#------------------------------------------------------------------------------ #$Date: 2022-01-16 18:04:14 +0200 (Sun, 16 Jan 2022) $ #$Revision: 272079 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/56/59/1565988.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565988 _cell_angle_alpha 98.356 _cell_angle_beta 99.482 _cell_angle_gamma 100.719 _cell_length_a 8.1759 _cell_length_b 10.9024 _cell_length_c 11.1088 _exptl_crystal_F_000 446.00 _reflns_d_resolution_high 0.8191 _cod_data_source_file cmpd2.fcf _cod_data_source_block ada271_tw _shelx_title ' ada271_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.90 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1508.12 1604.00 31.08 o 3 0 0 456.06 432.37 8.78 o 4 0 0 523.49 524.73 15.35 o 5 0 0 1706.19 1602.07 37.90 o 6 0 0 199.59 187.56 6.94 o 7 0 0 184.45 187.14 6.27 o 8 0 0 7.15 7.03 0.64 o 9 0 0 214.41 228.22 7.82 o -9 1 0 3.28 11.81 1.65 o -8 1 0 33.11 35.34 2.10 o -7 1 0 2.06 24.66 2.36 o -6 1 0 309.15 296.02 11.08 o -5 1 0 371.18 379.10 10.51 o -4 1 0 292.77 319.64 8.03 o -3 1 0 52.32 50.90 1.58 o -2 1 0 15.04 19.11 0.82 o -1 1 0 27.93 27.73 1.89 o 0 1 0 1323.20 1138.54 54.79 o 1 1 0 1624.00 1932.25 35.47 o 2 1 0 1624.64 1767.35 34.81 o 3 1 0 764.89 842.65 16.24 o 4 1 0 89.51 99.10 4.09 o 5 1 0 175.32 233.22 7.32 o 6 1 0 1.78 11.71 1.57 o 7 1 0 5.86 10.26 1.10 o 8 1 0 4.44 9.53 0.73 o 9 1 0 2.49 2.49 0.37 o -9 2 0 393.08 424.17 12.30 o -7 2 0 166.71 172.94 5.17 o -6 2 0 871.42 892.36 35.43 o -5 2 0 329.81 333.00 9.43 o -4 2 0 90.33 117.39 4.30 o -3 2 0 1932.39 1734.56 39.80 o -2 2 0 55.27 59.30 3.24 o -1 2 0 3978.53 3458.06 135.40 o 0 2 0 6791.06 7103.33 198.89 o 1 2 0 398.57 385.19 8.00 o 2 2 0 5023.98 5531.95 114.76 o 3 2 0 5944.80 6426.15 133.48 o 4 2 0 401.12 395.82 10.77 o 5 2 0 233.89 347.19 12.66 o 6 2 0 100.98 151.99 3.90 o 7 2 0 198.36 255.98 5.96 o 8 2 0 349.65 383.94 9.04 o 9 2 0 23.20 25.91 2.12 o -9 3 0 22.02 23.69 1.23 o -8 3 0 46.44 46.79 1.70 o -7 3 0 20.76 20.02 1.43 o -6 3 0 61.15 90.84 15.65 o -5 3 0 68.66 77.02 3.82 o -4 3 0 54.92 53.52 2.80 o -3 3 0 2433.63 2317.36 49.22 o -2 3 0 93.42 79.85 2.87 o -1 3 0 3167.73 3476.82 91.58 o 0 3 0 399.08 415.23 9.46 o 1 3 0 2154.38 2203.42 43.21 o 2 3 0 65.39 91.50 3.85 o 3 3 0 767.04 826.59 20.17 o 4 3 0 179.29 179.97 6.54 o 5 3 0 44.68 136.82 40.49 o 6 3 0 44.81 57.21 1.61 o 7 3 0 4.32 3.79 0.40 o 8 3 0 8.06 5.80 0.97 o -9 4 0 22.01 20.14 1.19 o -8 4 0 1.12 2.23 0.43 o -7 4 0 262.74 250.16 9.49 o -6 4 0 408.81 353.57 10.76 o -5 4 0 384.64 437.82 13.54 o -4 4 0 1165.44 1030.71 29.20 o -3 4 0 2966.37 2941.81 62.45 o -2 4 0 5181.33 5423.07 133.84 o -1 4 0 6390.39 6334.88 142.24 o 0 4 0 741.17 733.18 19.43 o 1 4 0 426.36 383.19 9.87 o 2 4 0 2958.89 2810.48 64.05 o 3 4 0 604.45 553.77 15.60 o 4 4 0 74.20 100.35 5.67 o 5 4 0 35.68 40.95 1.28 o 6 4 0 1.93 3.16 0.39 o 7 4 0 158.54 172.25 5.28 o 8 4 0 108.97 110.28 3.24 o -9 5 0 49.76 59.83 2.34 o -8 5 0 41.36 36.32 1.59 o -7 5 0 1.08 2.24 0.51 o -6 5 0 49.54 45.16 2.11 o -5 5 0 0.56 9.04 1.49 o -4 5 0 107.20 57.67 3.14 o -3 5 0 23.95 26.16 2.29 o -2 5 0 3.10 15.56 2.05 o -1 5 0 547.07 565.64 13.39 o 0 5 0 259.27 257.73 7.71 o 1 5 0 359.47 359.06 9.02 o 2 5 0 312.55 302.16 9.67 o 3 5 0 66.31 64.30 3.63 o 4 5 0 546.69 545.25 11.31 o 5 5 0 2.37 1.58 0.31 o 6 5 0 8.63 15.39 0.78 o 7 5 0 27.54 26.80 0.91 o 8 5 0 0.96 2.17 0.27 o -9 6 0 100.63 95.17 4.04 o -8 6 0 42.58 39.32 1.65 o -7 6 0 10.20 9.14 0.84 o -6 6 0 3.90 6.22 0.72 o -5 6 0 1035.42 742.20 24.38 o -4 6 0 561.59 421.38 12.19 o -3 6 0 596.20 566.90 15.41 o -2 6 0 2087.74 1990.21 47.00 o -1 6 0 549.56 502.88 13.77 o 0 6 0 607.64 551.01 16.19 o 1 6 0 3371.21 3116.51 87.38 o 2 6 0 2016.37 1839.96 47.43 o 3 6 0 86.91 80.24 5.51 o 4 6 0 269.53 243.96 5.56 o 5 6 0 94.49 99.97 2.58 o 6 6 0 16.90 20.07 0.90 o 7 6 0 67.93 54.50 1.40 o -9 7 0 18.99 27.46 1.80 o -8 7 0 131.45 146.95 4.38 o -7 7 0 221.44 227.51 6.60 o -6 7 0 73.45 85.15 3.58 o -5 7 0 1571.53 1571.78 36.32 o -4 7 0 205.01 191.78 10.47 o -3 7 0 99.38 96.45 4.80 o -2 7 0 110.00 120.20 8.06 o -1 7 0 177.95 169.37 8.73 o 0 7 0 866.51 864.56 31.65 o 1 7 0 28.00 25.75 3.24 o 2 7 0 977.53 885.89 21.61 o 3 7 0 421.85 420.49 9.18 o 4 7 0 19.09 23.88 1.07 o 5 7 0 61.68 63.19 1.76 o 6 7 0 8.34 9.15 0.52 o 7 7 0 0.20 0.70 0.17 o -8 8 0 110.23 118.96 3.63 o -7 8 0 89.14 91.71 3.07 o -6 8 0 365.65 360.61 9.26 o -5 8 0 1628.14 1536.43 32.90 o -4 8 0 68.63 60.88 1.85 o -3 8 0 3.92 5.92 0.57 o -2 8 0 373.02 330.47 11.37 o -1 8 0 502.71 445.66 14.31 o 0 8 0 1395.09 1318.30 34.82 o 1 8 0 874.65 811.28 17.26 o 2 8 0 6.40 4.40 0.46 o 3 8 0 9.27 4.95 0.47 o 4 8 0 519.64 507.97 10.97 o 5 8 0 80.38 100.53 2.63 o 6 8 0 32.84 30.60 0.92 o -8 9 0 3.01 3.20 0.62 o -7 9 0 41.74 35.17 1.49 o -6 9 0 8.90 12.59 0.91 o -5 9 0 22.96 23.24 1.21 o -4 9 0 171.63 160.78 3.89 o -3 9 0 48.80 51.66 2.25 o -2 9 0 31.36 31.49 1.39 o -1 9 0 40.40 39.77 1.83 o 0 9 0 8.84 7.90 0.64 o 1 9 0 59.48 58.93 1.90 o 2 9 0 86.47 78.57 2.12 o 3 9 0 77.16 75.85 2.19 o 4 9 0 9.94 15.32 0.74 o 5 9 0 75.19 81.41 2.09 o -7 10 0 41.87 52.61 1.97 o -6 10 0 100.03 105.23 3.35 o -5 10 0 634.68 636.92 16.95 o -4 10 0 364.26 364.22 8.45 o -3 10 0 696.77 648.70 13.43 o -2 10 0 330.61 295.23 6.89 o -1 10 0 36.46 34.90 1.96 o 0 10 0 215.03 202.52 5.98 o 1 10 0 296.73 283.41 6.87 o 2 10 0 135.08 126.19 3.05 o 3 10 0 50.06 53.07 1.71 o 4 10 0 11.44 11.12 0.60 o -7 11 0 20.31 21.52 2.83 o -6 11 0 0.03 0.22 0.21 o -5 11 0 26.28 27.84 1.16 o -4 11 0 10.77 13.24 0.74 o -3 11 0 40.83 45.80 1.52 o -2 11 0 2.84 2.71 0.42 o -1 11 0 61.98 64.92 2.00 o 0 11 0 224.12 205.07 4.73 o 1 11 0 34.55 29.73 1.12 o 2 11 0 6.06 6.51 0.63 o 3 11 0 48.39 41.15 1.29 o -5 12 0 37.84 39.48 1.49 o -4 12 0 37.47 38.08 1.63 o -3 12 0 166.61 158.82 4.13 o -2 12 0 230.05 198.17 4.60 o -1 12 0 262.10 240.38 5.80 o 0 12 0 95.56 96.11 3.27 o 1 12 0 12.09 11.87 0.57 o 2 12 0 82.78 78.96 2.76 o -3 13 0 26.41 25.24 0.87 o -2 13 0 31.89 24.43 1.06 o -1 13 0 4.29 4.21 0.42 o 0 -13 1 13.45 14.62 1.52 o 1 -13 1 2.40 1.67 0.26 o 2 -13 1 110.92 106.81 3.26 o 3 -13 1 105.51 99.53 2.55 o -2 -12 1 8.99 7.17 0.49 o -1 -12 1 16.30 17.36 0.80 o 0 -12 1 1.75 2.59 0.34 o 1 -12 1 131.28 125.38 3.24 o 2 -12 1 31.28 32.70 1.40 o 3 -12 1 1.28 0.87 0.29 o 4 -12 1 0.76 0.31 0.21 o 5 -12 1 0.78 0.86 0.23 o -3 -11 1 149.53 139.52 4.14 o -2 -11 1 67.33 64.08 1.99 o -1 -11 1 56.48 55.95 1.71 o 0 -11 1 3.72 5.09 0.57 o 1 -11 1 6.57 8.78 0.67 o 2 -11 1 297.61 284.62 7.40 o 3 -11 1 514.20 472.63 15.20 o 4 -11 1 720.86 646.57 19.25 o 5 -11 1 303.71 308.77 8.80 o 6 -11 1 93.75 112.75 3.84 o 7 -11 1 75.99 86.07 4.16 o -4 -10 1 16.56 14.89 0.73 o -3 -10 1 16.62 15.74 0.79 o -2 -10 1 13.63 11.36 0.80 o -1 -10 1 3.73 4.19 0.48 o 0 -10 1 59.02 54.26 1.81 o 1 -10 1 22.41 17.64 1.03 o 2 -10 1 0.38 0.72 0.33 o 3 -10 1 39.07 38.11 1.40 o 4 -10 1 0.50 0.76 0.32 o 5 -10 1 9.37 10.44 0.75 o 6 -10 1 15.37 20.18 1.34 o 7 -10 1 1.65 16.44 3.34 o -5 -9 1 177.68 153.90 3.71 o -4 -9 1 187.54 193.49 4.71 o -3 -9 1 57.41 54.09 1.70 o -2 -9 1 6.01 4.49 0.45 o -1 -9 1 100.51 87.82 2.57 o 0 -9 1 173.05 155.12 4.14 o 1 -9 1 475.32 440.55 13.53 o 2 -9 1 27.16 23.87 1.37 o 3 -9 1 55.70 57.99 2.01 o 4 -9 1 591.46 561.22 12.62 o 5 -9 1 966.22 912.61 18.76 o 6 -9 1 776.80 731.19 19.53 o 7 -9 1 294.91 300.52 10.84 o 8 -9 1 37.85 39.19 1.64 o -6 -8 1 0.09 0.45 0.21 o -5 -8 1 32.15 28.77 1.04 o -4 -8 1 24.53 21.54 1.04 o -3 -8 1 68.69 65.84 1.87 o -2 -8 1 2.76 3.58 0.73 o -1 -8 1 33.21 33.25 1.47 o 0 -8 1 35.76 38.13 3.72 o 1 -8 1 215.00 208.44 11.31 o 2 -8 1 36.14 32.07 3.76 o 3 -8 1 142.22 136.79 4.61 o 4 -8 1 170.03 165.86 4.15 o 5 -8 1 1.05 2.52 0.49 o 6 -8 1 8.79 9.57 0.95 o 7 -8 1 25.78 25.93 1.58 o 8 -8 1 43.77 48.52 2.45 o -7 -7 1 79.00 74.94 2.08 o -6 -7 1 180.72 183.70 4.14 o -5 -7 1 503.15 484.36 10.46 o -4 -7 1 2.71 1.59 0.35 o -3 -7 1 6.14 7.91 0.63 o -2 -7 1 521.46 476.97 15.96 o -1 -7 1 503.25 443.44 15.17 o 0 -7 1 53.34 40.20 3.39 o 1 -7 1 1167.56 1161.12 35.49 o 2 -7 1 897.84 835.44 21.80 o 3 -7 1 769.84 765.10 28.82 o 4 -7 1 848.29 763.38 28.64 o 5 -7 1 49.23 57.30 2.23 o 6 -7 1 569.89 608.66 18.37 o 7 -7 1 579.49 573.97 15.59 o 8 -7 1 176.33 170.76 5.44 o 9 -7 1 89.95 100.91 6.76 o -7 -6 1 64.40 58.90 1.67 o -6 -6 1 63.04 52.21 1.81 o -5 -6 1 20.43 17.53 0.90 o -4 -6 1 114.61 118.64 2.99 o -3 -6 1 32.87 33.28 3.26 o -2 -6 1 19.66 16.69 2.29 o -1 -6 1 681.74 687.94 19.06 o 0 -6 1 672.45 694.39 17.64 o 1 -6 1 630.04 644.34 16.85 o 2 -6 1 395.61 404.92 11.54 o 3 -6 1 4.24 8.72 1.72 o 4 -6 1 461.06 441.08 29.80 o 5 -6 1 475.57 445.30 12.32 o 6 -6 1 474.86 524.92 14.46 o 7 -6 1 348.53 317.61 9.19 o 8 -6 1 3.45 2.50 0.51 o 9 -6 1 22.29 15.42 1.28 o -8 -5 1 263.05 208.94 4.90 o -7 -5 1 278.44 260.02 6.23 o -6 -5 1 227.07 226.67 4.89 o -5 -5 1 296.02 301.51 6.75 o -4 -5 1 1.27 2.76 0.74 o -3 -5 1 266.52 234.05 7.81 o -2 -5 1 1363.68 1122.48 22.94 o -1 -5 1 74.82 45.06 1.78 o 0 -5 1 68.31 43.88 2.77 o 1 -5 1 3419.26 3388.24 84.46 o 2 -5 1 1258.77 1358.73 32.51 o 3 -5 1 1007.10 918.87 22.67 o 4 -5 1 535.83 515.32 14.33 o 5 -5 1 425.29 437.73 15.80 o 6 -5 1 1848.66 1690.33 55.43 o 7 -5 1 390.96 379.81 10.60 o 8 -5 1 70.21 80.61 3.12 o 9 -5 1 91.38 98.61 3.45 o -8 -4 1 52.83 58.04 1.52 o -7 -4 1 1.10 4.16 0.47 o -6 -4 1 4.95 9.72 0.65 o -5 -4 1 0.99 3.17 0.39 o -4 -4 1 16.51 17.48 2.03 o -3 -4 1 12.16 8.88 0.97 o -2 -4 1 113.56 118.29 3.14 o -1 -4 1 434.15 400.68 7.82 o 0 -4 1 13.75 8.28 0.98 o 1 -4 1 23.58 18.22 1.47 o 2 -4 1 19.82 26.61 2.00 o 3 -4 1 550.41 587.99 14.00 o 4 -4 1 12.11 15.00 2.12 o 5 -4 1 173.28 191.71 8.37 o 6 -4 1 6.95 3.80 0.59 o 7 -4 1 263.53 243.57 7.79 o 8 -4 1 50.47 49.33 2.23 o 9 -4 1 0.45 1.20 0.32 o -9 -3 1 51.36 44.21 2.81 o -8 -3 1 434.28 448.52 10.35 o -7 -3 1 32.23 37.83 1.34 o -6 -3 1 60.71 69.46 2.02 o -5 -3 1 110.45 135.18 12.58 o -4 -3 1 145.78 164.05 10.16 o -3 -3 1 1252.43 1206.90 24.62 o -2 -3 1 1062.85 981.90 18.79 o -1 -3 1 144.18 130.67 3.42 o 0 -3 1 357.03 288.34 6.55 o 1 -3 1 1473.20 1079.33 23.47 o 2 -3 1 2103.60 1864.17 39.84 o 3 -3 1 5411.22 5336.99 111.48 o 4 -3 1 1370.63 1253.94 38.75 o 5 -3 1 474.56 438.02 15.20 o 6 -3 1 1091.51 980.84 32.37 o 7 -3 1 254.20 240.19 8.96 o 8 -3 1 305.48 286.75 7.50 o 9 -3 1 175.04 162.17 5.09 o -9 -2 1 3.36 7.11 0.76 o -8 -2 1 1.99 3.53 0.48 o -7 -2 1 0.22 1.24 0.53 o -6 -2 1 0.60 0.98 0.33 o -5 -2 1 3.71 13.24 3.31 o -4 -2 1 11.84 14.91 1.13 o -3 -2 1 957.47 984.67 18.96 o -2 -2 1 724.91 716.55 13.88 o -1 -2 1 127.07 129.56 3.87 o 0 -2 1 363.78 331.29 10.51 o 1 -2 1 69.22 78.41 5.18 o 2 -2 1 315.11 345.45 8.52 o 3 -2 1 36.13 33.36 1.89 o 4 -2 1 30.97 34.95 2.40 o 5 -2 1 204.26 184.68 6.34 o 6 -2 1 335.59 269.40 21.66 o 7 -2 1 51.42 52.59 2.32 o 8 -2 1 106.47 93.78 3.95 o 9 -2 1 28.19 34.12 1.49 o -9 -1 1 119.95 147.39 6.71 o -8 -1 1 193.29 202.46 5.15 o -7 -1 1 34.53 39.52 1.42 o -6 -1 1 161.65 248.37 23.94 o -5 -1 1 380.00 680.43 23.52 o -4 -1 1 1959.72 2130.63 40.10 o -3 -1 1 1355.02 1428.32 27.01 o -2 -1 1 22.16 29.22 1.86 o -1 -1 1 2577.60 2836.65 66.17 o 1 -1 1 2316.91 2237.51 61.39 o 2 -1 1 8.74 6.57 0.96 o 3 -1 1 383.03 514.69 20.66 o 4 -1 1 1129.54 1447.98 38.09 o 5 -1 1 1606.85 1520.87 39.65 o 6 -1 1 1025.81 904.25 23.24 o 7 -1 1 27.11 32.00 1.72 o 9 -1 1 98.16 130.52 7.21 o -9 0 1 47.40 45.35 1.99 o -8 0 1 32.19 39.63 1.46 o -7 0 1 129.44 106.96 3.12 o -6 0 1 11.43 98.59 15.05 o -5 0 1 265.29 303.31 7.83 o -4 0 1 79.70 99.06 3.61 o -3 0 1 52.78 59.03 1.81 o -2 0 1 6.70 10.26 1.16 o -1 0 1 54.59 36.43 1.20 o 0 0 1 1392.06 1276.95 49.89 o 1 0 1 1526.01 1881.68 52.27 o 2 0 1 326.10 768.66 31.52 o 4 0 1 11.02 32.10 2.29 o 5 0 1 92.39 155.96 6.52 o 6 0 1 38.98 40.58 1.52 o 7 0 1 20.21 20.77 1.22 o 8 0 1 4.42 5.46 0.54 o 9 0 1 0.15 1.21 0.68 o -9 1 1 108.50 118.44 8.68 o -8 1 1 0.58 0.65 0.39 o -7 1 1 23.12 20.45 1.28 o -6 1 1 101.70 85.27 5.36 o -5 1 1 129.88 110.62 4.31 o -4 1 1 2117.74 2247.58 41.97 o -3 1 1 605.98 652.85 12.10 o -2 1 1 287.64 298.49 6.50 o -1 1 1 2606.79 2843.93 52.03 o 0 1 1 2464.87 2505.95 51.98 o 1 1 1 8156.01 7680.70 419.31 o 2 1 1 13431.86 13491.21 521.16 o 3 1 1 5230.17 5356.25 120.52 o 4 1 1 152.73 124.44 4.41 o 5 1 1 18.98 17.22 1.86 o 6 1 1 1091.39 1080.61 28.61 o 7 1 1 953.80 929.40 33.40 o 8 1 1 224.30 233.51 7.71 o 9 1 1 0.47 1.28 0.35 o -9 2 1 99.92 94.22 7.25 o -8 2 1 35.26 40.94 1.99 o -7 2 1 142.11 145.90 4.67 o -6 2 1 77.39 187.87 32.82 o -5 2 1 33.57 36.68 3.19 o -4 2 1 213.72 253.51 5.94 o -3 2 1 4.90 7.11 0.57 o -2 2 1 629.35 602.02 12.47 o -1 2 1 6447.88 6067.96 143.61 o 0 2 1 411.27 454.60 10.06 o 1 2 1 7711.90 9878.84 220.36 o 2 2 1 463.49 505.96 12.50 o 3 2 1 54.08 127.71 9.39 o 4 2 1 134.42 142.66 4.98 o 5 2 1 303.76 305.83 9.18 o 6 2 1 30.65 49.22 3.12 o 7 2 1 55.14 68.42 2.58 o 8 2 1 25.36 30.75 1.21 o -9 3 1 6.59 11.16 0.96 o -7 3 1 491.66 570.44 16.94 o -6 3 1 683.18 787.37 45.03 o -5 3 1 134.31 118.17 8.74 o -4 3 1 673.80 645.17 16.25 o -3 3 1 953.45 873.80 19.46 o -2 3 1 2660.31 2559.51 55.31 o -1 3 1 4478.07 4615.32 95.92 o 0 3 1 238.56 237.21 6.35 o 1 3 1 1696.70 1850.67 46.32 o 2 3 1 1628.77 1860.54 39.68 o 3 3 1 1066.59 1575.18 42.98 o 4 3 1 327.32 519.87 19.16 o 5 3 1 192.17 203.94 4.24 o 6 3 1 193.31 227.31 5.25 o 7 3 1 156.09 234.25 9.64 o 8 3 1 142.94 179.78 7.18 o -9 4 1 59.41 72.49 2.75 o -8 4 1 27.93 28.88 2.15 o -7 4 1 80.75 99.08 3.96 o -6 4 1 138.32 118.05 5.22 o -5 4 1 194.07 185.25 7.99 o -4 4 1 239.09 233.40 7.48 o -3 4 1 318.23 292.42 7.62 o -2 4 1 37.86 73.77 4.88 o -1 4 1 178.51 182.40 4.97 o 0 4 1 31.41 46.56 3.08 o 1 4 1 110.47 115.94 3.87 o 2 4 1 80.57 85.30 3.67 o 3 4 1 489.21 629.40 21.06 o 4 4 1 201.43 211.72 7.65 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2.52 0.46 o -3 3 12 13.16 16.79 0.97 o -2 3 12 12.23 9.88 0.74 o -1 3 12 101.76 97.02 4.43 o 0 3 12 19.38 18.10 1.00 o -3 4 12 139.36 113.98 3.48 o -2 4 12 9.77 13.20 0.86 o -1 4 12 126.49 130.16 5.51 o -2 -5 13 104.90 106.86 5.98 o -1 -5 13 143.65 159.57 4.16 o 0 -5 13 140.75 144.92 4.68 o -3 -4 13 12.13 15.04 0.93 o -2 -4 13 0.06 0.34 0.41 o -1 -4 13 21.21 17.90 1.00 o 0 -4 13 6.21 5.60 0.61 o -3 -3 13 83.55 101.58 2.69 o -2 -3 13 11.62 11.51 0.86 o -1 -3 13 122.23 129.31 3.88 o 0 -3 13 18.39 15.21 1.19 o 1 -3 13 114.98 120.16 4.39 o -4 -2 13 4.19 5.06 0.61 o -3 -2 13 3.84 8.00 0.70 o -2 -2 13 2.61 3.36 0.41 o -1 -2 13 0.33 1.78 0.34 o 0 -2 13 102.81 109.63 3.60 o 1 -2 13 14.53 15.65 1.12 o -4 -1 13 21.59 21.11 1.01 o -3 -1 13 173.63 180.73 5.61 o -2 -1 13 132.72 138.29 3.91 o -1 -1 13 23.17 30.76 1.30 o 0 -1 13 25.42 27.29 1.34 o -4 0 13 175.47 196.45 6.79 o -3 0 13 2.42 5.14 0.57 o -2 0 13 8.17 12.34 0.85 o -1 0 13 33.83 31.97 1.35 o 0 0 13 9.18 12.74 1.31 o -3 1 13 2.63 2.67 0.62 o -2 1 13 5.79 5.19 0.52 o -1 1 13 42.45 43.61 1.83 o