 3 -6 4 -2.10 1.90 3 -6 4 -1.80 1.30 -4 6 -4 5.40 1.40 -4 6 -4 2.60 1.40 -4 6 -4 -0.30 3.80 -4 6 -4 4.90 1.30 4 -6 4 4.20 1.50 4 -6 4 3.10 2.20 -5 6 -4 1.20 1.60 -5 6 -4 -0.50 1.20 5 -6 4 -1.20 2.30 -6 6 -4 4.70 1.60 6 -6 4 3.70 3.50 -7 6 -4 9.20 1.90 7 -6 4 17.10 5.70 -8 6 -4 1.80 2.00 8 -6 4 0.00 7.60 10 5 -4 5.50 3.90 -10 -5 4 5.80 1.90 -10 -5 4 6.60 1.10 9 5 -4 1.30 3.20 9 5 -4 -2.40 6.70 -9 -5 4 1.40 0.80 -9 -5 4 -0.10 1.20 8 5 -4 11.70 4.60 8 5 -4 9.50 1.30 8 5 -4 12.00 2.90 -8 -5 4 13.00 1.70 -8 -5 4 12.20 1.40 7 5 -4 1.50 2.30 7 5 -4 -2.90 2.90 7 5 -4 0.00 0.80 -7 -5 4 0.20 0.80 -7 -5 4 0.30 0.70 6 5 -4 -0.80 2.60 6 5 -4 0.00 1.80 6 5 -4 0.20 0.70 -6 -5 4 1.00 0.80 -6 -5 4 0.10 1.60 -6 -5 4 0.30 0.70 5 5 -4 97.29 5.40 5 5 -4 89.59 3.40 5 5 -4 98.19 3.00 -5 -5 4 93.59 4.10 -5 -5 4 97.99 3.20 -5 -5 4 99.79 3.10 4 5 -4 0.00 0.80 4 5 -4 0.20 0.60 4 5 -4 2.00 2.50 4 5 -4 0.40 1.70 -4 -5 4 0.10 0.60 3 5 -4 60.19 2.20 3 5 -4 61.39 2.10 3 5 -4 58.89 3.30 3 5 -4 65.49 3.60 3 5 -4 63.49 2.30 -3 -5 4 57.89 2.20 -3 -5 4 63.39 2.10 2 5 -4 34.00 1.60 2 5 -4 31.10 2.50 2 5 -4 33.30 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16.40 2.70 -5 -6 -4 101.29 3.50 5 6 4 99.79 3.00 5 6 4 124.69 4.40 5 6 4 105.69 5.70 -6 -6 -4 -0.10 0.90 6 6 4 2.10 2.80 -7 -6 -4 6.60 1.20 7 6 4 10.00 4.40 -8 -6 -4 1.80 1.20 8 6 4 5.00 4.50 -9 -6 -4 7.70 1.60 9 6 4 9.40 5.10 -10 -6 -4 2.60 1.60 10 6 4 5.60 6.60 7 -7 -4 10.60 6.00 -7 7 4 3.50 1.60 -7 7 4 0.40 1.80 6 -7 -4 -2.80 4.40 -6 7 4 0.80 1.30 5 -7 -4 24.00 4.50 -5 7 4 19.60 3.20 -5 7 4 19.40 1.90 4 -7 -4 27.90 4.00 -4 7 4 19.30 1.80 -4 7 4 24.20 3.20 3 -7 -4 11.60 2.60 -3 7 4 11.70 1.50 -3 7 4 9.60 1.90 -3 7 4 8.50 1.00 -3 7 4 11.60 1.60 2 -7 -4 117.99 5.10 -2 7 4 117.09 4.70 -2 7 4 110.09 3.90 -2 7 4 109.89 3.70 -2 7 4 108.59 4.20 -1 7 4 7.50 1.10 -1 7 4 8.70 2.20 -1 7 4 6.30 1.70 -1 7 4 7.70 1.40 -1 7 4 6.70 1.40 -1 7 4 5.40 1.40 0 7 4 130.29 5.50 0 7 4 131.99 4.40 0 7 4 131.59 4.50 0 7 4 132.99 4.30 0 7 4 127.89 4.00 0 7 4 130.99 5.20 1 7 4 0.50 1.40 1 7 4 -0.10 0.80 1 7 4 -0.10 0.80 1 7 4 -0.10 1.10 1 7 4 1.70 0.90 2 7 4 19.40 1.40 2 7 4 18.10 1.60 2 7 4 19.90 2.10 2 7 4 18.60 1.50 2 7 4 18.20 1.50 2 7 4 18.80 2.20 3 7 4 69.09 3.10 3 7 4 58.79 3.20 3 7 4 59.49 2.30 3 7 4 60.79 3.70 3 7 4 60.09 2.30 3 7 4 57.39 2.50 -4 -7 -4 9.40 1.10 4 7 4 10.50 2.20 4 7 4 9.00 0.90 4 7 4 7.80 1.20 4 7 4 8.60 0.90 -5 -7 -4 26.90 1.70 5 7 4 21.20 1.50 5 7 4 26.50 4.00 -6 -7 -4 9.90 1.40 6 7 4 8.20 0.70 6 7 4 7.90 3.20 -7 -7 -4 19.70 1.90 7 7 4 21.10 4.50 -8 -7 -4 1.80 1.30 8 7 4 5.30 4.90 9 7 4 2.10 6.00 -10 -7 -4 0.40 1.70 10 7 4 4.90 7.10 6 -8 -4 5.30 5.10 -6 8 4 2.80 2.00 -6 8 4 5.50 1.70 5 -8 -4 0.60 3.30 -5 8 4 1.20 1.40 4 -8 -4 -2.10 2.50 -4 8 4 0.60 1.30 3 -8 -4 1.50 2.10 -3 8 4 5.30 1.80 -3 8 4 1.20 1.40 -3 8 4 0.80 2.00 2 -8 -4 25.10 3.30 -2 8 4 24.00 2.00 -2 8 4 26.90 2.90 -2 8 4 26.40 2.20 -2 8 4 19.80 2.80 -1 8 4 39.00 3.00 -1 8 4 43.40 4.30 -1 8 4 38.60 3.10 -1 8 4 40.00 2.60 -1 8 4 37.40 2.60 0 8 4 2.50 1.90 0 8 4 6.60 1.90 0 8 4 1.60 1.70 0 8 4 3.00 1.30 0 8 4 2.50 1.40 1 8 4 18.80 2.80 1 8 4 16.40 2.10 1 8 4 18.00 2.60 1 8 4 20.00 2.70 2 8 4 11.80 1.50 2 8 4 13.80 2.30 2 8 4 12.10 2.30 2 8 4 10.60 1.30 2 8 4 9.80 1.50 3 8 4 18.00 2.60 3 8 4 19.20 1.70 3 8 4 19.80 2.90 3 8 4 19.60 1.80 3 8 4 17.70 1.50 4 8 4 14.10 2.60 4 8 4 13.50 1.10 4 8 4 13.30 1.40 4 8 4 16.00 1.60 4 8 4 14.70 2.50 5 8 4 -0.20 2.30 5 8 4 0.70 0.80 -6 -8 -4 8.80 1.40 6 8 4 10.70 3.80 -7 -8 -4 13.50 1.90 7 8 4 15.20 5.10 -8 -8 -4 5.90 1.50 8 8 4 5.10 5.70 -9 -8 -4 1.40 1.60 9 8 4 1.10 6.00 5 -9 -4 21.00 9.00 -5 9 4 9.30 2.10 -5 9 4 7.00 2.30 4 -9 -4 3.30 3.70 -4 9 4 3.50 1.80 3 -9 -4 -1.00 2.70 -3 9 4 1.90 1.80 -3 9 4 2.20 1.80 -2 9 4 0.10 2.20 -2 9 4 1.80 1.70 -1 9 4 7.60 2.60 -1 9 4 8.60 2.30 -1 9 4 9.90 2.40 -1 9 4 6.30 1.90 0 9 4 18.40 2.50 0 9 4 21.40 2.80 0 9 4 24.40 3.20 1 9 4 5.40 2.70 1 9 4 7.10 2.40 1 9 4 6.20 1.50 2 9 4 2.90 1.20 2 9 4 2.30 3.00 2 9 4 5.20 1.90 2 9 4 3.60 1.40 3 9 4 1.00 0.90 3 9 4 1.40 1.90 3 9 4 2.20 1.50 3 9 4 3.20 1.20 4 9 4 10.00 2.70 4 9 4 9.80 1.40 4 9 4 9.50 1.40 4 9 4 8.70 1.30 5 9 4 -1.40 2.70 5 9 4 -1.10 1.00 6 9 4 1.20 3.60 7 9 4 -1.90 4.70 -8 -9 -4 1.90 1.60 8 9 4 1.30 5.70 -9 -9 -4 1.40 1.90 9 9 4 -0.70 6.80 -3 10 4 10.00 2.50 -2 10 4 7.50 2.90 -2 10 4 6.80 2.30 -1 10 4 -1.90 2.10 -1 10 4 -3.40 3.00 0 10 4 1.80 2.00 0 10 4 5.30 2.00 0 10 4 1.40 3.20 1 10 4 1.70 2.00 1 10 4 5.50 1.90 1 10 4 3.20 1.60 1 10 4 4.40 3.50 2 10 4 4.90 2.20 2 10 4 5.10 1.50 2 10 4 7.20 3.70 2 10 4 6.20 1.70 3 10 4 11.90 1.90 3 10 4 10.10 2.80 3 10 4 17.20 4.30 3 10 4 9.40 1.40 4 10 4 3.60 1.50 4 10 4 0.90 1.00 4 10 4 -2.00 3.90 4 10 4 0.00 2.60 5 10 4 -2.10 3.20 5 10 4 -2.40 3.30 6 10 4 -3.10 3.20 6 10 4 -2.30 4.20 7 10 4 -4.40 5.30 7 10 4 1.90 3.50 -1 11 4 9.40 4.20 0 11 4 0.80 2.60 0 11 4 -1.20 4.50 0 11 4 1.70 2.10 1 11 4 2.80 2.20 1 11 4 1.60 2.60 1 11 4 0.10 2.50 1 11 4 -2.00 4.40 1 11 4 0.70 1.90 2 11 4 -5.30 4.50 2 11 4 -0.10 1.50 2 11 4 4.40 2.20 2 11 4 -0.10 2.60 2 11 4 1.50 2.40 3 11 4 2.60 3.10 3 11 4 2.40 1.60 3 11 4 4.90 2.10 3 11 4 9.70 5.60 4 11 4 8.00 5.80 4 11 4 -1.30 3.30 4 11 4 1.20 1.30 5 11 4 3.20 5.70 5 11 4 -5.20 3.90 6 11 4 4.00 6.20 6 10 -5 -4.70 5.10 -6 -10 5 -0.10 1.60 5 10 -5 1.40 5.60 -5 -10 5 4.00 1.60 4 10 -5 1.10 5.00 -4 -10 5 1.90 1.60 3 10 -5 -0.60 11.00 3 10 -5 3.10 2.30 3 10 -5 -1.10 1.90 -3 -10 5 4.30 1.70 2 10 -5 -4.90 2.10 2 10 -5 1.90 2.30 2 10 -5 -1.00 4.90 -2 -10 5 1.20 1.50 1 10 -5 -1.00 5.00 1 10 -5 -0.80 2.20 -1 -10 5 0.80 1.70 0 10 -5 1.20 2.40 0 10 -5 -5.90 2.50 0 10 -5 -4.70 4.80 -1 10 -5 12.10 4.80 -1 10 -5 8.50 2.80 -2 10 -5 5.30 3.80 -2 10 -5 2.80 2.70 6 9 -5 3.90 4.30 -6 -9 5 4.40 1.50 5 9 -5 5.90 4.30 -5 -9 5 4.70 1.50 4 9 -5 1.00 4.00 4 9 -5 -1.00 1.20 -4 -9 5 1.00 1.20 3 9 -5 4.60 3.90 -3 -9 5 3.20 1.30 2 9 -5 -2.70 1.70 2 9 -5 0.10 1.80 2 9 -5 -0.50 3.60 -2 -9 5 0.80 1.20 1 9 -5 6.10 1.90 1 9 -5 10.90 4.20 1 9 -5 2.80 1.90 -1 -9 5 5.40 1.50 0 9 -5 6.90 2.20 0 9 -5 12.50 4.20 0 9 -5 11.80 2.40 0 -9 5 11.40 1.80 -1 9 -5 -0.90 3.50 -1 9 -5 -0.90 2.00 -1 9 -5 -1.20 2.30 -2 9 -5 3.20 3.10 -2 9 -5 1.50 2.10 -3 9 -5 3.40 2.50 -4 9 -5 -2.50 2.30 -4 9 -5 3.00 1.90 4 -9 5 2.00 2.20 8 8 -5 1.50 4.50 -8 -8 5 0.70 1.10 7 8 -5 5.80 3.20 -7 -8 5 1.90 1.10 6 8 -5 6.80 3.20 6 8 -5 4.20 3.50 -6 -8 5 2.80 1.10 5 8 -5 -0.20 3.10 -5 -8 5 2.50 1.10 4 8 -5 12.30 1.70 4 8 -5 20.50 4.00 -4 -8 5 17.80 1.90 3 8 -5 12.40 1.50 3 8 -5 16.50 3.70 -3 -8 5 15.20 1.80 2 8 -5 3.50 2.90 2 8 -5 0.30 1.60 -2 -8 5 0.70 1.00 1 8 -5 3.20 3.00 1 8 -5 2.50 1.50 1 8 -5 0.70 1.50 -1 -8 5 1.50 1.00 0 8 -5 2.40 1.60 0 8 -5 3.30 3.10 0 8 -5 1.70 1.50 0 -8 5 2.00 1.10 -1 8 -5 11.20 2.30 -1 8 -5 15.00 3.30 -1 8 -5 17.60 2.40 1 -8 5 11.70 1.80 -2 8 -5 0.70 1.60 -2 8 -5 1.90 2.20 -2 8 -5 2.20 2.60 -3 8 -5 1.40 2.00 -3 8 -5 -0.30 1.80 -3 8 -5 -0.90 1.80 3 -8 5 0.60 1.30 -4 8 -5 1.50 2.00 -4 8 -5 6.30 1.70 4 -8 5 3.10 1.90 -5 8 -5 2.70 1.30 -5 8 -5 -0.20 2.40 5 -8 5 5.80 3.00 9 7 -5 1.50 4.30 9 7 -5 15.50 7.90 -9 -7 5 2.90 1.10 8 7 -5 2.90 3.60 8 7 -5 10.70 5.40 -8 -7 5 6.10 1.10 7 7 -5 5.30 3.90 7 7 -5 1.50 3.30 -7 -7 5 2.20 1.00 6 7 -5 3.50 1.30 6 7 -5 4.40 3.00 6 7 -5 2.70 2.60 -6 -7 5 2.80 1.00 5 7 -5 0.80 2.30 5 7 -5 1.90 2.60 5 7 -5 -0.80 1.10 -5 -7 5 -1.10 0.80 4 7 -5 9.10 1.00 4 7 -5 11.60 2.70 -4 -7 5 9.10 1.20 3 7 -5 3.10 2.30 3 7 -5 2.00 0.90 3 7 -5 2.90 1.20 -3 -7 5 1.50 0.90 2 7 -5 22.30 2.10 2 7 -5 25.50 3.60 -2 -7 5 23.10 1.70 -2 -7 5 21.60 1.70 1 7 -5 109.79 5.30 1 7 -5 104.29 4.10 1 7 -5 103.89 4.10 -1 -7 5 109.99 3.80 -1 -7 5 113.29 4.10 0 7 -5 1.50 1.20 0 7 -5 -0.40 1.30 0 7 -5 2.50 2.30 0 -7 5 2.30 1.00 0 -7 5 1.00 1.10 -1 7 -5 91.69 4.10 -1 7 -5 90.39 3.90 -1 7 -5 88.09 4.90 1 -7 5 103.39 4.10 1 -7 5 97.59 3.60 -2 7 -5 -1.70 1.30 -2 7 -5 -0.30 1.40 -2 7 -5 0.10 2.10 -2 7 -5 -4.20 2.80 2 -7 5 -0.60 1.10 2 -7 5 -1.10 1.10 2 -7 5 0.30 1.00 -3 7 -5 0.30 1.70 -3 7 -5 1.20 1.50 -3 7 -5 1.90 1.80 3 -7 5 2.40 1.50 3 -7 5 1.80 1.40 -4 7 -5 4.20 2.00 -4 7 -5 7.60 1.80 -5 7 -5 1.00 1.00 -5 7 -5 0.60 1.60 5 -7 5 -1.10 2.80 -6 7 -5 9.50 2.30 6 -7 5 14.50 4.70 -7 7 -5 -1.00 2.00 7 -7 5 13.30 6.40 10 6 -5 20.40 9.60 10 6 -5 -1.80 4.70 -10 -6 5 1.80 1.80 9 6 -5 8.10 7.60 9 6 -5 -1.20 3.60 -9 -6 5 1.10 1.40 -9 -6 5 2.00 1.00 8 6 -5 4.80 5.00 8 6 -5 3.30 3.20 -8 -6 5 3.70 1.30 -8 -6 5 3.60 1.00 7 6 -5 2.60 2.70 7 6 -5 1.90 1.10 7 6 -5 2.00 3.80 -7 -6 5 1.10 0.90 -7 -6 5 3.40 1.10 6 6 -5 25.20 1.80 6 6 -5 29.20 3.80 6 6 -5 32.00 4.80 -6 -6 5 29.10 2.90 -6 -6 5 30.60 1.80 5 6 -5 19.80 3.10 5 6 -5 19.20 1.60 5 6 -5 17.00 2.70 -5 -6 5 18.50 1.50 4 6 -5 3.30 0.90 4 6 -5 3.00 2.20 4 6 -5 4.40 2.10 -4 -6 5 1.40 0.80 3 6 -5 5.90 0.90 3 6 -5 5.20 0.90 3 6 -5 5.30 1.90 -3 -6 5 5.20 0.80 -3 -6 5 5.90 1.00 2 6 -5 17.50 1.70 2 6 -5 24.80 1.60 2 6 -5 23.70 1.80 2 6 -5 26.80 3.10 -2 -6 5 22.10 1.50 -2 -6 5 26.10 1.60 1 6 -5 36.40 2.00 1 6 -5 35.70 2.20 1 6 -5 35.90 3.20 -1 -6 5 35.40 1.90 -1 -6 5 36.90 2.00 0 6 -5 168.58 6.20 0 6 -5 161.98 5.50 0 6 -5 185.18 5.60 0 6 -5 159.98 5.40 0 -6 5 174.98 5.50 0 -6 5 164.98 5.20 -1 6 -5 6.10 2.20 -1 6 -5 3.80 1.30 -1 6 -5 6.80 1.50 1 -6 5 3.40 0.90 1 -6 5 3.20 1.00 -2 6 -5 35.60 2.30 -2 6 -5 32.90 2.70 -2 6 -5 27.80 3.80 -2 6 -5 34.20 3.00 2 -6 5 35.70 2.20 2 -6 5 36.20 2.40 2 -6 5 33.80 2.00 -3 6 -5 22.90 4.60 -3 6 -5 35.60 2.60 -3 6 -5 36.40 2.40 -3 6 -5 33.00 2.90 3 -6 5 34.50 2.10 3 -6 5 36.40 2.60 3 -6 5 33.60 2.80 -4 6 -5 24.90 2.20 -4 6 -5 26.80 2.00 -4 6 -5 15.90 4.50 -4 6 -5 25.00 3.10 4 -6 5 20.50 3.30 4 -6 5 26.20 2.70 -5 6 -5 10.10 1.70 -5 6 -5 5.10 2.00 -5 6 -5 10.00 1.30 5 -6 5 12.00 3.10 5 -6 5 9.60 2.00 -6 6 -5 2.00 1.10 -6 6 -5 3.40 1.60 6 -6 5 -0.30 3.20 -7 6 -5 0.30 1.70 7 -6 5 0.20 4.80 10 5 -5 21.70 9.80 10 5 -5 3.00 4.10 -10 -5 5 4.00 1.10 -10 -5 5 2.60 1.60 9 5 -5 12.90 7.90 9 5 -5 8.20 3.60 -9 -5 5 5.30 1.40 -9 -5 5 6.40 1.10 8 5 -5 2.50 1.20 8 5 -5 4.00 5.10 8 5 -5 5.30 2.80 -8 -5 5 3.00 0.90 -8 -5 5 4.30 1.20 7 5 -5 -4.80 3.20 7 5 -5 0.90 0.90 7 5 -5 0.70 2.20 -7 -5 5 0.30 0.80 -7 -5 5 0.60 0.90 6 5 -5 0.30 0.70 6 5 -5 -1.90 2.60 6 5 -5 0.50 2.10 -6 -5 5 0.60 0.80 -6 -5 5 1.20 0.70 -6 -5 5 -0.10 1.70 5 5 -5 0.90 1.20 5 5 -5 0.50 0.70 5 5 -5 2.10 1.90 5 5 -5 0.50 2.30 -5 -5 5 1.60 1.30 -5 -5 5 0.50 0.70 4 5 -5 69.69 3.80 4 5 -5 69.99 2.70 4 5 -5 70.99 4.20 4 5 -5 73.69 2.50 -4 -5 5 72.89 2.60 3 5 -5 34.80 1.50 3 5 -5 32.00 1.70 3 5 -5 35.20 2.90 3 5 -5 36.10 1.60 -3 -5 5 30.80 1.60 -3 -5 5 33.40 1.50 2 5 -5 40.30 1.80 2 5 -5 41.80 1.90 2 5 -5 40.60 2.80 2 5 -5 39.50 1.70 -2 -5 5 41.00 1.80 -2 -5 5 38.80 1.80 1 5 -5 4.40 1.70 1 5 -5 1.40 0.80 1 5 -5 1.10 0.80 1 5 -5 2.00 0.70 -1 -5 5 0.70 0.60 -1 -5 5 0.60 0.60 0 5 -5 1.90 0.80 0 5 -5 3.20 1.70 0 5 -5 0.80 0.90 0 5 -5 2.50 1.10 0 -5 5 1.40 0.70 0 -5 5 0.10 0.70 -1 5 -5 208.48 6.90 -1 5 -5 211.88 6.60 -1 5 -5 213.08 6.40 -1 5 -5 220.28 6.30 1 -5 5 220.28 6.30 1 -5 5 223.28 6.70 1 -5 5 213.68 6.20 -2 5 -5 -0.10 1.80 -2 5 -5 0.40 1.50 -2 5 -5 0.30 0.80 -2 5 -5 -0.40 0.90 2 -5 5 -0.90 0.60 2 -5 5 -0.80 0.90 2 -5 5 -1.00 0.70 -3 5 -5 4.20 1.30 -3 5 -5 2.50 2.70 -3 5 -5 1.60 1.00 -3 5 -5 2.60 1.20 -3 5 -5 2.20 1.30 3 -5 5 0.80 1.10 3 -5 5 1.50 1.30 3 -5 5 2.00 0.90 -4 5 -5 9.50 1.30 -4 5 -5 6.30 1.80 -4 5 -5 1.20 3.30 -4 5 -5 6.50 1.30 4 -5 5 6.20 2.00 -5 5 -5 30.90 1.60 -5 5 -5 29.00 3.10 -5 5 -5 29.50 2.20 5 -5 5 29.60 2.70 5 -5 5 24.70 4.10 -6 5 -5 19.80 2.10 -6 5 -5 21.40 1.40 -6 5 -5 18.30 2.80 6 -5 5 21.20 2.80 -7 5 -5 1.90 1.40 7 -5 5 -3.20 4.50 -8 5 -5 0.10 1.70 8 -5 5 1.90 6.00 10 4 -5 7.80 9.60 10 4 -5 -2.80 3.50 -10 -4 5 1.10 1.00 -10 -4 5 -2.10 1.40 9 4 -5 3.80 2.90 9 4 -5 3.20 6.70 -9 -4 5 3.40 1.00 -9 -4 5 4.10 1.40 8 4 -5 19.40 3.20 8 4 -5 16.10 1.60 8 4 -5 17.60 5.20 -8 -4 5 13.70 1.60 -8 -4 5 16.00 1.50 7 4 -5 20.30 3.00 7 4 -5 13.20 1.50 7 4 -5 20.80 4.30 -7 -4 5 18.90 1.50 -7 -4 5 17.90 1.40 6 4 -5 29.80 4.60 6 4 -5 34.80 3.00 6 4 -5 34.80 1.60 6 4 -5 36.30 2.00 -6 -4 5 39.10 1.70 -6 -4 5 36.10 1.80 -6 -4 5 30.30 3.50 5 4 -5 -0.20 1.60 5 4 -5 0.60 0.60 5 4 -5 -0.70 0.80 -5 -4 5 -0.40 1.50 -5 -4 5 0.90 0.70 -5 -4 5 -0.10 0.60 4 4 -5 11.20 1.00 4 4 -5 11.00 2.30 4 4 -5 10.50 1.80 4 4 -5 12.30 1.20 -4 -4 5 10.70 1.00 -4 -4 5 9.50 2.10 -4 -4 5 10.70 1.10 3 4 -5 1.20 0.40 3 4 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2.70 1.00 3 7 -6 4.60 2.60 -3 -7 6 3.10 0.90 2 7 -6 0.10 2.30 2 7 -6 0.00 1.10 -2 -7 6 0.30 0.90 -2 -7 6 -0.10 0.80 1 7 -6 51.69 4.40 1 7 -6 50.69 3.10 1 7 -6 54.89 2.90 -1 -7 6 62.39 2.70 -1 -7 6 63.19 2.90 0 7 -6 48.60 2.90 0 7 -6 46.90 3.10 0 7 -6 46.30 4.40 0 -7 6 50.09 2.70 0 -7 6 47.50 2.50 -1 7 -6 3.30 2.60 -1 7 -6 4.00 1.80 -1 7 -6 2.30 1.50 1 -7 6 2.90 1.10 1 -7 6 3.30 1.20 -2 7 -6 -1.30 2.00 -2 7 -6 -1.40 1.30 -2 7 -6 -0.30 1.40 2 -7 6 0.40 1.00 2 -7 6 -0.10 1.00 2 -7 6 0.70 1.20 -3 7 -6 0.50 1.60 -3 7 -6 3.50 1.90 -3 7 -6 0.90 1.60 3 -7 6 1.20 1.20 3 -7 6 0.50 1.20 3 -7 6 5.30 1.60 -4 7 -6 13.30 1.90 -4 7 -6 11.80 2.10 4 -7 6 14.90 2.60 4 -7 6 12.70 2.30 -5 7 -6 5.90 2.00 -5 7 -6 7.30 1.40 5 -7 6 9.20 3.20 -6 7 -6 0.10 3.00 6 -7 6 2.10 4.20 9 6 -6 -1.40 4.10 9 6 -6 18.10 7.40 -9 -6 6 3.50 1.20 8 6 -6 7.90 3.70 8 6 -6 16.00 6.20 -8 -6 6 7.50 1.20 7 6 -6 5.90 2.90 7 6 -6 4.20 3.90 7 6 -6 3.80 1.30 -7 -6 6 3.50 2.60 -7 -6 6 6.40 1.20 6 6 -6 1.10 1.00 6 6 -6 1.20 2.60 6 6 -6 5.50 2.90 -6 -6 6 2.60 1.70 -6 -6 6 2.70 1.00 5 6 -6 5.50 1.10 5 6 -6 7.70 2.30 5 6 -6 5.20 2.40 -5 -6 6 6.80 1.00 4 6 -6 17.20 1.70 4 6 -6 19.30 1.20 4 6 -6 21.80 3.10 -4 -6 6 18.80 1.50 3 6 -6 16.80 1.40 3 6 -6 15.40 1.60 3 6 -6 21.50 3.20 -3 -6 6 16.80 1.50 -3 -6 6 16.80 1.30 2 6 -6 3.60 1.00 2 6 -6 5.70 2.40 2 6 -6 4.10 1.00 -2 -6 6 4.90 1.00 -2 -6 6 3.80 0.90 1 6 -6 7.40 1.20 1 6 -6 4.10 1.20 1 6 -6 5.90 1.10 1 6 -6 7.60 1.20 1 6 -6 12.80 2.60 -1 -6 6 7.70 1.00 -1 -6 6 6.50 1.10 0 6 -6 22.40 2.00 0 6 -6 22.20 1.90 0 6 -6 27.60 2.30 0 6 -6 25.50 3.40 0 -6 6 30.00 1.80 0 -6 6 28.10 2.00 -1 6 -6 201.08 7.10 -1 6 -6 198.98 6.60 -1 6 -6 192.38 6.30 1 -6 6 213.18 6.60 1 -6 6 200.68 6.10 -2 6 -6 67.79 3.70 -2 6 -6 67.59 3.50 -2 6 -6 63.89 3.00 2 -6 6 67.19 3.30 2 -6 6 66.99 2.80 2 -6 6 59.19 3.40 -3 6 -6 1.30 1.50 -3 6 -6 3.00 1.50 -3 6 -6 2.80 1.70 -3 6 -6 -3.50 2.80 3 -6 6 1.90 1.00 3 -6 6 0.40 1.40 3 -6 6 3.20 1.30 -4 6 -6 -0.80 1.90 -4 6 -6 -0.20 1.20 -4 6 -6 -0.30 1.20 4 -6 6 0.10 1.90 4 -6 6 0.40 1.40 -5 6 -6 8.00 1.70 -5 6 -6 10.30 2.50 -5 6 -6 10.90 1.40 5 -6 6 15.40 3.30 5 -6 6 6.90 1.80 -6 6 -6 2.70 1.60 -6 6 -6 2.70 1.20 6 -6 6 0.20 3.40 7 -6 6 2.30 4.80 10 5 -6 22.20 10.10 10 5 -6 -2.20 4.20 -10 -5 6 1.50 1.20 -10 -5 6 2.40 1.70 9 5 -6 3.90 3.50 9 5 -6 11.10 6.90 -9 -5 6 2.40 1.40 -9 -5 6 2.40 1.00 8 5 -6 8.60 3.10 8 5 -6 7.10 6.00 8 5 -6 7.30 1.50 -8 -5 6 8.00 1.20 -8 -5 6 7.30 1.40 7 5 -6 9.20 1.30 7 5 -6 9.50 2.80 7 5 -6 10.40 4.40 -7 -5 6 12.20 1.50 -7 -5 6 12.80 1.50 6 5 -6 3.70 0.90 6 5 -6 5.20 2.30 6 5 -6 6.70 3.10 -6 -5 6 6.30 1.10 -6 -5 6 6.50 1.00 -6 -5 6 4.40 2.00 5 5 -6 4.40 2.40 5 5 -6 7.20 1.00 5 5 -6 9.70 2.50 -5 -5 6 5.30 0.90 -5 -5 6 4.20 1.50 4 5 -6 34.80 2.00 4 5 -6 27.70 1.60 4 5 -6 31.00 3.10 -4 -5 6 31.50 1.60 -4 -5 6 26.30 1.90 3 5 -6 6.80 1.00 3 5 -6 10.80 2.30 3 5 -6 7.60 1.00 3 5 -6 7.40 0.90 -3 -5 6 6.50 0.90 -3 -5 6 6.50 0.90 2 5 -6 81.29 2.70 2 5 -6 74.79 3.90 2 5 -6 78.29 2.70 2 5 -6 74.89 2.70 -2 -5 6 82.09 2.90 -2 -5 6 79.69 2.80 1 5 -6 28.80 1.50 1 5 -6 29.20 1.90 1 5 -6 28.40 1.60 1 5 -6 30.70 2.80 -1 -5 6 28.70 1.70 -1 -5 6 26.80 1.60 0 5 -6 30.60 1.90 0 5 -6 29.60 2.00 0 5 -6 30.80 1.70 0 5 -6 31.10 2.90 0 -5 6 30.50 1.90 0 -5 6 29.40 1.60 -1 5 -6 20.10 1.80 -1 5 -6 20.90 2.10 -1 5 -6 27.30 2.80 1 -5 6 18.40 1.80 1 -5 6 17.90 1.40 -2 5 -6 3.20 1.10 -2 5 -6 3.40 1.70 -2 5 -6 2.70 1.10 -2 5 -6 2.70 1.20 -2 5 -6 4.80 2.00 2 -5 6 6.20 1.60 2 -5 6 3.90 1.20 2 -5 6 3.00 0.90 2 -5 6 4.30 1.20 -3 5 -6 278.37 8.30 -3 5 -6 246.38 9.30 -3 5 -6 269.87 8.20 -3 5 -6 282.97 8.60 3 -5 6 268.87 8.00 3 -5 6 290.27 8.60 3 -5 6 303.27 8.70 3 -5 6 288.27 8.40 -4 5 -6 43.20 3.10 -4 5 -6 42.80 2.20 -4 5 -6 41.50 2.40 4 -5 6 39.30 2.80 4 -5 6 41.60 2.70 4 -5 6 37.00 2.20 4 -5 6 39.20 3.50 -5 5 -6 8.40 2.10 -5 5 -6 7.80 1.20 -5 5 -6 11.10 1.70 5 -5 6 7.80 1.80 5 -5 6 11.70 3.30 -6 5 -6 3.80 1.10 -6 5 -6 1.20 2.00 -6 5 -6 1.50 1.40 6 -5 6 -0.30 1.40 6 -5 6 -3.80 3.80 -7 5 -6 2.60 1.60 7 -5 6 -6.30 5.90 -8 5 -6 10.00 3.70 8 -5 6 15.60 7.20 10 4 -6 11.10 8.80 10 4 -6 -4.00 3.50 -10 -4 6 -1.00 1.40 -10 -4 6 1.30 1.20 9 4 -6 0.90 3.20 9 4 -6 0.80 6.90 -9 -4 6 0.40 1.10 -9 -4 6 0.00 0.90 8 4 -6 6.90 5.20 8 4 -6 7.80 2.80 8 4 -6 7.60 1.50 -8 -4 6 8.00 1.20 -8 -4 6 6.00 1.20 7 4 -6 11.00 4.50 7 4 -6 10.30 2.60 7 4 -6 7.90 1.20 -7 -4 6 9.50 1.10 -7 -4 6 10.80 1.40 6 4 -6 56.29 5.10 6 4 -6 53.69 2.20 6 4 -6 58.49 3.70 6 4 -6 61.49 2.80 -6 -4 6 58.69 2.30 -6 -4 6 50.29 4.10 -6 -4 6 60.59 2.30 5 4 -6 2.70 0.70 5 4 -6 2.90 1.80 5 4 -6 2.20 0.90 5 4 -6 -1.70 2.20 -5 -4 6 2.40 0.80 -5 -4 6 2.20 0.70 -5 -4 6 2.00 1.70 4 4 -6 4.80 1.90 4 4 -6 3.30 0.90 4 4 -6 1.90 0.70 4 4 -6 0.40 1.70 -4 -4 6 1.70 0.70 3 4 -6 86.49 2.70 3 4 -6 90.49 2.90 3 4 -6 89.89 2.60 3 4 -6 85.19 3.80 -3 -4 6 85.09 2.80 -3 -4 6 83.79 2.80 -3 -4 6 82.09 3.00 2 4 -6 2.50 0.60 2 4 -6 4.10 1.70 2 4 -6 2.20 0.70 2 4 -6 2.90 0.70 -2 -4 6 1.20 0.60 -2 -4 6 1.40 0.60 1 4 -6 99.09 3.10 1 4 -6 97.09 4.00 1 4 -6 96.19 3.20 -1 -4 6 97.99 3.30 -1 -4 6 99.29 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19.50 1.40 -1 -5 7 18.90 1.60 0 5 -7 1.10 1.00 0 5 -7 -0.60 1.90 0 5 -7 -0.20 0.80 0 5 -7 1.30 1.00 0 -5 7 -0.80 0.70 0 -5 7 -0.80 0.70 -1 5 -7 13.60 2.20 -1 5 -7 12.70 1.70 -1 5 -7 14.40 1.50 -1 5 -7 15.30 2.00 1 -5 7 10.70 1.30 1 -5 7 11.60 1.70 1 -5 7 13.90 2.20 -2 5 -7 40.00 2.70 -2 5 -7 38.60 2.10 -2 5 -7 37.50 2.90 -2 5 -7 36.80 2.20 -2 5 -7 37.30 3.10 2 -5 7 37.60 2.20 2 -5 7 42.90 2.90 2 -5 7 39.20 2.40 2 -5 7 38.30 2.00 -3 5 -7 0.60 1.40 -3 5 -7 0.80 1.30 -3 5 -7 1.00 1.20 -3 5 -7 -1.00 2.00 3 -5 7 -0.40 1.20 3 -5 7 0.00 1.00 3 -5 7 0.90 1.60 3 -5 7 1.70 0.90 -4 5 -7 122.09 5.00 -4 5 -7 123.19 4.20 -4 5 -7 121.59 4.40 -4 5 -7 101.09 6.20 4 -5 7 122.59 4.80 4 -5 7 127.29 4.30 4 -5 7 115.39 4.70 4 -5 7 131.59 5.50 -5 5 -7 58.19 2.90 -5 5 -7 56.89 4.00 -5 5 -7 54.69 2.50 5 -5 7 59.19 3.50 5 -5 7 58.29 3.20 5 -5 7 58.49 5.40 -6 5 -7 3.00 1.00 -6 5 -7 3.00 2.10 -6 5 -7 1.10 1.40 6 -5 7 1.30 1.40 6 -5 7 -1.20 4.20 6 -5 7 7.50 2.00 -7 5 -7 2.30 1.60 -7 5 -7 2.40 1.30 7 -5 7 2.10 1.80 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2.60 0.80 -1 -4 7 5.80 1.60 0 4 -7 167.18 4.90 0 4 -7 164.28 5.70 0 4 -7 164.58 5.10 0 4 -7 162.88 5.00 0 -4 7 174.28 5.60 0 -4 7 161.38 4.90 0 -4 7 170.08 5.20 -1 4 -7 22.50 1.60 -1 4 -7 20.70 2.30 -1 4 -7 20.90 1.80 1 -4 7 20.40 1.30 1 -4 7 18.90 1.60 1 -4 7 23.10 2.10 -2 4 -7 2.10 0.90 -2 4 -7 3.90 0.90 -2 4 -7 5.00 1.50 -2 4 -7 3.60 1.50 -2 4 -7 2.90 1.00 2 -4 7 3.00 1.10 2 -4 7 7.00 1.60 2 -4 7 1.10 0.80 2 -4 7 2.60 0.80 -3 4 -7 121.69 3.90 -3 4 -7 114.99 4.10 -3 4 -7 118.29 4.00 -3 4 -7 115.89 4.50 -3 4 -7 112.69 5.10 3 -4 7 115.49 4.30 3 -4 7 115.09 4.30 3 -4 7 118.99 4.70 3 -4 7 121.39 3.90 3 -4 7 114.99 4.00 -4 4 -7 3.40 1.10 -4 4 -7 4.50 1.50 -4 4 -7 1.70 1.00 -4 4 -7 1.70 1.10 -4 4 -7 2.10 2.40 4 -4 7 4.50 1.00 4 -4 7 3.10 1.70 4 -4 7 1.30 2.00 4 -4 7 3.60 1.30 -5 4 -7 24.00 1.50 -5 4 -7 22.00 3.80 -5 4 -7 24.80 2.90 -5 4 -7 22.80 1.90 5 -4 7 17.30 2.40 5 -4 7 18.00 3.90 5 -4 7 24.00 2.30 -6 4 -7 14.80 2.40 -6 4 -7 17.00 1.40 -6 4 -7 16.40 1.90 6 -4 7 18.70 4.10 6 -4 7 17.00 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5 -8 16.10 1.70 -7 5 -8 15.30 2.10 7 -5 8 13.00 2.30 7 -5 8 27.00 7.10 -8 5 -8 0.30 1.90 8 -5 8 3.80 8.60 10 4 -8 29.10 13.50 10 4 -8 1.90 3.90 -10 -4 8 2.40 1.90 9 4 -8 7.30 7.20 9 4 -8 0.60 3.20 -9 -4 8 3.80 1.30 -9 -4 8 2.40 1.40 8 4 -8 6.90 3.10 8 4 -8 9.40 5.20 -8 -4 8 6.40 1.30 -8 -4 8 9.00 1.40 7 4 -8 35.10 5.50 7 4 -8 37.90 4.10 -7 -4 8 40.40 2.00 -7 -4 8 39.60 2.10 6 4 -8 1.40 2.40 6 4 -8 -3.10 2.40 6 4 -8 -0.30 1.00 -6 -4 8 -2.60 2.10 -6 -4 8 0.50 0.80 5 4 -8 20.00 2.80 5 4 -8 14.80 1.40 5 4 -8 18.40 2.80 5 4 -8 18.00 1.60 -5 -4 8 17.30 1.40 -5 -4 8 13.00 2.60 4 4 -8 26.30 2.90 4 4 -8 22.00 1.50 4 4 -8 19.40 2.60 4 4 -8 23.80 1.20 4 4 -8 25.50 1.60 -4 -4 8 25.30 1.50 -4 -4 8 25.90 1.50 -4 -4 8 24.20 2.40 3 4 -8 103.99 3.30 3 4 -8 96.49 4.50 3 4 -8 107.09 3.20 3 4 -8 105.19 3.30 -3 -4 8 105.09 3.40 -3 -4 8 100.09 3.30 2 4 -8 51.89 3.20 2 4 -8 51.99 2.00 2 4 -8 52.99 2.00 2 4 -8 51.09 2.00 -2 -4 8 51.59 2.20 -2 -4 8 51.49 2.10 1 4 -8 2.60 1.80 1 4 -8 1.20 0.70 1 4 -8 0.60 0.70 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3.30 1.40 -6 4 -8 0.90 1.80 6 -4 8 2.20 1.70 6 -4 8 -3.10 1.90 6 -4 8 -2.60 3.20 -7 4 -8 24.10 3.00 -7 4 -8 26.40 2.40 -7 4 -8 29.80 2.00 7 -4 8 28.60 3.30 7 -4 8 31.90 6.00 7 -4 8 26.80 3.20 -8 4 -8 11.90 1.60 -8 4 -8 15.00 2.40 8 -4 8 13.00 2.60 8 -4 8 17.90 7.90 -9 4 -8 3.60 2.10 9 -4 8 8.30 9.10 10 3 -8 16.70 12.30 10 3 -8 -2.80 3.10 -10 -3 8 2.60 1.40 -10 -3 8 1.50 1.40 9 3 -8 20.60 7.80 9 3 -8 8.70 3.10 -9 -3 8 12.10 1.60 -9 -3 8 7.50 1.40 8 3 -8 2.30 2.50 8 3 -8 -4.00 4.10 -8 -3 8 0.50 1.00 -8 -3 8 0.90 1.00 7 3 -8 2.20 2.30 7 3 -8 -1.10 1.30 -7 -3 8 0.10 0.80 -7 -3 8 0.20 0.90 6 3 -8 6.60 1.20 6 3 -8 5.20 2.50 6 3 -8 10.00 2.30 6 3 -8 8.20 1.20 -6 -3 8 7.80 1.00 -6 -3 8 8.10 1.10 5 3 -8 68.79 3.70 5 3 -8 61.49 2.40 5 3 -8 59.09 4.00 5 3 -8 65.39 2.50 -5 -3 8 61.49 4.40 -5 -3 8 65.89 2.30 -5 -3 8 68.19 2.20 -5 -3 8 65.89 2.40 4 3 -8 226.28 6.10 4 3 -8 230.18 6.20 4 3 -8 216.08 7.20 4 3 -8 234.48 6.30 4 3 -8 190.78 7.50 -4 -3 8 223.08 7.60 -4 -3 8 227.38 6.20 -4 -3 8 224.48 6.30 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1.70 -7 -3 9 15.60 1.40 6 3 -9 22.50 3.40 6 3 -9 23.70 3.20 6 3 -9 18.10 1.70 6 3 -9 21.80 1.80 -6 -3 9 22.00 1.40 -6 -3 9 22.00 1.60 -6 -3 9 22.50 1.40 -6 -3 9 18.40 3.80 5 3 -9 26.70 3.00 5 3 -9 20.10 3.10 5 3 -9 20.80 1.50 5 3 -9 22.20 1.50 -5 -3 9 19.30 3.80 -5 -3 9 24.70 1.40 -5 -3 9 23.50 1.50 4 3 -9 116.89 5.00 4 3 -9 119.59 4.70 4 3 -9 121.49 3.80 4 3 -9 125.69 3.80 4 3 -9 124.59 3.70 -4 -3 9 121.69 3.80 -4 -3 9 129.39 3.80 -4 -3 9 118.39 5.30 3 3 -9 104.29 3.10 3 3 -9 97.39 3.40 3 3 -9 103.79 3.20 3 3 -9 101.09 4.30 3 3 -9 102.69 3.20 -3 -3 9 99.39 3.30 -3 -3 9 103.59 3.30 -3 -3 9 101.99 4.20 2 3 -9 43.50 1.70 2 3 -9 40.40 2.90 2 3 -9 42.50 1.70 2 3 -9 41.20 1.70 -2 -3 9 39.70 1.80 -2 -3 9 42.50 2.60 -2 -3 9 44.40 2.00 1 3 -9 104.69 3.30 1 3 -9 106.59 4.30 1 3 -9 108.69 3.30 1 3 -9 107.29 3.40 -1 -3 9 101.69 3.30 -1 -3 9 105.49 3.50 -1 -3 9 103.29 4.00 0 3 -9 1.50 0.80 0 3 -9 0.80 0.60 0 3 -9 -0.40 0.50 0 3 -9 0.20 1.30 0 -3 9 0.90 0.60 0 -3 9 0.30 0.80 0 -3 9 0.10 1.30 -1 3 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28.70 1.70 3 4 -10 30.70 3.50 -3 -4 10 26.80 1.70 -3 -4 10 29.80 1.90 2 4 -10 15.30 2.50 2 4 -10 12.40 1.40 2 4 -10 10.50 1.10 2 4 -10 13.60 1.30 -2 -4 10 12.50 1.70 -2 -4 10 18.40 2.50 -2 -4 10 12.90 1.30 1 4 -10 138.29 4.40 1 4 -10 138.49 4.30 1 4 -10 134.39 5.50 1 4 -10 134.49 4.40 -1 -4 10 139.39 4.60 -1 -4 10 139.09 5.30 -1 -4 10 137.49 4.30 0 4 -10 55.89 2.50 0 4 -10 55.39 3.50 0 4 -10 57.89 2.50 0 4 -10 57.99 2.30 0 -4 10 62.49 3.50 0 -4 10 56.49 2.40 0 -4 10 57.19 2.80 -1 4 -10 84.79 3.00 -1 4 -10 81.89 3.20 -1 4 -10 85.39 3.40 -1 4 -10 79.99 3.90 1 -4 10 82.19 3.50 1 -4 10 77.89 3.80 1 -4 10 77.59 3.00 -2 4 -10 10.30 1.40 -2 4 -10 10.00 1.50 -2 4 -10 10.30 1.90 -2 4 -10 11.70 1.40 2 -4 10 13.80 2.40 2 -4 10 11.60 1.30 2 -4 10 11.80 1.60 -3 4 -10 0.00 1.40 -3 4 -10 -0.30 1.20 -3 4 -10 0.30 1.10 -3 4 -10 1.70 1.40 3 -4 10 1.40 0.90 3 -4 10 0.20 1.10 3 -4 10 -0.20 1.90 -4 4 -10 72.09 3.80 -4 4 -10 71.69 3.10 -4 4 -10 73.69 3.10 -4 4 -10 69.19 4.40 4 -4 10 73.59 2.90 4 -4 10 62.69 3.80 4 -4 10 71.49 5.00 4 -4 10 64.59 4.30 -5 4 -10 3.10 1.20 -5 4 -10 2.60 1.80 -5 4 -10 3.10 1.40 -5 4 -10 -0.10 2.80 5 -4 10 -0.70 2.30 5 -4 10 -2.40 3.20 5 -4 10 2.70 1.10 5 -4 10 3.60 1.50 -6 4 -10 -0.40 1.00 -6 4 -10 0.60 1.30 -6 4 -10 -1.80 2.00 6 -4 10 -3.70 2.50 6 -4 10 1.10 1.70 -7 4 -10 2.50 1.60 -7 4 -10 1.90 1.20 7 -4 10 0.40 1.90 7 -4 10 -5.20 4.90 -8 4 -10 11.10 2.20 -8 4 -10 12.80 1.90 8 -4 10 22.20 8.30 8 -4 10 8.30 2.10 9 3 -10 1.00 3.20 9 3 -10 -1.20 6.30 -9 -3 10 0.50 1.30 -9 -3 10 0.40 1.30 8 3 -10 -0.50 4.60 8 3 -10 -1.10 2.80 -8 -3 10 0.10 1.10 -8 -3 10 1.80 1.10 7 3 -10 0.10 2.60 7 3 -10 -3.40 3.00 -7 -3 10 0.30 0.90 -7 -3 10 -0.40 1.00 6 3 -10 55.99 4.50 6 3 -10 47.50 2.50 6 3 -10 55.59 4.00 6 3 -10 58.29 2.80 -6 -3 10 53.39 2.20 -6 -3 10 52.09 2.40 5 3 -10 92.49 4.30 5 3 -10 87.99 3.10 5 3 -10 85.69 3.10 5 3 -10 85.39 4.40 -5 -3 10 73.19 5.20 -5 -3 10 90.39 3.10 -5 -3 10 89.29 3.00 4 3 -10 2.90 1.30 4 3 -10 6.20 2.30 4 3 -10 4.70 1.00 4 3 -10 6.00 1.00 4 3 -10 3.50 0.70 -4 -3 10 3.70 2.20 -4 -3 10 4.30 0.90 -4 -3 10 4.60 0.90 3 3 -10 16.40 2.50 3 3 -10 12.30 1.10 3 3 -10 10.20 1.40 3 3 -10 11.30 1.10 3 3 -10 11.60 1.20 -3 -3 10 13.70 1.30 -3 -3 10 14.90 2.70 -3 -3 10 15.10 1.40 2 3 -10 4.40 0.80 2 3 -10 3.30 0.70 2 3 -10 5.60 2.10 2 3 -10 3.90 0.70 -2 -3 10 3.90 1.60 -2 -3 10 4.70 1.00 -2 -3 10 2.10 0.70 1 3 -10 293.87 8.10 1 3 -10 292.27 8.10 1 3 -10 292.07 9.00 1 3 -10 295.67 8.00 -1 -3 10 287.27 8.80 -1 -3 10 287.67 8.10 -1 -3 10 293.37 8.30 0 3 -10 122.09 3.90 0 3 -10 119.39 3.70 0 3 -10 124.39 4.70 0 3 -10 119.99 3.90 0 -3 10 126.19 3.80 0 -3 10 117.19 4.50 0 -3 10 122.59 4.10 -1 3 -10 3.70 0.90 -1 3 -10 3.80 0.80 -1 3 -10 5.50 1.70 -1 3 -10 6.00 0.90 1 -3 10 5.80 1.80 1 -3 10 5.00 0.90 1 -3 10 5.10 1.20 -2 3 -10 88.49 3.50 -2 3 -10 97.59 3.30 -2 3 -10 89.79 3.60 -2 3 -10 92.89 3.10 -2 3 -10 92.29 3.20 2 -3 10 91.09 4.00 2 -3 10 94.79 3.30 2 -3 10 90.29 3.10 2 -3 10 90.09 3.60 2 -3 10 92.99 4.00 -3 3 -10 0.00 1.00 -3 3 -10 0.50 0.90 -3 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5 3 -11 5.70 1.20 5 3 -11 2.10 1.60 5 3 -11 3.40 1.10 -5 -3 11 4.40 1.00 -5 -3 11 3.60 0.90 4 3 -11 21.20 1.40 4 3 -11 21.50 1.50 4 3 -11 19.60 3.10 4 3 -11 21.30 2.10 4 3 -11 22.10 1.60 -4 -3 11 24.50 1.60 -4 -3 11 22.50 1.60 -4 -3 11 20.10 3.60 3 3 -11 183.98 6.70 3 3 -11 191.88 5.40 3 3 -11 187.48 5.40 3 3 -11 182.38 5.50 3 3 -11 187.48 5.40 -3 -3 11 186.38 5.50 -3 -3 11 186.18 5.60 -3 -3 11 174.78 6.40 -3 -3 11 192.08 6.50 2 3 -11 54.29 2.10 2 3 -11 50.19 3.50 2 3 -11 53.89 2.00 2 3 -11 52.39 2.10 -2 -3 11 54.89 3.20 -2 -3 11 56.89 2.50 -2 -3 11 49.30 2.20 1 3 -11 19.10 1.40 1 3 -11 20.70 1.30 1 3 -11 19.60 1.50 1 3 -11 20.60 2.50 -1 -3 11 20.70 1.40 -1 -3 11 17.70 2.30 -1 -3 11 22.20 1.80 0 3 -11 4.90 0.90 0 3 -11 3.00 0.90 0 3 -11 4.40 1.80 0 3 -11 5.00 1.00 0 -3 11 3.70 1.80 0 -3 11 4.80 0.90 0 -3 11 4.80 1.10 -1 3 -11 110.99 4.30 -1 3 -11 112.89 3.50 -1 3 -11 114.99 3.70 -1 3 -11 111.29 3.80 1 -3 11 106.29 4.50 1 -3 11 111.09 4.00 1 -3 11 103.59 3.60 -2 3 -11 26.60 2.00 -2 3 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26 -1.90 5.40 2 -5 -26 7.70 2.40 -2 5 26 7.00 2.10 1 -5 -26 -0.30 2.00 -1 5 26 -0.90 1.60 0 -5 -26 1.40 2.00 0 5 26 0.10 1.60 0 5 26 -2.90 1.60 -1 -5 -26 -1.10 1.80 1 5 26 -2.40 1.80 1 5 26 -0.20 1.40 -2 -5 -26 1.40 2.20 2 5 26 3.00 2.80 2 5 26 1.00 1.50 2 5 26 0.70 1.70 -3 -5 -26 -0.20 3.50 -3 -5 -26 2.30 0.90 3 5 26 1.30 1.40 3 5 26 -0.10 2.30 -4 -5 -26 2.60 1.10 -4 -5 -26 1.50 2.30 4 5 26 -3.50 2.10 4 5 26 1.20 3.10 4 5 26 1.10 1.30 -5 -5 -26 1.20 2.40 -5 -5 -26 3.60 1.40 5 5 26 1.10 1.30 5 5 26 -3.30 2.40 5 5 26 -0.30 4.60 -6 -5 -26 2.50 1.70 -6 -5 -26 2.60 3.10 6 5 26 0.90 5.80 6 5 26 2.70 3.00 1 -6 -26 7.00 2.40 -1 6 26 5.00 1.90 0 -6 -26 12.30 2.70 0 6 26 9.90 1.90 -1 -6 -26 -0.40 2.10 1 6 26 -0.20 1.50 1 6 26 2.00 3.70 2 6 26 -2.40 2.10 2 6 26 -0.90 2.40 2 6 26 0.10 1.40 -3 -6 -26 2.70 2.50 3 6 26 -0.80 1.90 3 6 26 0.10 3.60 3 6 26 -0.20 1.40 -4 -6 -26 5.20 2.80 -4 -6 -26 6.70 1.20 4 6 26 4.90 3.40 4 6 26 1.00 2.20 4 6 26 4.80 1.50 -5 -6 -26 5.40 3.10 -5 -6 -26 7.30 1.60 5 6 26 6.40 1.40 5 6 26 5.60 4.20 5 6 26 -0.20 2.50 1 7 26 2.90 3.00 -2 -7 -26 6.70 3.00 2 7 26 4.80 3.50 2 7 26 6.00 1.70 -3 -7 -26 0.50 2.60 3 7 26 0.30 3.10 3 7 26 0.30 1.50 -4 -7 -26 0.40 2.90 4 7 26 -0.50 1.40 4 7 26 -0.10 3.70 1 2 -27 1.20 1.60 1 2 -27 -1.10 2.90 -1 -2 27 -4.00 2.00 0 2 -27 9.10 3.30 0 2 -27 11.20 2.00 0 -2 27 8.40 2.40 -1 2 -27 -3.00 3.00 -1 2 -27 0.60 1.70 1 -2 27 0.80 2.20 -2 2 -27 11.40 2.20 -2 2 -27 8.10 3.50 2 -2 27 10.60 2.30 2 1 -27 11.80 3.20 -2 -1 27 2.90 2.80 -2 -1 27 8.50 2.70 -2 -1 27 7.40 2.40 1 1 -27 10.60 3.00 1 1 -27 11.10 1.50 -1 -1 27 9.50 2.80 -1 -1 27 5.30 2.20 0 1 -27 6.70 2.80 0 1 -27 4.90 1.40 0 -1 27 0.50 1.90 0 -1 27 -2.30 2.50 0 -1 27 -0.20 2.50 -1 1 -27 -0.40 2.50 -1 1 -27 0.50 1.40 1 -1 27 -1.40 1.80 1 -1 27 -0.10 2.70 -2 1 -27 -1.70 1.40 -2 1 -27 0.10 2.50 2 -1 27 0.50 1.90 -3 1 -27 4.50 2.80 -3 1 -27 4.00 1.80 3 -1 27 4.20 2.10 3 -1 27 -5.40 4.70 2 0 -27 -1.30 2.40 -2 0 27 0.30 2.00 -2 0 27 -1.50 2.30 1 0 -27 15.60 1.50 1 0 -27 17.60 3.20 -1 0 27 16.10 3.20 -1 0 27 9.10 2.70 -1 0 27 10.40 2.40 0 0 -27 24.30 3.40 0 0 -27 18.50 1.60 0 0 27 18.20 3.80 0 0 27 18.30 2.40 0 0 27 16.60 3.40 -1 0 -27 1.60 1.10 -1 0 -27 0.60 2.30 1 0 27 -0.90 1.90 1 0 27 -0.80 2.60 1 0 27 -2.00 2.60 -2 0 -27 6.90 2.70 2 0 27 1.00 3.30 2 0 27 1.10 2.90 -3 0 -27 0.50 2.50 -3 0 -27 3.20 1.50 3 0 27 -1.40 4.90 3 0 27 -1.10 3.80 3 0 27 3.00 1.90 -4 0 -27 10.40 3.10 -4 0 -27 11.40 2.00 4 0 27 10.80 2.30 4 0 27 2.30 5.30 2 -1 -27 16.80 3.70 -2 1 27 15.00 2.40 -2 1 27 8.40 2.80 -1 1 27 4.60 1.90 -1 1 27 1.40 2.40 0 -1 -27 13.60 4.60 0 -1 -27 12.50 1.20 0 1 27 10.00 2.70 0 1 27 13.00 3.10 0 1 27 12.10 2.50 -1 -1 -27 0.20 2.30 -1 -1 -27 1.70 0.90 1 1 27 -0.40 2.30 1 1 27 -0.40 2.50 1 1 27 2.40 1.60 -2 -1 -27 -0.80 2.30 -2 -1 -27 2.60 1.10 2 1 27 -1.80 2.80 2 1 27 1.70 1.60 2 1 27 -3.80 2.20 -3 -1 -27 5.00 1.30 -3 -1 -27 4.10 2.50 3 1 27 4.60 1.70 3 1 27 2.70 3.60 3 1 27 1.80 2.70 -4 -1 -27 -0.80 1.50 -4 -1 -27 -0.60 2.30 4 1 27 1.80 1.70 4 1 27 -3.20 4.10 4 1 27 -1.40 5.10 -5 -1 -27 0.00 2.60 -5 -1 -27 0.50 1.60 5 1 27 1.00 1.60 2 -2 -27 0.90 2.20 -2 2 27 -3.80 1.90 -2 2 27 0.80 1.90 1 -2 -27 37.70 3.60 -1 2 27 40.30 3.20 -1 2 27 27.30 4.00 0 -2 -27 7.60 2.60 0 2 27 5.50 2.20 -1 -2 -27 2.80 4.00 -1 -2 -27 2.90 0.80 1 2 27 4.30 2.70 1 2 27 -0.20 2.20 1 2 27 3.00 1.60 -2 -2 -27 1.90 1.00 -2 -2 -27 -0.20 2.40 2 2 27 -1.30 2.30 2 2 27 0.70 1.40 2 2 27 0.40 2.70 -3 -2 -27 2.90 2.20 -3 -2 -27 2.60 1.20 3 2 27 3.20 1.60 3 2 27 -1.00 2.50 3 2 27 5.20 3.70 -4 -2 -27 12.10 3.10 -4 -2 -27 13.30 1.80 4 2 27 9.20 4.60 4 2 27 12.80 1.90 4 2 27 4.50 2.70 -5 -2 -27 0.50 2.50 -5 -2 -27 2.80 1.70 5 2 27 3.60 5.30 5 2 27 3.60 1.70 2 -3 -27 0.50 2.20 -2 3 27 0.40 1.70 1 -3 -27 2.40 2.20 -1 3 27 1.30 2.10 -1 3 27 1.80 1.70 0 -3 -27 13.30 2.70 0 3 27 5.20 2.00 -1 -3 -27 0.40 2.00 1 3 27 1.40 2.80 1 3 27 -2.70 2.10 1 3 27 0.40 1.40 -2 -3 -27 6.70 1.10 -2 -3 -27 1.40 3.10 2 3 27 7.70 1.70 2 3 27 3.30 2.00 2 3 27 6.50 2.90 -3 -3 -27 3.80 2.40 -3 -3 -27 4.90 1.10 3 3 27 2.80 3.00 3 3 27 3.20 1.50 3 3 27 1.40 2.20 -4 -3 -27 5.40 1.40 -4 -3 -27 3.10 2.50 4 3 27 4.30 3.60 4 3 27 1.10 2.60 4 3 27 3.80 1.60 -5 -3 -27 4.10 1.60 -5 -3 -27 5.00 2.80 5 3 27 4.50 1.70 5 3 27 3.10 4.90 2 -4 -27 22.30 3.10 -2 4 27 21.80 2.60 1 -4 -27 -2.00 2.00 -1 4 27 -0.10 1.60 0 -4 -27 2.70 2.00 0 4 27 1.40 1.90 0 4 27 2.80 2.60 -1 -4 -27 1.40 2.20 1 4 27 -3.60 2.10 1 4 27 0.40 1.60 -2 -4 -27 4.50 3.50 2 4 27 5.20 1.60 2 4 27 0.40 1.90 2 4 27 2.50 2.90 -3 -4 -27 3.50 2.30 -3 -4 -27 5.00 1.10 3 4 27 3.40 2.10 3 4 27 3.60 1.50 3 4 27 2.00 3.70 -4 -4 -27 0.90 1.10 -4 -4 -27 3.90 2.70 4 4 27 -2.90 2.40 4 4 27 1.80 1.50 -5 -4 -27 1.70 2.70 -5 -4 -27 1.20 1.50 5 4 27 1.40 1.50 5 4 27 3.80 4.80 5 4 27 -1.80 3.80 1 -5 -27 23.70 3.40 -1 5 27 24.20 2.60 0 -5 -27 17.00 3.10 0 5 27 9.60 2.00 1 5 27 0.90 1.60 -2 -5 -27 -0.50 2.30 2 5 27 -0.10 1.50 2 5 27 1.00 2.40 2 5 27 -0.30 2.70 -3 -5 -27 0.70 1.00 -3 -5 -27 -0.60 2.30 3 5 27 0.40 3.50 3 5 27 3.20 1.50 3 5 27 -1.10 2.20 -4 -5 -27 12.70 1.50 -4 -5 -27 12.40 3.10 4 5 27 13.00 5.10 4 5 27 12.30 1.80 -5 -5 -27 3.40 1.50 -5 -5 -27 3.40 3.00 5 5 27 2.10 1.50 5 5 27 -0.60 5.20 -1 -6 -27 0.10 2.60 1 6 27 1.00 2.10 -2 -6 -27 8.60 2.90 2 6 27 6.70 3.30 2 6 27 10.80 1.80 -3 -6 -27 -0.30 2.70 3 6 27 -0.10 1.50 3 6 27 1.60 3.10 -4 -6 -27 -0.10 2.80 -4 -6 -27 3.20 1.30 4 6 27 -0.60 4.20 4 6 27 1.50 1.50 0 1 -28 6.00 3.30 0 1 -28 5.30 1.50 0 -1 28 2.50 2.30 0 -1 28 1.80 4.30 -1 1 -28 0.80 1.50 -1 1 -28 0.60 2.80 1 -1 28 -0.20 2.10 -2 1 -28 2.20 1.70 -2 1 -28 4.30 3.20 2 -1 28 0.10 2.10 1 0 -28 2.80 2.90 -1 0 28 0.40 2.10 -1 0 28 3.20 2.70 0 0 -28 2.30 1.10 0 0 -28 0.40 2.70 0 0 28 0.40 2.00 0 0 28 -0.50 2.70 -1 0 -28 4.20 2.80 -1 0 -28 1.80 1.20 1 0 28 3.10 1.90 1 0 28 -3.00 2.90 -2 0 -28 14.60 1.90 -2 0 -28 13.40 3.30 2 0 28 8.60 2.10 -3 0 -28 5.70 3.20 -3 0 -28 3.90 1.60 3 0 28 -0.30 4.40 3 0 28 6.80 2.10 1 -1 -28 15.60 3.10 -1 1 28 10.80 2.40 0 -1 -28 -1.90 2.30 0 1 28 -0.40 2.60 0 1 28 -0.80 1.80 -1 -1 -28 3.60 1.00 -1 -1 -28 -0.70 2.50 1 1 28 -1.30 2.80 1 1 28 -3.80 3.00 1 1 28 1.20 1.80 -2 -1 -28 -1.40 2.40 -2 -1 -28 0.80 1.10 2 1 28 -1.60 2.00 2 1 28 -1.20 3.10 -3 -1 -28 9.10 3.10 -3 -1 -28 6.10 1.60 3 1 28 0.30 3.90 -4 -1 -28 11.50 2.00 -4 -1 -28 9.10 3.00 4 1 28 2.30 5.10 4 1 28 6.30 2.20 1 -2 -28 2.70 2.40 -1 2 28 0.40 1.90 0 -2 -28 4.60 2.60 0 2 28 3.80 2.90 0 2 28 3.90 1.80 -1 -2 -28 8.90 2.90 1 2 28 4.70 2.10 1 2 28 4.70 3.20 1 2 28 4.60 3.60 -2 -2 -28 3.60 2.40 -2 -2 -28 5.00 1.10 2 2 28 3.40 3.20 2 2 28 -0.40 3.60 2 2 28 0.10 1.80 -3 -2 -28 3.60 1.30 -3 -2 -28 0.20 2.30 3 2 28 1.80 1.70 3 2 28 0.30 3.80 -4 -2 -28 3.00 2.70 -4 -2 -28 5.80 1.70 4 2 28 5.50 1.80 4 2 28 3.30 4.40 1 -3 -28 3.00 2.50 -1 3 28 1.40 2.00 0 -3 -28 14.00 2.90 0 3 28 18.10 2.30 -1 -3 -28 -3.30 1.90 1 3 28 0.80 2.60 1 3 28 1.50 2.70 -2 -3 -28 13.20 3.10 -2 -3 -28 12.90 1.40 2 3 28 14.20 2.00 2 3 28 13.30 4.00 -3 -3 -28 3.90 1.20 -3 -3 -28 1.10 2.30 3 3 28 1.30 3.30 3 3 28 1.20 1.60 -4 -3 -28 3.70 1.40 -4 -3 -28 -0.70 2.30 4 3 28 0.70 1.60 0 -4 -28 0.90 2.30 0 4 28 1.80 1.80 -1 -4 -28 2.60 2.30 1 4 28 1.20 2.10 1 4 28 2.70 2.90 -2 -4 -28 4.20 2.60 2 4 28 4.60 4.00 2 4 28 5.20 1.80 -3 -4 -28 3.50 1.10 -3 -4 -28 3.60 2.50 3 4 28 3.80 1.70 3 4 28 1.90 3.60 -4 -4 -28 7.20 2.90 -4 -4 -28 6.30 1.40 4 4 28 -2.10 4.60 4 4 28 3.00 1.70 -1 -5 -28 10.20 3.10 1 5 28 12.00 2.10 -2 -5 -28 14.00 3.20 2 5 28 12.70 2.00 2 5 28 8.20 3.50 -3 -5 -28 -2.50 2.50 3 5 28 -1.80 1.50 3 5 28 0.30 3.70 -1 -1 -29 24.00 3.80 1 1 29 15.50 2.40 1 1 29 15.90 3.90 -2 -1 -29 17.10 3.70 -2 -1 -29 15.20 1.80 2 1 29 7.30 3.90 2 1 29 15.10 2.40 0 -2 -29 3.10 2.90 0 2 29 2.90 2.10 0 2 29 3.40 3.10 -1 -2 -29 6.80 2.90 1 2 29 3.60 2.00 1 2 29 3.60 3.20 -2 -2 -29 7.20 2.90 -2 -2 -29 13.00 2.00 2 2 29 7.00 2.10 2 2 29 5.30 3.60 -3 -2 -29 2.70 2.80 -3 -2 -29 1.10 1.40 3 2 29 0.80 1.90 3 2 29 1.10 4.20 -1 -3 -29 26.00 3.80 1 3 29 28.90 3.20 -2 -3 -29 5.10 2.90 2 3 29 4.00 1.80 -3 -3 -29 12.70 1.70 -3 -3 -29 11.50 3.10 3 3 29 9.70 5.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 914 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.40037(4) 0.68522(4) 0.70446(2) 0.03427(11) Uani 1 1 d . . . . . N1 N 0.3161(3) 0.7512(3) 0.79695(9) 0.0336(4) Uani 1 1 d . . . . . O1 O 0.6592(3) 0.6995(4) 0.70078(12) 0.0608(6) Uani 1 1 d D . . . . H1A H 0.6849(16) 0.754(5) 0.6684(10) 0.091 Uiso 1 1 calc DR U . . . Cl1 Cl 0.79657(10) 0.34410(11) 0.52397(4) 0.0558(2) Uani 1 1 d . . . . . Cl2 Cl -0.17281(10) 0.73003(11) 0.85336(4) 0.0558(2) Uani 1 1 d . . . . . N2 N 0.1966(3) 0.9643(3) 0.86192(11) 0.0434(5) Uani 1 1 d . . . . . O2 O 0.4674(3) 0.6198(4) 0.61263(11) 0.0664(7) Uani 1 1 d D . . . . H2B H 0.387(3) 0.588(6) 0.6012(10) 0.100 Uiso 1 1 calc DR U . . . O3 O 0.1465(3) 0.6607(3) 0.69498(11) 0.0491(5) Uani 1 1 d D . . . . H3A H 0.1132(18) 0.721(4) 0.6597(9) 0.074 Uiso 1 1 calc DR U . . . C3 C 0.2134(3) 0.8385(4) 0.91445(12) 0.0418(6) Uani 1 1 d . . . . . N3 N 0.2803(3) 0.6735(3) 0.91367(10) 0.0402(5) Uani 1 1 d . . . . . H1B H 0.686(6) 0.702(6) 0.7341(9) 0.092(16) Uiso 1 1 d D . . . . H13 H 0.784(3) 0.913(5) 0.586(2) 0.080(13) Uiso 1 1 d D . . . . H14 H 0.949(14) 0.779(19) 0.573(4) 0.53(13) Uiso 1 1 d D . . . . H3B H 0.076(4) 0.695(5) 0.7265(12) 0.090(15) Uiso 1 1 d D . . . . C14 C 0.1470(6) 0.7660(6) 1.03117(15) 0.0767(12) Uani 1 1 d . . . . . H14A H 0.0642 0.7006 1.0273 0.115 Uiso 1 1 calc R U . . . H14B H 0.1106 0.8228 1.0693 0.115 Uiso 1 1 calc R U . . . H14C H 0.2575 0.6913 1.0367 0.115 Uiso 1 1 calc R U . . . N4 N 0.3112(3) 0.9614(3) 0.68750(10) 0.0391(5) Uani 1 1 d . . . . . C4 C 0.4296(4) 0.3233(4) 0.88561(15) 0.0492(7) Uani 1 1 d . . . . . O4 O 0.1600(3) 0.8905(3) 0.97166(10) 0.0616(6) Uani 1 1 d . . . . . O5A O 0.9462(13) 0.2092(14) 0.5312(4) 0.120(3) Uani 0.696(9) 1 d . . P A 1 O5B O 0.900(3) 0.209(4) 0.5542(10) 0.120(3) Uani 0.304(9) 1 d . . P A 2 C5 C 0.5132(4) 0.2053(4) 0.84724(17) 0.0556(7) Uani 1 1 d . . . . . H5 H 0.5520 0.0895 0.8622 0.067 Uiso 1 1 calc R U . . . N5 N 0.2324(3) 1.0235(3) 0.74490(10) 0.0386(5) Uani 1 1 d . . . . . O6 O 0.7998(4) 0.4710(5) 0.56167(17) 0.0894(9) Uani 1 1 d . . . . . C1 C 0.2473(3) 0.9111(3) 0.80482(11) 0.0341(5) Uani 1 1 d . . . . . C2 C 0.3284(3) 0.6398(3) 0.85263(11) 0.0333(5) Uani 1 1 d . . . . . C6 C 0.5302(4) 0.2902(4) 0.78084(14) 0.0438(6) Uani 1 1 d . . . . . N6 N 0.4591(3) 0.4537(3) 0.77745(10) 0.0382(5) Uani 1 1 d . . . . . O7A O 0.6223(8) 0.3063(10) 0.5391(4) 0.0923(19) Uani 0.696(9) 1 d . . P A 1 O7B O 0.6930(18) 0.241(3) 0.5487(10) 0.0923(19) Uani 0.304(9) 1 d . . P A 2 N7 N 0.3982(3) 0.4743(3) 0.84225(10) 0.0376(4) Uani 1 1 d . . . . . C7 C 0.6133(5) 0.2196(4) 0.72037(18) 0.0613(8) Uani 1 1 d . . . . . H7A H 0.5357 0.2537 0.6861 0.092 Uiso 1 1 calc R U . . . H7B H 0.6414 0.0973 0.7309 0.092 Uiso 1 1 calc R U . . . H7C H 0.7169 0.2619 0.7047 0.092 Uiso 1 1 calc R U . . . O8 O 0.8060(5) 0.4096(5) 0.45455(14) 0.0925(10) Uani 1 1 d . . . . . C8 C 0.3714(6) 0.3011(5) 0.95826(17) 0.0752(11) Uani 1 1 d . . . . . H8A H 0.2494 0.3456 0.9647 0.113 Uiso 1 1 calc R U . . . H8B H 0.4311 0.3614 0.9800 0.113 Uiso 1 1 calc R U . . . H8C H 0.3958 0.1820 0.9770 0.113 Uiso 1 1 calc R U . . . O9A O -0.3402(8) 0.7377(15) 0.8508(4) 0.147(3) Uani 0.696(9) 1 d . . P A 1 O9B O -0.275(2) 0.606(3) 0.8457(11) 0.147(3) Uani 0.304(9) 1 d . . P A 2 C9 C 0.2708(4) 1.0883(4) 0.63815(13) 0.0420(6) Uani 1 1 d . . . . . H2A H 0.564(2) 0.581(5) 0.595(2) 0.090(15) Uiso 1 1 d D . . . . C11 C 0.1407(4) 1.1869(3) 0.72981(14) 0.0450(6) Uani 1 1 d . . . . . C10 C 0.1647(4) 1.2303(4) 0.66250(15) 0.0499(7) Uani 1 1 d . . . . . H10 H 0.1194 1.3344 0.6372 0.060 Uiso 1 1 calc R U . . . O10 O -0.1759(6) 0.8415(6) 0.8988(2) 0.1268(15) Uani 1 1 d . . . . . O12 O -0.1042(6) 0.8013(7) 0.79012(18) 0.1325(16) Uani 1 1 d . . . . . C12 C 0.0346(5) 1.2852(4) 0.78031(17) 0.0629(9) Uani 1 1 d . . . . . H12A H -0.0317 1.3890 0.7581 0.094 Uiso 1 1 calc R U . . . H12B H 0.1086 1.3118 0.8081 0.094 Uiso 1 1 calc R U . . . H12C H -0.0419 1.2183 0.8075 0.094 Uiso 1 1 calc R U . . . O13 O 0.8845(4) 0.8465(5) 0.60444(14) 0.0876(9) Uani 1 1 d D . . . . C13 C 0.3368(5) 1.0683(5) 0.56797(14) 0.0590(8) Uani 1 1 d . . . . . H13A H 0.2538 1.0304 0.5480 0.089 Uiso 1 1 calc R U . . . H13B H 0.4435 0.9856 0.5675 0.089 Uiso 1 1 calc R U . . . H13C H 0.3558 1.1759 0.5430 0.089 Uiso 1 1 calc R U . . . O11 O -0.0511(6) 0.5904(6) 0.8770(3) 0.156(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.03560(18) 0.0400(2) 0.02641(16) -0.01088(12) -0.00133(12) -0.00279(14) N1 0.0360(10) 0.0380(11) 0.0266(9) -0.0080(8) -0.0009(7) -0.0061(8) O1 0.0418(11) 0.0947(19) 0.0446(12) -0.0044(12) -0.0018(9) -0.0191(12) Cl1 0.0511(4) 0.0698(5) 0.0457(4) -0.0151(3) -0.0034(3) -0.0074(4) Cl2 0.0485(4) 0.0723(5) 0.0425(4) -0.0150(3) -0.0027(3) -0.0007(4) N2 0.0527(13) 0.0453(12) 0.0320(10) -0.0138(9) 0.0044(9) -0.0091(10) O2 0.0615(14) 0.0930(18) 0.0442(12) -0.0375(12) -0.0081(10) 0.0086(14) O3 0.0458(11) 0.0601(13) 0.0442(11) -0.0076(9) -0.0080(9) -0.0156(10) C3 0.0418(13) 0.0560(16) 0.0293(11) -0.0142(11) 0.0014(9) -0.0107(12) N3 0.0389(11) 0.0540(13) 0.0263(9) -0.0072(9) 0.0007(8) -0.0086(10) C14 0.086(3) 0.098(3) 0.0279(13) -0.0074(16) 0.0082(15) 0.006(2) N4 0.0478(12) 0.0414(12) 0.0283(9) -0.0098(8) 0.0035(8) -0.0105(10) C4 0.0478(15) 0.0458(16) 0.0477(15) 0.0053(12) -0.0060(12) -0.0071(13) O4 0.0772(15) 0.0731(15) 0.0290(9) -0.0185(9) 0.0066(9) -0.0034(12) O5A 0.125(6) 0.131(3) 0.078(5) -0.044(5) -0.032(4) 0.066(4) O5B 0.125(6) 0.131(3) 0.078(5) -0.044(5) -0.032(4) 0.066(4) C5 0.0600(19) 0.0402(15) 0.0598(18) 0.0011(13) -0.0100(14) -0.0018(14) N5 0.0505(12) 0.0353(11) 0.0284(9) -0.0080(8) 0.0040(8) -0.0083(9) O6 0.0713(17) 0.114(2) 0.099(2) -0.0594(19) 0.0021(15) -0.0243(17) C1 0.0359(12) 0.0372(12) 0.0299(11) -0.0090(9) 0.0014(9) -0.0091(10) C2 0.0280(10) 0.0414(13) 0.0303(11) -0.0052(9) -0.0020(8) -0.0078(10) C6 0.0416(14) 0.0396(14) 0.0494(15) -0.0088(11) -0.0081(11) -0.0039(11) N6 0.0396(11) 0.0387(11) 0.0349(10) -0.0087(8) -0.0043(8) -0.0024(9) O7A 0.059(4) 0.124(6) 0.106(3) -0.043(4) 0.014(3) -0.037(3) O7B 0.059(4) 0.124(6) 0.106(3) -0.043(4) 0.014(3) -0.037(3) N7 0.0379(11) 0.0408(11) 0.0312(10) -0.0035(8) -0.0021(8) -0.0052(9) C7 0.064(2) 0.0519(18) 0.066(2) -0.0249(16) -0.0055(16) 0.0050(15) O8 0.110(2) 0.122(3) 0.0523(15) -0.0027(16) -0.0134(15) -0.043(2) C8 0.091(3) 0.069(2) 0.0456(17) 0.0132(16) 0.0066(17) -0.003(2) O9A 0.056(4) 0.232(11) 0.172(5) -0.032(7) -0.020(4) -0.062(5) O9B 0.056(4) 0.232(11) 0.172(5) -0.032(7) -0.020(4) -0.062(5) C9 0.0514(15) 0.0414(14) 0.0343(12) -0.0028(10) -0.0016(10) -0.0163(12) C11 0.0552(16) 0.0340(13) 0.0439(14) -0.0078(11) 0.0009(12) -0.0077(12) C10 0.0635(18) 0.0372(14) 0.0447(15) 0.0001(11) -0.0046(13) -0.0076(13) O10 0.159(4) 0.129(3) 0.099(3) -0.063(2) 0.009(3) -0.020(3) O12 0.124(3) 0.192(5) 0.068(2) -0.007(2) 0.020(2) -0.034(3) C12 0.082(2) 0.0414(16) 0.0577(19) -0.0143(14) 0.0050(17) 0.0015(16) O13 0.089(2) 0.106(2) 0.0557(15) -0.0061(15) 0.0096(14) -0.0139(18) C13 0.076(2) 0.066(2) 0.0314(13) -0.0040(13) 0.0031(13) -0.0154(17) O11 0.130(4) 0.108(3) 0.223(6) -0.004(3) -0.072(4) 0.005(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O2 Co1 N1 176.26(9) . . O2 Co1 O1 85.04(10) . . N1 Co1 O1 98.69(9) . . O2 Co1 O3 87.07(10) . . N1 Co1 O3 89.20(8) . . O1 Co1 O3 172.11(9) . . O2 Co1 N6 107.46(10) . . N1 Co1 N6 73.14(8) . . O1 Co1 N6 86.82(9) . . O3 Co1 N6 95.45(8) . . O2 Co1 N4 105.67(10) . . N1 Co1 N4 73.98(8) . . O1 Co1 N4 93.48(10) . . O3 Co1 N4 88.75(9) . . N6 Co1 N4 146.77(8) . . C2 N1 C1 115.2(2) . . C2 N1 Co1 122.80(17) . . C1 N1 Co1 122.00(16) . . Co1 O1 H1A 109.5 . . Co1 O1 H1B 113(3) . . H1A O1 H1B 124.5 . . O7B Cl1 O5B 77.1(18) . . O7B Cl1 O6 116.3(8) . . O5B Cl1 O6 102.5(12) . . O7B Cl1 O8 119.1(8) . . O5B Cl1 O8 126.6(8) . . O6 Cl1 O8 111.1(2) . . O6 Cl1 O5A 110.9(5) . . O8 Cl1 O5A 104.4(4) . . O6 Cl1 O7A 106.3(3) . . O8 Cl1 O7A 103.5(3) . . O5A Cl1 O7A 120.4(7) . . O9A Cl2 O11 127.6(5) . . O9A Cl2 O12 108.1(4) . . O11 Cl2 O12 107.2(3) . . O9A Cl2 O10 102.6(5) . . O11 Cl2 O10 101.7(3) . . O12 Cl2 O10 108.3(3) . . O11 Cl2 O9B 86.2(9) . . O12 Cl2 O9B 109.6(9) . . O10 Cl2 O9B 136.8(9) . . C1 N2 C3 113.2(2) . . Co1 O2 H2B 109.5 . . Co1 O2 H2A 129(3) . . H2B O2 H2A 115.2 . . Co1 O3 H3A 109.5 . . Co1 O3 H3B 112(3) . . H3A O3 H3B 106.9 . . O4 C3 N3 119.3(2) . . O4 C3 N2 113.5(2) . . N3 C3 N2 127.2(2) . . C2 N3 C3 112.6(2) . . O4 C14 H14A 109.5 . . O4 C14 H14B 109.5 . . H14A C14 H14B 109.5 . . O4 C14 H14C 109.5 . . H14A C14 H14C 109.5 . . H14B C14 H14C 109.5 . . C9 N4 N5 105.1(2) . . C9 N4 Co1 139.81(17) . . N5 N4 Co1 112.78(15) . . C5 C4 N7 105.4(3) . . C5 C4 C8 129.8(3) . . N7 C4 C8 124.8(3) . . C3 O4 C14 119.0(3) . . Cl1 O5B O7B 50.7(11) . . C4 C5 C6 107.5(3) . . C4 C5 H5 126.3 . . C6 C5 H5 126.3 . . C11 N5 N4 111.0(2) . . C11 N5 C1 131.8(2) . . N4 N5 C1 117.0(2) . . N2 C1 N1 125.7(2) . . N2 C1 N5 120.9(2) . . N1 C1 N5 113.3(2) . . N1 C2 N3 126.1(2) . . N1 C2 N7 113.4(2) . . N3 C2 N7 120.5(2) . . N6 C6 C5 110.3(3) . . N6 C6 C7 121.0(3) . . C5 C6 C7 128.8(3) . . C6 N6 N7 105.2(2) . . C6 N6 Co1 140.72(19) . . N7 N6 Co1 113.96(15) . . Cl1 O7B O5B 52.2(13) . . C4 N7 N6 111.7(2) . . C4 N7 C2 131.9(2) . . N6 N7 C2 116.2(2) . . C6 C7 H7A 109.5 . . C6 C7 H7B 109.5 . . H7A C7 H7B 109.5 . . C6 C7 H7C 109.5 . . H7A C7 H7C 109.5 . . H7B C7 H7C 109.5 . . C4 C8 H8A 109.5 . . C4 C8 H8B 109.5 . . H8A C8 H8B 109.5 . . C4 C8 H8C 109.5 . . H8A C8 H8C 109.5 . . H8B C8 H8C 109.5 . . N4 C9 C10 110.9(2) . . N4 C9 C13 120.2(3) . . C10 C9 C13 129.0(3) . . C10 C11 N5 106.2(2) . . C10 C11 C12 130.0(3) . . N5 C11 C12 123.8(3) . . C11 C10 C9 106.9(3) . . C11 C10 H10 126.5 . . C9 C10 H10 126.5 . . C11 C12 H12A 109.5 . . C11 C12 H12B 109.5 . . H12A C12 H12B 109.5 . . C11 C12 H12C 109.5 . . H12A C12 H12C 109.5 . . H12B C12 H12C 109.5 . . H13 O13 H14 109(2) . . C9 C13 H13A 109.5 . . C9 C13 H13B 109.5 . . H13A C13 H13B 109.5 . . C9 C13 H13C 109.5 . . H13A C13 H13C 109.5 . . H13B C13 H13C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Co1 O2 2.019(2) . Co1 N1 2.0481(19) . Co1 O1 2.091(2) . Co1 O3 2.125(2) . Co1 N6 2.175(2) . Co1 N4 2.178(2) . N1 C2 1.314(3) . N1 C1 1.326(3) . O1 H1A 0.754(10) . O1 H1B 0.748(10) . Cl1 O7B 1.296(17) . Cl1 O5B 1.32(2) . Cl1 O6 1.412(3) . Cl1 O8 1.416(3) . Cl1 O5A 1.433(8) . Cl1 O7A 1.474(6) . Cl2 O9A 1.335(6) . Cl2 O11 1.377(4) . Cl2 O12 1.404(4) . Cl2 O10 1.415(4) . Cl2 O9B 1.48(2) . N2 C1 1.304(3) . N2 C3 1.334(4) . O2 H2B 0.822(10) . O2 H2A 0.825(10) . O3 H3A 0.832(10) . O3 H3B 0.839(10) . C3 O4 1.304(3) . C3 N3 1.333(4) . N3 C2 1.316(3) . C14 O4 1.437(4) . C14 H14A 0.9600 . C14 H14B 0.9600 . C14 H14C 0.9600 . N4 C9 1.317(3) . N4 N5 1.382(3) . C4 C5 1.356(5) . C4 N7 1.368(4) . C4 C8 1.483(4) . O5B O7B 1.63(3) . C5 C6 1.405(4) . C5 H5 0.9300 . N5 C11 1.368(4) . N5 C1 1.385(3) . C2 N7 1.384(3) . C6 N6 1.319(3) . C6 C7 1.474(4) . N6 N7 1.375(3) . C7 H7A 0.9600 . C7 H7B 0.9600 . C7 H7C 0.9600 . C8 H8A 0.9600 . C8 H8B 0.9600 . C8 H8C 0.9600 . C9 C10 1.402(4) . C9 C13 1.485(4) . C11 C10 1.352(4) . C11 C12 1.481(4) . C10 H10 0.9300 . C12 H12A 0.9600 . C12 H12B 0.9600 . C12 H12C 0.9600 . O13 H13 0.942(10) . O13 H14 0.951(10) . C13 H13A 0.9600 . C13 H13B 0.9600 . C13 H13C 0.9600 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C1 N2 C3 O4 -178.8(2) . . . . C1 N2 C3 N3 2.8(4) . . . . O4 C3 N3 C2 180.0(2) . . . . N2 C3 N3 C2 -1.8(4) . . . . N3 C3 O4 C14 -10.6(4) . . . . N2 C3 O4 C14 170.9(3) . . . . O6 Cl1 O5B O7B 114.5(9) . . . . O8 Cl1 O5B O7B -116.8(14) . . . . N7 C4 C5 C6 0.1(4) . . . . C8 C4 C5 C6 176.7(4) . . . . C9 N4 N5 C11 1.5(3) . . . . Co1 N4 N5 C11 -164.63(18) . . . . C9 N4 N5 C1 176.8(2) . . . . Co1 N4 N5 C1 10.7(3) . . . . C3 N2 C1 N1 -2.7(4) . . . . C3 N2 C1 N5 177.3(2) . . . . C2 N1 C1 N2 1.6(4) . . . . Co1 N1 C1 N2 -177.3(2) . . . . C2 N1 C1 N5 -178.4(2) . . . . Co1 N1 C1 N5 2.7(3) . . . . C11 N5 C1 N2 -14.8(4) . . . . N4 N5 C1 N2 171.0(2) . . . . C11 N5 C1 N1 165.1(3) . . . . N4 N5 C1 N1 -9.0(3) . . . . C1 N1 C2 N3 -0.4(4) . . . . Co1 N1 C2 N3 178.57(19) . . . . C1 N1 C2 N7 179.0(2) . . . . Co1 N1 C2 N7 -2.1(3) . . . . C3 N3 C2 N1 0.4(4) . . . . C3 N3 C2 N7 -178.9(2) . . . . C4 C5 C6 N6 -0.6(4) . . . . C4 C5 C6 C7 179.1(3) . . . . C5 C6 N6 N7 0.8(3) . . . . C7 C6 N6 N7 -178.9(3) . . . . C5 C6 N6 Co1 -175.2(2) . . . . C7 C6 N6 Co1 5.1(5) . . . . O6 Cl1 O7B O5B -97.8(10) . . . . O8 Cl1 O7B O5B 125.0(9) . . . . C5 C4 N7 N6 0.4(3) . . . . C8 C4 N7 N6 -176.4(3) . . . . C5 C4 N7 C2 -174.8(3) . . . . C8 C4 N7 C2 8.4(5) . . . . C6 N6 N7 C4 -0.7(3) . . . . Co1 N6 N7 C4 176.47(19) . . . . C6 N6 N7 C2 175.3(2) . . . . Co1 N6 N7 C2 -7.5(3) . . . . N1 C2 N7 C4 -178.7(3) . . . . N3 C2 N7 C4 0.8(4) . . . . N1 C2 N7 N6 6.4(3) . . . . N3 C2 N7 N6 -174.2(2) . . . . N5 N4 C9 C10 -1.1(3) . . . . Co1 N4 C9 C10 158.9(2) . . . . N5 N4 C9 C13 179.0(3) . . . . Co1 N4 C9 C13 -21.1(5) . . . . N4 N5 C11 C10 -1.4(3) . . . . C1 N5 C11 C10 -175.8(3) . . . . N4 N5 C11 C12 176.7(3) . . . . C1 N5 C11 C12 2.3(5) . . . . N5 C11 C10 C9 0.7(3) . . . . C12 C11 C10 C9 -177.3(3) . . . . N4 C9 C10 C11 0.3(4) . . . . C13 C9 C10 C11 -179.8(3) . . . .