#------------------------------------------------------------------------------ #$Date: 2024-06-05 05:22:27 +0300 (Wed, 05 Jun 2024) $ #$Revision: 292202 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571778.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1571778 loop_ _publ_author_name 'Yang, Jun' 'Zhang, Cuijuan' 'Chu, Jiaxiang' _publ_section_title ; (2,5-Dimethylimidazole){N,N′,N′′,N′′′-[porphyrin-5,10,15,20-tetrayltetra(2,1-phenylene)]tetrakis(pyridine-3-carboxamide)}manganese(II) chlorobenzene disolvate ; _journal_coeditor_code HB4469 _journal_issue 6 _journal_name_full IUCrData _journal_paper_doi 10.1107/S2414314624004978 _journal_volume 9 _journal_year 2024 _chemical_formula_iupac '[Mn (C68 H44 N12 O4) (C5 H8 N2)], 2C6 H5 Cl' _chemical_formula_moiety 'C73 H52 Mn N14 O4, 2(C6 H5 Cl)' _chemical_formula_sum 'C85 H62 Cl2 Mn N14 O4' _chemical_formula_weight 1469.32 _chemical_name_systematic '(2,5-Dimethylimidazole){N,N',N'',N'''-[porphyrin-5,10,15,20-tetrayltetra(2,1-phenylene)]tetrakis(pyridine-3-carboxamide)}manganese(II) chlorobenzene disolvate' _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_Hall 'P 2c -2n' _space_group_name_H-M_alt 'P n a 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 30.247(4) _cell_length_b 13.713(2) _cell_length_c 17.205(2) _cell_measurement_reflns_used 9672 _cell_measurement_temperature 101.15 _cell_measurement_theta_max 26.26 _cell_measurement_theta_min 2.51 _cell_volume 7136.2(16) _computing_cell_refinement ; SAINT (Bruker, 2014) ; _computing_data_collection ; APEX2 (Bruker, 2014) ; _computing_data_reduction ; SAINT (Bruker, 2014) ; _computing_molecular_graphics ; Olex2 1.5 (Dolomanov et al., 2009) ; _computing_publication_material ; Olex2 1.5 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 101.15 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0705 _diffrn_reflns_av_unetI/netI 0.0382 _diffrn_reflns_limit_h_max 37 _diffrn_reflns_limit_h_min -37 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 142482 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.553 _diffrn_reflns_theta_min 2.005 _diffrn_source_current 1.0 _diffrn_source_power 0.05 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.325 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.5677 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour black _exptl_crystal_density_diffrn 1.368 _exptl_crystal_description block _exptl_crystal_F_000 3044 _exptl_crystal_size_max 0.613 _exptl_crystal_size_mid 0.55 _exptl_crystal_size_min 0.353 _refine_diff_density_max 0.978 _refine_diff_density_min -1.031 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.41(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.063 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 946 _refine_ls_number_reflns 14653 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.063 _refine_ls_R_factor_all 0.1065 _refine_ls_R_factor_gt 0.0804 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1079P)^2^+24.1645P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2106 _refine_ls_wR_factor_ref 0.2401 _reflns_number_gt 12171 _reflns_number_total 14653 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb4469.cif _cod_data_source_block I _cod_database_code 1571778 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.826 _shelx_estimated_absorpt_t_max 0.894 _shelx_hkl_file ; -2 0 0 205.88 13.50 -2 0 0 244.98 13.50 -2 0 0 228.18 13.80 2 0 0 256.07 13.60 2 0 0 214.28 13.80 2 0 0 229.78 13.80 -2 0 0 212.88 13.80 -2 0 0 218.38 13.60 3 0 0 -0.90 1.00 3 0 0 0.80 1.30 3 0 0 0.40 0.60 -3 0 0 -0.80 0.60 -3 0 0 -0.10 1.90 -3 0 0 -1.00 1.10 -3 0 0 -1.10 0.90 3 0 0 0.30 0.90 -3 0 0 2.60 1.00 -4 0 0 363.66 22.40 -4 0 0 345.37 22.00 -4 0 0 393.66 23.90 4 0 0 337.17 22.10 4 0 0 399.16 23.90 5 0 0 19.20 2.90 -5 0 0 24.60 3.70 -5 0 0 12.20 4.00 6 0 0 1273.67 80.89 6 0 0 1305.47 80.09 6 0 0 1575.64 80.49 -6 0 0 1391.16 80.99 6 0 0 1273.77 80.99 8 0 0 5386.46 349.17 -8 0 0 6480.65 349.77 -8 0 0 5375.36 347.87 -8 0 0 6510.45 348.07 -8 0 0 6463.65 348.77 -8 0 0 5832.12 350.66 -9 0 0 58.69 8.10 10 0 0 5.10 2.30 10 0 0 9.50 4.40 10 0 0 8.70 5.30 -10 0 0 3.20 7.50 10 0 0 13.00 4.10 -10 0 0 9.90 3.30 -10 0 0 18.00 3.20 -10 0 0 14.70 4.80 11 0 0 7.10 4.30 11 0 0 3.00 5.60 -11 0 0 3.10 8.20 -11 0 0 5.00 4.70 11 0 0 0.40 2.10 -11 0 0 0.30 2.60 11 0 0 7.60 4.60 -12 0 0 21.60 6.80 -12 0 0 15.40 4.30 12 0 0 30.30 6.20 12 0 0 26.60 8.30 -12 0 0 42.80 11.10 13 0 0 0.70 6.70 -13 0 0 10.10 3.90 13 0 0 2.90 5.20 -13 0 0 4.20 6.50 13 0 0 4.00 4.90 14 0 0 117.79 13.50 -14 0 0 132.29 11.60 14 0 0 106.19 16.50 14 0 0 103.09 14.90 -14 0 0 148.09 18.40 -14 0 0 84.59 17.40 15 0 0 1.20 5.90 -15 0 0 24.00 14.40 15 0 0 2.40 7.30 15 0 0 -0.40 5.70 -15 0 0 5.90 8.40 -15 0 0 -3.00 3.70 -16 0 0 44.90 15.90 -16 0 0 25.20 5.70 16 0 0 25.80 10.40 -16 0 0 19.80 11.00 16 0 0 17.70 9.40 -17 0 0 -2.80 4.20 17 0 0 -2.70 8.70 -17 0 0 -3.10 11.50 17 0 0 4.60 10.20 -1 -1 0 2.20 0.60 -2 1 0 0.80 0.90 -2 1 0 1.20 0.40 2 -1 0 0.30 0.50 2 -1 0 0.00 0.50 2 -1 0 0.60 0.80 2 -1 0 1.70 0.50 2 1 0 0.10 0.70 2 1 0 0.00 0.80 2 1 0 0.80 1.00 -2 -1 0 0.30 0.60 -2 -1 0 1.10 0.90 -2 1 0 0.50 0.50 -2 -1 0 0.80 0.90 -2 -1 0 -0.60 0.80 -2 -1 0 0.70 0.40 2 1 0 0.00 1.20 -2 1 0 1.40 0.60 -2 1 0 0.90 0.40 2 -1 0 0.40 0.70 2 1 0 0.60 0.70 -2 -1 0 0.30 1.10 -2 1 0 0.00 0.80 -3 -1 0 3557.94 186.98 -3 -1 0 3281.37 187.08 3 1 0 3124.69 186.78 3 -1 0 3243.58 186.68 -3 1 0 2883.61 186.18 -3 1 0 3141.49 186.68 3 1 0 3335.37 187.08 -4 1 0 108.99 7.70 4 -1 0 125.59 8.70 -4 -1 0 115.29 8.70 4 1 0 119.39 8.70 4 1 0 132.49 8.90 4 -1 0 114.29 7.50 -4 1 0 102.69 7.80 4 -1 0 117.19 7.90 4 1 0 102.99 7.80 -4 -1 0 116.09 7.80 5 -1 0 793.52 43.00 -5 1 0 720.63 43.30 5 -1 0 717.03 42.70 5 1 0 644.04 44.70 -5 -1 0 692.83 43.60 5 1 0 751.32 43.20 5 -1 0 765.32 44.30 -5 -1 0 636.94 43.40 5 -1 0 693.43 43.40 5 1 0 782.72 42.80 -5 -1 0 665.03 44.40 -5 1 0 695.53 42.80 -5 -1 0 743.03 43.20 5 1 0 677.03 43.60 -5 -1 0 797.12 42.70 -5 1 0 735.43 42.70 -6 1 0 8.90 2.20 6 -1 0 7.40 1.90 -6 -1 0 6.80 1.70 -6 1 0 8.30 1.70 -6 -1 0 9.60 2.70 -7 -1 0 132.69 13.00 -7 -1 0 128.49 11.00 -7 -1 0 132.49 9.50 7 -1 0 142.09 9.50 7 -1 0 117.59 9.80 7 -1 0 122.59 9.00 -7 1 0 136.69 9.50 7 1 0 141.39 9.60 -7 1 0 126.39 10.00 -7 -1 0 148.89 11.10 -7 1 0 114.19 9.40 -7 1 0 150.78 11.00 7 1 0 124.89 10.50 -8 1 0 98.89 8.30 -8 -1 0 97.29 8.10 -8 -1 0 107.39 10.00 -9 1 0 618.54 36.30 9 -1 0 563.24 35.90 9 -1 0 546.05 37.80 9 1 0 565.74 38.40 -9 -1 0 645.64 38.70 -9 -1 0 631.94 36.20 9 -1 0 599.24 35.60 9 1 0 663.33 35.80 -9 1 0 571.64 39.60 9 -1 0 575.04 38.20 9 1 0 547.05 37.80 -9 1 0 530.25 35.80 -9 -1 0 601.74 40.30 -9 1 0 624.34 37.20 9 1 0 559.04 36.60 -10 -1 0 61.49 9.40 10 1 0 45.30 5.60 -11 1 0 166.48 13.50 -11 1 0 195.08 20.10 11 -1 0 156.08 20.60 -11 1 0 185.98 16.00 -11 -1 0 205.58 17.60 -11 -1 0 181.38 19.80 11 -1 0 197.98 14.10 11 1 0 183.38 15.90 11 1 0 177.28 18.60 -11 -1 0 190.98 13.90 11 1 0 194.98 12.90 11 -1 0 180.68 16.10 11 1 0 213.58 16.70 11 -1 0 176.58 13.00 -11 1 0 179.78 13.70 -12 -1 0 53.79 13.60 -12 -1 0 98.09 13.90 -12 1 0 94.39 12.60 -12 1 0 106.79 17.40 12 -1 0 70.89 9.10 12 1 0 98.79 12.20 12 -1 0 79.29 11.50 -13 -1 0 375.16 29.20 13 1 0 371.56 30.70 -13 1 0 387.36 25.10 13 1 0 374.96 28.90 -13 -1 0 409.16 25.30 -13 -1 0 326.17 31.50 13 -1 0 374.46 25.30 13 1 0 393.36 24.00 13 -1 0 344.77 27.70 13 1 0 388.26 27.80 13 -1 0 335.07 25.50 13 -1 0 351.96 30.10 -13 1 0 390.96 28.60 14 -1 0 20.00 7.30 14 -1 0 29.90 8.20 -14 -1 0 46.40 16.70 -14 1 0 12.30 4.20 14 -1 0 22.30 4.80 14 1 0 32.90 7.80 -14 1 0 35.70 14.40 14 1 0 17.80 9.80 14 1 0 14.50 7.00 -14 -1 0 39.80 9.90 -14 -1 0 10.70 4.50 -15 1 0 3.60 7.90 -15 1 0 -9.30 13.20 -15 -1 0 -14.40 8.80 15 1 0 -9.60 6.60 -15 1 0 -5.10 3.80 15 1 0 -7.30 6.60 15 1 0 -1.00 6.00 15 -1 0 -7.00 6.40 -15 -1 0 0.90 3.80 -15 -1 0 -20.50 12.30 15 -1 0 0.70 6.90 16 1 0 3.60 6.90 -16 1 0 6.00 4.60 -16 1 0 5.10 18.80 16 -1 0 3.10 8.00 -16 -1 0 0.20 4.20 -16 -1 0 24.90 11.20 -16 1 0 8.30 8.30 16 -1 0 2.40 6.60 -17 1 0 -3.40 4.20 -17 -1 0 0.00 4.80 17 1 0 14.10 11.40 17 1 0 -3.10 9.40 0 -2 0 476.85 29.00 0 -2 0 522.95 29.40 0 -2 0 475.95 29.00 0 2 0 498.65 28.90 0 2 0 499.15 29.40 1 2 0 0.10 0.60 -1 2 0 0.90 0.50 -1 -2 0 0.50 1.00 -1 -2 0 2.10 0.70 1 -2 0 1.30 0.40 -1 -2 0 -0.20 0.80 1 -2 0 1.00 0.50 1 2 0 2.30 0.80 1 -2 0 0.40 0.50 -1 2 0 1.80 0.50 -1 2 0 0.50 0.50 -1 2 0 0.60 0.40 1 -2 0 0.70 0.60 -1 -2 0 1.30 0.60 -1 2 0 1.70 0.80 1 -2 0 1.80 0.50 -1 -2 0 1.90 0.70 1 2 0 1.40 1.40 1 2 0 0.40 0.60 1 2 0 0.80 0.70 1 2 0 1.10 0.50 -1 -2 0 0.60 0.70 1 -2 0 1.40 0.40 -2 -2 0 4243.08 224.88 -2 -2 0 3510.65 224.28 -2 -2 0 4231.08 224.18 2 2 0 3543.95 224.28 -2 2 0 3689.73 223.68 2 2 0 3888.91 224.08 2 2 0 4011.50 224.78 2 -2 0 4217.98 223.98 -2 -2 0 3762.52 224.28 2 2 0 3631.74 224.28 -3 -2 0 28.40 2.80 3 2 0 27.00 4.00 3 -2 0 28.50 2.70 -3 -2 0 31.90 3.60 3 2 0 39.50 5.20 -3 -2 0 35.60 5.10 -3 2 0 24.70 2.70 -3 2 0 34.20 3.30 3 2 0 27.30 3.40 3 -2 0 28.60 3.00 3 -2 0 36.20 3.60 3 -2 0 29.80 3.00 3 -2 0 33.00 3.70 -3 -2 0 34.20 4.10 -3 2 0 33.10 3.00 -4 -2 0 948.51 57.79 4 -2 0 1052.89 57.99 -4 -2 0 1035.20 58.79 4 2 0 952.10 57.69 4 -2 0 1024.90 58.29 4 2 0 878.41 57.69 -4 2 0 882.01 57.69 4 -2 0 983.60 57.69 4 2 0 1065.19 59.69 -4 2 0 1055.99 57.69 4 -2 0 972.90 57.79 -4 -2 0 883.61 58.49 4 2 0 1025.00 58.19 -4 2 0 1003.40 58.39 -4 2 0 1072.79 58.19 4 -2 0 996.40 58.59 4 2 0 894.71 58.59 -4 -2 0 1035.40 59.69 -4 2 0 1007.10 58.79 4 2 0 936.41 58.59 -5 2 0 0.30 1.20 5 -2 0 5.10 2.90 -5 2 0 0.70 1.20 -5 2 0 3.10 1.60 5 -2 0 3.00 1.30 5 2 0 1.90 1.60 -5 -2 0 2.90 1.30 -5 2 0 1.30 1.10 5 2 0 2.30 1.40 5 2 0 5.60 2.40 -5 -2 0 3.90 2.30 5 -2 0 4.00 1.50 5 2 0 11.00 4.70 6 -2 0 458.35 26.50 6 -2 0 432.86 26.30 6 2 0 412.86 27.70 6 2 0 400.36 27.10 6 -2 0 439.46 25.90 -6 -2 0 459.65 26.20 6 2 0 460.75 27.10 6 2 0 383.06 27.20 6 2 0 423.96 26.00 -6 2 0 409.56 26.30 -6 2 0 434.66 26.90 6 -2 0 390.16 25.30 -6 2 0 458.35 26.40 6 2 0 418.86 26.60 -6 2 0 425.56 28.10 -6 -2 0 453.05 27.30 -6 -2 0 438.16 27.60 -7 -2 0 90.09 9.30 -7 -2 0 83.59 10.70 8 -2 0 801.52 49.40 8 -2 0 829.62 47.80 -8 2 0 828.22 51.19 -8 2 0 846.22 48.40 8 -2 0 745.03 47.20 -8 -2 0 745.13 48.90 8 -2 0 741.83 49.20 8 2 0 875.31 48.20 -8 2 0 899.21 47.90 -8 2 0 836.22 49.50 8 2 0 815.72 48.10 -8 -2 0 845.22 48.30 -8 2 0 810.82 48.70 -8 -2 0 863.61 49.99 8 2 0 755.82 49.10 8 2 0 744.63 50.29 8 2 0 742.23 49.80 8 -2 0 719.83 49.30 -9 -2 0 68.89 9.70 9 -2 0 55.39 5.00 -9 2 0 40.90 6.60 10 2 0 61.69 7.60 -10 -2 0 74.29 11.40 10 2 0 84.29 12.80 -10 2 0 68.49 9.20 -10 -2 0 77.29 12.10 10 2 0 84.39 9.80 10 2 0 72.99 7.50 -10 -2 0 72.29 7.50 -10 2 0 62.19 10.80 10 -2 0 94.39 10.10 10 -2 0 65.39 7.10 10 -2 0 87.49 11.90 10 -2 0 80.79 6.30 -10 2 0 84.39 9.60 -10 2 0 61.79 7.40 11 -2 0 5.70 5.70 -11 -2 0 8.70 3.20 11 2 0 15.50 6.80 -11 -2 0 8.40 6.60 11 2 0 10.80 6.90 -11 -2 0 3.20 7.20 11 2 0 8.90 4.60 -11 2 0 13.80 8.60 11 -2 0 8.60 2.60 -11 2 0 7.80 4.30 -11 2 0 8.90 2.90 12 -2 0 416.46 27.70 12 -2 0 452.45 26.20 -12 -2 0 405.46 35.70 12 2 0 394.76 33.20 12 -2 0 391.36 31.20 12 2 0 399.76 29.60 -12 2 0 378.76 35.20 -12 -2 0 454.65 27.80 -12 2 0 452.95 29.70 12 2 0 394.36 30.90 12 -2 0 373.06 29.80 -12 2 0 423.76 27.60 -12 -2 0 467.55 31.60 12 2 0 454.05 27.80 12 2 0 418.36 27.80 13 2 0 21.30 4.70 13 2 0 13.30 5.40 -13 2 0 31.20 6.70 13 2 0 36.50 9.20 -13 -2 0 20.50 4.40 13 -2 0 16.50 5.60 14 2 0 111.69 17.80 14 -2 0 138.29 16.70 -14 -2 0 133.09 11.90 14 -2 0 129.99 16.50 14 2 0 121.39 15.10 -14 -2 0 90.89 20.80 -14 2 0 115.49 11.50 -14 2 0 109.29 19.60 -14 -2 0 101.09 15.70 15 -2 0 -3.90 6.60 15 2 0 3.40 7.60 15 2 0 -5.30 7.70 -15 2 0 7.40 13.00 15 -2 0 -6.70 6.10 -15 -2 0 -9.90 13.30 -15 2 0 0.40 6.50 -15 -2 0 0.30 10.00 -15 2 0 -4.60 3.60 -15 -2 0 1.30 4.00 -16 -2 0 93.39 10.30 16 2 0 57.59 13.60 -16 -2 0 72.89 19.70 -16 -2 0 51.29 15.00 16 -2 0 72.89 13.60 -16 2 0 39.60 20.10 -16 2 0 76.99 13.80 16 -2 0 58.99 11.70 16 2 0 65.99 18.60 -16 2 0 74.99 10.20 -17 2 0 -11.60 8.80 17 -2 0 -9.90 8.50 -17 -2 0 -3.20 16.80 17 2 0 -7.70 8.10 -17 2 0 -9.60 3.90 17 2 0 -13.80 8.50 0 -3 0 7.80 1.90 0 3 0 3.20 1.20 0 3 0 7.60 1.80 0 3 0 5.90 1.20 0 -3 0 4.90 1.40 0 3 0 4.20 0.90 0 3 0 3.50 1.30 0 -3 0 4.90 1.30 0 -3 0 5.60 1.30 0 -3 0 4.10 0.90 1 -3 0 510.65 30.70 -1 -3 0 550.04 31.20 -1 3 0 456.95 30.80 -1 3 0 507.05 30.70 1 3 0 475.95 30.70 1 -3 0 481.65 30.50 1 -3 0 515.45 31.20 -1 3 0 497.65 30.70 1 -3 0 497.95 30.90 1 3 0 576.54 31.40 -1 3 0 538.35 30.50 -1 -3 0 561.54 31.10 1 -3 0 519.45 30.70 1 3 0 526.35 31.40 -1 -3 0 555.94 31.50 1 3 0 545.05 31.20 1 3 0 499.35 31.50 -1 -3 0 579.94 31.70 1 -3 0 539.15 30.40 -1 -3 0 506.25 30.80 -1 3 0 482.05 30.50 -1 3 0 544.15 31.30 2 -3 0 19.60 2.20 -2 -3 0 11.70 2.60 -2 3 0 15.90 2.20 2 3 0 10.90 2.50 3 3 0 1071.39 69.49 -3 3 0 1251.17 69.29 3 3 0 1149.29 69.49 3 3 0 1105.49 69.99 3 -3 0 1178.68 69.29 3 3 0 1181.88 70.89 -3 -3 0 1179.28 69.89 -3 -3 0 1249.47 70.49 3 3 0 1270.57 69.99 -3 3 0 1266.47 69.39 -3 -3 0 1166.28 69.29 3 -3 0 1095.19 69.29 3 -3 0 1105.19 68.79 3 -3 0 1146.49 69.39 -3 -3 0 1170.98 70.09 -3 -3 0 1212.88 69.99 3 3 0 1102.19 68.99 3 3 0 1171.28 70.59 -3 3 0 1263.57 69.49 3 -3 0 1127.29 69.19 -3 -3 0 1282.27 70.99 -3 3 0 1214.58 69.09 -3 -3 0 1251.47 69.09 -4 3 0 49.90 5.30 -4 -3 0 41.70 6.00 -4 -3 0 49.70 5.70 5 -3 0 2640.24 151.48 -5 3 0 2749.02 151.68 5 3 0 2604.24 151.28 5 3 0 2453.05 153.48 -5 -3 0 2765.52 152.38 5 3 0 2656.83 152.68 5 3 0 2598.94 152.08 -5 -3 0 2452.25 152.58 -5 3 0 2887.61 151.98 5 3 0 2577.84 152.68 5 3 0 2527.95 151.58 -5 -3 0 2675.93 151.38 -5 -3 0 2359.36 152.48 5 -3 0 2784.32 151.98 5 -3 0 2624.04 152.58 -5 -3 0 2364.16 152.38 5 3 0 2449.35 152.38 -5 -3 0 2507.15 153.58 5 -3 0 2813.82 151.38 7 -3 0 652.33 42.60 -7 -3 0 698.63 43.00 7 3 0 641.54 42.70 -7 -3 0 665.63 41.40 -7 3 0 733.23 41.70 -7 -3 0 661.33 44.50 -7 3 0 691.93 42.20 7 3 0 624.04 42.80 7 -3 0 676.83 42.10 -7 3 0 770.32 41.40 -7 3 0 671.83 41.60 -7 3 0 693.43 43.50 7 -3 0 688.73 41.40 7 3 0 721.33 43.70 7 -3 0 736.23 41.70 -8 -3 0 121.39 12.30 8 -3 0 110.19 10.40 8 3 0 119.09 10.70 -8 -3 0 89.39 14.80 -9 -3 0 72.59 7.40 9 -3 0 66.89 7.30 -9 3 0 95.49 9.20 9 3 0 72.49 7.70 9 3 0 92.39 9.70 9 -3 0 71.19 7.60 -9 3 0 73.19 7.30 -9 3 0 78.29 7.70 10 3 0 124.19 12.70 10 -3 0 126.19 12.20 -10 3 0 146.49 15.30 -10 -3 0 107.99 16.30 11 -3 0 124.49 12.60 -11 -3 0 121.09 17.40 -11 3 0 130.59 10.70 11 -3 0 110.29 11.10 11 3 0 128.29 13.90 11 -3 0 137.69 14.20 -11 3 0 121.49 16.50 11 3 0 131.99 13.10 11 3 0 127.59 12.90 -11 3 0 108.29 12.20 -11 -3 0 132.29 10.70 -11 3 0 128.99 12.00 11 3 0 117.99 16.80 11 3 0 121.59 11.00 -11 -3 0 127.79 16.30 12 3 0 157.68 13.40 -12 3 0 148.89 12.80 12 -3 0 162.28 14.60 -12 3 0 156.28 14.80 13 3 0 290.97 22.90 -13 3 0 306.77 21.40 13 3 0 308.67 25.70 13 3 0 282.17 27.00 13 3 0 297.67 25.70 13 -3 0 277.77 23.50 -13 3 0 320.37 24.00 13 -3 0 306.17 25.30 13 3 0 348.17 24.30 -13 -3 0 333.47 21.60 -13 -3 0 255.87 26.70 13 -3 0 321.87 25.20 -14 3 0 11.40 4.30 -14 -3 0 12.20 4.50 14 3 0 6.80 8.30 14 -3 0 6.00 5.90 -14 -3 0 20.50 16.30 -14 3 0 22.00 15.00 -14 3 0 13.50 6.70 14 -3 0 4.80 7.70 14 3 0 7.10 6.50 14 3 0 24.40 9.00 15 -3 0 6.30 7.60 15 3 0 36.50 10.60 -15 3 0 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418.36 27.90 3 15 0 397.76 31.30 -3 15 0 363.16 29.80 -3 15 0 455.95 31.70 3 15 0 440.86 28.30 3 15 0 374.46 30.50 -3 15 0 361.36 31.80 3 15 0 405.16 27.90 3 -15 0 339.07 30.40 3 -15 0 391.46 26.30 -3 -15 0 397.16 27.60 -4 -15 0 71.39 11.50 -4 15 0 52.89 9.00 -5 15 0 60.69 9.20 -5 -15 0 39.00 14.00 -5 15 0 40.00 6.00 -5 15 0 37.80 8.50 -5 15 0 49.50 12.20 5 -15 0 53.39 9.80 -5 -15 0 34.30 7.80 5 15 0 43.80 7.80 -5 15 0 43.20 7.70 5 15 0 28.30 8.40 5 15 0 36.40 9.80 6 15 0 2.30 6.60 6 15 0 5.40 7.50 6 -15 0 7.00 7.90 6 15 0 0.30 5.60 -6 -15 0 -3.50 6.30 -6 15 0 -3.90 3.40 6 15 0 3.60 4.00 -6 15 0 -4.60 4.40 -6 15 0 7.30 9.60 -6 15 0 1.60 4.30 -6 15 0 0.00 3.50 -6 -15 0 9.80 12.60 -6 15 0 -0.40 4.30 7 15 0 56.89 14.40 7 15 0 64.99 13.10 -7 -15 0 81.19 17.30 -7 15 0 80.39 9.50 -7 15 0 91.39 10.90 -7 15 0 112.29 14.30 -7 -15 0 87.49 14.10 -7 15 0 98.29 11.90 -7 15 0 76.19 11.10 7 15 0 76.49 11.30 -8 15 0 0.20 4.50 8 15 0 -7.70 6.10 -8 15 0 -4.60 4.30 8 -15 0 -6.30 6.10 8 15 0 -0.20 4.90 8 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22 -3.50 2.60 7 0 22 -0.50 4.50 7 0 22 2.80 4.30 7 0 22 6.70 6.70 -7 0 22 0.10 4.80 -8 0 -22 208.38 22.80 8 0 -22 266.17 18.10 -8 0 -22 261.07 19.50 -8 0 -22 238.58 17.80 8 0 22 241.78 20.50 -8 0 22 213.68 19.60 -8 0 22 251.97 18.00 8 0 22 198.08 32.90 -9 0 22 21.10 6.00 9 0 22 23.90 7.70 -9 0 -22 34.80 7.10 9 0 -22 29.20 7.10 -9 0 -22 19.20 4.90 -9 0 22 15.50 7.70 -9 0 22 16.60 4.50 -9 0 -22 36.40 11.60 9 0 22 27.60 7.10 -10 0 22 20.00 10.40 -10 0 -22 11.30 9.90 -10 0 -22 6.90 5.20 -10 0 22 6.50 7.50 10 0 22 7.00 6.10 10 0 22 12.40 6.80 -11 0 -22 151.78 15.80 -11 0 -22 152.98 22.50 11 0 22 92.19 15.20 -11 0 22 110.29 17.40 11 0 -22 132.69 14.30 11 0 22 106.99 15.60 -11 0 -22 132.89 12.80 12 0 22 6.20 7.80 12 0 22 3.80 7.70 -12 0 -22 -9.60 10.60 -12 0 -22 2.80 6.30 -12 0 -22 -1.70 4.10 12 0 22 0.50 5.50 -13 0 -22 -2.30 11.10 13 0 22 -14.80 7.00 13 0 22 -0.30 7.00 -13 0 22 -8.30 7.40 -14 0 -22 12.40 15.40 0 1 -22 1776.32 110.99 0 1 22 1836.42 110.39 0 1 22 1849.21 109.59 0 1 -22 1865.71 108.49 0 -1 -22 1830.42 108.69 0 -1 22 1895.71 109.79 0 -1 22 1793.92 111.19 0 -1 -22 1923.31 110.69 0 1 -22 1944.71 109.19 0 -1 -22 1821.42 108.59 0 1 -22 1860.61 110.59 0 1 22 1882.71 108.89 0 1 22 1922.71 109.39 0 -1 22 1833.22 108.69 0 -1 22 1824.92 110.99 1 1 -22 10.00 4.70 1 -1 22 5.40 4.20 1 -1 22 7.90 3.00 -1 1 22 7.90 3.60 1 1 -22 -0.10 3.50 -1 1 22 4.50 3.60 -1 -1 -22 14.20 3.10 -1 -1 -22 5.50 3.40 1 -1 22 5.70 4.50 1 1 -22 7.40 2.10 -1 1 22 6.10 2.00 -1 1 22 12.90 2.70 -1 -1 -22 7.20 3.90 -1 -1 22 7.20 4.20 1 -1 -22 6.20 3.40 -1 -1 22 7.70 2.50 -1 -1 22 3.90 3.90 -1 1 -22 15.30 4.60 1 1 22 9.60 3.80 1 1 22 4.90 3.70 1 -1 -22 9.50 3.40 1 1 22 11.10 2.80 -1 1 -22 12.40 3.30 -1 1 -22 10.90 4.30 -1 1 -22 10.30 2.60 -1 -1 22 7.20 2.90 2 -1 22 24.50 5.90 2 -1 22 50.29 8.10 2 1 -22 42.80 4.90 -2 1 22 49.90 7.30 2 1 -22 37.20 6.00 -2 1 22 34.60 4.30 -2 -1 22 31.80 6.30 3 1 -22 113.89 9.30 -3 1 22 116.19 10.20 3 -1 22 119.89 12.20 3 -1 22 110.99 12.10 3 1 -22 108.79 8.10 3 1 -22 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-2 22 60.49 12.00 10 2 22 99.49 14.50 10 -2 -22 96.99 12.20 -10 2 -22 93.09 16.60 10 2 22 74.79 14.20 -10 2 -22 86.19 12.40 -10 2 -22 75.19 9.80 -10 -2 22 68.99 13.90 11 -2 22 94.19 13.40 -11 -2 -22 105.59 11.10 11 -2 22 96.99 15.40 -11 -2 -22 84.69 17.20 -11 2 -22 105.19 10.60 11 2 22 65.09 11.30 11 2 22 73.99 14.30 11 2 22 64.39 14.30 -11 2 -22 56.79 14.20 -11 2 -22 115.19 13.20 -11 -2 22 58.59 15.10 12 -2 22 28.40 11.20 -12 -2 -22 26.30 8.60 12 -2 22 22.80 8.90 -12 -2 -22 3.00 11.60 12 -2 22 16.30 8.20 -12 -2 -22 26.70 6.20 -12 2 -22 14.60 5.00 12 2 22 32.20 9.00 12 2 22 5.20 8.10 -12 2 -22 34.00 13.10 12 2 22 22.20 11.80 -12 2 -22 24.10 7.30 -13 -2 -22 5.10 12.10 13 -2 22 24.00 8.70 13 -2 22 11.20 15.30 13 -2 22 28.10 10.00 -13 -2 -22 22.60 10.80 -13 -2 -22 38.20 7.90 13 2 22 9.30 9.30 -13 2 -22 21.80 10.60 -13 2 -22 27.40 9.60 13 2 22 20.10 14.20 13 2 22 25.50 9.00 -13 2 -22 22.10 12.90 0 -3 22 40.00 5.20 0 3 22 40.40 7.00 0 3 -22 51.79 5.00 0 -3 -22 47.20 6.80 0 3 22 43.50 6.10 0 3 -22 63.39 8.20 0 3 22 56.39 8.50 0 3 22 53.29 5.40 0 -3 22 58.89 8.50 0 3 -22 40.40 7.00 1 3 -22 24.30 5.70 -1 -3 -22 37.30 4.50 -1 -3 -22 36.00 6.50 1 -3 22 24.30 6.30 -1 3 22 33.70 4.40 1 3 -22 39.40 5.70 -1 -3 -22 25.90 4.40 -1 3 22 29.40 5.00 -1 -3 -22 29.10 4.00 -1 3 22 20.50 6.10 1 -3 22 30.10 5.90 1 3 -22 38.40 6.10 -1 3 22 26.30 3.50 1 3 -22 32.70 3.80 -1 3 22 27.90 4.70 1 3 22 36.60 4.70 -1 -3 22 29.10 5.50 -1 3 -22 31.90 4.50 -1 3 -22 30.10 5.40 1 3 22 31.40 6.20 -1 -3 22 27.20 6.80 -1 3 -22 31.10 6.20 -1 -3 22 23.70 4.80 1 3 22 30.10 5.10 1 3 22 24.30 5.20 1 -3 -22 32.50 5.20 2 3 -22 35.20 3.70 2 3 -22 45.50 6.00 -2 -3 -22 48.70 6.30 -2 3 22 44.00 4.80 2 3 -22 46.80 6.30 2 -3 22 34.20 6.50 -2 3 22 35.60 5.10 -2 3 22 41.10 5.50 2 -3 22 44.40 7.70 2 3 -22 29.30 5.70 -2 3 22 34.40 5.40 -2 -3 -22 44.30 7.30 2 -3 -22 41.90 5.90 -2 -3 22 40.70 4.00 2 3 22 41.50 7.00 2 3 22 35.90 6.30 2 3 22 46.40 5.60 -2 3 -22 48.10 7.80 -2 3 -22 45.50 5.50 -2 3 -22 46.30 6.60 2 3 22 32.30 5.50 -2 -3 22 32.30 5.30 -2 3 -22 29.60 6.60 -2 -3 22 26.00 7.30 -2 -3 22 35.90 6.50 -3 -3 -22 256.07 16.70 -3 3 22 244.78 16.20 -3 3 22 234.68 15.10 3 3 -22 248.88 16.30 -3 3 22 235.88 15.40 3 -3 22 231.38 19.10 -3 -3 -22 223.58 16.80 3 3 -22 231.68 18.50 3 -3 22 223.78 18.50 -3 -3 -22 211.98 19.40 3 3 22 223.48 17.90 -3 3 -22 267.77 17.30 -3 -3 22 203.18 20.00 3 -3 -22 234.48 16.00 -3 3 -22 242.48 20.10 -3 -3 22 229.88 17.90 -3 3 -22 199.38 19.00 3 3 22 224.58 18.90 -3 3 -22 227.68 15.90 -4 3 22 5.90 1.60 4 3 -22 3.10 4.20 -4 3 22 5.20 1.80 -4 -3 -22 10.60 3.30 -4 3 22 9.00 3.30 -4 -3 -22 0.50 4.90 4 -3 22 7.10 4.80 4 -3 22 6.50 5.20 -4 -3 -22 7.80 5.20 4 3 -22 6.20 2.80 -4 3 22 3.90 1.90 -4 3 22 8.10 2.00 4 3 -22 3.90 2.90 -4 3 -22 10.70 3.30 -4 -3 22 -1.60 6.20 4 3 22 -3.20 4.00 4 3 22 7.00 4.20 -4 -3 22 0.10 2.50 4 -3 -22 5.70 2.40 4 3 22 -3.80 4.10 -4 3 -22 5.20 4.40 -4 3 -22 0.10 4.50 -4 3 -22 3.60 2.70 -4 -3 22 0.70 4.80 5 3 -22 134.79 12.40 5 3 -22 140.49 11.30 5 3 -22 119.39 13.10 -5 -3 -22 124.09 16.00 -5 -3 -22 122.49 12.80 5 3 -22 138.89 10.70 -5 3 22 134.09 11.00 -5 -3 -22 136.29 11.70 -5 3 22 134.19 8.70 5 -3 22 131.19 14.40 5 -3 22 159.78 14.90 -5 -3 22 135.49 16.90 -5 -3 22 146.99 13.40 -5 3 -22 141.79 12.20 -5 -3 22 137.79 12.10 5 3 22 139.99 14.10 5 3 22 137.79 13.60 -5 3 -22 108.49 13.50 -5 3 -22 149.39 15.00 -5 3 -22 122.19 10.90 -6 -3 -22 10.90 4.00 -6 3 22 7.40 4.80 6 3 -22 4.80 3.80 -6 -3 -22 9.80 7.60 6 -3 22 22.90 5.50 6 3 -22 12.70 3.50 6 -3 22 9.80 5.60 -6 -3 -22 15.50 5.30 6 3 -22 9.30 2.80 6 -3 22 5.60 6.30 6 3 22 13.20 5.50 6 3 22 12.10 5.20 -6 3 -22 5.60 6.00 -6 -3 22 7.10 5.30 6 3 22 4.70 5.90 -6 -3 22 11.00 5.30 -6 3 -22 12.20 4.20 -6 -3 22 8.80 8.10 -6 3 -22 11.70 3.70 -6 3 -22 0.90 5.00 -7 3 22 91.69 10.70 7 3 -22 82.39 7.70 7 -3 22 93.39 13.30 -7 -3 -22 91.39 12.30 7 3 -22 79.49 9.60 -7 -3 -22 77.19 9.30 7 -3 22 76.29 11.30 -7 -3 22 69.79 13.60 7 3 22 88.19 11.90 -7 3 -22 70.99 10.70 -7 -3 22 89.39 11.80 7 3 22 83.09 12.40 -7 3 -22 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23 31.10 12.40 7 7 23 21.60 8.20 7 7 23 14.60 11.90 7 7 23 19.10 6.70 -7 7 -23 40.00 9.80 -7 7 -23 29.80 7.60 -7 7 -23 22.10 5.80 8 -7 23 34.80 10.40 -8 7 23 64.59 9.30 8 -7 23 59.89 10.70 8 7 -23 39.90 7.60 -8 7 23 49.40 7.50 8 7 -23 45.40 10.80 8 -7 23 55.69 8.90 -8 -7 -23 25.30 12.60 -8 -7 -23 58.79 8.30 -8 -7 -23 45.70 9.60 8 7 23 34.10 10.00 -8 7 -23 66.89 12.60 8 7 23 59.09 12.20 -8 -7 23 38.90 9.10 -8 -7 23 32.80 13.60 8 7 23 54.29 9.70 -8 7 -23 47.20 9.50 -8 7 -23 57.29 7.70 9 7 -23 6.60 5.80 -9 7 23 2.70 3.90 -9 7 23 -3.40 4.90 -9 7 23 7.90 2.90 9 7 -23 3.00 7.10 -9 -7 -23 5.80 4.80 9 -7 23 1.50 5.60 9 7 -23 3.80 6.20 -9 -7 -23 -14.10 10.00 9 7 -23 8.20 4.90 9 -7 23 16.70 7.80 -9 -7 -23 -6.40 7.70 9 -7 23 -10.30 7.50 -9 7 -23 4.60 6.30 -9 7 -23 6.60 7.90 -9 7 -23 1.70 4.10 9 7 23 -4.40 6.90 9 7 23 2.00 5.70 9 7 23 7.40 8.60 -9 -7 23 1.40 7.40 -9 -7 23 11.60 11.60 -9 7 -23 8.60 4.80 -10 -7 -23 33.30 9.40 -10 -7 -23 29.00 12.80 -10 7 23 37.50 6.30 10 -7 23 27.30 11.90 10 7 -23 39.70 7.30 10 -7 23 32.80 7.70 -10 7 23 43.20 8.20 10 7 -23 28.20 11.90 -10 -7 -23 32.50 7.20 10 7 -23 43.30 9.60 10 7 -23 20.10 6.10 10 -7 23 32.50 10.00 10 7 23 24.50 11.00 -10 7 -23 29.00 7.90 -10 -7 23 45.70 15.20 10 7 23 23.60 10.00 -10 7 -23 46.10 12.80 -10 7 -23 29.20 6.40 10 7 23 39.60 9.00 -10 -7 23 33.30 10.20 -10 7 -23 46.50 7.40 11 -7 23 -1.50 6.80 -11 -7 -23 20.50 8.60 11 7 -23 7.80 6.00 11 -7 23 4.20 5.10 -11 -7 -23 7.10 5.50 -11 -7 -23 -9.60 11.80 -11 7 23 3.10 5.10 11 -7 23 9.10 9.80 11 7 -23 4.90 5.80 11 7 23 12.30 10.30 -11 7 -23 -2.10 9.10 -11 -7 23 8.30 9.50 11 7 23 -4.00 7.30 11 7 23 0.40 5.40 -11 7 -23 1.40 4.30 -11 7 -23 0.80 6.20 -11 7 -23 7.70 5.50 -12 -7 -23 16.90 10.20 12 7 -23 29.30 6.70 -12 -7 -23 29.30 7.20 12 -7 23 30.60 9.80 12 7 -23 28.00 11.10 -12 7 -23 44.90 8.60 -12 7 -23 15.20 8.10 -12 -7 23 19.60 11.50 -12 7 -23 30.70 7.00 12 7 23 44.60 12.30 -12 7 -23 36.40 13.30 12 7 23 21.60 12.50 12 7 23 23.80 8.90 0 -8 23 -9.50 4.70 0 -8 23 -11.90 8.20 0 8 -23 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5.90 3 1 -28 31.50 5.50 -3 1 -28 26.90 7.20 -3 1 -28 38.00 5.90 3 1 28 24.10 8.10 -3 -1 28 21.90 4.70 -3 1 -28 23.70 6.90 -3 -1 28 25.70 6.30 3 1 28 18.20 7.00 -3 -1 28 31.70 6.90 3 1 28 25.80 7.10 -3 1 -28 27.30 4.70 -4 -1 -28 -1.50 3.40 -4 -1 -28 2.20 4.00 -4 1 28 1.30 3.20 -4 1 28 -3.50 4.20 4 -1 28 7.10 6.40 4 1 -28 -1.30 3.00 -4 -1 -28 2.20 6.20 4 -1 28 -0.80 4.30 4 -1 28 -5.30 5.40 4 -1 -28 1.70 3.30 4 1 28 -5.70 5.40 -4 1 -28 -1.40 5.00 -4 -1 28 -5.50 4.40 -4 1 -28 1.60 3.20 -4 1 -28 -0.50 5.30 -4 -1 28 -1.50 4.10 -4 1 -28 3.80 3.70 4 1 28 0.30 4.70 4 1 28 4.10 6.40 -5 1 28 17.20 4.30 5 -1 28 22.60 8.00 -5 1 28 15.40 5.70 -5 -1 -28 14.80 5.20 5 1 -28 21.40 4.70 5 -1 28 14.50 6.30 5 -1 28 8.00 5.70 -5 -1 -28 6.40 6.00 -5 -1 -28 21.90 4.80 -5 1 28 14.10 3.40 -5 1 -28 16.30 4.60 -5 1 -28 19.30 7.30 -5 1 -28 10.40 4.30 5 1 28 2.90 5.60 -5 -1 28 14.70 6.40 5 1 28 17.10 6.20 5 -1 -28 13.80 5.10 6 -1 28 96.19 13.60 -6 -1 -28 92.29 9.70 6 -1 28 81.39 12.80 -6 1 28 76.09 8.60 -6 -1 -28 77.99 11.40 -6 -1 -28 73.19 12.90 6 1 28 82.39 12.30 6 1 28 63.69 11.80 -6 1 -28 93.79 12.40 -6 -1 28 80.39 11.60 -6 1 -28 71.69 12.70 6 1 28 93.99 13.40 -6 1 -28 82.79 9.40 -6 -1 28 56.39 10.10 -7 1 28 62.29 7.80 7 -1 28 67.49 10.60 7 -1 28 68.99 12.40 -7 -1 -28 58.19 11.30 7 1 -28 71.79 9.00 -7 1 28 51.79 9.40 -7 -1 -28 33.80 11.00 7 -1 28 55.89 10.10 -7 -1 -28 70.49 8.90 -7 -1 28 49.60 8.60 7 1 28 58.49 10.60 -7 1 -28 42.00 10.80 7 1 28 42.40 10.30 -7 1 -28 69.59 10.80 -7 -1 28 49.80 9.50 -7 1 -28 69.19 8.80 7 1 28 51.89 9.50 7 -1 -28 66.29 9.40 -8 -1 -28 70.59 9.70 -8 1 28 53.09 11.10 8 -1 28 66.39 13.20 8 -1 28 66.99 10.90 -8 -1 -28 55.89 18.70 -8 1 28 72.69 7.90 8 -1 28 62.69 11.20 -8 -1 -28 85.69 12.20 -8 -1 28 82.59 13.40 8 1 28 81.09 13.30 8 1 28 65.89 12.30 8 1 28 74.29 11.70 -8 1 -28 63.09 13.40 -8 -1 28 48.10 10.30 -8 1 -28 59.99 8.20 -8 1 -28 83.99 11.80 9 -1 28 0.40 5.80 -9 -1 -28 -10.50 8.90 -9 -1 -28 4.80 4.60 -9 -1 -28 0.50 5.70 -9 1 28 -0.30 2.80 9 -1 28 -2.40 5.20 9 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-1 2 -28 17.40 4.10 1 2 28 7.60 5.20 -1 2 -28 6.80 4.80 -1 -2 28 10.50 5.50 -1 2 -28 8.70 3.00 -1 -2 28 10.70 5.70 1 -2 -28 8.60 4.30 -1 -2 28 12.20 2.80 1 2 28 5.60 4.10 -2 2 28 48.30 5.50 -2 2 28 70.59 9.30 -2 -2 -28 45.60 8.60 2 2 -28 64.59 7.00 -2 -2 -28 66.99 8.00 -2 2 28 62.69 8.00 2 2 -28 34.20 7.40 2 -2 28 41.70 8.10 2 2 -28 65.69 9.00 -2 2 -28 58.69 13.50 -2 -2 28 40.90 8.10 -2 2 -28 37.70 7.80 -2 -2 28 62.09 5.20 -2 -2 28 42.40 7.70 2 2 28 47.10 9.30 2 -2 -28 58.89 8.60 2 2 28 58.79 9.40 -2 2 -28 54.59 7.00 2 2 28 44.10 8.10 2 2 28 49.00 7.40 -2 2 -28 65.89 8.70 3 2 -28 106.99 8.70 -3 -2 -28 101.79 10.70 -3 2 28 108.39 9.80 3 -2 28 106.29 13.30 -3 -2 -28 87.09 14.30 -3 -2 -28 100.99 10.10 3 -2 28 99.09 13.40 3 2 -28 88.09 12.60 -3 2 28 90.09 7.40 -3 2 28 92.49 11.00 3 2 -28 119.49 11.10 3 2 28 96.99 14.30 -3 2 -28 103.19 13.60 3 2 28 83.79 12.10 -3 -2 28 92.39 12.60 -3 2 -28 103.09 9.40 3 2 28 75.59 13.10 -3 2 -28 111.89 11.10 3 -2 -28 108.29 10.90 -3 -2 28 87.39 12.80 -3 -2 28 84.19 13.20 -3 2 -28 103.99 13.80 4 -2 28 46.10 9.10 -4 -2 -28 34.90 5.80 4 2 -28 43.30 9.00 4 2 -28 34.30 6.00 -4 2 28 43.30 6.30 -4 -2 -28 30.40 8.40 -4 -2 -28 44.40 6.90 4 2 -28 45.50 5.40 -4 2 28 28.90 4.60 -4 2 28 28.40 6.80 4 -2 28 36.30 7.90 -4 2 -28 30.60 7.90 4 2 28 43.60 8.90 4 2 28 30.60 7.90 -4 2 -28 33.70 5.20 4 2 28 38.70 7.70 -4 2 -28 43.30 6.50 4 -2 -28 50.09 7.10 -4 2 -28 37.10 8.20 -4 -2 28 32.80 7.60 -4 -2 28 25.20 7.10 -5 -2 -28 39.60 9.40 -5 -2 -28 52.79 6.90 5 -2 28 35.90 8.00 -5 -2 -28 53.09 7.70 -5 2 28 47.50 6.10 5 -2 28 24.70 7.90 5 -2 28 60.49 10.10 5 2 -28 53.39 7.80 -5 2 28 33.70 5.40 -5 2 28 28.90 7.40 -5 2 -28 31.00 5.60 -5 2 -28 51.59 7.40 5 -2 -28 44.30 7.10 -5 -2 28 37.40 8.00 -5 2 -28 35.00 9.50 5 2 28 53.99 9.40 5 2 28 40.50 16.00 5 2 28 38.80 9.10 -5 -2 28 24.40 7.50 -5 2 -28 34.20 7.80 -6 -2 -28 -2.10 7.60 6 -2 28 16.00 6.80 6 -2 28 12.70 6.50 6 2 -28 12.80 4.40 -6 2 28 6.90 2.50 -6 2 28 8.40 5.70 -6 -2 -28 16.20 4.90 -6 -2 -28 10.50 5.00 -6 2 28 10.80 2.90 6 -2 28 8.50 7.50 6 2 28 10.80 6.20 6 -2 -28 12.00 3.60 -6 -2 28 10.30 6.80 6 2 28 5.30 6.00 -6 2 -28 3.60 5.50 -6 2 -28 15.00 4.40 6 2 28 0.60 6.80 -6 -2 28 3.30 6.00 -6 2 -28 10.00 7.30 -6 2 -28 13.80 5.00 -7 -2 -28 9.80 6.00 7 -2 28 28.00 8.30 7 -2 28 19.80 7.20 -7 -2 -28 15.30 8.90 -7 -2 -28 27.60 5.70 -7 2 28 9.90 6.20 7 -2 28 26.80 9.70 7 2 -28 25.70 5.80 7 2 28 19.60 6.90 -7 -2 28 12.00 9.10 -7 2 -28 20.00 5.60 -7 -2 28 5.00 7.60 -7 2 -28 26.10 5.30 -7 2 -28 21.90 11.60 7 2 28 13.30 7.80 -7 2 -28 9.80 6.50 7 2 28 12.70 7.10 8 -2 28 -11.20 7.00 8 -2 28 4.70 6.20 -8 2 28 2.60 5.90 -8 -2 -28 9.20 6.30 8 2 -28 7.90 4.70 8 -2 28 4.60 5.80 -8 -2 -28 9.70 4.60 -8 -2 -28 -7.20 9.30 -8 -2 28 1.70 7.60 -8 2 -28 3.90 9.30 -8 2 -28 9.60 4.60 -8 -2 28 1.90 8.00 8 2 28 -5.40 4.50 8 2 28 0.20 5.30 -8 2 -28 0.20 4.30 -9 -2 -28 2.40 5.60 -9 2 28 0.00 4.10 9 -2 28 6.60 6.20 -9 -2 -28 5.20 10.50 -9 -2 -28 -8.30 3.90 9 -2 28 -9.00 7.50 -9 2 28 -1.20 6.80 -9 -2 28 -3.60 8.40 -9 2 -28 3.40 5.70 9 2 28 -4.60 6.30 -9 -2 28 -7.00 7.70 -9 2 -28 -12.20 7.80 9 2 28 1.00 5.70 -9 2 -28 4.90 4.40 -10 -2 -28 6.30 4.80 10 -2 28 -9.00 12.40 -10 -2 -28 3.70 6.60 10 -2 28 5.90 6.80 -10 2 28 8.90 8.50 -10 -2 -28 -8.30 10.20 10 -2 28 2.30 6.90 10 2 28 3.80 7.10 -10 2 -28 -1.00 4.50 -10 -2 28 -5.30 7.70 -10 2 -28 -3.30 9.90 -10 2 -28 2.80 5.00 -10 -2 28 0.80 9.20 10 2 28 -1.70 8.30 -11 -2 -28 99.09 13.30 11 -2 28 107.39 16.20 11 -2 28 106.59 16.30 -11 -2 -28 115.29 15.60 11 2 28 77.69 13.40 -11 -2 28 62.89 15.20 11 2 28 89.89 16.60 11 2 28 94.89 14.30 -11 2 -28 86.19 14.10 -11 2 -28 90.59 17.80 0 3 28 63.09 7.30 0 3 -28 81.79 10.30 0 3 28 59.49 10.50 0 3 -28 66.49 6.80 0 3 -28 74.09 8.40 0 3 28 66.19 10.10 0 -3 28 72.39 10.10 0 -3 -28 53.39 8.80 0 3 28 70.99 9.00 -1 -3 -28 40.10 7.60 1 3 -28 35.60 5.00 1 -3 28 27.20 7.50 1 3 -28 34.10 6.30 -1 -3 -28 26.30 4.80 -1 3 28 30.50 5.20 1 3 -28 34.90 5.10 -1 -3 -28 41.50 5.30 1 3 -28 19.60 6.90 -1 3 28 39.80 13.30 -1 3 28 35.10 6.20 1 3 28 35.10 5.70 -1 -3 28 20.60 6.60 -1 3 -28 35.50 7.00 -1 3 -28 22.10 6.30 1 3 28 21.20 5.90 -1 -3 28 33.30 4.00 -1 3 -28 34.10 5.30 -1 -3 28 24.50 7.20 1 3 28 38.10 8.00 1 -3 -28 32.70 6.60 -1 3 -28 27.80 4.10 -2 -3 -28 17.90 4.70 -2 -3 -28 27.00 7.30 2 3 -28 22.30 5.40 -2 -3 -28 31.50 5.40 2 -3 28 26.50 6.60 -2 3 28 29.10 5.70 2 -3 28 30.40 7.10 2 3 -28 25.20 4.40 2 3 -28 14.80 6.20 -2 3 28 45.40 11.60 -2 3 28 27.20 4.70 -2 3 28 25.30 4.90 2 3 28 28.70 7.60 -2 -3 28 18.40 6.80 -2 -3 28 25.70 6.80 2 3 28 20.70 4.20 -2 3 -28 27.20 5.30 -2 3 -28 23.20 6.50 2 -3 -28 28.30 5.30 2 3 28 25.50 5.90 2 3 28 19.10 6.00 -2 3 -28 22.70 4.20 -2 -3 28 18.40 3.00 -3 -3 -28 54.29 6.80 -3 -3 -28 45.20 7.40 3 -3 28 64.49 14.20 -3 3 28 54.19 6.40 3 -3 28 50.79 9.10 3 3 -28 41.90 7.70 -3 3 28 39.00 5.50 -3 -3 -28 49.20 10.20 3 3 28 46.00 8.70 3 3 28 36.90 7.10 3 -3 -28 46.30 6.60 -3 3 -28 48.60 8.70 3 3 28 48.30 9.50 -3 -3 28 30.40 8.00 -3 3 -28 55.89 9.30 -3 3 -28 57.79 7.20 4 3 -28 0.30 2.40 -4 -3 -28 -1.90 4.00 4 -3 28 1.20 6.00 -4 3 28 4.50 2.30 -4 3 28 4.10 2.30 -4 3 28 -2.50 3.90 4 -3 28 3.80 4.70 4 3 -28 -1.70 4.40 -4 -3 -28 -3.40 8.60 4 3 -28 3.30 3.30 -4 -3 -28 4.90 3.80 4 3 28 -1.70 5.20 -4 3 -28 -0.20 2.80 -4 -3 28 -4.40 5.30 -4 3 -28 4.00 5.70 4 3 28 -2.30 4.40 -4 3 -28 -2.10 4.80 4 -3 -28 6.70 3.50 4 3 28 4.60 5.60 -4 3 -28 4.80 3.80 -5 -3 -28 17.90 5.30 5 -3 28 28.40 7.80 5 3 -28 24.90 6.20 -5 3 28 17.80 5.50 5 3 -28 21.90 3.50 5 -3 28 16.10 6.10 -5 -3 -28 21.30 5.10 -5 -3 -28 8.20 8.20 5 -3 28 11.00 7.20 5 3 -28 21.30 5.00 -5 3 -28 32.10 8.10 -5 3 -28 17.50 7.30 -5 -3 28 7.10 8.70 5 3 28 16.20 8.50 -5 3 -28 13.50 4.00 5 -3 -28 19.30 4.40 -5 3 -28 13.70 6.30 5 3 28 16.30 5.90 -5 -3 28 5.00 6.30 5 3 28 18.60 7.40 6 -3 28 40.80 8.70 6 3 -28 34.90 6.10 6 -3 28 29.60 8.20 -6 -3 -28 34.90 7.20 -6 -3 -28 17.00 8.50 -6 3 28 25.30 6.70 6 3 28 22.00 8.00 -6 -3 28 25.90 8.30 6 3 28 34.00 8.90 6 3 28 28.60 7.50 -6 3 -28 25.70 9.00 -6 -3 28 22.90 8.00 -6 3 -28 15.10 6.40 -6 3 -28 27.30 5.50 7 -3 28 14.70 6.90 -7 -3 -28 0.80 5.00 7 3 -28 8.90 4.20 -7 -3 -28 12.00 4.90 -7 -3 -28 9.20 9.80 7 -3 28 5.40 5.70 7 -3 28 -1.50 7.10 -7 -3 28 -5.60 6.40 -7 3 -28 9.90 5.60 7 3 28 6.40 6.40 -7 -3 28 -6.40 7.50 7 3 28 4.90 5.40 -7 3 -28 3.50 4.00 7 3 28 5.20 7.10 -7 3 -28 -3.80 5.80 -7 3 -28 12.40 8.70 -8 -3 -28 58.09 8.00 8 3 -28 72.39 11.10 8 -3 28 58.79 12.60 -8 -3 -28 47.50 8.00 -8 -3 -28 44.10 13.70 8 -3 28 48.40 9.60 -8 3 -28 34.60 11.20 -8 3 -28 56.09 8.80 -8 -3 28 45.20 11.40 -8 -3 28 35.50 10.50 8 3 28 49.90 10.60 -8 3 -28 49.80 7.30 8 3 28 31.90 9.60 8 3 28 45.10 9.40 9 -3 28 0.00 5.80 -9 3 28 1.00 6.20 -9 -3 -28 -19.60 9.90 -9 -3 -28 -7.80 5.30 -9 -3 -28 -0.20 4.40 -9 3 28 5.80 7.30 9 -3 28 -1.60 8.50 9 -3 28 0.40 5.60 9 3 -28 6.80 5.20 9 3 28 2.70 6.60 -9 3 -28 -0.20 4.20 -9 -3 28 2.90 8.30 9 3 28 10.10 6.40 -9 3 -28 -0.40 8.60 -9 3 -28 8.60 6.70 -9 3 -28 -1.50 4.50 -9 -3 28 -3.50 9.60 -10 -3 -28 25.60 7.90 10 -3 28 28.30 8.90 -10 -3 -28 21.10 5.90 -10 -3 -28 13.90 13.20 10 -3 28 26.20 7.80 -10 -3 28 18.80 11.90 -10 -3 28 12.30 9.40 -10 3 -28 23.80 12.30 -10 3 -28 21.90 7.20 10 3 28 23.40 9.80 -10 3 -28 19.70 5.90 10 3 28 27.20 11.20 -11 -3 -28 -12.70 10.90 11 -3 28 -8.50 6.60 -11 -3 -28 -1.40 7.00 -11 -3 -28 -10.80 4.30 11 3 28 -5.70 7.20 -11 3 -28 -0.50 5.80 -11 3 -28 3.90 11.40 -11 3 -28 -7.10 5.00 11 3 28 4.90 10.50 0 -4 28 30.10 8.00 0 4 28 33.60 6.10 0 4 28 35.30 5.60 0 4 -28 29.30 4.10 0 4 -28 33.20 5.50 0 4 28 27.60 7.80 0 4 28 36.90 5.40 0 4 -28 44.70 7.50 0 -4 28 31.10 7.20 0 -4 -28 33.20 6.90 0 4 -28 27.30 7.40 -1 4 28 4.10 4.00 -1 4 28 2.80 5.60 1 4 -28 10.20 4.50 -1 4 28 3.70 2.90 1 4 -28 5.30 5.20 -1 -4 -28 5.80 5.30 1 -4 28 -1.30 5.40 1 4 -28 1.70 3.30 1 -4 28 5.20 5.40 1 4 -28 2.20 2.40 -1 4 28 4.00 4.30 1 -4 -28 -0.70 4.00 -1 4 -28 4.30 2.80 1 4 28 2.20 3.40 1 4 28 2.20 5.10 -1 4 -28 2.80 3.40 1 4 28 1.30 2.50 1 4 28 -0.40 4.20 -1 4 -28 6.40 5.40 -1 -4 28 -1.20 5.30 -1 -4 28 -0.50 2.70 -1 4 -28 3.50 4.40 -1 -4 28 0.70 5.60 2 4 -28 71.49 9.30 2 4 -28 46.50 9.00 -2 -4 -28 64.79 10.60 -2 4 28 69.59 6.50 -2 -4 -28 62.69 8.90 -2 4 28 62.39 6.90 2 -4 28 80.69 13.20 -2 -4 -28 53.19 8.70 2 4 -28 71.49 8.10 2 -4 28 69.59 14.10 2 4 -28 50.09 7.30 -2 4 28 81.09 10.20 2 4 28 54.09 9.70 -2 -4 28 60.89 6.40 -2 4 -28 50.99 9.10 2 4 28 59.29 9.50 -2 -4 28 53.69 11.20 -2 4 -28 73.39 7.40 -2 -4 28 53.79 9.00 2 4 28 46.50 8.20 -2 4 -28 81.29 9.20 2 -4 -28 64.69 9.20 2 4 28 68.29 7.60 3 4 -28 24.50 7.20 -3 4 28 37.40 5.90 3 -4 28 38.60 8.10 3 4 -28 41.60 6.40 -3 4 28 23.10 5.40 -3 -4 -28 31.40 8.50 -3 -4 -28 29.40 6.70 -3 -4 -28 31.90 5.80 3 -4 28 46.80 9.20 -3 4 28 45.40 5.00 3 -4 -28 39.60 6.10 3 4 28 29.30 5.20 -3 -4 28 24.90 8.70 3 4 28 35.60 6.50 3 4 28 27.60 7.80 -3 4 -28 50.39 6.60 -3 4 -28 46.90 8.60 -3 4 -28 42.40 6.40 -3 4 -28 49.10 9.10 3 4 28 32.10 7.60 -3 -4 28 30.10 7.60 -4 4 28 16.80 6.60 -4 4 28 15.00 2.80 -4 -4 -28 9.80 7.40 -4 -4 -28 16.90 5.10 4 4 -28 9.10 5.80 4 4 -28 20.30 4.10 4 4 -28 18.90 4.70 4 -4 28 17.20 6.50 4 -4 28 10.70 7.10 -4 4 28 14.50 4.60 -4 -4 -28 10.70 6.20 -4 4 -28 11.00 6.70 4 -4 -28 23.00 4.80 4 4 28 12.80 5.30 -4 4 -28 26.20 5.60 -4 -4 28 18.20 8.10 -4 -4 28 17.20 7.20 4 4 28 3.00 6.10 4 4 28 11.30 6.50 -4 4 -28 16.10 6.20 -4 4 -28 16.30 4.20 -5 4 28 69.89 9.60 5 4 -28 64.79 9.70 -5 4 28 87.79 13.30 -5 -4 -28 86.99 10.10 5 -4 28 68.49 11.00 -5 -4 -28 72.29 13.50 -5 -4 -28 66.59 11.10 5 -4 28 84.69 13.30 -5 4 -28 79.89 8.80 -5 -4 28 57.49 9.80 5 4 28 94.39 13.20 5 4 28 82.49 11.40 -5 4 -28 89.89 11.00 -5 4 -28 58.79 11.40 6 -4 28 25.50 7.60 -6 -4 -28 15.60 9.40 -6 4 28 34.70 8.20 6 -4 28 14.90 8.60 6 4 -28 8.20 5.30 -6 -4 -28 17.30 5.10 6 4 -28 16.80 3.60 -6 -4 -28 18.80 6.20 -6 4 28 6.70 4.90 6 4 -28 24.60 5.50 6 -4 28 19.20 7.40 6 4 28 23.70 7.70 -6 4 -28 17.30 5.10 -6 -4 28 8.80 8.30 -6 4 -28 13.10 4.40 6 4 28 27.20 7.10 -6 -4 28 14.70 7.00 6 4 28 15.20 7.30 -6 4 -28 21.70 6.90 7 -4 28 3.30 6.30 -7 4 28 2.80 4.80 7 -4 28 5.40 6.20 7 4 -28 1.60 5.00 7 4 -28 8.00 3.20 -7 -4 -28 1.60 5.80 -7 -4 -28 5.10 4.20 7 4 -28 4.80 4.40 7 -4 28 7.70 8.40 -7 -4 -28 -8.00 8.30 7 4 28 0.90 5.90 -7 4 -28 5.30 6.40 7 4 28 0.50 5.10 -7 4 -28 7.20 7.90 -7 4 -28 4.80 4.20 -7 4 -28 4.70 4.50 7 4 28 3.10 6.50 -7 -4 28 1.60 7.90 -8 4 28 -6.30 3.10 8 -4 28 -14.10 6.50 -8 -4 -28 -3.90 5.90 8 -4 28 -8.00 5.40 -8 -4 -28 -0.10 4.50 -8 -4 -28 -7.80 9.50 8 -4 28 -1.90 5.30 -8 4 28 -2.70 5.60 -8 4 -28 -2.20 4.00 -8 -4 28 1.60 6.70 -8 4 -28 -6.40 7.70 -8 -4 28 -5.90 10.00 -8 4 -28 -7.40 4.30 8 4 28 -7.40 4.60 -8 4 -28 -1.40 6.10 8 4 28 -3.50 5.00 -9 -4 -28 12.90 5.00 9 -4 28 23.10 8.30 9 -4 28 2.40 8.80 9 4 -28 24.20 7.70 -9 -4 -28 13.30 11.20 -9 -4 -28 6.20 7.40 9 -4 28 16.30 7.50 -9 -4 28 17.20 12.00 -9 4 -28 27.90 7.20 -9 4 -28 13.60 5.40 -9 4 -28 0.50 9.90 9 4 28 14.80 8.30 -9 4 -28 7.90 7.40 -9 -4 28 12.30 8.30 9 4 28 15.00 7.10 -10 -4 -28 -8.80 11.30 -10 -4 -28 14.90 7.60 10 -4 28 6.40 6.90 10 -4 28 8.50 9.10 -10 -4 -28 19.30 6.20 10 -4 28 14.60 11.10 10 4 28 13.70 8.00 -10 4 -28 3.30 6.80 -10 4 -28 15.90 7.50 10 4 28 4.30 7.40 -10 4 -28 2.20 9.20 -10 -4 28 -6.90 8.60 -10 -4 28 1.00 8.60 10 4 28 1.00 13.60 11 -4 28 27.90 8.70 -11 -4 -28 34.20 7.60 -11 -4 -28 2.80 13.90 11 4 28 25.80 12.00 -11 4 -28 18.90 6.00 11 4 28 35.90 10.90 -11 4 -28 31.60 20.80 0 5 -28 95.49 11.40 0 -5 -28 81.19 12.60 0 5 28 79.99 10.40 0 5 -28 62.59 10.70 0 -5 28 101.99 14.90 0 5 28 83.99 9.00 0 5 28 86.99 8.70 0 -5 28 94.69 12.70 0 5 28 86.79 12.70 0 5 -28 100.49 10.30 0 5 -28 83.59 7.90 1 -5 28 6.30 6.10 -1 5 28 6.70 2.40 1 5 -28 3.30 5.20 -1 -5 -28 7.30 6.10 1 5 -28 6.50 3.70 1 5 -28 9.20 4.70 -1 5 28 10.00 3.10 1 5 -28 3.50 2.40 1 -5 -28 5.60 4.60 -1 5 -28 16.30 4.40 1 5 28 13.90 4.90 -1 -5 28 7.10 5.60 1 5 28 6.10 2.60 1 5 28 -1.10 4.80 -1 5 -28 7.70 3.40 1 5 28 5.90 3.70 -1 5 -28 13.60 5.00 -1 5 -28 16.90 7.10 -1 -5 28 9.60 7.90 -2 5 28 89.49 12.40 2 -5 28 91.39 12.80 -2 5 28 80.99 9.30 2 5 -28 62.69 9.80 -2 -5 -28 58.79 10.30 2 -5 28 66.69 10.30 2 5 -28 83.89 9.20 2 5 -28 73.29 6.30 -2 5 28 74.09 6.70 2 5 -28 91.49 10.70 -2 5 -28 88.39 9.80 -2 5 -28 77.19 11.50 2 5 28 82.89 8.20 -2 -5 28 58.89 11.60 -2 -5 28 67.69 10.50 2 5 28 63.59 10.70 2 -5 -28 76.59 10.70 -2 5 -28 74.09 7.80 2 5 28 77.59 9.90 3 5 -28 11.90 6.80 -3 -5 -28 8.00 7.80 3 5 -28 9.10 4.20 3 -5 28 11.10 6.70 -3 5 28 9.70 3.90 3 -5 28 11.60 6.50 3 5 -28 8.90 3.70 -3 5 28 12.20 6.30 -3 -5 -28 10.80 4.80 -3 5 -28 8.70 5.90 -3 -5 28 3.80 5.80 3 -5 -28 1.50 4.00 3 5 28 10.40 5.00 -3 5 -28 16.10 4.70 -3 5 -28 1.30 4.30 -3 -5 28 6.80 8.30 -3 5 -28 11.90 3.50 3 5 28 7.70 6.10 -4 -5 -28 13.00 5.00 -4 5 28 5.50 3.90 4 -5 28 8.50 6.30 4 5 -28 11.50 4.70 -4 -5 -28 9.80 8.20 -4 -5 -28 -4.00 7.30 4 -5 28 12.80 7.70 4 5 -28 3.90 4.70 -4 5 28 9.10 5.90 -4 5 28 8.50 2.60 4 5 -28 9.20 3.80 -4 5 -28 17.20 4.90 -4 -5 28 3.30 8.20 -4 5 -28 2.50 3.30 4 5 28 -0.20 5.50 -4 5 -28 8.60 5.50 -4 5 -28 1.50 5.20 -4 -5 28 3.80 5.60 4 5 28 5.30 4.90 4 5 28 6.90 6.00 -5 -5 -28 5.00 6.40 -5 5 28 4.20 2.20 5 5 -28 5.50 5.60 5 -5 28 8.40 6.50 -5 5 28 8.00 5.90 5 -5 28 -3.60 6.70 5 5 -28 9.30 3.80 5 5 -28 5.40 3.60 -5 -5 -28 0.50 8.50 -5 5 28 3.30 3.80 -5 -5 -28 2.80 4.40 -5 -5 28 3.60 9.20 -5 5 -28 13.80 4.90 -5 5 -28 6.20 5.70 -5 5 -28 6.90 3.60 5 5 28 12.20 7.40 5 5 28 5.20 5.60 -5 5 -28 5.80 5.70 5 5 28 11.10 6.50 6 -5 28 41.60 10.30 6 5 -28 30.70 7.80 -6 5 28 36.90 8.70 6 5 -28 41.10 6.60 -6 -5 -28 26.70 6.30 -6 5 28 21.70 5.80 6 -5 28 40.40 9.10 6 5 -28 36.00 6.30 -6 -5 -28 23.90 7.50 -6 5 -28 33.40 9.20 -6 5 -28 16.00 6.30 -6 -5 28 23.30 10.30 -6 -5 28 26.50 8.50 6 5 28 30.00 7.20 7 5 -28 35.00 7.70 7 -5 28 54.09 10.20 -7 -5 -28 38.40 8.50 7 5 -28 55.89 7.20 -7 5 28 55.89 10.10 -7 5 28 37.20 6.70 7 -5 28 58.69 11.20 -7 -5 -28 15.40 11.10 -7 -5 -28 46.60 7.30 7 -5 28 43.50 10.10 -7 5 -28 44.70 7.20 7 5 28 49.00 10.20 7 5 28 40.40 8.80 -7 5 -28 27.70 6.30 -7 5 -28 47.00 10.10 -7 -5 28 31.00 9.00 -7 5 -28 31.60 8.10 -7 -5 28 32.80 12.30 -8 5 28 52.79 9.50 -8 -5 -28 34.30 9.60 -8 5 28 26.30 5.70 -8 -5 -28 19.30 12.90 8 -5 28 34.90 10.30 -8 -5 -28 34.20 7.20 8 -5 28 44.20 10.20 -8 5 28 22.00 7.20 8 -5 28 46.20 9.50 8 5 -28 44.70 7.10 8 5 28 48.20 10.60 8 5 28 23.80 7.60 -8 5 -28 33.30 9.20 -8 5 -28 30.20 6.10 -8 -5 28 28.30 12.70 -8 5 -28 35.80 7.20 -8 -5 28 14.70 9.20 -8 5 -28 32.90 10.20 -9 5 28 -5.30 6.00 9 5 -28 0.70 6.00 -9 -5 -28 -8.00 4.30 -9 -5 -28 -3.10 9.80 9 -5 28 -2.40 6.30 9 -5 28 -8.00 5.20 -9 5 -28 -3.50 3.80 9 5 28 -13.60 6.30 9 5 28 -2.80 7.30 -9 5 -28 -2.90 6.30 9 5 28 -4.70 4.40 -9 5 -28 -3.40 7.80 -9 -5 28 -6.20 7.30 -9 5 -28 -8.10 4.40 -9 -5 28 3.50 11.30 10 -5 28 59.09 14.90 -10 -5 -28 24.30 13.30 -10 -5 -28 54.49 10.90 10 -5 28 42.90 12.50 -10 5 28 50.19 9.50 10 -5 28 59.09 9.70 -10 -5 -28 45.40 9.30 -10 5 -28 42.90 13.20 -10 5 -28 42.70 7.40 -10 -5 28 24.50 12.70 -10 -5 28 46.20 12.10 -10 5 -28 56.19 12.80 10 5 28 59.99 13.10 0 6 -28 155.08 13.30 0 -6 28 158.18 18.10 0 6 28 142.09 11.20 0 6 28 118.19 12.60 0 -6 -28 104.39 14.40 0 6 28 131.39 9.80 0 6 28 145.99 15.80 0 6 -28 118.99 10.10 0 -6 28 115.49 14.70 1 -6 28 94.99 14.80 -1 6 28 80.09 6.50 -1 6 28 72.99 10.00 1 6 -28 69.29 7.10 -1 -6 -28 60.79 11.10 -1 6 28 80.39 7.00 1 6 -28 51.69 9.70 1 6 -28 93.19 10.80 -1 6 28 78.89 12.60 1 -6 28 70.79 10.40 -1 6 -28 74.69 7.90 -1 6 -28 67.79 10.30 1 6 28 59.69 10.40 -1 -6 28 69.79 12.20 1 -6 -28 64.19 9.70 -1 -6 28 59.99 10.00 -1 6 -28 83.49 11.30 1 6 28 74.89 8.70 1 6 28 60.19 10.30 2 6 -28 71.09 6.30 -2 6 28 84.29 12.90 2 -6 28 54.49 10.10 2 6 -28 63.69 10.20 -2 6 28 77.99 8.80 -2 -6 -28 61.69 11.20 2 -6 28 67.19 10.10 -2 6 -28 67.99 11.10 2 6 28 51.19 9.90 2 6 28 56.49 9.00 -2 6 -28 91.29 11.60 2 -6 -28 70.39 9.50 2 6 28 78.09 9.60 -2 6 -28 65.59 7.80 -2 -6 28 63.89 13.30 -2 -6 28 61.09 12.20 -3 -6 -28 52.39 10.90 -3 6 28 67.79 8.10 3 -6 28 57.49 10.20 3 -6 28 84.09 13.10 3 6 -28 50.79 9.50 3 6 -28 64.59 8.50 -3 6 28 72.29 11.00 3 6 28 44.30 8.70 3 6 28 73.59 9.70 -3 -6 28 35.00 10.90 -3 6 -28 76.79 10.00 -3 6 -28 38.60 8.80 -3 6 -28 79.49 12.60 -3 6 -28 50.99 7.30 3 6 28 56.19 9.80 -3 -6 28 50.79 10.00 4 6 -28 1.50 3.50 -4 -6 -28 -6.20 5.40 -4 -6 -28 -11.50 7.20 4 -6 28 -0.10 5.90 -4 6 28 2.30 2.70 4 6 -28 -2.40 3.40 4 -6 28 -1.80 6.60 4 6 -28 -1.30 4.50 -4 6 28 -3.20 5.10 -4 6 -28 0.60 3.10 4 6 28 2.40 4.50 -4 6 -28 -1.10 5.30 -4 -6 28 -3.10 8.60 -4 6 -28 -4.50 3.30 4 6 28 -1.90 5.90 4 6 28 -2.80 5.60 -5 -6 -28 91.09 11.80 -5 6 28 117.79 13.90 -5 6 28 81.59 9.60 -5 -6 -28 71.79 14.70 -5 -6 -28 73.49 10.20 5 6 -28 84.89 13.00 5 -6 28 98.59 14.70 -5 6 -28 102.99 15.40 -5 6 -28 110.39 10.00 -5 6 -28 100.79 11.60 -5 -6 28 72.09 11.60 5 6 28 93.59 12.10 -5 -6 28 72.19 14.80 5 6 28 53.49 15.70 -5 6 -28 68.49 11.10 5 6 28 90.39 14.50 -6 6 28 7.70 2.60 -6 -6 -28 -0.60 10.10 6 -6 28 -2.30 6.00 -6 6 28 3.00 4.10 6 -6 28 8.40 8.10 -6 -6 -28 -10.20 6.60 6 6 -28 2.70 3.90 6 6 -28 4.10 6.30 -6 6 28 5.20 5.80 -6 -6 -28 1.70 4.70 -6 6 28 -1.80 4.20 6 6 -28 7.20 3.80 6 6 28 10.20 5.70 -6 -6 28 -9.10 9.40 -6 6 -28 -3.00 3.10 -6 6 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-6 28 -0.80 6.50 -9 6 28 5.60 6.00 -9 6 -28 -4.30 5.80 -9 -6 28 12.70 13.20 9 6 28 12.50 9.00 -9 -6 28 -6.70 8.00 -9 6 -28 6.60 5.00 -9 6 -28 4.80 9.30 -9 6 -28 6.90 5.10 9 6 28 15.20 7.30 9 6 28 24.00 10.30 10 6 -28 24.10 7.10 -10 -6 -28 26.00 8.10 10 -6 28 24.80 11.80 10 -6 28 9.50 7.00 10 -6 28 13.80 7.20 -10 -6 -28 22.50 9.20 -10 -6 -28 7.70 13.70 -10 6 28 6.40 6.20 10 6 28 11.30 7.20 -10 6 -28 13.90 7.50 -10 6 -28 21.60 6.70 -10 6 -28 -1.80 7.00 -10 6 -28 36.40 21.60 10 6 28 15.40 11.40 -10 -6 28 5.00 13.00 10 6 28 12.50 9.50 -10 -6 28 -3.40 9.30 0 -7 28 83.19 11.50 0 -7 28 50.69 11.20 0 7 -28 63.29 10.30 0 7 28 74.09 7.10 0 7 -28 57.29 7.00 0 -7 -28 44.20 9.50 0 7 -28 65.89 9.60 0 7 28 66.69 6.10 0 7 28 66.59 11.10 1 -7 28 -3.70 5.60 -1 7 28 -4.10 4.70 1 -7 28 -3.70 6.30 -1 7 28 4.20 3.70 1 7 -28 2.00 3.90 1 7 -28 5.30 4.20 -1 -7 -28 -5.00 6.70 1 7 -28 2.20 2.30 1 7 -28 2.80 6.00 1 7 28 3.00 3.20 -1 7 -28 2.20 5.30 1 7 28 4.00 4.50 1 7 28 -1.00 5.00 -1 7 -28 1.40 4.00 -1 -7 28 -2.20 7.80 -1 -7 28 8.20 6.00 1 -7 -28 1.10 6.40 -2 7 28 33.00 5.50 -2 7 28 33.40 8.40 -2 -7 -28 18.10 8.30 2 -7 28 43.30 9.50 2 7 -28 19.30 9.40 2 7 -28 41.30 7.10 2 7 -28 31.70 4.00 2 7 -28 26.40 6.30 2 -7 28 50.99 9.30 -2 -7 28 37.20 10.40 -2 7 -28 28.70 5.30 2 7 28 34.90 8.40 -2 7 -28 35.00 8.10 -2 7 -28 33.80 6.70 2 7 28 20.50 6.50 -2 7 -28 39.90 8.10 -2 -7 28 41.10 8.30 2 7 28 32.20 5.90 -3 7 28 14.70 3.90 3 7 -28 26.90 5.50 3 7 -28 6.70 6.00 3 7 -28 28.40 6.50 -3 -7 -28 -0.40 8.00 3 -7 28 11.50 7.20 3 -7 28 16.60 7.80 -3 7 28 28.60 7.80 -3 7 -28 13.30 4.20 3 7 28 13.80 6.00 -3 -7 28 10.40 6.80 -3 7 -28 19.90 7.50 -3 7 -28 13.50 5.70 3 7 28 6.00 5.00 -3 7 -28 20.50 5.90 3 7 28 17.90 6.20 -3 -7 28 15.80 9.90 -4 -7 -28 2.70 5.30 -4 -7 -28 8.00 9.30 -4 7 28 8.40 3.70 4 -7 28 6.90 6.90 -4 7 28 5.20 3.20 -4 7 28 12.50 5.00 4 7 -28 12.80 5.70 -4 7 28 7.70 5.80 4 -7 28 3.70 6.80 -4 7 -28 18.80 7.80 -4 7 -28 15.80 4.70 4 7 28 15.90 7.70 -4 7 -28 16.50 4.90 4 7 28 -0.90 5.80 4 7 28 15.80 5.30 -4 7 -28 15.10 7.20 -4 -7 28 4.20 7.10 -4 -7 28 -1.40 9.60 5 7 -28 0.70 3.80 -5 7 28 -6.40 4.80 5 -7 28 3.20 6.40 -5 7 28 -2.70 2.50 5 -7 28 1.70 6.50 -5 7 28 -2.50 3.90 5 7 -28 1.50 3.40 5 7 28 -10.70 5.30 -5 -7 28 -11.40 5.80 -5 7 -28 -2.80 5.50 -5 7 -28 -3.10 3.60 -5 -7 28 14.20 10.50 5 7 28 -1.20 3.90 -5 7 -28 -6.90 5.10 -5 7 -28 1.30 4.20 -6 7 28 44.00 8.80 6 -7 28 43.40 10.50 -6 7 28 22.60 6.40 6 7 -28 21.70 7.50 6 7 -28 45.60 7.70 6 7 -28 40.10 6.60 -6 7 28 41.40 5.60 6 -7 28 37.70 9.70 -6 -7 -28 32.80 6.90 -6 -7 -28 19.70 7.90 -6 -7 28 38.00 13.90 6 7 28 28.10 8.00 -6 7 -28 23.50 8.00 -6 7 -28 28.70 5.90 6 7 28 39.70 8.30 -6 7 -28 42.70 9.80 -6 7 -28 42.30 7.10 -6 -7 28 17.50 8.50 7 7 -28 6.20 6.70 -7 7 28 15.60 5.40 -7 -7 -28 17.50 6.00 7 7 -28 22.90 5.70 -7 -7 -28 5.80 10.50 7 7 -28 16.90 5.30 -7 7 28 9.30 6.00 7 -7 28 11.40 8.60 7 -7 28 13.30 7.70 7 7 28 6.40 7.20 -7 7 -28 8.30 7.50 -7 -7 28 16.20 8.40 -7 7 -28 18.00 5.30 -7 7 -28 17.10 5.90 -7 7 -28 18.30 8.60 7 7 28 3.70 5.50 7 7 28 18.30 9.40 -7 -7 28 3.20 12.80 -8 7 28 32.20 8.30 -8 -7 -28 30.30 7.10 8 -7 28 27.00 11.00 8 7 -28 30.80 6.30 -8 7 28 24.10 6.10 -8 -7 -28 18.40 12.60 8 -7 28 37.70 10.40 -8 -7 -28 24.20 11.30 8 -7 28 31.90 8.20 8 7 -28 28.30 8.70 8 7 -28 26.50 8.20 -8 7 -28 42.10 11.80 8 7 28 30.90 8.30 -8 7 -28 26.60 8.50 -8 -7 28 11.30 13.50 8 7 28 39.10 10.60 8 7 28 29.60 10.30 -8 7 -28 37.40 7.30 -8 7 -28 29.50 6.40 -8 -7 28 16.10 10.10 9 -7 28 -1.40 5.50 9 7 -28 -2.90 5.40 9 7 -28 -3.00 4.80 -9 -7 -28 -8.50 7.60 9 -7 28 -19.80 9.00 -9 -7 -28 -14.30 10.60 9 -7 28 3.40 8.60 -9 -7 -28 -4.50 4.80 9 7 -28 -13.60 6.10 -9 7 28 -10.50 4.40 -9 7 -28 0.40 4.40 9 7 28 -3.50 7.20 -9 -7 28 -4.40 9.00 9 7 28 4.00 8.10 -9 7 -28 -2.10 4.80 -9 7 -28 -7.70 7.40 -9 -7 28 -7.20 12.40 -10 7 28 15.20 7.30 10 -7 28 10.00 7.20 10 7 28 31.00 12.40 -10 7 -28 23.00 9.20 -10 7 -28 14.80 6.90 -10 7 -28 2.20 9.50 0 8 28 22.70 7.50 0 8 28 14.50 2.60 0 8 -28 14.50 5.20 0 -8 28 18.30 7.60 0 8 -28 12.10 5.00 0 8 28 14.30 5.20 0 8 28 18.30 3.20 0 -8 28 2.30 8.50 0 8 -28 11.90 6.60 -1 -8 -28 -16.60 14.70 1 -8 28 14.30 7.80 1 8 -28 26.90 6.20 1 8 -28 18.70 3.90 1 8 -28 12.20 6.10 -1 8 28 16.60 7.60 1 -8 28 7.50 8.20 -1 8 28 11.70 4.70 1 8 -28 20.60 6.30 -1 -8 28 14.50 9.70 -1 8 -28 24.90 6.70 -1 8 -28 22.80 7.50 -1 8 -28 19.70 4.10 1 8 28 7.30 5.70 1 8 28 14.60 3.70 1 8 28 16.60 7.40 -1 -8 28 16.30 6.90 -1 8 -28 23.40 6.10 -2 -8 -28 -11.30 7.10 2 8 -28 4.20 4.30 2 -8 28 7.30 6.20 2 -8 28 -0.30 7.10 -2 8 28 7.60 5.40 2 8 -28 -2.20 2.20 2 8 -28 -0.60 4.20 2 8 -28 0.50 4.90 -2 -8 28 1.70 9.10 -2 8 -28 -0.20 3.00 -2 8 -28 -0.80 5.20 -2 8 -28 1.50 6.30 2 8 28 -4.70 5.50 2 8 28 -8.10 4.20 -2 8 -28 5.20 4.40 2 8 28 -1.70 3.00 -2 -8 28 -0.60 6.40 -3 8 28 197.98 14.40 -3 8 28 161.28 14.10 3 8 -28 216.98 17.20 3 -8 28 187.38 21.10 -3 8 28 212.98 19.20 -3 8 28 189.78 18.50 3 -8 28 172.38 18.40 -3 -8 -28 141.09 20.70 3 8 -28 185.58 12.70 -3 -8 28 196.58 18.40 -3 8 -28 189.88 15.30 -3 8 -28 153.08 19.90 -3 8 -28 211.78 19.10 -3 -8 28 161.98 22.30 3 8 28 181.88 19.30 3 8 28 209.48 22.40 4 -8 28 27.80 9.00 4 8 -28 38.90 8.20 -4 8 28 30.40 6.90 -4 8 28 37.90 7.90 -4 -8 -28 11.10 9.60 4 8 -28 35.40 7.10 4 -8 28 23.40 7.90 -4 8 28 24.30 4.70 4 8 -28 43.00 7.20 -4 8 -28 39.50 5.90 -4 -8 28 20.70 10.40 -4 8 -28 37.70 9.10 4 8 28 22.80 7.60 -4 -8 28 20.50 7.70 -4 8 -28 14.10 7.10 5 -8 28 42.10 10.80 5 8 -28 39.10 7.30 -5 8 28 32.60 6.00 5 8 -28 32.00 8.70 -5 8 28 38.70 7.30 5 8 -28 48.90 8.70 -5 8 28 55.19 10.10 5 -8 28 54.59 11.40 -5 -8 -28 18.60 13.30 -5 -8 28 32.10 9.40 5 8 28 43.80 10.00 -5 8 -28 30.00 8.50 -5 8 -28 46.60 7.80 -5 -8 28 17.90 13.30 -5 8 -28 25.00 8.80 6 -8 28 1.20 7.70 -6 -8 -28 -5.40 6.30 -6 8 28 8.50 3.20 6 8 -28 -0.90 6.90 6 8 -28 10.80 5.90 -6 8 28 -4.00 5.30 6 -8 28 2.40 7.70 -6 8 28 2.70 4.40 6 8 -28 3.10 4.90 -6 -8 28 -8.60 10.90 -6 8 -28 4.60 4.30 -6 8 -28 -3.00 5.50 6 8 28 9.80 5.80 6 8 28 6.80 8.30 -6 -8 28 4.60 7.80 -6 8 -28 11.40 5.10 -6 8 -28 -3.10 5.80 6 8 28 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3 36 1.90 3.90 -1 3 36 1.20 5.70 -1 3 36 0.00 8.40 1 3 -36 4.80 7.00 1 3 36 -2.00 7.10 -1 3 -36 10.90 7.40 1 3 36 3.30 4.60 -1 -3 36 5.20 5.90 1 3 36 5.50 6.90 -1 -3 36 4.50 7.00 -1 3 -36 4.30 4.90 2 -3 36 -0.50 7.70 -2 3 36 1.30 3.80 -2 3 36 -8.70 7.90 2 3 -36 -5.50 6.40 -2 -3 36 -2.50 5.80 2 3 36 -10.50 5.30 2 3 36 -0.30 6.70 -2 -3 36 2.60 6.50 -2 3 -36 1.50 4.60 -2 3 -36 2.20 6.20 -3 3 36 5.10 7.70 3 -3 36 15.40 7.20 3 -3 36 5.40 7.80 -3 3 36 6.20 6.00 3 -3 36 6.40 8.20 -3 3 -36 17.70 7.70 3 3 36 17.20 8.60 3 3 36 4.20 6.60 3 3 36 14.50 6.30 -3 3 -36 7.20 5.60 -3 -3 36 -1.70 6.50 -3 -3 36 7.60 7.00 -3 3 -36 18.10 5.80 4 -3 36 3.20 6.70 4 -3 36 -1.80 11.30 -4 3 36 0.20 7.90 4 -3 36 -14.00 6.90 -4 -3 -36 -5.90 4.80 -4 -3 36 -7.90 6.60 -4 3 -36 -0.30 4.80 4 3 36 -3.00 5.10 4 3 36 -9.30 6.50 -4 3 -36 -4.80 4.60 -4 3 -36 -7.20 7.20 4 3 36 -7.00 6.10 -5 -3 -36 -8.00 11.10 0 4 -36 65.39 11.40 0 -4 36 54.49 11.50 0 4 -36 83.99 10.80 0 4 -36 61.49 12.30 0 4 36 77.59 10.30 0 4 36 83.79 13.60 1 -4 36 -1.60 8.70 1 4 -36 -5.90 5.40 -1 4 36 -0.70 6.40 1 4 -36 -5.90 6.20 1 -4 36 -3.10 7.30 1 4 -36 -8.20 4.30 -1 4 36 -1.70 3.30 1 4 36 -3.30 6.30 -1 -4 36 -2.40 6.70 1 4 36 0.20 3.90 -1 4 -36 -6.90 5.70 -1 -4 36 -11.00 6.00 -1 4 -36 -11.90 5.20 2 4 -36 20.20 8.50 2 4 -36 30.50 8.90 -2 4 36 32.00 9.70 -2 4 36 31.80 7.90 2 -4 36 29.00 9.20 2 -4 36 39.80 9.80 -2 -4 36 30.60 9.20 2 4 36 14.80 8.10 -2 4 -36 22.70 6.40 2 4 36 33.30 7.10 2 4 36 27.30 9.20 -2 4 -36 53.19 10.40 -2 4 -36 42.40 7.10 -2 -4 36 34.90 9.70 3 -4 36 25.70 9.00 -3 4 36 25.70 9.80 3 4 -36 18.80 9.70 -3 4 36 13.60 7.10 3 4 36 19.50 8.90 -3 -4 36 20.00 8.70 -3 -4 36 11.30 8.50 -3 4 -36 29.00 9.60 3 4 36 20.40 6.70 3 4 36 11.60 8.10 -3 4 -36 23.60 6.30 -3 4 -36 13.90 7.90 -4 4 36 -9.90 5.90 4 -4 36 -7.80 6.70 -4 4 -36 -9.00 5.70 -4 4 -36 -6.90 4.50 4 4 36 -11.40 6.40 0 5 36 30.80 8.20 0 5 36 44.50 10.30 0 5 -36 45.60 10.60 0 5 36 56.99 8.50 0 -5 36 42.60 10.80 0 -5 36 70.29 12.40 1 5 -36 5.00 6.10 1 5 -36 9.30 6.80 -1 5 36 8.20 6.90 -1 5 36 -3.40 6.30 1 5 -36 1.10 4.30 1 -5 36 4.10 7.60 1 -5 36 5.00 7.70 -1 5 -36 9.40 5.00 1 5 36 3.30 8.00 1 5 36 2.30 4.10 -1 5 -36 6.90 6.80 -1 -5 36 -2.30 6.70 -1 -5 36 -5.80 7.40 2 5 -36 -8.80 5.40 -2 5 36 -5.10 6.50 2 -5 36 -1.40 6.80 2 5 -36 -7.10 4.20 2 5 -36 -2.80 5.60 2 5 36 -5.20 3.60 -2 5 -36 -9.20 4.50 -2 -5 36 -5.70 7.00 -2 -5 36 -4.40 7.20 2 5 36 -12.60 5.50 -2 5 -36 2.40 4.60 -2 5 -36 -6.90 6.20 2 5 36 -12.90 5.60 -2 5 -36 -5.90 6.20 3 -5 36 3.00 7.10 3 5 -36 -6.10 6.30 -3 5 36 5.30 6.90 3 5 -36 0.90 6.60 -3 5 -36 1.60 4.90 -3 5 -36 -4.70 5.90 -3 5 -36 -3.30 5.00 3 5 36 -1.30 4.20 -3 5 -36 3.00 7.00 -3 -5 36 -4.40 8.00 3 5 36 -0.10 6.40 0 6 36 24.80 4.80 0 6 36 20.20 7.90 0 6 -36 24.30 8.30 0 6 36 31.50 10.20 0 6 -36 42.30 7.70 0 -6 36 31.50 10.30 1 -6 36 -6.00 7.20 -1 6 36 5.20 7.00 1 6 -36 -1.80 4.20 1 6 -36 -3.10 5.60 1 -6 36 -0.20 8.20 -1 6 36 -6.60 2.90 -1 6 36 -4.00 6.40 -1 -6 36 -5.70 8.20 1 6 36 -1.90 3.30 1 6 36 -6.10 5.90 -1 6 -36 -8.70 6.20 -1 6 -36 -3.70 4.60 -1 6 -36 -1.60 6.40 1 6 36 4.20 7.30 2 6 -36 19.50 8.60 -2 6 -36 23.40 9.90 -2 6 -36 27.40 8.70 0 0 37 10.40 8.90 0 0 37 -5.00 4.90 -1 0 -37 19.60 12.10 -1 0 37 37.80 11.20 -1 0 37 34.90 7.60 -1 0 37 39.90 9.70 1 0 37 35.40 8.00 1 0 37 28.20 8.60 1 0 37 52.89 12.20 -2 0 37 -1.60 6.60 2 0 37 -5.80 6.80 2 0 37 2.80 6.10 -2 0 -37 -8.10 9.10 -2 0 -37 -6.50 5.40 2 0 37 -1.60 6.70 -3 0 37 -4.40 4.10 3 0 37 -2.50 5.80 -3 0 -37 1.70 5.30 -3 0 37 -11.10 6.30 3 0 37 -2.80 6.50 -3 0 -37 5.80 8.70 3 0 37 -1.10 7.40 0 1 -37 0.30 11.50 0 -1 37 -7.10 5.50 0 -1 37 -1.10 5.60 0 1 37 2.10 4.70 0 1 37 -1.00 7.50 0 1 37 -7.60 5.70 -1 1 37 6.40 6.60 1 -1 37 3.60 6.10 1 -1 37 10.10 9.10 -1 1 37 11.20 5.10 -1 1 37 6.00 8.80 1 -1 37 10.30 7.60 1 1 37 7.70 7.00 1 1 37 14.60 8.10 -1 -1 37 6.10 6.00 -1 1 -37 6.70 8.90 1 1 37 9.90 6.00 -2 1 37 -4.10 3.80 -2 1 37 -6.30 7.30 2 -1 37 4.30 8.00 2 -1 37 -8.00 6.50 -2 1 37 -10.10 5.30 -2 1 -37 -5.50 6.00 2 1 37 -1.20 6.70 -2 -1 37 -6.50 4.40 2 1 37 -4.80 4.80 -2 1 -37 -3.00 7.60 3 -1 37 9.80 6.70 3 -1 37 -4.60 6.20 -3 1 37 -2.40 3.90 -3 1 37 -6.40 7.00 -3 -1 -37 -7.90 4.80 -3 -1 -37 -12.60 8.80 -3 1 -37 -2.70 8.00 -3 -1 37 -5.40 4.30 3 1 37 -0.40 6.80 -3 1 -37 -9.00 4.90 -3 1 -37 -6.10 5.00 0 2 -37 8.00 8.20 0 -2 37 6.40 6.20 0 2 37 -6.60 6.80 0 -2 37 0.70 6.80 0 2 37 -4.20 6.10 0 2 37 -2.80 3.60 -1 2 37 24.50 7.30 -1 2 37 19.30 5.50 1 -2 37 20.40 8.70 -1 2 37 20.80 8.40 1 2 37 25.30 9.70 -1 2 -37 20.90 7.20 -1 2 -37 27.80 9.00 1 2 37 24.60 6.40 -1 -2 37 5.80 7.30 -1 -2 37 16.30 7.40 2 -2 37 34.50 9.40 -2 2 37 17.00 9.30 -2 2 37 21.30 7.70 -2 2 37 22.50 5.30 2 -2 37 26.90 9.30 2 -2 37 21.50 10.10 -2 -2 37 16.20 7.50 -2 -2 37 36.00 8.80 -2 2 -37 12.70 6.00 2 2 37 10.80 7.00 2 2 37 41.80 10.80 2 2 37 21.50 6.60 -2 2 -37 13.00 8.90 -3 2 -37 -6.60 8.20 0 3 37 -4.30 6.70 0 3 -37 -5.40 7.20 0 3 -37 -9.10 7.20 0 3 37 -2.20 6.30 0 -3 37 -7.10 6.40 0 3 37 0.60 3.90 1 3 -37 3.80 8.00 -1 3 37 7.00 4.20 -1 3 37 -4.50 5.90 1 -3 37 2.80 7.00 1 -3 37 7.70 6.70 -1 3 37 9.70 8.00 -1 -3 37 -1.40 7.10 -1 3 -37 3.00 8.30 -1 3 -37 3.00 4.90 1 3 37 -4.80 6.30 1 3 37 7.60 4.60 1 3 37 -2.40 6.20 -2 3 37 -2.80 7.50 -2 3 37 -5.50 3.30 2 -3 37 -4.70 6.00 -2 3 -37 -3.60 4.50 -2 3 -37 -16.30 13.60 2 3 37 9.70 5.90 -2 -3 37 -5.00 7.50 2 3 37 -9.30 6.50 0 4 -37 -5.40 9.50 0 4 -37 -5.00 6.20 0 4 37 -0.20 3.90 0 4 -37 -0.10 5.40 0 4 37 7.50 8.00 0 -4 37 0.10 6.80 -1 4 37 25.30 8.90 1 4 -37 19.00 7.90 1 -4 37 6.10 7.70 -1 4 -37 12.90 10.10 -1 4 -37 -2.50 8.50 1 4 37 15.60 8.70 -1 -4 37 8.90 8.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 14539 _shelx_res_file ; TITL yj_a.res in P2(1) New:Pna21 yj.res created by SHELXL-2018/3 at 16:13:14 on 13-Feb-2024 CELL 0.71073 30.247 13.713 17.205 90 90 90 ZERR 4 0.004 0.002 0.002 0 0 0 LATT -1 SYMM -X,-Y,0.5+Z SYMM 0.5-X,0.5+Y,0.5+Z SYMM 0.5+X,0.5-Y,+Z SFAC C H Cl Mn N O UNIT 340 248 8 4 56 16 L.S. 40 PLAN 2 TEMP -172 CONF BOND $H MORE -1 fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 OMIT 0 1 -1 OMIT 1 8 -6 OMIT 1 8 6 OMIT 5 8 -5 REM REM REM WGHT 0.107900 24.164499 BASF 0.40984 FVAR 0.34662 MN1 4 0.455248 0.066144 0.178769 11.00000 0.03946 0.02226 = 0.02266 0.00080 -0.00001 -0.00164 N1 5 0.434794 -0.079286 0.205350 11.00000 0.04086 0.01663 = 0.02119 -0.00199 -0.00207 -0.00308 N2 5 0.429781 0.106595 0.290340 11.00000 0.04264 0.02140 = 0.01976 0.00058 0.00271 -0.00259 N3 5 0.439295 0.212323 0.145159 11.00000 0.04394 0.02206 = 0.02081 0.00140 -0.00298 0.00128 N4 5 0.442878 0.027079 0.059497 11.00000 0.03932 0.02154 = 0.02046 0.00055 -0.00132 0.00003 C4 1 0.436011 -0.157279 0.155346 11.00000 0.04079 0.01144 = 0.02305 0.00030 -0.00052 -0.00024 C1 1 0.429268 -0.114667 0.279456 11.00000 0.03538 0.02101 = 0.02460 0.00250 0.00062 -0.00405 C19 1 0.424335 0.042645 0.351485 11.00000 0.03440 0.02194 = 0.02007 -0.00175 -0.00091 0.00084 C16 1 0.426774 0.199793 0.319264 11.00000 0.04534 0.02181 = 0.02271 0.00620 0.00070 0.00368 C14 1 0.434736 0.291341 0.194154 11.00000 0.04183 0.02288 = 0.02509 -0.00211 -0.00215 -0.00065 C11 1 0.439498 0.248900 0.069874 11.00000 0.03879 0.02162 = 0.02565 0.00459 -0.00119 -0.00017 C9 1 0.440926 0.089958 -0.003039 11.00000 0.03419 0.02818 = 0.02123 0.00213 0.00110 0.00009 C6 1 0.442378 -0.065494 0.030035 11.00000 0.04131 0.02759 = 0.01864 -0.00256 -0.00340 -0.00302 C3 1 0.432274 -0.247736 0.200425 11.00000 0.04776 0.01556 = 0.02522 0.00391 0.00157 -0.00513 AFIX 43 H3 2 0.432566 -0.312405 0.180631 11.00000 -1.20000 AFIX 0 C2 1 0.428301 -0.220633 0.276270 11.00000 0.04541 0.02445 = 0.02555 0.00442 0.00154 -0.00209 AFIX 43 H2 2 0.425412 -0.263366 0.319432 11.00000 -1.20000 AFIX 0 C18 1 0.418091 0.099144 0.422098 11.00000 0.05663 0.02646 = 0.01859 0.00109 0.00332 -0.00048 AFIX 43 H18 2 0.413455 0.073443 0.472722 11.00000 -1.20000 AFIX 0 C17 1 0.420034 0.194491 0.403130 11.00000 0.05540 0.02144 = 0.01937 -0.00509 -0.00235 0.00285 AFIX 43 H17 2 0.417493 0.248084 0.437833 11.00000 -1.20000 AFIX 0 C13 1 0.433979 0.379872 0.147906 11.00000 0.04393 0.02833 = 0.03082 0.00021 -0.00412 -0.00505 AFIX 43 H13 2 0.431639 0.444585 0.167184 11.00000 -1.20000 AFIX 0 C12 1 0.437211 0.353462 0.072396 11.00000 0.04938 0.01764 = 0.03362 0.00198 -0.00343 -0.00340 AFIX 43 H12 2 0.437852 0.396232 0.028974 11.00000 -1.20000 AFIX 0 C8 1 0.440356 0.033737 -0.074767 11.00000 0.04961 0.03100 = 0.02237 0.00353 0.00015 0.00260 AFIX 43 H8 2 0.439129 0.059094 -0.126106 11.00000 -1.20000 AFIX 0 C7 1 0.441917 -0.062146 -0.054303 11.00000 0.04757 0.02973 = 0.02380 -0.00418 0.00071 -0.00137 AFIX 43 H7 2 0.442578 -0.116402 -0.088618 11.00000 -1.20000 AFIX 0 C5 1 0.439142 -0.152327 0.074166 11.00000 0.03642 0.02694 = 0.02251 0.00003 -0.00087 -0.00376 C20 1 0.423831 -0.058209 0.347011 11.00000 0.03372 0.03120 = 0.01883 0.00219 -0.00072 -0.00169 C15 1 0.428696 0.285213 0.275052 11.00000 0.03931 0.02313 = 0.02372 0.00100 -0.00285 0.00351 C10 1 0.438970 0.191478 0.001104 11.00000 0.03752 0.02380 = 0.02404 0.00774 -0.00220 -0.00146 C38 1 0.431673 0.245017 -0.074157 11.00000 0.05295 0.02391 = 0.02144 0.00566 0.00029 -0.00341 C43 1 0.390151 0.287415 -0.089579 11.00000 0.04834 0.02747 = 0.02810 0.00266 0.00085 -0.00121 C42 1 0.382280 0.334791 -0.159895 11.00000 0.05311 0.03704 = 0.03169 0.01168 -0.00227 0.00192 AFIX 43 H42 2 0.354400 0.363857 -0.170375 11.00000 -1.20000 AFIX 0 C41 1 0.416180 0.338495 -0.214296 11.00000 0.06836 0.03666 = 0.02451 0.00354 0.00029 -0.00253 AFIX 43 H41 2 0.411037 0.370699 -0.262340 11.00000 -1.20000 AFIX 0 C40 1 0.456840 0.297269 -0.201078 11.00000 0.05638 0.03551 = 0.03205 0.00642 0.00619 -0.00101 AFIX 43 H40 2 0.479286 0.299728 -0.239652 11.00000 -1.20000 AFIX 0 C39 1 0.464530 0.251790 -0.130032 11.00000 0.04478 0.02857 = 0.03757 0.00434 0.00451 0.00046 AFIX 43 H39 2 0.492859 0.224862 -0.119639 11.00000 -1.20000 AFIX 0 C26 1 0.436249 -0.245483 0.028953 11.00000 0.04183 0.02763 = 0.02010 -0.00264 0.00206 -0.00169 C31 1 0.397905 -0.268983 -0.013310 11.00000 0.04960 0.02494 = 0.02538 -0.00214 -0.00465 -0.00273 C30 1 0.395632 -0.354063 -0.057331 11.00000 0.05861 0.03030 = 0.02724 -0.00873 -0.00398 -0.00304 AFIX 43 H30 2 0.369625 -0.368807 -0.085973 11.00000 -1.20000 AFIX 0 C29 1 0.431085 -0.416598 -0.059231 11.00000 0.06458 0.02650 = 0.03174 -0.00535 0.00166 -0.00109 AFIX 43 H29 2 0.429615 -0.474211 -0.089785 11.00000 -1.20000 AFIX 0 C28 1 0.469285 -0.396186 -0.016607 11.00000 0.06989 0.02557 = 0.03335 -0.00269 0.00459 0.00519 AFIX 43 H28 2 0.493690 -0.439754 -0.018096 11.00000 -1.20000 AFIX 0 C27 1 0.471406 -0.311907 0.027940 11.00000 0.04685 0.02601 = 0.02969 0.00036 -0.00065 -0.00067 AFIX 43 H27 2 0.497053 -0.299127 0.058142 11.00000 -1.20000 AFIX 0 C62 1 0.413333 -0.114341 0.419445 11.00000 0.04433 0.02352 = 0.01900 0.00113 0.00016 0.00232 C67 1 0.372515 -0.161343 0.426863 11.00000 0.04173 0.03130 = 0.02241 0.00760 0.00308 -0.00079 C66 1 0.363020 -0.217885 0.494811 11.00000 0.05338 0.03718 = 0.03174 0.01096 0.00552 -0.00304 AFIX 43 H66 2 0.335455 -0.250347 0.500374 11.00000 -1.20000 AFIX 0 C65 1 0.394990 -0.224111 0.552231 11.00000 0.06812 0.03166 = 0.02072 0.00446 0.00333 -0.00108 AFIX 43 H65 2 0.389080 -0.261811 0.597376 11.00000 -1.20000 AFIX 0 C64 1 0.435523 -0.176752 0.545730 11.00000 0.06143 0.03594 = 0.02052 0.00294 0.00012 0.00837 AFIX 43 H64 2 0.457141 -0.182661 0.585507 11.00000 -1.20000 AFIX 0 C63 1 0.443870 -0.120355 0.479678 11.00000 0.04180 0.03405 = 0.02450 0.00106 -0.00273 -0.00407 AFIX 43 H63 2 0.470918 -0.085468 0.475856 11.00000 -1.20000 AFIX 0 C50 1 0.421588 0.379254 0.317382 11.00000 0.04827 0.01497 = 0.02809 -0.00021 -0.00075 0.00034 C55 1 0.380584 0.401984 0.351720 11.00000 0.04639 0.02071 = 0.03247 -0.00007 0.00092 -0.00341 C54 1 0.374928 0.488112 0.392440 11.00000 0.05910 0.02230 = 0.03719 -0.00286 0.01004 0.00400 AFIX 43 H54 2 0.347039 0.502786 0.414984 11.00000 -1.20000 AFIX 0 C53 1 0.410064 0.553713 0.400591 11.00000 0.06958 0.02128 = 0.03798 -0.00784 0.00847 -0.00520 AFIX 43 H53 2 0.406239 0.612243 0.429356 11.00000 -1.20000 AFIX 0 C52 1 0.450748 0.532672 0.366233 11.00000 0.06091 0.02516 = 0.03605 -0.00050 -0.00230 -0.00169 AFIX 43 H52 2 0.474763 0.576813 0.371583 11.00000 -1.20000 AFIX 0 C51 1 0.456004 0.447396 0.324381 11.00000 0.04989 0.01940 = 0.03368 -0.00027 0.00050 -0.00052 AFIX 43 H51 2 0.483525 0.434614 0.299801 11.00000 -1.20000 AFIX 0 C21 1 0.550026 -0.032379 0.189648 11.00000 0.06011 0.03851 = 0.05004 -0.00472 -0.00885 0.01698 AFIX 43 H21 2 0.539801 -0.088773 0.163089 11.00000 -1.20000 AFIX 0 C22 1 0.591089 -0.020832 0.218803 11.00000 0.06525 0.05540 = 0.04310 -0.01458 -0.00721 0.01814 C23 1 0.628233 -0.093875 0.228988 11.00000 0.06385 0.11721 = 0.11536 -0.02479 -0.01255 0.02420 AFIX 137 H23A 2 0.654723 -0.070274 0.202121 11.00000 -1.50000 H23B 2 0.619323 -0.156791 0.206977 11.00000 -1.50000 H23C 2 0.634676 -0.101800 0.284452 11.00000 -1.50000 AFIX 0 C24 1 0.551600 0.112217 0.242452 11.00000 0.04642 0.03272 = 0.02482 0.00556 0.00126 0.00042 C25 1 0.540319 0.210452 0.270539 11.00000 0.05440 0.03306 = 0.04407 0.00691 -0.01455 -0.00373 AFIX 137 H25A 2 0.565198 0.236989 0.300271 11.00000 -1.50000 H25B 2 0.514134 0.206798 0.303958 11.00000 -1.50000 H25C 2 0.534110 0.253002 0.226096 11.00000 -1.50000 AFIX 0 C44 1 0.320546 0.333544 -0.021953 11.00000 0.04846 0.04636 = 0.03225 0.00835 -0.00254 0.00560 C45 1 0.296703 0.318316 0.053816 11.00000 0.04471 0.03858 = 0.03087 0.00349 -0.00317 -0.00040 C49 1 0.319955 0.297830 0.121422 11.00000 0.05012 0.04248 = 0.03394 0.00529 -0.00003 -0.00356 AFIX 43 H49 2 0.351180 0.291514 0.118252 11.00000 -1.20000 AFIX 0 C46 1 0.251778 0.329969 0.059026 11.00000 0.05250 0.07432 = 0.03401 -0.00493 -0.00172 0.00392 AFIX 43 H46 2 0.235080 0.347755 0.014461 11.00000 -1.20000 AFIX 0 C47 1 0.231154 0.315746 0.129068 11.00000 0.04090 0.11727 = 0.04800 -0.01162 0.00084 -0.00296 AFIX 43 H47 2 0.199932 0.321103 0.133299 11.00000 -1.20000 AFIX 0 C48 1 0.256182 0.293821 0.192426 11.00000 0.05678 0.08700 = 0.03578 -0.00578 -0.00143 -0.01705 AFIX 43 H48 2 0.241461 0.283059 0.240442 11.00000 -1.20000 AFIX 0 C32 1 0.345266 -0.157027 -0.073797 11.00000 0.05847 0.03276 = 0.03025 -0.00127 -0.00738 0.00300 C33 1 0.316524 -0.072202 -0.056512 11.00000 0.06738 0.03046 = 0.03913 0.00353 -0.01713 0.00525 C34 1 0.326762 -0.010771 0.006366 11.00000 0.08516 0.03100 = 0.04758 -0.00785 -0.02941 0.01511 AFIX 43 H34 2 0.351483 -0.025289 0.038401 11.00000 -1.20000 AFIX 0 C37 1 0.282044 -0.048322 -0.104572 11.00000 0.10393 0.04296 = 0.05643 -0.00749 -0.03965 0.02032 AFIX 43 H37 2 0.276962 -0.085239 -0.150433 11.00000 -1.20000 AFIX 0 C35 1 0.301825 0.068755 0.021774 11.00000 0.14131 0.03089 = 0.05967 -0.01677 -0.05524 0.03196 AFIX 43 H35 2 0.308722 0.110647 0.064047 11.00000 -1.20000 AFIX 0 C36 1 0.266165 0.087141 -0.025631 11.00000 0.20910 0.06737 = 0.07532 -0.02340 -0.07236 0.07499 AFIX 43 H36 2 0.248724 0.143239 -0.015163 11.00000 -1.20000 AFIX 0 C68 1 0.307446 -0.210570 0.346772 11.00000 0.04747 0.04226 = 0.03638 0.00466 0.00492 -0.01513 C69 1 0.288591 -0.194813 0.267715 11.00000 0.04751 0.03784 = 0.03510 -0.01040 -0.00072 -0.00246 C73 1 0.315583 -0.176860 0.204092 11.00000 0.05116 0.03291 = 0.03204 0.00541 -0.00255 0.00064 AFIX 43 H73 2 0.346403 -0.169205 0.212802 11.00000 -1.20000 AFIX 0 C70 1 0.243516 -0.204195 0.255158 11.00000 0.04656 0.10575 = 0.04459 -0.02159 0.00218 -0.01321 AFIX 43 H70 2 0.223972 -0.218568 0.296836 11.00000 -1.20000 AFIX 0 C71 1 0.227885 -0.192148 0.180837 11.00000 0.04141 0.13173 = 0.06163 -0.03775 -0.00799 0.00585 AFIX 43 H71 2 0.196986 -0.194992 0.171200 11.00000 -1.20000 AFIX 0 C72 1 0.257064 -0.175752 0.119338 11.00000 0.05981 0.06773 = 0.05051 -0.02423 -0.00833 0.01725 AFIX 43 H72 2 0.245625 -0.168762 0.068217 11.00000 -1.20000 AFIX 0 C56 1 0.320226 0.298621 0.400624 11.00000 0.04608 0.04270 = 0.02981 -0.00324 0.00386 0.00219 C57 1 0.293679 0.211439 0.378892 11.00000 0.05779 0.02411 = 0.02918 0.00473 0.00538 -0.00076 C58 1 0.310090 0.140465 0.327240 11.00000 0.07639 0.03246 = 0.04059 -0.00461 0.01002 -0.01025 AFIX 43 H58 2 0.337908 0.149512 0.302639 11.00000 -1.20000 AFIX 0 C61 1 0.253439 0.195725 0.412510 11.00000 0.06788 0.04706 = 0.05917 -0.01279 0.01815 -0.01593 AFIX 43 H61 2 0.243320 0.241724 0.449769 11.00000 -1.20000 AFIX 0 C59 1 0.285838 0.058791 0.312774 11.00000 0.14369 0.03965 = 0.05575 -0.01983 0.03977 -0.03701 AFIX 43 H59 2 0.296744 0.009203 0.279320 11.00000 -1.20000 AFIX 0 C60 1 0.246393 0.050142 0.346740 11.00000 0.17135 0.05092 = 0.06021 -0.00770 0.02892 -0.05996 AFIX 43 H60 2 0.230164 -0.007726 0.336369 11.00000 -1.20000 AFIX 66 C1S 1 0.349611 0.564892 0.121302 11.00000 0.05718 0.05989 = 0.07694 0.01862 -0.00750 0.00340 AFIX 43 H1S 2 0.377136 0.566780 0.094747 11.00000 -1.20000 AFIX 65 C5S 1 0.310305 0.567624 0.079502 11.00000 0.09432 0.06183 = 0.14628 -0.00541 -0.00321 0.00884 AFIX 43 H5S 2 0.310965 0.571380 0.024379 11.00000 -1.20000 AFIX 65 C4S 1 0.270033 0.564862 0.118355 11.00000 0.07590 0.04147 = 0.24849 0.03210 0.02967 -0.00520 C2S 1 0.269067 0.559366 0.199008 11.00000 0.06541 0.12690 = 0.07174 0.03116 0.00566 -0.00512 AFIX 43 H2S 2 0.241542 0.557478 0.225562 11.00000 -1.20000 AFIX 65 C6S 1 0.308373 0.556633 0.240809 11.00000 0.09724 0.10242 = 0.10145 0.03808 0.02760 0.01056 AFIX 43 H6S 2 0.307712 0.552877 0.295932 11.00000 -1.20000 AFIX 65 C3S 1 0.348645 0.559396 0.201957 11.00000 0.08223 0.05544 = 0.11443 0.02145 -0.00452 -0.00904 AFIX 43 H3S 2 0.375509 0.557528 0.230526 11.00000 -1.20000 AFIX 0 C7S 1 0.097193 0.036677 0.152201 11.00000 0.06656 0.05134 = 0.03922 0.01590 0.00358 0.01023 C8S 1 0.114428 0.088277 0.214550 11.00000 0.08208 0.05021 = 0.04040 0.00967 0.00714 0.01920 AFIX 43 H8S 2 0.095431 0.111217 0.254540 11.00000 -1.20000 AFIX 0 C9S 1 0.157389 0.105429 0.218138 11.00000 0.10238 0.06534 = 0.05227 -0.01932 -0.00531 -0.00365 AFIX 43 H9S 2 0.168861 0.144867 0.258808 11.00000 -1.20000 AFIX 0 C10S 1 0.123563 -0.003453 0.096700 11.00000 0.07633 0.05778 = 0.03688 -0.00130 0.00101 0.00418 AFIX 43 H10S 2 0.111343 -0.041601 0.055922 11.00000 -1.20000 AFIX 0 C11S 1 0.168055 0.012528 0.101131 11.00000 0.07746 0.10283 = 0.04822 -0.01160 0.00383 0.01861 AFIX 43 H11S 2 0.187073 -0.012897 0.062139 11.00000 -1.20000 AFIX 0 C12S 1 0.185825 0.066544 0.163279 11.00000 0.07537 0.12810 = 0.07453 -0.02638 0.00344 -0.00933 AFIX 43 H12S 2 0.216837 0.076154 0.167499 11.00000 -1.20000 AFIX 0 CL1S 3 0.220986 0.573026 0.071524 11.00000 0.08495 0.13132 = 0.11779 0.02115 -0.00173 -0.00065 CL2S 3 0.040235 0.022267 0.143912 11.00000 0.06161 0.16958 = 0.06819 0.03031 -0.00201 0.01185 N5 5 0.525173 0.049557 0.204069 11.00000 0.04451 0.03381 = 0.02861 0.00123 0.00090 -0.00248 N6 5 0.592209 0.071583 0.250521 11.00000 0.03865 0.05469 = 0.03775 -0.00337 -0.00352 0.00298 AFIX 43 H6 2 0.615329 0.099384 0.272268 11.00000 -1.20000 AFIX 0 N7 5 0.361744 -0.203339 -0.011008 11.00000 0.05145 0.03091 = 0.02419 0.00105 -0.00429 0.00167 AFIX 43 H7A 2 0.349239 -0.192075 0.034294 11.00000 -1.20000 AFIX 0 N8 5 0.356806 0.279131 -0.031318 11.00000 0.04889 0.03515 = 0.02552 0.00710 -0.00055 0.00108 AFIX 43 H8A 2 0.360605 0.232130 0.002861 11.00000 -1.20000 AFIX 0 N9 5 0.345212 0.335209 0.342503 11.00000 0.04655 0.03021 = 0.02741 -0.00320 0.00522 -0.00414 AFIX 43 H9 2 0.339016 0.315991 0.294934 11.00000 -1.20000 AFIX 0 N10 5 0.341787 -0.153537 0.365927 11.00000 0.04303 0.02955 = 0.03379 0.00404 -0.00304 -0.00996 AFIX 43 H10 2 0.345720 -0.102892 0.335286 11.00000 -1.20000 AFIX 0 N11 5 0.300465 -0.169681 0.130550 11.00000 0.05598 0.05069 = 0.03612 0.00075 -0.00596 0.00836 N12 5 0.300588 0.286467 0.191125 11.00000 0.05484 0.06289 = 0.02769 0.00185 0.00258 -0.01143 N13 5 0.254453 0.029610 -0.086618 11.00000 0.16278 0.07002 = 0.07124 -0.02280 -0.04679 0.05910 N14 5 0.226828 0.118128 0.395986 11.00000 0.10916 0.06552 = 0.08030 -0.01209 0.02564 -0.04254 O1 6 0.320467 0.329764 0.467812 11.00000 0.07651 0.05933 = 0.03334 -0.01523 0.01630 -0.01940 O2 6 0.354857 -0.178700 -0.141536 11.00000 0.06899 0.05642 = 0.02331 -0.00207 -0.00680 0.00159 O3 6 0.292927 -0.273761 0.390283 11.00000 0.13626 0.09855 = 0.03817 0.01540 -0.01259 -0.08383 O4 6 0.306644 0.391901 -0.069052 11.00000 0.09834 0.10151 = 0.04474 0.03146 0.01663 0.05591 HKLF 4 1 0 0 1 1 0 0 0 1 0 REM yj_a.res in P2(1) New:Pna21 REM wR2 = 0.2401, GooF = S = 1.063, Restrained GooF = 1.063 for all data REM R1 = 0.0804 for 12171 Fo > 4sig(Fo) and 0.1065 for all 14653 data REM 946 parameters refined using 1 restraints END WGHT 0.1077 24.1624 REM Highest difference peak 0.978, deepest hole -1.031, 1-sigma level 0.100 Q1 1 0.2275 0.5226 0.1794 11.00000 0.05 0.98 Q2 1 0.1855 0.5477 0.0474 11.00000 0.05 0.74 ; _shelx_res_checksum 45622 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mn Mn1 0.45525(4) 0.06614(8) 0.17877(7) 0.0281(3) Uani d 1 . . N N1 0.4348(2) -0.0793(4) 0.2054(4) 0.0262(13) Uani d 1 . . N N2 0.4298(2) 0.1066(5) 0.2903(4) 0.0279(13) Uani d 1 . . N N3 0.4393(2) 0.2123(5) 0.1452(4) 0.0289(13) Uani d 1 . . N N4 0.4429(2) 0.0271(5) 0.0595(4) 0.0271(13) Uani d 1 . . C C4 0.4360(3) -0.1573(5) 0.1553(4) 0.0251(15) Uani d 1 . . C C1 0.4293(3) -0.1147(5) 0.2795(4) 0.0270(15) Uani d 1 . . C C19 0.4243(2) 0.0426(5) 0.3515(4) 0.0255(14) Uani d 1 . . C C16 0.4268(3) 0.1998(6) 0.3193(5) 0.0300(16) Uani d 1 . . C C14 0.4347(3) 0.2913(5) 0.1942(4) 0.0299(16) Uani d 1 . . C C11 0.4395(3) 0.2489(6) 0.0699(5) 0.0287(15) Uani d 1 . . C C9 0.4409(3) 0.0900(6) -0.0030(4) 0.0279(15) Uani d 1 . . C C6 0.4424(3) -0.0655(6) 0.0300(4) 0.0292(16) Uani d 1 . . C C3 0.4323(3) -0.2477(5) 0.2004(4) 0.0295(16) Uani d 1 . . H H3 0.432566 -0.312405 0.180631 0.035 Uiso calc 1 . . C C2 0.4283(3) -0.2206(6) 0.2763(5) 0.0318(17) Uani d 1 . . H H2 0.425412 -0.263366 0.319432 0.038 Uiso calc 1 . . C C18 0.4181(3) 0.0991(6) 0.4221(4) 0.0339(18) Uani d 1 . . H H18 0.413455 0.073443 0.472722 0.041 Uiso calc 1 . . C C17 0.4200(3) 0.1945(6) 0.4031(4) 0.0321(17) Uani d 1 . . H H17 0.417493 0.248084 0.437833 0.038 Uiso calc 1 . . C C13 0.4340(3) 0.3799(6) 0.1479(5) 0.0344(17) Uani d 1 . . H H13 0.431639 0.444585 0.167184 0.041 Uiso calc 1 . . C C12 0.4372(3) 0.3535(6) 0.0724(5) 0.0335(17) Uani d 1 . . H H12 0.437852 0.396232 0.028974 0.040 Uiso calc 1 . . C C8 0.4404(3) 0.0337(6) -0.0748(5) 0.0343(18) Uani d 1 . . H H8 0.439129 0.059094 -0.126106 0.041 Uiso calc 1 . . C C7 0.4419(3) -0.0621(6) -0.0543(5) 0.0337(17) Uani d 1 . . H H7 0.442578 -0.116402 -0.088618 0.040 Uiso calc 1 . . C C5 0.4391(3) -0.1523(6) 0.0742(4) 0.0286(16) Uani d 1 . . C C20 0.4238(3) -0.0582(6) 0.3470(4) 0.0279(15) Uani d 1 . . C C15 0.4287(3) 0.2852(6) 0.2751(4) 0.0287(16) Uani d 1 . . C C10 0.4390(3) 0.1915(5) 0.0011(5) 0.0285(15) Uani d 1 . . C C38 0.4317(3) 0.2450(6) -0.0742(4) 0.0328(17) Uani d 1 . . C C43 0.3902(3) 0.2874(6) -0.0896(5) 0.0346(17) Uani d 1 . . C C42 0.3823(3) 0.3348(7) -0.1599(5) 0.041(2) Uani d 1 . . H H42 0.354400 0.363857 -0.170375 0.049 Uiso calc 1 . . C C41 0.4162(4) 0.3385(7) -0.2143(5) 0.043(2) Uani d 1 . . H H41 0.411037 0.370699 -0.262340 0.052 Uiso calc 1 . . C C40 0.4568(3) 0.2973(7) -0.2011(5) 0.041(2) Uani d 1 . . H H40 0.479286 0.299728 -0.239652 0.050 Uiso calc 1 . . C C39 0.4645(3) 0.2518(6) -0.1300(5) 0.0370(18) Uani d 1 . . H H39 0.492859 0.224862 -0.119639 0.044 Uiso calc 1 . . C C26 0.4362(3) -0.2455(6) 0.0290(4) 0.0299(16) Uani d 1 . . C C31 0.3979(3) -0.2690(6) -0.0133(5) 0.0333(17) Uani d 1 . . C C30 0.3956(3) -0.3541(6) -0.0573(5) 0.0387(19) Uani d 1 . . H H30 0.369625 -0.368807 -0.085973 0.046 Uiso calc 1 . . C C29 0.4311(3) -0.4166(6) -0.0592(5) 0.041(2) Uani d 1 . . H H29 0.429615 -0.474211 -0.089785 0.049 Uiso calc 1 . . C C28 0.4693(4) -0.3962(6) -0.0166(5) 0.043(2) Uani d 1 . . H H28 0.493690 -0.439754 -0.018096 0.052 Uiso calc 1 . . C C27 0.4714(3) -0.3119(6) 0.0279(5) 0.0342(17) Uani d 1 . . H H27 0.497053 -0.299127 0.058142 0.041 Uiso calc 1 . . C C62 0.4133(3) -0.1143(5) 0.4194(4) 0.0289(16) Uani d 1 . . C C67 0.3725(3) -0.1613(6) 0.4269(4) 0.0318(17) Uani d 1 . . C C66 0.3630(3) -0.2179(7) 0.4948(5) 0.041(2) Uani d 1 . . H H66 0.335455 -0.250347 0.500374 0.049 Uiso calc 1 . . C C65 0.3950(3) -0.2241(6) 0.5522(5) 0.040(2) Uani d 1 . . H H65 0.389080 -0.261811 0.597376 0.048 Uiso calc 1 . . C C64 0.4355(3) -0.1768(7) 0.5457(5) 0.039(2) Uani d 1 . . H H64 0.457141 -0.182661 0.585507 0.047 Uiso calc 1 . . C C63 0.4439(3) -0.1204(6) 0.4797(5) 0.0334(17) Uani d 1 . . H H63 0.470918 -0.085468 0.475856 0.040 Uiso calc 1 . . C C50 0.4216(3) 0.3793(5) 0.3174(5) 0.0304(16) Uani d 1 . . C C55 0.3806(3) 0.4020(6) 0.3517(5) 0.0332(17) Uani d 1 . . C C54 0.3749(3) 0.4881(6) 0.3924(5) 0.0395(19) Uani d 1 . . H H54 0.347039 0.502786 0.414984 0.047 Uiso calc 1 . . C C53 0.4101(4) 0.5537(6) 0.4006(5) 0.043(2) Uani d 1 . . H H53 0.406239 0.612243 0.429356 0.052 Uiso calc 1 . . C C52 0.4507(3) 0.5327(6) 0.3662(5) 0.041(2) Uani d 1 . . H H52 0.474763 0.576813 0.371583 0.049 Uiso calc 1 . . C C51 0.4560(3) 0.4474(6) 0.3244(5) 0.0343(18) Uani d 1 . . H H51 0.483525 0.434614 0.299801 0.041 Uiso calc 1 . . C C21 0.5500(3) -0.0324(7) 0.1896(7) 0.050(2) Uani d 1 . . H H21 0.539801 -0.088773 0.163089 0.059 Uiso calc 1 . . C C22 0.5911(4) -0.0208(8) 0.2188(6) 0.055(3) Uani d 1 . . C C23 0.6282(5) -0.0939(14) 0.2290(11) 0.099(5) Uani d 1 . . H H23A 0.654723 -0.070274 0.202121 0.148 Uiso calc 1 . . H H23B 0.619323 -0.156791 0.206977 0.148 Uiso calc 1 . . H H23C 0.634676 -0.101800 0.284452 0.148 Uiso calc 1 . . C C24 0.5516(3) 0.1122(6) 0.2425(5) 0.0347(17) Uani d 1 . . C C25 0.5403(3) 0.2105(7) 0.2705(6) 0.044(2) Uani d 1 . . H H25A 0.565198 0.236989 0.300271 0.066 Uiso calc 1 . . H H25B 0.514134 0.206798 0.303958 0.066 Uiso calc 1 . . H H25C 0.534110 0.253002 0.226096 0.066 Uiso calc 1 . . C C44 0.3205(3) 0.3335(7) -0.0220(5) 0.042(2) Uani d 1 . . C C45 0.2967(3) 0.3183(7) 0.0538(5) 0.0381(19) Uani d 1 . . C C49 0.3200(3) 0.2978(7) 0.1214(5) 0.042(2) Uani d 1 . . H H49 0.351180 0.291514 0.118252 0.051 Uiso calc 1 . . C C46 0.2518(4) 0.3300(9) 0.0590(6) 0.054(3) Uani d 1 . . H H46 0.235080 0.347755 0.014461 0.064 Uiso calc 1 . . C C47 0.2312(4) 0.3157(12) 0.1291(7) 0.069(4) Uani d 1 . . H H47 0.199932 0.321103 0.133299 0.082 Uiso calc 1 . . C C48 0.2562(4) 0.2938(10) 0.1924(6) 0.060(3) Uani d 1 . . H H48 0.241461 0.283059 0.240442 0.072 Uiso calc 1 . . C C32 0.3453(3) -0.1570(7) -0.0738(5) 0.040(2) Uani d 1 . . C C33 0.3165(4) -0.0722(7) -0.0565(6) 0.046(2) Uani d 1 . . C C34 0.3268(4) -0.0108(7) 0.0064(6) 0.055(3) Uani d 1 . . H H34 0.351483 -0.025289 0.038401 0.065 Uiso calc 1 . . C C37 0.2820(5) -0.0483(8) -0.1046(7) 0.068(4) Uani d 1 . . H H37 0.276962 -0.085239 -0.150433 0.081 Uiso calc 1 . . C C35 0.3018(5) 0.0688(8) 0.0218(7) 0.077(5) Uani d 1 . . H H35 0.308722 0.110647 0.064047 0.093 Uiso calc 1 . . C C36 0.2662(8) 0.0871(11) -0.0256(9) 0.117(8) Uani d 1 . . H H36 0.248724 0.143239 -0.015163 0.141 Uiso calc 1 . . C C68 0.3074(3) -0.2106(7) 0.3468(5) 0.042(2) Uani d 1 . . C C69 0.2886(3) -0.1948(7) 0.2677(5) 0.0401(19) Uani d 1 . . C C73 0.3156(3) -0.1769(6) 0.2041(5) 0.0387(19) Uani d 1 . . H H73 0.346403 -0.169205 0.212802 0.046 Uiso calc 1 . . C C70 0.2435(4) -0.2042(11) 0.2552(7) 0.066(3) Uani d 1 . . H H70 0.223972 -0.218568 0.296836 0.079 Uiso calc 1 . . C C71 0.2279(4) -0.1921(12) 0.1808(8) 0.078(4) Uani d 1 . . H H71 0.196986 -0.194992 0.171200 0.094 Uiso calc 1 . . C C72 0.2571(4) -0.1758(9) 0.1193(7) 0.059(3) Uani d 1 . . H H72 0.245625 -0.168762 0.068217 0.071 Uiso calc 1 . . C C56 0.3202(3) 0.2986(7) 0.4006(5) 0.0395(19) Uani d 1 . . C C57 0.2937(3) 0.2114(6) 0.3789(5) 0.0370(18) Uani d 1 . . C C58 0.3101(4) 0.1405(7) 0.3272(6) 0.050(2) Uani d 1 . . H H58 0.337908 0.149512 0.302639 0.060 Uiso calc 1 . . C C61 0.2534(4) 0.1957(8) 0.4125(7) 0.058(3) Uani d 1 . . H H61 0.243320 0.241724 0.449769 0.070 Uiso calc 1 . . C C59 0.2858(6) 0.0588(9) 0.3128(7) 0.080(5) Uani d 1 . . H H59 0.296744 0.009203 0.279320 0.096 Uiso calc 1 . . C C60 0.2464(6) 0.0501(10) 0.3467(8) 0.094(6) Uani d 1 . . H H60 0.230164 -0.007726 0.336369 0.113 Uiso calc 1 . . C C1S 0.3496(2) 0.5649(7) 0.1213(5) 0.065(3) Uani d 1 . . H H1S 0.377136 0.566780 0.094747 0.078 Uiso calc 1 . . C C5S 0.3103(3) 0.5676(7) 0.0795(5) 0.101(6) Uani d 1 . . H H5S 0.310965 0.571380 0.024379 0.121 Uiso calc 1 . . C C4S 0.2700(2) 0.5649(7) 0.1184(7) 0.122(9) Uani d 1 . . C C2S 0.2691(3) 0.5594(8) 0.1990(7) 0.088(5) Uani d 1 . . H H2S 0.241542 0.557478 0.225562 0.106 Uiso calc 1 . . C C6S 0.3084(3) 0.5566(8) 0.2408(5) 0.100(6) Uani d 1 . . H H6S 0.307712 0.552877 0.295932 0.120 Uiso calc 1 . . C C3S 0.3486(3) 0.5594(7) 0.2020(5) 0.084(5) Uani d 1 . . H H3S 0.375509 0.557528 0.230526 0.101 Uiso calc 1 . . C C7S 0.0972(4) 0.0367(8) 0.1522(6) 0.052(2) Uani d 1 . . C C8S 0.1144(4) 0.0883(8) 0.2146(6) 0.058(3) Uani d 1 . . H H8S 0.095431 0.111217 0.254540 0.069 Uiso calc 1 . . C C9S 0.1574(5) 0.1054(10) 0.2181(8) 0.073(4) Uani d 1 . . H H9S 0.168861 0.144867 0.258808 0.088 Uiso calc 1 . . C C10S 0.1236(4) -0.0035(9) 0.0967(6) 0.057(3) Uani d 1 . . H H10S 0.111343 -0.041601 0.055922 0.068 Uiso calc 1 . . C C11S 0.1681(5) 0.0125(12) 0.1011(8) 0.076(4) Uani d 1 . . H H11S 0.187073 -0.012897 0.062139 0.091 Uiso calc 1 . . C C12S 0.1858(5) 0.0665(14) 0.1633(9) 0.093(5) Uani d 1 . . H H12S 0.216837 0.076154 0.167499 0.111 Uiso calc 1 . . Cl Cl1S 0.22099(16) 0.5730(4) 0.0715(3) 0.1114(16) Uani d 1 . . Cl Cl2S 0.04023(12) 0.0223(4) 0.1439(2) 0.0998(15) Uani d 1 . . N N5 0.5252(2) 0.0496(5) 0.2041(4) 0.0356(15) Uani d 1 . . N N6 0.5922(3) 0.0716(6) 0.2505(5) 0.0437(18) Uani d 1 . . H H6 0.615329 0.099384 0.272268 0.052 Uiso calc 1 . . N N7 0.3617(2) -0.2033(5) -0.0110(4) 0.0355(15) Uani d 1 . . H H7A 0.349239 -0.192075 0.034294 0.043 Uiso calc 1 . . N N8 0.3568(3) 0.2791(5) -0.0313(4) 0.0365(15) Uani d 1 . . H H8A 0.360605 0.232130 0.002861 0.044 Uiso calc 1 . . N N9 0.3452(2) 0.3352(5) 0.3425(4) 0.0347(15) Uani d 1 . . H H9 0.339016 0.315991 0.294934 0.042 Uiso calc 1 . . N N10 0.3418(2) -0.1535(5) 0.3659(4) 0.0355(15) Uani d 1 . . H H10 0.345720 -0.102892 0.335286 0.043 Uiso calc 1 . . N N11 0.3005(3) -0.1697(6) 0.1306(5) 0.0476(19) Uani d 1 . . N N12 0.3006(3) 0.2865(7) 0.1911(4) 0.0485(19) Uani d 1 . . N N13 0.2545(6) 0.0296(9) -0.0866(7) 0.101(5) Uani d 1 . . N N14 0.2268(4) 0.1181(9) 0.3960(8) 0.085(4) Uani d 1 . . O O1 0.3205(3) 0.3298(6) 0.4678(4) 0.0564(19) Uani d 1 . . O O2 0.3549(2) -0.1787(5) -0.1415(4) 0.0496(17) Uani d 1 . . O O3 0.2929(4) -0.2738(8) 0.3903(5) 0.091(4) Uani d 1 . . O O4 0.3066(3) 0.3919(8) -0.0691(5) 0.082(3) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Mn1 0.0395(6) 0.0223(5) 0.0227(5) -0.0016(4) 0.0000(5) 0.0008(5) N1 0.041(4) 0.017(3) 0.021(3) -0.003(2) -0.002(2) -0.002(2) N2 0.043(4) 0.021(3) 0.020(3) -0.003(3) 0.003(3) 0.001(2) N3 0.044(4) 0.022(3) 0.021(3) 0.001(3) -0.003(3) 0.001(3) N4 0.039(3) 0.022(3) 0.020(3) 0.000(3) -0.001(3) 0.001(2) C4 0.041(4) 0.011(3) 0.023(3) 0.000(3) -0.001(3) 0.000(3) C1 0.035(4) 0.021(4) 0.025(4) -0.004(3) 0.001(3) 0.002(3) C19 0.034(4) 0.022(3) 0.020(3) 0.001(3) -0.001(3) -0.002(3) C16 0.045(4) 0.022(4) 0.023(4) 0.004(3) 0.001(3) 0.006(3) C14 0.042(4) 0.023(3) 0.025(4) -0.001(3) -0.002(3) -0.002(3) C11 0.039(4) 0.022(4) 0.026(4) 0.000(3) -0.001(3) 0.005(3) C9 0.034(4) 0.028(4) 0.021(3) 0.000(3) 0.001(3) 0.002(3) C6 0.041(4) 0.028(4) 0.019(3) -0.003(3) -0.003(3) -0.003(3) C3 0.048(4) 0.016(3) 0.025(4) -0.005(3) 0.002(3) 0.004(3) C2 0.045(4) 0.024(4) 0.026(4) -0.002(3) 0.002(3) 0.004(3) C18 0.057(5) 0.026(4) 0.019(4) 0.000(3) 0.003(3) 0.001(3) C17 0.055(5) 0.021(4) 0.019(4) 0.003(3) -0.002(3) -0.005(3) C13 0.044(4) 0.028(4) 0.031(4) -0.005(3) -0.004(3) 0.000(3) C12 0.049(5) 0.018(4) 0.034(4) -0.003(3) -0.003(4) 0.002(3) C8 0.050(5) 0.031(4) 0.022(4) 0.003(4) 0.000(3) 0.004(3) C7 0.048(5) 0.030(4) 0.024(4) -0.001(3) 0.001(3) -0.004(3) C5 0.036(4) 0.027(4) 0.023(4) -0.004(3) -0.001(3) 0.000(3) C20 0.034(4) 0.031(4) 0.019(3) -0.002(3) -0.001(3) 0.002(3) C15 0.039(4) 0.023(4) 0.024(4) 0.004(3) -0.003(3) 0.001(3) C10 0.038(4) 0.024(4) 0.024(4) -0.001(3) -0.002(3) 0.008(3) C38 0.053(5) 0.024(4) 0.021(4) -0.003(3) 0.000(3) 0.006(3) C43 0.048(5) 0.027(4) 0.028(4) -0.001(3) 0.001(4) 0.003(3) C42 0.053(5) 0.037(5) 0.032(4) 0.002(4) -0.002(4) 0.012(4) C41 0.068(6) 0.037(5) 0.025(4) -0.003(4) 0.000(4) 0.004(3) C40 0.056(5) 0.036(4) 0.032(4) -0.001(4) 0.006(4) 0.006(4) C39 0.045(4) 0.029(4) 0.038(4) 0.000(3) 0.005(4) 0.004(3) C26 0.042(4) 0.028(4) 0.020(3) -0.002(3) 0.002(3) -0.003(3) C31 0.050(5) 0.025(4) 0.025(4) -0.003(3) -0.005(3) -0.002(3) C30 0.059(5) 0.030(4) 0.027(4) -0.003(4) -0.004(4) -0.009(3) C29 0.065(6) 0.027(4) 0.032(4) -0.001(4) 0.002(4) -0.005(3) C28 0.070(6) 0.026(4) 0.033(4) 0.005(4) 0.005(4) -0.003(3) C27 0.047(5) 0.026(4) 0.030(4) -0.001(3) -0.001(3) 0.000(3) C62 0.044(4) 0.024(4) 0.019(3) 0.002(3) 0.000(3) 0.001(3) C67 0.042(4) 0.031(4) 0.022(4) -0.001(3) 0.003(3) 0.008(3) C66 0.053(5) 0.037(4) 0.032(4) -0.003(4) 0.006(4) 0.011(4) C65 0.068(6) 0.032(4) 0.021(4) -0.001(4) 0.003(4) 0.004(3) C64 0.061(6) 0.036(4) 0.021(4) 0.008(4) 0.000(4) 0.003(3) C63 0.042(4) 0.034(4) 0.024(4) -0.004(3) -0.003(3) 0.001(3) C50 0.048(5) 0.015(3) 0.028(4) 0.000(3) -0.001(3) 0.000(3) C55 0.046(4) 0.021(3) 0.032(4) -0.003(3) 0.001(3) 0.000(3) C54 0.059(5) 0.022(4) 0.037(5) 0.004(4) 0.010(4) -0.003(3) C53 0.070(6) 0.021(4) 0.038(5) -0.005(4) 0.008(4) -0.008(3) C52 0.061(6) 0.025(4) 0.036(5) -0.002(4) -0.002(4) 0.000(3) C51 0.050(5) 0.019(4) 0.034(4) -0.001(3) 0.001(3) 0.000(3) C21 0.060(6) 0.039(4) 0.050(6) 0.017(4) -0.009(5) -0.005(4) C22 0.065(7) 0.055(6) 0.043(6) 0.018(5) -0.007(5) -0.015(5) C23 0.064(9) 0.117(14) 0.115(13) 0.024(9) -0.013(9) -0.025(11) C24 0.046(5) 0.033(4) 0.025(4) 0.000(3) 0.001(3) 0.006(3) C25 0.054(5) 0.033(4) 0.044(5) -0.004(4) -0.015(4) 0.007(4) C44 0.048(5) 0.046(5) 0.032(5) 0.006(4) -0.003(4) 0.008(4) C45 0.045(5) 0.039(5) 0.031(4) 0.000(4) -0.003(4) 0.003(4) C49 0.050(5) 0.042(5) 0.034(4) -0.004(4) 0.000(4) 0.005(4) C46 0.053(6) 0.074(7) 0.034(5) 0.004(5) -0.002(4) -0.005(5) C47 0.041(5) 0.117(11) 0.048(6) -0.003(6) 0.001(5) -0.012(7) C48 0.057(6) 0.087(8) 0.036(6) -0.017(6) -0.001(4) -0.006(5) C32 0.058(5) 0.033(4) 0.030(4) 0.003(4) -0.007(4) -0.001(3) C33 0.067(6) 0.030(4) 0.039(5) 0.005(4) -0.017(5) 0.004(4) C34 0.085(8) 0.031(5) 0.048(6) 0.015(5) -0.029(5) -0.008(4) C37 0.104(10) 0.043(6) 0.056(7) 0.020(6) -0.040(7) -0.007(5) C35 0.141(13) 0.031(5) 0.060(7) 0.032(6) -0.055(8) -0.017(5) C36 0.21(2) 0.067(9) 0.075(10) 0.075(12) -0.072(12) -0.023(8) C68 0.047(5) 0.042(5) 0.036(5) -0.015(4) 0.005(4) 0.005(4) C69 0.048(5) 0.038(5) 0.035(5) -0.002(4) -0.001(4) -0.010(4) C73 0.051(5) 0.033(4) 0.032(4) 0.001(4) -0.003(4) 0.005(3) C70 0.047(6) 0.106(10) 0.045(6) -0.013(6) 0.002(5) -0.022(6) C71 0.041(5) 0.132(12) 0.062(7) 0.006(6) -0.008(6) -0.038(9) C72 0.060(6) 0.068(7) 0.051(6) 0.017(6) -0.008(5) -0.024(5) C56 0.046(5) 0.043(5) 0.030(4) 0.002(4) 0.004(4) -0.003(4) C57 0.058(5) 0.024(4) 0.029(4) -0.001(3) 0.005(4) 0.005(3) C58 0.076(7) 0.032(5) 0.041(5) -0.010(5) 0.010(5) -0.005(4) C61 0.068(7) 0.047(6) 0.059(7) -0.016(5) 0.018(6) -0.013(5) C59 0.144(13) 0.040(6) 0.056(7) -0.037(7) 0.040(8) -0.020(5) C60 0.171(17) 0.051(7) 0.060(8) -0.060(9) 0.029(9) -0.008(6) C1S 0.057(7) 0.060(7) 0.077(8) 0.003(5) -0.007(6) 0.019(6) C5S 0.094(12) 0.062(9) 0.146(17) 0.009(8) -0.003(11) -0.005(10) C4S 0.076(10) 0.041(7) 0.25(3) -0.005(6) 0.030(13) 0.032(11) C2S 0.065(8) 0.127(14) 0.072(10) -0.005(8) 0.006(7) 0.031(10) C6S 0.097(12) 0.102(13) 0.101(13) 0.011(10) 0.028(10) 0.038(11) C3S 0.082(9) 0.055(7) 0.114(14) -0.009(6) -0.005(8) 0.021(8) C7S 0.067(6) 0.051(6) 0.039(5) 0.010(5) 0.004(5) 0.016(4) C8S 0.082(8) 0.050(6) 0.040(6) 0.019(6) 0.007(5) 0.010(5) C9S 0.102(11) 0.065(8) 0.052(7) -0.004(7) -0.005(7) -0.019(6) C10S 0.076(8) 0.058(6) 0.037(5) 0.004(6) 0.001(5) -0.001(5) C11S 0.077(9) 0.103(11) 0.048(7) 0.019(8) 0.004(6) -0.012(7) C12S 0.075(9) 0.128(14) 0.075(10) -0.009(9) 0.003(7) -0.026(9) Cl1S 0.085(3) 0.131(4) 0.118(4) -0.001(3) -0.002(3) 0.021(3) Cl2S 0.0616(18) 0.170(5) 0.068(2) 0.012(2) -0.0020(16) 0.030(3) N5 0.045(4) 0.034(4) 0.029(3) -0.002(3) 0.001(3) 0.001(3) N6 0.039(4) 0.055(5) 0.038(4) 0.003(3) -0.004(3) -0.003(4) N7 0.051(4) 0.031(3) 0.024(3) 0.002(3) -0.004(3) 0.001(3) N8 0.049(4) 0.035(4) 0.026(3) 0.001(3) -0.001(3) 0.007(3) N9 0.047(4) 0.030(3) 0.027(3) -0.004(3) 0.005(3) -0.003(3) N10 0.043(4) 0.030(4) 0.034(4) -0.010(3) -0.003(3) 0.004(3) N11 0.056(5) 0.051(5) 0.036(4) 0.008(4) -0.006(4) 0.001(4) N12 0.055(5) 0.063(5) 0.028(4) -0.011(4) 0.003(3) 0.002(4) N13 0.163(13) 0.070(8) 0.071(7) 0.059(8) -0.047(8) -0.023(6) N14 0.109(9) 0.066(7) 0.080(8) -0.043(7) 0.026(7) -0.012(6) O1 0.077(5) 0.059(4) 0.033(4) -0.019(4) 0.016(3) -0.015(3) O2 0.069(5) 0.056(4) 0.023(3) 0.002(3) -0.007(3) -0.002(3) O3 0.136(9) 0.099(7) 0.038(4) -0.084(7) -0.013(5) 0.015(4) O4 0.098(7) 0.102(7) 0.045(4) 0.056(6) 0.017(4) 0.031(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 Mn1 N2 . . 86.9(2) y N1 Mn1 N3 . . 150.0(3) y N1 Mn1 N4 . . 85.5(2) y N1 Mn1 N5 . . 98.1(3) y N2 Mn1 N4 . . 148.9(3) y N2 Mn1 N5 . . 101.4(3) y N3 Mn1 N2 . . 85.3(2) y N3 Mn1 N4 . . 86.4(2) y N3 Mn1 N5 . . 111.8(3) y N4 Mn1 N5 . . 109.5(3) y C4 N1 Mn1 . . 125.8(5) ? C4 N1 C1 . . 108.0(6) ? C1 N1 Mn1 . . 124.3(5) ? C19 N2 Mn1 . . 124.2(5) ? C16 N2 Mn1 . . 126.1(5) ? C16 N2 C19 . . 107.9(6) ? C14 N3 Mn1 . . 126.3(5) ? C14 N3 C11 . . 106.7(6) ? C11 N3 Mn1 . . 126.1(5) ? C9 N4 Mn1 . . 126.5(5) ? C6 N4 Mn1 . . 125.9(5) ? C6 N4 C9 . . 106.9(6) ? N1 C4 C3 . . 109.0(6) ? N1 C4 C5 . . 126.0(7) ? C5 C4 C3 . . 125.0(7) ? N1 C1 C2 . . 108.7(7) ? N1 C1 C20 . . 125.9(7) ? C20 C1 C2 . . 125.4(7) ? N2 C19 C18 . . 108.3(6) ? N2 C19 C20 . . 126.4(7) ? C20 C19 C18 . . 125.3(7) ? N2 C16 C17 . . 108.7(6) ? N2 C16 C15 . . 125.4(7) ? C15 C16 C17 . . 125.9(7) ? N3 C14 C13 . . 108.9(6) ? N3 C14 C15 . . 124.8(7) ? C15 C14 C13 . . 126.2(7) ? N3 C11 C12 . . 109.4(7) ? N3 C11 C10 . . 125.2(7) ? C10 C11 C12 . . 125.3(7) ? N4 C9 C8 . . 109.3(6) ? N4 C9 C10 . . 125.8(7) ? C10 C9 C8 . . 124.9(7) ? N4 C6 C7 . . 110.0(7) ? N4 C6 C5 . . 125.7(7) ? C5 C6 C7 . . 124.2(7) ? C4 C3 H3 . . 126.8 ? C2 C3 C4 . . 106.4(7) ? C2 C3 H3 . . 126.8 ? C1 C2 H2 . . 126.1 ? C3 C2 C1 . . 107.9(7) ? C3 C2 H2 . . 126.1 ? C19 C18 H18 . . 126.0 ? C17 C18 C19 . . 108.0(7) ? C17 C18 H18 . . 126.0 ? C16 C17 H17 . . 126.5 ? C18 C17 C16 . . 107.1(7) ? C18 C17 H17 . . 126.5 ? C14 C13 H13 . . 126.2 ? C12 C13 C14 . . 107.5(7) ? C12 C13 H13 . . 126.2 ? C11 C12 H12 . . 126.3 ? C13 C12 C11 . . 107.5(7) ? C13 C12 H12 . . 126.3 ? C9 C8 H8 . . 126.5 ? C7 C8 C9 . . 107.0(7) ? C7 C8 H8 . . 126.5 ? C6 C7 H7 . . 126.6 ? C8 C7 C6 . . 106.8(7) ? C8 C7 H7 . . 126.6 ? C4 C5 C6 . . 125.4(7) ? C4 C5 C26 . . 118.2(7) ? C6 C5 C26 . . 116.3(7) ? C1 C20 C62 . . 115.4(7) ? C19 C20 C1 . . 126.5(7) ? C19 C20 C62 . . 118.0(7) ? C16 C15 C14 . . 126.4(7) ? C16 C15 C50 . . 116.8(7) ? C14 C15 C50 . . 116.7(7) ? C11 C10 C38 . . 116.6(7) ? C9 C10 C11 . . 126.5(7) ? C9 C10 C38 . . 116.7(7) ? C43 C38 C10 . . 119.6(7) ? C39 C38 C10 . . 121.6(8) ? C39 C38 C43 . . 118.7(7) ? C38 C43 N8 . . 117.7(7) ? C42 C43 C38 . . 120.5(8) ? C42 C43 N8 . . 121.8(8) ? C43 C42 H42 . . 120.8 ? C41 C42 C43 . . 118.4(9) ? C41 C42 H42 . . 120.8 ? C42 C41 H41 . . 118.8 ? C40 C41 C42 . . 122.3(8) ? C40 C41 H41 . . 118.8 ? C41 C40 H40 . . 120.7 ? C41 C40 C39 . . 118.7(9) ? C39 C40 H40 . . 120.7 ? C38 C39 C40 . . 121.3(8) ? C38 C39 H39 . . 119.4 ? C40 C39 H39 . . 119.4 ? C31 C26 C5 . . 120.8(7) ? C27 C26 C5 . . 121.1(7) ? C27 C26 C31 . . 118.1(7) ? C26 C31 N7 . . 118.5(7) ? C30 C31 C26 . . 120.9(8) ? C30 C31 N7 . . 120.6(7) ? C31 C30 H30 . . 120.1 ? C29 C30 C31 . . 119.8(8) ? C29 C30 H30 . . 120.1 ? C30 C29 H29 . . 119.7 ? C30 C29 C28 . . 120.5(8) ? C28 C29 H29 . . 119.7 ? C29 C28 H28 . . 120.2 ? C27 C28 C29 . . 119.7(9) ? C27 C28 H28 . . 120.2 ? C26 C27 H27 . . 119.6 ? C28 C27 C26 . . 120.9(8) ? C28 C27 H27 . . 119.6 ? C67 C62 C20 . . 120.0(7) ? C63 C62 C20 . . 120.6(7) ? C63 C62 C67 . . 119.4(7) ? C62 C67 C66 . . 120.1(8) ? C62 C67 N10 . . 118.7(7) ? N10 C67 C66 . . 121.2(8) ? C67 C66 H66 . . 120.8 ? C65 C66 C67 . . 118.4(8) ? C65 C66 H66 . . 120.8 ? C66 C65 H65 . . 119.0 ? C66 C65 C64 . . 121.9(8) ? C64 C65 H65 . . 119.0 ? C65 C64 H64 . . 120.6 ? C65 C64 C63 . . 118.9(8) ? C63 C64 H64 . . 120.6 ? C62 C63 C64 . . 121.2(8) ? C62 C63 H63 . . 119.4 ? C64 C63 H63 . . 119.4 ? C55 C50 C15 . . 121.4(7) ? C51 C50 C15 . . 120.6(8) ? C51 C50 C55 . . 118.0(7) ? C50 C55 N9 . . 118.3(7) ? C54 C55 C50 . . 120.7(8) ? C54 C55 N9 . . 121.0(8) ? C55 C54 H54 . . 119.8 ? C55 C54 C53 . . 120.4(9) ? C53 C54 H54 . . 119.8 ? C54 C53 H53 . . 120.2 ? C52 C53 C54 . . 119.6(8) ? C52 C53 H53 . . 120.2 ? C53 C52 H52 . . 120.1 ? C51 C52 C53 . . 119.8(9) ? C51 C52 H52 . . 120.1 ? C50 C51 H51 . . 119.3 ? C52 C51 C50 . . 121.5(8) ? C52 C51 H51 . . 119.3 ? C22 C21 H21 . . 125.0 ? C22 C21 N5 . . 109.9(9) ? N5 C21 H21 . . 125.0 ? C21 C22 C23 . . 130.4(11) ? C21 C22 N6 . . 106.1(9) ? N6 C22 C23 . . 122.9(11) ? C22 C23 H23A . . 109.5 ? C22 C23 H23B . . 109.5 ? C22 C23 H23C . . 109.5 ? H23A C23 H23B . . 109.5 ? H23A C23 H23C . . 109.5 ? H23B C23 H23C . . 109.5 ? N5 C24 C25 . . 127.4(8) ? N5 C24 N6 . . 109.0(8) ? N6 C24 C25 . . 123.6(8) ? C24 C25 H25A . . 109.5 ? C24 C25 H25B . . 109.5 ? C24 C25 H25C . . 109.5 ? H25A C25 H25B . . 109.5 ? H25A C25 H25C . . 109.5 ? H25B C25 H25C . . 109.5 ? N8 C44 C45 . . 114.9(8) ? O4 C44 C45 . . 120.3(9) ? O4 C44 N8 . . 124.9(9) ? C49 C45 C44 . . 120.8(8) ? C46 C45 C44 . . 121.0(8) ? C46 C45 C49 . . 118.1(9) ? C45 C49 H49 . . 118.3 ? N12 C49 C45 . . 123.4(9) ? N12 C49 H49 . . 118.3 ? C45 C46 H46 . . 120.3 ? C47 C46 C45 . . 119.5(10) ? C47 C46 H46 . . 120.3 ? C46 C47 H47 . . 120.6 ? C48 C47 C46 . . 118.8(10) ? C48 C47 H47 . . 120.6 ? C47 C48 H48 . . 118.0 ? N12 C48 C47 . . 123.9(10) ? N12 C48 H48 . . 118.0 ? N7 C32 C33 . . 115.2(8) ? O2 C32 C33 . . 121.0(8) ? O2 C32 N7 . . 123.7(9) ? C34 C33 C32 . . 119.7(8) ? C37 C33 C32 . . 120.8(9) ? C37 C33 C34 . . 119.3(9) ? C33 C34 H34 . . 119.6 ? C35 C34 C33 . . 120.8(10) ? C35 C34 H34 . . 119.6 ? C33 C37 H37 . . 119.8 ? C33 C37 N13 . . 120.4(11) ? N13 C37 H37 . . 119.8 ? C34 C35 H35 . . 121.0 ? C34 C35 C36 . . 118.0(11) ? C36 C35 H35 . . 121.0 ? C35 C36 H36 . . 118.1 ? N13 C36 C35 . . 123.7(13) ? N13 C36 H36 . . 118.1 ? N10 C68 C69 . . 115.8(8) ? O3 C68 C69 . . 121.5(9) ? O3 C68 N10 . . 122.6(9) ? C73 C69 C68 . . 121.4(8) ? C70 C69 C68 . . 120.3(9) ? C70 C69 C73 . . 118.2(9) ? C69 C73 H73 . . 118.2 ? N11 C73 C69 . . 123.6(9) ? N11 C73 H73 . . 118.2 ? C69 C70 H70 . . 120.9 ? C71 C70 C69 . . 118.2(11) ? C71 C70 H70 . . 120.9 ? C70 C71 H71 . . 119.8 ? C70 C71 C72 . . 120.5(11) ? C72 C71 H71 . . 119.8 ? C71 C72 H72 . . 119.2 ? N11 C72 C71 . . 121.6(11) ? N11 C72 H72 . . 119.2 ? N9 C56 C57 . . 114.5(8) ? O1 C56 C57 . . 121.2(8) ? O1 C56 N9 . . 124.2(9) ? C58 C57 C56 . . 121.6(8) ? C61 C57 C56 . . 120.1(8) ? C61 C57 C58 . . 118.2(9) ? C57 C58 H58 . . 120.2 ? C59 C58 C57 . . 119.6(11) ? C59 C58 H58 . . 120.2 ? C57 C61 H61 . . 117.9 ? N14 C61 C57 . . 124.1(11) ? N14 C61 H61 . . 117.9 ? C58 C59 H59 . . 120.8 ? C60 C59 C58 . . 118.4(12) ? C60 C59 H59 . . 120.8 ? C59 C60 H60 . . 117.0 ? C59 C60 N14 . . 126.0(11) ? N14 C60 H60 . . 117.0 ? C5S C1S H1S . . 120.0 ? C5S C1S C3S . . 120.0 ? C3S C1S H1S . . 120.0 ? C1S C5S H5S . . 120.0 ? C1S C5S C4S . . 120.0 ? C4S C5S H5S . . 120.0 ? C5S C4S Cl1S . . 122.5(7) ? C2S C4S C5S . . 120.0 ? C2S C4S Cl1S . . 117.4(7) ? C4S C2S H2S . . 120.0 ? C4S C2S C6S . . 120.0 ? C6S C2S H2S . . 120.0 ? C2S C6S H6S . . 120.0 ? C3S C6S C2S . . 120.0 ? C3S C6S H6S . . 120.0 ? C1S C3S H3S . . 120.0 ? C6S C3S C1S . . 120.0 ? C6S C3S H3S . . 120.0 ? C8S C7S Cl2S . . 119.6(9) ? C10S C7S C8S . . 121.9(11) ? C10S C7S Cl2S . . 118.5(10) ? C7S C8S H8S . . 120.1 ? C9S C8S C7S . . 119.8(11) ? C9S C8S H8S . . 120.1 ? C8S C9S H9S . . 119.7 ? C8S C9S C12S . . 120.7(13) ? C12S C9S H9S . . 119.7 ? C7S C10S H10S . . 120.9 ? C7S C10S C11S . . 118.3(11) ? C11S C10S H10S . . 120.9 ? C10S C11S H11S . . 119.9 ? C10S C11S C12S . . 120.2(12) ? C12S C11S H11S . . 119.9 ? C9S C12S C11S . . 118.9(14) ? C9S C12S H12S . . 120.5 ? C11S C12S H12S . . 120.5 ? C21 N5 Mn1 . . 125.6(6) ? C24 N5 Mn1 . . 127.6(6) ? C24 N5 C21 . . 106.6(8) ? C22 N6 H6 . . 125.8 ? C24 N6 C22 . . 108.3(8) ? C24 N6 H6 . . 125.8 ? C31 N7 H7A . . 117.9 ? C32 N7 C31 . . 124.2(7) ? C32 N7 H7A . . 117.9 ? C43 N8 H8A . . 115.8 ? C44 N8 C43 . . 128.4(7) ? C44 N8 H8A . . 115.8 ? C55 N9 H9 . . 117.3 ? C56 N9 C55 . . 125.4(8) ? C56 N9 H9 . . 117.3 ? C67 N10 H10 . . 114.7 ? C68 N10 C67 . . 130.6(7) ? C68 N10 H10 . . 114.7 ? C72 N11 C73 . . 117.8(9) ? C49 N12 C48 . . 116.2(9) ? C36 N13 C37 . . 117.4(12) ? C61 N14 C60 . . 113.5(12) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Mn1 N1 . 2.138(6) y Mn1 N2 . 2.141(6) y Mn1 N3 . 2.141(6) y Mn1 N4 . 2.154(6) y Mn1 N5 . 2.171(8) y N1 C4 . 1.373(9) ? N1 C1 . 1.374(10) ? N2 C19 . 1.379(10) ? N2 C16 . 1.374(10) ? N3 C14 . 1.380(10) ? N3 C11 . 1.389(10) ? N4 C9 . 1.380(10) ? N4 C6 . 1.367(10) ? C4 C3 . 1.467(9) ? C4 C5 . 1.402(10) ? C1 C2 . 1.454(11) ? C1 C20 . 1.406(11) ? C19 C18 . 1.453(10) ? C19 C20 . 1.385(11) ? C16 C17 . 1.459(10) ? C16 C15 . 1.398(11) ? C14 C13 . 1.452(11) ? C14 C15 . 1.406(11) ? C11 C12 . 1.436(11) ? C11 C10 . 1.421(11) ? C9 C8 . 1.455(11) ? C9 C10 . 1.395(11) ? C6 C7 . 1.452(11) ? C6 C5 . 1.416(11) ? C3 H3 . 0.9500 ? C3 C2 . 1.362(11) ? C2 H2 . 0.9500 ? C18 H18 . 0.9500 ? C18 C17 . 1.349(11) ? C17 H17 . 0.9500 ? C13 H13 . 0.9500 ? C13 C12 . 1.352(12) ? C12 H12 . 0.9500 ? C8 H8 . 0.9500 ? C8 C7 . 1.362(12) ? C7 H7 . 0.9500 ? C5 C26 . 1.498(11) ? C20 C62 . 1.499(10) ? C15 C50 . 1.497(11) ? C10 C38 . 1.505(10) ? C38 C43 . 1.409(12) ? C38 C39 . 1.386(12) ? C43 C42 . 1.394(12) ? C43 N8 . 1.427(11) ? C42 H42 . 0.9500 ? C42 C41 . 1.389(14) ? C41 H41 . 0.9500 ? C41 C40 . 1.373(14) ? C40 H40 . 0.9500 ? C40 C39 . 1.392(12) ? C39 H39 . 0.9500 ? C26 C31 . 1.406(11) ? C26 C27 . 1.400(12) ? C31 C30 . 1.393(11) ? C31 N7 . 1.417(11) ? C30 H30 . 0.9500 ? C30 C29 . 1.373(13) ? C29 H29 . 0.9500 ? C29 C28 . 1.397(14) ? C28 H28 . 0.9500 ? C28 C27 . 1.388(12) ? C27 H27 . 0.9500 ? C62 C67 . 1.399(11) ? C62 C63 . 1.391(11) ? C67 C66 . 1.432(11) ? C67 N10 . 1.405(11) ? C66 H66 . 0.9500 ? C66 C65 . 1.385(13) ? C65 H65 . 0.9500 ? C65 C64 . 1.392(14) ? C64 H64 . 0.9500 ? C64 C63 . 1.398(12) ? C63 H63 . 0.9500 ? C50 C55 . 1.409(12) ? C50 C51 . 1.404(12) ? C55 C54 . 1.384(11) ? C55 N9 . 1.417(11) ? C54 H54 . 0.9500 ? C54 C53 . 1.399(14) ? C53 H53 . 0.9500 ? C53 C52 . 1.395(14) ? C52 H52 . 0.9500 ? C52 C51 . 1.382(12) ? C51 H51 . 0.9500 ? C21 H21 . 0.9500 ? C21 C22 . 1.349(15) ? C21 N5 . 1.374(11) ? C22 C23 . 1.515(17) ? C22 N6 . 1.380(13) ? C23 H23A . 0.9800 ? C23 H23B . 0.9800 ? C23 H23C . 0.9800 ? C24 C25 . 1.471(13) ? C24 N5 . 1.347(11) ? C24 N6 . 1.356(12) ? C25 H25A . 0.9800 ? C25 H25B . 0.9800 ? C25 H25C . 0.9800 ? C44 C45 . 1.504(13) ? C44 N8 . 1.336(12) ? C44 O4 . 1.214(12) ? C45 C49 . 1.388(13) ? C45 C46 . 1.371(14) ? C49 H49 . 0.9500 ? C49 N12 . 1.344(12) ? C46 H46 . 0.9500 ? C46 C47 . 1.371(16) ? C47 H47 . 0.9500 ? C47 C48 . 1.361(16) ? C48 H48 . 0.9500 ? C48 N12 . 1.347(14) ? C32 C33 . 1.482(13) ? C32 N7 . 1.349(11) ? C32 O2 . 1.237(11) ? C33 C34 . 1.406(13) ? C33 C37 . 1.371(14) ? C34 H34 . 0.9500 ? C34 C35 . 1.352(15) ? C37 H37 . 0.9500 ? C37 N13 . 1.391(16) ? C35 H35 . 0.9500 ? C35 C36 . 1.376(19) ? C36 H36 . 0.9500 ? C36 N13 . 1.360(18) ? C68 C69 . 1.491(13) ? C68 N10 . 1.341(11) ? C68 O3 . 1.226(12) ? C69 C73 . 1.388(13) ? C69 C70 . 1.386(14) ? C73 H73 . 0.9500 ? C73 N11 . 1.349(12) ? C70 H70 . 0.9500 ? C70 C71 . 1.373(18) ? C71 H71 . 0.9500 ? C71 C72 . 1.396(18) ? C72 H72 . 0.9500 ? C72 N11 . 1.329(14) ? C56 C57 . 1.488(12) ? C56 N9 . 1.350(11) ? C56 O1 . 1.232(11) ? C57 C58 . 1.408(13) ? C57 C61 . 1.365(14) ? C58 H58 . 0.9500 ? C58 C59 . 1.362(15) ? C61 H61 . 0.9500 ? C61 N14 . 1.364(15) ? C59 H59 . 0.9500 ? C59 C60 . 1.33(2) ? C60 H60 . 0.9500 ? C60 N14 . 1.39(2) ? C1S H1S . 0.9500 ? C1S C5S . 1.3900 ? C1S C3S . 1.3900 ? C5S H5S . 0.9500 ? C5S C4S . 1.3900 ? C4S C2S . 1.3900 ? C4S Cl1S . 1.692(8) ? C2S H2S . 0.9500 ? C2S C6S . 1.3900 ? C6S H6S . 0.9500 ? C6S C3S . 1.3900 ? C3S H3S . 0.9500 ? C7S C8S . 1.387(16) ? C7S C10S . 1.360(15) ? C7S Cl2S . 1.740(12) ? C8S H8S . 0.9500 ? C8S C9S . 1.322(19) ? C9S H9S . 0.9500 ? C9S C12S . 1.38(2) ? C10S H10S . 0.9500 ? C10S C11S . 1.366(19) ? C11S H11S . 0.9500 ? C11S C12S . 1.41(2) ? C12S H12S . 0.9500 ? N6 H6 . 0.8800 ? N7 N11 . 3.098(12) ? N8 H8A . 0.8800 ? N9 H9 . 0.8800 ? N10 H10 . 0.8800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N6 H6 O2 2_655 0.88 2.05 2.858(11) 153 N7 H7A N11 . 0.88 2.24 3.094(11) 164 N9 H9 N12 . 0.88 2.17 3.009(10) 159 C5S H5S N14 3_554 0.95 2.57 3.421(16) 150 C36 H36 O3 3_554 0.95 2.35 2.99(2) 124 C60 H60 O4 3_545 0.95 2.40 3.062(18) 126 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Mn1 N1 C4 C3 . . . . 163.1(5) ? Mn1 N1 C4 C5 . . . . -18.4(11) ? Mn1 N1 C1 C2 . . . . -163.2(5) ? Mn1 N1 C1 C20 . . . . 18.9(11) ? Mn1 N2 C19 C18 . . . . 164.8(5) ? Mn1 N2 C19 C20 . . . . -16.6(11) ? Mn1 N2 C16 C17 . . . . -163.8(5) ? Mn1 N2 C16 C15 . . . . 17.8(12) ? Mn1 N3 C14 C13 . . . . 167.0(5) ? Mn1 N3 C14 C15 . . . . -17.1(12) ? Mn1 N3 C11 C12 . . . . -166.6(6) ? Mn1 N3 C11 C10 . . . . 17.3(12) ? Mn1 N4 C9 C8 . . . . 169.2(5) ? Mn1 N4 C9 C10 . . . . -11.9(11) ? Mn1 N4 C6 C7 . . . . -168.4(5) ? Mn1 N4 C6 C5 . . . . 16.3(12) ? N1 C4 C3 C2 . . . . 0.8(9) ? N1 C4 C5 C6 . . . . 1.2(14) ? N1 C4 C5 C26 . . . . -175.0(7) ? N1 C1 C2 C3 . . . . -1.3(9) ? N1 C1 C20 C19 . . . . -2.0(13) ? N1 C1 C20 C62 . . . . 173.4(7) ? N2 C19 C18 C17 . . . . -0.3(10) ? N2 C19 C20 C1 . . . . 0.8(13) ? N2 C19 C20 C62 . . . . -174.5(7) ? N2 C16 C17 C18 . . . . -1.5(10) ? N2 C16 C15 C14 . . . . -1.2(14) ? N2 C16 C15 C50 . . . . 175.9(8) ? N3 C14 C13 C12 . . . . 1.1(10) ? N3 C14 C15 C16 . . . . 0.7(14) ? N3 C14 C15 C50 . . . . -176.3(7) ? N3 C11 C12 C13 . . . . -2.2(10) ? N3 C11 C10 C9 . . . . -4.3(14) ? N3 C11 C10 C38 . . . . 170.1(8) ? N4 C9 C8 C7 . . . . 0.1(9) ? N4 C9 C10 C11 . . . . 1.3(14) ? N4 C9 C10 C38 . . . . -173.1(7) ? N4 C6 C7 C8 . . . . -2.4(10) ? N4 C6 C5 C4 . . . . -0.1(14) ? N4 C6 C5 C26 . . . . 176.2(8) ? C4 N1 C1 C2 . . . . 1.8(9) ? C4 N1 C1 C20 . . . . -176.1(8) ? C4 C3 C2 C1 . . . . 0.3(9) ? C4 C5 C26 C31 . . . . 105.8(9) ? C4 C5 C26 C27 . . . . -73.7(10) ? C1 N1 C4 C3 . . . . -1.6(9) ? C1 N1 C4 C5 . . . . 176.8(8) ? C1 C20 C62 C67 . . . . -68.3(10) ? C1 C20 C62 C63 . . . . 111.7(9) ? C19 N2 C16 C17 . . . . 1.3(9) ? C19 N2 C16 C15 . . . . -177.2(8) ? C19 C18 C17 C16 . . . . 1.0(10) ? C19 C20 C62 C67 . . . . 107.5(9) ? C19 C20 C62 C63 . . . . -72.5(10) ? C16 N2 C19 C18 . . . . -0.6(9) ? C16 N2 C19 C20 . . . . 178.1(8) ? C16 C15 C50 C55 . . . . -65.6(10) ? C16 C15 C50 C51 . . . . 114.0(9) ? C14 N3 C11 C12 . . . . 2.9(9) ? C14 N3 C11 C10 . . . . -173.1(8) ? C14 C13 C12 C11 . . . . 0.7(10) ? C14 C15 C50 C55 . . . . 111.7(9) ? C14 C15 C50 C51 . . . . -68.7(10) ? C11 N3 C14 C13 . . . . -2.5(9) ? C11 N3 C14 C15 . . . . 173.4(8) ? C11 C10 C38 C43 . . . . -68.7(10) ? C11 C10 C38 C39 . . . . 113.0(9) ? C9 N4 C6 C7 . . . . 2.4(9) ? C9 N4 C6 C5 . . . . -172.8(8) ? C9 C8 C7 C6 . . . . 1.3(10) ? C9 C10 C38 C43 . . . . 106.3(9) ? C9 C10 C38 C39 . . . . -72.0(10) ? C6 N4 C9 C8 . . . . -1.6(9) ? C6 N4 C9 C10 . . . . 177.4(8) ? C6 C5 C26 C31 . . . . -70.7(10) ? C6 C5 C26 C27 . . . . 109.7(9) ? C3 C4 C5 C6 . . . . 179.4(8) ? C3 C4 C5 C26 . . . . 3.2(12) ? C2 C1 C20 C19 . . . . -179.6(8) ? C2 C1 C20 C62 . . . . -4.2(12) ? C18 C19 C20 C1 . . . . 179.2(8) ? C18 C19 C20 C62 . . . . 3.9(12) ? C17 C16 C15 C14 . . . . -179.3(8) ? C17 C16 C15 C50 . . . . -2.3(13) ? C13 C14 C15 C16 . . . . 175.9(8) ? C13 C14 C15 C50 . . . . -1.1(12) ? C12 C11 C10 C9 . . . . -179.7(8) ? C12 C11 C10 C38 . . . . -5.3(12) ? C8 C9 C10 C11 . . . . -179.9(8) ? C8 C9 C10 C38 . . . . 5.7(12) ? C7 C6 C5 C4 . . . . -174.7(8) ? C7 C6 C5 C26 . . . . 1.6(12) ? C5 C4 C3 C2 . . . . -177.7(8) ? C5 C6 C7 C8 . . . . 172.9(8) ? C5 C26 C31 C30 . . . . 178.0(8) ? C5 C26 C31 N7 . . . . -1.1(11) ? C5 C26 C27 C28 . . . . -177.3(8) ? C20 C1 C2 C3 . . . . 176.6(8) ? C20 C19 C18 C17 . . . . -179.0(8) ? C20 C62 C67 C66 . . . . 177.8(8) ? C20 C62 C67 N10 . . . . -0.9(11) ? C20 C62 C63 C64 . . . . -176.5(8) ? C15 C16 C17 C18 . . . . 177.0(8) ? C15 C14 C13 C12 . . . . -174.7(8) ? C15 C50 C55 C54 . . . . 178.3(8) ? C15 C50 C55 N9 . . . . -2.7(12) ? C15 C50 C51 C52 . . . . -177.0(8) ? C10 C11 C12 C13 . . . . 173.8(8) ? C10 C9 C8 C7 . . . . -178.8(8) ? C10 C38 C43 C42 . . . . -178.1(8) ? C10 C38 C43 N8 . . . . 1.3(11) ? C10 C38 C39 C40 . . . . 176.8(8) ? C38 C43 C42 C41 . . . . 0.4(13) ? C38 C43 N8 C44 . . . . 159.6(9) ? C43 C38 C39 C40 . . . . -1.6(13) ? C43 C42 C41 C40 . . . . 0.0(14) ? C42 C43 N8 C44 . . . . -21.0(14) ? C42 C41 C40 C39 . . . . -1.2(14) ? C41 C40 C39 C38 . . . . 2.0(13) ? C39 C38 C43 C42 . . . . 0.3(12) ? C39 C38 C43 N8 . . . . 179.7(7) ? C26 C31 C30 C29 . . . . 0.5(13) ? C26 C31 N7 C32 . . . . 118.2(9) ? C31 C26 C27 C28 . . . . 3.1(12) ? C31 C30 C29 C28 . . . . 0.8(14) ? C30 C31 N7 C32 . . . . -61.0(12) ? C30 C29 C28 C27 . . . . -0.1(14) ? C29 C28 C27 C26 . . . . -1.9(13) ? C27 C26 C31 C30 . . . . -2.5(12) ? C27 C26 C31 N7 . . . . 178.4(7) ? C62 C67 C66 C65 . . . . 0.3(13) ? C62 C67 N10 C68 . . . . 158.0(9) ? C67 C62 C63 C64 . . . . 3.5(12) ? C67 C66 C65 C64 . . . . 0.4(14) ? C66 C67 N10 C68 . . . . -20.7(14) ? C66 C65 C64 C63 . . . . 0.8(13) ? C65 C64 C63 C62 . . . . -2.8(13) ? C63 C62 C67 C66 . . . . -2.2(12) ? C63 C62 C67 N10 . . . . 179.2(7) ? C50 C55 C54 C53 . . . . -0.5(13) ? C50 C55 N9 C56 . . . . 128.5(9) ? C55 C50 C51 C52 . . . . 2.6(13) ? C55 C54 C53 C52 . . . . 1.1(14) ? C54 C55 N9 C56 . . . . -52.5(13) ? C54 C53 C52 C51 . . . . 0.1(14) ? C53 C52 C51 C50 . . . . -2.0(13) ? C51 C50 C55 C54 . . . . -1.3(12) ? C51 C50 C55 N9 . . . . 177.7(7) ? C21 C22 N6 C24 . . . . 2.2(12) ? C22 C21 N5 Mn1 . . . . -174.5(7) ? C22 C21 N5 C24 . . . . 0.2(12) ? C23 C22 N6 C24 . . . . -169.7(13) ? C25 C24 N5 Mn1 . . . . -5.7(12) ? C25 C24 N5 C21 . . . . 179.7(9) ? C25 C24 N6 C22 . . . . 179.3(9) ? C44 C45 C49 N12 . . . . 177.9(9) ? C44 C45 C46 C47 . . . . -179.8(11) ? C45 C44 N8 C43 . . . . -168.8(8) ? C45 C49 N12 C48 . . . . 1.5(15) ? C45 C46 C47 C48 . . . . 2(2) ? C49 C45 C46 C47 . . . . -3.7(17) ? C46 C45 C49 N12 . . . . 1.7(15) ? C46 C47 C48 N12 . . . . 1(2) ? C47 C48 N12 C49 . . . . -2.9(18) ? C32 C33 C34 C35 . . . . 177.9(12) ? C32 C33 C37 N13 . . . . 178.1(13) ? C33 C32 N7 C31 . . . . -163.5(8) ? C33 C34 C35 C36 . . . . 0(2) ? C33 C37 N13 C36 . . . . 8(3) ? C34 C33 C37 N13 . . . . -7(2) ? C34 C35 C36 N13 . . . . 0(3) ? C37 C33 C34 C35 . . . . 3(2) ? C35 C36 N13 C37 . . . . -4(3) ? C68 C69 C73 N11 . . . . 174.6(9) ? C68 C69 C70 C71 . . . . -177.9(12) ? C69 C68 N10 C67 . . . . -165.4(9) ? C69 C73 N11 C72 . . . . 3.2(15) ? C69 C70 C71 C72 . . . . 3(2) ? C73 C69 C70 C71 . . . . -2.0(18) ? C70 C69 C73 N11 . . . . -1.2(15) ? C70 C71 C72 N11 . . . . -1(2) ? C71 C72 N11 C73 . . . . -2.0(17) ? C56 C57 C58 C59 . . . . 175.9(11) ? C56 C57 C61 N14 . . . . 179.8(12) ? C57 C56 N9 C55 . . . . -164.5(8) ? C57 C58 C59 C60 . . . . 2(2) ? C57 C61 N14 C60 . . . . 6(2) ? C58 C57 C61 N14 . . . . -3.9(18) ? C58 C59 C60 N14 . . . . 1(3) ? C61 C57 C58 C59 . . . . -0.4(17) ? C59 C60 N14 C61 . . . . -5(3) ? C1S C5S C4S C2S . . . . 0.0 ? C1S C5S C4S Cl1S . . . . 177.2(8) ? C5S C1S C3S C6S . . . . 0.0 ? C5S C4S C2S C6S . . . . 0.0 ? C4S C2S C6S C3S . . . . 0.0 ? C2S C6S C3S C1S . . . . 0.0 ? C3S C1S C5S C4S . . . . 0.0 ? C7S C8S C9S C12S . . . . -5(2) ? C7S C10S C11S C12S . . . . 2(2) ? C8S C7S C10S C11S . . . . -3.5(18) ? C8S C9S C12S C11S . . . . 3(3) ? C10S C7S C8S C9S . . . . 4.8(17) ? C10S C11S C12S C9S . . . . -2(3) ? Cl1S C4S C2S C6S . . . . -177.3(7) ? Cl2S C7S C8S C9S . . . . -175.1(10) ? Cl2S C7S C10S C11S . . . . 176.5(10) ? N5 C21 C22 C23 . . . . 169.6(14) ? N5 C21 C22 N6 . . . . -1.5(13) ? N5 C24 N6 C22 . . . . -2.1(10) ? N6 C24 N5 Mn1 . . . . 175.8(5) ? N6 C24 N5 C21 . . . . 1.2(10) ? N7 C31 C30 C29 . . . . 179.6(8) ? N7 C32 C33 C34 . . . . 37.1(14) ? N7 C32 C33 C37 . . . . -148.0(11) ? N8 C43 C42 C41 . . . . -179.0(8) ? N8 C44 C45 C49 . . . . 34.5(13) ? N8 C44 C45 C46 . . . . -149.5(10) ? N9 C55 C54 C53 . . . . -179.5(8) ? N9 C56 C57 C58 . . . . 36.3(13) ? N9 C56 C57 C61 . . . . -147.5(10) ? N10 C67 C66 C65 . . . . 178.9(8) ? N10 C68 C69 C73 . . . . 39.6(13) ? N10 C68 C69 C70 . . . . -144.7(11) ? O1 C56 C57 C58 . . . . -140.0(10) ? O1 C56 C57 C61 . . . . 36.2(14) ? O1 C56 N9 C55 . . . . 11.7(15) ? O2 C32 C33 C34 . . . . -139.0(11) ? O2 C32 C33 C37 . . . . 35.9(16) ? O2 C32 N7 C31 . . . . 12.6(15) ? O3 C68 C69 C73 . . . . -138.5(12) ? O3 C68 C69 C70 . . . . 37.2(17) ? O3 C68 N10 C67 . . . . 12.7(18) ? O4 C44 C45 C49 . . . . -145.3(11) ? O4 C44 C45 C46 . . . . 30.7(16) ? O4 C44 N8 C43 . . . . 11.0(17) ? loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.59(4) 2 0.41(4)