#------------------------------------------------------------------------------ #$Date: 2021-08-19 01:11:09 +0300 (Thu, 19 Aug 2021) $ #$Revision: 268125 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/43/1564371.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564371 loop_ _publ_author_name 'Weng, Guo-Guo' 'Hong, Ben-Kun' 'Bao, Song-Song' 'Wen, Yujie' 'Wu, Lan-Qing' 'Huang, Xin-Da' 'Jia, Jia-Ge' 'Wen, Ge-Hua' 'Li, Shuhua' 'Peng, Luming' 'Zheng, Li-Min' _publ_section_title ; From helix to superhelix: hierarchical assembly of homochiral van der Waals 1D coordination polymers ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC01913A _journal_year 2021 _chemical_absolute_configuration rm _chemical_formula_moiety 'C27 H57 N3 O9 P3 Tb, C2 H4 O2, 2(H2 O)' _chemical_formula_sum 'C29 H65 N3 O13 P3 Tb' _chemical_formula_weight 915.67 _space_group_crystal_system hexagonal _space_group_IT_number 169 _space_group_name_Hall 'P 61' _space_group_name_H-M_alt 'P 61' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2021-07-02 deposited with the CCDC. 2021-08-13 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 17.0310(6) _cell_length_b 17.0310(6) _cell_length_c 23.5742(12) _cell_measurement_reflns_used 9714 _cell_measurement_temperature 193(2) _cell_measurement_theta_max 60.627 _cell_measurement_theta_min 3.07 _cell_volume 5921.7(4) _computing_cell_refinement 'SAINT V8.40A (Bruker Nano, Inc., 2019)' _computing_data_collection 'APEX 3' _computing_data_reduction 'SAINT V8.40A (Bruker Nano, Inc., 2019)' _computing_molecular_graphics SHELXTL _computing_publication_material SHELXTL _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 193(2) _diffrn_detector_area_resol_mean 4K _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker D8 with Metal-jet' _diffrn_measurement_method CCD _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0804 _diffrn_reflns_av_unetI/netI 0.0496 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 57328 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 60.646 _diffrn_reflns_theta_min 3.075 _exptl_absorpt_coefficient_mu 10.389 _exptl_absorpt_correction_T_max 0.7519 _exptl_absorpt_correction_T_min 0.3540 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.541 _exptl_crystal_description rod-like _exptl_crystal_F_000 2844 _exptl_crystal_size_max 0.300 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.100 _refine_diff_density_max 1.009 _refine_diff_density_min -0.612 _refine_diff_density_rms 0.103 _refine_ls_abs_structure_details ; Flack x determined using 3864 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.009(3) _refine_ls_extinction_coef 0.00063(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 456 _refine_ls_number_reflns 9006 _refine_ls_number_restraints 37 _refine_ls_restrained_S_all 1.036 _refine_ls_R_factor_all 0.0395 _refine_ls_R_factor_gt 0.0368 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0525P)^2^+4.6663P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0889 _refine_ls_wR_factor_ref 0.0907 _reflns_Friedel_coverage 0.942 _reflns_Friedel_fraction_full 0.996 _reflns_Friedel_fraction_max 0.989 _reflns_number_gt 8579 _reflns_number_total 9006 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc01913a2.cif _cod_data_source_block 1 _cod_original_cell_volume 5921.7(5) _cod_database_code 1564371 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.147 _shelx_estimated_absorpt_t_max 0.423 _shelx_res_file ; TITL 11 in P6(1) 1.res created by SHELXL-2018/3 at 10:35:19 on 01-Jul-2021 CELL 1.34139 17.03100 17.03100 23.57420 90.0000 90.0000 120.0000 ZERR 6.00 0.00057 0.00057 0.00120 0.0000 0.0000 0.0000 LATT -1 SYMM -Y, X-Y, 0.33333+Z SYMM -X+Y, -X, 0.66667+Z SYMM -X, -Y, 0.5+Z SYMM Y, -X+Y, 0.83333+Z SYMM X-Y, X, 0.16667+Z SFAC C H N O P Tb UNIT 174 390 18 78 18 6 OMIT -3 5 -14 OMIT -3 4 -15 OMIT 0 1 -16 L.S. 10 ACTA BOND $H FMAP 2 PLAN 5 HTAB O10 O9 HTAB O1W O6 HTAB O2W O3 HTAB O2W O2_$1 HTAB N1 O3_$2 HTAB N1 O8_$1 HTAB N2 O4_$2 HTAB N2 O2W HTAB N3 O9_$2 HTAB N3 O6 EQIV $1 y, -x+y, z-1/6 EQIV $2 x-y, x, z+1/6 CONF FREE Tb1 P2 FREE Tb1 P1 SIMU 0.01 0.02 N2 C10 C11 SIMU 0.01 0.02 C23 C24 C25 C26 C27 SIMU 0.01 0.02 O1 O2 O3 SIZE 0.3 0.15 0.1 TEMP -80.170 WGHT 0.052500 4.666300 EXTI 0.000631 FVAR 0.08078 TB1 6 0.000305 0.027561 0.001022 11.00000 0.01255 0.01322 = 0.01358 0.00030 0.00007 0.00705 P1 5 0.130018 -0.033944 -0.043696 11.00000 0.01312 0.01399 = 0.01577 -0.00077 -0.00074 0.00742 P2 5 -0.168988 -0.140726 0.047298 11.00000 0.01259 0.01359 = 0.01637 -0.00097 -0.00160 0.00599 P3 5 -0.099633 0.129249 0.082829 11.00000 0.01836 0.02114 = 0.01723 0.00190 0.00120 0.01352 O1 4 0.087331 0.010142 -0.079622 11.00000 0.01672 0.01673 = 0.01920 0.00245 -0.00297 0.01068 O2 4 0.088279 -0.046620 0.015103 11.00000 0.01740 0.02146 = 0.01393 -0.00062 -0.00132 0.01147 O3 4 0.126446 -0.116490 -0.068858 11.00000 0.02168 0.01675 = 0.02284 -0.00247 -0.00318 0.01141 O4 4 -0.133470 -0.124373 -0.013432 11.00000 0.02470 0.01565 = 0.01379 0.00038 -0.00265 0.01110 O5 4 -0.092390 -0.064807 0.081614 11.00000 0.01668 0.01763 = 0.01493 0.00168 0.00012 0.00660 O6 4 -0.260728 -0.151114 0.055405 11.00000 0.01631 0.02276 = 0.02697 -0.00037 -0.00128 0.00894 O7 4 -0.084627 0.090025 0.028996 11.00000 0.02925 0.03768 = 0.01733 0.00140 0.00038 0.02611 O8 4 -0.066394 0.106152 0.136833 11.00000 0.03103 0.02788 = 0.01571 0.00449 0.00221 0.02144 O9 4 -0.062546 0.229707 0.075812 11.00000 0.02943 0.02161 = 0.03255 0.00486 0.00228 0.01405 AFIX 6 O10 4 -0.132504 0.325603 0.099165 11.00000 0.06131 0.04921 = 0.05091 0.01475 0.01778 0.04311 H10C 2 -0.120651 0.281787 0.091481 11.00000 -1.50000 AFIX 0 O11 4 -0.175928 0.256647 0.181816 11.00000 0.10281 0.07030 = 0.04728 0.01429 0.02518 0.06099 AFIX 6 O1W 4 -0.396726 -0.296372 0.114269 11.00000 0.07238 0.08903 = 0.16426 0.05833 0.02799 0.01821 H1WA 2 -0.364820 -0.241539 0.093345 11.00000 -1.50000 H1WB 2 -0.455212 -0.326509 0.097362 11.00000 -1.50000 AFIX 6 O2W 4 -0.056206 -0.247821 -0.058483 11.00000 0.02274 0.02739 = 0.02770 0.00555 -0.00061 0.01227 H2WA 2 0.006430 -0.228365 -0.062318 11.00000 -1.50000 H2WB 2 -0.087854 -0.222683 -0.077360 11.00000 -1.50000 AFIX 0 C1 1 0.250526 0.049553 -0.040419 11.00000 0.01841 0.02170 = 0.02565 -0.00443 -0.00029 0.01077 AFIX 23 H1A 2 0.281963 0.023742 -0.018588 11.00000 -1.20000 H1B 2 0.275572 0.061818 -0.079380 11.00000 -1.20000 AFIX 0 C2 1 0.365353 0.216750 -0.023588 11.00000 0.01690 0.01351 = 0.02569 0.00597 0.00520 0.00553 AFIX 13 H2 2 0.371725 0.231629 -0.064966 11.00000 -1.20000 AFIX 0 C3 1 0.369916 0.296948 0.008497 11.00000 0.02372 0.02042 = 0.04643 -0.00041 -0.00113 0.01111 AFIX 137 H3A 2 0.316955 0.302529 -0.001182 11.00000 -1.50000 H3B 2 0.425349 0.352744 -0.002169 11.00000 -1.50000 H3C 2 0.370368 0.286975 0.049409 11.00000 -1.50000 AFIX 0 C4 1 0.439003 0.193933 -0.007552 11.00000 0.01593 0.01787 = 0.02940 0.00118 0.00285 0.00549 AFIX 13 H4 2 0.428589 0.140660 -0.031027 11.00000 -1.20000 AFIX 0 C5 1 0.440494 0.169110 0.053967 11.00000 0.02959 0.04490 = 0.03906 0.00799 0.00433 0.02554 AFIX 23 H5A 2 0.382067 0.114491 0.063477 11.00000 -1.20000 H5B 2 0.447319 0.219312 0.078518 11.00000 -1.20000 AFIX 0 C6 1 0.518486 0.150431 0.066009 11.00000 0.04218 0.06370 = 0.05083 0.01167 0.00023 0.03956 AFIX 23 H6A 2 0.519515 0.138453 0.107018 11.00000 -1.20000 H6B 2 0.507513 0.095486 0.045039 11.00000 -1.20000 AFIX 0 C7 1 0.609404 0.228990 0.048814 11.00000 0.03465 0.07392 = 0.06943 -0.01328 -0.01721 0.03521 AFIX 23 H7A 2 0.657221 0.212946 0.054774 11.00000 -1.20000 H7B 2 0.623948 0.282541 0.072541 11.00000 -1.20000 AFIX 0 C8 1 0.606760 0.251526 -0.013559 11.00000 0.01752 0.04540 = 0.07381 0.00913 0.00998 0.01144 AFIX 23 H8A 2 0.665898 0.304078 -0.024464 11.00000 -1.20000 H8B 2 0.596387 0.199240 -0.037301 11.00000 -1.20000 AFIX 0 C9 1 0.531731 0.273628 -0.024394 11.00000 0.01753 0.02984 = 0.05055 0.00652 0.00651 0.00613 AFIX 23 H9A 2 0.531067 0.287528 -0.065108 11.00000 -1.20000 H9B 2 0.543925 0.327979 -0.002254 11.00000 -1.20000 AFIX 0 C10 1 -0.177317 -0.246547 0.071240 11.00000 0.01568 0.01607 = 0.02244 0.00655 0.00322 0.00557 AFIX 23 H10A 2 -0.193485 -0.255533 0.111993 11.00000 -1.20000 H10B 2 -0.226188 -0.297857 0.049986 11.00000 -1.20000 AFIX 0 C11 1 -0.093716 -0.332926 0.080646 11.00000 0.02306 0.01376 = 0.02825 0.00205 0.00120 0.00997 AFIX 13 H11 2 -0.125920 -0.351596 0.117928 11.00000 -1.20000 AFIX 0 C12 1 -0.148070 -0.407238 0.038564 11.00000 0.03169 0.01834 = 0.03494 -0.00451 -0.00765 0.01142 AFIX 137 H12A 2 -0.118328 -0.390550 0.001414 11.00000 -1.50000 H12B 2 -0.209200 -0.415665 0.035479 11.00000 -1.50000 H12C 2 -0.152025 -0.463823 0.051436 11.00000 -1.50000 AFIX 0 C13 1 0.003637 -0.314639 0.089953 11.00000 0.02892 0.01910 = 0.02142 -0.00192 -0.00306 0.01579 AFIX 13 H13 2 0.033215 -0.263555 0.117691 11.00000 -1.20000 AFIX 0 C14 1 0.000734 -0.396875 0.117520 11.00000 0.03622 0.02401 = 0.04804 0.00823 -0.00023 0.01908 AFIX 23 H14A 2 -0.029971 -0.449578 0.091704 11.00000 -1.20000 H14B 2 -0.034930 -0.411825 0.153035 11.00000 -1.20000 AFIX 0 C15 1 0.095677 -0.379431 0.130805 11.00000 0.04346 0.02829 = 0.05771 0.00705 -0.01083 0.02408 AFIX 23 H15A 2 0.123163 -0.332209 0.160519 11.00000 -1.20000 H15B 2 0.091446 -0.435654 0.145925 11.00000 -1.20000 AFIX 0 C16 1 0.156326 -0.349031 0.078971 11.00000 0.03464 0.03410 = 0.06965 -0.00593 -0.01097 0.02557 AFIX 23 H16A 2 0.133654 -0.399364 0.051246 11.00000 -1.20000 H16B 2 0.218512 -0.333434 0.090130 11.00000 -1.20000 AFIX 0 C17 1 0.158774 -0.266330 0.051178 11.00000 0.02582 0.02805 = 0.04134 -0.00147 -0.00008 0.01342 AFIX 23 H17A 2 0.187827 -0.213969 0.077371 11.00000 -1.20000 H17B 2 0.195642 -0.250265 0.016127 11.00000 -1.20000 AFIX 0 C18 1 0.063125 -0.285684 0.036647 11.00000 0.02774 0.03170 = 0.02606 -0.00062 0.00025 0.01628 AFIX 23 H18A 2 0.035923 -0.334443 0.007858 11.00000 -1.20000 H18B 2 0.066252 -0.230575 0.020420 11.00000 -1.20000 AFIX 0 C19 1 -0.221717 0.082032 0.090286 11.00000 0.02485 0.02302 = 0.03608 0.00539 0.00410 0.01613 AFIX 23 H19A 2 -0.232055 0.122916 0.115082 11.00000 -1.20000 H19B 2 -0.246824 0.082419 0.052479 11.00000 -1.20000 AFIX 0 C20 1 -0.372768 -0.042602 0.126587 11.00000 0.01899 0.02581 = 0.03390 0.00138 -0.00052 0.00762 AFIX 13 H20 2 -0.398853 -0.102268 0.146550 11.00000 -1.20000 AFIX 0 C21 1 -0.378375 0.023857 0.166940 11.00000 0.03393 0.03849 = 0.04501 0.00554 0.00541 0.02435 AFIX 137 H21A 2 -0.332693 0.040791 0.196823 11.00000 -1.50000 H21B 2 -0.438881 -0.004508 0.184064 11.00000 -1.50000 H21C 2 -0.367174 0.078202 0.145989 11.00000 -1.50000 AFIX 0 C22 1 -0.431266 -0.056570 0.073332 11.00000 0.02266 0.04262 = 0.04418 -0.00210 -0.00468 0.01032 AFIX 13 H22 2 -0.406091 0.003384 0.053831 11.00000 -1.20000 AFIX 0 C23 1 -0.528947 -0.087827 0.088457 11.00000 0.02329 0.06541 = 0.09038 -0.01623 -0.00364 0.01245 AFIX 23 H23A 2 -0.553778 -0.145310 0.109954 11.00000 -1.20000 H23B 2 -0.530320 -0.042161 0.113785 11.00000 -1.20000 AFIX 0 C24 1 -0.589567 -0.102454 0.038430 11.00000 0.03077 0.08145 = 0.11651 -0.03763 -0.02157 0.02635 AFIX 23 H24A 2 -0.653010 -0.128187 0.051441 11.00000 -1.20000 H24B 2 -0.571006 -0.043724 0.019655 11.00000 -1.20000 AFIX 0 C25 1 -0.583323 -0.166171 -0.002963 11.00000 0.04635 0.08321 = 0.11559 -0.05278 -0.03287 0.03887 AFIX 23 H25A 2 -0.608173 -0.226628 0.014862 11.00000 -1.20000 H25B 2 -0.620863 -0.172748 -0.036643 11.00000 -1.20000 AFIX 0 C26 1 -0.489108 -0.134245 -0.021315 11.00000 0.05861 0.10338 = 0.08182 -0.04271 -0.03846 0.05028 AFIX 23 H26A 2 -0.465083 -0.075854 -0.041687 11.00000 -1.20000 H26B 2 -0.487703 -0.178958 -0.047512 11.00000 -1.20000 AFIX 0 C27 1 -0.428959 -0.121767 0.031985 11.00000 0.04186 0.08939 = 0.06667 -0.02559 -0.01490 0.04702 AFIX 23 H27A 2 -0.451017 -0.181177 0.050732 11.00000 -1.20000 H27B 2 -0.365622 -0.099276 0.019764 11.00000 -1.20000 AFIX 0 C28 1 -0.170093 0.312513 0.148210 11.00000 0.03958 0.03109 = 0.04284 0.00311 0.00077 0.01555 C29 1 -0.210315 0.372769 0.158930 11.00000 0.05893 0.04523 = 0.06492 -0.00100 0.01156 0.03452 AFIX 137 H29A 2 -0.270192 0.337077 0.176465 11.00000 -1.50000 H29B 2 -0.216321 0.397930 0.122874 11.00000 -1.50000 H29C 2 -0.170486 0.422329 0.184396 11.00000 -1.50000 AFIX 0 N1 3 0.269921 0.136644 -0.013794 11.00000 0.01414 0.01675 = 0.02215 -0.00158 0.00023 0.00694 AFIX 23 H1C 2 0.260738 0.127707 0.024248 11.00000 -1.20000 H1D 2 0.229185 0.151813 -0.027263 11.00000 -1.20000 AFIX 0 N2 3 -0.090502 -0.246035 0.062695 11.00000 0.01616 0.01404 = 0.02363 0.00110 0.00051 0.00748 AFIX 23 H2A 2 -0.046129 -0.199128 0.082704 11.00000 -1.20000 H2B 2 -0.075258 -0.236008 0.025330 11.00000 -1.20000 AFIX 0 N3 3 -0.274081 -0.011418 0.113692 11.00000 0.02040 0.02034 = 0.02439 -0.00024 -0.00165 0.01192 AFIX 23 H3D 2 -0.246717 -0.014228 0.146173 11.00000 -1.20000 H3E 2 -0.271847 -0.050631 0.088409 11.00000 -1.20000 AFIX 0 HKLF 4 REM 11 in P6(1) REM wR2 = 0.0907, GooF = S = 1.035, Restrained GooF = 1.036 for all data REM R1 = 0.0368 for 8579 Fo > 4sig(Fo) and 0.0395 for all 9006 data REM 456 parameters refined using 37 restraints END WGHT 0.0523 4.7212 REM Highest difference peak 1.009, deepest hole -0.612, 1-sigma level 0.103 Q1 1 -0.0607 -0.0382 -0.0004 11.00000 0.05 1.01 Q2 1 0.0678 0.0303 0.0015 11.00000 0.05 0.99 Q3 1 0.0004 0.0355 0.0489 11.00000 0.05 0.89 Q4 1 -0.0059 0.0885 -0.0005 11.00000 0.05 0.89 Q5 1 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8.75 12 -8 0 49.94 4.74 4 -12 0 55.89 5.04 12 -8 0 51.11 4.68 8 4 0 49.61 5.01 4 -12 0 51.79 4.32 -12 8 0 45.93 4.32 -8 -4 0 48.56 4.64 4 -12 0 50.37 4.32 8 4 0 48.29 5.14 -4 12 0 41.75 5.32 8 4 0 55.51 4.86 -9 -3 0 3.07 0.76 9 3 0 3.89 1.23 3 -12 0 3.33 0.50 -3 12 0 3.50 1.51 3 -12 0 4.88 1.32 9 3 0 5.43 1.58 9 3 0 3.00 0.74 12 -9 0 4.23 0.82 12 -9 0 4.55 1.02 10 2 0 0.73 0.94 -2 12 0 2.61 1.49 2 -12 0 0.37 0.30 2 -12 0 1.48 1.06 10 2 0 -0.58 1.17 12 -10 0 0.68 0.53 -10 -2 0 0.40 0.54 12 -10 0 1.33 0.82 -1 12 0 1.66 1.46 1 -12 0 0.97 1.03 12 -11 0 0.82 0.87 11 1 0 0.80 0.96 0 -12 0 6.60 0.99 12 0 0 11.61 1.79 0 12 0 5.14 2.09 0 -12 0 9.10 1.71 12 0 0 8.94 2.08 12 -12 0 8.70 1.40 12 -13 0 13.23 1.94 13 -1 0 11.11 1.99 -1 -12 0 13.48 2.05 1 12 0 13.06 2.85 13 -1 0 10.81 2.34 -2 -11 0 36.20 3.73 13 -2 0 41.22 4.25 13 -2 0 34.63 3.75 -2 -11 0 33.14 3.33 11 -13 0 39.35 3.64 2 11 0 41.33 4.68 -13 2 0 30.84 3.31 -13 3 0 63.82 6.61 13 -3 0 76.96 6.89 3 10 0 75.85 6.68 -3 -10 0 73.26 6.72 3 10 0 68.68 7.49 13 -3 0 73.80 7.08 10 -13 0 72.95 6.65 -13 4 0 2.44 0.55 13 -4 0 3.75 1.39 -9 13 0 4.21 1.45 4 9 0 3.27 1.80 4 9 0 4.76 1.11 13 -4 0 3.93 1.13 -4 -9 0 3.59 0.96 5 8 0 29.23 3.85 5 8 0 28.18 3.55 -8 13 0 33.14 3.79 -5 -8 0 30.10 3.04 5 8 0 36.73 3.37 13 -5 0 30.44 3.20 -5 -8 0 27.64 3.15 13 -5 0 31.96 3.37 -13 5 0 26.80 2.73 -7 13 0 1.92 1.22 6 7 0 3.73 1.25 -6 -7 0 2.17 0.65 13 -6 0 3.44 1.00 6 7 0 3.38 1.34 -13 6 0 2.54 0.45 6 7 0 5.11 1.57 -6 -7 0 1.59 0.75 13 -6 0 3.49 1.15 -13 7 0 13.60 1.36 -7 -6 0 13.05 1.69 -6 13 0 16.84 2.66 7 6 0 17.86 2.38 7 6 0 13.36 2.26 13 -7 0 16.77 2.00 7 6 0 15.78 2.40 13 -7 0 14.42 1.94 13 -8 0 43.53 4.18 8 5 0 37.02 4.40 8 5 0 44.96 4.58 13 -8 0 44.94 4.13 -8 -5 0 42.04 4.01 8 5 0 40.13 4.32 -5 13 0 44.25 4.94 13 -9 0 52.40 4.80 -9 -4 0 46.11 4.75 -4 13 0 42.40 5.57 13 -9 0 48.96 4.99 9 4 0 51.59 5.19 9 4 0 57.37 5.43 4 -13 0 58.64 5.25 9 4 0 52.92 4.86 10 3 0 43.99 4.79 13 -10 0 43.79 4.19 3 -13 0 55.55 5.09 13 -10 0 44.61 4.37 10 3 0 39.67 5.00 10 3 0 42.45 4.00 -3 13 0 48.10 5.34 13 -11 0 9.23 1.56 11 2 0 7.62 1.71 -2 13 0 11.13 2.63 11 2 0 12.40 2.37 2 -13 0 13.59 2.08 12 1 0 8.50 2.26 12 1 0 9.30 1.84 13 -12 0 9.59 1.56 -1 13 0 8.31 2.47 0 13 0 2.35 1.87 13 -13 0 2.53 1.13 13 0 0 3.66 1.33 13 0 0 0.36 1.48 1 13 0 2.11 1.90 14 -1 0 3.26 1.31 13 -14 0 2.49 1.15 14 -1 0 0.47 1.55 14 -2 0 24.39 3.44 2 12 0 24.86 3.88 12 -14 0 24.74 2.81 14 -2 0 24.08 3.04 3 11 0 25.80 4.15 14 -3 0 30.66 3.37 14 -3 0 27.29 3.71 11 -14 0 29.72 3.17 3 11 0 32.61 3.20 14 -4 0 1.38 1.02 -4 -10 0 -0.11 0.77 4 10 0 1.94 1.28 4 10 0 -0.90 0.69 4 10 0 0.42 1.58 14 -4 0 1.48 1.30 5 9 0 8.45 1.88 5 9 0 5.82 2.02 -14 5 0 5.59 0.84 -5 -9 0 6.69 1.25 14 -5 0 7.61 1.49 5 9 0 6.68 1.43 14 -5 0 8.43 1.71 -9 14 0 8.33 2.02 6 8 0 2.70 1.61 6 8 0 3.69 1.33 14 -6 0 2.80 1.08 -8 14 0 3.14 1.47 6 8 0 2.38 1.42 14 -6 0 2.86 1.22 7 7 0 1.82 1.35 -7 14 0 3.68 1.48 7 7 0 1.82 1.27 7 7 0 3.01 1.40 14 -7 0 1.89 1.02 -6 14 0 6.48 1.99 14 -8 0 5.02 1.20 8 6 0 1.93 1.48 14 -8 0 5.13 1.22 8 6 0 4.97 1.62 14 -9 0 1.30 0.84 9 5 0 1.11 0.89 9 5 0 0.65 1.22 9 5 0 2.22 1.40 14 -9 0 1.20 0.91 10 4 0 22.03 2.18 10 4 0 20.16 2.86 14 -10 0 20.81 2.33 10 4 0 19.69 3.03 14 -10 0 22.30 2.53 -4 14 0 19.41 3.38 11 3 0 1.50 1.56 14 -11 0 2.38 1.08 -3 14 0 3.68 1.88 11 3 0 2.29 1.34 14 -11 0 1.72 0.77 14 -12 0 23.32 2.59 12 2 0 21.17 3.37 12 2 0 20.42 2.86 -2 14 0 17.12 3.49 13 1 0 12.08 2.59 -1 14 0 9.29 2.75 13 1 0 11.71 2.20 14 -13 0 16.24 2.11 14 -14 0 12.04 1.89 14 0 0 12.81 2.20 0 14 0 10.33 2.84 14 0 0 11.36 2.49 14 -15 0 35.53 3.66 15 -1 0 31.66 3.90 15 -1 0 31.56 4.18 1 14 0 30.61 4.72 13 -15 0 11.53 1.81 15 -2 0 11.10 2.04 15 -2 0 9.70 2.37 2 13 0 10.97 2.74 3 12 0 10.32 2.72 15 -3 0 12.80 2.10 15 -3 0 17.19 2.73 4 11 0 36.07 3.44 4 11 0 30.11 3.98 4 11 0 29.74 4.33 15 -4 0 30.65 3.86 15 -4 0 31.60 3.62 5 10 0 1.46 0.95 5 10 0 0.53 1.44 15 -5 0 1.25 1.32 -10 15 0 1.14 1.17 5 10 0 0.05 1.52 15 -5 0 1.23 1.04 -9 15 0 12.65 2.51 6 9 0 10.55 2.40 15 -6 0 9.75 1.91 6 9 0 8.71 2.11 6 9 0 9.91 1.80 15 -6 0 9.29 1.75 7 8 0 2.63 1.53 7 8 0 3.64 1.34 15 -7 0 4.80 1.30 7 8 0 3.40 1.63 15 -7 0 3.69 1.34 8 7 0 2.50 1.47 -7 15 0 0.55 1.45 15 -8 0 2.69 1.12 15 -8 0 2.80 1.17 8 7 0 1.29 1.29 8 7 0 2.12 1.29 15 -9 0 1.91 1.03 -6 15 0 1.73 1.51 9 6 0 1.42 1.40 15 -9 0 2.01 0.95 9 6 0 0.50 0.99 9 6 0 -0.09 1.38 10 5 0 1.35 1.49 10 5 0 2.16 0.74 15 -10 0 2.99 1.11 10 5 0 1.16 1.40 15 -10 0 1.61 0.87 -5 15 0 3.51 1.77 11 4 0 2.64 1.69 15 -11 0 0.79 0.79 11 4 0 2.73 1.48 15 -11 0 1.67 1.07 -4 15 0 1.38 1.68 12 3 0 13.45 2.71 15 -12 0 15.28 2.13 -3 15 0 13.80 3.03 12 3 0 11.65 2.27 15 -13 0 5.21 1.40 -2 15 0 5.45 2.29 13 2 0 5.28 2.09 13 2 0 4.62 1.65 14 1 0 20.76 3.31 15 -14 0 18.53 2.52 -1 15 0 16.40 3.54 14 1 0 20.31 3.03 15 -15 0 24.24 2.87 15 0 0 20.54 3.14 15 0 0 20.82 3.44 0 15 0 24.97 4.14 15 -16 0 37.77 3.56 16 -1 0 31.64 4.19 16 -1 0 25.24 3.62 1 15 0 28.20 4.59 16 -2 0 43.31 4.89 2 14 0 37.36 5.39 16 -2 0 41.81 4.50 3 13 0 3.74 1.74 16 -3 0 3.87 1.88 3 13 0 5.39 2.35 16 -3 0 4.41 1.52 16 -4 0 0.92 1.46 4 12 0 0.58 1.77 4 12 0 1.51 1.56 16 -4 0 0.69 1.16 5 11 0 1.95 1.64 16 -5 0 4.67 1.35 5 11 0 2.67 1.00 5 11 0 2.72 1.84 16 -5 0 3.46 1.60 6 10 0 15.41 2.78 -10 16 0 12.32 2.59 16 -6 0 10.43 1.92 6 10 0 11.21 2.38 16 -6 0 13.40 2.28 6 10 0 12.57 1.94 7 9 0 25.79 3.50 -9 16 0 28.69 3.85 7 9 0 24.30 3.54 7 9 0 24.39 3.06 16 -7 0 25.09 3.03 16 -7 0 26.36 3.22 16 -8 0 20.60 2.86 16 -8 0 25.87 2.87 -8 16 0 21.81 3.65 8 8 0 26.02 3.12 8 8 0 21.43 3.12 8 8 0 23.18 3.36 16 -9 0 10.79 1.78 9 7 0 7.07 1.91 -7 16 0 11.21 2.58 16 -9 0 10.94 1.73 9 7 0 9.47 2.16 9 7 0 7.98 1.64 16 -10 0 19.92 2.37 10 6 0 18.36 2.19 10 6 0 18.00 2.98 16 -10 0 22.59 2.66 10 6 0 20.77 3.08 -6 16 0 19.03 3.55 11 5 0 27.31 3.63 -5 16 0 27.90 4.23 16 -11 0 27.13 2.94 11 5 0 29.23 3.77 16 -11 0 27.98 3.18 16 -12 0 37.81 3.86 -4 16 0 32.43 4.78 12 4 0 32.78 4.13 12 4 0 37.08 4.38 13 3 0 15.78 2.81 13 3 0 11.74 2.23 -3 16 0 8.70 2.70 16 -13 0 11.50 1.88 -2 16 0 20.19 3.73 14 2 0 15.70 3.03 16 -14 0 18.52 2.50 14 2 0 15.59 2.69 15 1 0 10.27 2.52 15 1 0 10.79 2.19 16 -15 0 11.07 1.90 -1 16 0 13.37 3.19 0 16 0 11.66 2.88 16 0 0 10.13 2.49 16 -16 0 16.71 2.29 16 0 0 11.16 2.25 17 -1 0 5.55 1.71 1 16 0 5.46 2.01 17 -1 0 9.18 2.30 1 16 0 6.70 2.45 17 -2 0 27.12 3.55 17 -2 0 31.17 3.97 2 15 0 29.80 3.92 2 15 0 28.10 4.46 17 -3 0 28.62 3.74 3 14 0 30.30 4.31 3 14 0 24.28 3.67 17 -3 0 25.26 3.30 17 -4 0 19.28 2.83 17 -4 0 19.15 3.08 4 13 0 19.70 3.19 4 13 0 21.33 3.66 5 12 0 35.46 4.64 5 12 0 37.02 4.31 17 -5 0 32.87 3.88 17 -5 0 35.34 4.16 6 11 0 59.06 6.10 17 -6 0 62.41 5.92 6 11 0 54.99 6.18 17 -6 0 52.47 5.62 7 10 0 43.76 5.41 7 10 0 50.40 5.48 17 -7 0 49.65 5.14 -10 17 0 47.60 5.51 7 10 0 51.25 4.95 17 -7 0 52.80 5.11 8 9 0 27.59 3.10 17 -8 0 24.57 3.02 -9 17 0 27.43 3.85 8 9 0 22.15 3.51 8 9 0 21.82 3.27 17 -8 0 27.80 3.17 9 8 0 15.75 2.80 -8 17 0 13.49 2.99 17 -9 0 16.07 2.35 9 8 0 17.74 2.44 17 -9 0 19.59 2.50 9 8 0 19.35 2.72 10 7 0 9.00 1.93 10 7 0 6.12 1.14 17 -10 0 6.18 1.51 -7 17 0 6.83 2.25 10 7 0 6.61 1.99 17 -10 0 6.67 1.41 11 6 0 29.60 3.68 11 6 0 28.05 3.74 17 -11 0 28.97 3.26 -6 17 0 28.77 4.27 17 -11 0 26.13 2.96 17 -12 0 34.01 3.72 12 5 0 32.15 4.20 12 5 0 34.92 4.08 -5 17 0 30.47 4.65 17 -13 0 28.59 3.22 13 4 0 25.24 3.68 -4 17 0 30.97 4.43 13 4 0 25.20 3.71 17 -14 0 5.92 1.56 14 3 0 6.71 1.87 14 3 0 8.20 2.22 -3 17 0 6.10 2.44 17 -15 0 4.11 1.38 15 2 0 3.31 1.90 15 2 0 3.78 1.71 -2 17 0 4.05 2.37 16 1 0 11.01 2.27 16 1 0 9.96 2.47 17 -16 0 15.26 2.17 -1 17 0 9.73 2.90 17 0 0 20.03 2.78 0 17 0 17.31 3.33 0 17 0 18.43 2.93 17 0 0 13.68 2.66 1 17 0 23.05 3.84 18 -1 0 18.81 2.93 18 -1 0 17.38 2.63 1 17 0 21.08 3.20 2 16 0 24.79 3.98 18 -2 0 22.85 3.29 2 16 0 21.43 3.24 18 -2 0 19.78 2.86 3 15 0 12.00 2.47 3 15 0 10.77 2.69 18 -3 0 16.89 2.61 18 -3 0 15.82 2.35 18 -4 0 23.56 3.15 18 -4 0 19.13 2.83 4 14 0 18.54 3.00 4 14 0 16.28 3.17 18 -5 0 37.81 3.94 5 13 0 27.06 3.95 18 -5 0 32.12 3.69 5 13 0 28.81 4.28 18 -6 0 27.70 3.56 18 -6 0 28.60 3.39 6 12 0 25.50 3.82 6 12 0 28.81 3.84 18 -7 0 32.97 3.69 7 11 0 30.10 3.90 18 -7 0 31.52 3.57 7 11 0 25.69 3.92 18 -8 0 10.51 1.91 8 10 0 8.66 1.55 18 -8 0 9.89 1.82 8 10 0 8.38 2.15 8 10 0 8.17 1.82 -9 18 0 4.12 1.84 9 9 0 3.77 1.75 9 9 0 2.47 1.10 18 -9 0 3.19 1.29 18 -9 0 4.23 1.32 9 9 0 3.20 1.35 18 -10 0 11.03 1.88 10 8 0 10.07 2.28 -8 18 0 13.60 2.86 18 -10 0 10.82 1.73 10 8 0 11.81 2.11 11 7 0 22.41 3.08 11 7 0 21.01 3.19 18 -11 0 21.32 2.77 -7 18 0 26.95 3.77 18 -11 0 18.60 2.43 18 -12 0 42.40 4.40 12 6 0 36.67 4.63 -6 18 0 49.15 5.59 12 6 0 43.63 4.81 13 5 0 31.04 4.24 13 5 0 37.88 4.31 -5 18 0 44.13 5.22 18 -13 0 33.52 3.82 -4 18 0 8.09 2.53 14 4 0 7.20 1.91 18 -14 0 8.05 1.66 14 4 0 7.59 2.04 15 3 0 2.82 1.69 15 3 0 3.03 1.54 -3 18 0 4.92 2.39 18 -15 0 5.31 1.42 16 2 0 1.29 1.32 -2 18 0 4.48 2.25 16 2 0 2.41 1.66 18 -16 0 2.92 1.25 17 1 0 8.09 1.78 17 1 0 11.78 2.23 -1 18 0 10.11 2.65 18 0 0 21.23 3.11 18 0 0 19.85 2.82 0 18 0 23.52 3.75 0 18 0 22.27 3.11 1 18 0 25.46 3.44 19 -1 0 22.82 2.84 19 -1 0 15.42 2.46 1 18 0 20.53 2.80 19 -2 0 7.88 1.60 2 17 0 6.12 1.78 2 17 0 7.05 1.98 19 -2 0 6.75 1.78 19 -3 0 7.89 1.90 3 16 0 7.16 2.25 3 16 0 5.31 1.72 19 -4 0 17.61 2.54 4 15 0 16.31 3.01 4 15 0 20.27 2.96 19 -4 0 17.12 2.64 5 14 0 32.31 3.91 19 -5 0 35.72 3.84 5 14 0 25.38 3.97 19 -5 0 30.01 3.49 6 13 0 26.15 3.46 6 13 0 19.96 3.29 19 -6 0 26.24 3.25 19 -6 0 21.80 2.98 7 12 0 10.43 2.28 19 -7 0 11.62 2.04 7 12 0 14.01 2.39 19 -7 0 10.96 1.95 8 11 0 11.85 2.38 8 11 0 14.35 2.35 19 -8 0 18.62 2.42 19 -8 0 14.29 2.19 9 10 0 6.55 1.94 19 -9 0 5.94 1.47 9 10 0 3.33 1.10 9 10 0 4.31 1.30 19 -9 0 4.83 1.39 -10 19 0 6.86 1.82 -9 19 0 7.15 2.24 19 -10 0 7.30 1.55 19 -10 0 7.26 1.51 10 9 0 7.95 1.96 10 9 0 6.68 1.51 11 8 0 15.45 2.42 11 8 0 15.54 2.68 19 -11 0 18.69 2.36 -8 19 0 15.07 3.23 12 7 0 37.42 4.00 19 -12 0 33.75 3.83 -7 19 0 39.20 4.83 12 7 0 33.06 4.13 13 6 0 45.54 4.86 19 -13 0 43.95 4.60 -6 19 0 50.64 5.72 13 6 0 42.86 4.97 14 5 0 3.62 1.66 19 -14 0 6.72 1.44 14 5 0 5.76 1.76 -5 19 0 5.85 2.12 19 -15 0 1.26 1.09 15 4 0 2.11 1.42 15 4 0 1.24 1.44 -4 19 0 4.79 2.17 16 3 0 2.70 1.82 19 -16 0 5.60 1.37 -3 19 0 4.25 3.05 -2 19 0 11.51 2.48 17 2 0 5.79 1.53 17 2 0 10.43 2.04 -1 19 0 21.02 3.40 -1 19 0 16.56 2.63 18 1 0 16.16 2.37 19 0 0 15.74 2.49 0 19 0 17.36 2.78 19 0 0 17.10 2.43 0 19 0 16.90 2.46 2 18 0 11.38 2.02 2 18 0 13.29 2.23 20 -2 0 11.57 1.87 20 -2 0 11.12 2.26 3 17 0 4.85 1.61 20 -3 0 4.20 1.39 20 -3 0 4.13 1.15 3 17 0 4.93 1.46 4 16 0 9.63 1.96 20 -4 0 6.77 1.48 20 -4 0 9.34 1.83 4 16 0 8.17 1.91 5 15 0 5.31 1.72 20 -5 0 7.23 1.58 5 15 0 8.75 1.86 20 -5 0 7.63 1.71 6 14 0 18.58 2.80 20 -6 0 19.64 3.69 20 -6 0 22.66 3.30 7 13 0 23.26 3.16 20 -7 0 23.41 3.96 7 13 0 22.22 3.50 20 -7 0 23.59 2.88 20 -8 0 7.41 1.47 8 12 0 4.71 1.32 20 -8 0 6.73 1.52 8 12 0 7.25 1.82 20 -9 0 4.17 1.37 11 -20 0 2.56 0.74 20 -9 0 3.15 1.18 9 11 0 2.85 1.57 10 10 0 2.81 1.18 -10 20 0 7.58 2.13 20 -10 0 2.85 1.17 10 10 0 2.09 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4.08 0.84 3 -10 -4 3.41 0.54 -3 10 -4 5.39 1.66 3 -10 -4 4.39 0.52 -10 7 -4 3.69 0.41 7 3 -4 2.62 0.92 -3 10 -4 3.42 3.53 -3 10 -4 4.17 1.67 3 -10 -4 3.29 1.14 7 3 -4 2.64 0.93 -10 7 4 5.78 0.61 -7 -3 4 5.18 0.86 7 3 4 5.93 2.02 10 -7 4 5.54 0.95 3 -10 4 6.02 0.59 7 3 4 5.18 0.99 7 3 4 5.63 1.10 -3 10 4 6.15 0.79 -3 10 4 4.32 1.35 7 3 4 8.81 1.54 -3 10 4 8.01 3.42 10 -7 4 6.56 1.00 7 3 4 4.86 1.87 8 2 -4 57.25 4.88 -2 10 -4 42.46 6.43 -8 -2 -4 47.15 4.57 -2 10 -4 45.30 7.92 2 -10 -4 45.58 4.88 10 -8 -4 49.01 4.54 8 2 -4 52.37 4.70 8 2 -4 46.84 5.06 10 -8 -4 48.52 4.59 -2 10 -4 45.42 5.46 -8 -2 -4 55.01 4.64 2 -10 -4 51.20 4.44 -2 10 4 37.88 6.40 8 2 4 30.90 2.70 8 2 4 28.99 3.02 2 -10 4 34.56 2.62 -2 10 4 34.30 5.68 10 -8 4 30.22 2.79 -2 10 4 26.22 3.45 8 2 4 31.93 3.69 10 -8 4 29.65 2.88 8 2 4 22.69 3.63 -2 10 4 23.47 2.75 8 2 4 25.68 3.23 -2 10 4 28.76 5.96 -8 -2 4 27.94 2.82 -1 10 -4 52.37 7.34 1 -10 -4 48.71 4.54 9 1 -4 47.80 4.87 -1 10 -4 50.09 5.71 -10 9 -4 51.14 4.86 -1 10 -4 52.63 8.31 9 1 -4 47.37 5.21 -1 10 -4 51.04 7.09 -10 9 -4 50.52 4.88 9 1 -4 55.72 4.68 -9 -1 -4 47.30 4.65 -9 -1 -4 46.19 4.65 1 -10 -4 53.92 5.07 10 -9 -4 51.33 4.70 -1 10 4 52.54 7.54 -1 10 4 53.73 8.17 9 1 4 41.47 4.88 9 1 4 46.17 4.65 -1 10 4 45.25 5.16 9 1 4 46.87 5.40 -9 -1 4 42.52 4.45 -1 10 4 48.91 4.51 10 -9 4 50.38 4.56 -1 10 4 62.75 7.50 -1 10 4 55.39 8.53 1 -10 4 55.64 4.34 10 -9 4 45.64 4.39 10 0 -4 54.03 5.37 0 10 -4 52.09 9.69 -10 0 -4 50.41 4.71 -10 0 -4 45.28 4.73 -10 10 -4 57.27 5.87 0 -10 -4 52.91 4.64 -10 10 -4 49.45 5.72 10 -10 -4 50.24 4.75 0 -10 -4 52.82 5.11 0 10 -4 46.52 8.32 0 10 4 73.52 10.31 0 -10 4 72.69 6.03 10 0 4 71.52 6.36 10 -10 4 67.87 6.23 0 10 4 67.54 6.23 10 0 4 66.23 6.63 -10 0 4 61.74 6.10 -1 -10 -4 59.81 5.51 1 10 -4 70.61 6.87 10 -11 -4 62.54 5.64 -11 1 -4 53.85 5.53 11 -1 -4 62.32 5.86 -1 -10 -4 62.77 5.99 11 -1 -4 61.66 6.16 11 -1 4 57.23 5.68 1 10 4 60.94 6.05 -11 1 4 52.31 5.06 10 -11 4 55.10 5.24 1 10 4 56.48 5.28 11 -1 4 59.23 5.37 11 -2 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2.24 6 -11 -4 19.89 2.39 -6 11 -4 15.56 2.77 -11 5 -4 19.15 1.80 11 -5 -4 17.84 2.24 5 6 -4 22.36 2.57 6 -11 -4 19.10 1.66 5 6 -4 15.40 4.51 5 6 -4 21.38 2.83 -5 -6 -4 16.47 1.96 5 6 -4 20.03 2.34 -5 -6 -4 15.26 2.17 6 -11 -4 19.97 1.68 5 6 4 33.59 5.65 5 6 4 29.69 2.99 -11 5 4 23.59 2.41 11 -5 4 27.74 2.91 -5 -6 4 26.57 2.62 11 -5 4 29.83 2.77 5 6 4 23.01 3.09 5 6 4 29.47 2.99 5 6 4 30.72 5.85 -6 11 4 25.48 4.48 -6 11 4 24.93 3.16 11 -6 -4 9.51 1.40 6 5 -4 7.27 1.70 -11 6 -4 8.33 0.92 -6 -5 -4 8.47 1.23 6 5 -4 8.09 1.62 6 5 -4 8.21 1.72 5 -11 -4 8.60 0.85 11 -6 -4 10.13 1.44 5 -11 -4 10.09 1.68 -6 -5 -4 9.88 1.39 5 -11 -4 10.08 0.92 6 5 4 25.70 3.11 6 5 4 33.67 5.13 -5 11 4 29.17 2.60 6 5 4 23.82 4.91 -5 11 4 28.40 3.33 6 5 4 31.05 3.17 6 5 4 27.29 3.02 -11 6 4 25.35 2.50 -5 11 4 33.92 4.97 11 -6 4 27.15 2.91 11 -6 4 29.57 2.85 -11 7 -4 18.13 1.59 -7 -4 -4 16.67 1.90 -4 11 -4 16.42 2.89 11 -7 -4 17.26 1.99 7 4 -4 19.21 2.73 7 4 -4 19.33 2.35 11 -7 -4 18.14 2.07 4 -11 -4 16.26 1.60 4 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44.91 4.19 -2 11 4 38.87 5.06 11 -9 4 46.19 4.35 -2 11 4 54.80 4.44 9 2 4 50.42 6.19 11 -9 4 53.75 4.54 -9 -2 4 40.19 4.39 1 -11 -4 44.96 3.98 10 1 -4 36.42 4.23 10 1 -4 34.78 3.76 -1 11 -4 25.05 4.39 11 -10 -4 35.45 3.52 10 1 -4 34.55 3.35 1 -11 -4 37.07 3.32 -10 -1 -4 34.56 3.44 10 1 4 67.81 7.22 10 1 4 79.22 7.01 -1 11 4 68.22 6.75 1 -11 4 82.10 6.57 -10 -1 4 70.70 6.72 11 -10 4 79.01 6.86 11 0 -4 46.28 4.63 0 -11 -4 36.38 4.15 0 11 -4 30.49 4.81 11 0 -4 43.99 4.14 0 -11 -4 38.99 3.65 11 -11 -4 40.96 3.87 0 11 4 74.31 6.96 0 11 4 53.22 5.98 11 0 4 72.98 6.64 -11 0 4 59.24 5.92 11 0 4 69.57 6.23 0 -11 4 66.58 5.81 11 -11 4 72.81 6.13 -12 1 -4 122.41 11.72 -1 -11 -4 135.27 12.14 12 -1 -4 155.85 12.51 1 11 -4 138.88 12.97 -1 -11 -4 128.52 11.69 11 -12 -4 128.22 11.83 12 -1 4 159.26 13.86 -12 1 4 141.27 13.53 1 11 4 157.70 14.51 12 -1 4 166.81 14.22 10 -12 -4 78.03 6.50 -2 -10 -4 65.78 6.33 2 10 -4 72.82 7.55 -12 2 -4 63.87 6.32 -2 -10 -4 70.98 6.75 12 -2 -4 66.85 6.67 12 -2 -4 82.05 7.07 12 -2 4 51.46 4.83 -12 2 4 46.71 4.53 -10 12 4 56.31 5.23 2 10 4 62.93 5.70 12 -2 4 49.04 5.12 2 10 4 46.86 4.74 10 -12 4 41.61 4.31 10 -12 4 48.81 4.69 -2 -10 4 53.99 4.49 9 -12 -4 49.08 4.30 9 -12 -4 42.81 4.02 3 9 -4 39.52 3.92 -3 -9 -4 37.95 3.89 -12 3 -4 38.08 3.82 12 -3 -4 42.88 4.21 -3 -9 -4 45.32 4.32 12 -3 -4 39.84 4.42 9 -12 4 27.41 2.71 -12 3 4 24.04 2.40 3 9 4 30.12 2.92 -3 -9 4 27.00 2.49 3 9 4 25.69 3.40 -9 12 4 18.16 3.14 12 -3 4 26.79 2.80 12 -3 4 24.24 3.04 4 8 -4 25.85 2.75 8 -12 -4 27.02 2.71 -4 -8 -4 25.45 2.60 -8 12 -4 23.13 3.38 8 -12 -4 28.69 2.98 -12 4 -4 24.88 2.45 12 -4 -4 27.73 2.89 4 8 -4 25.45 3.67 12 -4 -4 25.93 3.08 4 8 -4 29.14 3.25 -4 -8 -4 22.46 2.86 4 8 4 23.45 2.54 12 -4 4 23.26 2.43 -12 4 4 20.31 2.00 12 -4 4 21.40 2.66 -8 12 4 27.62 2.93 4 8 4 19.37 2.94 -4 -8 4 17.54 2.09 12 -5 -4 26.88 3.00 -5 -7 -4 24.20 2.76 5 7 -4 31.18 3.11 -7 12 -4 32.77 3.89 -12 5 -4 28.73 2.60 5 7 -4 31.98 3.77 12 -5 -4 31.22 3.13 -5 -7 -4 24.76 3.01 7 -12 -4 26.01 3.13 5 7 -4 30.16 3.39 -7 12 4 22.67 3.24 5 7 4 31.27 3.14 -5 -7 4 26.25 2.69 5 7 4 27.72 3.17 -12 5 4 24.97 2.51 12 -5 4 33.39 2.95 5 7 4 29.83 3.45 12 -5 4 30.41 3.10 -12 6 -4 3.92 0.64 6 6 -4 4.11 1.53 -6 -6 -4 5.16 0.89 -6 -6 -4 5.42 1.20 12 -6 -4 4.91 1.14 12 -6 -4 5.58 1.20 6 6 -4 5.96 1.44 6 -12 -4 7.62 1.52 6 6 -4 5.21 1.43 -6 12 -4 5.96 1.87 6 6 4 8.34 1.70 6 6 4 7.29 1.48 -6 12 4 6.78 1.79 -6 -6 4 7.53 1.10 12 -6 4 9.91 1.53 12 -6 4 7.54 1.26 -12 6 4 7.86 0.92 6 6 4 10.65 1.81 12 -7 -4 4.48 1.07 7 5 -4 5.92 1.56 -7 -5 -4 5.13 0.93 -5 12 -4 4.64 1.80 5 -12 -4 5.42 1.43 7 5 -4 6.13 1.50 12 -7 -4 4.98 1.10 5 -12 -4 5.42 0.59 -12 7 -4 4.66 0.58 7 5 -4 4.85 1.48 7 5 4 18.74 2.38 -12 7 4 18.42 1.67 7 5 4 19.00 2.34 -7 -5 4 17.19 1.95 12 -7 4 17.58 2.06 -5 12 4 13.82 2.58 12 -7 4 19.51 2.09 7 5 4 18.60 2.45 12 -8 -4 49.59 4.46 -8 -4 -4 40.98 4.34 -4 12 -4 57.99 5.71 8 4 -4 48.36 4.71 12 -8 -4 42.61 4.45 8 4 -4 50.20 4.83 -8 -4 -4 46.09 4.46 8 4 -4 43.98 4.95 4 -12 -4 43.18 4.73 4 -12 -4 48.17 4.13 -4 12 4 30.54 4.18 8 4 4 39.89 3.82 12 -8 4 35.30 3.49 -12 8 4 35.56 3.16 8 4 4 37.69 3.56 -8 -4 4 33.25 3.44 8 4 4 33.59 3.93 12 -8 4 40.31 3.58 -9 -3 -4 42.00 4.27 3 -12 -4 50.09 4.74 9 3 -4 49.94 5.03 9 3 -4 46.06 4.44 12 -9 -4 39.06 4.31 3 -12 -4 47.93 4.07 12 -9 -4 49.15 4.33 -3 12 -4 43.05 5.39 9 3 -4 40.58 4.60 3 -12 4 61.97 4.71 -9 -3 4 46.91 4.91 9 3 4 44.15 5.36 9 3 4 53.06 5.22 -3 12 4 51.70 5.79 12 -9 4 51.69 4.90 12 -9 4 57.53 5.05 10 2 -4 34.24 4.08 12 -10 -4 40.50 3.83 -10 -2 -4 35.78 3.72 10 2 -4 38.98 3.71 2 -12 -4 37.37 3.54 -2 12 -4 47.54 5.17 10 2 -4 39.29 4.49 2 -12 -4 41.87 4.20 -10 -2 4 54.92 5.58 2 -12 4 64.02 5.36 -2 12 4 53.83 6.44 12 -10 4 67.18 5.73 10 2 4 67.43 6.27 10 2 4 62.49 5.91 12 -10 4 60.02 5.50 11 1 -4 13.27 2.48 -11 -1 -4 11.61 1.59 11 1 -4 11.50 1.99 12 -11 -4 13.74 1.77 1 -12 -4 11.40 1.34 11 1 4 36.75 3.76 1 -12 4 32.30 3.20 -1 12 4 42.63 4.61 11 1 4 40.37 4.25 12 -11 4 39.72 4.30 -1 12 4 33.51 3.49 12 -12 -4 22.72 2.51 0 -12 -4 23.83 2.90 0 12 -4 18.50 3.65 12 0 -4 19.32 2.80 0 -12 -4 21.59 2.19 12 0 -4 22.57 3.21 12 -12 4 49.69 4.80 12 0 4 51.39 4.99 0 -12 4 48.18 4.46 0 12 4 51.51 4.73 12 0 4 50.80 5.42 13 -1 -4 39.49 4.06 13 -1 -4 32.11 4.29 1 12 -4 33.59 4.84 12 -13 -4 32.88 3.62 -1 -12 -4 38.68 3.95 13 -1 4 56.10 5.82 13 -1 4 59.77 5.45 1 12 4 50.71 6.12 -1 -12 4 50.20 4.92 12 -13 4 63.76 5.34 1 12 4 51.96 5.17 -2 -11 -4 44.88 4.24 -2 -11 -4 45.83 4.69 13 -2 -4 47.80 5.07 11 -13 -4 45.82 4.46 2 11 -4 44.13 5.55 -2 -11 4 38.32 3.86 2 11 4 44.65 4.22 13 -2 4 45.79 4.34 13 -2 4 39.42 4.67 2 11 4 35.76 4.90 11 -13 4 49.34 4.21 -3 -10 -4 38.06 4.82 13 -3 -4 55.10 5.27 3 10 -4 55.41 5.87 13 -3 -4 58.14 5.00 10 -13 -4 52.06 4.69 -13 3 -4 43.83 4.47 13 -3 4 14.93 2.45 3 10 4 18.17 2.15 10 -13 4 15.27 1.53 -13 3 4 15.55 1.66 3 10 4 15.98 2.88 -3 -10 4 16.43 1.72 4 9 -4 46.38 5.27 -13 4 -4 38.84 3.90 4 9 -4 42.37 4.11 9 -13 -4 41.47 4.13 -4 -9 -4 38.29 4.01 4 9 -4 48.15 4.75 13 -4 -4 53.79 4.74 13 -4 -4 46.78 4.40 -4 -9 -4 41.30 4.38 -4 -9 4 27.54 2.88 -13 4 4 26.66 2.77 4 9 4 33.50 3.51 13 -4 4 32.87 3.25 4 9 4 32.74 3.88 4 9 4 28.32 3.29 -9 13 4 36.85 3.83 -13 5 -4 20.60 2.29 -5 -8 -4 20.30 2.45 5 8 -4 33.33 3.51 8 -13 -4 24.83 3.10 -5 -8 -4 25.45 2.82 13 -5 -4 27.95 2.86 -8 13 -4 25.10 3.51 5 8 -4 30.46 2.82 5 8 4 32.52 3.26 -13 5 4 25.93 2.61 -8 13 4 32.60 3.63 5 8 4 28.30 3.31 -5 -8 4 26.84 2.77 5 8 4 26.82 3.61 13 -5 4 29.11 3.24 13 -5 4 30.65 3.03 -6 -7 -4 7.14 1.39 -6 -7 -4 4.17 0.86 6 7 -4 5.18 1.85 -13 6 -4 5.87 0.76 -7 13 -4 5.83 1.91 6 7 -4 6.71 1.48 13 -6 -4 6.41 1.39 7 -13 -4 7.16 1.77 13 -6 4 16.60 2.02 -6 -7 4 10.26 1.48 6 7 4 13.54 2.08 13 -6 4 14.82 1.78 6 7 4 10.97 1.99 -13 6 4 10.74 1.23 -7 13 4 15.58 2.45 6 7 4 13.08 2.25 -7 -6 -4 3.59 1.03 7 6 -4 4.13 1.32 -13 7 -4 2.31 0.40 -7 -6 -4 2.97 0.73 7 6 -4 2.81 1.45 13 -7 -4 4.63 1.14 -6 13 -4 3.36 1.63 13 -7 4 2.33 0.89 7 6 4 1.89 1.09 -6 13 4 1.92 1.36 -7 -6 4 0.49 0.57 7 6 4 2.47 1.15 7 6 4 2.71 1.31 -13 7 4 1.61 0.35 13 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-13 -4 43.70 4.38 12 1 -4 41.24 4.39 12 1 4 33.46 3.53 12 1 4 31.80 3.93 13 -12 4 33.43 3.32 -1 13 4 24.13 4.16 13 -13 -4 42.51 4.59 13 0 -4 45.20 4.91 13 0 -4 49.14 5.38 0 13 -4 47.37 5.84 0 -13 -4 50.40 4.90 13 0 4 41.71 4.34 13 -13 4 43.10 4.15 0 13 4 41.10 5.17 13 0 4 36.10 4.68 14 -1 -4 67.90 6.89 14 -1 -4 70.79 7.28 -1 -13 -4 74.69 6.83 13 -14 -4 63.64 6.53 1 13 -4 75.05 7.84 13 -14 4 70.03 6.32 1 13 4 80.45 7.53 14 -1 4 61.12 6.81 14 -1 4 58.45 6.40 12 -14 -4 53.95 5.17 -2 -12 -4 57.01 5.40 2 12 -4 52.25 6.32 14 -2 -4 56.78 5.85 14 -2 -4 47.87 5.39 2 12 4 66.11 6.92 14 -2 4 59.20 6.45 14 -2 4 62.46 6.10 2 12 4 65.21 6.27 -3 -11 -4 18.87 2.71 14 -3 -4 21.56 2.77 11 -14 -4 24.07 2.57 14 -3 -4 21.95 3.17 3 11 -4 20.13 3.68 14 -3 4 13.61 2.15 14 -3 4 15.25 2.56 3 11 4 16.97 3.03 4 10 -4 9.53 2.63 14 -4 -4 19.84 2.57 -14 4 -4 10.17 1.41 4 10 -4 14.19 2.39 4 10 4 23.86 3.54 -10 14 4 21.65 3.17 14 -4 4 24.34 2.75 4 10 4 22.89 3.08 14 -4 4 25.14 3.15 14 -5 -4 22.04 2.62 -14 5 -4 15.82 1.99 -9 14 -4 22.79 3.24 14 -5 -4 20.92 2.81 5 9 -4 21.21 3.44 5 9 -4 19.30 3.05 -5 -9 -4 21.93 2.53 5 9 -4 22.00 2.34 14 -5 4 34.51 3.48 5 9 4 31.63 3.78 -9 14 4 39.23 4.20 -14 5 4 26.86 2.99 5 9 4 37.97 4.18 5 9 4 34.56 3.83 14 -5 4 36.13 3.77 6 8 -4 40.12 3.99 6 8 -4 30.70 3.30 -8 14 -4 28.00 4.06 6 8 -4 26.01 3.94 14 -6 -4 29.45 3.36 14 -6 -4 32.71 3.53 -6 -8 -4 30.39 3.28 8 -14 -4 30.70 3.59 -8 14 4 31.81 3.79 6 8 4 22.69 3.39 6 8 4 30.24 3.42 6 8 4 31.20 3.31 14 -6 4 29.20 3.22 14 -6 4 31.75 3.08 -14 6 4 23.06 2.49 -7 -7 -4 11.19 1.78 7 7 -4 11.55 2.38 14 -7 -4 13.23 2.06 7 7 -4 10.40 2.26 7 7 -4 15.51 2.27 14 -7 -4 14.81 2.07 -7 14 -4 15.34 3.00 7 -14 -4 15.61 2.37 14 -7 4 6.64 1.28 14 -7 4 5.07 1.77 -7 14 4 7.39 2.04 7 7 4 4.73 1.49 7 7 4 7.81 1.74 7 7 4 3.86 1.45 8 6 -4 4.92 1.60 6 -14 -4 5.44 1.56 8 6 -4 4.46 1.59 14 -8 -4 5.80 1.30 8 6 -4 3.65 1.44 -6 14 -4 7.96 2.25 14 -8 -4 3.68 1.22 -8 -6 -4 3.94 1.08 8 6 4 1.81 1.22 14 -8 4 2.55 1.00 8 6 4 2.98 1.47 -6 14 4 3.47 1.97 14 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46.14 4.50 14 -14 -4 39.07 4.59 0 -14 -4 47.38 4.90 14 0 -4 54.29 5.19 0 14 -4 45.58 5.92 14 0 -4 51.99 5.53 0 14 4 19.44 3.74 14 0 4 21.36 3.47 14 -14 4 24.90 2.83 14 0 4 23.93 2.97 15 -1 -4 59.66 6.53 1 14 -4 52.89 6.97 15 -1 -4 58.20 6.25 14 -15 -4 62.78 5.92 -1 -14 -4 69.62 6.17 1 14 4 35.28 4.89 15 -1 4 34.39 3.78 15 -1 4 30.63 4.25 2 13 -4 93.45 8.76 15 -2 -4 76.15 7.66 -2 -13 -4 76.04 7.49 15 -2 -4 79.53 7.97 13 -15 -4 76.51 7.35 15 -2 4 47.70 5.74 2 13 4 61.76 6.32 15 -2 4 52.15 5.33 -3 -12 -4 85.71 7.71 12 -15 -4 82.70 7.53 15 -3 -4 85.37 8.10 3 12 -4 64.05 8.39 3 12 -4 89.17 8.20 15 -3 -4 80.11 7.76 15 -3 4 81.62 7.75 3 12 4 81.49 7.22 15 -3 4 76.97 7.32 3 12 4 73.25 7.97 3 12 4 73.26 7.58 15 -4 -4 37.38 4.01 4 11 -4 29.07 4.03 15 -4 -4 29.54 3.58 -4 -11 -4 28.24 3.43 4 11 -4 39.08 4.72 4 11 4 41.42 4.48 11 -15 4 36.66 3.46 4 11 4 37.17 4.06 15 -4 4 44.35 4.57 15 -4 4 42.18 4.11 4 11 4 42.96 4.92 15 -5 -4 44.38 4.83 5 10 -4 40.83 5.43 15 -5 -4 45.82 4.66 5 10 -4 47.62 5.08 -5 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37.21 4.48 18 -14 4 42.67 4.35 14 4 4 42.25 4.89 -4 18 4 52.31 5.79 18 -15 -4 34.33 3.83 15 3 -4 30.81 4.22 -3 18 -4 44.17 5.18 15 3 -4 34.01 4.17 -3 18 4 40.94 5.51 18 -15 4 45.98 4.29 15 3 4 36.21 4.39 15 3 4 43.91 4.79 16 2 -4 54.71 5.88 -2 18 -4 67.29 6.73 16 2 -4 53.34 5.88 18 -16 -4 55.35 5.52 -2 18 4 47.51 5.57 16 2 4 44.70 4.89 16 2 4 38.06 4.37 17 1 -4 65.94 6.81 -1 18 -4 64.94 6.75 -1 18 -4 75.80 7.45 17 1 -4 61.05 6.49 17 1 4 70.75 7.10 -1 18 4 72.89 7.68 0 18 -4 48.80 5.27 0 18 -4 48.79 5.72 18 0 -4 47.50 5.05 0 18 4 52.42 5.30 0 18 4 53.34 5.80 18 0 4 56.95 5.37 18 0 4 44.71 4.92 1 18 -4 25.51 3.56 19 -1 -4 27.13 2.98 1 18 -4 20.27 3.11 19 -1 -4 19.63 2.82 -1 -18 4 32.72 3.35 19 -1 4 36.14 3.79 1 18 4 30.04 3.65 1 18 4 37.56 4.17 2 17 -4 32.55 3.98 19 -2 -4 29.70 3.35 19 -2 -4 22.03 3.10 2 17 -4 23.18 3.47 19 -2 4 24.76 3.21 19 -2 4 38.61 3.74 2 17 4 35.31 3.65 2 17 4 28.57 3.96 3 16 -4 40.01 6.30 3 16 -4 28.18 5.41 3 16 4 57.69 5.71 3 16 4 56.41 6.49 19 -3 4 52.57 5.38 19 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287.94 27.82 -4 10 5 284.87 30.25 -10 6 5 317.00 27.18 3 -10 -5 316.99 23.84 7 3 -5 256.25 24.16 3 -10 -5 233.81 24.21 10 -7 -5 296.60 24.00 -7 -3 -5 272.76 23.99 -10 7 -5 284.22 23.71 -3 10 -5 284.90 25.02 -7 -3 -5 287.83 24.08 10 -7 -5 279.85 24.01 -3 10 -5 232.73 26.26 -10 7 -5 303.42 23.72 10 -7 -5 293.94 23.86 7 3 -5 230.42 24.30 3 -10 5 278.31 21.60 7 3 5 267.75 22.01 10 -7 5 252.82 21.86 -10 7 5 255.13 21.62 7 3 5 245.94 23.37 -3 10 5 217.42 21.74 10 -7 5 285.28 21.87 7 3 5 238.81 21.91 7 3 5 260.02 22.15 7 3 5 228.44 23.12 -3 10 5 237.82 25.31 -7 -3 5 212.36 21.77 -3 10 5 296.35 25.77 -8 -2 -5 168.65 14.83 8 2 -5 191.68 15.06 8 2 -5 139.11 15.14 -2 10 -5 185.36 15.92 -2 10 -5 185.54 17.85 10 -8 -5 170.05 14.61 -2 10 -5 147.13 18.51 10 -8 -5 172.46 14.80 -8 -2 -5 155.93 14.77 -2 10 -5 167.83 17.26 10 -8 -5 172.69 14.75 8 2 -5 166.83 14.89 8 2 5 158.56 13.29 2 -10 5 165.22 12.93 -8 -2 5 134.11 13.08 -2 10 5 153.50 16.75 10 -8 5 142.62 13.08 -8 -2 5 141.48 13.05 8 2 5 144.43 12.96 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9.75 -12 7 -5 112.68 9.71 -7 -5 -5 110.24 10.01 5 -12 -5 105.78 10.30 -5 12 -5 100.26 10.97 7 5 5 99.41 8.53 7 5 5 98.11 8.63 7 5 5 94.97 8.50 -7 -5 5 84.15 8.18 12 -7 5 98.26 8.29 12 -7 5 88.25 8.32 -12 7 5 85.39 7.97 4 -12 -5 155.92 13.11 -8 -4 -5 125.39 13.36 12 -8 -5 149.67 13.39 12 -8 -5 160.81 13.37 8 4 -5 134.67 13.73 4 -12 -5 157.23 13.70 8 4 -5 175.86 13.70 8 4 -5 147.95 13.66 12 -8 5 129.39 11.07 8 4 5 129.06 11.06 8 4 5 131.13 11.46 -12 8 5 110.34 10.74 8 4 5 126.67 11.25 12 -8 5 124.90 11.05 9 3 -5 203.14 17.75 3 -12 -5 197.87 17.41 9 3 -5 216.52 18.20 12 -9 -5 200.08 17.57 12 -9 -5 181.49 17.61 9 3 -5 224.31 17.99 -9 -3 -5 184.07 17.77 -3 12 -5 173.77 18.55 3 -12 -5 232.46 18.07 3 -12 5 142.46 11.08 9 3 5 132.88 11.84 -3 12 5 136.84 12.22 9 3 5 140.12 11.61 -9 -3 5 111.62 11.26 -3 12 5 136.15 11.31 -9 -3 5 107.57 11.29 12 -9 5 122.58 11.30 12 -9 5 130.51 11.41 -2 12 -5 86.51 9.78 10 2 -5 98.73 9.36 2 -12 -5 109.56 9.43 -10 -2 -5 93.67 8.71 10 2 -5 97.07 8.73 2 -12 5 66.86 5.47 12 -10 5 58.72 5.80 -10 -2 5 52.51 5.68 12 -10 5 69.09 5.84 -2 12 5 63.23 5.72 10 2 5 63.90 6.00 -2 12 5 64.43 6.68 1 -12 -5 44.42 5.03 11 1 -5 41.17 5.25 12 -11 -5 50.11 4.68 11 1 -5 57.72 5.06 -1 12 5 48.80 4.89 1 -12 5 37.74 3.36 11 1 5 32.51 4.22 -1 12 5 32.34 3.59 11 1 5 40.44 3.92 0 -12 -5 41.85 4.83 0 -12 -5 48.66 4.41 12 0 -5 48.36 5.29 0 12 -5 42.80 5.70 12 -12 -5 48.61 4.55 12 0 -5 48.93 4.87 12 0 5 39.68 4.58 12 0 5 40.38 4.10 0 -12 5 34.61 3.60 0 12 5 49.24 5.08 12 -12 5 43.87 3.99 13 -1 -5 96.35 8.53 13 -1 -5 73.80 7.99 1 12 -5 69.54 8.81 -1 -12 -5 99.53 8.22 12 -13 -5 85.08 7.78 12 -13 5 111.56 9.17 -1 -12 5 94.75 8.89 13 -1 5 93.40 9.58 1 12 5 96.36 9.98 13 -1 5 107.00 9.30 13 -2 -5 101.43 9.62 11 -13 -5 93.11 9.04 2 11 -5 95.98 10.15 13 -2 -5 106.29 9.36 -2 -11 -5 105.12 9.41 13 -2 5 78.94 7.29 11 -13 5 84.99 7.20 -2 -11 5 69.30 6.92 2 11 5 78.37 7.99 13 -2 5 80.97 7.70 2 11 5 80.77 7.28 13 -3 -5 220.20 17.87 13 -3 -5 217.94 18.09 3 10 -5 164.32 18.39 10 -13 -5 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9.22 10 3 -5 94.82 9.70 -3 13 -5 127.78 11.17 10 3 -5 95.11 9.51 10 3 -5 91.48 9.18 3 -13 -5 111.93 9.62 10 3 5 80.77 7.76 10 3 5 76.73 8.11 -3 13 5 75.49 8.11 13 -10 5 77.70 7.07 13 -10 5 83.31 7.26 11 2 -5 80.70 7.17 13 -11 -5 73.29 7.35 11 2 -5 79.98 7.71 -2 13 -5 88.06 8.68 11 2 -5 83.60 8.08 11 2 5 84.20 7.37 13 -11 5 71.93 6.72 11 2 5 71.98 6.90 -2 13 5 64.62 7.52 12 1 -5 45.06 5.29 13 -12 -5 45.82 4.57 1 -13 -5 46.34 4.94 -1 13 -5 48.39 5.87 12 1 -5 47.12 4.93 12 1 5 37.24 3.98 12 1 5 27.81 4.24 13 -12 5 36.31 3.75 -1 13 5 47.72 5.04 0 -13 -5 39.09 4.14 13 0 -5 31.14 4.43 13 0 -5 38.41 4.20 0 13 -5 31.43 4.93 13 -13 -5 36.92 3.78 13 0 5 47.39 5.67 13 0 5 49.18 5.25 13 -13 5 56.23 5.14 0 13 5 59.23 6.25 13 -14 -5 31.85 3.50 -1 -13 -5 36.85 3.88 14 -1 -5 31.07 3.85 14 -1 -5 33.44 4.30 1 13 -5 31.24 4.73 13 -14 5 30.24 3.16 1 13 5 27.06 4.18 14 -1 5 29.15 3.75 14 -1 5 26.60 3.21 12 -14 -5 26.70 2.91 -2 -12 -5 24.46 3.16 14 -2 -5 26.07 3.18 14 -2 -5 33.60 3.80 2 12 -5 16.46 3.77 2 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14.56 2.58 -4 15 -5 17.26 3.48 15 -11 5 29.27 3.20 11 4 5 25.18 3.44 -4 15 5 36.67 4.58 11 4 5 31.17 3.85 -3 15 -5 21.53 3.87 15 -12 -5 22.29 2.65 12 3 -5 15.83 2.84 12 3 -5 19.92 3.26 3 -15 -5 20.63 2.92 15 -12 5 30.07 3.13 12 3 5 27.70 3.75 -3 15 5 23.93 4.24 12 3 5 28.52 3.34 15 -13 -5 19.21 2.47 13 2 -5 15.04 2.67 -2 15 -5 17.88 3.62 13 2 -5 15.36 2.95 2 -15 -5 16.92 2.78 -2 15 5 16.04 3.50 13 2 5 21.51 2.79 13 2 5 18.29 3.18 15 -13 5 22.47 2.62 1 -15 -5 25.80 3.45 15 -14 -5 25.42 3.18 14 1 -5 24.94 3.81 14 1 -5 26.06 3.58 -1 15 -5 35.42 4.64 15 -14 5 26.50 2.90 14 1 5 21.16 3.48 -1 15 5 17.64 3.66 14 1 5 23.76 2.91 15 0 -5 8.68 2.27 15 0 -5 10.21 2.76 0 15 -5 9.44 3.17 15 -15 -5 12.21 2.47 15 0 5 9.21 2.53 0 15 5 8.67 2.97 16 -1 -5 5.50 2.15 1 15 -5 4.32 2.40 15 -16 -5 7.96 1.54 -1 -15 -5 6.79 1.75 16 -1 -5 6.11 1.82 1 15 -5 4.36 1.91 16 -1 5 8.07 2.30 1 15 5 6.32 2.39 16 -1 5 7.23 1.58 16 -2 -5 8.33 1.94 2 14 -5 6.36 2.12 2 14 -5 6.29 2.60 -2 -14 -5 8.65 1.86 16 -2 -5 8.19 2.31 2 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44.79 4.81 16 -7 5 49.42 4.65 7 9 5 47.79 4.73 7 9 5 42.27 4.82 -9 16 5 34.22 5.13 -8 16 -5 58.82 6.58 8 8 -5 52.45 6.04 8 8 -5 56.06 5.58 16 -8 -5 57.23 5.69 8 8 -5 59.53 6.17 16 -8 -5 60.72 5.69 8 8 5 55.67 5.79 8 8 5 64.71 5.96 16 -8 5 56.86 5.51 16 -8 5 57.46 5.60 -8 16 5 53.95 6.36 8 8 5 54.86 5.61 7 -16 -5 38.26 4.27 9 7 -5 32.97 4.19 -7 16 -5 39.05 5.06 9 7 -5 35.51 4.45 9 7 -5 42.15 4.14 16 -9 -5 35.82 3.99 16 -9 -5 36.98 3.96 16 -9 5 28.87 3.10 9 7 5 25.18 3.38 9 7 5 24.73 2.86 -7 16 5 32.46 4.23 16 -9 5 28.95 3.11 9 7 5 33.07 3.74 -9 -7 5 27.95 2.93 16 -10 -5 26.81 3.14 6 -16 -5 27.09 3.51 10 6 -5 26.07 3.77 -6 16 -5 25.52 4.04 10 6 -5 25.49 3.30 10 6 -5 28.10 3.18 -6 16 5 21.31 3.64 16 -10 5 20.59 2.32 10 6 5 18.55 2.80 16 -10 5 19.21 2.47 10 6 5 20.75 3.06 11 5 -5 17.04 2.24 -5 16 -5 19.22 3.65 11 5 -5 20.87 2.99 16 -11 -5 21.40 2.70 11 5 -5 20.71 3.21 5 -16 -5 26.32 3.12 -5 16 5 23.02 4.00 11 5 5 27.27 3.55 11 5 5 18.81 3.01 16 -11 5 28.11 2.91 12 4 -5 15.01 2.75 16 -12 -5 17.47 2.39 12 4 -5 14.92 2.77 -4 16 -5 18.51 3.65 4 -16 -5 16.91 2.74 12 4 5 33.64 3.90 12 4 5 25.49 3.33 16 -12 5 30.18 3.18 -4 16 5 22.22 4.13 16 -13 -5 28.05 3.44 13 3 -5 30.73 4.00 -3 16 -5 33.62 4.79 3 -16 -5 34.38 3.81 13 3 -5 25.92 3.95 -3 16 5 46.41 5.57 13 3 5 36.16 4.41 16 -13 5 42.88 4.22 13 3 5 41.01 4.83 -2 16 -5 36.72 5.38 14 2 -5 43.38 4.78 16 -14 -5 40.42 4.24 14 2 -5 37.99 4.58 16 -14 5 38.86 3.94 14 2 5 34.54 4.05 -2 16 5 33.07 5.05 14 2 5 40.53 4.59 16 -15 -5 36.52 3.63 15 1 -5 25.63 3.87 -1 16 -5 32.66 4.83 15 1 -5 30.56 4.13 -1 16 5 19.56 3.75 15 1 5 19.50 3.15 15 1 5 18.47 2.67 0 16 -5 9.57 2.85 16 -16 -5 16.98 2.37 16 0 -5 13.40 2.60 16 0 -5 14.11 2.50 16 0 5 7.95 2.20 0 16 5 8.85 2.68 16 0 5 7.83 1.67 17 -1 -5 11.82 2.24 17 -1 -5 13.22 2.57 1 16 -5 14.34 3.14 1 16 -5 8.59 2.21 17 -1 5 12.74 2.53 17 -1 5 12.20 1.96 1 16 5 13.08 2.43 1 16 5 13.74 2.88 17 -2 -5 14.45 2.80 2 15 -5 15.37 2.88 17 -2 -5 14.18 2.40 2 15 -5 14.79 3.24 2 15 5 14.90 2.54 17 -2 5 15.21 2.73 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5.55 13 -2 7 54.46 5.60 13 -2 7 53.48 5.12 3 10 -7 114.44 12.08 10 -13 -7 119.00 10.96 3 10 -7 115.46 11.47 13 -3 -7 126.00 11.46 10 -13 -7 134.21 11.24 -3 -10 -7 119.12 11.37 13 -3 -7 130.12 11.26 13 -3 7 65.47 6.57 3 10 7 73.36 6.95 -10 13 7 56.94 6.60 3 10 7 80.83 6.49 10 -13 7 60.83 5.70 -4 -9 -7 88.99 9.22 9 -13 -7 86.12 8.61 4 9 -7 98.59 9.79 -13 4 -7 87.41 8.69 4 9 -7 109.12 9.31 9 -13 -7 96.66 8.93 13 -4 -7 102.72 9.09 13 -4 -7 106.12 8.93 9 -13 7 46.64 4.35 13 -4 7 52.33 5.11 -13 4 7 40.81 4.37 4 9 7 52.29 5.09 4 9 7 59.00 5.49 13 -4 7 50.19 4.71 -9 13 7 51.82 5.35 5 8 -7 30.13 3.35 -8 13 -7 30.46 4.32 13 -5 -7 36.83 3.81 5 8 -7 36.05 4.60 5 8 -7 33.24 3.99 -13 5 -7 32.10 3.14 -5 -8 -7 32.77 3.76 8 -13 -7 40.18 3.90 13 -5 -7 34.57 3.63 13 -5 7 28.74 4.20 13 -5 7 29.72 3.04 5 8 7 27.97 3.25 -13 5 7 26.40 2.68 5 8 7 34.32 3.39 5 8 7 27.41 3.57 -8 13 7 33.44 3.83 -6 -7 -7 37.65 4.48 7 -13 -7 54.47 4.75 6 7 -7 46.40 4.37 6 7 -7 35.12 4.97 -7 13 -7 34.00 5.23 13 -6 -7 51.97 4.54 6 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5.06 13 -15 -7 39.45 4.31 15 -2 -7 43.51 5.15 15 -2 -7 44.11 4.73 2 13 -7 44.20 5.90 15 -2 7 41.71 4.95 2 13 7 47.69 4.41 2 13 7 41.98 4.69 15 -2 7 42.43 4.42 2 13 7 44.68 5.52 3 12 -7 61.58 6.17 3 12 -7 56.16 6.66 15 -3 -7 58.44 6.04 -3 -12 -7 56.49 5.70 15 -3 -7 47.78 5.61 3 12 7 34.95 4.08 15 -3 7 36.85 4.36 3 12 7 40.98 3.95 15 -3 7 35.51 3.80 3 12 7 34.27 4.70 15 -4 -7 89.75 7.82 4 11 -7 85.55 8.51 15 -4 -7 72.03 7.48 -4 -11 -7 73.51 7.47 4 11 -7 73.20 7.86 15 -4 7 42.29 4.40 -11 15 7 35.80 4.94 4 11 7 53.88 4.71 4 11 7 45.37 5.16 4 11 7 43.02 4.72 15 -4 7 47.23 4.91 5 10 -7 35.30 4.44 5 10 -7 41.86 5.22 15 -5 -7 36.47 4.09 15 -5 -7 40.46 4.38 -5 -10 -7 34.13 4.07 10 -15 7 27.59 2.70 15 -5 7 29.43 3.62 5 10 7 32.66 3.52 15 -5 7 29.97 3.20 -10 15 7 26.62 3.87 5 10 7 31.74 3.96 5 10 7 33.85 3.58 6 9 -7 78.11 6.92 6 9 -7 60.30 5.97 -6 -9 -7 55.51 6.26 6 9 -7 58.23 7.00 15 -6 -7 68.49 6.45 15 -6 -7 65.38 6.32 9 -15 -7 73.70 6.51 6 9 7 76.82 6.42 15 -6 7 61.51 6.23 6 9 7 62.96 6.25 9 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39.50 4.13 16 -6 7 34.46 3.78 16 -6 7 38.96 4.15 6 10 7 39.07 4.15 6 10 7 35.70 4.30 10 -16 7 34.41 3.33 -10 16 7 41.29 4.81 7 9 -7 48.02 5.56 7 9 -7 40.79 4.48 7 9 -7 45.19 5.28 16 -7 -7 49.50 5.03 16 -7 -7 49.50 4.91 -7 -9 -7 49.25 4.76 7 9 7 39.05 4.38 -9 16 7 39.77 5.08 16 -7 7 42.37 4.15 9 -16 7 39.66 3.65 -7 -9 7 38.58 3.95 7 9 7 35.74 4.22 7 9 7 35.76 4.24 16 -7 7 38.78 3.95 -8 16 -7 61.81 7.43 8 -16 -7 80.68 6.97 16 -8 -7 66.28 6.64 8 8 -7 69.85 6.49 -8 -8 -7 69.31 6.52 16 -8 -7 63.37 6.60 8 8 7 53.96 5.26 -8 16 7 44.13 6.09 16 -8 7 54.58 5.30 8 -16 7 56.37 5.03 8 8 7 63.35 5.73 16 -8 7 51.62 5.20 8 8 7 47.50 5.41 -8 -8 7 58.22 5.25 7 -16 -7 85.07 7.76 -7 16 -7 73.68 8.39 16 -9 -7 78.39 7.45 9 7 -7 73.03 7.40 9 7 -7 82.42 7.96 9 7 -7 80.43 7.76 9 7 7 95.83 8.19 16 -9 7 80.54 7.59 -9 -7 7 79.93 7.58 16 -9 7 84.50 7.60 9 7 7 76.26 7.79 16 -10 -7 70.42 6.57 10 6 -7 65.24 6.95 -6 16 -7 73.07 7.74 10 6 -7 55.96 6.52 10 6 -7 68.50 6.67 6 -16 -7 79.52 6.95 -10 -6 7 66.89 6.00 10 6 7 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3.01 -7 15 -8 22.45 3.72 8 7 -8 20.50 3.31 -8 -7 -8 19.71 2.73 8 7 -8 20.31 2.62 8 7 -8 18.38 3.14 15 -8 -8 22.66 2.76 8 7 8 9.56 1.62 -7 15 8 6.88 2.17 8 7 8 9.62 1.74 7 -15 8 9.64 1.57 -8 -7 8 10.76 1.70 15 -8 8 10.94 1.75 15 -8 8 9.65 1.57 8 7 8 8.80 2.04 6 -15 -8 23.11 3.02 15 -9 -8 19.44 2.54 -6 15 -8 16.71 3.50 -9 -6 -8 19.28 2.45 9 6 -8 11.15 2.68 9 6 -8 19.87 2.67 9 6 -8 16.19 2.85 -6 15 8 13.80 2.93 9 6 8 11.64 2.25 -9 -6 8 11.42 1.65 15 -9 8 12.26 1.71 9 6 8 9.51 1.84 15 -9 8 10.17 1.67 5 -15 -8 55.00 5.15 15 -10 -8 42.25 4.60 10 5 -8 49.10 5.19 -5 15 -8 49.55 6.03 10 5 -8 38.44 4.71 10 5 -8 46.03 4.94 10 5 8 20.72 3.16 -5 15 8 24.80 3.80 10 5 8 16.25 2.54 15 -10 8 23.53 2.47 -10 -5 8 20.49 2.32 4 -15 -8 32.87 3.76 -4 15 -8 30.06 4.56 15 -11 -8 31.62 3.32 11 4 -8 29.21 3.77 11 4 -8 24.99 3.68 11 4 -8 26.51 3.16 11 4 8 8.40 1.58 11 4 8 6.15 2.07 15 -11 8 10.34 1.55 -4 15 8 8.86 2.54 12 3 -8 28.66 4.19 12 3 -8 44.61 4.47 3 -15 -8 39.08 4.25 -3 15 -8 28.06 4.97 15 -12 -8 35.28 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30.43 3.58 10 3 -9 33.90 3.87 3 -13 -9 31.19 3.83 13 -10 -9 34.55 3.39 10 3 -9 28.23 3.89 -3 13 -9 27.88 4.88 10 3 -9 30.67 3.58 -3 13 9 26.08 2.85 13 -10 9 30.47 2.85 -3 13 9 17.85 3.67 10 3 9 29.84 3.55 -10 -3 9 27.86 2.75 -2 13 -9 34.17 5.34 13 -11 -9 36.38 3.70 11 2 -9 31.41 4.42 2 -13 -9 43.91 4.38 11 2 -9 34.37 3.74 11 2 -9 34.02 4.13 11 2 9 28.46 3.02 -2 13 9 35.19 4.24 -2 13 9 23.54 2.86 13 -11 9 26.73 2.89 11 2 9 28.57 3.64 12 1 -9 22.06 2.94 12 1 -9 18.76 3.33 1 -13 -9 14.98 2.79 -1 13 -9 29.46 4.71 13 -12 -9 16.35 2.35 -1 13 9 16.44 2.15 12 1 9 15.79 2.17 12 1 9 18.81 2.91 -1 13 9 18.06 3.31 13 0 -9 10.44 2.14 0 -13 -9 12.24 2.38 13 -13 -9 8.76 1.62 13 0 -9 7.92 2.42 0 13 -9 11.83 3.20 13 0 9 7.67 1.45 0 13 9 10.82 2.57 13 0 9 7.26 2.09 0 13 9 9.90 1.58 1 13 -9 0.98 2.32 -1 -13 -9 5.10 1.77 14 -1 -9 2.27 1.49 13 -14 -9 2.96 1.18 14 -1 -9 2.06 1.88 1 13 -9 2.08 1.68 14 -1 9 1.76 1.63 14 -1 9 1.22 0.91 1 13 9 3.27 1.92 1 13 9 2.73 1.08 14 -2 -9 21.00 3.34 2 12 -9 18.17 3.82 2 12 -9 23.36 3.35 12 -14 -9 20.08 2.43 -2 -12 -9 19.29 3.03 14 -2 -9 14.08 2.59 2 12 9 9.30 2.36 14 -2 9 7.05 2.02 14 -2 9 8.80 1.45 2 12 9 9.85 1.77 2 12 9 8.87 1.70 14 -3 -9 18.86 2.74 3 11 -9 24.98 4.30 14 -3 -9 22.03 3.18 3 11 -9 14.39 2.92 -3 -11 -9 20.80 2.98 11 -14 -9 18.69 2.41 3 11 9 3.93 1.85 14 -3 9 6.65 1.83 3 11 9 7.88 1.63 3 11 9 4.14 1.35 -11 14 9 6.26 1.77 14 -3 9 5.87 1.26 -4 -10 -9 20.69 3.09 10 -14 -9 26.74 3.09 14 -4 -9 24.56 3.37 4 10 -9 17.06 3.72 14 -4 -9 24.68 2.94 4 10 -9 16.85 3.16 4 10 9 19.55 2.67 14 -4 9 19.47 2.90 14 -4 9 21.52 2.35 4 10 9 21.08 3.17 -10 14 9 18.61 3.10 4 10 9 19.33 2.62 14 -5 -9 80.73 7.45 14 -5 -9 85.43 7.26 5 9 -9 66.32 7.53 5 9 -9 70.42 8.03 -5 -9 -9 71.41 7.39 9 -14 -9 76.33 7.29 5 9 9 51.47 5.13 14 -5 9 51.20 5.21 5 9 9 41.62 5.37 14 -5 9 48.66 4.83 -9 14 9 63.69 5.91 -5 -9 9 53.42 5.06 9 -14 9 46.79 4.56 5 9 9 60.46 5.34 -6 -8 -9 81.89 8.72 14 -6 -9 97.86 8.71 6 8 -9 83.11 8.40 8 -14 -9 104.77 8.82 6 8 -9 101.43 9.45 14 -6 -9 89.44 8.54 -8 14 -9 84.75 9.45 6 8 -9 94.75 9.01 -8 14 9 59.44 5.48 -8 14 9 55.62 6.40 -6 -8 9 64.91 5.69 6 8 9 69.51 6.03 6 8 9 55.29 5.92 14 -6 9 57.56 5.80 14 -6 9 59.82 5.49 6 8 9 53.07 5.68 8 -14 9 54.74 5.30 14 -7 -9 67.20 6.33 -7 -7 -9 64.83 6.45 7 7 -9 58.56 6.65 7 -14 -9 64.60 6.51 7 7 -9 66.90 6.16 14 -7 -9 65.86 6.25 -7 14 9 44.10 5.85 7 7 9 56.84 5.42 7 7 9 57.89 5.59 7 -14 9 55.29 5.03 7 7 9 50.14 5.25 14 -7 9 53.27 5.08 -7 -7 9 56.70 5.24 14 -7 9 55.02 5.30 8 6 -9 25.48 3.12 6 -14 -9 32.83 3.50 -8 -6 -9 22.03 3.07 14 -8 -9 24.33 3.00 8 6 -9 23.52 3.65 -6 14 -9 26.91 4.27 8 6 -9 29.27 3.54 -6 14 9 31.45 3.87 -6 14 9 24.48 2.46 -8 -6 9 22.48 2.65 14 -8 9 22.04 2.70 6 -14 9 26.06 2.67 8 6 9 19.24 2.71 8 6 9 22.28 2.63 14 -8 9 23.82 2.56 8 6 9 27.02 3.27 -9 -5 -9 18.28 2.52 -5 14 -9 19.83 4.05 9 5 -9 17.84 2.73 5 -14 -9 22.09 3.03 14 -9 -9 19.96 2.51 9 5 -9 17.02 2.93 9 5 -9 18.91 2.95 5 -14 9 39.79 4.09 9 5 9 37.34 4.15 -9 -5 9 42.69 4.05 14 -9 9 42.98 4.06 -5 14 9 46.75 5.31 9 5 9 40.77 4.58 14 -9 9 40.08 4.00 10 4 -9 14.17 2.51 -4 14 -9 13.36 3.44 10 4 -9 13.65 2.34 14 -10 -9 13.58 2.13 -10 -4 -9 12.28 1.97 4 -14 -9 16.35 2.66 10 4 -9 14.23 2.51 -4 14 9 19.59 2.14 -10 -4 9 17.73 2.16 14 -10 9 19.52 2.25 10 4 9 19.60 2.44 -4 14 9 17.73 3.41 10 4 9 23.81 3.06 11 3 -9 23.62 2.95 -11 -3 -9 23.24 3.38 3 -14 -9 30.92 3.61 -3 14 -9 20.85 4.38 11 3 -9 24.55 3.63 14 -11 -9 26.03 2.97 11 3 -9 30.60 3.50 -3 14 9 34.57 4.41 11 3 9 21.05 2.94 14 -11 9 25.51 2.90 -3 14 9 33.40 2.92 11 3 9 24.59 3.62 -2 14 -9 38.53 5.53 12 2 -9 45.85 4.64 12 2 -9 29.96 4.55 2 -14 -9 42.71 4.67 14 -12 -9 40.03 4.10 12 2 9 36.17 4.22 12 2 9 40.39 4.82 -2 14 9 40.88 4.23 -2 14 9 50.54 5.57 14 -12 9 47.03 4.20 13 1 -9 21.97 3.78 1 -14 -9 29.12 3.67 -1 14 -9 29.45 4.74 13 1 -9 26.70 3.55 14 -13 -9 28.46 3.13 -1 14 9 21.29 3.65 13 1 9 22.50 3.23 13 1 9 19.01 2.45 14 0 -9 9.65 2.64 0 14 -9 15.55 3.53 14 -14 -9 11.00 1.83 14 0 -9 10.88 2.22 0 -14 -9 13.94 2.48 14 0 9 6.66 1.40 14 0 9 10.32 2.28 0 14 9 9.09 2.54 15 -1 -9 3.79 2.03 -1 -14 -9 6.73 1.84 14 -15 -9 6.19 1.43 1 14 -9 3.32 2.48 15 -1 -9 5.88 1.80 1 14 -9 5.49 2.05 1 14 9 5.39 1.59 1 14 9 9.18 2.57 15 -1 9 7.01 1.97 -1 -14 9 8.60 1.58 2 13 -9 9.67 4.94 2 13 -9 17.47 3.78 -2 -13 -9 12.00 2.55 13 -15 -9 12.26 2.40 15 -2 -9 13.15 2.96 15 -2 -9 9.23 3.29 2 13 9 16.56 2.26 2 13 9 15.17 3.39 -2 -13 9 17.63 2.40 2 13 9 18.51 2.56 15 -2 9 15.37 2.18 15 -2 9 17.48 3.73 3 12 -9 17.93 3.62 15 -3 -9 13.48 2.36 15 -3 -9 18.55 2.98 3 12 -9 11.35 2.67 -3 -12 -9 15.00 2.56 3 12 9 14.34 2.82 15 -3 9 15.95 2.66 3 12 9 12.66 2.17 15 -3 9 10.25 1.77 3 12 9 13.78 2.13 -3 -12 9 17.55 2.28 -4 -11 -9 21.28 2.84 15 -4 -9 25.10 3.32 15 -4 -9 18.25 2.76 4 11 -9 15.83 3.54 4 11 -9 17.36 3.13 15 -4 9 11.18 2.31 -11 15 9 13.51 2.56 4 11 9 13.15 2.12 15 -4 9 11.01 1.76 4 11 9 15.70 2.85 -4 -11 9 14.80 2.15 4 11 9 16.97 2.35 5 10 -9 38.63 5.58 -5 -10 -9 40.18 4.76 10 -15 -9 50.84 4.85 15 -5 -9 38.31 4.59 15 -5 -9 47.24 5.03 5 10 -9 51.07 5.21 -10 15 9 29.98 3.96 15 -5 9 30.07 3.47 5 10 9 25.43 3.20 5 10 9 28.57 3.78 10 -15 9 27.06 2.52 15 -5 9 24.52 2.93 -5 -10 9 32.85 3.28 5 10 9 30.15 3.46 15 -6 -9 93.17 8.36 6 9 -9 84.99 8.60 6 9 -9 81.14 8.88 15 -6 -9 81.05 8.15 9 -15 -9 93.22 8.36 6 9 9 56.12 5.51 -6 -9 9 67.16 5.55 6 9 9 52.62 5.65 6 9 9 47.78 5.66 15 -6 9 62.11 5.67 9 -15 9 59.05 5.01 -9 15 9 45.87 6.08 15 -6 9 50.86 5.23 15 -7 -9 114.44 10.42 -8 15 -9 105.33 11.31 7 8 -9 116.58 10.85 7 8 -9 107.07 10.13 8 -15 -9 127.54 10.65 7 8 -9 102.31 10.94 -7 -8 -9 120.48 10.59 15 -7 -9 109.89 10.39 7 8 9 99.04 7.97 7 8 9 81.26 7.69 8 -15 9 73.31 7.22 15 -7 9 79.66 7.60 7 8 9 77.82 7.58 15 -7 9 77.92 7.38 -7 -8 9 83.43 7.54 -8 15 9 83.15 8.47 8 7 -9 93.48 8.42 7 -15 -9 100.55 8.83 8 7 -9 105.27 9.17 8 7 -9 85.68 8.90 15 -8 -9 90.01 8.49 -7 15 -9 88.16 9.64 -8 -7 -9 77.90 8.52 8 7 9 79.68 7.23 15 -8 9 75.94 7.18 7 -15 9 79.96 7.15 8 7 9 81.28 7.71 -8 -7 9 80.39 7.33 15 -8 9 73.72 7.29 8 7 9 79.69 7.42 6 -15 -9 51.86 5.40 15 -9 -9 46.44 5.03 -6 15 -9 46.91 6.23 9 6 -9 56.53 5.51 9 6 -9 49.15 5.54 9 6 -9 57.58 5.17 -9 -6 -9 44.98 5.02 9 6 9 65.13 6.81 -9 -6 9 64.14 6.33 6 -15 9 76.82 6.36 15 -9 9 70.79 6.32 9 6 9 56.88 6.42 -6 15 9 80.66 7.64 15 -9 9 65.25 6.32 10 5 -9 32.72 3.94 10 5 -9 39.54 4.37 -10 -5 -9 29.19 3.65 5 -15 -9 42.13 4.25 15 -10 -9 34.15 3.73 10 5 -9 32.54 4.01 -5 15 -9 41.76 5.28 5 -15 9 56.44 4.86 15 -10 9 50.33 4.72 -10 -5 9 48.07 4.69 10 5 9 43.27 4.83 -5 15 9 54.95 6.07 10 5 9 40.81 5.20 15 -11 -9 11.55 1.94 11 4 -9 12.71 2.47 -4 15 -9 11.07 3.03 11 4 -9 13.37 2.12 4 -15 -9 15.97 2.69 11 4 -9 14.89 2.51 -4 15 9 25.52 4.38 15 -11 9 31.44 3.17 4 -15 9 32.25 3.30 11 4 9 26.35 3.22 11 4 9 33.67 4.00 -3 15 -9 28.44 4.90 12 3 -9 26.72 3.96 15 -12 -9 34.48 3.61 3 -15 -9 36.08 4.08 12 3 -9 32.14 4.05 15 -12 9 43.02 3.92 12 3 9 33.79 3.95 12 3 9 41.97 4.72 -3 15 9 37.43 5.20 -2 15 -9 38.59 5.31 2 -15 -9 38.40 4.53 15 -13 -9 35.37 4.38 13 2 -9 28.94 4.46 13 2 9 28.71 3.16 15 -14 -9 9.45 1.73 1 -15 -9 12.69 2.32 14 1 -9 10.26 2.45 -1 15 -9 8.59 2.76 14 1 -9 9.29 2.11 -1 15 9 13.93 3.05 14 1 9 9.69 2.33 14 1 9 9.21 1.60 15 0 -9 -0.53 1.67 0 -15 -9 2.42 1.56 15 -15 -9 0.77 1.09 0 15 -9 0.77 2.18 15 0 -9 -0.74 1.32 0 15 -9 0.92 1.63 0 15 9 0.80 1.78 15 0 9 -0.65 1.48 0 -15 9 3.02 1.16 1 15 -9 9.22 2.51 1 15 -9 13.26 3.18 -1 -15 -9 13.37 2.28 16 -1 -9 11.15 2.63 16 -1 -9 13.06 2.33 -1 -15 9 16.03 2.11 1 15 9 10.04 2.69 16 -1 9 15.86 2.75 1 15 9 10.45 2.10 -2 -14 -9 17.51 2.60 2 14 -9 13.10 2.65 16 -2 -9 13.79 2.43 2 14 -9 14.41 3.18 16 -2 -9 13.32 2.76 2 14 9 22.07 3.56 16 -2 9 12.46 2.24 -2 -14 9 23.43 2.54 2 14 9 16.66 2.53 16 -2 9 17.14 2.91 16 -3 -9 8.84 2.34 3 13 -9 7.28 2.62 16 -3 -9 4.95 1.70 -3 -13 -9 7.86 1.80 3 13 -9 4.80 1.95 3 13 9 12.35 2.63 16 -3 9 5.91 1.43 3 13 9 10.06 1.61 3 13 9 9.02 1.81 -3 -13 9 12.62 1.93 16 -3 9 9.44 2.18 -4 -12 -9 27.39 3.36 4 12 -9 24.39 4.43 16 -4 -9 25.45 3.90 4 12 -9 28.35 4.00 16 -4 -9 29.38 3.48 -4 -12 9 16.82 2.27 4 12 9 11.02 2.41 4 12 9 16.71 2.27 16 -4 9 14.33 2.48 4 12 9 9.59 1.98 16 -4 9 12.76 1.97 -5 -11 -9 30.36 4.51 16 -5 9 13.74 1.95 5 11 9 12.00 2.17 -5 -11 9 19.00 2.78 6 10 -9 82.77 8.22 6 10 -9 84.75 8.52 16 -6 -9 86.34 7.89 -6 -10 -9 74.74 7.73 16 -6 -9 78.59 7.73 6 10 9 56.82 5.78 16 -6 9 54.42 5.51 -10 16 9 58.88 6.55 -6 -10 9 55.75 5.69 6 10 9 60.45 6.04 10 -16 9 59.52 5.14 6 10 9 59.66 5.97 16 -6 9 67.04 5.95 7 9 -9 105.11 10.22 9 -16 -9 105.72 9.88 -7 -9 -9 113.06 9.87 16 -7 -9 93.59 9.70 7 9 -9 109.28 10.44 -7 -9 9 86.27 7.83 16 -7 9 78.19 7.65 7 9 9 83.10 7.94 -9 16 9 94.00 8.84 7 9 9 78.24 7.84 9 -16 9 82.74 7.43 7 9 9 86.01 8.09 16 -7 9 88.49 7.93 8 -16 -9 79.75 6.99 8 8 -9 61.03 7.12 8 8 -9 65.91 7.16 -8 -8 -9 71.05 6.72 16 -8 -9 74.66 6.75 -8 16 -9 59.94 7.48 8 8 -9 68.35 6.44 16 -8 9 70.68 6.51 -8 -8 9 82.07 6.56 8 -16 9 71.46 6.23 -8 16 9 63.76 7.42 8 8 9 66.96 6.79 8 8 9 67.65 6.32 16 -8 9 62.43 6.32 8 8 9 59.97 6.48 9 7 -9 74.93 7.65 -7 16 -9 66.38 8.01 9 7 -9 75.41 7.04 7 -16 -9 79.37 7.40 9 7 -9 81.47 7.55 -9 -7 -9 76.17 7.07 16 -9 -9 67.77 7.08 16 -9 9 76.72 7.12 16 -9 9 73.05 7.14 -7 16 9 80.87 8.30 -9 -7 9 81.13 7.22 9 7 9 77.17 7.67 10 6 -9 29.50 4.08 10 6 -9 30.82 3.50 10 6 -9 27.48 3.67 16 -10 -9 32.08 3.51 -6 16 -9 28.31 4.50 6 -16 -9 37.51 3.96 -10 -6 9 35.20 3.53 6 -16 9 37.19 3.61 -6 16 9 39.59 4.87 10 6 9 38.52 4.21 10 6 9 28.44 3.63 16 -10 9 32.38 3.50 11 5 -9 12.95 2.18 11 5 9 11.71 1.97 16 -11 9 15.48 2.01 4 -16 -9 20.98 2.91 -4 16 -9 21.76 4.01 16 -12 -9 15.70 2.38 12 4 -9 14.12 2.51 12 4 -9 13.72 2.69 12 4 9 10.76 2.26 4 -16 9 22.43 2.36 12 4 9 15.83 2.90 16 -12 9 16.23 2.18 -4 16 9 18.76 3.50 13 3 -9 21.39 3.21 -3 16 -9 23.78 4.02 16 -13 -9 16.52 2.56 3 -16 -9 19.59 3.01 13 3 -9 17.58 2.94 3 -16 9 27.19 3.05 13 3 9 22.82 3.63 -3 16 9 27.23 4.37 14 2 -9 25.57 3.64 14 2 -9 24.57 3.62 2 -16 -9 29.05 3.63 16 -14 -9 27.14 3.20 -2 16 -9 31.41 4.79 2 -16 9 40.25 4.02 -2 16 9 43.19 5.28 14 2 9 31.23 4.52 1 -16 -9 4.18 1.69 15 1 -9 5.13 1.84 16 -15 -9 5.66 1.45 -1 16 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3.01 17 -5 -9 16.70 2.78 17 -5 -9 12.20 2.26 5 12 9 6.39 1.58 5 12 9 9.03 2.11 17 -5 9 9.52 1.96 5 12 9 14.19 2.00 -5 -12 9 9.76 1.67 17 -5 9 6.10 1.43 6 11 -9 33.80 4.83 -6 -11 -9 35.06 3.82 17 -6 -9 33.12 3.93 17 -6 -9 38.10 4.23 6 11 -9 33.76 4.45 17 -6 9 36.68 3.57 -11 17 9 39.65 4.29 6 11 9 25.13 3.33 17 -6 9 25.84 3.13 6 11 9 30.46 3.52 6 11 9 29.37 3.65 -7 -10 -9 74.19 7.33 7 10 -9 73.77 7.87 7 10 -9 87.70 8.16 17 -7 -9 77.30 7.48 17 -7 9 62.98 6.16 7 10 9 71.17 6.62 7 10 9 59.90 6.34 -7 -10 9 72.73 6.36 17 -7 9 69.49 6.47 7 10 9 64.44 6.37 8 9 -9 61.34 6.83 -8 -9 -9 66.67 6.28 17 -8 -9 65.14 6.35 8 9 -9 65.18 6.83 8 9 9 54.42 6.22 -9 17 9 76.83 7.36 -8 -9 9 72.72 6.25 8 9 9 61.09 5.96 17 -8 9 65.83 6.11 17 -8 9 66.82 6.24 9 8 -9 61.28 6.51 8 -17 -9 71.24 6.51 9 8 -9 67.04 6.77 9 8 -9 58.71 5.95 -8 17 -9 67.42 7.16 17 -9 -9 60.98 6.23 -9 -8 9 59.61 5.37 -8 17 9 57.28 6.50 17 -9 9 57.14 5.31 17 -9 9 56.27 5.27 9 8 9 46.90 5.37 10 7 -9 26.20 3.36 7 -17 -9 36.68 3.79 10 7 -9 27.85 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144.48 12.81 -7 13 -11 126.49 13.50 -6 -7 -11 129.07 12.74 13 -6 -11 131.76 12.47 6 7 -11 166.00 13.49 6 7 11 73.07 7.52 13 -6 11 80.28 7.12 -6 -7 11 90.44 7.40 13 -6 11 81.14 7.45 -7 13 11 80.78 8.07 7 -13 11 77.55 7.05 6 7 11 68.62 7.50 6 7 11 75.92 7.28 13 -7 -11 157.53 12.69 -6 13 -11 141.05 13.95 7 6 -11 140.26 12.60 -7 -6 -11 142.28 12.91 6 -13 -11 120.42 12.84 7 6 -11 145.57 13.03 7 6 -11 137.89 13.23 6 -13 11 102.96 8.50 -6 13 11 96.11 9.42 7 6 11 112.16 9.04 13 -7 11 90.22 8.43 13 -7 11 88.91 8.62 -7 -6 11 96.67 8.62 7 6 11 90.13 8.70 7 6 11 82.00 8.55 -5 13 -11 128.05 12.33 5 -13 -11 116.19 11.08 8 5 -11 115.10 11.04 8 5 -11 118.47 10.82 13 -8 -11 103.10 10.60 8 5 -11 133.53 11.30 5 -13 11 81.44 8.32 8 5 11 84.83 8.34 -5 13 11 99.52 9.33 -8 -5 11 96.75 8.37 -5 13 11 88.52 8.27 8 5 11 104.74 8.87 13 -8 11 95.65 8.74 -4 13 -11 41.46 6.57 -9 -4 -11 46.03 5.24 9 4 -11 59.65 5.62 9 4 -11 51.10 5.44 13 -9 -11 53.54 5.07 4 -13 -11 51.30 5.60 9 4 -11 58.91 5.56 -4 13 11 48.32 5.89 9 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0 28 2.47 1.18 -5 6 -28 -0.20 1.53 -6 1 -28 4.33 1.63 -1 -5 -28 3.47 1.62 -5 6 28 1.05 1.16 6 -1 28 6.48 1.21 -1 -5 28 2.88 1.11 -6 1 28 4.19 1.31 1 5 28 1.49 1.00 -5 6 28 1.87 1.30 1 5 28 3.76 1.22 -4 6 -28 4.95 2.05 -6 2 -28 7.01 1.96 -2 -4 -28 6.97 1.90 2 4 28 3.53 1.07 -4 6 28 3.24 1.39 -4 6 28 3.33 1.22 -2 -4 28 2.86 1.16 -6 2 28 4.74 1.46 2 4 28 5.02 1.33 -6 3 -28 3.27 1.65 -3 -3 -28 4.09 1.69 -3 6 -28 0.56 1.40 -3 -3 28 -0.79 1.01 -3 6 28 0.57 1.01 -3 6 28 0.46 1.14 3 3 28 0.85 1.04 -6 3 28 -0.39 1.05 -4 -2 -28 2.33 1.48 -2 6 -28 -2.60 1.34 -6 4 -28 0.66 1.55 2 -6 -28 3.42 1.37 -6 4 28 1.31 1.14 -4 -2 28 4.14 1.30 -2 6 28 1.63 1.28 -2 6 28 4.84 1.37 -6 4 28 3.99 1.40 4 2 28 4.90 1.27 -5 -1 -28 0.91 1.38 1 -6 -28 3.61 1.37 -6 5 -28 -1.00 1.36 -6 5 28 1.74 1.28 -5 -1 28 0.26 1.03 -1 6 28 1.75 1.07 -6 5 28 0.85 1.06 -1 6 28 0.84 1.18 -5 -1 28 -1.55 1.05 5 1 28 2.01 0.93 1 -6 28 0.11 0.84 0 -6 -28 3.23 1.35 -6 0 -28 2.34 1.41 -6 6 -28 -1.41 1.32 6 0 28 5.03 1.11 0 6 28 3.21 1.21 -6 0 28 3.23 1.31 0 -6 28 2.48 1.06 -6 6 28 5.41 1.56 0 6 28 3.18 1.22 -6 6 28 1.53 1.07 -6 7 -28 2.55 1.85 -1 -6 -28 5.69 1.65 -7 1 -28 4.61 1.59 -6 7 28 5.96 1.58 -1 -6 28 2.65 1.08 -6 7 28 2.24 1.09 1 6 28 0.94 0.90 1 6 28 4.03 1.24 -7 1 28 3.36 1.29 -2 -5 -28 5.02 1.63 -5 7 -28 4.45 1.93 -7 2 -28 3.99 1.60 -7 2 28 4.25 1.38 -2 -5 28 3.98 1.30 -5 7 28 4.10 1.46 2 5 28 6.65 1.42 -5 7 28 6.08 1.37 2 5 28 9.12 1.78 -7 3 -28 0.86 1.43 -4 7 -28 -1.97 1.23 -3 -4 -28 4.01 1.64 -7 3 28 0.74 1.13 -4 7 28 0.85 1.06 -3 -4 28 0.74 1.07 3 4 28 1.20 1.02 -4 7 28 1.54 1.29 -4 -3 -28 4.28 1.68 -7 4 -28 2.24 1.63 3 -7 -28 3.26 1.26 -3 7 -28 -0.20 1.69 -4 -3 28 1.65 1.12 -7 4 28 1.05 1.17 -3 7 28 3.41 1.17 -3 7 28 1.35 1.20 4 3 28 3.93 1.17 -7 5 -28 0.43 1.56 -5 -2 -28 2.72 1.39 2 -7 28 -0.17 0.76 -2 7 28 -0.97 0.82 -5 -2 28 0.72 1.04 5 2 28 2.28 1.10 -7 5 28 0.90 1.20 -2 7 28 -0.04 0.96 1 -7 -28 2.00 1.33 -6 -1 -28 1.86 1.38 -7 6 -28 0.76 1.52 -1 7 28 -0.28 1.04 -7 6 28 -0.39 1.02 1 -7 28 -1.06 0.73 -7 6 28 -0.06 0.91 -1 7 28 0.82 0.98 6 1 28 2.05 0.98 -6 -1 28 -1.08 0.92 -7 0 -28 4.03 1.51 0 -7 -28 3.99 1.41 -7 7 -28 3.31 1.75 -7 7 28 0.31 0.87 -7 0 28 2.02 1.21 0 -7 28 0.78 0.91 0 7 28 0.63 0.86 0 7 28 1.41 1.01 -7 7 28 1.22 1.19 -1 -7 -28 10.84 2.14 -8 1 -28 15.09 2.47 -7 8 28 4.59 1.50 -7 8 28 5.10 1.25 -8 1 28 5.74 1.62 -1 -7 28 3.69 1.16 1 7 28 8.20 1.46 -8 2 -28 10.16 2.12 -2 -6 -28 13.31 2.22 -2 -6 28 3.11 1.24 -6 8 28 5.45 1.23 2 6 28 7.64 1.38 -6 8 28 6.99 1.63 -8 2 28 3.79 1.39 -3 -5 -28 2.26 1.41 -8 3 -28 0.16 1.18 3 5 28 4.57 1.15 -5 8 28 3.29 1.18 -5 8 28 3.58 1.34 -3 -5 28 0.38 1.03 -8 3 28 2.28 1.20 -8 4 -28 -0.27 1.21 -4 8 -28 0.92 1.36 -4 -4 -28 0.95 1.24 -4 8 28 3.05 1.12 4 4 28 4.33 1.13 -4 8 28 5.71 1.27 -4 -4 28 0.85 1.05 -8 4 28 2.29 1.29 -8 5 -28 -0.39 1.40 -5 -3 -28 1.78 1.36 -3 8 28 -0.33 0.98 -8 5 28 -1.70 1.03 -3 8 28 -0.89 0.86 -5 -3 28 -1.26 0.84 5 3 28 1.66 0.93 -8 6 -28 0.34 1.54 2 -8 -28 4.63 1.55 -6 -2 -28 5.75 1.60 -8 6 28 -0.90 1.15 -6 -2 28 -0.60 1.02 -2 8 28 -0.28 0.91 6 2 28 0.75 1.19 -2 8 28 -0.08 0.85 -7 -1 -28 6.44 1.79 -8 7 -28 4.70 1.89 -8 7 28 2.18 0.97 -7 -1 28 2.44 1.25 -8 7 28 2.93 1.51 -1 8 28 2.81 1.12 7 1 28 3.88 0.98 -1 8 28 2.95 1.84 0 0 -29 -0.10 1.15 0 0 29 -1.05 0.92 0 0 29 -2.07 0.73 0 1 -29 1.47 1.17 -1 0 -29 2.29 1.30 0 -1 -29 2.38 1.20 -1 1 -29 0.67 1.21 1 -1 -29 5.12 1.36 0 1 29 -0.14 1.02 1 -1 29 -0.13 0.89 0 -1 29 1.37 1.11 1 0 29 0.07 0.86 1 0 29 -0.13 0.96 1 -1 29 0.66 0.93 -1 1 29 0.52 1.09 -1 1 29 0.61 0.91 -1 0 29 -1.77 0.77 -1 0 29 0.12 1.01 0 -1 29 0.35 0.81 0 1 29 0.35 0.91 -1 -1 -29 0.64 1.22 -1 2 -29 0.33 1.33 -2 1 -29 0.39 1.28 1 -2 -29 -0.61 1.15 -1 2 29 0.25 1.05 -1 2 29 1.21 1.04 -1 -1 29 -0.96 0.88 1 -2 29 -0.31 0.90 1 1 29 -1.69 0.88 2 -1 29 -1.37 0.79 -1 -1 29 -1.34 0.82 2 -1 29 -0.59 0.82 1 1 29 1.26 1.00 -2 1 29 -0.29 1.09 -2 1 29 0.51 0.89 -2 2 -29 1.89 1.43 0 2 -29 3.14 1.91 0 -2 -29 0.88 1.25 -2 0 -29 1.45 1.38 -2 2 29 -1.19 0.96 0 2 29 -0.23 0.91 0 2 29 -0.60 1.00 -2 0 29 -0.41 1.04 2 0 29 -1.12 0.78 -2 2 29 0.64 0.98 0 -2 29 -0.88 0.94 2 0 29 -0.87 0.76 -1 -2 -29 4.86 1.65 -3 1 -29 8.30 1.94 -2 3 -29 4.44 1.61 -1 -2 29 9.08 1.65 1 2 29 8.13 1.59 -3 1 29 6.47 1.41 2 -3 29 8.34 1.45 -2 3 29 6.57 1.67 -2 3 29 9.25 1.63 1 2 29 9.14 1.57 -3 1 29 7.55 1.65 -3 2 -29 10.70 2.33 1 -3 -29 13.93 2.26 -2 -1 -29 10.46 2.31 -3 2 29 1.67 1.10 -1 3 29 5.95 1.31 -2 -1 29 5.18 1.44 1 -3 29 1.65 1.00 2 1 29 4.21 1.05 -1 3 29 2.04 1.21 2 1 29 2.00 0.97 -3 2 29 5.33 1.46 0 -3 -29 6.66 1.70 -3 0 -29 4.84 1.78 -3 3 -29 7.56 1.99 -3 3 29 5.40 1.55 -3 3 29 4.91 1.28 -3 0 29 3.03 1.36 0 3 29 3.78 1.17 3 -3 29 5.78 1.31 -3 0 29 5.44 1.21 0 3 29 6.90 1.55 0 -3 29 5.91 1.39 3 0 29 3.95 1.09 -1 -3 -29 23.01 3.04 -4 1 -29 19.09 3.11 -4 1 29 8.42 1.84 -3 4 29 14.37 2.12 1 3 29 12.76 2.01 1 3 29 18.45 2.13 -3 4 29 18.69 2.50 -4 1 29 14.85 2.39 -1 -3 29 13.33 2.15 -2 -2 -29 23.62 3.21 -4 2 -29 20.58 3.12 -2 4 -29 20.36 3.04 -2 4 29 17.75 2.30 -4 2 29 15.18 2.22 -4 2 29 17.56 2.59 -2 -2 29 15.52 2.36 2 2 29 15.92 2.19 -2 4 29 17.53 2.57 2 -4 29 14.12 2.06 -3 -1 -29 23.43 3.24 -1 4 -29 26.20 3.12 1 -4 -29 25.32 3.06 -4 3 -29 16.63 3.11 1 -4 29 10.31 1.81 -4 3 29 8.22 1.64 -1 4 29 15.63 1.96 3 1 29 14.62 1.84 -4 3 29 8.99 1.99 -1 4 29 9.78 1.90 -3 -1 29 11.20 1.96 -4 0 -29 14.85 2.86 0 -4 -29 22.80 2.83 -4 4 29 6.61 1.62 -4 0 29 12.93 2.00 0 -4 29 8.28 1.54 0 4 29 13.15 1.79 4 0 29 7.17 1.88 0 4 29 6.74 1.47 -4 4 29 6.74 1.50 -1 -4 -29 19.12 2.69 -5 1 -29 16.54 2.66 -4 5 -29 14.19 2.68 -5 1 29 16.37 2.26 -4 5 29 10.15 1.96 1 4 29 13.49 2.19 1 4 29 16.08 2.08 -4 5 29 13.01 2.06 -1 -4 29 11.79 2.06 -2 -3 -29 27.49 3.52 -5 2 -29 25.61 3.51 2 3 29 21.52 2.62 -3 5 29 22.02 2.61 2 3 29 21.84 2.53 -5 2 29 21.35 2.78 -5 2 29 20.28 2.60 -2 -3 29 16.92 2.61 -3 5 29 19.51 2.79 -5 3 -29 16.76 2.78 2 -5 -29 20.19 2.91 -2 5 -29 17.04 2.74 -3 -2 -29 17.02 2.82 -5 3 29 18.35 2.47 -5 3 29 12.86 2.12 -2 5 29 13.21 2.32 3 2 29 16.21 2.15 -2 5 29 17.66 2.28 1 -5 -29 14.70 2.18 -5 4 -29 8.24 2.12 -4 -1 -29 11.83 2.36 -1 5 29 6.50 1.50 -1 5 29 8.15 1.56 -4 -1 29 6.64 1.53 -5 4 29 8.55 1.61 1 -5 29 7.68 1.49 4 1 29 9.47 1.63 -5 4 29 8.21 1.71 -5 0 -29 9.89 1.89 -5 5 -29 5.38 1.92 0 -5 29 8.41 1.56 0 5 29 15.07 1.93 -5 5 29 9.94 1.86 -5 5 29 8.09 1.61 -5 0 29 11.57 1.94 -6 1 -29 23.82 3.10 -1 -5 -29 21.77 2.99 -1 -5 29 17.20 2.60 -6 1 29 22.75 2.84 -5 6 29 20.56 2.53 -5 6 29 25.04 2.90 -6 2 -29 9.29 2.03 -4 6 -29 14.14 2.64 -2 -4 29 13.10 2.27 2 4 29 20.81 2.31 -6 2 29 19.32 2.48 -4 6 29 14.86 2.50 -4 6 29 18.54 2.35 -3 -3 -29 26.37 3.35 -6 3 -29 21.29 3.33 -3 6 -29 26.57 4.43 3 3 29 17.37 2.08 -3 6 29 13.39 2.28 -3 6 29 17.69 2.18 -6 3 29 14.02 2.26 -6 3 29 10.76 1.94 -6 4 -29 3.00 1.51 -4 -2 -29 5.71 1.59 2 -6 29 2.47 1.19 -6 4 29 6.12 1.36 -6 4 29 6.12 1.44 4 2 29 4.35 1.24 -4 -2 29 4.94 1.35 -2 6 29 8.00 1.48 -2 6 29 6.00 1.51 1 -6 -29 12.57 2.70 -6 5 -29 6.03 1.85 -5 -1 -29 7.50 1.79 -1 6 29 11.26 2.06 1 -6 29 13.06 2.45 -6 5 29 12.16 1.98 -6 5 29 14.56 2.38 -1 6 29 18.43 2.05 0 -6 -29 27.38 3.64 0 6 29 22.56 2.46 -6 6 29 21.66 2.45 0 6 29 16.21 2.32 -6 0 29 15.88 2.52 -6 6 29 19.35 2.72 -7 3 -29 16.07 2.78 -3 -4 29 5.27 1.48 -4 7 29 9.70 1.86 -7 3 29 7.31 1.70 -4 7 29 10.08 1.55 -7 3 29 7.95 1.67 -7 4 -29 2.75 1.53 -4 -3 -29 6.70 1.66 -3 7 29 8.93 1.78 -3 7 29 7.75 1.45 4 3 29 10.25 2.17 -7 4 29 4.87 1.55 0 0 30 17.72 2.41 0 -1 -30 54.59 5.08 -1 0 -30 40.47 5.33 1 0 30 29.88 3.22 0 1 30 23.94 3.25 1 0 30 31.77 3.54 -1 1 30 27.78 3.37 -1 1 30 38.45 3.99 -2 1 -30 39.36 5.20 1 1 30 45.84 4.64 -2 1 30 43.51 3.95 -1 2 30 36.23 4.50 1 -2 30 29.09 4.00 -2 0 -30 85.39 9.33 -2 2 -30 84.62 8.23 -2 2 30 43.01 5.16 0 2 30 67.03 5.96 0 2 30 54.65 5.42 -1 -2 -30 105.74 10.55 -3 1 -30 98.76 10.71 -3 1 30 54.58 5.65 -1 -2 30 58.44 5.59 -3 2 -30 100.57 9.31 -2 -1 -30 82.38 9.13 -2 -1 30 71.15 6.54 -3 2 30 70.50 6.56 2 1 30 67.58 6.29 1 -3 30 59.71 6.38 0 -3 -30 113.87 9.96 -3 3 -30 99.34 10.04 -3 3 30 88.04 7.66 -3 0 30 71.36 7.50 -1 -3 30 46.56 5.64 -4 1 30 55.67 5.28 -4 2 -30 105.68 9.83 -2 -2 -30 77.46 8.94 -4 2 30 57.50 5.55 -4 2 30 57.51 5.75 -3 -1 -30 66.71 8.04 -3 -1 30 71.37 6.90 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 72350 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z+1/3' '-x+y, -x, z+2/3' '-x, -y, z+1/2' 'y, -x+y, z+5/6' 'x-y, x, z+1/6' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Tb1 Tb 0.00031(3) 0.02756(2) 0.00102(2) 0.01285(10) Uani 1 1 d . . . . . P1 P 0.13002(10) -0.03394(10) -0.04370(6) 0.0140(3) Uani 1 1 d . . . . . P2 P -0.16899(10) -0.14073(10) 0.04730(6) 0.0144(3) Uani 1 1 d . . . . . P3 P -0.09963(11) 0.12925(11) 0.08283(7) 0.0173(3) Uani 1 1 d . . . . . O1 O 0.0873(3) 0.0101(3) -0.07962(17) 0.0165(9) Uani 1 1 d . . . . . O2 O 0.0883(3) -0.0466(3) 0.01510(16) 0.0168(8) Uani 1 1 d . . . . . O3 O 0.1264(3) -0.1165(3) -0.06886(18) 0.0196(9) Uani 1 1 d . . . . . O4 O -0.1335(3) -0.1244(3) -0.01343(16) 0.0176(9) Uani 1 1 d . . . . . O5 O -0.0924(3) -0.0648(3) 0.08161(17) 0.0173(9) Uani 1 1 d . . . . . O6 O -0.2607(3) -0.1511(3) 0.05541(19) 0.0224(9) Uani 1 1 d . . . . . O7 O -0.0846(3) 0.0900(3) 0.02900(18) 0.0239(10) Uani 1 1 d . . . . . O8 O -0.0664(3) 0.1062(3) 0.13683(17) 0.0219(9) Uani 1 1 d . . . . . O9 O -0.0625(3) 0.2297(3) 0.0758(2) 0.0273(10) Uani 1 1 d . . . . . O10 O -0.1325(5) 0.3256(4) 0.0992(3) 0.0469(16) Uani 1 1 d G . . . . H10C H -0.120651 0.281787 0.091481 0.070 Uiso 1 1 d G U . . . O11 O -0.1759(6) 0.2566(5) 0.1818(3) 0.066(2) Uani 1 1 d . . . . . O1W O -0.3967(7) -0.2964(8) 0.1143(6) 0.118(4) Uani 1 1 d G . . . . H1WA H -0.364820 -0.241539 0.093345 0.178 Uiso 1 1 d G U . . . H1WB H -0.455212 -0.326509 0.097362 0.178 Uiso 1 1 d G U . . . O2W O -0.0562(3) -0.2478(3) -0.0585(2) 0.0261(10) Uani 1 1 d G . . . . H2WA H 0.006430 -0.228365 -0.062318 0.039 Uiso 1 1 d G U . . . H2WB H -0.087854 -0.222683 -0.077360 0.039 Uiso 1 1 d G U . . . C1 C 0.2505(4) 0.0496(4) -0.0404(3) 0.0216(13) Uani 1 1 d . . . . . H1A H 0.281963 0.023742 -0.018588 0.026 Uiso 1 1 calc R U . . . H1B H 0.275572 0.061818 -0.079380 0.026 Uiso 1 1 calc R U . . . C2 C 0.3654(4) 0.2168(4) -0.0236(3) 0.0196(12) Uani 1 1 d . . . . . H2 H 0.371725 0.231629 -0.064966 0.024 Uiso 1 1 calc R U . . . C3 C 0.3699(5) 0.2969(4) 0.0085(3) 0.0302(15) Uani 1 1 d . . . . . H3A H 0.316955 0.302529 -0.001182 0.045 Uiso 1 1 calc R U . . . H3B H 0.425349 0.352744 -0.002169 0.045 Uiso 1 1 calc R U . . . H3C H 0.370368 0.286975 0.049409 0.045 Uiso 1 1 calc R U . . . C4 C 0.4390(4) 0.1939(4) -0.0076(3) 0.0224(13) Uani 1 1 d . . . . . H4 H 0.428589 0.140660 -0.031027 0.027 Uiso 1 1 calc R U . . . C5 C 0.4405(5) 0.1691(6) 0.0540(3) 0.0348(17) Uani 1 1 d . . . . . H5A H 0.382067 0.114491 0.063477 0.042 Uiso 1 1 calc R U . . . H5B H 0.447319 0.219312 0.078518 0.042 Uiso 1 1 calc R U . . . C6 C 0.5185(6) 0.1504(7) 0.0660(4) 0.046(2) Uani 1 1 d . . . . . H6A H 0.519515 0.138453 0.107018 0.056 Uiso 1 1 calc R U . . . H6B H 0.507513 0.095486 0.045039 0.056 Uiso 1 1 calc R U . . . C7 C 0.6094(6) 0.2290(8) 0.0488(5) 0.056(3) Uani 1 1 d . . . . . H7A H 0.657221 0.212946 0.054774 0.067 Uiso 1 1 calc R U . . . H7B H 0.623948 0.282541 0.072541 0.067 Uiso 1 1 calc R U . . . C8 C 0.6068(5) 0.2515(6) -0.0136(4) 0.047(2) Uani 1 1 d . . . . . H8A H 0.665898 0.304078 -0.024464 0.057 Uiso 1 1 calc R U . . . H8B H 0.596387 0.199240 -0.037301 0.057 Uiso 1 1 calc R U . . . C9 C 0.5317(5) 0.2736(5) -0.0244(4) 0.0352(17) Uani 1 1 d . . . . . H9A H 0.531067 0.287528 -0.065108 0.042 Uiso 1 1 calc R U . . . H9B H 0.543925 0.327979 -0.002254 0.042 Uiso 1 1 calc R U . . . C10 C -0.1773(4) -0.2465(4) 0.0712(3) 0.0191(12) Uani 1 1 d . U . . . H10A H -0.193485 -0.255533 0.111993 0.023 Uiso 1 1 calc R U . . . H10B H -0.226188 -0.297857 0.049986 0.023 Uiso 1 1 calc R U . . . C11 C -0.0937(5) -0.3329(4) 0.0806(3) 0.0213(13) Uani 1 1 d . U . . . H11 H -0.125920 -0.351596 0.117928 0.026 Uiso 1 1 calc R U . . . C12 C -0.1481(5) -0.4072(5) 0.0386(3) 0.0288(15) Uani 1 1 d . . . . . H12A H -0.118328 -0.390550 0.001414 0.043 Uiso 1 1 calc R U . . . H12B H -0.209200 -0.415665 0.035479 0.043 Uiso 1 1 calc R U . . . H12C H -0.152025 -0.463823 0.051436 0.043 Uiso 1 1 calc R U . . . C13 C 0.0036(5) -0.3146(4) 0.0900(3) 0.0215(13) Uani 1 1 d . . . . . H13 H 0.033215 -0.263555 0.117691 0.026 Uiso 1 1 calc R U . . . C14 C 0.0007(5) -0.3969(5) 0.1175(4) 0.0343(17) Uani 1 1 d . . . . . H14A H -0.029971 -0.449578 0.091704 0.041 Uiso 1 1 calc R U . . . H14B H -0.034930 -0.411825 0.153035 0.041 Uiso 1 1 calc R U . . . C15 C 0.0957(6) -0.3794(6) 0.1308(4) 0.0404(19) Uani 1 1 d . . . . . H15A H 0.123163 -0.332209 0.160519 0.049 Uiso 1 1 calc R U . . . H15B H 0.091446 -0.435654 0.145925 0.049 Uiso 1 1 calc R U . . . C16 C 0.1563(6) -0.3490(6) 0.0790(4) 0.042(2) Uani 1 1 d . . . . . H16A H 0.133654 -0.399364 0.051246 0.051 Uiso 1 1 calc R U . . . H16B H 0.218512 -0.333434 0.090130 0.051 Uiso 1 1 calc R U . . . C17 C 0.1588(5) -0.2663(5) 0.0512(3) 0.0318(16) Uani 1 1 d . . . . . H17A H 0.187827 -0.213969 0.077371 0.038 Uiso 1 1 calc R U . . . H17B H 0.195642 -0.250265 0.016127 0.038 Uiso 1 1 calc R U . . . C18 C 0.0631(5) -0.2857(5) 0.0366(3) 0.0279(15) Uani 1 1 d . . . . . H18A H 0.035923 -0.334443 0.007858 0.033 Uiso 1 1 calc R U . . . H18B H 0.066252 -0.230575 0.020420 0.033 Uiso 1 1 calc R U . . . C19 C -0.2217(5) 0.0820(5) 0.0903(3) 0.0261(14) Uani 1 1 d . . . . . H19A H -0.232055 0.122916 0.115082 0.031 Uiso 1 1 calc R U . . . H19B H -0.246824 0.082419 0.052479 0.031 Uiso 1 1 calc R U . . . C20 C -0.3728(5) -0.0426(5) 0.1266(3) 0.0278(15) Uani 1 1 d . . . . . H20 H -0.398853 -0.102268 0.146550 0.033 Uiso 1 1 calc R U . . . C21 C -0.3784(5) 0.0239(5) 0.1669(4) 0.0364(16) Uani 1 1 d . . . . . H21A H -0.332693 0.040791 0.196823 0.055 Uiso 1 1 calc R U . . . H21B H -0.438881 -0.004508 0.184064 0.055 Uiso 1 1 calc R U . . . H21C H -0.367174 0.078202 0.145989 0.055 Uiso 1 1 calc R U . . . C22 C -0.4313(5) -0.0566(6) 0.0733(4) 0.0392(18) Uani 1 1 d . . . . . H22 H -0.406091 0.003384 0.053831 0.047 Uiso 1 1 calc R U . . . C23 C -0.5289(6) -0.0878(8) 0.0885(5) 0.064(3) Uani 1 1 d . U . . . H23A H -0.553778 -0.145310 0.109954 0.077 Uiso 1 1 calc R U . . . H23B H -0.530320 -0.042161 0.113785 0.077 Uiso 1 1 calc R U . . . C24 C -0.5896(7) -0.1025(9) 0.0384(6) 0.077(3) Uani 1 1 d . U . . . H24A H -0.653010 -0.128187 0.051441 0.092 Uiso 1 1 calc R U . . . H24B H -0.571006 -0.043724 0.019655 0.092 Uiso 1 1 calc R U . . . C25 C -0.5833(7) -0.1662(9) -0.0030(6) 0.079(3) Uani 1 1 d . U . . . H25A H -0.608173 -0.226628 0.014862 0.095 Uiso 1 1 calc R U . . . H25B H -0.620863 -0.172748 -0.036643 0.095 Uiso 1 1 calc R U . . . C26 C -0.4891(8) -0.1342(10) -0.0213(5) 0.077(3) Uani 1 1 d . U . . . H26A H -0.465083 -0.075854 -0.041687 0.092 Uiso 1 1 calc R U . . . H26B H -0.487703 -0.178958 -0.047512 0.092 Uiso 1 1 calc R U . . . C27 C -0.4290(7) -0.1218(8) 0.0320(5) 0.060(3) Uani 1 1 d . U . . . H27A H -0.451017 -0.181177 0.050732 0.072 Uiso 1 1 calc R U . . . H27B H -0.365622 -0.099276 0.019764 0.072 Uiso 1 1 calc R U . . . C28 C -0.1701(6) 0.3125(6) 0.1482(4) 0.0388(18) Uani 1 1 d . . . . . C29 C -0.2103(7) 0.3728(7) 0.1589(4) 0.053(2) Uani 1 1 d . . . . . H29A H -0.270192 0.337077 0.176465 0.079 Uiso 1 1 calc R U . . . H29B H -0.216321 0.397930 0.122874 0.079 Uiso 1 1 calc R U . . . H29C H -0.170486 0.422329 0.184396 0.079 Uiso 1 1 calc R U . . . N1 N 0.2699(3) 0.1366(3) -0.0138(2) 0.0180(10) Uani 1 1 d . . . . . H1C H 0.260738 0.127707 0.024248 0.022 Uiso 1 1 calc R U . . . H1D H 0.229185 0.151813 -0.027263 0.022 Uiso 1 1 calc R U . . . N2 N -0.0905(3) -0.2460(3) 0.0627(2) 0.0180(10) Uani 1 1 d . U . . . H2A H -0.046129 -0.199128 0.082704 0.022 Uiso 1 1 calc R U . . . H2B H -0.075258 -0.236008 0.025330 0.022 Uiso 1 1 calc R U . . . N3 N -0.2741(4) -0.0114(4) 0.1137(2) 0.0209(11) Uani 1 1 d . . . . . H3D H -0.246717 -0.014228 0.146173 0.025 Uiso 1 1 calc R U . . . H3E H -0.271847 -0.050631 0.088409 0.025 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Tb1 0.01255(15) 0.01322(19) 0.01358(14) 0.00030(15) 0.00007(9) 0.00705(17) P1 0.0131(7) 0.0140(7) 0.0158(7) -0.0008(5) -0.0007(5) 0.0074(6) P2 0.0126(7) 0.0136(7) 0.0164(7) -0.0010(6) -0.0016(6) 0.0060(6) P3 0.0184(8) 0.0211(8) 0.0172(7) 0.0019(6) 0.0012(6) 0.0135(7) O1 0.017(2) 0.017(2) 0.019(2) 0.0025(17) -0.0030(17) 0.0107(17) O2 0.017(2) 0.021(2) 0.014(2) -0.0006(15) -0.0013(16) 0.0115(18) O3 0.022(2) 0.017(2) 0.023(2) -0.0025(16) -0.0032(18) 0.0114(19) O4 0.025(2) 0.016(2) 0.014(2) 0.0004(15) -0.0026(16) 0.0111(18) O5 0.017(2) 0.018(2) 0.015(2) 0.0017(16) 0.0001(17) 0.0066(19) O6 0.016(2) 0.023(2) 0.027(2) -0.0004(19) -0.0013(18) 0.0089(19) O7 0.029(3) 0.038(3) 0.017(2) 0.0014(19) 0.0004(18) 0.026(2) O8 0.031(2) 0.028(2) 0.016(2) 0.0045(18) 0.0022(18) 0.021(2) O9 0.029(3) 0.022(2) 0.033(3) 0.005(2) 0.002(2) 0.014(2) O10 0.061(4) 0.049(4) 0.051(4) 0.015(3) 0.018(3) 0.043(4) O11 0.103(6) 0.070(5) 0.047(4) 0.014(3) 0.025(4) 0.061(5) O1W 0.072(7) 0.089(8) 0.164(10) 0.058(7) 0.028(7) 0.018(6) O2W 0.023(2) 0.027(3) 0.028(2) 0.006(2) -0.001(2) 0.012(2) C1 0.018(3) 0.022(3) 0.026(3) -0.004(3) 0.000(3) 0.011(3) C2 0.017(3) 0.014(3) 0.026(3) 0.006(2) 0.005(2) 0.006(2) C3 0.024(3) 0.020(3) 0.046(4) 0.000(3) -0.001(3) 0.011(3) C4 0.016(3) 0.018(3) 0.029(3) 0.001(3) 0.003(2) 0.005(2) C5 0.030(4) 0.045(5) 0.039(4) 0.008(3) 0.004(3) 0.026(4) C6 0.042(5) 0.064(6) 0.051(5) 0.012(4) 0.000(4) 0.040(5) C7 0.035(5) 0.074(7) 0.069(6) -0.013(5) -0.017(4) 0.035(5) C8 0.018(4) 0.045(5) 0.074(7) 0.009(4) 0.010(4) 0.011(3) C9 0.018(3) 0.030(4) 0.051(5) 0.007(3) 0.007(3) 0.006(3) C10 0.016(3) 0.016(3) 0.022(3) 0.007(2) 0.003(2) 0.006(2) C11 0.023(3) 0.014(3) 0.028(3) 0.002(2) 0.001(3) 0.010(2) C12 0.032(4) 0.018(3) 0.035(4) -0.005(3) -0.008(3) 0.011(3) C13 0.029(3) 0.019(3) 0.021(3) -0.002(2) -0.003(3) 0.016(3) C14 0.036(4) 0.024(4) 0.048(5) 0.008(3) 0.000(3) 0.019(3) C15 0.043(5) 0.028(4) 0.058(5) 0.007(4) -0.011(4) 0.024(4) C16 0.035(4) 0.034(4) 0.070(6) -0.006(4) -0.011(4) 0.026(4) C17 0.026(4) 0.028(4) 0.041(4) -0.001(3) 0.000(3) 0.013(3) C18 0.028(4) 0.032(4) 0.026(3) -0.001(3) 0.000(3) 0.016(3) C19 0.025(3) 0.023(3) 0.036(4) 0.005(3) 0.004(3) 0.016(3) C20 0.019(3) 0.026(3) 0.034(4) 0.001(3) -0.001(3) 0.008(3) C21 0.034(4) 0.038(4) 0.045(4) 0.006(4) 0.005(4) 0.024(3) C22 0.023(4) 0.043(5) 0.044(5) -0.002(4) -0.005(3) 0.010(3) C23 0.023(4) 0.065(6) 0.090(7) -0.016(6) -0.004(4) 0.012(4) C24 0.031(4) 0.081(7) 0.117(8) -0.038(6) -0.022(5) 0.026(5) C25 0.046(5) 0.083(6) 0.116(8) -0.053(6) -0.033(5) 0.039(5) C26 0.059(6) 0.103(7) 0.082(7) -0.043(6) -0.038(5) 0.050(5) C27 0.042(5) 0.089(7) 0.067(6) -0.026(5) -0.015(4) 0.047(5) C28 0.040(4) 0.031(4) 0.043(4) 0.003(3) 0.001(3) 0.016(4) C29 0.059(6) 0.045(5) 0.065(6) -0.001(5) 0.012(5) 0.035(5) N1 0.014(2) 0.017(2) 0.022(3) -0.0016(19) 0.0002(19) 0.007(2) N2 0.016(2) 0.014(2) 0.024(3) 0.001(2) 0.001(2) 0.007(2) N3 0.020(3) 0.020(3) 0.024(3) 0.000(2) -0.002(2) 0.012(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2543 0.3332 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Tb Tb -4.4782 11.8047 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O7 Tb1 O5 80.65(15) . 5_554 ? O7 Tb1 O8 86.04(17) . 5_554 ? O5 Tb1 O8 80.95(15) 5_554 5_554 ? O7 Tb1 O1 83.94(15) . 6 ? O5 Tb1 O1 156.91(13) 5_554 6 ? O8 Tb1 O1 80.92(15) 5_554 6 ? O7 Tb1 O2 155.20(14) . . ? O5 Tb1 O2 122.90(14) 5_554 . ? O8 Tb1 O2 104.10(15) 5_554 . ? O1 Tb1 O2 75.60(14) 6 . ? O7 Tb1 O5 73.85(15) . . ? O5 Tb1 O5 121.44(15) 5_554 . ? O8 Tb1 O5 145.63(15) 5_554 . ? O1 Tb1 O5 69.66(14) 6 . ? O2 Tb1 O5 85.83(13) . . ? O7 Tb1 O4 93.47(16) . . ? O5 Tb1 O4 71.83(14) 5_554 . ? O8 Tb1 O4 152.46(14) 5_554 . ? O1 Tb1 O4 126.47(14) 6 . ? O2 Tb1 O4 87.68(13) . . ? O5 Tb1 O4 58.52(14) . . ? O7 Tb1 O1 145.25(14) . . ? O5 Tb1 O1 69.39(13) 5_554 . ? O8 Tb1 O1 72.54(14) 5_554 . ? O1 Tb1 O1 117.97(14) 6 . ? O2 Tb1 O1 59.13(13) . . ? O5 Tb1 O1 137.11(12) . . ? O4 Tb1 O1 93.52(13) . . ? O7 Tb1 Tb1 112.96(11) . 5_554 ? O5 Tb1 Tb1 35.44(11) 5_554 5_554 ? O8 Tb1 Tb1 70.25(10) 5_554 5_554 ? O1 Tb1 Tb1 144.75(11) 6 5_554 ? O2 Tb1 Tb1 91.83(9) . 5_554 ? O5 Tb1 Tb1 143.28(10) . 5_554 ? O4 Tb1 Tb1 84.78(9) . 5_554 ? O1 Tb1 Tb1 34.27(9) . 5_554 ? O7 Tb1 Tb1 72.65(11) . 6 ? O5 Tb1 Tb1 147.42(11) 5_554 6 ? O8 Tb1 Tb1 114.71(10) 5_554 6 ? O1 Tb1 Tb1 37.08(11) 6 6 ? O2 Tb1 Tb1 82.56(9) . 6 ? O5 Tb1 Tb1 32.90(10) . 6 ? O4 Tb1 Tb1 91.20(9) . 6 ? O1 Tb1 Tb1 141.11(9) . 6 ? Tb1 Tb1 Tb1 173.235(3) 5_554 6 ? O3 P1 O2 115.5(3) . . ? O3 P1 O1 115.7(2) . . ? O2 P1 O1 105.7(2) . . ? O3 P1 C1 104.5(3) . . ? O2 P1 C1 109.6(3) . . ? O1 P1 C1 105.4(3) . . ? O6 P2 O4 116.0(3) . . ? O6 P2 O5 115.6(3) . . ? O4 P2 O5 104.4(2) . . ? O6 P2 C10 106.4(3) . . ? O4 P2 C10 107.4(3) . . ? O5 P2 C10 106.5(3) . . ? O9 P3 O7 110.0(3) . . ? O9 P3 O8 112.7(3) . . ? O7 P3 O8 114.8(2) . . ? O9 P3 C19 104.4(3) . . ? O7 P3 C19 107.0(3) . . ? O8 P3 C19 107.1(3) . . ? P1 O1 Tb1 151.3(3) . 5_554 ? P1 O1 Tb1 95.3(2) . . ? Tb1 O1 Tb1 108.65(17) 5_554 . ? P1 O2 Tb1 99.7(2) . . ? P2 O4 Tb1 97.8(2) . . ? P2 O5 Tb1 150.6(3) . 6 ? P2 O5 Tb1 97.8(2) . . ? Tb1 O5 Tb1 111.66(18) 6 . ? P3 O7 Tb1 137.3(3) . . ? P3 O8 Tb1 138.4(3) . 6 ? C28 O10 H10C 110.0 . . ? H1WA O1W H1WB 104.1 . . ? H2WA O2W H2WB 126.1 . . ? N1 C1 P1 113.4(4) . . ? N1 C1 H1A 108.9 . . ? P1 C1 H1A 108.9 . . ? N1 C1 H1B 108.9 . . ? P1 C1 H1B 108.9 . . ? H1A C1 H1B 107.7 . . ? C3 C2 N1 106.2(5) . . ? C3 C2 C4 114.9(5) . . ? N1 C2 C4 112.1(5) . . ? C3 C2 H2 107.8 . . ? N1 C2 H2 107.8 . . ? C4 C2 H2 107.8 . . ? C2 C3 H3A 109.5 . . ? C2 C3 H3B 109.5 . . ? H3A C3 H3B 109.5 . . ? C2 C3 H3C 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? C5 C4 C9 110.0(6) . . ? C5 C4 C2 115.9(5) . . ? C9 C4 C2 108.8(5) . . ? C5 C4 H4 107.3 . . ? C9 C4 H4 107.3 . . ? C2 C4 H4 107.3 . . ? C4 C5 C6 111.8(6) . . ? C4 C5 H5A 109.3 . . ? C6 C5 H5A 109.3 . . ? C4 C5 H5B 109.3 . . ? C6 C5 H5B 109.3 . . ? H5A C5 H5B 107.9 . . ? C7 C6 C5 112.1(7) . . ? C7 C6 H6A 109.2 . . ? C5 C6 H6A 109.2 . . ? C7 C6 H6B 109.2 . . ? C5 C6 H6B 109.2 . . ? H6A C6 H6B 107.9 . . ? C6 C7 C8 109.6(7) . . ? C6 C7 H7A 109.8 . . ? C8 C7 H7A 109.8 . . ? C6 C7 H7B 109.8 . . ? C8 C7 H7B 109.8 . . ? H7A C7 H7B 108.2 . . ? C9 C8 C7 111.0(7) . . ? C9 C8 H8A 109.4 . . ? C7 C8 H8A 109.4 . . ? C9 C8 H8B 109.4 . . ? C7 C8 H8B 109.4 . . ? H8A C8 H8B 108.0 . . ? C8 C9 C4 111.0(6) . . ? C8 C9 H9A 109.4 . . ? C4 C9 H9A 109.4 . . ? C8 C9 H9B 109.4 . . ? C4 C9 H9B 109.4 . . ? H9A C9 H9B 108.0 . . ? N2 C10 P2 111.5(4) . . ? N2 C10 H10A 109.3 . . ? P2 C10 H10A 109.3 . . ? N2 C10 H10B 109.3 . . ? P2 C10 H10B 109.3 . . ? H10A C10 H10B 108.0 . . ? C12 C11 N2 110.1(5) . . ? C12 C11 C13 114.2(5) . . ? N2 C11 C13 109.4(5) . . ? C12 C11 H11 107.6 . . ? N2 C11 H11 107.6 . . ? C13 C11 H11 107.6 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C14 C13 C18 111.0(6) . . ? C14 C13 C11 109.8(6) . . ? C18 C13 C11 114.8(5) . . ? C14 C13 H13 107.0 . . ? C18 C13 H13 107.0 . . ? C11 C13 H13 107.0 . . ? C13 C14 C15 111.4(6) . . ? C13 C14 H14A 109.3 . . ? C15 C14 H14A 109.3 . . ? C13 C14 H14B 109.3 . . ? C15 C14 H14B 109.3 . . ? H14A C14 H14B 108.0 . . ? C16 C15 C14 112.1(7) . . ? C16 C15 H15A 109.2 . . ? C14 C15 H15A 109.2 . . ? C16 C15 H15B 109.2 . . ? C14 C15 H15B 109.2 . . ? H15A C15 H15B 107.9 . . ? C15 C16 C17 111.0(6) . . ? C15 C16 H16A 109.4 . . ? C17 C16 H16A 109.4 . . ? C15 C16 H16B 109.4 . . ? C17 C16 H16B 109.4 . . ? H16A C16 H16B 108.0 . . ? C18 C17 C16 111.1(6) . . ? C18 C17 H17A 109.4 . . ? C16 C17 H17A 109.4 . . ? C18 C17 H17B 109.4 . . ? C16 C17 H17B 109.4 . . ? H17A C17 H17B 108.0 . . ? C17 C18 C13 110.3(6) . . ? C17 C18 H18A 109.6 . . ? C13 C18 H18A 109.6 . . ? C17 C18 H18B 109.6 . . ? C13 C18 H18B 109.6 . . ? H18A C18 H18B 108.1 . . ? N3 C19 P3 116.7(4) . . ? N3 C19 H19A 108.1 . . ? P3 C19 H19A 108.1 . . ? N3 C19 H19B 108.1 . . ? P3 C19 H19B 108.1 . . ? H19A C19 H19B 107.3 . . ? C21 C20 N3 109.6(6) . . ? C21 C20 C22 110.4(6) . . ? N3 C20 C22 114.0(6) . . ? C21 C20 H20 107.5 . . ? N3 C20 H20 107.5 . . ? C22 C20 H20 107.5 . . ? C20 C21 H21A 109.5 . . ? C20 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C20 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C27 C22 C23 109.0(8) . . ? C27 C22 C20 113.0(7) . . ? C23 C22 C20 111.9(8) . . ? C27 C22 H22 107.6 . . ? C23 C22 H22 107.6 . . ? C20 C22 H22 107.6 . . ? C24 C23 C22 114.6(10) . . ? C24 C23 H23A 108.6 . . ? C22 C23 H23A 108.6 . . ? C24 C23 H23B 108.6 . . ? C22 C23 H23B 108.6 . . ? H23A C23 H23B 107.6 . . ? C25 C24 C23 109.8(10) . . ? C25 C24 H24A 109.7 . . ? C23 C24 H24A 109.7 . . ? C25 C24 H24B 109.7 . . ? C23 C24 H24B 109.7 . . ? H24A C24 H24B 108.2 . . ? C26 C25 C24 112.4(10) . . ? C26 C25 H25A 109.1 . . ? C24 C25 H25A 109.1 . . ? C26 C25 H25B 109.1 . . ? C24 C25 H25B 109.1 . . ? H25A C25 H25B 107.9 . . ? C25 C26 C27 109.3(11) . . ? C25 C26 H26A 109.8 . . ? C27 C26 H26A 109.8 . . ? C25 C26 H26B 109.8 . . ? C27 C26 H26B 109.8 . . ? H26A C26 H26B 108.3 . . ? C22 C27 C26 111.5(8) . . ? C22 C27 H27A 109.3 . . ? C26 C27 H27A 109.3 . . ? C22 C27 H27B 109.3 . . ? C26 C27 H27B 109.3 . . ? H27A C27 H27B 108.0 . . ? O11 C28 O10 124.5(8) . . ? O11 C28 C29 122.7(8) . . ? O10 C28 C29 112.8(7) . . ? C28 C29 H29A 109.5 . . ? C28 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C28 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C1 N1 C2 115.6(5) . . ? C1 N1 H1C 108.4 . . ? C2 N1 H1C 108.4 . . ? C1 N1 H1D 108.4 . . ? C2 N1 H1D 108.4 . . ? H1C N1 H1D 107.4 . . ? C10 N2 C11 114.0(5) . . ? C10 N2 H2A 108.8 . . ? C11 N2 H2A 108.8 . . ? C10 N2 H2B 108.8 . . ? C11 N2 H2B 108.8 . . ? H2A N2 H2B 107.7 . . ? C19 N3 C20 114.5(5) . . ? C19 N3 H3D 108.6 . . ? C20 N3 H3D 108.6 . . ? C19 N3 H3E 108.6 . . ? C20 N3 H3E 108.6 . . ? H3D N3 H3E 107.6 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Tb1 O7 2.280(4) . ? Tb1 O5 2.312(4) 5_554 ? Tb1 O8 2.329(4) 5_554 ? Tb1 O1 2.352(4) 6 ? Tb1 O2 2.417(4) . ? Tb1 O5 2.468(4) . ? Tb1 O4 2.471(4) . ? Tb1 O1 2.518(4) . ? Tb1 Tb1 3.9566(2) 5_554 ? Tb1 Tb1 3.9566(2) 6 ? P1 O3 1.499(4) . ? P1 O2 1.523(4) . ? P1 O1 1.535(4) . ? P1 C1 1.823(7) . ? P2 O6 1.494(5) . ? P2 O4 1.525(4) . ? P2 O5 1.530(5) . ? P2 C10 1.825(6) . ? P3 O9 1.508(5) . ? P3 O7 1.514(5) . ? P3 O8 1.523(4) . ? P3 C19 1.824(7) . ? O10 C28 1.286(10) . ? O10 H10C 0.8838 . ? O11 C28 1.203(10) . ? O1W H1WA 0.9504 . ? O1W H1WB 0.9504 . ? O2W H2WA 0.9500 . ? O2W H2WB 0.9500 . ? C1 N1 1.488(8) . ? C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? C2 C3 1.529(9) . ? C2 N1 1.529(8) . ? C2 C4 1.535(9) . ? C2 H2 1.0000 . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 H3C 0.9800 . ? C4 C5 1.514(10) . ? C4 C9 1.533(9) . ? C4 H4 1.0000 . ? C5 C6 1.539(10) . ? C5 H5A 0.9900 . ? C5 H5B 0.9900 . ? C6 C7 1.510(14) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C8 1.526(13) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C8 C9 1.523(11) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C10 N2 1.488(8) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C11 C12 1.507(9) . ? C11 N2 1.514(8) . ? C11 C13 1.542(9) . ? C11 H11 1.0000 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C14 1.522(9) . ? C13 C18 1.533(9) . ? C13 H13 1.0000 . ? C14 C15 1.523(11) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 C16 1.514(13) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C16 C17 1.535(11) . ? C16 H16A 0.9900 . ? C16 H16B 0.9900 . ? C17 C18 1.531(10) . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C19 N3 1.488(8) . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C20 C21 1.518(11) . ? C20 N3 1.519(8) . ? C20 C22 1.545(11) . ? C20 H20 1.0000 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 C27 1.493(13) . ? C22 C23 1.514(12) . ? C22 H22 1.0000 . ? C23 C24 1.504(16) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C24 C25 1.502(16) . ? C24 H24A 0.9900 . ? C24 H24B 0.9900 . ? C25 C26 1.478(16) . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C26 C27 1.567(14) . ? C26 H26A 0.9900 . ? C26 H26B 0.9900 . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C28 C29 1.513(12) . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? N1 H1C 0.9100 . ? N1 H1D 0.9100 . ? N2 H2A 0.9100 . ? N2 H2B 0.9100 . ? N3 H3D 0.9100 . ? N3 H3E 0.9100 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag O10 H10C O9 0.88 1.67 2.517(7) 160.3 . yes O1W H1WA O6 0.95 1.89 2.771(10) 152.5 . yes O2W H2WA O3 0.95 1.98 2.790(7) 141.3 . yes O2W H2WB O2 0.95 2.18 2.868(6) 128.7 5_554 yes N1 H1C O3 0.91 1.76 2.661(7) 171.1 6 yes N1 H1D O8 0.91 2.29 3.163(7) 159.7 5_554 yes N2 H2A O4 0.91 1.93 2.738(7) 147.6 6 yes N2 H2B O2W 0.91 2.03 2.919(7) 165.7 . yes N3 H3D O9 0.91 2.41 3.131(7) 136.5 6 yes N3 H3E O6 0.91 1.97 2.853(7) 162.2 . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O3 P1 O1 Tb1 -13.0(6) . . . 5_554 ? O2 P1 O1 Tb1 -142.1(5) . . . 5_554 ? C1 P1 O1 Tb1 101.9(5) . . . 5_554 ? O3 P1 O1 Tb1 133.7(2) . . . . ? O2 P1 O1 Tb1 4.6(2) . . . . ? C1 P1 O1 Tb1 -111.5(2) . . . . ? O3 P1 O2 Tb1 -134.0(2) . . . . ? O1 P1 O2 Tb1 -4.8(2) . . . . ? C1 P1 O2 Tb1 108.3(3) . . . . ? O6 P2 O4 Tb1 117.3(2) . . . . ? O5 P2 O4 Tb1 -11.1(2) . . . . ? C10 P2 O4 Tb1 -123.8(2) . . . . ? O6 P2 O5 Tb1 61.9(6) . . . 6 ? O4 P2 O5 Tb1 -169.5(5) . . . 6 ? C10 P2 O5 Tb1 -56.1(6) . . . 6 ? O6 P2 O5 Tb1 -117.5(2) . . . . ? O4 P2 O5 Tb1 11.1(2) . . . . ? C10 P2 O5 Tb1 124.5(2) . . . . ? O9 P3 O7 Tb1 112.4(4) . . . . ? O8 P3 O7 Tb1 -15.9(6) . . . . ? C19 P3 O7 Tb1 -134.7(4) . . . . ? O9 P3 O8 Tb1 -145.5(4) . . . 6 ? O7 P3 O8 Tb1 -18.5(6) . . . 6 ? C19 P3 O8 Tb1 100.2(4) . . . 6 ? O3 P1 C1 N1 -177.2(4) . . . . ? O2 P1 C1 N1 -52.9(5) . . . . ? O1 P1 C1 N1 60.4(5) . . . . ? C3 C2 C4 C5 59.9(8) . . . . ? N1 C2 C4 C5 -61.4(8) . . . . ? C3 C2 C4 C9 -64.6(8) . . . . ? N1 C2 C4 C9 174.1(5) . . . . ? C9 C4 C5 C6 -54.3(9) . . . . ? C2 C4 C5 C6 -178.2(7) . . . . ? C4 C5 C6 C7 55.2(11) . . . . ? C5 C6 C7 C8 -55.6(11) . . . . ? C6 C7 C8 C9 57.6(10) . . . . ? C7 C8 C9 C4 -58.7(10) . . . . ? C5 C4 C9 C8 56.5(9) . . . . ? C2 C4 C9 C8 -175.6(7) . . . . ? O6 P2 C10 N2 177.4(4) . . . . ? O4 P2 C10 N2 52.6(5) . . . . ? O5 P2 C10 N2 -58.8(5) . . . . ? C12 C11 C13 C14 -65.6(8) . . . . ? N2 C11 C13 C14 170.4(5) . . . . ? C12 C11 C13 C18 60.2(7) . . . . ? N2 C11 C13 C18 -63.8(7) . . . . ? C18 C13 C14 C15 55.6(8) . . . . ? C11 C13 C14 C15 -176.5(6) . . . . ? C13 C14 C15 C16 -54.6(9) . . . . ? C14 C15 C16 C17 54.3(9) . . . . ? C15 C16 C17 C18 -55.5(9) . . . . ? C16 C17 C18 C13 56.7(8) . . . . ? C14 C13 C18 C17 -56.7(8) . . . . ? C11 C13 C18 C17 178.1(5) . . . . ? O9 P3 C19 N3 -163.5(5) . . . . ? O7 P3 C19 N3 79.9(6) . . . . ? O8 P3 C19 N3 -43.7(6) . . . . ? C21 C20 C22 C27 -179.7(8) . . . . ? N3 C20 C22 C27 56.4(10) . . . . ? C21 C20 C22 C23 -56.3(9) . . . . ? N3 C20 C22 C23 179.9(7) . . . . ? C27 C22 C23 C24 -54.5(12) . . . . ? C20 C22 C23 C24 179.8(9) . . . . ? C22 C23 C24 C25 54.1(14) . . . . ? C23 C24 C25 C26 -55.8(16) . . . . ? C24 C25 C26 C27 57.6(16) . . . . ? C23 C22 C27 C26 54.8(13) . . . . ? C20 C22 C27 C26 179.9(9) . . . . ? C25 C26 C27 C22 -57.9(14) . . . . ? P1 C1 N1 C2 -164.6(4) . . . . ? C3 C2 N1 C1 -178.7(5) . . . . ? C4 C2 N1 C1 -52.5(7) . . . . ? P2 C10 N2 C11 -178.8(4) . . . . ? C12 C11 N2 C10 73.3(7) . . . . ? C13 C11 N2 C10 -160.4(5) . . . . ? P3 C19 N3 C20 172.0(5) . . . . ? C21 C20 N3 C19 -56.2(8) . . . . ? C22 C20 N3 C19 68.1(8) . . . . ?