#------------------------------------------------------------------------------ #$Date: 2021-10-15 01:13:57 +0300 (Fri, 15 Oct 2021) $ #$Revision: 269952 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/49/1564921.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564921 loop_ _publ_author_name 'D\"utsch, Luis' 'Riesinger, Christoph' 'Balazs, Gabor' 'Seidl, Michael' 'Scheer, Manfred' _publ_section_title ; Structural Diversity of Mixed Polypnictogen Complexes: Dicationic E2E'2 (E, E' = P, As, Sb, Bi) Chains, Cycles and Cages Stabilized by Transition Metals ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC04924K _journal_year 2021 _chemical_formula_moiety 'C28 H20 As2.07 Bi1.93 Mo4 O8, 2(Al C16 Cl12 F24 O4), 2(C H2 Cl2)' _chemical_formula_sum 'C62 H24 Al2 As2.07 Bi1.93 Cl28 F48 Mo4 O16' _chemical_formula_weight 3925.55 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2021-07-28 _audit_creation_method ; Olex2 1.5-alpha (compiled 2021.07.19 svn.r715e62df for OlexSys, GUI svn.r6380) ; _audit_update_record ; 2021-08-24 deposited with the CCDC. 2021-10-08 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 96.234(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 13.3028(2) _cell_length_b 27.6708(4) _cell_length_c 14.6789(3) _cell_measurement_reflns_used 25056 _cell_measurement_temperature 123.0(1) _cell_measurement_theta_max 34.3910 _cell_measurement_theta_min 3.1690 _cell_volume 5371.34(16) _computing_cell_refinement 'CrysAlisPro 1.171.41.21a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.41.21a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.41.21a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 123.00(10) _diffrn_detector_area_resol_mean 7.9851 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.930 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 39.00 110.00 1.00 15.00 -- 32.12 178.00-120.00 71 2 \w -15.00 76.00 1.00 15.00 -- 32.12 -99.00 60.00 91 3 \w -42.00 82.00 1.00 15.00 -- 32.12 -19.00 60.00 124 4 \w 11.00 75.00 1.00 15.00 -- 32.12 57.00 120.00 64 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Single source at offset/far, Eos' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0391 _diffrn_reflns_av_unetI/netI 0.0513 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.930 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 43 _diffrn_reflns_limit_k_min -42 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 51984 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.930 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 34.590 _diffrn_reflns_theta_min 2.945 _exptl_absorpt_coefficient_mu 5.090 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.106 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.21a (Rigaku Oxford Diffraction, 2019) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour black _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 2.427 _exptl_crystal_description block _exptl_crystal_F_000 3709 _exptl_crystal_recrystallization_method 'The material was recrystallised from a mixture of CH2Cl2 and hexane by solvent layering' _exptl_crystal_size_max 0.984 _exptl_crystal_size_mid 0.237 _exptl_crystal_size_min 0.128 _refine_diff_density_max 1.920 _refine_diff_density_min -1.979 _refine_diff_density_rms 0.164 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.068 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 743 _refine_ls_number_reflns 21333 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.068 _refine_ls_R_factor_all 0.0481 _refine_ls_R_factor_gt 0.0378 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0320P)^2^+5.1461P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0816 _refine_ls_wR_factor_ref 0.0856 _reflns_Friedel_coverage 0.000 _reflns_number_gt 18316 _reflns_number_total 21333 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc04924k2.cif _cod_data_source_block ld448_abs _cod_database_code 1564921 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.562 _shelx_estimated_absorpt_t_min 0.082 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Others Fixed Sof: Bi1(0.965) As2(0.035) 3.a Secondary CH2 refined with riding coordinates: C201(H20A,H20B) 3.b Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C3(H3), C4(H4), C5(H5), C8(H8), C9(H9), C10(H10), C11(H11), C12(H12) ; _shelx_res_file ; TITL ld448_abs_a.res in P2(1)/n ld448_abs.res created by SHELXL-2018/3 at 12:01:52 on 28-Jul-2021 REM Old TITL LD448_abs in P2/n REM SHELXT solution in P2(1)/n: R1 0.079, Rweak 0.011, Alpha 0.042 REM 1.593 for 253 systematic absences, Orientation as input REM Formula found by SHELXT: C38 O4 F28 Al Cl14 As Mo2 Bi CELL 0.71073 13.3028 27.6708 14.6789 90 96.234 90 ZERR 2 0.0002 0.0004 0.0003 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Al As Bi Cl F Mo O UNIT 124 48 4 4.14 3.86 56 96 8 32 L.S. 10 PLAN 5 SIZE 0.128 0.237 0.984 TEMP -150.15(10) CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta OMIT 0 18 1 REM REM REM WGHT 0.032000 5.146100 FVAR 0.15860 PART 1 BI1 5 0.075296 0.529564 1.084363 10.96500 0.01175 0.01148 = 0.01680 -0.00237 0.00100 0.00077 PART 0 MO2 8 0.021431 0.629662 1.052684 11.00000 0.01204 0.00959 = 0.01452 -0.00114 -0.00102 -0.00155 MO1 8 0.074090 0.436359 0.802030 11.00000 0.01053 0.01022 = 0.01542 -0.00105 0.00114 -0.00014 AS1 4 0.117239 0.431288 0.977472 11.00000 0.00978 0.01335 = 0.01690 -0.00201 -0.00367 -0.00040 CL1 6 0.905164 0.595150 0.576165 11.00000 0.01264 0.02885 = 0.02449 0.00154 0.00563 0.00278 CL2 6 0.813260 0.576924 0.741404 11.00000 0.01619 0.02209 = 0.01803 0.00663 -0.00162 -0.00088 CL3 6 0.861690 0.673725 0.692303 11.00000 0.01637 0.02099 = 0.02236 -0.00149 -0.00319 -0.00725 CL4 6 0.503826 0.734343 1.016204 11.00000 0.03639 0.02398 = 0.01574 -0.01001 0.00412 -0.00748 CL5 6 0.392262 0.652086 0.942081 11.00000 0.02342 0.02044 = 0.02406 -0.00334 0.00790 -0.00716 CL6 6 0.376039 0.741617 0.845382 11.00000 0.02579 0.02299 = 0.02616 -0.00190 0.00068 0.01149 CL7 6 0.681541 0.517598 0.900490 11.00000 0.01649 0.01637 = 0.01848 -0.00026 -0.00832 -0.00074 CL8 6 0.678552 0.461559 0.736520 11.00000 0.02037 0.02007 = 0.02296 -0.00272 0.00640 0.00626 CL9 6 0.565859 0.429808 0.881167 11.00000 0.02544 0.01060 = 0.01930 0.00418 -0.00061 0.00045 CL10 6 0.187267 0.565505 0.589170 11.00000 0.01325 0.01528 = 0.04146 0.00455 -0.00143 -0.00371 CL11 6 0.138637 0.664429 0.548215 11.00000 0.01352 0.02107 = 0.02630 0.00686 -0.00259 0.00607 CL12 6 0.235694 0.638018 0.725698 11.00000 0.02199 0.02974 = 0.01672 0.00421 0.00492 0.00733 CL13 6 0.406348 0.707745 0.254608 11.00000 0.04207 0.05307 = 0.07932 0.02635 0.01574 0.00203 CL14 6 0.616716 0.734474 0.254750 11.00000 0.05480 0.07449 = 0.05896 -0.00902 -0.00063 -0.03550 AL1 3 0.526836 0.613483 0.705041 11.00000 0.00736 0.00832 = 0.00854 -0.00055 -0.00120 -0.00112 F1 7 0.778941 0.673063 0.484349 11.00000 0.01949 0.03057 = 0.02296 0.01111 0.00826 -0.00179 F2 7 0.685828 0.708404 0.575130 11.00000 0.02305 0.01503 = 0.02545 0.00538 0.00080 0.00060 F3 7 0.617006 0.663515 0.467197 11.00000 0.01974 0.03391 = 0.01581 0.00834 -0.00470 -0.00134 F4 7 0.711756 0.579465 0.453312 11.00000 0.02420 0.03555 = 0.01464 -0.00926 0.00466 -0.00252 F5 7 0.576584 0.572344 0.520714 11.00000 0.01385 0.02494 = 0.02301 -0.00827 -0.00113 -0.00549 F6 7 0.712508 0.536049 0.575000 11.00000 0.02386 0.01418 = 0.02912 -0.00349 -0.00057 0.00086 F7 7 0.604862 0.771422 0.861537 11.00000 0.04186 0.01286 = 0.02817 -0.00663 0.00690 -0.00898 F8 7 0.544961 0.742897 0.730384 11.00000 0.03601 0.02206 = 0.01849 0.00621 -0.00031 -0.00371 F9 7 0.691729 0.721592 0.790142 11.00000 0.02322 0.02791 = 0.03615 -0.00274 0.01230 -0.00815 F10 7 0.699259 0.694670 0.967793 11.00000 0.02382 0.03323 = 0.03020 -0.00802 -0.01309 -0.00434 F11 7 0.696320 0.636453 0.871132 11.00000 0.01986 0.02683 = 0.03198 -0.00343 -0.00239 0.00907 F12 7 0.604341 0.632775 0.981462 11.00000 0.03133 0.02813 = 0.02479 0.01106 -0.00630 0.00351 F13 7 0.476657 0.534517 0.927335 11.00000 0.02951 0.02718 = 0.01660 -0.00064 0.00679 0.00597 F14 7 0.373255 0.559613 0.815267 11.00000 0.01507 0.01399 = 0.03347 0.00338 0.00547 0.00520 F15 7 0.372609 0.484545 0.854736 11.00000 0.02062 0.01561 = 0.04798 0.00799 0.01373 -0.00274 F16 7 0.449929 0.438226 0.701540 11.00000 0.03295 0.00958 = 0.02587 -0.00286 -0.01262 -0.00521 F17 7 0.500489 0.494343 0.615506 11.00000 0.03853 0.02582 = 0.01335 -0.00305 -0.00322 -0.00412 F18 7 0.359981 0.501942 0.672796 11.00000 0.01868 0.02236 = 0.03899 -0.00085 -0.01712 -0.00033 F19 7 0.261357 0.615756 0.419968 11.00000 0.01846 0.03744 = 0.01611 -0.00223 -0.00861 0.00378 F20 7 0.361728 0.561706 0.485783 11.00000 0.02490 0.01782 = 0.02380 -0.00925 -0.00284 0.00322 F21 7 0.422349 0.627390 0.438003 11.00000 0.01897 0.03809 = 0.01607 0.00283 0.00340 -0.00006 F22 7 0.324194 0.707063 0.485896 11.00000 0.02622 0.02196 = 0.02776 0.01395 -0.00351 -0.00017 F23 7 0.464362 0.694284 0.571057 11.00000 0.01738 0.01721 = 0.03379 0.00607 -0.00170 -0.00891 F24 7 0.331183 0.713670 0.632549 11.00000 0.03147 0.01282 = 0.03224 -0.00545 0.00261 0.00035 O1 9 0.290712 0.389204 0.830867 11.00000 0.01551 0.02305 = 0.04156 -0.00176 0.00398 0.00466 O2 9 0.170154 0.538177 0.844204 11.00000 0.02795 0.01467 = 0.04877 -0.00494 0.01675 -0.00442 O3 9 0.191139 0.642405 1.218219 11.00000 0.02693 0.03670 = 0.03299 0.00135 -0.01093 -0.01168 O4 9 -0.128210 0.691891 1.156101 11.00000 0.03663 0.01391 = 0.04141 -0.00274 0.01689 0.00045 O5 9 0.636847 0.629762 0.657242 11.00000 0.00970 0.01511 = 0.01088 0.00046 0.00141 -0.00211 O6 9 0.512346 0.655465 0.790639 11.00000 0.01352 0.01261 = 0.01491 -0.00692 -0.00004 -0.00123 O7 9 0.549508 0.555348 0.748457 11.00000 0.00939 0.00825 = 0.01642 0.00257 -0.00099 -0.00059 O8 9 0.412070 0.611470 0.634596 11.00000 0.00836 0.01260 = 0.01138 0.00092 -0.00358 -0.00090 C1 1 -0.057881 0.439800 0.681655 11.00000 0.02006 0.04200 = 0.01692 -0.00028 -0.00231 0.00163 AFIX 43 H1 2 -0.125910 0.445784 0.692432 11.00000 -1.20000 AFIX 0 C2 1 -0.013005 0.393767 0.675707 11.00000 0.03393 0.03209 = 0.01500 -0.00419 -0.00102 -0.01236 AFIX 43 H2 2 -0.045408 0.363506 0.681587 11.00000 -1.20000 AFIX 0 C3 1 0.088385 0.400824 0.659495 11.00000 0.03218 0.02300 = 0.01586 -0.00324 0.00522 0.00298 AFIX 43 H3 2 0.136149 0.375930 0.652580 11.00000 -1.20000 AFIX 0 C4 1 0.107547 0.451092 0.655179 11.00000 0.02525 0.02093 = 0.02056 0.00280 0.00645 0.00176 AFIX 43 H4 2 0.169765 0.465946 0.645095 11.00000 -1.20000 AFIX 0 C5 1 0.015031 0.475256 0.668947 11.00000 0.02940 0.02522 = 0.02050 0.00507 0.00181 0.00647 AFIX 43 H5 2 0.004805 0.509230 0.669403 11.00000 -1.20000 AFIX 0 C6 1 0.211804 0.406272 0.825299 11.00000 0.01882 0.01310 = 0.02241 -0.00326 0.00215 -0.00122 C7 1 0.136780 0.500464 0.831090 11.00000 0.01545 0.01411 = 0.02755 -0.00023 0.00764 0.00250 C8 1 0.125842 0.638496 0.935958 11.00000 0.02221 0.01851 = 0.02342 -0.00414 0.01074 -0.00336 AFIX 43 H8 2 0.179110 0.616304 0.929558 11.00000 -1.20000 AFIX 0 C9 1 0.133530 0.681351 0.987755 11.00000 0.02534 0.01813 = 0.02407 -0.00270 0.00844 -0.00845 AFIX 43 H9 2 0.193244 0.693307 1.021679 11.00000 -1.20000 AFIX 0 C10 1 0.038289 0.703413 0.980868 11.00000 0.04180 0.01264 = 0.03641 0.00609 0.01992 0.00199 AFIX 43 H10 2 0.022034 0.732625 1.009957 11.00000 -1.20000 AFIX 0 C11 1 -0.030037 0.674430 0.922630 11.00000 0.02546 0.03326 = 0.02938 0.01635 0.00188 0.00508 AFIX 43 H11 2 -0.099650 0.680921 0.905493 11.00000 -1.20000 AFIX 0 C12 1 0.024941 0.634203 0.895046 11.00000 0.02985 0.03092 = 0.01480 -0.00011 0.00230 -0.00991 AFIX 43 H12 2 -0.001288 0.608785 0.855935 11.00000 -1.20000 AFIX 0 C13 1 0.127773 0.635492 1.161099 11.00000 0.02057 0.01858 = 0.02313 -0.00271 -0.00145 -0.00567 C14 1 -0.074143 0.667784 1.121197 11.00000 0.02344 0.01145 = 0.02233 -0.00091 0.00268 -0.00382 C101 1 0.704117 0.622617 0.596448 11.00000 0.00998 0.01443 = 0.01205 -0.00073 0.00083 -0.00169 C102 1 0.815967 0.617571 0.648337 11.00000 0.01170 0.01728 = 0.01653 0.00215 0.00127 -0.00166 C103 1 0.697761 0.667617 0.529942 11.00000 0.01498 0.01978 = 0.01580 0.00319 0.00075 -0.00173 C104 1 0.676715 0.576821 0.535699 11.00000 0.01354 0.01951 = 0.01530 -0.00510 0.00079 -0.00275 C105 1 0.551231 0.686979 0.855972 11.00000 0.01330 0.01203 = 0.01223 -0.00131 0.00004 0.00021 C106 1 0.461299 0.703764 0.912967 11.00000 0.01931 0.01251 = 0.01607 -0.00412 0.00160 -0.00146 C107 1 0.598075 0.731735 0.809601 11.00000 0.02272 0.01315 = 0.02058 -0.00404 0.00223 -0.00565 C108 1 0.638343 0.662626 0.920610 11.00000 0.01944 0.02166 = 0.02012 -0.00205 -0.00464 -0.00041 C109 1 0.511221 0.513318 0.775008 11.00000 0.00929 0.01026 = 0.01238 -0.00043 -0.00066 -0.00074 C110 1 0.602958 0.481434 0.821595 11.00000 0.01252 0.00956 = 0.01280 -0.00059 -0.00281 0.00018 C111 1 0.432540 0.522901 0.844790 11.00000 0.01431 0.01291 = 0.02105 0.00252 0.00466 0.00160 C112 1 0.455274 0.486163 0.689763 11.00000 0.01918 0.01240 = 0.01799 0.00040 -0.00748 0.00050 C113 1 0.340665 0.632582 0.574494 11.00000 0.01112 0.01041 = 0.01192 0.00153 -0.00334 -0.00112 C114 1 0.230681 0.625978 0.607015 11.00000 0.01171 0.01325 = 0.01712 0.00469 -0.00046 0.00315 C115 1 0.345620 0.609087 0.477958 11.00000 0.01398 0.02168 = 0.01340 -0.00112 -0.00343 0.00126 C116 1 0.363720 0.687805 0.565229 11.00000 0.01669 0.01210 = 0.02245 0.00509 -0.00260 -0.00120 C201 1 0.530032 0.686768 0.247472 11.00000 0.03593 0.03333 = 0.03287 0.00548 -0.00564 -0.00011 AFIX 23 H20A 2 0.548857 0.663586 0.297815 11.00000 -1.20000 H20B 2 0.532592 0.669541 0.188658 11.00000 -1.20000 AFIX 0 PART 2 AS2 4 0.025949 0.534083 1.063439 10.03500 0.02049 HKLF 4 REM ld448_abs_a.res in P2(1)/n REM wR2 = 0.0856, GooF = S = 1.068, Restrained GooF = 1.068 for all data REM R1 = 0.0378 for 18316 Fo > 4sig(Fo) and 0.0481 for all 21333 data REM 743 parameters refined using 0 restraints END WGHT 0.0320 5.1396 REM Highest difference peak 1.920, deepest hole -1.979, 1-sigma level 0.164 Q1 1 0.0833 0.5590 1.1192 11.00000 0.05 1.92 Q2 1 0.0657 0.6182 1.0370 11.00000 0.05 1.89 Q3 1 0.0785 0.4992 1.1216 11.00000 0.05 1.72 Q4 1 0.0556 0.4580 0.9926 11.00000 0.05 1.63 Q5 1 0.0490 0.4404 0.8336 11.00000 0.05 1.36 ; _shelx_res_checksum 81782 _shelx_hkl_file ; 0 0 -3 0.85 0.46 0 0 -4 256.99 9.30 0 0 -5 1.72 0.84 0 0 -6 1520.72 41.38 0 0 7 -0.48 1.34 0 0 -7 3.00 1.54 0 0 8 1497.74 45.27 0 0 -8 1479.54 42.70 0 0 9 1.49 2.07 0 0 -9 1.87 1.41 0 0 10 34.78 5.34 0 0 -10 29.68 4.49 0 0 11 1.64 1.96 0 0 -11 0.62 1.83 0 0 12 538.84 24.52 0 0 13 2.73 2.69 0 0 14 63.07 8.14 0 0 15 -1.73 3.73 0 0 16 38.34 7.36 0 0 17 5.27 4.73 0 0 18 543.57 28.97 0 0 19 -0.33 3.83 0 0 20 2.41 4.38 0 0 21 2.08 4.57 0 0 22 -3.06 4.81 0 0 23 -1.02 5.29 0 1 -3 55.74 3.06 0 -1 -3 61.85 3.51 0 -1 -4 143.61 6.57 0 1 -4 140.93 6.12 0 1 -5 630.36 19.13 0 -1 -5 641.31 19.83 0 -1 -6 375.27 14.18 0 1 -6 377.50 13.67 0 -1 7 307.13 14.06 0 1 7 313.90 14.55 0 1 -7 288.50 12.30 0 -1 -7 289.29 12.81 0 -1 8 241.69 12.88 0 1 8 234.53 13.17 0 -1 -8 251.61 11.91 0 1 -8 232.59 11.25 0 -1 9 12.40 3.41 0 1 9 5.23 2.19 0 1 -9 9.31 2.40 0 -1 -9 9.29 2.55 0 -1 10 7.73 2.92 0 1 10 3.92 2.97 0 1 -10 4.21 2.05 0 -1 -10 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8.83 0 -13 7 182.09 6.82 0 13 -7 160.54 10.19 0 13 7 183.19 12.33 0 -13 8 232.63 8.88 0 13 -8 231.11 12.83 0 13 8 223.91 14.66 0 13 9 133.96 11.63 0 -13 9 162.27 7.59 0 13 -9 155.94 10.68 0 13 10 421.16 22.68 0 -13 10 443.31 15.86 0 13 -10 445.95 20.43 0 13 11 23.33 5.33 0 -13 11 32.87 3.88 0 13 -11 36.61 6.00 0 13 12 5.99 4.83 0 -13 12 5.19 2.18 0 13 -12 8.07 3.64 0 13 13 198.24 16.22 0 13 -13 188.07 13.68 0 13 14 106.64 12.36 0 13 -14 109.17 10.76 0 13 15 142.25 14.63 0 13 16 121.66 14.06 0 13 17 13.63 7.04 0 13 18 58.03 11.47 0 13 19 38.87 10.01 0 13 20 146.82 17.72 0 13 21 80.75 13.18 0 -14 0 382.31 15.13 0 14 0 396.58 13.45 0 -14 -1 52.96 4.66 0 14 1 49.20 4.23 0 14 -1 50.73 6.30 0 14 -1 59.02 3.25 0 -14 1 53.12 4.81 0 14 -2 18.84 3.79 0 -14 2 31.27 3.80 0 14 2 30.86 3.53 0 14 2 27.86 2.40 0 -14 -2 26.12 3.19 0 -14 -3 256.17 11.62 0 14 3 254.02 9.69 0 14 -3 266.64 16.62 0 14 3 257.92 12.49 0 14 -4 1280.43 40.81 0 -14 -4 1187.03 36.06 0 14 4 1207.71 34.35 0 14 4 1174.98 37.63 0 14 5 402.78 18.25 0 14 -5 389.43 17.34 0 -14 6 694.86 17.31 0 14 -6 626.38 24.06 0 14 6 651.62 26.32 0 14 -7 584.58 23.46 0 14 7 624.33 26.32 0 -14 7 667.70 17.70 0 14 -8 264.80 13.89 0 14 8 261.73 15.84 0 -14 8 252.08 9.05 0 14 -9 14.49 3.82 0 14 9 16.69 3.86 0 -14 9 10.73 2.00 0 14 -10 8.87 2.64 0 14 10 3.52 3.40 0 -14 10 7.83 2.00 0 -14 11 2.95 1.58 0 14 11 5.22 4.73 0 14 -11 5.27 3.91 0 14 12 1350.20 51.15 0 14 -12 1448.25 47.48 0 14 13 375.66 23.23 0 14 -13 421.03 21.34 0 14 14 314.39 21.84 0 14 15 405.14 26.24 0 14 16 98.42 13.03 0 14 17 55.03 10.55 0 14 18 145.04 16.65 0 14 19 -7.79 7.52 0 14 20 23.83 9.13 0 14 21 149.95 17.81 0 -15 0 7.02 2.63 0 15 0 7.43 2.09 0 -15 -1 15.41 2.65 0 15 1 12.87 2.26 0 15 -1 20.12 4.03 0 15 -1 17.84 1.86 0 -15 1 14.67 2.67 0 15 -2 10.69 3.04 0 -15 2 16.14 2.98 0 15 2 19.98 3.00 0 15 2 16.13 1.94 0 -15 -2 20.51 2.86 0 -15 -3 55.18 5.06 0 15 3 55.70 4.00 0 15 -3 51.72 6.88 0 15 3 62.39 5.70 0 15 -4 117.03 10.24 0 -15 -4 88.82 6.92 0 15 4 103.97 6.59 0 15 4 108.91 8.35 0 15 -5 2471.30 70.05 0 -15 -5 2462.95 67.47 0 15 5 2467.94 69.19 0 15 -6 197.23 11.89 0 15 6 218.25 13.45 0 15 7 227.70 14.02 0 -15 7 227.44 7.03 0 15 -7 199.95 12.21 0 -15 8 39.17 2.71 0 15 8 30.45 5.32 0 15 -8 40.23 5.23 0 -15 9 72.34 4.21 0 15 9 65.51 8.18 0 15 -9 64.55 7.02 0 15 10 8.90 4.28 0 15 -10 9.48 3.56 0 15 11 1072.08 42.60 0 15 -11 1139.40 40.15 0 15 12 5.17 4.53 0 15 -12 0.24 2.70 0 15 13 1581.17 58.09 0 15 -13 1653.86 54.00 0 15 14 495.82 28.38 0 15 15 63.92 10.17 0 15 16 39.47 8.88 0 15 17 144.29 16.21 0 15 18 87.66 12.68 0 15 19 99.64 14.37 0 15 20 67.23 12.95 0 -16 0 927.79 29.74 0 16 0 937.12 27.01 0 16 -1 79.54 8.25 0 16 1 62.57 5.12 0 16 1 58.50 6.71 0 16 -1 68.71 3.94 0 -16 1 55.77 5.32 0 -16 -1 49.12 4.83 0 -16 2 162.30 9.46 0 16 2 167.94 9.21 0 16 2 158.14 7.03 0 -16 -2 158.34 8.75 0 -16 -3 21.53 3.30 0 16 3 20.75 2.47 0 16 3 19.29 3.15 0 16 -3 17.22 4.26 0 16 4 643.45 21.45 0 16 4 586.53 23.03 0 -16 -4 577.57 21.70 0 16 -4 669.20 29.99 0 16 5 66.39 7.33 0 -16 -5 59.68 5.83 0 16 -5 67.18 8.04 0 16 6 2253.19 64.92 0 16 -6 2129.04 63.93 0 -16 -6 2271.07 63.22 0 16 7 431.01 20.88 0 16 -7 428.33 19.43 0 16 8 32.05 5.66 0 16 -8 27.15 4.84 0 16 9 128.72 11.41 0 16 -9 124.64 10.22 0 16 10 12.15 4.29 0 16 -10 13.28 3.58 0 16 11 20.68 5.52 0 16 -11 21.81 4.96 0 16 12 1013.84 42.20 0 16 -12 1089.40 40.21 0 16 13 170.44 15.85 0 16 -13 190.00 14.68 0 16 14 198.49 17.39 0 16 15 49.47 9.34 0 16 16 136.57 15.44 0 16 17 -3.95 5.42 0 16 18 99.39 13.98 0 16 19 56.72 11.78 0 16 20 168.30 19.27 0 -17 0 9.91 3.14 0 17 0 13.51 3.69 0 17 0 10.03 2.18 0 17 -1 919.56 31.62 0 17 1 825.36 28.93 0 17 -1 934.55 22.99 0 17 1 710.86 24.58 0 -17 1 739.23 26.62 0 -17 -1 762.41 26.38 0 -17 -2 388.91 15.91 0 17 2 411.79 15.98 0 17 2 393.46 13.35 0 -17 2 396.89 16.82 0 17 3 71.39 4.77 0 17 3 73.32 6.57 0 -17 -3 66.84 5.66 0 17 4 5.66 1.59 0 17 4 4.14 2.17 0 17 -4 -1.29 3.20 0 -17 -4 4.52 2.15 0 17 5 1647.73 50.07 0 -17 -5 1603.83 48.03 0 17 -5 1712.51 54.99 0 17 6 813.21 30.72 0 17 -6 792.37 31.26 0 -17 -6 827.02 29.43 0 17 7 610.74 25.76 0 17 -7 569.55 24.29 0 17 8 3.69 2.40 0 17 -8 3.50 2.67 0 17 9 0.72 2.77 0 17 -9 0.15 2.44 0 17 10 118.22 11.48 0 17 -10 119.86 10.54 0 17 11 445.87 24.40 0 17 -11 473.77 23.55 0 17 12 54.44 8.65 0 17 -12 52.48 7.59 0 17 13 251.10 19.08 0 17 -13 271.07 18.07 0 17 14 4.00 4.27 0 17 15 17.63 6.79 0 17 16 21.23 7.57 0 17 17 185.31 18.65 0 17 18 22.20 7.30 0 17 19 41.54 10.11 0 17 20 15.04 8.63 0 -18 0 566.90 20.82 0 18 0 543.19 17.60 0 18 1 65.33 9.33 0 18 -1 78.73 5.29 0 18 1 69.13 6.53 0 -18 1 63.57 7.29 0 -18 -1 46.23 6.12 0 18 -2 810.98 33.25 0 -18 -2 874.49 28.30 0 18 2 874.52 27.82 0 18 2 874.68 24.98 0 -18 2 850.67 29.22 0 18 3 596.99 18.55 0 18 3 649.79 22.20 0 -18 -3 610.05 21.14 0 18 4 221.06 12.37 0 18 4 219.94 11.47 0 18 -4 196.01 15.76 0 -18 -4 231.52 11.71 0 18 5 336.31 16.88 0 -18 -5 342.20 15.86 0 18 -5 368.62 21.98 0 18 6 2304.87 68.37 0 18 -6 2428.04 71.96 0 -18 -6 2388.83 66.89 0 18 7 987.03 36.05 0 18 -7 956.02 35.73 0 -18 -7 1012.44 34.71 0 18 8 3.24 2.23 0 18 -8 7.52 3.34 0 18 9 23.12 4.83 0 18 -9 20.02 4.55 0 18 10 180.10 14.24 0 18 -10 186.39 13.57 0 18 11 197.16 15.50 0 18 -11 226.93 15.71 0 18 12 1037.58 42.98 0 18 -12 1130.41 42.29 0 18 13 250.71 18.68 0 18 14 103.54 13.20 0 18 15 76.54 11.12 0 18 16 123.68 15.00 0 18 17 124.47 15.49 0 18 18 14.92 6.67 0 18 19 39.84 10.42 0 18 20 31.00 9.63 0 -19 0 53.94 6.51 0 19 0 64.81 5.72 0 19 1 3680.60 98.17 0 19 1 3563.59 94.06 0 -19 1 3479.91 97.49 0 -19 -1 3658.32 96.93 0 19 2 229.69 9.70 0 19 -2 249.84 16.09 0 -19 -2 216.93 11.84 0 -19 2 238.98 13.04 0 19 2 236.41 11.56 0 -19 -3 105.53 7.51 0 19 3 105.91 6.22 0 19 3 116.32 8.26 0 -19 -4 216.15 11.73 0 19 4 212.22 12.16 0 19 4 228.82 11.88 0 -19 -5 579.79 22.44 0 19 5 583.33 23.85 0 -19 -6 255.67 13.99 0 19 -6 271.83 18.12 0 19 6 257.60 15.10 0 19 7 18.94 3.94 0 19 -7 22.14 5.38 0 -19 -7 23.22 4.23 0 19 8 561.73 25.57 0 19 -8 545.95 25.22 0 -19 -8 582.57 24.77 0 19 9 39.67 6.55 0 19 -9 36.11 5.59 0 19 10 407.73 22.86 0 19 -10 423.81 22.30 0 19 11 153.15 14.02 0 19 -11 200.26 15.26 0 19 12 164.60 14.88 0 19 -12 176.17 14.57 0 19 13 84.20 11.04 0 19 14 241.24 19.19 0 19 15 2.33 4.69 0 19 16 1.44 5.15 0 19 17 139.96 16.01 0 19 18 14.57 7.12 0 19 19 22.42 8.52 0 19 20 12.57 7.39 0 20 0 3952.16 100.39 0 20 0 3746.35 93.61 0 -20 0 3709.37 98.76 0 -20 1 50.85 6.57 0 -20 -1 28.98 4.75 0 20 1 31.35 5.11 0 20 -1 42.27 7.40 0 20 -1 38.74 3.79 0 20 1 34.68 4.29 0 20 1 34.99 4.03 0 20 -2 1011.52 37.21 0 20 2 954.38 29.74 0 20 2 861.58 30.99 0 -20 -2 956.58 30.94 0 -20 2 934.18 32.11 0 20 2 965.77 27.63 0 -20 -3 380.95 16.35 0 20 3 350.15 13.58 0 20 3 394.87 16.39 0 -20 -4 42.23 5.61 0 20 4 40.56 5.40 0 20 -4 42.04 8.15 0 20 4 47.24 6.28 0 20 -5 325.19 22.12 0 -20 -5 294.03 14.88 0 20 5 300.07 15.76 0 -20 -6 422.17 18.42 0 20 -6 421.11 24.09 0 20 6 377.41 19.08 0 -20 -7 355.76 17.68 0 20 -7 378.24 21.23 0 20 7 336.88 18.57 0 20 8 58.48 7.35 0 20 -8 50.21 7.21 0 -20 -8 54.91 6.77 0 20 9 97.57 10.08 0 20 -9 98.39 9.95 0 -20 -9 92.70 8.91 0 20 10 179.26 14.44 0 20 -10 183.80 14.50 0 20 11 355.48 21.36 0 20 -11 367.65 21.39 0 20 12 21.03 6.38 0 20 -12 20.08 5.72 0 20 13 -0.37 4.99 0 20 14 7.18 4.36 0 20 15 5.27 5.37 0 20 16 33.87 8.20 0 20 17 52.06 10.32 0 20 18 167.11 17.85 0 20 19 30.95 9.23 0 21 0 69.81 8.15 0 21 0 71.44 5.44 0 -21 0 57.12 7.31 0 -21 -1 178.34 10.79 0 -21 1 171.47 11.00 0 21 1 170.11 10.73 0 21 -1 178.48 12.38 0 21 1 188.03 9.09 0 21 1 161.91 8.88 0 21 -2 426.93 21.93 0 21 2 406.45 16.04 0 21 2 376.86 17.37 0 -21 -2 401.96 17.29 0 -21 2 396.99 18.35 0 21 2 408.59 14.56 0 -21 -3 32.62 4.87 0 21 3 27.81 4.51 0 21 -3 38.93 8.50 0 21 3 42.64 5.74 0 21 4 1236.72 37.17 0 -21 -4 1248.95 36.66 0 21 -5 527.49 29.63 0 -21 -5 540.52 21.64 0 21 5 537.05 22.71 0 21 -6 74.87 10.81 0 -21 -6 69.26 7.00 0 21 6 76.29 7.97 0 -21 -7 508.78 21.88 0 21 7 483.35 23.15 0 21 -7 495.77 26.37 0 21 -8 50.45 7.77 0 -21 -8 47.88 6.61 0 21 8 54.10 7.20 0 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22 9 113.59 10.73 0 22 -10 694.22 31.42 0 -22 -10 673.55 28.99 0 22 10 666.16 30.51 0 -22 -11 395.63 21.63 0 22 -11 397.07 23.41 0 22 11 427.40 23.77 0 22 12 17.69 5.69 0 22 13 8.80 4.43 0 22 14 14.28 6.22 0 22 15 62.72 9.87 0 22 16 129.80 15.47 0 22 17 30.27 7.71 0 22 18 397.55 28.18 0 22 19 8.03 7.63 0 23 0 29.06 5.45 0 -23 0 20.93 5.07 0 23 -1 708.05 27.43 0 -23 1 653.80 25.98 0 -23 -1 680.38 25.37 0 23 1 637.36 24.14 0 23 1 673.63 21.40 0 23 1 691.52 22.06 0 23 2 923.31 32.24 0 -23 2 993.85 34.77 0 -23 -2 1030.32 33.77 0 23 2 1016.07 31.06 0 23 -3 295.55 19.71 0 -23 -3 276.84 14.48 0 23 3 257.01 14.18 0 23 3 274.38 13.70 0 23 4 494.64 20.44 0 -23 -4 515.57 20.97 0 23 5 89.07 8.16 0 23 -5 65.94 10.34 0 -23 -5 89.23 7.74 0 23 6 31.86 5.12 0 23 -6 23.86 7.01 0 -23 -6 30.20 4.95 0 23 7 6.33 2.98 0 23 -7 6.98 5.64 0 -23 -7 4.43 2.11 0 23 8 187.71 13.94 0 -23 -8 195.37 12.92 0 23 -8 192.67 16.47 0 23 9 132.33 11.58 0 -23 -9 138.38 11.10 0 23 -9 140.01 13.44 0 23 10 23.87 5.73 0 -23 -10 46.49 6.83 0 23 -10 36.77 8.35 0 23 11 232.32 17.03 0 -23 -11 229.55 15.62 0 23 -11 202.33 16.63 0 23 12 45.30 8.14 0 -23 -12 52.52 8.23 0 23 13 0.90 4.08 0 -23 -13 3.33 3.82 0 23 14 44.12 9.22 0 23 15 13.41 6.55 0 23 16 69.56 10.86 0 23 17 149.76 17.11 0 23 18 4.73 6.16 0 24 0 331.85 15.91 0 -24 0 300.58 15.74 0 24 1 179.34 10.96 0 24 -1 196.26 12.91 0 24 1 200.61 9.67 0 -24 -1 184.50 11.79 0 -24 1 186.17 12.03 0 24 -2 155.25 12.88 0 -24 2 145.13 11.03 0 -24 -2 153.55 10.45 0 24 2 122.53 9.06 0 24 2 141.42 8.43 0 24 -3 412.43 23.36 0 24 3 325.40 16.35 0 -24 -3 376.58 17.40 0 24 3 359.18 15.94 0 -24 -4 23.40 4.30 0 24 4 22.98 4.48 0 24 -4 21.04 7.16 0 24 -5 86.59 11.67 0 24 5 104.43 8.85 0 -24 -5 103.43 8.55 0 24 6 104.62 9.18 0 -24 -6 119.53 9.44 0 24 -6 116.15 14.00 0 24 7 322.64 18.11 0 24 -7 350.34 25.06 0 -24 -7 336.37 17.35 0 24 -8 13.57 6.53 0 -24 -8 15.16 3.83 0 24 8 10.53 4.60 0 24 9 306.64 18.44 0 -24 -9 295.30 16.79 0 24 -9 266.79 19.30 0 24 10 753.84 33.28 0 -24 -10 784.74 31.45 0 24 -10 775.21 35.71 0 24 11 44.45 7.63 0 24 -11 46.10 8.24 0 -24 -11 49.65 6.67 0 24 12 5.86 4.55 0 -24 -12 2.49 2.97 0 24 13 481.90 26.93 0 -24 -13 424.87 23.77 0 -24 -14 18.02 5.77 0 24 14 11.44 5.64 0 24 15 365.50 24.69 0 -24 -15 308.44 21.11 0 24 16 47.11 10.55 0 -24 -16 39.05 8.73 0 24 17 212.52 19.97 0 24 18 168.52 18.48 0 -25 0 5.39 3.53 0 25 0 11.35 3.72 0 -25 -1 92.89 8.30 0 -25 1 87.22 8.48 0 25 1 80.40 7.29 0 25 -1 86.47 8.54 0 -25 2 457.24 21.14 0 -25 -2 468.86 20.23 0 25 -2 516.53 24.25 0 25 -3 61.89 9.43 0 25 3 43.85 5.76 0 -25 -3 53.41 6.32 0 25 3 43.95 5.07 0 25 -4 155.67 14.92 0 25 4 143.93 9.83 0 25 4 128.42 10.07 0 -25 -4 141.58 10.30 0 -25 -5 25.94 4.59 0 25 -5 29.57 7.92 0 25 5 28.47 4.72 0 -25 -6 20.65 4.09 0 25 6 20.04 4.18 0 25 -6 10.85 4.55 0 25 7 115.55 10.46 0 -25 -7 116.86 9.77 0 25 -7 117.37 14.01 0 25 8 480.60 23.52 0 -25 -8 495.73 22.56 0 25 -8 537.18 30.74 0 -25 -9 34.47 5.97 0 25 9 37.65 6.76 0 25 -9 39.21 7.85 0 -25 -10 13.26 4.30 0 25 10 15.68 4.83 0 25 -10 15.02 6.21 0 25 11 9.25 4.96 0 -25 -11 6.71 4.01 0 25 -11 7.78 4.68 0 25 12 535.50 27.76 0 -25 -12 500.88 25.44 0 25 13 125.73 13.16 0 -25 -13 113.28 11.69 0 25 14 662.04 33.54 0 -25 -14 609.52 30.32 0 -25 -15 18.13 5.57 0 25 15 18.94 7.37 0 -25 -16 485.87 28.26 0 25 16 548.33 31.52 0 25 17 18.79 7.39 0 -25 -17 10.89 5.76 0 25 18 8.95 8.61 0 -25 -18 7.44 5.69 0 -26 0 105.99 9.30 0 26 0 106.83 8.76 0 -26 1 512.76 22.74 0 -26 -1 496.82 21.74 0 26 1 462.20 20.03 0 26 -1 522.59 22.98 0 -26 -2 34.39 5.72 0 -26 2 35.24 6.41 0 26 2 34.79 5.24 0 26 -2 34.12 7.35 0 -26 -3 310.63 15.95 0 26 3 288.85 14.67 0 26 -3 333.05 20.52 0 26 -4 24.76 7.44 0 26 4 22.27 4.06 0 26 4 25.81 4.75 0 -26 -4 23.95 4.60 0 -26 -5 21.36 4.68 0 26 -5 23.43 7.31 0 26 5 28.23 5.17 0 -26 -6 11.53 3.89 0 26 -6 6.27 5.54 0 26 6 15.74 4.34 0 -26 -7 19.62 4.21 0 26 7 16.64 3.81 0 26 -7 13.83 4.86 0 26 8 159.48 12.85 0 -26 -8 159.60 11.87 0 26 -8 167.13 16.79 0 26 9 358.32 20.70 0 -26 -9 361.18 19.38 0 26 -9 389.81 25.28 0 -26 -10 92.44 9.28 0 26 10 81.08 9.78 0 26 -10 77.37 10.99 0 26 11 39.46 7.85 0 -26 -11 44.64 6.97 0 26 12 14.59 4.69 0 -26 -12 0.14 4.03 0 26 13 323.05 21.83 0 -26 -13 301.24 19.21 0 26 14 0.51 4.24 0 -26 -14 2.61 4.59 0 -26 -15 376.94 23.16 0 26 15 360.59 24.67 0 26 16 20.25 7.84 0 -26 -16 9.59 6.03 0 26 17 56.01 10.24 0 -26 -17 46.05 9.11 0 -26 -18 20.65 7.72 0 -27 0 7.47 3.58 0 27 0 7.97 3.32 0 -27 -1 16.17 4.14 0 -27 1 17.41 4.65 0 27 1 23.72 4.55 0 27 -1 21.03 4.98 0 -27 2 1257.15 42.54 0 -27 -2 1256.34 41.00 0 27 -2 1344.26 45.21 0 -27 -3 73.20 7.54 0 27 3 65.42 6.65 0 27 -3 83.00 10.55 0 -27 -4 193.33 12.48 0 27 4 169.51 11.81 0 27 -4 194.14 17.13 0 27 -5 21.60 7.90 0 27 5 19.29 4.84 0 27 5 18.68 3.65 0 -27 -5 20.79 4.47 0 27 6 158.25 11.60 0 27 -6 117.94 14.89 0 -27 -6 146.19 11.15 0 -27 -7 3.46 3.45 0 27 7 -0.80 3.42 0 27 -7 2.36 3.60 0 27 8 728.98 30.71 0 -27 -8 744.58 29.72 0 27 -8 740.40 39.00 0 -27 -9 0.60 3.49 0 27 9 10.09 4.23 0 27 -9 6.10 6.44 0 -27 -10 115.59 10.46 0 27 10 101.69 10.90 0 27 -10 112.45 13.93 0 27 11 61.26 8.34 0 -27 -11 62.37 7.87 0 27 12 54.67 9.15 0 -27 -12 42.63 6.44 0 27 13 26.67 7.24 0 -27 -13 15.27 5.84 0 -27 -14 29.02 6.05 0 27 14 33.02 7.83 0 -27 -15 14.91 5.51 0 27 15 8.57 6.47 0 -27 -16 151.85 14.69 0 27 16 153.61 16.89 0 27 17 48.14 10.59 0 -27 -17 34.06 8.51 0 -27 -18 2.09 4.30 0 -28 0 286.53 16.49 0 28 0 272.11 15.12 0 -28 1 367.25 19.44 0 -28 -1 375.06 18.98 0 28 1 372.25 17.67 0 28 -1 386.87 19.37 0 -28 2 64.81 8.57 0 -28 -2 61.04 7.64 0 28 -2 81.05 10.16 0 -28 -3 140.70 10.70 0 28 -3 154.39 13.75 0 28 3 115.47 8.95 0 28 -4 13.14 8.46 0 -28 -4 12.33 3.72 0 28 4 11.03 4.90 0 28 -5 380.59 26.07 0 28 5 323.24 18.12 0 -28 -5 374.77 18.50 0 28 -6 13.63 5.91 0 28 6 25.70 5.92 0 28 6 23.92 4.99 0 -28 -6 14.94 4.60 0 28 7 64.06 7.78 0 -28 -7 62.71 7.57 0 28 -7 57.09 10.69 0 28 8 53.51 7.49 0 -28 -8 53.77 7.03 0 28 -8 50.13 10.61 0 28 9 219.39 15.66 0 -28 -9 222.05 14.97 0 28 -9 228.76 20.36 0 28 10 118.85 11.83 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314.95 22.22 -8 18 -4 175.84 16.51 -8 18 -5 590.48 31.98 -8 18 -6 386.65 25.32 -8 18 -7 158.00 16.13 -8 18 -8 246.10 20.68 -8 18 -9 141.31 16.44 -8 18 -10 108.69 14.53 -8 18 -11 8.41 9.02 -8 18 -12 138.62 17.53 -8 18 -13 95.29 14.76 -8 18 -14 43.60 11.36 -8 18 -15 76.23 15.36 -8 18 -16 384.62 32.24 -8 18 -17 9.90 13.42 -8 18 -18 88.18 18.87 -8 19 18 11.05 6.11 8 -19 -18 17.30 7.51 -8 19 17 62.43 10.29 8 -19 -17 67.92 11.26 -8 19 16 21.49 6.95 8 -19 -16 15.11 5.62 -8 19 15 172.91 15.93 8 -19 -15 207.45 18.96 -8 19 14 -1.26 4.09 8 -19 -14 14.57 6.55 -8 19 13 589.10 29.88 8 -19 -13 639.02 32.58 8 -19 -12 31.05 7.61 -8 19 12 18.67 4.77 -8 19 12 18.13 4.35 8 -19 -11 158.54 14.46 -8 19 11 150.15 11.36 -8 19 11 154.16 13.24 -8 19 11 146.13 16.78 8 -19 -10 296.21 19.15 -8 19 10 276.59 16.25 -8 19 10 287.17 18.09 -8 19 10 254.90 21.09 8 -19 -9 11.53 3.51 -8 19 9 13.88 4.24 -8 19 9 19.55 5.13 -8 19 9 23.89 4.84 8 -19 -8 182.29 13.98 -8 19 8 173.62 15.09 -8 19 8 162.87 13.19 -8 19 8 165.64 12.89 8 -19 -7 977.15 37.84 -8 19 7 999.89 40.52 -8 19 7 1046.15 39.14 -8 19 7 1100.15 39.83 8 -19 -6 148.98 12.17 -8 19 6 149.78 13.06 -8 19 6 162.47 13.11 -8 19 6 164.16 13.71 8 -19 -5 1507.98 51.90 -8 19 5 1568.44 52.52 -8 19 5 1636.52 54.83 8 -19 -4 82.99 8.86 -8 19 4 91.23 10.41 -8 19 4 91.21 9.12 -8 19 4 116.32 12.26 -8 19 3 197.79 13.57 -8 19 3 237.14 18.92 -8 19 3 229.01 17.36 8 -19 -3 198.89 14.46 -8 19 2 1.53 4.30 8 -19 -2 3.91 2.93 -8 19 2 3.37 2.70 -8 19 2 2.32 3.49 -8 19 1 50.46 7.49 8 -19 -1 46.58 7.26 -8 19 1 34.23 5.44 -8 19 1 49.18 9.80 -8 19 0 441.96 21.47 8 -19 0 435.95 24.36 -8 19 0 429.10 21.32 8 -19 1 2.78 2.96 -8 19 -1 8.79 3.54 -8 19 -1 14.55 5.99 8 -19 2 18.25 5.79 -8 19 -2 20.18 4.51 -8 19 -2 21.68 7.39 8 -19 3 100.39 12.06 -8 19 -3 118.55 11.12 -8 19 -3 128.95 15.17 -8 19 -4 473.04 28.93 -8 19 -5 172.79 17.13 -8 19 -6 14.09 5.48 -8 19 -7 22.89 6.89 -8 19 -8 2.87 5.21 -8 19 -9 298.63 24.09 -8 19 -10 7.12 8.25 -8 19 -11 328.50 26.18 -8 19 -12 7.44 6.13 -8 19 -13 5.35 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32.21 11.99 11 -18 -17 196.47 19.22 -11 18 17 183.14 17.43 11 -18 -16 32.42 7.59 -11 18 16 40.49 8.81 11 -18 -15 335.85 23.88 -11 18 15 315.94 22.26 11 -18 -14 76.36 11.65 -11 18 14 75.23 10.87 11 -18 -13 59.19 9.87 -11 18 13 59.56 9.11 11 -18 -12 10.81 4.73 -11 18 12 6.24 4.60 -11 18 12 -2.99 5.63 11 -18 -11 23.63 6.17 -11 18 11 17.71 5.82 -11 18 11 17.03 5.78 11 -18 -10 -0.27 3.98 -11 18 10 -2.76 4.35 -11 18 10 5.80 3.66 -11 18 9 758.03 37.80 -11 18 9 751.54 35.26 -11 18 9 836.41 33.47 11 -18 -9 770.22 33.87 -11 18 8 193.76 14.42 11 -18 -8 169.07 14.28 -11 18 8 179.45 15.63 -11 18 8 173.64 15.99 11 -18 -7 4.80 4.20 -11 18 7 0.43 3.45 -11 18 7 5.67 4.23 -11 18 7 2.80 3.52 11 -18 -6 27.70 6.19 -11 18 6 35.49 6.82 -11 18 6 29.59 6.13 -11 18 6 34.66 8.02 11 -18 -5 51.95 8.09 -11 18 5 49.47 9.75 -11 18 5 43.51 7.15 -11 18 5 56.79 7.88 11 -18 -4 20.99 5.63 -11 18 4 11.58 5.19 -11 18 4 18.97 5.30 -11 18 4 16.35 5.05 11 -18 -3 152.52 15.09 -11 18 3 161.55 18.28 -11 18 3 156.56 13.07 -11 18 3 136.05 13.16 11 -18 -2 87.62 12.59 -11 18 2 73.09 11.80 -11 18 2 89.78 11.18 -11 18 2 91.41 9.90 -11 18 1 130.70 11.92 -11 18 1 131.25 13.39 11 -18 -1 167.21 16.63 -11 18 0 36.20 6.50 -11 18 0 39.05 7.84 11 -18 0 28.17 8.15 -11 18 -1 278.92 18.52 -11 18 -1 278.27 20.70 11 -18 1 244.43 21.82 -11 18 -2 23.29 6.90 -11 18 -2 13.72 6.33 11 -18 2 19.28 7.12 -11 18 -3 121.62 14.55 -11 18 -3 141.27 13.91 -11 18 -4 50.37 9.25 -11 18 -4 51.15 9.16 -11 18 -5 47.95 9.82 -11 18 -5 53.70 9.40 -11 18 -6 80.98 12.62 -11 18 -6 85.23 11.76 -11 18 -7 150.96 17.57 -11 18 -7 168.58 16.35 -11 18 -8 480.49 34.78 -11 18 -9 349.66 29.03 -11 18 -10 17.93 10.10 -11 18 -11 36.91 12.31 -11 18 -12 20.05 9.44 -11 18 -13 179.40 22.19 -11 18 -14 86.45 22.52 -11 18 -15 77.74 15.88 -11 19 17 47.65 8.85 11 -19 -17 58.26 10.77 -11 19 16 306.40 22.17 11 -19 -16 307.94 23.63 -11 19 15 171.10 16.28 11 -19 -15 176.84 17.79 -11 19 14 332.26 22.61 11 -19 -14 317.03 23.33 -11 19 13 17.47 4.77 11 -19 -13 20.48 6.75 -11 19 12 13.33 5.77 -11 19 12 16.00 7.20 11 -19 -12 14.00 4.56 -11 19 11 61.70 9.60 11 -19 -11 72.18 10.05 -11 19 11 56.24 10.67 11 -19 -10 24.70 5.93 -11 19 10 25.78 5.15 -11 19 10 29.18 7.31 -11 19 10 26.47 6.90 11 -19 -9 8.25 5.30 -11 19 9 -0.44 3.29 -11 19 9 5.11 4.26 -11 19 9 7.79 4.99 -11 19 8 326.14 20.00 -11 19 8 289.96 20.66 -11 19 8 269.88 20.23 11 -19 -8 284.92 19.01 -11 19 7 241.43 17.42 -11 19 7 218.70 17.73 11 -19 -7 230.85 16.87 -11 19 6 4.10 3.10 -11 19 6 2.60 3.90 -11 19 6 1.96 3.72 11 -19 -6 0.29 3.84 -11 19 5 19.70 5.36 -11 19 5 11.41 5.22 -11 19 5 7.80 3.57 11 -19 -5 6.49 3.83 11 -19 -4 144.27 14.05 -11 19 4 146.84 16.79 -11 19 4 125.81 12.16 -11 19 4 139.76 13.77 -11 19 3 46.65 9.73 11 -19 -3 39.67 7.96 -11 19 3 31.82 6.94 -11 19 3 32.86 6.43 -11 19 2 82.97 12.20 -11 19 2 75.41 9.22 -11 19 2 69.51 10.55 11 -19 -2 74.56 10.86 -11 19 1 153.01 12.96 -11 19 1 156.64 15.72 11 -19 -1 174.86 17.14 -11 19 0 47.32 7.54 -11 19 0 61.49 10.12 11 -19 0 46.76 9.31 -11 19 -1 139.08 13.11 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3.73 -11 21 5 26.33 6.50 -11 21 5 38.15 7.93 -11 21 5 27.32 6.28 11 -21 -5 35.10 7.16 11 -21 -4 263.52 19.20 -11 21 4 293.69 22.87 -11 21 4 261.10 18.07 -11 21 4 303.49 22.14 -11 21 3 48.07 9.28 -11 21 3 37.17 7.13 11 -21 -3 40.00 7.86 -11 21 3 46.86 9.78 11 -21 -2 179.34 16.93 -11 21 2 199.06 18.19 -11 21 2 198.78 18.53 -11 21 2 182.48 14.49 -11 21 1 13.55 4.13 11 -21 -1 21.17 7.19 -11 21 0 0.58 3.70 -11 21 0 4.60 4.56 11 -21 0 9.51 5.73 -11 21 -1 9.56 4.61 -11 21 -1 5.68 5.63 11 -21 1 8.75 6.22 -11 21 -2 56.19 9.43 -11 21 -2 53.67 10.85 11 -21 2 42.12 9.88 -11 21 -3 418.22 30.77 -11 21 -3 423.41 25.75 -11 21 -4 216.71 21.87 -11 21 -4 172.47 16.63 -11 21 -5 15.66 6.09 -11 21 -5 12.21 5.43 -11 21 -6 88.44 15.01 -11 21 -6 86.58 12.41 -11 21 -7 15.47 10.81 -11 21 -7 10.84 6.23 -11 21 -8 42.17 9.08 -11 21 -8 39.07 10.11 -11 21 -9 204.67 23.42 -11 21 -10 92.14 18.83 -11 21 -11 333.23 30.95 -11 21 -12 122.72 20.17 -11 21 -13 25.26 15.51 -11 21 -14 133.31 21.03 -11 22 16 3.22 4.98 11 -22 -16 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8.11 -11 23 10 30.72 6.57 -11 23 10 30.32 8.53 11 -23 -9 29.03 6.28 -11 23 9 36.23 8.06 -11 23 9 28.79 6.41 -11 23 9 25.26 7.02 11 -23 -8 155.86 14.38 -11 23 8 158.37 15.95 -11 23 8 171.43 15.20 -11 23 8 169.17 16.64 11 -23 -7 36.56 7.19 -11 23 7 37.17 8.51 -11 23 7 43.90 7.94 -11 23 7 41.87 7.87 11 -23 -6 45.32 7.90 -11 23 6 56.17 10.31 -11 23 6 42.57 7.85 -11 23 6 55.42 9.74 -11 23 5 85.98 12.23 -11 23 5 52.68 8.70 -11 23 5 67.35 9.76 11 -23 -5 66.83 10.01 11 -23 -4 400.50 25.13 -11 23 4 530.56 29.51 -11 23 4 431.72 24.65 -11 23 4 528.90 32.14 11 -23 -3 391.68 25.33 -11 23 3 486.19 27.97 -11 23 3 405.46 23.64 -11 23 3 446.00 31.01 11 -23 -2 412.00 26.79 -11 23 2 467.60 26.28 -11 23 2 471.10 32.46 -11 23 2 408.15 23.31 -11 23 1 46.28 7.93 -11 23 1 58.84 11.53 11 -23 -1 58.79 11.02 -11 23 0 247.45 18.08 -11 23 0 269.65 26.33 11 -23 0 280.55 22.85 -11 23 -1 202.47 16.57 -11 23 -1 215.36 22.94 11 -23 1 206.73 19.80 -11 23 -2 18.51 5.55 11 -23 2 14.11 5.49 -11 23 -3 363.75 31.63 -11 23 -3 330.92 22.96 -11 23 -4 319.89 30.29 -11 23 -4 356.32 24.39 -11 23 -5 82.55 15.89 -11 23 -5 104.71 13.27 -11 23 -6 10.58 9.44 -11 23 -6 -3.02 5.07 -11 23 -7 146.85 21.94 -11 23 -7 145.46 16.74 -11 23 -8 11.76 11.01 -11 23 -8 0.48 5.12 -11 23 -9 137.00 21.92 -11 23 -10 74.53 15.83 -11 23 -11 178.80 24.26 -11 23 -12 10.44 11.38 -11 23 -13 38.49 12.91 -11 24 15 12.88 6.42 11 -24 -15 4.21 6.29 -11 24 14 18.08 7.25 11 -24 -14 22.01 8.15 -11 24 13 35.68 8.15 11 -24 -13 29.44 9.05 -11 24 12 35.43 8.35 11 -24 -12 66.69 11.38 -11 24 11 47.19 9.20 -11 24 11 35.34 7.52 11 -24 -11 57.70 10.23 11 -24 -10 4.36 4.93 -11 24 10 8.95 4.67 -11 24 10 9.86 4.91 -11 24 10 -2.92 4.76 11 -24 -9 45.29 7.66 -11 24 9 58.10 9.60 -11 24 9 50.16 8.63 -11 24 9 44.22 9.42 11 -24 -8 370.01 23.33 -11 24 8 396.38 25.66 -11 24 8 365.75 22.14 -11 24 8 367.29 24.99 11 -24 -7 29.19 6.88 -11 24 7 41.33 8.65 -11 24 7 24.50 6.58 -11 24 7 29.44 6.52 -11 24 6 132.89 15.35 -11 24 6 127.16 13.33 -11 24 6 123.10 12.90 11 -24 -6 111.41 12.11 -11 24 5 88.10 13.59 11 -24 -5 77.20 10.42 -11 24 5 86.30 10.54 -11 24 5 95.56 11.54 -11 24 4 42.79 8.01 -11 24 4 49.05 10.84 -11 24 4 24.60 5.76 11 -24 -4 44.96 8.41 11 -24 -3 698.86 35.35 -11 24 3 760.01 35.93 -11 24 3 691.26 32.84 -11 24 2 241.82 17.70 11 -24 -2 269.68 21.36 11 -24 -1 124.54 14.35 -11 24 1 117.97 12.18 11 -24 0 623.73 35.94 -11 24 0 728.82 45.82 -11 24 0 634.04 30.79 11 -24 1 125.92 15.50 -11 24 -1 140.11 20.53 -11 24 -1 142.63 13.94 11 -24 2 61.05 12.32 -11 24 -2 74.72 10.80 -11 24 -2 85.46 16.70 -11 24 -3 188.76 17.41 -11 24 -3 195.96 25.50 -11 24 -4 23.28 6.25 -11 24 -4 27.58 10.86 -11 24 -5 258.57 20.88 -11 24 -5 272.11 31.10 -11 24 -6 250.46 21.38 -11 24 -6 281.99 31.20 -11 24 -7 -2.47 4.87 -11 24 -7 8.84 10.96 -11 24 -8 60.54 11.32 -11 24 -8 57.81 15.16 -11 24 -9 14.17 8.64 -11 24 -10 141.68 23.38 -11 24 -11 63.57 18.41 -11 24 -12 48.18 16.56 -11 25 15 4.77 5.22 11 -25 -14 39.92 8.78 -11 25 14 41.22 8.15 11 -25 -13 156.95 16.67 -11 25 13 116.56 13.18 11 -25 -12 1.55 5.12 -11 25 12 2.22 4.11 11 -25 -11 7.21 5.69 -11 25 11 -0.57 4.04 -11 25 10 13.59 6.57 11 -25 -10 8.09 4.66 -11 25 10 4.25 4.69 -11 25 9 151.43 16.25 -11 25 9 144.98 13.62 11 -25 -9 150.16 14.79 -11 25 9 167.59 16.36 11 -25 -8 8.97 4.57 -11 25 8 30.94 7.98 -11 25 8 16.72 4.94 -11 25 8 21.48 7.01 -11 25 7 114.03 14.20 -11 25 7 113.42 12.70 11 -25 -7 108.19 12.25 -11 25 7 108.10 12.97 -11 25 6 18.01 6.79 11 -25 -6 11.97 4.00 -11 25 6 19.28 6.10 -11 25 6 21.51 6.13 11 -25 -5 218.11 17.41 -11 25 5 262.85 19.10 -11 25 5 226.52 17.96 -11 25 5 272.14 23.33 -11 25 4 20.45 5.76 -11 25 4 40.96 9.87 11 -25 -4 33.46 7.66 11 -25 -3 173.81 16.25 -11 25 3 211.80 21.94 -11 25 3 186.32 15.33 11 -25 -2 40.62 8.45 -11 25 2 45.30 7.80 11 -25 -1 1156.89 50.76 -11 25 1 1096.29 44.54 11 -25 0 19.45 7.41 -11 25 0 27.52 9.39 -11 25 0 17.75 5.89 11 -25 1 791.85 42.78 -11 25 -1 829.76 37.64 11 -25 2 5.15 4.36 -11 25 -2 4.13 7.73 -11 25 -2 9.51 5.30 -11 25 -3 105.47 20.88 -11 25 -3 71.50 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105.49 12.42 12 -14 -14 44.27 8.04 -12 14 14 40.90 7.64 12 -14 -13 7.04 4.29 -12 14 13 10.72 5.46 -12 -14 13 7.57 4.40 12 -14 -12 215.99 16.88 -12 -14 12 227.66 15.39 -12 14 12 197.78 16.90 -12 14 12 217.43 20.48 12 -14 -11 37.62 6.79 -12 -14 11 43.09 6.82 -12 14 11 54.86 10.39 -12 14 11 40.46 8.21 12 -14 -10 323.62 20.33 -12 14 10 337.22 22.44 -12 14 9 47.07 8.99 -12 14 9 52.23 10.49 12 -14 -9 41.80 7.21 -12 14 8 56.04 7.26 -12 14 8 53.39 9.53 -12 14 8 55.05 9.31 12 -14 -8 45.07 7.51 -12 14 7 55.63 7.02 -12 14 7 39.56 9.29 -12 14 7 48.41 7.99 12 -14 -7 57.59 8.63 -12 14 6 110.92 10.55 -12 14 6 95.90 15.06 -12 14 6 116.68 12.26 12 -14 -6 126.19 12.82 -12 14 5 -3.23 3.77 12 -14 -5 -2.66 4.53 -12 14 5 -1.68 3.26 -12 14 5 0.10 3.91 -12 14 4 565.91 26.02 -12 14 4 574.72 27.67 12 -14 -3 136.31 15.68 -12 14 3 127.59 11.83 -12 14 3 124.69 11.54 -12 -14 2 3.19 2.76 -12 14 2 6.37 4.24 -12 14 2 3.57 4.35 -12 14 2 -0.89 2.98 12 -14 -2 1.94 4.36 12 -14 -1 15.66 5.21 -12 -14 1 28.50 4.75 -12 14 1 25.74 5.21 -12 14 1 26.93 6.11 12 -14 0 129.76 16.56 -12 14 0 143.08 12.20 -12 14 0 137.34 13.36 -12 14 -1 222.90 16.36 12 -14 1 210.00 20.45 -12 14 -1 245.39 18.44 12 -14 2 1313.57 56.59 -12 14 -2 1171.80 46.63 -12 14 -2 1243.09 49.86 -12 14 -3 164.75 14.85 -12 14 -3 154.58 15.68 -12 14 -4 150.77 14.59 -12 14 -4 141.08 16.07 -12 14 -5 15.07 4.44 -12 14 -5 13.38 6.41 -12 14 -6 157.98 15.57 -12 14 -6 161.45 17.73 -12 14 -7 34.02 7.52 -12 14 -7 16.60 7.89 -12 14 -8 63.72 11.02 -12 14 -8 86.13 14.36 -12 14 -9 69.92 11.27 -12 14 -9 78.85 13.46 -12 14 -10 197.79 21.53 -12 14 -11 1.68 5.95 -12 14 -12 193.37 21.94 -12 14 -13 31.32 10.50 -12 14 -14 12.22 10.42 -12 14 -15 3.77 9.89 12 -15 -18 6.84 5.91 12 -15 -17 26.32 7.46 -12 15 17 39.00 9.87 12 -15 -16 36.15 8.70 -12 15 16 16.15 6.32 12 -15 -15 17.72 6.18 -12 15 15 28.76 7.69 12 -15 -14 13.25 6.16 -12 15 14 11.57 5.57 12 -15 -13 240.94 18.36 -12 15 13 228.42 18.36 12 -15 -12 14.45 5.91 -12 15 12 -3.89 3.82 -12 15 12 10.66 6.94 12 -15 -11 121.42 12.58 -12 -15 11 129.68 11.42 -12 15 11 111.52 12.46 -12 15 11 134.66 15.19 12 -15 -10 41.39 7.53 -12 15 10 39.47 8.27 -12 15 10 34.06 8.33 -12 15 9 249.77 19.85 12 -15 -9 286.94 18.81 -12 15 9 274.47 21.00 12 -15 -8 351.65 21.56 -12 15 8 337.87 24.19 -12 15 8 359.23 19.23 -12 15 8 399.07 24.89 12 -15 -7 3.54 3.21 -12 15 7 5.53 4.33 -12 15 7 8.93 3.44 -12 15 7 5.79 3.31 12 -15 -6 1.17 4.80 -12 15 6 5.76 2.92 -12 15 6 4.43 3.39 -12 15 6 5.16 5.29 12 -15 -5 226.85 18.41 -12 15 5 191.33 13.84 -12 15 5 213.58 16.27 -12 15 4 331.75 19.49 -12 15 4 368.06 21.20 12 -15 -3 409.54 27.63 -12 15 3 359.23 20.70 -12 15 3 348.71 20.59 -12 15 2 81.44 9.69 -12 15 2 55.34 10.35 12 -15 -2 81.93 12.73 -12 15 2 84.45 9.73 -12 15 1 64.14 8.31 -12 -15 1 42.00 5.36 12 -15 -1 65.70 11.91 -12 15 1 66.92 9.42 -12 15 0 210.26 15.55 -12 15 0 212.03 16.87 12 -15 1 1723.72 70.23 -12 15 -1 1770.29 59.81 -12 15 -1 1760.40 62.74 12 -15 2 8.51 6.52 -12 15 -2 5.55 5.11 -12 15 -2 12.70 7.33 -12 15 -3 194.13 17.54 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20 7 39.08 7.72 -12 20 7 42.60 9.11 12 -20 -6 52.73 8.71 -12 20 6 59.27 10.91 -12 20 6 54.39 9.02 -12 20 6 62.96 9.14 12 -20 -5 1.04 4.11 -12 20 5 2.35 4.52 -12 20 5 4.65 3.50 -12 20 5 0.96 3.88 12 -20 -4 188.31 17.17 -12 20 4 200.73 20.67 -12 20 4 179.17 15.32 -12 20 4 191.00 16.63 -12 20 3 61.60 11.24 -12 20 3 44.97 8.10 -12 20 3 59.17 9.31 12 -20 -3 60.02 10.39 -12 20 2 11.89 4.25 -12 20 2 16.60 5.54 12 -20 -2 10.43 5.72 -12 20 1 35.88 6.99 -12 20 1 42.47 8.98 12 -20 -1 46.59 10.83 -12 20 0 116.76 12.43 -12 20 0 105.78 13.90 12 -20 0 107.21 14.95 -12 20 -1 18.40 6.27 -12 20 -1 14.74 7.23 12 -20 1 3.60 5.88 -12 20 -2 105.91 12.68 -12 20 -2 96.02 14.00 12 -20 2 91.43 14.34 -12 20 -3 631.89 37.82 -12 20 -3 648.57 33.76 -12 20 -4 124.44 17.72 -12 20 -4 91.88 12.62 -12 20 -5 67.75 13.20 -12 20 -5 68.95 11.22 -12 20 -6 334.92 24.65 -12 20 -6 302.43 27.28 -12 20 -7 5.08 5.74 -12 20 -7 16.91 11.01 -12 20 -8 121.79 15.31 -12 20 -8 131.26 18.69 -12 20 -9 19.82 8.50 -12 20 -9 29.97 11.89 -12 20 -10 2.48 6.08 -12 20 -10 4.36 8.60 -12 20 -11 114.40 21.60 -12 20 -12 147.06 20.86 -12 20 -13 100.93 20.24 -12 21 15 163.95 16.23 12 -21 -15 153.58 16.88 -12 21 14 256.66 20.20 12 -21 -14 304.43 22.34 -12 21 13 22.20 8.48 -12 21 13 18.20 6.43 12 -21 -13 22.80 7.22 -12 21 12 113.83 15.57 -12 21 12 95.88 11.70 12 -21 -12 119.46 13.96 -12 21 11 104.41 14.46 -12 21 11 116.17 12.87 12 -21 -11 97.50 11.64 -12 21 10 202.39 19.32 -12 21 10 232.54 18.19 12 -21 -10 198.10 16.80 12 -21 -9 71.22 9.84 -12 21 9 80.38 9.90 -12 21 9 76.40 10.79 -12 21 9 73.21 11.57 12 -21 -8 6.01 4.16 -12 21 8 6.35 3.82 -12 21 8 10.54 5.23 -12 21 8 14.79 5.79 -12 21 7 109.39 12.07 -12 21 7 114.57 14.17 -12 21 7 96.51 12.26 12 -21 -7 115.29 12.51 12 -21 -6 179.37 16.05 -12 21 6 175.74 16.06 -12 21 6 188.48 16.55 12 -21 -5 280.58 20.31 -12 21 5 300.95 24.58 -12 21 5 276.18 19.87 -12 21 5 294.38 21.17 12 -21 -4 216.51 18.22 -12 21 4 245.16 22.09 -12 21 4 197.63 16.20 -12 21 4 226.47 18.92 12 -21 -3 440.29 28.25 -12 21 3 396.13 26.31 -12 21 3 385.17 23.22 12 -21 -2 74.71 12.34 -12 21 2 48.06 9.36 -12 21 2 48.15 8.09 12 -21 -1 0.17 4.97 -12 21 1 2.85 4.73 -12 21 1 2.95 3.86 12 -21 0 24.68 7.36 -12 21 0 33.09 8.51 -12 21 0 30.66 7.63 12 -21 1 228.58 23.00 -12 21 -1 246.31 22.11 -12 21 -1 210.19 17.24 12 -21 2 233.30 22.92 -12 21 -2 238.80 22.36 -12 21 -2 293.24 20.92 -12 21 -3 46.97 12.09 -12 21 -3 46.99 9.26 -12 21 -4 473.12 34.04 -12 21 -4 484.09 29.35 -12 21 -5 7.87 7.63 -12 21 -5 8.38 5.34 -12 21 -6 56.57 12.38 -12 21 -6 54.02 10.68 -12 21 -7 361.59 26.82 -12 21 -7 345.78 30.46 -12 21 -8 82.99 12.87 -12 21 -8 88.79 16.43 -12 21 -9 88.51 13.61 -12 21 -9 92.16 18.30 -12 21 -10 266.08 23.43 -12 21 -10 249.89 27.56 -12 21 -11 57.36 15.18 -12 21 -12 112.24 21.83 -12 21 -13 108.72 19.74 12 -22 -15 97.64 13.20 -12 22 15 102.04 12.99 12 -22 -14 31.59 7.93 -12 22 14 16.23 6.32 12 -22 -13 67.69 10.70 -12 22 13 68.87 10.51 -12 22 13 59.06 12.08 12 -22 -12 41.42 9.52 -12 22 12 28.36 7.71 -12 22 12 31.08 7.70 12 -22 -11 95.37 11.82 -12 22 11 106.87 11.78 -12 22 11 98.35 13.72 -12 22 10 94.20 11.58 -12 22 10 81.69 12.59 12 -22 -10 91.79 11.77 -12 22 9 49.72 8.68 -12 22 9 50.58 8.84 -12 22 9 42.36 8.37 12 -22 -9 56.81 9.27 -12 22 8 190.26 16.60 -12 22 8 192.47 17.91 12 -22 -8 162.28 14.63 -12 22 8 188.31 16.96 -12 22 7 371.49 24.23 -12 22 7 378.99 25.30 -12 22 7 344.38 23.74 12 -22 -7 344.44 22.27 12 -22 -6 107.08 12.12 -12 22 6 124.23 14.98 -12 22 6 115.00 12.83 -12 22 6 146.11 14.77 12 -22 -5 18.17 5.85 -12 22 5 28.53 7.71 -12 22 5 12.34 4.86 -12 22 5 22.54 5.92 12 -22 -4 567.88 31.42 -12 22 4 620.27 35.39 -12 22 4 542.32 28.79 -12 22 4 600.47 33.94 -12 22 3 34.04 8.35 12 -22 -3 26.54 8.28 -12 22 3 16.14 5.05 -12 22 3 28.61 7.74 12 -22 -2 110.31 14.39 -12 22 2 65.47 9.28 -12 22 2 89.09 12.56 12 -22 -1 55.22 10.63 -12 22 1 37.52 7.31 -12 22 1 48.39 10.42 12 -22 0 45.93 10.84 -12 22 0 54.15 8.88 -12 22 0 44.17 10.51 12 -22 1 17.56 6.35 -12 22 -1 36.56 7.81 -12 22 -1 30.42 8.52 12 -22 2 18.14 7.70 -12 22 -2 20.25 7.83 -12 22 -2 25.90 7.02 -12 22 -3 350.05 29.60 -12 22 -3 361.80 24.49 -12 22 -4 18.63 8.17 -12 22 -4 7.30 5.50 -12 22 -5 74.17 15.26 -12 22 -5 69.36 11.35 -12 22 -6 25.19 11.41 -12 22 -6 13.55 6.83 -12 22 -7 30.85 12.21 -12 22 -7 40.89 10.73 -12 22 -8 21.19 7.24 -12 22 -8 9.87 9.09 -12 22 -9 435.43 30.17 -12 22 -9 421.80 37.39 -12 22 -10 38.30 9.11 -12 22 -10 29.94 15.70 -12 22 -11 482.33 41.27 -12 22 -12 45.67 16.39 -12 23 15 7.37 4.52 12 -23 -14 84.92 12.63 -12 23 14 58.56 9.86 12 -23 -13 11.23 6.68 -12 23 13 7.60 6.17 -12 23 13 5.62 7.21 12 -23 -12 84.78 12.46 -12 23 12 70.90 10.35 -12 23 12 88.80 13.98 12 -23 -11 162.09 15.72 -12 23 11 168.08 15.04 -12 23 11 128.25 16.58 -12 23 10 65.77 9.95 -12 23 10 84.84 13.18 12 -23 -10 68.39 10.48 -12 23 9 99.11 12.62 -12 23 9 77.47 10.11 -12 23 9 79.96 12.33 12 -23 -9 73.43 10.27 -12 23 8 103.43 12.95 -12 23 8 83.66 11.48 -12 23 8 68.52 10.91 12 -23 -8 65.33 9.63 12 -23 -7 295.62 20.80 -12 23 7 352.51 23.64 -12 23 7 309.90 22.68 -12 23 7 369.81 24.93 12 -23 -6 267.54 19.98 -12 23 6 301.36 22.65 -12 23 6 290.94 21.02 -12 23 6 310.28 23.62 12 -23 -5 191.96 17.01 -12 23 5 211.36 19.21 -12 23 5 188.37 16.18 -12 23 5 206.03 19.25 12 -23 -4 131.95 14.57 -12 23 4 164.84 16.64 -12 23 4 123.33 12.71 -12 23 4 155.78 17.28 12 -23 -3 579.92 33.00 -12 23 3 612.16 33.79 -12 23 3 536.38 28.37 -12 23 3 594.85 35.41 12 -23 -2 148.63 16.80 -12 23 2 151.66 17.70 -12 23 2 149.08 13.87 12 -23 -1 5.99 6.53 -12 23 1 6.46 5.02 -12 23 1 11.33 7.53 12 -23 0 270.73 23.85 -12 23 0 246.41 18.70 -12 23 0 275.69 25.61 12 -23 1 22.20 8.49 -12 23 -1 36.24 7.86 -12 23 -1 18.56 7.53 12 -23 2 19.41 7.84 -12 23 -2 33.09 7.28 -12 23 -2 35.69 11.04 -12 23 -3 125.82 14.22 -12 23 -3 117.98 17.77 -12 23 -4 116.98 14.10 -12 23 -4 110.48 18.60 -12 23 -5 68.91 12.05 -12 23 -5 69.62 16.82 -12 23 -6 7.24 5.40 -12 23 -6 4.10 6.82 -12 23 -7 254.39 22.71 -12 23 -7 224.54 28.54 -12 23 -8 88.79 14.50 -12 23 -8 124.19 21.67 -12 23 -9 50.95 11.71 -12 23 -9 26.51 16.88 -12 23 -10 175.54 19.52 -12 23 -10 165.55 24.12 -12 23 -11 14.06 7.27 -12 23 -11 20.00 20.24 -12 23 -12 101.25 20.75 12 -24 -14 39.31 8.79 -12 24 14 18.05 5.62 12 -24 -13 119.92 15.00 -12 24 13 100.62 12.16 12 -24 -12 16.41 8.00 -12 24 12 7.90 6.25 -12 24 12 8.65 4.40 12 -24 -11 20.30 5.93 -12 24 11 26.27 6.82 -12 24 11 31.54 8.87 12 -24 -10 119.14 13.49 -12 24 10 111.98 14.78 -12 24 10 119.90 12.72 -12 24 9 472.31 30.44 -12 24 9 459.69 26.32 12 -24 -9 458.33 27.11 -12 24 9 485.24 29.51 12 -24 -8 133.47 13.81 -12 24 8 144.14 14.27 -12 24 8 142.00 15.29 -12 24 8 174.62 17.32 12 -24 -7 581.58 30.72 -12 24 7 680.52 33.80 -12 24 7 616.31 33.73 -12 24 7 671.49 36.35 12 -24 -6 4.95 4.13 -12 24 6 9.73 4.17 -12 24 6 5.69 3.89 -12 24 6 12.38 5.74 12 -24 -5 11.38 4.08 -12 24 5 13.19 5.89 -12 24 5 10.41 5.39 -12 24 5 24.66 8.44 12 -24 -4 127.45 13.92 -12 24 4 158.38 16.07 -12 24 4 127.23 13.00 -12 24 4 172.95 18.64 12 -24 -3 447.31 27.91 -12 24 3 455.20 32.03 -12 24 3 398.50 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6.26 -12 25 9 9.23 5.07 12 -25 -9 0.57 3.81 -12 25 8 471.22 30.30 -12 25 8 448.36 26.08 12 -25 -8 463.04 27.00 -12 25 8 463.66 29.29 -12 25 7 2.84 5.25 12 -25 -7 4.14 4.63 -12 25 7 5.33 5.55 -12 25 7 -5.93 5.32 -12 25 6 152.71 15.60 -12 25 6 160.47 17.53 -12 25 6 137.08 14.73 12 -25 -6 137.40 13.95 12 -25 -5 7.07 4.63 -12 25 5 8.38 5.16 -12 25 5 8.02 5.41 -12 25 5 13.39 8.34 12 -25 -4 62.64 10.63 -12 25 4 62.24 9.78 -12 25 4 68.40 12.35 12 -25 -3 233.32 19.69 -12 25 3 219.50 17.40 -12 25 3 265.02 24.87 12 -25 -2 939.93 44.90 -12 25 2 1018.99 53.07 -12 25 1 17.77 11.95 -12 25 1 13.52 5.64 12 -25 -1 7.45 7.05 -12 25 0 161.89 21.54 -12 25 0 140.06 13.97 12 -25 0 165.07 18.46 -12 25 -1 2.27 8.51 -12 25 -1 0.73 4.50 12 -25 1 -1.54 5.46 -12 25 -2 17.72 11.53 -12 25 -2 15.43 5.78 -12 25 -3 22.05 12.41 -12 25 -3 24.09 7.29 -12 25 -4 14.54 10.52 -12 25 -4 23.08 7.59 -12 25 -5 18.60 13.94 -12 25 -5 9.15 5.28 -12 25 -6 116.13 22.59 -12 25 -6 119.29 15.79 -12 25 -7 46.53 15.32 -12 25 -7 38.83 9.61 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151.21 14.97 12 -26 1 156.82 18.37 -12 26 -2 -6.74 5.54 -12 26 -2 -7.85 7.01 -12 26 -3 25.24 7.51 -12 26 -3 32.16 13.57 -12 26 -4 -6.90 6.72 -12 26 -4 4.97 11.19 -12 26 -5 143.22 17.03 -12 26 -5 130.49 24.36 -12 26 -6 86.39 13.49 -12 26 -6 94.68 22.51 -12 26 -7 -1.33 6.00 -12 26 -7 -11.83 15.02 -12 26 -8 23.11 8.70 -12 26 -8 67.73 21.96 -12 26 -9 242.34 23.20 -12 26 -9 285.89 37.10 -12 26 -10 15.89 6.28 -12 26 -10 14.56 12.93 -12 27 13 123.78 13.66 -12 27 12 60.98 9.78 12 -27 -12 81.78 12.77 -12 27 11 26.37 6.64 12 -27 -11 37.44 9.36 -12 27 10 109.78 12.16 12 -27 -10 106.06 13.19 12 -27 -9 21.70 7.19 -12 27 9 24.89 8.21 -12 27 9 12.94 6.02 -12 27 9 14.39 5.14 12 -27 -8 312.37 22.39 -12 27 8 336.11 21.91 -12 27 8 382.18 26.41 -12 27 8 362.07 27.03 -12 27 7 164.92 16.53 -12 27 7 168.90 18.88 12 -27 -7 139.26 14.69 -12 27 6 26.92 7.15 -12 27 6 32.47 9.17 12 -27 -6 32.19 7.99 12 -27 -5 465.12 28.15 -12 27 5 523.39 29.37 -12 27 5 511.46 35.08 12 -27 -4 20.34 6.89 -12 27 4 13.11 4.77 -12 27 4 19.04 9.61 12 -27 -3 60.78 11.18 -12 27 3 50.37 8.70 -12 27 3 70.57 14.80 12 -27 -2 559.64 33.92 -12 27 2 561.05 30.08 12 -27 -1 3.23 6.11 -12 27 1 11.44 7.38 -12 27 1 13.95 5.36 12 -27 0 16.93 6.84 -12 27 0 12.45 4.72 12 -27 1 -10.85 8.65 -12 27 -1 4.44 4.51 -12 27 -1 -1.51 11.27 -12 27 -2 104.57 12.39 -12 27 -2 119.30 22.26 -12 27 -3 4.28 5.22 -12 27 -3 4.79 9.56 -12 27 -4 38.28 9.27 -12 27 -4 37.06 16.21 -12 27 -5 11.31 6.51 -12 27 -5 5.52 10.91 -12 27 -6 47.85 9.33 -12 27 -6 73.01 21.11 -12 27 -7 -0.75 6.25 -12 27 -7 29.72 17.30 -12 27 -8 429.05 49.14 -12 27 -8 403.58 29.90 -12 27 -9 85.64 24.49 -12 27 -9 56.68 13.13 -12 28 13 170.40 15.58 -12 28 12 40.95 7.94 -12 28 11 88.12 11.12 12 -28 -11 76.46 12.03 -12 28 10 -1.39 4.78 12 -28 -10 -3.58 4.55 12 -28 -9 39.18 8.32 -12 28 9 47.57 10.93 -12 28 8 46.55 10.28 -12 28 8 60.27 10.95 12 -28 -8 32.03 7.52 -12 28 7 14.93 6.55 -12 28 7 1.16 4.73 12 -28 -7 19.41 6.25 -12 28 6 166.91 19.64 12 -28 -6 152.30 15.94 -12 28 6 160.38 16.31 12 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4.38 7.25 -12 29 5 126.85 14.57 -12 29 5 160.15 21.00 12 -29 -5 122.51 14.39 -12 29 4 11.25 5.43 -12 29 4 16.36 8.38 12 -29 -4 19.08 6.66 -12 29 3 169.16 15.69 -12 29 3 187.67 23.55 12 -29 -3 162.42 17.22 -12 29 2 121.02 13.30 -12 29 2 135.91 20.73 12 -29 -2 111.90 14.61 12 -29 -1 7.94 6.62 -12 29 1 20.69 10.00 -12 29 1 8.34 4.20 12 -29 0 36.45 9.39 -12 29 0 37.78 15.19 -12 29 0 34.61 8.17 12 -29 1 0.71 5.97 -12 29 -1 8.51 5.38 -12 29 -2 135.55 14.98 -12 29 -2 175.61 31.45 -12 29 -3 8.57 5.13 -12 29 -3 50.47 21.44 -12 29 -4 116.05 15.63 -12 29 -4 162.90 33.33 -12 29 -5 -3.56 6.30 -12 29 -5 -9.28 13.61 -12 29 -6 88.35 13.98 -12 29 -6 116.17 29.33 -12 29 -7 60.60 12.41 -12 29 -7 92.92 24.19 -12 29 -8 165.13 19.32 -12 29 -8 218.00 42.90 12 -30 -10 81.31 12.36 -12 30 10 90.22 14.24 12 -30 -9 0.97 4.75 -12 30 9 6.48 5.78 12 -30 -8 69.49 10.77 -12 30 8 69.79 12.69 12 -30 -7 2.40 3.91 -12 30 7 4.28 5.79 12 -30 -6 74.59 11.33 -12 30 6 89.90 16.54 12 -30 -5 26.98 7.76 -12 30 5 38.58 11.21 -12 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8.32 5.23 -13 15 5 3.62 4.15 13 -15 -4 534.54 33.21 -13 15 4 469.60 25.26 -13 15 4 475.88 24.61 13 -15 -3 3.82 5.88 -13 15 3 -1.08 3.72 -13 15 3 12.76 5.03 -13 15 3 1.28 3.68 13 -15 -2 180.85 20.59 -13 15 2 191.51 15.87 -13 15 2 176.31 14.78 13 -15 -1 63.67 12.93 -13 15 1 56.85 8.60 -13 15 1 60.84 9.17 -13 15 0 791.62 34.42 -13 15 0 743.54 35.57 13 -15 1 13.48 8.39 -13 15 -1 8.42 4.21 -13 15 -1 14.31 5.69 -13 15 -2 921.81 43.39 -13 15 -2 962.60 40.99 -13 15 -3 20.80 6.35 -13 15 -3 26.89 8.20 -13 15 -4 155.66 15.54 -13 15 -4 125.38 15.39 -13 15 -5 7.56 5.01 -13 15 -5 14.19 7.50 -13 15 -6 32.07 8.18 -13 15 -6 37.63 9.66 -13 15 -7 0.69 5.23 -13 15 -7 12.21 8.50 -13 15 -8 0.74 5.27 -13 15 -8 1.98 5.60 -13 15 -9 39.03 9.37 -13 15 -9 25.76 9.03 -13 15 -10 24.25 8.04 -13 15 -10 24.04 9.44 -13 15 -11 11.91 5.78 -13 15 -11 20.32 11.30 -13 15 -12 98.97 14.70 -13 15 -12 105.36 17.75 -13 15 -13 46.46 15.56 13 -16 -17 6.47 5.50 -13 16 16 8.86 6.72 13 -16 -16 2.48 6.45 -13 16 15 12.62 5.92 13 -16 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102.50 12.61 -13 23 7 147.15 15.87 -13 23 7 109.74 13.36 -13 23 7 123.93 14.40 13 -23 -6 238.32 19.18 -13 23 6 235.55 20.76 -13 23 6 233.12 19.33 -13 23 6 228.99 20.02 13 -23 -5 -0.37 4.91 -13 23 5 -0.31 5.46 -13 23 5 6.07 4.18 -13 23 5 -4.12 5.73 13 -23 -4 299.43 23.36 -13 23 4 350.92 26.18 -13 23 4 270.13 20.20 -13 23 4 319.79 24.69 -13 23 3 68.52 9.93 13 -23 -3 57.77 11.43 -13 23 3 64.74 11.24 -13 23 2 119.59 13.37 13 -23 -2 130.64 16.29 -13 23 2 112.77 15.15 13 -23 -1 108.55 15.38 -13 23 1 110.52 16.38 -13 23 1 97.76 11.80 13 -23 0 107.31 16.29 -13 23 0 88.34 14.78 -13 23 0 107.43 12.73 13 -23 1 71.36 14.14 -13 23 -1 65.47 10.24 -13 23 -1 68.75 12.72 -13 23 -2 45.73 9.37 -13 23 -2 53.28 12.39 -13 23 -3 142.28 15.60 -13 23 -3 134.24 18.92 -13 23 -4 6.15 5.52 -13 23 -4 5.53 9.46 -13 23 -5 148.47 17.28 -13 23 -5 137.25 21.90 -13 23 -6 6.71 4.95 -13 23 -6 16.25 12.45 -13 23 -7 206.08 26.90 -13 23 -7 202.25 20.90 -13 23 -8 213.58 28.13 -13 23 -8 182.06 19.75 -13 23 -9 107.01 21.18 -13 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35.54 9.36 -18 15 2 20.84 7.47 -18 15 1 51.62 10.21 -18 15 1 48.72 11.11 -18 15 0 173.12 19.04 -18 15 0 154.17 18.58 -18 15 -1 222.30 21.53 -18 15 -1 236.35 23.28 -18 15 -2 -1.35 7.23 -18 15 -2 2.03 5.32 -18 15 -3 215.36 21.38 -18 15 -3 177.34 20.90 -18 15 -4 106.62 17.26 -18 15 -4 84.03 14.19 -18 15 -5 46.07 11.68 -18 16 9 55.68 14.36 -18 16 8 225.92 22.14 -18 16 8 226.46 27.96 -18 16 7 8.66 6.27 -18 16 6 66.87 12.06 18 -16 -5 1.72 5.95 -18 16 5 -3.60 6.39 18 -16 -4 19.34 11.11 -18 16 4 28.05 8.01 18 -16 -3 -15.85 11.78 -18 16 3 2.63 5.90 -18 16 2 26.92 8.86 -18 16 1 68.05 13.18 -18 16 1 54.08 11.05 -18 16 0 17.38 8.90 -18 16 0 0.38 4.88 -18 16 -1 4.58 6.36 -18 16 -1 6.18 6.39 -18 16 -2 233.96 24.24 -18 16 -2 214.49 21.03 -18 16 -3 43.09 13.32 -18 16 -3 21.69 8.66 -18 16 -4 2.69 8.01 -18 16 -4 -2.75 5.73 -18 16 -5 33.89 9.49 18 -17 -9 242.53 23.30 18 -17 -8 13.62 7.49 -18 17 8 9.82 8.36 18 -17 -7 -0.57 6.42 -18 17 7 8.56 6.81 18 -17 -6 45.15 12.47 -18 17 6 48.55 10.69 18 -17 -5 60.82 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5 230.63 21.61 18 -19 -5 211.90 27.64 -18 19 4 40.50 9.38 18 -19 -4 43.45 15.70 -18 19 3 47.61 10.14 18 -19 -3 55.91 17.69 -18 19 2 6.27 6.82 18 -19 -2 0.36 6.89 -18 19 1 5.22 5.52 -18 19 1 10.45 7.70 -18 19 0 129.54 17.03 -18 19 0 131.46 18.19 -18 19 -1 312.65 25.60 -18 19 -1 289.16 26.36 -18 19 -2 27.41 12.12 -18 19 -3 159.01 21.16 18 -20 -8 15.90 6.63 18 -20 -7 22.23 7.82 18 -20 -6 148.67 22.04 18 -20 -5 55.45 14.65 -18 20 4 130.95 16.15 18 -20 -4 121.55 21.81 -18 20 3 126.47 16.04 18 -20 -3 111.04 23.00 -18 20 2 39.54 9.14 18 -20 -2 17.46 6.97 -18 20 1 152.19 19.57 -18 20 0 142.97 19.28 -18 20 -1 35.99 12.32 -18 20 -2 80.27 15.70 18 -21 -6 8.38 8.02 18 -21 -5 179.88 24.14 18 -21 -4 55.57 16.54 18 -21 -3 32.93 14.22 18 -21 -2 43.22 15.94 -18 21 2 37.01 10.67 -18 21 1 -3.78 6.61 -18 21 0 132.42 19.22 -18 21 -1 0.52 6.42 18 -22 -4 74.28 17.19 18 -22 -3 76.10 17.34 18 -22 -2 -8.59 9.98 -18 22 2 -1.47 7.43 -18 22 1 118.10 17.01 -18 22 0 5.54 6.96 -18 23 2 88.44 15.07 -19 0 10 -3.65 7.49 -19 0 9 6.51 5.89 -19 0 8 1.99 5.48 -19 0 7 36.39 9.18 -19 0 6 2.80 5.06 -19 0 5 38.25 8.14 -19 0 4 -1.51 5.32 -19 0 3 62.61 10.78 -19 0 2 1.01 4.57 -19 0 1 443.33 28.59 -19 0 0 0.78 6.15 -19 0 -1 200.67 18.83 -19 0 -2 -0.60 5.34 -19 0 -3 70.74 11.03 -19 0 -4 -6.26 6.05 -19 0 -4 7.27 6.07 -19 0 -5 19.53 8.85 -19 0 -5 20.72 7.56 -19 0 -6 1.61 9.49 -19 0 -7 444.45 34.05 -19 1 10 158.75 19.32 -19 1 9 101.68 14.85 -19 -1 9 76.70 13.39 -19 1 8 13.88 6.99 -19 -1 8 16.11 7.61 -19 -1 7 14.12 6.72 -19 1 7 20.70 7.20 -19 -1 6 121.44 15.20 -19 1 6 115.62 15.30 -19 1 5 25.17 7.95 -19 -1 5 15.42 6.36 -19 -1 4 163.89 17.68 -19 1 4 153.21 16.70 -19 -1 3 31.07 8.30 -19 1 3 22.42 7.31 -19 -1 2 -5.71 5.64 -19 1 2 8.89 6.00 -19 -1 1 34.82 8.58 -19 1 1 20.02 6.55 -19 -1 0 545.66 31.79 -19 1 0 571.24 32.51 -19 -1 -1 2.22 5.68 -19 1 -1 10.71 6.49 -19 -1 -2 49.27 9.79 -19 1 -2 49.95 9.72 -19 1 -3 3.93 6.85 -19 -1 -3 -0.64 5.76 -19 1 -3 3.97 5.29 -19 -1 -4 17.36 6.41 -19 1 -4 35.45 9.82 -19 1 -4 21.81 7.68 -19 -1 -4 27.24 7.48 -19 -1 -5 26.12 8.94 -19 1 -5 31.73 9.48 -19 1 -5 28.56 7.36 -19 -1 -6 308.83 26.63 -19 1 -6 331.40 28.60 -19 1 -6 351.49 24.89 -19 -1 -7 34.05 11.70 -19 1 -7 36.87 11.74 -19 2 10 72.07 12.06 -19 2 9 24.99 9.29 -19 -2 9 8.15 5.80 -19 -2 8 152.78 17.79 -19 2 8 171.51 18.60 -19 -2 7 18.02 6.01 -19 2 7 12.75 6.67 -19 -2 6 6.50 6.58 -19 2 6 3.08 5.70 -19 2 5 16.22 6.35 -19 -2 5 23.48 7.15 -19 -2 4 16.35 6.70 -19 2 4 11.60 5.59 -19 -2 3 74.99 11.34 -19 2 3 73.59 11.53 -19 -2 2 136.18 15.39 -19 2 2 130.97 15.29 -19 -2 1 2.05 4.59 -19 2 1 5.11 4.77 -19 2 0 8.10 4.81 -19 -2 0 15.75 6.61 -19 2 -1 146.92 15.88 -19 -2 -1 130.43 14.63 -19 -2 -2 177.65 17.51 -19 2 -2 185.06 17.70 -19 2 -3 5.02 5.35 -19 -2 -3 -6.24 5.68 -19 -2 -4 127.29 15.96 -19 2 -4 133.36 16.86 -19 2 -4 125.80 14.65 -19 -2 -5 9.30 6.76 -19 2 -5 16.95 8.70 -19 2 -5 20.81 8.03 -19 -2 -6 187.85 21.18 -19 2 -6 177.90 22.23 -19 2 -6 162.88 17.36 -19 -2 -7 273.90 26.50 -19 2 -7 294.70 27.68 -19 2 -7 258.91 21.64 -19 3 10 224.01 22.08 -19 3 9 225.98 22.14 -19 -3 8 -0.84 5.65 -19 3 8 -6.60 5.91 -19 -3 7 83.89 13.06 -19 3 7 76.83 12.95 -19 -3 6 24.71 8.37 -19 3 6 13.08 6.31 -19 3 5 58.36 10.58 -19 -3 5 68.69 11.87 -19 -3 4 165.73 17.16 -19 3 4 175.46 18.39 -19 -3 3 52.39 9.83 -19 3 3 68.99 11.46 -19 -3 2 5.08 4.38 -19 3 2 2.28 4.97 -19 3 1 38.11 9.22 -19 -3 1 40.71 9.19 -19 3 0 6.53 5.64 -19 -3 0 10.70 5.85 -19 3 -1 44.59 9.47 -19 -3 -1 36.87 8.36 -19 -3 -2 8.13 6.02 -19 3 -2 4.81 5.32 -19 3 -3 29.32 8.06 -19 3 -3 21.00 6.13 -19 -3 -4 0.03 5.79 -19 3 -4 -6.64 5.95 -19 3 -4 -8.95 5.26 -19 3 -5 113.96 16.12 -19 -3 -5 112.19 16.48 -19 3 -5 101.15 13.30 -19 3 -6 145.29 16.39 -19 3 -6 199.31 22.36 -19 -3 -6 155.94 19.16 -19 3 -7 36.40 8.23 -19 3 -7 39.86 10.87 -19 -3 -7 42.93 11.51 -19 4 10 178.63 20.24 -19 4 9 207.58 21.05 -19 4 8 165.37 18.72 -19 -4 8 120.70 16.28 -19 -4 7 17.07 6.75 -19 4 7 33.71 9.29 -19 -4 6 82.53 13.04 -19 4 6 85.61 14.04 -19 -4 5 70.48 12.30 -19 4 5 59.81 11.49 -19 4 4 10.24 6.14 -19 -4 4 -2.48 4.72 -19 -4 3 25.25 7.70 -19 4 3 22.52 8.37 -19 -4 2 136.62 15.28 -19 4 2 121.59 15.08 -19 4 1 -4.58 5.13 -19 -4 1 12.09 6.17 -19 4 0 -0.20 4.95 -19 -4 0 4.88 4.41 -19 -4 -1 10.30 4.31 -19 4 -1 16.37 5.08 -19 4 -2 176.19 17.47 -19 4 -3 13.93 7.82 -19 4 -3 4.87 4.75 -19 4 -4 108.35 16.33 -19 4 -4 94.74 13.30 -19 4 -5 17.83 9.71 -19 -4 -5 8.92 7.99 -19 4 -5 11.55 6.00 -19 4 -6 125.35 14.85 -19 -4 -6 127.70 16.60 -19 4 -6 108.76 16.71 -19 4 -7 78.86 12.44 -19 -4 -7 78.34 14.65 -19 5 10 36.40 10.61 -19 5 9 214.37 21.57 -19 -5 8 6.15 6.13 -19 5 8 -2.49 6.77 -19 -5 7 15.43 6.43 -19 5 7 4.73 4.60 -19 -5 6 4.43 5.32 -19 5 6 8.18 5.17 -19 -5 5 34.02 8.19 -19 5 5 26.49 7.91 -19 5 4 10.01 7.48 -19 -5 4 -0.38 5.40 -19 5 3 17.66 5.78 -19 -5 3 8.44 4.62 -19 -5 2 7.18 4.47 -19 5 2 5.20 4.94 -19 5 1 21.05 6.66 -19 -5 1 29.13 8.02 -19 -5 0 8.74 5.10 -19 5 0 7.54 5.79 -19 5 -1 192.40 18.52 -19 5 -2 23.60 9.53 -19 5 -2 15.20 6.17 -19 5 -3 255.01 23.45 -19 5 -3 244.46 21.26 -19 5 -4 37.66 10.65 -19 5 -4 39.23 9.26 -19 5 -5 79.00 12.74 -19 5 -5 98.69 15.76 -19 -5 -5 84.29 13.55 -19 5 -6 0.40 5.08 -19 5 -6 -0.65 8.02 -19 -5 -6 5.42 6.54 -19 5 -7 -4.61 5.83 -19 -5 -7 0.13 6.85 -19 6 9 6.05 7.22 -19 6 8 127.75 17.12 -19 -6 7 16.84 7.93 -19 6 7 17.00 7.46 -19 -6 6 6.56 4.66 -19 6 6 17.48 6.34 -19 -6 5 302.65 23.19 -19 6 5 284.71 23.54 -19 -6 4 19.57 7.09 -19 6 4 22.62 7.09 -19 6 3 10.68 8.16 -19 -6 3 4.22 4.52 -19 6 2 62.45 10.90 -19 -6 2 56.18 9.91 -19 -6 1 8.37 6.19 -19 6 1 -5.22 6.49 -19 6 0 37.77 9.05 -19 6 -1 104.49 13.77 -19 6 -2 237.32 21.84 -19 6 -2 213.35 19.52 -19 6 -3 17.17 8.38 -19 6 -3 28.05 6.72 -19 6 -4 35.16 9.29 -19 6 -4 37.26 9.27 -19 6 -5 -2.73 6.33 -19 6 -5 -10.26 6.65 -19 -6 -5 11.53 7.23 -19 6 -6 0.76 5.83 -19 -6 -6 5.62 7.50 -19 6 -6 1.16 7.24 -19 -6 -7 9.90 8.06 -19 7 9 319.09 26.78 -19 7 8 34.08 9.47 -19 -7 7 187.02 19.38 -19 7 7 226.56 21.45 -19 -7 6 214.74 20.06 -19 7 6 221.13 21.04 -19 -7 5 75.24 11.48 -19 7 5 53.79 10.85 -19 -7 4 5.17 5.94 -19 7 4 -3.12 5.23 -19 -7 3 208.96 18.87 -19 7 3 222.94 20.74 -19 7 2 21.08 7.04 -19 -7 2 29.06 7.74 -19 7 1 63.52 11.27 -19 7 0 33.39 9.02 -19 7 -1 8.31 6.79 -19 7 -2 296.95 25.31 -19 7 -2 280.20 23.03 -19 7 -3 73.54 13.42 -19 7 -3 91.51 12.98 -19 7 -4 13.95 8.88 -19 7 -4 9.45 5.18 -19 7 -5 82.07 14.60 -19 7 -5 78.71 12.73 -19 7 -6 80.57 15.89 -19 7 -6 74.00 12.65 -19 8 9 47.83 11.97 -19 8 8 182.98 19.90 -19 8 7 163.38 18.78 -19 -8 6 -4.21 4.73 -19 8 6 15.74 8.16 -19 -8 5 87.47 12.49 -19 8 5 84.18 13.41 -19 -8 4 127.47 14.77 -19 8 4 127.32 16.11 -19 -8 3 35.31 8.48 -19 8 3 41.61 9.62 -19 8 2 333.42 25.19 -19 8 1 -4.43 6.58 -19 8 0 42.11 9.86 -19 8 -1 84.50 12.60 -19 8 -2 145.51 18.30 -19 8 -2 135.19 16.19 -19 8 -3 11.58 6.83 -19 8 -3 18.79 6.72 -19 8 -4 170.24 20.22 -19 8 -4 168.07 17.91 -19 8 -5 12.93 7.86 -19 8 -5 7.11 7.34 -19 8 -6 48.75 11.96 -19 9 8 45.09 11.03 -19 9 7 94.65 15.17 -19 9 6 7.91 5.56 -19 -9 5 6.74 4.63 -19 9 5 3.81 6.34 -19 -9 4 12.99 5.43 -19 9 4 21.78 7.57 -19 9 3 297.23 24.38 -19 9 2 6.48 5.57 -19 9 1 305.37 24.64 -19 9 0 83.42 12.05 -19 9 -1 6.11 5.81 -19 9 -2 130.82 17.54 -19 9 -2 109.52 15.13 -19 9 -3 171.95 20.12 -19 9 -3 172.03 18.15 -19 9 -4 51.77 13.00 -19 9 -4 43.01 9.73 -19 9 -5 21.79 9.67 -19 9 -5 41.76 10.18 -19 10 8 142.07 16.89 -19 10 7 17.75 8.80 -19 10 6 7.70 6.36 -19 -10 5 21.69 7.77 -19 10 5 22.77 7.23 -19 10 4 539.20 34.42 -19 10 3 5.68 6.66 -19 10 2 557.13 34.35 -19 10 1 28.44 7.99 -19 10 0 268.38 22.89 -19 10 -1 -2.59 5.85 -19 10 -1 9.97 5.65 -19 10 -2 4.81 6.86 -19 10 -2 19.69 8.73 -19 10 -3 5.61 6.87 -19 10 -3 7.90 6.96 -19 10 -4 304.97 27.53 -19 10 -4 333.40 25.91 -19 10 -5 12.46 8.09 -19 11 7 108.35 15.99 -19 11 6 85.18 13.88 -19 11 5 251.54 22.68 -19 11 4 66.72 12.20 -19 11 3 317.80 25.15 -19 11 2 43.68 10.25 -19 11 1 151.52 17.63 -19 11 0 179.00 18.91 -19 11 -1 19.17 9.41 -19 11 -1 1.81 7.03 -19 11 -2 100.83 16.09 -19 11 -2 99.49 15.13 -19 11 -3 204.79 22.31 -19 11 -3 209.18 20.91 -19 11 -4 30.48 11.07 -19 11 -4 21.97 6.43 -19 11 -5 28.52 9.86 -19 12 7 139.62 17.71 -19 12 6 54.85 12.14 -19 12 5 138.61 16.84 -19 12 4 312.77 25.42 -19 12 3 37.78 9.48 -19 12 2 37.63 9.69 -19 12 1 89.72 13.31 -19 12 0 101.66 14.47 -19 12 -1 243.74 23.70 -19 12 -1 237.91 21.65 -19 12 -2 26.13 11.30 -19 12 -2 7.94 5.97 -19 12 -3 23.94 10.05 -19 12 -3 34.59 10.12 -19 12 -4 90.59 15.32 -19 13 6 86.38 14.03 -19 13 5 32.66 10.37 -19 13 4 204.32 20.53 -19 13 3 131.78 16.28 -19 13 2 6.99 5.36 -19 13 1 21.32 6.84 -19 13 0 15.47 8.14 -19 13 -1 8.38 9.18 -19 13 -1 7.49 4.94 -19 13 -2 287.02 26.05 -19 13 -2 260.38 23.22 -19 13 -3 121.13 17.97 -19 13 -4 27.52 11.26 -19 14 5 337.57 27.00 -19 14 4 2.44 5.63 -19 14 3 8.22 5.85 -19 14 2 -4.47 7.32 -19 14 1 23.23 9.31 -19 14 0 11.19 7.75 -19 14 -1 80.55 14.16 -19 14 -1 102.87 15.01 -19 14 -2 8.44 9.08 -19 14 -3 33.81 12.46 -19 15 4 60.55 11.76 -19 15 3 19.12 7.23 -19 15 2 37.09 8.98 -19 15 1 -4.28 6.80 -19 15 -1 6.53 6.52 -19 15 -2 230.07 24.10 -19 15 -3 77.96 14.26 -19 16 0 2.90 6.66 -19 16 -1 44.79 10.51 -19 16 -2 10.82 8.26 -19 17 0 32.37 10.20 -19 17 -1 20.16 7.60 -19 18 0 20.92 7.90 -19 18 -1 229.13 24.36 -19 19 0 195.31 21.71 -20 0 7 12.19 7.16 -20 0 6 73.10 13.13 -20 0 5 2.47 5.71 -20 0 4 16.37 7.01 -20 0 3 12.25 7.40 -20 0 2 47.12 10.34 -20 0 1 8.12 6.76 -20 0 0 873.83 44.02 -20 0 -1 -6.11 6.81 -20 0 -2 27.28 8.16 -20 0 -3 3.67 5.40 -20 0 -5 -8.25 8.84 -20 -1 8 3.35 5.51 -20 -1 7 193.59 20.17 -20 1 7 200.97 20.60 -20 -1 6 8.49 6.42 -20 1 6 28.68 9.66 -20 1 5 104.43 14.80 -20 -1 5 120.67 15.79 -20 -1 4 4.33 5.69 -20 1 4 5.43 5.45 -20 -1 3 49.67 10.42 -20 1 3 44.56 9.89 -20 -1 2 11.41 5.38 -20 1 2 19.30 8.99 -20 -1 1 506.76 31.43 -20 1 1 438.31 29.95 -20 -1 0 -4.20 5.32 -20 1 0 12.96 7.29 -20 -1 -1 354.69 25.58 -20 1 -1 339.75 25.51 -20 -1 -2 79.36 12.49 -20 1 -2 57.47 10.56 -20 -1 -3 7.78 5.12 -20 1 -3 3.71 5.44 -20 1 -4 -2.75 4.69 -20 1 -5 56.75 12.83 -20 -2 8 38.94 10.76 -20 2 7 -1.87 6.52 -20 -2 7 2.19 5.15 -20 -2 6 63.56 11.97 -20 2 6 63.92 12.06 -20 2 5 64.73 12.57 -20 -2 5 83.65 12.66 -20 2 4 -9.93 7.24 -20 -2 4 2.46 4.95 -20 -2 3 147.91 16.81 -20 2 3 113.44 15.19 -20 -2 2 33.67 9.33 -20 2 2 39.13 9.18 -20 -2 1 21.61 7.12 -20 2 1 30.43 8.91 -20 -2 0 384.92 26.91 -20 2 0 402.64 28.41 -20 2 -1 107.55 14.53 -20 -2 -1 127.16 15.05 -20 2 -2 12.88 6.49 -20 -2 -2 8.91 6.31 -20 2 -3 72.37 12.11 -20 2 -4 22.47 8.44 -20 2 -5 115.89 17.57 -20 2 -5 116.39 15.38 -20 -3 8 12.27 7.25 -20 -3 7 9.33 6.16 -20 3 7 6.79 6.15 -20 -3 6 49.38 10.72 -20 3 6 65.28 12.37 -20 -3 5 5.87 6.05 -20 3 5 9.66 7.35 -20 3 4 11.21 5.84 -20 -3 4 14.07 6.69 -20 -3 3 2.39 4.88 -20 3 3 -10.92 7.89 -20 -3 2 69.20 11.47 -20 3 2 65.75 11.95 -20 -3 1 157.14 16.84 -20 3 1 156.53 17.47 -20 3 0 11.00 6.68 -20 -3 0 19.65 6.26 -20 3 -1 79.38 12.89 -20 -3 -1 63.44 10.97 -20 3 -2 222.77 20.28 -20 3 -3 62.70 11.10 -20 3 -4 -3.48 5.90 -20 -4 8 -8.64 7.50 -20 -4 7 39.28 10.29 -20 -4 6 99.91 13.86 -20 4 6 75.91 12.67 -20 -4 5 41.14 11.17 -20 4 5 15.92 8.07 -20 4 4 29.55 8.65 -20 -4 4 38.57 9.83 -20 4 3 -1.70 7.04 -20 -4 3 -2.05 6.62 -20 -4 2 4.13 5.93 -20 4 2 3.35 5.73 -20 -4 1 10.13 5.19 -20 4 1 6.02 5.46 -20 4 0 30.13 8.99 -20 -4 0 26.48 7.92 -20 4 -1 220.79 21.16 -20 4 -2 9.23 5.14 -20 4 -3 58.41 11.05 -20 4 -4 130.05 17.57 -20 4 -4 133.97 16.02 -20 -5 7 4.10 5.54 -20 -5 6 -5.16 6.24 -20 5 6 4.25 5.25 -20 -5 5 106.53 14.72 -20 5 5 89.13 14.01 -20 -5 4 48.78 10.65 -20 5 4 51.89 11.31 -20 5 3 12.12 5.91 -20 -5 3 18.15 7.61 -20 -5 2 20.63 7.68 -20 5 2 10.06 6.39 -20 -5 1 -0.16 5.56 -20 5 1 3.91 5.36 -20 5 0 32.40 8.78 -20 5 -1 21.71 10.18 -20 5 -2 140.24 16.53 -20 5 -3 2.40 6.37 -20 5 -4 -0.03 6.02 -20 -6 7 28.51 9.12 -20 -6 6 154.07 17.24 -20 6 6 151.70 17.87 -20 -6 5 1.55 5.22 -20 6 5 15.13 8.41 -20 -6 4 53.46 10.56 -20 6 4 53.31 11.38 -20 -6 3 7.83 6.22 -20 6 3 8.21 5.06 -20 6 2 -0.51 5.79 -20 -6 2 3.38 5.53 -20 6 1 24.09 7.95 -20 6 0 5.58 5.54 -20 6 -1 224.70 21.53 -20 6 -2 128.47 16.62 -20 6 -4 45.89 13.25 -20 -7 6 2.83 5.23 -20 7 5 283.96 24.77 -20 -7 5 259.86 21.96 -20 7 4 124.29 16.76 -20 -7 4 110.29 14.58 -20 7 3 -8.04 6.12 -20 -7 3 6.46 4.52 -20 7 2 27.17 8.35 -20 7 1 -3.10 6.53 -20 7 0 28.05 8.42 -20 7 -1 65.18 12.72 -20 7 -2 262.01 22.95 -20 7 -4 32.22 10.90 -20 -8 6 47.90 9.95 -20 -8 5 107.61 14.42 -20 8 4 155.22 18.61 -20 8 3 168.36 18.85 -20 8 2 -2.66 5.97 -20 8 1 97.89 14.07 -20 8 0 3.06 5.65 -20 8 -1 51.05 11.71 -20 8 -3 108.63 17.27 -20 9 3 93.51 14.54 -20 9 2 219.72 21.99 -20 9 1 22.94 8.30 -20 9 -3 5.15 7.89 -20 10 -3 166.11 20.58 -21 -1 1 69.24 12.42 -21 -1 0 234.37 22.09 -21 -2 2 -6.33 6.78 -21 -2 1 193.92 19.92 -21 -2 0 6.98 6.91 -21 -3 3 24.45 8.26 -21 -3 2 25.48 9.27 -21 -3 1 130.25 16.73 -21 -4 3 32.87 8.91 -21 -4 2 28.67 7.92 -21 -5 3 7.41 8.48 0 0 0 0.00 0.00 TITL LD448_abs in P2/n REM P2/n (#13 in standard setting) CELL 0.71073 13.302777 27.670849 14.678927 90.0000 96.2345 90.0000 ZERR 2.00 0.000205 0.000415 0.000303 0.0000 0.0017 0.0000 LATT 1 SYMM -x+1/2, y,-z+1/2 SFAC C H O F Al Cl As Mo Bi UNIT 124.00 48.00 32.00 96.00 4.00 56.00 4.00 8.00 4.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 95195 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Bi1 Bi 0.07530(2) 0.52956(2) 1.08436(2) 0.01338(3) Uani 0.965 1 d . . P A 1 Mo2 Mo 0.02143(2) 0.62966(2) 1.05268(2) 0.01223(5) Uani 1 1 d . . . . . Mo1 Mo 0.07409(2) 0.43636(2) 0.80203(2) 0.01207(5) Uani 1 1 d . . . . . As1 As 0.11724(2) 0.43129(2) 0.97747(2) 0.01372(6) Uani 1 1 d . . . . . Cl1 Cl 0.90516(5) 0.59515(3) 0.57617(6) 0.02173(15) Uani 1 1 d . . . . . Cl2 Cl 0.81326(5) 0.57692(3) 0.74140(5) 0.01902(14) Uani 1 1 d . . . . . Cl3 Cl 0.86169(5) 0.67373(3) 0.69230(6) 0.02029(14) Uani 1 1 d . . . . . Cl4 Cl 0.50383(7) 0.73434(3) 1.01620(6) 0.02527(16) Uani 1 1 d . . . . . Cl5 Cl 0.39226(6) 0.65209(3) 0.94208(6) 0.02225(15) Uani 1 1 d . . . . . Cl6 Cl 0.37604(6) 0.74162(3) 0.84538(6) 0.02514(16) Uani 1 1 d . . . . . Cl7 Cl 0.68154(5) 0.51760(3) 0.90049(5) 0.01786(13) Uani 1 1 d . . . . . Cl8 Cl 0.67855(6) 0.46156(3) 0.73652(6) 0.02084(15) Uani 1 1 d . . . . . Cl9 Cl 0.56586(6) 0.42981(2) 0.88117(5) 0.01867(13) Uani 1 1 d . . . . . Cl10 Cl 0.18727(5) 0.56550(3) 0.58917(7) 0.02365(16) Uani 1 1 d . . . . . Cl11 Cl 0.13864(5) 0.66443(3) 0.54822(6) 0.02065(14) Uani 1 1 d . . . . . Cl12 Cl 0.23569(6) 0.63802(3) 0.72570(6) 0.02261(15) Uani 1 1 d . . . . . Cl13 Cl 0.40635(10) 0.70775(5) 0.25461(11) 0.0575(4) Uani 1 1 d . . . . . Cl14 Cl 0.61672(11) 0.73447(6) 0.25475(11) 0.0632(4) Uani 1 1 d . . . . . Al1 Al 0.52684(6) 0.61348(3) 0.70504(6) 0.00823(14) Uani 1 1 d . . . . . F1 F 0.77894(14) 0.67306(8) 0.48435(14) 0.0239(4) Uani 1 1 d . . . . . F2 F 0.68583(14) 0.70840(7) 0.57513(14) 0.0213(4) Uani 1 1 d . . . . . F3 F 0.61701(14) 0.66351(8) 0.46720(14) 0.0236(4) Uani 1 1 d . . . . . F4 F 0.71176(15) 0.57946(8) 0.45331(14) 0.0246(4) Uani 1 1 d . . . . . F5 F 0.57658(13) 0.57234(7) 0.52071(14) 0.0208(4) Uani 1 1 d . . . . . F6 F 0.71251(15) 0.53605(7) 0.57500(15) 0.0226(4) Uani 1 1 d . . . . . F7 F 0.60486(17) 0.77142(7) 0.86154(15) 0.0274(5) Uani 1 1 d . . . . . F8 F 0.54496(16) 0.74290(7) 0.73038(14) 0.0258(4) Uani 1 1 d . . . . . F9 F 0.69173(15) 0.72159(8) 0.79014(16) 0.0284(5) Uani 1 1 d . . . . . F10 F 0.69926(15) 0.69467(8) 0.96779(16) 0.0303(5) Uani 1 1 d . . . . . F11 F 0.69632(15) 0.63645(8) 0.87113(16) 0.0266(4) Uani 1 1 d . . . . . F12 F 0.60434(16) 0.63277(8) 0.98146(15) 0.0288(5) Uani 1 1 d . . . . . F13 F 0.47666(16) 0.53452(7) 0.92734(14) 0.0241(4) Uani 1 1 d . . . . . F14 F 0.37326(13) 0.55961(6) 0.81527(15) 0.0206(4) Uani 1 1 d . . . . . F15 F 0.37261(15) 0.48455(7) 0.85474(17) 0.0273(5) Uani 1 1 d . . . . . F16 F 0.44993(16) 0.43823(7) 0.70154(15) 0.0240(4) Uani 1 1 d . . . . . F17 F 0.50049(17) 0.49434(8) 0.61551(14) 0.0263(4) Uani 1 1 d . . . . . F18 F 0.35998(14) 0.50194(8) 0.67280(16) 0.0282(5) Uani 1 1 d . . . . . F19 F 0.26136(14) 0.61576(8) 0.41997(14) 0.0248(4) Uani 1 1 d . . . . . F20 F 0.36173(15) 0.56171(7) 0.48578(14) 0.0226(4) Uani 1 1 d . . . . . F21 F 0.42235(14) 0.62739(8) 0.43800(14) 0.0243(4) Uani 1 1 d . . . . . F22 F 0.32419(15) 0.70706(7) 0.48590(15) 0.0258(4) Uani 1 1 d . . . . . F23 F 0.46436(14) 0.69428(7) 0.57106(15) 0.0231(4) Uani 1 1 d . . . . . F24 F 0.33118(16) 0.71367(7) 0.63255(15) 0.0256(4) Uani 1 1 d . . . . . O1 O 0.29071(17) 0.38920(9) 0.8309(2) 0.0266(5) Uani 1 1 d . . . . . O2 O 0.1702(2) 0.53818(8) 0.8442(2) 0.0295(6) Uani 1 1 d . . . . . O3 O 0.1911(2) 0.64241(11) 1.2182(2) 0.0332(6) Uani 1 1 d . . . . . O4 O -0.1282(2) 0.69189(8) 1.1561(2) 0.0297(6) Uani 1 1 d . . . . . O5 O 0.63685(14) 0.62976(7) 0.65724(14) 0.0119(4) Uani 1 1 d . . . . . O6 O 0.51235(15) 0.65546(7) 0.79064(15) 0.0138(4) Uani 1 1 d . . . . . O7 O 0.54951(14) 0.55535(7) 0.74846(15) 0.0115(4) Uani 1 1 d . . . . . O8 O 0.41207(14) 0.61147(7) 0.63460(14) 0.0111(3) Uani 1 1 d . . . . . C1 C -0.0579(3) 0.43980(15) 0.6817(2) 0.0266(7) Uani 1 1 d . . . . . H1 H -0.125910 0.445784 0.692432 0.032 Uiso 1 1 calc R U . . . C2 C -0.0130(3) 0.39377(14) 0.6757(2) 0.0273(7) Uani 1 1 d . . . . . H2 H -0.045408 0.363506 0.681587 0.033 Uiso 1 1 calc R U . . . C3 C 0.0884(3) 0.40082(13) 0.6595(2) 0.0235(7) Uani 1 1 d . . . . . H3 H 0.136149 0.375930 0.652580 0.028 Uiso 1 1 calc R U . . . C4 C 0.1075(3) 0.45109(12) 0.6552(2) 0.0220(6) Uani 1 1 d . . . . . H4 H 0.169765 0.465946 0.645095 0.026 Uiso 1 1 calc R U . . . C5 C 0.0150(3) 0.47526(13) 0.6689(3) 0.0251(7) Uani 1 1 d . . . . . H5 H 0.004805 0.509230 0.669403 0.030 Uiso 1 1 calc R U . . . C6 C 0.2118(2) 0.40627(11) 0.8253(2) 0.0181(6) Uani 1 1 d . . . . . C7 C 0.1368(2) 0.50046(11) 0.8311(2) 0.0186(6) Uani 1 1 d . . . . . C8 C 0.1258(2) 0.63850(11) 0.9360(2) 0.0208(6) Uani 1 1 d . . . . . H8 H 0.179110 0.616304 0.929558 0.025 Uiso 1 1 calc R U . . . C9 C 0.1335(3) 0.68135(12) 0.9878(2) 0.0221(6) Uani 1 1 d . . . . . H9 H 0.193244 0.693307 1.021679 0.027 Uiso 1 1 calc R U . . . C10 C 0.0383(3) 0.70341(12) 0.9809(3) 0.0291(8) Uani 1 1 d . . . . . H10 H 0.022034 0.732625 1.009957 0.035 Uiso 1 1 calc R U . . . C11 C -0.0300(3) 0.67443(14) 0.9226(3) 0.0294(8) Uani 1 1 d . . . . . H11 H -0.099650 0.680921 0.905493 0.035 Uiso 1 1 calc R U . . . C12 C 0.0249(3) 0.63420(14) 0.8950(2) 0.0252(7) Uani 1 1 d . . . . . H12 H -0.001288 0.608785 0.855935 0.030 Uiso 1 1 calc R U . . . C13 C 0.1278(2) 0.63549(12) 1.1611(2) 0.0210(6) Uani 1 1 d . . . . . C14 C -0.0741(2) 0.66778(11) 1.1212(2) 0.0191(6) Uani 1 1 d . . . . . C101 C 0.7041(2) 0.62262(10) 0.5964(2) 0.0122(5) Uani 1 1 d . . . . . C102 C 0.8160(2) 0.61757(11) 0.6483(2) 0.0152(5) Uani 1 1 d . . . . . C103 C 0.6978(2) 0.66762(11) 0.5299(2) 0.0169(5) Uani 1 1 d . . . . . C104 C 0.6767(2) 0.57682(11) 0.5357(2) 0.0162(5) Uani 1 1 d . . . . . C105 C 0.5512(2) 0.68698(10) 0.8560(2) 0.0126(5) Uani 1 1 d . . . . . C106 C 0.4613(2) 0.70376(10) 0.9130(2) 0.0160(5) Uani 1 1 d . . . . . C107 C 0.5981(2) 0.73174(11) 0.8096(2) 0.0188(6) Uani 1 1 d . . . . . C108 C 0.6383(2) 0.66263(12) 0.9206(2) 0.0209(6) Uani 1 1 d . . . . . C109 C 0.51122(19) 0.51332(10) 0.77501(19) 0.0108(5) Uani 1 1 d . . . . . C110 C 0.6030(2) 0.48143(10) 0.8216(2) 0.0119(5) Uani 1 1 d . . . . . C111 C 0.4325(2) 0.52290(10) 0.8448(2) 0.0159(5) Uani 1 1 d . . . . . C112 C 0.4553(2) 0.48616(11) 0.6898(2) 0.0172(5) Uani 1 1 d . . . . . C113 C 0.3407(2) 0.63258(10) 0.5745(2) 0.0115(5) Uani 1 1 d . . . . . C114 C 0.2307(2) 0.62598(10) 0.6070(2) 0.0142(5) Uani 1 1 d . . . . . C115 C 0.3456(2) 0.60909(12) 0.4780(2) 0.0167(5) Uani 1 1 d . . . . . C116 C 0.3637(2) 0.68781(11) 0.5652(2) 0.0174(6) Uani 1 1 d . . . . . C201 C 0.5300(3) 0.68677(15) 0.2475(3) 0.0347(9) Uani 1 1 d . . . . . H20A H 0.548857 0.663586 0.297815 0.042 Uiso 1 1 calc R U . . . H20B H 0.532592 0.669541 0.188658 0.042 Uiso 1 1 calc R U . . . As2 As 0.0259(9) 0.5341(4) 1.0634(8) 0.0205(18) Uiso 0.035 1 d . . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Bi1 0.01175(5) 0.01148(5) 0.01680(6) -0.00237(4) 0.00100(4) 0.00077(4) Mo2 0.01204(10) 0.00959(9) 0.01452(11) -0.00114(8) -0.00102(8) -0.00155(8) Mo1 0.01053(9) 0.01022(9) 0.01542(11) -0.00105(8) 0.00114(8) -0.00014(8) As1 0.00978(11) 0.01335(12) 0.01690(14) -0.00201(11) -0.00367(10) -0.00040(10) Cl1 0.0126(3) 0.0289(4) 0.0245(4) 0.0015(3) 0.0056(3) 0.0028(3) Cl2 0.0162(3) 0.0221(3) 0.0180(3) 0.0066(3) -0.0016(3) -0.0009(3) Cl3 0.0164(3) 0.0210(3) 0.0224(4) -0.0015(3) -0.0032(3) -0.0072(3) Cl4 0.0364(4) 0.0240(4) 0.0157(3) -0.0100(3) 0.0041(3) -0.0075(3) Cl5 0.0234(3) 0.0204(3) 0.0241(4) -0.0033(3) 0.0079(3) -0.0072(3) Cl6 0.0258(4) 0.0230(4) 0.0262(4) -0.0019(3) 0.0007(3) 0.0115(3) Cl7 0.0165(3) 0.0164(3) 0.0185(3) -0.0003(3) -0.0083(2) -0.0007(2) Cl8 0.0204(3) 0.0201(3) 0.0230(4) -0.0027(3) 0.0064(3) 0.0063(3) Cl9 0.0254(3) 0.0106(3) 0.0193(3) 0.0042(3) -0.0006(3) 0.0005(3) Cl10 0.0133(3) 0.0153(3) 0.0415(5) 0.0046(3) -0.0014(3) -0.0037(3) Cl11 0.0135(3) 0.0211(3) 0.0263(4) 0.0069(3) -0.0026(3) 0.0061(3) Cl12 0.0220(3) 0.0297(4) 0.0167(3) 0.0042(3) 0.0049(3) 0.0073(3) Cl13 0.0421(6) 0.0531(7) 0.0793(10) 0.0264(7) 0.0157(6) 0.0020(6) Cl14 0.0548(7) 0.0745(9) 0.0590(9) -0.0090(7) -0.0006(6) -0.0355(7) Al1 0.0074(3) 0.0083(3) 0.0085(4) -0.0005(3) -0.0012(3) -0.0011(3) F1 0.0195(9) 0.0306(10) 0.0230(10) 0.0111(9) 0.0083(8) -0.0018(8) F2 0.0230(9) 0.0150(8) 0.0255(10) 0.0054(8) 0.0008(8) 0.0006(7) F3 0.0197(9) 0.0339(11) 0.0158(9) 0.0083(8) -0.0047(7) -0.0013(8) F4 0.0242(9) 0.0356(11) 0.0146(9) -0.0093(8) 0.0047(8) -0.0025(9) F5 0.0139(8) 0.0249(9) 0.0230(10) -0.0083(8) -0.0011(7) -0.0055(7) F6 0.0239(9) 0.0142(8) 0.0291(11) -0.0035(8) -0.0006(8) 0.0009(7) F7 0.0419(12) 0.0129(8) 0.0282(11) -0.0066(8) 0.0069(10) -0.0090(8) F8 0.0360(11) 0.0221(9) 0.0185(10) 0.0062(8) -0.0003(8) -0.0037(9) F9 0.0232(9) 0.0279(10) 0.0361(13) -0.0027(9) 0.0123(9) -0.0082(8) F10 0.0238(9) 0.0332(11) 0.0302(12) -0.0080(10) -0.0131(9) -0.0043(9) F11 0.0199(9) 0.0268(10) 0.0320(12) -0.0034(9) -0.0024(8) 0.0091(8) F12 0.0313(10) 0.0281(11) 0.0248(11) 0.0111(9) -0.0063(9) 0.0035(9) F13 0.0295(10) 0.0272(10) 0.0166(9) -0.0006(8) 0.0068(8) 0.0060(8) F14 0.0151(8) 0.0140(8) 0.0335(11) 0.0034(8) 0.0055(8) 0.0052(7) F15 0.0206(9) 0.0156(8) 0.0480(14) 0.0080(9) 0.0137(9) -0.0027(8) F16 0.0330(10) 0.0096(8) 0.0259(11) -0.0029(7) -0.0126(8) -0.0052(7) F17 0.0385(11) 0.0258(10) 0.0133(9) -0.0030(8) -0.0032(8) -0.0041(9) F18 0.0187(9) 0.0224(10) 0.0390(13) -0.0008(9) -0.0171(8) -0.0003(8) F19 0.0185(8) 0.0374(11) 0.0161(9) -0.0022(9) -0.0086(7) 0.0038(8) F20 0.0249(9) 0.0178(9) 0.0238(10) -0.0093(8) -0.0028(8) 0.0032(8) F21 0.0190(9) 0.0381(11) 0.0161(9) 0.0028(9) 0.0034(7) -0.0001(8) F22 0.0262(10) 0.0220(9) 0.0278(11) 0.0139(9) -0.0035(8) -0.0002(8) F23 0.0174(8) 0.0172(8) 0.0338(12) 0.0061(8) -0.0017(8) -0.0089(7) F24 0.0315(10) 0.0128(8) 0.0322(12) -0.0054(8) 0.0026(9) 0.0004(8) O1 0.0155(10) 0.0231(11) 0.0416(16) -0.0018(11) 0.0040(10) 0.0047(9) O2 0.0280(12) 0.0147(10) 0.0488(18) -0.0049(11) 0.0167(12) -0.0044(10) O3 0.0269(12) 0.0367(15) 0.0330(15) 0.0014(13) -0.0109(11) -0.0117(12) O4 0.0366(14) 0.0139(10) 0.0414(16) -0.0027(11) 0.0169(13) 0.0005(10) O5 0.0097(8) 0.0151(9) 0.0109(9) 0.0005(7) 0.0014(7) -0.0021(7) O6 0.0135(8) 0.0126(9) 0.0149(10) -0.0069(8) 0.0000(7) -0.0012(7) O7 0.0094(8) 0.0082(8) 0.0164(10) 0.0026(7) -0.0010(7) -0.0006(7) O8 0.0084(8) 0.0126(8) 0.0114(9) 0.0009(7) -0.0036(7) -0.0009(7) C1 0.0201(14) 0.042(2) 0.0169(15) -0.0003(15) -0.0023(12) 0.0016(14) C2 0.0339(18) 0.0321(18) 0.0150(15) -0.0042(14) -0.0010(13) -0.0124(15) C3 0.0322(17) 0.0230(15) 0.0159(15) -0.0032(13) 0.0052(13) 0.0030(14) C4 0.0253(15) 0.0209(14) 0.0206(16) 0.0028(13) 0.0064(13) 0.0018(13) C5 0.0294(17) 0.0252(16) 0.0205(16) 0.0051(13) 0.0018(13) 0.0065(14) C6 0.0188(13) 0.0131(12) 0.0224(15) -0.0033(11) 0.0021(11) -0.0012(11) C7 0.0155(12) 0.0141(12) 0.0276(17) -0.0002(12) 0.0076(12) 0.0025(10) C8 0.0222(14) 0.0185(13) 0.0234(16) -0.0041(12) 0.0107(13) -0.0034(12) C9 0.0253(15) 0.0181(13) 0.0241(16) -0.0027(12) 0.0084(13) -0.0084(12) C10 0.042(2) 0.0126(13) 0.036(2) 0.0061(13) 0.0199(17) 0.0020(14) C11 0.0255(16) 0.0333(19) 0.0294(19) 0.0163(16) 0.0019(14) 0.0051(15) C12 0.0298(16) 0.0309(17) 0.0148(15) -0.0001(13) 0.0023(13) -0.0099(14) C13 0.0206(14) 0.0186(14) 0.0231(16) -0.0027(12) -0.0015(12) -0.0057(12) C14 0.0234(14) 0.0114(12) 0.0223(16) -0.0009(11) 0.0027(12) -0.0038(11) C101 0.0100(10) 0.0144(11) 0.0121(12) -0.0007(10) 0.0008(9) -0.0017(9) C102 0.0117(11) 0.0173(12) 0.0165(14) 0.0022(11) 0.0013(10) -0.0017(10) C103 0.0150(12) 0.0198(13) 0.0158(14) 0.0032(11) 0.0008(10) -0.0017(11) C104 0.0135(11) 0.0195(13) 0.0153(13) -0.0051(11) 0.0008(10) -0.0028(11) C105 0.0133(11) 0.0120(11) 0.0122(12) -0.0013(10) 0.0000(9) 0.0002(10) C106 0.0193(13) 0.0125(11) 0.0161(14) -0.0041(10) 0.0016(11) -0.0015(10) C107 0.0227(14) 0.0131(12) 0.0206(15) -0.0040(11) 0.0022(12) -0.0056(11) C108 0.0194(13) 0.0217(14) 0.0201(15) -0.0020(12) -0.0046(12) -0.0004(12) C109 0.0093(10) 0.0103(10) 0.0124(12) -0.0004(9) -0.0007(9) -0.0007(9) C110 0.0125(11) 0.0096(10) 0.0128(12) -0.0006(9) -0.0028(9) 0.0002(9) C111 0.0143(12) 0.0129(11) 0.0211(15) 0.0025(11) 0.0047(11) 0.0016(10) C112 0.0192(13) 0.0124(12) 0.0180(14) 0.0004(11) -0.0075(11) 0.0005(11) C113 0.0111(10) 0.0104(11) 0.0119(12) 0.0015(9) -0.0033(9) -0.0011(9) C114 0.0117(11) 0.0133(11) 0.0171(14) 0.0047(10) -0.0005(10) 0.0031(10) C115 0.0140(12) 0.0217(14) 0.0134(13) -0.0011(11) -0.0034(10) 0.0013(11) C116 0.0167(12) 0.0121(12) 0.0225(15) 0.0051(11) -0.0026(11) -0.0012(10) C201 0.036(2) 0.033(2) 0.033(2) 0.0055(17) -0.0056(17) -0.0001(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 14 7 -14 0.1251 -14 -7 14 0.1103 -1 39 -3 0.0598 2 -39 2 0.0661 0 -39 1 0.0927 11 -28 -9 0.1052 16 1 -13 0.1468 15 0 -14 0.1194 -3 -34 -9 0.3050 17 5 -11 0.1868 13 -5 13 0.4476 8 -7 17 0.4475 13 -27 4 0.2623 -14 14 13 0.1218 -3 -37 6 0.0836 11 22 11 0.4460 -14 -1 15 0.1099 -8 -1 -17 0.4706 -8 -13 -16 0.4563 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Mo2 Bi1 Bi1 103.077(8) . 3_567 ? Mo2 Bi1 Mo1 66.752(7) . 3_567 ? Mo2 Bi1 As1 141.768(9) . . ? Mo1 Bi1 Bi1 100.852(7) 3_567 3_567 ? Mo1 Bi1 As1 136.388(8) 3_567 . ? As1 Bi1 Bi1 50.435(6) . 3_567 ? As1 Bi1 Bi1 60.963(7) 3_567 3_567 ? As1 Bi1 Mo2 51.859(8) 3_567 . ? As1 Bi1 Mo1 53.576(8) 3_567 3_567 ? As1 Bi1 As1 111.398(7) 3_567 . ? Bi1 Mo2 Mo1 56.649(6) . 3_567 ? As1 Mo2 Bi1 63.076(9) 3_567 . ? As1 Mo2 Mo1 52.435(10) 3_567 3_567 ? As1 Mo2 As2 49.4(3) 3_567 . ? C8 Mo2 Bi1 93.54(8) . . ? C8 Mo2 Mo1 150.11(8) . 3_567 ? C8 Mo2 As1 115.27(8) . 3_567 ? C8 Mo2 C9 35.01(11) . . ? C8 Mo2 As2 97.9(2) . . ? C9 Mo2 Bi1 119.58(8) . . ? C9 Mo2 Mo1 160.60(10) . 3_567 ? C9 Mo2 As1 145.99(9) . 3_567 ? C9 Mo2 As2 128.5(2) . . ? C10 Mo2 Bi1 152.04(8) . . ? C10 Mo2 Mo1 151.27(8) . 3_567 ? C10 Mo2 As1 128.19(11) . 3_567 ? C10 Mo2 C8 58.61(12) . . ? C10 Mo2 C9 34.96(13) . . ? C10 Mo2 C12 59.08(14) . . ? C10 Mo2 As2 154.5(2) . . ? C11 Mo2 Bi1 133.80(11) . . ? C11 Mo2 Mo1 139.21(9) . 3_567 ? C11 Mo2 As1 93.92(10) . 3_567 ? C11 Mo2 C8 58.99(13) . . ? C11 Mo2 C9 58.82(13) . . ? C11 Mo2 C10 35.82(15) . . ? C11 Mo2 C12 35.52(14) . . ? C11 Mo2 As2 125.9(3) . . ? C12 Mo2 Bi1 100.42(10) . . ? C12 Mo2 Mo1 138.83(9) . 3_567 ? C12 Mo2 As1 87.39(9) . 3_567 ? C12 Mo2 C8 35.38(12) . . ? C12 Mo2 C9 58.61(13) . . ? C12 Mo2 As2 96.3(3) . . ? C13 Mo2 Bi1 79.00(9) . . ? C13 Mo2 Mo1 79.27(9) . 3_567 ? C13 Mo2 As1 129.31(9) . 3_567 ? C13 Mo2 C8 98.54(13) . . ? C13 Mo2 C9 81.33(13) . . ? C13 Mo2 C10 101.19(15) . . ? C13 Mo2 C11 136.60(14) . . ? C13 Mo2 C12 133.88(13) . . ? C13 Mo2 As2 91.3(3) . . ? C14 Mo2 Bi1 125.74(9) . . ? C14 Mo2 Mo1 69.15(9) . 3_567 ? C14 Mo2 As1 87.01(9) . 3_567 ? C14 Mo2 C8 140.72(12) . . ? C14 Mo2 C9 110.45(12) . . ? C14 Mo2 C10 82.12(12) . . ? C14 Mo2 C11 89.15(14) . . ? C14 Mo2 C12 123.62(14) . . ? C14 Mo2 C13 89.47(14) . . ? C14 Mo2 As2 120.5(2) . . ? Bi1 Mo1 Mo2 56.601(6) 3_567 3_567 ? As1 Mo1 Bi1 62.221(9) . 3_567 ? As1 Mo1 Mo2 50.251(9) . 3_567 ? As1 Mo1 As2 48.9(3) . 3_567 ? C1 Mo1 Bi1 85.20(8) . 3_567 ? C1 Mo1 Mo2 101.96(9) . 3_567 ? C1 Mo1 As1 144.91(8) . . ? C1 Mo1 C2 34.67(14) . . ? C1 Mo1 As2 98.9(3) . 3_567 ? C2 Mo1 Bi1 107.66(9) . 3_567 ? C2 Mo1 Mo2 92.39(9) . 3_567 ? C2 Mo1 As1 141.68(9) . . ? C2 Mo1 As2 119.6(3) . 3_567 ? C3 Mo1 Bi1 141.45(9) . 3_567 ? C3 Mo1 Mo2 115.87(9) . 3_567 ? C3 Mo1 As1 147.05(9) . . ? C3 Mo1 C1 58.11(13) . . ? C3 Mo1 C2 34.65(12) . . ? C3 Mo1 As2 154.2(3) . 3_567 ? C4 Mo1 Bi1 134.70(8) . 3_567 ? C4 Mo1 Mo2 150.38(9) . 3_567 ? C4 Mo1 As1 154.99(9) . . ? C4 Mo1 C1 59.35(12) . . ? C4 Mo1 C2 58.88(12) . . ? C4 Mo1 C3 35.67(12) . . ? C4 Mo1 C5 36.51(12) . . ? C4 Mo1 As2 145.1(3) . 3_567 ? C5 Mo1 Bi1 98.34(9) . 3_567 ? C5 Mo1 Mo2 135.80(9) . 3_567 ? C5 Mo1 As1 153.39(9) . . ? C5 Mo1 C1 35.20(13) . . ? C5 Mo1 C2 58.52(14) . . ? C5 Mo1 C3 59.25(13) . . ? C5 Mo1 As2 109.8(3) . 3_567 ? C6 Mo1 Bi1 135.21(10) . 3_567 ? C6 Mo1 Mo2 94.10(9) . 3_567 ? C6 Mo1 As1 73.00(10) . . ? C6 Mo1 C1 137.48(13) . . ? C6 Mo1 C2 106.52(13) . . ? C6 Mo1 C3 79.42(13) . . ? C6 Mo1 C4 88.10(13) . . ? C6 Mo1 C5 124.16(13) . . ? C6 Mo1 As2 121.9(3) . 3_567 ? C7 Mo1 Bi1 83.31(8) . 3_567 ? C7 Mo1 Mo2 123.96(9) . 3_567 ? C7 Mo1 As1 77.97(10) . . ? C7 Mo1 C1 112.74(14) . . ? C7 Mo1 C2 139.85(14) . . ? C7 Mo1 C3 119.64(13) . . ? C7 Mo1 C4 85.59(13) . . ? C7 Mo1 C5 82.00(14) . . ? C7 Mo1 C6 88.84(12) . . ? C7 Mo1 As2 78.2(2) . 3_567 ? Bi1 As1 Bi1 68.600(7) 3_567 . ? Mo2 As1 Bi1 119.476(11) 3_567 . ? Mo2 As1 Bi1 65.067(9) 3_567 3_567 ? Mo2 As1 Mo1 77.313(12) 3_567 . ? Mo1 As1 Bi1 64.205(9) . 3_567 ? Mo1 As1 Bi1 114.142(12) . . ? As2 As1 Mo1 66.7(3) 3_567 . ? O5 Al1 O8 119.05(10) . . ? O6 Al1 O5 106.34(10) . . ? O6 Al1 O7 112.38(11) . . ? O6 Al1 O8 106.89(10) . . ? O7 Al1 O5 105.37(10) . . ? O7 Al1 O8 106.96(10) . . ? C101 O5 Al1 150.93(19) . . ? C105 O6 Al1 151.34(18) . . ? C109 O7 Al1 147.98(18) . . ? C113 O8 Al1 151.08(18) . . ? Mo1 C1 H1 121.9 . . ? C2 C1 Mo1 74.0(2) . . ? C2 C1 H1 125.7 . . ? C5 C1 Mo1 70.0(2) . . ? C5 C1 H1 125.7 . . ? C5 C1 C2 108.6(3) . . ? Mo1 C2 H2 123.4 . . ? C1 C2 Mo1 71.3(2) . . ? C1 C2 H2 126.1 . . ? C3 C2 Mo1 70.7(2) . . ? C3 C2 C1 107.7(3) . . ? C3 C2 H2 126.1 . . ? Mo1 C3 H3 121.4 . . ? C2 C3 Mo1 74.61(19) . . ? C2 C3 H3 125.6 . . ? C2 C3 C4 108.9(3) . . ? C4 C3 Mo1 70.10(19) . . ? C4 C3 H3 125.6 . . ? Mo1 C4 H4 119.1 . . ? C3 C4 Mo1 74.23(19) . . ? C3 C4 H4 126.6 . . ? C3 C4 C5 106.9(3) . . ? C5 C4 Mo1 72.07(19) . . ? C5 C4 H4 126.6 . . ? Mo1 C5 H5 119.6 . . ? C1 C5 Mo1 74.8(2) . . ? C1 C5 C4 108.0(3) . . ? C1 C5 H5 126.0 . . ? C4 C5 Mo1 71.4(2) . . ? C4 C5 H5 126.0 . . ? O1 C6 Mo1 174.3(3) . . ? O2 C7 Mo1 176.7(3) . . ? Mo2 C8 H8 121.0 . . ? C9 C8 Mo2 72.87(17) . . ? C9 C8 H8 126.0 . . ? C9 C8 C12 108.1(3) . . ? C12 C8 Mo2 71.93(17) . . ? C12 C8 H8 126.0 . . ? Mo2 C9 H9 122.2 . . ? C8 C9 Mo2 72.12(17) . . ? C8 C9 H9 125.8 . . ? C10 C9 Mo2 71.61(17) . . ? C10 C9 C8 108.5(3) . . ? C10 C9 H9 125.8 . . ? Mo2 C10 H10 120.4 . . ? C9 C10 Mo2 73.43(19) . . ? C9 C10 H10 125.9 . . ? C9 C10 C11 108.1(3) . . ? C11 C10 Mo2 71.98(19) . . ? C11 C10 H10 125.9 . . ? Mo2 C11 H11 120.8 . . ? C10 C11 Mo2 72.2(2) . . ? C10 C11 H11 126.3 . . ? C12 C11 Mo2 72.5(2) . . ? C12 C11 C10 107.4(3) . . ? C12 C11 H11 126.3 . . ? Mo2 C12 H12 121.1 . . ? C8 C12 Mo2 72.69(19) . . ? C8 C12 C11 108.0(3) . . ? C8 C12 H12 126.0 . . ? C11 C12 Mo2 72.0(2) . . ? C11 C12 H12 126.0 . . ? O3 C13 Mo2 173.6(3) . . ? O4 C14 Mo2 175.5(3) . . ? O5 C101 C102 110.3(2) . . ? O5 C101 C103 107.4(2) . . ? O5 C101 C104 111.4(2) . . ? C103 C101 C102 110.3(2) . . ? C104 C101 C102 110.3(2) . . ? C104 C101 C103 107.0(2) . . ? Cl2 C102 Cl1 107.89(16) . . ? Cl3 C102 Cl1 107.34(14) . . ? Cl3 C102 Cl2 108.16(17) . . ? C101 C102 Cl1 113.0(2) . . ? C101 C102 Cl2 109.03(18) . . ? C101 C102 Cl3 111.2(2) . . ? F1 C103 F3 107.2(2) . . ? F1 C103 C101 113.9(2) . . ? F2 C103 F1 107.5(2) . . ? F2 C103 F3 106.5(2) . . ? F2 C103 C101 111.3(2) . . ? F3 C103 C101 110.0(2) . . ? F4 C104 C101 112.7(2) . . ? F5 C104 F4 107.1(3) . . ? F5 C104 C101 109.6(2) . . ? F6 C104 F4 107.1(2) . . ? F6 C104 F5 107.3(2) . . ? F6 C104 C101 112.8(3) . . ? O6 C105 C106 107.9(2) . . ? O6 C105 C107 109.8(2) . . ? O6 C105 C108 110.6(2) . . ? C107 C105 C106 110.6(2) . . ? C108 C105 C106 110.7(2) . . ? C108 C105 C107 107.4(2) . . ? Cl4 C106 Cl5 107.68(16) . . ? Cl6 C106 Cl4 108.82(15) . . ? Cl6 C106 Cl5 107.16(17) . . ? C105 C106 Cl4 113.4(2) . . ? C105 C106 Cl5 109.10(19) . . ? C105 C106 Cl6 110.4(2) . . ? F7 C107 F9 106.7(3) . . ? F7 C107 C105 113.9(3) . . ? F8 C107 F7 107.8(3) . . ? F8 C107 F9 106.3(3) . . ? F8 C107 C105 111.3(2) . . ? F9 C107 C105 110.4(2) . . ? F10 C108 C105 113.2(3) . . ? F11 C108 F10 106.8(3) . . ? F11 C108 F12 106.7(3) . . ? F11 C108 C105 109.8(3) . . ? F12 C108 F10 107.1(3) . . ? F12 C108 C105 113.0(3) . . ? O7 C109 C110 107.8(2) . . ? O7 C109 C111 110.2(2) . . ? O7 C109 C112 110.1(2) . . ? C111 C109 C110 110.3(2) . . ? C111 C109 C112 108.0(2) . . ? C112 C109 C110 110.5(2) . . ? Cl8 C110 Cl7 107.12(14) . . ? Cl9 C110 Cl7 107.89(16) . . ? Cl9 C110 Cl8 107.87(14) . . ? C109 C110 Cl7 109.58(18) . . ? C109 C110 Cl8 109.56(19) . . ? C109 C110 Cl9 114.54(18) . . ? F13 C111 F14 107.5(2) . . ? F13 C111 F15 107.5(3) . . ? F13 C111 C109 112.2(2) . . ? F14 C111 F15 107.5(2) . . ? F14 C111 C109 109.4(2) . . ? F15 C111 C109 112.6(2) . . ? F16 C112 C109 113.4(2) . . ? F17 C112 F16 108.1(3) . . ? F17 C112 F18 107.3(3) . . ? F17 C112 C109 110.8(2) . . ? F18 C112 F16 106.5(2) . . ? F18 C112 C109 110.4(2) . . ? O8 C113 C114 110.8(2) . . ? O8 C113 C115 108.3(2) . . ? O8 C113 C116 110.3(2) . . ? C115 C113 C114 110.6(2) . . ? C115 C113 C116 107.3(2) . . ? C116 C113 C114 109.4(2) . . ? Cl11 C114 Cl10 107.24(16) . . ? Cl12 C114 Cl10 107.40(15) . . ? Cl12 C114 Cl11 108.46(15) . . ? C113 C114 Cl10 110.88(19) . . ? C113 C114 Cl11 113.08(19) . . ? C113 C114 Cl12 109.6(2) . . ? F19 C115 C113 113.7(2) . . ? F20 C115 F19 107.8(3) . . ? F20 C115 C113 110.7(2) . . ? F21 C115 F19 107.2(2) . . ? F21 C115 F20 106.8(2) . . ? F21 C115 C113 110.5(2) . . ? F22 C116 F23 107.3(2) . . ? F22 C116 C113 113.7(3) . . ? F23 C116 C113 109.1(2) . . ? F24 C116 F22 107.7(2) . . ? F24 C116 F23 106.4(3) . . ? F24 C116 C113 112.2(2) . . ? Cl13 C201 H20A 109.4 . . ? Cl13 C201 H20B 109.4 . . ? Cl14 C201 Cl13 111.2(2) . . ? Cl14 C201 H20A 109.4 . . ? Cl14 C201 H20B 109.4 . . ? H20A C201 H20B 108.0 . . ? Mo2 As2 As2 131.1(7) . 3_567 ? Mo1 As2 Mo2 74.0(3) 3_567 . ? Mo1 As2 As2 128.8(6) 3_567 3_567 ? As1 As2 Mo2 61.8(3) 3_567 . ? As1 As2 Mo1 64.4(3) 3_567 3_567 ? As1 As2 As2 88.1(6) 3_567 3_567 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Bi1 Bi1 3.4273(3) 3_567 ? Bi1 Mo2 2.8860(3) . ? Bi1 Mo1 2.8877(2) 3_567 ? Bi1 As1 3.2184(3) . ? Bi1 As1 2.8377(3) 3_567 ? Mo2 Mo1 3.1763(3) 3_567 ? Mo2 As1 2.5032(4) 3_567 ? Mo2 C8 2.333(3) . ? Mo2 C9 2.342(3) . ? Mo2 C10 2.319(3) . ? Mo2 C11 2.316(4) . ? Mo2 C12 2.323(3) . ? Mo2 C13 2.018(4) . ? Mo2 C14 2.005(3) . ? Mo2 As2 2.650(10) . ? Mo1 As1 2.5808(4) . ? Mo1 C1 2.354(4) . ? Mo1 C2 2.388(4) . ? Mo1 C3 2.338(3) . ? Mo1 C4 2.285(3) . ? Mo1 C5 2.293(4) . ? Mo1 C6 2.008(3) . ? Mo1 C7 1.987(3) . ? Mo1 As2 2.629(10) 3_567 ? As1 As2 2.158(12) 3_567 ? Cl1 C102 1.786(3) . ? Cl2 C102 1.773(3) . ? Cl3 C102 1.765(3) . ? Cl4 C106 1.774(3) . ? Cl5 C106 1.777(3) . ? Cl6 C106 1.767(3) . ? Cl7 C110 1.781(3) . ? Cl8 C110 1.774(3) . ? Cl9 C110 1.773(3) . ? Cl10 C114 1.780(3) . ? Cl11 C114 1.774(3) . ? Cl12 C114 1.768(3) . ? Cl13 C201 1.759(4) . ? Cl14 C201 1.748(4) . ? Al1 O5 1.7493(19) . ? Al1 O6 1.737(2) . ? Al1 O7 1.744(2) . ? Al1 O8 1.749(2) . ? F1 C103 1.339(3) . ? F2 C103 1.327(4) . ? F3 C103 1.342(4) . ? F4 C104 1.344(3) . ? F5 C104 1.332(3) . ? F6 C104 1.331(4) . ? F7 C107 1.334(4) . ? F8 C107 1.330(4) . ? F9 C107 1.338(4) . ? F10 C108 1.342(4) . ? F11 C108 1.330(4) . ? F12 C108 1.331(4) . ? F13 C111 1.327(4) . ? F14 C111 1.329(3) . ? F15 C111 1.345(3) . ? F16 C112 1.341(3) . ? F17 C112 1.320(4) . ? F18 C112 1.338(4) . ? F19 C115 1.345(4) . ? F20 C115 1.331(4) . ? F21 C115 1.331(3) . ? F22 C116 1.336(4) . ? F23 C116 1.344(3) . ? F24 C116 1.330(4) . ? O1 C6 1.146(4) . ? O2 C7 1.142(4) . ? O3 C13 1.139(4) . ? O4 C14 1.142(4) . ? O5 C101 1.345(3) . ? O6 C105 1.356(4) . ? O7 C109 1.344(3) . ? O8 C113 1.356(3) . ? C1 H1 0.9500 . ? C1 C2 1.413(6) . ? C1 C5 1.406(5) . ? C2 H2 0.9500 . ? C2 C3 1.408(5) . ? C3 H3 0.9500 . ? C3 C4 1.417(5) . ? C4 H4 0.9500 . ? C4 C5 1.434(5) . ? C5 H5 0.9500 . ? C8 H8 0.9500 . ? C8 C9 1.406(5) . ? C8 C12 1.415(5) . ? C9 H9 0.9500 . ? C9 C10 1.400(5) . ? C10 H10 0.9500 . ? C10 C11 1.425(6) . ? C11 H11 0.9500 . ? C11 C12 1.415(5) . ? C12 H12 0.9500 . ? C101 C102 1.602(4) . ? C101 C103 1.579(4) . ? C101 C104 1.569(4) . ? C105 C106 1.601(4) . ? C105 C107 1.574(4) . ? C105 C108 1.568(4) . ? C109 C110 1.598(4) . ? C109 C111 1.565(4) . ? C109 C112 1.575(4) . ? C113 C114 1.598(4) . ? C113 C115 1.567(4) . ? C113 C116 1.567(4) . ? C201 H20A 0.9900 . ? C201 H20B 0.9900 . ? As2 As2 2.69(2) 3_567 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Mo2 C8 C9 C10 -62.8(2) . . . . ? Mo2 C8 C12 C11 63.8(2) . . . . ? Mo2 C9 C10 C11 -64.1(2) . . . . ? Mo2 C10 C11 C12 -64.5(2) . . . . ? Mo2 C11 C12 C8 -64.2(2) . . . . ? Mo1 C1 C2 C3 -61.7(3) . . . . ? Mo1 C1 C5 C4 64.2(3) . . . . ? Mo1 C2 C3 C4 -62.1(3) . . . . ? Mo1 C3 C4 C5 -65.2(2) . . . . ? Mo1 C4 C5 C1 -66.4(3) . . . . ? Al1 O5 C101 C102 -124.4(4) . . . . ? Al1 O5 C101 C103 115.3(4) . . . . ? Al1 O5 C101 C104 -1.5(5) . . . . ? Al1 O6 C105 C106 -170.8(3) . . . . ? Al1 O6 C105 C107 68.7(5) . . . . ? Al1 O6 C105 C108 -49.6(5) . . . . ? Al1 O7 C109 C110 -171.8(3) . . . . ? Al1 O7 C109 C111 -51.4(5) . . . . ? Al1 O7 C109 C112 67.6(4) . . . . ? Al1 O8 C113 C114 -129.0(3) . . . . ? Al1 O8 C113 C115 109.5(4) . . . . ? Al1 O8 C113 C116 -7.7(5) . . . . ? O5 Al1 O6 C105 -29.6(4) . . . . ? O5 Al1 O7 C109 -158.0(4) . . . . ? O5 Al1 O8 C113 -55.5(4) . . . . ? O5 C101 C102 Cl1 167.19(19) . . . . ? O5 C101 C102 Cl2 47.2(3) . . . . ? O5 C101 C102 Cl3 -72.0(3) . . . . ? O5 C101 C103 F1 160.9(2) . . . . ? O5 C101 C103 F2 39.2(3) . . . . ? O5 C101 C103 F3 -78.7(3) . . . . ? O5 C101 C104 F4 153.5(2) . . . . ? O5 C101 C104 F5 34.3(3) . . . . ? O5 C101 C104 F6 -85.2(3) . . . . ? O6 Al1 O5 C101 -179.3(4) . . . . ? O6 Al1 O7 C109 86.6(4) . . . . ? O6 Al1 O8 C113 64.8(4) . . . . ? O6 C105 C106 Cl4 166.9(2) . . . . ? O6 C105 C106 Cl5 46.8(3) . . . . ? O6 C105 C106 Cl6 -70.7(3) . . . . ? O6 C105 C107 F7 157.2(3) . . . . ? O6 C105 C107 F8 35.1(3) . . . . ? O6 C105 C107 F9 -82.7(3) . . . . ? O6 C105 C108 F10 161.0(2) . . . . ? O6 C105 C108 F11 41.9(3) . . . . ? O6 C105 C108 F12 -77.1(3) . . . . ? O7 Al1 O5 C101 61.2(4) . . . . ? O7 Al1 O6 C105 85.2(4) . . . . ? O7 Al1 O8 C113 -174.6(4) . . . . ? O7 C109 C110 Cl7 46.8(3) . . . . ? O7 C109 C110 Cl8 -70.5(2) . . . . ? O7 C109 C110 Cl9 168.18(19) . . . . ? O7 C109 C111 F13 -75.4(3) . . . . ? O7 C109 C111 F14 43.7(3) . . . . ? O7 C109 C111 F15 163.2(2) . . . . ? O7 C109 C112 F16 155.5(2) . . . . ? O7 C109 C112 F17 33.6(3) . . . . ? O7 C109 C112 F18 -85.1(3) . . . . ? O8 Al1 O5 C101 -58.7(4) . . . . ? O8 Al1 O6 C105 -157.7(4) . . . . ? O8 Al1 O7 C109 -30.4(4) . . . . ? O8 C113 C114 Cl10 -73.9(3) . . . . ? O8 C113 C114 Cl11 165.65(19) . . . . ? O8 C113 C114 Cl12 44.5(3) . . . . ? O8 C113 C115 F19 160.9(2) . . . . ? O8 C113 C115 F20 39.5(3) . . . . ? O8 C113 C115 F21 -78.6(3) . . . . ? O8 C113 C116 F22 155.5(2) . . . . ? O8 C113 C116 F23 35.7(3) . . . . ? O8 C113 C116 F24 -82.0(3) . . . . ? C1 C2 C3 Mo1 62.1(3) . . . . ? C1 C2 C3 C4 0.0(4) . . . . ? C2 C1 C5 Mo1 -64.4(3) . . . . ? C2 C1 C5 C4 -0.3(4) . . . . ? C2 C3 C4 Mo1 65.0(3) . . . . ? C2 C3 C4 C5 -0.1(4) . . . . ? C3 C4 C5 Mo1 66.6(2) . . . . ? C3 C4 C5 C1 0.2(4) . . . . ? C5 C1 C2 Mo1 61.9(3) . . . . ? C5 C1 C2 C3 0.2(4) . . . . ? C8 C9 C10 Mo2 63.1(2) . . . . ? C8 C9 C10 C11 -1.0(4) . . . . ? C9 C8 C12 Mo2 -64.4(2) . . . . ? C9 C8 C12 C11 -0.6(4) . . . . ? C9 C10 C11 Mo2 65.0(2) . . . . ? C9 C10 C11 C12 0.6(4) . . . . ? C10 C11 C12 Mo2 64.3(2) . . . . ? C10 C11 C12 C8 0.0(4) . . . . ? C12 C8 C9 Mo2 63.8(2) . . . . ? C12 C8 C9 C10 1.0(4) . . . . ? C102 C101 C103 F1 40.6(3) . . . . ? C102 C101 C103 F2 -81.2(3) . . . . ? C102 C101 C103 F3 161.0(2) . . . . ? C102 C101 C104 F4 -83.6(3) . . . . ? C102 C101 C104 F5 157.2(2) . . . . ? C102 C101 C104 F6 37.7(3) . . . . ? C103 C101 C102 Cl1 -74.3(3) . . . . ? C103 C101 C102 Cl2 165.78(19) . . . . ? C103 C101 C102 Cl3 46.6(3) . . . . ? C103 C101 C104 F4 36.3(3) . . . . ? C103 C101 C104 F5 -82.9(3) . . . . ? C103 C101 C104 F6 157.7(2) . . . . ? C104 C101 C102 Cl1 43.7(3) . . . . ? C104 C101 C102 Cl2 -76.3(2) . . . . ? C104 C101 C102 Cl3 164.50(19) . . . . ? C104 C101 C103 F1 -79.4(3) . . . . ? C104 C101 C103 F2 158.9(2) . . . . ? C104 C101 C103 F3 41.0(3) . . . . ? C106 C105 C107 F7 38.3(4) . . . . ? C106 C105 C107 F8 -83.8(3) . . . . ? C106 C105 C107 F9 158.4(3) . . . . ? C106 C105 C108 F10 -79.5(3) . . . . ? C106 C105 C108 F11 161.4(2) . . . . ? C106 C105 C108 F12 42.4(3) . . . . ? C107 C105 C106 Cl4 -73.1(3) . . . . ? C107 C105 C106 Cl5 166.9(2) . . . . ? C107 C105 C106 Cl6 49.4(3) . . . . ? C107 C105 C108 F10 41.3(3) . . . . ? C107 C105 C108 F11 -77.9(3) . . . . ? C107 C105 C108 F12 163.2(3) . . . . ? C108 C105 C106 Cl4 45.8(3) . . . . ? C108 C105 C106 Cl5 -74.3(3) . . . . ? C108 C105 C106 Cl6 168.2(2) . . . . ? C108 C105 C107 F7 -82.6(3) . . . . ? C108 C105 C107 F8 155.3(2) . . . . ? C108 C105 C107 F9 37.5(3) . . . . ? C110 C109 C111 F13 43.5(3) . . . . ? C110 C109 C111 F14 162.7(2) . . . . ? C110 C109 C111 F15 -77.9(3) . . . . ? C110 C109 C112 F16 36.5(3) . . . . ? C110 C109 C112 F17 -85.3(3) . . . . ? C110 C109 C112 F18 155.9(2) . . . . ? C111 C109 C110 Cl7 -73.6(2) . . . . ? C111 C109 C110 Cl8 169.19(19) . . . . ? C111 C109 C110 Cl9 47.8(3) . . . . ? C111 C109 C112 F16 -84.2(3) . . . . ? C111 C109 C112 F17 154.0(2) . . . . ? C111 C109 C112 F18 35.2(3) . . . . ? C112 C109 C110 Cl7 167.12(19) . . . . ? C112 C109 C110 Cl8 49.9(3) . . . . ? C112 C109 C110 Cl9 -71.5(3) . . . . ? C112 C109 C111 F13 164.3(2) . . . . ? C112 C109 C111 F14 -76.5(3) . . . . ? C112 C109 C111 F15 42.9(3) . . . . ? C114 C113 C115 F19 39.2(3) . . . . ? C114 C113 C115 F20 -82.2(3) . . . . ? C114 C113 C115 F21 159.7(2) . . . . ? C114 C113 C116 F22 -82.4(3) . . . . ? C114 C113 C116 F23 157.8(2) . . . . ? C114 C113 C116 F24 40.1(3) . . . . ? C115 C113 C114 Cl10 46.3(3) . . . . ? C115 C113 C114 Cl11 -74.2(3) . . . . ? C115 C113 C114 Cl12 164.70(19) . . . . ? C115 C113 C116 F22 37.7(3) . . . . ? C115 C113 C116 F23 -82.1(3) . . . . ? C115 C113 C116 F24 160.2(2) . . . . ? C116 C113 C114 Cl10 164.4(2) . . . . ? C116 C113 C114 Cl11 43.9(3) . . . . ? C116 C113 C114 Cl12 -77.3(3) . . . . ? C116 C113 C115 F19 -80.1(3) . . . . ? C116 C113 C115 F20 158.5(2) . . . . ? C116 C113 C115 F21 40.5(3) . . . . ?