#------------------------------------------------------------------------------ #$Date: 2021-08-07 03:30:49 +0300 (Sat, 07 Aug 2021) $ #$Revision: 267978 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/43/1564333.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564333 loop_ _publ_author_name 'McLaughlin, Calum' 'Bitai, Jacqueline' 'Barber, Lydia' 'Slawin, Alexandra' 'Smith, Andrew D.' _publ_section_title ; Catalytic Enantioselective Synthesis of 1,4-Dihydropyridines via the Addition of C(1)-Ammonium Enolates to Pyridinium Salts ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC03860E _journal_year 2021 _chemical_formula_moiety 'C35 H34 Cl2 N2 O3 S' _chemical_formula_sum 'C35 H34 Cl2 N2 O3 S' _chemical_formula_weight 633.63 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_date 2019-09-26 _audit_creation_method 'by CrystalStructure 4.3' _audit_update_record ; 2021-06-23 deposited with the CCDC. 2021-08-06 downloaded from the CCDC. ; _cell_angle_alpha 90.0000 _cell_angle_beta 96.078(3) _cell_angle_gamma 90.0000 _cell_formula_units_Z 8 _cell_length_a 27.4341(8) _cell_length_b 14.0679(4) _cell_length_c 16.1319(5) _cell_measurement_reflns_used 20689 _cell_measurement_temperature 93 _cell_measurement_theta_max 28.23 _cell_measurement_theta_min 2.00 _cell_volume 6191.0(3) _computing_cell_refinement 'CrysAlisPro 1.171.39.8d (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.8d (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.8d (Rigaku OD, 2015)' _computing_molecular_graphics 'CrystalStructure 4.3' _computing_publication_material 'CrystalStructure 4.3 (Rigaku, 2018)' _computing_structure_refinement 'SHELXL Version 2018/3 (Sheldrick, 2008)' _computing_structure_solution 'SHELXT Version 2018/2 (Sheldrick, 2014)' _diffrn_ambient_temperature 93 _diffrn_detector_area_resol_mean 5.811 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.872 _diffrn_measurement_device_type 'Rigaku XtaLAB P200' _diffrn_measurement_method \w _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0627 _diffrn_reflns_av_unetI/netI 0.0320 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.872 _diffrn_reflns_limit_h_max 34 _diffrn_reflns_limit_h_min -36 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 35889 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.872 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.304 _diffrn_reflns_theta_min 2.016 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.316 _exptl_absorpt_correction_T_max 0.991 _exptl_absorpt_correction_T_min 0.667 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.8d (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.360 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 2656.00 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.030 _refine_diff_density_max 0.37 _refine_diff_density_min -0.39 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.089 _refine_ls_hydrogen_treatment mixed _refine_ls_number_parameters 393 _refine_ls_number_reflns 6726 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0436 _refine_ls_R_factor_gt 0.0372 _refine_ls_shift/su_max 0.001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w = 1/[\s^2^(Fo^2^)+(0.0623P)^2^+2.7228P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1037 _refine_ls_wR_factor_ref 0.1065 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5755 _reflns_number_total 6726 _reflns_threshold_expression F^2^>2.0\s(F^2^) _cod_data_source_file d1sc03860e2.cif _cod_data_source_block 31 _cod_database_code 1564333 _shelx_res_file ; TITL CMAS4 shelxl.res created by SHELXL-2018/3 at 21:25:32 on 26-Sep-2019 CELL 0.71073 27.43410 14.06790 16.13190 90.00000 96.07800 90.00000 ZERR 8 0.00080 0.00040 0.00050 0.00000 0.00300 0.00000 LATT 7 SYMM -X, +Y, .50-Z SFAC C H N O S CL UNIT 280 272 16 24 8 16 OMIT 1 1 0 L.S. 20 FMAP 2 PLAN 5 WPDB -2 HTAB BOND $H CONF LIST 4 TEMP -180.0 ACTA SIZE 0.120 0.120 0.030 DFIX 0.9800 0.0050 N22 H22 WGHT 0.062300 2.722800 FVAR 0.40561 CL1 6 0.046040 0.422889 0.527964 11.00000 0.04456 0.05021 = 0.03711 0.00509 0.01547 0.01758 CL2 6 0.102352 0.332655 0.406925 11.00000 0.03415 0.06964 = 0.04073 -0.02073 0.00916 0.00159 S3 5 0.220957 0.648435 0.345831 11.00000 0.01543 0.01495 = 0.01580 0.00143 0.00298 0.00118 O3 4 0.235623 0.717939 0.410112 11.00000 0.02297 0.01696 = 0.02140 -0.00126 0.00250 -0.00245 O4 4 0.234648 0.668249 0.263581 11.00000 0.02183 0.02008 = 0.01937 0.00586 0.00647 0.00405 O21 4 0.180689 0.475295 0.608071 11.00000 0.02380 0.02717 = 0.02017 -0.00091 0.00699 -0.00710 N1 3 0.290834 0.405136 0.345299 11.00000 0.01581 0.01654 = 0.01597 0.00044 0.00290 0.00139 N22 3 0.210169 0.620021 0.650423 11.00000 0.01790 0.02051 = 0.01914 -0.00002 0.00793 0.00020 C2 1 0.273960 0.494708 0.330516 11.00000 0.01351 0.01573 = 0.01440 0.00129 -0.00015 -0.00167 AFIX 43 H2 2 0.284794 0.529273 0.285310 11.00000 -1.20000 AFIX 0 C3 1 0.242337 0.536522 0.377689 11.00000 0.01360 0.01530 = 0.01502 0.00130 -0.00068 -0.00072 C4 1 0.225016 0.491623 0.455196 11.00000 0.01364 0.01992 = 0.01307 0.00153 0.00183 -0.00092 AFIX 13 H4 2 0.188443 0.496176 0.449936 11.00000 -1.20000 AFIX 0 C5 1 0.238242 0.387576 0.453655 11.00000 0.01962 0.01843 = 0.01581 0.00447 0.00044 -0.00408 AFIX 43 H5 2 0.223377 0.345835 0.489851 11.00000 -1.20000 AFIX 0 C6 1 0.269455 0.350784 0.404676 11.00000 0.01942 0.01488 = 0.01825 0.00249 -0.00081 -0.00166 AFIX 43 H6 2 0.277560 0.285268 0.410129 11.00000 -1.20000 AFIX 0 C7 1 0.328796 0.365151 0.298990 11.00000 0.01819 0.01847 = 0.01778 -0.00309 0.00277 0.00311 AFIX 23 H7A 2 0.328633 0.399602 0.245448 11.00000 -1.20000 H7B 2 0.320671 0.297859 0.285963 11.00000 -1.20000 AFIX 0 C8 1 0.380067 0.369850 0.344716 11.00000 0.01694 0.01388 = 0.01837 0.00180 0.00262 0.00092 C9 1 0.390190 0.411238 0.422924 11.00000 0.01867 0.02319 = 0.02307 -0.00387 0.00424 0.00265 AFIX 43 H9 2 0.364350 0.438130 0.450027 11.00000 -1.20000 AFIX 0 C10 1 0.437806 0.413477 0.461579 11.00000 0.02224 0.03262 = 0.02146 -0.00467 0.00130 -0.00148 AFIX 43 H10 2 0.444410 0.442527 0.514744 11.00000 -1.20000 AFIX 0 C11 1 0.475914 0.373566 0.423148 11.00000 0.01662 0.03621 = 0.02420 0.00534 0.00190 0.00152 AFIX 43 H11 2 0.508472 0.375007 0.449871 11.00000 -1.20000 AFIX 0 C12 1 0.465996 0.331657 0.345509 11.00000 0.02078 0.03370 = 0.02421 0.00487 0.00798 0.00876 AFIX 43 H12 2 0.491837 0.303867 0.318998 11.00000 -1.20000 AFIX 0 C13 1 0.418589 0.330082 0.306361 11.00000 0.02348 0.02190 = 0.01792 0.00009 0.00526 0.00421 AFIX 43 H13 2 0.412196 0.301676 0.252889 11.00000 -1.20000 AFIX 0 C14 1 0.156573 0.639370 0.342240 11.00000 0.01602 0.01545 = 0.01996 0.00160 0.00443 0.00324 C15 1 0.129786 0.607689 0.269730 11.00000 0.02072 0.01981 = 0.02031 -0.00038 0.00190 0.00407 AFIX 43 H15 2 0.145570 0.592847 0.221699 11.00000 -1.20000 AFIX 0 C16 1 0.079297 0.598174 0.269016 11.00000 0.02156 0.02506 = 0.02952 -0.00101 -0.00262 0.00261 AFIX 43 H16 2 0.060249 0.577465 0.219713 11.00000 -1.20000 AFIX 0 C17 1 0.056576 0.618585 0.339421 11.00000 0.01649 0.02724 = 0.04205 0.00203 0.00535 0.00301 AFIX 43 H17 2 0.022089 0.611136 0.338166 11.00000 -1.20000 AFIX 0 C18 1 0.083519 0.649774 0.411777 11.00000 0.02314 0.02943 = 0.03148 -0.00188 0.01240 0.00392 AFIX 43 H18 2 0.067586 0.663476 0.459891 11.00000 -1.20000 AFIX 0 C19 1 0.134084 0.660964 0.413693 11.00000 0.02211 0.02219 = 0.02141 -0.00265 0.00499 0.00226 AFIX 43 H19 2 0.152950 0.682902 0.462743 11.00000 -1.20000 AFIX 0 C20 1 0.245250 0.546435 0.536650 11.00000 0.01429 0.01718 = 0.01412 0.00073 0.00283 0.00003 AFIX 13 H20 2 0.248132 0.614725 0.520666 11.00000 -1.20000 AFIX 0 C21 1 0.208340 0.542577 0.601314 11.00000 0.01319 0.02175 = 0.01311 0.00382 0.00029 0.00237 C23 1 0.176428 0.637128 0.712945 11.00000 0.02192 0.02468 = 0.01673 -0.00028 0.00615 0.00560 AFIX 23 H23A 2 0.192995 0.676968 0.758049 11.00000 -1.20000 H23B 2 0.168080 0.575636 0.737735 11.00000 -1.20000 AFIX 0 C24 1 0.129462 0.686123 0.677358 11.00000 0.02251 0.02260 = 0.01331 -0.00354 0.00329 0.00488 C25 1 0.130930 0.770270 0.632734 11.00000 0.02563 0.02528 = 0.02359 0.00102 0.00336 0.00119 AFIX 43 H25 2 0.161647 0.797087 0.623336 11.00000 -1.20000 AFIX 0 C26 1 0.087741 0.815624 0.601668 11.00000 0.03795 0.03052 = 0.02691 0.00550 0.00243 0.00980 AFIX 43 H26 2 0.089089 0.873353 0.571442 11.00000 -1.20000 AFIX 0 C27 1 0.042737 0.776738 0.614732 11.00000 0.02725 0.05172 = 0.02284 0.00166 0.00297 0.01866 AFIX 43 H27 2 0.013233 0.807639 0.593533 11.00000 -1.20000 AFIX 0 C28 1 0.041083 0.692946 0.658679 11.00000 0.02065 0.05662 = 0.03494 0.00608 0.00700 0.00238 AFIX 43 H28 2 0.010373 0.665848 0.667727 11.00000 -1.20000 AFIX 0 C29 1 0.084217 0.648271 0.689645 11.00000 0.02618 0.03294 = 0.03043 0.00784 0.00780 0.00178 AFIX 43 H29 2 0.082709 0.590580 0.719875 11.00000 -1.20000 AFIX 0 C30 1 0.295520 0.515923 0.575827 11.00000 0.01374 0.02285 = 0.01184 -0.00206 0.00268 0.00134 C31 1 0.302791 0.431708 0.621260 11.00000 0.01774 0.02301 = 0.01590 -0.00080 0.00338 -0.00174 AFIX 43 H31 2 0.275891 0.390221 0.625894 11.00000 -1.20000 AFIX 0 C32 1 0.348957 0.407752 0.659861 11.00000 0.02342 0.02248 = 0.01589 0.00116 0.00262 0.00378 AFIX 43 H32 2 0.353227 0.349761 0.689927 11.00000 -1.20000 AFIX 0 C33 1 0.389097 0.467877 0.654965 11.00000 0.01605 0.02867 = 0.01630 -0.00425 0.00193 0.00456 C34 1 0.381776 0.551365 0.609454 11.00000 0.01566 0.02586 = 0.01850 -0.00456 0.00423 -0.00306 AFIX 43 H34 2 0.408656 0.592965 0.605035 11.00000 -1.20000 AFIX 0 C35 1 0.335680 0.575282 0.570103 11.00000 0.01908 0.02013 = 0.01501 -0.00096 0.00438 0.00070 AFIX 43 H35 2 0.331623 0.632649 0.539071 11.00000 -1.20000 AFIX 0 C36 1 0.438604 0.442876 0.699663 11.00000 0.01872 0.03936 = 0.02734 -0.00074 -0.00160 0.00644 AFIX 137 H36A 2 0.464113 0.479438 0.675740 11.00000 -1.20000 H36B 2 0.444753 0.374787 0.693246 11.00000 -1.20000 H36C 2 0.439072 0.458182 0.759007 11.00000 -1.20000 AFIX 0 C41 1 0.095966 0.347968 0.514021 11.00000 0.02505 0.02817 = 0.03274 -0.00069 0.00001 -0.00016 AFIX 23 H41A 2 0.090872 0.285315 0.539689 11.00000 -1.20000 H41B 2 0.126417 0.375892 0.542341 11.00000 -1.20000 AFIX 0 H22 2 0.230462 0.672831 0.636067 11.00000 0.04753 HKLF 4 REM CMAS4 REM wR2 = 0.1065, GooF = S = 1.089, Restrained GooF = 1.089 for all data REM R1 = 0.0372 for 5755 Fo > 4sig(Fo) and 0.0436 for all 6726 data REM 393 parameters refined using 1 restraints END WGHT 0.0608 2.6311 REM Instructions for potential hydrogen bonds EQIV $1 -x+1/2, y-1/2, -z+1/2 HTAB C7 O4_$1 EQIV $2 x, -y+1, z-1/2 HTAB C15 O21_$2 HTAB C20 S3 HTAB C20 O3 EQIV $3 -x+1/2, -y+3/2, -z+1 HTAB C20 O3_$3 HTAB C41 O21 HTAB N22 S3_$3 HTAB N22 O3_$3 REM Highest difference peak 0.368, deepest hole -0.385, 1-sigma level 0.056 Q1 1 0.2717 0.5258 0.5549 11.00000 0.05 0.37 Q2 1 0.3562 0.3655 0.3297 11.00000 0.05 0.36 Q3 1 0.2193 0.6405 0.4042 11.00000 0.05 0.35 Q4 1 0.1077 0.6498 0.4150 11.00000 0.05 0.34 Q5 1 0.1868 0.6530 0.3402 11.00000 0.05 0.33 ; _shelx_res_checksum 72655 _shelx_hkl_file ; -1 -1 0 -1.44 1.21 1 -1 0 -0.42 0.81 1 1 0 -0.01 0.59 1 -1 0 -0.06 0.78 2 0 -1 -0.48 0.52 -2 0 1 0.59 0.96 -1 -1 1 1793.96 8.76 1 1 -1 1791.65 14.11 -1 1 1 1536.58 9.06 -1 1 1 1445.35 9.67 -1 -1 1 1700.89 7.27 2 0 1 1.41 2.14 -2 0 -1 0.64 0.93 -2 0 -1 -0.94 1.59 2 0 1 1.19 0.64 -2 0 -1 0.44 0.59 2 0 1 -0.53 0.62 1 1 1 228.48 5.61 -1 1 -1 289.60 4.79 1 -1 1 228.31 4.22 -1 -1 -1 262.41 5.01 -1 -1 -1 218.74 5.62 1 -1 1 246.91 7.22 1 1 1 2.04 3.09 1 1 1 256.27 4.25 -1 -1 -1 232.99 4.16 1 -1 1 271.17 4.55 -1 -1 -1 -0.19 2.91 -1 1 -1 -0.59 3.37 1 1 1 -0.09 2.92 0 0 -2 84.89 4.43 0 0 2 79.86 4.43 0 0 2 71.11 5.40 0 0 -2 67.16 5.71 -3 -1 0 22.81 3.51 3 -1 0 40.70 2.46 -3 1 0 42.91 2.51 3 1 0 36.92 2.36 3 1 0 45.78 3.77 3 1 0 38.54 2.49 -3 -1 0 41.19 2.38 3 -1 0 44.17 2.47 -3 1 0 41.81 2.51 -3 -1 0 45.12 2.51 2 0 -2 491.61 11.07 -2 0 2 431.53 9.91 -2 0 2 451.05 11.27 3 1 -1 2316.47 115.05 -3 1 1 5283.03 116.18 -3 1 1 5524.41 116.10 -3 -1 1 5159.41 115.64 3 1 -1 5279.79 115.93 3 1 -1 5434.57 117.83 3 -1 -1 5232.91 116.12 -3 -1 1 5491.17 116.08 3 -1 -1 841.22 114.79 -3 -1 1 3125.17 116.51 0 -2 0 3629.26 113.46 0 -2 0 2717.06 113.12 0 -2 0 3252.77 113.10 0 2 0 4095.51 113.95 1 -1 -2 53.98 4.06 -1 1 2 54.74 3.15 -1 -1 2 54.86 4.12 1 -1 -2 45.00 2.94 -1 1 2 37.06 2.97 -1 -1 2 65.32 8.46 -1 -1 2 56.61 3.55 1 -1 -2 54.71 4.09 -1 1 2 77.44 4.06 -1 -1 2 60.68 2.80 4 0 0 1.21 2.45 4 0 0 2.81 1.51 4 0 0 2.85 1.26 -4 0 0 1.78 1.71 -4 0 0 2.29 1.46 -3 1 -1 1180.29 46.15 -3 -1 -1 1234.85 46.11 3 1 1 1213.45 47.47 -3 -1 -1 1175.97 47.38 -3 -1 -1 1175.85 46.11 3 -1 1 1153.86 45.92 3 -1 1 1267.09 46.15 3 1 1 1203.34 46.11 -3 1 -1 1071.83 47.13 3 -1 1 1127.21 47.15 2 0 2 934.91 35.77 -2 0 -2 945.64 34.50 2 0 2 961.07 34.61 -2 0 -2 890.86 35.59 1 1 2 2163.89 93.08 -1 1 -2 2815.50 93.46 -1 -1 -2 2265.17 93.58 -1 -1 -2 2093.02 93.85 1 1 2 2133.38 94.01 1 -1 2 2495.96 95.21 1 -1 2 2668.79 93.43 -1 1 -2 2401.28 95.21 1 1 2 2078.29 93.55 1 -1 2 2738.09 92.81 1 1 2 2344.34 92.82 4 0 -1 2.80 1.55 -4 0 1 -0.30 1.39 4 0 -1 -0.80 2.55 -4 0 1 0.32 2.06 4 0 -1 0.41 1.42 0 2 -1 64.84 4.69 0 -2 1 77.27 4.44 0 2 -1 74.30 4.56 0 2 1 73.46 4.41 0 -2 -1 64.40 4.35 0 -2 -1 68.51 4.22 0 -2 -1 90.36 4.64 0 2 1 54.80 4.51 0 -2 1 65.49 4.68 -2 2 0 7702.43 280.96 2 -2 0 6561.40 280.41 2 2 0 6867.49 281.59 -2 -2 0 6679.00 281.39 2 2 0 6430.56 280.45 2 -2 0 6877.08 280.71 -2 -2 0 6696.42 280.49 -2 2 0 7600.11 280.94 -4 0 -1 0.02 1.64 4 0 1 1.16 1.32 -4 0 -1 0.86 3.10 4 0 1 1.48 3.41 4 0 1 0.04 0.90 -2 2 1 891.18 32.11 -2 -2 1 1033.27 32.06 2 2 -1 826.63 33.14 -2 -2 1 865.17 31.58 2 -2 -1 1032.22 32.42 2 -2 -1 884.38 31.99 -2 -2 1 842.58 32.96 2 2 -1 899.59 31.64 -3 1 2 790.31 33.21 3 -1 -2 897.85 33.33 3 1 -2 825.59 33.07 -3 1 2 887.02 33.06 -3 -1 2 828.09 32.73 -3 -1 2 853.82 33.29 3 1 -2 815.96 34.32 -3 -1 2 891.27 34.57 -3 -1 2 817.71 33.09 2 -2 1 3957.79 144.32 -2 -2 -1 3894.41 144.24 -2 2 -1 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2.60 2.96 0 -8 0 5.24 5.94 0 -8 0 3.17 5.90 0 -8 0 3.30 5.64 -5 -7 -3 89.65 10.50 5 -7 3 95.62 7.43 5 -7 3 87.11 11.46 5 7 3 90.70 6.67 -5 -7 -3 78.99 6.60 -5 7 -3 111.19 8.74 -5 -7 -3 105.56 9.60 -5 7 -3 116.40 9.21 5 7 3 86.17 9.53 5 -7 3 82.23 8.40 5 -7 3 107.83 7.40 10 2 6 1778.77 21.06 -10 -2 -6 1773.40 21.76 10 -2 6 1624.94 20.00 -10 2 -6 1669.77 21.45 10 2 6 1741.48 35.69 10 -2 6 1761.71 35.69 -10 -2 -6 1764.28 36.15 10 -2 6 1759.08 27.78 -10 -2 -6 1795.67 24.10 -10 -2 -6 1667.55 18.57 10 2 6 1901.55 29.93 -8 -2 -7 191.44 10.35 -8 -2 -7 180.39 15.05 8 -2 7 213.79 12.04 8 2 7 200.72 12.75 8 -2 7 190.37 8.70 -8 -2 -7 190.09 8.46 -8 2 -7 197.74 9.14 -8 -2 -7 174.54 8.78 8 -2 7 207.84 15.68 8 2 7 195.51 8.99 8 -2 -8 69.65 4.70 8 -2 -8 57.19 7.67 -8 -2 8 57.90 4.15 8 -2 -8 68.75 6.83 8 2 -8 61.74 7.18 -8 2 8 70.84 7.44 8 2 -8 62.59 4.01 -8 -2 8 66.02 6.29 -8 -2 8 56.63 9.50 -8 2 8 67.90 5.84 -8 2 8 68.98 9.23 8 2 -8 67.91 5.36 -8 2 8 53.00 4.95 -8 -2 8 70.73 14.24 -10 -6 -1 17.78 3.69 10 6 1 16.45 3.99 10 -6 1 19.52 4.25 -10 -6 -1 18.76 4.40 -10 -6 -1 26.54 9.78 -10 6 -1 23.71 4.78 10 -6 1 24.58 4.63 10 6 1 19.41 3.08 10 -6 1 15.87 5.31 -10 6 -1 31.15 9.00 -7 3 -7 126.42 6.77 7 -3 7 101.78 8.05 -7 -3 -7 96.19 7.24 -7 -3 -7 91.84 5.69 7 -3 7 90.25 11.32 -7 -3 -7 55.79 6.04 -7 -3 -7 95.51 11.67 7 3 7 70.70 10.29 7 -3 7 98.74 5.56 7 3 7 102.07 9.42 7 3 7 101.21 5.88 -1 -1 -9 729.43 18.53 -1 1 -9 720.26 9.05 -1 -1 -9 647.87 23.51 1 1 9 720.24 19.30 -1 1 -9 707.91 26.51 1 -1 9 773.10 19.46 1 1 9 708.51 22.13 -1 -1 -9 756.27 10.85 1 -1 9 707.77 9.12 1 1 9 736.75 10.77 -10 4 6 702.91 35.29 10 4 -6 939.26 41.57 -10 -4 6 939.50 36.23 10 4 -6 919.71 36.37 -10 4 6 1117.35 38.82 -10 -4 6 937.63 37.56 10 4 -6 957.54 37.48 -10 4 6 882.82 38.19 10 -4 -6 937.35 37.11 10 4 -6 867.98 37.08 13 -3 3 1901.69 73.94 -13 -3 -3 1977.17 74.63 -13 3 -3 1825.39 74.96 13 -3 3 1914.52 78.42 -13 -3 -3 2082.54 80.51 -13 3 -3 1896.05 74.42 -13 3 -3 1870.23 79.45 13 3 3 2177.06 75.84 13 3 3 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2549.62 69.70 -3 -7 -4 1903.79 69.63 -3 7 -4 2405.09 70.73 -3 -7 -4 1868.54 67.33 -9 -1 8 466.48 18.85 9 1 -8 480.20 18.84 9 -1 -8 400.40 20.22 9 1 -8 450.22 20.14 -9 1 8 474.14 22.72 9 1 -8 436.68 22.38 -9 1 8 415.96 25.10 -9 1 8 471.80 20.91 9 -1 -8 429.15 18.99 -9 -1 8 458.07 20.59 -9 1 8 452.48 19.25 -9 -1 8 526.97 24.37 -2 -8 0 2949.84 118.08 2 -8 0 3765.24 118.75 -2 -8 0 2880.39 115.81 -2 8 0 3089.29 118.64 2 -8 0 3005.15 117.37 -2 8 0 2912.34 117.12 2 8 0 2962.68 118.58 -2 -8 0 3498.58 118.79 2 -8 0 3413.00 117.61 2 0 9 1.89 6.51 -2 0 -9 0.42 4.14 2 0 9 -0.97 8.39 -2 0 -9 1.50 1.71 -2 0 -9 7.88 10.62 2 0 9 1.42 1.81 0 4 8 306.85 18.29 0 -4 -8 316.10 19.30 0 4 8 292.68 15.65 0 -4 8 377.01 14.00 0 -4 8 350.53 14.62 0 -4 8 332.40 18.83 0 -4 8 333.22 17.45 0 -4 -8 300.90 17.57 0 -4 -8 376.67 16.51 0 -4 -8 349.56 14.76 0 4 8 351.56 18.96 0 -4 8 353.39 24.08 0 4 -8 314.32 15.95 0 -4 8 441.38 14.79 11 -5 -4 88.18 7.07 -11 5 4 52.46 6.51 -11 -5 4 64.19 10.72 11 -5 -4 71.00 6.22 -11 5 4 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36.52 3.48 -14 8 -1 16.84 14.51 -14 -8 -1 23.77 5.11 -14 8 -1 6.60 4.91 14 -8 1 8.64 4.88 21 1 0 2331.58 91.85 -21 -1 0 2304.98 87.11 -21 -1 0 2334.18 87.43 -21 1 0 2294.11 87.04 -21 1 0 2381.95 93.24 -21 1 0 2155.57 86.95 21 1 0 2015.15 85.53 21 -1 0 1803.03 85.18 21 -1 0 2531.22 92.13 -1 -9 7 143.76 9.14 -1 9 7 127.50 10.27 -1 -9 7 128.68 8.09 1 -9 -7 119.42 8.67 -1 -9 7 121.18 8.65 -1 -9 7 147.94 10.31 -1 -9 7 134.23 10.49 -1 -9 7 102.95 17.39 1 -9 -7 121.03 10.89 -9 -9 -4 1188.03 53.35 9 -9 4 1312.99 53.56 9 9 4 1153.90 57.42 9 -9 4 1193.56 54.53 9 -9 4 1250.82 59.15 -9 -9 -4 1223.86 51.38 -7 7 9 2.79 6.17 7 7 -9 16.03 4.09 -7 -7 9 9.60 5.79 -7 -7 9 12.17 5.72 -7 -7 9 22.65 21.87 7 -7 -9 14.08 6.20 7 -7 -9 16.21 7.73 -7 -7 9 13.42 4.42 -7 7 9 11.79 5.50 -7 -7 9 14.71 3.29 14 -4 -9 119.51 12.82 -14 -4 9 116.57 9.45 14 4 -9 117.09 12.73 -14 4 9 120.01 9.38 14 4 -9 115.64 9.93 14 -4 -9 126.01 8.62 -14 4 9 112.61 9.37 -14 4 9 118.58 10.56 -14 -4 9 116.43 8.02 -14 4 9 131.77 10.30 14 4 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1211.09 50.13 0 -10 -5 1195.68 49.31 0 -10 -5 1249.78 50.50 0 -10 -5 1093.88 48.06 -2 -10 5 17.26 3.88 -2 10 5 15.48 7.12 2 -10 -5 12.23 6.37 -2 10 5 16.64 6.30 2 -10 -5 17.94 4.43 -1 -5 -11 1.05 4.80 -1 -5 -11 4.45 10.48 1 -5 11 6.36 2.59 -1 -5 -11 4.65 2.73 1 -5 11 -4.91 13.82 1 5 11 3.45 4.56 -1 -5 -11 5.09 6.42 -1 5 -11 2.23 4.51 -1 -5 -11 -0.25 5.17 1 5 11 7.24 8.29 13 -7 5 325.64 15.48 -13 -7 -5 361.26 17.16 -13 -7 -5 310.07 16.36 -13 7 -5 401.20 17.77 13 7 5 327.51 18.09 -13 7 -5 273.02 23.84 13 7 5 295.79 21.76 -13 7 -5 362.64 18.72 13 -7 5 333.47 21.72 5 -5 -11 245.84 13.80 5 5 -11 209.68 12.97 5 -5 -11 187.24 11.68 -5 5 11 233.31 13.50 5 5 -11 269.46 12.89 5 -5 -11 212.73 16.03 -5 5 11 242.68 16.51 -5 -5 11 224.69 15.01 5 -5 -11 237.03 11.41 5 -5 -11 142.94 16.46 -5 -5 11 225.98 12.14 -13 1 -9 227.44 10.96 13 1 9 229.49 18.45 -13 -1 -9 213.79 10.94 13 1 9 241.45 10.69 -13 -1 -9 188.45 8.26 13 -1 9 223.99 10.46 13 -1 9 247.64 20.02 -10 -6 -8 162.32 9.51 10 6 8 161.61 15.36 -10 -6 -8 165.79 10.61 10 6 8 171.34 9.81 -10 6 -8 186.57 10.82 10 6 8 174.13 13.84 10 -6 8 157.91 16.49 10 -6 8 167.79 8.95 -18 -4 6 24.10 5.55 18 4 -6 30.91 10.07 -18 4 6 35.14 6.70 -18 4 6 27.12 6.12 -18 4 6 23.67 5.79 -18 -4 6 30.47 6.07 18 4 -6 26.28 6.20 6 10 -4 2662.80 120.12 -6 -10 4 3026.18 115.80 -6 10 4 2662.78 119.40 -6 10 4 2719.12 118.41 -4 0 -12 13.41 5.32 4 0 12 23.37 11.70 1 -9 7 1897.98 69.99 1 -9 7 1488.36 78.15 1 9 7 1699.90 70.93 1 -9 7 1595.15 68.03 1 -9 7 1931.83 69.49 1 -9 7 1618.70 67.56 -1 -9 -7 1555.24 68.27 -1 -9 -7 1580.12 70.06 1 -9 7 1869.66 68.99 -1 -9 -7 1663.13 71.76 1 9 7 1576.65 70.17 -14 -2 10 94.75 9.02 -14 -2 10 103.31 24.57 14 2 -10 101.25 6.42 14 -2 -10 87.30 7.25 -14 2 10 74.53 7.20 -14 2 10 83.81 13.11 14 -2 -10 93.36 11.16 14 2 -10 91.51 9.98 -14 2 10 92.58 8.21 -14 -2 10 100.32 13.47 -14 2 10 82.30 10.57 -14 -2 10 94.26 6.43 -12 4 10 249.54 14.79 12 4 -10 251.99 15.18 12 4 -10 275.26 12.42 12 -4 -10 284.26 13.11 -12 4 10 148.18 12.51 12 -4 -10 270.24 17.81 -12 4 10 257.69 14.86 -12 -4 10 129.67 29.11 -12 4 10 246.18 15.40 -12 -4 10 236.88 14.20 -12 -4 10 261.89 12.32 -17 -5 6 -0.15 4.79 -17 5 6 1.40 5.05 17 5 -6 0.27 8.82 -17 5 6 1.83 5.30 -17 5 6 0.64 4.84 17 5 -6 1.73 4.51 -17 -5 6 -0.96 3.89 -19 5 1 82.90 8.10 -19 5 1 71.32 11.02 -19 -5 1 82.99 7.57 19 -5 -1 94.59 9.76 -19 5 1 85.60 8.31 19 5 -1 80.63 12.43 -19 -5 1 86.59 7.43 20 -2 -5 335.41 18.81 -20 2 5 330.91 16.77 20 2 -5 334.52 21.51 -20 2 5 358.05 20.91 -20 -2 5 357.11 23.61 -20 -2 5 321.18 16.73 12 6 7 2212.80 100.15 12 6 7 2358.98 94.17 -12 -6 -7 1520.71 94.55 -12 -6 -7 1993.53 93.92 -12 -6 -7 2551.97 94.61 12 -6 7 2559.07 93.91 -12 6 -7 3370.42 98.81 -12 -6 -7 2463.99 94.36 12 -6 7 2460.94 101.58 12 6 7 2685.10 98.13 -15 -7 -3 2348.03 96.54 -15 7 -3 2451.14 96.71 15 -7 3 2233.84 95.39 15 7 3 2697.17 96.56 -15 7 -3 2106.09 102.34 15 -7 3 2274.63 99.02 -15 7 -3 2620.72 98.71 -19 5 2 53.77 7.40 -19 -5 2 118.28 8.78 19 -5 -2 69.45 8.27 -19 -5 2 114.55 8.44 -19 5 2 59.91 7.52 19 5 -2 76.34 13.48 -19 5 2 48.08 8.98 16 -2 7 925.13 38.28 -16 -2 -7 941.36 37.50 16 2 7 949.64 46.37 16 -2 7 913.55 45.40 -16 2 -7 903.81 38.94 -16 -2 -7 889.08 38.95 16 2 7 960.34 38.64 4 -8 8 299.65 14.02 4 8 8 210.79 16.70 -4 -8 -8 234.48 14.49 -4 -8 -8 233.65 17.85 -4 -8 -8 155.69 13.86 4 -8 8 246.71 12.44 4 -8 8 260.77 13.13 -4 8 -8 314.76 16.19 -4 -8 -8 236.96 12.97 4 -8 8 234.17 13.76 4 -8 8 231.14 22.31 16 2 -9 1205.54 50.34 16 2 -9 1070.04 48.30 -16 -2 9 1110.25 45.13 -16 2 9 1067.85 45.86 -16 -2 9 1137.86 47.40 -16 2 9 1134.51 47.29 16 2 -9 1148.15 44.93 16 -2 -9 1134.33 45.40 16 -2 -9 1118.37 50.47 -16 -2 9 1274.98 52.79 -16 2 9 1233.87 49.29 -11 1 -10 255.73 12.10 -11 1 -10 260.82 13.93 11 -1 10 237.03 20.95 -11 -1 -10 237.44 12.09 -11 -1 -10 250.22 14.12 11 1 10 235.47 20.17 5 3 -12 19.46 4.62 -5 3 12 24.25 5.17 5 -3 -12 26.95 2.91 5 -3 -12 26.56 6.64 5 -3 -12 28.55 8.21 -5 3 12 29.18 10.03 5 3 -12 21.14 6.89 -5 -3 12 28.88 5.43 5 -3 -12 23.49 3.21 5 -3 -12 6.98 13.26 -5 -3 12 36.77 15.67 17 -5 4 326.54 15.69 17 5 4 370.53 23.45 -17 5 -4 342.43 24.99 -17 -5 -4 334.73 16.44 17 -5 4 317.79 21.09 -17 -5 -4 287.59 16.10 -17 5 -4 353.21 16.43 -17 5 -4 319.60 17.16 17 5 4 354.96 17.97 15 7 -5 179.05 16.89 -15 -7 5 186.03 11.06 -15 -7 5 189.32 11.97 -15 7 5 200.85 13.40 16 -4 6 47.79 11.95 -16 -4 -6 55.22 5.21 -16 4 -6 63.95 5.13 -16 4 -6 58.27 6.50 16 4 6 53.50 9.07 16 -4 6 49.06 6.46 -16 -4 -6 54.29 6.14 16 4 6 52.02 12.44 4 -6 10 835.88 29.23 4 -6 10 789.37 42.29 -4 -6 -10 741.49 31.92 -4 -6 -10 749.96 36.47 -4 -6 -10 775.39 34.04 -4 -6 -10 716.18 29.93 4 6 10 749.80 35.88 -19 5 0 -5.07 9.22 19 5 0 10.05 4.16 -19 5 0 2.15 4.61 -19 -5 0 1.01 4.26 -19 -5 0 4.47 4.55 19 -5 0 2.18 5.93 -19 5 0 1.68 4.55 19 -5 0 -8.45 7.87 13 5 -9 644.45 26.77 -13 5 9 625.25 27.22 13 5 -9 731.32 25.27 -13 -5 9 661.19 26.54 13 5 -9 663.09 31.44 13 -5 -9 694.03 25.99 13 -5 -9 733.79 31.86 -13 -5 9 633.84 24.43 -16 -4 8 1.75 5.30 -16 4 8 -1.15 5.10 -16 4 8 1.06 5.06 16 4 -8 6.03 8.05 -16 4 8 2.14 5.37 16 4 -8 3.62 3.78 -16 -4 8 3.42 4.55 16 4 -8 2.98 5.17 16 -4 -8 4.56 4.97 21 -1 1 84.70 6.68 -21 1 -1 96.47 14.80 21 -1 1 95.42 13.02 -21 1 -1 85.02 7.58 -21 -1 -1 74.52 8.28 21 1 1 81.80 6.62 21 1 1 92.98 13.20 15 -5 6 1326.34 62.93 15 -5 6 1326.74 57.02 -15 -5 -6 1348.87 57.57 -15 -5 -6 1338.54 57.07 15 5 6 1437.63 60.34 -15 5 -6 1469.43 59.22 -1 -3 -12 538.21 28.62 -1 3 -12 572.69 21.68 1 3 12 583.00 18.84 -1 -3 -12 597.38 24.35 1 3 12 559.86 26.53 18 6 -1 46.71 5.05 -18 -6 1 23.78 4.89 -18 6 1 18.80 5.62 -18 -6 1 38.21 6.17 18 -6 -1 24.88 7.13 -18 6 1 28.42 6.81 -18 6 1 19.59 9.07 20 4 -1 1458.18 62.55 -20 4 1 1299.72 56.64 20 -4 -1 1383.31 58.43 -20 4 1 1386.39 57.21 -20 4 1 1339.74 59.24 -20 -4 1 1351.04 56.68 -20 -4 1 1338.61 56.12 2 -10 5 131.25 10.94 2 -10 5 90.77 6.78 -2 -10 -5 103.65 8.24 -2 -10 -5 123.39 12.82 -2 -10 -5 104.27 9.27 2 10 5 106.44 11.18 2 -10 5 101.55 7.35 2 -10 5 96.53 15.65 1 -11 0 70.30 6.91 -1 -11 0 84.11 10.75 -1 -11 0 81.04 7.18 -1 11 0 74.67 9.46 1 -11 0 79.96 10.57 1 11 0 78.85 10.49 -11 -9 4 15.02 4.35 -11 9 4 12.89 7.02 -11 -9 4 18.38 5.52 18 4 4 393.50 18.57 -18 -4 -4 320.26 17.07 18 -4 4 321.31 15.70 18 4 4 347.70 23.56 -18 4 -4 360.49 16.69 -18 4 -4 355.78 24.83 -18 4 -4 355.70 17.96 18 -4 4 370.00 22.80 -18 -4 -4 327.53 16.52 15 1 8 113.68 6.00 -15 -1 -8 10.70 3.69 -15 -1 -8 95.25 6.55 -15 1 -8 11.84 1.68 15 -1 8 102.56 13.22 -15 1 -8 96.68 6.15 15 -1 8 89.76 5.59 15 1 8 95.99 13.64 4 -10 -5 1922.80 76.41 -4 10 5 1733.38 76.18 -4 -10 5 1953.12 74.34 -4 10 5 1880.28 73.18 -4 -10 5 1736.00 72.79 10 8 -7 4366.27 168.83 -10 8 7 3814.43 171.23 10 8 -7 4217.76 174.76 -10 8 7 4394.17 171.27 -10 -8 7 4465.14 168.60 -10 -8 7 4435.20 169.81 18 0 -8 787.68 35.16 -18 0 8 832.05 37.47 18 0 -8 842.12 39.19 -18 0 8 866.87 36.01 20 4 -2 933.23 44.89 -20 4 2 960.77 41.95 -20 -4 2 880.15 39.51 -20 4 2 938.46 39.97 -20 4 2 848.03 39.60 20 -4 -2 971.62 40.79 -20 -4 2 899.02 39.04 -8 10 -2 267.94 16.98 -8 10 -2 262.82 16.45 8 10 2 228.24 17.62 8 -10 2 209.67 17.97 8 -10 2 218.40 14.68 -8 -10 -2 227.73 13.18 -8 -10 3 1380.07 58.36 -8 -10 3 1238.24 56.73 -8 10 3 1431.38 60.80 7 5 10 414.35 25.77 -7 -5 -10 389.29 21.16 -7 -5 -10 383.23 20.03 7 5 10 438.20 19.33 -7 -5 -10 403.93 19.06 -19 3 6 679.44 29.82 19 -3 -6 725.38 30.08 -19 3 6 531.60 29.52 -19 -3 6 710.38 30.91 19 3 -6 724.39 35.13 -19 -3 6 593.33 28.72 -19 3 6 771.68 31.98 -18 -6 2 266.64 14.99 -18 -6 2 247.74 13.96 -18 6 2 240.96 16.35 -18 6 2 255.19 15.39 -18 6 2 260.92 16.23 -14 8 -2 111.21 9.37 14 8 2 97.81 6.84 -14 -8 -2 103.36 8.44 -14 -8 -2 90.24 7.91 14 -8 2 110.25 8.29 -14 8 -2 114.37 9.87 14 -8 2 103.40 10.92 1 11 -1 1.56 7.30 -1 -11 1 -2.17 8.06 -1 -11 1 -1.18 3.82 1 -11 -1 1.08 7.35 1 -11 -1 1.98 3.95 -1 11 1 -1.48 6.76 19 -1 -7 5675.89 213.61 -19 -1 7 5692.24 212.85 19 1 -7 5627.26 215.20 -19 1 7 5483.57 211.30 -19 1 7 5920.28 215.35 -19 1 7 5113.40 212.39 -19 -1 7 4924.50 210.68 -19 -1 7 5739.46 216.61 11 7 -8 2.28 8.87 -11 7 8 4.13 5.05 11 -7 -8 1.21 7.82 11 7 -8 6.31 3.31 -11 -7 8 5.67 4.65 11 7 -8 8.51 3.98 11 -7 -8 0.95 5.49 -11 -7 8 6.11 3.43 -11 7 8 5.18 5.90 -5 -9 7 139.04 9.58 5 -9 -7 140.00 12.01 -5 -9 7 140.67 8.46 -5 -9 7 166.56 11.66 -5 9 7 162.11 12.11 17 3 -8 46.87 10.44 -17 -3 8 37.14 5.79 -17 -3 8 49.38 8.07 17 3 -8 46.74 5.22 -17 3 8 51.81 8.14 17 -3 -8 40.66 6.61 17 3 -8 44.10 7.48 -17 3 8 42.21 6.14 -17 3 8 42.24 6.44 1 11 1 5.39 6.92 -1 -11 -1 2.19 4.07 -1 -11 -1 3.48 8.13 1 -11 1 7.57 8.54 -1 -11 -1 6.53 4.73 -1 11 -1 1.86 6.74 1 -11 1 2.54 3.97 -18 -6 0 38.74 5.43 18 6 0 44.78 4.85 -18 -6 0 44.10 5.80 -18 6 0 35.78 6.78 18 -6 0 43.16 6.55 -18 6 0 28.33 10.47 18 -6 0 59.01 8.44 18 6 0 53.10 11.86 -18 6 0 36.00 5.71 8 -6 9 553.71 33.12 8 6 9 614.07 29.79 8 6 9 554.89 24.16 8 6 9 471.65 29.37 -8 -6 -9 412.54 24.91 -8 -6 -9 492.68 25.47 8 -6 9 556.90 23.47 -8 6 -9 664.72 26.30 -8 -6 -9 561.37 24.26 5 7 9 191.62 16.90 -5 -7 -9 200.93 14.02 -5 -7 -9 219.80 18.21 5 -7 9 236.31 11.47 -5 -7 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10.52 16 -6 4 168.14 16.20 -16 6 -4 186.16 12.65 21 -1 -4 0.22 7.93 -21 -1 4 -3.31 5.03 -21 -1 4 -5.77 6.69 -21 1 4 2.86 9.80 -21 -1 4 -4.09 11.88 -21 1 4 -1.39 4.00 -21 1 4 -2.74 5.57 21 1 -4 4.68 8.97 15 -5 -8 51.88 6.40 -15 5 8 61.46 7.45 -15 5 8 42.27 4.15 15 5 -8 49.42 9.99 15 5 -8 58.42 5.57 -15 5 8 56.20 7.35 -15 -5 8 61.62 5.62 -15 5 8 25.94 3.55 -15 -5 8 48.72 6.41 15 5 -8 57.27 6.90 -20 0 6 3.78 4.20 20 0 -6 6.30 8.32 -20 0 6 0.95 5.55 -20 0 6 2.47 10.59 -16 6 6 85.78 8.62 -16 -6 6 91.94 8.29 -16 -6 6 90.48 7.06 -16 6 6 98.69 9.43 16 6 -6 105.01 13.08 16 6 -6 90.77 7.06 8 2 -12 10.29 4.57 -8 -2 12 9.36 5.36 -8 2 12 11.49 5.30 8 2 -12 10.76 6.72 -8 2 12 20.01 10.70 -8 -2 12 0.47 13.94 8 -2 -12 8.58 3.34 -8 2 12 3.74 8.98 8 -2 -12 11.52 6.28 -11 3 11 53.07 8.65 -11 -3 11 52.17 4.45 -11 -3 11 54.78 7.94 -11 3 11 49.27 10.23 11 -3 -11 60.97 5.53 11 3 -11 57.65 8.62 -11 3 11 59.15 7.35 11 3 -11 63.79 4.63 -11 -3 11 58.33 16.91 -12 2 11 3257.58 124.88 -12 2 11 2444.72 120.44 -12 -2 11 3224.40 119.71 12 2 -11 3334.87 125.05 -12 2 11 3079.80 122.53 12 -2 -11 2630.26 124.61 -12 -2 11 2982.56 133.03 -12 2 11 3311.95 128.26 12 2 -11 3220.65 119.57 12 -2 -11 3229.37 119.99 -12 -2 11 3033.31 122.15 -13 -7 7 319.70 15.38 -13 7 7 328.42 18.19 13 7 -7 282.23 14.02 -13 7 7 300.82 17.10 13 7 -7 305.11 15.53 13 7 -7 301.45 21.36 -13 -7 7 322.38 16.62 9 -1 -12 14.57 2.41 9 -1 -12 8.74 6.99 9 1 -12 14.39 4.58 9 -1 -12 11.65 4.86 -9 -1 12 1.69 13.56 -9 1 12 11.53 11.83 9 1 -12 14.78 2.08 -9 -1 12 14.11 5.11 9 1 -12 10.35 7.06 -9 -1 12 12.78 9.50 -9 1 12 12.97 4.97 -9 1 12 8.88 8.57 20 2 3 2.07 10.22 -20 2 -3 0.90 3.96 -20 -2 -3 4.67 5.31 20 -2 3 -2.83 9.77 20 2 3 1.46 5.43 -20 -2 -3 3.09 5.01 20 2 3 3.60 3.79 20 -2 3 0.77 3.05 -20 2 -3 2.26 3.58 -14 8 4 69.41 8.45 -14 -8 4 75.04 6.66 14 8 -4 70.64 12.46 -14 -8 4 77.98 7.53 12 8 -6 173.41 15.65 -12 8 6 162.59 11.43 12 8 -6 122.43 5.97 -12 -8 6 164.26 9.25 -12 -8 6 158.02 10.17 -12 8 6 142.59 11.66 3 -9 7 333.95 17.48 -3 -9 -7 351.03 22.06 -3 -9 -7 341.60 19.02 3 -9 7 340.29 27.89 3 -9 7 413.45 18.73 -3 -9 -7 324.06 17.51 3 -9 7 354.88 16.96 3 9 7 341.58 20.74 11 -9 3 340.96 17.74 -11 -9 -3 345.41 18.29 11 -9 3 298.61 20.87 11 9 3 304.42 22.20 -11 9 -3 362.86 20.15 11 -9 3 320.22 18.69 17 3 6 588.89 28.47 17 3 6 617.29 32.70 -17 3 -6 596.13 24.29 17 -3 6 548.47 31.14 -17 -3 -6 526.66 25.40 -17 3 -6 555.86 25.83 -17 -3 -6 574.06 24.58 -15 1 10 321.47 15.25 15 -1 -10 288.95 19.30 15 1 -10 289.68 18.29 15 -1 -10 291.92 14.37 15 1 -10 287.06 14.20 -15 -1 10 301.15 32.42 -15 1 10 297.09 16.78 -15 1 10 329.58 20.00 -15 -1 10 304.36 16.71 -15 1 10 259.67 22.38 -15 -1 10 315.30 14.66 -15 -1 10 274.97 20.08 3 -11 0 541.15 26.36 3 -11 0 645.43 29.25 -3 -11 0 576.83 26.59 -3 -11 0 635.74 30.91 -3 11 0 576.01 28.32 3 11 0 576.37 30.44 -20 4 3 198.06 13.02 20 -4 -3 245.18 14.01 -20 -4 3 193.32 12.71 -20 -4 3 207.27 12.24 -20 4 3 209.19 14.67 -20 4 3 215.98 12.99 20 4 -3 202.86 17.12 11 5 -10 470.91 22.33 -11 -5 10 513.31 19.98 -11 5 10 487.88 21.62 -11 -5 10 518.44 22.28 -11 5 10 513.38 23.16 -11 5 10 493.29 21.89 11 -5 -10 480.46 25.79 11 5 -10 558.65 20.65 11 -5 -10 504.12 21.14 19 -5 1 259.15 17.60 19 -5 1 216.17 13.77 -19 -5 -1 267.33 14.40 19 5 1 251.30 19.37 19 5 1 267.08 13.28 -19 5 -1 223.73 19.01 -19 -5 -1 262.51 14.07 -19 5 -1 248.55 14.30 4 2 12 119.82 14.46 -4 -2 -12 144.19 6.88 -4 -2 -12 123.17 10.07 -3 5 -11 19.33 4.90 -3 -5 -11 0.77 6.38 -3 -5 -11 20.31 3.18 3 5 11 19.11 9.55 3 -5 11 17.71 13.80 -3 -5 -11 21.50 7.00 -3 -5 -11 18.79 5.49 3 5 11 15.93 5.68 -3 -5 -11 13.14 11.62 7 -5 -11 19.96 8.33 -7 -5 11 16.23 7.26 7 -5 -11 24.58 4.71 7 5 -11 18.66 5.25 -7 5 11 17.04 7.49 7 5 -11 20.93 5.26 -7 5 11 12.67 5.79 -7 5 11 10.93 5.30 -7 -5 11 18.26 4.72 -14 -6 -6 99.10 10.88 14 6 6 114.44 10.88 14 -6 6 88.30 7.64 14 -6 6 101.92 14.00 -14 6 -6 112.99 9.36 -14 6 -6 134.69 8.50 -14 -6 -6 96.32 7.74 -14 6 -6 95.92 18.96 -14 -6 -6 108.61 7.83 3 11 -1 343.94 22.49 -3 -11 1 376.61 18.59 -3 11 1 372.41 20.16 3 -11 -1 353.16 18.56 -18 6 3 234.38 14.55 18 6 -3 242.93 18.76 -18 6 3 267.76 15.60 -18 -6 3 227.92 13.02 10 -8 6 1895.18 73.16 -10 -8 -6 1793.95 73.73 -10 -8 -6 1820.85 72.91 -10 8 -6 1978.56 90.70 10 -8 6 1785.73 73.12 -10 8 -6 2118.63 76.66 10 8 6 1717.49 78.64 10 8 6 1890.59 75.19 10 -8 6 1843.39 80.56 8 -8 7 851.45 33.99 8 8 7 824.90 36.52 8 -8 7 802.72 42.45 -8 8 -7 1009.56 37.97 8 8 7 737.39 38.64 -8 -8 -7 757.55 33.97 -8 -8 -7 604.27 35.17 -8 -8 -7 741.48 33.91 -8 -8 8 398.92 18.03 -8 8 8 406.08 21.67 -8 8 8 416.71 21.57 8 -8 -8 369.43 22.26 -8 -8 8 404.14 19.39 -8 -8 8 440.49 20.92 8 8 -8 362.30 24.03 8 8 -8 360.28 16.96 -5 -1 -12 1571.00 40.45 -5 1 -12 1699.81 41.08 -5 -1 -12 1665.84 32.67 5 1 12 1572.30 49.45 1 -11 -2 103.47 11.04 1 11 -2 89.86 11.22 -1 -11 2 107.22 12.47 -1 11 2 89.94 9.87 1 -11 -2 91.64 7.83 -1 -11 2 98.69 7.90 -6 -10 -4 933.87 42.65 6 -10 4 1173.58 43.87 -6 -10 -4 1085.22 48.33 6 10 4 1000.24 46.82 6 -10 4 979.48 49.70 -6 10 -4 1113.74 46.52 -6 -10 -4 925.33 41.25 6 -10 4 943.22 44.85 -18 0 -6 1589.83 65.07 18 0 6 1597.83 71.54 -18 0 -6 1609.28 63.52 -3 -11 -1 350.88 18.10 3 11 1 345.65 21.29 3 -11 1 390.16 29.59 3 -11 1 338.75 17.88 3 -11 1 384.95 21.29 -3 -11 -1 416.57 23.37 1 -11 2 136.63 12.80 1 11 2 122.59 11.89 -1 -11 -2 135.96 9.46 1 -11 2 118.26 8.74 -1 -11 -2 122.53 12.87 -1 11 -2 113.22 12.10 -1 -11 -2 135.12 9.65 -19 3 -4 4195.89 178.62 -19 3 -4 4946.06 178.45 -19 -3 -4 4738.77 178.25 19 3 4 4980.12 179.92 19 -3 4 4780.24 184.07 -19 -3 -4 4016.22 178.38 19 3 4 4617.74 185.37 18 6 1 100.33 7.27 18 -6 1 95.00 10.63 -18 -6 -1 92.97 7.87 -18 6 -1 89.50 8.22 -18 6 -1 82.12 13.34 -18 -6 -1 105.06 7.95 18 -6 1 99.73 8.34 18 6 1 117.29 13.80 -7 3 12 1586.84 66.70 -7 3 12 1757.12 69.65 7 3 -12 1661.63 69.12 7 -3 -12 1741.05 64.28 7 -3 -12 1586.95 66.79 -7 3 12 1453.78 69.90 7 -3 -12 1633.63 70.48 7 3 -12 1471.46 65.46 -7 -3 12 1660.14 66.29 -7 -3 12 1599.93 79.42 -6 -4 -11 119.28 10.04 -6 -4 -11 153.01 8.46 -6 -4 -11 131.51 6.94 6 -4 11 138.96 17.35 6 4 11 128.86 14.25 -6 4 -11 116.21 8.87 17 7 -1 426.75 18.73 -17 7 1 417.70 22.65 -17 7 1 385.35 21.76 -17 -7 1 429.75 20.98 -17 -7 1 450.47 22.00 -21 3 1 44.95 6.35 -21 3 1 52.25 11.00 -21 -3 1 54.59 7.02 -21 3 1 48.93 6.34 -21 -3 1 53.37 7.70 21 -3 -1 58.37 9.73 21 3 -1 54.55 10.90 -9 9 6 169.39 12.23 -9 -9 6 174.78 11.12 -9 9 6 144.19 13.13 -9 -9 6 162.60 9.93 20 4 1 175.05 10.40 20 -4 1 149.49 14.04 20 -4 1 135.93 10.16 -20 4 -1 144.11 15.02 -20 -4 -1 178.91 11.06 -20 4 -1 169.57 11.60 -20 -4 -1 160.24 10.92 9 -7 -9 700.22 27.20 -9 -7 9 646.77 24.47 9 7 -9 581.15 24.53 9 7 -9 658.41 25.14 -9 7 9 529.22 23.24 -9 7 9 630.20 28.40 -9 7 9 629.36 27.70 9 -7 -9 614.67 30.24 -9 -7 9 639.32 26.28 9 -1 11 810.18 40.46 -9 -1 -11 740.42 32.71 -9 -1 -11 715.72 29.57 -9 1 -11 684.68 29.51 -9 1 -11 783.45 32.84 10 4 -11 0.51 2.60 -10 4 11 -0.48 6.94 10 -4 -11 -4.20 7.82 10 4 -11 2.48 5.67 10 -4 -11 0.49 3.54 -10 -4 11 3.38 3.34 -10 4 11 1.63 4.67 -10 -4 11 2.17 5.67 -10 -4 11 -4.20 15.57 10 4 -11 3.55 4.07 -10 4 11 0.13 5.18 -10 4 11 2.53 6.95 -1 7 10 666.54 28.64 1 -7 -10 590.21 25.90 -1 -7 10 645.77 24.95 1 -7 -10 609.76 30.36 1 7 -10 593.46 26.03 -1 -7 10 607.53 39.28 1 -7 -10 573.70 30.76 -1 -7 10 676.92 26.07 -1 -7 10 646.84 28.83 1 -7 -10 756.21 29.72 -1 7 10 588.38 29.64 13 1 -11 720.90 36.04 -13 1 11 581.71 31.35 -13 1 11 862.18 37.72 -13 1 11 555.39 39.56 -13 -1 11 546.86 39.86 13 -1 -11 784.94 31.15 -13 1 11 788.26 33.85 13 -1 -11 775.02 36.79 -13 -1 11 781.53 33.74 -13 -1 11 815.34 38.53 13 1 -11 770.26 30.86 -13 -1 11 800.59 31.12 19 1 5 767.47 40.12 -19 1 -5 727.01 34.22 -19 -1 -5 769.37 34.42 -19 1 -5 837.88 33.31 -19 -1 -5 811.62 33.45 19 -1 5 821.15 40.75 -21 3 2 21.55 10.37 -21 3 2 21.96 5.14 -21 -3 2 18.91 6.07 21 3 -2 22.02 10.10 21 -3 -2 17.96 7.88 -21 3 2 17.95 5.21 -21 -3 2 15.16 5.98 -21 1 -2 13.35 4.72 21 1 2 10.21 4.06 21 -1 2 12.05 10.48 21 -1 2 13.00 3.89 21 1 2 8.05 10.37 -21 -1 -2 9.28 5.69 4 -10 5 113.08 7.89 4 10 5 110.95 12.97 -4 -10 -5 113.65 8.69 -4 -10 -5 120.03 9.59 4 -10 5 135.35 9.88 4 -10 5 108.02 11.66 4 -10 5 106.72 16.90 -4 10 -5 139.66 12.02 -4 -10 -5 127.12 14.36 -3 -7 10 1012.47 45.56 -3 7 10 979.61 45.79 -3 7 10 1057.19 45.93 3 -7 -10 1061.78 43.44 -3 -7 10 1018.50 57.19 -3 -7 10 1080.02 42.22 -3 -7 10 1082.21 43.51 3 -7 -10 1134.23 46.98 3 -7 -10 1001.06 47.35 3 7 -10 953.27 43.23 -13 9 1 536.96 27.83 -13 -9 1 552.38 25.27 -13 9 1 524.14 26.51 -17 1 9 755.57 31.53 17 -1 -9 689.47 30.77 17 -1 -9 748.69 33.70 17 1 -9 741.76 35.40 17 1 -9 648.77 34.40 17 -1 -9 793.81 36.35 17 1 -9 696.73 30.69 -17 -1 9 743.13 33.26 -17 1 9 789.28 36.12 -17 -1 9 711.62 31.09 -17 -1 9 788.34 38.41 -17 1 9 706.43 32.97 2 -4 -12 7.12 3.90 -2 -4 12 9.58 4.77 2 -4 -12 7.77 7.34 2 -4 -12 9.81 12.39 -2 4 12 10.11 4.59 -2 4 12 11.28 8.53 2 4 -12 8.76 5.24 2 -4 -12 12.40 5.31 2 -4 -12 8.87 2.52 -3 -3 -12 228.47 9.41 -3 -3 -12 210.93 14.20 3 3 12 219.52 11.40 -3 -3 -12 255.10 11.30 3 3 12 230.83 19.07 -3 3 -12 209.44 12.82 18 -2 -8 481.94 24.90 -18 -2 8 557.98 25.78 18 2 -8 562.04 29.26 -18 2 8 505.37 25.07 -18 2 8 541.23 26.76 18 2 -8 525.88 26.60 18 -2 -8 474.69 23.29 18 2 -8 512.95 23.14 -18 2 8 532.63 24.24 -18 -2 8 532.54 23.65 -2 -8 9 3713.15 146.09 -2 8 9 3521.51 147.78 2 -8 -9 3735.91 149.63 -2 8 9 3915.53 148.65 -2 -8 9 3475.03 158.24 2 -8 -9 3549.65 146.04 -2 -8 9 3759.13 145.21 -2 -8 9 4150.11 146.69 2 -8 -9 3432.64 147.91 -2 -8 9 3777.18 147.43 -17 7 2 1132.88 44.02 -17 7 2 1184.61 45.35 17 7 -2 1032.60 39.19 -17 -7 2 1149.91 42.58 -7 -9 -6 82.57 7.41 -7 9 -6 114.05 10.24 7 -9 6 86.24 7.79 -7 -9 -6 89.29 13.41 7 -9 6 106.83 8.25 7 -9 6 109.22 8.13 7 -9 6 95.30 15.16 7 9 6 80.03 11.51 -7 -9 -6 88.39 7.62 10 0 -12 778.92 35.49 10 0 -12 787.26 39.33 -10 0 12 808.19 40.32 -10 0 12 867.46 36.59 -10 0 12 828.88 45.08 10 0 -12 845.98 33.32 -17 -7 0 117.26 9.05 17 7 0 136.22 8.33 -17 7 0 93.68 10.22 -17 -7 0 117.24 9.63 -17 7 0 93.29 9.28 -3 11 2 105.57 12.09 3 11 -2 84.14 11.42 -3 -11 2 84.99 7.33 -3 11 2 91.20 9.08 3 -11 -2 93.48 8.02 -6 10 5 414.52 25.25 -6 -10 5 465.61 21.90 -6 -10 5 515.37 23.50 6 10 -5 435.19 26.83 -6 10 5 473.72 25.04 -13 -9 0 37.77 5.92 -13 9 0 21.69 6.51 -19 5 4 162.22 11.85 -19 5 4 140.82 10.98 19 5 -4 151.47 15.58 -19 -5 4 157.07 10.01 -19 5 4 160.53 11.18 9 -9 5 122.86 11.47 9 9 5 113.24 13.75 -9 -9 -5 119.36 8.94 -9 9 -5 156.76 12.28 -9 -9 -5 123.48 7.82 9 -9 5 133.94 15.06 9 -9 5 134.34 9.41 -11 -7 -7 1302.84 56.84 -11 -7 -7 1232.86 53.61 -11 -7 -7 1385.58 54.39 11 -7 7 1308.69 53.57 11 7 7 1350.80 57.08 11 -7 7 1235.88 60.29 -11 7 -7 1458.42 56.25 11 7 7 1186.05 59.71 8 -10 3 256.78 20.91 -8 10 -3 309.26 19.16 8 -10 3 275.19 17.31 8 10 3 261.33 20.27 12 -6 -9 2315.96 55.19 12 -6 -9 2096.50 61.82 -12 6 9 666.55 51.52 -12 -6 9 2111.85 52.73 -12 -6 9 2230.11 56.24 12 6 -9 2276.55 53.95 12 6 -9 2139.87 63.37 -12 6 9 693.46 48.72 12 6 -9 2049.74 54.61 -12 6 9 2010.10 56.48 8 10 -4 1797.71 85.17 -8 -10 4 1912.05 80.01 -8 10 4 1987.49 83.91 -8 -10 4 2012.19 81.35 21 -3 0 63.90 6.55 -21 -3 0 71.55 8.04 -21 3 0 80.68 7.46 -21 -3 0 68.33 7.44 -21 3 0 77.94 12.05 21 3 0 87.87 12.04 -21 3 0 69.99 7.28 21 -3 0 80.35 11.68 0 -8 -9 707.18 38.58 0 8 9 760.91 38.87 0 -8 9 813.94 37.77 0 -8 9 817.79 47.95 0 8 9 862.97 38.93 0 -8 -9 842.91 36.52 0 -8 -9 839.64 39.53 0 -8 9 862.75 35.47 0 -8 9 871.58 36.20 -20 0 -4 326.38 15.58 -20 0 -4 304.18 16.27 20 0 4 302.17 21.90 -10 10 1 38.72 9.07 -10 -10 1 42.47 6.75 -10 -10 1 20.56 5.19 -10 10 1 23.48 8.35 -4 -4 12 -3.37 15.09 4 -4 -12 -0.29 3.31 4 4 -12 0.16 5.22 4 -4 -12 0.79 2.40 4 -4 -12 0.85 5.35 4 4 -12 0.91 3.93 -4 -4 12 1.23 5.20 -4 4 12 -2.80 8.58 4 -4 -12 -0.55 11.41 -4 4 12 1.51 4.36 4 -4 -12 -1.45 7.26 -14 0 -9 3.04 3.51 14 0 9 0.81 2.96 14 0 9 -3.85 10.19 -13 -9 2 1854.55 74.15 -13 -9 2 1736.50 72.86 -13 9 2 1721.23 74.63 -13 9 2 1929.20 76.27 20 2 -6 4.36 8.90 -20 -2 6 4.78 5.16 -20 2 6 6.13 9.18 20 -2 -6 -5.94 7.64 -20 -2 6 25.51 13.99 -20 -2 6 3.02 7.33 -20 2 6 2.40 4.38 10 -10 0 179.79 13.30 10 10 0 148.90 14.97 -10 -10 0 169.63 10.95 -10 10 0 166.04 12.91 -14 6 8 85.93 8.72 -14 -6 8 92.66 6.77 14 6 -8 85.29 7.39 -14 6 8 67.00 8.31 14 6 -8 96.67 7.30 -14 -6 8 88.09 8.10 14 6 -8 93.59 12.44 9 -7 8 1580.80 55.37 -9 -7 -8 1621.60 56.34 9 7 8 1452.63 62.21 9 -7 8 1504.75 64.83 9 7 8 1450.77 55.71 9 7 8 1720.98 60.38 -9 -7 -8 1465.31 56.37 -12 0 -10 2572.80 100.82 -12 0 -10 2549.60 102.52 12 0 10 2625.23 110.28 0 -4 -12 1149.62 51.02 0 4 12 1219.93 50.63 0 -4 -12 1269.04 43.37 0 4 12 1220.60 43.36 0 4 -12 1124.93 44.42 0 -4 -12 1069.86 40.66 0 -4 -12 1133.80 46.75 0 -4 12 1231.24 41.65 15 7 4 270.14 14.71 -15 7 -4 248.59 13.77 -15 7 -4 185.23 20.22 -15 7 -4 257.08 15.50 15 -7 4 209.25 16.80 -15 -7 -4 224.25 13.13 15 -7 4 214.98 12.09 -15 -7 -4 206.69 12.59 12 4 9 602.65 25.40 -12 -4 -9 568.61 25.80 12 -4 9 574.58 24.75 12 -4 9 541.63 32.92 12 4 9 493.42 31.63 -12 -4 -9 578.26 26.43 -12 4 -9 575.69 26.26 -12 -4 -9 546.98 25.12 -12 -4 -9 609.29 24.56 17 1 7 67.95 6.02 17 1 7 62.14 12.51 -17 -1 -7 69.89 6.92 -17 1 -7 65.47 6.43 17 -1 7 67.52 12.83 -17 -1 -7 72.81 5.45 17 -1 7 67.79 5.99 -20 4 4 7.12 5.30 20 4 -4 3.89 9.14 -20 4 4 6.49 4.98 20 -4 -4 8.32 6.40 -20 -4 4 4.21 5.30 -20 4 4 5.70 8.31 -7 -9 7 1661.76 64.45 -7 -9 7 1724.07 63.24 -7 -9 7 1822.53 66.38 7 -9 -7 1783.09 67.93 -7 9 7 1622.55 66.05 3 11 2 317.69 20.37 -3 -11 -2 297.03 15.49 3 -11 2 326.71 19.91 3 -11 2 320.37 25.53 3 -11 2 307.42 16.25 -3 -11 -2 319.57 16.67 -3 -11 -2 378.98 21.55 14 -8 3 1630.78 70.25 -14 -8 -3 1844.56 71.75 -14 8 -3 1329.86 77.32 14 8 3 1813.12 70.31 14 -8 3 1701.16 74.24 -14 8 -3 1708.83 72.66 14 8 3 1464.76 75.17 -14 8 -3 2071.95 73.53 -4 8 9 528.57 25.53 -4 -8 9 483.20 35.58 4 -8 -9 553.88 24.55 -4 -8 9 576.03 24.71 4 -8 -9 515.96 28.18 -4 -8 9 557.95 23.47 -4 8 9 481.28 26.57 1 -7 10 46.30 4.24 1 7 10 36.30 7.21 -1 -7 -10 42.26 5.05 1 7 10 39.23 9.23 1 -7 10 48.64 4.74 -1 -7 -10 22.38 8.03 1 -7 10 43.87 8.02 -1 -7 -10 45.11 7.94 1 -7 10 33.09 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39.49 -9 5 -11 885.42 38.35 9 5 11 835.63 44.82 9 -5 11 909.57 47.71 -2 0 14 1686.96 78.59 2 0 -14 1712.50 68.09 -23 -1 -2 680.10 30.43 -23 1 -2 658.55 30.20 23 -1 2 683.14 36.34 23 1 2 674.31 36.44 18 0 8 3.13 11.86 -18 0 -8 0.34 4.24 -18 -8 1 757.81 32.37 -18 8 1 776.19 33.93 -18 -8 1 737.89 33.07 18 8 -1 703.99 38.84 0 10 8 193.44 13.95 0 -10 8 211.69 11.82 0 -10 8 227.19 12.85 0 -10 -8 186.00 11.86 0 -10 -8 192.20 14.26 0 -10 8 194.19 11.04 0 -10 8 191.65 23.17 5 -11 5 266.55 24.01 -5 -11 -5 288.61 20.77 5 11 5 277.20 19.29 -5 -11 -5 247.23 14.92 -5 11 -5 293.96 18.58 -20 6 -2 983.48 44.05 20 6 2 1160.42 51.61 -20 6 -2 953.02 50.32 -20 6 -2 995.88 45.30 20 -6 2 1025.67 47.28 20 6 2 1128.23 43.74 -20 -6 -2 986.89 44.11 -8 -10 -6 607.28 29.10 8 -10 6 612.41 36.76 8 10 6 590.12 33.47 13 -5 -11 13.16 5.11 13 -5 -11 8.30 8.92 -13 5 11 13.05 6.15 13 5 -11 0.86 3.55 -13 -5 11 0.30 6.20 -13 5 11 6.11 5.35 -13 5 11 1.08 5.56 13 5 -11 -2.49 5.91 -13 5 11 4.57 5.99 -13 -5 11 -5.65 23.35 -9 3 13 683.75 32.43 9 3 -13 583.49 30.78 -9 -3 13 608.82 42.28 -9 -3 13 652.21 28.96 9 -3 -13 595.99 33.08 -9 3 13 638.51 29.19 -9 3 13 617.57 33.29 9 -3 -13 625.51 26.19 19 -5 5 1810.04 79.26 -19 -5 -5 1882.88 73.50 19 5 5 1969.27 75.98 -19 -5 -5 1618.78 73.65 -19 5 -5 1758.33 74.69 19 5 5 1747.61 81.20 -19 5 -5 1953.10 73.61 -8 10 7 576.51 32.32 -8 -10 7 630.90 29.32 -8 -10 7 637.17 28.30 -8 10 7 650.48 31.80 8 -10 -7 670.55 33.02 -3 -11 6 306.59 16.19 -3 -11 6 276.80 14.73 3 -11 -6 285.00 17.77 -3 11 6 259.19 18.23 3 -11 -6 260.61 15.32 -3 11 6 279.92 16.02 -21 -5 -2 962.48 39.47 -21 5 -2 843.63 38.98 -21 5 -2 862.06 40.01 -21 5 -2 885.02 45.64 21 -5 2 994.80 44.14 21 5 2 931.36 45.76 21 5 2 900.00 39.12 4 12 1 2303.38 98.50 4 -12 1 2263.06 102.13 -4 -12 -1 2479.40 95.14 4 -12 1 2278.37 94.70 6 6 -12 272.82 15.34 -6 6 12 259.23 15.73 -6 6 12 223.75 16.41 6 -6 -12 252.04 13.33 6 -6 -12 229.48 14.13 6 -6 -12 240.08 18.42 22 0 4 127.48 15.80 -22 0 -4 115.11 8.34 -22 0 -4 103.54 8.87 -11 1 13 2317.66 92.59 11 -1 -13 2003.36 95.52 11 -1 -13 2269.75 89.14 -11 -1 13 2426.04 92.69 -11 1 13 2516.26 97.26 -11 -1 13 2378.28 104.81 -11 1 13 2385.06 101.04 11 1 -13 2166.75 95.37 -17 5 9 2432.79 80.61 17 5 -9 2190.19 84.76 -17 -5 9 2200.13 79.26 17 5 -9 2210.87 77.14 -17 5 9 2386.69 81.13 17 5 -9 2119.00 78.95 -17 -5 9 2330.07 77.31 -1 -11 -6 338.33 18.02 1 11 6 375.36 21.07 -1 -11 -6 341.19 19.19 1 -11 6 330.39 17.07 1 -11 6 324.14 27.59 -2 -4 -13 70.29 9.91 -2 -4 -13 76.04 4.50 2 4 13 63.83 13.71 -2 4 -13 60.09 7.61 -2 -4 -13 80.54 7.07 -20 2 -6 588.45 27.65 -20 -2 -6 546.24 27.40 20 2 6 613.04 34.95 -20 -2 -6 585.03 26.48 20 -2 6 614.47 34.41 4 0 -14 26.42 9.16 4 0 -14 23.19 4.71 -4 0 14 21.04 5.35 -4 0 14 25.00 13.99 23 3 0 30.54 11.91 23 -3 0 4.85 9.72 -23 3 0 -5.04 12.02 -23 3 0 2.26 5.07 -23 -3 0 2.96 6.45 -23 -3 0 1.38 6.09 -23 3 0 -2.69 5.50 -13 -3 12 0.76 6.46 13 3 -12 1.05 7.11 -13 -3 12 -3.04 15.81 13 3 -12 1.30 2.96 -13 3 12 1.36 5.89 -13 3 12 -0.91 4.42 -13 3 12 -4.47 9.92 -13 3 12 -0.53 10.82 13 -3 -12 -0.87 4.92 -18 8 2 13.51 8.04 -18 -8 2 7.04 5.40 -18 8 2 9.60 6.14 -18 -8 2 8.62 4.46 -18 2 10 160.82 10.50 -18 2 10 163.02 13.88 18 2 -10 146.70 9.32 18 2 -10 156.59 14.53 18 -2 -10 153.37 14.72 18 2 -10 142.05 12.67 -18 -2 10 154.32 12.09 18 -2 -10 146.30 10.15 -18 -2 10 153.29 9.57 -18 2 10 148.36 11.29 -21 3 7 297.48 16.12 -21 -3 7 262.67 15.24 -21 3 7 283.81 16.79 -21 -3 7 294.00 17.46 -21 3 7 309.83 18.64 21 3 -7 266.13 20.26 23 1 -5 305.89 20.56 -23 -1 5 254.60 16.72 23 -1 -5 315.22 19.41 -23 1 5 266.60 16.64 -23 1 5 351.17 22.34 -23 -1 5 301.12 16.04 -23 1 5 288.21 15.94 -7 11 5 465.13 27.20 -7 -11 5 543.47 25.09 -7 -11 5 501.42 23.55 -7 11 5 520.66 26.94 -23 3 3 9.06 6.11 -23 3 3 17.54 11.14 -23 3 3 11.41 5.50 -23 -3 3 12.33 7.41 23 3 -3 7.51 10.68 23 -3 -3 16.80 8.90 -23 -3 3 15.16 6.14 18 6 5 490.91 23.72 18 -6 5 443.24 27.25 -18 -6 -5 446.10 21.32 -18 6 -5 460.17 23.38 -18 -6 -5 415.79 21.25 -18 6 -5 437.45 21.13 18 6 5 444.46 28.45 -19 7 4 10.47 5.64 -19 -7 4 9.63 4.42 19 7 -4 20.59 10.11 -19 7 4 14.22 6.53 -2 -6 -12 -1.52 6.92 2 6 12 5.18 9.97 -2 6 -12 3.25 4.78 -2 -6 -12 7.33 5.85 -2 -6 -12 6.95 3.30 2 -6 12 -5.51 15.63 -2 -6 -12 -0.47 6.91 2 6 12 8.78 6.06 -3 1 14 -1.05 12.93 -3 -1 14 -10.84 16.50 -3 1 14 8.07 4.47 3 -1 -14 10.27 4.39 3 1 -14 5.96 3.71 3 1 -14 6.68 6.63 18 8 0 318.64 12.73 -18 -8 0 188.09 13.66 -18 8 0 274.32 19.16 -18 -8 0 207.99 14.42 -18 8 0 224.43 15.22 -8 -8 -9 303.03 15.77 8 -8 9 277.38 25.78 8 8 9 281.74 21.25 -8 -8 -9 289.36 16.58 -8 8 10 290.19 18.21 8 -8 -10 266.64 19.51 -8 -8 10 356.37 34.74 -8 8 10 335.07 18.50 -8 -8 10 313.06 16.18 -8 -8 10 301.73 14.52 8 8 -10 282.11 14.46 -7 9 9 20.53 6.72 7 -9 -9 21.85 8.57 -7 -9 9 24.47 4.26 -7 9 9 24.44 8.62 -7 9 9 -2.53 2.25 -7 -9 9 27.49 5.51 -7 -9 9 40.17 22.69 -4 -10 8 2009.85 78.16 4 -10 -8 1871.95 77.48 4 -10 -8 1843.44 80.28 -4 -10 8 1993.35 76.90 -4 -10 8 1936.71 93.57 -4 10 8 1986.28 77.49 -16 -8 -4 49.04 6.49 -16 8 -4 24.55 16.18 -16 8 -4 68.60 8.44 16 8 4 52.08 12.45 16 -8 4 51.13 12.05 -16 8 -4 64.68 8.67 -16 -8 -4 54.86 6.94 16 8 4 53.46 8.01 4 -12 -2 -2.75 4.76 -4 12 2 0.32 5.93 -4 -12 2 -0.56 4.30 -16 8 6 233.18 14.68 -16 -8 6 246.97 14.02 -16 -8 6 254.59 12.76 16 8 -6 227.12 19.51 -16 8 6 231.15 14.51 10 10 5 1182.16 57.44 -10 -10 -5 1161.65 52.21 10 -10 5 1258.59 59.44 1 1 -14 1119.57 53.66 -1 1 14 1336.79 60.32 -1 -1 14 1266.10 61.95 1 -1 -14 1242.19 54.97 1 1 -14 1189.72 49.48 1 -1 -14 1317.01 50.19 0 0 -14 346.85 15.68 0 0 14 356.73 26.20 -14 2 12 19.87 6.08 14 -2 -12 21.68 4.51 14 2 -12 22.57 3.62 -14 -2 12 21.97 6.71 14 -2 -12 19.14 8.59 14 2 -12 26.90 8.14 -14 2 12 23.20 9.52 -14 2 12 22.76 11.17 -14 -2 12 21.05 15.99 0 -12 3 664.86 30.78 0 12 3 695.27 33.66 19 3 -9 73.79 9.46 19 3 -9 74.65 12.26 -19 3 9 86.67 8.00 -19 -3 9 75.15 7.20 -19 -3 9 93.73 10.43 -19 3 9 90.78 9.30 -19 3 9 81.16 10.71 -17 -5 -7 3226.32 115.94 17 5 7 2646.06 123.27 -17 -5 -7 2799.27 116.29 -17 5 -7 3219.81 117.90 -17 5 -7 3731.62 116.17 17 -5 7 3224.11 125.25 -6 -2 -13 151.56 6.85 -6 -2 -13 155.30 11.53 6 2 13 175.53 20.27 -20 -4 -5 138.05 10.56 20 -4 5 166.76 17.06 -20 -4 -5 160.01 9.69 -20 4 -5 157.22 9.66 20 4 5 149.06 17.29 -20 4 -5 153.09 11.08 -12 -4 12 3182.76 118.07 12 4 -12 3001.65 118.94 -12 4 12 3232.45 119.17 -12 -4 12 2819.74 129.59 -12 4 12 3022.47 119.69 12 -4 -12 3426.94 115.87 12 -4 -12 3245.28 122.76 -12 4 12 3143.95 118.42 -6 10 -7 8.03 6.91 -6 -10 -7 3.99 4.22 -6 -10 -7 3.69 5.89 6 -10 7 1.69 13.33 6 10 7 0.52 8.35 -13 9 -5 549.34 45.46 -13 -9 -5 623.07 29.95 13 9 5 577.68 35.55 -13 -9 -5 714.08 31.19 13 -9 5 635.30 35.01 -13 9 -5 671.20 32.45 13 9 5 642.85 30.11 -13 9 -5 736.37 31.70 -9 11 4 8.99 7.22 -9 -11 4 -1.47 4.84 -9 -11 4 1.63 4.37 -9 11 4 6.21 8.03 -21 1 8 -2.70 10.68 21 1 -8 -0.49 8.59 21 -1 -8 1.59 7.67 -21 -1 8 -0.50 4.49 -21 1 8 3.33 4.58 -21 1 8 0.54 5.86 -21 -1 8 1.98 6.71 -2 -12 3 173.22 11.54 2 12 -3 161.03 15.76 2 -12 -3 197.80 13.45 -2 12 3 200.94 13.93 -20 0 9 -1.45 4.50 20 0 -9 1.98 8.19 -20 0 9 2.57 10.89 -20 0 9 2.28 6.30 20 0 -9 1.95 8.19 -21 5 5 939.08 41.26 21 5 -5 935.76 44.88 -21 -5 5 922.01 38.45 -21 5 5 931.66 38.61 14 10 -1 18.39 10.47 -14 10 1 26.61 8.42 -14 -10 1 20.82 5.30 -14 10 1 20.84 7.52 14 -6 -10 130.77 13.41 -14 -6 10 132.12 9.83 -14 6 10 105.36 10.05 14 6 -10 128.19 9.22 -14 -6 10 136.46 7.77 -14 6 10 117.12 10.24 14 6 -10 140.61 8.08 14 6 -10 118.90 13.80 -9 -3 -12 49.65 7.31 -9 -3 -12 59.06 4.28 -9 3 -12 29.55 4.63 -9 -3 -12 50.04 4.88 9 -3 12 46.87 14.37 9 3 12 41.80 11.96 24 0 -1 3.05 9.64 -24 0 1 -0.47 5.96 -24 0 1 -5.62 5.44 -22 0 7 -2.79 4.57 22 0 -7 -1.16 7.95 -22 0 7 3.05 6.41 -22 0 7 7.79 11.86 24 0 -2 72.91 12.18 -24 0 2 63.14 8.21 -24 0 2 53.95 7.10 -5 -1 14 103.47 8.27 -5 1 14 125.87 8.99 -5 -1 14 115.25 18.32 5 1 -14 110.55 7.80 -5 1 14 106.88 16.57 5 -1 -14 119.48 8.40 5 1 -14 107.21 11.71 19 7 2 297.72 15.07 19 7 2 322.66 22.18 -19 7 -2 253.96 15.31 -19 7 -2 271.28 16.93 19 -7 2 245.61 18.36 -19 -7 -2 243.26 14.78 -19 7 -2 234.90 21.72 -12 -10 5 277.68 16.38 -12 -10 5 278.49 15.22 -12 10 5 280.34 17.81 -2 -10 -8 193.98 13.94 2 -10 8 208.54 12.00 2 10 8 180.14 14.93 2 -10 8 195.66 11.17 2 -10 8 188.62 23.24 -2 -10 -8 185.57 11.81 -5 -3 -13 208.75 9.21 5 -3 13 213.60 20.92 -5 -3 -13 199.49 13.95 -5 3 -13 191.36 12.85 -5 -3 -13 237.58 10.62 5 3 13 234.25 20.18 14 8 6 163.78 17.06 -14 -8 -6 158.06 10.86 14 -8 6 190.81 18.31 -14 -8 -6 180.44 11.51 -14 8 -6 175.67 12.76 14 8 6 177.80 13.36 -14 8 -6 218.12 12.64 18 8 -3 688.29 35.80 -18 -8 3 605.29 28.16 -18 8 3 539.00 29.23 -18 8 3 744.61 33.17 18 4 7 297.13 23.06 18 -4 7 303.39 22.51 -18 -4 -7 256.58 15.19 -18 4 -7 313.99 13.94 -18 -4 -7 278.58 14.03 -18 4 -7 277.59 15.64 22 -4 2 -1.77 9.39 -22 4 -2 -2.73 11.99 -22 4 -2 0.82 5.06 22 4 2 14.14 6.14 -22 4 -2 -2.18 5.01 -20 6 5 165.74 13.69 -20 -6 5 188.74 12.47 -20 -6 5 173.95 11.26 -20 6 5 153.53 12.18 20 6 -5 169.96 10.75 20 6 -5 174.93 17.77 -9 11 -3 180.41 14.53 9 11 3 156.85 17.38 9 -11 3 178.54 17.48 -15 9 -3 3159.69 114.78 15 -9 3 2834.05 116.19 15 9 3 2493.89 117.93 -15 9 -3 2829.85 114.73 15 9 3 2815.07 110.89 -15 -9 -3 2812.09 113.15 -4 -12 -2 2016.16 79.65 4 -12 2 1829.81 86.09 4 12 2 1970.64 83.48 4 -12 2 1896.15 79.05 15 1 10 386.66 27.49 -15 1 -10 395.55 18.73 15 -1 10 419.26 27.97 -15 -1 -10 401.26 18.70 -14 -10 0 22.34 5.62 14 10 0 20.82 10.69 -14 10 0 16.84 8.22 -14 -10 0 18.67 5.88 17 7 -7 1588.51 66.58 -17 7 7 1774.38 70.89 -17 -7 7 1754.44 69.54 -17 -7 7 1671.59 67.59 17 7 -7 1642.29 74.66 -17 7 7 1609.46 70.02 -6 0 14 4676.93 168.67 6 0 -14 4173.17 167.74 6 0 -14 3841.80 171.76 -6 0 14 4389.55 178.97 5 11 -6 1099.29 56.53 -5 11 6 1140.17 54.75 5 -11 -6 1205.63 52.19 -5 -11 6 1277.65 52.76 5 -11 -6 1291.25 54.61 -5 -11 6 1275.86 51.62 16 -6 7 32.75 12.90 -16 6 -7 60.20 6.24 -16 6 -7 45.14 7.25 16 6 7 42.41 9.70 -16 -6 -7 37.25 5.54 -16 -6 -7 39.62 5.19 -14 -10 2 25.90 5.68 -14 10 2 32.77 8.76 -14 -10 2 53.37 7.74 -14 10 2 33.06 7.15 2 -12 3 6.49 4.35 2 -12 3 0.46 15.72 2 12 3 7.66 9.26 16 6 -9 710.45 30.45 -16 -6 9 791.02 31.89 -16 6 9 729.09 32.50 -16 -6 9 752.91 29.56 16 6 -9 716.16 36.52 23 -3 1 2297.80 87.32 -23 -3 -1 2133.40 81.98 23 3 1 1800.35 80.72 -23 -3 -1 1824.36 81.54 -23 3 -1 2156.08 88.23 -23 3 -1 2085.46 81.81 23 3 1 2195.15 88.30 -18 -8 -1 523.20 26.01 -18 8 -1 550.37 27.03 18 8 1 528.24 33.17 -18 -8 -1 539.65 26.61 -13 -1 -11 7.42 3.88 -13 1 -11 7.90 3.51 13 1 11 10.15 11.42 13 -1 11 6.43 13.75 -13 -1 -11 9.24 4.92 -7 1 -13 184.38 10.76 7 1 13 172.98 17.70 -7 -1 -13 179.14 11.05 -3 -11 -6 -4.15 4.46 3 -11 6 5.51 12.85 3 11 6 -9.58 10.24 -3 -11 -6 9.06 6.53 3 -11 6 -2.51 4.01 -10 2 -12 237.85 13.14 -10 -2 -12 220.25 13.33 -10 -2 -12 223.00 10.38 10 -2 12 222.66 21.60 10 2 12 203.51 20.14 15 9 -5 223.95 19.68 -15 -9 5 240.44 13.33 -15 -9 5 273.50 15.04 11 11 -1 1113.56 50.20 -11 11 1 1133.41 48.21 -11 11 1 932.65 45.03 -11 -11 1 913.35 42.62 -11 -11 1 1043.18 44.57 -11 -7 -9 -1.41 4.81 -11 7 -9 -3.35 5.47 11 -7 9 3.70 12.59 -11 -7 -9 6.22 6.72 -11 -7 -9 -0.34 3.85 11 7 9 5.49 11.37 8 -4 12 379.47 26.86 -8 -4 -12 358.03 15.35 -8 -4 -12 406.90 16.11 -8 -4 -12 337.78 18.65 8 4 12 337.74 24.66 -17 1 11 665.18 31.92 17 1 -11 545.09 29.60 17 -1 -11 552.09 30.86 -17 -1 11 584.93 27.77 -17 1 11 609.27 26.24 -17 1 11 574.91 27.98 17 1 -11 584.73 25.12 -17 -1 11 588.12 25.43 8 4 -13 -0.94 4.25 -8 4 13 -2.11 5.31 8 -4 -13 -3.87 8.95 8 -4 -13 1.79 3.37 -8 -4 13 0.91 5.63 -8 4 13 2.65 9.50 -8 -4 13 -0.57 16.64 -8 4 13 -8.05 9.32 8 4 -13 -1.65 5.78 13 7 8 853.87 38.52 -13 -7 -8 712.26 37.19 13 -7 8 788.16 42.20 13 7 8 736.40 41.20 -13 -7 -8 930.34 35.42 -13 7 -8 812.87 36.13 -13 -7 -8 763.67 34.18 -13 -7 -8 738.77 34.32 2 -2 -14 1042.24 39.51 2 -2 -14 1022.37 44.93 -2 -2 14 998.13 52.41 -2 2 14 1001.89 48.31 2 2 -14 901.67 42.34 -23 3 4 69.44 8.12 -23 -3 4 70.23 9.68 23 3 -4 79.34 12.93 -23 -3 4 72.24 7.89 -23 3 4 69.01 12.15 -23 3 4 68.40 7.66 18 -2 8 103.54 15.35 18 2 8 132.52 16.93 -18 -2 -8 110.80 6.11 -18 -2 -8 105.48 7.71 -18 2 -8 108.88 7.62 -24 0 0 160.43 11.64 24 0 0 173.26 16.48 -24 0 0 172.67 11.61 -11 -11 0 104.90 9.16 -11 11 0 94.36 11.22 24 0 -3 7.21 10.29 -24 0 3 -3.52 5.27 -24 0 3 0.51 6.03 17 -7 5 845.30 43.20 -17 7 -5 935.95 37.76 -17 -7 -5 847.53 36.77 -17 7 -5 867.78 38.88 17 7 5 942.85 39.18 -12 0 13 5.12 14.39 12 0 -13 4.39 8.28 12 0 -13 -2.26 2.58 -12 0 13 5.69 5.73 1 1 14 1.50 11.88 -1 -1 -14 3.48 6.51 1 -1 14 5.22 12.19 22 4 -5 220.79 19.15 -22 4 5 188.98 13.58 -22 4 5 226.76 13.85 -22 4 5 227.43 15.35 -22 -4 5 187.74 12.80 22 2 4 196.19 18.75 -22 -2 -4 169.84 11.99 22 -2 4 195.59 17.79 -22 2 -4 167.95 11.79 -22 -2 -4 187.46 11.61 -22 2 -4 194.51 11.11 -6 -12 0 247.66 14.96 6 12 0 291.46 20.04 4 2 -14 492.46 26.84 4 -2 -14 553.70 24.34 -4 -2 14 578.82 36.72 4 -2 -14 541.49 28.76 4 2 -14 508.20 23.40 -4 2 14 554.61 24.66 -4 2 14 515.10 31.28 3 -5 -13 1011.11 48.98 3 -5 -13 1274.94 55.64 -3 5 13 1145.61 55.29 -3 5 13 1327.37 52.16 3 -5 -13 1278.09 48.84 3 -5 -13 1362.20 51.66 3 5 -13 1148.29 51.73 -6 -12 1 153.99 11.11 -6 12 1 133.46 14.05 -6 12 1 143.86 14.97 -11 -9 8 434.12 21.33 -11 9 8 413.45 22.84 11 9 -8 388.48 26.32 -11 -9 8 432.56 19.69 11 -9 -8 488.39 25.91 -5 -7 -11 106.49 9.58 -5 -7 -11 103.17 7.16 5 -7 11 104.26 18.19 -5 -7 -11 95.32 10.38 5 7 11 91.26 13.49 -1 5 13 504.62 22.36 1 -5 -13 449.40 24.86 1 5 -13 405.86 21.60 1 -5 -13 479.94 19.06 -1 5 13 442.59 26.20 1 -5 -13 519.17 22.02 4 12 -3 204.53 17.03 -4 12 3 216.01 15.97 -4 12 3 180.68 12.34 4 -12 -3 152.31 11.17 -4 -12 3 160.27 10.98 -9 7 11 1.83 4.99 -9 -7 11 -0.56 4.86 9 -7 -11 1.80 5.51 9 7 -11 -1.38 4.33 -9 7 11 -1.63 5.77 -9 7 11 -0.37 6.71 9 -7 -11 1.35 8.50 -11 11 2 657.60 34.62 -11 11 2 831.66 37.77 -11 -11 2 744.63 33.51 11 11 -2 867.35 40.43 -11 -11 2 647.67 31.84 -6 -10 8 2846.90 99.15 -6 10 8 2655.58 101.83 6 -10 -8 2849.49 102.75 -6 -10 8 2791.52 97.83 14 10 1 588.90 36.01 -14 -10 -1 690.51 31.56 -14 -10 -1 632.61 30.65 12 8 -9 3.43 4.25 12 8 -9 0.95 3.47 12 -8 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526.55 26.81 16 0 -16 452.63 29.96 -16 0 16 501.27 37.57 23 -1 10 395.21 29.37 23 1 10 389.90 29.48 -23 -1 -10 345.46 17.83 4 -14 7 221.01 26.02 -4 -14 -7 217.08 15.10 4 -14 7 221.73 13.93 4 14 7 219.76 18.38 11 11 10 649.48 39.12 -11 11 -10 828.79 38.42 11 -11 10 764.87 45.62 -11 -11 -10 722.03 33.84 -30 -2 2 33.81 8.12 -30 2 2 12.13 7.05 -30 2 2 9.90 6.88 30 2 -2 64.70 18.03 -30 -2 2 45.35 9.37 -12 -12 -8 32.65 6.98 12 12 8 45.10 13.86 -12 12 -8 14.64 10.08 12 -12 8 28.06 15.79 -27 -7 2 93.10 10.91 -27 7 2 67.33 11.34 -27 -7 2 86.81 10.31 -27 7 2 79.07 9.99 27 7 -2 88.33 17.84 -18 12 5 20.14 8.70 -18 12 5 11.12 11.08 -18 -12 5 17.42 6.65 -18 -12 5 16.46 7.71 -19 -9 -8 46.22 6.83 -19 9 -8 48.66 8.51 19 9 8 47.31 14.74 19 -9 8 60.19 18.27 -19 -9 -8 44.19 7.25 3 -15 4 46.60 7.22 3 15 4 37.71 11.19 -21 1 14 4.75 15.41 -21 1 14 2.07 7.94 21 -1 -14 3.04 10.93 -21 -1 14 -0.58 18.02 -21 -1 14 0.47 8.14 21 1 -14 2.18 9.30 -15 -13 5 319.26 18.06 -15 -13 5 337.82 19.54 -15 13 5 313.03 23.13 15 13 -5 260.62 24.68 -15 13 5 280.24 21.46 -2 -8 -15 350.09 23.33 2 -8 15 360.12 35.18 2 8 15 353.34 25.60 -12 0 17 1.03 16.99 12 0 -17 -1.63 10.07 -27 7 1 246.90 17.04 -27 -7 1 277.93 17.50 27 7 -1 278.25 25.09 -27 7 1 262.71 19.24 -27 -7 1 265.87 17.38 -21 -11 -1 167.10 13.33 -21 11 -1 187.29 15.06 -21 -11 -1 182.67 13.40 -21 11 -1 166.40 15.56 14 6 -15 114.20 11.16 14 -6 -15 132.37 17.64 -14 6 15 131.53 12.67 -14 -6 15 116.79 29.25 -14 -6 15 152.39 13.93 28 0 5 1.28 16.03 -28 0 -5 2.08 6.33 12 -6 14 78.52 21.16 12 6 14 115.63 19.83 -12 -6 -14 108.72 10.92 9 -9 -14 125.52 16.44 9 -9 -14 111.39 8.78 9 9 -14 100.09 8.53 -9 9 14 97.85 11.89 9 -3 16 98.80 20.97 -9 -3 -16 94.60 10.85 9 3 16 86.88 19.20 -30 2 1 444.51 24.94 -30 -2 1 458.58 25.37 -30 2 1 448.00 24.86 30 2 -1 552.76 33.95 -30 -2 1 537.42 25.78 -29 3 -2 268.25 17.52 -29 3 -2 278.56 17.01 -29 -3 -2 294.85 18.10 21 -3 11 132.40 21.04 21 3 11 128.57 20.80 -21 3 -11 122.27 10.16 -21 -3 -11 113.93 9.62 -10 -12 -9 336.14 18.97 10 12 9 276.09 24.39 10 -12 9 342.76 30.04 -27 5 -4 86.43 10.61 -27 -5 -4 70.44 10.37 -27 -5 -4 70.33 9.16 27 5 4 90.88 18.08 -27 5 -4 83.92 8.63 -15 -11 -8 2.87 6.10 15 11 8 -0.80 13.13 -15 11 -8 5.04 8.77 -15 -11 -8 3.46 5.51 6 0 17 -16.08 17.44 -6 0 -17 -4.00 7.86 -30 -2 3 411.46 21.76 -30 2 3 347.86 21.46 -30 2 3 336.14 20.95 30 2 -3 397.93 30.33 -30 -2 3 392.36 22.85 -26 8 2 30.86 7.96 -26 -8 2 34.87 8.23 -26 -8 2 38.28 8.03 26 8 -2 32.65 14.74 -26 8 2 28.74 9.49 27 3 -9 2.80 8.68 27 3 -9 0.36 12.54 -27 -3 9 -5.18 9.43 -27 3 9 0.21 7.83 -27 -3 9 4.61 6.43 -25 -3 11 188.28 15.68 -25 3 11 142.06 13.10 25 3 -11 164.28 18.66 25 3 -11 146.10 14.61 -25 3 11 166.18 14.30 25 -3 -11 176.71 19.14 -19 -11 7 661.20 31.28 -19 -11 7 676.32 33.26 -19 11 7 655.57 35.81 19 11 -7 662.18 39.93 -22 10 -3 62.62 9.57 -22 -10 -3 53.23 8.30 -22 10 -3 40.00 9.81 -11 13 8 52.38 11.35 11 -13 -8 59.72 13.18 -11 -13 8 63.32 9.22 -11 -13 8 67.20 7.78 -11 13 8 35.70 12.60 11 13 -8 53.01 14.75 -16 8 -11 100.35 10.96 16 -8 11 106.50 20.83 -16 -8 -11 84.84 8.28 16 8 11 78.98 17.53 -12 -14 4 76.25 9.86 -12 14 4 76.49 13.98 -12 14 4 60.08 12.77 12 14 -4 61.78 15.21 -12 -14 4 71.43 8.61 -27 7 3 62.48 9.60 -27 -7 3 66.05 10.14 -27 -7 3 68.11 10.08 -27 7 3 68.17 11.23 27 7 -3 64.42 16.10 -5 -15 4 112.35 11.31 -5 -15 4 102.03 10.14 -26 8 1 65.87 9.54 -26 -8 1 76.83 10.05 26 8 -1 96.12 18.03 -26 8 1 47.38 10.94 -26 -8 1 78.64 10.29 -16 -8 13 -0.95 30.50 -16 -8 13 4.52 8.04 -16 8 13 -2.45 8.06 16 -8 -13 -1.12 12.07 -8 -4 -16 -0.24 8.51 8 4 16 3.96 15.17 8 -4 16 -21.42 20.57 -8 4 -16 1.68 6.11 -28 6 2 53.83 9.41 28 6 -2 37.51 16.21 -28 -6 2 37.75 9.92 -28 6 2 48.06 8.54 -28 -6 2 35.38 9.27 -5 -13 -9 77.82 8.90 5 -13 9 92.75 23.16 5 13 9 66.82 13.18 -18 -12 -3 63.53 9.44 18 12 3 60.80 16.30 -18 12 -3 76.71 12.50 -18 12 -3 65.60 10.94 8 -4 -17 36.49 12.70 8 4 -17 20.14 7.98 -8 4 17 19.13 13.02 -8 -4 17 20.83 21.13 20 8 -11 78.12 16.67 20 -8 -11 119.02 17.93 -20 8 11 98.52 12.81 -20 -8 11 111.30 11.97 -20 8 11 90.91 11.85 -14 -10 -10 35.21 6.35 14 -10 10 29.46 16.74 14 10 10 28.60 14.12 -14 -10 -10 39.79 7.00 -14 10 -10 10.35 9.36 7 15 2 1.66 11.50 -7 -15 -2 15.98 6.92 7 -15 2 8.25 6.13 -21 9 9 72.07 10.96 21 9 -9 68.70 16.06 -21 -9 9 89.06 9.02 -21 9 9 72.79 12.78 -21 -9 9 81.61 10.87 8 -8 14 268.82 29.00 -8 -8 -14 256.29 13.40 -8 -8 -14 230.28 16.48 21 11 -4 188.78 22.68 -21 -11 4 174.52 12.84 -21 11 4 153.35 14.96 -21 11 4 140.44 15.54 18 -2 13 27.59 17.88 18 2 13 43.33 17.94 -18 -2 -13 29.41 5.78 8 -8 -15 50.31 13.55 8 8 -15 45.11 7.01 -8 8 15 43.04 9.58 -28 -6 1 262.25 17.05 -28 -6 1 252.05 16.89 28 6 -1 277.20 24.93 -28 6 1 236.57 16.22 -2 4 -17 63.11 9.25 2 4 17 78.19 17.43 -2 -4 -17 70.17 11.84 2 -4 17 82.66 21.30 22 4 10 31.62 16.28 22 -4 10 55.71 17.96 -22 -4 -10 24.45 7.30 -22 4 -10 29.96 7.06 -15 -3 16 11.60 19.58 15 -3 -16 11.31 11.00 15 3 -16 12.39 8.90 -15 -3 16 8.34 8.12 -15 3 16 8.38 8.47 -19 -1 15 286.20 31.49 -19 -1 15 332.50 20.12 -19 1 15 296.59 19.44 -19 1 15 311.10 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18.99 23 -1 -13 274.94 22.00 23 1 -13 272.84 20.57 -24 6 10 77.90 11.84 -24 -6 10 86.49 12.39 -24 -6 10 80.10 10.03 -24 6 10 78.96 11.66 24 6 -10 67.25 15.74 -14 -12 -7 3.86 6.00 -14 12 -7 6.61 8.78 14 12 7 -1.17 13.28 -14 -12 -7 5.90 6.39 -26 8 3 88.51 10.84 26 8 -3 105.78 17.81 -26 -8 3 88.94 9.91 -26 8 3 74.82 11.85 -26 -8 3 92.67 10.95 -4 -6 -16 -0.79 9.07 4 -6 16 -5.95 19.47 -4 6 -16 -0.36 6.30 4 6 16 -1.96 14.05 -30 2 0 260.93 17.81 -30 2 0 261.65 18.36 -30 -2 0 303.24 19.13 -28 6 3 11.72 8.00 -28 -6 3 9.09 8.28 -28 -6 3 6.08 8.35 -28 6 3 3.90 7.63 28 6 -3 14.25 14.67 15 11 -10 152.58 19.36 -15 -11 10 171.64 13.47 -15 11 10 139.26 14.05 -15 11 10 139.68 15.19 15 -11 -10 149.31 18.03 -28 4 7 788.45 40.15 28 4 -7 873.74 46.39 -28 4 7 812.97 39.63 -28 -4 7 893.80 39.13 -14 -4 16 40.72 9.20 14 4 -16 45.20 9.93 -14 4 16 45.14 9.22 -14 -4 16 40.86 24.06 -25 -3 -8 58.57 8.49 -25 3 -8 59.09 7.99 25 -3 8 89.31 19.28 25 3 8 59.14 17.89 -29 -3 6 697.46 36.36 -29 3 6 708.32 35.71 29 3 -6 775.44 42.16 -29 3 6 694.86 35.98 -29 -3 6 807.04 35.46 3 7 -16 18.52 6.58 3 -7 -16 24.62 10.97 -3 7 16 24.15 13.75 -9 -9 -13 281.85 15.03 -9 -9 -13 270.63 17.28 9 -9 13 288.76 29.49 22 10 -6 63.82 16.76 -22 -10 6 84.49 9.27 -22 10 6 68.51 11.91 -22 -10 6 72.56 10.84 -22 10 6 65.37 11.04 -26 -8 0 21.31 7.59 26 8 0 21.65 15.57 -26 8 0 20.72 7.48 -26 -8 0 23.45 7.99 -23 9 7 -13.20 8.61 -23 -9 7 0.69 6.72 23 9 -7 -5.16 14.58 -23 -9 7 -3.07 7.93 -23 9 7 -1.56 8.82 12 -10 11 33.34 17.42 -12 -10 -11 25.55 5.91 -12 10 -11 17.15 9.34 12 10 11 25.20 13.90 -1 -15 5 66.04 8.12 1 -15 -5 67.83 9.00 -1 -15 5 77.57 23.10 -20 -2 -12 8.97 5.42 20 -2 12 0.94 15.59 -20 2 -12 4.97 5.34 20 2 12 9.49 16.43 -10 -10 13 135.26 11.38 -10 10 13 126.15 12.97 -10 -10 13 129.86 28.91 10 -10 -13 125.60 10.18 10 -10 -13 135.26 17.53 -5 -11 -12 490.39 23.79 5 -11 12 489.80 39.24 5 11 12 421.96 28.51 -30 2 4 524.41 28.98 -30 -2 4 600.55 28.78 30 2 -4 592.12 35.04 -30 2 4 558.14 28.43 -30 -2 4 563.72 29.77 10 -6 -16 1252.74 57.14 -10 -6 16 1123.70 68.12 -10 6 16 1226.37 51.39 16 -10 9 -4.79 15.57 16 10 9 2.41 13.20 -16 -10 -9 1.94 5.17 -16 -10 -9 3.07 5.46 -16 10 -9 0.25 7.43 25 5 -10 325.09 26.46 -25 -5 10 370.66 20.07 -25 5 10 418.79 24.50 -25 5 10 309.57 22.03 -25 -5 10 368.73 23.26 -30 0 5 12.20 7.51 -30 0 5 12.17 8.13 16 -2 14 31.71 17.03 -16 10 11 11.56 8.56 16 -10 -11 11.18 12.12 16 10 -11 18.54 13.71 -16 -10 11 12.56 7.67 -16 10 11 11.50 10.50 18 8 10 172.45 21.38 -18 -8 -10 174.86 10.98 -18 8 -10 156.96 13.02 18 -8 10 169.65 21.87 -18 -8 -10 160.79 11.56 -16 -2 16 251.09 30.35 -16 -2 16 256.74 17.45 -16 2 16 198.61 22.69 16 2 -16 219.34 18.78 -16 2 16 278.38 18.24 16 -2 -16 260.61 21.60 -28 -6 0 32.28 8.68 28 6 0 28.08 17.08 -28 -6 0 20.28 9.29 -28 6 0 29.66 7.80 10 -14 -6 10.21 9.89 10 14 -6 3.66 13.38 -10 -14 6 23.01 7.55 -10 14 6 18.43 10.62 -10 -14 6 14.60 6.12 -10 14 6 15.75 10.73 -23 7 10 0.26 9.04 -23 7 10 -1.79 8.07 -23 -7 10 2.10 8.99 23 7 -10 -2.86 14.00 -23 -7 10 -4.36 8.26 12 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15.83 -9 -11 -11 110.82 9.84 -9 11 -11 140.68 12.81 -5 -9 -14 10.85 8.92 -5 -9 -14 3.55 4.56 5 -9 14 -3.74 20.06 5 9 14 3.77 11.71 -28 2 -5 -1.74 6.45 -28 -2 -5 0.38 6.96 28 -2 5 -12.56 16.25 28 2 5 1.31 14.84 -28 -2 -5 -1.01 6.16 -7 -7 -15 -0.68 8.21 7 -7 15 3.94 18.33 7 7 15 1.25 14.00 -22 8 -7 27.89 9.29 -22 -8 -7 42.61 6.54 -22 -8 -7 32.18 7.38 -3 -15 5 84.57 10.28 -3 -15 5 89.66 9.39 -3 -15 5 85.61 25.41 3 -15 -5 90.17 9.79 -1 -13 10 539.69 43.30 1 -13 -10 512.94 25.97 0 -14 8 116.58 10.63 0 -14 8 102.53 9.28 0 -14 -8 100.02 10.21 0 -14 8 84.46 24.27 -25 7 8 25.04 10.37 -25 -7 8 14.48 9.47 25 7 -8 30.08 14.99 -25 -7 8 13.34 9.01 -8 -14 -6 17.17 6.90 8 14 6 5.84 11.36 8 -14 6 17.96 5.44 -13 11 11 360.27 23.86 -13 11 11 439.20 26.28 -13 -11 11 398.64 22.20 -13 -11 11 332.94 49.50 13 -11 -11 384.68 27.12 -19 11 -5 3.53 7.48 -19 -11 -5 5.55 6.01 -19 -11 -5 2.87 6.20 19 11 5 4.35 14.02 -19 11 -5 0.56 8.60 -8 -14 7 174.85 12.37 8 -14 -7 167.12 12.84 -8 -14 7 181.64 13.76 -8 14 7 186.87 17.39 8 14 -7 153.79 18.82 -21 -11 -2 225.98 15.82 -21 11 -2 301.40 19.37 -21 -11 -2 245.82 16.50 21 11 2 204.87 23.13 -21 11 -2 285.64 19.77 -3 -13 10 48.67 25.29 3 -13 -10 44.76 7.88 -3 -13 10 48.79 7.67 -3 13 10 52.79 11.79 -26 0 11 -1.52 8.40 -26 0 11 -0.86 6.68 26 0 -11 0.63 9.39 -25 -9 2 5.27 6.96 -25 -9 2 5.40 6.75 -25 9 2 4.42 6.88 -25 9 2 2.15 9.01 25 9 -2 -1.74 14.47 -17 11 9 363.61 23.61 -17 -11 9 386.74 21.59 -17 -11 9 351.24 19.25 17 11 -9 349.98 28.52 -17 11 9 357.25 24.81 4 12 11 429.75 28.34 4 -12 11 508.35 39.80 -4 -12 -11 457.35 23.21 11 3 -17 31.68 9.50 -11 3 17 28.86 13.13 -11 -3 17 29.63 21.60 -20 10 -6 54.65 9.53 -20 -10 -6 47.88 7.96 20 10 6 43.59 15.43 -20 -10 -6 31.85 7.17 -25 9 1 3.47 7.06 -25 9 1 -0.31 9.88 -25 -9 1 5.83 6.62 -25 -9 1 3.12 6.43 25 9 -1 0.88 13.06 -8 -12 -10 17.98 6.34 8 12 10 4.31 11.17 8 -12 10 15.38 19.44 -6 -2 -17 26.10 9.14 6 2 17 28.13 17.98 6 -2 17 18.44 18.41 -7 -5 -16 -5.83 8.12 7 5 16 -6.41 15.71 7 -5 16 -11.67 17.96 8 -12 -11 17.99 6.16 -8 -12 11 21.49 6.91 -8 -12 11 6.90 23.49 -8 12 11 15.96 9.74 8 -12 -11 19.30 11.42 25 5 7 74.51 17.45 25 -5 7 76.08 17.79 -25 5 -7 53.74 8.82 -25 -5 -7 57.87 9.89 13 -3 15 10.75 19.24 -13 -3 -15 34.02 8.53 13 3 15 11.92 16.23 17 13 -2 108.32 18.76 -17 13 2 138.70 16.67 -17 -13 2 134.20 11.36 -17 13 2 126.11 13.85 -5 -5 17 711.39 48.36 5 -5 -17 675.04 36.34 -5 5 17 661.25 37.97 5 5 -17 613.02 31.97 -18 10 10 2.76 9.95 -18 10 10 8.10 7.97 -18 -10 10 9.96 7.55 18 10 -10 9.46 13.49 18 -10 -10 20.20 13.09 -17 -13 0 28.30 7.09 -17 -13 0 24.82 7.87 -17 13 0 32.98 10.18 17 13 0 33.30 15.62 5 15 4 234.81 19.46 5 -15 4 218.16 14.42 -1 -5 17 3.83 19.66 -1 5 17 -1.86 13.33 1 -5 -17 4.33 9.98 1 5 -17 2.19 6.41 -27 -1 10 -0.25 8.36 -27 -1 10 0.53 6.94 -27 1 10 12.81 8.66 -27 1 10 0.95 6.64 27 1 -10 6.91 10.12 -22 6 -9 334.07 20.36 -22 -6 -9 318.05 18.51 22 -6 9 350.32 27.72 11 -5 15 667.47 44.35 -11 -5 -15 611.48 30.79 11 5 15 602.93 38.77 5 3 17 6.86 17.66 -5 3 -17 22.54 7.64 -5 -3 -17 25.79 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-5 18 56.35 29.28 10 -14 -12 0.38 13.52 10 -14 -12 2.53 6.07 16 12 11 110.15 20.03 -16 -12 -11 106.38 10.80 10 6 -19 2.52 7.75 -26 12 1 55.29 10.54 11 17 -2 -0.43 13.31 -26 -10 -6 22.95 7.35 14 14 9 18.81 15.80 -14 -14 -9 4.94 7.73 -14 14 -9 2.34 10.87 15 -15 -8 15.47 15.56 12 14 10 463.19 32.92 -12 14 -10 516.10 30.06 -17 -13 -9 81.32 9.93 -17 13 -9 89.76 13.76 -12 0 20 297.72 29.69 -14 -12 -12 282.76 17.16 14 12 12 248.09 24.82 11 17 1 18.21 13.75 -35 -1 2 130.84 13.91 -35 1 2 166.22 14.69 -6 -14 -12 870.14 40.23 7 7 18 156.07 23.20 7 -13 -14 67.31 8.60 7 -13 -14 57.26 15.71 -34 -4 0 2.41 9.72 -34 4 0 -2.47 8.17 -28 -10 -3 18.53 8.00 3 7 -19 -3.14 7.35 -19 15 -1 0.62 9.86 -3 -15 -11 226.67 15.95 -35 1 3 471.95 26.82 0 4 20 411.66 32.97 -26 12 0 277.97 20.44 13 5 -19 178.77 15.50 -33 -5 -2 24.08 10.69 -35 -1 1 21.86 9.56 -35 1 1 36.20 8.96 5 7 -19 56.94 9.15 -18 12 -10 5.75 10.76 -27 -3 -11 25.09 7.89 -27 3 -11 16.52 7.20 -32 -6 -3 17.69 10.08 2 -14 -13 52.07 8.84 -11 -13 -12 31.15 7.52 11 13 12 18.75 14.30 11 -13 12 26.95 22.06 -22 14 0 374.37 24.74 3 3 20 28.21 18.40 -20 -2 18 298.20 33.94 20 2 -18 268.88 21.65 1 7 -19 0.40 7.15 -22 12 -7 508.11 30.04 -22 -12 -7 476.18 25.77 4 6 19 50.18 17.89 4 -14 -13 61.21 8.56 -16 -14 -8 4.91 7.02 16 14 8 -0.47 16.30 -16 14 -8 9.47 11.32 28 2 -14 46.26 12.64 25 1 -16 47.22 13.80 14 16 4 4.01 14.97 0 -14 -13 21.20 7.17 -21 -13 -6 14.63 7.67 8 10 16 120.51 19.70 -10 -14 -11 5.73 7.15 11 17 2 53.11 16.08 23 1 -17 79.56 14.84 -22 -10 -10 77.28 9.62 -22 10 -10 70.76 11.46 -35 1 0 1225.48 56.59 -35 -1 0 1330.52 57.66 -23 -7 -12 33.91 9.66 11 9 16 18.34 17.19 7 7 -19 106.75 11.06 -12 -2 20 38.82 23.65 -26 12 -1 34.69 11.04 -30 -8 -4 439.92 24.22 -12 -12 -13 137.47 11.37 12 12 13 134.51 19.51 -23 -5 16 53.88 33.79 -34 -4 -1 110.22 12.77 -30 0 -9 -0.84 7.02 -24 -6 -12 118.95 11.68 -30 4 -8 65.04 10.60 -22 14 -1 48.77 11.51 7 9 17 -11.31 16.85 -19 15 -2 189.68 18.23 13 -13 -13 23.36 7.26 -24 -12 -5 61.04 9.65 -29 -9 -4 105.75 11.11 6 -14 -13 54.70 8.96 14 -12 -14 35.72 7.73 -17 -11 -12 35.16 7.57 -28 4 -10 68.84 10.35 -28 -4 -10 84.22 10.74 -25 -5 15 271.04 41.79 -27 7 -9 50.83 10.25 -26 8 -9 201.96 17.99 9 11 15 1.68 14.16 -23 11 -8 -3.70 9.81 2 4 20 534.89 37.95 12 10 15 37.34 18.44 -13 -1 20 285.48 30.90 -22 -8 -12 190.68 13.93 -19 13 -8 747.17 38.65 -19 -13 -8 582.25 31.52 12 16 6 75.67 16.23 11 15 9 13.26 13.69 13 15 8 20.87 14.96 -13 15 -8 20.33 12.31 27 1 -15 42.81 12.19 10 8 17 -7.54 17.86 9 -13 -14 110.84 10.54 -25 -11 -6 67.69 9.35 -24 -4 16 37.14 27.42 -29 1 -10 52.26 8.52 -29 -1 -10 59.51 9.70 -15 -11 -13 0.88 6.02 -2 -14 -13 12.07 6.72 -27 -11 -3 21.50 8.11 -20 12 -9 41.00 12.12 -19 -11 -11 44.91 8.29 12 6 -19 141.96 12.91 -25 -5 -12 122.08 11.81 -35 -1 -1 280.73 18.88 -28 6 -9 21.19 9.58 -28 0 -11 -1.34 6.61 -25 9 -9 19.43 10.18 -35 3 2 27.36 9.42 -22 -4 17 136.67 36.17 12 -14 -12 15.14 7.15 11 17 3 8.25 12.99 -26 -4 15 166.07 40.67 -30 2 -9 212.37 15.77 -28 -10 -4 -1.99 7.39 32 0 -11 -2.28 12.32 31 1 -12 17.21 12.06 -9 -13 -13 42.28 7.70 9 7 -19 20.74 7.31 30 0 -13 3.37 11.88 -22 14 -2 161.70 16.73 -35 -3 1 127.90 14.14 -35 3 1 138.12 13.54 17 3 -19 38.09 12.61 -17 -3 19 41.73 24.18 15 15 7 16.08 14.85 16 4 -19 309.01 21.70 -8 -14 -12 197.19 14.54 8 -14 -13 40.88 8.31 6 8 18 696.46 42.85 -21 -9 -12 105.08 10.61 -32 8 2 -1.32 8.99 -27 -5 14 7.54 39.36 -32 8 1 204.90 16.74 14 16 5 351.75 28.24 13 11 14 203.97 24.16 6 6 19 37.20 18.92 -31 9 1 167.59 15.53 23 3 -17 101.32 14.18 -23 -3 17 105.45 28.16 -25 -7 -11 65.69 11.11 10 12 14 -6.97 14.52 -35 -3 0 61.52 11.38 -35 3 0 64.47 10.57 1 5 20 1.35 15.60 1 -15 -12 76.26 10.24 -28 2 -11 22.89 7.85 -28 -2 -11 33.58 8.11 -18 -2 19 1164.39 68.26 15 5 -19 290.28 20.12 -25 13 0 278.04 21.64 -4 -14 -13 108.23 10.61 -21 11 -10 90.95 12.80 -33 7 2 539.11 29.78 6 18 -2 79.54 15.41 -24 -8 -11 209.29 15.57 33 1 -10 26.57 12.44 -29 5 -9 2.28 8.35 -24 10 -9 3.47 8.87 -33 7 1 4.86 8.45 -26 -6 -11 6.93 8.33 -32 8 0 14.51 8.78 29 1 -14 -1.44 11.40 -3 1 21 261.66 28.05 -31 9 0 -2.83 8.01 -6 0 21 -10.54 19.80 -5 1 21 83.53 21.94 -14 -2 20 25.55 22.93 -20 -4 18 140.34 31.89 20 4 -18 100.15 13.57 11 -13 -14 159.38 12.86 -30 10 1 -4.18 9.91 -29 -3 -10 127.24 12.26 -29 3 -10 98.72 11.64 -27 -11 -4 8.02 7.50 -28 -4 14 -2.42 34.89 11 17 4 13.29 13.99 -21 -13 -7 8.98 7.55 -25 13 -1 13.67 9.69 -14 -14 -10 304.72 19.90 14 14 10 330.80 28.36 -33 7 0 19.71 8.36 4 8 -19 34.14 8.10 -24 -12 -6 67.31 9.96 6 18 -3 10.16 13.57 10 10 16 0.46 16.07 -35 -3 -1 -3.93 9.15 -23 -9 -11 13.15 7.95 2 8 -19 16.08 7.30 -7 1 21 22.10 18.42 21 3 -18 153.12 17.75 -21 -3 18 380.71 49.19 -30 10 0 84.34 12.48 -4 2 21 145.02 24.10 9 9 17 1.39 16.45 13 13 12 177.44 22.50 -13 -13 -12 190.13 13.88 12 14 11 -2.56 15.34 12 16 7 200.73 21.10 -8 0 21 -11.94 18.76 -20 -10 -12 357.48 20.43 10 -14 -13 25.28 7.44 -16 -14 -9 49.33 9.27 -16 14 -9 76.61 13.87 -2 2 21 20.44 19.08 6 8 -19 -7.32 7.21 -27 -5 -11 512.53 26.86 24 2 -17 3.92 11.35 3 5 20 -4.93 18.16 26 2 -16 26.06 12.30 -34 6 1 838.31 40.93 8 18 0 173.22 19.91 8 18 -1 12.87 13.98 -28 -10 -5 88.39 10.42 -16 -12 -12 11.09 6.62 -36 0 1 -5.86 9.38 11 11 15 -2.25 15.86 5 7 19 25.72 18.20 8 18 -2 18.49 14.47 -6 -14 -13 32.13 7.68 -13 15 -9 32.03 11.82 13 15 9 27.23 14.70 -14 -12 -13 24.19 7.23 -19 13 -9 59.48 13.23 -23 11 -9 -0.31 9.55 8 8 18 12.59 17.11 -3 3 21 52.01 20.00 -36 0 0 3.39 8.34 -29 11 0 -4.90 8.89 -11 -13 -13 2.31 6.27 -26 8 -10 15.23 10.05 -27 7 -10 5.10 8.62 -10 0 21 -16.26 20.52 -36 2 1 278.17 19.46 -1 3 21 103.49 22.66 -27 -11 -5 427.40 24.08 -28 -4 -11 77.11 10.83 18 4 -19 632.29 34.65 31 1 -13 13.05 11.88 -33 -7 -2 110.25 14.12 -25 9 -10 96.16 12.38 -19 -3 19 9.14 24.64 -35 5 1 27.17 9.63 -28 6 -10 2.60 9.45 -29 -1 -11 98.24 10.72 -36 -2 0 30.83 10.09 -16 -2 20 615.31 47.22 12 12 14 -3.90 14.77 10 18 1 108.05 18.56 ; _shelx_hkl_checksum 47246 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.04604(2) 0.42289(4) 0.52796(3) 0.04317(13) Uani 1 1 d . . . . . Cl2 Cl 0.10235(2) 0.33265(4) 0.40693(3) 0.04780(14) Uani 1 1 d . . . . . S3 S 0.22096(2) 0.64843(2) 0.34583(2) 0.01530(10) Uani 1 1 d . . . . . O3 O 0.23562(3) 0.71794(7) 0.41011(6) 0.0204(2) Uani 1 1 d . . . . . O4 O 0.23465(4) 0.66825(7) 0.26358(6) 0.0201(2) Uani 1 1 d . . . . . O21 O 0.18069(4) 0.47529(7) 0.60807(6) 0.0234(2) Uani 1 1 d . . . . . N1 N 0.29083(4) 0.40514(8) 0.34530(7) 0.0160(2) Uani 1 1 d . . . . . N22 N 0.21017(4) 0.62002(9) 0.65042(7) 0.0188(2) Uani 1 1 d D . . . . C2 C 0.27396(4) 0.49471(9) 0.33052(8) 0.0147(3) Uani 1 1 d . . . . . H2 H 0.284794 0.529273 0.285310 0.018 Uiso 1 1 calc R U . . . C3 C 0.24234(5) 0.53652(9) 0.37769(8) 0.0148(3) Uani 1 1 d . . . . . C4 C 0.22502(5) 0.49162(10) 0.45520(8) 0.0155(3) Uani 1 1 d . . . . . H4 H 0.188443 0.496176 0.449936 0.019 Uiso 1 1 calc R U . . . C5 C 0.23824(5) 0.38758(10) 0.45366(8) 0.0181(3) Uani 1 1 d . . . . . H5 H 0.223377 0.345835 0.489851 0.022 Uiso 1 1 calc R U . . . C6 C 0.26946(5) 0.35078(9) 0.40468(9) 0.0177(3) Uani 1 1 d . . . . . H6 H 0.277560 0.285268 0.410129 0.021 Uiso 1 1 calc R U . . . C7 C 0.32880(5) 0.36515(10) 0.29899(9) 0.0181(3) Uani 1 1 d . . . . . H7A H 0.328633 0.399602 0.245448 0.022 Uiso 1 1 calc R U . . . H7B H 0.320671 0.297859 0.285963 0.022 Uiso 1 1 calc R U . . . C8 C 0.38007(5) 0.36985(9) 0.34472(8) 0.0163(3) Uani 1 1 d . . . . . C9 C 0.39019(5) 0.41124(10) 0.42292(9) 0.0215(3) Uani 1 1 d . . . . . H9 H 0.364350 0.438130 0.450027 0.026 Uiso 1 1 calc R U . . . C10 C 0.43781(5) 0.41348(11) 0.46158(9) 0.0255(3) Uani 1 1 d . . . . . H10 H 0.444410 0.442527 0.514744 0.031 Uiso 1 1 calc R U . . . C11 C 0.47591(5) 0.37357(12) 0.42315(9) 0.0257(3) Uani 1 1 d . . . . . H11 H 0.508472 0.375007 0.449871 0.031 Uiso 1 1 calc R U . . . C12 C 0.46600(5) 0.33166(11) 0.34551(9) 0.0258(3) Uani 1 1 d . . . . . H12 H 0.491837 0.303867 0.318998 0.031 Uiso 1 1 calc R U . . . C13 C 0.41859(5) 0.33008(10) 0.30636(9) 0.0209(3) Uani 1 1 d . . . . . H13 H 0.412196 0.301676 0.252889 0.025 Uiso 1 1 calc R U . . . C14 C 0.15657(5) 0.63937(9) 0.34224(9) 0.0170(3) Uani 1 1 d . . . . . C15 C 0.12979(5) 0.60769(10) 0.26973(9) 0.0203(3) Uani 1 1 d . . . . . H15 H 0.145570 0.592847 0.221699 0.024 Uiso 1 1 calc R U . . . C16 C 0.07930(5) 0.59817(11) 0.26902(10) 0.0258(3) Uani 1 1 d . . . . . H16 H 0.060249 0.577465 0.219713 0.031 Uiso 1 1 calc R U . . . C17 C 0.05658(5) 0.61859(11) 0.33942(11) 0.0284(3) Uani 1 1 d . . . . . H17 H 0.022089 0.611136 0.338166 0.034 Uiso 1 1 calc R U . . . C18 C 0.08352(6) 0.64977(11) 0.41178(10) 0.0273(3) Uani 1 1 d . . . . . H18 H 0.067586 0.663476 0.459891 0.033 Uiso 1 1 calc R U . . . C19 C 0.13408(5) 0.66096(10) 0.41369(9) 0.0217(3) Uani 1 1 d . . . . . H19 H 0.152950 0.682902 0.462743 0.026 Uiso 1 1 calc R U . . . C20 C 0.24525(5) 0.54643(9) 0.53665(8) 0.0151(3) Uani 1 1 d . . . . . H20 H 0.248132 0.614725 0.520666 0.018 Uiso 1 1 calc R U . . . C21 C 0.20834(5) 0.54258(10) 0.60131(8) 0.0161(3) Uani 1 1 d . . . . . C23 C 0.17643(5) 0.63713(10) 0.71294(9) 0.0208(3) Uani 1 1 d . . . . . H23A H 0.192995 0.676968 0.758049 0.025 Uiso 1 1 calc R U . . . H23B H 0.168080 0.575636 0.737735 0.025 Uiso 1 1 calc R U . . . C24 C 0.12946(5) 0.68612(10) 0.67736(8) 0.0194(3) Uani 1 1 d . . . . . C25 C 0.13093(5) 0.77027(11) 0.63273(9) 0.0248(3) Uani 1 1 d . . . . . H25 H 0.161647 0.797087 0.623336 0.030 Uiso 1 1 calc R U . . . C26 C 0.08774(6) 0.81562(12) 0.60167(10) 0.0319(4) Uani 1 1 d . . . . . H26 H 0.089089 0.873353 0.571442 0.038 Uiso 1 1 calc R U . . . C27 C 0.04274(6) 0.77674(13) 0.61473(10) 0.0339(4) Uani 1 1 d . . . . . H27 H 0.013233 0.807639 0.593533 0.041 Uiso 1 1 calc R U . . . C28 C 0.04108(6) 0.69295(14) 0.65868(11) 0.0371(4) Uani 1 1 d . . . . . H28 H 0.010373 0.665848 0.667727 0.045 Uiso 1 1 calc R U . . . C29 C 0.08422(6) 0.64827(12) 0.68964(10) 0.0295(3) Uani 1 1 d . . . . . H29 H 0.082709 0.590580 0.719875 0.035 Uiso 1 1 calc R U . . . C30 C 0.29552(5) 0.51592(10) 0.57583(8) 0.0160(3) Uani 1 1 d . . . . . C31 C 0.30279(5) 0.43171(10) 0.62126(8) 0.0188(3) Uani 1 1 d . . . . . H31 H 0.275891 0.390221 0.625894 0.023 Uiso 1 1 calc R U . . . C32 C 0.34896(5) 0.40775(10) 0.65986(8) 0.0206(3) Uani 1 1 d . . . . . H32 H 0.353227 0.349761 0.689927 0.025 Uiso 1 1 calc R U . . . C33 C 0.38910(5) 0.46788(11) 0.65497(8) 0.0203(3) Uani 1 1 d . . . . . C34 C 0.38178(5) 0.55137(10) 0.60945(8) 0.0198(3) Uani 1 1 d . . . . . H34 H 0.408656 0.592965 0.605035 0.024 Uiso 1 1 calc R U . . . C35 C 0.33568(5) 0.57528(10) 0.57010(8) 0.0179(3) Uani 1 1 d . . . . . H35 H 0.331623 0.632649 0.539071 0.021 Uiso 1 1 calc R U . . . C36 C 0.43860(5) 0.44288(12) 0.69966(10) 0.0288(3) Uani 1 1 d . . . . . H36A H 0.464113 0.479438 0.675740 0.035 Uiso 1 1 calc R U . . . H36B H 0.444753 0.374787 0.693246 0.035 Uiso 1 1 calc R U . . . H36C H 0.439072 0.458182 0.759007 0.035 Uiso 1 1 calc R U . . . C41 C 0.09597(6) 0.34797(11) 0.51402(10) 0.0289(3) Uani 1 1 d . . . . . H41A H 0.090872 0.285315 0.539689 0.035 Uiso 1 1 calc R U . . . H41B H 0.126417 0.375892 0.542341 0.035 Uiso 1 1 calc R U . . . H22 H 0.2305(6) 0.6728(10) 0.6361(12) 0.048(6) Uiso 1 1 d D . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0446(3) 0.0502(3) 0.0371(3) 0.00509(19) 0.01547(19) 0.0176(2) Cl2 0.0342(2) 0.0696(3) 0.0407(3) -0.0207(2) 0.00916(19) 0.0016(2) S3 0.01543(17) 0.01495(17) 0.01580(18) 0.00143(11) 0.00298(12) 0.00118(11) O3 0.0230(5) 0.0170(5) 0.0214(5) -0.0013(4) 0.0025(4) -0.0025(4) O4 0.0218(5) 0.0201(5) 0.0194(5) 0.0059(4) 0.0065(4) 0.0041(4) O21 0.0238(5) 0.0272(6) 0.0202(5) -0.0009(4) 0.0070(4) -0.0071(4) N1 0.0158(5) 0.0165(6) 0.0160(6) 0.0004(4) 0.0029(4) 0.0014(4) N22 0.0179(6) 0.0205(6) 0.0191(6) 0.0000(5) 0.0079(5) 0.0002(4) C2 0.0135(6) 0.0157(6) 0.0144(6) 0.0013(5) -0.0002(5) -0.0017(5) C3 0.0136(6) 0.0153(6) 0.0150(6) 0.0013(5) -0.0007(5) -0.0007(5) C4 0.0136(6) 0.0199(7) 0.0131(6) 0.0015(5) 0.0018(5) -0.0009(5) C5 0.0196(6) 0.0184(7) 0.0158(7) 0.0045(5) 0.0004(5) -0.0041(5) C6 0.0194(6) 0.0149(6) 0.0183(7) 0.0025(5) -0.0008(5) -0.0017(5) C7 0.0182(6) 0.0185(7) 0.0178(7) -0.0031(5) 0.0028(5) 0.0031(5) C8 0.0169(6) 0.0139(6) 0.0184(7) 0.0018(5) 0.0026(5) 0.0009(5) C9 0.0187(7) 0.0232(7) 0.0231(7) -0.0039(6) 0.0042(5) 0.0027(5) C10 0.0222(7) 0.0326(8) 0.0215(7) -0.0047(6) 0.0013(6) -0.0015(6) C11 0.0166(7) 0.0362(9) 0.0242(8) 0.0053(6) 0.0019(6) 0.0015(6) C12 0.0208(7) 0.0337(8) 0.0242(8) 0.0049(6) 0.0080(6) 0.0088(6) C13 0.0235(7) 0.0219(7) 0.0179(7) 0.0001(5) 0.0053(5) 0.0042(5) C14 0.0160(6) 0.0155(6) 0.0200(7) 0.0016(5) 0.0044(5) 0.0032(5) C15 0.0207(7) 0.0198(7) 0.0203(7) -0.0004(5) 0.0019(5) 0.0041(5) C16 0.0216(7) 0.0251(8) 0.0295(8) -0.0010(6) -0.0026(6) 0.0026(6) C17 0.0165(7) 0.0272(8) 0.0421(9) 0.0020(7) 0.0053(6) 0.0030(6) C18 0.0231(7) 0.0294(8) 0.0315(9) -0.0019(6) 0.0124(6) 0.0039(6) C19 0.0221(7) 0.0222(7) 0.0214(7) -0.0027(6) 0.0050(6) 0.0023(5) C20 0.0143(6) 0.0172(6) 0.0141(6) 0.0007(5) 0.0028(5) 0.0000(5) C21 0.0132(6) 0.0217(7) 0.0131(6) 0.0038(5) 0.0003(5) 0.0024(5) C23 0.0219(7) 0.0247(7) 0.0167(7) -0.0003(5) 0.0062(5) 0.0056(5) C24 0.0225(7) 0.0226(7) 0.0133(6) -0.0035(5) 0.0033(5) 0.0049(5) C25 0.0256(7) 0.0253(8) 0.0236(8) 0.0010(6) 0.0034(6) 0.0012(6) C26 0.0379(9) 0.0305(9) 0.0269(8) 0.0055(7) 0.0024(7) 0.0098(7) C27 0.0273(8) 0.0517(11) 0.0228(8) 0.0017(7) 0.0030(6) 0.0187(7) C28 0.0206(8) 0.0566(12) 0.0349(9) 0.0061(8) 0.0070(7) 0.0024(7) C29 0.0262(8) 0.0329(9) 0.0304(9) 0.0078(7) 0.0078(6) 0.0018(6) C30 0.0137(6) 0.0228(7) 0.0118(6) -0.0021(5) 0.0027(5) 0.0013(5) C31 0.0177(6) 0.0230(7) 0.0159(7) -0.0008(5) 0.0034(5) -0.0017(5) C32 0.0234(7) 0.0225(7) 0.0159(7) 0.0012(5) 0.0026(5) 0.0038(5) C33 0.0161(6) 0.0287(7) 0.0163(7) -0.0042(6) 0.0019(5) 0.0046(5) C34 0.0157(6) 0.0259(7) 0.0185(7) -0.0046(5) 0.0042(5) -0.0031(5) C35 0.0191(6) 0.0201(7) 0.0150(7) -0.0010(5) 0.0044(5) 0.0007(5) C36 0.0187(7) 0.0394(9) 0.0273(8) -0.0007(7) -0.0016(6) 0.0064(6) C41 0.0251(8) 0.0282(8) 0.0327(9) -0.0007(6) 0.0000(6) -0.0002(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; H H 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Table 6.1.1.4) ; N N 0.0061 0.0033 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; O O 0.0106 0.0060 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; S S 0.1246 0.1234 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; Cl Cl 0.1484 0.1585 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 S3 O3 116.57(6) . . ? O4 S3 C3 109.51(6) . . ? O3 S3 C3 109.85(6) . . ? O4 S3 C14 109.90(6) . . ? O3 S3 C14 105.84(6) . . ? C3 S3 C14 104.44(6) . . ? C2 N1 C6 117.89(11) . . ? C2 N1 C7 121.21(11) . . ? C6 N1 C7 120.87(11) . . ? C21 N22 C23 123.63(12) . . ? C21 N22 H22 117.8(12) . . ? C23 N22 H22 117.4(13) . . ? C3 C2 N1 122.33(12) . . ? C3 C2 H2 118.8 . . ? N1 C2 H2 118.8 . . ? C2 C3 C4 123.95(12) . . ? C2 C3 S3 116.45(10) . . ? C4 C3 S3 119.60(10) . . ? C5 C4 C3 107.02(11) . . ? C5 C4 C20 115.15(11) . . ? C3 C4 C20 111.70(11) . . ? C5 C4 H4 107.6 . . ? C3 C4 H4 107.6 . . ? C20 C4 H4 107.6 . . ? C6 C5 C4 123.95(12) . . ? C6 C5 H5 118.0 . . ? C4 C5 H5 118.0 . . ? C5 C6 N1 122.41(12) . . ? C5 C6 H6 118.8 . . ? N1 C6 H6 118.8 . . ? N1 C7 C8 114.18(11) . . ? N1 C7 H7A 108.7 . . ? C8 C7 H7A 108.7 . . ? N1 C7 H7B 108.7 . . ? C8 C7 H7B 108.7 . . ? H7A C7 H7B 107.6 . . ? C9 C8 C13 118.80(12) . . ? C9 C8 C7 122.99(12) . . ? C13 C8 C7 118.20(12) . . ? C10 C9 C8 120.37(13) . . ? C10 C9 H9 119.8 . . ? C8 C9 H9 119.8 . . ? C9 C10 C11 120.51(14) . . ? C9 C10 H10 119.7 . . ? C11 C10 H10 119.7 . . ? C12 C11 C10 119.38(14) . . ? C12 C11 H11 120.3 . . ? C10 C11 H11 120.3 . . ? C13 C12 C11 120.29(13) . . ? C13 C12 H12 119.9 . . ? C11 C12 H12 119.9 . . ? C12 C13 C8 120.65(13) . . ? C12 C13 H13 119.7 . . ? C8 C13 H13 119.7 . . ? C15 C14 C19 121.64(13) . . ? C15 C14 S3 119.31(10) . . ? C19 C14 S3 119.00(11) . . ? C14 C15 C16 118.44(13) . . ? C14 C15 H15 120.8 . . ? C16 C15 H15 120.8 . . ? C17 C16 C15 120.58(14) . . ? C17 C16 H16 119.7 . . ? C15 C16 H16 119.7 . . ? C16 C17 C18 120.76(14) . . ? C16 C17 H17 119.6 . . ? C18 C17 H17 119.6 . . ? C17 C18 C19 119.72(14) . . ? C17 C18 H18 120.1 . . ? C19 C18 H18 120.1 . . ? C18 C19 C14 118.86(14) . . ? C18 C19 H19 120.6 . . ? C14 C19 H19 120.6 . . ? C30 C20 C21 110.13(10) . . ? C30 C20 C4 115.73(11) . . ? C21 C20 C4 110.59(10) . . ? C30 C20 H20 106.6 . . ? C21 C20 H20 106.6 . . ? C4 C20 H20 106.6 . . ? O21 C21 N22 123.94(12) . . ? O21 C21 C20 123.29(12) . . ? N22 C21 C20 112.76(11) . . ? N22 C23 C24 112.85(11) . . ? N22 C23 H23A 109.0 . . ? C24 C23 H23A 109.0 . . ? N22 C23 H23B 109.0 . . ? C24 C23 H23B 109.0 . . ? H23A C23 H23B 107.8 . . ? C29 C24 C25 118.56(13) . . ? C29 C24 C23 120.59(13) . . ? C25 C24 C23 120.85(13) . . ? C24 C25 C26 120.49(14) . . ? C24 C25 H25 119.8 . . ? C26 C25 H25 119.8 . . ? C27 C26 C25 120.15(15) . . ? C27 C26 H26 119.9 . . ? C25 C26 H26 119.9 . . ? C28 C27 C26 119.58(15) . . ? C28 C27 H27 120.2 . . ? C26 C27 H27 120.2 . . ? C27 C28 C29 119.99(16) . . ? C27 C28 H28 120.0 . . ? C29 C28 H28 120.0 . . ? C24 C29 C28 121.23(15) . . ? C24 C29 H29 119.4 . . ? C28 C29 H29 119.4 . . ? C35 C30 C31 118.25(12) . . ? C35 C30 C20 119.55(12) . . ? C31 C30 C20 122.13(12) . . ? C32 C31 C30 120.85(13) . . ? C32 C31 H31 119.6 . . ? C30 C31 H31 119.6 . . ? C31 C32 C33 120.88(13) . . ? C31 C32 H32 119.6 . . ? C33 C32 H32 119.6 . . ? C34 C33 C32 118.11(12) . . ? C34 C33 C36 121.46(13) . . ? C32 C33 C36 120.42(13) . . ? C33 C34 C35 121.21(13) . . ? C33 C34 H34 119.4 . . ? C35 C34 H34 119.4 . . ? C30 C35 C34 120.70(13) . . ? C30 C35 H35 119.7 . . ? C34 C35 H35 119.7 . . ? C33 C36 H36A 109.5 . . ? C33 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C33 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? Cl1 C41 Cl2 110.89(9) . . ? Cl1 C41 H41A 109.5 . . ? Cl2 C41 H41A 109.5 . . ? Cl1 C41 H41B 109.5 . . ? Cl2 C41 H41B 109.5 . . ? H41A C41 H41B 108.1 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C41 1.7615(16) . ? Cl2 C41 1.7680(17) . ? S3 O4 1.4439(10) . ? S3 O3 1.4508(10) . ? S3 C3 1.7387(13) . ? S3 C14 1.7657(13) . ? O21 C21 1.2250(17) . ? N1 C2 1.3549(17) . ? N1 C6 1.4018(17) . ? N1 C7 1.4574(17) . ? N22 C21 1.3449(18) . ? N22 C23 1.4594(17) . ? N22 H22 0.971(5) . ? C2 C3 1.3482(18) . ? C2 H2 0.9500 . ? C3 C4 1.5212(18) . ? C4 C5 1.5089(19) . ? C4 C20 1.5732(17) . ? C4 H4 1.0000 . ? C5 C6 1.330(2) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C7 C8 1.5189(18) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C8 C9 1.3906(19) . ? C8 C13 1.3968(19) . ? C9 C10 1.387(2) . ? C9 H9 0.9500 . ? C10 C11 1.389(2) . ? C10 H10 0.9500 . ? C11 C12 1.385(2) . ? C11 H11 0.9500 . ? C12 C13 1.385(2) . ? C12 H12 0.9500 . ? C13 H13 0.9500 . ? C14 C15 1.387(2) . ? C14 C19 1.3972(19) . ? C15 C16 1.390(2) . ? C15 H15 0.9500 . ? C16 C17 1.382(2) . ? C16 H16 0.9500 . ? C17 C18 1.385(2) . ? C17 H17 0.9500 . ? C18 C19 1.393(2) . ? C18 H18 0.9500 . ? C19 H19 0.9500 . ? C20 C30 1.5169(17) . ? C20 C21 1.5297(17) . ? C20 H20 1.0000 . ? C23 C24 1.5193(19) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C24 C29 1.384(2) . ? C24 C25 1.388(2) . ? C25 C26 1.392(2) . ? C25 H25 0.9500 . ? C26 C27 1.387(2) . ? C26 H26 0.9500 . ? C27 C28 1.379(3) . ? C27 H27 0.9500 . ? C28 C29 1.386(2) . ? C28 H28 0.9500 . ? C29 H29 0.9500 . ? C30 C35 1.3933(19) . ? C30 C31 1.3963(19) . ? C31 C32 1.3923(19) . ? C31 H31 0.9500 . ? C32 C33 1.397(2) . ? C32 H32 0.9500 . ? C33 C34 1.388(2) . ? C33 C36 1.5103(19) . ? C34 C35 1.3948(19) . ? C34 H34 0.9500 . ? C35 H35 0.9500 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C41 H41A 0.9900 . ? C41 H41B 0.9900 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DA _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_angle_DHA _geom_hbond_publ_flag N22 H22 O3 . . 7_566 2.9443(16) 0.971(16) 1.982(17) 170.6(16) no loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C6 N1 C2 C3 8.55(18) . . . . ? C7 N1 C2 C3 -173.56(12) . . . . ? N1 C2 C3 C4 4.4(2) . . . . ? N1 C2 C3 S3 -175.58(10) . . . . ? O4 S3 C3 C2 10.88(12) . . . . ? O3 S3 C3 C2 -118.35(10) . . . . ? C14 S3 C3 C2 128.54(10) . . . . ? O4 S3 C3 C4 -169.12(10) . . . . ? O3 S3 C3 C4 61.65(11) . . . . ? C14 S3 C3 C4 -51.46(11) . . . . ? C2 C3 C4 C5 -14.97(17) . . . . ? S3 C3 C4 C5 165.02(9) . . . . ? C2 C3 C4 C20 111.91(14) . . . . ? S3 C3 C4 C20 -68.09(13) . . . . ? C3 C4 C5 C6 14.78(17) . . . . ? C20 C4 C5 C6 -110.03(14) . . . . ? C4 C5 C6 N1 -4.3(2) . . . . ? C2 N1 C6 C5 -8.74(19) . . . . ? C7 N1 C6 C5 173.36(12) . . . . ? C2 N1 C7 C8 98.43(14) . . . . ? C6 N1 C7 C8 -83.74(15) . . . . ? N1 C7 C8 C9 -1.83(19) . . . . ? N1 C7 C8 C13 177.73(12) . . . . ? C13 C8 C9 C10 0.5(2) . . . . ? C7 C8 C9 C10 -179.94(13) . . . . ? C8 C9 C10 C11 -0.7(2) . . . . ? C9 C10 C11 C12 0.2(2) . . . . ? C10 C11 C12 C13 0.4(2) . . . . ? C11 C12 C13 C8 -0.6(2) . . . . ? C9 C8 C13 C12 0.1(2) . . . . ? C7 C8 C13 C12 -179.46(13) . . . . ? O4 S3 C14 C15 29.54(13) . . . . ? O3 S3 C14 C15 156.20(11) . . . . ? C3 S3 C14 C15 -87.85(12) . . . . ? O4 S3 C14 C19 -152.83(11) . . . . ? O3 S3 C14 C19 -26.17(13) . . . . ? C3 S3 C14 C19 89.78(12) . . . . ? C19 C14 C15 C16 0.4(2) . . . . ? S3 C14 C15 C16 177.99(11) . . . . ? C14 C15 C16 C17 -0.9(2) . . . . ? C15 C16 C17 C18 0.6(2) . . . . ? C16 C17 C18 C19 0.2(2) . . . . ? C17 C18 C19 C14 -0.6(2) . . . . ? C15 C14 C19 C18 0.3(2) . . . . ? S3 C14 C19 C18 -177.24(11) . . . . ? C5 C4 C20 C30 35.75(15) . . . . ? C3 C4 C20 C30 -86.58(14) . . . . ? C5 C4 C20 C21 -90.34(13) . . . . ? C3 C4 C20 C21 147.33(11) . . . . ? C23 N22 C21 O21 -5.6(2) . . . . ? C23 N22 C21 C20 175.36(11) . . . . ? C30 C20 C21 O21 -97.29(15) . . . . ? C4 C20 C21 O21 31.87(17) . . . . ? C30 C20 C21 N22 81.71(14) . . . . ? C4 C20 C21 N22 -149.13(11) . . . . ? C21 N22 C23 C24 -86.46(16) . . . . ? N22 C23 C24 C29 127.42(15) . . . . ? N22 C23 C24 C25 -53.35(18) . . . . ? C29 C24 C25 C26 0.4(2) . . . . ? C23 C24 C25 C26 -178.80(13) . . . . ? C24 C25 C26 C27 -0.3(2) . . . . ? C25 C26 C27 C28 0.0(3) . . . . ? C26 C27 C28 C29 0.2(3) . . . . ? C25 C24 C29 C28 -0.3(2) . . . . ? C23 C24 C29 C28 178.98(15) . . . . ? C27 C28 C29 C24 0.0(3) . . . . ? C21 C20 C30 C35 -126.16(13) . . . . ? C4 C20 C30 C35 107.52(14) . . . . ? C21 C20 C30 C31 50.76(16) . . . . ? C4 C20 C30 C31 -75.57(16) . . . . ? C35 C30 C31 C32 0.0(2) . . . . ? C20 C30 C31 C32 -176.91(12) . . . . ? C30 C31 C32 C33 0.8(2) . . . . ? C31 C32 C33 C34 -1.0(2) . . . . ? C31 C32 C33 C36 177.79(13) . . . . ? C32 C33 C34 C35 0.5(2) . . . . ? C36 C33 C34 C35 -178.31(13) . . . . ? C31 C30 C35 C34 -0.58(19) . . . . ? C20 C30 C35 C34 176.46(12) . . . . ? C33 C34 C35 C30 0.3(2) . . . . ?