#------------------------------------------------------------------------------ #$Date: 2021-08-19 01:11:09 +0300 (Thu, 19 Aug 2021) $ #$Revision: 268125 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/43/1564370.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564370 loop_ _publ_author_name 'Weng, Guo-Guo' 'Hong, Ben-Kun' 'Bao, Song-Song' 'Wen, Yujie' 'Wu, Lan-Qing' 'Huang, Xin-Da' 'Jia, Jia-Ge' 'Wen, Ge-Hua' 'Li, Shuhua' 'Peng, Luming' 'Zheng, Li-Min' _publ_section_title ; From helix to superhelix: hierarchical assembly of homochiral van der Waals 1D coordination polymers ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC01913A _journal_year 2021 _chemical_absolute_configuration rm _chemical_formula_moiety 'C27 H57 N3 O9 P3 Tb, C2 H4 O2, 2(H2 O)' _chemical_formula_sum 'C29 H65 N3 O13 P3 Tb' _chemical_formula_weight 915.67 _space_group_crystal_system hexagonal _space_group_IT_number 170 _space_group_name_Hall 'P 65' _space_group_name_H-M_alt 'P 65' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2021-07-02 deposited with the CCDC. 2021-08-13 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 17.0143(5) _cell_length_b 17.0143(5) _cell_length_c 23.5290(10) _cell_measurement_reflns_used 9966 _cell_measurement_temperature 193(2) _cell_measurement_theta_max 27.475 _cell_measurement_theta_min 2.215 _cell_volume 5898.8(4) _computing_cell_refinement 'SAINT V8.40A (Bruker Nano, Inc., 2019)' _computing_data_collection 'APEX 3' _computing_data_reduction 'SAINT V8.40A (Bruker Nano, Inc., 2019)' _computing_molecular_graphics SHELXTL _computing_publication_material SHELXTL _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 193(2) _diffrn_detector_area_resol_mean 4K _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker D8 with TXS' _diffrn_measurement_method CCD _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0512 _diffrn_reflns_av_unetI/netI 0.0331 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 55509 _diffrn_reflns_point_group_measured_fraction_full 0.902 _diffrn_reflns_point_group_measured_fraction_max 0.885 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.500 _diffrn_reflns_theta_min 2.215 _exptl_absorpt_coefficient_mu 1.982 _exptl_absorpt_correction_T_max 0.7519 _exptl_absorpt_correction_T_min 0.3540 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.547 _exptl_crystal_description rod-like _exptl_crystal_F_000 2844 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.978 _refine_diff_density_min -0.442 _refine_diff_density_rms 0.076 _refine_ls_abs_structure_details ; Flack x determined using 2983 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.010(5) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.039 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 452 _refine_ls_number_reflns 7990 _refine_ls_number_restraints 37 _refine_ls_restrained_S_all 1.042 _refine_ls_R_factor_all 0.0295 _refine_ls_R_factor_gt 0.0255 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0301P)^2^+4.0442P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0574 _refine_ls_wR_factor_ref 0.0597 _reflns_Friedel_coverage 0.729 _reflns_Friedel_fraction_full 0.799 _reflns_Friedel_fraction_max 0.765 _reflns_number_gt 7514 _reflns_number_total 7990 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc01913a2.cif _cod_data_source_block 2 _cod_database_code 1564370 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.637 _shelx_estimated_absorpt_t_max 0.826 _shelx_res_file ; TITL 11 in P6(5) 2.res created by SHELXL-2018/3 at 12:45:50 on 01-Jul-2021 CELL 0.71073 17.0143 17.0143 23.5290 90.000 90.000 120.000 ZERR 6.000 0.0005 0.0005 0.0010 0.000 0.000 0.000 LATT -1 SYMM -Y, X-Y, 2/3+Z SYMM -X+Y, -X, 1/3+Z SYMM -X, -Y, 1/2+Z SYMM Y, -X+Y, 1/6+Z SYMM X-Y, X, 5/6+Z SFAC C H N O P Tb UNIT 174 390 18 78 18 6 L.S. 10 ACTA BOND $H FMAP 2 PLAN 5 CONF HTAB O10 O9 HTAB O1W O6 HTAB O2W O3 HTAB O2W O2_$1 HTAB N1 O3_$2 HTAB N1 O8_$1 HTAB N2 O2W HTAB N2 O4_$2 HTAB N3 O6 HTAB N3 O9_$2 EQIV $1 y, -x+y+1, z+1/6 EQIV $2 x-y+1, x, z-1/6 FREE Tb1 P2 FREE Tb1 P1 SIMU 0.01 0.02 N2 C10 C11 SIMU 0.01 0.02 C23 C24 C25 C26 C27 SIMU 0.01 0.02 O1 O2 O3 SIZE 0.25 0.1 0.1 TEMP -80.170 WGHT 0.030100 4.044200 FVAR 0.22901 TB1 6 0.999354 0.972416 0.998957 11.00000 0.01524 0.01598 = 0.01029 0.00010 0.00019 0.00813 P1 5 0.870119 1.034248 1.043667 11.00000 0.01674 0.01802 = 0.01220 -0.00070 -0.00010 0.00966 P2 5 1.168799 1.140497 0.952788 11.00000 0.01421 0.01586 = 0.01376 -0.00085 -0.00119 0.00688 P3 5 1.098758 0.869981 0.917147 11.00000 0.02242 0.02518 = 0.01540 0.00229 0.00159 0.01678 O1 4 0.912564 0.990454 1.079753 11.00000 0.02042 0.01965 = 0.01357 0.00000 -0.00085 0.01160 O2 4 0.911850 1.046937 0.984786 11.00000 0.02521 0.02331 = 0.01288 0.00058 -0.00024 0.01515 O3 4 0.873451 1.117106 1.068990 11.00000 0.02362 0.01891 = 0.01773 -0.00173 -0.00103 0.01242 O4 4 1.132628 1.124281 1.013574 11.00000 0.02383 0.01766 = 0.01334 -0.00139 -0.00290 0.00976 O5 4 1.092570 1.064766 0.918418 11.00000 0.01751 0.02019 = 0.01339 -0.00219 -0.00354 0.00701 O6 4 1.260808 1.150940 0.944702 11.00000 0.01813 0.02540 = 0.02634 -0.00305 -0.00202 0.01148 O7 4 1.083589 0.909579 0.971194 11.00000 0.03348 0.04255 = 0.01339 -0.00192 -0.00016 0.02906 O8 4 1.065521 0.892999 0.863151 11.00000 0.03498 0.03164 = 0.01223 0.00017 0.00036 0.02498 O9 4 1.061484 0.769123 0.924377 11.00000 0.03400 0.02556 = 0.02696 0.00496 0.00296 0.01646 AFIX 6 O10 4 1.132304 0.674327 0.900777 11.00000 0.06422 0.05612 = 0.04508 0.01300 0.01463 0.04512 H10C 2 1.114377 0.714172 0.906793 11.00000 -1.50000 AFIX 0 O11 4 1.175549 0.742928 0.818396 11.00000 0.11145 0.07423 = 0.04216 0.01508 0.02291 0.06671 AFIX 6 O1W 4 1.396987 1.297546 0.886277 11.00000 0.08872 0.11432 = 0.18505 0.06852 0.05051 0.03205 H1WA 2 1.361668 1.246634 0.909941 11.00000 -1.50000 H1WB 2 1.452951 1.298424 0.882372 11.00000 -1.50000 AFIX 0 O2W 4 1.056054 1.248166 1.058303 11.00000 0.02560 0.02591 = 0.02709 0.00587 0.00073 0.01226 AFIX 3 H2WA 2 1.004433 1.255752 1.058710 11.00000 -1.50000 H2WB 2 1.069242 1.214840 1.085800 11.00000 -1.50000 AFIX 0 C1 1 0.749213 0.950371 1.040337 11.00000 0.01925 0.02293 = 0.02372 -0.00381 0.00029 0.00964 AFIX 23 H1A 2 0.724057 0.938321 1.079350 11.00000 -1.20000 H1B 2 0.717783 0.976072 1.018292 11.00000 -1.20000 AFIX 0 C2 1 0.634597 0.783603 1.023526 11.00000 0.01873 0.02015 = 0.02663 0.00564 0.00481 0.00685 AFIX 13 H2 2 0.627985 0.768420 1.064944 11.00000 -1.20000 AFIX 0 C3 1 0.629994 0.703659 0.991249 11.00000 0.02666 0.01929 = 0.04374 0.00098 0.00166 0.00994 AFIX 137 H3A 2 0.680656 0.695319 1.002885 11.00000 -1.50000 H3B 2 0.633885 0.715796 0.950328 11.00000 -1.50000 H3C 2 0.572483 0.648498 0.999797 11.00000 -1.50000 AFIX 0 C4 1 0.561512 0.806518 1.007526 11.00000 0.01990 0.02475 = 0.02843 0.00251 0.00505 0.00992 AFIX 13 H4 2 0.571838 0.859743 1.031119 11.00000 -1.20000 AFIX 0 C5 1 0.560427 0.831566 0.945913 11.00000 0.02905 0.04826 = 0.03386 0.00585 0.00279 0.02541 AFIX 23 H5A 2 0.553622 0.781418 0.921223 11.00000 -1.20000 H5B 2 0.618884 0.886335 0.936472 11.00000 -1.20000 AFIX 0 C6 1 0.481843 0.850206 0.934206 11.00000 0.05027 0.07254 = 0.04476 0.00914 -0.00188 0.04540 AFIX 23 H6A 2 0.492732 0.904819 0.955648 11.00000 -1.20000 H6B 2 0.481102 0.863053 0.893233 11.00000 -1.20000 AFIX 0 C7 1 0.391122 0.772084 0.950703 11.00000 0.03530 0.07297 = 0.07019 -0.01360 -0.01252 0.03372 AFIX 23 H7A 2 0.376705 0.718769 0.926676 11.00000 -1.20000 H7B 2 0.343491 0.788442 0.944643 11.00000 -1.20000 AFIX 0 C8 1 0.392888 0.748513 1.013389 11.00000 0.02035 0.05364 = 0.07701 0.01200 0.01307 0.01497 AFIX 23 H8A 2 0.402782 0.800377 1.037492 11.00000 -1.20000 H8B 2 0.333716 0.695519 1.023910 11.00000 -1.20000 AFIX 0 C9 1 0.468441 0.726746 1.023930 11.00000 0.02204 0.03184 = 0.05874 0.01045 0.00656 0.00916 AFIX 23 H9A 2 0.456385 0.672649 1.001455 11.00000 -1.20000 H9B 2 0.468915 0.712227 1.064630 11.00000 -1.20000 AFIX 0 C10 1 1.177215 1.246716 0.929079 11.00000 0.01610 0.01881 = 0.02064 0.00566 0.00119 0.00790 AFIX 23 H10A 2 1.225642 1.297903 0.950762 11.00000 -1.20000 H10B 2 1.194022 1.256307 0.888350 11.00000 -1.20000 AFIX 0 C11 1 1.093578 1.332955 0.919145 11.00000 0.02559 0.01623 = 0.02092 0.00256 0.00134 0.01041 AFIX 13 H11 2 1.125899 1.351712 0.881821 11.00000 -1.20000 AFIX 0 C12 1 1.147549 1.406734 0.961493 11.00000 0.03512 0.01977 = 0.03327 -0.00394 -0.00384 0.01367 AFIX 137 H12A 2 1.117294 1.389866 0.998563 11.00000 -1.50000 H12B 2 1.151963 1.463599 0.948649 11.00000 -1.50000 H12C 2 1.208580 1.414841 0.964878 11.00000 -1.50000 AFIX 0 C13 1 0.996227 1.314641 0.910049 11.00000 0.02885 0.02126 = 0.02249 -0.00127 -0.00327 0.01576 AFIX 13 H13 2 0.966505 1.263502 0.882269 11.00000 -1.20000 AFIX 0 C14 1 0.998240 1.396787 0.882703 11.00000 0.03882 0.02605 = 0.04311 0.01041 0.00291 0.02008 AFIX 23 H14A 2 1.028833 1.449376 0.908704 11.00000 -1.20000 H14B 2 1.034025 1.412194 0.847137 11.00000 -1.20000 AFIX 0 C15 1 0.904078 1.379781 0.869427 11.00000 0.04719 0.03080 = 0.06317 0.01096 -0.00627 0.02698 AFIX 23 H15A 2 0.908459 1.436315 0.854642 11.00000 -1.20000 H15B 2 0.876692 1.332962 0.839387 11.00000 -1.20000 AFIX 0 C16 1 0.843665 1.348883 0.920840 11.00000 0.03568 0.03568 = 0.06624 -0.00203 -0.00852 0.02520 AFIX 23 H16A 2 0.781334 1.332744 0.909500 11.00000 -1.20000 H16B 2 0.865774 1.399268 0.948584 11.00000 -1.20000 AFIX 0 C17 1 0.841585 1.266810 0.948951 11.00000 0.03004 0.03391 = 0.04121 0.00095 -0.00126 0.01878 AFIX 23 H17A 2 0.805000 1.251235 0.984187 11.00000 -1.20000 H17B 2 0.812128 1.214059 0.922987 11.00000 -1.20000 AFIX 0 C18 1 0.937129 1.285783 0.963340 11.00000 0.02776 0.03188 = 0.02549 -0.00232 -0.00137 0.01732 AFIX 23 H18A 2 0.964579 1.334495 0.992233 11.00000 -1.20000 H18B 2 0.933851 1.230478 0.979470 11.00000 -1.20000 AFIX 0 C19 1 1.221097 0.917893 0.909012 11.00000 0.02555 0.02758 = 0.04311 0.01021 0.01029 0.01840 AFIX 23 H19A 2 1.246618 0.916785 0.946620 11.00000 -1.20000 H19B 2 1.231359 0.877587 0.883525 11.00000 -1.20000 AFIX 0 C20 1 1.372020 1.043292 0.873895 11.00000 0.02386 0.02704 = 0.02804 0.00515 0.00158 0.00765 AFIX 13 H20 2 1.398193 1.102760 0.853579 11.00000 -1.20000 AFIX 0 C21 1 1.377414 0.975545 0.834264 11.00000 0.03473 0.04271 = 0.05601 0.00914 0.00841 0.02366 AFIX 137 H21A 2 1.329818 0.955796 0.805319 11.00000 -1.50000 H21B 2 1.368918 0.922872 0.856179 11.00000 -1.50000 H21C 2 1.436982 1.004307 0.815753 11.00000 -1.50000 AFIX 0 C22 1 1.430179 1.057144 0.927608 11.00000 0.02814 0.05303 = 0.04659 -0.00219 -0.00573 0.01079 AFIX 13 H22 2 1.405565 0.997375 0.947376 11.00000 -1.20000 AFIX 0 C23 1 1.528006 1.089316 0.910688 11.00000 0.02558 0.08060 = 0.09447 -0.02012 -0.00482 0.01100 AFIX 23 H23A 2 1.552494 1.147332 0.889719 11.00000 -1.20000 H23B 2 1.529430 1.044116 0.884855 11.00000 -1.20000 AFIX 0 C24 1 1.589548 1.103149 0.963195 11.00000 0.04099 0.09332 = 0.12289 -0.03634 -0.02742 0.03198 AFIX 23 H24A 2 1.570178 1.044155 0.981952 11.00000 -1.20000 H24B 2 1.653451 1.129020 0.950967 11.00000 -1.20000 AFIX 0 C25 1 1.581445 1.165634 1.003193 11.00000 0.05312 0.09638 = 0.12432 -0.06596 -0.03512 0.04165 AFIX 23 H25A 2 1.621109 1.175513 1.036383 11.00000 -1.20000 H25B 2 1.603384 1.224963 0.984253 11.00000 -1.20000 AFIX 0 C26 1 1.487910 1.132031 1.023366 11.00000 0.07029 0.13017 = 0.09149 -0.05268 -0.03872 0.06403 AFIX 23 H26A 2 1.485628 1.175991 1.049912 11.00000 -1.20000 H26B 2 1.464550 1.073108 1.043096 11.00000 -1.20000 AFIX 0 C27 1 1.428441 1.120504 0.966498 11.00000 0.05155 0.11082 = 0.07824 -0.01909 -0.01308 0.05926 AFIX 23 H27A 2 1.364849 1.099678 0.977523 11.00000 -1.20000 H27B 2 1.452832 1.180163 0.947549 11.00000 -1.20000 AFIX 0 C28 1 1.170494 0.687259 0.851585 11.00000 0.03956 0.03408 = 0.04276 -0.00121 0.00033 0.01756 C29 1 1.209930 0.626686 0.841088 11.00000 0.06383 0.05433 = 0.06284 0.00079 0.01126 0.03935 AFIX 137 H29A 2 1.267541 0.660682 0.820618 11.00000 -1.50000 H29B 2 1.167416 0.574318 0.818288 11.00000 -1.50000 H29C 2 1.220512 0.605615 0.877522 11.00000 -1.50000 AFIX 0 N1 3 0.729837 0.863193 1.013984 11.00000 0.01607 0.01968 = 0.01829 -0.00157 -0.00078 0.00784 AFIX 23 H1C 2 0.770372 0.847908 1.027785 11.00000 -1.20000 H1D 2 0.739406 0.871987 0.975886 11.00000 -1.20000 AFIX 0 N2 3 1.089756 1.245447 0.937283 11.00000 0.02356 0.01353 = 0.01684 0.00124 -0.00003 0.00947 AFIX 23 H2A 2 1.074008 1.235173 0.974640 11.00000 -1.20000 H2B 2 1.045701 1.198599 0.916972 11.00000 -1.20000 AFIX 0 N3 3 1.272807 1.011226 0.886454 11.00000 0.02620 0.02354 = 0.01895 -0.00072 -0.00246 0.01454 AFIX 23 H3D 2 1.269946 1.049812 0.912052 11.00000 -1.20000 H3E 2 1.245693 1.014441 0.853890 11.00000 -1.20000 AFIX 0 HKLF 4 REM 11 in P6(5) REM wR2 = 0.0597, GooF = S = 1.039, Restrained GooF = 1.042 for all data REM R1 = 0.0255 for 7514 Fo > 4sig(Fo) and 0.0295 for all 7990 data REM 452 parameters refined using 37 restraints END WGHT 0.0281 4.6732 REM Highest difference peak 0.978, deepest hole -0.442, 1-sigma level 0.076 Q1 1 1.3936 1.0217 0.9858 11.00000 0.05 0.98 Q2 1 1.4116 1.0932 0.9325 11.00000 0.05 0.64 Q3 1 1.5144 1.1348 0.9272 11.00000 0.05 0.58 Q4 1 1.5416 1.1021 1.0244 11.00000 0.05 0.49 Q5 1 1.0344 0.9367 0.9976 11.00000 0.05 0.47 ; _shelx_res_checksum 86736 _shelx_hkl_file ; -1 2 0 7238.98 172.18 -1 2 0 6737.53 170.28 1 -2 0 6823.42 170.08 1 -2 0 6649.53 171.48 1 -2 0 6960.70 171.68 -1 -1 0 6845.52 170.78 2 -1 0 6634.54 169.78 -2 1 0 6528.35 169.68 0 -2 0 4698.33 122.29 0 -2 0 4962.70 119.99 2 0 0 4879.81 121.09 0 2 0 5017.30 120.19 -2 2 0 4888.71 123.49 2 -2 0 4491.05 119.99 2 -2 0 4910.41 123.09 2 -2 0 4799.82 124.59 -2 0 0 4734.83 121.39 2 0 0 4614.04 121.29 0 2 0 4783.82 121.39 -2 2 0 4697.63 120.09 3 -2 0 9868.71 244.98 1 -3 0 9905.11 242.58 1 -3 0 9652.93 242.68 1 -3 0 9534.45 243.68 -3 2 0 9323.97 240.78 3 -2 0 9489.15 240.98 -1 3 0 9583.44 242.48 -1 3 0 9999.00 244.58 -1 3 0 9926.61 243.48 2 1 0 9419.96 242.18 2 1 0 9729.13 242.68 -3 2 0 9938.71 245.48 -2 -1 0 9139.39 242.48 -2 3 0 1174.98 35.70 2 -3 0 1210.28 36.40 -1 -2 0 1201.68 34.00 -1 -2 0 1177.18 34.20 3 -1 0 1083.59 32.60 -3 1 0 1124.69 32.70 1 2 0 1184.78 33.70 1 2 0 1168.08 34.20 1 2 0 1222.58 30.30 -2 3 0 1164.48 32.20 2 -3 0 1146.59 34.90 -2 3 0 1201.38 37.00 2 -3 0 1188.58 32.30 0 3 0 2417.16 66.79 -3 3 0 2374.06 62.59 -3 0 0 2313.97 64.49 3 0 0 2289.07 64.29 3 0 0 2379.06 63.89 3 -3 0 2453.85 62.79 3 -3 0 2413.56 66.69 3 -3 0 2398.26 68.99 0 3 0 2399.46 66.29 -3 3 0 2606.64 68.09 0 3 0 2469.65 62.79 0 3 0 2396.66 64.49 0 -3 0 2447.06 62.39 4 -3 0 983.40 36.70 -1 4 0 1071.89 34.30 1 -4 0 1066.39 33.50 -4 3 0 963.30 29.30 -3 -1 0 977.60 31.10 3 1 0 1038.70 31.80 3 1 0 1011.40 31.10 -4 3 0 1096.19 35.70 -1 4 0 1074.39 32.60 4 -3 0 1022.50 34.30 -1 4 0 1068.29 32.50 1 -4 0 1049.79 31.20 -3 -1 0 1022.90 31.90 4 -3 0 992.10 29.60 2 -4 0 1160.68 36.20 -2 4 0 1165.28 33.10 4 -2 0 1117.59 32.60 4 -2 0 1139.09 37.90 -2 -2 0 1124.79 34.50 2 2 0 1093.79 33.90 2 -4 0 1123.19 35.60 -2 -2 0 1128.19 34.30 2 2 0 1096.79 34.10 -2 4 0 1160.48 36.80 -2 4 0 1202.68 37.60 2 -4 0 1138.39 33.30 -4 2 0 1098.69 32.50 1 3 0 7914.01 198.88 3 -4 0 7758.72 202.68 -4 1 0 7554.94 197.78 1 3 0 7764.12 199.98 -3 4 0 8042.60 202.28 1 3 0 7912.01 194.28 -3 4 0 7728.53 196.38 -1 -3 0 7672.13 199.08 3 -4 0 7956.20 200.88 3 -4 0 8160.48 196.68 4 -1 0 7672.73 197.88 -1 -3 0 7546.65 199.48 0 -4 0 695.13 20.80 4 -4 0 694.93 25.60 4 0 0 681.63 22.40 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50.09 13.20 12 -9 0 56.49 17.10 9 3 0 37.60 10.60 -3 12 0 42.40 11.20 3 -12 0 44.50 11.80 12 -8 0 373.66 32.70 -4 12 0 403.86 23.90 -12 8 0 382.76 19.50 -8 -4 0 410.46 26.30 8 4 0 403.36 20.80 12 -8 0 425.26 27.60 4 -12 0 408.96 23.10 4 -12 0 418.66 26.10 7 5 0 742.83 26.40 -7 -5 0 725.23 35.10 12 -7 0 757.32 38.80 -12 7 0 767.52 30.30 5 -12 0 732.43 34.10 -7 -5 0 762.22 36.60 5 -12 0 786.52 36.90 12 -7 0 764.82 44.10 12 -6 0 366.66 27.70 6 -12 0 331.77 23.90 6 -12 0 343.97 23.50 -6 -6 0 316.57 23.40 -6 -6 0 337.97 22.40 -12 6 0 325.97 19.20 -6 12 0 335.07 19.50 12 -6 0 321.77 30.00 7 -12 0 -6.00 6.40 12 -5 0 -2.50 10.30 -12 5 0 -4.00 6.10 -5 -7 0 -11.70 6.80 7 -12 0 -3.20 6.70 7 -12 0 -6.80 8.10 12 -5 0 35.70 13.90 -7 12 0 1.40 5.90 -5 -7 0 10.70 7.90 8 -12 0 76.99 11.00 -12 4 0 88.89 12.90 12 -4 0 107.99 20.30 8 -12 0 75.29 13.60 8 -12 0 113.29 18.40 -4 -8 0 65.59 12.80 -8 12 0 97.29 11.50 -12 3 0 8.70 7.40 9 -12 0 19.90 11.40 9 -12 0 5.60 8.80 12 -3 0 6.50 12.30 9 -12 0 16.60 6.50 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-10 0 352.06 25.40 13 -10 0 416.86 35.50 10 3 0 361.26 22.50 3 -13 0 359.96 25.80 4 -13 0 393.66 26.60 -9 -4 0 411.06 27.70 13 -9 0 389.86 35.10 -4 13 0 371.16 24.60 -13 9 0 418.56 21.00 4 -13 0 385.76 23.20 9 4 0 381.26 21.00 -8 -5 0 350.16 25.70 -5 13 0 363.46 22.90 8 5 0 345.57 17.10 13 -8 0 365.06 33.40 5 -13 0 314.17 22.80 -13 8 0 319.17 19.40 13 -8 0 369.36 30.20 5 -13 0 379.56 26.50 6 -13 0 143.29 19.10 -6 13 0 115.79 14.20 -7 -6 0 123.79 17.90 13 -7 0 113.09 22.20 -13 7 0 132.19 14.80 6 -13 0 117.49 16.60 -7 -6 0 115.09 18.10 13 -7 0 124.99 20.00 13 -6 0 13.60 14.40 -13 6 0 18.90 8.30 -7 13 0 6.80 6.20 7 -13 0 12.30 8.50 -6 -7 0 11.90 9.30 -6 -7 0 16.70 9.90 7 -13 0 20.00 12.30 8 -13 0 187.18 16.00 8 -13 0 205.78 19.80 -8 13 0 182.68 14.50 -13 5 0 199.38 17.20 8 -13 0 193.08 23.20 13 -5 0 171.38 25.30 -5 -8 0 195.78 20.20 13 -5 0 155.98 24.90 9 -13 0 9.50 12.60 -13 4 0 27.00 10.10 4 9 0 12.40 12.80 -4 -9 0 11.00 10.10 9 -13 0 1.30 8.40 -9 13 0 15.40 6.10 13 -4 0 26.70 14.80 3 10 0 595.24 38.00 13 -3 0 564.64 37.10 10 -13 0 537.55 31.90 -10 13 0 574.04 24.80 10 -13 0 536.15 36.80 -13 3 0 614.94 31.40 -3 -10 0 590.84 33.80 10 -13 0 554.74 25.00 2 11 0 239.68 28.70 11 -13 0 251.97 16.30 11 -13 0 274.17 23.40 -11 13 0 267.27 16.20 11 -13 0 253.57 29.70 13 -2 0 270.87 27.90 -2 -11 0 264.57 24.20 -13 2 0 283.17 22.40 1 12 0 99.19 19.90 -1 -12 0 75.79 16.90 -13 1 0 64.89 14.60 -12 13 0 67.39 9.30 12 -13 0 77.19 20.00 13 -1 0 79.69 17.80 12 -13 0 95.49 16.90 12 -13 0 100.69 11.90 0 13 0 3.00 11.80 13 -13 0 12.00 15.30 13 -13 0 14.30 7.20 13 -13 0 7.20 10.60 13 0 0 23.30 13.60 -13 13 0 24.20 7.50 -13 0 0 12.00 11.20 0 -13 0 28.30 13.80 -13 -1 0 97.19 17.90 14 -13 0 119.79 19.10 -14 13 0 98.29 11.60 -1 14 0 63.89 17.30 1 -14 0 73.49 15.80 14 -13 0 113.29 24.80 13 1 0 68.49 16.00 2 -14 0 138.69 21.00 2 -14 0 144.79 13.80 12 2 0 179.18 19.90 -12 -2 0 149.09 21.20 -2 14 0 152.28 21.00 14 -12 0 133.49 19.40 14 -12 0 134.69 26.00 -14 12 0 169.98 21.10 11 3 0 7.60 9.70 3 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12.00 9 -14 0 53.49 14.40 10 -14 0 -10.90 11.80 14 -4 0 -4.20 13.60 -10 14 0 8.10 7.20 -4 -10 0 5.00 8.60 4 10 0 10.40 14.00 -14 4 0 6.10 9.10 10 -14 0 12.10 9.10 10 -14 0 -0.20 7.70 -3 -11 0 191.78 24.00 14 -3 0 198.18 27.10 -14 3 0 190.88 19.70 3 11 0 159.68 24.30 11 -14 0 208.08 21.30 11 -14 0 194.18 26.80 -11 14 0 183.78 14.30 11 -14 0 205.18 15.70 12 -14 0 151.18 13.90 2 12 0 149.19 24.00 12 -14 0 168.28 21.60 -2 -12 0 164.88 22.00 12 -14 0 106.89 22.90 -14 2 0 132.89 19.80 14 -2 0 205.78 26.20 -12 14 0 152.68 13.00 -14 1 0 -1.80 10.70 1 13 0 1.50 12.30 13 -14 0 0.30 6.10 14 -1 0 15.20 14.50 -13 14 0 24.30 7.00 13 -14 0 -9.30 14.90 13 -14 0 -1.30 10.00 -1 -13 0 13.10 11.90 -14 0 0 88.59 17.80 14 -14 0 125.79 18.80 14 -14 0 136.29 25.20 14 0 0 78.59 18.40 -14 14 0 102.49 11.60 0 -14 0 109.49 20.20 0 14 0 89.29 19.80 15 -14 0 138.89 27.60 -14 -1 0 136.09 21.20 14 1 0 164.68 21.20 15 -14 0 122.29 20.00 1 -15 0 127.79 20.70 -1 15 0 108.09 20.20 -2 15 0 49.00 15.10 -13 -2 0 58.89 21.30 15 -13 0 53.09 14.40 15 -13 0 12.10 15.10 2 -15 0 35.70 15.50 13 2 0 9.40 11.10 -15 13 0 64.99 10.70 2 -15 0 27.60 12.90 -12 -3 0 111.39 19.40 -3 15 0 95.49 17.40 3 -15 0 103.09 13.60 -15 12 0 100.69 12.50 12 3 0 132.09 20.50 3 -15 0 86.29 16.40 15 -12 0 108.99 28.20 15 -12 0 110.99 17.90 4 -15 0 13.80 8.40 -4 15 0 -0.40 10.00 15 -11 0 3.90 16.60 4 -15 0 3.80 10.80 11 4 0 13.80 8.60 -15 11 0 -0.50 6.50 -11 -4 0 15.90 11.70 15 -11 0 6.20 10.20 5 -15 0 34.70 11.40 15 -10 0 -12.60 14.80 15 -10 0 -1.10 10.90 -10 -5 0 14.50 10.70 -5 15 0 3.80 7.30 5 -15 0 17.80 12.60 -15 10 0 11.40 7.20 10 5 0 10.00 7.00 15 -9 0 10.70 12.40 6 -15 0 8.70 10.20 -9 -6 0 22.00 12.40 -6 15 0 10.10 8.50 15 -9 0 19.70 16.30 -15 9 0 15.70 7.60 6 -15 0 22.60 9.90 15 -8 0 45.80 14.40 -8 -7 0 -2.30 9.70 15 -8 0 -5.70 16.00 -15 8 0 14.50 8.70 7 -15 0 7.60 11.50 -7 15 0 27.80 9.20 7 -15 0 5.20 10.70 15 -7 0 29.20 15.00 -8 15 0 15.40 8.30 -7 -8 0 22.00 10.10 8 -15 0 28.30 12.20 15 -7 0 2.00 12.50 -15 7 0 25.80 10.00 8 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23.70 0 15 0 157.18 24.90 15 -15 0 129.29 20.50 -16 15 0 100.49 12.40 -15 -1 0 79.49 19.00 16 -15 0 65.39 21.50 15 1 0 79.89 16.60 -1 16 0 91.99 20.10 16 -15 0 71.49 15.70 1 -16 0 91.79 19.70 -2 16 0 183.08 24.40 2 -16 0 133.39 22.90 16 -14 0 74.69 23.90 -14 -2 0 118.09 21.70 -16 14 0 143.79 14.80 16 -14 0 109.19 18.50 14 2 0 131.99 17.80 -16 13 0 127.09 13.80 16 -13 0 91.69 17.30 16 -13 0 99.19 24.70 -13 -3 0 103.89 20.00 -3 16 0 124.59 19.60 3 -16 0 83.29 17.70 13 3 0 95.19 14.80 3 -16 0 107.19 13.40 16 -12 0 251.07 35.10 12 4 0 291.17 19.00 -12 -4 0 276.07 30.60 4 -16 0 313.67 27.80 16 -12 0 258.97 24.10 4 -16 0 237.58 19.80 -16 12 0 256.37 18.20 -4 16 0 270.87 23.80 -11 -5 0 202.38 26.00 16 -11 0 192.18 23.70 5 -16 0 200.98 19.20 11 5 0 199.28 14.40 16 -11 0 199.08 31.70 -5 16 0 210.08 20.90 -16 11 0 192.18 16.30 5 -16 0 174.38 26.70 16 -10 0 103.19 26.30 16 -10 0 110.19 20.30 -10 -6 0 101.59 19.70 -6 16 0 144.49 18.70 -16 10 0 132.69 15.90 6 -16 0 133.89 19.90 6 -16 0 123.19 17.80 16 -9 0 78.19 18.80 16 -9 0 78.39 23.20 -9 -7 0 103.39 20.00 7 -16 0 105.49 17.60 -16 9 0 77.59 13.60 7 -16 0 59.59 14.50 -7 16 0 108.79 15.60 16 -8 0 156.18 24.60 -16 8 0 160.78 18.40 8 -16 0 184.98 20.30 -8 16 0 161.08 16.00 -8 -8 0 162.18 22.10 16 -8 0 173.88 26.90 8 -16 0 147.89 21.50 16 -7 0 157.28 27.30 9 -16 0 199.88 25.30 7 9 0 149.79 34.80 -9 16 0 179.48 15.90 -16 7 0 184.48 19.00 16 -7 0 169.08 25.20 -7 -9 0 156.08 22.30 9 -16 0 180.28 23.00 16 -6 0 89.19 23.70 10 -16 0 92.69 17.20 -16 6 0 75.79 14.80 10 -16 0 61.89 18.60 6 10 0 60.89 34.50 -10 16 0 69.59 11.80 -6 -10 0 50.79 23.30 16 -6 0 87.09 23.00 -16 5 0 46.60 12.90 5 11 0 19.50 25.20 -5 -11 0 20.40 11.90 16 -5 0 60.19 20.30 11 -16 0 11.90 14.40 16 -5 0 27.20 17.40 11 -16 0 14.50 11.40 12 -16 0 2.30 14.90 -12 16 0 1.90 6.50 -4 -12 0 8.60 10.10 12 -16 0 13.40 11.80 16 -4 0 22.20 15.50 4 12 0 3.20 16.10 -16 4 0 -15.90 9.50 -3 -13 0 34.40 14.00 13 -16 0 44.40 14.90 3 13 0 54.99 19.10 13 -16 0 94.59 20.90 -13 16 0 54.79 10.10 16 -3 0 45.40 18.10 -14 16 0 320.37 18.40 -16 2 0 391.06 31.10 14 -16 0 310.77 36.60 -2 -14 0 337.67 29.20 2 14 0 367.86 34.70 14 -16 0 339.87 27.70 16 -2 0 371.96 32.20 15 -16 0 202.88 30.20 1 15 0 205.68 27.50 -16 1 0 183.58 25.00 -15 16 0 251.27 19.00 -1 -15 0 192.68 26.70 15 -16 0 201.48 24.70 -16 0 0 60.49 18.00 16 -16 0 99.29 24.40 16 -16 0 78.99 17.50 0 16 0 44.40 17.70 0 -16 0 80.59 18.90 16 0 0 53.89 18.10 17 -16 0 63.89 23.70 -16 -1 0 43.70 17.70 1 -17 0 56.99 18.00 16 1 0 62.89 15.80 17 -16 0 73.39 17.10 -17 16 0 58.09 10.80 -1 17 0 64.79 18.10 -15 -2 0 25.50 15.50 -17 15 0 29.10 8.10 2 -17 0 8.80 11.20 -2 17 0 28.90 14.90 17 -15 0 30.20 18.80 17 -15 0 24.00 12.00 15 2 0 29.10 12.80 3 -17 0 69.49 11.70 17 -14 0 84.29 17.80 -14 -3 0 90.19 20.90 -3 17 0 68.79 16.20 -17 14 0 83.39 12.00 3 -17 0 51.59 17.50 14 3 0 49.40 12.70 17 -14 0 31.80 20.50 -4 17 0 225.38 26.30 17 -13 0 219.38 24.70 -13 -4 0 246.28 29.40 -17 13 0 238.48 17.40 13 4 0 212.78 17.80 4 -17 0 211.58 18.70 4 -17 0 205.68 26.80 17 -13 0 204.58 31.50 5 -17 0 236.38 20.80 17 -12 0 228.28 32.40 -17 12 0 245.78 18.40 -12 -5 0 264.07 30.80 12 5 0 255.97 15.60 -5 17 0 229.88 22.30 17 -12 0 214.18 23.70 5 -17 0 187.58 24.10 17 -11 0 179.28 23.90 6 -17 0 195.68 24.70 17 -11 0 208.68 31.60 -11 -6 0 206.98 28.20 6 -17 0 199.68 21.00 -17 11 0 221.28 18.20 -6 17 0 218.88 24.20 -17 10 0 55.29 11.70 17 -10 0 50.29 22.00 17 -10 0 52.99 16.00 7 -17 0 38.80 15.70 -10 -7 0 50.49 17.70 7 -17 0 39.10 13.60 -7 17 0 80.99 14.90 17 -9 0 147.49 23.80 8 -17 0 126.19 20.40 -17 9 0 142.69 17.20 17 -9 0 119.49 25.90 8 -17 0 112.59 19.30 -8 17 0 119.59 16.00 17 -8 0 232.98 34.20 9 -17 0 173.48 24.20 -8 -9 0 179.78 25.00 9 -17 0 211.28 24.80 17 -8 0 230.48 29.90 -17 8 0 231.28 20.90 -9 17 0 200.08 18.10 8 9 0 202.48 32.50 7 10 0 373.06 37.20 10 -17 0 356.96 31.50 -7 -10 0 345.47 30.50 -10 17 0 379.16 22.00 17 -7 0 363.56 34.30 -17 7 0 352.46 25.50 10 -17 0 326.27 27.70 -17 6 0 398.86 28.20 -6 -11 0 413.26 32.70 6 11 0 410.56 38.00 17 -6 0 381.56 36.60 -11 17 0 387.66 22.60 11 -17 0 387.86 34.90 11 -17 0 400.06 29.70 17 -6 0 407.96 38.30 17 -5 0 249.38 32.20 17 -5 0 230.58 34.90 -5 -12 0 243.98 29.40 12 -17 0 295.57 34.40 -12 17 0 252.07 18.20 -17 5 0 262.87 24.00 12 -17 0 293.17 27.10 5 12 0 276.57 34.60 17 -4 0 131.09 30.40 -17 4 0 109.89 21.00 13 -17 0 176.68 28.50 -4 -13 0 103.59 20.80 17 -4 0 113.49 24.20 4 13 0 144.39 26.80 13 -17 0 150.28 21.90 17 -3 0 210.38 28.40 3 14 0 190.68 29.90 -17 3 0 180.88 24.30 14 -17 0 195.78 23.60 -3 -14 0 192.38 25.90 -14 17 0 200.28 18.40 14 -17 0 180.68 29.30 17 -2 0 204.78 29.00 -2 -15 0 215.88 28.10 -17 2 0 213.58 26.90 2 15 0 226.28 30.90 15 -17 0 242.98 34.80 -15 17 0 243.58 19.80 15 -17 0 214.28 25.60 1 16 0 76.29 19.80 -1 -16 0 37.60 15.20 16 -17 0 40.30 18.80 -17 1 0 25.50 15.00 17 -1 0 55.29 17.80 16 -17 0 45.50 15.00 0 -17 0 160.48 25.30 -17 0 0 102.29 21.80 17 -17 0 136.39 20.50 -17 17 0 155.18 20.70 17 0 0 151.18 23.30 0 17 0 137.19 24.20 17 -17 0 151.08 29.00 18 -17 0 83.29 17.80 17 1 0 81.49 18.60 -1 18 0 69.39 19.50 1 -18 0 47.40 16.50 -17 -1 0 70.49 19.00 -18 17 0 93.59 12.20 18 -17 0 175.48 31.30 16 2 0 -31.90 9.00 -18 16 0 -2.90 6.90 -2 18 0 5.10 12.40 18 -16 0 -14.00 11.10 -16 -2 0 2.50 12.70 18 -16 0 -5.30 18.00 2 -18 0 1.80 13.30 -15 -3 0 2.00 13.70 18 -15 0 -26.30 12.90 3 -18 0 0.90 9.50 15 3 0 -7.80 9.10 -18 15 0 5.60 7.70 18 -15 0 0.70 11.60 -14 -4 0 56.39 17.80 18 -14 0 46.10 20.80 -4 18 0 84.39 18.00 4 -18 0 69.49 13.50 -18 14 0 52.99 11.30 18 -14 0 60.89 16.40 4 -18 0 96.29 19.20 -18 13 0 231.28 18.60 -5 18 0 266.67 25.40 13 5 0 274.97 16.60 -13 -5 0 236.78 30.70 5 -18 0 282.57 22.50 18 -13 0 207.68 24.60 18 -13 0 252.77 35.50 5 -18 0 249.08 27.50 6 -18 0 361.86 26.00 -6 18 0 356.76 27.30 -18 12 0 307.97 21.50 6 -18 0 346.27 30.60 18 -12 0 280.17 26.40 -12 -6 0 311.47 30.80 18 -12 0 300.97 39.00 7 -18 0 162.38 23.90 18 -11 0 166.08 29.80 -7 18 0 169.98 20.50 18 -11 0 158.28 22.50 7 -18 0 182.08 22.40 -11 -7 0 183.78 25.60 -18 11 0 171.38 19.20 18 -10 0 102.69 20.30 18 -10 0 131.69 28.60 -8 18 0 93.19 16.30 8 -18 0 60.19 16.80 -18 10 0 84.19 15.20 8 -18 0 102.59 19.00 -9 18 0 29.50 9.70 9 -18 0 14.50 11.80 -18 9 0 28.90 12.00 9 -18 0 23.30 13.60 18 -9 0 21.40 18.40 18 -9 0 22.00 15.30 9 9 0 17.80 16.60 -18 8 0 92.29 15.70 10 -18 0 74.79 19.60 10 -18 0 90.19 20.00 -8 -10 0 86.59 17.80 18 -8 0 60.29 19.50 18 -8 0 83.79 23.70 -10 18 0 102.29 15.00 8 10 0 52.29 21.10 11 -18 0 204.58 28.50 11 -18 0 244.68 30.30 -7 -11 0 161.68 23.90 -11 18 0 217.88 17.60 7 11 0 274.17 36.70 18 -7 0 211.08 31.90 -18 7 0 223.38 22.20 18 -7 0 247.18 34.10 18 -6 0 239.58 34.30 -6 -12 0 143.79 22.40 18 -6 0 203.08 30.90 12 -18 0 222.48 26.40 -18 6 0 219.08 24.60 -12 18 0 219.38 17.40 12 -18 0 179.68 27.90 6 12 0 262.07 35.60 -18 5 0 297.37 26.20 18 -5 0 267.37 37.20 13 -18 0 196.28 30.00 13 -18 0 274.37 25.70 -5 -13 0 146.59 23.90 18 -5 0 228.38 31.30 5 13 0 265.97 36.10 18 -4 0 150.68 32.10 14 -18 0 117.79 20.40 -4 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17 -19 0 40.90 15.50 -2 -17 0 49.50 16.40 19 -2 0 59.29 20.20 -1 -18 0 116.39 22.60 1 18 0 188.88 29.70 19 -1 0 198.58 27.40 18 -19 0 189.68 25.00 -19 1 0 146.29 26.70 -18 19 0 152.08 15.50 18 -19 0 244.98 37.70 0 -19 0 118.99 23.20 -19 0 0 93.99 22.30 19 0 0 100.79 22.60 19 -19 0 157.28 31.90 0 19 0 132.79 25.20 19 -19 0 98.59 20.00 20 -18 0 138.99 21.50 -20 18 0 130.99 15.90 -2 20 0 155.88 25.80 18 2 0 135.89 20.00 20 -18 0 114.79 30.00 2 -20 0 109.09 23.90 -18 -2 0 89.89 24.20 20 -17 0 27.10 19.90 20 -17 0 13.90 13.80 -17 -3 0 -7.70 14.70 17 3 0 8.00 11.20 -20 17 0 4.50 9.30 3 -20 0 17.10 15.50 -3 20 0 19.90 14.30 -16 -4 0 1.90 15.00 16 4 0 0.70 9.00 -20 16 0 -13.50 8.70 4 -20 0 2.50 12.00 20 -16 0 -21.50 12.80 -4 20 0 11.30 13.10 20 -16 0 -7.90 16.60 -15 -5 0 9.50 14.70 20 -15 0 -19.60 12.10 5 -20 0 4.10 11.00 -5 20 0 -1.90 12.50 20 -15 0 7.00 18.90 5 -20 0 22.00 13.80 -14 -6 0 171.48 29.50 -20 14 0 164.48 18.70 6 -20 0 204.58 22.40 6 -20 0 178.48 26.70 20 -14 0 240.08 37.40 20 -14 0 187.28 23.60 -6 20 0 151.08 22.50 20 -13 0 340.47 43.00 7 -20 0 407.66 29.70 7 -20 0 441.76 35.10 -7 20 0 378.76 28.90 -20 13 0 398.36 26.50 20 -13 0 411.56 32.10 12 8 0 350.76 45.00 20 -12 0 360.26 31.00 8 -20 0 422.46 34.50 20 -12 0 353.76 44.50 8 -20 0 377.86 29.20 -8 20 0 367.66 27.40 -20 12 0 369.36 25.90 9 -20 0 145.59 25.80 20 -11 0 129.79 21.50 9 -20 0 136.99 23.60 -9 20 0 196.28 22.00 -20 11 0 193.38 22.40 20 -11 0 151.68 30.90 11 9 0 99.49 28.70 10 -20 0 34.80 15.90 -10 20 0 30.60 11.70 20 -10 0 19.50 16.30 10 -20 0 16.10 14.30 10 10 0 39.10 22.10 -20 10 0 31.60 13.10 20 -10 0 21.00 18.80 -20 9 0 29.10 13.90 11 -20 0 27.50 14.20 -11 20 0 22.50 11.00 20 -9 0 -8.20 14.90 9 11 0 41.30 21.70 20 -9 0 19.10 19.90 11 -20 0 18.30 15.70 12 -20 0 64.59 18.30 20 -8 0 45.80 21.90 -20 8 0 57.19 16.70 8 12 0 15.50 17.60 12 -20 0 57.29 18.40 20 -8 0 62.19 24.00 -12 20 0 44.00 12.50 -20 7 0 191.08 25.40 13 -20 0 236.08 32.40 -13 20 0 205.08 18.20 20 -7 0 105.09 26.80 13 -20 0 204.98 26.40 7 13 0 258.27 36.90 20 -7 0 255.67 34.20 -7 -13 0 225.48 30.40 6 14 0 135.09 26.80 -14 20 0 175.78 17.40 -20 6 0 140.19 23.50 -6 -14 0 139.89 24.30 14 -20 0 150.98 28.40 20 -6 0 160.98 28.70 14 -20 0 148.99 23.20 20 -6 0 111.09 29.30 -5 -15 0 59.89 20.60 5 15 0 38.90 21.50 -20 5 0 58.69 16.70 20 -5 0 36.80 26.20 -15 20 0 65.39 17.80 15 -20 0 69.39 17.00 15 -20 0 80.79 23.00 20 -5 0 74.29 21.20 20 -4 0 82.79 29.00 -4 -16 0 38.10 15.80 4 16 0 82.29 24.00 -16 20 0 110.09 15.80 16 -20 0 71.69 17.60 -20 4 0 64.89 19.30 16 -20 0 76.49 22.50 20 -4 0 95.79 22.80 17 -20 0 30.70 14.50 -17 20 0 17.60 8.90 17 -20 0 14.60 20.60 3 17 0 25.50 18.10 20 -3 0 0.80 16.40 -3 -17 0 39.10 15.90 20 -3 0 14.00 27.80 -20 3 0 35.80 15.00 2 18 0 84.49 23.50 18 -20 0 88.49 25.10 18 -20 0 100.39 20.80 20 -2 0 115.79 24.10 -20 2 0 69.79 21.00 -2 -18 0 52.69 20.00 21 -16 0 43.20 23.10 -5 21 0 37.10 15.80 5 -21 0 14.40 13.40 -21 16 0 8.30 11.10 21 -16 0 -2.20 14.30 21 -15 0 324.67 43.40 21 -15 0 305.37 28.50 6 -21 0 278.47 25.10 6 -21 0 309.07 31.60 -6 21 0 275.37 27.40 -21 15 0 266.47 22.80 21 -14 0 601.74 51.59 7 -21 0 602.44 42.60 -7 21 0 510.65 40.60 7 -21 0 543.15 34.60 14 7 0 545.35 52.99 21 -14 0 568.44 37.30 -21 14 0 507.65 30.60 -21 13 0 351.96 25.50 21 -13 0 381.26 45.30 21 -13 0 318.77 30.20 13 8 0 271.57 43.20 8 -21 0 407.86 34.50 -8 21 0 355.76 28.70 9 -21 0 200.08 28.50 -21 12 0 209.08 23.30 12 9 0 176.08 35.20 21 -12 0 148.19 31.10 -9 21 0 201.68 23.10 21 -12 0 175.18 24.20 9 -21 0 235.08 27.40 11 10 0 94.59 28.90 -21 11 0 125.29 19.50 -10 21 0 171.98 21.30 21 -11 0 149.39 29.40 10 -21 0 163.18 24.30 10 -21 0 112.09 21.50 21 -11 0 135.99 23.50 -21 10 0 84.99 16.60 21 -10 0 41.90 19.30 -11 21 0 128.09 17.90 10 11 0 61.49 25.70 21 -10 0 44.50 22.10 11 -21 0 43.50 16.70 -21 9 0 77.49 19.00 -12 21 0 85.39 14.60 9 12 0 57.19 25.70 12 -21 0 73.79 19.30 21 -9 0 75.39 23.20 12 -21 0 111.29 22.20 21 -9 0 54.69 23.10 13 -21 0 67.89 18.20 21 -8 0 59.99 24.00 8 13 0 93.09 24.70 -21 8 0 77.99 20.10 21 -8 0 74.19 26.30 -13 21 0 99.09 15.60 13 -21 0 93.79 22.70 7 14 0 125.39 29.50 21 -7 0 83.49 26.40 14 -21 0 99.39 20.10 14 -21 0 129.19 26.90 -14 21 0 134.99 15.70 21 -7 0 89.29 26.90 -7 -14 0 105.09 22.30 -21 7 0 109.39 21.40 21 -6 0 94.59 24.10 21 -6 0 9.40 25.70 15 -21 0 53.79 17.00 6 15 0 86.09 25.90 15 -21 0 69.29 22.10 -6 -15 0 81.19 21.10 -21 6 0 86.39 19.40 -21 5 0 70.99 19.30 5 16 0 48.70 21.20 16 -21 0 63.19 18.80 16 -21 0 68.39 24.60 -5 -16 0 71.69 19.60 21 -5 0 131.19 27.40 21 -5 0 24.80 27.80 -22 12 0 153.08 26.90 12 10 0 162.98 36.60 -10 22 0 219.08 24.80 22 -12 0 116.59 31.00 10 -22 0 161.98 26.70 22 -12 0 117.39 23.30 10 -22 0 105.89 22.10 -11 22 0 190.58 22.20 11 11 0 194.18 37.40 -22 11 0 216.28 25.60 11 -22 0 203.08 28.30 22 -11 0 174.68 26.60 22 -11 0 228.68 37.20 11 -22 0 224.78 28.90 22 -10 0 60.29 22.00 10 12 0 56.79 26.40 12 -22 0 78.29 19.70 -12 22 0 53.99 15.20 -22 10 0 64.69 18.20 12 -22 0 69.29 20.30 22 -10 0 59.59 23.00 2 -1 1 328.97 12.10 1 -2 1 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1 9 -2 187.68 12.70 0 10 2 530.85 29.80 -10 0 2 462.35 26.20 10 -10 2 456.95 31.40 0 -10 2 426.46 26.10 10 -10 2 464.75 22.20 10 0 2 462.65 26.30 -10 10 2 467.95 17.60 10 -10 2 465.65 24.30 -10 0 -2 542.55 28.10 0 10 -2 524.15 24.60 0 -10 -2 522.55 29.60 -10 10 -2 529.65 32.80 -10 10 -2 498.95 23.70 10 -10 -2 533.55 31.90 0 -10 -2 534.25 19.40 10 -10 -2 545.75 36.50 10 -10 -2 538.15 20.00 0 10 -2 531.95 30.80 1 -11 2 1173.18 39.10 10 1 2 1120.99 42.10 1 -11 2 1171.28 47.00 11 -10 2 1080.79 41.80 11 -10 2 1124.49 53.09 -10 -1 2 1002.60 43.60 -1 11 2 1075.89 45.80 -11 10 2 1072.79 34.20 -1 11 -2 1100.69 42.30 1 -11 -2 1092.09 36.10 -11 10 -2 1116.39 39.50 11 -10 -2 1098.59 35.40 1 -11 -2 1034.40 45.90 11 -10 -2 1053.99 54.69 -10 -1 -2 1146.69 45.50 -11 10 -2 1189.58 51.49 11 -10 -2 1099.89 49.90 -1 11 -2 1139.19 48.00 11 -9 2 691.03 30.40 -2 11 2 662.93 32.00 2 -11 2 647.94 32.60 9 2 2 673.73 28.20 -9 -2 2 695.83 33.60 -11 9 2 659.93 24.00 2 -11 2 693.63 28.60 11 -9 2 679.13 38.90 2 -11 -2 637.64 26.40 11 -9 -2 730.83 42.70 11 -9 -2 656.33 24.40 -9 -2 -2 596.34 30.60 -2 11 -2 660.13 35.80 -2 11 -2 665.33 33.30 11 -9 -2 602.84 35.50 -11 9 -2 696.43 27.70 2 -11 -2 694.23 34.70 -11 9 -2 612.74 35.60 -8 -3 2 92.39 14.10 11 -8 2 90.19 12.70 8 3 2 101.99 10.40 3 -11 2 87.49 13.80 11 -8 2 97.79 18.90 3 -11 2 89.79 12.30 -3 11 2 82.29 14.40 -11 8 2 102.49 9.40 3 -11 -2 55.39 12.10 11 -8 -2 77.29 16.10 11 -8 -2 61.09 7.80 11 -8 -2 64.19 16.90 -8 -3 -2 50.39 11.60 -11 8 -2 56.89 10.90 -8 -3 -2 45.90 9.90 -3 11 -2 65.09 12.40 3 -11 -2 54.89 10.70 -4 11 2 197.78 15.30 7 4 2 207.68 10.70 4 -11 2 247.68 19.10 -11 7 2 228.78 13.50 -7 -4 2 227.48 18.60 11 -7 2 255.07 18.50 -4 11 2 238.08 14.20 4 -11 2 206.08 17.00 11 -7 2 177.38 23.30 4 -11 -2 277.47 19.50 -4 11 -2 295.57 20.10 4 -11 -2 268.87 21.00 11 -7 -2 307.27 29.50 -7 -4 -2 261.47 19.30 11 -7 -2 266.07 14.70 -11 7 -2 277.17 16.50 -7 -4 -2 245.68 17.90 11 -6 2 468.55 32.10 5 -11 2 517.25 26.90 5 -11 2 534.75 27.30 11 -6 2 478.05 26.70 -6 -5 2 494.65 28.20 -5 11 2 546.65 23.30 -11 6 2 507.05 22.30 -5 11 2 497.05 20.90 11 -6 -2 547.75 39.10 11 -6 -2 562.54 23.90 -6 -5 -2 574.24 29.40 -11 6 -2 556.64 25.40 -6 -5 -2 588.44 28.70 5 -11 -2 619.14 31.70 5 -11 -2 574.14 29.40 -6 11 2 158.88 11.80 -6 11 2 161.18 12.60 6 -11 2 166.38 17.80 11 -5 2 177.08 21.80 11 -5 2 179.08 18.80 6 -11 2 175.28 15.90 -5 -6 2 174.58 17.50 -11 5 2 184.78 13.80 -6 11 -2 234.08 16.60 5 6 -2 232.48 11.50 6 -11 -2 246.58 21.60 -11 5 -2 217.78 15.90 6 -11 -2 219.68 19.80 -5 -6 -2 232.08 18.50 -5 -6 -2 239.78 18.60 5 6 -2 233.88 26.90 -7 11 2 247.38 13.40 -4 -7 2 213.08 18.20 7 -11 2 209.38 20.20 -11 4 2 214.98 15.80 7 -11 2 258.97 17.90 11 -4 2 249.08 23.50 11 -4 2 240.88 13.20 -7 11 -2 225.68 16.50 -11 4 -2 220.18 16.80 11 -4 -2 234.08 29.10 7 -11 -2 201.88 19.40 -4 -7 -2 212.08 17.80 4 7 -2 225.88 10.80 -4 -7 -2 192.48 17.60 7 -11 -2 230.08 22.60 4 7 -2 206.38 21.10 8 -11 2 406.46 21.10 -3 -8 2 404.36 24.80 11 -3 2 388.06 27.50 -11 3 2 405.46 22.30 8 -11 2 448.76 28.60 8 -11 2 394.66 22.80 11 -3 2 423.06 18.80 -8 11 2 425.56 17.20 8 -11 -2 336.07 24.70 3 8 -2 368.76 26.80 -3 -8 -2 330.47 22.30 -3 -8 -2 329.87 22.60 -11 3 -2 324.07 20.30 3 8 -2 364.76 15.10 8 -11 -2 402.76 29.20 -8 11 -2 349.96 19.30 8 -11 -2 321.37 16.20 9 -11 2 71.29 12.00 9 -11 2 47.10 14.30 -2 -9 2 65.39 12.70 9 -11 2 53.99 9.10 -9 11 2 69.79 7.50 11 -2 2 57.99 14.40 -11 2 2 50.79 10.50 2 9 -2 27.50 12.50 -9 11 -2 26.10 7.60 9 -11 -2 38.10 6.30 -2 -9 -2 23.10 9.80 9 -11 -2 23.00 12.20 9 -11 -2 31.80 11.20 -11 2 -2 23.80 8.10 2 9 -2 24.90 6.10 -10 11 2 379.26 15.40 -11 1 2 354.36 23.80 1 10 2 378.76 28.10 11 -1 2 349.17 24.90 -1 -10 2 338.07 23.80 10 -11 2 416.96 30.40 -1 -10 -2 398.76 26.20 -11 1 -2 387.96 23.80 10 -11 -2 444.76 29.90 1 10 -2 425.46 20.70 10 -11 -2 482.95 34.20 1 10 -2 444.06 29.60 10 -11 -2 440.96 17.80 -10 11 -2 438.16 21.80 11 -11 2 1370.26 59.39 11 0 2 1285.17 49.90 11 -11 2 1287.27 47.70 -11 0 2 1295.57 50.79 -11 11 2 1279.97 39.00 0 11 2 1247.68 53.29 0 -11 2 1362.06 53.09 0 -11 -2 1489.55 44.20 0 11 -2 1536.85 51.59 0 -11 -2 1451.55 57.69 -11 0 -2 1542.25 56.39 0 11 -2 1495.85 59.59 11 -11 -2 1536.65 45.60 11 -11 -2 1507.05 60.99 11 -11 -2 1428.46 65.79 -11 11 -2 1583.04 50.39 12 -11 2 1860.21 75.49 -1 12 2 1863.01 68.29 11 1 2 1917.41 63.99 -11 -1 2 1896.31 67.79 -12 11 2 1866.01 54.29 1 -12 2 1807.42 58.59 12 -11 2 1911.51 63.59 1 -12 2 1935.61 69.29 12 -11 -2 2049.20 75.29 -12 11 -2 2012.70 62.89 -1 12 -2 1849.91 70.99 12 -11 -2 2070.89 82.49 -11 -1 -2 1977.10 69.29 1 -12 -2 1957.10 58.09 -1 12 -2 1941.71 66.09 1 -12 -2 1944.21 71.49 12 -11 -2 1925.51 57.29 2 -12 2 937.51 35.60 2 -12 2 937.81 42.20 -10 -2 2 919.41 41.90 -2 12 2 912.11 41.00 12 -10 2 838.62 47.10 10 2 2 957.30 36.30 -12 10 2 893.21 30.80 12 -10 2 954.70 38.30 12 -10 -2 841.62 43.90 -10 -2 -2 809.22 38.50 -12 10 -2 839.82 44.40 -12 10 -2 884.61 34.00 12 -10 -2 876.11 31.40 -2 12 -2 846.42 40.40 2 -12 -2 886.61 32.60 12 -10 -2 892.41 51.39 2 -12 -2 923.51 42.90 -12 9 2 199.18 12.80 12 -9 2 209.98 26.10 3 -12 2 166.88 14.80 12 -9 2 205.78 17.30 3 -12 2 178.48 17.90 -3 12 2 181.18 17.10 -9 -3 2 192.68 21.40 9 3 2 201.68 14.10 12 -9 -2 207.08 24.90 -12 9 -2 199.58 14.90 3 -12 -2 194.38 15.80 3 -12 -2 193.88 20.00 -3 12 -2 179.18 18.60 -9 -3 -2 191.68 19.20 12 -9 -2 187.68 12.40 12 -9 -2 182.48 27.30 -8 -4 2 187.58 21.60 4 -12 2 140.49 16.20 12 -8 2 154.68 15.30 8 4 2 136.69 9.90 -12 8 2 142.99 11.40 12 -8 2 171.78 24.90 4 -12 2 121.59 16.40 12 -8 -2 147.49 21.70 4 -12 -2 175.08 20.50 4 -12 -2 138.99 16.00 -12 8 -2 141.49 13.40 -4 12 -2 154.18 17.50 -8 -4 -2 135.69 18.20 12 -8 -2 170.68 26.80 12 -8 -2 129.19 11.30 -8 -4 -2 161.38 16.80 -5 12 2 274.97 18.20 -5 12 2 273.17 17.80 12 -7 2 248.28 26.00 -7 -5 2 273.77 22.50 5 -12 2 265.87 20.20 5 -12 2 293.27 20.70 12 -7 2 268.47 20.40 -12 7 2 266.37 16.30 -7 -5 -2 329.57 23.10 12 -7 -2 348.37 32.00 5 -12 -2 308.87 23.30 -5 12 -2 269.27 20.10 12 -7 -2 291.27 26.10 5 -12 -2 280.37 21.90 -7 -5 -2 311.67 21.30 -12 7 -2 318.97 19.00 -12 6 2 542.45 25.00 -6 12 2 532.65 22.50 -6 -6 2 504.35 28.90 6 -12 2 615.24 30.20 12 -6 2 494.85 34.20 6 -12 2 573.04 30.30 12 -6 2 573.14 31.00 -6 12 2 545.45 24.10 -6 -6 -2 563.04 29.40 -6 12 -2 589.34 27.80 -12 6 -2 530.05 26.00 6 -12 -2 587.54 32.50 -6 -6 -2 524.35 29.10 12 -6 -2 557.04 36.80 6 -12 -2 509.85 30.00 12 -6 -2 584.34 40.50 -5 -7 2 321.87 23.80 -7 12 2 347.67 16.30 7 -12 2 314.07 21.70 -7 12 2 342.37 17.10 -12 5 2 335.37 19.90 12 -5 2 353.16 26.00 7 -12 2 342.87 24.50 12 -5 2 341.47 27.90 7 -12 -2 363.76 25.80 12 -5 -2 329.27 30.40 5 7 -2 347.27 14.20 -12 5 -2 367.26 21.40 -5 -7 -2 337.57 22.60 5 7 -2 317.97 28.30 -5 -7 -2 329.37 23.30 7 -12 -2 348.77 26.40 8 -12 2 788.52 39.30 -8 12 2 761.72 27.70 8 -12 2 791.02 34.80 -4 -8 2 834.62 38.30 12 -4 2 730.13 28.50 -12 4 2 784.12 33.00 12 -4 2 763.02 41.00 -4 -8 -2 716.33 35.60 -12 4 -2 726.33 32.60 8 -12 -2 713.93 36.90 4 8 -2 728.53 23.80 4 8 -2 728.43 41.20 8 -12 -2 809.12 41.70 12 -4 -2 656.03 44.50 -4 -8 -2 714.73 34.90 -8 12 -2 738.63 31.20 12 -3 2 766.42 40.20 -9 12 2 771.62 26.80 9 -12 2 803.62 41.20 9 -12 2 828.52 35.60 -12 3 2 776.12 34.30 -3 -9 2 740.03 37.00 -3 -9 -2 664.23 34.00 3 9 -2 664.13 38.80 9 -12 -2 642.24 35.40 9 -12 -2 648.04 38.70 -12 3 -2 650.63 31.10 -3 -9 -2 667.13 33.50 -9 12 -2 640.14 28.30 9 -12 -2 626.04 24.70 3 9 -2 607.84 22.70 -12 2 2 411.36 25.00 2 10 2 440.06 30.80 -2 -10 2 445.26 27.80 12 -2 2 426.46 29.00 -10 12 2 405.56 17.00 10 -12 2 409.96 30.90 10 -12 2 369.36 23.60 2 10 -2 407.76 19.40 10 -12 -2 445.56 34.40 10 -12 -2 421.96 18.50 -2 -10 -2 431.96 27.50 2 10 -2 434.76 31.40 -10 12 -2 417.56 21.80 -12 2 -2 397.16 24.90 10 -12 -2 440.76 29.70 11 -12 2 800.62 44.40 12 -1 2 781.62 38.70 1 11 2 844.72 42.90 -11 12 2 770.02 26.50 11 -12 2 838.02 35.90 -12 1 2 777.72 37.50 -1 -11 2 777.72 39.70 -12 1 -2 949.21 40.40 11 -12 -2 870.91 29.70 -1 -11 -2 835.32 41.00 11 -12 -2 989.00 51.19 1 11 -2 803.92 39.80 11 -12 -2 867.71 43.70 -11 12 -2 871.91 38.50 1 11 -2 831.72 44.10 12 -12 2 1063.39 53.59 0 -12 2 1002.20 46.20 12 -12 2 1076.29 42.60 12 0 2 1044.80 44.30 0 12 2 1044.90 48.50 -12 0 2 979.90 44.60 -12 12 2 1022.80 32.80 -12 0 -2 1145.79 47.90 12 -12 -2 1099.89 51.39 0 12 -2 1156.98 52.19 12 -12 -2 1151.58 58.89 0 -12 -2 1169.88 50.39 -12 12 -2 1141.69 41.30 12 -12 -2 1092.09 36.30 -1 13 2 763.42 39.10 1 -13 2 661.83 36.80 -12 -1 2 675.33 36.70 13 -12 2 676.33 32.40 13 -12 2 643.64 43.90 -13 12 2 651.93 24.50 12 1 2 665.13 33.10 -1 13 -2 730.83 39.80 1 -13 -2 737.13 27.40 13 -12 -2 825.72 43.10 1 -13 -2 697.63 39.00 -13 12 -2 730.63 30.70 -12 -1 -2 658.03 37.10 13 -12 -2 747.33 48.00 13 -11 2 850.71 49.60 -2 13 2 929.71 42.40 2 -13 2 1048.90 46.40 11 2 2 911.41 37.10 13 -11 2 944.21 39.40 -13 11 2 927.11 31.90 -11 -2 2 922.91 43.40 2 -13 2 936.61 44.40 13 -11 -2 949.51 54.09 13 -11 -2 930.01 47.60 -11 -2 -2 947.41 44.00 -13 11 -2 945.71 36.20 2 -13 -2 977.50 34.90 13 -11 -2 936.61 32.70 2 -13 -2 954.30 45.00 -2 13 -2 857.91 43.60 3 -13 2 261.07 23.10 13 -10 2 290.07 32.50 3 -13 2 266.77 18.80 10 3 2 281.27 16.70 -10 -3 2 258.57 23.20 -13 10 2 266.97 15.20 -3 13 2 254.97 20.80 13 -10 2 265.57 20.40 -13 10 -2 269.47 18.10 -10 -3 -2 265.67 22.90 13 -10 -2 256.97 15.30 3 -13 -2 239.68 17.40 13 -10 -2 312.67 34.80 13 -10 -2 319.17 27.90 -3 13 -2 276.07 22.40 3 -13 -2 274.87 24.50 4 -13 2 337.87 24.60 13 -9 2 337.97 30.80 -9 -4 2 372.86 26.00 -4 13 2 299.67 21.40 4 -13 2 301.57 21.00 -13 9 2 307.77 17.20 13 -9 2 326.07 22.40 9 4 2 346.17 16.00 4 -13 -2 265.57 19.00 -4 13 -2 318.77 23.00 4 -13 -2 291.67 23.60 -9 -4 -2 257.57 21.60 13 -9 -2 240.98 24.90 13 -9 -2 274.07 15.90 13 -9 -2 271.47 33.80 -13 9 -2 250.07 17.60 -5 13 2 549.35 27.60 13 -8 2 637.74 39.70 -8 -5 2 520.85 31.70 5 -13 2 523.75 30.60 13 -8 2 566.24 30.20 5 -13 2 559.54 29.60 -13 8 2 602.24 25.10 5 -13 -2 551.64 32.90 -5 13 -2 588.44 30.40 13 -8 -2 622.14 42.20 -13 8 -2 549.25 26.80 -8 -5 -2 574.04 31.80 13 -8 -2 547.45 37.00 5 -13 -2 565.54 29.90 -8 -5 -2 552.44 30.70 6 -13 2 793.22 37.70 -6 13 2 794.32 32.20 13 -7 2 742.63 43.90 6 -13 2 759.32 36.70 13 -7 2 834.22 38.40 -13 7 2 827.92 32.50 6 -13 -2 769.02 39.80 6 -13 -2 830.12 39.10 -6 13 -2 757.42 35.00 13 -7 -2 818.52 46.20 13 -7 -2 868.11 49.50 -13 7 -2 809.02 33.60 -7 -6 -2 741.93 37.70 -7 -6 -2 783.82 37.80 -7 13 2 624.74 26.60 -7 13 2 603.64 24.90 -13 6 2 674.33 29.40 -6 -7 2 665.33 34.90 13 -6 2 608.64 34.40 7 -13 2 654.33 33.00 13 -6 2 683.33 40.30 7 -13 2 647.94 34.30 -13 6 -2 588.14 29.20 6 7 -2 608.34 21.20 -6 -7 -2 617.24 33.00 -7 13 -2 624.94 29.80 -6 -7 -2 703.73 35.10 7 -13 -2 600.34 34.20 13 -6 -2 614.44 41.50 13 -6 -2 599.24 43.10 7 -13 -2 628.84 34.60 6 7 -2 644.54 40.10 13 -5 2 670.23 40.10 13 -5 2 634.04 25.50 -5 -8 2 601.64 34.40 -8 13 2 592.74 24.00 -13 5 2 654.43 30.20 8 -13 2 621.84 32.30 13 -5 2 659.53 37.60 -8 13 2 653.53 25.50 8 -13 2 709.23 36.90 13 -5 -2 647.04 44.50 13 -5 -2 674.33 42.90 -13 5 -2 600.54 29.90 5 8 -2 643.94 40.40 8 -13 -2 648.54 36.20 -5 -8 -2 647.94 33.80 5 8 -2 645.74 21.20 -8 13 -2 609.54 28.60 8 -13 -2 607.14 35.90 -5 -8 -2 668.93 34.40 9 -13 2 1445.16 60.39 9 -13 2 1467.55 53.79 -4 -9 2 1355.66 56.29 -13 4 2 1405.36 51.99 13 -4 2 1481.15 61.09 -9 13 2 1440.56 44.70 4 9 -2 1512.25 64.19 9 -13 -2 1426.76 58.19 -4 -9 -2 1436.76 56.09 13 -4 -2 1403.26 65.19 9 -13 -2 1423.76 61.69 -13 4 -2 1343.77 51.69 -9 13 -2 1416.56 49.80 -4 -9 -2 1439.36 56.29 10 -13 2 1065.49 43.50 10 -13 2 1128.79 52.19 13 -3 2 1015.90 48.70 -13 3 2 1038.80 43.60 3 10 2 987.90 51.19 -10 13 2 1029.10 33.80 -3 -10 2 1094.49 48.20 10 -13 -2 992.80 46.40 -13 3 -2 890.31 40.20 -10 13 -2 1034.40 42.80 10 -13 -2 924.51 33.00 10 -13 -2 1022.80 51.39 -3 -10 -2 926.01 43.60 13 -3 -2 872.51 50.49 3 10 -2 963.70 31.90 3 10 -2 976.40 48.90 2 11 2 235.08 27.00 11 -13 2 236.88 29.60 13 -2 2 222.88 25.50 -11 13 2 219.38 11.90 -2 -11 2 218.48 21.30 11 -13 2 217.08 19.00 -13 2 2 187.78 19.80 -11 13 -2 149.59 14.40 -13 2 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22.30 7.20 10 -7 -3 23.50 13.30 -7 -3 -3 25.10 8.90 3 -10 -3 15.40 9.60 10 -7 -3 10.40 4.50 -3 10 -3 15.40 8.10 10 -6 3 19.20 11.40 -10 6 3 33.50 7.30 4 -10 3 30.40 8.10 -4 10 3 37.30 7.10 -4 10 3 36.20 8.10 10 -6 3 39.10 8.50 4 -10 3 30.50 9.00 -6 -4 -3 33.30 9.60 4 -10 -3 27.80 11.10 10 -6 -3 34.60 6.30 -4 10 -3 49.60 10.50 -6 -4 -3 36.10 9.20 10 -6 -3 19.40 13.20 4 -10 -3 43.80 10.90 -10 6 -3 25.50 7.50 5 -10 3 110.49 14.60 10 -5 3 95.29 16.10 -10 5 3 98.49 10.50 -5 10 3 101.59 8.40 10 -5 3 99.79 12.70 5 -10 3 84.79 12.20 -5 10 3 97.99 9.60 5 5 -3 110.59 18.40 -10 5 -3 95.69 12.30 -5 -5 -3 117.89 14.50 -5 10 -3 127.49 14.20 5 -10 -3 138.79 21.70 5 -10 -3 111.79 17.10 10 -5 -3 105.29 9.80 -5 -5 -3 104.99 13.50 10 -4 3 301.37 23.80 -6 10 3 385.26 15.10 6 -10 3 372.06 23.80 -6 10 3 364.26 15.70 -10 4 3 364.66 19.10 10 -4 3 402.56 15.80 10 -4 3 363.76 23.10 -4 -6 3 366.86 22.60 -4 -6 -3 384.16 22.30 6 -10 -3 323.77 25.50 -6 10 -3 353.66 20.10 -10 4 -3 335.67 19.60 4 6 -3 382.66 27.20 -4 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54.79 7.90 5 -11 -3 42.90 11.80 -11 6 -3 43.30 9.30 -6 -5 -3 59.09 11.80 -5 11 -3 31.30 8.90 -6 -5 -3 62.09 12.00 11 -6 -3 40.00 13.70 5 -11 -3 62.59 13.70 6 5 -3 16.50 11.50 -5 -6 3 246.48 19.20 6 -11 3 227.08 17.60 11 -5 3 225.58 18.60 -6 11 3 252.87 12.80 -6 11 3 238.18 13.30 6 -11 3 248.58 19.80 11 -5 3 230.48 22.90 -11 5 3 234.98 15.70 -11 5 -3 227.08 16.80 -5 -6 -3 231.28 18.40 6 -11 -3 213.88 21.00 11 -5 -3 256.67 30.10 -5 -6 -3 200.08 16.80 6 -11 -3 244.78 20.80 -6 11 -3 219.08 17.10 5 6 -3 239.58 22.30 11 -4 3 660.93 29.80 -7 11 3 731.03 25.00 -11 4 3 762.42 30.80 7 -11 3 785.42 36.20 7 -11 3 749.13 32.00 11 -4 3 697.43 36.70 -7 11 3 744.93 24.40 -4 -7 3 691.93 34.00 7 -11 -3 750.42 37.90 7 -11 -3 720.13 38.50 4 7 -3 758.92 40.20 -4 -7 -3 717.23 33.20 -4 -7 -3 682.63 33.40 4 7 -3 705.43 24.80 11 -4 -3 692.33 44.20 -11 4 -3 701.73 31.00 -7 11 -3 687.73 34.50 -8 11 3 283.27 12.40 -3 -8 3 287.67 21.20 8 -11 3 293.07 24.00 11 -3 3 282.07 14.50 11 -3 3 215.08 21.40 -11 3 3 258.37 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247.68 30.20 21 -14 -3 249.58 40.20 -14 -7 -3 184.78 26.80 7 -21 -3 232.28 25.30 -21 14 -3 216.28 23.80 21 -14 -3 170.88 27.80 21 -13 3 350.56 26.10 8 -21 3 339.47 32.30 -8 21 3 412.16 27.90 8 -21 3 341.77 30.10 -21 13 3 328.47 24.70 21 -13 3 354.06 45.60 8 -21 -3 301.97 27.40 21 -13 -3 230.78 38.80 8 -21 -3 271.97 29.30 13 8 -3 236.28 40.70 21 -13 -3 258.47 33.90 -13 -8 -3 348.17 34.70 -8 21 -3 236.48 27.50 -9 21 3 430.96 27.10 21 -12 3 359.56 34.90 -21 12 3 424.16 29.00 9 -21 3 447.36 33.90 9 -21 3 399.26 34.30 21 -12 3 491.85 47.10 -9 21 -3 387.56 32.10 12 9 -3 413.86 50.09 9 -21 -3 382.76 31.20 -21 12 -3 408.86 28.20 21 -12 -3 364.96 36.80 21 -12 -3 307.97 43.00 9 -21 -3 385.96 34.60 -12 -9 -3 397.56 37.60 10 -21 3 444.46 35.40 10 -21 3 494.15 36.80 21 -11 3 434.66 43.70 -21 11 3 477.05 30.60 -10 21 3 442.96 27.00 21 -11 -3 442.96 42.30 10 -21 -3 445.16 38.10 10 -21 -3 526.75 38.00 -21 11 -3 498.75 33.20 11 10 -3 402.16 49.40 21 -11 -3 409.26 49.20 -10 21 -3 462.05 32.20 21 -10 3 449.36 42.90 21 -10 3 416.06 29.60 -11 21 3 434.86 24.40 11 -21 3 481.95 37.20 -21 10 3 513.95 31.90 10 11 3 414.36 50.79 11 -21 3 483.95 35.10 -21 10 -3 535.85 34.30 11 -21 -3 547.15 41.50 11 -21 -3 486.75 38.40 21 -10 -3 530.35 49.30 21 -10 -3 600.54 49.10 -11 21 -3 536.75 34.30 10 11 -3 518.05 48.90 12 -21 3 406.16 34.00 21 -9 3 415.26 31.50 12 -21 3 500.65 39.00 -12 21 3 469.15 23.70 -21 9 3 434.96 38.00 21 -9 3 449.36 44.60 9 12 3 471.65 46.10 21 -9 -3 414.16 45.90 9 12 -3 567.34 50.09 12 -21 -3 488.95 39.60 21 -9 -3 539.05 50.09 12 -21 -3 558.64 40.80 -21 9 -3 550.44 36.20 -9 -12 -3 462.75 38.80 -12 21 -3 541.25 33.20 13 -21 3 308.47 28.90 21 -8 3 295.97 37.90 21 -8 3 240.98 28.80 13 -21 3 301.57 36.10 8 13 3 224.28 37.10 -21 8 3 344.17 30.90 -13 21 -3 341.07 26.60 13 -21 -3 339.27 35.10 13 -21 -3 254.07 32.40 21 -8 -3 279.77 41.30 21 -8 -3 285.47 46.40 8 13 -3 233.38 36.50 -8 -13 -3 278.47 30.20 -21 8 -3 272.77 28.10 21 -7 3 278.67 36.20 -21 7 3 224.28 27.90 14 -21 3 185.88 29.60 21 -7 3 205.48 28.70 14 -21 3 252.57 25.80 7 14 3 182.18 33.90 21 -7 -3 231.18 37.00 14 -21 -3 169.58 30.10 -14 21 -3 239.28 22.70 7 14 -3 235.98 37.80 21 -7 -3 247.68 40.20 -7 -14 -3 121.29 24.70 14 -21 -3 206.58 28.60 -21 7 -3 192.38 26.40 -21 6 3 285.47 32.40 15 -21 3 293.97 26.50 21 -6 3 220.58 33.20 21 -6 3 228.78 32.70 6 15 3 234.68 37.00 15 -21 3 252.37 34.20 -15 21 -3 220.68 23.00 -6 -15 -3 196.68 27.60 -21 6 -3 265.87 30.30 6 15 -3 208.98 34.50 21 -6 -3 203.18 33.60 15 -21 -3 274.47 37.10 21 -6 -3 198.38 42.00 15 -21 -3 188.38 28.30 21 -5 3 261.07 33.10 16 -21 3 273.27 25.20 16 -21 3 177.88 29.80 21 -5 3 151.48 33.20 -21 5 3 185.48 27.70 5 16 3 191.88 33.30 21 -5 -3 208.68 34.70 -21 5 -3 132.29 23.00 16 -21 -3 176.28 32.20 -5 -16 -3 152.68 26.00 5 16 -3 139.99 31.40 -16 21 -3 228.98 22.10 21 -5 -3 216.98 43.80 16 -21 -3 209.98 29.10 0 0 4 1.40 3.10 0 0 -4 2.20 6.10 0 0 -4 0.00 3.10 -1 1 4 1472.35 46.40 0 -1 4 1359.46 40.00 1 0 4 1422.16 41.90 1 0 4 1366.96 39.50 -1 0 4 1412.86 39.40 1 -1 4 1336.77 39.80 0 1 4 1323.97 38.40 0 1 4 1420.46 44.30 -1 1 4 1370.96 38.00 -1 1 -4 1353.76 39.80 -1 0 -4 1376.06 41.00 -1 0 -4 1389.66 39.30 1 -1 -4 1370.16 37.70 0 -1 -4 1373.36 43.10 1 0 -4 1344.47 38.90 -1 1 -4 1373.36 39.60 0 1 -4 1337.27 39.70 1 -1 -4 1397.76 45.30 0 -1 -4 1392.26 38.20 -1 -1 4 228.18 11.70 1 1 4 196.78 10.00 2 -1 4 223.88 10.80 2 -1 4 205.78 10.90 1 -2 4 237.98 11.70 -2 1 4 212.28 9.60 -1 2 4 215.48 8.70 -1 2 4 232.08 15.70 1 -2 4 211.78 11.50 2 -1 4 203.38 10.90 1 1 4 205.68 12.70 1 1 -4 205.08 11.50 2 -1 -4 233.08 9.80 -1 2 -4 212.68 11.80 -2 1 -4 188.38 10.50 -2 1 -4 211.88 10.90 1 -2 -4 206.98 8.50 -1 -1 -4 186.38 11.90 -2 1 -4 205.28 10.20 -1 -1 -4 205.58 10.20 2 -1 -4 237.28 17.50 1 -2 -4 231.28 15.40 -1 2 -4 216.08 11.20 2 0 4 704.53 23.90 2 -2 4 707.83 24.30 2 0 4 716.63 24.00 -2 2 4 763.12 31.30 0 2 4 736.03 28.10 0 2 4 738.83 22.40 -2 0 4 708.93 24.20 -2 2 4 730.63 20.80 2 -2 4 726.23 24.80 0 -2 4 729.13 25.00 2 0 4 723.73 23.30 2 -2 -4 756.02 21.10 -2 2 -4 720.73 24.80 -2 2 -4 715.13 24.80 2 -2 -4 756.12 31.70 0 -2 -4 742.93 28.10 -2 0 -4 725.23 23.40 2 0 -4 749.82 24.50 -2 0 -4 734.13 23.30 0 2 -4 715.33 25.50 0 -2 -4 739.53 22.50 -1 3 4 370.46 20.10 2 1 4 299.97 13.70 2 1 4 319.27 15.00 3 -2 4 335.27 15.50 -3 2 4 348.77 12.40 3 -2 4 341.67 14.90 1 -3 4 318.57 15.00 -2 -1 4 339.47 16.20 -1 3 4 326.07 11.80 -3 2 4 330.77 21.50 1 -3 4 321.47 15.30 3 -2 -4 339.97 11.90 -2 -1 -4 341.37 14.60 2 1 -4 313.77 15.70 -3 2 -4 333.27 14.80 -1 3 -4 323.67 14.70 3 -2 -4 317.97 21.20 -2 -1 -4 316.17 13.90 -2 -1 -4 337.37 12.70 -3 2 -4 340.77 15.50 -1 3 -4 323.47 15.60 -1 3 -4 343.97 13.20 1 -3 -4 305.67 18.00 1 -3 -4 343.77 11.70 3 -1 4 8.50 4.60 3 -1 4 9.80 4.00 1 2 4 7.70 3.60 2 -3 4 -1.00 3.70 2 -3 4 -0.70 4.10 -2 3 4 3.20 2.10 -3 1 4 7.60 4.30 1 2 4 7.70 5.40 -2 3 4 5.00 7.00 -1 -2 4 1.90 4.80 3 -1 4 5.50 3.30 2 -3 -4 2.50 7.10 -2 3 -4 2.60 4.30 -1 -2 -4 6.60 4.00 -2 3 -4 11.00 5.10 -1 -2 -4 3.80 5.40 1 2 -4 12.60 5.90 -3 1 -4 8.70 4.60 2 -3 -4 5.10 2.00 -3 1 -4 7.40 4.10 3 -1 -4 4.20 4.20 -2 3 -4 6.80 2.80 -3 1 -4 4.30 2.40 3 0 4 1923.21 55.69 0 3 4 1968.90 53.29 3 0 4 1938.11 53.79 0 3 4 2042.40 60.79 3 -3 4 1993.00 56.99 0 -3 4 1944.41 57.49 -3 3 4 1938.01 64.39 3 0 4 1983.20 54.09 -3 3 4 1980.40 49.99 3 -3 4 1791.12 55.19 3 -3 -4 1899.61 48.80 -3 3 -4 1867.11 54.99 -3 0 -4 1904.91 51.59 3 0 -4 1890.91 55.39 0 -3 -4 1919.11 52.19 -3 0 -4 1927.51 53.39 3 -3 -4 2004.10 63.79 -3 0 -4 1941.01 54.79 0 3 -4 1887.11 53.79 -3 3 -4 1942.21 55.99 -3 3 -4 1847.32 50.39 0 3 -4 1883.81 56.39 0 3 -4 1955.60 54.29 0 -3 -4 1930.31 58.29 3 1 4 150.28 8.30 1 -4 4 164.28 10.70 1 -4 4 160.18 9.80 4 -3 4 164.78 10.30 -4 3 4 176.28 16.50 4 -3 4 149.69 11.50 -1 4 4 183.08 14.40 -1 4 4 155.58 7.90 3 1 4 156.78 9.90 1 -4 4 145.29 11.20 3 1 4 155.88 10.00 4 -3 -4 166.98 6.60 1 -4 -4 177.88 8.40 -1 4 -4 164.18 9.70 -3 -1 -4 171.08 9.80 1 -4 -4 198.78 14.60 -3 -1 -4 185.18 9.10 -3 -1 -4 159.78 10.50 -4 3 -4 167.08 10.90 4 -3 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289.67 25.10 7 -16 4 324.17 26.00 -7 16 4 265.17 18.70 -16 9 4 280.67 19.80 16 -9 4 279.67 44.10 16 -9 4 252.77 18.00 -9 -7 -4 288.07 26.50 -7 16 -4 227.28 25.10 -9 -7 -4 250.27 24.30 9 7 -4 212.88 31.20 16 -9 -4 229.68 33.00 7 -16 -4 228.78 24.00 16 -9 -4 245.68 36.80 7 -16 -4 268.97 34.00 -16 9 -4 211.48 19.50 16 -8 4 409.56 35.80 16 -8 4 381.06 17.60 8 -16 4 413.26 28.70 8 -16 4 461.75 31.50 16 -8 4 415.56 24.50 -16 8 4 408.56 24.90 -8 16 4 436.46 21.80 16 -8 -4 364.56 37.60 8 -16 -4 416.26 32.60 -8 -8 -4 351.66 28.70 -8 16 -4 360.06 26.00 -8 -8 -4 360.26 29.20 8 8 -4 358.06 36.70 -16 8 -4 337.07 24.20 16 -8 -4 343.77 64.09 8 -16 -4 349.37 29.00 -9 16 4 404.16 19.70 9 -16 4 443.36 28.60 16 -7 4 386.76 26.10 -9 16 4 415.86 19.30 16 -7 4 414.16 36.10 16 -7 4 408.06 18.80 -16 7 4 418.26 26.40 9 -16 4 441.86 31.80 -9 16 -4 415.16 26.70 7 9 -4 417.46 18.00 -7 -9 -4 388.46 34.00 -7 -9 -4 418.36 30.80 -16 7 -4 383.66 26.20 16 -7 -4 404.06 40.20 9 -16 -4 392.96 31.30 9 -16 -4 420.46 33.10 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540.55 39.20 0 -16 -4 522.65 38.00 16 0 -4 502.95 40.00 16 -16 -4 508.65 38.40 16 -16 -4 472.35 43.90 -16 0 -4 441.36 34.70 17 -16 4 426.46 24.70 1 -17 4 461.55 35.90 16 1 4 438.46 27.30 17 -16 4 439.86 41.50 16 1 -4 483.65 37.70 -17 16 -4 400.26 26.40 17 -16 -4 341.07 44.30 17 -16 -4 441.66 37.50 1 -17 -4 448.46 35.00 -16 -1 -4 405.96 32.80 -1 17 -4 408.26 36.10 15 2 4 396.06 23.00 2 -17 4 364.06 31.90 17 -15 4 290.87 37.20 17 -15 4 361.76 21.70 -2 17 4 367.36 31.10 17 -15 -4 419.56 36.20 -2 17 -4 445.96 35.90 17 -15 -4 359.46 44.70 2 -17 -4 419.86 34.60 -15 -2 -4 349.27 31.20 2 -17 -4 403.76 19.40 15 2 -4 370.16 33.90 -17 15 -4 426.06 26.10 -3 17 4 337.27 27.60 -17 14 4 326.77 15.80 17 -14 4 365.66 27.70 17 -14 4 373.86 37.50 3 -17 4 348.67 31.40 14 3 4 348.87 23.50 17 -14 -4 477.35 38.50 -3 17 -4 357.26 32.10 3 -17 -4 401.26 24.10 3 -17 -4 396.16 33.00 17 -14 -4 356.76 44.50 17 -14 -4 371.76 16.80 14 3 -4 347.87 31.20 14 3 -4 338.27 42.20 -14 -3 -4 333.27 30.50 -17 14 -4 399.06 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4 -15 39.70 14.00 4 9 -15 1.70 14.30 -4 -9 -15 31.40 12.60 10 -13 15 32.40 16.30 13 -3 15 36.90 13.50 13 -3 -15 44.60 28.90 -13 3 -15 54.59 15.50 13 -3 -15 52.39 13.50 -3 -10 -15 38.20 12.00 -10 13 -15 67.59 19.00 -3 -10 -15 72.39 19.30 3 10 -15 74.19 20.70 10 -13 -15 83.89 24.60 -3 -10 -15 58.39 9.70 11 -13 15 36.60 16.70 -13 2 -15 50.39 16.10 -11 13 -15 42.30 15.80 -2 -11 -15 44.60 9.60 -2 -11 -15 48.80 16.00 13 -2 -15 52.89 16.00 11 -13 -15 52.49 21.90 2 11 -15 37.80 17.30 -2 -11 -15 104.89 16.00 13 -2 -15 87.99 36.20 13 -1 15 -22.80 11.90 12 -13 15 15.40 14.30 13 -1 -15 22.00 26.50 -1 -12 -15 27.00 14.90 -13 1 -15 -0.70 9.50 12 -13 -15 42.00 23.30 -12 13 -15 -3.10 12.20 1 12 -15 27.40 16.30 13 -1 -15 23.60 15.00 -1 -12 -15 11.50 9.60 13 -13 15 6.10 12.80 13 -13 -15 7.90 20.30 -13 0 -15 0.70 12.30 -13 13 -15 25.90 14.90 0 -13 -15 6.90 14.90 13 0 -15 2.90 12.50 0 -13 -15 14.90 10.30 0 13 -15 5.70 14.80 14 -13 15 58.39 20.00 1 -14 -15 84.19 22.50 -14 13 -15 62.99 18.00 -13 -1 -15 55.99 16.50 -1 14 -15 55.39 18.90 1 -14 -15 76.69 14.00 13 1 -15 69.79 20.90 14 -13 -15 87.29 29.20 14 -12 15 162.28 26.50 -14 12 -15 199.78 27.00 -2 14 -15 150.88 26.80 2 -14 -15 146.79 18.10 12 2 -15 162.48 26.70 -12 -2 -15 154.48 17.30 2 -14 -15 142.89 26.10 -12 -2 -15 144.59 22.80 14 -12 -15 128.29 32.80 14 -11 15 151.58 27.50 -11 -3 -15 137.19 23.10 11 3 -15 141.39 25.40 3 -14 -15 112.59 25.00 14 -11 -15 139.29 31.60 -14 11 -15 162.38 23.80 -11 -3 -15 140.39 17.40 -3 14 -15 98.99 21.90 3 -14 -15 145.09 14.70 14 -10 15 201.68 29.50 -10 -4 -15 185.08 18.70 10 4 -15 176.48 29.70 4 -14 -15 174.08 30.10 -10 -4 -15 200.68 26.40 -4 14 -15 167.78 26.50 -14 10 -15 175.98 24.80 14 -10 -15 99.89 29.30 14 -9 15 222.18 29.70 9 5 -15 248.78 33.00 5 -14 -15 234.08 33.40 14 -9 -15 216.68 11.70 -9 -5 -15 247.08 22.30 -9 -5 -15 251.27 28.10 -14 9 -15 171.78 25.00 -5 14 -15 212.38 29.70 14 -9 -15 224.88 42.50 14 -8 15 302.27 30.60 -6 14 15 289.57 16.20 -8 -6 -15 376.16 27.50 -14 8 -15 333.87 30.30 8 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14 -3 15 89.49 18.70 11 -14 15 59.99 19.40 3 11 -15 84.99 21.10 -14 3 -15 25.30 14.40 14 -3 -15 91.09 36.00 11 -14 -15 86.09 25.60 14 -3 -15 28.70 13.50 -3 -11 -15 54.49 8.40 -11 14 -15 32.40 15.50 -3 -11 -15 58.19 15.00 -3 -11 -15 50.89 15.70 14 -2 15 38.80 13.20 12 -14 15 40.10 16.20 14 -2 -15 36.70 30.60 -14 2 -15 42.40 16.20 -2 -12 -15 27.90 14.50 -2 -12 -15 31.80 12.90 -12 14 -15 25.10 15.00 14 -2 -15 12.50 12.40 -12 14 -15 -11.60 12.50 2 12 -15 10.70 14.60 12 -14 -15 64.79 24.60 13 -14 15 -3.90 13.80 13 -14 -15 -11.70 16.70 -1 -13 -15 14.70 8.70 -14 1 -15 -0.20 11.30 14 -1 -15 -7.50 27.10 14 -1 -15 12.60 16.70 1 13 -15 -11.40 12.20 -1 -13 -15 25.10 16.00 -13 14 -15 -9.90 10.40 -1 -13 -15 0.30 10.50 14 -14 15 15.00 15.70 14 0 -15 26.90 15.40 0 -14 -15 5.20 9.40 0 -14 -15 -3.10 10.00 14 -14 -15 8.90 19.20 -14 14 -15 13.60 14.70 0 14 -15 12.20 17.50 0 -14 -15 -1.60 14.30 -14 0 -15 15.90 14.10 15 -14 15 73.89 20.70 15 -14 -15 107.89 29.70 1 -15 -15 81.99 16.00 -15 14 -15 97.19 20.90 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20.20 16 -15 15 94.99 23.50 15 1 -15 49.40 20.40 -16 15 -15 42.40 18.80 -1 16 -15 44.80 20.70 -15 -1 -15 62.89 18.80 16 -15 -15 28.80 22.50 1 -16 -15 26.20 16.20 1 -16 -15 21.60 10.10 16 -14 15 43.20 20.50 -2 16 15 108.49 20.90 2 -16 -15 69.09 20.10 2 -16 -15 97.79 16.90 -2 16 -15 108.89 24.80 -16 14 -15 110.09 23.60 14 2 -15 126.39 26.00 -14 -2 -15 110.69 22.40 -3 16 15 151.08 21.50 16 -13 15 81.69 22.40 -3 16 -15 109.99 25.40 3 -16 -15 117.99 24.30 -16 13 -15 132.79 24.70 3 -16 -15 113.09 19.80 16 -13 -15 96.29 30.70 -13 -3 -15 117.99 21.90 -13 -3 -15 142.39 18.40 13 3 -15 100.59 22.90 -4 16 15 128.99 18.10 16 -12 15 120.09 26.30 4 -16 -15 92.69 20.20 12 4 -15 157.88 27.80 16 -12 -15 84.49 29.40 -12 -4 -15 161.58 20.10 -12 -4 -15 133.89 21.90 -16 12 -15 111.09 22.00 -4 16 -15 133.29 27.00 4 -16 -15 108.79 24.80 16 -11 15 87.59 23.30 -5 16 15 107.19 15.20 -11 -5 -15 113.99 21.90 -16 11 -15 75.99 18.60 5 -16 -15 85.59 24.70 16 -11 -15 116.39 34.20 11 5 -15 84.09 22.80 -11 -5 -15 90.09 16.10 -5 16 -15 115.49 23.50 -6 16 15 108.59 12.40 16 -10 15 79.19 22.00 6 -16 -15 102.79 24.30 10 6 -15 92.19 24.20 -10 -6 -15 80.49 16.20 16 -10 -15 111.09 33.70 -16 10 -15 101.69 20.10 -6 16 -15 70.49 20.20 -10 -6 -15 74.29 18.30 16 -9 15 332.67 33.00 -9 -7 -15 214.48 27.20 7 -16 -15 260.07 37.90 9 7 -15 223.28 33.70 -7 16 -15 252.27 32.40 -9 -7 -15 249.58 30.90 16 -9 -15 221.88 15.10 16 -9 -15 192.48 40.60 -16 9 -15 268.87 27.70 16 -8 15 362.06 34.50 16 -8 -15 372.86 22.00 -8 -8 -15 350.76 29.60 8 8 -15 352.46 36.20 -8 16 -15 416.16 37.00 16 -8 -15 343.37 54.49 8 -16 -15 404.96 42.30 -8 -8 -15 392.56 29.90 -16 8 -15 371.46 32.40 9 -16 15 377.26 34.00 16 -7 15 392.46 34.80 16 -7 -15 391.06 56.99 -16 7 -15 348.17 31.20 -9 16 -15 380.76 34.90 -7 -9 -15 372.96 30.40 16 -7 -15 377.26 24.80 7 9 -15 423.56 39.70 -7 -9 -15 398.36 30.20 9 -16 -15 401.26 42.60 16 -6 15 251.17 30.40 10 -16 15 280.37 34.70 -6 -10 -15 282.97 26.40 -16 6 -15 250.37 30.60 6 10 -15 304.77 38.80 -6 -10 -15 259.87 27.30 10 -16 -15 264.57 37.80 16 -6 -15 238.68 46.10 16 -6 -15 308.77 24.50 -10 16 -15 314.87 31.60 16 -5 15 145.39 23.30 11 -16 15 173.38 27.90 -11 16 -15 163.18 25.60 5 11 -15 162.78 28.80 -16 5 -15 167.28 24.30 -5 -11 -15 149.79 24.20 16 -5 -15 199.58 24.80 16 -5 -15 164.28 42.50 11 -16 -15 175.38 33.40 -5 -11 -15 173.08 24.20 12 -16 15 99.79 22.30 16 -4 15 102.09 19.90 -16 4 -15 65.29 17.40 12 -16 -15 135.19 31.70 16 -4 -15 90.49 20.70 4 12 -15 79.39 23.40 16 -4 -15 98.49 36.20 -4 -12 -15 96.79 18.80 -4 -12 -15 93.59 19.90 -12 16 -15 76.69 19.60 16 -3 15 26.20 13.90 13 -16 15 60.69 20.80 -13 16 -15 62.59 18.80 16 -3 -15 33.70 19.40 -3 -13 -15 44.30 15.50 -3 -13 -15 59.19 18.10 3 13 -15 34.20 18.40 -16 3 -15 27.70 14.40 13 -16 -15 21.90 20.70 16 -3 -15 110.39 41.10 14 -16 15 37.70 18.90 -2 -14 -15 17.30 12.10 2 14 -15 33.70 19.60 16 -2 -15 38.60 32.10 -2 -14 -15 23.90 14.50 -14 16 -15 22.30 14.10 16 -2 -15 24.80 15.40 14 -16 -15 27.70 20.10 -16 2 -15 18.80 15.20 15 -16 15 22.40 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-1 -28 41.90 15.80 -8 7 -28 68.69 22.90 7 1 -28 64.59 20.20 -7 -1 -28 -1.50 14.90 8 -6 -28 -1.50 10.80 2 -8 -28 -5.30 9.50 6 2 -28 -9.60 28.90 -8 6 -28 37.00 19.60 -2 8 -28 10.70 17.50 6 2 -28 -7.80 14.30 8 -6 -28 -13.70 25.30 -8 6 -28 -46.20 16.40 -6 -2 -28 6.00 13.60 -2 8 -28 0.60 26.90 2 -8 -28 -14.90 18.20 -6 -2 -28 -41.10 15.30 3 -8 -28 -6.00 19.90 8 -5 -28 -3.10 23.20 -3 8 -28 -39.00 22.60 5 3 -28 -8.10 23.60 5 3 -28 17.10 16.10 -8 5 -28 4.30 17.20 -5 -3 -28 -16.60 11.10 8 -5 -28 -7.00 11.80 -5 -3 -28 -4.00 17.80 8 -4 -28 46.60 32.30 -4 -4 -28 7.80 13.20 4 -8 -28 -22.10 19.80 -8 4 -28 -12.10 14.30 -4 8 -28 58.99 18.50 -8 4 -28 44.00 18.10 4 -8 -28 31.00 12.10 8 -4 -28 38.90 15.50 -4 -4 -28 24.50 19.20 4 4 -28 43.20 32.70 4 4 -28 25.00 17.70 -4 8 -28 -22.80 24.20 -3 -5 -28 48.10 16.30 3 5 -28 27.70 14.90 3 5 -28 74.39 34.80 5 -8 -28 9.70 10.60 -8 3 -28 -9.20 13.80 -8 3 -28 34.20 16.70 -3 -5 -28 21.70 19.40 8 -3 -28 19.00 12.80 5 -8 -28 49.40 28.50 8 -3 -28 14.30 28.40 -5 8 -28 89.49 23.70 -5 8 -28 -28.60 23.50 -8 2 -28 86.09 21.40 -2 -6 -28 78.99 25.70 -6 8 -28 55.99 30.10 8 -2 -28 64.79 19.30 8 -2 -28 59.89 34.90 -8 2 -28 66.39 17.80 6 -8 -28 87.39 15.90 -6 8 -28 66.89 22.30 2 6 -28 98.09 24.60 -2 -6 -28 71.29 18.10 6 -8 -28 82.69 32.30 2 6 -28 91.99 34.80 -1 -7 -28 62.49 17.90 7 -8 -28 99.89 16.30 1 7 -28 66.59 20.80 -1 -7 -28 59.79 25.90 1 7 -28 47.20 34.90 7 -8 -28 96.99 35.80 -7 8 -28 52.69 25.10 8 -1 -28 56.69 33.80 -8 1 -28 87.99 18.60 8 -1 -28 96.29 20.60 -7 8 -28 79.09 22.50 -8 1 -28 115.49 23.80 0 0 -29 0.00 12.00 0 0 -29 -34.00 21.40 -1 0 -29 4.90 12.60 0 1 -29 9.70 16.10 -1 0 -29 -34.50 19.70 0 -1 -29 16.10 14.70 1 0 -29 34.00 16.60 0 -1 -29 -6.70 23.60 0 1 -29 -5.70 25.00 1 -1 -29 15.40 14.70 1 0 -29 38.60 27.30 1 -1 -29 -2.30 23.20 -1 1 -29 -34.10 20.30 -1 1 -29 17.40 14.90 -2 1 -29 -6.90 22.10 -1 2 -29 -3.10 12.30 -2 1 -29 16.60 15.10 1 1 -29 16.10 14.50 2 -1 -29 -6.60 23.50 -1 -1 -29 -0.80 13.10 2 -1 -29 4.00 13.80 1 -2 -29 13.00 24.60 1 1 -29 33.20 26.70 -1 -1 -29 21.30 20.70 -1 2 -29 -47.40 21.30 -2 0 -29 -0.20 14.30 0 -2 -29 7.70 13.30 2 0 -29 -23.00 22.70 0 -2 -29 9.80 21.30 -2 2 -29 0.90 26.60 0 2 -29 -29.50 23.70 -2 0 -29 -27.60 19.60 0 2 -29 5.30 14.40 2 -2 -29 -9.70 11.60 -2 2 -29 32.00 16.80 2 0 -29 23.80 15.80 2 -2 -29 6.00 22.80 2 1 -29 31.60 18.10 1 -3 -29 84.59 30.20 1 -3 -29 56.39 17.10 2 1 -29 47.00 29.90 -2 -1 -29 58.49 18.30 3 -2 -29 50.79 17.10 -1 3 -29 5.80 26.40 3 -2 -29 59.39 31.30 -2 -1 -29 60.49 26.40 -1 3 -29 70.49 19.60 -3 2 -29 10.20 23.90 -3 2 -29 49.50 18.50 -2 3 -29 93.69 22.60 -1 -2 -29 112.99 31.30 3 -1 -29 80.89 19.40 3 -1 -29 10.00 25.60 -3 1 -29 84.69 27.50 -2 3 -29 106.79 34.90 2 -3 -29 77.69 20.20 1 2 -29 76.59 30.70 -1 -2 -29 127.99 22.50 -3 1 -29 66.29 19.90 1 2 -29 64.89 20.50 2 -3 -29 72.99 31.80 -3 0 -29 52.79 26.80 -3 3 -29 44.60 25.70 0 -3 -29 28.80 24.50 -3 3 -29 65.39 20.80 3 0 -29 56.29 19.80 3 0 -29 26.70 29.60 -3 0 -29 57.69 20.50 0 3 -29 68.99 20.00 0 -3 -29 83.09 19.20 0 3 -29 67.09 32.30 3 -3 -29 81.59 18.50 3 -3 -29 12.90 25.20 1 -4 -29 161.98 24.20 4 -3 -29 208.68 27.60 -4 3 -29 139.99 33.80 -3 -1 -29 143.79 25.90 3 1 -29 161.68 26.90 -3 -1 -29 199.88 36.20 4 -3 -29 103.89 36.40 3 1 -29 131.69 36.20 -4 3 -29 170.48 28.90 -1 4 -29 116.79 36.70 -1 4 -29 107.59 23.80 1 -4 -29 152.98 36.40 2 2 -29 277.87 34.70 4 -2 -29 159.18 41.30 -4 2 -29 192.18 29.50 2 2 -29 182.68 42.50 -2 -2 -29 239.88 40.30 -2 -2 -29 238.28 30.10 -2 4 -29 204.38 43.30 4 -2 -29 212.38 29.10 -4 2 -29 225.88 37.30 2 -4 -29 273.87 30.30 2 -4 -29 180.08 40.20 -2 4 -29 215.58 33.60 1 3 -29 141.69 40.10 -4 1 -29 143.59 54.79 -3 4 -29 162.58 37.60 3 -4 -29 184.48 25.00 4 -1 -29 165.08 26.20 3 -4 -29 187.78 42.40 -4 1 -29 166.88 28.70 1 3 -29 186.08 30.30 4 -1 -29 155.58 42.50 -3 4 -29 149.19 27.90 -1 -3 -29 185.78 37.60 -1 -3 -29 178.98 26.60 0 -4 -29 172.98 25.10 4 0 -29 77.99 34.90 -4 4 -29 149.99 27.90 -4 4 -29 85.69 30.10 -4 0 -29 134.39 25.20 4 0 -29 157.78 25.90 0 -4 -29 121.09 33.10 4 -4 -29 144.09 23.40 0 4 -29 167.38 28.40 4 -4 -29 107.39 35.70 -4 0 -29 107.69 29.00 0 4 -29 76.49 30.90 -1 5 -29 50.19 31.30 -4 -1 -29 125.49 28.00 5 -4 -29 64.49 32.10 4 1 -29 66.89 32.10 1 -5 -29 75.99 27.80 -5 4 -29 47.80 26.50 -1 5 -29 129.49 24.80 4 1 -29 71.99 21.00 -5 4 -29 109.19 23.60 5 -4 -29 80.99 18.60 -4 -1 -29 108.89 24.00 1 -5 -29 90.39 19.00 -2 5 -29 165.98 30.00 2 -5 -29 175.78 24.50 2 -5 -29 200.48 39.50 -3 -2 -29 194.88 34.50 3 2 -29 115.99 25.30 5 -3 -29 87.69 33.30 5 -3 -29 195.58 26.50 3 2 -29 201.08 43.90 -5 3 -29 188.38 31.40 -5 3 -29 132.79 30.30 -3 -2 -29 145.89 25.40 -2 5 -29 133.69 37.10 2 3 -29 208.98 47.10 -5 2 -29 274.87 36.30 -2 -3 -29 236.78 39.20 2 3 -29 249.88 33.00 -5 2 -29 196.88 33.10 3 -5 -29 260.47 25.80 -3 5 -29 237.48 41.40 -3 5 -29 206.68 31.30 3 -5 -29 216.48 42.80 5 -2 -29 196.78 47.10 -2 -3 -29 227.38 30.00 5 -2 -29 232.48 29.40 -1 -4 -29 159.58 33.60 -5 1 -29 216.28 29.60 -5 1 -29 127.09 28.30 -4 5 -29 128.09 43.40 -4 5 -29 147.29 29.40 1 4 -29 78.29 33.90 5 -1 -29 101.09 39.40 5 -1 -29 165.28 26.70 1 4 -29 157.98 26.80 4 -5 -29 167.78 23.50 4 -5 -29 159.48 40.20 -1 -4 -29 191.28 25.90 5 0 -29 130.89 25.40 0 5 -29 182.68 31.20 -5 5 -29 155.28 35.40 -5 0 -29 119.19 26.60 5 -5 -29 66.69 31.70 5 0 -29 79.89 36.30 0 5 -29 58.09 32.90 0 -5 -29 101.29 31.00 -5 0 -29 116.89 24.20 -5 5 -29 185.18 31.60 5 -5 -29 182.38 23.80 0 -5 -29 145.19 22.80 1 -6 -29 147.29 34.80 6 -5 -29 123.49 41.40 1 -6 -29 132.79 20.90 5 1 -29 88.79 37.60 -5 -1 -29 154.88 27.70 -5 -1 -29 130.69 26.60 6 -5 -29 134.39 22.00 5 1 -29 87.49 20.20 -1 6 -29 64.09 30.90 -1 6 -29 108.39 27.50 -6 5 -29 138.19 30.40 -6 5 -29 142.69 27.50 4 2 -29 32.80 31.70 -2 6 -29 77.59 21.10 4 2 -29 59.59 19.70 2 -6 -29 44.50 27.20 -4 -2 -29 54.69 22.40 -2 6 -29 48.50 29.20 -6 4 -29 42.70 18.40 -6 4 -29 31.90 24.80 6 -4 -29 60.59 16.20 6 -4 -29 77.49 36.90 -4 -2 -29 33.40 14.70 2 -6 -29 49.20 14.90 6 -3 -29 207.48 27.10 -3 6 -29 150.58 28.90 3 3 -29 146.69 42.80 -3 6 -29 152.98 35.60 3 -6 -29 248.68 26.80 -6 3 -29 178.88 32.00 3 -6 -29 230.78 42.00 -6 3 -29 156.58 30.40 6 -3 -29 164.78 43.10 -3 -3 -29 173.48 33.30 -3 -3 -29 184.48 27.90 3 3 -29 201.58 31.50 4 -6 -29 252.07 27.30 -2 -4 -29 235.98 28.90 -6 2 -29 198.68 31.30 6 -2 -29 182.28 25.50 2 4 -29 189.78 29.70 -2 -4 -29 124.09 31.50 6 -2 -29 170.68 43.90 -6 2 -29 191.28 30.30 4 -6 -29 192.58 40.00 2 4 -29 205.58 44.30 -4 6 -29 207.58 32.60 -5 6 -29 212.68 35.40 1 5 -29 163.78 42.70 6 -1 -29 183.28 45.50 1 5 -29 192.18 32.80 5 -6 -29 209.98 43.00 -6 1 -29 201.88 30.40 -5 6 -29 158.58 35.80 -6 1 -29 248.88 33.70 -1 -5 -29 254.47 39.00 6 -1 -29 236.58 31.90 -1 -5 -29 190.88 27.60 5 -6 -29 265.67 24.90 6 -6 -29 203.58 46.20 6 0 -29 255.67 32.70 0 -6 -29 238.78 27.50 0 6 -29 265.87 36.10 -6 6 -29 276.77 37.10 6 0 -29 161.98 43.60 0 -6 -29 213.18 36.30 -6 6 -29 247.18 37.70 0 6 -29 178.58 42.30 -6 0 -29 239.88 31.60 -6 0 -29 267.17 32.70 0 0 -30 270.47 34.10 0 0 -30 279.17 46.20 1 -1 -30 414.26 35.10 -1 1 -30 451.05 56.89 1 0 -30 408.86 37.30 1 0 -30 350.56 54.79 0 1 -30 402.66 37.50 -1 0 -30 508.65 60.69 1 -1 -30 419.56 57.69 0 1 -30 476.65 58.89 -1 1 -30 432.26 40.20 0 -1 -30 452.05 38.40 -1 0 -30 482.65 38.50 0 -1 -30 435.36 56.39 1 1 -30 721.13 47.60 -1 -1 -30 617.84 59.49 2 -1 -30 645.44 65.79 -2 1 -30 637.74 46.20 1 -2 -30 695.03 45.10 2 -1 -30 687.43 45.50 -1 2 -30 634.04 62.79 -1 -1 -30 665.33 45.50 -1 2 -30 653.63 47.60 1 1 -30 688.73 68.29 1 -2 -30 688.23 66.59 -2 1 -30 614.74 59.09 0 -2 -30 821.22 49.30 2 -2 -30 827.32 70.99 0 2 -30 753.62 51.39 0 2 -30 899.61 71.69 2 0 -30 783.92 71.19 2 -2 -30 857.91 50.29 -2 2 -30 787.72 51.89 0 -2 -30 844.12 66.99 2 0 -30 735.43 49.00 -2 0 -30 839.52 63.19 -2 0 -30 827.92 50.49 -2 2 -30 810.12 65.49 -1 3 -30 891.61 71.49 3 -2 -30 805.72 48.60 -3 2 -30 877.81 65.89 2 1 -30 874.81 75.19 1 -3 -30 809.12 48.90 -2 -1 -30 830.02 64.39 2 1 -30 786.62 50.69 -2 -1 -30 976.20 52.69 -3 2 -30 815.62 53.99 1 -3 -30 887.31 70.39 -1 3 -30 911.11 56.09 3 -2 -30 760.42 70.89 -2 3 -30 932.91 70.39 1 2 -30 898.11 75.69 1 2 -30 846.22 53.59 -2 3 -30 871.41 55.19 -1 -2 -30 865.11 66.29 2 -3 -30 787.52 47.40 -3 1 -30 853.31 53.09 3 -1 -30 860.61 51.69 3 -1 -30 925.71 76.79 -3 1 -30 749.62 61.99 -1 -2 -30 905.61 51.69 2 -3 -30 823.12 71.49 0 -3 -30 945.61 70.79 3 -3 -30 901.21 50.89 3 -3 -30 892.71 74.99 0 3 -30 940.71 57.69 -3 0 -30 949.80 66.79 3 0 -30 957.40 79.29 -3 3 -30 967.80 58.49 -3 3 -30 941.91 69.99 -3 0 -30 926.61 54.99 3 0 -30 929.61 53.79 0 -3 -30 956.40 52.59 0 3 -30 967.00 75.39 4 -3 -30 990.40 51.89 -4 3 -30 921.21 63.69 3 1 -30 925.21 80.09 -4 3 -30 893.21 57.19 1 -4 -30 929.01 50.59 1 -4 -30 885.41 68.89 3 1 -30 946.41 55.49 -1 4 -30 916.61 74.09 4 -3 -30 764.02 72.79 -3 -1 -30 925.61 54.09 -3 -1 -30 877.01 63.09 -1 4 -30 848.92 55.59 -2 4 -30 751.52 66.59 -2 -2 -30 883.31 64.19 4 -2 -30 822.32 49.00 4 -2 -30 822.52 74.79 -2 4 -30 832.32 55.49 2 2 -30 865.71 53.49 2 2 -30 696.43 69.39 -4 2 -30 805.22 59.29 -2 -2 -30 809.62 49.70 -4 2 -30 748.83 51.19 2 -4 -30 873.51 71.19 2 -4 -30 842.42 47.60 4 -1 -30 750.02 74.69 -3 4 -30 796.92 54.19 -3 4 -30 844.72 66.09 4 -1 -30 817.52 50.29 -1 -3 -30 850.11 64.99 -1 -3 -30 804.82 48.20 1 3 -30 745.53 73.29 -4 1 -30 698.93 57.59 1 3 -30 780.32 52.29 3 -4 -30 856.41 47.50 3 -4 -30 900.81 73.79 -4 1 -30 752.22 51.29 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 19112 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z+2/3' '-x+y, -x, z+1/3' '-x, -y, z+1/2' 'y, -x+y, z+1/6' 'x-y, x, z+5/6' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Tb1 Tb 0.99935(2) 0.97242(2) 0.99896(2) 0.01369(6) Uani 1 1 d . . . . . P1 P 0.87012(8) 1.03425(8) 1.04367(6) 0.0152(3) Uani 1 1 d . . . . . P2 P 1.16880(8) 1.14050(8) 0.95279(6) 0.0149(2) Uani 1 1 d . . . . . P3 P 1.09876(9) 0.86998(9) 0.91715(6) 0.0188(3) Uani 1 1 d . . . . . O1 O 0.9126(2) 0.9905(2) 1.07975(16) 0.0172(8) Uani 1 1 d . . . . . O2 O 0.9119(2) 1.0469(2) 0.98479(15) 0.0191(7) Uani 1 1 d . . . . . O3 O 0.8735(2) 1.1171(2) 1.06899(16) 0.0193(8) Uani 1 1 d . . . . . O4 O 1.1326(2) 1.1243(2) 1.01357(15) 0.0186(7) Uani 1 1 d . . . . . O5 O 1.0926(2) 1.0648(2) 0.91842(16) 0.0181(8) Uani 1 1 d . . . . . O6 O 1.2608(2) 1.1509(2) 0.94470(17) 0.0230(8) Uani 1 1 d . . . . . O7 O 1.0836(3) 0.9096(3) 0.97119(16) 0.0253(8) Uani 1 1 d . . . . . O8 O 1.0655(3) 0.8930(3) 0.86315(16) 0.0226(8) Uani 1 1 d . . . . . O9 O 1.0615(3) 0.7691(3) 0.92438(18) 0.0281(9) Uani 1 1 d . . . . . O10 O 1.1323(4) 0.6743(4) 0.9008(2) 0.0485(13) Uani 1 1 d G . . . . H10C H 1.114377 0.714172 0.906793 0.073 Uiso 1 1 d G U . . . O11 O 1.1755(4) 0.7429(4) 0.8184(2) 0.0669(17) Uani 1 1 d . . . . . O1W O 1.3970(6) 1.2975(7) 0.8863(6) 0.138(4) Uani 1 1 d G . . . . H1WA H 1.361668 1.246634 0.909941 0.207 Uiso 1 1 d G U . . . H1WB H 1.452951 1.298424 0.882372 0.207 Uiso 1 1 d G U . . . O2W O 1.0561(2) 1.2482(3) 1.05830(17) 0.0265(8) Uani 1 1 d . . . . . H2WA H 1.004433 1.255752 1.058710 0.040 Uiso 1 1 d R U . . . H2WB H 1.069242 1.214840 1.085800 0.040 Uiso 1 1 d R U . . . C1 C 0.7492(3) 0.9504(3) 1.0403(2) 0.0224(11) Uani 1 1 d . . . . . H1A H 0.724057 0.938321 1.079350 0.027 Uiso 1 1 calc R U . . . H1B H 0.717783 0.976072 1.018292 0.027 Uiso 1 1 calc R U . . . C2 C 0.6346(3) 0.7836(3) 1.0235(3) 0.0231(11) Uani 1 1 d . . . . . H2 H 0.627985 0.768420 1.064944 0.028 Uiso 1 1 calc R U . . . C3 C 0.6300(4) 0.7037(3) 0.9912(3) 0.0306(13) Uani 1 1 d . . . . . H3A H 0.680656 0.695319 1.002885 0.046 Uiso 1 1 calc R U . . . H3B H 0.633885 0.715796 0.950328 0.046 Uiso 1 1 calc R U . . . H3C H 0.572483 0.648498 0.999797 0.046 Uiso 1 1 calc R U . . . C4 C 0.5615(3) 0.8065(3) 1.0075(3) 0.0249(12) Uani 1 1 d . . . . . H4 H 0.571838 0.859743 1.031119 0.030 Uiso 1 1 calc R U . . . C5 C 0.5604(4) 0.8316(4) 0.9459(3) 0.0344(14) Uani 1 1 d . . . . . H5A H 0.553622 0.781418 0.921223 0.041 Uiso 1 1 calc R U . . . H5B H 0.618884 0.886335 0.936472 0.041 Uiso 1 1 calc R U . . . C6 C 0.4818(5) 0.8502(6) 0.9342(4) 0.0493(19) Uani 1 1 d . . . . . H6A H 0.492732 0.904819 0.955648 0.059 Uiso 1 1 calc R U . . . H6B H 0.481102 0.863053 0.893233 0.059 Uiso 1 1 calc R U . . . C7 C 0.3911(5) 0.7721(6) 0.9507(4) 0.057(2) Uani 1 1 d . . . . . H7A H 0.376705 0.718769 0.926676 0.068 Uiso 1 1 calc R U . . . H7B H 0.343491 0.788442 0.944643 0.068 Uiso 1 1 calc R U . . . C8 C 0.3929(4) 0.7485(5) 1.0134(4) 0.052(2) Uani 1 1 d . . . . . H8A H 0.402782 0.800377 1.037492 0.062 Uiso 1 1 calc R U . . . H8B H 0.333716 0.695519 1.023910 0.062 Uiso 1 1 calc R U . . . C9 C 0.4684(4) 0.7267(4) 1.0239(3) 0.0395(16) Uani 1 1 d . . . . . H9A H 0.456385 0.672649 1.001455 0.047 Uiso 1 1 calc R U . . . H9B H 0.468915 0.712227 1.064630 0.047 Uiso 1 1 calc R U . . . C10 C 1.1772(3) 1.2467(3) 0.9291(2) 0.0189(10) Uani 1 1 d . U . . . H10A H 1.225642 1.297903 0.950762 0.023 Uiso 1 1 calc R U . . . H10B H 1.194022 1.256307 0.888350 0.023 Uiso 1 1 calc R U . . . C11 C 1.0936(4) 1.3330(3) 0.9191(2) 0.0209(10) Uani 1 1 d . U . . . H11 H 1.125899 1.351712 0.881821 0.025 Uiso 1 1 calc R U . . . C12 C 1.1475(4) 1.4067(4) 0.9615(3) 0.0294(13) Uani 1 1 d . . . . . H12A H 1.117294 1.389866 0.998563 0.044 Uiso 1 1 calc R U . . . H12B H 1.151963 1.463599 0.948649 0.044 Uiso 1 1 calc R U . . . H12C H 1.208580 1.414841 0.964878 0.044 Uiso 1 1 calc R U . . . C13 C 0.9962(4) 1.3146(3) 0.9100(2) 0.0228(11) Uani 1 1 d . . . . . H13 H 0.966505 1.263502 0.882269 0.027 Uiso 1 1 calc R U . . . C14 C 0.9982(4) 1.3968(4) 0.8827(3) 0.0343(14) Uani 1 1 d . . . . . H14A H 1.028833 1.449376 0.908704 0.041 Uiso 1 1 calc R U . . . H14B H 1.034025 1.412194 0.847137 0.041 Uiso 1 1 calc R U . . . C15 C 0.9041(5) 1.3798(4) 0.8694(3) 0.0437(18) Uani 1 1 d . . . . . H15A H 0.908459 1.436315 0.854642 0.052 Uiso 1 1 calc R U . . . H15B H 0.876692 1.332962 0.839387 0.052 Uiso 1 1 calc R U . . . C16 C 0.8437(5) 1.3489(5) 0.9208(3) 0.0426(17) Uani 1 1 d . . . . . H16A H 0.781334 1.332744 0.909500 0.051 Uiso 1 1 calc R U . . . H16B H 0.865774 1.399268 0.948584 0.051 Uiso 1 1 calc R U . . . C17 C 0.8416(4) 1.2668(4) 0.9490(3) 0.0338(14) Uani 1 1 d . . . . . H17A H 0.805000 1.251235 0.984187 0.041 Uiso 1 1 calc R U . . . H17B H 0.812128 1.214059 0.922987 0.041 Uiso 1 1 calc R U . . . C18 C 0.9371(4) 1.2858(4) 0.9633(3) 0.0273(12) Uani 1 1 d . . . . . H18A H 0.964579 1.334495 0.992233 0.033 Uiso 1 1 calc R U . . . H18B H 0.933851 1.230478 0.979470 0.033 Uiso 1 1 calc R U . . . C19 C 1.2211(4) 0.9179(4) 0.9090(3) 0.0298(14) Uani 1 1 d . . . . . H19A H 1.246618 0.916785 0.946620 0.036 Uiso 1 1 calc R U . . . H19B H 1.231359 0.877587 0.883525 0.036 Uiso 1 1 calc R U . . . C20 C 1.3720(4) 1.0433(4) 0.8739(3) 0.0286(12) Uani 1 1 d . . . . . H20 H 1.398193 1.102760 0.853579 0.034 Uiso 1 1 calc R U . . . C21 C 1.3774(4) 0.9755(4) 0.8343(4) 0.0426(16) Uani 1 1 d . . . . . H21A H 1.329818 0.955796 0.805319 0.064 Uiso 1 1 calc R U . . . H21B H 1.368918 0.922872 0.856179 0.064 Uiso 1 1 calc R U . . . H21C H 1.436982 1.004307 0.815753 0.064 Uiso 1 1 calc R U . . . C22 C 1.4302(4) 1.0571(5) 0.9276(3) 0.0468(18) Uani 1 1 d . . . . . H22 H 1.405565 0.997375 0.947376 0.056 Uiso 1 1 calc R U . . . C23 C 1.5280(5) 1.0893(7) 0.9107(5) 0.074(3) Uani 1 1 d . U . . . H23A H 1.552494 1.147332 0.889719 0.089 Uiso 1 1 calc R U . . . H23B H 1.529430 1.044116 0.884855 0.089 Uiso 1 1 calc R U . . . C24 C 1.5895(6) 1.1031(7) 0.9632(5) 0.086(3) Uani 1 1 d . U . . . H24A H 1.570178 1.044155 0.981952 0.104 Uiso 1 1 calc R U . . . H24B H 1.653451 1.129020 0.950967 0.104 Uiso 1 1 calc R U . . . C25 C 1.5814(6) 1.1656(7) 1.0032(5) 0.089(3) Uani 1 1 d . U . . . H25A H 1.621109 1.175513 1.036383 0.107 Uiso 1 1 calc R U . . . H25B H 1.603384 1.224963 0.984253 0.107 Uiso 1 1 calc R U . . . C26 C 1.4879(6) 1.1320(8) 1.0234(5) 0.091(3) Uani 1 1 d . U . . . H26A H 1.485628 1.175991 1.049912 0.109 Uiso 1 1 calc R U . . . H26B H 1.464550 1.073108 1.043096 0.109 Uiso 1 1 calc R U . . . C27 C 1.4284(6) 1.1205(7) 0.9665(4) 0.072(3) Uani 1 1 d . U . . . H27A H 1.364849 1.099678 0.977523 0.086 Uiso 1 1 calc R U . . . H27B H 1.452832 1.180163 0.947549 0.086 Uiso 1 1 calc R U . . . C28 C 1.1705(4) 0.6873(4) 0.8516(3) 0.0392(15) Uani 1 1 d . . . . . C29 C 1.2099(5) 0.6267(5) 0.8411(4) 0.056(2) Uani 1 1 d . . . . . H29A H 1.267541 0.660682 0.820618 0.084 Uiso 1 1 calc R U . . . H29B H 1.167416 0.574318 0.818288 0.084 Uiso 1 1 calc R U . . . H29C H 1.220512 0.605615 0.877522 0.084 Uiso 1 1 calc R U . . . N1 N 0.7298(3) 0.8632(3) 1.01398(19) 0.0185(9) Uani 1 1 d . . . . . H1C H 0.770372 0.847908 1.027785 0.022 Uiso 1 1 calc R U . . . H1D H 0.739406 0.871987 0.975886 0.022 Uiso 1 1 calc R U . . . N2 N 1.0898(3) 1.2454(3) 0.93728(19) 0.0179(8) Uani 1 1 d . U . . . H2A H 1.074008 1.235173 0.974640 0.021 Uiso 1 1 calc R U . . . H2B H 1.045701 1.198599 0.916972 0.021 Uiso 1 1 calc R U . . . N3 N 1.2728(3) 1.0112(3) 0.8865(2) 0.0220(9) Uani 1 1 d . . . . . H3D H 1.269946 1.049812 0.912052 0.026 Uiso 1 1 calc R U . . . H3E H 1.245693 1.014441 0.853890 0.026 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Tb1 0.01524(9) 0.01598(14) 0.01029(9) 0.00010(15) 0.00019(7) 0.00813(13) P1 0.0167(6) 0.0180(6) 0.0122(7) -0.0007(5) -0.0001(5) 0.0097(5) P2 0.0142(5) 0.0159(6) 0.0138(7) -0.0008(5) -0.0012(5) 0.0069(5) P3 0.0224(7) 0.0252(7) 0.0154(6) 0.0023(5) 0.0016(5) 0.0168(6) O1 0.0204(19) 0.0197(15) 0.014(2) 0.0000(15) -0.0009(15) 0.0116(14) O2 0.0252(17) 0.0233(16) 0.013(2) 0.0006(13) -0.0002(14) 0.0151(15) O3 0.0236(18) 0.0189(15) 0.018(2) -0.0017(14) -0.0010(15) 0.0124(15) O4 0.0238(17) 0.0177(16) 0.013(2) -0.0014(13) -0.0029(14) 0.0098(14) O5 0.0175(19) 0.0202(18) 0.013(2) -0.0022(14) -0.0035(15) 0.0070(15) O6 0.0181(17) 0.0254(19) 0.026(2) -0.0030(16) -0.0020(16) 0.0115(15) O7 0.033(2) 0.043(2) 0.013(2) -0.0019(17) -0.0002(16) 0.0291(19) O8 0.035(2) 0.0316(19) 0.012(2) 0.0002(15) 0.0004(16) 0.0250(17) O9 0.034(2) 0.026(2) 0.027(2) 0.0050(17) 0.0030(18) 0.0165(17) O10 0.064(3) 0.056(3) 0.045(3) 0.013(3) 0.015(3) 0.045(3) O11 0.111(5) 0.074(4) 0.042(4) 0.015(3) 0.023(3) 0.067(4) O1W 0.089(6) 0.114(7) 0.185(10) 0.069(7) 0.051(7) 0.032(5) O2W 0.0256(19) 0.0259(19) 0.027(2) 0.0059(16) 0.0007(17) 0.0123(16) C1 0.019(2) 0.023(2) 0.024(3) -0.004(2) 0.000(2) 0.010(2) C2 0.019(2) 0.020(2) 0.027(3) 0.006(2) 0.005(2) 0.0069(19) C3 0.027(2) 0.019(2) 0.044(4) 0.001(3) 0.002(3) 0.010(2) C4 0.020(2) 0.025(2) 0.028(3) 0.003(2) 0.005(2) 0.010(2) C5 0.029(3) 0.048(4) 0.034(4) 0.006(3) 0.003(3) 0.025(3) C6 0.050(4) 0.073(5) 0.045(5) 0.009(4) -0.002(4) 0.045(4) C7 0.035(4) 0.073(5) 0.070(6) -0.014(5) -0.013(4) 0.034(4) C8 0.020(3) 0.054(4) 0.077(6) 0.012(4) 0.013(3) 0.015(3) C9 0.022(3) 0.032(3) 0.059(5) 0.010(3) 0.007(3) 0.009(2) C10 0.016(2) 0.019(2) 0.021(3) 0.006(2) 0.001(2) 0.0079(19) C11 0.026(3) 0.016(2) 0.021(3) 0.0026(19) 0.001(2) 0.010(2) C12 0.035(3) 0.020(2) 0.033(4) -0.004(2) -0.004(3) 0.014(2) C13 0.029(3) 0.021(3) 0.022(3) -0.001(2) -0.003(2) 0.016(2) C14 0.039(3) 0.026(3) 0.043(4) 0.010(3) 0.003(3) 0.020(3) C15 0.047(4) 0.031(3) 0.063(5) 0.011(3) -0.006(3) 0.027(3) C16 0.036(3) 0.036(3) 0.066(5) -0.002(3) -0.009(3) 0.025(3) C17 0.030(3) 0.034(3) 0.041(4) 0.001(3) -0.001(3) 0.019(3) C18 0.028(3) 0.032(3) 0.025(3) -0.002(2) -0.001(2) 0.017(2) C19 0.026(3) 0.028(3) 0.043(4) 0.010(3) 0.010(3) 0.018(2) C20 0.024(3) 0.027(3) 0.028(3) 0.005(2) 0.002(2) 0.008(2) C21 0.035(3) 0.043(3) 0.056(5) 0.009(3) 0.008(4) 0.024(3) C22 0.028(3) 0.053(4) 0.047(5) -0.002(4) -0.006(3) 0.011(3) C23 0.026(4) 0.081(6) 0.094(7) -0.020(5) -0.005(4) 0.011(4) C24 0.041(4) 0.093(6) 0.123(7) -0.036(5) -0.027(5) 0.032(4) C25 0.053(4) 0.096(5) 0.124(7) -0.066(6) -0.035(5) 0.042(4) C26 0.070(5) 0.130(7) 0.091(7) -0.053(6) -0.039(5) 0.064(5) C27 0.052(4) 0.111(7) 0.078(7) -0.019(5) -0.013(4) 0.059(5) C28 0.040(3) 0.034(3) 0.043(4) -0.001(3) 0.000(3) 0.018(3) C29 0.064(5) 0.054(4) 0.063(6) 0.001(4) 0.011(4) 0.039(4) N1 0.0161(18) 0.0197(19) 0.018(2) -0.0016(16) -0.0008(16) 0.0078(16) N2 0.024(2) 0.0135(19) 0.017(2) 0.0012(17) 0.0000(17) 0.0095(16) N3 0.026(2) 0.024(2) 0.019(2) -0.0007(18) -0.0025(18) 0.0145(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Tb Tb -0.1723 4.1537 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O7 Tb1 O5 80.43(13) . 5_565 ? O7 Tb1 O8 86.00(13) . 5_565 ? O5 Tb1 O8 81.07(13) 5_565 5_565 ? O7 Tb1 O1 84.05(13) . 6_654 ? O5 Tb1 O1 156.80(10) 5_565 6_654 ? O8 Tb1 O1 80.73(13) 5_565 6_654 ? O7 Tb1 O2 155.25(13) . . ? O5 Tb1 O2 123.07(13) 5_565 . ? O8 Tb1 O2 104.04(12) 5_565 . ? O1 Tb1 O2 75.54(11) 6_654 . ? O7 Tb1 O4 93.86(13) . . ? O5 Tb1 O4 71.84(11) 5_565 . ? O8 Tb1 O4 152.51(12) 5_565 . ? O1 Tb1 O4 126.65(13) 6_654 . ? O2 Tb1 O4 87.38(11) . . ? O7 Tb1 O5 73.90(13) . . ? O5 Tb1 O5 121.17(13) 5_565 . ? O8 Tb1 O5 145.70(13) 5_565 . ? O1 Tb1 O5 69.95(12) 6_654 . ? O2 Tb1 O5 85.89(11) . . ? O4 Tb1 O5 58.53(12) . . ? O7 Tb1 O1 145.20(13) . . ? O5 Tb1 O1 69.56(12) 5_565 . ? O8 Tb1 O1 72.61(12) 5_565 . ? O1 Tb1 O1 117.87(12) 6_654 . ? O2 Tb1 O1 59.13(12) . . ? O4 Tb1 O1 93.16(11) . . ? O5 Tb1 O1 137.04(10) . . ? O7 Tb1 Tb1 72.70(10) . 6_654 ? O5 Tb1 Tb1 147.24(10) 5_565 6_654 ? O8 Tb1 Tb1 114.64(9) 5_565 6_654 ? O1 Tb1 Tb1 37.22(10) 6_654 6_654 ? O2 Tb1 Tb1 82.56(8) . 6_654 ? O4 Tb1 Tb1 91.33(8) . 6_654 ? O5 Tb1 Tb1 33.05(9) . 6_654 ? O1 Tb1 Tb1 141.12(8) . 6_654 ? O7 Tb1 Tb1 112.86(10) . 5_565 ? O5 Tb1 Tb1 35.56(10) 5_565 5_565 ? O8 Tb1 Tb1 70.33(9) 5_565 5_565 ? O1 Tb1 Tb1 144.64(9) 6_654 5_565 ? O2 Tb1 Tb1 91.88(8) . 5_565 ? O4 Tb1 Tb1 84.59(8) . 5_565 ? O5 Tb1 Tb1 143.11(9) . 5_565 ? O1 Tb1 Tb1 34.31(9) . 5_565 ? Tb1 Tb1 Tb1 173.266(2) 6_654 5_565 ? O3 P1 O2 115.5(2) . . ? O3 P1 O1 115.5(2) . . ? O2 P1 O1 105.9(2) . . ? O3 P1 C1 104.4(2) . . ? O2 P1 C1 109.6(2) . . ? O1 P1 C1 105.4(2) . . ? O6 P2 O5 115.5(2) . . ? O6 P2 O4 116.3(2) . . ? O5 P2 O4 104.4(2) . . ? O6 P2 C10 106.5(2) . . ? O5 P2 C10 106.7(2) . . ? O4 P2 C10 106.9(2) . . ? O9 P3 O8 112.8(2) . . ? O9 P3 O7 109.9(2) . . ? O8 P3 O7 114.68(18) . . ? O9 P3 C19 104.8(2) . . ? O8 P3 C19 106.6(3) . . ? O7 P3 C19 107.3(3) . . ? P1 O1 Tb1 151.7(2) . 5_565 ? P1 O1 Tb1 95.10(18) . . ? Tb1 O1 Tb1 108.46(14) 5_565 . ? P1 O2 Tb1 99.57(17) . . ? P2 O4 Tb1 97.77(16) . . ? P2 O5 Tb1 150.8(2) . 6_654 ? P2 O5 Tb1 97.77(19) . . ? Tb1 O5 Tb1 111.39(15) 6_654 . ? P3 O7 Tb1 137.4(2) . . ? P3 O8 Tb1 138.3(2) . 6_654 ? C28 O10 H10C 110.5 . . ? H1WA O1W H1WB 104.1 . . ? H2WA O2W H2WB 125.5 . . ? N1 C1 P1 113.5(3) . . ? N1 C1 H1A 108.9 . . ? P1 C1 H1A 108.9 . . ? N1 C1 H1B 108.9 . . ? P1 C1 H1B 108.9 . . ? H1A C1 H1B 107.7 . . ? N1 C2 C4 112.2(4) . . ? N1 C2 C3 106.1(4) . . ? C4 C2 C3 114.9(5) . . ? N1 C2 H2 107.8 . . ? C4 C2 H2 107.8 . . ? C3 C2 H2 107.8 . . ? C2 C3 H3A 109.5 . . ? C2 C3 H3B 109.5 . . ? H3A C3 H3B 109.5 . . ? C2 C3 H3C 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? C5 C4 C2 115.8(5) . . ? C5 C4 C9 109.7(5) . . ? C2 C4 C9 109.0(4) . . ? C5 C4 H4 107.3 . . ? C2 C4 H4 107.3 . . ? C9 C4 H4 107.3 . . ? C4 C5 C6 111.2(5) . . ? C4 C5 H5A 109.4 . . ? C6 C5 H5A 109.4 . . ? C4 C5 H5B 109.4 . . ? C6 C5 H5B 109.4 . . ? H5A C5 H5B 108.0 . . ? C7 C6 C5 112.6(6) . . ? C7 C6 H6A 109.1 . . ? C5 C6 H6A 109.1 . . ? C7 C6 H6B 109.1 . . ? C5 C6 H6B 109.1 . . ? H6A C6 H6B 107.8 . . ? C6 C7 C8 109.6(6) . . ? C6 C7 H7A 109.8 . . ? C8 C7 H7A 109.8 . . ? C6 C7 H7B 109.8 . . ? C8 C7 H7B 109.8 . . ? H7A C7 H7B 108.2 . . ? C9 C8 C7 110.4(6) . . ? C9 C8 H8A 109.6 . . ? C7 C8 H8A 109.6 . . ? C9 C8 H8B 109.6 . . ? C7 C8 H8B 109.6 . . ? H8A C8 H8B 108.1 . . ? C8 C9 C4 111.5(5) . . ? C8 C9 H9A 109.3 . . ? C4 C9 H9A 109.3 . . ? C8 C9 H9B 109.3 . . ? C4 C9 H9B 109.3 . . ? H9A C9 H9B 108.0 . . ? N2 C10 P2 111.2(3) . . ? N2 C10 H10A 109.4 . . ? P2 C10 H10A 109.4 . . ? N2 C10 H10B 109.4 . . ? P2 C10 H10B 109.4 . . ? H10A C10 H10B 108.0 . . ? C12 C11 N2 110.0(4) . . ? C12 C11 C13 114.0(4) . . ? N2 C11 C13 109.0(4) . . ? C12 C11 H11 107.9 . . ? N2 C11 H11 107.9 . . ? C13 C11 H11 107.9 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C14 C13 C18 110.6(4) . . ? C14 C13 C11 110.2(4) . . ? C18 C13 C11 114.8(5) . . ? C14 C13 H13 107.0 . . ? C18 C13 H13 107.0 . . ? C11 C13 H13 107.0 . . ? C15 C14 C13 112.1(5) . . ? C15 C14 H14A 109.2 . . ? C13 C14 H14A 109.2 . . ? C15 C14 H14B 109.2 . . ? C13 C14 H14B 109.2 . . ? H14A C14 H14B 107.9 . . ? C16 C15 C14 112.0(6) . . ? C16 C15 H15A 109.2 . . ? C14 C15 H15A 109.2 . . ? C16 C15 H15B 109.2 . . ? C14 C15 H15B 109.2 . . ? H15A C15 H15B 107.9 . . ? C15 C16 C17 111.5(5) . . ? C15 C16 H16A 109.3 . . ? C17 C16 H16A 109.3 . . ? C15 C16 H16B 109.3 . . ? C17 C16 H16B 109.3 . . ? H16A C16 H16B 108.0 . . ? C18 C17 C16 111.5(5) . . ? C18 C17 H17A 109.3 . . ? C16 C17 H17A 109.3 . . ? C18 C17 H17B 109.3 . . ? C16 C17 H17B 109.3 . . ? H17A C17 H17B 108.0 . . ? C13 C18 C17 110.2(5) . . ? C13 C18 H18A 109.6 . . ? C17 C18 H18A 109.6 . . ? C13 C18 H18B 109.6 . . ? C17 C18 H18B 109.6 . . ? H18A C18 H18B 108.1 . . ? N3 C19 P3 116.8(3) . . ? N3 C19 H19A 108.1 . . ? P3 C19 H19A 108.1 . . ? N3 C19 H19B 108.1 . . ? P3 C19 H19B 108.1 . . ? H19A C19 H19B 107.3 . . ? C21 C20 N3 108.9(4) . . ? C21 C20 C22 109.9(5) . . ? N3 C20 C22 114.0(5) . . ? C21 C20 H20 108.0 . . ? N3 C20 H20 108.0 . . ? C22 C20 H20 108.0 . . ? C20 C21 H21A 109.5 . . ? C20 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C20 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C27 C22 C23 109.2(7) . . ? C27 C22 C20 112.7(6) . . ? C23 C22 C20 110.0(7) . . ? C27 C22 H22 108.3 . . ? C23 C22 H22 108.3 . . ? C20 C22 H22 108.3 . . ? C22 C23 C24 112.2(8) . . ? C22 C23 H23A 109.2 . . ? C24 C23 H23A 109.2 . . ? C22 C23 H23B 109.2 . . ? C24 C23 H23B 109.2 . . ? H23A C23 H23B 107.9 . . ? C25 C24 C23 108.4(8) . . ? C25 C24 H24A 110.0 . . ? C23 C24 H24A 110.0 . . ? C25 C24 H24B 110.0 . . ? C23 C24 H24B 110.0 . . ? H24A C24 H24B 108.4 . . ? C26 C25 C24 113.4(8) . . ? C26 C25 H25A 108.9 . . ? C24 C25 H25A 108.9 . . ? C26 C25 H25B 108.9 . . ? C24 C25 H25B 108.9 . . ? H25A C25 H25B 107.7 . . ? C25 C26 C27 105.5(9) . . ? C25 C26 H26A 110.6 . . ? C27 C26 H26A 110.6 . . ? C25 C26 H26B 110.6 . . ? C27 C26 H26B 110.6 . . ? H26A C26 H26B 108.8 . . ? C22 C27 C26 111.8(7) . . ? C22 C27 H27A 109.3 . . ? C26 C27 H27A 109.3 . . ? C22 C27 H27B 109.3 . . ? C26 C27 H27B 109.3 . . ? H27A C27 H27B 107.9 . . ? O11 C28 O10 123.4(6) . . ? O11 C28 C29 123.7(7) . . ? O10 C28 C29 112.9(6) . . ? C28 C29 H29A 109.5 . . ? C28 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C28 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C1 N1 C2 115.7(4) . . ? C1 N1 H1C 108.4 . . ? C2 N1 H1C 108.4 . . ? C1 N1 H1D 108.4 . . ? C2 N1 H1D 108.4 . . ? H1C N1 H1D 107.4 . . ? C10 N2 C11 113.4(4) . . ? C10 N2 H2A 108.9 . . ? C11 N2 H2A 108.9 . . ? C10 N2 H2B 108.9 . . ? C11 N2 H2B 108.9 . . ? H2A N2 H2B 107.7 . . ? C19 N3 C20 114.4(4) . . ? C19 N3 H3D 108.7 . . ? C20 N3 H3D 108.7 . . ? C19 N3 H3E 108.7 . . ? C20 N3 H3E 108.7 . . ? H3D N3 H3E 107.6 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Tb1 O7 2.271(4) . ? Tb1 O5 2.313(4) 5_565 ? Tb1 O8 2.328(4) 5_565 ? Tb1 O1 2.347(4) 6_654 ? Tb1 O2 2.413(3) . ? Tb1 O4 2.465(3) . ? Tb1 O5 2.466(4) . ? Tb1 O1 2.518(4) . ? Tb1 Tb1 3.94884(18) 6_654 ? Tb1 Tb1 3.94892(15) 5_565 ? P1 O3 1.505(4) . ? P1 O2 1.522(4) . ? P1 O1 1.528(4) . ? P1 C1 1.827(5) . ? P2 O6 1.497(4) . ? P2 O5 1.525(4) . ? P2 O4 1.527(4) . ? P2 C10 1.827(5) . ? P3 O9 1.512(4) . ? P3 O8 1.519(4) . ? P3 O7 1.520(4) . ? P3 C19 1.827(6) . ? O10 C28 1.291(8) . ? O10 H10C 0.8829 . ? O11 C28 1.197(8) . ? O1W H1WA 0.9492 . ? O1W H1WB 0.9493 . ? O2W H2WA 0.9495 . ? O2W H2WB 0.9579 . ? C1 N1 1.485(6) . ? C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? C2 N1 1.522(6) . ? C2 C4 1.525(7) . ? C2 C3 1.525(7) . ? C2 H2 1.0000 . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 H3C 0.9800 . ? C4 C5 1.514(8) . ? C4 C9 1.533(7) . ? C4 H4 1.0000 . ? C5 C6 1.545(8) . ? C5 H5A 0.9900 . ? C5 H5B 0.9900 . ? C6 C7 1.499(11) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C8 1.533(11) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C8 C9 1.526(8) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C10 N2 1.490(6) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C11 C12 1.503(8) . ? C11 N2 1.519(6) . ? C11 C13 1.540(7) . ? C11 H11 1.0000 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C14 1.523(7) . ? C13 C18 1.527(8) . ? C13 H13 1.0000 . ? C14 C15 1.511(8) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 C16 1.502(10) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C16 C17 1.529(8) . ? C16 H16A 0.9900 . ? C16 H16B 0.9900 . ? C17 C18 1.529(8) . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C19 N3 1.477(7) . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C20 C21 1.521(9) . ? C20 N3 1.521(7) . ? C20 C22 1.549(9) . ? C20 H20 1.0000 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 C27 1.426(12) . ? C22 C23 1.522(10) . ? C22 H22 1.0000 . ? C23 C24 1.559(13) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C24 C25 1.477(13) . ? C24 H24A 0.9900 . ? C24 H24B 0.9900 . ? C25 C26 1.475(13) . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C26 C27 1.629(12) . ? C26 H26A 0.9900 . ? C26 H26B 0.9900 . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C28 C29 1.505(9) . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? N1 H1C 0.9100 . ? N1 H1D 0.9100 . ? N2 H2A 0.9100 . ? N2 H2B 0.9100 . ? N3 H3D 0.9100 . ? N3 H3E 0.9100 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag O10 H10C O9 0.88 1.64 2.511(6) 167.3 . yes O1W H1WA O6 0.95 1.86 2.775(9) 160.3 . yes O2W H2WA O3 0.95 2.31 2.786(5) 110.4 . yes O2W H2WB O2 0.96 1.96 2.869(5) 156.7 5_565 yes N1 H1D O3 0.91 1.75 2.657(6) 171.8 6_654 yes N1 H1C O8 0.91 2.28 3.147(5) 158.9 5_565 yes N2 H2A O2W 0.91 2.02 2.910(6) 165.0 . yes N2 H2B O4 0.91 1.92 2.732(6) 148.4 6_654 yes N3 H3D O6 0.91 1.96 2.838(6) 161.6 . yes N3 H3E O9 0.91 2.40 3.120(6) 136.1 6_654 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O3 P1 O1 Tb1 12.7(5) . . . 5_565 ? O2 P1 O1 Tb1 141.9(4) . . . 5_565 ? C1 P1 O1 Tb1 -102.0(5) . . . 5_565 ? O3 P1 O1 Tb1 -134.05(18) . . . . ? O2 P1 O1 Tb1 -4.79(19) . . . . ? C1 P1 O1 Tb1 111.3(2) . . . . ? O3 P1 O2 Tb1 134.31(18) . . . . ? O1 P1 O2 Tb1 5.0(2) . . . . ? C1 P1 O2 Tb1 -108.1(2) . . . . ? O6 P2 O4 Tb1 -117.21(19) . . . . ? O5 P2 O4 Tb1 11.29(19) . . . . ? C10 P2 O4 Tb1 124.05(18) . . . . ? O6 P2 O5 Tb1 -62.2(5) . . . 6_654 ? O4 P2 O5 Tb1 168.8(4) . . . 6_654 ? C10 P2 O5 Tb1 55.9(4) . . . 6_654 ? O6 P2 O5 Tb1 117.7(2) . . . . ? O4 P2 O5 Tb1 -11.28(18) . . . . ? C10 P2 O5 Tb1 -124.18(19) . . . . ? O9 P3 O7 Tb1 -112.7(3) . . . . ? O8 P3 O7 Tb1 15.6(5) . . . . ? C19 P3 O7 Tb1 133.8(3) . . . . ? O9 P3 O8 Tb1 145.7(3) . . . 6_654 ? O7 P3 O8 Tb1 18.8(4) . . . 6_654 ? C19 P3 O8 Tb1 -99.8(4) . . . 6_654 ? O3 P1 C1 N1 177.5(4) . . . . ? O2 P1 C1 N1 53.2(4) . . . . ? O1 P1 C1 N1 -60.3(4) . . . . ? N1 C2 C4 C5 61.4(6) . . . . ? C3 C2 C4 C5 -59.8(6) . . . . ? N1 C2 C4 C9 -174.3(5) . . . . ? C3 C2 C4 C9 64.4(7) . . . . ? C2 C4 C5 C6 178.1(5) . . . . ? C9 C4 C5 C6 54.3(7) . . . . ? C4 C5 C6 C7 -55.7(9) . . . . ? C5 C6 C7 C8 56.0(9) . . . . ? C6 C7 C8 C9 -57.2(8) . . . . ? C7 C8 C9 C4 58.5(8) . . . . ? C5 C4 C9 C8 -56.9(7) . . . . ? C2 C4 C9 C8 175.4(6) . . . . ? O6 P2 C10 N2 -177.8(4) . . . . ? O5 P2 C10 N2 58.3(4) . . . . ? O4 P2 C10 N2 -52.9(4) . . . . ? C12 C11 C13 C14 65.9(7) . . . . ? N2 C11 C13 C14 -170.8(5) . . . . ? C12 C11 C13 C18 -59.7(6) . . . . ? N2 C11 C13 C18 63.6(6) . . . . ? C18 C13 C14 C15 -55.7(7) . . . . ? C11 C13 C14 C15 176.3(5) . . . . ? C13 C14 C15 C16 54.4(7) . . . . ? C14 C15 C16 C17 -53.4(8) . . . . ? C15 C16 C17 C18 54.8(8) . . . . ? C14 C13 C18 C17 56.3(6) . . . . ? C11 C13 C18 C17 -178.3(4) . . . . ? C16 C17 C18 C13 -56.1(7) . . . . ? O9 P3 C19 N3 164.5(4) . . . . ? O8 P3 C19 N3 44.7(5) . . . . ? O7 P3 C19 N3 -78.6(5) . . . . ? C21 C20 C22 C27 179.7(7) . . . . ? N3 C20 C22 C27 -57.8(8) . . . . ? C21 C20 C22 C23 57.6(8) . . . . ? N3 C20 C22 C23 -179.9(6) . . . . ? C27 C22 C23 C24 56.7(10) . . . . ? C20 C22 C23 C24 -179.2(7) . . . . ? C22 C23 C24 C25 -54.8(11) . . . . ? C23 C24 C25 C26 59.5(13) . . . . ? C24 C25 C26 C27 -60.2(13) . . . . ? C23 C22 C27 C26 -59.0(11) . . . . ? C20 C22 C27 C26 178.5(7) . . . . ? C25 C26 C27 C22 60.6(12) . . . . ? P1 C1 N1 C2 164.9(4) . . . . ? C4 C2 N1 C1 52.0(6) . . . . ? C3 C2 N1 C1 178.2(5) . . . . ? P2 C10 N2 C11 179.0(4) . . . . ? C12 C11 N2 C10 -73.1(6) . . . . ? C13 C11 N2 C10 161.1(4) . . . . ? P3 C19 N3 C20 -173.0(4) . . . . ? C21 C20 N3 C19 54.6(7) . . . . ? C22 C20 N3 C19 -68.4(7) . . . . ?