Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1564337
Preview
| Coordinates | 1564337.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C14 H31 B O2 Si |
|---|---|
| Calculated formula | C14 H31 B O2 Si |
| Title of publication | Synthesis of hydrosilylboronates via the monoborylation of a dihydrosilane Si‒H bond and their application for the generation of dialkylhydrosilyl anions |
| Authors of publication | Takeuchi, Takumi; Shishido, Ryosuke; Kubota, Koji; Ito, Hajime |
| Journal of publication | Chemical Science |
| Year of publication | 2021 |
| a | 12.7304 ± 0.0006 Å |
| b | 14.6636 ± 0.0006 Å |
| c | 9.7331 ± 0.0004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1816.91 ± 0.14 Å3 |
| Cell temperature | 173 K |
| Ambient diffraction temperature | 173 K |
| Number of distinct elements | 5 |
| Space group number | 62 |
| Hermann-Mauguin space group symbol | P n m a |
| Hall space group symbol | -P 2ac 2n |
| Residual factor for all reflections | 0.0948 |
| Residual factor for significantly intense reflections | 0.0772 |
| Weighted residual factors for significantly intense reflections | 0.2346 |
| Weighted residual factors for all reflections included in the refinement | 0.2568 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 268011 (current) | 2021-08-11 | cif/ Adding structures of 1564337 via cif-deposit CGI script. |
1564337.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.