#------------------------------------------------------------------------------ #$Date: 2024-06-07 01:15:37 +0300 (Fri, 07 Jun 2024) $ #$Revision: 292232 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571783.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571783 loop_ _publ_author_name 'Qu, Chulin' 'Gong, Xinxin' 'Sun, Yufen' 'Gao, Hu' 'Cai, Fangjian' 'Zhao, Yue' 'Wu, Fan' 'Shen, Zhen' _publ_section_title ; Synergistic meso-\b regulation of porphyrin: squeezing the band gap into near-infrared I/II region ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC01806K _journal_year 2024 _chemical_formula_moiety 'C96 H108 N4 Pt Si4' _chemical_formula_sum 'C96 H108 N4 Pt Si4' _chemical_formula_weight 1625.31 _space_group_crystal_system tetragonal _space_group_IT_number 88 _space_group_name_Hall '-I 4ad' _space_group_name_H-M_alt 'I 41/a :2' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_block_doi 10.5517/ccdc.csd.cc2g1btp _audit_creation_date 2022-09-17 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _audit_update_record ; 2023-05-25 deposited with the CCDC. 2024-06-03 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 19.3505(3) _cell_length_b 19.3505(3) _cell_length_c 21.7466(5) _cell_measurement_reflns_used 9949 _cell_measurement_temperature 193.00 _cell_measurement_theta_max 59.56 _cell_measurement_theta_min 3.97 _cell_volume 8142.8(3) _computing_cell_refinement 'SAINT V8.40B (Bruker, 2019)' _computing_data_collection 'APEX4 V2022.1-1 (Bruker, 2022)' _computing_data_reduction 'SAINT V8.40B (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/2 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 193.00 _diffrn_detector CPAD _diffrn_detector_area_resol_mean 7.41 _diffrn_detector_type 'Bruker PHOTON II' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE Metaljet PHOTON II' _diffrn_measurement_method '\w and \f shutterless scans' _diffrn_measurement_specimen_support 'nylon loop' _diffrn_radiation_monochromator 'Helios Multi-layer Optic' _diffrn_radiation_probe x-ray _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0422 _diffrn_reflns_av_unetI/netI 0.0179 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 51232 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 59.870 _diffrn_reflns_theta_min 2.659 _diffrn_source MetalJet _diffrn_source_current 2.86 _diffrn_source_power 0.19937059999999998 _diffrn_source_type 'Liquid Metal source' _diffrn_source_voltage 69.71 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.824 _exptl_absorpt_correction_T_max 0.3096 _exptl_absorpt_correction_T_min 0.2148 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0785 before and 0.0500 after correction. The Ratio of minimum to maximum transmission is 0.6938. The \l/2 correction factor is Not present. ; _exptl_crystal_density_diffrn 1.326 _exptl_crystal_description block _exptl_crystal_F_000 3384 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.409 _refine_diff_density_min -0.529 _refine_diff_density_rms 0.053 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 243 _refine_ls_number_reflns 4536 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.054 _refine_ls_R_factor_all 0.0236 _refine_ls_R_factor_gt 0.0207 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0275P)^2^+9.1472P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0534 _refine_ls_wR_factor_ref 0.0546 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4195 _reflns_number_total 4536 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc01806k2.cif _cod_data_source_block 20220916syf_0m _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_radiation_probe' value 'X-ray' was changed to 'x-ray' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas ; _cod_original_sg_symbol_H-M 'I 41/a' _cod_database_code 1571783 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.765 _shelx_estimated_absorpt_t_min 0.710 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C22(H22), C19(H19), C16(H16) 2.b Aromatic/amide H refined with riding coordinates: C3(H3), C10(H10), C8(H8), C5(H5), C6(H6), C7(H7) 2.c Idealised Me refined as rotating group: C20(H20A,H20B,H20C), C23(H23A,H23B,H23C), C24(H24A,H24B,H24C), C21(H21A,H21B, H21C), C18(H18A,H18B,H18C), C17(H17A,H17B,H17C) ; _shelx_res_file ; TITL 20220916syf_0m_a.res in I4(1)/a 20220916syf_0m.res created by SHELXL-2019/2 at 15:34:35 on 17-Sep-2022 REM Old TITL 20220916syf_0m in I4(1)/a REM SHELXT solution in I4(1)/a: R1 0.079, Rweak 0.005, Alpha 0.016 REM 0.856 for 122 systematic absences, Orientation as input REM Formula found by SHELXT: C92 N4 O4 Si4 Pt CELL 1.34139 19.3505 19.3505 21.7466 90 90 90 ZERR 4 0.0003 0.0003 0.0005 0 0 0 LATT 2 SYMM 0.5-X,-Y,0.5+Z SYMM 0.75-Y,0.25+X,0.25+Z SYMM 0.75+Y,0.75-X,0.75+Z SFAC C H N Pt Si DISP C 0.0137 0.0067 57.1 DISP H 0 0 0.6 DISP N 0.0241 0.0134 109.9 DISP Pt -5.3886 5.5592 43704.6 DISP Si 0.2153 0.2529 1947.9 UNIT 384 432 16 4 16 L.S. 10 PLAN 5 SIZE 0.1 0.12 0.13 TEMP -80.15 CONF BOND list 4 MORE -1 BOND $H fmap 2 acta SIZE 0.1 0.12 0.13 TEMP -80.15 REM REM REM WGHT 0.027500 9.147201 FVAR 0.18405 PT1 4 0.500000 0.750000 0.625000 10.25000 0.01546 0.01546 = 0.02793 0.00000 0.00000 0.00000 SI1 5 0.136325 0.605359 0.540179 11.00000 0.02057 0.02894 = 0.03612 -0.00185 -0.00597 -0.00243 N1 3 0.469395 0.651299 0.616944 11.00000 0.01702 0.01830 = 0.02821 0.00034 -0.00087 -0.00002 C1 1 0.512146 0.594816 0.618777 11.00000 0.02054 0.01499 = 0.02899 0.00124 0.00087 0.00074 C11 1 0.407611 0.558803 0.579484 11.00000 0.02018 0.01908 = 0.03033 -0.00041 -0.00003 0.00132 C4 1 0.447680 0.423199 0.553590 11.00000 0.02605 0.02015 = 0.02948 -0.00142 0.00098 0.00064 C13 1 0.345272 0.671226 0.605611 11.00000 0.01858 0.01886 = 0.02885 0.00038 -0.00235 -0.00065 C2 1 0.475329 0.535506 0.594135 11.00000 0.02001 0.01971 = 0.02911 0.00098 -0.00032 -0.00074 C3 1 0.495449 0.469032 0.580630 11.00000 0.02216 0.02032 = 0.03640 -0.00126 -0.00180 0.00213 AFIX 43 H3 2 0.541165 0.454138 0.589457 11.00000 -1.20000 AFIX 0 C9 1 0.379658 0.446246 0.539645 11.00000 0.02529 0.02158 = 0.03278 -0.00256 -0.00098 0.00007 C14 1 0.279607 0.643060 0.587430 11.00000 0.02099 0.01899 = 0.03216 -0.00236 -0.00093 0.00251 C10 1 0.360430 0.515046 0.552813 11.00000 0.02191 0.02182 = 0.03897 -0.00402 -0.00379 0.00155 AFIX 43 H10 2 0.315229 0.530953 0.543307 11.00000 -1.20000 AFIX 0 C12 1 0.404673 0.631093 0.597733 11.00000 0.01842 0.01796 = 0.02835 -0.00015 -0.00232 -0.00244 C8 1 0.332584 0.398829 0.512688 11.00000 0.02819 0.02729 = 0.04231 -0.00843 -0.00399 0.00033 AFIX 43 H8 2 0.287081 0.413641 0.502927 11.00000 -1.20000 AFIX 0 C15 1 0.224308 0.622698 0.569459 11.00000 0.02359 0.02519 = 0.03747 -0.00375 -0.00230 0.00066 C5 1 0.466005 0.353859 0.539138 11.00000 0.02916 0.02199 = 0.03798 -0.00332 -0.00143 0.00480 AFIX 43 H5 2 0.511562 0.338038 0.547320 11.00000 -1.20000 AFIX 0 C6 1 0.419083 0.309918 0.513739 11.00000 0.03753 0.01970 = 0.03607 -0.00478 0.00152 0.00180 AFIX 43 H6 2 0.432002 0.263630 0.504805 11.00000 -1.20000 AFIX 0 C7 1 0.351577 0.332564 0.500618 11.00000 0.03385 0.02471 = 0.03857 -0.00843 -0.00266 -0.00433 AFIX 43 H7 2 0.319089 0.301373 0.483228 11.00000 -1.20000 AFIX 0 C22 1 0.130837 0.516870 0.503926 11.00000 0.03306 0.03624 = 0.04113 -0.00673 -0.00539 -0.00719 AFIX 13 H22 2 0.081926 0.510955 0.490043 11.00000 -1.20000 AFIX 0 C19 1 0.074071 0.614198 0.606450 11.00000 0.02530 0.04005 = 0.04211 -0.00735 -0.00276 -0.00206 AFIX 13 H19 2 0.067737 0.664812 0.613825 11.00000 -1.20000 AFIX 0 C20 1 0.100222 0.582885 0.666950 11.00000 0.04013 0.04309 = 0.04360 -0.00010 0.00285 -0.00407 AFIX 137 H20A 2 0.103698 0.532589 0.662668 11.00000 -1.50000 H20B 2 0.067841 0.594077 0.700137 11.00000 -1.50000 H20C 2 0.145832 0.601989 0.676687 11.00000 -1.50000 AFIX 0 C16 1 0.122301 0.673129 0.479445 11.00000 0.03692 0.04137 = 0.05229 0.01000 -0.00858 0.00110 AFIX 13 H16 2 0.162114 0.669045 0.450353 11.00000 -1.20000 AFIX 0 C23 1 0.175695 0.510406 0.446654 11.00000 0.05965 0.05014 = 0.04151 -0.00732 0.00123 0.00403 AFIX 137 H23A 2 0.160899 0.544519 0.416058 11.00000 -1.50000 H23B 2 0.170923 0.463825 0.429486 11.00000 -1.50000 H23C 2 0.224123 0.518717 0.457573 11.00000 -1.50000 AFIX 0 C24 1 0.145548 0.457912 0.548473 11.00000 0.06771 0.03182 = 0.05684 0.00069 0.00755 -0.00298 AFIX 137 H24A 2 0.191200 0.464514 0.567078 11.00000 -1.50000 H24B 2 0.144649 0.413892 0.526203 11.00000 -1.50000 H24C 2 0.110258 0.457404 0.580792 11.00000 -1.50000 AFIX 0 C21 1 0.002355 0.584597 0.590596 11.00000 0.02686 0.10214 = 0.05583 -0.01954 0.00277 -0.01508 AFIX 137 H21A 2 -0.014550 0.605876 0.552570 11.00000 -1.50000 H21B 2 -0.029892 0.594606 0.624184 11.00000 -1.50000 H21C 2 0.005881 0.534475 0.584949 11.00000 -1.50000 AFIX 0 C18 1 0.057023 0.662593 0.440815 11.00000 0.05725 0.06412 = 0.06800 0.01428 -0.02758 0.00385 AFIX 137 H18A 2 0.057121 0.615882 0.423402 11.00000 -1.50000 H18B 2 0.056022 0.696607 0.407439 11.00000 -1.50000 H18C 2 0.016133 0.668543 0.466870 11.00000 -1.50000 AFIX 0 C17 1 0.125165 0.746307 0.505209 11.00000 0.08688 0.03858 = 0.09408 0.01587 -0.03165 0.00044 AFIX 137 H17A 2 0.085825 0.753742 0.532806 11.00000 -1.50000 H17B 2 0.123165 0.779623 0.471315 11.00000 -1.50000 H17C 2 0.168348 0.752617 0.528074 11.00000 -1.50000 AFIX 0 HKLF 4 REM 20220916syf_0m_a.res in I4(1)/a REM wR2 = 0.0546, GooF = S = 1.054, Restrained GooF = 1.054 for all data REM R1 = 0.0207 for 4195 Fo > 4sig(Fo) and 0.0236 for all 4536 data REM 243 parameters refined using 0 restraints END WGHT 0.0275 9.1526 REM Highest difference peak 0.409, deepest hole -0.529, 1-sigma level 0.053 Q1 1 0.4841 0.6838 0.6228 11.00000 0.05 0.41 Q2 1 0.1310 0.6475 0.5219 11.00000 0.05 0.40 Q3 1 0.4787 0.8007 0.5954 11.00000 0.05 0.37 Q4 1 0.5467 0.7802 0.5962 11.00000 0.05 0.34 Q5 1 0.4595 0.3883 0.5458 11.00000 0.05 0.33 ; _shelx_res_checksum 24766 _shelx_hkl_file ; 1 1 0 0.50 0.60 1 1 0 1.00 2.10 -1 1 0 0.80 0.90 -1 -1 0 1.30 0.70 0 2 0 2696.63 86.09 0 2 0 2789.92 85.89 2 0 0 2624.64 86.19 0 -2 0 2708.53 85.89 -2 0 0 2642.34 83.49 2 0 0 2685.73 83.59 -2 2 0 936.21 32.70 2 2 0 957.90 31.50 -2 -2 0 975.50 31.60 2 2 0 914.11 35.00 3 1 0 6.50 4.20 -1 3 0 -0.10 2.20 1 -3 0 0.90 2.30 -3 1 0 0.20 1.30 -1 -3 0 0.50 2.10 1 3 0 -1.00 1.90 1 3 0 -0.10 4.00 3 -1 0 6.80 3.10 3 -1 0 -0.90 1.20 3 3 0 -3.00 5.40 -3 -3 0 -0.90 1.80 -3 3 0 1.20 2.70 3 -3 0 -2.60 2.80 3 3 0 -2.30 1.60 3 -3 0 1.10 4.40 3 -3 0 6.50 2.30 -4 -2 0 2888.61 89.09 -2 4 0 2885.11 94.39 2 -4 0 2742.73 94.39 4 2 0 2858.71 97.09 4 2 0 2852.11 88.99 0 4 0 1762.42 59.49 4 0 0 1644.84 59.39 4 0 0 1749.03 54.09 -4 0 0 1762.72 53.89 0 4 0 1750.72 58.79 0 -4 0 1614.64 58.59 2 4 0 657.93 24.60 4 -2 0 607.94 23.60 -4 2 0 617.34 23.50 4 -2 0 607.54 24.10 -2 -4 0 625.34 24.60 2 4 0 654.33 28.40 4 -4 0 352.96 13.70 4 -4 0 328.97 14.80 4 4 0 397.76 22.80 -4 -4 0 358.76 15.60 -4 4 0 398.46 18.40 4 -4 0 299.17 19.80 4 -4 0 363.16 13.20 4 4 0 378.16 15.40 -3 5 0 5.10 4.40 3 -5 0 1.20 4.20 5 3 0 13.80 7.50 5 3 0 1.40 1.50 -3 5 0 4.40 1.60 5 3 0 1.50 1.70 -5 -3 0 2.80 1.80 1 -5 0 3.90 4.20 5 1 0 5.00 6.30 -1 5 0 5.20 4.10 1 5 0 0.00 3.40 1 5 0 -1.50 5.90 5 -1 0 -1.10 4.90 5 -1 0 2.30 2.10 -1 -5 0 3.70 3.80 -5 1 0 0.30 1.70 5 -3 0 3.80 4.70 -3 -5 0 6.20 3.70 3 5 0 0.00 2.90 5 -3 0 5.00 3.70 3 5 0 -8.60 6.30 -5 3 0 -5.70 3.00 5 -5 0 0.50 1.50 -5 5 0 2.90 4.70 5 -5 0 5.50 4.40 -5 -5 0 -2.30 3.30 5 5 0 6.40 8.10 5 5 0 5.90 2.50 5 -5 0 0.00 5.30 -5 5 0 -0.20 1.30 5 5 0 1.20 1.70 5 5 0 0.00 3.10 6 4 0 2040.90 76.79 4 -6 0 2017.10 72.39 6 4 0 2004.60 64.29 6 4 0 1840.62 64.69 6 4 0 1900.81 63.89 -6 -4 0 2014.40 64.49 -4 6 0 2062.49 72.09 -4 6 0 1977.70 63.69 6 2 0 1288.27 44.50 2 -6 0 1464.15 52.79 -2 6 0 1438.76 52.29 -2 6 0 1336.07 44.50 6 2 0 1332.87 54.29 2 -6 0 1353.16 44.40 0 -6 0 3803.52 129.49 6 0 0 4065.69 121.19 6 0 0 3833.52 130.29 0 6 0 4008.00 130.19 6 0 0 3767.52 122.89 0 6 0 4087.99 129.79 0 -6 0 3735.93 122.19 -6 2 0 677.13 22.00 6 -2 0 667.73 25.90 -6 2 0 627.24 22.10 6 -2 0 670.13 28.80 6 -2 0 658.83 23.70 2 6 0 687.53 28.70 -2 -6 0 661.33 28.80 -6 2 0 738.93 25.60 -2 -6 0 657.13 22.70 6 -2 0 634.74 24.10 2 6 0 656.73 24.70 2 6 0 752.92 33.50 6 -4 0 3019.00 98.59 -6 4 0 2926.11 97.59 -4 -6 0 2917.01 97.59 6 -4 0 2839.42 95.39 -4 -6 0 2866.81 91.29 4 6 0 2819.32 92.29 -6 4 0 2939.81 91.59 6 -4 0 2782.32 93.49 4 6 0 2888.81 93.69 4 6 0 2945.71 96.99 6 -4 0 2834.42 92.59 4 6 0 3084.39 106.09 6 6 0 646.64 23.10 6 -6 0 554.94 34.90 -6 -6 0 662.23 27.30 6 -6 0 626.24 22.90 -6 -6 0 616.34 21.40 -6 6 0 631.14 22.40 -6 6 0 707.63 31.40 6 6 0 623.44 24.20 6 6 0 649.43 26.30 6 6 0 664.83 36.90 6 -6 0 605.84 23.70 7 5 0 -0.60 2.30 -5 7 0 1.50 1.80 7 5 0 -6.00 9.40 -7 -5 0 -2.60 3.50 7 5 0 1.80 1.90 5 -7 0 2.80 4.40 5 -7 0 3.60 1.90 7 5 0 -3.30 3.10 7 5 0 -0.40 1.70 5 -7 0 13.20 8.10 -5 7 0 -3.20 7.10 5 -7 0 4.00 1.90 5 -7 0 1.40 7.80 -3 7 0 -2.10 6.40 7 3 0 0.20 2.10 3 -7 0 0.80 1.50 3 -7 0 4.50 6.90 7 3 0 6.70 8.90 7 3 0 0.90 1.70 -3 7 0 -0.90 1.50 7 3 0 4.60 2.00 7 1 0 -12.30 7.30 7 1 0 0.80 1.70 7 1 0 0.20 1.40 1 -7 0 0.70 1.50 -1 7 0 -2.20 1.30 1 -7 0 -3.40 5.70 -1 7 0 -1.90 5.50 7 1 0 -2.10 1.90 7 -1 0 4.40 2.00 -7 1 0 4.70 2.20 7 -1 0 1.90 2.10 7 -1 0 1.10 2.60 -1 -7 0 5.40 5.80 -1 -7 0 1.40 1.50 1 7 0 0.20 5.20 1 7 0 0.40 7.90 7 -1 0 -4.60 6.40 -7 3 0 0.60 3.80 7 -3 0 3.20 2.40 3 7 0 1.80 5.00 -3 -7 0 0.30 1.30 3 7 0 7.50 3.50 7 -3 0 -8.20 6.60 -7 3 0 0.90 1.20 3 7 0 2.30 1.60 3 7 0 19.70 9.50 7 -3 0 -1.70 4.30 7 -3 0 -0.80 1.80 -3 -7 0 6.60 5.80 5 7 0 10.80 5.50 7 -5 0 2.60 2.40 -5 -7 0 3.70 1.40 5 7 0 3.90 3.10 7 -5 0 4.60 6.50 7 -5 0 -7.40 6.40 -7 5 0 -0.20 1.50 5 7 0 -2.00 1.60 -7 5 0 4.60 5.80 7 -5 0 1.10 2.00 -5 -7 0 -6.50 5.80 5 7 0 0.00 10.10 -7 7 0 4.80 1.90 -7 7 0 -4.10 8.30 7 -7 0 5.10 2.20 7 7 0 -1.50 5.70 7 -7 0 -0.90 1.80 -7 -7 0 -0.30 1.20 7 7 0 2.50 12.30 7 7 0 -2.10 6.30 -7 -7 0 -2.80 5.90 7 7 0 3.60 2.20 -8 -6 0 846.12 29.20 6 -8 0 865.41 31.00 -6 8 0 962.10 31.60 -8 -6 0 926.21 32.90 8 6 0 858.21 30.70 8 6 0 935.81 49.60 6 -8 0 822.42 32.50 -6 8 0 956.40 42.70 8 6 0 903.81 32.90 8 6 0 893.81 31.70 6 -8 0 850.61 44.30 6 -8 0 913.91 30.90 4 -8 0 1663.33 67.79 -4 8 0 1753.02 56.49 8 4 0 1765.82 72.59 -4 8 0 1827.72 67.69 4 -8 0 1742.03 56.09 8 4 0 1701.83 57.59 8 4 0 1639.54 56.19 8 4 0 1641.14 56.39 2 -8 0 27.40 9.20 -2 8 0 29.50 3.70 2 -8 0 25.90 3.40 -2 8 0 27.90 9.00 8 2 0 31.30 3.40 8 2 0 30.20 11.30 8 2 0 37.40 4.90 8 2 0 32.40 4.10 0 8 0 6815.42 210.08 8 0 0 6344.87 201.08 0 -8 0 6379.86 199.38 0 -8 0 6484.45 210.38 8 0 0 6172.28 200.28 8 0 0 6435.26 210.98 0 8 0 6384.06 199.68 8 0 0 6062.99 199.18 -2 -8 0 693.03 24.90 8 -2 0 620.34 32.60 2 8 0 719.83 25.50 -8 2 0 753.62 25.60 2 8 0 720.13 33.30 8 -2 0 706.03 26.10 2 8 0 692.63 24.90 -2 -8 0 733.43 34.20 -8 2 0 760.32 27.40 2 8 0 767.42 38.00 8 -2 0 716.43 26.80 8 -2 0 742.33 28.30 8 -4 0 2101.79 75.59 8 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7.10 14 2 0 62.69 24.90 14 2 0 64.29 6.50 -2 14 0 71.29 6.50 14 0 0 3797.22 146.59 0 14 0 3567.14 120.09 0 -14 0 3823.72 122.69 14 0 0 3749.52 122.29 0 14 0 3717.13 122.79 14 0 0 3962.60 126.09 14 0 0 3917.31 124.59 2 14 0 2004.30 65.89 14 -2 0 2024.40 67.99 -14 2 0 1841.12 62.59 -2 -14 0 1984.10 65.89 14 -2 0 1922.21 64.79 2 14 0 1930.31 64.49 14 -2 0 2012.20 69.19 14 -2 0 1848.22 85.89 -14 4 0 130.79 7.30 -4 -14 0 142.09 8.70 14 -4 0 150.28 8.30 14 -4 0 144.49 11.10 14 -4 0 159.88 28.40 4 14 0 127.79 8.20 14 -4 0 127.49 9.90 14 -6 0 1718.03 61.79 -6 -14 0 1775.72 59.59 6 14 0 1688.53 59.69 -14 6 0 1729.13 58.39 14 -6 0 1819.52 64.59 14 -8 0 1448.06 52.29 8 14 0 1450.85 50.89 -14 8 0 1414.36 49.50 14 -8 0 1412.66 54.89 -8 -14 0 1400.26 49.40 10 14 0 24.90 34.90 14 -10 0 41.00 6.90 -14 10 0 44.40 6.00 -10 -14 0 39.60 5.30 14 -10 0 53.39 9.00 10 14 0 51.99 7.00 12 14 0 1203.08 44.70 -12 -14 0 1034.80 93.49 -12 -14 0 1227.38 41.80 14 -12 0 1137.79 44.10 -14 12 0 1146.49 43.50 14 -12 0 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35.10 25.30 1 15 0 -5.80 3.10 -1 -15 0 2.20 2.60 -15 3 0 2.60 2.10 3 15 0 1.10 4.40 3 15 0 2.70 2.50 15 -3 0 -0.60 3.50 15 -3 0 -8.00 2.70 -3 -15 0 0.80 2.30 15 -3 0 0.10 2.90 15 -3 0 2.30 27.00 -15 5 0 -1.50 2.00 -5 -15 0 2.20 2.40 15 -5 0 -1.00 3.00 15 -5 0 -4.30 3.70 5 15 0 3.70 2.60 -7 -15 0 1.80 2.10 7 15 0 5.30 3.20 -15 7 0 3.10 2.10 15 -7 0 6.00 4.60 15 -7 0 8.10 4.00 15 -9 0 -0.20 4.20 -15 9 0 -0.60 2.60 15 -9 0 1.40 3.50 9 15 0 -4.90 2.90 -9 -15 0 -0.30 2.30 -15 11 0 -0.40 3.20 -11 -15 0 23.30 42.80 -11 -15 0 1.80 2.50 11 15 0 2.10 3.50 15 -11 0 -1.90 5.00 15 -11 0 3.30 3.90 15 -13 0 9.50 4.50 15 -13 0 3.90 5.50 -13 -15 0 -10.20 48.30 13 15 0 0.80 3.40 -13 -15 0 1.90 3.10 -15 13 0 -1.90 3.20 15 -15 0 0.50 5.80 15 15 0 4.80 4.00 -15 15 0 -1.30 3.20 16 14 0 809.52 32.50 -14 16 0 736.93 31.60 14 -16 0 752.92 35.40 16 12 0 651.23 77.89 12 -16 0 674.73 32.00 -12 16 0 633.04 27.90 16 12 0 615.54 38.10 16 12 0 650.23 28.50 -16 -12 0 547.85 80.79 -10 16 0 161.88 11.70 16 10 0 173.38 46.40 16 10 0 149.69 24.70 16 10 0 163.78 11.90 10 -16 0 153.48 14.00 -16 -10 0 102.19 54.49 16 8 0 817.52 73.69 16 8 0 819.32 33.00 8 -16 0 831.12 36.00 -8 16 0 788.42 32.50 8 -16 0 775.82 31.10 -16 -8 0 743.63 81.59 16 8 0 817.42 45.80 16 8 0 760.22 31.10 16 6 0 366.36 51.99 16 6 0 355.76 18.40 -6 16 0 346.17 18.20 6 -16 0 371.86 17.60 16 6 0 355.26 18.00 16 6 0 380.96 20.10 -16 -6 0 414.06 57.89 -16 -4 0 984.00 78.89 -4 16 0 994.30 38.60 16 4 0 1018.90 39.20 16 4 0 1022.20 41.00 4 -16 0 1049.49 38.20 16 4 0 996.40 38.50 16 4 0 937.51 69.69 16 2 0 163.58 11.70 16 2 0 164.78 10.90 16 2 0 161.18 12.60 -2 16 0 178.18 11.30 16 2 0 157.48 35.20 2 -16 0 163.48 10.50 2 -16 0 144.09 39.60 16 0 0 301.27 16.30 0 -16 0 297.07 14.90 16 0 0 279.87 17.00 16 0 0 229.58 38.80 0 -16 0 372.66 53.09 16 0 0 290.27 14.70 0 16 0 275.17 14.90 -2 -16 0 350.16 16.50 16 -2 0 311.67 18.60 16 -2 0 325.87 15.40 2 16 0 347.77 16.50 16 -2 0 278.27 41.50 16 -2 0 360.56 18.30 2 16 0 315.77 14.50 16 -4 0 447.76 22.00 4 16 0 453.95 19.10 -4 -16 0 446.46 20.00 -16 4 0 431.66 17.50 16 -4 0 470.75 23.90 6 16 0 292.17 14.50 -6 -16 0 292.37 14.70 16 -6 0 294.57 18.50 -16 6 0 254.27 12.70 16 -6 0 289.47 16.90 -8 -16 0 83.99 7.70 16 -8 0 93.99 9.80 8 16 0 99.39 8.60 16 -8 0 98.89 11.30 -16 8 0 96.39 7.70 -10 -16 0 610.74 24.90 16 -10 0 647.14 30.90 16 -10 0 602.44 27.30 -10 -16 0 512.45 72.09 -16 10 0 604.34 25.20 10 16 0 624.24 26.50 -12 -16 0 703.83 27.90 -16 12 0 736.53 29.60 16 -12 0 746.33 34.70 12 16 0 711.93 30.10 16 -12 0 736.63 30.60 -12 -16 0 586.74 77.69 16 -14 0 491.25 23.10 16 -14 0 521.95 27.40 -16 14 0 500.05 22.90 14 16 0 518.15 23.90 -14 -16 0 512.55 20.70 16 16 0 280.87 16.40 -16 16 0 266.77 15.90 16 -16 0 278.17 20.00 -15 17 0 5.50 5.10 17 15 0 3.90 5.30 15 -17 0 -2.10 7.40 17 13 0 1.60 4.00 -13 17 0 7.60 4.20 13 -17 0 -8.00 5.30 17 11 0 9.60 17.50 17 11 0 41.40 49.40 -17 -11 0 51.19 60.59 -17 -9 0 100.89 58.29 17 9 0 20.70 24.20 17 9 0 -10.80 41.70 9 -17 0 4.10 4.70 17 7 0 12.20 38.80 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168.08 12.90 20 4 0 134.79 65.69 -4 20 0 179.08 13.00 20 4 0 200.78 14.60 4 -20 0 190.18 12.30 20 4 0 182.88 13.40 -2 20 0 586.24 27.20 20 2 0 609.64 29.70 20 2 0 672.13 29.00 2 -20 0 641.74 27.10 20 2 0 374.96 77.99 20 2 0 630.94 27.00 20 0 0 509.75 23.30 0 -20 0 409.36 83.79 0 -20 0 561.14 24.40 20 0 0 530.55 26.80 20 0 0 561.54 26.20 -2 -20 0 322.07 17.00 20 -2 0 293.57 19.50 -2 -20 0 285.47 68.59 20 -2 0 334.97 18.90 20 -4 0 772.52 35.90 -4 -20 0 643.14 82.49 -4 -20 0 800.82 32.30 20 -4 0 835.22 34.80 -6 -20 0 592.84 25.20 20 -6 0 568.34 29.10 20 -6 0 562.04 27.20 -20 8 0 295.67 14.40 20 -8 0 276.87 19.60 -8 -20 0 289.27 15.60 20 -8 0 331.97 18.40 8 20 0 309.47 15.60 -20 10 0 174.18 11.50 10 20 0 190.28 12.50 20 -10 0 213.68 17.20 20 -10 0 220.68 14.70 -10 -20 0 214.28 12.30 20 -12 0 344.97 18.60 -12 -20 0 353.46 16.30 12 20 0 335.67 17.40 -20 12 0 328.97 16.60 20 -12 0 373.96 23.40 20 -14 0 220.18 18.80 -13 21 0 -4.50 5.70 13 -21 0 1.40 8.00 21 13 0 0.70 5.70 21 11 0 -1.00 6.40 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1276.67 43.50 9 8 -3 1305.77 44.00 8 -9 -3 1223.48 42.20 9 8 -3 1193.58 42.30 8 -9 -3 1260.27 43.50 9 8 -3 1359.06 68.89 -9 -8 -3 1253.37 41.30 -8 9 3 1302.47 62.09 8 -9 3 1210.78 42.20 -9 -8 3 1312.47 71.59 -9 -8 3 1262.47 41.60 9 8 3 1281.27 48.10 8 -9 3 1288.07 46.20 -9 -8 3 1276.57 52.79 8 -9 3 1158.58 61.79 9 8 3 1251.57 66.79 -8 9 3 1192.98 43.10 9 8 3 1271.37 44.10 8 -9 3 1311.47 43.80 8 -9 3 1174.58 51.69 9 8 3 1175.18 42.10 9 6 -3 67.39 5.70 -6 9 -3 81.09 5.80 -9 -6 -3 66.19 4.20 9 6 -3 58.19 18.10 9 6 -3 82.39 6.30 6 -9 -3 75.39 5.40 9 6 -3 63.69 6.30 6 -9 -3 61.39 17.70 -9 -6 -3 73.79 7.00 -6 9 -3 53.79 14.60 6 -9 -3 66.09 5.30 -9 -6 3 74.29 4.30 6 -9 3 79.09 5.70 -9 -6 3 98.29 11.90 9 6 3 77.99 19.20 -9 -6 3 81.79 10.00 6 -9 3 106.89 18.80 -6 9 3 73.69 5.60 6 -9 3 80.49 14.80 6 -9 3 75.79 5.40 -9 -6 3 66.39 20.40 9 6 3 83.09 7.40 -6 9 3 66.19 16.20 9 6 3 79.59 5.80 9 6 3 73.89 6.10 9 6 3 71.09 7.10 9 4 -3 27.40 4.10 9 4 -3 26.60 4.20 4 -9 -3 36.20 13.90 9 4 -3 30.50 14.50 -4 9 -3 23.30 3.80 9 4 -3 27.60 4.30 4 -9 -3 27.00 3.80 4 -9 -3 28.00 3.50 -4 9 -3 26.70 11.80 9 4 3 32.00 5.30 -4 9 3 10.70 11.80 9 4 3 26.50 4.00 4 -9 3 41.90 14.30 9 4 3 23.30 3.90 -9 -4 3 22.00 2.40 4 -9 3 27.80 3.80 4 -9 3 43.40 13.20 -9 -4 3 23.90 15.20 4 -9 3 35.30 4.20 9 4 3 9.90 11.90 -4 9 3 31.80 4.20 9 2 -3 287.57 13.20 2 -9 -3 266.07 24.80 2 -9 -3 300.57 12.40 -2 9 -3 275.37 12.50 9 2 -3 284.27 13.00 9 2 -3 293.77 24.90 9 2 -3 288.47 12.50 -2 9 -3 243.18 22.20 2 -9 3 284.07 25.80 -9 -2 3 274.87 26.40 2 -9 3 266.37 26.40 9 2 3 302.77 14.40 -2 9 3 273.37 23.80 9 2 3 307.87 25.40 -2 9 3 319.27 12.80 -2 9 3 260.67 11.40 9 2 3 278.97 12.20 9 2 3 290.47 12.90 2 -9 3 298.27 12.40 9 0 -3 1969.80 66.09 0 -9 -3 1971.40 78.29 9 0 -3 2002.10 66.69 9 0 -3 1913.61 77.39 9 0 -3 1953.50 65.29 0 9 -3 2026.90 76.59 0 9 -3 2000.70 65.49 0 -9 -3 1951.90 65.09 9 0 -3 2013.30 66.49 0 -9 3 1886.81 77.49 0 -9 3 1941.01 65.09 0 -9 3 2097.09 85.29 9 0 3 1968.40 66.09 0 9 3 2008.30 65.19 -9 0 3 2031.40 65.39 0 9 3 2167.88 75.59 9 0 3 2035.20 67.39 0 9 3 1930.91 64.79 9 0 3 1908.51 64.69 -9 0 3 2127.49 77.09 0 9 3 2088.89 78.39 -9 0 3 1981.20 63.19 9 0 3 2052.79 80.19 -9 2 -3 1470.35 48.10 9 -2 -3 1550.04 49.60 2 9 -3 1492.05 48.90 9 -2 -3 1529.75 55.49 -2 -9 -3 1385.46 61.09 9 -2 -3 1466.55 50.89 -2 -9 -3 1546.65 49.60 9 -2 -3 1507.65 59.69 2 9 -3 1490.55 60.29 2 9 -3 1560.64 49.99 9 -2 -3 1476.05 50.99 2 9 3 1505.75 62.99 9 -2 3 1482.25 52.79 2 9 3 1488.25 49.70 9 -2 3 1534.45 52.19 -9 2 3 1481.35 54.29 2 9 3 1432.56 49.30 9 -2 3 1487.95 50.69 9 -2 3 1440.96 62.29 -2 -9 3 1486.65 61.49 9 -2 3 1418.96 48.50 2 9 3 1559.44 61.59 -9 2 3 1475.25 48.20 9 -2 3 1496.15 54.69 -9 2 3 1557.74 53.79 -2 -9 3 1458.55 49.40 9 -4 -3 1008.70 36.80 9 -4 -3 1007.70 34.50 -4 -9 -3 1001.40 46.90 -9 4 -3 1016.70 34.10 -9 4 -3 1034.70 41.00 9 -4 -3 1016.80 36.40 -4 -9 -3 1016.70 34.60 4 9 -3 1030.30 34.90 9 -4 -3 937.51 43.30 4 9 -3 1032.70 45.10 9 -4 3 1091.89 38.00 4 9 3 982.90 35.40 -9 4 3 1096.19 42.80 4 9 3 935.01 37.70 9 -4 3 968.70 41.90 4 9 3 1021.40 45.70 9 -4 3 1040.20 36.30 -4 -9 3 974.40 46.10 -9 4 3 999.00 34.10 9 -4 3 1025.50 47.10 4 9 3 1064.79 51.29 -4 -9 3 989.70 34.50 6 9 -3 366.76 33.60 -9 6 -3 319.77 13.00 9 -6 -3 322.97 15.40 -6 -9 -3 289.57 12.40 6 9 -3 297.37 13.40 9 -6 -3 319.77 27.30 -6 -9 -3 321.97 25.40 -9 6 -3 287.77 23.40 -6 -9 3 308.67 12.60 -6 -9 3 270.87 24.50 9 -6 3 291.37 25.00 -9 6 3 319.57 24.40 9 -6 3 292.47 25.30 9 -6 3 312.87 15.60 6 9 3 321.47 31.00 6 9 3 309.97 16.20 9 -6 3 298.57 13.90 -9 6 3 285.97 12.70 6 9 3 297.57 13.80 -9 8 -3 101.79 17.50 -8 -9 -3 102.59 5.90 8 9 -3 106.09 7.10 9 -8 -3 96.69 7.40 -9 8 -3 97.19 6.60 9 -8 -3 81.09 20.80 8 9 -3 130.59 26.30 9 -8 -3 102.89 8.60 8 9 -3 87.29 8.30 8 9 -3 106.49 6.90 8 9 3 143.29 24.80 9 -8 3 104.69 8.90 8 9 3 91.79 11.50 -8 -9 3 107.69 6.10 -9 8 3 94.09 17.90 8 9 3 99.79 7.50 9 -8 3 76.39 19.60 9 -8 3 92.89 7.10 9 -8 3 99.29 17.90 -8 -9 3 80.89 18.30 -9 8 3 103.69 6.80 9 -10 -3 421.66 20.80 10 9 -3 438.46 42.30 10 9 -3 409.16 20.00 10 9 -3 384.56 16.70 10 9 -3 431.96 18.70 -10 -9 -3 412.56 16.00 9 -10 -3 426.96 18.10 9 -10 -3 407.26 17.10 -9 10 -3 431.66 18.30 -10 -9 3 459.25 46.10 -10 -9 3 422.06 30.40 9 -10 3 391.46 18.10 10 9 3 416.56 18.80 10 9 3 505.95 44.40 10 9 3 403.66 26.60 10 9 3 388.06 17.40 9 -10 3 418.16 18.10 9 -10 3 440.46 21.00 -9 10 3 442.26 18.20 -10 -9 3 419.76 16.20 -7 10 -3 753.12 28.10 7 -10 -3 750.52 27.30 -7 10 -3 775.92 46.30 -10 -7 -3 754.42 25.40 10 7 -3 736.53 50.19 10 7 -3 748.73 30.80 10 7 -3 755.92 28.40 7 -10 -3 703.83 27.20 7 -10 -3 703.13 49.10 10 7 -3 734.03 27.50 7 -10 3 757.82 30.40 7 -10 3 637.14 49.30 10 7 3 722.43 27.20 7 -10 3 726.43 27.10 -10 -7 3 823.62 55.69 10 7 3 753.32 28.50 -10 -7 3 766.72 27.50 7 -10 3 754.42 38.00 7 -10 3 770.02 27.70 -7 10 3 810.82 49.99 10 7 3 730.23 50.29 -10 -7 3 721.63 25.60 10 7 3 756.92 30.50 -7 10 3 729.43 27.90 5 -10 -3 616.04 24.50 5 -10 -3 660.73 24.00 10 5 -3 695.53 25.60 -5 10 -3 646.24 25.20 10 5 -3 709.63 44.70 10 5 -3 682.13 26.00 -5 10 -3 710.63 42.10 -10 -5 -3 669.63 22.40 5 -10 -3 636.14 43.60 10 5 -3 673.53 25.40 10 5 3 671.43 27.50 10 5 3 650.63 25.10 5 -10 3 665.53 38.10 10 5 3 665.43 43.60 -5 10 3 685.73 43.30 -10 -5 3 664.13 22.60 5 -10 3 675.63 44.00 -10 -5 3 724.53 48.00 5 -10 3 661.23 24.70 -5 10 3 652.43 25.20 5 -10 3 696.33 24.50 -5 10 3 657.53 23.60 10 5 3 682.03 25.60 -3 10 -3 109.69 17.30 10 3 -3 147.49 8.80 10 3 -3 148.79 8.60 -3 10 -3 159.88 8.60 3 -10 -3 137.99 21.30 10 3 -3 164.48 23.00 3 -10 -3 153.88 8.30 10 3 -3 145.79 8.80 -3 10 3 141.29 7.20 -10 -3 3 169.78 24.90 10 3 3 167.78 10.40 10 3 3 137.79 8.10 -3 10 3 163.38 8.70 10 3 3 156.18 23.00 -3 10 3 109.99 18.70 3 -10 3 159.88 23.20 -10 -3 3 146.29 6.10 3 -10 3 130.49 19.90 10 3 3 147.09 8.70 3 -10 3 154.78 8.20 -1 10 -3 458.65 30.80 1 -10 -3 466.15 34.10 10 1 -3 483.45 20.10 10 1 -3 488.75 20.10 10 1 -3 507.05 33.90 -1 10 -3 518.85 19.70 1 -10 -3 518.55 19.30 10 1 -3 482.35 19.20 10 1 3 484.25 19.00 1 -10 3 466.65 36.60 -1 10 3 499.45 19.40 -1 10 3 539.85 33.80 1 -10 3 527.05 34.70 10 1 3 469.95 19.80 -1 10 3 493.65 18.50 -10 -1 3 476.05 16.80 10 1 3 532.15 34.90 1 -10 3 499.05 19.20 -10 -1 3 548.25 34.10 10 1 3 495.45 21.30 1 10 -3 1806.22 59.69 -1 -10 -3 1944.71 61.09 10 -1 -3 1840.22 73.99 1 10 -3 1797.72 73.19 10 -1 -3 1786.52 63.49 10 -1 -3 1847.72 60.89 1 10 -3 1820.62 61.19 10 -1 -3 1860.61 62.39 10 -1 -3 1854.01 62.29 -10 1 -3 1829.82 58.89 -1 -10 -3 1832.42 76.29 -10 1 3 1837.32 58.99 10 -1 3 1882.21 62.19 10 -1 3 1780.82 75.79 1 10 3 1787.52 74.09 10 -1 3 1801.52 60.19 -10 1 3 1874.11 61.79 10 -1 3 1886.41 63.49 10 -1 3 1889.81 60.29 -1 -10 3 1896.81 83.49 -10 1 3 1902.91 69.59 1 10 3 1797.62 60.59 -1 -10 3 1867.91 75.69 1 10 3 1862.51 60.99 10 -1 3 1870.21 59.89 -1 -10 3 1856.41 60.89 1 10 3 1835.82 73.79 -10 3 -3 459.25 17.10 3 10 -3 468.15 18.40 3 10 -3 454.35 17.80 -3 -10 -3 441.16 32.00 10 -3 -3 459.95 26.50 -3 -10 -3 498.85 18.40 10 -3 -3 464.95 18.00 3 10 -3 449.26 29.80 10 -3 -3 441.06 28.70 10 -3 -3 489.65 20.00 10 -3 -3 455.35 19.90 3 10 3 452.15 18.50 3 10 3 468.05 18.00 3 10 3 479.55 31.40 10 -3 3 490.15 21.00 -3 -10 3 472.45 31.60 -3 -10 3 511.45 18.50 10 -3 3 492.65 26.80 10 -3 3 428.56 23.40 10 -3 3 450.95 17.10 10 -3 3 481.35 19.60 -10 3 3 493.45 24.20 -10 3 3 465.65 17.20 10 -3 3 497.55 32.30 3 10 3 520.55 35.10 10 -5 -3 735.03 28.00 10 -5 -3 724.83 28.70 -10 5 -3 669.43 25.50 5 10 -3 695.13 26.30 -5 -10 -3 744.33 26.10 10 -5 -3 692.73 25.80 10 -5 -3 725.23 38.50 -10 5 -3 672.63 33.90 10 -5 3 757.42 39.70 -5 -10 3 730.53 26.10 10 -5 3 724.13 37.00 5 10 3 727.03 27.10 5 10 3 754.42 46.20 -10 5 3 757.62 25.90 10 -5 3 735.33 29.50 5 10 3 751.82 30.20 -10 5 3 734.13 35.90 10 -5 3 713.93 27.60 10 -7 -3 89.49 8.10 -10 7 -3 91.79 6.20 10 -7 -3 95.29 7.40 -10 7 -3 90.39 17.20 7 10 -3 106.09 7.10 10 -7 -3 66.29 19.80 -7 -10 -3 94.99 5.90 7 10 -3 100.09 25.30 7 10 3 87.89 9.40 -7 -10 3 93.99 6.00 7 10 3 84.69 6.80 10 -7 3 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1399.16 53.69 -5 -16 3 1328.97 93.79 -5 -16 3 1343.27 48.50 16 -7 -3 475.25 23.40 7 16 -3 476.15 21.10 16 -7 -3 484.55 25.00 -16 7 -3 438.06 20.00 -7 -16 -3 512.25 21.40 -7 -16 3 558.64 65.09 -7 -16 3 496.85 21.40 -16 7 3 507.85 20.50 16 -7 3 501.45 23.60 16 -7 3 457.15 25.50 7 16 3 458.35 21.50 16 -9 -3 47.50 8.90 9 16 -3 48.50 6.60 -16 9 -3 36.90 5.70 16 -9 -3 29.20 6.70 -9 -16 -3 28.40 5.20 16 -9 3 32.90 8.00 9 16 3 13.70 42.30 16 -9 3 39.50 6.70 9 16 3 36.00 6.50 -16 9 3 37.60 5.60 -9 -16 3 9.60 44.10 -9 -16 3 29.80 5.30 16 -11 -3 449.26 22.10 -16 11 -3 468.85 21.00 -11 -16 -3 462.65 19.90 16 -11 -3 440.26 25.30 11 16 -3 466.45 21.60 16 -11 3 462.55 25.70 11 16 3 481.85 69.59 -16 11 3 472.45 20.90 16 -11 3 490.55 22.70 11 16 3 447.06 21.70 -11 -16 3 299.67 60.89 -11 -16 3 439.56 19.90 16 -13 -3 270.17 15.90 -16 13 -3 285.57 15.40 -13 -16 -3 257.67 13.10 13 16 -3 276.27 15.90 16 -13 -3 292.87 19.00 16 -13 3 310.07 19.90 16 -13 3 241.18 16.50 -16 13 3 267.87 14.80 -13 -16 3 110.79 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224.58 14.40 17 0 3 231.08 12.70 17 0 3 221.28 16.20 17 0 3 231.18 43.40 0 -17 3 182.08 48.30 17 -2 -3 74.99 7.60 17 -2 -3 75.09 9.60 17 -2 -3 77.19 9.00 -2 -17 -3 78.19 7.70 17 -2 3 20.80 40.40 17 -2 3 75.39 10.30 -2 -17 3 74.59 7.30 -2 -17 3 26.40 36.40 2 17 3 78.69 7.00 17 -2 3 67.69 9.00 4 17 -3 597.34 25.30 -17 4 -3 625.64 24.40 17 -4 -3 701.73 30.20 -4 -17 -3 702.43 27.70 17 -4 -3 641.44 30.20 -4 -17 3 686.13 73.79 -4 -17 3 688.13 27.60 17 -4 3 663.63 29.40 -17 4 3 636.34 24.40 17 -4 3 719.83 32.30 4 17 3 648.84 26.30 -6 -17 -3 433.86 19.80 17 -6 -3 391.76 22.60 17 -6 -3 414.66 22.10 -17 6 -3 449.46 18.60 6 17 -3 442.96 19.50 -6 -17 3 335.07 56.19 6 17 3 438.06 19.90 17 -6 3 447.86 22.20 -6 -17 3 424.16 19.80 17 -6 3 447.56 24.40 -17 6 3 412.96 18.10 -17 8 -3 189.78 11.10 17 -8 -3 182.48 13.50 -8 -17 -3 173.88 11.30 8 17 -3 192.38 11.90 17 -8 -3 160.78 14.60 -8 -17 3 183.78 11.50 -17 8 3 199.08 11.20 17 -8 3 183.18 13.40 8 17 3 193.78 12.20 17 -8 3 198.08 16.10 -8 -17 3 223.58 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168.58 8.80 -1 -11 4 169.18 24.00 1 11 4 184.98 23.40 -11 1 4 168.18 7.70 -1 -11 4 176.78 9.30 11 -1 4 175.78 11.20 1 11 4 182.48 9.30 -11 1 4 162.08 19.70 1 11 4 237.68 28.90 -11 1 4 168.88 12.40 1 11 4 179.68 9.50 11 -1 4 168.78 23.70 -1 -11 4 186.98 29.10 11 -1 4 175.48 10.30 3 11 -4 57.89 5.00 11 -3 -4 61.59 5.40 11 -3 -4 74.29 15.00 11 -3 -4 61.39 6.50 11 -3 -4 70.29 6.70 3 11 -4 65.69 5.80 -11 3 -4 66.69 4.60 -3 -11 -4 72.09 5.50 11 -3 4 64.79 17.50 11 -3 4 64.59 5.10 3 11 4 46.20 18.30 -11 3 4 76.49 4.80 -11 3 4 70.49 11.30 -3 -11 4 54.49 5.00 11 -3 4 57.39 10.70 3 11 4 59.49 5.60 11 -3 4 78.99 7.80 -3 -11 4 73.69 22.50 11 -3 4 71.59 6.40 3 11 4 65.59 5.60 -5 -11 -4 148.69 8.40 5 11 -4 149.88 8.60 11 -5 -4 146.59 10.30 -11 5 -4 152.18 8.20 11 -5 -4 158.48 10.20 11 -5 -4 123.89 20.80 -11 5 4 151.58 8.00 5 11 4 166.18 28.20 11 -5 4 155.78 9.70 11 -5 4 148.69 23.30 -11 5 4 129.49 17.40 11 -5 4 129.79 18.40 5 11 4 155.58 12.20 11 -5 4 164.58 11.20 5 11 4 157.28 9.40 -5 -11 4 175.78 32.70 -5 -11 4 151.98 8.40 -11 7 -4 48.80 4.80 -7 -11 -4 47.60 4.40 7 11 -4 44.60 4.90 11 -7 -4 39.00 6.80 11 -7 -4 39.00 5.90 7 11 4 47.80 8.20 11 -7 4 66.89 20.10 -7 -11 4 40.70 4.20 -7 -11 4 36.90 23.10 11 -7 4 48.50 6.50 -11 7 4 33.60 4.60 7 11 4 38.00 5.60 7 11 4 11.70 19.60 11 -7 4 46.70 7.70 -11 9 -4 307.67 14.60 11 -9 -4 292.47 15.20 11 -9 -4 312.67 17.40 9 11 -4 309.57 14.90 -9 -11 -4 289.07 13.10 -9 -11 4 312.97 13.60 9 11 4 282.97 18.20 -9 -11 4 336.27 46.60 -11 9 4 298.07 14.30 11 -9 4 309.97 17.60 11 -9 4 311.37 15.30 9 11 4 275.67 14.80 9 11 4 282.47 40.00 -11 -11 -4 233.28 11.10 11 11 -4 218.88 13.20 11 -11 -4 253.37 13.50 -11 11 -4 242.18 13.20 11 -11 -4 256.57 16.10 -11 11 4 238.78 13.00 11 -11 4 237.28 13.30 -11 -11 4 233.68 44.80 11 -11 4 251.57 16.00 11 11 4 218.58 19.90 11 11 4 257.57 14.20 11 11 4 237.08 41.10 -11 -11 4 237.18 11.50 12 10 -4 616.74 25.90 10 -12 -4 619.54 24.80 -12 -10 -4 612.74 22.30 12 10 -4 589.14 27.90 10 -12 -4 616.24 28.70 -10 12 -4 611.64 25.50 12 10 4 592.54 56.09 -12 -10 4 592.74 62.09 -10 12 4 591.74 25.20 10 -12 4 593.74 25.00 12 10 4 625.94 26.20 -12 -10 4 582.44 22.60 10 -12 4 626.14 28.40 12 10 4 595.54 34.60 8 -12 -4 1165.58 42.00 -8 12 -4 1196.28 43.60 12 8 -4 1228.78 44.10 12 8 -4 1188.88 42.60 -12 -8 -4 1155.28 39.80 12 8 -4 1185.08 45.00 12 8 -4 1236.88 75.49 -12 -8 4 1238.48 40.40 -12 -8 4 1268.57 77.29 12 8 4 1259.27 44.40 -8 12 4 1244.28 43.60 8 -12 4 1213.48 46.10 8 -12 4 1244.08 43.10 12 8 4 1204.98 47.40 12 8 4 1073.99 42.10 12 8 4 1124.29 72.59 -6 12 -4 2352.86 78.29 6 -12 -4 2240.58 75.79 12 6 -4 2315.37 78.09 12 6 -4 2336.47 106.49 -12 -6 -4 2244.78 73.99 6 -12 -4 2408.26 77.39 12 6 -4 2307.17 78.39 12 6 -4 2369.76 78.49 -6 12 4 2381.46 78.19 12 6 4 2365.56 78.59 -12 -6 4 2411.46 109.19 12 6 4 2286.77 77.59 6 -12 4 2273.87 77.19 12 6 4 2360.76 106.69 6 -12 4 2359.06 80.39 12 6 4 2393.26 81.29 -12 -6 4 2282.87 74.49 6 -12 4 2351.66 76.49 12 4 -4 1883.11 63.59 4 -12 -4 1700.93 90.09 4 -12 -4 1970.20 62.59 -4 12 -4 1923.51 87.39 -12 -4 -4 1774.82 58.69 -4 12 -4 1862.71 63.09 12 4 -4 1795.62 63.09 12 4 -4 1831.72 62.99 12 4 -4 1889.21 87.69 4 -12 4 1860.71 82.69 12 4 4 1943.41 88.09 4 -12 4 1825.02 62.29 12 4 4 1912.71 63.09 12 4 4 1922.01 65.79 -12 -4 4 1891.11 88.19 -4 12 4 1958.60 63.19 -4 12 4 1779.72 60.29 -4 12 4 1801.42 86.59 -12 -4 4 1817.02 59.09 12 4 4 1839.12 63.09 4 -12 4 1650.03 86.79 12 2 -4 729.13 46.90 12 2 -4 673.73 27.10 -2 12 -4 660.53 26.40 2 -12 -4 700.03 26.00 2 -12 -4 730.53 53.79 -2 12 -4 697.33 48.20 12 2 -4 706.43 26.50 -12 -2 -4 664.03 22.80 12 2 -4 692.83 26.90 12 2 4 705.83 28.80 2 -12 4 631.74 50.09 -2 12 4 686.03 49.40 12 2 4 653.03 47.00 -2 12 4 702.63 26.40 -12 -2 4 642.74 22.90 -2 12 4 664.03 24.60 -12 -2 4 603.04 44.90 12 2 4 689.73 26.90 2 -12 4 710.23 48.30 2 -12 4 671.03 25.80 12 2 4 668.13 25.90 0 -12 -4 1435.66 73.69 0 12 -4 1405.46 69.79 -12 0 -4 1436.66 48.10 0 12 -4 1532.35 51.49 0 -12 -4 1470.45 50.79 12 0 -4 1485.35 50.99 12 0 -4 1463.75 69.39 12 0 -4 1480.55 52.19 0 12 -4 1420.36 48.60 12 0 -4 1515.35 52.69 12 0 4 1500.65 52.19 12 0 4 1516.45 71.69 0 -12 4 1600.74 51.19 -12 0 4 1462.55 64.59 0 12 4 1509.95 50.99 0 12 4 1508.55 50.29 12 0 4 1431.86 50.19 0 12 4 1462.35 71.69 0 -12 4 1552.84 77.49 -12 0 4 1447.16 48.10 12 0 4 1551.24 54.19 12 -2 -4 776.62 35.80 -2 -12 -4 821.52 30.40 2 12 -4 821.62 29.30 12 -2 -4 823.72 32.30 12 -2 -4 823.52 32.00 -12 2 -4 857.01 28.70 12 -2 -4 833.82 30.40 2 12 -4 838.62 30.70 12 -2 4 912.91 50.59 12 -2 4 816.12 29.30 12 -2 4 843.42 32.00 -2 -12 4 781.02 30.20 12 -2 4 852.31 33.60 2 12 4 863.01 48.90 2 12 4 841.22 30.50 -12 2 4 813.52 28.50 -2 -12 4 848.32 58.39 -12 2 4 872.01 32.60 2 12 4 813.92 30.20 -4 -12 -4 723.23 26.60 4 12 -4 721.43 26.20 -12 4 -4 710.33 25.50 12 -4 -4 769.12 29.10 12 -4 -4 753.62 29.20 4 12 -4 684.73 26.30 12 -4 -4 696.23 26.30 12 -4 -4 643.74 41.10 -12 4 4 698.03 25.40 -4 -12 4 689.83 26.50 -4 -12 4 715.33 55.89 4 12 4 626.44 29.50 12 -4 4 719.23 28.30 4 12 4 679.63 47.70 12 -4 4 653.63 36.40 -12 4 4 715.03 36.10 4 12 4 731.23 27.30 12 -4 4 747.43 30.40 12 -4 4 662.93 45.40 12 -6 -4 905.81 35.20 -6 -12 -4 837.22 31.50 -12 6 -4 884.11 31.60 6 12 -4 845.42 32.00 12 -6 -4 852.71 33.80 6 12 4 897.31 33.10 12 -6 4 831.82 50.79 -6 -12 4 901.11 32.00 12 -6 4 884.51 33.80 -6 -12 4 808.12 63.79 -12 6 4 868.91 31.30 12 -6 4 917.91 36.20 6 12 4 840.62 57.29 8 12 -4 762.12 29.90 12 -8 -4 747.93 31.00 12 -8 -4 783.02 33.00 -12 8 -4 759.22 29.40 -8 -12 -4 764.62 28.70 8 12 4 773.22 34.60 -12 8 4 817.42 29.50 8 12 4 791.22 30.70 8 12 4 746.63 59.79 -8 -12 4 782.52 29.00 -8 -12 4 785.72 65.29 12 -8 4 769.32 30.90 12 -8 4 854.21 34.20 12 -10 -4 925.51 35.70 12 -10 -4 929.21 38.70 -12 10 -4 951.10 35.10 10 12 -4 931.21 35.40 -10 -12 -4 888.11 33.00 -10 -12 4 892.81 73.79 10 12 4 900.71 40.50 10 12 4 905.21 35.70 -12 10 4 917.71 34.60 -10 -12 4 909.11 33.30 12 -10 4 964.20 39.00 10 12 4 1009.80 70.99 12 -10 4 896.41 35.40 12 -12 -4 826.52 32.90 12 12 -4 886.11 34.00 12 -12 -4 865.71 37.50 -12 12 -4 862.71 33.40 -12 -12 -4 798.42 30.10 -12 -12 4 800.22 30.50 -12 12 4 825.22 33.00 12 12 4 846.42 71.79 -12 -12 4 846.52 75.99 12 -12 4 821.72 33.10 12 12 4 870.11 34.30 12 -12 4 868.31 37.00 12 12 4 797.82 40.10 11 -13 -4 0.60 3.60 13 11 -4 0.50 3.60 11 -13 -4 9.50 5.70 -11 13 -4 4.20 3.60 -13 -11 -4 0.80 2.30 -13 -11 4 -18.30 36.20 -11 13 4 5.40 3.20 13 11 4 2.40 3.60 11 -13 4 -4.80 5.40 13 11 4 -7.70 32.10 13 11 4 -0.50 16.50 11 -13 4 8.10 4.90 -13 -11 4 9.00 2.90 9 -13 -4 301.17 14.90 9 -13 -4 320.87 14.90 -13 -9 -4 300.17 12.50 13 9 -4 326.37 16.60 13 9 -4 280.37 14.60 -9 13 -4 327.27 16.30 13 9 -4 347.67 20.00 13 9 4 325.17 16.60 -9 13 4 306.07 16.10 -13 -9 4 285.17 12.70 9 -13 4 300.97 15.50 -13 -9 4 263.17 46.00 9 -13 4 336.27 18.60 13 9 4 356.16 33.60 13 9 4 317.27 45.60 13 9 4 275.97 17.20 13 7 -4 47.80 12.70 7 -13 -4 34.00 5.20 -7 13 -4 32.40 5.70 13 7 -4 38.30 25.40 -13 -7 -4 40.90 3.60 13 7 -4 35.10 6.00 13 7 -4 46.80 6.60 7 -13 4 42.50 5.60 -13 -7 4 36.30 3.90 13 7 4 47.10 7.70 -13 -7 4 35.80 28.10 7 -13 4 37.00 5.20 -7 13 4 39.20 6.30 7 -13 4 43.50 7.10 13 7 4 21.10 24.10 13 7 4 39.80 5.90 -5 13 -4 280.47 14.20 5 -13 -4 276.97 13.40 13 5 -4 251.67 36.10 13 5 -4 266.07 14.00 13 5 -4 237.78 13.80 13 5 -4 263.97 14.20 13 5 4 243.48 13.40 -5 13 4 264.47 13.60 13 5 4 288.47 37.70 5 -13 4 230.98 32.00 -13 -5 4 253.47 38.00 13 5 4 285.17 16.20 13 5 4 274.37 14.00 -13 -5 4 261.37 10.40 5 -13 4 267.77 13.40 -3 13 -4 9.90 29.80 13 3 -4 38.20 22.60 13 3 -4 15.40 4.10 3 -13 -4 2.90 35.30 13 3 -4 16.50 4.10 -3 13 -4 16.60 4.30 13 3 -4 16.10 4.30 3 -13 -4 21.50 4.30 13 3 4 23.40 5.30 13 3 4 21.20 4.20 -13 -3 4 8.40 20.60 -3 13 4 13.50 3.20 -3 13 4 17.50 4.10 3 -13 4 19.20 4.00 13 3 4 19.10 4.50 -3 13 4 -21.50 29.50 13 3 4 35.60 20.50 3 -13 4 14.40 33.20 -13 -3 4 23.90 2.60 3 -13 4 23.20 22.10 13 1 -4 313.57 16.40 1 -13 -4 341.47 15.60 13 1 -4 350.96 15.90 -1 13 -4 352.96 16.10 13 1 -4 347.77 16.90 13 1 -4 288.57 36.40 -13 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13 -4 1.60 3.50 13 -13 -4 9.50 4.50 -13 -13 -4 1.20 2.80 13 13 -4 -0.50 3.50 13 13 4 -24.60 38.80 13 -13 4 0.90 5.00 13 -13 4 2.10 6.50 -13 13 4 -5.40 2.80 -13 -13 4 4.00 2.70 13 13 4 -2.50 3.30 -13 -13 4 -7.50 42.30 13 13 4 1.60 17.60 14 12 -4 336.47 18.00 -12 14 -4 356.26 17.90 12 -14 -4 313.27 16.70 -14 -12 -4 323.37 14.10 12 -14 -4 340.27 20.80 14 12 4 343.97 30.50 12 -14 4 339.57 20.70 12 -14 4 295.17 17.30 -12 14 4 318.67 17.10 14 12 4 254.37 51.29 -14 -12 4 320.27 14.50 14 12 4 349.77 18.10 -14 -12 4 312.07 59.39 14 10 -4 835.62 34.10 -10 14 -4 843.12 33.90 10 -14 -4 875.91 37.40 -14 -10 -4 795.32 29.10 14 10 -4 828.62 36.70 10 -14 4 803.62 31.80 10 -14 4 862.21 36.80 -10 14 4 854.21 33.80 -14 -10 4 803.12 76.79 14 10 4 901.01 45.80 14 10 4 914.51 34.90 -14 -10 4 814.02 29.60 14 10 4 820.42 72.29 8 -14 -4 1266.27 46.10 14 8 -4 1353.66 48.30 14 8 -4 1285.47 46.60 -8 14 -4 1325.17 48.00 14 8 -4 1296.67 50.29 14 8 4 1268.57 52.59 -14 -8 4 1349.07 88.79 8 -14 4 1325.47 46.30 8 -14 4 1307.17 50.29 14 8 4 1357.66 48.40 14 8 4 1167.68 46.20 14 8 4 1276.87 82.39 -14 -8 4 1276.67 43.10 -8 14 4 1361.46 48.00 14 6 -4 914.31 37.50 14 6 -4 944.51 38.40 14 6 -4 1027.60 69.99 6 -14 -4 987.40 37.10 14 6 -4 1043.80 38.70 -6 14 -4 1048.00 38.50 6 -14 4 915.21 36.70 6 -14 4 1038.70 40.60 -14 -6 4 1106.39 72.59 14 6 4 953.80 66.99 14 6 4 1049.70 38.00 14 6 4 1067.89 41.50 14 6 4 1046.10 38.60 -6 14 4 1017.10 38.30 4 -14 -4 657.33 27.50 14 4 -4 730.03 29.20 -4 14 -4 703.23 28.60 14 4 -4 660.53 54.89 14 4 -4 735.33 29.20 14 4 -4 683.83 28.50 14 4 4 770.12 57.99 4 -14 4 756.52 28.20 14 4 4 717.93 28.70 4 -14 4 675.83 56.39 -4 14 4 713.93 28.50 -14 -4 4 633.24 56.39 14 4 4 736.13 31.30 14 4 4 698.73 28.30 -2 14 -4 1337.07 48.70 14 2 -4 1277.97 73.29 2 -14 -4 1420.76 48.40 14 2 -4 1350.46 48.60 14 2 -4 1373.36 49.90 14 2 -4 1312.97 49.20 2 -14 4 1463.55 48.70 -2 14 4 1340.47 46.20 2 -14 4 1329.07 76.29 -14 -2 4 1252.27 69.39 14 2 4 1422.26 51.99 14 2 4 1388.66 48.40 14 2 4 1368.66 49.50 14 2 4 1338.37 74.49 -2 14 4 1398.76 48.70 -14 0 -4 285.37 11.70 0 14 -4 323.57 15.30 0 -14 -4 318.97 14.90 14 0 -4 316.37 15.00 14 0 -4 304.77 16.20 14 0 -4 318.87 16.20 -14 0 4 305.67 11.90 14 0 4 282.37 14.00 0 14 4 294.67 13.70 14 0 4 302.87 15.80 0 14 4 332.37 15.10 0 -14 4 268.47 14.20 14 0 4 297.37 17.30 14 0 4 270.27 34.30 0 -14 4 348.77 44.90 14 -2 -4 1064.29 40.60 -2 -14 -4 1131.69 38.80 -14 2 -4 1045.90 35.90 2 14 -4 1077.29 38.50 14 -2 -4 1057.79 38.20 14 -2 -4 1065.59 40.40 2 14 -4 1002.90 36.50 14 -2 4 1024.40 36.80 -2 -14 4 1122.59 71.89 2 14 4 1063.99 38.10 -14 2 4 1025.30 35.80 14 -2 4 975.10 61.79 2 14 4 1042.10 37.90 -2 -14 4 1025.50 38.30 14 -2 4 1067.79 40.20 14 -2 4 1127.79 42.70 -14 4 -4 2547.75 81.69 14 -4 -4 2554.34 85.99 -4 -14 -4 2535.65 83.39 14 -4 -4 2449.35 82.79 4 14 -4 2441.06 82.29 14 -4 -4 2496.85 86.19 4 14 4 2592.94 111.29 4 14 4 2531.85 83.59 14 -4 4 2603.64 85.69 -4 -14 4 2487.15 83.39 -14 4 4 2492.65 81.39 14 -4 4 2345.97 105.59 -4 -14 4 2413.66 120.49 14 -4 4 2582.94 87.99 14 -6 -4 943.41 38.50 6 14 -4 950.50 35.00 -6 -14 -4 1010.00 35.30 -14 6 -4 866.31 33.90 14 -6 -4 929.31 37.40 -6 -14 4 979.10 35.20 14 -6 4 919.41 37.00 6 14 4 925.91 66.59 -6 -14 4 885.51 72.89 14 -6 4 990.80 40.00 -14 6 4 927.51 34.00 6 14 4 1000.90 36.10 -8 -14 -4 67.79 6.60 14 -8 -4 86.89 8.60 -14 8 -4 87.69 7.20 8 14 -4 86.49 7.80 14 -8 -4 102.79 9.80 8 14 4 106.69 35.30 -8 -14 4 78.29 37.50 8 14 4 85.29 8.00 -14 8 4 86.79 6.90 -8 -14 4 88.29 7.10 14 -8 4 77.49 8.20 14 -8 4 77.79 11.00 10 14 -4 597.74 25.20 14 -10 -4 590.54 26.10 -10 -14 -4 592.14 23.50 -14 10 -4 561.34 24.40 14 -10 -4 596.74 28.80 10 14 4 556.24 63.69 -10 -14 4 524.95 66.99 -14 10 4 573.44 24.30 10 14 4 596.94 25.80 -10 -14 4 564.14 23.40 14 -10 4 590.64 29.00 14 -10 4 570.54 25.60 14 -12 -4 1241.28 46.40 12 14 -4 1219.68 46.40 -14 12 -4 1203.38 45.80 14 -12 -4 1252.07 50.59 -12 -14 -4 1239.58 43.50 14 -12 4 1210.28 46.50 -12 -14 4 1222.68 43.80 14 -12 4 1304.07 50.89 -12 -14 4 1141.09 92.99 -14 12 4 1231.58 45.60 12 14 4 1155.48 88.99 12 14 4 1317.77 47.40 14 -14 -4 365.86 18.80 14 14 -4 365.16 19.20 -14 14 -4 354.76 18.80 14 -14 -4 345.47 22.20 -14 -14 -4 380.16 16.20 -14 -14 4 370.16 16.50 14 14 4 396.66 19.90 14 14 4 383.96 65.99 -14 14 4 389.16 19.00 -14 -14 4 349.57 68.59 14 -14 4 384.06 22.50 14 -14 4 366.66 19.70 13 -15 -4 23.20 7.20 -13 15 -4 13.90 5.20 15 13 -4 19.90 5.50 -15 -13 4 19.20 5.00 -15 -13 4 24.70 50.79 15 13 4 31.60 47.40 15 13 4 5.90 19.10 -13 15 4 26.60 5.40 15 13 4 17.10 5.40 13 -15 4 16.90 7.00 11 -15 -4 3.30 4.70 15 11 -4 1.10 3.90 -11 15 -4 1.90 3.30 11 -15 4 -1.00 4.40 -11 15 4 2.50 3.50 15 11 4 1.10 3.30 15 11 4 9.60 38.10 -15 -11 4 -51.09 42.20 15 11 4 33.40 24.00 -9 15 -4 5.60 3.80 9 -15 -4 11.50 4.80 15 9 -4 -5.10 4.10 15 9 -4 10.90 11.30 9 -15 -4 8.20 5.00 15 9 -4 5.40 4.00 15 9 4 -24.70 32.80 9 -15 4 4.90 5.00 -9 15 4 1.90 3.40 15 9 4 9.40 23.20 -15 -9 4 -7.10 38.70 9 -15 4 -9.30 8.00 15 9 4 3.30 3.50 15 7 -4 -5.30 13.10 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107.29 5 4 -9 2054.39 64.89 -4 5 -9 2026.30 65.89 4 -5 -9 1957.70 65.29 -5 -4 -9 1966.90 64.99 5 4 -9 1976.90 65.79 -5 -4 -9 1851.11 79.39 4 -5 -9 1969.80 82.99 5 4 9 1869.51 77.49 -5 -4 9 2071.19 65.19 5 4 9 1946.51 82.89 -4 5 9 2037.60 65.59 -5 -4 9 1921.71 79.99 -5 -4 9 2013.10 76.49 4 -5 9 2077.09 82.59 5 4 9 2047.20 66.69 4 -5 9 1989.20 65.09 -4 5 9 2041.00 81.19 4 -5 9 2032.20 66.49 4 -5 9 1912.61 84.39 5 4 9 2112.09 81.59 4 -5 9 1842.62 77.89 -5 -4 9 2010.60 87.59 5 4 9 2003.00 67.29 -4 5 9 1973.60 78.59 4 -5 9 1951.60 65.89 2 -5 -9 132.49 7.50 -5 -2 -9 129.99 18.30 -5 -2 -9 145.99 7.60 5 2 -9 132.09 7.40 2 -5 -9 130.89 19.50 5 2 -9 138.49 8.10 -2 5 -9 134.39 8.00 -5 -2 9 139.99 7.30 -2 5 9 126.89 17.80 -5 -2 9 152.88 23.00 5 2 9 165.58 19.00 5 2 9 143.29 8.50 2 -5 9 124.09 20.60 -2 5 9 141.89 7.70 5 2 9 101.39 15.40 5 2 9 155.98 21.70 5 2 9 128.39 8.60 2 -5 9 113.39 16.70 2 -5 9 134.29 7.40 -5 -2 9 115.29 16.40 2 -5 9 137.79 7.40 -2 5 9 157.18 19.30 2 -5 9 175.68 22.80 -2 5 9 158.88 17.50 5 0 -9 2005.60 66.79 5 0 -9 2032.20 68.09 0 -5 -9 2117.59 67.69 -5 0 -9 2131.19 67.59 0 5 -9 1967.90 67.89 5 0 -9 1958.20 81.99 0 -5 -9 2060.39 83.19 0 -5 9 2094.79 67.49 0 -5 9 2044.30 85.29 0 5 9 2127.79 82.49 5 0 9 2111.89 84.89 5 0 9 2056.49 80.39 5 0 9 2033.20 68.49 0 -5 9 2130.89 80.29 0 5 9 2018.80 67.29 -5 0 9 2066.69 67.09 5 0 9 2069.29 81.69 0 -5 9 2073.29 86.99 -5 0 9 2070.79 80.29 5 0 9 2072.19 68.69 -5 0 9 2228.18 85.79 0 5 9 2025.80 78.89 0 5 9 2004.60 81.29 -2 -5 -9 342.37 14.00 2 5 -9 338.07 14.20 -2 -5 -9 305.37 27.10 -5 2 -9 343.67 14.00 5 -2 -9 314.47 27.90 2 5 -9 325.17 13.80 5 -2 -9 321.77 13.30 5 -2 9 341.57 23.80 2 5 9 292.37 25.00 5 -2 9 291.37 24.70 -2 -5 9 338.07 13.80 2 5 9 308.27 24.90 -5 2 9 327.97 25.40 2 5 9 326.37 15.30 5 -2 9 324.77 14.60 5 -2 9 320.27 14.80 -2 -5 9 347.87 25.80 -2 -5 9 371.66 31.00 5 -2 9 316.17 13.00 -5 2 9 316.87 13.40 2 5 9 360.66 27.10 5 -2 9 295.67 26.70 2 5 9 321.27 13.40 -5 2 9 342.07 26.90 -2 -5 9 363.96 31.50 4 5 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1178.18 66.09 6 2 12 1199.68 43.20 -6 -2 12 1200.38 41.20 6 2 12 1168.98 40.80 6 2 12 1165.18 60.59 6 2 12 1201.98 42.50 2 -6 12 1179.78 41.30 2 -6 12 1145.49 62.79 2 -6 12 1061.99 70.39 -6 -2 12 1160.68 64.59 -2 6 12 1130.59 55.09 -6 -2 12 1251.67 65.49 2 -6 12 1135.89 41.20 2 -6 12 1198.08 64.99 -2 6 12 1206.48 60.39 6 2 12 1242.58 64.59 -2 6 12 1251.77 41.90 6 0 -12 2057.09 66.59 0 6 -12 1962.70 67.79 -6 0 -12 1966.10 67.19 6 0 -12 1882.61 92.09 0 -6 -12 1922.71 92.09 0 -6 -12 2003.10 67.49 0 6 12 2001.00 88.79 0 6 12 1995.10 83.89 -6 0 12 2095.89 90.69 6 0 12 2144.29 87.99 0 -6 12 1952.00 94.89 6 0 12 2200.58 92.79 0 -6 12 1983.80 67.09 0 -6 12 2009.80 92.69 0 6 12 2082.39 67.29 0 -6 12 1969.60 86.59 -6 0 12 1926.61 86.89 6 0 12 1955.70 65.69 -6 0 12 2085.99 66.99 6 0 12 2053.79 68.49 0 6 12 2124.29 87.59 6 0 12 1884.81 89.09 -2 -6 -12 429.46 44.60 2 6 -12 493.45 20.10 6 -2 -12 495.65 21.70 6 -2 -12 457.85 18.90 -6 2 -12 470.45 19.80 6 -2 -12 405.56 49.70 -2 -6 -12 488.75 19.90 2 6 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12 12.50 4.30 9 -7 12 13.60 4.60 -7 -9 12 45.00 27.80 7 9 12 30.50 26.00 9 9 -12 54.49 7.30 9 9 -12 66.49 7.60 9 -9 -12 57.89 7.70 -9 -9 -12 74.89 6.80 9 -9 -12 67.29 7.80 -9 9 -12 77.29 7.70 9 -9 12 71.49 9.20 9 -9 12 65.89 32.50 9 9 12 96.39 12.50 9 9 12 84.29 30.30 -9 9 12 78.69 7.50 9 9 12 75.39 8.20 -9 -9 12 67.49 6.60 -9 -9 12 78.99 32.60 -8 10 -12 590.14 25.00 8 -10 -12 600.34 25.30 10 8 -12 523.15 24.30 8 -10 -12 543.65 23.20 10 8 -12 552.04 24.80 -10 -8 -12 552.24 23.00 10 8 12 553.04 33.60 -10 -8 12 568.14 23.20 8 -10 12 580.34 25.50 10 8 12 606.04 26.20 -10 -8 12 512.45 58.79 10 8 12 630.54 55.79 -8 10 12 577.64 24.70 10 6 -12 240.88 13.80 -6 10 -12 251.17 13.80 -10 -6 -12 240.68 12.30 10 6 -12 211.68 14.00 6 -10 -12 230.28 13.40 6 -10 -12 222.08 12.50 -10 -6 12 260.67 12.50 -6 10 12 248.08 13.60 10 6 12 231.08 41.80 10 6 12 240.88 14.20 -10 -6 12 257.47 42.30 6 -10 12 269.77 38.50 6 -10 12 217.58 13.50 10 6 12 222.68 19.40 6 -10 12 240.48 12.60 10 4 -12 1258.27 46.60 -4 10 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1744.43 95.99 4 -12 12 1523.35 88.79 4 -12 12 1631.04 56.99 12 4 12 1612.84 58.69 12 4 12 1639.14 61.09 -12 -4 12 1556.84 91.79 4 -12 12 1580.14 56.69 12 4 12 1614.74 58.19 -4 12 12 1762.22 58.29 -12 -4 12 1706.73 55.99 -12 -2 -12 882.21 33.10 12 2 -12 923.51 36.20 -2 12 -12 896.01 35.40 12 2 -12 904.71 37.20 2 -12 -12 924.61 35.00 -2 12 12 888.91 34.90 -2 12 12 933.91 35.40 12 2 12 865.31 65.99 2 -12 12 890.21 67.29 -12 -2 12 909.61 33.40 -12 -2 12 893.01 65.79 2 -12 12 910.01 34.70 12 2 12 970.40 38.80 12 2 12 909.81 37.20 12 2 12 860.61 34.70 -12 0 -12 210.08 11.50 12 0 -12 222.08 14.60 0 -12 -12 216.68 12.60 0 12 -12 230.68 13.10 12 0 12 221.28 12.50 -12 0 12 193.78 11.30 0 12 12 230.98 12.60 -12 0 12 120.39 31.10 0 -12 12 233.78 12.60 12 0 12 226.58 40.20 12 0 12 217.98 16.60 12 0 12 239.58 15.30 0 12 12 196.68 12.70 0 -12 12 192.38 38.30 -12 2 -12 1436.56 51.69 -2 -12 -12 1541.65 53.09 12 -2 -12 1488.35 55.79 2 12 -12 1502.05 52.79 12 -2 12 1511.45 88.89 2 12 12 1466.85 80.79 -12 2 12 1455.15 51.59 -12 2 12 1427.96 77.39 12 -2 12 1469.85 55.39 2 12 12 1555.34 53.99 12 -2 12 1478.55 55.89 -2 -12 12 1444.26 86.69 2 12 12 1448.16 51.69 -2 -12 12 1499.05 52.79 12 -4 -12 1931.31 69.19 -4 -12 -12 1862.01 65.89 4 12 -12 1843.42 64.89 -12 4 -12 1929.91 65.79 12 -4 12 1963.50 69.69 12 -4 12 1817.12 100.19 4 12 12 1949.01 96.69 12 -4 12 1960.80 68.89 -4 -12 12 1874.91 102.99 -4 -12 12 1871.91 65.89 -12 4 12 1915.81 65.39 4 12 12 1981.90 67.59 12 -6 -12 285.57 17.30 6 12 -12 268.87 14.50 -6 -12 -12 290.37 15.00 -12 6 -12 272.47 14.80 -6 -12 12 279.97 14.80 -12 6 12 283.57 14.80 -6 -12 12 266.27 48.20 6 12 12 323.07 16.90 6 12 12 232.88 46.40 12 -6 12 217.38 42.90 12 -6 12 295.97 17.60 12 -6 12 267.07 16.90 -12 8 -12 491.95 22.50 12 -8 -12 525.25 24.90 -8 -12 -12 493.25 21.90 8 12 -12 468.35 22.20 8 12 12 487.55 27.50 -8 -12 12 516.55 22.30 8 12 12 492.55 59.49 -8 -12 12 410.86 57.99 8 12 12 535.05 24.50 -12 8 12 530.45 22.70 12 -8 12 398.86 55.59 12 -8 12 513.35 25.50 12 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9.40 4 -5 -21 124.29 12.50 5 4 -21 109.19 11.80 4 -5 -21 114.09 10.60 -5 -4 21 117.99 9.80 -5 -4 21 106.59 42.30 -4 5 21 43.80 38.10 4 -5 21 88.89 10.10 -4 5 21 105.79 9.50 5 4 21 147.49 51.29 4 -5 21 87.89 41.30 5 4 21 109.79 10.40 5 4 21 94.79 36.70 -5 -2 -21 171.08 11.90 2 -5 -21 156.28 11.70 -2 5 -21 157.18 11.50 5 2 -21 162.98 13.70 -2 5 21 63.99 52.99 -2 5 21 162.38 11.40 2 -5 21 158.88 11.60 5 2 21 149.59 39.80 -5 -2 21 95.69 39.00 -2 5 21 162.68 38.50 5 2 21 147.99 11.60 2 -5 21 163.28 44.10 -5 -2 21 145.19 11.10 5 2 21 114.19 45.70 0 -5 -21 257.97 14.90 5 0 -21 228.88 14.80 -5 0 -21 232.68 14.70 5 0 -21 271.47 17.80 0 -5 21 223.88 13.80 5 0 21 148.39 41.60 0 5 21 220.28 13.90 5 0 21 228.18 14.10 0 5 21 131.59 38.50 -5 0 21 267.57 15.00 0 5 21 263.37 54.99 5 0 21 222.18 47.70 -5 0 21 162.48 41.40 0 -5 21 140.89 42.40 5 -2 -21 264.87 17.40 5 -2 -21 216.48 14.60 2 5 -21 225.78 14.40 -2 -5 -21 234.18 14.20 -5 2 -21 237.28 14.50 5 -2 21 215.18 13.60 2 5 21 174.78 51.39 2 5 21 285.27 46.50 -2 -5 21 219.88 13.70 5 -2 21 248.88 50.79 -5 2 21 238.28 14.30 2 5 21 234.28 14.10 5 -2 21 222.88 46.60 -2 -5 21 206.68 47.90 -5 2 21 169.28 43.90 5 -4 -21 149.49 13.40 5 -4 -21 123.59 11.90 -5 4 -21 171.48 11.50 -4 -5 -21 147.19 11.20 4 5 21 161.08 48.10 -4 -5 21 107.79 41.20 5 -4 21 121.79 45.30 4 5 21 174.48 41.00 5 -4 21 193.28 44.20 -5 4 21 133.79 44.10 4 5 21 151.88 11.90 -4 -5 21 134.19 10.50 -5 4 21 145.89 11.20 6 5 -21 138.19 12.90 5 -6 -21 115.79 11.30 -6 -5 -21 134.59 10.70 -5 6 -21 127.49 10.40 5 -6 -21 155.48 12.90 -5 6 21 129.89 10.70 6 5 21 126.59 11.40 -6 -5 21 77.29 44.70 -5 6 21 67.49 39.90 5 -6 21 105.99 49.10 6 5 21 144.89 56.89 5 -6 21 96.69 47.20 -6 -5 21 130.69 10.50 6 3 -21 40.30 7.90 3 -6 -21 34.30 7.70 -3 6 -21 34.00 6.40 -6 -3 -21 25.50 6.10 3 -6 -21 27.80 6.20 6 3 21 49.20 35.70 6 3 21 -10.80 45.20 -6 -3 21 28.90 6.10 -6 -3 21 32.50 38.40 -3 6 21 65.99 37.40 3 -6 21 44.10 40.00 3 -6 21 26.60 6.30 6 3 21 25.20 6.20 -3 6 21 34.50 7.00 6 1 -21 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133.59 11.90 -4 11 21 138.69 10.90 11 4 21 159.58 11.50 -4 11 21 119.49 10.80 -11 -2 -21 351.76 18.00 2 -11 -21 366.46 18.40 2 -11 -21 351.06 18.90 11 2 -21 343.77 20.80 -2 11 -21 353.26 17.90 -2 11 21 343.37 18.00 11 2 21 347.97 18.10 -11 -2 21 386.66 18.50 2 -11 21 340.97 17.30 -2 11 21 370.66 19.20 -11 0 -21 129.19 10.30 0 -11 -21 123.59 10.30 11 0 -21 128.09 13.10 0 11 -21 115.89 10.70 0 11 21 124.29 11.10 0 -11 21 116.59 10.20 -11 0 21 133.99 10.50 -2 -11 -21 19.50 5.50 2 11 -21 15.30 6.20 11 -2 -21 12.30 6.30 2 11 21 29.70 6.50 -11 2 21 21.20 5.40 -2 -11 21 32.30 6.00 11 -4 -21 376.06 21.80 -4 -11 -21 342.97 18.00 4 11 -21 310.97 18.50 -11 4 -21 317.27 17.10 4 11 21 332.57 18.80 -11 4 21 351.56 18.10 -4 -11 21 315.27 17.30 -6 -11 -21 28.90 6.60 -11 6 -21 39.10 7.00 11 -6 -21 23.40 7.40 -11 6 21 23.70 6.50 6 11 21 30.10 7.50 -6 -11 21 25.00 6.30 -8 -11 -21 21.00 6.30 11 -8 -21 15.40 7.30 -11 8 -21 13.70 6.40 -8 -11 21 20.70 6.40 -11 8 21 12.60 6.70 8 11 21 19.80 7.60 -11 10 -21 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-7 0 -25 66.09 9.50 0 -7 -25 42.10 7.60 0 -7 25 50.59 7.50 0 7 25 37.80 9.00 -7 0 25 62.99 9.10 -7 2 -25 114.29 12.10 -2 -7 -25 86.79 9.70 7 -2 -25 99.69 13.00 2 7 -25 82.29 10.40 -2 -7 -25 98.59 11.00 2 7 25 93.99 11.30 -2 -7 25 100.59 10.20 -7 2 25 76.39 9.70 7 -4 -25 83.09 12.30 -4 -7 -25 52.89 8.60 -7 4 -25 71.79 9.70 4 7 -25 68.49 9.70 4 7 25 62.89 9.90 -4 -7 25 53.49 8.60 -7 4 25 67.29 9.60 6 7 -25 34.50 7.90 7 -6 -25 54.09 10.20 -7 6 -25 48.40 8.80 -6 -7 -25 34.50 8.00 6 7 25 26.40 7.90 -6 -7 25 27.70 7.50 -7 6 25 23.00 7.00 -8 -7 -25 8.10 6.50 -7 8 -25 19.10 7.50 -8 -7 25 9.20 6.20 -8 -5 -25 95.89 10.30 5 -8 -25 72.99 10.00 8 5 -25 87.29 11.50 -5 8 -25 91.19 10.20 8 5 25 96.69 10.70 -8 -5 25 106.29 11.30 -5 8 25 98.19 10.70 3 -8 -25 264.17 16.80 -3 8 -25 273.77 15.80 8 3 -25 270.17 18.60 -8 -3 -25 285.97 16.60 8 3 25 221.88 15.10 -3 8 25 261.27 17.30 -8 -3 25 282.87 16.50 -3 8 25 290.27 19.70 8 1 -25 140.79 15.50 1 -8 -25 135.89 11.60 -1 8 -25 141.89 12.30 -8 -1 -25 121.59 12.60 1 -8 -25 135.19 12.50 -1 8 25 110.09 12.50 -8 -1 25 150.38 12.60 1 -8 25 117.69 11.70 -1 -8 -25 25.10 7.20 -1 -8 -25 20.70 6.70 8 -1 -25 24.60 9.60 1 8 -25 27.20 7.20 -8 1 -25 39.20 8.30 -1 -8 25 19.50 6.40 1 8 25 30.60 8.20 -8 1 25 16.20 7.10 -3 -8 -25 9.20 6.60 -3 -8 -25 7.40 6.60 -8 3 -25 4.80 6.90 3 8 -25 -0.50 5.90 8 -3 -25 17.20 9.20 -3 -8 25 12.70 6.50 3 8 25 9.10 7.30 -8 3 25 11.60 6.70 5 8 -25 185.78 17.40 8 -5 -25 241.28 17.40 -5 -8 -25 236.38 15.00 -8 5 -25 222.78 15.20 -5 -8 25 251.77 15.40 5 8 25 235.98 15.20 -8 5 25 230.18 15.40 -7 -8 -25 59.19 8.40 -8 7 -25 71.69 9.30 7 8 25 48.10 11.40 -7 -8 25 67.59 8.60 -9 -6 -25 158.38 12.40 -9 -6 25 169.88 12.50 -6 9 25 152.18 14.20 -4 9 -25 40.20 13.40 -9 -4 -25 44.60 7.40 9 4 -25 39.40 9.20 -4 9 25 34.30 8.70 -9 -4 25 44.20 8.10 9 2 -25 80.09 11.20 -9 -2 -25 75.19 9.50 -2 9 25 71.89 10.50 0 9 -25 124.69 12.50 9 0 -25 164.38 15.90 -9 0 -25 151.88 12.90 0 -9 -25 153.18 12.80 0 -9 25 107.29 14.00 0 9 25 150.98 14.30 -9 0 25 152.68 12.90 -2 -9 -25 39.20 8.30 -9 2 -25 39.40 8.10 2 9 -25 32.80 10.90 9 -2 -25 30.30 9.30 -9 2 25 40.10 8.00 2 9 25 44.90 8.90 -2 -9 25 25.50 6.80 9 -4 -25 96.99 12.20 -4 -9 -25 83.39 9.40 -9 4 -25 66.19 9.00 4 9 25 84.09 9.80 -4 -9 25 73.59 8.90 -9 4 25 78.99 9.30 -6 -9 -25 22.50 6.80 -9 6 -25 21.20 6.50 6 9 25 14.70 7.40 -6 -9 25 16.90 6.80 -9 6 25 18.40 7.50 -10 -5 25 1.10 8.10 10 3 -25 14.50 8.40 -10 -3 -25 -1.90 5.50 -10 -3 25 4.20 6.00 -3 10 25 14.80 6.80 10 1 -25 246.38 17.80 -10 -1 -25 237.78 15.00 -10 -1 25 253.07 15.50 -1 10 25 250.27 16.40 10 -1 -25 193.58 16.90 -10 1 -25 170.88 13.30 -1 -10 -25 155.98 12.70 -10 1 25 163.78 13.10 1 10 25 163.98 14.40 10 -3 -25 13.30 8.20 -10 3 -25 13.40 6.60 -3 -10 -25 15.30 6.60 -10 3 25 15.20 6.90 3 10 25 10.80 7.00 -10 5 -25 75.99 12.40 -11 -2 25 0.40 7.40 11 0 -25 94.89 11.50 -11 0 -25 124.19 12.00 -11 0 25 97.89 11.00 0 11 25 93.99 10.30 11 -2 -25 14.40 9.20 -11 2 -25 14.00 11.00 2 11 25 -1.30 8.10 -11 2 25 6.50 7.40 0 0 -26 -3.00 4.80 0 0 26 -7.30 5.70 -1 1 -26 67.59 8.30 1 -1 -26 81.59 8.90 1 1 -26 72.09 8.40 -1 -1 -26 77.59 8.90 1 -1 -26 83.49 11.00 1 -1 26 95.19 9.70 -1 -1 26 72.59 8.90 -1 1 26 82.09 9.20 1 1 26 111.19 10.50 0 2 -26 13.60 5.80 2 0 -26 5.20 7.50 0 -2 -26 -0.60 5.20 -2 0 -26 3.40 5.40 2 0 -26 4.40 7.00 -2 0 26 3.70 5.10 0 -2 26 -3.90 5.60 2 0 26 2.20 4.90 -2 2 -26 20.10 6.50 -2 -2 -26 26.00 6.80 2 -2 -26 28.00 8.30 2 2 -26 31.10 9.30 2 -2 -26 24.60 7.30 -2 2 26 34.50 6.50 2 2 26 38.40 7.10 -2 -2 26 14.60 5.90 2 -2 26 15.00 5.90 3 1 -26 96.29 12.10 -1 3 -26 118.29 11.20 1 -3 -26 108.19 11.00 1 -3 -26 128.29 14.10 -3 -1 -26 118.09 11.40 -3 -1 26 115.59 10.80 1 -3 26 103.89 10.60 3 1 26 115.69 10.30 1 3 -26 260.07 16.10 -3 1 -26 286.57 16.80 -1 -3 -26 262.17 16.10 3 -1 -26 292.87 19.40 -3 1 26 263.17 15.60 3 -1 26 278.57 15.40 1 3 26 293.27 17.00 -1 -3 26 282.17 15.60 3 -3 -26 143.59 14.70 -3 -3 -26 122.89 11.90 3 3 -26 116.09 13.90 -3 3 -26 140.19 12.00 -3 -3 26 124.09 11.60 -3 3 26 115.39 11.20 3 3 26 136.19 11.60 -4 -2 -26 4.10 6.00 -2 4 -26 -1.00 5.70 2 -4 -26 3.40 7.00 2 -4 -26 -4.40 6.30 4 2 -26 -1.30 7.10 -4 -2 26 2.40 5.50 4 2 26 -0.10 5.20 -2 4 26 5.30 6.40 0 -4 -26 -11.00 6.20 -4 0 -26 10.40 6.40 0 4 -26 7.80 6.00 0 -4 -26 7.30 5.60 4 0 -26 9.70 8.60 0 4 26 7.30 6.40 0 -4 26 5.70 5.90 4 0 26 -7.70 5.50 -4 0 26 7.00 5.90 -2 -4 -26 24.90 6.90 2 4 -26 29.70 8.90 -4 2 -26 33.90 7.40 4 -2 -26 28.50 8.90 -4 2 26 20.40 6.60 -2 -4 26 21.10 6.30 2 4 26 29.20 7.50 -4 4 -26 0.80 6.80 4 4 -26 -4.70 6.80 4 -4 -26 4.30 7.30 -4 -4 -26 4.30 6.10 -4 -4 26 -0.20 6.20 -4 4 26 -6.40 5.00 4 4 26 -6.30 5.70 -5 -3 -26 54.89 8.40 5 3 -26 63.69 10.30 3 -5 -26 53.09 9.40 -3 5 -26 74.09 9.40 -3 5 26 64.59 8.90 5 3 26 64.89 8.10 -1 5 -26 178.48 13.40 1 -5 -26 211.18 16.10 5 1 -26 201.78 17.40 -5 -1 -26 183.18 14.30 1 -5 -26 213.28 13.70 5 1 26 188.58 12.80 -1 5 26 203.08 15.80 -5 -1 26 209.68 14.40 -1 -5 -26 182.88 15.10 -1 -5 -26 160.48 13.50 1 5 -26 193.58 15.70 -5 1 -26 191.88 14.20 5 -1 -26 196.28 17.30 1 5 26 176.48 14.70 -1 -5 26 159.38 12.30 -5 1 26 183.78 13.60 -3 -5 -26 107.89 12.10 3 5 -26 119.79 14.00 5 -3 -26 128.99 14.30 -5 3 -26 109.99 12.40 3 5 26 107.89 12.40 -3 -5 26 126.69 11.80 -5 3 26 125.79 12.00 -5 -5 -26 81.19 9.70 -5 5 -26 67.99 9.10 5 -5 -26 98.09 11.70 5 5 -26 92.99 11.60 -5 5 26 63.09 8.80 -5 -5 26 81.69 9.70 5 5 26 62.59 8.70 6 4 -26 10.00 7.40 -4 6 -26 10.60 6.20 4 -6 -26 -0.40 7.30 -6 -4 -26 -7.20 5.30 6 4 26 -4.10 5.80 -6 -4 26 -5.80 5.90 2 -6 -26 7.50 7.20 -2 6 -26 1.90 6.20 6 2 -26 -3.30 6.60 -6 -2 -26 6.40 6.00 -6 -2 26 2.60 6.10 -2 6 26 3.00 7.20 6 0 -26 -4.30 7.40 0 -6 -26 2.30 6.60 -6 0 -26 7.10 6.80 0 -6 -26 -4.90 5.60 -6 0 26 -5.50 6.00 0 6 26 -0.50 6.10 6 -2 -26 47.30 10.30 -2 -6 -26 67.99 9.00 -6 2 -26 59.99 9.00 2 6 -26 56.89 9.80 -2 -6 -26 63.39 9.10 2 6 26 74.69 10.00 -6 2 26 73.19 9.70 -2 -6 26 56.99 7.90 -4 -6 -26 3.20 6.30 6 -4 -26 5.50 8.00 4 6 -26 7.10 7.20 -6 4 -26 -6.60 5.90 -4 -6 26 -1.30 5.80 4 6 26 1.00 6.20 -6 4 26 -3.30 5.80 -6 -6 -26 -1.80 5.50 -6 6 -26 12.30 9.40 -6 -6 26 3.20 6.00 -7 -5 -26 222.88 14.10 -7 -5 26 198.88 13.90 7 3 -26 211.38 16.40 3 -7 -26 204.58 20.10 -7 -3 -26 203.28 14.00 -7 -3 26 222.28 14.60 -3 7 26 201.68 15.70 1 -7 -26 119.79 13.00 7 1 -26 140.19 15.50 -7 -1 -26 134.69 12.30 -1 7 26 149.69 13.00 -7 -1 26 120.49 12.20 -1 -7 -26 67.39 8.60 7 -1 -26 60.89 11.30 -7 1 -26 64.39 8.60 1 7 -26 56.89 9.60 -1 -7 -26 47.90 9.20 -7 1 26 48.30 7.90 1 7 26 51.09 9.00 -3 -7 -26 127.29 12.30 7 -3 -26 175.48 15.50 3 7 -26 164.38 14.50 -7 3 -26 167.38 13.60 -3 -7 26 136.99 12.60 -7 3 26 159.08 13.20 3 7 26 163.98 13.70 -7 5 -26 173.78 13.00 -5 -7 -26 151.08 12.30 7 -5 -26 167.38 16.10 5 7 26 184.68 17.70 -8 -4 -26 14.90 6.50 -8 -4 26 23.60 7.30 -4 8 26 25.40 7.60 -8 -2 -26 6.40 5.90 8 2 -26 2.20 7.70 -2 8 26 4.20 6.90 -8 -2 26 -1.10 5.50 -8 0 -26 15.50 7.00 8 0 -26 8.10 8.60 0 8 26 5.50 6.80 -8 0 26 19.50 7.00 -2 -8 -26 21.10 10.30 -8 2 -26 22.20 6.70 8 -2 -26 21.20 8.10 -8 2 26 23.30 7.00 2 8 26 22.30 7.70 -8 4 -26 1.50 7.00 4 8 26 6.70 10.50 9 1 -26 106.09 14.00 -9 -1 -26 154.18 14.00 -1 9 26 141.79 13.40 -9 -1 26 143.59 15.60 9 -1 -26 287.77 19.50 -9 1 -26 268.67 16.50 1 9 26 246.08 17.30 0 -1 -27 69.19 15.00 1 0 -27 70.29 11.20 -1 0 -27 52.79 7.70 0 1 -27 70.19 11.30 0 -1 -27 57.69 10.80 0 -1 27 44.00 7.60 0 1 27 47.60 7.80 1 0 27 43.90 7.30 1 -2 -27 30.20 9.00 2 1 -27 33.50 8.60 -2 -1 -27 39.20 7.70 -1 2 27 31.40 7.90 2 1 27 23.60 6.70 -2 1 -27 47.60 7.80 -1 -2 -27 64.09 10.50 -1 -2 -27 59.49 8.00 1 2 -27 59.59 9.80 2 -1 -27 62.69 9.90 1 2 27 65.79 8.70 2 -3 -27 55.99 10.10 3 2 -27 49.40 9.30 -3 -2 -27 51.49 8.20 0 -3 -27 21.10 8.10 0 3 -27 23.70 8.60 3 0 -27 34.40 9.70 -3 0 -27 25.90 7.00 0 3 27 27.70 7.60 2 3 -27 38.00 8.90 -3 2 -27 47.20 8.10 -2 -3 -27 51.39 7.70 3 -2 -27 43.80 9.20 2 3 27 35.20 7.30 3 -4 -27 86.19 10.80 -4 -3 -27 87.09 10.20 4 3 -27 121.89 13.60 1 -4 -27 84.59 10.60 4 1 -27 60.09 10.10 -4 -1 -27 63.09 8.20 -1 4 27 72.89 9.50 -4 -1 27 89.79 12.90 4 -1 -27 46.50 9.60 1 4 -27 52.49 9.00 -4 1 -27 53.89 8.80 -1 -4 -27 58.19 9.70 1 4 27 63.59 9.10 4 -3 -27 134.09 14.30 -4 3 -27 138.39 19.20 3 4 -27 95.59 10.90 -3 -4 -27 104.59 11.60 5 2 -27 34.10 9.30 -5 -2 -27 39.10 7.10 2 -5 -27 42.20 12.80 -2 5 27 36.10 7.70 -5 0 -27 34.20 7.20 0 5 -27 26.80 7.50 5 0 -27 37.80 9.20 0 -5 -27 30.10 8.90 0 5 27 25.20 7.60 5 -2 -27 44.50 9.30 -5 2 -27 58.49 11.80 2 5 -27 47.80 8.90 2 5 27 39.80 8.20 6 1 -27 75.59 10.00 -6 -1 -27 66.89 11.30 -1 6 27 58.69 8.90 6 -1 -27 121.09 14.20 1 6 27 123.69 14.60 0 0 -28 120.49 18.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 67923 _olex2_submission_special_instructions 'No special instructions were received' _site XU loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pt1 Pt 0.500000 0.750000 0.625000 0.01962(5) Uani 1 4 d S T P . . Si1 Si 0.13632(2) 0.60536(3) 0.54018(2) 0.02854(11) Uani 1 1 d . . . . . N1 N 0.46939(7) 0.65130(7) 0.61694(6) 0.0212(3) Uani 1 1 d . . . . . C1 C 0.51215(9) 0.59482(8) 0.61878(8) 0.0215(3) Uani 1 1 d . . . . . C11 C 0.40761(9) 0.55880(8) 0.57948(8) 0.0232(3) Uani 1 1 d . . . . . C4 C 0.44768(9) 0.42320(9) 0.55359(8) 0.0252(3) Uani 1 1 d . . . . . C13 C 0.34527(8) 0.67123(8) 0.60561(8) 0.0221(3) Uani 1 1 d . . . . . C2 C 0.47533(8) 0.53551(8) 0.59414(8) 0.0229(3) Uani 1 1 d . . . . . C3 C 0.49545(9) 0.46903(9) 0.58063(9) 0.0263(4) Uani 1 1 d . . . . . H3 H 0.541165 0.454138 0.589457 0.032 Uiso 1 1 calc R U . . . C9 C 0.37966(9) 0.44625(9) 0.53964(9) 0.0265(4) Uani 1 1 d . . . . . C14 C 0.27961(9) 0.64306(8) 0.58743(8) 0.0240(3) Uani 1 1 d . . . . . C10 C 0.36043(9) 0.51505(9) 0.55281(9) 0.0276(4) Uani 1 1 d . . . . . H10 H 0.315229 0.530953 0.543307 0.033 Uiso 1 1 calc R U . . . C12 C 0.40467(8) 0.63109(8) 0.59773(8) 0.0216(3) Uani 1 1 d . . . . . C8 C 0.33258(10) 0.39883(10) 0.51269(9) 0.0326(4) Uani 1 1 d . . . . . H8 H 0.287081 0.413641 0.502927 0.039 Uiso 1 1 calc R U . . . C15 C 0.22431(9) 0.62270(9) 0.56946(9) 0.0287(4) Uani 1 1 d . . . . . C5 C 0.46601(10) 0.35386(9) 0.53914(9) 0.0297(4) Uani 1 1 d . . . . . H5 H 0.511562 0.338038 0.547320 0.036 Uiso 1 1 calc R U . . . C6 C 0.41908(10) 0.30992(9) 0.51374(9) 0.0311(4) Uani 1 1 d . . . . . H6 H 0.432002 0.263630 0.504805 0.037 Uiso 1 1 calc R U . . . C7 C 0.35158(10) 0.33256(10) 0.50062(9) 0.0324(4) Uani 1 1 d . . . . . H7 H 0.319089 0.301373 0.483228 0.039 Uiso 1 1 calc R U . . . C22 C 0.13084(11) 0.51687(11) 0.50393(10) 0.0368(4) Uani 1 1 d . . . . . H22 H 0.081926 0.510955 0.490043 0.044 Uiso 1 1 calc R U . . . C19 C 0.07407(10) 0.61420(11) 0.60645(10) 0.0358(4) Uani 1 1 d . . . . . H19 H 0.067737 0.664812 0.613825 0.043 Uiso 1 1 calc R U . . . C20 C 0.10022(12) 0.58288(12) 0.66695(10) 0.0423(5) Uani 1 1 d . . . . . H20A H 0.103698 0.532589 0.662668 0.063 Uiso 1 1 calc R U . . . H20B H 0.067841 0.594077 0.700137 0.063 Uiso 1 1 calc R U . . . H20C H 0.145832 0.601989 0.676687 0.063 Uiso 1 1 calc R U . . . C16 C 0.12230(12) 0.67313(12) 0.47945(11) 0.0435(5) Uani 1 1 d . . . . . H16 H 0.162114 0.669045 0.450353 0.052 Uiso 1 1 calc R U . . . C23 C 0.17569(14) 0.51041(13) 0.44665(11) 0.0504(6) Uani 1 1 d . . . . . H23A H 0.160899 0.544519 0.416058 0.076 Uiso 1 1 calc R U . . . H23B H 0.170923 0.463825 0.429486 0.076 Uiso 1 1 calc R U . . . H23C H 0.224123 0.518717 0.457573 0.076 Uiso 1 1 calc R U . . . C24 C 0.14555(15) 0.45791(12) 0.54847(12) 0.0521(6) Uani 1 1 d . . . . . H24A H 0.191200 0.464514 0.567078 0.078 Uiso 1 1 calc R U . . . H24B H 0.144649 0.413892 0.526203 0.078 Uiso 1 1 calc R U . . . H24C H 0.110258 0.457404 0.580792 0.078 Uiso 1 1 calc R U . . . C21 C 0.00236(12) 0.58460(17) 0.59060(13) 0.0616(8) Uani 1 1 d . . . . . H21A H -0.014550 0.605876 0.552570 0.092 Uiso 1 1 calc R U . . . H21B H -0.029892 0.594606 0.624184 0.092 Uiso 1 1 calc R U . . . H21C H 0.005881 0.534475 0.584949 0.092 Uiso 1 1 calc R U . . . C18 C 0.05702(15) 0.66259(15) 0.44081(14) 0.0631(7) Uani 1 1 d . . . . . H18A H 0.057121 0.615882 0.423402 0.095 Uiso 1 1 calc R U . . . H18B H 0.056022 0.696607 0.407439 0.095 Uiso 1 1 calc R U . . . H18C H 0.016133 0.668543 0.466870 0.095 Uiso 1 1 calc R U . . . C17 C 0.12517(18) 0.74631(14) 0.50521(16) 0.0732(9) Uani 1 1 d . . . . . H17A H 0.085825 0.753742 0.532806 0.110 Uiso 1 1 calc R U . . . H17B H 0.123165 0.779623 0.471315 0.110 Uiso 1 1 calc R U . . . H17C H 0.168348 0.752617 0.528074 0.110 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pt1 0.01546(6) 0.01546(6) 0.02793(8) 0.000 0.000 0.000 Si1 0.0206(2) 0.0289(2) 0.0361(3) -0.0018(2) -0.00597(19) -0.00243(18) N1 0.0170(6) 0.0183(7) 0.0282(7) 0.0003(5) -0.0009(5) 0.0000(5) C1 0.0205(8) 0.0150(7) 0.0290(9) 0.0012(6) 0.0009(6) 0.0007(6) C11 0.0202(8) 0.0191(8) 0.0303(9) -0.0004(6) 0.0000(7) 0.0013(6) C4 0.0261(9) 0.0202(8) 0.0295(9) -0.0014(7) 0.0010(7) 0.0006(6) C13 0.0186(8) 0.0189(8) 0.0288(8) 0.0004(6) -0.0024(6) -0.0006(6) C2 0.0200(8) 0.0197(8) 0.0291(9) 0.0010(7) -0.0003(7) -0.0007(6) C3 0.0222(8) 0.0203(8) 0.0364(10) -0.0013(7) -0.0018(7) 0.0021(6) C9 0.0253(8) 0.0216(8) 0.0328(9) -0.0026(7) -0.0010(7) 0.0001(7) C14 0.0210(8) 0.0190(8) 0.0322(9) -0.0024(7) -0.0009(7) 0.0025(6) C10 0.0219(8) 0.0218(8) 0.0390(10) -0.0040(7) -0.0038(7) 0.0015(6) C12 0.0184(8) 0.0180(8) 0.0283(8) -0.0001(6) -0.0023(6) -0.0024(6) C8 0.0282(9) 0.0273(9) 0.0423(11) -0.0084(8) -0.0040(8) 0.0003(7) C15 0.0236(9) 0.0252(9) 0.0375(10) -0.0037(7) -0.0023(7) 0.0007(7) C5 0.0292(9) 0.0220(8) 0.0380(10) -0.0033(7) -0.0014(8) 0.0048(7) C6 0.0375(10) 0.0197(8) 0.0361(10) -0.0048(7) 0.0015(8) 0.0018(7) C7 0.0338(10) 0.0247(9) 0.0386(10) -0.0084(8) -0.0027(8) -0.0043(7) C22 0.0331(10) 0.0362(11) 0.0411(11) -0.0067(9) -0.0054(8) -0.0072(8) C19 0.0253(9) 0.0400(11) 0.0421(11) -0.0073(9) -0.0028(8) -0.0021(8) C20 0.0401(12) 0.0431(12) 0.0436(12) -0.0001(10) 0.0028(9) -0.0041(9) C16 0.0369(11) 0.0414(12) 0.0523(13) 0.0100(10) -0.0086(10) 0.0011(9) C23 0.0597(15) 0.0501(14) 0.0415(12) -0.0073(10) 0.0012(11) 0.0040(11) C24 0.0677(16) 0.0318(11) 0.0568(15) 0.0007(10) 0.0075(12) -0.0030(11) C21 0.0269(11) 0.102(2) 0.0558(16) -0.0195(15) 0.0028(10) -0.0151(12) C18 0.0572(16) 0.0641(17) 0.0680(18) 0.0143(14) -0.0276(14) 0.0038(13) C17 0.087(2) 0.0386(14) 0.094(2) 0.0159(14) -0.0317(18) 0.0004(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pt Pt -5.3886 5.5592 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2153 0.2529 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Pt1 N1 169.99(8) . 6_564 ? N1 Pt1 N1 90.437(7) . 15_566 ? N1 Pt1 N1 169.99(8) 12_767 15_566 ? N1 Pt1 N1 90.436(7) 6_564 12_767 ? N1 Pt1 N1 90.436(7) . 12_767 ? N1 Pt1 N1 90.436(7) 6_564 15_566 ? C15 Si1 C22 111.12(9) . . ? C15 Si1 C19 107.98(9) . . ? C15 Si1 C16 104.37(9) . . ? C19 Si1 C22 111.43(10) . . ? C16 Si1 C22 109.33(10) . . ? C16 Si1 C19 112.41(10) . . ? C1 N1 Pt1 125.30(11) . . ? C1 N1 C12 109.34(13) . . ? C12 N1 Pt1 124.40(11) . . ? N1 C1 C13 124.08(15) . 12_767 ? N1 C1 C2 108.84(14) . . ? C13 C1 C2 126.96(15) 12_767 . ? C2 C11 C12 106.24(14) . . ? C10 C11 C2 120.78(15) . . ? C10 C11 C12 132.98(16) . . ? C3 C4 C9 119.90(15) . . ? C3 C4 C5 121.47(16) . . ? C9 C4 C5 118.63(16) . . ? C1 C13 C14 116.83(15) 15_566 . ? C12 C13 C1 124.32(15) . 15_566 ? C12 C13 C14 118.84(15) . . ? C11 C2 C1 106.50(14) . . ? C3 C2 C1 132.72(16) . . ? C3 C2 C11 120.63(16) . . ? C4 C3 H3 120.3 . . ? C2 C3 C4 119.46(16) . . ? C2 C3 H3 120.3 . . ? C10 C9 C4 119.76(16) . . ? C10 C9 C8 121.61(17) . . ? C8 C9 C4 118.63(16) . . ? C15 C14 C13 175.9(2) . . ? C11 C10 C9 119.46(16) . . ? C11 C10 H10 120.3 . . ? C9 C10 H10 120.3 . . ? N1 C12 C11 108.67(14) . . ? N1 C12 C13 123.57(15) . . ? C13 C12 C11 126.85(15) . . ? C9 C8 H8 119.5 . . ? C7 C8 C9 121.06(18) . . ? C7 C8 H8 119.5 . . ? C14 C15 Si1 171.37(16) . . ? C4 C5 H5 119.6 . . ? C6 C5 C4 120.83(17) . . ? C6 C5 H5 119.6 . . ? C5 C6 H6 119.8 . . ? C5 C6 C7 120.47(17) . . ? C7 C6 H6 119.8 . . ? C8 C7 C6 120.37(17) . . ? C8 C7 H7 119.8 . . ? C6 C7 H7 119.8 . . ? Si1 C22 H22 106.4 . . ? C23 C22 Si1 112.57(15) . . ? C23 C22 H22 106.4 . . ? C23 C22 C24 110.61(19) . . ? C24 C22 Si1 113.77(15) . . ? C24 C22 H22 106.4 . . ? Si1 C19 H19 106.8 . . ? C20 C19 Si1 114.13(14) . . ? C20 C19 H19 106.8 . . ? C20 C19 C21 110.0(2) . . ? C21 C19 Si1 111.76(15) . . ? C21 C19 H19 106.8 . . ? C19 C20 H20A 109.5 . . ? C19 C20 H20B 109.5 . . ? C19 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? Si1 C16 H16 106.1 . . ? C18 C16 Si1 114.30(17) . . ? C18 C16 H16 106.1 . . ? C17 C16 Si1 112.61(18) . . ? C17 C16 H16 106.1 . . ? C17 C16 C18 110.8(2) . . ? C22 C23 H23A 109.5 . . ? C22 C23 H23B 109.5 . . ? C22 C23 H23C 109.5 . . ? H23A C23 H23B 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C22 C24 H24A 109.5 . . ? C22 C24 H24B 109.5 . . ? C22 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C19 C21 H21A 109.5 . . ? C19 C21 H21B 109.5 . . ? C19 C21 H21C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pt1 N1 2.0073(14) . ? Pt1 N1 2.0073(14) 6_564 ? Pt1 N1 2.0073(14) 15_566 ? Pt1 N1 2.0073(14) 12_767 ? Si1 C15 1.8484(19) . ? Si1 C22 1.888(2) . ? Si1 C19 1.886(2) . ? Si1 C16 1.881(2) . ? N1 C1 1.371(2) . ? N1 C12 1.377(2) . ? C1 C13 1.405(2) 12_767 ? C1 C2 1.453(2) . ? C11 C2 1.422(2) . ? C11 C10 1.374(2) . ? C11 C12 1.455(2) . ? C4 C3 1.410(2) . ? C4 C9 1.422(2) . ? C4 C5 1.423(2) . ? C13 C14 1.438(2) . ? C13 C12 1.398(2) . ? C2 C3 1.376(2) . ? C3 H3 0.9500 . ? C9 C10 1.412(2) . ? C9 C8 1.420(2) . ? C14 C15 1.205(2) . ? C10 H10 0.9500 . ? C8 H8 0.9500 . ? C8 C7 1.359(3) . ? C5 H5 0.9500 . ? C5 C6 1.361(3) . ? C6 H6 0.9500 . ? C6 C7 1.407(3) . ? C7 H7 0.9500 . ? C22 H22 1.0000 . ? C22 C23 1.523(3) . ? C22 C24 1.524(3) . ? C19 H19 1.0000 . ? C19 C20 1.534(3) . ? C19 C21 1.540(3) . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C16 H16 1.0000 . ? C16 C18 1.531(3) . ? C16 C17 1.524(4) . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Pt1 N1 C1 C13 20.0(2) . . . 12_767 ? Pt1 N1 C1 C2 -163.77(11) . . . . ? Pt1 N1 C12 C11 162.64(11) . . . . ? Pt1 N1 C12 C13 -27.6(2) . . . . ? N1 C1 C2 C11 -2.00(19) . . . . ? N1 C1 C2 C3 173.38(19) . . . . ? C1 N1 C12 C11 -6.66(19) . . . . ? C1 N1 C12 C13 163.10(16) . . . . ? C1 C13 C12 N1 3.1(3) 15_566 . . . ? C1 C13 C12 C11 170.98(17) 15_566 . . . ? C1 C2 C3 C4 -176.65(18) . . . . ? C11 C2 C3 C4 -1.8(3) . . . . ? C4 C9 C10 C11 -0.6(3) . . . . ? C4 C9 C8 C7 0.4(3) . . . . ? C4 C5 C6 C7 0.7(3) . . . . ? C13 C1 C2 C11 174.08(17) 12_767 . . . ? C13 C1 C2 C3 -10.5(3) 12_767 . . . ? C2 C11 C10 C9 -0.2(3) . . . . ? C2 C11 C12 N1 5.26(19) . . . . ? C2 C11 C12 C13 -164.07(17) . . . . ? C3 C4 C9 C10 0.2(3) . . . . ? C3 C4 C9 C8 -179.71(18) . . . . ? C3 C4 C5 C6 179.17(18) . . . . ? C9 C4 C3 C2 1.0(3) . . . . ? C9 C4 C5 C6 -1.4(3) . . . . ? C9 C8 C7 C6 -1.1(3) . . . . ? C14 C13 C12 N1 -175.92(16) . . . . ? C14 C13 C12 C11 -8.1(3) . . . . ? C10 C11 C2 C1 177.51(16) . . . . ? C10 C11 C2 C3 1.4(3) . . . . ? C10 C11 C12 N1 -174.10(19) . . . . ? C10 C11 C12 C13 16.6(3) . . . . ? C10 C9 C8 C7 -179.54(19) . . . . ? C12 N1 C1 C13 -170.80(16) . . . 12_767 ? C12 N1 C1 C2 5.41(19) . . . . ? C12 C11 C2 C1 -1.95(19) . . . . ? C12 C11 C2 C3 -178.01(16) . . . . ? C12 C11 C10 C9 179.04(19) . . . . ? C8 C9 C10 C11 179.35(18) . . . . ? C15 Si1 C22 C23 -64.81(18) . . . . ? C15 Si1 C22 C24 62.03(19) . . . . ? C15 Si1 C19 C20 -41.15(17) . . . . ? C15 Si1 C19 C21 -166.78(18) . . . . ? C15 Si1 C16 C18 170.68(19) . . . . ? C15 Si1 C16 C17 -61.7(2) . . . . ? C5 C4 C3 C2 -179.63(18) . . . . ? C5 C4 C9 C10 -179.21(18) . . . . ? C5 C4 C9 C8 0.9(3) . . . . ? C5 C6 C7 C8 0.6(3) . . . . ? C22 Si1 C19 C20 81.14(17) . . . . ? C22 Si1 C19 C21 -44.5(2) . . . . ? C22 Si1 C16 C18 51.7(2) . . . . ? C22 Si1 C16 C17 179.38(19) . . . . ? C19 Si1 C22 C23 174.72(15) . . . . ? C19 Si1 C22 C24 -58.44(19) . . . . ? C19 Si1 C16 C18 -72.6(2) . . . . ? C19 Si1 C16 C17 55.1(2) . . . . ? C16 Si1 C22 C23 49.86(19) . . . . ? C16 Si1 C22 C24 176.70(16) . . . . ? C16 Si1 C19 C20 -155.74(15) . . . . ? C16 Si1 C19 C21 78.6(2) . . . . ?