#------------------------------------------------------------------------------ #$Date: 2024-06-05 05:20:26 +0300 (Wed, 05 Jun 2024) $ #$Revision: 292200 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571776.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1571776 loop_ _publ_author_name 'Sobczak, Szymon' 'Katrusiak, Andrzej' _publ_section_title ; Structural insight into piezo-solvatochromism of Reichardt's dye. ; _journal_issue 4 _journal_name_full IUCrJ _journal_paper_doi 10.1107/S2052252524004603 _journal_volume 11 _journal_year 2024 _chemical_formula_moiety 'C29 H21 N O, 4(C2 H6 O), O' _chemical_formula_sum 'C37 H45 N O6' _chemical_formula_weight 599.74 _chemical_name_common ; ET(1)*4C2H5OH*H2O ; _chemical_name_systematic ; 4-(2,4,6-triphenylpyridinium-1-yl)-phenolate ethanol solvate ; _chemical_properties_physical Moisture-sensitive _space_group_crystal_system trigonal _space_group_IT_number 161 _space_group_name_Hall 'R 3 -2"c' _space_group_name_H-M_alt 'R 3 c :H' _atom_sites_solution_hydrogens mixed _audit_creation_date 2024-02-15 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2024-02-20 deposited with the CCDC. 2024-02-20 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 18 _cell_length_a 23.645(8) _cell_length_b 23.645(8) _cell_length_c 30.91(2) _cell_measurement_reflns_used 654 _cell_measurement_temperature 293.00 _cell_measurement_theta_max 26.372 _cell_measurement_theta_min 2.4680 _cell_volume 14966(12) _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.778 _diffrn_measured_fraction_theta_max 0.363 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'New Xcalibur, EosS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.2296 _diffrn_reflns_av_unetI/netI 0.5157 _diffrn_reflns_Laue_measured_fraction_full 0.778 _diffrn_reflns_Laue_measured_fraction_max 0.363 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -28 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 5030 _diffrn_reflns_point_group_measured_fraction_full 0.731 _diffrn_reflns_point_group_measured_fraction_max 0.294 _diffrn_reflns_theta_full 25.400 _diffrn_reflns_theta_max 26.372 _diffrn_reflns_theta_min 3.303 _exptl_absorpt_coefficient_mu 0.080 _exptl_absorpt_correction_T_max 0.992 _exptl_absorpt_correction_T_min 0.981 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear red' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.198 _exptl_crystal_description block _exptl_crystal_F_000 5796 _exptl_crystal_preparation 'crystallized in DAC,solvatochromic' _exptl_crystal_recrystallization_method 'crystallized at high pressure' _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.14 _refine_diff_density_max 0.240 _refine_diff_density_min -0.219 _refine_diff_density_rms 0.053 _refine_ls_abs_structure_details ; Flack x determined using 125 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -5.4(10) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 0.952 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 361 _refine_ls_number_reflns 2002 _refine_ls_number_restraints 462 _refine_ls_restrained_S_all 0.873 _refine_ls_R_factor_all 0.3771 _refine_ls_R_factor_gt 0.1248 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1651P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2723 _refine_ls_wR_factor_ref 0.4036 _reflns_Friedel_coverage 0.612 _reflns_Friedel_fraction_full 0.684 _reflns_Friedel_fraction_max 0.223 _reflns_number_gt 504 _reflns_number_total 2002 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file lt5066.cif _cod_data_source_block et1_ethanol_0_76gpa _cod_original_cell_volume 14968(16) _cod_original_sg_symbol_H-M 'R 3 c' _cod_database_code 1571776 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.989 _shelx_estimated_absorpt_t_min 0.969 _exptl_absorpt_special_details ; Data were collected at room temperature (295(2) K) and pressure of 0.76(2) GPa (760000 kPa). ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2. Restrained distances O1-H2E_$1 1.85 with sigma of 0.05 H4E_$2-O1 1.9 with sigma of 0.1 H2E-O2E 0.89 with sigma of 0.005 O2E-H1E 1.9 with sigma of 0.02 H4E-O4E 0.89 with sigma of 0.01 O4E-H4E 0.89 with sigma of 0.01 H4E-C8E 1.8 with sigma of 0.02 H3E-O4E 1.9 with sigma of 0.05 O4E-C8E \\sim O3E-C6E \\sim O2E-C3E \\sim O1E-C2E with sigma of 0.02 C8'-C1' \\sim C4-C3 \\sim C8-C1 with sigma of 0.02 O4E-C7E \\sim O3E-C5E \\sim O2E-C4E \\sim O1E-C1E with sigma of 0.02 C7-C2 \\sim C7-C2' with sigma of 0.02 C17-C1 \\sim C17-C1' with sigma of 0.02 C14-C1' \\sim C14-C1 with sigma of 0.02 C4-C2' \\sim C4-C2 with sigma of 0.02 C2E-C1E \\sim C4E-C3E \\sim C6E-C5E \\sim C8E-C7E with sigma of 0.02 O1-C16' \\sim O1-C16 with sigma of 0.02 C2'-C1' \\sim C3-C2' \\sim C3-C2 \\sim C2-C1 with sigma of 0.02 N1-C1 \\sim N1-C1' with sigma of 0.02 3. Restrained planarity C5, H5, C4, C5', H5', C6', H6', C7, H7, C6, H6, C3 with sigma of 0.1 4. Rigid bond restraints C4E, C3E, O2E with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 C7E, C8E, O4E with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 C5E, C6E, O3E with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 C1E, C2E, O1E with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 C5, C4, C5', C6', C6, C7 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 5. Uiso/Uaniso restraints and constraints O2E \\sim C3E \\sim C4E: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A O4E \\sim C8E \\sim C7E: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A C5E \\sim C6E \\sim O3E: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A O1E \\sim C2E \\sim C1E: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A C5' \\sim C6 \\sim C7 \\sim C4 \\sim C6' \\sim C5: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A Uanis(O2E) \\sim Ueq, Uanis(C6E) \\sim Ueq, Uanis(C2') \\sim Ueq, Uanis(C7) \\sim Ueq, Uanis(C8') \\sim Ueq, Uanis(C13') \\sim Ueq, Uanis(C5E) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C10') \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O4E) \\sim Ueq, Uanis(C8E) \\sim Ueq, Uanis(C7E) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04 6. Rigid body (RIGU) restrains C13, C3, C2, C2', C4, C1, C1', C5, C5', N1, C8, C8', C6, C6', C14, C9, C13', C9', C7, C15', C15, C12, C10, C12', C10', C16', C16, C11, C11', C17, O1 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 O4E, C8E, C7E with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C4E, C3E, O2E with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 O2E, C3E, C4E with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C8E, C7E, O4E with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C1E, O1E, C2E with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C2E, O1E, C1E with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 O3E, C6E, C5E with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 7. Others Fixed Sof: O1W(0.333333) 8.a Secondary CH2 refined with riding coordinates: C3E(H3EA,H3EB), C2E(H2EA,H2EB), C6E(H6EA,H6EB), C8E(H8EA,H8EB) 8.b Aromatic/amide H refined with riding coordinates: C2'(H2'), C2(H2), C13'(H13'), C9'(H9'), C10'(H10'), C11'(H11'), C12'(H12'), C15'(H15'), C16'(H16'), C16(H16), C15(H15), C13(H13), C12(H12), C11(H11), C10(H10), C9(H9), C5(H5), C5'(H5'), C6'(H6'), C7(H7), C6(H6) 8.c Fitted hexagon refined as free rotating group: C13'(C8',C9',C10',C11',C12'), C15'(C16',C17,C16,C15,C14), C8(C13,C12,C11,C10, C9), C5(C4,C5',C6',C7,C6) 8.d Idealised Me refined as rotating group: C1E(H1EA,H1EB,H1EC), C4E(H4EA,H4EB,H4EC), C5E(H5EA,H5EB,H5EC), C7E(H7EA,H7EB, H7EC) 8.e Idealised tetrahedral OH refined as rotating group: O1E(H1E), O3E(H3E) ; _shelx_res_file ; TITL et_etanol_0_76_3 in R3c #161 et1_ethanol_0_76gpa.res created by SHELXL-2018/3 at 16:45:08 on 19-Feb-2024 REM Best SHELXD solution FINAL CC 70.12 REM Fragments: 103 CELL 0.71073 23.644525 23.644525 30.914719 90 90 120 ZERR 18 0.008433 0.008433 0.024719 0 0 0 LATT -3 SYMM -Y,+X-Y,+Z SYMM +Y-X,-X,+Z SYMM +Y-X,+Y,0.5+Z SYMM +X,+X-Y,0.5+Z SYMM -Y,-X,0.5+Z SFAC C H N O UNIT 666 810 18 108 EQIV $1 0.333-Y,0.667-X,0.167+Z EQIV $2 -0.333+Y-X,0.333+Y,-0.167+Z DFIX 1.85 0.05 O1 H2E_$1 ISOR 0.01 0.02 O2E C6E C2' C7 C8' C13' C5E RIGU C13 C3 C2 C2' C4 C1 C1' C5 C5' N1 C8 C8' C6 C6' C14 C9 C13' C9' C7 = C15' C15 C12 C10 C12' C10' C16' C16 C11 C11' C17 O1 RIGU O4E C8E C7E SADI O4E C8E O3E C6E O2E C3E O1E C2E SADI C8' C1' C4 C3 C8 C1 SADI O4E C7E O3E C5E O2E C4E O1E C1E SADI C7 C2 C7 C2' RIGU C4E C3E O2E SADI C17 C1 C17 C1' RIGU O2E C3E C4E SADI C14 C1' C14 C1 SIMU O2E C3E C4E SADI C4 C2' C4 C2 RIGU C8E C7E O4E FLAT C5 H5 C4 C5' H5' C6' H6' C7 H7 C6 H6 C3 DFIX 1.9 0.1 H4E_$2 O1 DELU C4E C3E O2E DFIX 0.89 0.005 H2E O2E SIMU O4E C8E C7E DFIX 1.9 O2E H1E DELU C7E C8E O4E RIGU C1E O1E C2E SADI C2E C1E C4E C3E C6E C5E C8E C7E SADI O1 C16' O1 C16 RIGU C2E O1E C1E RIGU O3E C6E C5E DELU C5E C6E O3E SIMU C5E C6E O3E DELU C1E C2E O1E SIMU O1E C2E C1E ISOR 0.01 0.02 C10' DFIX 0.89 0.01 H4E O4E ISOR 0.02 0.04 O4E C8E C7E DFIX 0.89 0.01 O4E H4E DFIX 1.8 H4E C8E DFIX 1.9 0.05 H3E O4E SADI C2' C1' C3 C2' C3 C2 C2 C1 SADI N1 C1 N1 C1' SIMU C5' C6 C7 C4 C6' C5 DELU C5 C4 C5' C6' C6 C7 L.S. 85 PLAN 11 SIZE 0.14 0.2 0.4 CONF FREE O4E C7E FREE O1 C16' FREE O1 C16 FREE C17 C1' FREE C17 C1 FREE C4 C2 FREE C4 C2' FREE C14 C1 FREE C14 C1' FREE C6' C2' FREE C7 C2' FREE C7 C2 FREE C6 C2 FREE O1E C1E FREE O2E C4E FREE O3E C5E MORE -1 BOND $H fmap 2 53 acta 30 OMIT -17 19 -6 OMIT -17 20 -4 OMIT -14 25 -9 OMIT -12 14 10 OMIT -12 28 11 OMIT -11 11 -16 OMIT -10 12 14 OMIT -9 15 21 OMIT -8 9 10 OMIT -8 10 6 OMIT -8 19 -15 OMIT -6 8 16 OMIT -5 9 -2 OMIT -5 9 16 OMIT -5 19 0 OMIT -4 5 0 OMIT -4 11 -3 OMIT -4 15 -19 OMIT -4 15 14 OMIT -3 4 -4 OMIT -3 5 1 OMIT -3 11 -2 OMIT -2 3 -5 OMIT -2 4 -3 OMIT -2 4 3 OMIT -2 5 -1 OMIT -1 3 2 OMIT -1 5 0 OMIT -1 17 0 REM REM REM WGHT 0.167000 EXTI 0.000374 FVAR 0.33096 N1 3 -0.002328 0.478033 0.118201 11.00000 0.06546 0.07008 = 0.07505 0.01177 0.00262 0.04546 C1' 1 -0.024110 0.438471 0.154625 11.00000 0.07008 0.04718 = 0.04790 -0.01863 -0.02579 0.02307 C2' 1 -0.024341 0.380688 0.150633 11.00000 0.07269 0.06130 = 0.07388 0.00589 -0.00939 0.03934 AFIX 43 H2' 2 -0.042456 0.350714 0.173107 11.00000 -1.20000 AFIX 0 C3 1 0.000454 0.363622 0.115542 11.00000 0.10214 0.07523 = 0.08559 0.00228 0.00340 0.05405 C2 1 0.030073 0.407572 0.082008 11.00000 0.06897 0.05703 = 0.07683 -0.01398 -0.01562 0.03378 AFIX 43 H2 2 0.045848 0.397287 0.057460 11.00000 -1.20000 AFIX 0 C1 1 0.034664 0.468093 0.087472 11.00000 0.07430 0.04440 = 0.08219 -0.00987 0.00629 0.02090 AFIX 66 C13' 1 -0.054591 0.438781 0.226323 11.00000 0.08012 0.06678 = 0.06841 0.00335 0.00387 0.03318 AFIX 43 H13' 2 -0.022554 0.427889 0.231899 11.00000 -1.20000 AFIX 65 C8' 1 -0.063699 0.454235 0.184478 11.00000 0.06564 0.05489 = 0.06664 -0.00323 -0.00414 0.02227 C9' 1 -0.111581 0.470514 0.176144 11.00000 0.08549 0.05489 = 0.09266 0.00961 0.00912 0.03816 AFIX 43 H9' 2 -0.117674 0.480854 0.148147 11.00000 -1.20000 AFIX 65 C10' 1 -0.150356 0.471339 0.209655 11.00000 0.08709 0.09319 = 0.09261 -0.00595 0.00574 0.04191 AFIX 43 H10' 2 -0.182392 0.482231 0.204079 11.00000 -1.20000 AFIX 65 C11' 1 -0.141248 0.455885 0.251501 11.00000 0.11521 0.09426 = 0.07827 -0.04016 -0.01044 0.05334 AFIX 43 H11' 2 -0.167191 0.456438 0.273922 11.00000 -1.20000 AFIX 65 C12' 1 -0.093366 0.439606 0.259836 11.00000 0.10763 0.03365 = 0.07545 -0.00752 0.01478 0.02337 AFIX 43 H12' 2 -0.087273 0.429266 0.287833 11.00000 -1.20000 AFIX 0 O1 4 0.005807 0.716278 0.119103 11.00000 0.18328 0.05704 = 0.11118 0.02535 0.00987 0.07330 AFIX 66 C15' 1 -0.028412 0.556663 0.086978 11.00000 0.10421 0.04835 = 0.10156 0.00074 -0.03092 0.03847 AFIX 43 H15' 2 -0.048425 0.527031 0.064529 11.00000 -1.20000 AFIX 65 C16' 1 -0.029767 0.614756 0.087579 11.00000 0.08842 0.04461 = 0.09819 0.02169 0.00625 0.02907 AFIX 43 H16' 2 -0.050686 0.623992 0.065532 11.00000 -1.20000 AFIX 65 C17 1 0.000145 0.659045 0.121131 11.00000 0.09785 0.04179 = 0.11053 0.01633 -0.00107 0.03252 C16 1 0.031412 0.645242 0.154082 11.00000 0.14415 0.08513 = 0.10420 -0.00261 -0.01468 0.07716 AFIX 43 H16 2 0.051425 0.674874 0.176531 11.00000 -1.20000 AFIX 65 C15 1 0.032767 0.587149 0.153482 11.00000 0.06452 0.06739 = 0.04367 0.02225 0.03689 0.04059 AFIX 43 H15 2 0.053687 0.577914 0.175529 11.00000 -1.20000 AFIX 65 C14 1 0.002855 0.542859 0.119930 11.00000 0.07253 0.07431 = 0.05762 0.01480 0.01882 0.04678 AFIX 66 C8 1 0.062304 0.508205 0.047616 11.00000 0.06654 0.04480 = 0.08419 -0.00848 0.00966 0.04172 C13 1 0.050824 0.486942 0.004921 11.00000 0.12982 0.07733 = 0.08229 -0.01128 0.01955 0.04383 AFIX 43 H13 2 0.019347 0.444097 -0.001441 11.00000 -1.20000 AFIX 65 C12 1 0.086391 0.529715 -0.028265 11.00000 0.12285 0.11626 = 0.07980 -0.00406 -0.00345 0.00246 AFIX 43 H12 2 0.078710 0.515489 -0.056831 11.00000 -1.20000 AFIX 65 C11 1 0.133438 0.593752 -0.018756 11.00000 0.04662 0.10439 = 0.07837 -0.00802 0.03342 0.02594 AFIX 43 H11 2 0.157234 0.622370 -0.040960 11.00000 -1.20000 AFIX 65 C10 1 0.144919 0.615016 0.023938 11.00000 0.08878 0.04827 = 0.07887 0.00468 0.01088 0.03335 AFIX 43 H10 2 0.176397 0.657860 0.030300 11.00000 -1.20000 AFIX 65 C9 1 0.109353 0.572243 0.057124 11.00000 0.10235 0.03518 = 0.08167 0.00013 0.02155 0.04104 AFIX 43 H9 2 0.117034 0.586469 0.085690 11.00000 -1.20000 AFIX 66 C5 1 0.048727 0.293293 0.095791 11.00000 0.11013 0.07299 = 0.11329 0.00237 0.03567 0.05490 AFIX 43 H5 2 0.083826 0.329442 0.083058 11.00000 -1.20000 AFIX 65 C4 1 -0.000611 0.299540 0.115655 11.00000 0.06890 0.07492 = 0.09904 0.01370 0.01322 0.04365 C5' 1 -0.053071 0.245511 0.134685 11.00000 0.08859 0.07028 = 0.13246 0.01862 0.02537 0.04386 AFIX 43 H5' 2 -0.086081 0.249691 0.147976 11.00000 -1.20000 AFIX 65 C6' 1 -0.056193 0.185235 0.133852 11.00000 0.10237 0.07582 = 0.10247 0.01673 0.00665 0.05324 AFIX 43 H6' 2 -0.091292 0.149086 0.146585 11.00000 -1.20000 AFIX 65 C7 1 -0.006856 0.178987 0.113989 11.00000 0.10207 0.07256 = 0.09409 0.00043 -0.00460 0.05199 AFIX 43 H7 2 -0.008946 0.138658 0.113431 11.00000 -1.20000 AFIX 65 C6 1 0.045604 0.233015 0.094958 11.00000 0.14408 0.07662 = 0.11243 -0.00507 0.04496 0.06433 AFIX 43 H6 2 0.078613 0.228835 0.081667 11.00000 -1.20000 AFIX 0 O1E 4 -0.139443 0.401728 0.078385 11.00000 0.08916 0.16443 = 0.23913 -0.00417 0.01655 0.08028 AFIX 147 H1E 2 -0.115119 0.395675 0.062577 11.00000 -1.50000 AFIX 0 C1E 1 -0.216235 0.434577 0.073744 11.00000 0.08425 0.27894 = 0.29473 -0.07601 -0.02283 0.12333 AFIX 137 H1EA 2 -0.263081 0.410312 0.072696 11.00000 -1.50000 H1EB 2 -0.200642 0.475522 0.059087 11.00000 -1.50000 H1EC 2 -0.202126 0.442456 0.103351 11.00000 -1.50000 AFIX 0 C3E 1 -0.133588 0.282731 0.043297 11.00000 0.20038 0.20963 = 0.17658 -0.01117 0.00374 0.05751 AFIX 23 H3EA 2 -0.104426 0.267777 0.053353 11.00000 -1.20000 H3EB 2 -0.152097 0.292239 0.068362 11.00000 -1.20000 AFIX 0 C2E 1 -0.191300 0.398851 0.053524 11.00000 0.06177 0.16091 = 0.24078 -0.04320 -0.00392 0.04538 AFIX 23 H2EA 2 -0.225655 0.353737 0.050341 11.00000 -1.20000 H2EB 2 -0.175507 0.416518 0.024902 11.00000 -1.20000 AFIX 0 O2E 4 -0.098318 0.340030 0.017781 11.00000 0.20865 0.17382 = 0.18363 -0.02958 0.01278 0.06722 H2E 2 -0.062118 0.339938 0.009949 11.00000 -1.50000 C4E 1 -0.183591 0.234061 0.018173 11.00000 0.16312 0.17420 = 0.21657 -0.01022 -0.01473 0.08107 AFIX 137 H4EA 2 -0.219554 0.205892 0.036508 11.00000 -1.50000 H4EB 2 -0.167516 0.208976 0.003709 11.00000 -1.50000 H4EC 2 -0.197948 0.253982 -0.002905 11.00000 -1.50000 AFIX 0 C6E 1 0.196495 0.583652 0.169805 11.00000 0.15715 0.16775 = 0.16629 -0.00435 -0.00099 0.08202 AFIX 23 H6EA 2 0.215887 0.573152 0.145703 11.00000 -1.20000 H6EB 2 0.218408 0.582682 0.196084 11.00000 -1.20000 AFIX 0 O3E 4 0.129287 0.536727 0.172559 11.00000 0.14482 0.18088 = 0.21452 0.00118 -0.05639 0.08123 AFIX 147 H3E 2 0.120784 0.521399 0.197055 11.00000 -1.50000 AFIX 0 C5E 1 0.205052 0.646052 0.164037 11.00000 0.21269 0.17611 = 0.19153 0.01459 0.01103 0.09635 AFIX 137 H5EA 2 0.244654 0.677608 0.178015 11.00000 -1.50000 H5EB 2 0.168709 0.647753 0.176439 11.00000 -1.50000 H5EC 2 0.207673 0.655681 0.133692 11.00000 -1.50000 AFIX 0 C8E 1 0.138957 0.403235 0.200448 11.00000 0.18506 0.21557 = 0.20046 0.00953 0.02459 0.10119 AFIX 23 H8EA 2 0.136992 0.395322 0.169549 11.00000 -1.20000 H8EB 2 0.120265 0.361553 0.215264 11.00000 -1.20000 AFIX 0 C7E 1 0.204052 0.443529 0.213416 11.00000 0.22103 0.25845 = 0.24550 -0.00618 -0.04302 0.11440 AFIX 137 H7EA 2 0.205053 0.458165 0.242519 11.00000 -1.50000 H7EB 2 0.224879 0.480596 0.194484 11.00000 -1.50000 H7EC 2 0.226735 0.419379 0.212112 11.00000 -1.50000 AFIX 0 O4E 4 0.103005 0.435514 0.211013 11.00000 0.22704 0.22287 = 0.20461 0.07350 0.08846 0.12682 H4E 2 0.103118 0.432556 0.239730 11.00000 -1.50000 O2W 4 0.333333 0.666667 0.055157 10.33333 0.27446 O3W 4 -0.333333 0.333333 -0.044460 10.33333 0.39701 O1W 4 -0.299470 0.358740 0.169787 10.33333 0.07559 HKLF 4 REM et_etanol_0_76_3 in R3c #161 REM wR2 = 0.4050, GooF = S = 0.950, Restrained GooF = 0.867 for all data REM R1 = 0.1237 for 504 Fo > 4sig(Fo) and 0.3825 for all 2002 data REM 361 parameters refined using 510 restraints END WGHT 0.1666 0.0000 REM Highest difference peak 0.251, deepest hole -0.229, 1-sigma level 0.052 Q1 1 0.0027 0.7349 0.1205 11.00000 0.05 0.25 Q2 1 -0.2029 0.3291 -0.0486 11.00000 0.05 0.22 Q3 1 0.1001 0.3968 0.0880 11.00000 0.05 0.20 Q4 1 -0.2878 0.3363 -0.0562 11.00000 0.05 0.18 Q5 1 -0.3333 0.3813 -0.0481 11.00000 0.05 0.18 Q6 1 -0.0731 0.4919 0.0358 11.00000 0.05 0.17 Q7 1 -0.2341 0.4746 0.0466 11.00000 0.05 0.17 Q8 1 -0.0384 0.4788 0.0711 11.00000 0.05 0.15 Q9 1 -0.1827 0.5173 0.1626 11.00000 0.05 0.15 Q10 1 -0.1109 0.2995 0.1609 11.00000 0.05 0.15 Q11 1 -0.2494 0.3880 0.0922 11.00000 0.05 0.15 ; _shelx_res_checksum 20220 _shelx_hkl_file ; 2 -2 4 1395.22 235.011 3 0 3 -6 2472.30 730.419 4 0 3 -6 2252.25 737.828 16 0 3 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1183.46 349.307 16 -1 4 -5 1621.24 451.148 4 -1 4 -5 1248.42 345.442 16 -4 1 -2 127.598 128.999 4 -1 4 -2-56.2491 66.8908 7 -4 1 1 118.082 51.4574 5 4 -3 1 85.8152 64.5229 8 4 -3 1 207.730 127.743 3 4 -3 1 94.6818 52.2291 1 4 -3 4 475.014 243.768 8 3 -4 4 718.475 199.088 6 3 -4 4 509.619 129.389 3 4 -3 4 515.568 164.884 3 -3 -1 4 546.137 155.819 12 4 -3 4 774.494 349.923 6 3 -4 7 155.928 160.071 3 3 -4 7 534.839 199.971 6 -2 4 -6 1057.20 745.572 4 2 2 -6 1795.43 1172.91 16 -2 4 -3 1115.79 311.053 7 -2 4 -3 1074.29 221.325 2 -4 2 -3 776.619 360.059 4 -4 2 0 420.241 142.492 5 -4 2 0 346.099 153.982 12 4 -2 0 468.722 147.989 8 4 -2 0 533.891 149.262 3 2 -4 3 1174.81 239.090 3 4 -2 3 1044.20 209.611 3 2 -4 3 1404.73 393.920 1 4 -2 3 776.891 295.557 8 2 -4 3 911.979 317.519 6 2 -4 6 464.112 646.027 6 2 -4 6 9.28336 27.9708 3 -3 4 -7 34.6310 198.737 4 3 1 -4 642.838 211.494 9 -3 4 -4 464.683 168.334 4 -3 4 -4 508.177 161.003 5 -4 3 -4 334.324 118.584 5 3 1 -4 212.969 158.852 16 -3 4 -4 593.456 167.062 2 -4 3 -4-2.77634 551.913 4 -3 4 -4 270.788 110.298 7 4 -1 -1 70.7669 89.8372 8 -4 3 -1 117.184 82.7201 5 -4 3 -1 161.433 83.1026 2 -3 4 -1 90.5646 33.1254 7 -3 4 -1 136.498 105.935 2 -4 3 -1 152.881 114.825 4 4 -1 -1 138.301 93.1071 9 4 -1 2 21.6960 34.0652 3 1 -4 5 1995.96 300.662 3 1 -4 5 2284.93 635.387 6 -1 -3 5 2976.52 676.468 6 1 -4 8 3190.60 825.506 6 1 -4 8 2032.34 323.949 3 -4 4 -8 4050.01 1248.51 4 -4 4 -5 784.615 768.635 4 -4 4 -5 284.875 271.068 5 4 0 -5 1010.15 1119.31 16 -4 4 -2 19831.2 980.391 5 4 0 -2 24811.1 2372.51 16 -4 4 -2 21609.8 1107.53 2 -4 4 -2 21365.1 1394.99 4 4 0 -2 22141.1 1375.61 9 0 -4 4 32977.6 2026.30 6 0 -4 7 125.547 200.593 6 0 -4 7-0.88767 35.0785 3 0 5 -11-15.1187 376.139 4 0 5 -11 163.310 781.786 16 0 5 -8-225.204 275.769 16 0 5 -5-67.8496 101.040 2 0 5 -5-76.9211 96.9284 7 0 5 -2 63727.2 2802.52 7 -5 0 1 298.255 226.523 5 5 -5 1 115.075 383.786 1 5 -5 1 22.4204 142.658 8 5 -5 4 5068.44 704.594 8 5 -5 4 5134.77 851.152 6 5 -5 4 3335.07 778.452 1 -5 0 4 5437.77 687.426 12 5 -5 4 4604.87 597.527 3 5 -5 7 205.003 348.499 6 5 -5 10 1183.17 355.530 3 -1 5 -9 620.610 612.964 16 -1 5 -9 763.720 315.118 4 1 4 -9 899.944 277.079 9 1 4 -9 299.594 500.320 4 1 4 -9 366.458 482.445 16 1 4 -6 11816.6 968.070 4 1 4 -6 13555.1 1389.56 7 -1 5 -6 9744.56 1706.34 16 1 4 -6 9702.26 1759.15 16 -1 5 -6 10848.9 1125.57 4 1 4 -6 11971.5 944.926 9 -1 5 -3 2757.90 399.479 2 -5 1 -3 2917.92 1050.95 4 1 4 -3 2344.71 497.844 7 -1 5 -3 2020.28 465.336 7 -5 1 0 16.5425 214.530 5 5 -4 0 122.653 60.5078 8 5 -4 0 251.533 206.309 1 -5 1 0-237.953 365.940 4 5 -4 3 8707.62 1070.87 6 -4 -1 3 9145.33 632.761 5 5 -4 3 6295.33 1314.12 1 5 -4 3 8994.12 793.520 3 4 -5 3 9562.48 787.460 8 5 -4 3 9316.26 994.222 8 4 -5 3 9127.04 1287.65 1 4 -5 3 8189.64 832.869 3 5 -4 6 37.5304 73.2907 3 5 -4 6-38.5938 137.095 6 4 -5 6 67.4446 79.2976 3 4 -5 6 24.9283 251.578 6 4 -5 9 5207.85 1143.13 6 4 -5 9 3313.38 537.387 3 -2 5 -10 345.988 272.219 16 -2 5 -10 213.995 284.436 4 -2 5 -7 1541.24 681.829 16 2 3 -7 1705.96 874.348 16 2 3 -7 2254.71 422.978 9 -2 5 -4 19373.8 1590.20 7 2 3 -4 21865.0 1442.19 7 2 3 -4 17891.9 2711.52 16 2 3 -4 18027.7 1335.14 9 -5 2 -4 18326.4 1134.45 2 -2 5 -4 22443.1 1122.89 2 -2 5 -4 18076.5 1287.64 4 5 -3 -1 9.16104 54.7896 9 -5 2 -1-42.8284 146.464 5 5 -3 -1 1.43822 50.5757 8 -5 2 -1-225.408 180.515 4 5 -3 2 16899.7 1199.53 9 5 -3 2 14732.9 886.017 3 5 -3 2 14775.8 1188.32 8 3 -5 2 20487.0 1610.31 1 5 -3 2 15263.6 1142.40 6 -3 -2 5 1767.24 379.939 6 3 -5 5 1591.75 296.495 3 -3 -2 5 1419.72 291.693 12 3 -5 5 1332.90 468.300 6 5 -3 5 1459.19 296.924 3 3 -5 8 964.959 265.549 3 3 -5 8 1432.11 470.035 6 -3 5 -8 607.045 292.112 16 3 2 -8 902.033 613.643 16 -3 5 -8 970.657 574.562 4 3 2 -5 1897.80 419.087 9 3 2 -5 2296.77 1185.15 16 -3 5 -5 1563.04 275.483 5 -3 5 -5 1607.65 351.488 2 -5 3 -5 1507.41 768.808 4 -3 5 -5 1161.94 458.425 7 -3 5 -5 1175.80 518.221 4 -3 5 -2 13780.1 951.703 2 -5 3 -2 14462.4 1034.66 5 5 -2 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120.633 5 8 -6 2 583.187 284.023 8 8 -6 5 351.626 220.655 8 6 -8 5-63.9654 578.961 1 8 -6 5 556.630 248.476 3 8 -6 5 753.971 446.505 6 6 -8 5 509.928 216.964 8 8 -6 8 5161.74 1258.32 6 6 -8 8 3551.31 673.102 3 6 -8 8 3547.87 996.155 6 -6 -2 8 3323.82 740.283 6 8 -6 8 3608.58 640.849 3 6 -8 11 3736.21 1378.91 6 6 -8 11 1459.79 464.798 3 6 -8 14 814.716 416.599 6 -3 8 -14-3.55996 126.929 5 -3 8 -14 581.909 270.517 4 -3 8 -11 994.002 295.632 5 3 5 -11 2236.42 1674.65 16 3 5 -11 980.185 377.426 9 -3 8 -11 1772.68 936.475 4 3 5 -8 2062.45 590.170 9 3 5 -8 1478.43 1016.59 16 -8 3 -5 4045.62 1254.77 4 -3 8 -5 3557.53 568.197 2 3 5 -5 2935.42 625.794 7 -3 8 -5 2817.02 745.190 7 -8 3 -5 3077.87 546.443 2 -8 3 -5 2198.64 574.121 5 8 -5 -2-65.2751 69.8762 9 -8 3 -2-48.3414 163.633 5 8 -5 -2 70.7324 121.655 8 -8 3 -2-151.162 245.128 4 8 -5 1 39.9560 171.086 9 -8 3 1 146.652 116.187 12 -8 3 1-19.7325 33.7459 5 8 -5 1 31.9998 70.0058 8 -8 3 1 83.6656 78.7109 2 8 -5 1 42.0568 201.343 1 8 -5 4 460.873 331.626 6 8 -5 4 366.357 353.210 8 8 -5 4 202.431 192.484 3 5 -8 4 848.868 661.470 1 5 -8 4 554.466 231.207 8 -5 -3 4 420.042 184.235 5 5 -8 7 352.500 205.593 3 8 -5 7 501.076 411.566 6 -5 -3 7 254.263 101.866 12 -5 -3 7 189.777 62.6416 6 5 -8 7 233.166 446.555 6 5 -8 10 1368.73 211.755 3 -5 -3 10 1835.85 702.166 6 5 -8 10 912.772 637.142 6 5 -8 13 60.7581 106.140 3 5 -8 13-405.876 801.072 6 -4 8 -12-169.980 510.830 16 4 4 -12 69.9743 195.459 9 -4 8 -12 81.4482 50.2623 5 4 4 -12-305.829 1031.08 16 -4 8 -9 238.947 271.650 16 -4 8 -9 29.7444 268.830 7 -4 8 -9 236.471 139.268 5 4 4 -9 192.067 202.605 9 4 4 -9 41.7703 541.418 16 -4 8 -6 723.720 423.600 7 4 4 -6 1071.84 402.196 7 -4 8 -6 969.790 287.056 2 4 4 -6 463.096 203.209 9 -8 4 -6 762.254 443.053 5 -8 4 -6 899.724 884.774 4 -8 4 -3 2879.26 769.334 4 -4 8 -3 2812.04 550.372 2 -8 4 -3 3411.82 674.821 5 4 4 -3 2642.08 552.081 7 8 -4 -3 2835.26 599.392 9 -4 8 -3 2596.81 730.075 7 8 -4 -3 3555.18 596.171 8 8 -4 0 142.579 239.334 16 -8 4 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156.205 9 8 -1 -6 2441.13 647.694 9 8 -1 -6 1143.80 1088.34 16 7 1 -6 2475.89 1044.10 16 -7 8 -6 2739.12 710.863 7 -8 7 -6 1864.94 381.992 12 -7 8 -6 2987.27 572.780 2 -8 7 -6 2882.72 697.421 7 7 1 -6 2319.88 486.518 8 -7 8 -6 2493.39 474.800 5 7 1 -6 2304.29 638.806 9 8 -1 -6 2784.31 538.275 8 -8 7 -6 2738.57 562.374 5 -8 7 -6 3513.64 722.114 2 7 1 -3 145.921 180.779 8 -8 7 -3-114.213 187.499 7 -7 8 -3-58.3106 78.1695 2 -7 8 -3-93.9549 177.827 7 8 -1 -3-183.156 286.407 9 8 -1 -3 25.7652 109.195 16 -8 7 -3 35.1486 90.4225 2 7 1 -3-109.320 200.180 9 -8 7 0 26.4361 130.508 2 8 -1 0 167.897 104.525 3 7 1 0 196.266 118.383 3 8 -1 3 2521.34 423.264 3 1 -8 6 896.744 427.031 1 -1 -7 6 542.914 266.315 1 -1 -7 9 4888.39 581.020 3 1 -8 9 3191.37 774.739 6 -1 -7 9 3566.55 943.732 6 1 -8 9 4639.94 652.302 3 1 -8 12 453.258 323.380 6 1 -8 12-17.9607 212.575 3 -1 -7 12 208.702 183.300 3 -1 -7 12-42.0300 399.364 6 1 -8 15 304.456 96.6838 3 -1 -7 15-154.976 518.695 6 1 -8 15 397.267 461.127 6 -8 8 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402.217 1 9 -6 3 161.182 40.8132 9 9 -6 3 305.117 171.424 3 9 -6 6 181.598 202.797 3 9 -6 6 29.1002 247.107 6 6 -9 6 294.588 202.689 8 9 -6 9 66.3798 262.642 8 6 -9 9 1130.63 564.426 3 6 -9 9 2229.56 1553.84 6 -6 -3 9 1700.71 683.846 6 9 -6 9 71.5921 922.210 6 6 -9 9 974.866 736.187 8 -6 -3 12 2763.38 833.399 6 6 -9 12 3865.24 1333.24 6 6 -9 12 2425.26 617.048 3 6 -9 15 1636.20 583.482 6 6 -9 15 703.323 318.316 3 4 5 -13 46.1292 118.764 9 4 5 -13 245.735 580.829 16 -4 9 -13 241.124 443.149 4 4 5 -13 40.7784 69.0408 4 -4 9 -13 38.6699 102.601 5 4 5 -10 1900.79 2159.13 16 -4 9 -10 204.750 440.125 4 4 5 -10 503.317 379.494 4 -4 9 -10 343.602 490.472 7 4 5 -10 408.369 414.949 9 4 5 -7 2017.65 598.263 7 -9 4 -7 1377.37 486.886 5 -9 4 -7 579.026 590.241 4 -4 9 -7 1789.55 474.296 2 -9 4 -4 1252.44 436.518 5 -4 9 -4 622.339 300.054 7 -4 9 -4 1176.67 365.176 2 9 -5 -1 4930.67 789.597 8 9 -5 -1 5929.71 867.193 9 -9 4 -1 6328.66 769.238 2 9 -5 -1 4889.09 1210.78 16 9 -5 -1 4844.63 1094.71 1 9 -5 2-31.9735 90.9226 16 9 -5 2-39.5367 131.368 3 -9 4 2-12.0685 51.7716 2 9 -5 2-31.7461 123.126 9 5 -9 5 3585.76 1067.88 1 9 -5 5 2677.65 531.149 3 9 -5 5 3059.06 711.393 6 -5 -4 5 2933.64 417.138 5 5 -9 5 3233.87 512.020 8 5 -9 8 791.601 289.750 8 5 -9 8 1112.51 326.053 3 5 -9 8 445.382 862.674 6 -5 -4 8 1332.97 194.733 12 -5 -4 8 351.493 473.784 6 -5 -4 11 1112.01 240.673 6 5 -9 11 563.876 307.525 6 5 -9 11 714.905 276.575 3 5 -9 14 952.290 372.047 3 5 -9 14 1857.80 941.395 6 -5 9 -14 233.208 844.947 16 -5 9 -14 629.438 330.315 5 -5 9 -11 537.969 206.447 5 5 4 -11 369.952 159.059 9 -5 9 -11 243.327 302.146 4 5 4 -11 475.248 108.358 8 5 4 -11 88.0455 339.318 4 5 4 -11 120.435 715.343 16 5 4 -8 939.017 256.981 9 -5 9 -8 1464.61 439.354 2 -5 9 -8 1017.60 208.070 7 -9 5 -8 1760.93 473.005 2 5 4 -8 1116.82 293.831 8 -5 9 -5 2821.72 799.947 7 5 4 -5 2930.29 592.911 7 -5 9 -5 2822.52 568.297 2 -9 5 -5 2705.07 617.668 5 9 -4 -2-6.45954 106.961 8 9 -4 -2 53.0928 114.691 9 5 4 -2 6.33567 56.7791 7 5 4 -2-81.0396 33.5085 9 9 -4 -2 5.38397 417.080 1 -9 5 -2 30.1698 70.4894 2 9 -4 -2 74.8569 257.105 16 -9 5 -2 63.5576 136.511 5 -9 5 -2-18.0449 105.474 12 -9 5 1 5072.43 680.343 2 9 -4 1 5807.87 919.429 3 -9 5 1 3974.63 576.852 7 9 -4 1 6170.45 1122.47 9 9 -4 1 5970.85 1144.73 8 -4 -5 4 771.084 125.778 5 9 -4 4 1234.27 363.854 3 4 -9 4 925.460 599.733 1 9 -4 4 1124.65 336.032 6 4 -9 7 1807.17 387.727 8 9 -4 7 1712.17 451.436 3 9 -4 7 1068.78 707.400 8 -4 -5 10-31.2591 478.516 6 4 -9 10-88.7504 200.722 3 -4 -5 13 135.433 42.5778 3 -4 -5 13-35.3309 481.519 6 4 -9 13 157.161 314.418 3 4 -9 13 386.713 456.181 6 4 -9 16-873.224 1041.58 6 4 -9 16-54.2782 255.573 3 -6 9 -15 12.5586 270.989 5 -6 9 -12 871.455 269.229 4 6 3 -12 952.018 880.134 16 6 3 -12 1114.24 429.868 9 -6 9 -12 2001.03 502.277 5 6 3 -9 70.5860 167.718 8 6 3 -9 81.1704 300.273 9 -6 9 -9 2499.68 1283.10 4 6 3 -9 2399.09 2039.10 16 -9 6 -9 822.204 555.516 5 -6 9 -9 1415.61 836.346 7 -6 9 -9 304.674 269.009 5 -6 9 -6 68.6626 370.597 7 -6 9 -6 140.111 152.252 2 6 3 -6 35.5483 300.250 9 -9 6 -6 307.644 42.1486 5 9 -3 -3 370.782 207.465 8 -9 6 -3 708.889 307.376 5 6 3 -3 504.153 231.029 7 -9 6 -3 106.625 87.4387 7 -6 9 -3 344.957 230.725 2 -9 6 -3 306.768 179.859 12 9 -3 -3 371.751 302.802 1 -9 6 -3 359.255 190.825 2 -6 9 -3 186.377 151.497 7 9 -3 -3 603.331 342.581 9 9 -3 0-136.731 196.214 8 9 -3 0-92.0148 279.392 9 -9 6 0-17.6853 153.852 7 -9 6 0-6.26311 51.0414 2 9 -3 0 23.8821 55.9285 3 9 -3 3 5235.83 768.571 6 9 -3 3 3893.80 558.943 3 9 -3 6-73.8702 505.122 8 3 -9 6 177.728 102.961 8 3 -9 6 397.600 606.937 1 9 -3 6 64.0176 207.414 3 -3 -6 9 2237.92 1145.49 6 3 -9 9 1726.94 624.098 3 3 -9 9 2967.71 1458.10 6 3 -9 12 271.282 446.617 6 -3 -6 12 175.797 118.994 3 -3 -6 12 481.017 581.014 6 3 -9 12 184.463 192.919 3 3 -9 15 247.201 192.853 3 -3 -6 15 741.085 556.587 6 3 -9 15-122.249 319.932 6 -7 9 -13-104.009 42.8542 16 -7 9 -13 119.351 272.314 5 -9 7 -10-396.857 421.531 5 -7 9 -10-147.515 231.110 5 -7 9 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130.982 3 -2 -7 14 324.839 200.299 3 2 -9 14 169.658 178.430 6 -2 -7 14 245.751 384.287 6 2 -9 14-62.5102 191.453 3 2 -9 17-2.31888 118.414 3 2 -9 17 494.535 395.377 6 -8 9 -14 365.409 367.368 5 -9 8 -11 269.296 223.681 5 -8 9 -11 183.387 197.356 5 9 -1 -8 2584.49 781.493 9 -9 8 -8 3380.37 884.889 5 8 1 -8 2269.58 547.008 8 -8 9 -8 4972.75 1425.78 4 8 1 -8 2419.38 769.155 9 -9 8 -8 6388.42 1902.04 4 -8 9 -8 4308.74 1150.17 7 -8 9 -8 5413.02 1059.59 2 8 1 -8 3855.16 2080.08 16 9 -1 -8 2195.99 1402.35 16 9 -1 -8 2017.53 553.212 8 -8 9 -8 2847.49 713.315 5 -9 8 -5 489.659 208.865 2 8 1 -5 18.1327 213.777 16 -9 8 -5-12.7671 387.330 4 -8 9 -5-102.414 235.613 7 -9 8 -5 196.609 223.953 7 9 -1 -5 325.491 435.557 1 9 -1 -5 206.484 140.405 16 8 1 -5 146.552 139.905 9 9 -1 -5 218.843 213.172 9 -8 9 -5 287.874 146.629 2 -9 8 -5 7.45865 161.811 5 9 -1 -5 79.6893 173.708 8 -8 9 -2 488.736 181.554 7 8 1 -2 421.118 232.582 8 -9 8 -2 612.869 380.597 7 8 1 -2 693.349 157.327 3 -8 9 -2 606.169 247.297 2 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150.637 2 0 10 -7-213.264 388.315 7 -10 0 -1 104.843 591.852 5 -10 0 2 1550.75 521.377 4 10 -10 2 2123.57 1113.72 1 10 -10 2 1265.48 522.785 8 -10 0 2 1301.84 563.018 5 -10 0 5-87.1785 423.567 12 10 -10 5-298.737 341.478 9 10 -10 5-106.435 396.945 8 10 -10 8 792.628 588.787 8 10 -10 8 115.928 253.351 3 10 -10 11-66.2906 592.126 6 10 -10 11-1.88207 106.454 3 10 -10 14 3315.82 1256.03 6 10 -10 14 1852.27 770.179 3 -1 10 -17 316.585 317.244 4 1 9 -17-177.381 157.165 16 -1 10 -11 1337.18 724.560 7 -1 10 -8 94.9174 184.030 7 1 9 -8 282.145 114.553 2 -1 10 -8 167.420 64.7237 2 1 9 -5 173.620 426.504 7 -10 1 -2 395.252 73.3271 5 -9 -1 -2 620.050 372.288 5 -9 -1 1 1629.18 403.961 5 10 -9 1 1646.78 301.819 1 -10 1 1 2243.45 412.871 5 10 -9 1 1897.99 448.276 8 10 -9 4 2024.93 597.177 9 9 -10 4 203.226 725.037 1 10 -9 4 1645.87 702.379 8 -10 1 4 2381.24 497.333 2 -10 1 4 3299.33 876.274 12 9 -10 4 1565.77 559.747 8 9 -10 4 1995.31 502.601 9 -9 -1 4 1950.71 586.576 5 10 -9 7-272.352 611.372 6 -9 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291.854 1 10 -8 3 1277.27 330.877 8 10 -8 6 3256.11 1051.29 8 8 -10 6 2297.14 748.472 8 10 -8 6 2497.53 899.709 6 -10 2 6 1731.92 348.361 2 -8 -2 6 2126.66 638.060 12 8 -10 6 2516.28 515.918 9 10 -8 9 1100.55 464.130 3 10 -8 9 1230.05 187.482 6 8 -10 9 1494.20 650.004 6 -8 -2 9 871.153 396.617 6 10 -8 12-19.1000 241.109 3 8 -10 12 877.082 409.136 6 10 -8 12-225.642 726.345 6 8 -10 12 441.592 241.844 3 8 -10 15 959.203 462.701 6 8 -10 15 413.714 179.018 3 3 7 -16 113.354 88.8701 9 3 7 -16-464.830 604.087 16 -3 10 -16-40.7729 1124.33 4 -3 10 -13 38.3257 718.513 16 -3 10 -13 119.672 394.660 4 3 7 -13 252.199 333.481 4 3 7 -13 303.784 300.039 9 -3 10 -7 1163.56 771.151 7 3 7 -7 1374.23 686.154 7 3 7 -7 1769.40 371.816 2 -3 10 -7 1240.91 394.364 2 -10 3 -4 176.073 124.147 2 -10 3 -4-716.155 512.752 5 3 7 -4 399.616 308.614 7 -10 3 -4-46.0952 681.862 4 -10 3 -1 2431.09 603.189 5 -10 3 -1 2098.48 614.592 4 10 -7 -1 1849.65 736.004 1 10 -7 -1 2869.89 667.465 9 10 -7 -1 2305.05 567.243 8 10 -7 2 252.332 251.764 8 10 -7 2 322.228 624.067 1 -10 3 2 223.081 163.871 5 10 -7 2 278.080 232.011 9 10 -7 2 337.131 458.119 16 -10 3 2 283.525 172.582 2 -7 -3 2 340.347 262.763 5 7 -10 5-187.548 276.774 8 10 -7 5-283.032 579.437 6 -10 3 5 11.8833 109.049 2 10 -7 5-807.568 328.073 3 -7 -3 5-114.681 229.873 5 7 -10 8 373.007 221.538 3 10 -7 8 543.501 268.313 3 -7 -3 8 164.841 244.631 6 10 -7 8 1041.17 884.815 6 -7 -3 8 796.733 306.274 12 7 -10 11 184.572 449.949 6 -7 -3 11 203.634 165.199 6 10 -7 11 208.351 557.147 6 7 -10 11 420.109 247.506 3 7 -10 14 135.685 274.631 3 7 -10 14-1197.26 706.355 6 -4 10 -17 60.5858 847.034 16 -4 10 -14 621.393 273.627 4 -4 10 -14 1036.84 347.059 2 4 6 -14 339.702 461.623 16 4 6 -14 559.373 390.701 9 4 6 -11-1.33126 195.953 9 4 6 -8 3725.81 2620.18 16 -4 10 -8 571.966 294.879 2 -10 4 -5-219.376 205.299 5 -4 10 -5 848.656 370.836 7 -4 10 -5 509.383 221.241 2 4 6 -5 1220.59 597.157 7 10 -6 -2 398.520 642.441 1 10 -6 -2 531.662 319.187 9 -10 4 -2 278.037 179.854 5 10 -6 -2 377.585 236.994 8 -10 4 1 2748.40 488.615 2 10 -6 1 1695.99 906.115 1 10 -6 1 2027.29 869.805 16 -10 4 1 3120.55 592.665 5 10 -6 1 3069.01 674.979 9 10 -6 1 2955.28 662.271 8 6 -10 4 565.357 858.159 1 -10 4 4 406.493 140.934 2 10 -6 4 349.229 201.636 6 -6 -4 4 453.928 219.034 5 10 -6 4 403.935 178.180 3 10 -6 7 823.838 500.090 3 10 -6 7 638.148 686.778 6 -6 -4 7 1026.37 560.596 12 6 -10 10 489.587 113.341 6 10 -6 10 105.798 194.248 3 -6 -4 10 290.726 350.686 6 10 -6 10 745.079 755.625 6 6 -10 13 2988.05 873.994 6 -6 -4 13 3951.67 1218.02 6 6 -10 13 2515.05 595.583 3 6 -10 16 529.073 309.443 3 6 -10 16 595.042 117.273 6 -5 10 -15 479.317 521.067 4 5 5 -12 56.3641 189.602 9 -5 10 -12 83.9906 75.6877 5 -5 10 -12 65.7595 520.948 4 5 5 -12 269.151 934.045 16 -10 5 -9 338.775 86.5220 5 -10 5 -9-330.528 906.988 4 5 5 -9 356.312 760.723 16 5 5 -9 586.741 238.220 9 -10 5 -6 385.193 127.868 5 -5 10 -6 1117.55 349.258 2 -5 10 -6 619.129 316.978 7 5 5 -3 527.874 245.553 7 10 -5 -3 499.699 40.0669 1 10 -5 -3 201.176 379.634 16 5 5 -3 428.011 65.3543 9 10 -5 -3 532.941 265.920 9 -10 5 -3 1217.15 387.089 5 10 -5 -3 315.666 225.114 8 10 -5 0 150.298 253.134 16 -10 5 0 342.622 154.418 7 10 -5 0 45.8733 153.119 8 10 -5 0 237.377 210.114 9 -10 5 0 442.874 207.130 2 -10 5 0 641.346 332.323 12 -10 5 0 525.383 252.412 5 10 -5 3 860.548 349.679 6 -10 5 3 591.400 260.514 2 10 -5 3 864.756 334.432 3 5 -10 6 635.004 46.1828 8 10 -5 6 787.323 285.436 3 5 -10 6 970.364 630.099 1 10 -5 6 770.799 154.299 6 -5 -5 6 827.762 157.869 5 10 -5 9 988.074 316.301 3 -5 -5 9 362.259 501.694 6 5 -10 9 752.697 253.375 3 -5 -5 12-312.479 459.941 6 5 -10 12 800.600 626.241 6 5 -10 12 365.998 311.613 3 5 -10 15-95.9361 528.809 6 5 -10 15 583.202 315.667 3 -6 10 -16 154.479 259.502 5 6 4 -13 1258.21 497.015 9 6 4 -13 789.540 1269.99 16 -6 10 -13 1614.26 446.107 5 -6 10 -13 2011.94 708.768 4 -10 6 -10 213.940 96.6454 5 -6 10 -10 364.996 305.163 7 6 4 -10 67.0234 559.956 16 6 4 -10 337.859 168.804 8 6 4 -10 73.8470 207.602 9 -6 10 -7 830.303 583.228 7 -6 10 -7 378.216 235.073 2 6 4 -7 94.6438 228.603 9 6 4 -4 564.890 310.869 7 10 -4 -4 234.751 559.398 16 -6 10 -4 137.887 162.997 7 10 -4 -4 354.679 271.005 8 10 -4 -4 420.065 418.586 1 -6 10 -4 407.472 227.835 2 -10 6 -4 951.051 357.060 2 10 -4 -4 466.069 244.263 9 -10 6 -4 140.620 129.367 5 -10 6 -4-10.3294 547.772 4 -10 6 -1 2489.75 530.237 7 -10 6 -1 2588.36 486.643 2 10 -4 -1 2521.55 1115.46 16 10 -4 -1 2489.84 636.044 8 10 -4 -1 3238.99 742.655 9 10 -4 2 642.144 387.903 8 10 -4 2 146.187 245.493 9 -10 6 2 522.209 255.469 2 10 -4 2 566.016 238.988 3 -4 -6 5 563.675 122.006 5 10 -4 5 657.293 246.948 3 4 -10 5 535.957 414.146 1 10 -4 5 1202.14 493.782 6 4 -10 8 1136.12 943.947 1 -4 -6 8 283.722 222.699 12 4 -10 11 1024.64 693.523 6 -4 -6 11 295.445 577.629 6 -4 -6 11-53.5068 128.384 3 4 -10 11 396.924 424.275 3 4 -10 14 1237.82 569.855 6 -4 -6 14 1103.70 670.598 6 4 -10 14 1237.10 312.096 3 4 -10 17 329.180 134.033 6 4 -10 17 5.05784 158.810 3 -7 10 -14 120.828 293.726 5 -7 10 -14 61.9499 846.545 4 7 3 -11 250.958 97.9546 9 7 3 -11 199.040 238.189 8 7 3 -11-9.91240 801.648 16 -10 7 -11 449.898 523.378 5 -10 7 -11 315.198 215.674 2 -7 10 -8 455.438 347.819 4 -7 10 -8 710.328 372.532 2 -7 10 -8 190.058 250.046 7 7 3 -8 429.586 473.379 9 -10 7 -8 256.924 225.328 5 -10 7 -5-249.899 324.057 12 10 -3 -5-101.376 207.469 9 -7 10 -5-11.7637 379.694 7 10 -3 -5-65.7537 163.237 8 -10 7 -5-261.941 385.386 2 10 -3 -5-19.1730 206.702 1 -7 10 -5-32.1455 68.5885 2 10 -3 -5-208.242 834.605 16 -10 7 -5-909.059 528.833 5 10 -3 -2 69.6197 462.706 16 -10 7 -2 237.855 330.918 7 -10 7 -2 251.935 151.124 2 10 -3 -2 364.494 258.708 9 7 3 -2 574.744 276.601 7 10 -3 1 2369.97 766.896 8 10 -3 1 2604.93 512.266 3 -10 7 1 1921.24 512.533 2 10 -3 1 2525.98 772.219 9 10 -3 4 317.364 233.172 3 10 -3 4 756.882 304.316 6 3 -10 7 1378.60 444.279 8 3 -10 7 3379.41 1353.07 1 3 -10 10-501.172 564.159 6 -3 -7 10-156.699 129.449 6 -3 -7 13 843.420 570.588 6 3 -10 13 108.477 275.533 3 3 -10 16 347.335 345.018 3 3 -10 16 47.3708 529.724 6 -3 -7 16-156.166 499.060 6 -8 10 -15 487.523 348.448 5 -10 8 -12 373.234 108.424 2 -10 8 -12 154.801 289.773 5 -8 10 -12 433.581 351.674 4 8 2 -12 156.884 198.519 9 -8 10 -12 226.944 249.874 5 8 2 -9 868.264 310.657 9 -10 8 -9 1223.97 565.671 5 -8 10 -9 1893.92 731.785 7 -8 10 -9 2063.67 562.171 2 -8 10 -9 1162.19 321.032 5 8 2 -9 1232.87 364.600 8 -10 8 -9 778.426 721.117 4 8 2 -9 857.964 60.1206 16 10 -2 -6 1817.47 623.081 8 8 2 -6 1627.63 609.097 8 -8 10 -6 1874.66 555.341 2 -10 8 -6 5048.39 1301.74 7 -8 10 -6 3123.99 1034.13 7 10 -2 -6 2700.87 730.744 1 -10 8 -6 2545.44 792.038 5 8 2 -6 1347.45 711.969 9 10 -2 -6 1888.92 679.449 9 -8 10 -3 1431.13 369.332 7 -10 8 -3 1543.99 437.440 7 -8 10 -3 1815.10 475.422 2 10 -2 -3 1570.15 468.109 8 -10 8 -3 1669.03 400.159 2 10 -2 -3 1364.07 513.170 9 10 -2 0 64.4144 126.540 3 -10 8 0 11.1758 143.809 2 10 -2 0-61.3723 297.746 8 2 -10 6 5193.70 1443.59 1 -2 -8 6 1439.72 823.547 1 -2 -8 9 107.810 41.1991 12 2 -10 12 171.246 501.999 6 -2 -8 12-365.416 542.368 6 -2 -8 12-116.359 95.2329 3 2 -10 12 78.1424 61.5192 3 2 -10 15-1001.11 616.373 6 -2 -8 15-883.699 808.706 6 2 -10 15-138.537 271.484 3 2 -10 18 1266.16 835.890 6 2 -10 18 104.514 168.854 3 -9 10 -16 669.961 505.214 5 -10 9 -13 68.8088 127.278 5 -9 10 -13 292.103 431.325 5 -10 9 -13 523.299 364.252 2 -9 10 -13-232.463 298.087 4 9 1 -10-70.5039 140.960 9 -9 10 -10 15.5474 270.619 5 -9 10 -10-67.4451 316.466 4 9 1 -10 91.9207 171.746 8 -10 9 -10-587.768 480.989 4 9 1 -10 117.372 908.898 16 -10 9 -10 138.074 198.256 5 9 1 -7-32.9785 267.026 8 -9 10 -7-220.840 300.626 2 10 -1 -7-403.259 1250.94 16 -9 10 -7-523.742 559.549 7 -10 9 -7-358.760 568.159 7 9 1 -7-336.830 729.132 16 10 -1 -7-236.809 324.704 1 -10 9 -7-125.938 218.315 5 10 -1 -7-41.1328 204.805 8 10 -1 -7-86.4026 321.452 9 9 1 -7-2.23422 285.400 9 10 -1 -4 1079.87 532.550 8 -9 10 -4 1777.23 690.270 7 -10 9 -4 2671.52 808.774 7 10 -1 -4 1666.47 730.710 9 -9 10 -4 1181.43 412.040 2 10 -1 -4 1528.84 1591.64 16 9 1 -4 2136.94 1999.23 16 9 1 -4 842.541 768.777 9 -10 9 -4 1529.16 501.671 2 -10 9 -1 1898.19 457.819 2 9 1 -1 1671.81 278.612 3 1 -10 14 1117.67 1103.34 6 -1 -9 14-142.349 522.035 6 1 -10 14 305.496 63.2530 3 1 -10 17 1197.67 1234.91 6 -1 -9 17-478.427 784.106 6 1 -10 17-112.236 241.004 3 -10 10 -14 1573.74 713.575 4 -10 10 -14 1829.78 521.345 2 -10 10 -14 1543.00 614.135 5 -10 10 -11-1970.52 879.945 4 -10 10 -11 155.858 161.712 5 10 0 -8 384.090 259.640 8 10 0 -8 231.508 266.291 9 10 0 -8 408.657 535.299 16 -10 10 -8 832.940 682.771 7 -10 10 -8 643.905 413.908 2 -10 10 -8 225.975 239.883 5 10 0 -5-290.890 449.639 9 -10 10 -5-359.967 416.818 7 -10 10 -5-522.815 407.342 2 -10 10 -2 1659.55 698.278 7 -10 10 -2 1316.61 447.188 2 10 0 -2 961.144 303.089 3 0 -10 7-22.6392 73.0767 1 0 -10 13 95.0957 509.344 6 0 -10 16 1088.80 504.347 6 0 -10 19 560.483 841.251 6 0 11 -20-154.042 820.449 16 0 11 -8 1454.45 810.779 7 0 11 -8 2902.34 564.238 2 -11 0 -2 53.6757 258.154 4 -11 0 -2 328.644 391.651 5 -11 0 1 186.493 350.844 5 11 -11 4 3194.24 750.526 8 11 -11 4 585.641 819.762 1 -11 0 4 2789.49 647.176 5 11 -11 4 2689.82 607.599 9 11 -11 10 1724.71 859.371 8 11 -11 10 2593.30 1182.67 6 11 -11 13-191.919 506.732 8 11 -11 13 333.105 514.015 6 11 -11 13 120.464 378.290 3 11 -11 16 310.188 503.299 3 11 -11 16 480.978 1068.97 6 1 10 -18-324.876 372.953 16 -1 11 -9 1063.19 386.662 2 1 10 -9 1063.35 356.352 7 1 10 -6 98.9311 101.584 2 -1 11 -6-7.06984 73.1234 2 -11 1 -3-170.213 336.124 5 -11 1 -3-1113.78 1082.88 4 -11 1 0 159.265 24.8015 5 -10 -1 0-259.537 465.585 5 11 -10 3 12868.4 1460.45 8 11 -10 3 8747.68 1932.33 1 -10 -1 3 14373.5 1421.35 5 -11 1 3 14058.3 1351.20 5 11 -10 3 14079.7 1349.31 9 10 -11 3 12195.3 2164.31 1 10 -11 3 12156.9 1313.33 8 10 -11 6 175.972 224.423 9 11 -10 6 354.060 508.298 8 -11 1 6 252.685 131.756 2 11 -10 6 925.444 603.395 3 11 -10 6 390.544 350.845 9 -10 -1 6 258.792 112.644 12 10 -11 9 399.426 489.302 3 10 -11 9 411.369 165.395 8 11 -10 9 445.489 510.108 3 11 -10 9 668.656 800.283 6 11 -10 12 231.406 211.208 3 11 -10 12-40.0483 453.271 8 10 -11 12 195.019 265.578 6 11 -10 12 269.718 552.531 6 10 -11 12-54.1145 198.247 3 10 -11 15-155.724 278.474 3 10 -11 15-130.624 88.9317 6 11 -10 15-77.1372 850.223 6 11 -10 15 1.65775 290.655 3 -2 11 -19 1281.92 1092.15 4 -2 11 -19-482.982 639.017 16 2 9 -16 146.300 973.059 16 2 9 -13 549.914 637.032 16 -2 11 -10-149.860 379.355 7 2 9 -10-14.1789 233.438 7 2 9 -10 13.8716 168.192 9 -2 11 -7 1433.14 423.405 2 2 9 -7 1563.24 704.114 7 2 9 -7 1570.82 346.418 2 -2 11 -7 1177.28 594.434 7 -11 2 -4 318.029 386.212 4 -11 2 -4 119.054 322.306 5 -11 2 -1 2032.87 727.058 5 -11 2 -1 2738.27 714.667 4 11 -9 2 772.025 511.157 8 11 -9 2 1894.52 1307.09 1 -9 -2 2 627.263 349.988 5 11 -9 2 677.936 678.373 9 -11 2 2 96.3250 104.585 5 11 -9 2 296.949 402.045 16 9 -11 5 3161.01 634.039 8 11 -9 5 2212.97 442.814 8 -11 2 5 2338.79 369.952 2 9 -11 5 3361.19 523.650 9 -9 -2 5 3066.24 546.617 5 11 -9 5 2520.30 574.272 9 11 -9 5 1902.74 604.117 3 -9 -2 8 115.231 309.266 6 11 -9 8 541.792 805.716 6 9 -11 8 587.799 352.485 3 11 -9 8 46.9848 270.274 3 9 -11 11-551.706 862.321 6 11 -9 11-74.9615 691.289 6 11 -9 11 13.7071 92.5034 3 -9 -2 11 212.749 379.874 6 9 -11 14 277.770 361.703 3 11 -9 14 481.437 278.163 6 11 -9 14-242.897 192.789 3 9 -11 14 27.9612 767.454 6 9 -11 17 377.121 444.493 3 9 -11 17 206.867 745.108 6 3 8 -17 501.249 1140.68 16 3 8 -14-370.337 412.800 16 3 8 -14 369.171 413.357 9 3 8 -11 684.579 793.039 16 3 8 -8 1426.09 682.779 9 3 8 -8 1787.28 706.696 7 -3 11 -8 718.972 327.449 7 -3 11 -8 2154.34 532.550 2 -11 3 -5-230.751 514.416 5 -11 3 -2 2236.44 783.202 5 -11 3 -2 4629.79 1304.77 4 -8 -3 1 574.581 718.488 5 11 -8 1 317.941 412.543 8 11 -8 1 1.23001 758.026 1 11 -8 1 311.447 600.338 16 -11 3 1 474.989 448.830 2 11 -8 1 77.9846 251.323 9 -11 3 1 880.077 732.299 12 -11 3 1 2229.13 691.373 5 11 -8 4 1833.37 844.353 8 -11 3 4 863.910 269.201 2 -8 -3 4 1089.02 380.267 5 11 -8 4 2055.82 894.921 9 8 -11 4 2387.36 1091.21 1 11 -8 4 2091.67 751.563 3 8 -11 4 1221.73 496.198 8 11 -8 7 481.514 562.937 6 11 -8 7 323.568 234.434 3 -8 -3 7 546.907 247.918 12 11 -8 10 1486.60 555.973 3 8 -11 10 1026.88 218.004 6 -8 -3 10 1110.61 337.765 6 11 -8 10 989.423 446.931 6 8 -11 10 1630.79 544.028 3 8 -11 13-195.919 111.618 3 8 -11 13 1302.93 619.314 6 -8 -3 13 740.783 662.166 6 8 -11 16 25.7756 233.050 3 8 -11 16 521.726 1089.07 6 -4 11 -18 234.222 146.185 4 -4 11 -15 661.264 145.638 4 4 7 -15 822.492 729.495 16 -4 11 -15 178.310 642.198 16 -4 11 -15 528.330 354.630 2 -4 11 -12-64.4960 258.902 4 4 7 -12 42.1594 284.728 9 -4 11 -9 1057.13 387.429 2 -4 11 -9 716.064 438.770 7 -11 4 -6 168.502 241.663 5 -11 4 -6 716.341 321.732 2 4 7 -6 947.337 541.363 7 -4 11 -6 721.862 246.735 2 4 7 -6 876.981 733.380 9 -11 4 -3 1092.77 591.617 5 -11 4 -3 5425.50 1335.55 4 -11 4 0 2921.33 618.606 5 -11 4 0 2804.51 609.317 12 11 -7 0 2540.33 816.556 16 11 -7 0 1683.80 392.369 8 11 -7 0 1666.38 475.433 9 -7 -4 3 499.319 538.313 5 11 -7 3 1040.04 690.113 9 11 -7 3-101.421 408.941 8 -11 4 3 85.8248 206.338 2 11 -7 3 311.485 466.074 3 11 -7 6 428.504 757.846 6 7 -11 6-335.776 814.707 1 -7 -4 6-111.082 171.336 5 7 -11 6-129.587 165.918 8 11 -7 6-1004.76 384.526 3 7 -11 9 375.908 312.569 8 11 -7 9 266.217 259.285 3 -7 -4 9 336.808 196.307 6 7 -11 9 524.387 248.769 3 11 -7 9 1059.93 728.592 6 7 -11 12-389.664 540.971 8 7 -11 12 396.074 532.020 6 -7 -4 12-620.087 317.558 6 7 -11 15 556.188 450.915 3 7 -11 15-1940.38 939.142 6 7 -11 18-323.735 420.721 6 -5 11 -16-99.8041 145.098 4 5 6 -16 827.251 584.413 9 5 6 -16 15.8533 1349.16 16 5 6 -13 268.959 876.194 16 5 6 -13-79.8199 232.299 9 5 6 -10 299.852 378.776 9 -5 11 -7-126.696 255.789 2 -11 5 -7-809.621 616.589 5 -5 11 -7-227.463 525.760 7 -11 5 -4 2984.50 963.862 5 5 6 -4 1416.00 509.129 7 11 -6 -1 8081.92 1355.32 1 -11 5 -1 8431.55 954.639 2 11 -6 -1 9146.05 1784.09 16 11 -6 -1 8213.39 1139.85 9 11 -6 -1 7752.12 1070.89 8 -11 5 2 632.144 219.095 2 -11 5 2 561.056 135.743 7 11 -6 2 714.914 111.366 3 11 -6 2 630.939 581.670 16 11 -6 2 202.439 354.661 8 11 -6 2 332.928 415.834 9 -6 -5 5 779.664 389.126 5 11 -6 5 1206.21 666.878 6 6 -11 5 2212.80 1363.97 1 6 -11 5 1038.93 426.553 8 11 -6 5 1163.26 636.252 3 6 -11 8 105.150 193.961 8 11 -6 8 34.3710 189.249 3 6 -11 8-937.503 1232.80 1 11 -6 8-92.2396 466.411 6 -6 -5 8-180.843 193.407 12 6 -11 11-465.276 411.512 6 -6 -5 11 314.709 156.399 6 6 -11 11 22.4775 279.438 3 -6 -5 14 209.868 121.509 6 6 -11 14 361.227 296.105 3 6 -11 14 869.851 931.711 6 6 -11 17 191.096 133.211 3 6 -11 17 857.632 409.616 6 -6 11 -17-224.267 935.395 4 -6 11 -14 118.718 122.710 5 6 5 -14-144.789 306.217 16 6 5 -14 219.761 152.438 9 -6 11 -11-285.684 362.477 7 6 5 -11 11.3470 148.025 9 6 5 -8 151.549 179.210 8 -11 6 -8-503.839 339.548 5 6 5 -8-145.837 866.109 16 -6 11 -8 198.815 216.973 2 -11 6 -5 1682.40 1382.51 4 -6 11 -5 981.856 420.237 2 -6 11 -5 984.003 782.287 7 -11 6 -5 1456.16 740.875 5 11 -5 -2 744.438 242.184 8 -11 6 -2 672.813 269.435 2 11 -5 -2 803.584 369.858 1 -11 6 -2 258.172 221.986 7 -11 6 -2 996.178 252.552 5 11 -5 -2 699.832 215.420 9 -11 6 1 6629.63 752.977 7 -11 6 1 7277.20 867.450 2 11 -5 1 8260.38 1047.33 3 11 -5 1 8309.77 1961.49 16 11 -5 1 6716.79 1149.18 8 11 -5 1 6964.32 1140.25 9 11 -5 4 1726.59 527.795 3 -5 -6 4 1545.42 450.385 5 11 -5 4 2262.73 633.029 6 5 -11 7-3.80378 147.071 8 11 -5 7-12.2366 268.115 3 11 -5 7-572.781 442.825 6 5 -11 7-736.307 1140.79 1 5 -11 10 529.479 408.563 8 -5 -6 10 409.131 343.503 6 5 -11 13 379.445 708.493 6 -5 -6 13-400.501 258.497 6 5 -11 16 218.229 274.943 3 5 -11 16 1230.82 1051.04 6 -5 -6 16 939.200 739.760 6 -7 11 -15 111.792 606.119 4 -7 11 -15 32.0803 203.831 5 -7 11 -12 52.0976 69.6108 5 7 4 -12 286.506 400.744 9 7 4 -12 705.465 1653.33 16 7 4 -9 12.4087 158.731 9 -11 7 -9 338.392 207.054 5 -7 11 -9 179.946 82.5175 2 -7 11 -6-292.023 389.734 7 -7 11 -6-108.623 184.001 2 -11 7 -6-988.332 537.571 5 11 -4 -3-28.3790 169.104 8 -11 7 -3 272.374 300.859 2 11 -4 -3 25.7637 623.972 1 11 -4 -3 224.803 771.996 16 -11 7 -3 992.966 486.460 5 -11 7 -3 540.812 431.675 12 11 -4 -3 362.962 405.724 9 11 -4 0 1643.69 408.153 8 -11 7 0 1550.21 334.089 7 11 -4 0 1777.85 508.544 9 11 -4 0 1926.72 487.827 3 -11 7 0 1259.79 358.031 2 11 -4 3 361.293 317.342 3 11 -4 3 23.2015 217.693 6 4 -11 6 692.685 70.9948 1 11 -4 6 1448.60 611.413 6 -4 -7 6 771.975 81.8637 5 4 -11 6 1055.54 237.992 8 4 -11 9 1091.52 230.851 8 -4 -7 9 1054.35 363.327 12 4 -11 12-600.973 739.257 6 -4 -7 12 656.962 389.712 6 4 -11 12-133.078 270.092 3 4 -11 15 844.444 989.797 6 -4 -7 15 911.166 522.902 6 4 -11 15 631.374 293.795 3 4 -11 18-614.293 1440.63 6 4 -11 18 365.130 354.033 3 -8 11 -16 480.966 581.653 4 -8 11 -16-85.0982 230.964 5 8 3 -13 17.3679 157.763 8 8 3 -13-3.20625 133.060 9 -8 11 -13-106.474 164.587 5 -11 8 -10 1488.13 497.385 5 8 3 -10 790.106 278.911 8 -8 11 -10 1301.71 727.952 7 -11 8 -10 1275.72 559.388 4 8 3 -10 716.684 1244.21 16 8 3 -10 1353.16 529.618 9 11 -3 -7 386.963 253.054 16 8 3 -7 199.823 155.444 9 -8 11 -7 753.967 295.875 2 11 -3 -7 660.845 241.538 9 -11 8 -7 906.516 312.651 5 -11 8 -4 1202.57 500.790 2 -8 11 -4 1410.87 758.098 7 -8 11 -4 1186.22 493.547 2 11 -3 -4 341.913 1310.59 16 11 -3 -4 2106.64 787.086 9 11 -3 -4 1552.53 613.133 8 11 -3 -4 1570.86 698.900 1 -11 8 -4 1219.46 638.790 5 -11 8 -1 104.333 123.033 2 11 -3 -1 566.689 670.126 9 11 -3 2 230.306 258.475 3 11 -3 2 329.634 322.775 6 11 -3 5 348.827 436.160 6 11 -3 5-48.8063 120.757 9 -3 -8 14 158.105 272.820 6 3 -11 14 412.935 157.109 3 3 -11 17-656.221 1044.47 6 -3 -8 17 366.874 527.875 6 3 -11 17 305.607 339.177 3 -9 11 -17 48.5867 212.656 5 -9 11 -17-957.199 1239.08 4 -11 9 -14 288.002 475.839 5 -9 11 -14 1208.97 902.657 4 -9 11 -14-36.1503 248.899 5 9 2 -11-23.4181 485.947 8 -9 11 -11 11.0279 155.908 5 -11 9 -11-59.5157 301.661 4 9 2 -11 408.455 615.594 16 9 2 -11 138.916 305.824 9 -11 9 -11 115.407 294.189 5 11 -2 -8 229.903 250.291 8 -9 11 -8 213.163 151.573 2 -11 9 -8-140.582 321.495 4 -9 11 -8 928.635 804.715 7 -11 9 -8 241.395 254.750 12 11 -2 -8 252.606 460.190 16 9 2 -8 113.386 179.098 9 11 -2 -8 171.985 328.557 9 -11 9 -8 85.1510 144.176 5 -11 9 -5 2646.26 588.214 2 -11 9 -5 2283.70 564.701 5 -9 11 -5 2120.38 568.830 7 11 -2 -5 2898.32 668.244 8 11 -2 -5 2522.18 710.282 9 11 -2 -5 582.735 491.008 16 -9 11 -5 2840.77 564.960 2 9 2 -5 1325.45 1079.80 16 9 2 -5 2407.69 769.389 9 9 2 -2 1194.11 895.238 8 -11 9 -2 674.026 482.153 7 -11 9 -2 958.400 362.065 2 9 2 -2 735.695 201.274 3 11 -2 -2 935.129 689.448 9 11 -2 1 2143.80 508.491 3 11 -2 1 3211.53 1358.14 8 11 -2 4 564.329 87.9552 3 11 -2 4 444.873 365.239 9 2 -11 7 2021.19 324.220 1 -2 -9 7 1750.21 212.799 1 2 -11 13 279.215 668.184 6 -2 -9 13 68.4084 570.556 6 2 -11 16-595.637 517.066 6 -2 -9 16-372.207 702.494 6 2 -11 19-9.23297 713.386 6 -10 11 -15 191.000 696.721 4 -11 10 -15 73.7985 387.395 5 -10 11 -15 323.761 317.806 2 -10 11 -15-78.4464 257.238 5 -10 11 -12-42.8799 117.865 5 -11 10 -12 27.2277 334.391 5 11 -1 -9 513.236 105.593 8 -11 10 -9 646.904 365.767 5 10 1 -9-158.288 650.075 16 10 1 -9 380.288 322.881 9 -10 11 -9 1765.39 697.896 4 -11 10 -9 71.4032 259.682 4 -10 11 -9 1173.60 613.427 7 -10 11 -9 700.467 443.102 2 11 -1 -9 513.464 403.914 9 11 -1 -9 302.207 458.351 16 -10 11 -9 768.021 312.818 5 10 1 -6 32.1688 147.544 9 -11 10 -6 94.2233 60.3527 2 10 1 -6 29.4821 248.674 8 -10 11 -6 177.816 117.322 2 11 -1 -6 75.3161 109.109 9 -10 11 -3 10753.7 1549.94 7 -10 11 -3 12243.7 1350.42 2 11 -1 -3 12492.3 2890.03 16 -11 10 -3 12216.0 1327.40 2 10 1 -3 9255.21 1515.21 8 11 -1 -3 11336.3 1722.70 9 11 -1 -3 11020.7 1514.03 8 10 1 0-211.037 343.117 8 11 -1 0-44.9667 193.137 3 11 -1 3 193.195 357.857 8 11 -1 3-61.1333 73.0267 3 11 -1 3-115.328 415.979 9 -1 -10 6 26.4497 379.990 1 1 -11 6-54.1032 170.641 1 1 -11 15 8.65359 808.195 6 -1 -10 15 149.100 416.797 6 1 -11 15 0.10714 212.910 3 1 -11 18-88.9400 455.747 6 -1 -10 18 481.974 156.507 6 -11 11 -16 364.591 519.373 5 -11 11 -16-1776.78 1060.84 4 -11 11 -13 1606.67 655.266 4 -11 11 -13 71.4355 76.2405 5 11 0 -10 993.632 449.180 9 11 0 -10 948.788 859.365 16 -11 11 -10 2019.73 541.485 5 11 0 -10 1496.71 488.092 8 11 0 -7 224.102 393.105 8 -11 11 -7 83.3881 237.511 2 11 0 -7 183.968 247.395 9 11 0 -4 2265.14 756.119 8 -11 11 -4 1306.74 727.216 7 11 0 -4 2494.13 1451.18 16 11 0 -4 2191.32 809.464 9 -11 11 -4 2242.08 554.411 2 11 0 -1-36.5274 108.427 3 11 0 2 75.0557 58.4731 3 0 -11 17-373.347 193.089 6 0 -11 20 452.399 985.541 6 0 12 -12 1936.43 819.565 7 0 12 -9 92.2583 190.805 2 -12 0 0 2116.30 528.443 4 -12 0 0 2069.92 570.536 5 12 -12 3-112.520 238.456 8 -12 0 3-18.5857 208.345 5 12 -12 3 213.700 497.451 1 12 -12 6 1348.15 537.607 8 12 -12 6 1386.33 517.733 9 12 -12 9-207.335 578.096 8 12 -12 9 32.5535 452.920 3 12 -12 12 935.000 786.863 6 12 -12 15 299.302 493.213 6 12 -12 15 50.1853 180.049 3 -1 12 -19 56.9539 1259.39 16 -1 12 -10 37.1007 207.017 2 -1 12 -10 272.353 557.414 7 1 11 -10 237.661 417.643 7 1 11 -7 516.432 268.757 7 -1 12 -7 279.211 228.186 2 1 11 -7 204.695 87.4226 2 -1 12 -7 120.675 351.922 7 -12 1 -4-313.920 351.015 5 -12 1 -1 93.2968 360.131 5 -11 -1 -1 123.237 318.142 5 -12 1 -1 28.6377 282.188 4 -11 -1 -1 903.223 656.447 4 12 -11 2 133.758 243.259 8 -12 1 2-259.381 215.652 5 -11 -1 2-188.554 187.569 5 11 -12 5 743.157 309.786 8 11 -12 5 191.091 443.029 1 12 -11 5 807.452 314.652 9 -11 -1 5 934.366 409.964 5 -11 -1 5 633.006 385.242 12 11 -12 5 841.797 274.152 9 12 -11 8 7.32207 437.434 8 12 -11 8 17.3456 165.566 3 11 -12 11 75.8869 537.347 8 11 -12 11 36.4259 654.964 6 12 -11 11 341.188 399.195 6 11 -12 11 102.606 50.2627 3 12 -11 11 34.4500 237.270 3 12 -11 14 77.1795 277.450 3 11 -12 14 17.3623 1188.93 6 12 -11 14 101.201 263.267 6 11 -12 14 120.408 366.649 3 11 -12 17 129.059 215.298 3 11 -12 17 143.256 843.899 6 -2 12 -17 308.690 811.190 4 -2 12 -11 507.079 309.892 2 2 10 -11 328.333 540.853 7 -2 12 -8 167.678 271.615 7 -2 12 -8 243.451 147.682 2 2 10 -8 172.402 130.129 2 -12 2 -5 346.041 198.727 5 -12 2 -5 271.295 909.700 4 -12 2 -2 1337.17 636.961 5 -12 2 -2 2195.56 775.408 4 -10 -2 1 433.394 127.907 5 12 -10 1 429.884 216.210 8 -10 -2 1 1330.83 387.187 4 12 -10 1 740.836 702.780 1 12 -10 1 647.432 340.579 9 -12 2 1 642.947 280.451 5 10 -12 4 131.475 218.775 8 -10 -2 4 232.596 88.0099 5 -12 2 4 77.3514 198.148 2 12 -10 4-30.3528 178.228 9 10 -12 4 59.8402 934.664 1 12 -10 7-1.77124 341.739 8 -12 2 7 83.1657 47.0095 2 10 -12 7-42.6811 210.363 8 12 -10 10 1661.45 1254.87 6 10 -12 10 735.382 478.818 3 12 -10 10 657.347 432.851 3 12 -10 13-122.105 82.8021 3 10 -12 13 44.9341 209.813 8 10 -12 13 706.411 787.140 6 12 -10 13 651.146 789.141 6 10 -12 13-154.729 143.460 3 10 -12 16 526.757 381.479 3 10 -12 16-107.782 545.312 6 -3 12 -15-61.9210 340.823 4 -3 12 -12-97.5631 170.819 7 -3 12 -9 2234.93 532.497 2 -12 3 -6 1213.51 666.753 5 -3 12 -6 434.543 324.965 7 3 9 -6 671.747 520.280 7 -12 3 -6 857.717 487.449 4 3 9 -6 970.202 278.737 2 -12 3 -3 802.350 423.570 5 -12 3 -3 950.469 453.938 4 -12 3 -3 394.810 167.891 2 12 -9 0-872.336 372.433 8 -12 3 0 22.3916 199.139 4 12 -9 0-314.699 319.752 1 12 -9 0-128.468 185.312 9 -12 3 0-204.262 129.151 5 -9 -3 3 360.027 74.1674 5 12 -9 3 126.581 54.2558 8 -12 3 3 334.002 130.682 2 -12 3 3 218.785 203.633 12 12 -9 3 437.380 298.550 9 9 -12 6 1965.30 564.497 8 12 -9 6 1502.32 543.740 8 -12 3 6 1691.35 364.915 2 9 -12 6 2313.35 1065.04 1 -9 -3 6 1843.69 470.479 5 12 -9 6 1516.86 552.251 3 9 -12 9 1024.39 522.742 8 12 -9 9 697.895 580.416 6 12 -9 9 1129.37 583.362 3 12 -9 12-72.5697 149.292 3 9 -12 12 219.077 478.893 6 12 -9 12 577.355 922.727 6 9 -12 12 293.037 204.036 3 9 -12 15 302.348 651.471 6 9 -12 15-17.6096 117.990 3 9 -12 18-3.84018 180.853 3 9 -12 18 384.496 1119.59 6 -4 12 -16-84.0646 252.604 2 -4 12 -10 674.779 328.743 2 -4 12 -10 381.317 368.556 7 -12 4 -7 538.847 489.648 5 -4 12 -7 0.79403 227.757 7 -4 12 -7 80.7792 194.183 2 -12 4 -4-100.819 322.025 5 -12 4 -4-2361.81 871.964 4 12 -8 -1 1555.75 379.822 8 -12 4 -1 1806.83 449.337 5 12 -8 -1 1840.93 980.532 1 12 -8 -1 1459.41 454.008 9 12 -8 2 3884.03 781.336 8 -8 -4 2 3020.01 726.900 5 -12 4 2 3723.91 583.007 2 -12 4 2 3454.31 806.430 12 12 -8 2 3763.77 797.165 9 8 -12 5 325.670 132.879 8 -12 4 5 381.118 243.119 2 12 -8 5 271.465 174.277 3 8 -12 5 566.008 360.623 1 -8 -4 5 379.958 215.530 5 12 -8 8 150.968 85.4024 3 8 -12 8 42.3008 214.543 8 12 -8 8 293.281 264.226 8 12 -8 8-175.657 309.540 6 12 -8 8 322.207 421.280 9 -8 -4 8 406.698 324.355 12 8 -12 8 165.715 228.226 1 8 -12 11-962.435 478.692 8 12 -8 11 82.0950 125.762 3 12 -8 11-482.332 562.121 8 -8 -4 11 342.787 348.853 6 12 -8 11 311.906 754.003 6 8 -12 11 141.619 216.888 3 8 -12 14-152.905 486.596 6 -8 -4 14-32.5752 296.257 6 8 -12 14 523.188 380.413 3 8 -12 17-57.1278 352.052 6 8 -12 17 222.097 165.136 3 -5 12 -17-331.792 861.462 4 5 7 -17-394.447 1106.90 16 5 7 -17 88.4995 107.089 9 5 7 -14-199.652 1028.00 16 5 7 -14 72.7133 136.477 9 5 7 -11-270.252 265.641 16 -5 12 -11 80.5515 110.756 2 -12 5 -8 177.528 370.971 5 -5 12 -8 1156.45 564.833 7 -12 5 -8 1853.41 1414.43 4 -5 12 -8 1397.52 480.645 2 -12 5 -5 1202.89 546.948 5 5 7 -5 1705.96 543.172 7 -12 5 -5 1848.44 780.482 4 12 -7 -2 3415.54 712.320 8 12 -7 -2 2583.97 952.744 16 12 -7 -2 3022.80 1027.19 1 12 -7 -2 3046.93 666.745 9 -12 5 -2 2792.74 611.569 5 12 -7 1 772.287 256.511 8 12 -7 1 692.467 123.867 9 -12 5 1 501.718 143.880 2 -7 -5 4 2035.11 464.811 5 -12 5 4 2111.09 441.045 2 12 -7 4 1832.32 550.729 3 12 -7 7 640.477 597.413 8 7 -12 7 346.558 327.134 8 7 -12 7 1207.11 1012.13 1 12 -7 7 606.272 505.889 6 12 -7 7 458.991 370.230 3 12 -7 10 70.1753 325.037 8 -7 -5 13-979.432 663.740 6 7 -12 13-134.531 223.922 3 7 -12 16 214.873 575.993 6 7 -12 16-339.822 345.895 3 7 -12 19 307.087 433.942 3 7 -12 19 625.776 954.497 6 -6 12 -18-331.669 547.751 4 6 6 -15 131.233 1174.72 16 6 6 -15 84.4872 364.926 9 6 6 -12 931.669 1591.40 16 6 6 -12 268.987 122.362 9 -12 6 -9-208.757 426.689 5 -6 12 -9-53.0498 193.302 7 -12 6 -9-14.7979 1077.01 4 -6 12 -9 107.585 89.2822 2 -12 6 -6 727.951 405.343 5 -6 12 -6 244.213 504.023 7 6 6 -6 743.294 432.176 7 -12 6 -6 2086.96 1085.90 4 -6 12 -6 1317.75 449.041 2 -12 6 -3 300.088 346.204 5 6 6 -3 463.691 189.051 7 12 -6 -3 744.664 318.237 8 12 -6 -3 441.863 483.095 16 -12 6 -3 602.438 232.654 12 12 -6 -3 1348.15 818.479 1 12 -6 -3 852.875 301.661 9 -12 6 0 218.127 212.181 7 12 -6 0 178.916 86.1888 9 -12 6 0 354.410 163.881 2 -12 6 3 550.317 177.528 2 12 -6 3 884.923 317.316 3 12 -6 6 668.496 406.939 3 12 -6 6 338.619 276.041 8 12 -6 6 1226.57 387.322 6 -6 -6 6 1074.84 287.718 5 6 -12 6 679.493 448.136 1 6 -12 6 953.979 362.252 8 12 -6 9-216.127 48.0634 8 12 -6 9-31.5784 95.7658 3 12 -6 9-214.719 430.900 6 -6 -6 9 158.211 335.577 12 6 -12 12-511.617 686.858 6 -6 -6 12 255.835 524.063 6 6 -12 12-112.268 218.382 3 6 -12 15 451.970 649.934 6 -6 -6 15 379.508 634.662 6 6 -12 18 819.243 1267.63 6 6 -12 18-323.705 283.832 3 -7 12 -16 122.049 58.3065 2 7 5 -13-248.533 725.526 16 7 5 -13-60.9153 129.383 9 -12 7 -10-49.8833 247.418 5 -12 7 -10 88.0428 141.471 2 7 5 -10-95.0604 306.558 9 -12 7 -7 871.653 516.522 5 -7 12 -7 170.550 213.526 7 -7 12 -7 295.451 251.281 2 12 -5 -4 1848.91 525.081 8 12 -5 -4 2044.35 675.551 1 7 5 -4 2017.05 525.698 7 -12 7 -4 2147.30 529.083 2 -12 7 -4 1761.31 508.322 12 12 -5 -4 823.137 797.854 16 12 -5 -4 2150.78 656.290 9 -12 7 -4 1436.79 464.636 5 12 -5 -1 61.8020 669.757 1 12 -5 -1 451.952 237.955 9 -12 7 -1 614.088 201.430 2 12 -5 2 2564.58 595.671 8 -12 7 2 2695.54 590.887 2 12 -5 2 3753.69 712.234 3 12 -5 2 2822.32 616.735 9 12 -5 5 1932.02 529.489 3 -5 -7 5 1760.22 335.987 5 12 -5 5 2161.77 536.101 6 12 -5 8 1069.66 786.592 8 12 -5 8 832.536 677.267 6 5 -12 8 778.725 278.886 8 5 -12 14-181.672 434.939 6 -5 -7 14-521.984 466.838 6 5 -12 14-69.8604 238.532 3 5 -12 17 248.425 243.079 3 5 -12 17 434.984 467.632 6 -5 -7 17 985.257 758.452 6 -8 12 -17 297.845 916.278 4 -8 12 -14-705.547 484.542 4 8 4 -14 567.243 1160.82 16 -8 12 -14-60.7498 82.6478 5 8 4 -14 99.1040 356.596 9 -12 8 -11-419.781 295.147 5 -8 12 -11-351.661 351.896 4 -8 12 -11 135.893 782.528 7 8 4 -11 120.071 378.178 9 -12 8 -8-21.8312 169.190 4 8 4 -8 445.129 824.495 16 8 4 -8 786.094 674.638 9 -8 12 -8 442.442 280.829 2 -12 8 -8 378.445 302.485 5 12 -4 -5 250.786 100.198 8 8 4 -5 301.670 224.913 7 -12 8 -5 281.328 244.750 2 -8 12 -5 272.520 151.440 2 -12 8 -5 132.652 254.142 5 12 -4 -5 286.386 221.415 9 12 -4 -5 110.516 153.857 1 12 -4 -2 3201.82 669.399 8 8 4 -2 3066.34 648.184 7 12 -4 -2 4169.62 910.470 9 -12 8 -2 3186.06 595.023 2 8 4 -2 2447.84 972.040 9 12 -4 1 1216.73 244.785 8 -12 8 1 1419.49 397.664 2 12 -4 1 1086.84 235.842 9 12 -4 1 1728.61 411.455 3 12 -4 4-31.1230 102.310 3 12 -4 4 1.80803 209.741 6 4 -12 7 76.5581 168.725 8 4 -12 7 127.671 361.942 1 12 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1037.03 360.635 3 3 -12 9 1574.24 826.408 1 3 -12 15-165.935 481.391 6 -3 -9 15-753.630 464.392 6 3 -12 15-251.179 206.464 3 3 -12 18 214.127 897.357 6 -3 -9 18 477.968 826.502 6 -10 12 -16-253.659 266.151 2 -10 12 -16-116.039 782.439 4 -10 12 -16-113.898 171.442 5 -12 10 -13-381.727 392.085 5 10 2 -13 74.7937 260.517 8 10 2 -13-244.528 263.340 9 -10 12 -13-320.727 552.010 4 -12 10 -13 1601.35 1138.01 4 -10 12 -13-16.5093 307.791 5 10 2 -13-103.492 1077.11 16 10 2 -10 393.619 331.666 8 -10 12 -10 649.537 245.447 4 -10 12 -10 480.405 199.356 7 -12 10 -10 313.686 200.276 12 10 2 -10 457.248 97.8577 9 -12 10 -10 438.350 373.004 5 -10 12 -10 611.012 496.567 2 12 -2 -7-54.0847 243.600 8 10 2 -7-28.8489 354.889 8 -12 10 -7-635.025 477.345 4 -12 10 -7 161.560 306.978 2 12 -2 -7-4.52960 193.569 1 12 -2 -7 135.452 655.514 16 -12 10 -7 330.145 196.052 5 12 -2 -7 435.279 393.083 9 10 2 -7-131.920 399.271 9 -10 12 -7 169.642 75.1813 2 -10 12 -4-62.2621 122.388 2 12 -2 -4 116.297 36.1661 9 -12 10 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1379.55 648.488 9 -12 11 -5 846.829 317.379 2 11 1 -5 848.951 673.319 9 -12 11 -2-97.2143 398.726 7 -12 11 -2 136.945 238.078 2 12 -1 1 142.161 123.057 3 11 1 1 386.379 212.492 3 11 1 1 319.643 437.012 9 -1 -11 7 512.667 482.089 1 1 -12 7-179.397 524.764 1 1 -12 16-92.6941 549.453 6 -1 -11 16 1123.05 851.931 6 1 -12 19-225.068 748.711 6 -1 -11 19-304.697 832.578 6 -12 12 -15-142.174 353.959 5 -12 12 -12 483.178 384.664 5 12 0 -9 169.524 196.446 8 -12 12 -9 574.192 547.612 7 -12 12 -9-324.792 406.929 2 12 0 -9-165.036 279.436 9 12 0 -9-110.487 759.334 16 12 0 -6 831.403 329.084 8 -12 12 -6 71.6392 240.728 7 12 0 -6 826.878 500.412 9 -12 12 -6 970.456 447.092 2 12 0 -3-276.892 456.227 8 -12 12 -3-0.11493 172.019 2 12 0 0 1800.72 408.188 3 0 -12 18-3723.98 1340.49 6 0 -12 21-2331.41 1141.98 6 0 13 -13 119.547 576.502 7 0 13 -10 132.081 408.601 7 -13 0 -1 80.9737 397.726 5 -13 0 -1 610.089 331.063 4 -13 0 2 1189.58 500.586 5 13 -13 5 276.168 315.803 8 -13 0 5 213.576 387.376 12 13 -13 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370.519 7 2 11 -9 39.9115 457.209 7 -2 13 -9 105.339 160.122 2 -13 2 -3-1469.63 598.673 5 -11 -2 0 50.4446 75.5363 5 -11 -2 0-200.663 226.446 4 -13 2 0 152.961 233.986 5 13 -11 3-375.209 378.777 8 13 -11 3 7.76579 42.0690 1 -13 2 3-63.3186 209.897 12 -13 2 3-273.021 212.203 5 13 -11 3-12.0396 105.685 9 -11 -2 3 7.04842 257.938 5 11 -13 6 249.771 216.271 8 -11 -2 6-31.5734 406.885 12 13 -11 6 74.3796 276.105 9 13 -11 9 643.221 322.887 3 13 -11 12 298.039 1078.39 6 11 -13 12 272.892 653.103 3 13 -11 12 263.475 435.990 3 13 -11 15 600.179 513.599 3 11 -13 15 4.96357 556.836 6 13 -11 15 656.590 953.105 6 11 -13 15 51.1766 233.667 3 11 -13 18-2063.72 1138.74 6 11 -13 18-386.321 324.771 3 3 10 -16 659.809 524.128 16 -3 13 -16 384.274 348.560 2 -3 13 -13-308.261 725.489 7 -3 13 -10 201.163 164.976 2 -3 13 -10-61.7628 433.775 7 -3 13 -7 75.0810 54.8396 7 3 10 -7-25.7218 152.937 7 -13 3 -4-312.163 252.464 5 -13 3 -1 199.068 154.051 5 13 -10 2 290.557 261.861 8 -13 3 2-253.980 196.760 5 -13 3 2 45.4328 102.903 12 -10 -3 2 126.498 230.594 5 13 -10 2 413.292 317.893 9 13 -10 2-31.5791 181.211 1 10 -13 5 1391.94 513.773 8 13 -10 5 988.850 479.834 8 10 -13 5 1959.27 1025.83 1 -10 -3 5 1204.91 398.856 5 13 -10 5 1193.71 534.007 9 -13 3 5 1222.23 327.379 2 10 -13 8 376.344 272.137 8 10 -13 8 10.2898 737.643 1 13 -10 11-200.004 268.345 6 10 -13 11-75.1086 267.732 3 13 -10 11 55.7089 273.054 3 13 -10 14 188.967 260.435 3 10 -13 14 265.552 462.059 6 13 -10 14 229.701 730.823 6 10 -13 17-230.732 1216.89 6 10 -13 17 91.1975 374.928 3 -4 13 -17 624.148 466.745 4 4 9 -14-229.970 1462.25 16 -4 13 -8-49.8630 276.332 7 4 9 -8-244.658 585.166 7 -4 13 -8 196.906 112.028 2 4 9 -5 801.935 552.125 7 -13 4 -5 1294.74 628.181 5 -13 4 -2 736.550 138.245 4 -13 4 -2 433.141 380.315 5 13 -9 1 692.647 283.884 8 13 -9 1 327.042 1074.92 1 -13 4 1 1057.69 402.939 12 -13 4 1 1827.45 583.459 5 13 -9 1 1211.27 540.489 9 -9 -4 4 113.030 106.757 5 -13 4 4 220.244 139.038 2 13 -9 4 271.641 166.068 8 13 -9 4 236.714 56.1055 9 9 -13 7 284.993 19.1986 8 13 -9 10 301.439 361.848 3 13 -9 10 13.5910 477.863 6 9 -13 10-135.591 391.621 8 13 -9 13 226.971 411.359 3 9 -13 13-3.05616 303.302 6 13 -9 13 422.024 1068.45 6 9 -13 13 214.720 144.491 3 9 -13 16 36.6495 190.451 3 9 -13 16-4308.40 1535.29 6 9 -13 19-314.381 210.256 6 9 -13 19 824.888 533.320 3 5 8 -15 462.373 332.772 9 5 8 -9 454.476 651.290 7 -5 13 -9 594.477 304.577 2 -13 5 -6 334.648 316.660 5 -13 5 -6-34.2434 302.114 4 -13 5 -6 619.095 233.109 2 -13 5 -3 4108.27 1169.84 4 -13 5 -3 4513.36 1034.25 5 13 -8 0 37.2501 27.7265 8 -13 5 0 160.810 390.486 5 -13 5 0 52.2911 93.0682 2 13 -8 0-78.5892 218.881 16 13 -8 0-58.6718 101.951 1 13 -8 0 50.4799 250.800 9 -8 -5 3 239.745 197.855 5 13 -8 3 181.074 335.132 8 -13 5 3 111.218 151.563 2 13 -8 3 261.691 399.923 9 8 -13 6 2031.47 599.542 8 8 -13 6 1043.30 392.209 1 -8 -5 6 2349.65 501.723 5 13 -8 9 38.3913 102.286 3 13 -8 9-225.417 704.954 6 8 -13 9 533.403 890.754 1 13 -8 12-130.405 370.174 3 8 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1036.49 626.912 3 -7 13 -17 2068.74 1224.13 4 -7 13 -17 435.076 376.915 2 -7 13 -14 381.471 552.478 4 7 6 -14 274.093 419.128 16 7 6 -14 23.6660 208.541 9 -13 7 -11 69.8505 445.888 5 -7 13 -11 53.0713 170.750 2 -13 7 -8 298.688 312.092 5 -7 13 -8 139.859 239.052 7 -13 7 -8 793.032 1137.24 4 -7 13 -8 248.579 190.383 2 -13 7 -5 0.65650 549.394 4 7 6 -5-151.948 327.863 7 -13 7 -5-1112.53 466.420 5 7 6 -5 320.405 432.303 9 13 -6 -2 1559.95 672.423 8 13 -6 -2 1261.63 796.545 1 -13 7 -2 1250.33 458.762 2 13 -6 -2 801.734 828.181 16 -13 7 -2 666.256 369.359 12 -13 7 -2 1060.39 456.824 5 13 -6 -2 1528.56 580.884 9 13 -6 1-41.0004 107.302 8 -13 7 1 262.508 308.344 7 -13 7 1 53.9431 201.522 2 -6 -7 4 280.507 368.543 5 13 -6 4-45.6606 157.536 3 6 -13 7 329.751 166.651 8 13 -6 7 52.4180 143.604 3 6 -13 7 569.445 802.851 1 13 -6 7 958.106 970.074 6 13 -6 7 339.868 368.516 9 -6 -7 13 1193.55 662.743 6 6 -13 16-68.8862 527.822 6 -6 -7 16 205.801 621.025 6 6 -13 16 31.3046 253.706 3 6 -13 19-216.958 964.340 6 6 -13 19 439.876 267.881 3 8 5 -15-32.1837 156.447 9 8 5 -15-113.526 882.144 16 -13 8 -12 309.504 193.328 5 8 5 -12-388.031 500.817 16 8 5 -12 163.272 321.025 9 -13 8 -9 351.259 364.491 5 -8 13 -9 170.225 122.093 2 -8 13 -9 447.875 444.032 7 -13 8 -9-246.400 724.354 4 8 5 -9 18.5835 821.925 16 -8 13 -6 2518.03 910.460 7 8 5 -6 2312.71 654.011 7 -8 13 -6 2028.53 593.111 2 -13 8 -6 1526.72 641.298 5 -13 8 -6 1021.14 524.167 12 13 -5 -3 103.172 175.756 8 -13 8 -3 272.434 217.365 2 8 5 -3 293.137 118.800 7 -13 8 -3-42.0756 297.449 7 13 -5 -3 64.8620 332.451 16 13 -5 -3 102.435 207.696 9 -13 8 -3 121.517 183.267 5 8 5 -3 262.661 640.997 9 -13 8 0 41.8174 119.674 7 -13 8 0 163.327 133.925 2 13 -5 0 166.103 634.005 16 13 -5 0-34.1042 103.622 9 13 -5 3 4136.69 802.322 3 13 -5 6 587.215 380.704 3 13 -5 6 818.709 201.034 6 13 -5 6 1194.93 743.282 9 5 -13 15 11.7137 64.8445 6 -5 -8 15-138.789 557.497 6 5 -13 15-156.237 203.936 3 5 -13 18-3997.28 1485.08 6 -5 -8 18 104.144 332.467 6 -9 13 -19 1384.57 934.458 4 -9 13 -16 392.240 565.969 4 -13 9 -13 43.4064 121.603 5 -9 13 -13-463.293 612.464 4 9 4 -13 195.402 511.052 9 -13 9 -10 698.631 235.565 4 9 4 -10 331.551 477.310 9 -13 9 -10 450.929 341.113 5 -9 13 -7 475.354 258.331 7 -9 13 -7 513.429 325.097 2 -13 9 -7 551.906 250.790 5 -13 9 -7 241.046 189.692 12 13 -4 -4 325.867 317.549 9 13 -4 -4 246.454 125.621 8 -13 9 -4 270.166 171.943 2 9 4 -4 115.899 112.724 7 13 -4 -4 4.47899 459.597 16 -13 9 -1 571.340 377.686 7 13 -4 -1 950.246 820.691 16 -13 9 -1 1235.43 405.287 2 13 -4 -1 711.872 451.138 9 13 -4 2 1034.98 372.861 3 13 -4 5 1005.72 394.592 3 13 -4 5 1315.98 607.049 6 4 -13 8 283.097 417.381 1 -4 -9 11 110.189 214.812 12 4 -13 17 261.864 1275.99 6 -4 -9 17 10.5757 676.997 6 4 -13 17-112.975 314.738 3 4 -13 20 967.100 1568.46 6 -10 13 -17 593.529 437.472 2 -13 10 -14 175.304 93.3982 5 -13 10 -14 523.465 1150.79 4 10 3 -14 168.726 718.915 16 -10 13 -14 46.2397 70.7320 5 10 3 -14-42.2345 318.864 9 -13 10 -11 77.9655 1024.31 4 -10 13 -11-51.7131 413.764 7 10 3 -11 229.359 382.776 16 10 3 -11 153.736 287.795 9 -13 10 -11 299.084 276.862 5 13 -3 -8 69.0315 355.749 8 10 3 -8 599.432 505.620 8 -10 13 -8 501.972 542.429 7 13 -3 -8 1100.46 1096.30 16 10 3 -8 358.534 1255.27 16 -13 10 -8 430.024 244.748 12 13 -3 -8 729.047 471.495 9 -13 10 -8 680.834 345.145 5 10 3 -8 502.017 475.221 9 -10 13 -8 1022.02 407.645 2 -13 10 -5 1726.20 523.890 2 13 -3 -5 1158.22 457.414 9 -10 13 -5 968.402 206.246 7 13 -3 -5 1002.71 680.316 1 -10 13 -5 873.760 369.374 2 13 -3 -5 915.628 849.098 16 13 -3 -2 136.818 140.604 9 10 3 -2 176.764 67.4618 3 13 -3 -2 112.290 630.475 16 -13 10 -2 215.915 71.3923 2 13 -3 4-20.5697 43.5868 3 13 -3 4-180.731 272.281 6 -3 -10 10 278.137 274.155 12 3 -13 16 629.217 1032.12 6 -3 -10 16 480.008 840.297 6 3 -13 19 1249.00 1020.99 6 -3 -10 19 245.572 933.617 6 -11 13 -18-972.236 1299.21 4 -13 11 -15-39.5958 246.697 5 -13 11 -15-839.984 743.611 4 -11 13 -15-214.708 100.689 5 -11 13 -12 121.406 415.982 4 11 2 -12 1418.12 1261.09 16 11 2 -12 987.866 597.559 9 -13 11 -12 192.806 354.233 5 13 -2 -9 1141.82 482.459 8 11 2 -9 984.924 468.162 8 -11 13 -9 1685.28 598.793 2 13 -2 -9 1370.18 1830.90 16 13 -2 -9 953.008 566.149 9 -13 11 -9 922.747 434.191 5 11 2 -9 902.039 601.892 9 13 -2 -6 262.682 208.003 8 11 2 -6-162.481 274.022 8 -13 11 -6-218.211 159.754 2 -11 13 -6 57.2617 174.316 7 -11 13 -6-124.881 155.787 2 13 -2 -6 74.9893 339.920 9 13 -2 -3 34.5635 78.0928 8 -13 11 -3-124.993 393.423 7 -13 11 -3 144.962 109.396 2 13 -2 -3-60.8635 224.481 16 13 -2 -3 445.127 424.477 9 13 -2 0-19.3142 225.354 8 11 2 0 71.5873 97.5553 3 13 -2 0 249.808 436.584 3 11 2 0 391.849 587.113 9 13 -2 3 34.9118 178.005 3 2 -13 18-4742.64 1587.37 6 -2 -11 18-2850.58 1129.59 6 2 -13 21-3941.69 1536.29 6 -12 13 -16 11.5231 520.115 4 -12 13 -16 382.871 392.015 5 -13 12 -16 268.634 324.263 5 -13 12 -13 553.153 106.258 4 -12 13 -13 676.458 340.879 5 -13 12 -13 648.037 388.843 5 13 -1 -10 581.468 501.040 8 12 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130.452 186.110 7 -13 13 -5 216.588 238.108 2 13 0 -5 6.48764 429.138 9 13 0 1-43.1327 130.106 3 0 -13 19-2474.51 1148.06 6 0 14 -11 26.9415 239.369 7 -14 0 -2 803.592 670.551 5 -14 0 1 111.127 291.627 5 -14 0 4 952.835 442.455 5 -14 0 4 800.551 629.707 12 14 -14 7-52.2223 92.5927 8 14 -14 13-517.138 602.316 3 14 -14 16 1690.48 1983.80 6 -1 14 -9 192.082 416.008 7 1 13 -9 916.943 695.898 7 -1 14 -9 572.578 333.388 2 -14 1 -3 131.971 281.279 5 -13 -1 0 325.949 384.658 5 -14 1 0-337.390 465.472 5 -14 1 3 350.765 197.260 12 -14 1 3 101.942 107.659 5 -13 -1 3-82.2190 244.191 5 13 -14 6 308.907 394.655 8 14 -13 6 158.659 67.0205 8 -13 -1 6-317.956 212.127 12 14 -13 6 33.8106 1066.32 1 13 -14 9-38.9058 114.671 8 14 -13 9 261.549 236.225 8 13 -14 12-57.2291 354.330 3 14 -13 12-35.0031 174.864 3 13 -14 15 300.079 286.215 6 14 -13 15-245.204 704.303 6 14 -13 15-101.591 422.350 3 13 -14 15 306.835 378.909 3 13 -14 18 277.583 373.515 6 13 -14 18-88.5921 150.500 3 -2 14 -13-605.515 650.900 7 -2 14 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14 -11 1 81.0152 148.018 9 -14 3 1-240.700 278.212 12 -14 3 1 11.2986 111.731 5 14 -11 4 175.543 177.243 9 14 -11 4 164.731 175.409 8 -11 -3 4 26.6424 247.396 5 14 -11 4-479.046 477.023 1 11 -14 7 211.301 188.379 8 -11 -3 7 221.688 442.795 12 14 -11 7 366.883 560.938 8 14 -11 7 232.311 280.411 3 11 -14 10-192.933 519.003 8 14 -11 10 99.3051 689.872 6 14 -11 13-250.495 151.435 8 14 -11 13 847.658 1007.82 6 11 -14 13 259.928 175.226 3 14 -11 13-33.6084 384.179 3 11 -14 16-582.622 1134.36 6 11 -14 19 158.640 1388.34 6 11 -14 19-14.7877 413.166 3 -4 14 -12 127.429 226.643 2 4 10 -12-165.494 339.335 9 -4 14 -9-3.90524 487.476 7 4 10 -9 1093.52 790.784 7 -4 14 -9 534.544 331.612 2 -14 4 -6-553.535 451.182 5 4 10 -6 140.275 328.616 7 -14 4 -3-215.653 89.7101 5 14 -10 0 373.995 186.162 8 14 -10 0 242.060 353.804 1 -14 4 0 388.566 302.047 12 14 -10 0 666.017 390.321 9 -14 4 0 910.181 417.631 5 -10 -4 3 137.377 282.993 5 14 -10 3-44.3738 482.667 1 14 -10 3 452.553 395.568 9 10 -14 6-71.0051 240.221 8 14 -10 6 113.285 251.453 8 14 -10 6-35.2331 388.645 3 -14 4 6 168.587 147.084 2 -10 -4 6 76.9844 178.316 5 14 -10 9-143.733 529.346 8 14 -10 9 367.997 544.718 6 -10 -4 9 236.604 392.007 12 14 -10 9 49.6476 104.967 3 14 -10 12-34.1917 286.358 3 14 -10 12-658.447 552.990 8 14 -10 12 317.810 533.400 6 10 -14 15 582.738 1368.77 6 10 -14 15 214.940 96.0371 3 10 -14 18 1030.07 792.725 6 10 -14 18 449.381 591.491 3 -5 14 -19 994.591 1056.54 4 -5 14 -13-331.148 615.171 7 -5 14 -10 315.947 295.475 2 -5 14 -10-87.4086 390.575 7 5 9 -10 185.799 84.5626 9 -14 5 -7 955.289 641.382 5 5 9 -7 396.092 316.544 7 -14 5 -4 558.228 364.807 5 14 -9 -1-946.791 425.921 8 14 -9 -1-8.01521 529.740 1 -14 5 -1 199.676 239.063 12 14 -9 -1 99.4944 470.575 16 14 -9 -1-100.954 299.209 9 -14 5 -1-366.122 336.579 5 -9 -5 2 59.3189 371.758 5 -14 5 2 154.543 61.5845 2 14 -9 2 605.352 375.541 9 14 -9 2 73.4120 526.887 1 14 -9 5-252.380 437.260 8 14 -9 5 166.706 181.599 3 -14 5 5 137.621 103.250 2 -9 -5 5 218.331 67.1245 5 14 -9 8 267.667 221.151 6 -9 -5 8-228.978 70.5303 12 14 -9 8 84.0814 197.375 3 14 -9 11 577.565 426.736 3 14 -9 11 120.453 712.227 6 9 -14 14 135.598 189.564 3 9 -14 17-724.779 916.997 6 9 -14 20-179.794 1020.95 6 9 -14 20 669.707 500.091 3 -6 14 -17-361.464 645.227 4 6 8 -14 298.152 1396.31 16 -6 14 -11-20.4553 396.954 7 -14 6 -8 120.402 463.819 5 -6 14 -8 90.8438 246.928 7 -6 14 -8 299.302 183.545 2 6 8 -8 334.253 465.637 9 6 8 -5 338.475 225.234 7 -14 6 -5-182.962 380.733 5 14 -8 -2 377.595 310.377 8 14 -8 -2 1177.91 647.392 1 -14 6 -2 159.799 86.3135 5 14 -8 -2 295.701 366.536 16 -14 6 -2 355.950 362.097 12 14 -8 -2 588.471 370.418 9 14 -8 1 234.331 670.045 1 -14 6 1 1500.36 370.635 2 14 -8 1 2053.96 676.450 9 14 -8 4 1592.41 730.297 8 -8 -6 4 387.154 208.946 5 -14 6 4 930.765 336.903 2 14 -8 4 845.601 493.334 3 8 -14 7 919.986 416.916 8 14 -8 7 108.787 197.671 8 14 -8 7 1460.21 850.816 6 8 -14 7 1351.91 1123.28 1 14 -8 7 192.314 94.4956 3 14 -8 10 5.74835 143.083 3 14 -8 10-348.225 529.403 6 -8 -6 10 67.5177 219.875 12 8 -14 16 105.761 447.096 6 8 -14 16 343.800 182.970 3 8 -14 19 485.160 1376.87 6 7 7 -15 34.1050 249.004 9 -7 14 -12 290.052 364.372 2 7 7 -12-667.646 1255.62 16 -7 14 -9 84.5874 108.446 2 -14 7 -9 40.2050 164.735 2 -14 7 -6 461.656 385.229 5 7 7 -6 648.086 533.997 9 14 -7 -3-27.7402 215.962 8 14 -7 -3-41.6562 107.215 1 -14 7 -3-132.149 144.112 12 14 -7 -3 139.667 312.013 9 -14 7 -3-293.100 318.174 5 -14 7 0 944.476 318.998 2 14 -7 0 579.106 448.212 8 14 -7 0 1425.71 562.611 9 14 -7 0 552.619 733.554 16 14 -7 0 313.095 474.659 1 14 -7 3-99.7426 143.951 8 -14 7 3 12.6892 112.242 2 14 -7 3 132.324 308.924 3 14 -7 6 263.442 406.968 8 14 -7 6 994.288 485.936 6 14 -7 6 41.4833 206.101 3 14 -7 9 108.220 117.701 3 14 -7 9 270.676 457.799 6 -7 -7 9 258.392 465.344 12 7 -14 15 46.8288 135.070 3 7 -14 18-1760.29 1005.82 6 7 -14 18-411.546 326.562 3 7 -14 21-4264.31 1709.52 6 -8 14 -16 348.990 488.338 4 8 6 -16 127.159 323.129 9 8 6 -13 1.17437 475.466 9 -14 8 -10-29.3989 221.474 5 -8 14 -10-58.8146 212.046 2 -8 14 -10 243.261 187.782 7 -8 14 -7 759.231 468.920 7 -14 8 -7 1784.23 957.526 4 -8 14 -7 858.133 426.553 2 -14 8 -7 717.258 468.114 5 14 -6 -4 1318.74 531.005 8 8 6 -4 1081.56 409.742 7 14 -6 -4 468.093 513.283 1 -14 8 -4 476.228 378.276 5 14 -6 -4 993.729 482.280 9 14 -6 -1 1488.16 671.919 8 -14 8 -1 691.598 434.972 7 14 -6 -1 1917.85 939.838 16 14 -6 -1 2007.41 725.762 9 -14 8 -1 1695.61 472.477 2 14 -6 2 639.971 413.368 8 -14 8 2 503.861 304.550 2 14 -6 2 407.923 253.636 3 14 -6 5 5.37109 258.962 8 14 -6 5 300.822 127.481 6 14 -6 5 128.889 142.677 3 6 -14 8-987.424 1240.72 1 14 -6 8 108.912 130.905 3 14 -6 8 238.728 349.295 6 -6 -8 11-128.650 199.552 12 -6 -8 17 595.215 867.174 6 6 -14 17-138.925 86.4037 3 6 -14 20 88.2407 977.945 6 -9 14 -20-1024.33 880.078 4 9 5 -14-10.7993 316.052 16 9 5 -14-191.901 353.694 9 -14 9 -11-144.333 448.988 5 -14 9 -11-299.692 1223.49 4 9 5 -11 161.442 572.654 9 -14 9 -8 400.964 624.837 4 -9 14 -8-18.3569 325.067 7 -9 14 -8-40.3691 137.055 2 -14 9 -8 550.221 323.744 5 -14 9 -8-162.021 261.042 12 14 -5 -5-37.7732 163.934 8 14 -5 -5-298.619 522.581 1 -14 9 -5 22.0449 179.882 2 14 -5 -5 107.357 501.176 16 -14 9 -5-35.0016 65.6522 5 14 -5 -5-97.8785 188.549 9 14 -5 -2-53.1859 168.601 8 -14 9 -2 81.5643 122.093 7 14 -5 -2 10.5872 115.229 9 -14 9 -2-71.8692 203.729 2 -14 9 1-89.0048 106.761 7 14 -5 1-63.0650 245.484 3 -14 9 1 130.808 204.366 2 14 -5 4-90.7086 438.311 8 14 -5 4 406.909 325.529 3 14 -5 7 466.149 400.967 3 14 -5 7 291.103 379.067 6 -5 -9 10 292.056 293.105 12 5 -14 10 365.760 548.290 1 -5 -9 16 406.442 356.046 6 5 -14 19 2244.53 2022.82 6 -5 -9 19 471.121 911.405 6 5 -14 19 667.790 488.624 3 -10 14 -18-178.329 132.878 2 -10 14 -18 1071.38 1371.43 4 10 4 -15 551.149 1195.19 16 10 4 -15 102.027 319.901 9 -14 10 -12 322.593 791.129 4 10 4 -12 61.0377 135.860 9 -14 10 -12-883.377 495.984 5 -10 14 -9-40.8453 204.774 2 -14 10 -9 342.018 343.984 4 -10 14 -9 248.092 626.378 7 -14 10 -9 162.878 147.879 12 10 4 -9-358.348 1584.30 16 -14 10 -9-263.067 240.091 5 14 -4 -6 39.5345 139.025 8 -10 14 -6 392.407 425.694 7 14 -4 -6-9.27444 381.226 1 -14 10 -6-221.275 278.393 2 14 -4 -6-39.0945 695.541 16 -10 14 -6-40.9730 272.733 2 -14 10 -6 231.332 279.379 5 14 -4 -6 315.481 234.462 9 14 -4 -3 689.290 503.749 8 -14 10 -3 549.025 348.483 7 14 -4 -3 59.5000 143.595 9 -14 10 -3 82.7065 178.390 2 14 -4 0 512.526 530.465 8 -14 10 0 225.392 112.489 2 14 -4 3 370.947 261.855 3 14 -4 6 340.412 589.173 8 14 -4 6 70.9805 193.523 3 4 -14 18 16.5267 808.055 6 -4 -10 18 1366.20 2388.30 6 4 -14 21 417.948 346.072 6 -11 14 -19-987.968 766.850 4 -14 11 -13-537.985 448.942 4 11 3 -13-56.8223 318.475 9 -14 11 -13-343.863 465.559 5 -14 11 -10 392.224 361.088 5 11 3 -10-19.0093 344.687 9 14 -3 -7-7.14978 156.472 8 -11 14 -7-164.332 526.156 7 -14 11 -7 82.8760 136.156 2 14 -3 -7-203.220 408.108 16 -11 14 -7 169.420 235.230 2 14 -3 -7-58.7684 215.818 9 -14 11 -4 105.254 317.349 7 14 -3 -4-65.5646 314.538 9 -14 11 -4 143.904 132.155 2 -14 11 -1 146.400 142.138 2 11 3 -1 91.0190 193.843 9 14 -3 2 789.199 296.888 3 14 -3 5 1458.33 729.520 8 14 -3 5 563.817 271.639 3 3 -14 20 661.599 1362.41 6 -3 -11 20 252.728 1137.78 6 -12 14 -14 116.923 71.0120 4 -14 12 -14 11.5227 71.0013 5 12 2 -11 498.467 895.347 16 12 2 -11 9.67670 512.069 9 -14 12 -11 37.6211 132.864 5 -12 14 -8-104.909 179.985 2 -12 14 -8 303.053 481.586 7 -14 12 -8 261.288 484.038 2 14 -2 -8 565.286 840.992 16 12 2 -8 388.243 1055.84 16 14 -2 -8 940.870 644.105 9 12 2 -8 229.896 379.160 9 -12 14 -5 740.374 609.663 7 -14 12 -5 211.440 373.207 7 -12 14 -5 162.067 144.061 2 14 -2 -5 429.380 285.021 9 -14 12 -5 195.156 160.747 2 -14 12 -2 332.079 152.202 7 -14 12 -2 1245.99 514.403 2 14 -2 1-20.4971 57.9495 3 14 -2 4-12.1075 115.098 3 2 -14 10-431.691 698.986 1 -2 -12 19-1629.27 1377.39 6 2 -14 22-53.7940 154.803 6 -13 14 -18-1227.84 970.232 4 -13 14 -15 174.745 186.999 5 -14 13 -15 85.4036 61.1457 5 -14 13 -12 522.266 417.315 5 13 1 -12 23.5392 261.959 9 14 -1 -9 563.241 432.456 8 13 1 -9 248.012 428.908 8 -14 13 -9 8.10757 226.770 2 14 -1 -9-244.570 486.806 9 13 1 -9-67.1719 276.431 9 -14 13 -6-100.070 35.7081 2 14 -1 -6-67.5518 442.417 8 13 1 -6-217.408 292.073 8 -13 14 -6-169.900 404.753 7 -14 13 -6 1.11389 455.856 7 -13 14 -6-11.4588 56.3120 2 14 -1 -6-166.819 107.514 9 -14 13 -3 145.672 105.807 2 14 -1 3 562.203 267.426 3 14 -1 3 432.349 726.661 9 1 -14 21-325.007 1294.45 6 -1 -13 21-615.511 1361.13 6 -14 14 -16 1354.23 693.798 5 -14 14 -13 242.541 578.341 4 14 0 -10-70.6540 617.625 16 14 0 -10 111.317 139.650 9 -14 14 -7-43.4228 95.3490 2 14 0 -7-40.1422 469.037 8 -14 14 -7 92.6309 527.689 7 14 0 -7 28.3123 783.386 16 14 0 -7-210.233 172.932 9 14 0 2 276.380 235.759 3 -15 0 0 237.803 184.614 5 -15 0 3 366.897 306.574 5 15 -15 6 861.866 606.985 8 -15 0 6 713.998 502.910 12 15 -15 9 197.623 572.567 8 15 -15 15-75.4347 818.776 8 15 -15 15-416.363 682.798 3 15 -15 18-378.042 951.731 6 1 14 -13-683.232 591.552 7 1 14 -10 396.025 371.533 7 -14 -1 -1 1106.58 564.026 5 -15 1 -1 497.784 487.190 5 -15 1 2 306.902 226.540 5 -14 -1 2 204.071 260.429 5 -14 -1 5 678.605 546.973 5 -14 -1 5 279.450 361.894 12 15 -14 11 213.458 260.581 8 15 -14 11-21.9324 234.525 3 14 -15 14 924.504 670.836 3 15 -14 14 334.082 612.308 3 14 -15 17 1882.31 1863.37 6 15 -14 17-396.625 1692.93 6 14 -15 17 154.238 238.224 3 15 -14 17-1065.84 680.004 3 -2 15 -14 217.943 679.193 7 -2 15 -11 763.921 791.866 7 -15 2 -2 424.877 120.624 5 -13 -2 1-88.1019 368.504 5 -15 2 1 537.549 379.941 5 15 -13 4 559.339 252.671 9 -13 -2 4 494.191 99.0295 5 13 -15 10 401.592 134.982 8 15 -13 10 313.484 445.533 3 15 -13 13 122.808 623.713 6 15 -13 16 1045.95 1131.87 6 13 -15 16 154.288 377.719 3 15 -13 16 322.458 800.984 3 13 -15 19-118.755 890.746 6 3 12 -12-63.5528 362.549 7 -3 15 -12 155.808 317.199 2 -15 3 -3-337.446 280.400 4 -15 3 -3 39.4107 113.372 5 -15 3 0 652.012 357.022 5 -15 3 0 581.487 267.981 2 15 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601.215 1092.94 3 13 -16 20 41.5897 1082.19 6 13 -16 20 539.267 712.301 3 -4 16 -14-96.6112 307.704 7 -4 16 -11 2118.26 776.968 2 -4 16 -11-33.3216 466.080 7 4 12 -8 488.484 545.945 7 -16 4 -5 60.4728 293.320 5 -16 4 -5 239.105 397.733 4 -16 4 -2 907.332 589.442 5 -16 4 1-93.9198 321.061 12 -16 4 1-136.987 286.490 5 16 -12 4 277.949 138.563 8 16 -12 4 284.142 128.616 9 -12 -4 4 591.034 179.574 5 16 -12 7-5.65262 617.077 8 -12 -4 7-163.178 295.152 12 16 -12 10 130.718 60.5113 3 16 -12 13 38.1082 223.706 8 16 -12 13-624.620 987.587 6 16 -12 13-81.9698 107.724 3 12 -16 16-884.766 557.652 3 12 -16 19 119.580 1427.76 6 12 -16 19-309.682 351.483 3 -5 16 -12 356.049 801.290 7 5 11 -9 667.825 602.234 7 -16 5 -6 363.842 220.867 5 -16 5 -6 1911.19 1190.37 4 -16 5 -3-128.251 133.256 5 -16 5 0 509.674 452.780 5 -16 5 0 731.130 549.837 12 16 -11 0 1771.71 1065.03 1 -11 -5 3 709.015 393.456 5 16 -11 3 737.227 507.855 8 -16 5 3 765.091 348.459 2 16 -11 3 630.737 386.828 9 16 -11 6-60.3329 293.764 8 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360.693 408.343 8 16 -8 9 105.999 308.796 6 16 -8 9 55.6412 129.215 3 8 -16 21 175.498 584.876 6 8 -16 21-193.204 345.616 3 -9 16 -19 189.680 238.928 2 -9 16 -13 649.681 1080.63 7 -9 16 -10 321.609 144.842 2 -9 16 -10 79.6260 542.237 7 -16 9 -10 421.622 482.216 5 -16 9 -7-90.1487 266.863 12 -16 9 -7 42.1963 351.612 5 9 7 -7-137.199 502.645 9 16 -7 -4 18.7878 133.796 8 16 -7 -4 363.952 552.529 16 -16 9 -4 480.394 302.095 5 16 -7 -4-280.929 340.957 9 16 -7 -1 104.266 419.431 8 -16 9 -1 178.372 259.036 2 16 -7 -1 478.758 462.506 9 16 -7 2-269.370 289.830 8 -16 9 2 341.128 249.498 2 16 -7 5 270.211 405.142 8 16 -7 8 341.200 427.879 3 -10 16 -20-786.860 417.596 4 10 6 -17 414.200 589.982 9 10 6 -14-516.814 915.347 16 -10 16 -11-54.4206 92.7404 2 -16 10 -11 32.4384 340.313 5 -10 16 -8-237.460 241.363 2 -16 10 -8 64.7310 190.633 5 16 -6 -5 739.246 425.280 8 16 -6 -5 209.348 791.491 16 16 -6 -5 310.730 170.758 9 10 6 -5-242.936 537.081 9 16 -6 -2-71.8589 329.352 8 -16 10 -2-50.9160 80.2171 2 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-12-649.407 491.875 5 -19 11 -9 838.039 1128.92 4 -19 11 -9 841.465 529.600 12 -19 11 -9 563.721 480.934 5 19 -8 -3 302.470 405.817 8 19 -8 -3-301.737 50.8054 9 19 -8 0-344.376 75.4426 8 -19 11 0 193.876 220.241 2 19 -8 0 681.508 715.460 9 19 -8 6-198.383 410.176 3 19 -8 9 1292.36 1467.21 8 19 -8 9 204.373 493.573 3 -19 12 -13-184.198 200.245 2 -12 19 -13-408.389 458.902 2 -19 12 -13 695.263 736.302 5 -19 12 -10 800.657 805.236 4 -19 12 -10-331.899 152.162 5 -19 12 -4 293.289 245.239 2 19 -7 -4-357.553 286.666 9 -19 12 -1-43.6450 193.104 2 19 -7 -1 8.03219 181.948 8 19 -7 5 241.427 518.720 3 19 -7 8-711.486 1073.67 8 19 -7 8 413.572 455.837 3 -13 19 -20 249.638 169.276 2 -19 13 -14 84.8611 252.023 2 -19 13 -14-77.8796 238.512 5 -13 19 -11-788.353 475.625 2 -19 13 -11-369.050 537.814 5 -19 13 -5-544.389 386.377 2 19 -6 -5 243.039 293.150 9 -19 13 -2 6.10179 161.678 2 19 -6 -2 510.949 600.005 8 19 -6 1-39.6557 57.5829 8 19 -6 4-47.4931 326.091 3 19 -6 7 300.239 465.734 3 -19 14 -15-864.953 452.478 2 -19 14 -15 437.151 385.236 5 -14 19 -12 610.138 668.077 2 -19 14 -12 1888.60 774.297 5 -19 14 -6 1413.53 693.477 2 19 -5 -6 1105.66 1309.89 16 19 -5 -6 407.535 442.120 9 14 5 -6 688.962 393.249 9 -19 14 -3 88.4008 267.120 2 19 -5 -3-1225.16 687.961 8 19 -5 0 354.398 876.325 8 19 -5 3 199.783 200.216 3 19 -5 6 383.417 308.922 3 -19 15 -16 606.627 455.984 2 -19 15 -16 456.525 154.225 4 15 4 -16-302.610 1590.67 16 19 -4 -7 388.370 406.813 8 -19 15 -7-16.6806 350.841 2 19 -4 -7 38.0811 324.154 16 19 -4 -7-434.079 683.514 9 -19 15 -4 5.88578 247.175 2 15 4 -4 1336.12 1243.47 9 19 -4 5 777.226 461.931 3 -16 19 -20-39.8534 160.919 2 -19 16 -17-163.268 173.614 2 -19 16 -17 895.936 1421.25 4 -16 19 -11 216.574 400.989 7 -16 19 -11 361.322 430.408 2 19 -3 -8 963.475 858.657 8 -19 16 -8 460.504 437.884 2 19 -3 -8 69.9290 1322.33 16 19 -3 -8-213.419 224.196 9 19 -2 -9 374.188 733.869 9 19 -2 -6 4987.68 2210.28 8 17 2 -3-195.421 59.3203 9 19 -2 0-552.238 898.690 8 -18 19 -19 333.396 482.402 2 -18 19 -10 123.810 925.535 7 -18 19 -10 1169.28 571.915 2 19 0 -5 40.1081 803.398 8 -20 1 0 21.7684 256.590 5 -19 -1 3 10.4154 548.061 5 -19 -1 3 42.5152 619.466 12 -19 -1 6 19.7390 613.532 12 20 -19 12 618.742 817.824 8 -20 2 -1 27.4358 460.508 5 -20 2 2-7.66357 176.832 12 -18 -2 5 20.2676 313.432 12 -20 3 -2-143.554 296.439 5 -20 3 1 311.005 623.485 5 -20 3 1-665.357 519.993 12 20 -17 7-848.909 615.329 8 -20 4 -3 3.27063 113.304 5 -20 4 0 33.7522 637.588 12 -20 4 0 29.2041 486.348 5 -16 -4 6 26.8772 387.268 12 -16 -4 9 102.078 427.570 12 20 -16 15 790.984 696.760 8 20 -16 15-620.173 561.438 3 -20 5 -4-161.821 347.091 5 -20 5 -1 7.04896 355.295 12 -20 5 -1-12.2223 371.408 5 -15 -5 8 279.854 827.775 12 20 -15 14 239.983 753.181 8 20 -15 14 1001.74 698.070 3 -20 6 -5 262.484 503.323 5 -20 6 -2-167.959 94.0567 5 -14 -6 10-32.3402 579.631 12 20 -14 13-1336.30 765.949 3 -7 20 -15 134.240 562.528 7 -20 7 -6-442.981 465.227 5 -20 7 -3-116.889 525.851 5 -20 7 -3-269.519 320.302 2 20 -13 3 18.7383 299.694 9 -13 -7 9 0.23537 250.606 12 20 -13 12-512.591 463.642 3 -20 8 -7 21.2983 208.779 12 -20 8 -7-364.343 592.193 5 -20 8 -4-258.086 443.264 5 20 -12 2 739.956 729.402 9 20 -12 5-142.203 663.656 8 -12 -8 11 305.734 161.397 12 20 -12 11 48.0270 527.461 3 -20 9 -8-12.3041 166.573 12 -20 9 -8 193.996 562.640 5 -20 9 -5 3.24972 243.721 12 -20 9 -5-152.508 351.481 5 20 -11 1 282.233 359.332 9 20 -11 4 67.7220 279.465 8 -11 -9 10 700.817 715.261 12 20 -11 10-38.0550 475.195 3 -10 20 -21-1294.62 985.987 2 -20 10 -9-334.656 254.456 2 -20 10 -9 95.0984 399.651 12 -20 10 -9 104.227 404.399 5 -20 10 -6 96.4155 291.222 5 -20 10 0 1117.22 633.228 2 20 -10 0 316.246 587.366 9 20 -10 9 5.51130 209.220 3 -20 11 -10 704.885 851.540 4 -20 11 -10-125.097 205.237 2 -20 11 -10 25.8837 180.890 5 -20 11 -7 264.225 529.862 5 -20 11 -1 116.012 226.835 2 20 -9 -1-66.5080 235.379 9 20 -9 8-148.849 240.743 3 -12 20 -14-345.013 1111.67 7 -20 12 -11 45.2395 899.294 4 -20 12 -11-304.986 373.054 5 12 8 -11 740.018 1150.81 9 20 -8 -2-78.5589 377.594 9 20 -8 7 443.014 497.476 3 -13 20 -21 220.131 288.999 2 -20 13 -12-108.832 228.068 4 -20 13 -12-2404.87 916.286 5 13 7 -9-281.482 560.682 9 20 -7 -3 25.3572 433.564 8 20 -7 -3 74.8749 433.912 9 20 -7 6 309.129 514.541 3 20 -7 6-461.064 783.867 9 -14 20 -13-311.458 430.409 7 -14 20 -13-47.2403 175.459 2 -20 14 -13 29.8613 405.894 5 14 6 -7 127.721 307.860 9 20 -6 -4-89.5161 604.374 8 20 -6 -4 305.615 632.700 9 20 -6 5 95.4598 318.004 3 20 -6 5-629.694 586.215 9 20 -5 -5 14.5350 360.478 8 20 -5 -5 418.779 290.308 9 20 -5 4-191.752 326.313 8 20 -5 4-278.574 491.979 9 -16 20 -12-343.936 905.843 7 -16 20 -12 594.905 600.234 2 20 -4 -3-1089.58 714.312 8 20 -4 3-95.8438 613.064 8 20 -4 3 1282.62 857.529 9 17 3 -4-1073.59 822.539 9 20 -3 2-144.834 405.369 9 -18 20 -20 381.277 446.660 2 -18 20 -11-55.0588 438.098 2 20 -2 -8 488.976 886.424 8 -20 18 -8 192.347 270.552 2 20 -2 1 120.915 337.532 9 -20 19 -18 172.444 250.887 2 -20 19 -9-157.090 422.836 2 20 -1 -3-2051.05 1101.06 8 19 1 -3 439.579 539.226 9 20 -1 0-142.803 223.101 9 -20 20 -19 229.359 251.776 2 -21 1 2-40.0328 578.686 12 -20 -1 2-143.216 643.467 12 -21 2 1 108.031 786.965 5 -21 2 1 21.3027 809.687 12 -19 -2 4 14.9719 752.970 12 -19 -2 7-19.4439 253.374 12 -21 3 0 262.514 578.652 12 -21 3 0 32.1825 543.985 5 -21 3 3 33.2843 451.685 12 -18 -3 6 50.3539 415.593 12 21 -18 15 319.328 1116.69 8 -21 4 -1 70.2780 108.371 12 -21 4 -1-15.4356 449.793 5 -21 4 2 4.82851 499.434 12 21 -17 8 513.266 278.868 8 -21 5 -5-122.288 43.0588 5 -21 5 -2-9.86413 481.345 12 -21 5 -2 269.366 106.083 5 -21 5 1-0.55266 196.264 12 21 -16 7 135.448 281.917 8 -16 -5 7 54.8050 497.736 12 21 -16 10 711.082 1103.99 8 21 -16 16-1568.10 933.087 3 -21 6 -6-94.6268 525.279 5 -21 6 -3 16.2878 437.809 12 -21 6 -3 42.3866 518.845 5 21 -15 6-773.507 689.937 8 21 -15 9-2153.52 1085.61 8 21 -15 15-636.831 734.185 3 -21 7 -7-32.8206 497.555 5 -21 7 -4 25.1394 621.820 12 -21 7 -4 26.1792 672.251 5 21 -14 5 384.785 291.307 8 21 -14 8-25.1951 426.786 8 -14 -7 8-4.17879 311.053 12 21 -14 14-80.7026 102.114 3 -21 8 -8 890.348 718.918 5 -21 8 -5 49.9079 661.805 5 21 -13 4 216.851 151.397 8 21 -13 13 9.73482 287.247 3 -21 9 -9-177.695 390.636 12 -21 9 -9 341.557 486.926 5 -21 9 -6 204.830 129.481 5 -21 9 -6 32.2962 70.7385 2 21 -12 3 390.984 436.881 8 -12 -9 9 1.70528 262.758 12 21 -12 12-548.614 731.698 8 21 -12 12 65.0270 390.506 3 -21 10 -10 76.5438 715.803 12 -21 10 -10 209.596 596.789 5 -21 10 -7 13.4633 330.488 12 -21 10 -7 1071.22 717.200 5 21 -11 -1-274.585 345.862 9 21 -11 2 476.409 444.490 8 21 -11 8 298.991 330.972 9 21 -11 11-75.5614 1072.58 8 21 -11 11 19.3849 385.845 3 -21 11 -11-635.703 616.571 5 -21 11 -8-42.8507 237.002 5 21 -10 -2 165.348 104.555 9 21 -10 1 129.451 721.036 8 21 -10 7 94.1538 304.650 9 21 -10 10 418.834 1094.56 8 21 -10 10 117.318 258.026 3 -12 21 -21-147.557 17.4933 2 -21 12 -12-176.479 209.994 5 -21 12 -9 183.812 577.219 5 21 -9 -3 900.334 694.329 9 21 -9 0 34.8236 704.254 8 21 -9 3-221.372 576.096 8 21 -9 9-212.984 500.828 8 21 -9 9 87.6322 83.7713 3 -21 13 -13-576.709 395.611 4 -21 13 -13-397.929 148.734 5 21 -8 -4 258.139 381.350 9 21 -8 -1-68.7690 432.788 8 21 -8 2 340.577 664.711 8 21 -8 8 804.719 416.501 8 21 -8 8 542.732 844.654 3 -21 14 -14-1044.84 425.279 4 -21 14 -14-356.310 391.886 5 21 -7 -5 546.511 559.496 9 21 -7 1-72.7924 589.324 8 21 -7 7 1041.88 677.534 3 -15 21 -21 247.867 568.145 2 -21 15 -15-144.905 649.511 5 21 -6 -6 307.139 154.187 8 21 -6 -6 24.5154 318.373 9 21 -5 -7 206.098 482.380 8 21 -5 -7-302.029 530.323 9 16 5 -7 977.214 385.492 9 21 -4 -8 1330.14 961.357 8 21 -4 -8 373.355 889.393 9 21 -4 -5-148.476 611.093 8 21 -3 0-850.386 418.415 8 19 2 -4 531.932 1634.88 9 -20 21 -20 185.659 182.064 2 21 -1 -5 1251.31 1061.22 8 21 0 -3 1010.71 859.280 9 -22 1 1-129.953 446.150 12 -22 1 4 16.4293 2047.71 12 -22 2 0 26.8066 447.314 12 -22 2 0 9.85126 454.221 5 -22 2 3 49.6736 943.075 12 -20 -2 6 29.8211 694.870 12 -22 3 -1-0.68939 290.431 12 -22 3 -1-4.63499 285.411 5 -22 3 2 136.417 349.595 12 -19 -3 5 204.265 910.343 12 22 -19 11 332.518 456.450 8 -22 4 -2 424.552 1079.12 12 -22 4 -2 0.49412 455.519 5 -22 4 1 125.848 296.146 12 22 -18 10 297.991 961.887 8 -22 5 -3 185.717 924.454 12 -22 5 -3-46.7697 516.956 5 -22 5 0 187.998 482.142 12 -17 -5 6-0.61284 176.445 12 -17 -5 9-4.81317 724.340 12 22 -17 15-1861.28 1183.97 8 -22 6 -4-2.88459 418.641 12 -22 6 -4 49.1163 702.733 5 -22 6 -1 8.25717 541.107 12 22 -16 5 308.465 803.302 8 -16 -6 8-61.3623 520.794 12 22 -16 14-230.920 480.208 8 -22 7 -5 253.744 502.044 12 -22 7 -5-25.8825 564.219 5 -22 7 -2 69.4518 592.802 12 22 -15 4 237.736 863.551 8 -15 -7 10 3.96260 558.123 12 22 -15 13 479.725 528.963 8 -22 8 -6 14.8640 493.003 12 -22 8 -6-11.4061 302.977 5 -14 -8 9-31.6318 361.727 12 -22 9 -7 79.4348 758.148 5 22 -13 11-39.0354 295.322 3 -13 -9 11 13.7846 495.536 12 -22 10 -8 257.760 338.026 5 22 -12 1 10.4488 407.342 9 22 -12 10 628.422 609.194 3 -22 11 -9 687.907 647.885 12 -22 11 -9 87.7234 235.247 5 22 -11 0-36.5850 275.198 8 22 -11 0-219.877 172.566 9 22 -11 9-47.8597 183.530 3 -22 12 -10-122.962 268.091 2 -22 12 -10-37.1477 626.694 5 22 -10 -1 743.266 1035.97 8 22 -10 -1-205.331 521.219 9 22 -10 8-14.3961 139.760 3 13 9 -14 211.192 1365.18 9 -22 13 -11-61.0668 352.586 5 -22 13 -11-112.308 162.115 2 22 -9 -2-1779.52 880.797 8 22 -9 -2 410.985 642.117 9 22 -9 7 240.608 275.236 3 -14 22 -21-136.905 201.730 2 -22 14 -12 98.1180 385.066 2 14 8 -12-168.019 465.557 9 22 -8 -3-25.8123 315.787 8 -22 14 -3 188.737 269.786 2 15 7 -10 391.469 523.626 9 22 -7 -4 716.531 739.328 8 -22 15 -4 458.127 237.362 2 22 -7 5 59.9598 386.511 9 -22 16 -5-182.316 198.496 2 22 -6 -2 119.605 413.516 8 22 -6 4-713.794 1034.11 8 22 -6 4-598.279 989.228 9 -17 22 -21 16.7989 162.186 2 22 -5 3 240.176 956.993 8 22 -5 3-500.130 783.237 9 -22 18 -16-33.8250 107.761 2 18 4 -7 1606.76 2083.71 9 22 -4 2-471.468 340.396 9 -19 22 -20 441.520 381.897 2 -22 19 -17 87.4205 130.704 2 22 -3 -8 451.035 594.664 8 22 -3 1 144.541 469.618 9 -22 20 -18-427.655 318.941 2 22 -2 -3-418.258 678.492 8 -22 21 -19-648.922 393.784 2 21 1 -4-221.032 646.750 9 -23 0 4-28.3478 746.279 12 -23 1 3 0.36407 370.285 12 -23 2 2-0.71104 607.118 12 -23 3 1 251.771 621.729 12 -20 -3 7-9.89237 833.223 12 -23 4 0 153.679 620.775 12 -19 -4 6 5.34791 291.295 12 23 -19 15-21.8589 1108.42 8 -23 5 -1 125.200 233.255 12 -23 6 -5-11.0072 447.231 5 -23 6 -2 125.734 1019.51 12 -23 7 -6 21.7150 670.477 5 -23 7 -3-8.19413 462.223 12 23 -16 9 190.625 342.870 8 -23 8 -7-8.96581 215.004 5 -23 8 -4 0.61379 429.315 12 23 -15 5-68.8487 152.637 8 23 -15 8-372.663 1084.76 8 -15 -8 11-9.29051 530.004 12 -23 9 -8 310.040 745.503 5 -23 9 -5-14.9217 424.668 12 23 -14 4 370.349 198.811 8 23 -14 7 583.296 490.771 8 23 -14 13-38.5869 520.830 3 -23 10 -9 48.5502 625.028 5 23 -13 3-111.302 674.784 8 23 -13 6 329.927 384.069 8 23 -13 12 398.507 750.840 3 -23 11 -10 25.7088 573.167 5 -23 11 -7-737.616 388.881 2 23 -12 2 435.957 575.679 8 23 -12 5 422.683 589.129 8 23 -12 11 974.395 838.837 8 23 -12 11-281.039 89.8720 3 -23 12 -11 259.602 738.360 5 23 -11 1 253.446 206.530 8 23 -11 4 1046.06 1013.49 8 23 -11 7 283.387 605.916 9 23 -11 10-118.061 98.2666 8 23 -11 10-527.379 596.113 3 -23 13 -12 252.197 297.732 5 23 -10 3 1122.97 1240.93 8 23 -10 6 116.824 259.995 9 23 -10 9-1221.86 928.097 8 23 -10 9-590.187 651.419 3 -14 23 -22-764.182 760.785 2 -23 14 -13 388.207 353.456 5 23 -9 2-432.139 881.654 8 23 -9 8 259.251 1271.77 8 15 8 -14-29.2838 773.651 9 16 7 -12 1711.08 1298.53 9 17 6 -10 274.380 501.943 9 23 -6 -4 44.9201 589.796 8 23 -5 -5 596.418 1006.95 8 23 -5 1-358.935 904.156 8 -19 23 -21-1188.88 649.073 2 23 -4 0 150.118 121.671 8 20 3 -7 498.854 233.219 9 23 -2 -5-1434.74 981.645 8 23 -2 -2 223.190 813.712 9 22 1 -6 1012.42 749.796 9 23 -1 -3-3737.97 1681.79 9 23 0 -4-452.812 759.707 9 24 -19 10-95.2171 443.416 8 -24 6 -3-53.7709 244.978 5 24 -18 9 736.267 945.168 8 -18 -6 9-11.4461 340.421 12 -24 7 -4-11.4369 160.628 5 -24 7 -4-45.2595 549.932 12 24 -17 14-430.448 710.269 8 -24 8 -5-8.08965 272.135 12 -24 8 -5-54.7741 326.893 5 24 -16 13 282.983 323.063 8 -24 9 -6-1698.31 889.029 12 -24 9 -6 0.85700 317.179 5 24 -15 12 611.749 182.600 8 -24 10 -7-11.2670 610.357 5 24 -13 1 399.424 822.274 8 24 -12 0 92.3433 478.127 8 24 -11 -1-223.383 441.912 8 -24 14 -11 310.384 410.717 2 24 -10 -2 174.841 464.899 8 -24 15 -12 137.631 249.905 2 24 -9 0 155.217 688.696 8 -24 16 -13 126.738 352.713 2 24 -8 -1 669.818 904.885 8 24 -8 5 510.578 1019.49 8 -24 17 -14 409.711 421.039 2 24 -7 4 150.743 902.876 8 -24 18 -15 646.027 543.142 2 18 6 -12 375.125 325.144 9 -24 19 -16-384.072 306.674 2 19 5 -10-1710.40 1164.11 9 -24 20 -17-327.359 325.414 2 24 -4 -2-819.297 75.9167 8 -24 21 -18-409.002 293.489 2 22 2 -7 205.845 685.735 9 24 0 -6 584.100 1154.48 9 25 -20 15-185.660 252.591 8 25 -19 14 1001.79 1251.24 8 -25 9 -7 31.0076 403.974 5 -25 10 -8 49.7629 440.171 5 -25 11 -9 22.7713 689.750 5 -25 13 -8-370.023 330.946 2 -25 14 -9 2336.87 989.773 2 25 -11 6 308.060 385.194 9 25 -10 5-665.920 1088.89 9 25 -9 4 144.408 248.112 9 17 8 -15-122.474 821.575 9 25 -8 -3 162.495 531.614 8 25 -8 3 1242.60 963.854 9 25 -7 -4-79.4710 676.073 8 25 -7 2-738.725 640.565 9 25 -6 1-688.799 1586.44 8 25 -6 1 109.268 512.149 9 20 5 -12 163.224 700.599 9 25 -5 0-87.1579 332.490 9 21 4 -10 1275.72 1528.18 9 25 -4 -1 340.530 380.172 9 25 -3 -5 103.188 652.758 8 25 -3 -2-546.522 956.008 9 23 2 -9 747.836 687.930 9 25 -2 -3 199.093 191.731 9 25 0 -8-709.328 849.160 9 26 -18 8-123.651 674.781 8 26 -17 7-1161.25 902.891 8 26 -17 13 3.65945 763.878 8 26 -16 6-314.753 946.811 8 26 -16 12 1110.01 1153.51 8 26 -15 5-830.498 747.533 8 26 -15 11 98.5746 476.218 8 26 -14 4 395.885 826.745 8 26 -14 10-400.730 568.125 8 -26 13 -6-325.976 273.089 2 26 -13 3-2849.70 1365.66 8 26 -13 9-508.005 936.185 8 26 -12 2-868.331 750.874 8 26 -12 8-124.928 539.416 8 26 -11 1 745.550 1087.77 8 26 -11 7-1961.58 1234.79 8 26 -10 6 166.689 733.730 8 26 -9 5 113.769 193.147 8 19 7 -15-379.669 508.688 9 26 -5 -2-21.0844 741.901 8 22 4 -12-131.902 1241.01 9 23 3 -10-367.788 651.026 9 26 -3 -4-703.726 573.574 9 26 -2 -5-96.9532 1074.29 9 27 -19 13 243.512 471.478 8 -27 15 -9 234.147 279.126 2 -27 16 -10 149.855 311.349 2 -27 17 -11-378.824 169.239 2 27 -10 4 799.944 955.801 9 -27 18 -12 227.410 362.434 2 27 -9 3-273.426 354.509 8 27 -9 3-818.388 856.706 9 -27 19 -13 188.826 236.299 2 27 -8 2-25.8106 847.763 8 27 -8 2 503.819 846.267 9 27 -7 1 1574.27 1693.41 8 27 -7 1-937.324 797.713 9 27 -6 0 511.302 1147.03 9 27 -5 -4 60.1703 243.205 8 27 -5 -1 271.173 738.797 9 28 -16 11 2679.37 2183.12 8 28 -15 10 166.986 927.220 8 28 -14 9 922.920 1772.63 8 28 -13 8 1065.55 1411.08 8 -28 16 -8-26.3081 228.628 2 28 -12 4-782.600 1217.99 9 28 -12 7 205.174 298.806 8 28 -11 6 1366.75 1434.64 8 28 -8 0-23.6884 909.303 8 28 -7 -1 1180.91 1132.58 8 28 -7 -1 527.244 701.932 9 28 -6 -2-351.315 711.122 9 29 -13 6 296.047 326.246 8 29 -12 5 659.073 1044.06 8 29 -11 4-1691.87 1215.13 8 29 -10 3 188.882 577.161 8 0 0 0 0.00 0.00 0 TITL ET_etanol_0_76_3 in R3c REM R3c (#161 in standard setting) CELL 0.71073 23.644525 23.644525 30.914719 90.0000 90.0000 120.0000 ZERR 18.00 0.008433 0.008433 0.024719 0.0000 0.0000 0.0000 LATT -3 SYMM -y, x-y, z SYMM -x+y,-x, z SYMM -y,-x, z+1/2 SYMM -x+y, y, z+1/2 SYMM x, x-y, z+1/2 SFAC C H N O UNIT 666.00 810.00 18.00 108.00 SIZE 0.13 0.19 0.27 TREF HKLF 4 END ; _shelx_hkl_checksum 81445 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-x+y, y, z+1/2' 'x, x-y, z+1/2' '-y, -x, z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' '-x+y+2/3, y+1/3, z+5/6' 'x+2/3, x-y+1/3, z+5/6' '-y+2/3, -x+1/3, z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x+y+1/3, y+2/3, z+7/6' 'x+1/3, x-y+2/3, z+7/6' '-y+1/3, -x+2/3, z+7/6' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N -0.002(2) 0.4780(16) 0.1182(13) 0.065(9) Uani 1 1 d D . . . . C1' C -0.024(2) 0.4385(15) 0.1546(15) 0.058(12) Uani 1 1 d D . . . . C2' C -0.024(3) 0.3807(17) 0.1506(17) 0.067(13) Uani 1 1 d D U . . . H2' H -0.042456 0.350714 0.173107 0.080 Uiso 1 1 calc R U . . . C3 C 0.000(3) 0.364(2) 0.1155(17) 0.083(12) Uani 1 1 d D . . . . C2 C 0.030(2) 0.4076(14) 0.0820(18) 0.067(14) Uani 1 1 d D . . . . H2 H 0.045848 0.397287 0.057460 0.080 Uiso 1 1 calc R U . . . C1 C 0.035(2) 0.4681(16) 0.0875(15) 0.071(15) Uani 1 1 d D . . . . C13' C -0.0546(15) 0.4388(16) 0.2263(15) 0.073(13) Uani 1 1 d G U . . . H13' H -0.022554 0.427889 0.231899 0.088 Uiso 1 1 calc R U . . . C8' C -0.0637(17) 0.4542(16) 0.1845(13) 0.066(11) Uani 1 1 d DG U . . . C9' C -0.112(2) 0.4705(16) 0.1761(13) 0.076(15) Uani 1 1 d G . . . . H9' H -0.117674 0.480854 0.148147 0.092 Uiso 1 1 calc R U . . . C10' C -0.1504(14) 0.4713(16) 0.2097(18) 0.092(17) Uani 1 1 d G U . . . H10' H -0.182392 0.482231 0.204079 0.111 Uiso 1 1 calc R U . . . C11' C -0.1412(17) 0.4559(16) 0.2515(16) 0.095(17) Uani 1 1 d G . . . . H11' H -0.167191 0.456438 0.273922 0.115 Uiso 1 1 calc R U . . . C12' C -0.093(2) 0.4396(16) 0.2598(12) 0.078(14) Uani 1 1 d G . . . . H12' H -0.087273 0.429266 0.287833 0.093 Uiso 1 1 calc R U . . . O1 O 0.006(3) 0.7163(15) 0.119(2) 0.111(12) Uani 1 1 d D . . . . C15' C -0.0284(18) 0.5567(12) 0.0870(13) 0.08(2) Uani 1 1 d G . . . . H15' H -0.048425 0.527031 0.064529 0.101 Uiso 1 1 calc R U . . . C16' C -0.0298(17) 0.6148(15) 0.0876(13) 0.079(17) Uani 1 1 d DG . . . . H16' H -0.050686 0.623992 0.065532 0.095 Uiso 1 1 calc R U . . . C17 C 0.000(2) 0.6590(12) 0.1211(14) 0.084(14) Uani 1 1 d DG . . . . C16 C 0.0314(17) 0.6452(14) 0.1541(13) 0.10(2) Uani 1 1 d DG . . . . H16 H 0.051425 0.674874 0.176531 0.123 Uiso 1 1 calc R U . . . C15 C 0.0328(17) 0.5871(18) 0.1535(13) 0.055(14) Uani 1 1 d G . . . . H15 H 0.053687 0.577914 0.175529 0.066 Uiso 1 1 calc R U . . . C14 C 0.003(2) 0.5429(13) 0.1199(14) 0.064(12) Uani 1 1 d DG . . . . C8 C 0.0623(16) 0.5082(15) 0.0476(13) 0.059(12) Uani 1 1 d DG . . . . C13 C 0.0508(16) 0.4869(14) 0.0049(15) 0.10(2) Uani 1 1 d G . . . . H13 H 0.019347 0.444097 -0.001441 0.120 Uiso 1 1 calc R U . . . C12 C 0.0864(19) 0.530(2) -0.0283(12) 0.13(2) Uani 1 1 d G . . . . H12 H 0.078710 0.515489 -0.056831 0.158 Uiso 1 1 calc R U . . . C11 C 0.1334(15) 0.5938(19) -0.0188(15) 0.082(19) Uani 1 1 d G . . . . H11 H 0.157234 0.622370 -0.040960 0.098 Uiso 1 1 calc R U . . . C10 C 0.1449(13) 0.6150(12) 0.0239(17) 0.072(18) Uani 1 1 d G . . . . H10 H 0.176397 0.657860 0.030300 0.087 Uiso 1 1 calc R U . . . C9 C 0.1094(18) 0.5722(18) 0.0571(13) 0.070(15) Uani 1 1 d G . . . . H9 H 0.117034 0.586469 0.085690 0.084 Uiso 1 1 calc R U . . . C5 C 0.0487(17) 0.2933(13) 0.0958(15) 0.095(16) Uani 1 1 d G U . . . H5 H 0.083826 0.329442 0.083058 0.114 Uiso 1 1 calc R U . . . C4 C -0.001(2) 0.2995(13) 0.1157(16) 0.078(12) Uani 1 1 d DG U . . . C5' C -0.0531(18) 0.2455(18) 0.1347(15) 0.095(15) Uani 1 1 d G U . . . H5' H -0.086081 0.249691 0.147976 0.114 Uiso 1 1 calc R U . . . C6' C -0.0562(17) 0.1852(13) 0.1339(15) 0.090(15) Uani 1 1 d G U . . . H6' H -0.091292 0.149086 0.146585 0.108 Uiso 1 1 calc R U . . . C7 C -0.007(2) 0.1790(13) 0.1140(17) 0.086(11) Uani 1 1 d DG U . . . H7 H -0.008946 0.138658 0.113431 0.103 Uiso 1 1 calc R U . . . C6 C 0.0456(18) 0.2330(18) 0.0950(17) 0.107(16) Uani 1 1 d G U . . . H6 H 0.078613 0.228835 0.081667 0.128 Uiso 1 1 calc R U . . . O1E O -0.1394(18) 0.402(2) 0.078(2) 0.16(2) Uani 1 1 d D U . . . H1E H -0.115119 0.395675 0.062577 0.235 Uiso 1 1 calc DR U . . . C1E C -0.216(3) 0.435(4) 0.074(3) 0.20(4) Uani 1 1 d D U . . . H1EA H -0.263081 0.410312 0.072696 0.307 Uiso 1 1 calc R U . . . H1EB H -0.200642 0.475522 0.059087 0.307 Uiso 1 1 calc R U . . . H1EC H -0.202126 0.442456 0.103351 0.307 Uiso 1 1 calc R U . . . C3E C -0.134(4) 0.283(3) 0.043(2) 0.22(4) Uani 1 1 d D U . . . H3EA H -0.104426 0.267777 0.053353 0.259 Uiso 1 1 calc R U . . . H3EB H -0.152097 0.292239 0.068362 0.259 Uiso 1 1 calc R U . . . C2E C -0.191(3) 0.399(3) 0.054(2) 0.16(3) Uani 1 1 d D U . . . H2EA H -0.225655 0.353737 0.050341 0.191 Uiso 1 1 calc R U . . . H2EB H -0.175507 0.416518 0.024902 0.191 Uiso 1 1 calc R U . . . O2E O -0.098(3) 0.340(2) 0.018(2) 0.20(2) Uani 1 1 d D U . . . H2E H -0.062(8) 0.340(17) 0.010(4) 0.302 Uiso 1 1 d D U . . . C4E C -0.184(3) 0.234(3) 0.018(3) 0.19(3) Uani 1 1 d D U . . . H4EA H -0.219554 0.205892 0.036508 0.279 Uiso 1 1 calc R U . . . H4EB H -0.167516 0.208976 0.003709 0.279 Uiso 1 1 calc R U . . . H4EC H -0.197948 0.253982 -0.002905 0.279 Uiso 1 1 calc R U . . . C6E C 0.196(3) 0.584(3) 0.170(3) 0.16(3) Uani 1 1 d D U . . . H6EA H 0.215887 0.573152 0.145703 0.196 Uiso 1 1 calc R U . . . H6EB H 0.218408 0.582682 0.196084 0.196 Uiso 1 1 calc R U . . . O3E O 0.129(2) 0.537(2) 0.173(2) 0.18(3) Uani 1 1 d D U . . . H3E H 0.120784 0.521399 0.197055 0.270 Uiso 1 1 calc DR U . . . C5E C 0.205(3) 0.646(2) 0.164(3) 0.19(3) Uani 1 1 d D U . . . H5EA H 0.244654 0.677608 0.178015 0.291 Uiso 1 1 calc R U . . . H5EB H 0.168709 0.647753 0.176439 0.291 Uiso 1 1 calc R U . . . H5EC H 0.207673 0.655681 0.133692 0.291 Uiso 1 1 calc R U . . . C8E C 0.139(3) 0.403(3) 0.200(3) 0.20(3) Uani 1 1 d D U . . . H8EA H 0.136992 0.395322 0.169549 0.240 Uiso 1 1 calc R U . . . H8EB H 0.120265 0.361553 0.215264 0.240 Uiso 1 1 calc R U . . . C7E C 0.204(3) 0.444(4) 0.213(4) 0.24(3) Uani 1 1 d D U . . . H7EA H 0.205053 0.458165 0.242519 0.366 Uiso 1 1 calc R U . . . H7EB H 0.224879 0.480596 0.194484 0.366 Uiso 1 1 calc R U . . . H7EC H 0.226735 0.419379 0.212112 0.366 Uiso 1 1 calc R U . . . O4E O 0.103(3) 0.436(3) 0.2110(19) 0.21(3) Uani 1 1 d D U . . . H4E H 0.103(11) 0.433(11) 0.240(2) 0.318 Uiso 1 1 d D U . . . O2W O 0.333333 0.666667 0.055(7) 0.27(7) Uiso 1 3 d S . P . . O3W O -0.333333 0.333333 -0.044(11) 0.40(5) Uiso 1 3 d S . P . . O1W O -0.299(4) 0.359(4) 0.170(6) 0.08(4) Uiso 0.3333 1 d . . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.07(2) 0.07(2) 0.08(2) 0.012(19) 0.003(16) 0.05(2) C1' 0.07(3) 0.05(2) 0.05(2) -0.019(17) -0.03(2) 0.02(2) C2' 0.073(19) 0.061(15) 0.074(19) 0.006(11) -0.009(12) 0.039(14) C3 0.10(3) 0.08(3) 0.09(3) 0.00(2) 0.00(2) 0.05(3) C2 0.07(3) 0.06(2) 0.08(4) -0.01(2) -0.02(3) 0.03(3) C1 0.07(3) 0.044(19) 0.08(3) -0.010(19) 0.01(2) 0.02(2) C13' 0.080(18) 0.067(19) 0.068(15) 0.003(12) 0.004(11) 0.033(13) C8' 0.066(16) 0.055(17) 0.067(15) -0.003(11) -0.004(11) 0.022(12) C9' 0.09(3) 0.05(4) 0.09(3) 0.01(3) 0.01(2) 0.04(3) C10' 0.09(2) 0.09(2) 0.09(2) -0.006(13) 0.006(12) 0.042(16) C11' 0.12(4) 0.09(4) 0.08(3) -0.04(3) -0.01(3) 0.05(4) C12' 0.11(4) 0.03(3) 0.08(2) -0.01(3) 0.01(2) 0.02(3) O1 0.18(3) 0.06(2) 0.11(4) 0.03(3) 0.01(2) 0.07(3) C15' 0.10(4) 0.05(3) 0.10(4) 0.00(3) -0.03(3) 0.04(3) C16' 0.09(4) 0.04(3) 0.10(4) 0.02(2) 0.01(3) 0.03(3) C17 0.10(3) 0.04(3) 0.11(4) 0.02(3) 0.00(2) 0.03(3) C16 0.14(5) 0.09(3) 0.10(4) 0.00(3) -0.01(3) 0.08(4) C15 0.06(3) 0.07(3) 0.04(4) 0.02(2) 0.04(2) 0.04(3) C14 0.07(3) 0.07(2) 0.06(3) 0.015(19) 0.019(18) 0.05(2) C8 0.07(3) 0.045(19) 0.08(3) -0.008(17) 0.01(2) 0.04(2) C13 0.13(4) 0.08(3) 0.08(3) -0.01(2) 0.02(3) 0.04(3) C12 0.12(5) 0.12(4) 0.08(3) 0.00(3) 0.00(3) 0.00(3) C11 0.05(3) 0.10(3) 0.08(4) -0.01(3) 0.03(3) 0.03(3) C10 0.09(3) 0.05(2) 0.08(4) 0.00(2) 0.01(3) 0.03(2) C9 0.10(4) 0.04(2) 0.08(4) 0.00(2) 0.02(3) 0.04(2) C5 0.11(3) 0.073(19) 0.11(4) 0.00(2) 0.04(2) 0.05(2) C4 0.07(2) 0.07(2) 0.10(4) 0.01(2) 0.013(18) 0.04(2) C5' 0.09(2) 0.07(2) 0.13(4) 0.02(3) 0.03(2) 0.04(2) C6' 0.10(2) 0.076(19) 0.10(4) 0.02(2) 0.01(2) 0.053(19) C7 0.102(16) 0.073(14) 0.094(19) 0.000(13) -0.005(12) 0.052(12) C6 0.14(3) 0.08(2) 0.11(4) -0.01(2) 0.04(2) 0.06(2) O1E 0.09(3) 0.16(4) 0.24(7) 0.00(4) 0.02(3) 0.08(3) C1E 0.08(4) 0.28(7) 0.29(10) -0.08(6) -0.02(5) 0.12(4) C3E 0.20(6) 0.21(5) 0.18(7) -0.01(4) 0.00(5) 0.06(4) C2E 0.06(4) 0.16(5) 0.24(7) -0.04(4) 0.00(4) 0.05(3) O2E 0.21(3) 0.17(3) 0.18(4) -0.03(2) 0.01(2) 0.07(2) C4E 0.16(6) 0.17(4) 0.22(9) -0.01(5) -0.01(5) 0.08(3) C6E 0.16(3) 0.17(3) 0.17(3) -0.004(14) -0.001(14) 0.082(17) O3E 0.14(3) 0.18(3) 0.21(7) 0.00(4) -0.06(3) 0.08(2) C5E 0.21(4) 0.18(3) 0.19(4) 0.01(2) 0.01(3) 0.10(2) C8E 0.19(4) 0.22(4) 0.20(4) 0.01(3) 0.02(2) 0.10(3) C7E 0.22(4) 0.26(5) 0.25(6) -0.01(5) -0.04(4) 0.11(3) O4E 0.23(3) 0.22(4) 0.20(5) 0.07(3) 0.09(3) 0.13(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1' N1 C14 119(2) . . ? C1 N1 C1' 120(3) . . ? C1 N1 C14 118(2) . . ? N1 C1' C2' 114(4) . . ? N1 C1' C8' 114(3) . . ? C2' C1' C8' 128(4) . . ? C1' C2' H2' 117.5 . . ? C1' C2' C3 125(4) . . ? C3 C2' H2' 117.7 . . ? C2' C3 C4 120(2) . . ? C2 C3 C2' 120(3) . . ? C2 C3 C4 120(2) . . ? C3 C2 H2 122.0 . . ? C3 C2 C1 116(4) . . ? C1 C2 H2 122.4 . . ? N1 C1 C2 122(4) . . ? N1 C1 C8 125(3) . . ? C2 C1 C8 110(4) . . ? C8' C13' H13' 120.0 . . ? C8' C13' C12' 120.0 . . ? C12' C13' H13' 120.0 . . ? C13' C8' C1' 108(3) . . ? C9' C8' C1' 131(4) . . ? C9' C8' C13' 120.0 . . ? C8' C9' H9' 120.0 . . ? C10' C9' C8' 120.0 . . ? C10' C9' H9' 120.0 . . ? C9' C10' H10' 120.0 . . ? C9' C10' C11' 120.0 . . ? C11' C10' H10' 120.0 . . ? C10' C11' H11' 120.0 . . ? C10' C11' C12' 120.0 . . ? C12' C11' H11' 120.0 . . ? C13' C12' H12' 120.0 . . ? C11' C12' C13' 120.0 . . ? C11' C12' H12' 120.0 . . ? C16' C15' H15' 120.1 . . ? C16' C15' C14 120.0 . . ? C14 C15' H15' 119.9 . . ? C15' C16' H16' 120.0 . . ? C15' C16' C17 120.0 . . ? C17 C16' H16' 120.0 . . ? O1 C17 C16' 120.0(13) . . ? O1 C17 C16 119.5(13) . . ? C16' C17 C16 120.0 . . ? C17 C16 H16 120.0 . . ? C15 C16 C17 120.0 . . ? C15 C16 H16 120.0 . . ? C16 C15 H15 120.0 . . ? C16 C15 C14 120.0 . . ? C14 C15 H15 120.0 . . ? C15' C14 N1 116(3) . . ? C15 C14 N1 124(3) . . ? C15 C14 C15' 120.0 . . ? C13 C8 C1 128(3) . . ? C13 C8 C9 120.0 . . ? C9 C8 C1 112(3) . . ? C8 C13 H13 120.0 . . ? C8 C13 C12 120.0 . . ? C12 C13 H13 120.0 . . ? C13 C12 H12 120.0 . . ? C13 C12 C11 120.0 . . ? C11 C12 H12 120.0 . . ? C12 C11 H11 120.0 . . ? C10 C11 C12 120.0 . . ? C10 C11 H11 120.0 . . ? C11 C10 H10 120.0 . . ? C11 C10 C9 120.0 . . ? C9 C10 H10 120.0 . . ? C8 C9 H9 120.0 . . ? C10 C9 C8 120.0 . . ? C10 C9 H9 120.0 . . ? C4 C5 H5 120.3 . . ? C4 C5 C6 120.0 . . ? C6 C5 H5 119.7 . . ? C5 C4 C3 121(3) . . ? C5 C4 C5' 120.0 . . ? C5' C4 C3 119(3) . . ? C4 C5' H5' 120.0 . . ? C6' C5' C4 120.0 . . ? C6' C5' H5' 120.0 . . ? C5' C6' H6' 120.0 . . ? C7 C6' C5' 120.0 . . ? C7 C6' H6' 120.0 . . ? C6' C7 H7 120.0 . . ? C6' C7 C6 120.0 . . ? C6 C7 H7 120.0 . . ? C5 C6 H6 120.0 . . ? C7 C6 C5 120.0 . . ? C7 C6 H6 120.0 . . ? C2E O1E H1E 109.7 . . ? H1EA C1E H1EB 109.2 . . ? H1EA C1E H1EC 109.1 . . ? H1EB C1E H1EC 109.1 . . ? C2E C1E H1EA 110.5 . . ? C2E C1E H1EB 108.9 . . ? C2E C1E H1EC 110.0 . . ? H3EA C3E H3EB 108.3 . . ? O2E C3E H3EA 109.9 . . ? O2E C3E H3EB 109.5 . . ? C4E C3E H3EA 109.9 . . ? C4E C3E H3EB 110.1 . . ? C4E C3E O2E 109(4) . . ? O1E C2E C1E 110(4) . . ? O1E C2E H2EA 109.8 . . ? O1E C2E H2EB 109.8 . . ? C1E C2E H2EA 108.8 . . ? C1E C2E H2EB 110.2 . . ? H2EA C2E H2EB 108.1 . . ? C3E O2E H2E 105(10) . . ? C3E C4E H4EA 109.1 . . ? C3E C4E H4EB 109.7 . . ? C3E C4E H4EC 109.7 . . ? H4EA C4E H4EB 109.4 . . ? H4EA C4E H4EC 109.5 . . ? H4EB C4E H4EC 109.4 . . ? H6EA C6E H6EB 108.1 . . ? O3E C6E H6EA 108.6 . . ? O3E C6E H6EB 109.8 . . ? O3E C6E C5E 110(4) . . ? C5E C6E H6EA 110.0 . . ? C5E C6E H6EB 110.0 . . ? C6E O3E H3E 109.1 . . ? C6E C5E H5EA 112.5 . . ? C6E C5E H5EB 113.5 . . ? C6E C5E H5EC 111.7 . . ? H5EA C5E H5EB 105.9 . . ? H5EA C5E H5EC 106.2 . . ? H5EB C5E H5EC 106.5 . . ? H8EA C8E H8EB 108.3 . . ? C7E C8E H8EA 110.1 . . ? C7E C8E H8EB 109.4 . . ? O4E C8E H8EA 111.0 . . ? O4E C8E H8EB 109.6 . . ? O4E C8E C7E 108(4) . . ? C8E C7E H7EA 109.7 . . ? C8E C7E H7EB 109.0 . . ? C8E C7E H7EC 109.9 . . ? H7EA C7E H7EB 109.4 . . ? H7EA C7E H7EC 109.4 . . ? H7EB C7E H7EC 109.5 . . ? C8E O4E H4E 99(4) . . ? O1W O1W O1W 60.00(3) 2_565 3_455 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C1' 1.39(3) . ? N1 C1 1.39(3) . ? N1 C14 1.48(3) . ? C1' C2' 1.37(2) . ? C1' C8' 1.49(3) . ? C2' H2' 0.9300 . ? C2' C3 1.39(2) . ? C3 C2 1.38(2) . ? C3 C4 1.50(3) . ? C2 H2 0.9300 . ? C2 C1 1.39(2) . ? C1 C8 1.49(3) . ? C13' H13' 0.9300 . ? C13' C8' 1.3900 . ? C13' C12' 1.3900 . ? C8' C9' 1.3900 . ? C9' H9' 0.9300 . ? C9' C10' 1.3900 . ? C10' H10' 0.9300 . ? C10' C11' 1.3900 . ? C11' H11' 0.9300 . ? C11' C12' 1.3900 . ? C12' H12' 0.9300 . ? O1 C17 1.29(2) . ? C15' H15' 0.9300 . ? C15' C16' 1.3900 . ? C15' C14 1.3900 . ? C16' H16' 0.9300 . ? C16' C17 1.3900 . ? C17 C16 1.3900 . ? C16 H16 0.9300 . ? C16 C15 1.3900 . ? C15 H15 0.9300 . ? C15 C14 1.3900 . ? C8 C13 1.3900 . ? C8 C9 1.3900 . ? C13 H13 0.9300 . ? C13 C12 1.3900 . ? C12 H12 0.9300 . ? C12 C11 1.3900 . ? C11 H11 0.9300 . ? C11 C10 1.3900 . ? C10 H10 0.9300 . ? C10 C9 1.3900 . ? C9 H9 0.9300 . ? C5 H5 0.9300 . ? C5 C4 1.3900 . ? C5 C6 1.3900 . ? C4 C5' 1.3900 . ? C5' H5' 0.9300 . ? C5' C6' 1.3900 . ? C6' H6' 0.9300 . ? C6' C7 1.3900 . ? C7 H7 0.9300 . ? C7 C6 1.3900 . ? C6 H6 0.9300 . ? O1E H1E 0.8242 . ? O1E C2E 1.42(4) . ? C1E H1EA 0.9631 . ? C1E H1EB 0.9629 . ? C1E H1EC 0.9629 . ? C1E C2E 1.40(4) . ? C3E H3EA 0.9700 . ? C3E H3EB 0.9700 . ? C3E O2E 1.42(4) . ? C3E C4E 1.40(4) . ? C2E H2EA 0.9700 . ? C2E H2EB 0.9700 . ? O2E H2E 0.891(13) . ? C4E H4EA 0.9602 . ? C4E H4EB 0.9602 . ? C4E H4EC 0.9602 . ? C6E H6EA 0.9700 . ? C6E H6EB 0.9700 . ? C6E O3E 1.41(3) . ? C6E C5E 1.40(4) . ? O3E H3E 0.8200 . ? C5E H5EA 0.9883 . ? C5E H5EB 0.9909 . ? C5E H5EC 0.9862 . ? C8E H8EA 0.9700 . ? C8E H8EB 0.9700 . ? C8E C7E 1.40(4) . ? C8E O4E 1.44(3) . ? C7E H7EA 0.9604 . ? C7E H7EB 0.9604 . ? C7E H7EC 0.9604 . ? O4E H4E 0.891(11) . ? O1W O1W 1.25(13) 2_565 ? O1W O1W 1.25(13) 3_455 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C1' C2' C3 6(9) . . . . ? N1 C1' C8' C13' -150(4) . . . . ? N1 C1' C8' C9' 41(6) . . . . ? N1 C1 C8 C13 -121(5) . . . . ? N1 C1 C8 C9 66(6) . . . . ? C1' N1 C1 C2 26(10) . . . . ? C1' N1 C1 C8 -178(4) . . . . ? C1' N1 C14 C15' -128(4) . . . . ? C1' N1 C14 C15 48(6) . . . . ? C1' C2' C3 C2 2(12) . . . . ? C1' C2' C3 C4 178(5) . . . . ? C1' C8' C9' C10' 168(4) . . . . ? C2' C1' C8' C13' 53(6) . . . . ? C2' C1' C8' C9' -116(5) . . . . ? C2' C3 C2 C1 2(11) . . . . ? C2' C3 C4 C5 -147(5) . . . . ? C2' C3 C4 C5' 36(7) . . . . ? C3 C2 C1 N1 -16(9) . . . . ? C3 C2 C1 C8 -175(5) . . . . ? C3 C4 C5' C6' 178(4) . . . . ? C2 C3 C4 C5 29(7) . . . . ? C2 C3 C4 C5' -149(5) . . . . ? C2 C1 C8 C13 37(6) . . . . ? C2 C1 C8 C9 -136(4) . . . . ? C1 N1 C1' C2' -19(9) . . . . ? C1 N1 C1' C8' -179(4) . . . . ? C1 N1 C14 C15' 74(5) . . . . ? C1 N1 C14 C15 -110(4) . . . . ? C1 C8 C13 C12 -173(4) . . . . ? C1 C8 C9 C10 174(3) . . . . ? C13' C8' C9' C10' 0.0 . . . . ? C8' C1' C2' C3 163(6) . . . . ? C8' C13' C12' C11' 0.0 . . . . ? C8' C9' C10' C11' 0.0 . . . . ? C9' C10' C11' C12' 0.0 . . . . ? C10' C11' C12' C13' 0.0 . . . . ? C12' C13' C8' C1' -170(3) . . . . ? C12' C13' C8' C9' 0.0 . . . . ? O1 C17 C16 C15 -172(5) . . . . ? C15' C16' C17 O1 172(5) . . . . ? C15' C16' C17 C16 0.0 . . . . ? C16' C15' C14 N1 176(3) . . . . ? C16' C15' C14 C15 0.0 . . . . ? C16' C17 C16 C15 0.0 . . . . ? C17 C16 C15 C14 0.0 . . . . ? C16 C15 C14 N1 -175(3) . . . . ? C16 C15 C14 C15' 0.0 . . . . ? C14 N1 C1' C2' -177(5) . . . . ? C14 N1 C1' C8' 23(7) . . . . ? C14 N1 C1 C2 -176(5) . . . . ? C14 N1 C1 C8 -21(8) . . . . ? C14 C15' C16' C17 0.0 . . . . ? C8 C13 C12 C11 0.0 . . . . ? C13 C8 C9 C10 0.0 . . . . ? C13 C12 C11 C10 0.0 . . . . ? C12 C11 C10 C9 0.0 . . . . ? C11 C10 C9 C8 0.0 . . . . ? C9 C8 C13 C12 0.0 . . . . ? C5 C4 C5' C6' 0.0 . . . . ? C4 C3 C2 C1 -173(5) . . . . ? C4 C5 C6 C7 0.0 . . . . ? C4 C5' C6' C7 0.0 . . . . ? C5' C6' C7 C6 0.0 . . . . ? C6' C7 C6 C5 0.0 . . . . ? C6 C5 C4 C3 -178(4) . . . . ? C6 C5 C4 C5' 0.0 . . . . ?