#------------------------------------------------------------------------------ #$Date: 2024-08-05 21:02:59 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293757 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571784.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571784 loop_ _publ_author_name 'Qu, Chulin' 'Gong, Xinxin' 'Sun, Yufen' 'Gao, Hu' 'Cai, Fangjian' 'Zhao, Yue' 'Wu, Fan' 'Shen, Zhen' _publ_section_title ; Synergistic meso-β regulation of porphyrins: squeezing the band gap into the near-infrared I/II region. ; _journal_issue 27 _journal_name_full 'Chemical science' _journal_page_first 10491 _journal_page_last 10498 _journal_paper_doi 10.1039/d4sc01806k _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C96 H108 Cl N4 Si4 Zn, C8 H20 N' _chemical_formula_sum 'C104 H128 Cl N5 Si4 Zn' _chemical_formula_weight 1661.29 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2022-08-29 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _audit_update_record ; 2024-01-13 deposited with the CCDC. 2024-06-03 downloaded from the CCDC. ; _cell_angle_alpha 107.001(3) _cell_angle_beta 106.988(3) _cell_angle_gamma 94.445(3) _cell_formula_units_Z 2 _cell_length_a 16.0410(10) _cell_length_b 17.7484(11) _cell_length_c 19.0998(12) _cell_measurement_reflns_used 9869 _cell_measurement_temperature 193.00 _cell_measurement_theta_max 54.55 _cell_measurement_theta_min 2.30 _cell_volume 4893.7(5) _computing_cell_refinement 'SAINT V8.40B (Bruker, 2019)' _computing_data_collection 'APEX4 V2021.10-0 (Bruker, 2021)' _computing_data_reduction 'SAINT V8.40B (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/2 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 193.00 _diffrn_detector CPAD _diffrn_detector_area_resol_mean 7.41 _diffrn_detector_type 'Bruker PHOTON II' _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE Metaljet PHOTON II' _diffrn_measurement_method '\w and \f shutterless scans' _diffrn_measurement_specimen_support 'nylon loop' _diffrn_radiation_monochromator 'Helios Multi-layer Optic' _diffrn_radiation_probe x-ray _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0820 _diffrn_reflns_av_unetI/netI 0.0875 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 53920 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 53.906 _diffrn_reflns_theta_min 2.229 _diffrn_source MetalJet _diffrn_source_current 2.86 _diffrn_source_power 0.19937059999999998 _diffrn_source_type 'Liquid Metal source' _diffrn_source_voltage 69.71 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.928 _exptl_absorpt_correction_T_max 0.7512 _exptl_absorpt_correction_T_min 0.5411 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1412 before and 0.0826 after correction. The Ratio of minimum to maximum transmission is 0.7203. The \l/2 correction factor is Not present. ; _exptl_crystal_density_diffrn 1.127 _exptl_crystal_description block _exptl_crystal_F_000 1780 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.1 _refine_diff_density_max 1.822 _refine_diff_density_min -1.332 _refine_diff_density_rms 0.096 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1230 _refine_ls_number_reflns 17849 _refine_ls_number_restraints 700 _refine_ls_restrained_S_all 1.118 _refine_ls_R_factor_all 0.1918 _refine_ls_R_factor_gt 0.1177 _refine_ls_shift/su_max 0.043 _refine_ls_shift/su_mean 0.003 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1200P)^2^+16.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2874 _refine_ls_wR_factor_ref 0.3321 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8933 _reflns_number_total 17849 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc01806k2.cif _cod_data_source_block 20220716syf2_0m _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_radiation_probe' value 'X-ray' was changed to 'x-ray' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas Adding full bibliography for 1571783--1571784.cif. ; _cod_database_code 1571784 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.913 _shelx_estimated_absorpt_t_min 0.889 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C105-C111 = C108-C111 = C113-C107 = C113-C112 = C106-C110 = C106-C109 1.53 with sigma of 0.005 C117-C121 = C115-C93 = C116-C114 = C119-C118 1.5 with sigma of 0.005 C92-C53 = C93-C89 = C81-C1 = C91-C85 1.5 with sigma of 0.005 N5-C89 = N5-C85 = N5-C81 = N5-C92 1.5 with sigma of 0.005 C94-C82 = C87-C82 1.53 with sigma of 0.005 N5-C115 = N5-C114 = N5-C119 = N5-C117 1.5 with sigma of 0.005 C103-C102 = C103-C97 = C98-C101 = C101-C95 = C96-C99 = C96-C100 1.53 with sigma of 0.005 C121-C117 1.53 with sigma of 0.005 C116-N5 2.6 with sigma of 0.005 N5-C91 2.6 with sigma of 0.005 C110-C109 2.5 with sigma of 0.005 N5-C118 2.6 with sigma of 0.005 C112-C107 2.5 with sigma of 0.005 C108-C105 2.5 with sigma of 0.005 C102-C97 2.5 with sigma of 0.005 C95-C98 2.5 with sigma of 0.005 C100-C99 2.5 with sigma of 0.005 C1-N5 2.6 with sigma of 0.005 C121-N5 2.6 with sigma of 0.005 C81-C1 \\sim C117-C121 with sigma of 0.02 N5-C91 \\sim N5-C53 \\sim N5-C1 \\sim N5-C93 with sigma of 0.02 C92-C53 \\sim C81-C1 \\sim C91-C85 with sigma of 0.02 N5-C92 \\sim N5-C81 \\sim N5-C85 with sigma of 0.02 C116-C114 \\sim C91-C85 with sigma of 0.02 C115-C93 \\sim C120-C89 with sigma of 0.02 N5-C92 \\sim N5-C119 with sigma of 0.02 N5-C114 \\sim N5-C85 with sigma of 0.02 N5-C81 \\sim N5-C117 with sigma of 0.02 N5-C115 \\sim N5-C89 with sigma of 0.02 Si5-C58 \\sim Si4-C58 with sigma of 0.02 Si5-C111 \\sim Si5-C106 \\sim Si5-C113 with sigma of 0.02 Si4-C101 \\sim Si4-C103 \\sim Si4-C96 with sigma of 0.02 Si4-C97 \\sim Si4-C102 with sigma of 0.02 C106-C111 \\sim C113-C111 \\sim C113-C106 with sigma of 0.02 C96-C101 \\sim C103-C101 \\sim C103-C96 with sigma of 0.02 Si5-C105 \\sim Si5-C108 with sigma of 0.02 C89-C81 \\sim C89-C85 \\sim C85-C81 \\sim C92-C89 \\sim C92-C81 \\sim C92-C85 with sigma of 0.02 C119-C118 \\sim C92-C53 with sigma of 0.02 C115-C117 \\sim C119-C117 \\sim C115-C119 \\sim C115-C114 \\sim C117-C114 \\sim C119-C114 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints N5 \\sim C1 \\sim C81 \\sim C89 \\sim C117 \\sim C114 \\sim C92 \\sim C115 \\sim C119 \\sim C85 \\sim C120 \\sim C121 \\sim C116 \\sim C53 \\sim C93 \\sim C118 \\sim C91: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 within 2A Si3 \\sim C77 \\sim C82 \\sim C83 \\sim C86 \\sim C87 \\sim C94 \\sim C104 \\sim C78 \\sim C88: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A Si4 \\sim C95 \\sim C96 \\sim C98 \\sim C100 \\sim C101 \\sim Si5 \\sim C105 \\sim C106 \\sim C108 \\sim C109 \\sim C110 \\sim C111 \\sim C99 \\sim C97 \\sim C102 \\sim C103 \\sim C107 \\sim C112 \\sim C113: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A Si2 \\sim C68 \\sim C72 \\sim C73 \\sim C75 \\sim C79 \\sim C80 \\sim C84 \\sim C90 \\sim C76: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A Uanis(C116) \\sim Ueq, Uanis(C91) \\sim Ueq, Uanis(C121) \\sim Ueq, Uanis(C1) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C116) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 4. Others Sof(Si4)=Sof(C95)=Sof(H95A)=Sof(H95B)=Sof(H95C)=Sof(C96)=Sof(H96)=Sof(C97)= Sof(H97A)=Sof(H97B)=Sof(H97C)=Sof(C98)=Sof(H98A)=Sof(H98B)=Sof(H98C)=Sof(C99)= Sof(H99A)=Sof(H99B)=Sof(H99C)=Sof(C100)=Sof(H10A)=Sof(H10B)=Sof(H10C)= Sof(C101)=Sof(H101)=Sof(C102)=Sof(H10D)=Sof(H10E)=Sof(H10F)=Sof(C103)= Sof(H103)=1-FVAR(1) Sof(Si5)=Sof(C105)=Sof(H10J)=Sof(H10K)=Sof(H10L)=Sof(C106)=Sof(H106)= Sof(C107)=Sof(H10M)=Sof(H10N)=Sof(H10O)=Sof(C108)=Sof(H10P)=Sof(H10Q)= Sof(H10R)=Sof(C109)=Sof(H10S)=Sof(H10T)=Sof(H10U)=Sof(C110)=Sof(H11A)= Sof(H11B)=Sof(H11C)=Sof(C111)=Sof(H111)=Sof(C112)=Sof(H11D)=Sof(H11E)= Sof(H11F)=Sof(C113)=Sof(H113)=FVAR(1) Sof(C93)=Sof(H93A)=Sof(H93B)=Sof(H93C)=Sof(C114)=Sof(H11G)=Sof(H11H)= Sof(C115)=Sof(H11I)=Sof(H11J)=Sof(C116)=Sof(H11K)=Sof(H11L)=Sof(H11M)= Sof(C117)=Sof(H11N)=Sof(H11O)=Sof(C118)=Sof(H11P)=Sof(H11Q)=Sof(H11R)= Sof(C119)=Sof(H11S)=Sof(H11T)=Sof(C121)=Sof(H12D)=Sof(H12E)=Sof(H12F)=1-FVAR(2) Sof(C1)=Sof(H1A)=Sof(H1B)=Sof(H1C)=Sof(C53)=Sof(H53A)=Sof(H53B)=Sof(H53C)= Sof(C81)=Sof(H81A)=Sof(H81B)=Sof(C85)=Sof(H85A)=Sof(H85B)=Sof(C89)=Sof(H89A)= Sof(H89B)=Sof(C91)=Sof(H91A)=Sof(H91B)=Sof(H91C)=Sof(C92)=Sof(H92A)=Sof(H92B)= Sof(C120)=Sof(H12A)=Sof(H12B)=Sof(H12C)=FVAR(2) 5.a Riding coordinates: C1(H1A,H1B,H1C), C93(H93A,H93B,H93C), C94(H94A,H94B,H94C), C109(H10S,H10T, H10U), C110(H11A,H11B,H11C), C116(H11K,H11L,H11M), C120(H12A,H12B,H12C), C121(H12D,H12E,H12F) 5.b Ternary CH refined with riding coordinates: C46(H46), C49(H49), C62(H62), C68(H68), C72(H72), C73(H73), C77(H77), C82(H82), C83(H83), C96(H96), C101(H101), C103(H103), C106(H106), C111(H111), C113(H113) 5.c Secondary CH2 refined with riding coordinates: C81(H81A,H81B), C85(H85A,H85B), C89(H89A,H89B), C92(H92A,H92B), C114(H11G, H11H), C115(H11I,H11J), C117(H11N,H11O), C119(H11S,H11T) 5.d Aromatic/amide H refined with riding coordinates: C12(H12), C21(H21), C27(H27), C28(H28), C33(H33), C34(H34), C35(H35), C36(H36), C37(H37), C38(H38), C42(H42), C43(H43), C44(H44), C50(H50), C52(H52), C54(H54), C57(H57), C59(H59), C61(H61), C63(H63), C66(H66), C67(H67), C70(H70), C74(H74) 5.e Idealised Me refined as rotating group: C53(H53A,H53B,H53C), C55(H55A,H55B,H55C), C60(H60A,H60B,H60C), C64(H64A,H64B, H64C), C65(H65A,H65B,H65C), C69(H69A,H69B,H69C), C71(H71A,H71B,H71C), C75(H75A, H75B,H75C), C76(H76A,H76B,H76C), C78(H78A,H78B,H78C), C79(H79A,H79B,H79C), C80(H80A,H80B,H80C), C84(H84A,H84B,H84C), C86(H86A,H86B,H86C), C87(H87A,H87B, H87C), C88(H88A,H88B,H88C), C90(H90A,H90B,H90C), C91(H91A,H91B,H91C), C95(H95A, H95B,H95C), C97(H97A,H97B,H97C), C98(H98A,H98B,H98C), C99(H99A,H99B,H99C), C100(H10A,H10B,H10C), C102(H10D,H10E,H10F), C104(H10G,H10H,H10I), C105(H10J, H10K,H10L), C107(H10M,H10N,H10O), C108(H10P,H10Q,H10R), C112(H11D,H11E,H11F), C118(H11P,H11Q,H11R) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL 20220716syf2_0m_a.res in P-1 20220716syf2_0m.res created by SHELXL-2019/2 at 21:07:46 on 29-Aug-2022 REM Old TITL 20220716syf2_0m in P-1 REM SHELXT solution in P-1: R1 0.270, Rweak 0.090, Alpha 0.087 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C96 N4 O7 Si3 Cl2 Zn CELL 1.34139 16.041 17.7484 19.0998 107.001 106.988 94.445 ZERR 2 0.001 0.0011 0.0012 0.003 0.003 0.003 LATT 1 SFAC C H Cl N Si Zn DISP C 0.0137 0.0067 57.1 DISP Cl 0.3281 0.5435 4162.2 DISP H 0 0 0.6 DISP N 0.0241 0.0134 109.9 DISP Si 0.2153 0.2529 1947.9 DISP Zn -2.7473 0.5279 4188.7 UNIT 208 256 2 10 8 2 DFIX 1.53 0.005 C105 C111 C108 C111 C113 C107 C113 C112 C106 C110 C106 C109 SIMU 0.005 0.01 2 N5 C1 C81 C89 C117 C114 C92 C115 C119 C85 C120 C121 C116 = C53 C93 C118 C91 DFIX 1.5 0.005 C117 C121 C115 C93 C116 C114 C119 C118 SADI C81 C1 C117 C121 SADI N5 C91 N5 C53 N5 C1 N5 C93 ISOR 0.01 0.02 C116 C91 C121 C1 DANG 2.6 0.005 C116 N5 DFIX 1.5 0.005 C92 C53 C93 C89 C81 C1 C91 C85 SADI C92 C53 C81 C1 C91 C85 SADI N5 C92 N5 C81 N5 C85 SIMU 0.01 0.02 2 Si3 C77 C82 C83 C86 C87 C94 C104 C78 C88 DFIX 1.5 0.005 N5 C89 N5 C85 N5 C81 N5 C92 DFIX 1.53 0.005 C94 C82 C87 C82 SADI C116 C114 C91 C85 DANG 2.6 0.005 N5 C91 SADI C115 C93 C120 C89 SADI N5 C92 N5 C119 SADI N5 C114 N5 C85 SADI N5 C81 N5 C117 DANG 2.5 0.005 C110 C109 SADI N5 C115 N5 C89 SIMU 0.01 0.02 2 Si4 C95 C96 C98 C100 C101 Si5 C105 C106 C108 C109 C110 = C111 C99 C97 C102 C103 C107 C112 C113 DFIX 1.5 0.005 N5 C115 N5 C114 N5 C119 N5 C117 DANG 2.6 0.005 N5 C118 SADI Si5 C58 Si4 C58 DFIX 1.53 0.005 C103 C102 C103 C97 C98 C101 C101 C95 C96 C99 C96 C100 DANG 2.5 0.005 C112 C107 DANG 2.5 0.005 C108 C105 DANG 2.5 0.005 C102 C97 DANG 2.5 0.005 C95 C98 DANG 2.5 0.005 C100 C99 SADI Si5 C111 Si5 C106 Si5 C113 SADI Si4 C101 Si4 C103 Si4 C96 SADI Si4 C97 Si4 C102 SADI C106 C111 C113 C111 C113 C106 SADI C96 C101 C103 C101 C103 C96 SIMU 0.01 0.02 2 Si2 C68 C72 C73 C75 C79 C80 C84 C90 C76 SADI Si5 C105 Si5 C108 SADI C89 C81 C89 C85 C85 C81 C92 C89 C92 C81 C92 C85 SADI C119 C118 C92 C53 SADI C115 C117 C119 C117 C115 C119 C115 C114 C117 C114 C119 C114 ISOR 0.002 0.004 C116 DFIX 1.53 0.005 C121 C117 DANG 2.6 0.005 C1 N5 DANG 2.6 0.005 C121 N5 L.S. 1 PLAN 10 SIZE 0.1 0.12 0.13 TEMP -80.15 CONF BOND list 4 MORE -1 BOND $H ABIN fmap 2 acta SIZE 0.1 0.12 0.13 TEMP -80.15 SHEL 999 0.83 REM REM REM WGHT 0.120000 16.000000 FVAR 0.36278 0.48831 0.64417 ZN01 6 0.202777 0.454341 0.331840 11.00000 0.06260 0.05715 = 0.04532 0.01809 0.01354 0.00766 CL1 3 0.355251 0.456817 0.375947 11.00000 0.06130 0.09855 = 0.07315 0.03532 0.01013 0.01169 SI1 5 0.172509 0.254523 0.638459 11.00000 0.07997 0.06496 = 0.05340 0.02573 0.01605 0.01179 SI2 5 0.278571 0.840718 0.684327 11.00000 0.09696 0.06441 = 0.05706 0.00734 0.01513 0.00828 SI3 5 0.309342 0.663680 0.050827 11.00000 0.11386 0.09303 = 0.05461 0.02129 0.02939 -0.02001 PART 2 SI4 5 0.217165 0.082798 0.002139 -21.00000 0.18019 0.11379 = 0.07601 0.02976 0.06449 0.07308 PART 1 C1 1 0.642852 0.554339 0.419461 31.00000 0.05133 0.06585 = 0.04750 0.03191 0.00594 -0.01628 AFIX 3 H1A 2 0.624642 0.504789 0.374911 31.00000 -1.50000 H1B 2 0.680362 0.544169 0.465231 31.00000 -1.50000 H1C 2 0.676192 0.595349 0.408211 31.00000 -1.50000 AFIX 0 PART 0 N1 4 0.164168 0.483941 0.429512 11.00000 0.06163 0.04920 = 0.04516 0.01771 0.01455 0.00523 N2 4 0.161527 0.331918 0.314018 11.00000 0.06061 0.06055 = 0.04278 0.01683 0.00975 0.01169 N3 4 0.207417 0.576253 0.335870 11.00000 0.06206 0.05846 = 0.04349 0.01534 0.01162 0.00238 N4 4 0.178208 0.423133 0.212724 11.00000 0.06030 0.05630 = 0.04395 0.01319 0.01350 0.01220 C2 1 0.163483 0.270152 0.253468 11.00000 0.06340 0.04819 = 0.05166 0.01627 0.01682 0.01187 C3 1 0.153512 0.347292 0.160696 11.00000 0.06523 0.05961 = 0.04260 0.01448 0.01647 0.01650 C4 1 0.115973 0.474512 0.530400 11.00000 0.05893 0.06149 = 0.04609 0.01865 0.01230 0.01305 C5 1 0.131562 0.557180 0.537693 11.00000 0.05785 0.05996 = 0.04219 0.01802 0.01389 0.00662 C6 1 0.164672 0.560429 0.474681 11.00000 0.05996 0.05258 = 0.04922 0.01466 0.01294 0.00668 C7 1 0.150330 0.216417 0.345788 11.00000 0.06490 0.05253 = 0.05207 0.01871 0.01611 0.01022 C8 1 0.124613 0.350374 0.081632 11.00000 0.06795 0.05465 = 0.04653 0.01717 0.01402 0.00842 C9 1 0.232329 0.604352 0.283758 11.00000 0.06335 0.05167 = 0.04820 0.02011 0.01015 0.00024 C10 1 0.140768 0.431443 0.463961 11.00000 0.05474 0.04780 = 0.04378 0.01466 0.01126 0.00545 C11 1 0.152650 0.302191 0.371369 11.00000 0.06051 0.04828 = 0.05399 0.01953 0.01409 0.00722 C12 1 0.078729 0.450938 0.578933 11.00000 0.06777 0.05902 = 0.05016 0.02089 0.01573 0.00854 AFIX 43 H12 2 0.065149 0.395739 0.572413 11.00000 -1.20000 AFIX 0 C13 1 0.160558 0.276708 0.180929 11.00000 0.06371 0.05525 = 0.05215 0.01973 0.01792 0.01476 C14 1 0.075541 0.590461 0.644520 11.00000 0.05846 0.06660 = 0.04626 0.01991 0.01370 0.01194 C15 1 0.061200 0.508521 0.637461 11.00000 0.05780 0.06329 = 0.04803 0.02042 0.01183 0.00942 C16 1 0.145634 0.350040 0.441931 11.00000 0.05997 0.05356 = 0.04554 0.01521 0.01273 0.00546 C17 1 0.198776 0.631130 0.465372 11.00000 0.07311 0.05031 = 0.04454 0.01662 0.01291 0.00595 C18 1 0.219643 0.702050 0.532103 11.00000 0.07849 0.05970 = 0.04742 0.01871 0.01746 0.00687 C19 1 0.219308 0.638244 0.400462 11.00000 0.06696 0.05783 = 0.04758 0.01970 0.01158 0.00622 C20 1 0.160128 0.195731 0.271193 11.00000 0.06750 0.05545 = 0.04901 0.01937 0.01283 0.01322 C21 1 0.109290 0.613330 0.592171 11.00000 0.07481 0.05209 = 0.04925 0.01407 0.01548 0.00869 AFIX 43 H21 2 0.116615 0.667785 0.594653 11.00000 -1.20000 AFIX 0 C22 1 0.150361 0.312470 0.500032 11.00000 0.06412 0.05624 = 0.04814 0.01922 0.01318 0.00823 C23 1 0.140022 0.431802 0.089398 11.00000 0.05668 0.06258 = 0.04314 0.01815 0.01298 0.01053 C24 1 0.050300 0.316651 -0.055249 11.00000 0.07881 0.06319 = 0.04771 0.01651 0.01258 0.01070 C25 1 0.217016 0.557030 0.206680 11.00000 0.06239 0.05810 = 0.04841 0.02273 0.01455 0.00674 C26 1 0.063458 0.399748 -0.047138 11.00000 0.07043 0.06296 = 0.04640 0.01793 0.01491 0.01111 C27 1 0.109727 0.456503 0.025109 11.00000 0.06886 0.05755 = 0.05198 0.01751 0.01721 0.00861 AFIX 43 H27 2 0.120489 0.511613 0.030409 11.00000 -1.20000 AFIX 0 C28 1 0.139392 0.157088 0.377650 11.00000 0.08245 0.05865 = 0.05545 0.02151 0.02194 0.00784 AFIX 43 H28 2 0.130209 0.170038 0.426421 11.00000 -1.20000 AFIX 0 C29 1 0.178501 0.475782 0.171668 11.00000 0.05973 0.06040 = 0.04743 0.02184 0.01761 0.00924 C30 1 0.256749 0.713126 0.393417 11.00000 0.06796 0.04831 = 0.05027 0.01857 0.01350 -0.00016 C31 1 0.265933 0.690004 0.318429 11.00000 0.06965 0.05887 = 0.05548 0.02183 0.01148 0.00225 C32 1 0.141940 0.078118 0.337667 11.00000 0.07652 0.05434 = 0.05275 0.02086 0.01002 0.00179 C33 1 0.027670 0.421782 -0.113667 11.00000 0.07560 0.07045 = 0.04822 0.02342 0.01423 0.01499 AFIX 43 H33 2 0.037372 0.476632 -0.109527 11.00000 -1.20000 AFIX 0 C34 1 0.025022 0.623533 0.755493 11.00000 0.07053 0.08474 = 0.05253 0.02064 0.01907 0.02249 AFIX 43 H34 2 0.014532 0.662484 0.796681 11.00000 -1.20000 AFIX 0 C35 1 0.025282 0.487600 0.690792 11.00000 0.06243 0.07314 = 0.05433 0.02668 0.01649 0.01219 AFIX 43 H35 2 0.011735 0.432732 0.685492 11.00000 -1.20000 AFIX 0 C36 1 0.080829 0.293313 0.010938 11.00000 0.08819 0.05545 = 0.04947 0.01656 0.01526 0.01089 AFIX 43 H36 2 0.071128 0.238402 0.006586 11.00000 -1.20000 AFIX 0 C37 1 0.281858 0.790807 0.440509 11.00000 0.08748 0.06013 = 0.05743 0.02070 0.02041 -0.00031 AFIX 43 H37 2 0.273354 0.805926 0.489584 11.00000 -1.20000 AFIX 0 C38 1 0.054803 0.647391 0.703800 11.00000 0.07844 0.06681 = 0.05601 0.01804 0.02061 0.01843 AFIX 43 H38 2 0.061637 0.702233 0.707567 11.00000 -1.20000 AFIX 0 C39 1 0.160710 0.285090 0.552939 11.00000 0.07817 0.05308 = 0.05530 0.01621 0.01661 0.01243 C40 1 0.156817 0.058371 0.265722 11.00000 0.07924 0.05225 = 0.05146 0.01609 0.01758 0.00469 C41 1 0.244191 0.594098 0.156403 11.00000 0.08160 0.06084 = 0.04529 0.01362 0.01899 0.00210 C42 1 -0.020242 0.366631 -0.183392 11.00000 0.08767 0.06803 = 0.04690 0.01825 0.00828 0.00900 AFIX 43 H42 2 -0.044839 0.383088 -0.226989 11.00000 -1.20000 AFIX 0 C43 1 0.162743 0.118857 0.232072 11.00000 0.08921 0.05251 = 0.04753 0.01614 0.02183 0.01096 AFIX 43 H43 2 0.168566 0.105819 0.182015 11.00000 -1.20000 AFIX 0 C44 1 0.010042 0.543883 0.748670 11.00000 0.07618 0.07733 = 0.04571 0.02517 0.01768 0.01724 AFIX 43 H44 2 -0.011131 0.528341 0.784833 11.00000 -1.20000 AFIX 0 C45 1 0.172650 0.210394 0.123442 11.00000 0.08789 0.06288 = 0.05511 0.02665 0.02739 0.02054 C46 1 0.194709 0.349347 0.722360 11.00000 0.08369 0.08859 = 0.05230 0.02042 0.01829 0.01780 AFIX 13 H46 2 0.141768 0.375428 0.709768 11.00000 -1.20000 AFIX 0 C47 1 0.334339 0.825321 0.343787 11.00000 0.10172 0.07063 = 0.05726 0.01735 0.02459 -0.01476 C48 1 0.243161 0.759718 0.590869 11.00000 0.09504 0.06047 = 0.05821 0.01878 0.01947 0.00480 C49 1 0.064338 0.191678 0.621328 11.00000 0.09098 0.06639 = 0.06066 0.02612 0.02185 0.00798 AFIX 13 H49 2 0.068877 0.179418 0.670053 11.00000 -1.20000 AFIX 0 C50 1 0.303710 0.745961 0.294413 11.00000 0.10384 0.06020 = 0.04829 0.00943 0.02118 -0.00871 AFIX 43 H50 2 0.308989 0.730605 0.244111 11.00000 -1.20000 AFIX 0 C51 1 0.320657 0.849417 0.416869 11.00000 0.09486 0.05660 = 0.06731 0.01753 0.01763 -0.00567 C52 1 0.000921 0.261021 -0.129037 11.00000 0.12594 0.06040 = 0.04900 0.01861 0.01827 0.00483 AFIX 43 H52 2 -0.008406 0.205580 -0.135341 11.00000 -1.20000 AFIX 0 PART 1 C53 1 0.615852 0.797030 0.560997 31.00000 0.06459 0.05689 = 0.11238 0.04910 0.04203 0.01924 AFIX 137 H53A 2 0.556984 0.806363 0.535360 31.00000 -1.50000 H53B 2 0.661240 0.834250 0.556963 31.00000 -1.50000 H53C 2 0.623826 0.805649 0.615798 31.00000 -1.50000 AFIX 0 PART 0 C54 1 0.162820 -0.021710 0.228820 11.00000 0.10834 0.06145 = 0.05893 0.01671 0.02816 0.01106 AFIX 43 H54 2 0.172896 -0.035424 0.180399 11.00000 -1.20000 AFIX 0 C55 1 -0.011911 0.236292 0.606590 11.00000 0.08580 0.07817 = 0.07979 0.02463 0.02433 0.00483 AFIX 137 H55A 2 -0.000482 0.285436 0.650748 11.00000 -1.50000 H55B 2 -0.066723 0.202383 0.600024 11.00000 -1.50000 H55C 2 -0.017999 0.250004 0.559435 11.00000 -1.50000 AFIX 0 N5 4 0.541989 0.652554 0.471889 11.00000 0.09343 0.10291 = 0.11055 0.03615 0.00567 -0.00113 C56 1 0.269913 0.621799 0.114067 11.00000 0.09095 0.07295 = 0.05191 0.01907 0.02176 -0.00228 C57 1 0.131779 0.015899 0.369210 11.00000 0.12146 0.04965 = 0.06971 0.02007 0.03209 0.00056 AFIX 43 H57 2 0.120792 0.027761 0.417190 11.00000 -1.20000 AFIX 0 C58 1 0.188267 0.158910 0.075046 11.00000 0.11872 0.07683 = 0.05925 0.03046 0.03808 0.04280 C59 1 -0.033229 0.285110 -0.190692 11.00000 0.10676 0.07362 = 0.04626 0.01509 0.00428 -0.00131 AFIX 43 H59 2 -0.066400 0.246519 -0.239542 11.00000 -1.20000 AFIX 0 C60 1 0.042357 0.111839 0.556050 11.00000 0.08361 0.07444 = 0.08823 0.02408 0.01355 0.00070 AFIX 137 H60A 2 0.034988 0.121435 0.506780 11.00000 -1.50000 H60B 2 -0.012712 0.080943 0.552986 11.00000 -1.50000 H60C 2 0.090652 0.081762 0.566378 11.00000 -1.50000 AFIX 0 C61 1 0.137700 -0.061073 0.330992 11.00000 0.12309 0.05096 = 0.07915 0.02331 0.03730 0.00481 AFIX 43 H61 2 0.130342 -0.102318 0.352227 11.00000 -1.20000 AFIX 0 C62 1 0.270143 0.201252 0.653722 11.00000 0.08900 0.07075 = 0.07362 0.03566 0.01767 0.01358 AFIX 13 H62 2 0.324081 0.244057 0.676450 11.00000 -1.20000 AFIX 0 C63 1 0.154613 -0.078499 0.260648 11.00000 0.13296 0.05418 = 0.07195 0.01749 0.03608 0.01198 AFIX 43 H63 2 0.160353 -0.131496 0.235111 11.00000 -1.20000 AFIX 0 C64 1 0.202246 0.337032 0.799863 11.00000 0.11278 0.12089 = 0.05223 0.03351 0.02367 0.01790 AFIX 137 H64A 2 0.149774 0.300203 0.793618 11.00000 -1.50000 H64B 2 0.206387 0.388607 0.838878 11.00000 -1.50000 H64C 2 0.255403 0.314398 0.816719 11.00000 -1.50000 AFIX 0 C65 1 0.278840 0.144417 0.580014 11.00000 0.10417 0.09589 = 0.09378 0.03978 0.03452 0.03090 AFIX 137 H65A 2 0.229969 0.098601 0.557463 11.00000 -1.50000 H65B 2 0.335368 0.125459 0.592577 11.00000 -1.50000 H65C 2 0.276772 0.172665 0.542629 11.00000 -1.50000 AFIX 0 C66 1 0.350016 0.930002 0.465539 11.00000 0.15241 0.05882 = 0.06986 0.01129 0.03885 -0.01193 AFIX 43 H66 2 0.342512 0.946032 0.515001 11.00000 -1.20000 AFIX 0 C67 1 0.375232 0.885160 0.323280 11.00000 0.16910 0.07408 = 0.08961 0.01651 0.05144 -0.02491 AFIX 43 H67 2 0.384161 0.870827 0.274378 11.00000 -1.20000 AFIX 0 C68 1 0.191878 0.904031 0.682761 11.00000 0.11070 0.06170 = 0.09662 0.00776 0.00533 0.01164 AFIX 13 H68 2 0.215264 0.951756 0.731023 11.00000 -1.20000 AFIX 0 C69 1 0.273620 0.409263 0.731396 11.00000 0.15257 0.09403 = 0.08691 0.00383 0.03892 -0.03281 AFIX 137 H69A 2 0.328617 0.390664 0.752005 11.00000 -1.50000 H69B 2 0.273417 0.461557 0.767244 11.00000 -1.50000 H69C 2 0.269605 0.414123 0.680755 11.00000 -1.50000 AFIX 0 C70 1 0.388891 0.984978 0.442562 11.00000 0.20406 0.06543 = 0.09001 0.01357 0.06294 -0.03683 AFIX 43 H70 2 0.407080 1.039170 0.475609 11.00000 -1.20000 AFIX 0 C71 1 0.274892 0.158973 0.713593 11.00000 0.15538 0.09696 = 0.08049 0.04692 0.02147 0.03611 AFIX 137 H71A 2 0.279155 0.198258 0.763323 11.00000 -1.50000 H71B 2 0.327156 0.133147 0.720110 11.00000 -1.50000 H71C 2 0.221409 0.118405 0.695733 11.00000 -1.50000 AFIX 0 C72 1 0.383247 0.902379 0.692139 11.00000 0.11863 0.08741 = 0.12247 -0.01905 0.02039 -0.00459 AFIX 13 H72 2 0.361989 0.922003 0.647094 11.00000 -1.20000 AFIX 0 C73 1 0.286779 0.790482 0.758014 11.00000 0.13095 0.09988 = 0.06703 0.01815 0.02717 0.03289 AFIX 13 H73 2 0.224528 0.765593 0.748060 11.00000 -1.20000 AFIX 0 C74 1 0.402254 0.962499 0.371012 11.00000 0.21188 0.07665 = 0.09270 0.01661 0.06329 -0.04004 AFIX 43 H74 2 0.430149 1.001058 0.355602 11.00000 -1.20000 AFIX 0 C75 1 0.414710 0.980856 0.759268 11.00000 0.11493 0.08513 = 0.14587 -0.02576 -0.00008 0.00164 AFIX 137 H75A 2 0.367308 1.012675 0.756406 11.00000 -1.50000 H75B 2 0.466845 1.010731 0.756294 11.00000 -1.50000 H75C 2 0.430275 0.969795 0.808413 11.00000 -1.50000 AFIX 0 C76 1 0.336761 0.722720 0.751370 11.00000 0.16882 0.13768 = 0.09711 0.05459 0.03350 0.05373 AFIX 137 H76A 2 0.314733 0.685689 0.697901 11.00000 -1.50000 H76B 2 0.328482 0.694385 0.786518 11.00000 -1.50000 H76C 2 0.399905 0.743568 0.765326 11.00000 -1.50000 AFIX 0 C77 1 0.220723 0.726843 0.015939 11.00000 0.16704 0.11545 = 0.08157 0.03948 0.03747 0.00275 AFIX 13 H77 2 0.240625 0.752256 -0.018146 11.00000 -1.20000 AFIX 0 C78 1 0.133359 0.667426 -0.034379 11.00000 0.13261 0.14654 = 0.08487 0.04111 0.02299 0.01651 AFIX 137 H78A 2 0.109590 0.645200 -0.001390 11.00000 -1.50000 H78B 2 0.144845 0.623936 -0.073822 11.00000 -1.50000 H78C 2 0.090271 0.695485 -0.059817 11.00000 -1.50000 AFIX 0 C79 1 0.104563 0.864243 0.682613 11.00000 0.09743 0.09051 = 0.17257 0.00804 0.01910 0.02270 AFIX 137 H79A 2 0.075619 0.821441 0.632888 11.00000 -1.50000 H79B 2 0.066079 0.904043 0.690049 11.00000 -1.50000 H79C 2 0.115614 0.841554 0.724806 11.00000 -1.50000 AFIX 0 C80 1 0.176300 0.935252 0.613648 11.00000 0.17621 0.08053 = 0.13321 0.03318 -0.01375 0.03057 AFIX 137 H80A 2 0.231667 0.966623 0.617882 11.00000 -1.50000 H80B 2 0.130923 0.969163 0.613914 11.00000 -1.50000 H80C 2 0.156391 0.889849 0.565138 11.00000 -1.50000 AFIX 0 PART 1 C81 1 0.561029 0.570134 0.439227 31.00000 0.08834 0.09551 = 0.09994 0.03250 0.00564 -0.00432 AFIX 23 H81A 2 0.558177 0.542089 0.476522 31.00000 -1.20000 H81B 2 0.510492 0.542305 0.391246 31.00000 -1.20000 AFIX 0 PART 0 C82 1 0.409210 0.739163 0.111693 11.00000 0.15512 0.13947 = 0.09456 0.03088 0.03873 -0.04909 AFIX 13 H82 2 0.396408 0.773041 0.157991 11.00000 -1.20000 AFIX 0 C83 1 0.310167 0.583698 -0.032896 11.00000 0.18757 0.12545 = 0.09031 0.02110 0.05197 -0.01805 AFIX 13 H83 2 0.247007 0.555976 -0.058388 11.00000 -1.20000 AFIX 0 C84 1 0.317270 0.848706 0.841261 11.00000 0.22859 0.14618 = 0.06780 0.01920 0.03033 0.04359 AFIX 137 H84A 2 0.380606 0.870162 0.857460 11.00000 -1.50000 H84B 2 0.306917 0.820466 0.875859 11.00000 -1.50000 H84C 2 0.283813 0.892780 0.843776 11.00000 -1.50000 AFIX 0 PART 1 C85 1 0.504399 0.640686 0.533178 31.00000 0.10222 0.09939 = 0.10644 0.02908 0.00444 -0.00558 AFIX 23 H85A 2 0.499166 0.582889 0.526583 31.00000 -1.20000 H85B 2 0.550770 0.668928 0.583895 31.00000 -1.20000 AFIX 0 PART 0 C86 1 0.362228 0.517038 -0.010539 11.00000 0.18876 0.15433 = 0.13197 0.00918 0.02890 0.05911 AFIX 137 H86A 2 0.423209 0.541756 0.022736 11.00000 -1.50000 H86B 2 0.362838 0.476465 -0.057830 11.00000 -1.50000 H86C 2 0.332779 0.491739 0.017280 11.00000 -1.50000 AFIX 0 C87 1 0.439252 0.795188 0.072550 11.00000 0.19924 0.16131 = 0.14213 0.04798 0.06266 -0.06299 AFIX 137 H87A 2 0.472363 0.768076 0.039892 11.00000 -1.50000 H87B 2 0.477340 0.843882 0.112331 11.00000 -1.50000 H87C 2 0.387255 0.809414 0.040408 11.00000 -1.50000 AFIX 0 C88 1 0.214451 0.793670 0.084679 11.00000 0.27423 0.11994 = 0.12716 0.02986 0.08002 0.04091 AFIX 137 H88A 2 0.178253 0.830154 0.065702 11.00000 -1.50000 H88B 2 0.273982 0.823307 0.117407 11.00000 -1.50000 H88C 2 0.187086 0.770492 0.115103 11.00000 -1.50000 AFIX 0 PART 1 C89 1 0.473271 0.677072 0.416677 31.00000 0.09960 0.10970 = 0.12395 0.02572 0.00795 0.00231 AFIX 23 H89A 2 0.419878 0.634860 0.388420 31.00000 -1.20000 H89B 2 0.456293 0.727755 0.442198 31.00000 -1.20000 AFIX 0 PART 0 C90 1 0.452907 0.862561 0.674179 11.00000 0.16142 0.13266 = 0.20452 -0.03808 0.09774 -0.03465 AFIX 137 H90A 2 0.485148 0.846373 0.717971 11.00000 -1.50000 H90B 2 0.493775 0.899129 0.664491 11.00000 -1.50000 H90C 2 0.427243 0.815063 0.627845 11.00000 -1.50000 AFIX 0 PART 1 C91 1 0.420308 0.663375 0.541595 31.00000 0.06631 0.06289 = 0.06349 0.04592 -0.00650 -0.01346 AFIX 137 H91A 2 0.378345 0.657107 0.490448 31.00000 -1.50000 H91B 2 0.431389 0.719301 0.575040 31.00000 -1.50000 H91C 2 0.395383 0.628775 0.564883 31.00000 -1.50000 AFIX 0 C92 1 0.624347 0.711913 0.522230 31.00000 0.08711 0.10080 = 0.11430 0.03406 0.01282 -0.00009 AFIX 23 H92A 2 0.662750 0.713704 0.490305 31.00000 -1.20000 H92B 2 0.655954 0.691066 0.563455 31.00000 -1.20000 AFIX 0 PART 2 C93 1 0.489461 0.631381 0.316564 -31.00000 0.08966 0.11493 = 0.10779 0.03523 0.03152 -0.00378 AFIX 3 H93A 2 0.450921 0.582741 0.277054 -31.00000 -1.50000 H93B 2 0.551311 0.628361 0.320404 -31.00000 -1.50000 H93C 2 0.473511 0.678201 0.301984 -31.00000 -1.50000 AFIX 0 PART 0 C94 1 0.483880 0.695058 0.140757 11.00000 0.16717 0.25425 = 0.13286 0.07849 -0.01191 -0.06609 AFIX 3 H94A 2 0.541310 0.729948 0.157027 11.00000 -1.50000 H94B 2 0.481010 0.646268 0.098817 11.00000 -1.50000 H94C 2 0.476890 0.680878 0.184837 11.00000 -1.50000 AFIX 0 PART 2 C95 1 0.314820 0.028424 0.112760 -21.00000 0.16578 0.14134 = 0.11675 0.02301 0.07109 0.08702 AFIX 137 H95A 2 0.256315 0.030767 0.118670 -21.00000 -1.50000 H95B 2 0.359433 0.069009 0.157281 -21.00000 -1.50000 H95C 2 0.329175 -0.024795 0.110122 -21.00000 -1.50000 AFIX 0 C96 1 0.123203 -0.001286 -0.038489 -21.00000 0.19570 0.14048 = 0.10901 0.00898 0.04877 0.05952 AFIX 13 H96 2 0.133874 -0.036559 -0.085324 -21.00000 -1.20000 AFIX 0 C97 1 0.252228 0.208838 -0.057034 -21.00000 0.20030 0.14957 = 0.10575 0.03301 0.08203 0.04649 AFIX 137 H97A 2 0.208407 0.240843 -0.043982 -21.00000 -1.50000 H97B 2 0.261998 0.215384 -0.103391 -21.00000 -1.50000 H97C 2 0.308137 0.226850 -0.013603 -21.00000 -1.50000 AFIX 0 C98 1 0.385403 0.005364 0.009939 -21.00000 0.18922 0.16619 = 0.14716 -0.01375 0.02839 0.09140 AFIX 137 H98A 2 0.359858 -0.049563 -0.024895 -21.00000 -1.50000 H98B 2 0.434182 0.004486 0.054626 -21.00000 -1.50000 H98C 2 0.407827 0.036099 -0.017892 -21.00000 -1.50000 AFIX 0 C99 1 0.123503 -0.054948 0.010816 -21.00000 0.23685 0.15313 = 0.15629 0.00275 0.02405 0.02199 AFIX 137 H99A 2 0.160348 -0.095328 -0.000646 -21.00000 -1.50000 H99B 2 0.062809 -0.081609 -0.001010 -21.00000 -1.50000 H99C 2 0.147545 -0.022458 0.065852 -21.00000 -1.50000 AFIX 0 C100 1 0.029409 0.014257 -0.070868 -21.00000 0.21586 0.18424 = 0.14138 0.00699 0.02242 0.03380 AFIX 137 H10A 2 -0.011980 -0.036856 -0.096476 -21.00000 -1.50000 H10B 2 0.027997 0.042071 -0.108496 -21.00000 -1.50000 H10C 2 0.012155 0.047509 -0.028363 -21.00000 -1.50000 AFIX 0 C101 1 0.314095 0.044516 0.038016 -21.00000 0.18609 0.14799 = 0.11458 0.01629 0.04934 0.06807 AFIX 13 H101 2 0.352552 0.098523 0.065598 -21.00000 -1.20000 AFIX 0 C102 1 0.157921 0.081898 -0.156669 -21.00000 0.23843 0.18817 = 0.14247 0.03952 0.03351 0.03437 AFIX 137 H10D 2 0.171732 0.028934 -0.178080 -21.00000 -1.50000 H10E 2 0.167281 0.115437 -0.187304 -21.00000 -1.50000 H10F 2 0.095974 0.076247 -0.158547 -21.00000 -1.50000 AFIX 0 C103 1 0.218248 0.120912 -0.072777 -21.00000 0.19569 0.14496 = 0.09452 0.02553 0.06608 0.05437 AFIX 13 H103 2 0.272531 0.100937 -0.080675 -21.00000 -1.20000 AFIX 0 PART 0 C104 1 0.331249 0.618871 -0.094679 11.00000 0.34623 0.17173 = 0.12520 0.00868 0.12801 -0.05184 AFIX 137 H10G 2 0.278345 0.635722 -0.122475 11.00000 -1.50000 H10H 2 0.348702 0.577552 -0.131700 11.00000 -1.50000 H10I 2 0.379696 0.665019 -0.067945 11.00000 -1.50000 AFIX 0 PART 1 SI5 5 0.236482 0.093094 0.010556 21.00000 0.17440 0.12223 = 0.08138 0.02172 0.06226 0.07118 C105 1 0.342805 0.083361 0.154179 21.00000 0.17707 0.16509 = 0.12532 0.01437 0.02741 0.07679 AFIX 137 H10J 2 0.401955 0.115830 0.183122 21.00000 -1.50000 H10K 2 0.337156 0.036152 0.170295 21.00000 -1.50000 H10L 2 0.297923 0.115219 0.164782 21.00000 -1.50000 AFIX 0 C106 1 0.162532 0.008723 -0.066628 21.00000 0.18800 0.13356 = 0.10005 0.01286 0.05497 0.06523 AFIX 13 H106 2 0.198220 -0.004532 -0.102222 21.00000 -1.20000 AFIX 0 C107 1 0.314966 0.244186 -0.011373 21.00000 0.22255 0.16846 = 0.10971 0.02533 0.07802 0.03045 AFIX 137 H10M 2 0.270945 0.271160 0.007648 21.00000 -1.50000 H10N 2 0.317392 0.256400 -0.057645 21.00000 -1.50000 H10O 2 0.373251 0.262974 0.029029 21.00000 -1.50000 AFIX 0 C108 1 0.414190 0.087662 0.055095 21.00000 0.20724 0.18606 = 0.16262 0.00776 0.03399 0.04459 AFIX 137 H10P 2 0.398870 0.095839 0.004602 21.00000 -1.50000 H10Q 2 0.453768 0.048343 0.056468 21.00000 -1.50000 H10R 2 0.444036 0.138540 0.096243 21.00000 -1.50000 AFIX 0 C109 1 0.125434 -0.075265 -0.071110 21.00000 0.22186 0.14380 = 0.15114 0.04278 0.03960 0.02126 AFIX 3 H10S 2 0.168194 -0.092255 -0.032990 21.00000 -1.50000 H10T 2 0.114374 -0.113085 -0.123230 21.00000 -1.50000 H10U 2 0.069784 -0.074035 -0.059600 21.00000 -1.50000 AFIX 0 C110 1 0.089332 0.042611 -0.113226 21.00000 0.20967 0.16821 = 0.12067 0.01739 0.03995 0.05283 AFIX 3 H11A 2 0.045762 0.052881 -0.086346 21.00000 -1.50000 H11B 2 0.060312 0.004021 -0.165456 21.00000 -1.50000 H11C 2 0.114572 0.092811 -0.116956 21.00000 -1.50000 AFIX 0 C111 1 0.329399 0.056734 0.067586 21.00000 0.18209 0.15464 = 0.11338 0.00952 0.04892 0.07327 AFIX 13 H111 2 0.317882 -0.003117 0.047018 21.00000 -1.20000 AFIX 0 C112 1 0.308863 0.109721 -0.105086 21.00000 0.21292 0.16797 = 0.11994 0.01920 0.09420 0.03345 AFIX 137 H11D 2 0.359436 0.082984 -0.091322 21.00000 -1.50000 H11E 2 0.322967 0.147964 -0.129790 21.00000 -1.50000 H11F 2 0.256887 0.069709 -0.141140 21.00000 -1.50000 AFIX 0 C113 1 0.289055 0.154179 -0.031789 21.00000 0.19487 0.14356 = 0.09726 0.01876 0.07569 0.05042 AFIX 13 H113 2 0.349084 0.151514 0.001456 21.00000 -1.20000 AFIX 0 PART 2 C114 1 0.497251 0.611353 0.513461 -31.00000 0.09543 0.09729 = 0.10301 0.03271 0.00409 -0.00850 AFIX 23 H11G 2 0.465347 0.558201 0.476015 -31.00000 -1.20000 H11H 2 0.544523 0.601681 0.554911 -31.00000 -1.20000 AFIX 0 C115 1 0.478849 0.626748 0.390310 -31.00000 0.09690 0.10581 = 0.11581 0.02924 0.01014 -0.00154 AFIX 23 H11I 2 0.456582 0.569297 0.378496 -31.00000 -1.20000 H11J 2 0.428235 0.654115 0.394824 -31.00000 -1.20000 AFIX 0 C116 1 0.433165 0.649965 0.549822 -31.00000 0.07859 0.07050 = 0.06697 0.03916 0.01719 -0.00565 AFIX 3 H11K 2 0.376295 0.617225 0.513792 -31.00000 -1.50000 H11L 2 0.433645 0.705755 0.551652 -31.00000 -1.50000 H11M 2 0.441365 0.646805 0.601712 -31.00000 -1.50000 AFIX 0 C117 1 0.630334 0.631592 0.472543 -31.00000 0.08393 0.09653 = 0.10104 0.03471 0.00835 -0.00426 AFIX 23 H11N 2 0.664859 0.638750 0.527005 -31.00000 -1.20000 H11O 2 0.660496 0.672100 0.457563 -31.00000 -1.20000 AFIX 0 C118 1 0.616357 0.785961 0.586092 -31.00000 0.07351 0.08407 = 0.11576 0.03226 0.03321 0.01372 AFIX 137 H11P 2 0.672774 0.766868 0.590577 -31.00000 -1.50000 H11Q 2 0.593583 0.776704 0.625780 -31.00000 -1.50000 H11R 2 0.625534 0.843373 0.593479 -31.00000 -1.50000 AFIX 0 C119 1 0.550995 0.741602 0.507390 -31.00000 0.08906 0.10367 = 0.11661 0.03405 0.01350 0.00417 AFIX 23 H11S 2 0.564927 0.766172 0.470882 -31.00000 -1.20000 H11T 2 0.491908 0.752472 0.509175 -31.00000 -1.20000 AFIX 0 PART 1 C120 1 0.524180 0.687099 0.366403 31.00000 0.09356 0.11728 = 0.13378 0.02062 0.05414 -0.02290 AFIX 3 H12A 2 0.502450 0.637459 0.322003 31.00000 -1.50000 H12B 2 0.589020 0.695929 0.386893 31.00000 -1.50000 H12C 2 0.505340 0.732159 0.349853 31.00000 -1.50000 AFIX 0 PART 2 C121 1 0.638572 0.550161 0.423409 -31.00000 0.06866 0.06539 = 0.06469 0.04077 -0.00479 -0.01060 AFIX 3 H12D 2 0.619882 0.547731 0.369019 -31.00000 -1.50000 H12E 2 0.609102 0.501951 0.427529 -31.00000 -1.50000 H12F 2 0.702912 0.553361 0.442569 -31.00000 -1.50000 AFIX 0 HKLF 4 REM 20220716syf2_0m_a.res in P-1 REM wR2 = 0.3321, GooF = S = 1.051, Restrained GooF = 1.118 for all data REM R1 = 0.1177 for 8933 Fo > 4sig(Fo) and 0.1918 for all 17849 data REM 1230 parameters refined using 700 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 1.822, deepest hole -1.332, 1-sigma level 0.096 Q1 1 0.4594 0.6621 0.4752 11.00000 0.05 1.82 Q2 1 0.6576 0.5382 0.4135 11.00000 0.05 1.76 Q3 1 0.4014 0.6629 0.5539 11.00000 0.05 1.51 Q4 1 0.5514 0.6866 0.4797 11.00000 0.05 0.97 Q5 1 0.5571 0.6813 0.3978 11.00000 0.05 0.83 Q6 1 0.2257 0.6258 -0.0419 11.00000 0.05 0.83 Q7 1 0.4980 0.6848 0.3322 11.00000 0.05 0.75 Q8 1 0.4179 0.5976 0.0327 11.00000 0.05 0.69 Q9 1 0.4729 0.5943 0.3027 11.00000 0.05 0.66 Q10 1 0.6183 0.8142 0.5917 11.00000 0.05 0.61 ; _shelx_res_checksum 83652 _shelx_hkl_file ; 1 0 0 1296.27 67.59 2 0 0 6151.68 319.07 3 0 0 2866.31 150.08 4 0 0 1380.26 74.09 5 0 0 1117.09 58.19 5 0 0 1155.08 61.59 5 0 0 1090.69 58.09 6 0 0 1951.40 100.69 6 0 0 1828.32 96.69 6 0 0 1817.42 96.49 7 0 0 99.69 6.60 7 0 0 109.99 14.30 7 0 0 110.49 9.50 7 0 0 110.39 6.00 8 0 0 12.40 2.20 8 0 0 2.50 7.20 8 0 0 14.10 1.60 8 0 0 17.70 5.50 9 0 0 251.17 12.90 9 0 0 229.08 16.50 9 0 0 239.38 13.50 9 0 0 228.08 22.10 10 0 0 65.89 13.30 10 0 0 59.29 8.90 10 0 0 57.69 5.80 10 0 0 80.29 4.60 -11 0 0 10.90 6.80 11 0 0 12.80 2.00 11 0 0 7.40 3.30 11 0 0 8.00 6.80 11 0 0 -1.30 12.30 12 0 0 7.00 3.50 12 0 0 5.00 1.90 12 0 0 8.50 13.90 12 0 0 2.20 5.90 13 0 0 2.00 7.40 13 0 0 0.70 2.00 13 0 0 -2.80 3.40 14 0 0 23.40 9.10 14 0 0 33.00 5.00 14 0 0 42.80 3.80 15 0 0 0.50 6.50 15 0 0 1.80 2.20 15 0 0 7.90 3.90 16 0 0 1.20 3.30 16 0 0 5.40 2.40 16 0 0 2.40 6.90 17 0 0 -1.20 5.40 17 0 0 2.10 2.00 18 0 0 6.20 9.40 19 -1 0 4.40 12.80 18 -1 0 9.60 10.40 17 -1 0 1.30 2.10 17 -1 0 1.20 5.90 16 -1 0 -1.80 4.30 16 -1 0 -3.60 6.10 16 -1 0 -3.30 1.90 15 -1 0 -0.50 2.40 15 -1 0 0.20 6.90 15 -1 0 7.00 2.10 14 -1 0 3.90 2.20 14 -1 0 -1.90 3.40 14 -1 0 -3.40 6.60 13 -1 0 2.40 1.90 13 -1 0 1.40 7.70 13 -1 0 7.00 3.60 12 -1 0 5.80 3.30 12 -1 0 7.90 2.00 12 -1 0 4.30 6.50 11 -1 0 213.28 12.50 11 -1 0 226.48 11.80 11 -1 0 234.98 23.50 -11 1 0 187.58 14.90 -11 1 0 210.08 11.50 10 -1 0 339.17 18.80 10 -1 0 339.07 22.30 10 -1 0 389.16 28.40 10 -1 0 371.96 18.30 -10 1 0 317.77 18.10 -10 1 0 322.77 20.80 9 -1 0 7.30 2.30 9 -1 0 5.50 1.40 9 -1 0 2.90 5.40 9 -1 0 11.80 8.50 -9 1 0 9.50 1.50 -9 1 0 9.20 4.70 8 -1 0 321.37 23.60 8 -1 0 317.37 17.30 8 -1 0 345.77 20.30 8 -1 0 338.07 16.90 -8 1 0 283.97 16.90 7 -1 0 1593.04 81.89 7 -1 0 1609.14 86.49 7 -1 0 1538.75 82.09 6 -1 0 32.60 2.40 6 -1 0 30.40 6.90 6 -1 0 33.60 5.90 6 -1 0 30.30 2.90 5 -1 0 3992.30 211.28 5 -1 0 3986.00 211.28 5 -1 0 4278.47 214.28 4 -1 0 4312.67 232.28 4 -1 0 4672.73 234.58 3 -1 0 2886.71 149.09 3 -1 0 2695.23 149.59 -3 1 0 3004.30 149.39 2 -1 0 1672.03 80.89 2 -1 0 1467.95 80.89 -2 1 0 1644.14 80.99 -2 1 0 1389.96 80.19 -1 1 0 28.30 2.10 -1 1 0 32.20 3.10 0 -1 0 5755.92 281.57 0 1 0 4857.21 280.97 0 1 0 5689.93 281.57 -1 -1 0 911.51 46.50 1 1 0 813.02 47.00 1 1 0 939.81 46.60 2 1 0 5292.17 275.07 3 1 0 189.48 13.30 4 1 0 630.74 34.40 4 1 0 594.94 31.20 4 1 0 567.84 31.00 5 1 0 939.51 49.10 5 1 0 908.71 48.90 5 1 0 982.70 52.79 6 1 0 364.36 20.50 6 1 0 357.66 20.10 6 1 0 395.06 25.60 6 1 0 432.36 22.80 7 1 0 54.39 4.50 7 1 0 44.20 9.60 7 1 0 60.89 7.40 7 1 0 57.29 3.60 8 1 0 85.89 5.00 8 1 0 76.59 8.80 8 1 0 102.79 15.00 8 1 0 83.79 5.90 9 1 0 325.57 25.70 9 1 0 279.27 16.00 9 1 0 301.37 15.30 9 1 0 256.97 18.90 10 1 0 202.18 10.60 10 1 0 183.58 11.60 10 1 0 181.18 22.80 11 1 0 62.99 4.40 11 1 0 59.49 6.00 11 1 0 57.99 15.10 -12 -1 0 55.89 10.70 12 1 0 34.30 16.70 12 1 0 68.09 4.70 12 1 0 62.59 6.50 13 1 0 21.90 4.60 13 1 0 8.20 7.70 13 1 0 31.20 18.00 13 1 0 23.00 2.80 14 1 0 67.89 7.20 14 1 0 58.49 4.80 15 1 0 0.20 6.10 15 1 0 7.60 4.20 15 1 0 2.00 2.30 16 1 0 -3.30 5.60 16 1 0 2.90 2.10 16 1 0 -2.80 3.90 17 1 0 2.90 5.00 17 1 0 0.90 2.00 17 1 0 6.80 7.50 18 1 0 5.00 2.20 18 1 0 -4.60 9.30 19 -2 0 -1.10 13.80 18 -2 0 3.00 2.10 18 -2 0 -5.20 9.40 17 -2 0 -3.40 1.80 17 -2 0 -3.70 6.20 16 -2 0 0.10 2.00 16 -2 0 2.30 7.30 15 -2 0 3.60 7.40 15 -2 0 2.10 2.00 15 -2 0 -1.60 3.10 14 -2 0 22.20 9.10 13 -2 0 6.90 8.10 13 -2 0 10.70 3.00 13 -2 0 9.60 2.10 12 -2 0 225.58 12.00 12 -2 0 200.28 12.60 12 -2 0 208.68 17.50 -12 2 0 223.38 11.90 11 -2 0 -1.40 2.40 11 -2 0 -0.60 6.10 11 -2 0 0.00 1.60 -11 2 0 0.10 5.70 -11 2 0 3.80 1.80 10 -2 0 250.07 13.80 10 -2 0 231.58 17.30 10 -2 0 261.87 13.30 -10 2 0 243.68 15.90 -10 2 0 240.48 13.40 9 -2 0 260.77 21.60 9 -2 0 272.67 13.50 9 -2 0 250.87 13.90 9 -2 0 253.97 17.10 -9 2 0 244.48 15.70 -9 2 0 230.18 13.60 8 -2 0 25.10 6.10 8 -2 0 18.20 7.90 8 -2 0 26.80 2.40 8 -2 0 26.40 2.60 -8 2 0 24.20 2.40 -8 2 0 18.90 4.60 7 -2 0 1363.86 73.69 7 -2 0 1476.55 76.19 7 -2 0 1420.46 71.49 7 -2 0 1374.36 71.59 -7 2 0 1364.26 72.79 -7 2 0 1276.87 71.49 6 -2 0 70.09 10.60 6 -2 0 71.39 4.00 6 -2 0 77.69 6.80 6 -2 0 66.89 4.30 -6 2 0 62.29 6.70 -6 2 0 58.49 4.30 5 -2 0 3021.10 161.38 5 -2 0 3174.38 160.58 5 -2 0 2907.91 158.68 -5 2 0 3365.46 161.68 -5 2 0 2869.01 159.48 4 -2 0 394.86 20.00 4 -2 0 334.87 18.50 4 -2 0 364.66 20.90 -4 2 0 361.76 21.90 -4 2 0 315.47 19.50 3 -2 0 2365.76 119.39 -3 2 0 2023.70 118.09 -3 2 0 2433.36 119.89 -2 2 0 306.77 17.70 -2 2 0 350.16 19.50 1 -2 0 126.89 8.60 -1 2 0 114.19 7.10 -1 2 0 132.49 8.90 0 -2 0 1.40 2.00 0 2 0 4.30 1.40 0 2 0 5.10 2.50 -1 -2 0 678.53 35.90 1 2 0 636.74 35.20 1 2 0 722.23 36.20 1 2 0 636.34 36.50 -2 -2 0 8.70 2.50 2 2 0 9.20 3.20 2 2 0 15.80 5.10 3 2 0 753.42 41.50 3 2 0 826.92 44.70 3 2 0 826.32 41.70 4 2 0 2583.54 141.69 4 2 0 2836.82 145.09 4 2 0 2799.92 141.89 5 2 0 242.68 18.00 5 2 0 241.48 12.70 5 2 0 218.98 12.30 6 2 0 3.70 5.00 6 2 0 1.20 1.90 6 2 0 5.70 6.70 6 2 0 1.20 1.00 7 2 0 327.77 18.00 7 2 0 327.17 17.50 7 2 0 339.77 24.90 7 2 0 336.67 20.40 8 2 0 7.70 2.40 8 2 0 6.10 5.70 8 2 0 10.70 1.50 8 2 0 8.00 8.30 9 2 0 253.07 14.70 9 2 0 259.77 14.00 9 2 0 277.37 24.80 10 2 0 41.20 3.30 10 2 0 28.10 13.10 10 2 0 36.00 4.20 10 2 0 24.90 7.30 11 2 0 -0.10 1.80 11 2 0 0.20 5.40 11 2 0 8.10 13.70 11 2 0 -3.60 3.40 12 2 0 0.00 5.90 12 2 0 -4.90 15.20 12 2 0 -1.70 2.00 12 2 0 -0.10 3.90 13 2 0 120.79 9.90 13 2 0 136.89 8.00 13 2 0 116.89 24.50 14 2 0 6.00 2.40 14 2 0 -0.60 4.60 14 2 0 1.90 23.00 14 2 0 -0.90 6.60 15 2 0 5.20 4.60 15 2 0 0.50 6.00 15 2 0 11.00 2.60 16 2 0 2.80 2.30 16 2 0 7.30 4.60 16 2 0 0.00 5.30 17 2 0 1.70 2.10 17 2 0 -1.30 6.80 17 2 0 3.40 4.40 18 2 0 2.60 2.60 18 2 0 8.00 9.10 19 -3 0 12.70 14.10 18 -3 0 -1.40 2.50 18 -3 0 1.40 7.90 17 -3 0 -2.80 6.80 16 -3 0 3.90 2.00 16 -3 0 2.90 7.50 15 -3 0 1.90 7.40 15 -3 0 -1.00 1.90 14 -3 0 54.89 11.90 14 -3 0 78.49 5.10 13 -3 0 -3.10 1.80 13 -3 0 0.30 1.90 13 -3 0 -0.10 7.50 -13 3 0 2.10 2.20 12 -3 0 82.39 5.10 12 -3 0 62.59 5.30 12 -3 0 77.29 10.60 -12 3 0 84.59 5.50 11 -3 0 38.40 3.90 11 -3 0 27.80 7.70 11 -3 0 41.10 3.20 -11 3 0 35.40 6.60 -11 3 0 34.50 3.80 10 -3 0 0.50 1.40 10 -3 0 3.30 5.60 10 -3 0 2.40 2.00 -10 3 0 2.90 2.00 -10 3 0 0.00 4.70 9 -3 0 13.30 1.70 9 -3 0 10.10 2.00 9 -3 0 6.30 5.50 -9 3 0 8.10 4.50 -9 3 0 10.40 2.20 8 -3 0 110.99 9.80 8 -3 0 111.09 6.50 8 -3 0 116.69 6.30 -8 3 0 105.49 8.80 -8 3 0 103.29 6.70 7 -3 0 95.49 13.30 7 -3 0 109.59 6.10 7 -3 0 114.09 9.20 7 -3 0 107.89 6.30 -7 3 0 98.89 15.40 -7 3 0 101.89 6.70 -7 3 0 119.79 9.10 6 -3 0 88.49 4.90 6 -3 0 73.39 11.60 6 -3 0 92.89 7.80 -6 3 0 80.49 5.50 -6 3 0 74.99 7.40 -6 3 0 92.19 12.60 5 -3 0 178.68 14.20 5 -3 0 170.88 9.50 5 -3 0 192.58 11.40 -5 3 0 174.28 11.10 -5 3 0 162.28 9.80 -5 3 0 200.88 16.80 4 -3 0 235.38 13.30 4 -3 0 228.38 15.60 -4 3 0 207.88 13.10 -4 3 0 228.28 17.50 -3 3 0 2089.19 115.29 -3 3 0 2450.05 117.89 -3 3 0 2110.99 114.79 2 -3 0 274.77 17.00 -2 3 0 275.17 17.70 -2 3 0 250.37 14.90 1 -3 0 24.30 4.70 -1 3 0 31.50 4.20 -1 3 0 31.30 5.80 0 -3 0 303.47 18.40 0 3 0 289.97 16.80 0 3 0 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598.64 30.80 5 6 0 653.63 39.50 -6 -6 0 97.69 5.90 6 6 0 84.09 9.30 6 6 0 108.59 7.10 6 6 0 115.59 18.20 6 6 0 111.69 6.00 -7 -6 0 295.87 16.70 7 6 0 365.96 29.60 7 6 0 321.97 17.70 7 6 0 316.47 16.90 -8 -6 0 57.59 4.20 8 6 0 75.79 4.70 8 6 0 75.39 6.30 8 6 0 56.19 14.90 -9 -6 0 27.20 2.70 9 6 0 35.00 3.30 9 6 0 20.20 14.20 9 6 0 32.90 4.40 10 6 0 -15.70 13.80 10 6 0 -1.50 2.00 10 6 0 -4.10 3.70 10 6 0 -2.90 4.90 11 6 0 3.00 4.30 11 6 0 -14.40 15.40 11 6 0 -2.20 2.20 11 6 0 -1.70 4.20 12 6 0 -1.20 3.90 12 6 0 5.90 5.00 12 6 0 3.30 2.50 12 6 0 18.30 20.90 13 6 0 4.90 2.60 13 6 0 -9.40 22.20 13 6 0 3.30 5.40 13 6 0 0.40 4.90 14 6 0 2.10 2.50 14 6 0 0.80 5.10 14 6 0 5.10 5.20 14 6 0 -7.30 29.00 15 6 0 7.80 5.40 15 6 0 21.40 3.30 15 6 0 29.40 33.30 16 6 0 2.80 3.00 16 6 0 -3.60 6.40 17 6 0 5.80 4.20 17 6 0 2.00 8.10 17 -7 0 2.80 16.70 16 -7 0 2.00 1.70 16 -7 0 -0.50 9.80 -16 7 0 10.90 3.10 15 -7 0 -1.30 9.20 -15 7 0 2.90 3.30 14 -7 0 2.40 2.00 14 -7 0 0.20 8.70 -14 7 0 -1.60 3.20 13 -7 0 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17.10 6 13 -3 9.70 4.30 -6 -13 3 5.70 3.30 5 13 -3 -5.70 3.60 5 13 -3 -1.60 3.50 5 13 -3 -11.20 14.20 -5 -13 3 4.00 3.20 4 13 -3 10.90 15.30 4 13 -3 10.20 6.60 3 13 -3 137.89 21.50 3 13 -3 123.79 8.50 -3 -13 3 113.69 8.50 2 13 -3 156.08 23.40 2 13 -3 139.49 9.00 -2 -13 3 133.69 9.40 1 13 -3 170.38 23.60 1 13 -3 132.89 8.40 1 13 -3 132.09 8.30 -1 -13 3 120.99 9.00 0 13 -3 240.88 27.10 0 13 -3 237.08 13.30 0 13 -3 241.38 13.60 0 -13 3 228.08 13.80 -1 13 -3 5.60 3.20 -1 13 -3 -2.30 12.10 1 -13 3 14.90 3.70 -2 13 -3 73.29 16.90 -2 13 -3 81.39 6.50 2 -13 3 79.69 6.70 -3 13 -3 14.30 14.10 -3 13 -3 28.00 4.30 3 -13 3 28.20 4.30 -4 13 -3 8.00 3.80 4 -13 3 8.90 3.80 -5 13 -3 9.20 3.90 5 -13 3 11.20 3.90 -6 13 -3 10.50 4.00 6 -13 3 12.60 3.90 -7 13 -3 25.40 4.60 7 -13 3 16.90 4.20 -8 13 -3 3.40 4.10 8 -13 3 0.60 2.40 -9 13 -3 6.00 4.30 9 -13 3 -1.40 2.60 -10 13 -3 3.70 4.10 10 -13 3 3.90 2.90 -11 13 -3 -0.50 4.10 11 -13 3 2.80 2.70 -12 13 -3 22.20 4.90 12 -13 3 15.50 3.30 -13 13 -3 -0.20 3.90 13 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52.29 3.70 1 -11 3 28.90 26.50 1 -11 3 50.09 5.10 -2 11 -3 147.49 8.60 -2 11 -3 108.29 41.70 2 -11 3 120.29 8.50 -3 11 -3 27.90 3.50 -3 11 -3 20.40 45.10 3 -11 3 49.99 28.50 3 -11 3 34.70 3.80 -4 11 -3 90.39 6.90 -4 11 -3 76.49 51.39 4 -11 3 84.89 6.70 4 -11 3 120.79 32.50 -5 11 -3 160.98 10.20 -5 11 -3 131.99 59.19 5 -11 3 161.68 10.10 -6 11 -3 13.90 3.50 6 -11 3 8.00 3.30 -7 11 -3 139.69 9.10 7 -11 3 122.09 8.60 -8 11 -3 0.80 3.40 8 -11 3 -1.90 2.40 -9 11 -3 13.30 3.90 9 -11 3 10.70 2.80 -10 11 -3 10.30 4.20 10 -11 3 12.70 3.20 -11 11 -3 29.50 5.00 11 -11 3 39.90 4.10 -12 11 -3 5.10 4.10 12 -11 3 9.70 3.00 -13 11 -3 3.70 3.90 13 -11 3 1.20 2.50 -14 11 -3 0.00 3.70 14 -11 3 2.80 2.40 -15 11 -3 -3.20 3.20 15 -11 3 1.10 2.20 -16 11 -3 4.20 3.30 16 -11 3 8.30 2.30 16 10 -3 3.30 7.90 15 10 -3 5.80 8.50 14 10 -3 22.40 29.50 13 10 -3 7.00 5.10 13 10 -3 -18.10 24.60 13 10 -3 8.30 5.90 13 10 -3 -0.40 5.80 12 10 -3 34.30 23.40 12 10 -3 40.30 6.30 12 10 -3 59.49 8.10 11 10 -3 -0.80 5.30 11 10 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33.20 4.00 0 10 -3 108.49 30.10 0 10 -3 83.69 5.80 0 10 -3 84.19 5.30 0 10 -3 73.49 12.20 0 -10 3 88.49 22.80 0 -10 3 78.09 6.00 -1 10 -3 4.70 1.50 -1 10 -3 2.80 2.40 -1 10 -3 4.80 7.60 -1 10 -3 3.90 27.70 1 -10 3 1.70 2.50 1 -10 3 -6.20 18.80 -2 10 -3 325.77 17.90 -2 10 -3 426.96 53.99 2 -10 3 268.47 39.30 2 -10 3 325.27 17.90 -3 10 -3 -7.00 32.80 3 -10 3 -30.40 21.60 -4 10 -3 20.80 39.80 -4 10 -3 10.20 2.80 4 -10 3 11.50 2.90 4 -10 3 53.09 23.80 -5 10 -3 82.79 46.90 -5 10 -3 99.59 7.30 5 -10 3 102.59 28.60 5 -10 3 99.39 7.10 -6 10 -3 188.68 11.20 -6 10 -3 144.19 53.29 6 -10 3 180.18 11.00 -7 10 -3 16.00 3.50 7 -10 3 13.90 3.20 -9 10 -3 0.60 3.40 9 -10 3 3.50 2.50 -10 10 -3 23.70 4.20 10 -10 3 14.40 3.00 -11 10 -3 82.49 7.30 11 -10 3 77.79 6.00 -12 10 -3 3.30 3.80 12 -10 3 0.20 2.60 -13 10 -3 18.40 4.20 13 -10 3 20.00 3.10 -14 10 -3 -1.80 3.40 14 -10 3 -0.40 2.30 -15 10 -3 -2.00 3.00 15 -10 3 0.30 2.30 -16 10 -3 4.40 3.00 16 -10 3 3.90 2.30 17 -10 3 -0.50 2.70 16 9 -3 -1.80 9.50 15 9 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12.70 2.40 -3 -9 3 -7.90 17.50 2 9 -3 11.50 8.10 2 9 -3 11.10 2.20 2 9 -3 -9.30 21.70 2 9 -3 10.60 2.00 -2 -9 3 10.80 2.40 -2 -9 3 2.60 15.40 1 9 -3 1.50 2.00 1 9 -3 -1.20 21.40 1 9 -3 10.90 8.30 1 9 -3 3.80 1.90 -1 -9 3 6.80 2.40 -1 -9 3 11.40 15.00 0 9 -3 1.10 1.50 0 9 -3 -10.00 6.80 0 9 -3 1.20 2.10 0 9 -3 9.20 21.40 0 -9 3 -1.40 2.30 0 -9 3 13.10 14.90 -1 9 -3 8.80 2.50 -1 9 -3 47.00 23.60 -1 9 -3 11.00 1.60 1 -9 3 -20.30 15.50 1 -9 3 8.30 2.60 -2 9 -3 174.38 10.70 -2 9 -3 197.58 30.00 2 -9 3 178.48 30.00 2 -9 3 190.68 10.80 -3 9 -3 54.39 4.90 -3 9 -3 32.40 25.40 3 -9 3 52.19 4.90 3 -9 3 36.70 18.30 -4 9 -3 95.59 6.60 -4 9 -3 102.69 31.30 4 -9 3 63.79 21.60 4 -9 3 93.49 6.50 -5 9 -3 17.10 33.90 -5 9 -3 22.20 3.20 5 -9 3 34.70 22.60 5 -9 3 27.80 3.40 -6 9 -3 160.18 44.00 -6 9 -3 189.28 11.20 6 -9 3 185.38 10.90 -7 9 -3 5.50 3.10 -7 9 -3 8.70 52.29 7 -9 3 26.60 30.50 7 -9 3 5.30 2.50 -8 9 -3 16.90 3.50 8 -9 3 22.80 2.70 -9 9 -3 -1.50 3.00 9 -9 3 0.60 2.40 -10 9 -3 -0.40 3.20 10 -9 3 1.90 2.30 -11 9 -3 12.10 4.00 11 -9 3 16.30 3.00 -12 9 -3 16.50 4.10 12 -9 3 15.20 3.00 -13 9 -3 4.70 3.70 13 -9 3 4.20 2.70 -14 9 -3 3.00 3.40 14 -9 3 2.60 2.40 -15 9 -3 0.60 3.00 15 -9 3 0.10 2.20 -16 9 -3 7.70 2.80 16 -9 3 5.20 2.50 17 -9 3 1.90 2.10 17 8 -3 14.50 9.10 16 8 -3 -1.50 6.30 16 8 -3 6.10 5.60 16 8 -3 11.40 8.20 15 8 -3 1.20 5.30 15 8 -3 -1.60 6.40 15 8 -3 1.10 5.30 15 8 -3 -52.69 30.40 14 8 -3 20.50 4.90 14 8 -3 15.20 5.90 14 8 -3 4.60 24.70 13 8 -3 4.60 5.10 13 8 -3 1.70 6.00 13 8 -3 10.90 3.80 13 8 -3 -6.00 21.70 12 8 -3 -3.00 6.40 12 8 -3 5.00 5.20 12 8 -3 10.70 3.00 12 8 -3 7.30 21.50 11 8 -3 2.50 16.80 11 8 -3 1.80 4.40 11 8 -3 -2.40 4.90 11 8 -3 0.50 2.30 10 8 -3 1.50 5.70 10 8 -3 6.00 2.30 10 8 -3 2.80 4.30 10 8 -3 12.40 15.20 -10 -8 3 4.40 2.10 9 8 -3 -2.60 3.40 9 8 -3 6.90 14.20 9 8 -3 -2.30 5.80 9 8 -3 1.60 2.10 -9 -8 3 -0.40 1.90 8 8 -3 17.30 4.00 8 8 -3 12.70 7.50 8 8 -3 16.40 13.00 8 8 -3 24.40 2.60 -8 -8 3 18.20 2.60 7 8 -3 -0.60 5.20 7 8 -3 -3.20 2.80 7 8 -3 0.80 1.70 7 8 -3 -6.60 10.40 -7 -8 3 3.80 2.10 6 8 -3 65.09 9.70 6 8 -3 86.89 5.30 6 8 -3 60.09 12.40 6 8 -3 92.69 6.50 -6 -8 3 49.99 19.50 -6 -8 3 86.39 5.50 5 8 -3 3.20 6.10 5 8 -3 7.60 1.90 5 8 -3 3.30 8.20 5 8 -3 6.50 2.60 -5 -8 3 6.20 20.00 -5 -8 3 6.00 2.10 4 8 -3 53.09 4.70 4 8 -3 60.79 22.50 4 8 -3 48.00 8.40 4 8 -3 51.29 11.20 4 8 -3 51.89 4.00 -4 -8 3 72.69 16.00 -4 -8 3 54.29 4.30 3 8 -3 -1.10 7.10 3 8 -3 23.50 19.60 3 8 -3 -1.30 1.90 3 8 -3 0.00 1.50 -3 -8 3 1.60 11.90 -3 -8 3 -1.90 2.00 2 8 -3 247.28 13.50 2 8 -3 283.07 33.30 2 8 -3 242.58 13.30 2 8 -3 251.27 20.70 -2 -8 3 200.98 25.90 -2 -8 3 247.38 13.50 1 8 -3 122.29 15.40 1 8 -3 117.99 7.10 1 8 -3 106.89 7.20 1 8 -3 93.19 20.60 -1 -8 3 137.09 7.50 0 8 -3 110.09 13.70 0 8 -3 119.49 20.30 0 8 -3 113.59 7.10 0 8 -3 112.29 6.60 0 -8 3 110.39 7.20 0 -8 3 128.79 21.90 -1 8 -3 158.58 24.30 -1 8 -3 158.28 9.50 1 -8 3 148.59 23.80 1 -8 3 168.28 9.60 -2 8 -3 13.50 2.60 -2 8 -3 7.70 18.20 2 -8 3 22.50 2.90 2 -8 3 -5.10 13.20 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26.70 15 7 -3 0.90 5.70 15 7 -3 5.30 4.20 15 7 -3 2.10 5.80 14 7 -3 4.80 2.80 14 7 -3 -8.20 23.10 14 7 -3 -0.40 5.30 14 7 -3 -2.20 5.60 13 7 -3 2.50 2.40 13 7 -3 0.00 6.90 13 7 -3 3.50 4.70 13 7 -3 28.30 20.90 12 7 -3 -11.50 18.40 12 7 -3 1.20 5.30 12 7 -3 15.30 5.60 11 7 -3 -1.30 5.30 11 7 -3 17.20 4.50 11 7 -3 0.60 2.00 11 7 -3 7.80 14.90 10 7 -3 -5.10 11.90 10 7 -3 1.60 1.90 10 7 -3 -0.70 5.70 10 7 -3 -1.90 3.80 -10 -7 3 2.50 1.80 9 7 -3 50.59 6.10 9 7 -3 26.70 13.00 9 7 -3 45.10 3.70 8 7 -3 64.69 6.20 8 7 -3 68.99 4.40 8 7 -3 71.09 19.30 8 7 -3 46.10 9.50 -8 -7 3 58.79 4.40 7 7 -3 278.27 16.00 7 7 -3 317.37 27.20 7 7 -3 276.67 15.10 -7 -7 3 278.27 15.20 6 7 -3 398.96 21.40 6 7 -3 449.16 31.30 6 7 -3 392.96 25.40 -6 -7 3 398.66 32.00 -6 -7 3 405.76 21.60 5 7 -3 80.79 5.00 5 7 -3 88.29 13.70 5 7 -3 76.19 5.90 5 7 -3 77.59 9.50 -5 -7 3 81.89 5.30 -5 -7 3 83.89 13.80 4 7 -3 87.99 5.10 4 7 -3 92.29 14.60 4 7 -3 81.39 9.70 4 7 -3 80.89 5.80 4 7 -3 79.69 19.20 -4 -7 3 76.89 5.40 3 7 -3 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16.80 -4 -15 4 4.20 3.80 3 15 -4 79.09 7.00 3 15 -4 102.29 23.00 -3 -15 4 82.79 7.30 2 15 -4 14.20 16.60 2 15 -4 16.10 3.80 2 15 -4 9.50 5.50 -2 -15 4 10.00 4.30 1 15 -4 0.60 1.50 1 15 -4 6.50 15.60 1 15 -4 -5.30 3.10 -1 -15 4 1.20 3.80 0 15 -4 -4.00 16.20 0 15 -4 -1.70 2.90 0 -15 4 1.70 3.60 -1 15 -4 17.00 3.90 -1 15 -4 10.00 16.50 1 -15 4 17.10 4.50 -2 15 -4 9.00 17.00 -2 15 -4 4.30 3.60 2 -15 4 5.60 4.20 -3 15 -4 23.40 4.40 -3 15 -4 7.30 18.30 3 -15 4 22.00 4.70 -4 15 -4 63.59 22.50 -5 15 -4 8.60 22.80 -5 15 -4 14.00 4.40 5 -15 4 21.50 4.80 -6 15 -4 8.20 4.30 6 -15 4 7.60 4.30 -7 15 -4 29.90 5.20 7 -15 4 29.60 5.10 -8 15 -4 0.20 4.10 8 -15 4 -4.00 3.10 -9 15 -4 7.30 4.50 9 -15 4 5.90 3.30 -10 15 -4 18.40 4.60 10 -15 4 17.40 3.60 -11 15 -4 5.20 4.40 11 -15 4 24.80 3.60 -12 15 -4 2.70 4.40 12 -15 4 1.60 2.80 -13 15 -4 0.60 5.00 13 -15 4 0.10 2.40 -14 15 -4 11.00 5.60 -15 15 -4 0.00 5.10 13 14 -4 6.10 7.90 12 14 -4 3.50 7.80 11 14 -4 -13.70 28.60 11 14 -4 3.00 6.90 -11 -14 4 7.90 4.60 10 14 -4 24.30 26.50 10 14 -4 15.20 5.50 -10 -14 4 10.40 3.30 9 14 -4 -11.80 20.80 9 14 -4 -3.40 4.50 -9 -14 4 2.30 3.00 8 14 -4 18.20 5.50 8 14 -4 -5.70 4.30 8 14 -4 3.30 21.90 7 14 -4 12.50 4.60 7 14 -4 11.90 19.80 7 14 -4 -0.90 3.90 -7 -14 4 6.80 3.40 6 14 -4 30.20 5.00 6 14 -4 22.60 20.40 -6 -14 4 19.40 3.90 5 14 -4 9.10 4.20 5 14 -4 10.50 16.20 5 14 -4 1.20 4.50 -5 -14 4 7.10 3.60 4 14 -4 110.69 21.80 4 14 -4 125.69 8.60 -4 -14 4 113.39 8.30 3 14 -4 4.40 3.50 3 14 -4 -1.70 5.20 3 14 -4 14.80 14.70 -3 -14 4 6.40 3.70 2 14 -4 9.90 13.80 2 14 -4 -1.20 5.20 2 14 -4 8.50 3.30 -2 -14 4 4.30 3.70 1 14 -4 18.90 3.50 1 14 -4 17.00 15.20 1 14 -4 24.90 3.50 -1 -14 4 22.90 4.10 0 14 -4 445.46 23.30 0 14 -4 441.36 37.10 0 14 -4 404.16 23.60 0 -14 4 416.96 23.60 -1 14 -4 14.70 3.80 -1 14 -4 11.40 14.60 1 -14 4 21.90 4.30 -2 14 -4 331.17 18.60 -2 14 -4 323.07 31.20 2 -14 4 332.67 18.90 -3 14 -4 88.59 7.50 -3 14 -4 73.39 19.30 3 -14 4 83.89 7.30 -4 14 -4 31.90 18.50 -4 14 -4 34.90 5.00 4 -14 4 36.20 5.10 -5 14 -4 384.96 20.00 -5 14 -4 341.37 35.20 5 -14 4 307.87 19.80 -6 14 -4 61.69 6.50 -6 14 -4 87.59 22.60 6 -14 4 49.30 6.00 -7 14 -4 68.09 6.90 7 -14 4 56.99 6.90 -9 14 -4 6.10 4.60 9 -14 4 13.00 3.50 -10 14 -4 22.20 4.90 10 -14 4 33.80 4.30 -11 14 -4 40.60 5.60 11 -14 4 47.70 5.10 -12 14 -4 0.50 4.20 12 -14 4 -1.30 2.70 -13 14 -4 -0.90 4.00 13 -14 4 -3.30 2.30 -14 14 -4 -0.20 4.20 14 -14 4 -3.20 2.30 -15 14 -4 4.20 4.70 15 -14 4 1.00 2.40 14 13 -4 -4.60 6.90 13 13 -4 8.80 9.90 12 13 -4 -2.20 6.40 12 13 -4 -47.40 28.40 11 13 -4 3.90 5.20 11 13 -4 15.60 24.30 -11 -13 4 3.10 3.00 10 13 -4 1.90 3.80 10 13 -4 31.60 24.20 10 13 -4 7.70 4.90 -10 -13 4 5.60 3.00 9 13 -4 -1.00 3.70 9 13 -4 2.40 5.20 9 13 -4 -1.20 19.90 -9 -13 4 -2.60 2.80 8 13 -4 37.90 19.30 8 13 -4 63.99 7.10 -8 -13 4 61.29 5.60 7 13 -4 2.00 4.50 7 13 -4 -3.80 4.70 7 13 -4 -4.80 15.30 -7 -13 4 6.40 3.30 6 13 -4 47.20 5.70 6 13 -4 41.70 18.80 -6 -13 4 36.90 4.60 5 13 -4 25.90 4.50 5 13 -4 18.60 15.90 5 13 -4 4.00 5.80 -5 -13 4 14.00 3.60 4 13 -4 135.59 9.30 4 13 -4 152.08 23.70 -4 -13 4 124.09 8.60 3 13 -4 11.50 13.40 3 13 -4 1.10 3.50 3 13 -4 -0.80 5.90 -3 -13 4 4.20 3.60 2 13 -4 625.84 43.90 2 13 -4 588.74 30.80 -2 -13 4 527.85 31.00 1 13 -4 9.70 13.60 1 13 -4 10.10 3.00 1 13 -4 18.70 3.10 -1 -13 4 11.20 3.60 0 13 -4 264.57 26.60 0 13 -4 241.08 13.50 0 13 -4 242.88 13.90 0 -13 4 234.58 14.40 -1 13 -4 20.10 3.50 -1 13 -4 -4.30 12.40 1 -13 4 23.30 4.00 -2 13 -4 6.60 3.20 -2 13 -4 8.00 12.90 2 -13 4 8.50 3.50 -3 13 -4 11.40 13.10 -3 13 -4 1.70 3.20 3 -13 4 8.90 3.70 -4 13 -4 139.29 22.50 -4 13 -4 171.98 10.90 4 -13 4 170.18 10.90 -5 13 -4 11.70 3.90 -5 13 -4 20.40 14.70 5 -13 4 6.20 3.80 -6 13 -4 84.09 6.90 6 -13 4 70.49 7.00 -7 13 -4 -0.80 3.80 7 -13 4 2.00 3.60 -8 13 -4 14.90 4.30 -9 13 -4 -0.10 4.00 9 -13 4 1.50 3.00 -10 13 -4 8.50 4.40 10 -13 4 3.00 3.20 -11 13 -4 -2.00 4.00 11 -13 4 1.40 2.90 -12 13 -4 -0.50 3.90 12 -13 4 0.20 2.80 -13 13 -4 0.10 3.90 13 -13 4 0.40 2.60 -14 13 -4 0.50 3.80 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5.70 -1 12 -4 4.60 2.80 -1 12 -4 4.90 11.40 -1 12 -4 25.60 58.69 1 -12 4 4.60 36.20 1 -12 4 5.10 3.10 -2 12 -4 5.90 2.80 -2 12 -4 6.30 10.40 -2 12 -4 -71.79 59.19 2 -12 4 9.60 3.20 2 -12 4 3.40 37.70 -3 12 -4 19.20 61.49 -3 12 -4 59.39 12.50 -3 12 -4 30.00 3.80 3 -12 4 34.80 4.30 3 -12 4 17.90 41.70 -4 12 -4 1.10 3.10 4 -12 4 0.90 3.30 -5 12 -4 56.59 5.90 5 -12 4 52.89 5.80 -6 12 -4 -2.80 3.40 6 -12 4 2.60 3.40 -7 12 -4 86.49 7.10 7 -12 4 67.59 6.60 -8 12 -4 15.50 4.20 8 -12 4 5.90 3.40 -9 12 -4 3.90 3.80 9 -12 4 3.30 3.00 -10 12 -4 13.00 4.40 10 -12 4 14.00 3.50 -11 12 -4 2.10 4.00 11 -12 4 0.80 2.90 -12 12 -4 1.30 3.90 12 -12 4 0.30 2.80 -13 12 -4 12.20 4.10 13 -12 4 8.60 2.90 -14 12 -4 -0.30 3.40 14 -12 4 -1.20 2.30 -15 12 -4 1.10 3.40 15 -12 4 -0.20 2.30 -16 12 -4 -3.00 3.30 16 -12 4 -1.50 2.20 15 11 -4 11.50 9.80 14 11 -4 10.30 8.90 14 11 -4 7.80 9.70 13 11 -4 0.40 5.10 13 11 -4 -13.00 31.00 13 11 -4 1.30 6.20 12 11 -4 6.80 6.00 12 11 -4 5.70 6.40 12 11 -4 1.60 27.50 11 11 -4 11.30 5.60 11 11 -4 3.40 6.10 11 11 -4 17.40 22.80 -11 -11 4 7.20 2.90 10 11 -4 13.90 5.30 10 11 -4 27.70 22.20 10 11 -4 1.10 7.00 -10 -11 4 15.60 3.20 9 11 -4 4.20 6.40 9 11 -4 10.80 18.00 9 11 -4 21.80 5.40 -9 -11 4 13.80 3.10 8 11 -4 84.19 7.40 8 11 -4 90.09 22.40 -8 -11 4 63.49 5.80 7 11 -4 84.09 7.40 7 11 -4 45.90 18.10 -7 -11 4 60.59 5.70 6 11 -4 7.90 7.20 6 11 -4 7.30 13.60 5 11 -4 6.60 3.30 5 11 -4 18.00 12.10 5 11 -4 3.30 5.60 -5 -11 4 2.70 2.80 4 11 -4 6.30 3.00 4 11 -4 0.00 5.60 4 11 -4 -9.10 9.30 3 11 -4 13.70 3.00 3 11 -4 17.30 10.20 3 11 -4 14.80 2.00 -3 -11 4 13.10 2.90 2 11 -4 30.40 3.40 2 11 -4 31.40 3.50 2 11 -4 29.80 10.90 -2 -11 4 30.20 3.50 1 11 -4 97.09 6.40 1 11 -4 102.39 6.30 1 11 -4 84.89 13.50 -1 -11 4 71.29 31.50 -1 -11 4 90.29 6.70 0 11 -4 62.39 39.20 0 11 -4 20.40 3.00 0 11 -4 16.40 2.40 0 11 -4 16.10 10.00 0 -11 4 6.80 26.50 0 -11 4 18.90 3.20 -1 11 -4 14.90 2.80 -1 11 -4 12.60 1.90 -1 11 -4 21.10 9.80 -1 11 -4 4.80 38.80 1 -11 4 15.00 3.10 1 -11 4 52.19 29.00 -2 11 -4 64.49 41.50 -2 11 -4 46.40 4.80 -2 11 -4 33.80 10.50 2 -11 4 44.40 4.90 2 -11 4 47.20 28.90 -3 11 -4 -34.70 47.90 -3 11 -4 -2.10 2.50 3 -11 4 4.90 2.90 3 -11 4 -29.70 30.70 -4 11 -4 -64.89 55.29 -4 11 -4 1.40 2.90 4 -11 4 2.30 3.10 4 -11 4 -45.00 32.00 -5 11 -4 3.00 93.69 5 -11 4 -52.99 40.60 -6 11 -4 22.00 3.90 6 -11 4 29.20 4.00 -7 11 -4 4.50 3.50 7 -11 4 7.00 3.00 -8 11 -4 84.09 7.10 -9 11 -4 16.40 4.10 9 -11 4 9.40 2.80 -10 11 -4 1.70 3.80 10 -11 4 -1.80 2.40 -11 11 -4 102.39 8.10 11 -11 4 98.79 7.10 -12 11 -4 -1.50 3.60 12 -11 4 1.70 2.70 -13 11 -4 19.40 4.30 13 -11 4 25.90 3.50 -14 11 -4 1.30 3.20 14 -11 4 -0.40 2.40 -15 11 -4 -0.20 3.10 15 -11 4 0.10 2.20 -16 11 -4 16.70 3.30 16 -11 4 0.00 2.40 16 10 -4 9.40 7.90 15 10 -4 -1.70 5.30 15 10 -4 -0.70 6.90 14 10 -4 -40.60 26.30 14 10 -4 10.50 5.80 14 10 -4 -0.30 6.50 13 10 -4 6.60 24.00 13 10 -4 1.40 5.90 13 10 -4 5.20 5.80 12 10 -4 -5.60 5.30 12 10 -4 13.30 25.20 12 10 -4 4.70 5.50 12 10 -4 5.40 5.50 11 10 -4 -10.50 20.00 11 10 -4 1.40 4.80 11 10 -4 -3.50 6.40 11 10 -4 1.20 5.00 -11 -10 4 -0.80 2.60 10 10 -4 0.10 5.00 10 10 -4 11.00 19.40 10 10 -4 0.40 4.60 10 10 -4 0.50 4.60 -10 -10 4 -0.80 2.50 9 10 -4 29.70 4.60 9 10 -4 28.20 5.20 9 10 -4 32.70 19.20 -9 -10 4 18.70 3.20 8 10 -4 49.40 5.70 8 10 -4 45.10 4.80 8 10 -4 60.19 17.90 -8 -10 4 42.20 4.40 7 10 -4 57.69 5.30 7 10 -4 52.79 6.10 7 10 -4 49.50 15.40 -7 -10 4 49.40 4.70 6 10 -4 47.20 5.50 6 10 -4 53.79 14.10 -6 -10 4 39.90 4.60 5 10 -4 55.09 13.40 5 10 -4 87.19 6.40 -5 -10 4 74.49 5.70 4 10 -4 19.90 3.10 4 10 -4 12.90 9.50 4 10 -4 6.10 6.20 -4 -10 4 17.40 3.00 3 10 -4 63.79 4.30 3 10 -4 62.59 5.20 3 10 -4 75.19 12.80 -3 -10 4 62.49 5.20 2 10 -4 -0.50 1.80 2 10 -4 1.70 2.10 2 10 -4 -2.40 7.80 2 10 -4 21.10 29.90 -2 -10 4 2.70 2.40 -2 -10 4 13.90 22.80 1 10 -4 148.29 33.00 1 10 -4 114.39 16.60 1 10 -4 127.49 7.80 1 10 -4 132.79 7.70 -1 -10 4 108.99 25.30 -1 -10 4 131.39 8.20 0 10 -4 7.90 8.10 0 10 -4 -4.10 29.50 0 10 -4 5.50 1.80 0 10 -4 6.30 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14 9 -4 7.30 5.90 14 9 -4 5.00 5.90 14 9 -4 66.89 27.10 13 9 -4 16.20 6.10 13 9 -4 13.40 22.30 13 9 -4 7.10 5.50 13 9 -4 9.50 6.80 12 9 -4 2.70 6.50 12 9 -4 -1.50 20.00 12 9 -4 -0.10 4.90 12 9 -4 -2.50 4.70 11 9 -4 -1.20 17.30 11 9 -4 0.50 4.90 11 9 -4 2.30 5.10 -11 -9 4 -0.60 2.40 10 9 -4 6.40 3.60 10 9 -4 1.30 5.60 10 9 -4 2.60 4.30 -10 -9 4 0.80 2.40 9 9 -4 -0.60 13.20 9 9 -4 4.20 6.60 9 9 -4 6.30 4.00 9 9 -4 9.80 3.40 -9 -9 4 10.30 2.60 8 9 -4 -5.20 11.50 8 9 -4 5.30 7.30 8 9 -4 12.00 3.00 8 9 -4 11.10 4.00 -8 -9 4 11.20 2.70 7 9 -4 171.88 23.10 7 9 -4 146.79 9.30 7 9 -4 163.58 10.20 -7 -9 4 153.58 9.20 6 9 -4 9.30 2.60 6 9 -4 14.20 3.30 6 9 -4 8.50 9.60 6 9 -4 3.70 5.70 -6 -9 4 -31.90 24.60 5 9 -4 1.90 6.30 5 9 -4 4.80 2.70 5 9 -4 15.90 9.40 -5 -9 4 4.60 2.40 4 9 -4 20.60 9.20 4 9 -4 24.40 3.10 -4 -9 4 21.20 2.90 3 9 -4 20.70 2.00 3 9 -4 18.00 2.70 3 9 -4 37.60 26.90 -3 -9 4 16.90 2.80 -3 -9 4 22.60 18.00 2 9 -4 72.29 4.80 2 9 -4 63.99 11.30 2 9 -4 70.09 5.10 2 9 -4 51.89 24.10 -2 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8 -4 9.00 2.10 5 8 -4 11.30 9.40 5 8 -4 9.90 2.70 5 8 -4 5.80 6.70 -5 -8 4 10.70 2.30 -5 -8 4 12.70 15.10 4 8 -4 161.48 17.70 4 8 -4 164.98 9.70 4 8 -4 154.78 13.70 -4 -8 4 164.78 9.40 3 8 -4 242.38 36.70 3 8 -4 259.07 14.00 3 8 -4 260.07 21.00 3 8 -4 245.28 13.50 -3 -8 4 215.78 27.90 -3 -8 4 260.37 13.90 2 8 -4 32.90 3.70 2 8 -4 36.80 3.40 2 8 -4 31.00 8.90 2 8 -4 12.90 18.60 -2 -8 4 33.00 4.10 -2 -8 4 27.20 14.00 1 8 -4 2827.92 153.48 1 8 -4 2776.02 142.99 1 8 -4 2788.32 147.29 1 8 -4 2797.92 142.99 -1 -8 4 2517.25 149.39 -1 -8 4 2829.52 143.09 0 8 -4 75.39 4.70 0 8 -4 66.69 9.90 0 8 -4 77.49 5.40 0 8 -4 42.60 19.30 0 -8 4 73.69 5.60 0 -8 4 51.39 14.50 -1 8 -4 164.48 15.10 -1 8 -4 157.18 25.80 -1 8 -4 180.28 10.10 1 -8 4 176.88 10.20 1 -8 4 168.58 24.30 -2 8 -4 221.98 12.80 -2 8 -4 194.18 27.80 2 -8 4 265.47 28.10 2 -8 4 231.78 12.80 -3 8 -4 465.85 25.10 -3 8 -4 452.85 45.70 3 -8 4 463.65 38.60 3 -8 4 483.75 25.20 -4 8 -4 37.10 4.40 -4 8 -4 33.00 25.80 4 -8 4 44.90 4.40 4 -8 4 30.60 18.80 -5 8 -4 485.45 26.70 -5 8 -4 538.55 57.29 5 -8 4 529.25 26.70 5 -8 4 438.86 44.40 -6 8 -4 30.30 3.40 -6 8 -4 2.70 37.50 6 -8 4 56.49 24.80 6 -8 4 32.60 3.40 -7 8 -4 142.59 8.90 7 -8 4 149.29 8.40 7 -8 4 130.89 8.70 -8 8 -4 3.50 2.80 8 -8 4 4.40 2.20 -9 8 -4 138.39 8.60 9 -8 4 120.49 7.90 -10 8 -4 41.00 4.60 10 -8 4 5.80 17.30 10 -8 4 37.80 3.70 -12 8 -4 27.10 4.00 12 -8 4 15.70 2.90 -13 8 -4 12.80 3.50 13 -8 4 17.70 3.10 -14 8 -4 0.70 2.80 14 -8 4 2.50 2.50 -15 8 -4 4.90 2.60 15 -8 4 3.70 2.60 16 -8 4 2.40 2.10 17 -8 4 -1.10 2.30 17 7 -4 8.40 7.80 17 7 -4 7.60 7.00 16 7 -4 5.20 6.10 16 7 -4 -0.10 5.00 16 7 -4 15.20 41.50 16 7 -4 1.90 5.40 15 7 -4 29.90 6.70 15 7 -4 17.80 5.40 15 7 -4 21.60 26.40 14 7 -4 -0.40 3.50 14 7 -4 -3.10 6.30 14 7 -4 8.50 5.80 14 7 -4 6.80 21.30 13 7 -4 4.60 5.80 13 7 -4 0.30 19.40 12 7 -4 2.50 5.60 12 7 -4 7.80 2.50 12 7 -4 10.00 16.90 12 7 -4 6.90 5.00 11 7 -4 32.60 3.50 11 7 -4 25.60 15.40 11 7 -4 37.00 5.20 -11 -7 4 32.00 3.30 10 7 -4 -3.50 6.10 10 7 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16.20 3.00 12 -7 4 0.70 17.40 -13 7 -4 54.79 5.40 13 -7 4 58.29 5.00 -14 7 -4 16.10 3.20 14 -7 4 20.70 3.10 -15 7 -4 18.60 3.00 15 -7 4 13.50 2.80 16 -7 4 5.70 2.30 17 -7 4 -2.60 2.30 18 6 -4 -7.70 8.30 18 6 -4 5.10 7.30 17 6 -4 0.10 6.30 17 6 -4 3.80 4.90 17 6 -4 1.30 7.20 16 6 -4 3.60 4.80 16 6 -4 2.50 6.10 16 6 -4 1.30 5.30 16 6 -4 -1.90 27.10 15 6 -4 26.00 24.90 15 6 -4 45.50 5.10 15 6 -4 54.39 7.20 14 6 -4 0.80 4.60 14 6 -4 -16.90 20.60 14 6 -4 0.70 5.20 14 6 -4 -1.40 2.40 13 6 -4 70.79 23.50 13 6 -4 84.69 5.90 13 6 -4 96.79 8.50 12 6 -4 0.20 6.20 12 6 -4 -0.50 4.10 12 6 -4 29.30 17.30 11 6 -4 -0.90 1.80 11 6 -4 1.10 14.10 11 6 -4 2.30 6.00 11 6 -4 -5.10 3.80 -11 -6 4 5.80 2.90 10 6 -4 -1.40 6.50 10 6 -4 2.00 1.80 10 6 -4 7.10 11.70 10 6 -4 0.20 3.60 -10 -6 4 1.10 1.80 9 6 -4 127.69 14.10 9 6 -4 200.98 23.50 9 6 -4 157.38 8.70 9 6 -4 173.08 10.30 -9 -6 4 146.89 8.70 8 6 -4 145.59 19.50 8 6 -4 129.09 7.30 8 6 -4 120.69 12.60 8 6 -4 122.59 8.50 -8 -6 4 133.19 7.40 7 6 -4 103.99 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5 -4 9.60 5.40 15 5 -4 10.90 2.60 15 5 -4 5.00 6.70 -15 -5 4 16.00 15.70 14 5 -4 5.30 5.50 14 5 -4 1.70 5.80 14 5 -4 -12.60 20.20 14 5 -4 7.30 2.40 13 5 -4 -0.50 17.90 13 5 -4 3.10 2.20 13 5 -4 4.50 4.60 13 5 -4 -2.20 6.30 12 5 -4 30.10 3.20 12 5 -4 33.60 5.30 12 5 -4 16.00 7.50 12 5 -4 26.60 16.10 11 5 -4 27.00 2.90 11 5 -4 26.20 4.70 11 5 -4 14.20 14.20 10 5 -4 13.90 11.60 10 5 -4 21.70 2.30 10 5 -4 4.10 7.30 10 5 -4 21.10 3.80 -10 -5 4 18.50 2.20 9 5 -4 9.00 7.20 9 5 -4 26.80 12.00 9 5 -4 22.60 3.60 9 5 -4 18.50 2.10 -9 -5 4 16.90 2.10 8 5 -4 307.57 24.70 8 5 -4 259.47 14.60 8 5 -4 258.77 13.70 8 5 -4 231.18 17.80 -8 -5 4 248.98 13.70 7 5 -4 136.79 17.40 7 5 -4 143.19 8.80 7 5 -4 139.49 7.80 7 5 -4 138.39 12.30 -7 -5 4 144.19 7.90 6 5 -4 431.86 29.20 6 5 -4 406.16 21.90 6 5 -4 408.06 22.50 6 5 -4 441.76 26.00 -6 -5 4 409.76 22.00 5 5 -4 252.07 16.70 5 5 -4 234.78 12.50 5 5 -4 233.88 13.10 5 5 -4 237.08 19.70 -5 -5 4 196.18 20.50 -5 -5 4 235.58 18.90 -5 -5 4 236.98 12.70 4 5 -4 157.98 11.70 4 5 -4 142.59 14.30 4 5 -4 138.39 7.60 4 5 -4 136.79 8.10 -4 -5 4 114.59 14.90 -4 -5 4 130.09 16.20 -4 -5 4 136.09 7.80 3 5 -4 48.50 3.90 3 5 -4 42.60 7.30 -3 -5 4 49.70 3.80 -3 -5 4 52.09 9.80 2 5 -4 21.00 2.20 2 5 -4 22.70 2.80 2 5 -4 17.40 5.40 -2 -5 4 17.30 7.80 -2 -5 4 24.90 2.30 1 5 -4 46.50 7.20 1 5 -4 29.60 2.70 1 5 -4 33.40 2.90 -1 -5 4 25.90 7.80 -1 -5 4 32.00 3.20 0 5 -4 196.48 10.90 0 5 -4 188.88 13.20 0 5 -4 183.78 20.90 0 -5 4 200.88 18.50 0 -5 4 214.78 11.00 -1 5 -4 788.12 45.90 -1 5 -4 854.81 44.90 -1 5 -4 903.81 52.39 1 -5 4 846.32 50.69 1 -5 4 917.71 45.00 -2 5 -4 76.09 4.90 -2 5 -4 62.89 14.00 2 -5 4 74.79 12.40 2 -5 4 79.29 5.10 -3 5 -4 0.70 1.60 3 -5 4 0.30 1.80 3 -5 4 3.20 9.00 -4 5 -4 44.80 3.80 4 -5 4 34.70 7.90 4 -5 4 42.90 3.60 -5 5 -4 332.27 17.80 5 -5 4 325.57 17.60 5 -5 4 352.96 20.80 5 -5 4 300.27 29.00 -6 5 -4 34.90 3.70 6 -5 4 35.00 3.20 6 -5 4 27.10 13.20 6 -5 4 25.70 15.20 6 -5 4 37.30 7.30 -7 5 -4 617.74 31.20 7 -5 4 615.44 31.10 7 -5 4 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13.40 10 4 -4 4.20 10.60 10 4 -4 -4.50 6.00 10 4 -4 2.70 3.00 10 4 -4 4.40 1.60 -10 -4 4 3.40 1.60 9 4 -4 20.50 3.30 9 4 -4 16.00 7.70 9 4 -4 17.30 9.80 9 4 -4 24.60 2.30 -9 -4 4 19.60 2.10 8 4 -4 17.50 7.00 8 4 -4 23.20 9.20 8 4 -4 27.20 3.30 8 4 -4 21.50 2.30 -8 -4 4 22.20 2.10 7 4 -4 7.60 6.50 7 4 -4 7.40 2.50 7 4 -4 7.00 7.30 7 4 -4 10.00 1.40 -7 -4 4 7.50 1.50 6 4 -4 580.44 31.10 6 4 -4 652.73 37.80 6 4 -4 613.44 34.70 6 4 -4 576.84 31.60 -6 -4 4 577.44 31.20 5 4 -4 123.49 6.70 5 4 -4 109.89 13.60 5 4 -4 133.59 11.00 5 4 -4 116.79 7.40 -5 -4 4 112.89 14.80 -5 -4 4 114.19 6.90 -5 -4 4 145.89 13.10 4 4 -4 4.80 1.70 4 4 -4 9.80 5.90 4 4 -4 3.50 5.10 4 4 -4 6.40 1.10 -4 -4 4 2.40 5.70 -4 -4 4 8.00 1.60 -4 -4 4 -0.70 7.10 3 4 -4 38.80 6.80 3 4 -4 34.60 3.30 -3 -4 4 36.50 3.10 -3 -4 4 37.30 8.10 -3 -4 4 45.30 7.10 2 4 -4 406.66 21.10 2 4 -4 386.86 23.70 -2 -4 4 391.16 26.30 -2 -4 4 394.76 21.10 -2 -4 4 419.36 25.10 1 4 -4 136.09 7.30 1 4 -4 122.69 10.00 -1 -4 4 132.19 7.50 -1 -4 4 130.19 14.40 0 4 -4 325.27 19.30 0 4 -4 341.27 18.10 0 -4 4 360.16 18.20 0 -4 4 341.77 24.20 -1 4 -4 7.10 1.50 1 -4 4 8.40 7.10 -2 4 -4 52.89 3.80 2 -4 4 53.59 10.30 2 -4 4 56.79 4.00 -3 4 -4 146.09 8.00 3 -4 4 142.79 20.30 3 -4 4 134.29 8.30 -4 4 -4 806.12 43.40 4 -4 4 774.32 49.70 4 -4 4 863.91 45.50 4 -4 4 880.31 48.90 -5 4 -4 283.07 15.60 5 -4 4 282.07 26.60 5 -4 4 304.07 23.80 5 -4 4 303.67 18.20 5 -4 4 286.47 15.60 -6 4 -4 69.99 4.60 6 -4 4 67.69 4.30 6 -4 4 70.49 14.90 6 -4 4 48.50 11.90 6 -4 4 59.89 4.00 6 -4 4 71.59 7.90 -7 4 -4 179.28 9.90 7 -4 4 193.98 9.80 7 -4 4 173.68 9.70 7 -4 4 157.28 13.60 7 -4 4 154.88 24.40 -8 4 -4 247.88 12.80 8 -4 4 237.78 12.80 8 -4 4 219.78 12.60 8 -4 4 225.28 17.00 -9 4 -4 88.99 5.70 9 -4 4 82.69 5.50 9 -4 4 91.99 5.60 9 -4 4 72.79 11.00 10 -4 4 34.90 9.50 11 -4 4 9.60 2.20 11 -4 4 8.90 8.90 -12 4 -4 14.40 2.50 12 -4 4 16.60 2.70 12 -4 4 8.30 8.90 -13 4 -4 15.90 2.30 13 -4 4 15.30 2.80 13 -4 4 3.80 8.80 14 -4 4 1.90 2.20 14 -4 4 1.30 11.90 15 -4 4 5.60 21.10 15 -4 4 0.50 2.20 16 -4 4 -0.20 2.20 17 -4 4 1.70 2.50 19 3 -4 6.30 11.10 18 3 -4 0.30 4.60 18 3 -4 -2.60 6.40 17 3 -4 0.40 4.80 17 3 -4 -3.30 1.90 17 3 -4 1.10 5.60 16 3 -4 -4.80 4.50 16 3 -4 -1.80 4.50 16 3 -4 5.20 2.00 15 3 -4 22.90 5.20 15 3 -4 9.50 6.50 -15 -3 4 27.50 15.60 14 3 -4 54.09 20.40 14 3 -4 46.70 4.00 14 3 -4 53.29 6.40 -14 -3 4 25.20 12.70 13 3 -4 4.90 7.30 13 3 -4 -4.90 14.90 13 3 -4 1.10 4.30 13 3 -4 0.90 1.90 12 3 -4 3.70 3.70 12 3 -4 -10.50 13.40 12 3 -4 1.90 7.10 12 3 -4 4.90 1.90 11 3 -4 2.70 1.50 11 3 -4 4.70 3.30 11 3 -4 4.30 11.70 11 3 -4 0.60 6.60 10 3 -4 19.20 7.00 10 3 -4 22.50 3.60 10 3 -4 25.70 2.40 10 3 -4 16.70 11.50 -10 -3 4 21.80 2.20 9 3 -4 129.89 8.20 9 3 -4 123.39 17.90 9 3 -4 101.69 11.80 9 3 -4 129.99 7.00 -9 -3 4 131.99 7.10 8 3 -4 162.38 13.60 8 3 -4 180.18 10.40 8 3 -4 194.08 19.50 8 3 -4 168.78 9.40 -8 -3 4 175.68 9.50 7 3 -4 836.12 48.50 7 3 -4 862.01 45.40 7 3 -4 794.92 42.40 7 3 -4 778.82 41.90 -7 -3 4 770.62 41.90 6 3 -4 281.67 15.50 6 3 -4 275.77 14.90 6 3 -4 289.07 21.50 6 3 -4 296.77 18.70 -6 -3 4 280.77 15.00 5 3 -4 397.26 25.60 5 3 -4 393.56 20.90 5 3 -4 393.86 20.50 -5 -3 4 370.16 25.40 -5 -3 4 391.06 20.60 -5 -3 4 401.96 23.70 4 3 -4 20.50 1.70 4 3 -4 32.20 5.90 4 3 -4 21.40 2.30 4 3 -4 20.00 5.90 -4 -3 4 23.50 5.50 -4 -3 4 22.80 2.30 -4 -3 4 26.30 7.40 3 3 -4 178.88 13.70 3 3 -4 187.58 10.10 -3 -3 4 186.38 13.90 -3 -3 4 193.48 16.40 -3 -3 4 178.08 9.90 2 3 -4 3726.33 188.68 2 3 -4 3617.64 190.48 -2 -3 4 3702.53 191.18 -2 -3 4 3483.35 188.58 -2 -3 4 3690.73 192.28 1 3 -4 26.70 4.50 -1 -3 4 31.30 5.80 -1 -3 4 29.50 2.80 -1 -3 4 27.50 7.50 0 3 -4 5134.39 261.57 0 3 -4 4652.83 260.87 0 -3 4 5061.59 260.97 0 -3 4 5070.09 264.77 0 -3 4 5306.47 263.97 -1 3 -4 102.59 5.90 1 -3 4 107.79 10.80 1 -3 4 107.09 13.40 -2 3 -4 55.69 3.70 2 -3 4 58.89 9.90 2 -3 4 60.19 9.70 -3 3 -4 39.60 3.10 3 -3 4 46.30 6.20 3 -3 4 46.20 7.70 3 -3 4 41.20 2.90 3 -3 4 36.10 9.40 -4 3 -4 313.27 17.40 4 -3 4 311.97 25.30 4 -3 4 343.27 22.70 4 -3 4 360.86 19.70 4 -3 4 319.27 17.40 -5 3 -4 397.86 21.40 5 -3 4 406.16 26.90 5 -3 4 386.06 29.70 5 -3 4 446.46 24.00 5 -3 4 390.76 21.30 5 -3 4 401.06 21.40 -6 3 -4 98.99 6.00 6 -3 4 99.39 5.90 6 -3 4 104.79 5.90 6 -3 4 107.99 16.00 6 -3 4 84.49 15.00 6 -3 4 97.09 9.70 -7 3 -4 463.25 23.40 7 -3 4 453.65 23.40 7 -3 4 443.56 23.40 7 -3 4 414.06 31.00 7 -3 4 387.26 34.00 7 -3 4 455.45 26.70 -8 3 -4 575.64 29.10 8 -3 4 515.25 32.70 8 -3 4 576.64 29.20 8 -3 4 542.05 29.30 -9 3 -4 -0.60 1.60 9 -3 4 4.40 6.90 9 -3 4 2.80 1.80 9 -3 4 0.70 2.00 -10 3 -4 2.80 1.80 10 -3 4 1.10 1.80 10 -3 4 0.90 2.20 10 -3 4 -1.70 7.30 -11 3 -4 8.90 2.10 11 -3 4 4.10 8.50 11 -3 4 4.70 2.00 12 -3 4 42.10 11.00 13 -3 4 2.70 8.60 14 -3 4 3.10 9.50 14 -3 4 2.80 2.30 15 -3 4 -2.20 16.90 15 -3 4 -2.20 2.20 16 -3 4 -1.20 2.30 17 -3 4 1.40 2.60 19 2 -4 6.40 11.20 18 2 -4 1.50 6.90 17 2 -4 2.40 4.60 17 2 -4 4.30 2.00 17 2 -4 -1.30 5.30 16 2 -4 5.50 1.60 16 2 -4 11.40 5.00 16 2 -4 3.80 5.80 15 2 -4 10.50 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5 451.75 37.90 4 7 -5 1188.78 62.69 4 7 -5 1191.28 67.89 -4 -7 5 1234.78 69.49 -4 -7 5 1255.57 62.59 -4 -7 5 1113.19 70.49 3 7 -5 16.70 1.90 3 7 -5 19.70 2.70 3 7 -5 16.60 7.20 -3 -7 5 13.10 12.50 -3 -7 5 17.80 2.70 2 7 -5 1273.97 64.19 2 7 -5 1200.78 67.89 2 7 -5 1235.98 63.99 -2 -7 5 1286.07 64.29 -2 -7 5 1141.69 71.79 1 7 -5 34.60 3.40 1 7 -5 26.50 6.70 1 7 -5 31.30 3.40 -1 -7 5 9.70 11.90 -1 -7 5 36.30 4.00 0 7 -5 255.27 18.10 0 7 -5 247.48 33.10 0 7 -5 268.07 14.70 0 7 -5 273.47 14.60 0 -7 5 285.87 14.90 -1 7 -5 52.09 18.10 -1 7 -5 24.40 5.60 -1 7 -5 23.00 2.60 1 -7 5 26.00 3.10 1 -7 5 22.60 13.10 -2 7 -5 86.49 21.80 -2 7 -5 88.29 6.10 -2 7 -5 84.19 8.70 2 -7 5 99.09 6.30 2 -7 5 92.89 17.80 -3 7 -5 14.90 4.50 -3 7 -5 19.50 2.60 3 -7 5 6.70 15.30 3 -7 5 16.30 2.80 -4 7 -5 36.10 4.00 4 -7 5 27.10 17.40 4 -7 5 32.70 3.40 -5 7 -5 79.99 5.90 5 -7 5 123.59 22.60 5 -7 5 83.09 5.80 -6 7 -5 83.39 5.70 6 -7 5 82.69 5.20 6 -7 5 64.29 5.20 -7 7 -5 1.50 2.30 7 -7 5 -0.70 1.80 7 -7 5 -44.00 28.50 -8 7 -5 7.60 2.60 8 -7 5 10.50 2.20 -9 7 -5 2.70 2.70 9 -7 5 1.00 15.20 9 -7 5 3.30 2.30 10 -7 5 -1.50 17.30 -11 7 -5 30.80 3.80 11 -7 5 42.20 3.90 -12 7 -5 60.49 5.40 12 -7 5 57.09 5.20 -13 7 -5 1.50 2.60 13 -7 5 1.40 2.60 -14 7 -5 11.50 2.70 14 -7 5 10.40 2.80 -15 7 -5 3.50 3.50 15 -7 5 -0.50 2.20 16 -7 5 4.90 2.50 17 -7 5 2.50 2.90 18 6 -5 5.40 8.90 18 6 -5 0.90 7.40 17 6 -5 0.20 6.50 17 6 -5 2.00 6.40 16 6 -5 7.60 4.80 16 6 -5 0.10 6.20 16 6 -5 -0.70 26.10 16 6 -5 -0.80 5.30 15 6 -5 4.90 7.30 15 6 -5 7.50 4.30 15 6 -5 10.70 5.80 15 6 -5 -2.70 21.80 14 6 -5 41.60 6.90 14 6 -5 39.40 4.30 14 6 -5 32.60 22.00 13 6 -5 13.40 19.30 13 6 -5 5.10 2.50 13 6 -5 0.60 6.50 13 6 -5 6.00 4.80 12 6 -5 13.30 16.30 12 6 -5 23.10 5.10 12 6 -5 26.10 2.90 11 6 -5 13.40 14.30 11 6 -5 5.80 7.20 11 6 -5 19.70 2.50 11 6 -5 16.30 4.50 -11 -6 5 15.60 2.50 10 6 -5 1.00 1.80 10 6 -5 -1.20 11.50 10 6 -5 6.40 3.70 10 6 -5 5.30 7.50 -10 -6 5 5.90 2.20 9 6 -5 30.60 5.20 9 6 -5 16.00 2.20 9 6 -5 12.80 8.00 9 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3.30 13 -11 6 0.80 2.70 -14 11 -6 -3.50 2.80 14 -11 6 0.60 2.60 -15 11 -6 4.90 3.10 15 -11 6 0.30 2.70 16 -11 6 2.00 3.10 16 10 -6 2.80 5.60 16 10 -6 10.10 10.40 15 10 -6 -2.90 5.20 15 10 -6 1.30 6.30 14 10 -6 -1.30 5.80 14 10 -6 -31.30 22.70 14 10 -6 4.20 6.30 13 10 -6 28.10 24.00 13 10 -6 29.30 7.40 12 10 -6 38.20 6.70 12 10 -6 19.70 21.90 -12 -10 6 27.60 4.10 11 10 -6 2.00 4.90 11 10 -6 1.70 6.60 11 10 -6 19.80 19.30 -11 -10 6 2.20 3.00 10 10 -6 19.90 5.40 10 10 -6 10.50 17.80 10 10 -6 5.30 7.90 -10 -10 6 10.90 3.30 9 10 -6 4.80 4.60 9 10 -6 -1.10 13.40 9 10 -6 1.20 7.80 -9 -10 6 4.60 3.00 8 10 -6 52.29 6.30 8 10 -6 37.50 16.50 -8 -10 6 51.69 5.10 7 10 -6 6.90 3.70 7 10 -6 -1.20 5.20 7 10 -6 -1.20 11.10 -7 -10 6 3.20 2.80 6 10 -6 0.90 6.20 6 10 -6 0.00 3.30 6 10 -6 -3.20 10.40 -6 -10 6 4.40 2.80 5 10 -6 97.49 12.50 5 10 -6 114.19 7.70 5 10 -6 95.19 16.40 -5 -10 6 37.40 37.30 -5 -10 6 115.29 7.40 4 10 -6 115.09 17.00 4 10 -6 105.09 6.10 4 10 -6 102.89 7.30 -4 -10 6 101.89 7.20 -4 -10 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46.40 5.30 7 12 -7 4.80 4.30 7 12 -7 -18.30 13.90 7 12 -7 -2.00 6.20 -7 -12 7 1.10 3.50 6 12 -7 71.49 6.80 6 12 -7 35.30 15.70 -6 -12 7 61.59 6.10 5 12 -7 -0.60 5.00 5 12 -7 2.70 3.60 5 12 -7 5.30 12.90 -5 -12 7 -0.10 3.40 4 12 -7 16.20 13.00 4 12 -7 45.50 4.90 -4 -12 7 42.90 5.10 3 12 -7 2.60 10.90 3 12 -7 0.50 2.90 -3 -12 7 4.80 3.30 2 12 -7 38.90 3.90 2 12 -7 38.60 12.30 2 12 -7 42.70 4.50 -2 -12 7 32.20 4.40 1 12 -7 13.30 2.80 1 12 -7 3.10 9.80 1 12 -7 13.10 2.80 -1 -12 7 10.60 3.60 0 12 -7 13.50 2.80 0 12 -7 3.60 10.10 0 -12 7 18.50 3.80 -1 12 -7 41.20 4.10 -1 12 -7 36.50 11.10 1 -12 7 47.50 49.80 1 -12 7 39.40 4.80 -2 12 -7 15.20 10.50 2 -12 7 42.10 53.59 -3 12 -7 1.80 2.90 3 -12 7 -0.20 3.50 -4 12 -7 14.70 3.40 4 -12 7 10.00 4.00 -5 12 -7 73.19 6.00 5 -12 7 51.59 6.50 -6 12 -7 -3.90 3.10 6 -12 7 3.90 3.50 -7 12 -7 -2.20 3.50 7 -12 7 0.30 3.40 -8 12 -7 17.50 4.10 8 -12 7 12.70 3.30 -9 12 -7 1.30 3.60 9 -12 7 -2.30 3.10 -10 12 -7 3.40 3.60 10 -12 7 0.50 2.90 -11 12 -7 2.00 3.60 11 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7 21.40 30.20 1 10 -7 9.70 7.50 1 10 -7 14.00 2.50 1 10 -7 7.00 2.20 -1 -10 7 9.70 3.10 -1 -10 7 15.20 28.00 0 10 -7 9.10 7.00 0 10 -7 2.70 2.10 0 -10 7 6.10 3.00 0 -10 7 22.60 28.60 -1 10 -7 131.59 7.80 -1 10 -7 100.89 13.30 1 -10 7 90.99 32.90 1 -10 7 131.99 8.50 -2 10 -7 167.48 9.90 2 -10 7 162.68 10.40 2 -10 7 172.08 36.20 -3 10 -7 200.08 11.60 3 -10 7 205.08 39.20 3 -10 7 195.38 12.00 -4 10 -7 321.87 17.40 4 -10 7 303.57 17.70 -5 10 -7 108.99 7.60 5 -10 7 108.89 7.90 -6 10 -7 403.56 21.30 6 -10 7 369.26 21.20 -7 10 -7 7.80 3.20 7 -10 7 8.40 2.70 -8 10 -7 2.70 3.00 8 -10 7 0.10 2.60 -9 10 -7 7.40 3.30 9 -10 7 2.50 3.00 -10 10 -7 1.30 3.30 10 -10 7 2.00 2.70 -11 10 -7 14.60 3.80 11 -10 7 22.00 3.70 -12 10 -7 1.90 3.20 12 -10 7 0.40 2.60 -13 10 -7 1.60 2.90 13 -10 7 4.00 2.90 -14 10 -7 6.90 2.90 14 -10 7 5.80 3.10 -15 10 -7 4.50 2.60 15 -10 7 5.70 3.30 16 -10 7 6.60 3.40 17 9 -7 -3.30 9.10 17 9 -7 0.60 7.20 16 9 -7 1.10 6.20 16 9 -7 -10.90 7.40 15 9 -7 36.00 26.00 15 9 -7 -0.20 5.80 15 9 -7 -0.60 6.10 14 9 -7 -2.50 5.50 14 9 -7 0.70 20.90 14 9 -7 1.00 7.10 13 9 -7 13.50 6.00 13 9 -7 1.30 5.90 13 9 -7 -3.30 21.20 12 9 -7 0.10 6.30 12 9 -7 33.80 19.70 12 9 -7 14.10 5.70 -12 -9 7 12.90 3.30 11 9 -7 37.00 18.80 11 9 -7 75.29 7.70 -11 -9 7 56.79 5.40 10 9 -7 3.30 4.60 10 9 -7 11.90 15.50 10 9 -7 3.60 8.70 -10 -9 7 1.40 3.00 9 9 -7 360.56 33.50 9 9 -7 335.07 19.70 -9 -9 7 323.57 18.40 8 9 -7 63.19 6.60 8 9 -7 47.70 15.40 -8 -9 7 55.69 5.30 7 9 -7 2.80 7.20 7 9 -7 6.90 3.70 7 9 -7 0.40 10.10 -7 -9 7 4.90 2.90 6 9 -7 3.50 6.80 6 9 -7 0.40 3.00 6 9 -7 13.80 9.40 -6 -9 7 1.70 27.70 -6 -9 7 0.80 2.70 5 9 -7 18.10 8.90 5 9 -7 25.60 3.80 5 9 -7 27.80 10.40 -5 -9 7 28.80 25.00 -5 -9 7 28.40 3.50 4 9 -7 84.39 6.40 4 9 -7 89.49 5.20 4 9 -7 73.49 12.40 -4 -9 7 85.39 6.30 -4 -9 7 85.79 25.00 3 9 -7 280.87 15.60 3 9 -7 296.17 15.10 3 9 -7 261.97 21.90 -3 -9 7 223.78 37.30 -3 -9 7 240.98 34.00 -3 -9 7 292.57 15.70 2 9 -7 31.30 8.30 2 9 -7 31.30 3.30 2 9 -7 28.90 2.80 -2 -9 7 34.90 3.70 -2 -9 7 13.60 19.90 -2 -9 7 57.99 26.40 1 9 -7 464.95 24.40 1 9 -7 441.36 28.80 1 9 -7 451.15 24.50 -1 -9 7 454.25 42.80 -1 -9 7 475.05 24.80 -1 -9 7 457.35 48.20 0 9 -7 41.20 4.10 0 9 -7 42.00 7.70 0 -9 7 48.00 5.00 0 -9 7 41.90 25.60 -1 9 -7 496.15 30.10 -1 9 -7 526.85 27.80 1 -9 7 486.75 51.69 1 -9 7 552.24 28.10 2 -9 7 6.20 3.00 2 -9 7 -34.00 27.40 -3 9 -7 186.38 11.20 3 -9 7 200.58 11.60 3 -9 7 258.67 36.50 3 -9 7 160.48 30.40 -4 9 -7 41.70 4.50 4 -9 7 51.79 33.90 4 -9 7 -8.90 42.30 4 -9 7 34.50 4.20 -5 9 -7 2.80 2.60 5 -9 7 -14.90 39.20 5 -9 7 3.30 2.90 -6 9 -7 119.29 8.20 6 -9 7 126.99 7.80 -7 9 -7 4.80 2.90 7 -9 7 4.90 2.70 -8 9 -7 3.20 2.90 8 -9 7 4.70 2.40 -9 9 -7 -0.10 2.90 9 -9 7 -0.30 2.60 -10 9 -7 9.40 3.30 10 -9 7 3.90 2.70 -11 9 -7 4.10 3.30 11 -9 7 12.40 3.10 -12 9 -7 0.90 3.00 12 -9 7 -1.20 2.50 -13 9 -7 -0.30 2.70 13 -9 7 4.00 2.80 -14 9 -7 -1.70 2.50 14 -9 7 -0.70 2.70 -15 9 -7 3.00 2.30 15 -9 7 0.60 2.80 16 -9 7 3.10 3.30 18 8 -7 0.60 9.50 18 8 -7 -12.20 9.00 17 8 -7 0.10 8.60 17 8 -7 0.00 6.90 16 8 -7 4.40 7.60 16 8 -7 6.50 6.90 16 8 -7 70.69 30.80 -16 -8 7 16.80 20.20 15 8 -7 25.00 23.50 15 8 -7 7.30 5.70 15 8 -7 1.60 7.40 14 8 -7 19.20 5.90 14 8 -7 24.50 22.30 13 8 -7 14.60 5.80 13 8 -7 18.20 18.90 13 8 -7 4.60 6.30 12 8 -7 46.30 6.30 12 8 -7 37.30 20.00 -12 -8 7 37.00 4.50 11 8 -7 3.00 7.90 11 8 -7 20.10 5.30 11 8 -7 20.10 16.70 -11 -8 7 9.20 3.10 10 8 -7 2.80 4.20 10 8 -7 -9.70 14.60 10 8 -7 1.30 8.30 -10 -8 7 -3.90 2.60 9 8 -7 41.30 5.20 9 8 -7 41.80 13.70 -9 -8 7 39.60 4.50 8 8 -7 68.79 6.50 8 8 -7 52.89 14.50 -8 -8 7 56.99 5.20 -8 -8 7 1.20 32.50 7 8 -7 15.60 8.30 7 8 -7 37.70 12.10 7 8 -7 31.70 4.00 -7 -8 7 32.20 3.60 -7 -8 7 34.30 25.30 6 8 -7 65.39 6.10 6 8 -7 65.69 11.20 6 8 -7 60.09 11.90 -6 -8 7 91.49 23.30 -6 -8 7 71.09 5.50 5 8 -7 459.65 30.40 5 8 -7 423.26 22.70 5 8 -7 390.06 27.10 -5 -8 7 331.67 54.39 -5 -8 7 444.76 22.40 -5 -8 7 342.17 39.00 4 8 -7 146.39 8.00 4 8 -7 133.89 8.80 4 8 -7 154.18 16.50 -4 -8 7 101.09 24.00 -4 -8 7 138.99 21.20 -4 -8 7 150.08 8.80 3 8 -7 717.53 39.10 3 8 -7 755.12 44.20 3 8 -7 767.02 38.80 -3 -8 7 758.12 39.10 -3 -8 7 715.83 50.99 -3 -8 7 710.73 54.89 2 8 -7 88.29 12.50 2 8 -7 94.39 6.40 2 8 -7 97.39 5.90 -2 -8 7 92.79 21.40 -2 -8 7 66.49 16.70 -2 -8 7 96.29 6.60 1 8 -7 182.48 15.00 1 8 -7 179.28 10.30 -1 -8 7 204.38 33.80 -1 -8 7 184.38 10.80 -1 -8 7 188.08 27.90 0 8 -7 88.69 5.90 0 8 -7 87.89 10.00 0 -8 7 99.49 6.60 0 -8 7 75.69 22.30 0 -8 7 74.09 17.20 -1 8 -7 44.40 6.20 -1 8 -7 46.20 4.20 1 -8 7 52.69 5.10 1 -8 7 52.09 17.50 1 -8 7 52.29 22.20 -2 8 -7 38.70 4.00 2 -8 7 10.20 17.40 2 -8 7 30.10 22.40 2 -8 7 42.00 4.70 -3 8 -7 638.24 33.60 3 -8 7 588.14 56.79 3 -8 7 661.03 33.80 3 -8 7 615.74 50.69 -4 8 -7 322.77 16.90 4 -8 7 304.87 17.10 4 -8 7 252.47 42.00 -5 8 -7 37.60 4.20 5 -8 7 27.00 33.20 5 -8 7 28.60 3.60 -6 8 -7 11.70 2.70 6 -8 7 5.10 2.30 -7 8 -7 3.30 2.60 7 -8 7 7.90 2.40 -8 8 -7 1.90 2.60 8 -8 7 0.50 2.40 -9 8 -7 -0.30 2.60 9 -8 7 0.90 2.20 -10 8 -7 2.40 2.90 10 -8 7 4.00 2.70 -11 8 -7 51.79 5.40 11 -8 7 60.69 5.30 -12 8 -7 3.20 2.90 12 -8 7 4.60 2.80 -13 8 -7 16.40 3.00 13 -8 7 15.20 3.00 -14 8 -7 3.30 2.40 14 -8 7 10.90 2.90 15 -8 7 -2.20 2.70 16 -8 7 0.90 3.30 18 7 -7 -3.40 8.70 18 7 -7 0.40 8.60 17 7 -7 -0.60 7.10 17 7 -7 -1.00 7.20 16 7 -7 17.10 6.70 16 7 -7 0.70 7.20 -16 -7 7 3.60 18.20 15 7 -7 25.40 6.70 15 7 -7 7.20 8.80 15 7 -7 -18.30 21.10 14 7 -7 23.20 21.10 13 7 -7 69.99 21.90 13 7 -7 66.49 7.90 12 7 -7 -12.10 15.30 12 7 -7 -2.40 4.60 12 7 -7 0.30 7.90 -12 -7 7 -5.20 2.50 11 7 -7 61.09 7.20 11 7 -7 79.19 19.60 11 7 -7 48.50 5.60 -11 -7 7 55.89 5.10 10 7 -7 78.29 17.70 10 7 -7 86.29 7.80 10 7 -7 60.79 12.20 -10 -7 7 76.99 5.70 9 7 -7 15.10 4.10 9 7 -7 3.80 7.30 9 7 -7 2.70 10.50 -9 -7 7 7.20 2.70 8 7 -7 197.68 22.40 8 7 -7 173.08 11.00 8 7 -7 146.49 16.00 -8 -7 7 191.08 10.20 -8 -7 7 136.19 25.00 7 7 -7 129.79 8.80 7 7 -7 140.49 18.70 7 7 -7 116.79 13.50 -7 -7 7 141.59 8.20 -7 -7 7 148.89 22.50 6 7 -7 0.70 7.40 6 7 -7 2.60 7.70 6 7 -7 5.10 2.70 -6 -7 7 3.40 2.40 -6 -7 7 2.40 17.60 5 7 -7 39.60 9.30 5 7 -7 34.90 8.90 5 7 -7 44.70 4.70 -5 -7 7 35.80 4.30 -5 -7 7 32.90 16.10 -5 -7 7 53.09 20.50 4 7 -7 -2.20 1.20 4 7 -7 0.20 2.40 4 7 -7 -6.80 6.20 -4 -7 7 7.90 18.40 -4 -7 7 2.70 13.90 -4 -7 7 -0.60 2.30 3 7 -7 200.38 17.30 3 7 -7 197.58 11.70 3 7 -7 209.38 11.20 -3 -7 7 215.18 25.30 -3 -7 7 167.88 24.40 -3 -7 7 215.08 11.70 2 7 -7 0.00 2.30 2 7 -7 2.60 1.70 -2 -7 7 9.40 12.40 -2 -7 7 2.20 15.90 -2 -7 7 1.20 2.50 1 7 -7 479.15 28.80 1 7 -7 469.25 25.60 -1 -7 7 459.55 40.40 -1 -7 7 511.55 37.00 -1 -7 7 500.85 25.90 0 7 -7 34.30 3.50 0 7 -7 32.20 5.70 0 -7 7 31.00 17.50 0 -7 7 19.00 13.00 0 -7 7 36.10 4.30 -1 7 -7 58.89 4.40 1 -7 7 44.70 19.90 1 -7 7 52.29 5.00 -2 7 -7 45.20 4.00 2 -7 7 42.40 4.00 2 -7 7 11.10 21.80 2 -7 7 33.10 15.70 -3 7 -7 40.30 3.90 3 -7 7 45.00 4.60 3 -7 7 4.20 22.80 3 -7 7 23.60 17.40 -4 7 -7 113.49 6.70 4 -7 7 72.19 21.30 4 -7 7 87.59 27.10 4 -7 7 99.79 7.00 -5 7 -7 451.65 23.50 5 -7 7 443.16 23.40 5 -7 7 421.96 23.50 -6 7 -7 863.71 46.00 6 -7 7 884.91 45.90 -7 7 -7 6.60 2.60 7 -7 7 9.20 2.30 -8 7 -7 50.99 4.80 8 -7 7 51.29 4.50 -9 7 -7 4.60 2.70 9 -7 7 3.30 2.30 -10 7 -7 5.90 2.90 10 -7 7 5.30 2.40 -11 7 -7 58.19 5.40 11 -7 7 61.49 5.30 -12 7 -7 33.00 3.80 12 -7 7 40.60 4.40 -13 7 -7 1.10 2.30 13 -7 7 1.40 2.40 -14 7 -7 10.90 2.40 14 -7 7 12.70 3.10 15 -7 7 2.20 2.70 16 -7 7 -0.40 3.30 18 6 -7 -1.50 7.70 18 6 -7 -1.90 8.60 17 6 -7 9.50 6.10 17 6 -7 -0.90 7.40 16 6 -7 29.60 6.50 16 6 -7 -0.10 7.40 -16 -6 7 8.70 16.60 15 6 -7 20.10 19.70 15 6 -7 30.50 6.30 14 6 -7 -1.00 6.60 14 6 -7 9.50 5.40 14 6 -7 33.60 19.00 13 6 -7 11.50 8.40 13 6 -7 27.20 19.10 13 6 -7 20.60 5.80 13 6 -7 12.40 4.50 12 6 -7 9.60 5.00 12 6 -7 8.60 8.40 12 6 -7 10.30 3.80 12 6 -7 -6.40 14.30 -12 -6 7 9.30 2.90 11 6 -7 -0.40 4.00 11 6 -7 -8.90 12.80 11 6 -7 -4.30 3.10 11 6 -7 1.20 8.20 -11 -6 7 -4.20 2.50 10 6 -7 201.98 24.10 10 6 -7 147.49 10.40 10 6 -7 148.59 9.20 -10 -6 7 161.58 9.40 9 6 -7 331.37 18.30 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16 -8 9.50 4.00 5 -16 8 4.30 4.70 -6 16 -8 2.00 3.90 6 -16 8 9.20 3.60 -7 16 -8 11.30 4.30 -8 16 -8 -1.50 3.80 8 -16 8 1.30 3.30 -9 16 -8 6.00 4.10 9 -16 8 2.40 3.20 -10 16 -8 -2.90 4.10 10 -16 8 0.10 3.20 -11 16 -8 4.70 4.40 11 -16 8 -6.80 3.40 -12 16 -8 -1.70 4.90 12 -16 8 3.00 3.50 -13 16 -8 8.20 4.90 13 -16 8 1.20 3.70 13 15 -8 -0.90 9.20 12 15 -8 -3.70 5.10 12 15 -8 5.90 7.70 11 15 -8 -36.10 38.40 11 15 -8 1.10 4.90 11 15 -8 12.10 6.00 -11 -15 8 0.10 3.30 10 15 -8 8.00 29.20 10 15 -8 -0.90 5.10 10 15 -8 -1.40 5.70 -10 -15 8 1.90 3.20 9 15 -8 22.50 25.00 9 15 -8 1.60 7.00 9 15 -8 19.20 5.30 -9 -15 8 8.60 3.90 8 15 -8 -1.20 4.40 8 15 -8 24.50 24.50 8 15 -8 1.70 3.70 -8 -15 8 7.50 3.80 7 15 -8 14.90 23.00 7 15 -8 3.60 4.20 7 15 -8 5.60 4.60 -7 -15 8 8.20 4.10 6 15 -8 -0.90 22.90 6 15 -8 -0.90 4.60 -6 -15 8 1.80 4.10 5 15 -8 2.10 21.00 5 15 -8 12.50 4.20 5 15 -8 -0.30 5.30 -5 -15 8 11.90 4.40 4 15 -8 6.00 3.80 4 15 -8 -14.00 19.40 4 15 -8 -0.70 5.10 -4 -15 8 3.40 4.00 3 15 -8 3.50 18.60 3 15 -8 0.10 3.40 3 15 -8 3.20 6.00 -3 -15 8 2.30 4.20 2 15 -8 21.70 19.30 2 15 -8 19.90 5.30 -2 -15 8 26.70 5.10 1 15 -8 40.70 4.60 1 15 -8 4.90 18.50 -1 -15 8 39.20 5.70 0 15 -8 -2.40 2.90 0 15 -8 -29.80 19.10 0 -15 8 -0.70 4.40 -1 15 -8 24.50 4.00 1 -15 8 16.60 5.10 -2 15 -8 0.30 3.30 2 -15 8 6.10 4.80 -3 15 -8 0.20 3.40 3 -15 8 -2.30 4.20 -4 15 -8 57.69 6.10 4 -15 8 48.90 6.60 5 -15 8 184.58 12.60 6 -15 8 41.40 5.20 -7 15 -8 8.20 4.10 -8 15 -8 50.29 5.70 8 -15 8 43.50 5.10 -9 15 -8 1.10 3.90 9 -15 8 0.80 3.40 -10 15 -8 13.10 4.30 10 -15 8 10.20 3.60 -11 15 -8 45.30 5.80 11 -15 8 47.10 5.50 -12 15 -8 -2.50 4.20 12 -15 8 2.00 3.30 -13 15 -8 7.30 5.10 13 -15 8 7.60 3.70 14 14 -8 -0.60 7.40 13 14 -8 -1.50 5.00 13 14 -8 -1.90 8.90 12 14 -8 -1.20 6.80 12 14 -8 3.00 5.30 12 14 -8 -40.10 34.70 -12 -14 8 6.60 3.20 11 14 -8 2.00 5.50 11 14 -8 3.60 6.10 11 14 -8 27.90 30.30 -11 -14 8 -2.60 3.00 10 14 -8 -10.70 23.60 10 14 -8 8.30 5.60 10 14 -8 5.70 7.30 -10 -14 8 0.30 3.50 9 14 -8 51.09 26.20 -9 -14 8 20.00 4.30 8 14 -8 34.50 5.60 8 14 -8 14.10 20.70 -8 -14 8 21.50 4.60 7 14 -8 -0.80 5.10 7 14 -8 -3.10 20.70 7 14 -8 9.20 4.50 -7 -14 8 6.00 3.80 6 14 -8 23.10 19.50 6 14 -8 16.40 4.80 6 14 -8 4.80 6.10 -6 -14 8 5.20 3.90 5 14 -8 1.00 16.80 5 14 -8 2.50 3.90 5 14 -8 -2.30 5.90 -5 -14 8 0.90 4.00 4 14 -8 12.20 15.90 4 14 -8 -0.30 6.30 -4 -14 8 27.40 4.60 3 14 -8 5.60 3.50 3 14 -8 -0.30 14.80 3 14 -8 -3.70 1.50 -3 -14 8 0.70 4.20 2 14 -8 11.20 15.30 2 14 -8 8.50 3.20 2 14 -8 7.20 2.50 -2 -14 8 0.30 4.20 1 14 -8 26.80 16.50 1 14 -8 29.10 3.70 -1 -14 8 35.40 5.20 0 14 -8 96.29 7.10 0 14 -8 84.69 17.90 0 -14 8 96.19 8.60 -1 14 -8 9.30 3.30 -1 14 -8 6.90 18.50 1 -14 8 10.90 4.80 -2 14 -8 10.30 3.40 2 -14 8 12.90 4.90 -3 14 -8 32.90 4.40 3 -14 8 26.40 5.20 -4 14 -8 13.10 3.90 4 -14 8 4.50 4.50 -5 14 -8 73.09 6.60 5 -14 8 60.69 6.70 6 -14 8 91.79 7.60 -7 14 -8 31.20 5.10 7 -14 8 44.30 4.90 -8 14 -8 0.20 3.80 8 -14 8 0.60 3.20 -9 14 -8 18.50 4.50 9 -14 8 32.20 4.50 -10 14 -8 3.20 3.80 10 -14 8 1.60 3.20 -11 14 -8 6.10 4.10 11 -14 8 14.10 3.90 -12 14 -8 7.90 4.00 12 -14 8 1.40 3.00 -13 14 -8 -0.90 4.20 13 -14 8 5.90 3.90 -14 14 -8 1.70 4.10 14 -14 8 5.70 3.90 15 13 -8 -1.00 7.80 14 13 -8 5.40 5.40 14 13 -8 9.20 8.80 13 13 -8 -50.79 31.90 13 13 -8 -2.10 5.20 13 13 -8 4.20 6.70 12 13 -8 -2.90 22.70 12 13 -8 2.40 5.70 12 13 -8 0.10 5.90 -12 -13 8 9.60 3.00 11 13 -8 12.80 5.70 11 13 -8 30.10 24.10 11 13 -8 6.80 7.70 -11 -13 8 7.10 3.50 10 13 -8 -0.60 8.10 10 13 -8 -8.20 19.70 10 13 -8 4.70 4.90 -10 -13 8 -0.60 3.30 9 13 -8 9.30 22.40 9 13 -8 3.30 5.90 8 13 -8 11.90 19.20 8 13 -8 28.90 5.70 -8 -13 8 25.50 4.50 7 13 -8 2.00 4.40 7 13 -8 -1.10 6.40 7 13 -8 10.10 17.60 -7 -13 8 4.40 3.60 6 13 -8 36.00 18.40 6 13 -8 60.09 6.70 -6 -13 8 58.39 6.00 5 13 -8 0.90 4.00 5 13 -8 2.30 6.70 5 13 -8 -2.20 14.00 -5 -13 8 -0.50 3.60 4 13 -8 27.30 4.40 4 13 -8 11.90 7.60 4 13 -8 17.70 14.20 -4 -13 8 30.00 4.60 3 13 -8 11.10 13.40 3 13 -8 8.60 3.40 3 13 -8 3.20 1.50 -3 -13 8 0.90 4.00 2 13 -8 20.70 13.10 2 13 -8 9.70 3.20 2 13 -8 7.30 2.60 -2 -13 8 6.40 4.00 1 13 -8 127.19 7.90 1 13 -8 124.09 17.30 -1 -13 8 110.29 8.70 0 13 -8 38.90 13.40 0 13 -8 19.10 3.50 0 -13 8 24.40 4.70 -1 13 -8 148.09 9.30 -1 13 -8 132.39 20.90 1 -13 8 142.99 10.50 -2 13 -8 13.20 3.50 2 -13 8 11.30 4.50 -3 13 -8 205.48 12.50 3 -13 8 203.18 13.20 -4 13 -8 163.18 10.40 4 -13 8 158.08 11.10 -5 13 -8 7.40 3.70 5 -13 8 9.70 4.40 -6 13 -8 51.19 6.20 -7 13 -8 11.60 4.00 7 -13 8 4.90 3.20 -8 13 -8 14.30 4.10 8 -13 8 25.30 4.20 -9 13 -8 -6.90 3.40 9 -13 8 3.60 3.10 -10 13 -8 14.60 4.10 10 -13 8 13.80 3.90 -11 13 -8 1.90 3.60 11 -13 8 -1.00 3.20 -12 13 -8 -2.20 3.20 12 -13 8 -1.60 2.90 -13 13 -8 3.30 3.60 13 -13 8 -0.30 3.20 -14 13 -8 -2.80 3.70 14 -13 8 -0.80 3.70 15 12 -8 3.40 9.10 15 12 -8 -0.20 5.80 14 12 -8 -2.40 6.30 14 12 -8 2.60 5.70 13 12 -8 -5.00 22.30 13 12 -8 7.10 6.40 13 12 -8 -1.00 5.80 12 12 -8 0.90 7.20 12 12 -8 23.30 23.10 12 12 -8 4.20 5.70 -12 -12 8 0.50 2.90 11 12 -8 -1.40 7.80 11 12 -8 10.20 5.60 11 12 -8 -20.10 22.50 10 12 -8 3.30 5.20 10 12 -8 -20.50 17.30 10 12 -8 9.70 9.40 -10 -12 8 -1.30 3.30 9 12 -8 21.90 5.50 9 12 -8 32.90 19.90 -9 -12 8 32.20 4.40 8 12 -8 -0.10 7.20 8 12 -8 27.00 16.50 8 12 -8 13.60 4.90 -8 -12 8 14.70 4.00 7 12 -8 13.50 4.40 7 12 -8 32.70 15.60 -7 -12 8 6.40 3.80 6 12 -8 22.90 14.90 6 12 -8 3.90 7.40 6 12 -8 18.20 4.50 -6 -12 8 15.00 3.90 5 12 -8 54.29 5.80 5 12 -8 37.10 15.00 -5 -12 8 43.80 5.50 4 12 -8 -4.50 3.20 4 12 -8 -1.50 11.90 4 12 -8 1.40 1.50 -4 -12 8 -0.50 3.50 3 12 -8 56.69 13.90 3 12 -8 58.79 5.90 3 12 -8 69.09 4.70 -3 -12 8 63.19 6.50 2 12 -8 11.00 2.60 2 12 -8 11.80 3.20 2 12 -8 15.80 11.70 -2 -12 8 13.50 3.90 1 12 -8 134.29 8.20 1 12 -8 136.49 18.80 -1 -12 8 120.69 9.10 0 12 -8 11.90 10.80 0 12 -8 1.60 2.60 0 -12 8 2.50 3.60 -1 12 -8 5.90 2.80 -1 12 -8 18.20 11.00 1 -12 8 10.60 3.90 1 -12 8 44.00 59.09 -2 12 -8 6.20 2.90 2 -12 8 3.00 3.90 -3 12 -8 -1.00 2.70 3 -12 8 -0.80 3.80 -4 12 -8 213.88 12.60 4 -12 8 194.28 12.80 -5 12 -8 97.19 7.60 5 -12 8 91.99 7.80 -6 12 -8 6.90 3.50 6 -12 8 -2.80 2.70 -7 12 -8 18.70 4.10 7 -12 8 29.00 4.00 -8 12 -8 5.50 3.50 8 -12 8 5.00 3.20 -9 12 -8 -1.30 3.40 9 -12 8 0.20 3.00 -10 12 -8 2.90 3.50 10 -12 8 0.10 3.30 -11 12 -8 1.80 3.40 11 -12 8 3.30 3.00 -12 12 -8 -3.30 3.20 12 -12 8 5.30 3.00 -13 12 -8 8.70 3.60 13 -12 8 6.90 3.50 -14 12 -8 -0.80 3.00 14 -12 8 1.40 3.40 -15 12 -8 1.10 3.40 15 -12 8 3.60 3.60 16 11 -8 -3.70 7.70 16 11 -8 -2.70 6.50 15 11 -8 4.90 9.40 15 11 -8 1.80 6.10 14 11 -8 2.70 6.60 14 11 -8 -2.90 5.70 14 11 -8 24.60 25.50 13 11 -8 -2.40 5.60 13 11 -8 1.40 7.10 13 11 -8 2.50 22.20 12 11 -8 0.90 7.90 12 11 -8 -2.50 5.50 12 11 -8 -17.40 21.30 -12 -11 8 -1.10 3.00 11 11 -8 24.90 20.40 11 11 -8 -4.40 5.00 11 11 -8 2.10 6.40 -11 -11 8 3.00 3.30 10 11 -8 -20.60 17.00 10 11 -8 -2.00 6.60 10 11 -8 2.70 4.70 -10 -11 8 0.90 3.30 9 11 -8 -1.50 6.30 9 11 -8 15.40 16.70 9 11 -8 7.80 5.00 -9 -11 8 5.10 3.50 8 11 -8 100.49 22.00 8 11 -8 155.98 10.70 -8 -11 8 144.49 9.60 7 11 -8 92.39 17.50 7 11 -8 110.29 8.60 -7 -11 8 93.39 7.50 6 11 -8 64.49 6.40 6 11 -8 39.00 15.00 -6 -11 8 67.09 6.00 5 11 -8 93.59 16.40 5 11 -8 95.19 7.60 -5 -11 8 104.69 7.60 4 11 -8 24.70 2.70 4 11 -8 9.70 10.90 4 11 -8 24.50 3.90 -4 -11 8 17.80 3.90 3 11 -8 23.70 2.70 3 11 -8 23.60 3.80 -3 -11 8 22.60 3.90 2 11 -8 42.20 4.00 2 11 -8 35.50 11.10 2 11 -8 33.70 3.90 -2 -11 8 25.00 37.10 -2 -11 8 40.30 4.60 1 11 -8 -0.20 2.20 1 11 -8 -13.30 8.60 -1 -11 8 2.40 3.30 -1 -11 8 13.50 45.50 -1 -11 8 21.40 33.50 0 11 -8 25.40 3.10 0 11 -8 22.70 9.60 0 -11 8 -19.30 34.70 0 -11 8 25.60 4.10 0 -11 8 29.90 42.30 1 -11 8 82.69 38.50 1 -11 8 77.19 43.80 2 -11 8 60.29 39.30 2 -11 8 44.80 46.20 -3 11 -8 99.89 6.90 3 -11 8 100.59 7.90 -4 11 -8 50.79 5.40 4 -11 8 43.50 5.20 -5 11 -8 98.09 7.10 5 -11 8 75.89 7.40 -6 11 -8 23.80 3.90 -7 11 -8 25.40 4.10 7 -11 8 33.90 4.20 -8 11 -8 3.20 3.40 8 -11 8 5.30 2.90 -9 11 -8 9.10 3.60 9 -11 8 16.30 3.60 -10 11 -8 4.10 3.60 10 -11 8 -1.90 2.90 -11 11 -8 6.40 3.40 11 -11 8 16.20 3.30 -12 11 -8 -0.40 3.10 12 -11 8 1.40 2.80 -13 11 -8 25.60 3.90 13 -11 8 21.70 3.80 -14 11 -8 2.00 2.80 14 -11 8 3.50 3.40 -15 11 -8 -0.20 3.00 15 -11 8 1.10 3.70 17 10 -8 1.10 7.60 17 10 -8 0.40 7.70 16 10 -8 2.40 6.60 16 10 -8 -5.80 7.30 15 10 -8 38.60 28.30 15 10 -8 30.60 7.90 14 10 -8 5.30 6.40 14 10 -8 -0.60 7.20 14 10 -8 -22.80 21.50 13 10 -8 0.90 5.30 13 10 -8 -0.60 7.50 13 10 -8 -25.40 20.50 12 10 -8 -2.30 5.60 12 10 -8 1.50 20.10 12 10 -8 11.80 6.00 -12 -10 8 10.70 3.50 11 10 -8 16.00 5.60 11 10 -8 3.50 8.20 11 10 -8 30.50 18.90 -11 -10 8 15.80 3.70 10 10 -8 5.30 9.00 10 10 -8 12.10 17.60 10 10 -8 14.70 5.00 -10 -10 8 4.00 3.30 9 10 -8 10.60 4.90 9 10 -8 -5.80 14.50 9 10 -8 3.00 8.00 -9 -10 8 9.60 3.50 8 10 -8 189.98 25.80 8 10 -8 172.28 11.80 -8 -10 8 168.38 10.60 7 10 -8 92.89 17.40 7 10 -8 105.29 8.30 -7 -10 8 93.09 7.30 6 10 -8 28.70 4.40 6 10 -8 13.90 8.60 6 10 -8 21.20 12.40 -6 -10 8 32.60 4.10 5 10 -8 11.30 3.60 5 10 -8 22.90 11.50 -5 -10 8 17.20 3.60 4 10 -8 114.89 7.90 4 10 -8 80.59 14.40 4 10 -8 119.89 6.70 -4 -10 8 112.79 8.00 3 10 -8 131.69 8.80 3 10 -8 112.49 17.50 3 10 -8 148.09 8.10 -3 -10 8 135.39 9.00 2 10 -8 8.30 2.80 2 10 -8 13.30 2.30 2 10 -8 5.40 8.00 -2 -10 8 36.50 26.30 -2 -10 8 -5.00 34.50 -2 -10 8 11.40 3.20 1 10 -8 5.60 7.90 -1 -10 8 -14.90 27.00 -1 -10 8 -7.30 33.90 0 10 -8 6.10 2.30 0 10 -8 4.50 7.40 0 -10 8 18.90 28.40 0 -10 8 -23.50 34.30 0 -10 8 10.20 3.30 -1 10 -8 42.60 4.30 -1 10 -8 35.70 7.90 1 -10 8 56.29 28.30 1 -10 8 27.80 35.90 1 -10 8 44.30 4.60 -2 10 -8 262.27 14.60 2 -10 8 253.57 15.10 2 -10 8 255.57 44.80 2 -10 8 321.17 51.49 -3 10 -8 17.80 3.00 3 -10 8 48.10 42.60 3 -10 8 8.50 3.70 -4 10 -8 250.97 14.00 4 -10 8 239.48 14.40 -5 10 -8 85.29 6.40 5 -10 8 64.89 6.60 -6 10 -8 355.46 20.50 6 -10 8 385.06 20.30 -7 10 -8 3.40 3.00 7 -10 8 4.90 3.00 -8 10 -8 7.70 3.20 8 -10 8 2.80 2.50 -9 10 -8 12.40 3.40 9 -10 8 12.90 3.30 -10 10 -8 32.60 4.10 10 -10 8 24.50 3.60 -11 10 -8 12.50 3.50 11 -10 8 11.20 3.40 12 -10 8 7.40 3.10 -13 10 -8 9.60 3.20 13 -10 8 13.50 3.40 -14 10 -8 18.80 3.30 14 -10 8 20.70 3.80 -15 10 -8 1.10 2.40 15 -10 8 2.80 3.50 17 9 -8 0.10 8.80 17 9 -8 27.50 10.00 16 9 -8 -6.10 8.00 16 9 -8 -3.90 6.90 15 9 -8 5.50 6.30 15 9 -8 -1.50 7.20 15 9 -8 -5.20 23.30 14 9 -8 3.30 7.80 14 9 -8 28.90 21.80 14 9 -8 18.40 6.10 13 9 -8 3.60 20.00 13 9 -8 6.80 5.40 13 9 -8 -1.20 6.50 -13 -9 8 -3.50 3.00 12 9 -8 46.30 6.70 12 9 -8 8.70 8.40 12 9 -8 18.80 18.70 -12 -9 8 27.70 4.20 11 9 -8 62.89 20.60 -11 -9 8 42.00 5.10 10 9 -8 8.90 15.50 10 9 -8 38.30 5.70 -10 -9 8 32.30 4.10 9 9 -8 45.60 5.70 9 9 -8 29.60 14.80 -9 -9 8 43.00 4.50 8 9 -8 209.78 13.10 8 9 -8 205.38 25.50 -8 -9 8 196.18 12.00 7 9 -8 15.20 3.90 7 9 -8 -0.20 7.60 7 9 -8 16.20 12.00 -7 -9 8 15.60 3.40 6 9 -8 32.60 10.70 6 9 -8 3.70 7.70 6 9 -8 13.20 3.60 -6 -9 8 16.40 3.30 -6 -9 8 39.60 49.80 5 9 -8 13.10 1.80 5 9 -8 14.70 3.40 5 9 -8 5.90 9.50 5 9 -8 3.90 8.10 -5 -9 8 29.10 26.80 -5 -9 8 15.20 3.30 4 9 -8 1.30 2.60 4 9 -8 3.20 1.50 4 9 -8 -0.60 8.10 -4 -9 8 36.00 24.50 -4 -9 8 1.60 2.80 3 9 -8 22.00 8.40 3 9 -8 4.90 1.80 3 9 -8 3.00 2.70 -3 -9 8 40.30 22.90 -3 -9 8 7.10 27.90 -3 -9 8 2.20 2.90 2 9 -8 6.00 7.10 2 9 -8 0.70 2.40 2 9 -8 1.90 1.80 -2 -9 8 8.30 21.00 -2 -9 8 0.50 2.80 -2 -9 8 -24.90 27.50 1 9 -8 -7.60 6.60 1 9 -8 4.70 1.90 -1 -9 8 -11.20 21.10 -1 -9 8 5.40 2.90 -1 -9 8 15.90 27.20 0 9 -8 183.98 10.50 0 9 -8 176.98 14.90 0 -9 8 173.28 33.50 0 -9 8 132.99 27.00 0 -9 8 202.58 11.20 -1 9 -8 122.19 7.50 1 -9 8 96.09 24.00 1 -9 8 61.99 32.00 1 -9 8 125.49 8.30 -2 9 -8 210.28 11.80 2 -9 8 185.38 31.60 2 -9 8 200.88 37.30 2 -9 8 206.58 12.30 3 -9 8 -45.30 37.70 3 -9 8 29.10 29.40 -4 9 -8 143.39 8.70 4 -9 8 132.79 9.00 -5 9 -8 131.89 8.00 5 -9 8 107.99 8.10 -6 9 -8 15.10 3.10 6 -9 8 18.00 3.00 -7 9 -8 108.99 7.50 7 -9 8 106.89 7.40 -8 9 -8 8.70 3.00 8 -9 8 10.60 2.90 -9 9 -8 19.90 3.60 9 -9 8 17.40 3.00 -10 9 -8 103.39 7.40 10 -9 8 102.09 7.30 -11 9 -8 2.70 2.90 11 -9 8 2.50 2.80 -12 9 -8 1.70 2.80 12 -9 8 6.10 2.90 -13 9 -8 0.00 2.40 13 -9 8 3.20 3.10 -14 9 -8 -0.90 2.30 14 -9 8 -0.40 3.00 15 -9 8 0.70 3.30 18 8 -8 8.40 8.90 18 8 -8 -2.60 9.30 17 8 -8 -1.50 7.40 17 8 -8 7.30 8.80 16 8 -8 9.40 7.10 16 8 -8 2.90 6.90 -16 -8 8 8.60 17.00 15 8 -8 20.00 22.70 15 8 -8 1.00 7.40 15 8 -8 6.00 6.10 13 8 -8 22.90 6.40 13 8 -8 3.60 7.10 13 8 -8 8.10 18.20 -13 -8 8 14.80 3.10 12 8 -8 3.80 18.10 12 8 -8 3.30 8.30 12 8 -8 8.90 5.70 -12 -8 8 7.00 3.20 11 8 -8 6.60 16.30 11 8 -8 29.90 5.50 11 8 -8 10.40 10.00 -11 -8 8 17.10 3.60 10 8 -8 183.68 25.40 10 8 -8 142.29 10.50 -10 -8 8 130.59 8.90 9 8 -8 7.10 4.00 9 8 -8 -1.20 6.80 9 8 -8 1.90 12.50 -9 -8 8 -1.10 2.90 8 8 -8 377.96 31.10 8 8 -8 312.57 19.10 -8 -8 8 341.17 18.50 7 8 -8 35.30 9.80 7 8 -8 52.99 5.90 7 8 -8 63.29 13.90 -7 -8 8 62.39 28.00 -7 -8 8 56.99 5.10 6 8 -8 279.77 15.60 6 8 -8 288.27 24.20 6 8 -8 253.87 20.70 -6 -8 8 277.27 15.20 -6 -8 8 238.68 31.40 5 8 -8 10.80 3.10 5 8 -8 8.20 1.40 5 8 -8 4.10 8.00 5 8 -8 8.90 8.50 -5 -8 8 7.30 2.90 -5 -8 8 2.10 21.10 4 8 -8 21.40 3.20 4 8 -8 22.00 2.60 4 8 -8 25.80 8.80 -4 -8 8 3.20 19.90 -4 -8 8 34.70 26.30 -4 -8 8 23.10 3.40 3 8 -8 99.69 13.60 3 8 -8 115.09 7.40 3 8 -8 110.49 6.60 -3 -8 8 106.09 7.50 -3 -8 8 155.78 29.40 -3 -8 8 106.39 20.60 2 8 -8 144.29 14.70 2 8 -8 162.48 9.10 -2 -8 8 156.78 23.60 -2 -8 8 199.98 29.90 -2 -8 8 164.38 9.90 1 8 -8 230.38 12.60 1 8 -8 204.48 16.70 -1 -8 8 240.68 13.20 -1 -8 8 213.38 33.00 -1 -8 8 263.57 41.20 0 8 -8 9.10 5.60 0 8 -8 14.30 2.20 0 -8 8 15.30 3.10 0 -8 8 28.70 25.80 0 -8 8 25.70 17.70 -1 8 -8 48.00 4.10 1 -8 8 43.30 5.10 1 -8 8 28.60 19.00 1 -8 8 78.49 26.90 -2 8 -8 3.80 2.00 2 -8 8 -1.40 2.90 2 -8 8 -0.80 20.30 2 -8 8 -21.90 27.00 3 -8 8 -13.60 32.30 3 -8 8 -45.40 23.30 4 -8 8 -52.89 36.80 -5 8 -8 154.68 9.10 5 -8 8 132.79 9.20 5 -8 8 156.48 8.90 -6 8 -8 13.70 2.80 6 -8 8 10.40 2.50 -7 8 -8 48.30 4.80 7 -8 8 49.20 4.70 -8 8 -8 0.60 2.70 8 -8 8 2.60 2.20 -9 8 -8 11.30 3.10 9 -8 8 6.70 2.60 -10 8 -8 60.39 5.60 10 -8 8 68.69 5.60 -11 8 -8 0.70 2.80 11 -8 8 0.60 2.40 -12 8 -8 0.40 2.60 12 -8 8 5.80 2.80 -13 8 -8 4.10 2.40 13 -8 8 -1.60 2.60 -14 8 -8 5.40 2.20 14 -8 8 4.50 3.10 15 -8 8 4.60 3.20 16 -8 8 7.20 4.30 18 7 -8 -3.60 8.50 17 7 -8 -1.60 7.60 17 7 -8 3.90 8.20 16 7 -8 -1.30 7.00 16 7 -8 1.10 6.00 -16 -7 8 12.50 17.10 15 7 -8 0.90 21.20 15 7 -8 6.10 6.90 14 7 -8 6.40 5.60 14 7 -8 13.90 19.90 14 7 -8 1.60 7.20 13 7 -8 72.89 21.00 -13 -7 8 51.69 4.90 12 7 -8 81.59 8.30 12 7 -8 73.09 21.30 -12 -7 8 59.99 5.80 11 7 -8 -4.90 13.90 11 7 -8 1.30 4.30 11 7 -8 -1.70 8.40 -11 -7 8 -1.40 2.80 10 7 -8 77.09 7.30 10 7 -8 55.39 15.00 10 7 -8 42.00 11.40 -10 -7 8 62.59 5.40 9 7 -8 -10.70 10.40 9 7 -8 -1.20 7.30 9 7 -8 1.90 3.50 -9 -7 8 2.50 2.80 8 7 -8 25.30 11.20 8 7 -8 20.20 9.10 8 7 -8 29.80 4.10 -8 -7 8 33.00 3.70 -8 -7 8 56.29 25.40 7 7 -8 198.48 12.10 7 7 -8 202.88 17.50 7 7 -8 187.48 21.50 -7 -7 8 207.48 11.50 -7 -7 8 159.78 26.40 6 7 -8 267.27 15.30 6 7 -8 269.77 23.30 6 7 -8 251.97 19.80 -6 -7 8 273.17 14.90 -6 -7 8 267.27 35.80 5 7 -8 82.69 4.80 5 7 -8 80.49 6.30 5 7 -8 73.59 11.50 5 7 -8 63.49 11.00 -5 -7 8 86.79 6.00 -5 -7 8 96.49 26.30 -5 -7 8 70.99 18.70 4 7 -8 936.71 51.29 4 7 -8 894.31 45.60 4 7 -8 821.82 46.10 -4 -7 8 862.81 56.89 -4 -7 8 892.11 46.00 -4 -7 8 819.82 62.99 3 7 -8 0.10 6.50 3 7 -8 3.10 1.60 3 7 -8 8.80 2.50 -3 -7 8 4.20 2.60 -3 -7 8 24.50 22.40 -3 -7 8 21.20 15.20 2 7 -8 920.51 51.69 2 7 -8 917.81 48.10 -2 -7 8 927.11 64.49 -2 -7 8 914.91 58.59 -2 -7 8 928.21 48.40 1 7 -8 33.90 3.30 1 7 -8 32.30 6.40 -1 -7 8 25.40 15.00 -1 -7 8 23.10 21.90 -1 -7 8 31.00 3.60 0 7 -8 3.50 1.70 0 -7 8 -19.00 14.70 0 -7 8 -22.20 21.70 0 -7 8 2.20 2.70 -1 7 -8 75.29 4.90 1 -7 8 67.39 5.70 1 -7 8 43.00 18.20 1 -7 8 25.30 22.80 -2 7 -8 9.10 2.00 2 -7 8 7.40 2.80 2 -7 8 3.50 26.00 2 -7 8 44.40 17.10 -3 7 -8 23.70 2.60 3 -7 8 21.70 3.30 3 -7 8 10.40 29.20 3 -7 8 18.00 18.60 4 -7 8 24.30 31.10 -5 7 -8 74.99 5.30 5 -7 8 75.09 5.20 5 -7 8 55.09 5.30 -6 7 -8 4.80 2.30 6 -7 8 5.90 2.30 -7 7 -8 75.29 5.70 7 -7 8 72.09 5.40 -8 7 -8 95.29 6.40 8 -7 8 79.59 6.10 -9 7 -8 5.50 2.70 9 -7 8 4.00 2.30 -10 7 -8 54.09 5.10 -11 7 -8 13.40 3.00 11 -7 8 11.80 3.10 -12 7 -8 10.60 2.70 -13 7 -8 -1.40 2.10 13 -7 8 -3.40 2.30 -14 7 -8 3.10 2.00 14 -7 8 2.10 2.90 15 -7 8 -3.70 2.90 16 -7 8 0.50 3.40 18 6 -8 -3.80 8.80 17 6 -8 5.90 6.20 17 6 -8 4.40 8.30 -17 -6 8 -19.90 23.90 16 6 -8 -1.00 5.40 16 6 -8 9.20 6.00 -16 -6 8 -33.30 15.30 -15 -6 8 32.50 13.30 14 6 -8 33.60 6.60 14 6 -8 21.50 19.00 13 6 -8 16.90 8.90 13 6 -8 11.50 16.10 -13 -6 8 20.20 3.50 12 6 -8 133.59 9.70 12 6 -8 97.19 21.60 -12 -6 8 101.09 7.50 11 6 -8 1.60 8.20 11 6 -8 7.80 13.30 11 6 -8 2.30 4.10 -11 -6 8 1.40 2.90 10 6 -8 -7.80 11.00 10 6 -8 3.50 3.80 10 6 -8 -4.70 8.40 -10 -6 8 -2.50 2.70 9 6 -8 182.28 11.60 9 6 -8 179.98 22.80 -9 -6 8 178.38 10.70 8 6 -8 5.00 7.80 8 6 -8 0.90 3.00 8 6 -8 3.70 10.20 -8 -6 8 0.20 2.50 -8 -6 8 -3.60 20.10 7 6 -8 609.44 38.70 7 6 -8 653.23 41.70 7 6 -8 611.94 34.20 -7 -6 8 662.53 33.80 -7 -6 8 667.43 46.80 6 6 -8 129.89 13.20 6 6 -8 129.39 8.60 6 6 -8 161.08 16.70 -6 -6 8 129.69 8.10 -6 -6 8 134.79 27.50 -6 -6 8 115.39 19.60 5 6 -8 64.09 10.10 5 6 -8 54.69 10.50 5 6 -8 70.59 4.20 5 6 -8 67.89 5.80 -5 -6 8 60.99 16.70 -5 -6 8 71.99 5.40 -5 -6 8 90.89 24.30 4 6 -8 4.40 1.40 4 6 -8 1.30 2.60 4 6 -8 1.90 6.60 -4 -6 8 3.40 2.50 -4 -6 8 -4.30 12.60 -4 -6 8 -2.00 19.00 3 6 -8 26.50 3.30 3 6 -8 24.00 7.10 3 6 -8 25.00 2.80 -3 -6 8 29.80 3.30 -3 -6 8 36.70 18.60 -3 -6 8 27.10 13.10 2 6 -8 81.09 10.90 2 6 -8 89.19 5.60 -2 -6 8 84.69 15.70 -2 -6 8 103.89 6.60 -2 -6 8 79.79 20.60 1 6 -8 1.20 1.70 -1 -6 8 3.00 2.60 -1 -6 8 6.20 12.10 -1 -6 8 -15.10 18.50 0 6 -8 159.78 9.30 0 -6 8 159.08 9.90 0 -6 8 223.28 33.80 0 -6 8 186.48 24.70 -1 6 -8 125.79 7.60 1 -6 8 109.39 24.70 1 -6 8 169.08 25.00 1 -6 8 133.39 8.30 -2 6 -8 30.10 3.20 2 -6 8 44.70 24.80 2 -6 8 5.20 15.30 2 -6 8 27.00 3.30 -3 6 -8 197.68 10.80 3 -6 8 188.68 11.10 3 -6 8 186.18 30.80 3 -6 8 180.68 30.40 -4 6 -8 51.79 4.30 4 -6 8 54.09 3.70 4 -6 8 25.90 21.90 4 -6 8 59.39 4.10 4 -6 8 44.50 4.50 4 -6 8 15.90 29.80 -5 6 -8 83.89 5.50 5 -6 8 73.79 4.90 5 -6 8 81.69 5.40 -6 6 -8 1.60 2.10 6 -6 8 3.00 2.00 -7 6 -8 19.50 2.80 7 -6 8 14.00 2.20 -8 6 -8 1.40 2.40 8 -6 8 2.00 2.10 -9 6 -8 -0.70 2.40 9 -6 8 0.80 2.30 -10 6 -8 -0.40 2.40 10 -6 8 0.80 2.50 -11 6 -8 -0.40 2.30 11 -6 8 -2.50 2.30 -12 6 -8 26.10 3.10 12 -6 8 14.30 2.90 -13 6 -8 1.10 2.00 13 -6 8 -0.20 2.70 14 -6 8 10.80 2.90 15 -6 8 8.30 3.60 16 -6 8 2.20 3.70 19 5 -8 0.80 6.90 18 5 -8 -4.80 8.60 17 5 -8 20.90 6.50 17 5 -8 12.20 9.00 -17 -5 8 -32.80 18.20 16 5 -8 11.50 5.60 -16 -5 8 5.00 14.90 15 5 -8 37.40 6.30 15 5 -8 7.80 8.60 -15 -5 8 20.20 13.30 14 5 -8 9.30 7.90 14 5 -8 21.40 19.30 13 5 -8 1.50 7.80 13 5 -8 2.40 4.60 13 5 -8 5.10 15.10 -13 -5 8 3.10 2.80 12 5 -8 2.40 8.60 12 5 -8 15.20 14.40 -12 -5 8 6.10 3.10 11 5 -8 13.00 12.30 11 5 -8 6.70 3.90 11 5 -8 6.60 8.70 -11 -5 8 6.50 2.90 10 5 -8 3.40 8.00 10 5 -8 -7.60 10.10 10 5 -8 3.10 3.60 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1 -5 8 239.88 35.10 1 -5 8 180.38 23.90 -2 5 -8 231.18 12.50 2 -5 8 205.38 13.50 2 -5 8 287.67 38.00 2 -5 8 213.58 26.30 2 -5 8 248.08 13.00 -3 5 -8 20.80 2.20 3 -5 8 20.40 2.20 3 -5 8 15.60 2.80 3 -5 8 -19.40 24.10 3 -5 8 25.60 14.70 4 -5 8 1.80 1.70 4 -5 8 0.10 2.00 4 -5 8 4.70 1.70 4 -5 8 -2.60 16.00 -5 5 -8 175.18 9.90 5 -5 8 171.88 9.80 5 -5 8 175.78 9.80 -6 5 -8 25.10 2.70 6 -5 8 22.60 2.40 6 -5 8 17.50 2.30 6 -5 8 47.00 38.60 -7 5 -8 81.29 5.60 7 -5 8 81.49 5.50 -8 5 -8 19.30 2.70 8 -5 8 11.20 2.20 -9 5 -8 4.40 2.30 9 -5 8 2.90 2.30 -10 5 -8 -1.50 2.20 10 -5 8 2.00 2.40 -11 5 -8 6.20 2.40 11 -5 8 13.70 3.00 -12 5 -8 17.60 2.70 12 -5 8 26.50 3.40 -13 5 -8 6.90 2.00 13 -5 8 1.80 2.40 14 -5 8 13.60 3.00 15 -5 8 30.50 4.50 16 -5 8 10.90 4.00 19 4 -8 -0.80 8.30 18 4 -8 4.40 8.10 17 4 -8 0.40 5.80 -17 -4 8 5.70 16.70 16 4 -8 -2.70 6.80 16 4 -8 8.40 5.20 -16 -4 8 20.10 15.00 15 4 -8 1.10 7.20 15 4 -8 13.50 5.60 -15 -4 8 3.90 12.60 14 4 -8 3.10 4.90 14 4 -8 -1.70 7.20 -14 -4 8 5.20 13.00 -14 -4 8 2.60 2.80 13 4 -8 3.00 7.70 13 4 -8 17.00 14.90 13 4 -8 -0.90 4.20 -13 -4 8 -0.10 2.80 12 4 -8 23.20 13.80 12 4 -8 45.20 5.70 12 4 -8 13.80 9.20 -12 -4 8 32.60 4.00 11 4 -8 -4.90 7.80 11 4 -8 0.30 3.60 11 4 -8 7.70 11.70 -11 -4 8 1.00 2.70 10 4 -8 81.89 11.90 10 4 -8 113.29 8.20 10 4 -8 111.69 17.70 -10 -4 8 113.39 7.20 9 4 -8 -1.10 6.60 9 4 -8 8.80 8.80 9 4 -8 0.40 2.80 -9 -4 8 1.90 2.50 -9 -4 8 33.00 18.50 8 4 -8 40.30 8.80 8 4 -8 37.70 10.30 8 4 -8 30.30 4.00 -8 -4 8 16.30 16.10 -8 -4 8 32.90 3.40 7 4 -8 12.10 2.80 7 4 -8 12.60 7.70 7 4 -8 5.90 7.90 -7 -4 8 23.20 23.50 -7 -4 8 10.50 2.60 -7 -4 8 29.10 13.90 6 4 -8 9.90 2.90 6 4 -8 10.90 1.80 6 4 -8 12.70 7.30 6 4 -8 6.90 7.30 -6 -4 8 17.80 12.40 -6 -4 8 9.50 2.50 5 4 -8 213.18 18.80 5 4 -8 249.28 17.10 5 4 -8 220.68 13.40 -5 -4 8 244.88 23.10 -5 -4 8 233.68 13.00 4 4 -8 34.00 2.70 4 4 -8 27.60 7.60 -4 -4 8 33.80 4.00 -4 -4 8 28.90 11.00 3 4 -8 0.30 1.20 -3 -4 8 -1.10 2.20 -3 -4 8 -8.10 9.40 2 4 -8 120.79 6.80 -2 -4 8 119.49 7.60 -2 -4 8 112.09 15.10 1 4 -8 236.48 13.00 -1 -4 8 254.27 23.40 -1 -4 8 242.18 13.50 0 4 -8 1632.44 87.79 0 -4 8 1681.43 94.49 0 -4 8 1761.12 88.09 -1 4 -8 83.49 5.30 1 -4 8 79.99 22.30 1 -4 8 80.49 6.00 1 -4 8 90.19 7.90 1 -4 8 86.79 14.30 -2 4 -8 117.19 6.80 2 -4 8 126.59 17.60 2 -4 8 122.39 24.30 2 -4 8 125.09 7.50 2 -4 8 117.69 6.80 2 -4 8 105.09 7.70 -3 4 -8 29.60 3.00 3 -4 8 32.00 3.10 3 -4 8 23.30 13.90 3 -4 8 4.50 23.50 3 -4 8 32.70 2.90 -4 4 -8 356.66 18.20 4 -4 8 341.67 33.40 4 -4 8 363.96 18.20 4 -4 8 300.87 18.30 4 -4 8 341.17 18.40 4 -4 8 349.77 47.40 -5 4 -8 233.48 12.40 5 -4 8 217.28 12.60 5 -4 8 227.68 12.40 -6 4 -8 164.88 9.10 6 -4 8 155.18 9.10 6 -4 8 158.08 9.30 -7 4 -8 0.90 1.90 7 -4 8 2.50 1.80 7 -4 8 -2.00 1.90 -8 4 -8 91.39 5.90 8 -4 8 89.29 6.10 -9 4 -8 105.29 6.60 9 -4 8 102.49 6.80 -10 4 -8 9.40 2.30 10 -4 8 0.00 2.70 10 -4 8 7.40 2.50 -11 4 -8 24.80 2.90 11 -4 8 21.90 3.20 -12 4 -8 10.40 2.10 12 -4 8 10.80 2.90 13 -4 8 0.60 2.60 14 -4 8 27.30 3.70 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72.79 7.10 2 13 -9 -22.70 14.30 2 13 -9 -0.50 2.40 -2 -13 9 2.40 4.10 1 13 -9 30.20 3.60 1 13 -9 10.90 14.60 -1 -13 9 28.90 5.10 0 13 -9 138.69 20.80 0 13 -9 180.28 10.50 0 -13 9 172.98 11.90 -1 13 -9 185.68 11.10 1 -13 9 172.68 12.30 -2 13 -9 35.50 4.20 2 -13 9 33.90 5.40 -3 13 -9 15.90 3.60 3 -13 9 11.30 4.80 -4 13 -9 41.00 4.60 4 -13 9 35.10 5.40 -5 13 -9 0.20 3.40 5 -13 9 5.40 4.20 -7 13 -9 23.30 4.40 7 -13 9 30.50 4.30 -8 13 -9 14.20 4.10 8 -13 9 10.20 3.50 -9 13 -9 3.30 3.90 9 -13 9 9.00 3.70 -10 13 -9 81.89 7.20 10 -13 9 79.49 6.90 -11 13 -9 -0.50 3.40 11 -13 9 -0.20 3.40 -12 13 -9 9.10 3.70 12 -13 9 4.10 3.30 -13 13 -9 -2.70 3.60 13 -13 9 2.50 3.90 -14 13 -9 3.70 3.70 14 -13 9 2.60 3.90 16 12 -9 -7.50 12.80 16 12 -9 -3.00 8.30 15 12 -9 20.00 9.90 14 12 -9 -7.60 7.00 14 12 -9 7.90 6.60 13 12 -9 7.30 6.90 13 12 -9 -3.60 23.40 13 12 -9 -2.30 6.10 12 12 -9 1.80 5.60 12 12 -9 2.00 7.40 12 12 -9 51.49 24.30 11 12 -9 7.20 20.40 11 12 -9 12.60 9.20 11 12 -9 13.90 6.10 -11 -12 9 8.40 3.60 10 12 -9 5.20 20.30 10 12 -9 -6.50 5.10 10 12 -9 -1.40 6.60 -10 -12 9 9.30 3.70 9 12 -9 29.10 5.60 9 12 -9 25.30 19.30 -9 -12 9 25.50 4.30 8 12 -9 53.79 6.30 8 12 -9 51.99 18.70 -8 -12 9 46.40 5.40 7 12 -9 19.40 8.40 7 12 -9 15.40 16.60 6 12 -9 -1.10 4.80 6 12 -9 -0.40 3.80 6 12 -9 6.10 13.90 -6 -12 9 1.60 3.80 5 12 -9 37.80 15.70 5 12 -9 45.90 5.20 -5 -12 9 34.60 4.90 4 12 -9 19.00 4.00 -4 -12 9 14.30 4.30 3 12 -9 13.00 3.60 3 12 -9 2.60 11.70 3 12 -9 11.40 2.30 -3 -12 9 13.70 4.20 2 12 -9 1.40 11.60 2 12 -9 0.70 2.30 -2 -12 9 0.80 3.80 1 12 -9 121.49 7.40 1 12 -9 82.59 14.80 -1 -12 9 110.69 8.40 0 12 -9 32.70 12.20 0 12 -9 43.70 4.80 0 -12 9 48.00 5.40 -1 12 -9 -1.10 2.70 1 -12 9 -2.60 4.00 -2 12 -9 132.19 8.30 2 -12 9 114.89 9.40 -3 12 -9 136.69 8.90 3 -12 9 126.39 9.60 -4 12 -9 29.00 4.00 4 -12 9 18.00 4.60 -5 12 -9 47.80 5.40 5 -12 9 37.50 5.30 -6 12 -9 5.70 3.40 6 -12 9 4.50 2.60 6 -12 9 2.00 3.10 -7 12 -9 13.90 3.80 7 -12 9 9.90 3.30 -8 12 -9 46.00 5.30 8 -12 9 54.99 5.40 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5 11 -9 12.60 4.00 -5 -11 9 13.50 4.00 4 11 -9 288.77 26.00 4 11 -9 257.87 15.60 4 11 -9 279.17 14.60 -4 -11 9 260.97 15.70 3 11 -9 12.80 3.50 3 11 -9 5.70 10.30 3 11 -9 15.70 2.40 -3 -11 9 11.20 3.90 2 11 -9 158.08 19.00 2 11 -9 164.58 9.80 -2 -11 9 176.48 10.90 1 11 -9 140.09 8.30 1 11 -9 115.69 16.90 -1 -11 9 81.79 42.40 -1 -11 9 137.09 9.50 0 11 -9 567.44 29.70 0 11 -9 550.24 34.00 0 -11 9 559.64 30.30 0 -11 9 509.65 74.49 -1 11 -9 1.50 2.60 1 -11 9 -49.90 42.10 1 -11 9 35.20 53.59 1 -11 9 7.30 4.00 -2 11 -9 52.79 5.20 2 -11 9 57.39 6.50 -3 11 -9 119.69 7.70 3 -11 9 98.09 8.40 -4 11 -9 19.60 3.50 4 -11 9 19.50 4.40 -5 11 -9 170.68 10.20 5 -11 9 149.29 10.60 -6 11 -9 3.00 3.10 6 -11 9 -4.30 2.50 6 -11 9 2.00 3.00 -7 11 -9 20.50 3.80 7 -11 9 19.40 3.30 -8 11 -9 2.70 3.30 8 -11 9 6.40 3.50 -9 11 -9 -0.90 3.10 9 -11 9 0.60 2.70 -10 11 -9 16.50 3.80 10 -11 9 26.50 4.00 -11 11 -9 7.00 3.40 11 -11 9 3.80 3.10 -12 11 -9 -2.10 3.00 12 -11 9 -1.10 3.10 -13 11 -9 3.30 2.80 13 -11 9 0.70 3.20 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45.70 4.00 -3 -10 9 15.20 32.80 -3 -10 9 45.40 5.60 2 10 -9 35.20 9.70 2 10 -9 55.09 4.30 -2 -10 9 50.89 32.30 -2 -10 9 38.30 41.70 -2 -10 9 53.49 5.70 1 10 -9 49.90 10.30 1 10 -9 68.89 5.10 -1 -10 9 70.79 6.30 -1 -10 9 55.69 34.50 0 10 -9 11.00 2.50 0 10 -9 13.80 7.90 0 -10 9 13.50 3.70 0 -10 9 33.10 34.10 0 -10 9 14.90 40.80 -1 10 -9 2.40 2.30 1 -10 9 0.80 3.40 1 -10 9 -28.40 36.30 1 -10 9 36.80 44.10 -2 10 -9 334.67 18.00 2 -10 9 317.07 18.50 2 -10 9 317.67 56.99 -3 10 -9 19.20 3.20 3 -10 9 15.80 4.10 -4 10 -9 73.29 5.90 4 -10 9 62.09 6.60 -5 10 -9 1.80 2.80 5 -10 9 7.30 3.50 -6 10 -9 -0.10 2.90 6 -10 9 3.40 3.40 6 -10 9 0.80 2.80 -7 10 -9 23.30 3.70 7 -10 9 17.70 3.20 -8 10 -9 2.10 3.10 8 -10 9 4.80 3.10 -9 10 -9 -2.10 3.00 9 -10 9 3.00 2.80 -10 10 -9 39.00 4.60 10 -10 9 47.20 4.70 -11 10 -9 0.30 2.90 11 -10 9 0.10 2.80 -12 10 -9 4.90 3.10 12 -10 9 12.30 3.40 -13 10 -9 -1.10 2.60 13 -10 9 -1.00 2.90 -14 10 -9 1.10 2.50 14 -10 9 1.90 4.10 15 -10 9 2.20 3.80 17 9 -9 4.90 9.20 17 9 -9 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6.00 -3 -8 9 62.29 32.10 2 8 -9 737.33 43.50 2 8 -9 773.12 39.50 -2 -8 9 660.13 65.39 -2 -8 9 767.82 39.90 -2 -8 9 776.82 56.39 1 8 -9 29.80 7.40 1 8 -9 43.20 3.70 -1 -8 9 28.40 30.20 -1 -8 9 44.20 4.40 -1 -8 9 35.00 21.80 0 8 -9 96.49 6.20 0 -8 9 89.79 32.20 0 -8 9 101.49 7.20 0 -8 9 88.99 23.00 -1 8 -9 198.18 11.10 1 -8 9 165.68 36.50 1 -8 9 196.88 11.70 2 -8 9 -1.10 23.30 2 -8 9 -60.09 36.60 -3 8 -9 309.77 16.30 3 -8 9 280.27 16.60 -4 8 -9 11.60 2.60 4 -8 9 14.20 2.50 4 -8 9 3.70 3.10 4 -8 9 60.79 55.39 -5 8 -9 323.67 18.30 5 -8 9 344.57 18.30 -6 8 -9 9.20 2.80 6 -8 9 13.00 2.80 7 -8 9 20.10 2.80 -8 8 -9 -2.40 2.70 8 -8 9 -1.20 2.50 -9 8 -9 1.10 2.70 9 -8 9 -0.70 2.50 -10 8 -9 110.79 7.60 10 -8 9 110.29 7.70 -11 8 -9 63.19 5.20 11 -8 9 52.09 5.50 -12 8 -9 16.20 3.10 12 -8 9 26.00 3.70 -13 8 -9 27.30 3.20 13 -8 9 21.10 3.40 -14 8 -9 -1.40 2.00 14 -8 9 3.50 3.60 15 -8 9 0.60 3.50 18 7 -9 4.40 9.10 17 7 -9 15.40 9.10 17 7 -9 1.00 6.30 16 7 -9 -1.30 8.00 16 7 -9 9.50 6.50 -16 -7 9 -2.70 14.60 15 7 -9 12.60 6.00 14 7 -9 9.80 6.20 14 7 -9 18.60 19.10 14 7 -9 4.50 7.50 13 7 -9 -11.10 16.50 13 7 -9 -0.10 5.50 13 7 -9 -1.10 7.50 -13 -7 9 2.10 3.30 12 7 -9 4.70 5.20 12 7 -9 6.00 9.50 12 7 -9 5.60 15.10 -12 -7 9 9.00 3.40 11 7 -9 40.40 5.90 11 7 -9 35.30 15.00 11 7 -9 19.20 10.00 -11 -7 9 27.20 4.10 10 7 -9 1.40 7.60 10 7 -9 -9.40 11.70 10 7 -9 8.10 4.40 -10 -7 9 4.90 3.20 9 7 -9 513.05 39.00 9 7 -9 477.25 27.90 -9 -7 9 530.45 27.40 8 7 -9 -3.20 8.60 8 7 -9 0.00 3.50 8 7 -9 6.70 10.20 -8 -7 9 1.10 3.00 7 7 -9 348.47 26.50 7 7 -9 360.76 29.60 7 7 -9 379.46 21.30 -7 -7 9 391.66 20.80 -7 -7 9 479.95 46.20 6 7 -9 40.60 4.40 6 7 -9 37.30 10.10 6 7 -9 39.70 10.70 -6 -7 9 43.70 4.80 -6 -7 9 10.00 21.60 5 7 -9 240.58 20.90 5 7 -9 246.78 12.80 5 7 -9 224.08 18.20 5 7 -9 235.98 13.80 -5 -7 9 239.78 13.60 -5 -7 9 249.08 37.50 -5 -7 9 218.48 38.10 4 7 -9 -0.40 1.40 4 7 -9 -13.60 6.60 4 7 -9 -2.00 2.70 -4 -7 9 20.30 17.90 -4 -7 9 2.00 2.70 -4 -7 9 -20.50 28.00 3 7 -9 17.80 7.70 3 7 -9 13.70 1.90 -3 -7 9 0.60 17.70 -3 -7 9 8.80 2.90 -3 -7 9 43.10 27.20 2 7 -9 10.50 6.40 -2 -7 9 -22.20 25.50 -2 -7 9 12.10 17.30 -2 -7 9 21.10 3.30 1 7 -9 425.96 22.80 -1 -7 9 427.86 23.30 -1 -7 9 403.76 50.59 -1 -7 9 453.85 39.50 0 7 -9 303.27 16.20 0 -7 9 305.57 16.80 0 -7 9 286.97 47.30 0 -7 9 279.77 35.10 -1 7 -9 64.89 4.50 1 -7 9 6.90 30.40 1 -7 9 43.00 20.30 1 -7 9 59.19 5.50 2 -7 9 81.59 31.60 2 -7 9 15.50 20.30 -3 7 -9 151.78 8.50 3 -7 9 134.89 9.00 3 -7 9 132.69 28.30 3 -7 9 105.69 37.60 -4 7 -9 123.79 7.30 4 -7 9 42.20 43.70 4 -7 9 125.79 7.10 4 -7 9 109.29 6.60 4 -7 9 99.59 7.60 -5 7 -9 174.88 10.40 5 -7 9 181.28 10.40 -6 7 -9 144.69 9.00 6 -7 9 149.39 8.90 -7 7 -9 0.90 2.50 7 -7 9 2.90 2.30 -8 7 -9 123.09 7.90 8 -7 9 117.49 7.70 -9 7 -9 47.30 4.80 9 -7 9 55.19 4.90 -10 7 -9 36.40 4.50 10 -7 9 37.60 4.00 -11 7 -9 48.90 4.80 11 -7 9 58.79 5.20 -12 7 -9 -1.40 2.30 12 -7 9 0.50 2.60 -13 7 -9 5.40 2.20 13 -7 9 0.30 2.60 14 -7 9 0.00 3.20 15 -7 9 1.70 3.90 18 6 -9 -2.00 9.40 -17 -6 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6.00 -7 5 -9 4.90 2.20 7 -5 9 7.80 2.20 -8 5 -9 0.30 2.10 8 -5 9 0.80 2.20 8 -5 9 4.30 1.70 -9 5 -9 33.70 3.50 9 -5 9 35.40 3.70 -10 5 -9 13.60 2.60 10 -5 9 9.10 2.90 -11 5 -9 64.89 4.80 11 -5 9 62.59 5.20 -12 5 -9 4.10 2.10 12 -5 9 -0.60 2.50 -13 5 -9 4.10 2.00 13 -5 9 1.00 2.50 14 -5 9 1.60 3.00 15 -5 9 4.00 3.70 19 4 -9 -0.60 10.40 18 4 -9 -0.50 6.40 17 4 -9 0.60 6.40 -17 -4 9 1.10 15.30 16 4 -9 0.20 7.30 -16 -4 9 1.80 14.90 15 4 -9 8.50 5.40 15 4 -9 -1.00 7.20 -15 -4 9 6.20 11.30 14 4 -9 5.80 4.90 14 4 -9 1.90 8.00 -14 -4 9 -2.10 11.50 -14 -4 9 3.70 3.10 13 4 -9 -0.60 4.50 13 4 -9 -3.30 8.30 -13 -4 9 6.70 3.20 12 4 -9 -1.50 7.80 12 4 -9 -3.10 4.40 -12 -4 9 -3.70 3.10 11 4 -9 0.20 8.40 11 4 -9 6.20 11.50 11 4 -9 -0.80 3.90 -11 -4 9 3.10 3.00 10 4 -9 276.87 26.10 10 4 -9 249.97 15.40 -10 -4 9 264.77 14.80 9 4 -9 4.40 7.80 9 4 -9 0.00 3.30 9 4 -9 1.90 8.70 -9 -4 9 2.00 2.70 -9 -4 9 12.10 21.00 8 4 -9 45.40 5.40 8 4 -9 35.30 10.10 8 4 -9 43.00 9.20 -8 -4 9 44.60 4.70 -8 -4 9 78.99 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15 -10 5.70 6.70 -4 -15 10 22.80 5.30 3 15 -10 64.99 25.40 -3 -15 10 70.99 7.90 2 15 -10 70.29 5.20 -2 -15 10 73.79 8.10 1 15 -10 73.99 6.10 -1 -15 10 94.09 8.50 0 15 -10 123.79 8.30 0 -15 10 110.39 10.10 -1 15 -10 23.00 3.80 1 -15 10 13.60 5.30 -2 15 -10 2.90 3.20 2 -15 10 7.60 5.30 -3 15 -10 2.90 3.40 3 -15 10 3.70 4.40 -4 15 -10 2.10 3.50 4 -15 10 3.40 4.50 -5 15 -10 -0.20 3.60 5 -15 10 3.90 4.20 -6 15 -10 5.30 3.70 6 -15 10 7.00 3.50 6 -15 10 1.70 3.90 -7 15 -10 0.00 3.80 7 -15 10 3.70 3.20 -8 15 -10 0.20 3.60 8 -15 10 1.70 3.60 -9 15 -10 0.60 3.60 9 -15 10 4.00 3.50 -10 15 -10 9.30 4.30 10 -15 10 6.00 3.90 -11 15 -10 0.20 4.30 11 -15 10 -0.10 3.70 -12 15 -10 6.70 4.90 12 -15 10 2.30 4.20 14 14 -10 -4.50 7.30 14 14 -10 4.20 6.60 13 14 -10 5.10 6.90 13 14 -10 1.60 6.10 12 14 -10 1.00 6.60 12 14 -10 -4.20 5.90 12 14 -10 -9.80 30.50 -12 -14 10 1.20 3.50 11 14 -10 6.50 5.60 11 14 -10 -0.70 6.80 11 14 -10 20.50 26.80 -11 -14 10 3.70 3.50 10 14 -10 77.59 8.50 10 14 -10 53.79 27.60 -10 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-10 28.00 4.20 8 -12 10 26.80 6.10 -9 12 -10 21.80 4.20 9 -12 10 33.80 4.60 -10 12 -10 35.00 4.70 10 -12 10 38.70 4.70 -11 12 -10 53.69 5.70 11 -12 10 51.39 5.50 -12 12 -10 0.40 3.20 12 -12 10 -0.40 3.40 -13 12 -10 5.00 3.50 13 -12 10 -0.60 4.30 -14 12 -10 4.20 3.50 14 -12 10 8.30 3.70 16 11 -10 -0.10 8.80 16 11 -10 16.00 8.80 15 11 -10 3.10 8.50 15 11 -10 -1.70 7.20 14 11 -10 5.40 6.80 14 11 -10 -19.90 23.40 14 11 -10 -0.10 6.90 13 11 -10 2.50 5.80 13 11 -10 58.39 23.70 12 11 -10 -0.10 7.00 12 11 -10 5.70 5.70 12 11 -10 28.50 20.50 -12 -11 10 5.30 3.60 11 11 -10 14.50 20.40 11 11 -10 2.10 8.20 11 11 -10 0.50 5.50 -11 -11 10 -0.20 3.40 10 11 -10 67.09 7.30 10 11 -10 23.20 18.80 -10 -11 10 48.00 5.50 9 11 -10 -7.30 4.40 9 11 -10 3.20 7.20 9 11 -10 -8.80 16.30 -9 -11 10 5.10 3.80 8 11 -10 15.60 5.20 8 11 -10 0.30 14.90 8 11 -10 -0.80 5.80 7 11 -10 39.60 5.60 -7 -11 10 53.39 6.00 6 11 -10 95.29 19.40 6 11 -10 102.29 8.40 -6 -11 10 90.99 7.70 5 11 -10 6.60 8.00 5 11 -10 4.90 3.90 5 11 -10 7.80 12.50 -5 -11 10 3.50 3.80 4 11 -10 12.50 2.10 4 11 -10 38.60 12.80 4 11 -10 10.40 3.80 -4 -11 10 12.90 4.00 3 11 -10 -5.10 10.70 3 11 -10 -0.50 2.10 -3 -11 10 -1.60 3.60 2 11 -10 78.59 13.70 2 11 -10 94.69 6.20 -2 -11 10 92.09 7.50 1 11 -10 64.69 5.30 1 11 -10 60.49 12.10 -1 -11 10 68.99 7.00 0 11 -10 10.10 2.70 0 -11 10 54.99 68.09 0 -11 10 14.50 4.20 -1 11 -10 0.20 2.50 1 -11 10 -2.70 3.80 1 -11 10 -22.20 80.89 -2 11 -10 -4.10 2.60 2 -11 10 1.40 4.00 -3 11 -10 100.39 7.10 3 -11 10 92.79 8.20 -4 11 -10 4.10 3.20 4 -11 10 1.20 4.20 -5 11 -10 78.79 6.70 5 -11 10 79.89 6.40 -6 11 -10 104.39 7.60 6 -11 10 92.69 7.40 -7 11 -10 4.20 3.20 7 -11 10 2.30 3.10 -8 11 -10 11.50 3.50 8 -11 10 8.60 3.00 -9 11 -10 58.59 5.90 9 -11 10 65.19 5.90 -10 11 -10 12.00 3.60 10 -11 10 19.40 3.70 -11 11 -10 117.69 8.00 11 -11 10 109.29 8.10 -12 11 -10 0.40 2.90 12 -11 10 -0.30 3.30 -13 11 -10 -4.60 2.70 13 -11 10 2.30 3.60 -14 11 -10 4.40 2.90 14 -11 10 11.20 4.20 17 10 -10 -0.70 9.10 16 10 -10 1.10 8.20 16 10 -10 2.60 9.30 15 10 -10 -26.10 26.30 15 10 -10 -0.30 6.70 15 10 -10 -2.50 6.80 14 10 -10 6.80 8.10 14 10 -10 3.30 5.80 14 10 -10 15.30 22.70 13 10 -10 -5.00 5.30 13 10 -10 -25.50 19.70 13 10 -10 -0.30 6.80 -13 -10 10 -3.00 2.90 12 10 -10 25.70 21.10 12 10 -10 36.40 6.70 -12 -10 10 20.40 4.20 11 10 -10 -2.30 7.40 11 10 -10 -3.70 17.30 11 10 -10 8.70 5.70 -11 -10 10 3.40 3.70 10 10 -10 19.60 17.00 10 10 -10 7.40 9.10 10 10 -10 27.80 6.00 -10 -10 10 18.20 4.20 9 10 -10 142.09 10.80 -9 -10 10 155.98 10.00 8 10 -10 16.90 15.00 8 10 -10 44.30 5.70 -8 -10 10 37.10 4.70 7 10 -10 0.70 7.50 7 10 -10 -2.60 12.20 7 10 -10 10.40 4.20 -7 -10 10 6.30 3.70 6 10 -10 105.19 14.20 6 10 -10 142.09 9.60 6 10 -10 123.89 18.50 -6 -10 10 139.39 9.10 5 10 -10 59.09 13.80 5 10 -10 37.00 9.40 5 10 -10 32.10 2.80 4 10 -10 108.79 15.90 4 10 -10 119.99 7.10 -4 -10 10 118.09 8.70 3 10 -10 1.50 2.00 3 10 -10 -15.60 9.30 -3 -10 10 -2.90 3.40 2 10 -10 113.89 6.90 2 10 -10 88.19 13.20 -2 -10 10 45.10 39.30 -2 -10 10 114.79 8.20 1 10 -10 192.98 11.10 -1 -10 10 138.39 42.00 -1 -10 10 194.98 12.10 -1 -10 10 262.67 52.49 0 10 -10 1.20 2.30 0 -10 10 68.09 52.19 0 -10 10 0.60 3.70 0 -10 10 4.50 38.30 -1 10 -10 40.10 4.40 1 -10 10 42.80 5.10 1 -10 10 115.49 42.90 1 -10 10 9.30 55.89 -2 10 -10 155.78 9.00 2 -10 10 128.99 9.90 -3 10 -10 234.48 13.20 3 -10 10 220.98 14.00 -4 10 -10 360.36 19.40 4 -10 10 342.37 20.00 -5 10 -10 16.60 3.30 5 -10 10 12.10 2.90 -6 10 -10 83.89 6.70 6 -10 10 92.89 6.80 -7 10 -10 21.70 3.80 7 -10 10 29.90 3.60 -8 10 -10 0.70 3.10 8 -10 10 -1.00 2.60 -9 10 -10 30.40 4.10 9 -10 10 36.10 4.30 -10 10 -10 -1.70 2.80 10 -10 10 1.20 3.00 -11 10 -10 30.50 3.90 11 -10 10 24.20 3.70 -12 10 -10 11.30 3.10 12 -10 10 12.10 3.60 -13 10 -10 2.70 2.60 13 -10 10 2.90 3.40 -14 10 -10 5.50 2.60 14 -10 10 6.90 4.30 17 9 -10 0.10 9.50 16 9 -10 -2.00 7.50 16 9 -10 12.90 8.60 -16 -9 10 6.70 16.30 15 9 -10 7.90 8.20 15 9 -10 3.30 6.20 14 9 -10 -3.00 20.30 14 9 -10 -0.50 5.50 14 9 -10 -1.50 5.40 -14 -9 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833.32 43.40 -1 -9 10 828.82 43.90 -1 -9 10 824.52 82.09 -1 -9 10 805.82 70.49 0 9 -10 29.20 3.10 0 -9 10 45.20 31.10 0 -9 10 25.10 4.10 0 -9 10 68.59 44.70 -1 9 -10 135.99 8.40 1 -9 10 146.39 34.50 1 -9 10 136.89 9.30 1 -9 10 102.89 51.39 -2 9 -10 369.06 19.30 2 -9 10 335.37 19.80 -3 9 -10 -0.40 2.40 3 -9 10 -3.60 3.60 -4 9 -10 302.07 15.90 4 -9 10 292.67 15.80 4 -9 10 249.68 16.20 -5 9 -10 28.00 3.60 5 -9 10 30.40 3.70 -6 9 -10 1.00 2.70 6 -9 10 1.60 2.60 -7 9 -10 60.99 5.80 7 -9 10 72.79 5.70 -8 9 -10 4.50 3.00 8 -9 10 6.40 3.00 -9 9 -10 27.30 3.70 9 -9 10 27.30 3.90 -10 9 -10 5.00 2.90 10 -9 10 0.50 2.70 -11 9 -10 9.20 3.00 11 -9 10 8.20 3.20 -12 9 -10 -2.10 2.40 12 -9 10 0.80 3.10 -13 9 -10 1.30 2.40 13 -9 10 2.10 3.10 -14 9 -10 -1.60 2.30 14 -9 10 -0.50 4.10 18 8 -10 3.60 9.70 17 8 -10 -2.00 9.80 16 8 -10 15.40 7.10 -16 -8 10 9.50 17.50 15 8 -10 0.80 6.20 15 8 -10 2.30 6.00 14 8 -10 31.50 6.80 14 8 -10 34.20 21.00 13 8 -10 -0.50 5.50 13 8 -10 1.00 7.80 13 8 -10 9.30 17.20 -13 -8 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15.10 12 7 -10 -0.90 9.30 -12 -7 10 6.10 3.60 11 7 -10 19.50 10.70 11 7 -10 41.80 6.20 11 7 -10 34.50 15.40 -11 -7 10 35.60 4.50 10 7 -10 104.69 8.90 10 7 -10 69.99 16.80 -10 -7 10 107.89 7.70 9 7 -10 85.69 14.00 9 7 -10 133.99 21.10 9 7 -10 117.29 9.10 -9 -7 10 105.19 7.90 8 7 -10 402.06 23.00 8 7 -10 395.56 32.20 -8 -7 10 420.76 22.40 7 7 -10 53.79 12.40 7 7 -10 46.50 10.30 7 7 -10 43.70 5.00 -7 -7 10 52.29 5.50 6 7 -10 55.69 6.30 6 7 -10 63.69 10.60 6 7 -10 57.49 11.90 -6 -7 10 56.19 5.60 -6 -7 10 68.99 25.90 5 7 -10 13.40 1.80 5 7 -10 7.70 8.10 -5 -7 10 31.40 23.40 -5 -7 10 7.80 3.10 4 7 -10 14.90 8.30 -4 -7 10 2.20 22.50 -4 -7 10 -1.20 35.00 3 7 -10 194.38 10.70 -3 -7 10 168.08 26.50 -3 -7 10 211.08 39.80 -3 -7 10 199.38 11.60 2 7 -10 2.10 1.70 -2 -7 10 0.60 19.90 -2 -7 10 18.10 33.20 -2 -7 10 4.70 2.90 1 7 -10 99.79 6.00 -1 -7 10 81.09 22.80 -1 -7 10 137.49 37.30 -1 -7 10 89.29 7.00 0 7 -10 0.50 1.70 0 -7 10 4.20 20.30 0 -7 10 -1.60 2.80 0 -7 10 -8.40 34.30 -1 7 -10 31.40 3.40 1 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7.50 9 6 -10 20.40 11.80 9 6 -10 14.80 8.90 9 6 -10 21.40 4.60 -9 -6 10 19.90 3.80 8 6 -10 2.00 8.60 8 6 -10 16.80 10.20 8 6 -10 5.40 3.60 -8 -6 10 5.30 3.00 7 6 -10 -4.10 8.70 7 6 -10 0.90 8.30 7 6 -10 4.60 3.40 -7 -6 10 14.60 25.20 -7 -6 10 -2.10 2.80 6 6 -10 -1.60 8.10 6 6 -10 3.00 8.30 6 6 -10 4.80 3.30 -6 -6 10 5.30 2.80 -6 -6 10 -11.20 21.90 5 6 -10 27.80 2.60 5 6 -10 11.50 8.50 5 6 -10 26.50 9.10 -5 -6 10 49.90 20.70 -5 -6 10 44.60 35.20 -5 -6 10 29.60 3.60 4 6 -10 59.09 3.90 -4 -6 10 50.09 5.10 -4 -6 10 53.79 18.80 -4 -6 10 56.19 33.00 3 6 -10 328.77 17.30 -3 -6 10 344.67 52.19 -3 -6 10 301.37 36.10 -3 -6 10 323.87 18.00 2 6 -10 1.50 1.50 -2 -6 10 3.50 17.70 -2 -6 10 -31.20 31.30 -2 -6 10 0.00 2.90 1 6 -10 4.30 1.60 -1 -6 10 3.30 2.90 -1 -6 10 9.90 33.20 -1 -6 10 -1.60 17.40 0 6 -10 50.39 3.90 0 -6 10 12.10 33.10 0 -6 10 45.80 18.80 0 -6 10 46.00 5.20 -1 6 -10 30.30 3.20 1 -6 10 33.80 5.90 1 -6 10 37.50 34.90 1 -6 10 39.50 20.60 1 -6 10 32.90 3.90 -2 6 -10 40.30 3.70 2 -6 10 47.60 38.30 2 -6 10 41.90 5.40 2 -6 10 40.40 3.60 2 -6 10 41.30 5.00 2 -6 10 12.60 23.10 3 -6 10 38.90 45.20 -4 6 -10 206.48 11.50 4 -6 10 192.68 11.40 4 -6 10 209.68 11.40 -5 6 -10 -1.50 2.10 5 -6 10 0.00 1.80 -6 6 -10 61.19 5.00 6 -6 10 63.19 5.00 -7 6 -10 -0.80 2.30 7 -6 10 1.60 2.10 -8 6 -10 35.70 4.20 8 -6 10 37.90 4.30 -9 6 -10 68.49 5.30 9 -6 10 70.69 5.60 -10 6 -10 86.09 6.10 10 -6 10 85.79 6.40 -11 6 -10 59.69 4.70 11 -6 10 57.39 5.10 -12 6 -10 19.10 2.80 12 -6 10 31.40 3.80 -13 6 -10 -1.00 1.90 13 -6 10 -0.60 2.90 14 -6 10 -0.80 3.20 15 -6 10 6.10 4.00 19 5 -10 2.50 10.20 18 5 -10 -2.30 9.20 17 5 -10 -0.50 6.50 -17 -5 10 -22.10 15.30 16 5 -10 0.40 7.30 -16 -5 10 -1.20 14.60 15 5 -10 -1.40 6.80 -15 -5 10 -15.90 13.30 -15 -5 10 1.50 2.40 14 5 -10 2.70 8.50 14 5 -10 3.90 5.70 -14 -5 10 -3.80 12.60 -14 -5 10 8.80 3.70 13 5 -10 -4.00 8.00 -13 -5 10 2.60 3.30 12 5 -10 5.20 4.90 12 5 -10 3.60 8.90 -12 -5 10 3.90 3.60 11 5 -10 21.90 5.00 11 5 -10 29.70 13.80 11 5 -10 5.30 9.20 -11 -5 10 14.80 3.90 10 5 -10 49.50 13.20 10 5 -10 49.60 10.70 10 5 -10 55.09 6.70 -10 -5 10 50.19 5.60 9 5 -10 68.59 14.40 9 5 -10 78.89 11.50 9 5 -10 89.59 7.60 -9 -5 10 80.99 6.60 8 5 -10 32.50 4.60 8 5 -10 24.20 9.00 8 5 -10 23.40 9.60 -8 -5 10 -5.90 26.00 -8 -5 10 28.20 3.80 7 5 -10 40.70 3.30 7 5 -10 41.80 10.80 7 5 -10 38.10 9.80 -7 -5 10 50.79 21.90 -7 -5 10 48.60 4.90 6 5 -10 221.88 17.30 -6 -5 10 181.88 48.90 -6 -5 10 219.38 12.60 -6 -5 10 214.98 35.00 5 5 -10 195.68 15.10 5 5 -10 194.98 10.30 -5 -5 10 109.69 36.30 -5 -5 10 186.78 11.10 4 5 -10 115.29 6.40 -4 -5 10 77.19 19.40 -4 -5 10 105.59 7.40 -4 -5 10 130.29 35.30 3 5 -10 437.06 22.30 -3 -5 10 321.17 54.09 -3 -5 10 403.06 36.40 -3 -5 10 431.86 22.80 2 5 -10 149.29 8.60 -2 -5 10 165.08 33.40 -2 -5 10 136.79 21.30 -2 -5 10 160.88 9.60 -1 -5 10 -4.80 30.40 -1 -5 10 22.50 16.90 0 5 -10 85.39 5.30 0 -5 10 87.09 9.60 0 -5 10 64.99 17.90 0 -5 10 92.59 32.40 0 -5 10 83.19 6.60 -1 5 -10 8.50 1.70 1 -5 10 -0.40 18.10 1 -5 10 8.20 1.70 1 -5 10 -10.30 34.50 1 -5 10 5.30 2.80 1 -5 10 18.00 4.70 2 -5 10 -0.80 37.90 2 -5 10 15.40 20.70 -4 5 -10 32.60 3.60 4 -5 10 36.20 3.50 4 -5 10 40.40 3.50 4 -5 10 32.60 3.50 -5 5 -10 200.88 11.10 5 -5 10 205.08 11.10 5 -5 10 181.78 11.30 -6 5 -10 -0.60 2.00 6 -5 10 1.00 1.90 -7 5 -10 63.79 5.20 7 -5 10 78.39 5.30 -8 5 -10 54.79 4.70 8 -5 10 57.79 4.90 -9 5 -10 22.90 3.00 9 -5 10 19.40 2.90 -10 5 -10 93.99 6.30 10 -5 10 92.19 6.70 -11 5 -10 11.70 2.40 11 -5 10 7.30 2.70 -12 5 -10 5.40 2.10 12 -5 10 2.20 2.50 13 -5 10 0.30 2.80 14 -5 10 13.70 4.20 19 4 -10 -0.30 10.30 18 4 -10 -0.70 8.30 17 4 -10 1.60 7.30 -17 -4 10 -20.90 15.00 16 4 -10 0.80 7.40 -16 -4 10 -6.90 14.30 15 4 -10 0.40 7.60 -15 -4 10 -2.50 2.70 -15 -4 10 -15.50 12.90 14 4 -10 -7.10 7.20 -14 -4 10 0.20 3.30 -14 -4 10 -2.80 10.30 13 4 -10 11.00 9.30 13 4 -10 14.90 5.20 -13 -4 10 20.80 12.50 -13 -4 10 11.70 3.80 12 4 -10 9.10 9.70 12 4 -10 18.00 5.20 -12 -4 10 18.50 4.00 11 4 -10 9.10 8.70 11 4 -10 8.90 4.50 -11 -4 10 13.60 3.70 10 4 -10 128.19 14.50 10 4 -10 121.69 9.60 -10 -4 10 126.99 8.60 9 4 -10 118.49 12.70 9 4 -10 120.09 8.90 -9 -4 10 114.89 8.10 8 4 -10 38.50 9.60 -8 -4 10 45.00 5.10 -8 -4 10 32.60 23.40 7 4 -10 8.20 1.40 7 4 -10 10.90 8.30 -7 -4 10 32.60 20.20 -7 -4 10 12.00 3.00 6 4 -10 4.40 7.30 -6 -4 10 6.10 2.80 -6 -4 10 1.30 17.40 5 4 -10 55.29 8.90 -5 -4 10 54.39 16.50 -5 -4 10 39.40 4.80 4 4 -10 10.80 1.60 -4 -4 10 23.50 14.70 -4 -4 10 4.70 2.80 3 4 -10 1086.09 56.19 -3 -4 10 1091.89 56.59 -3 -4 10 1052.69 65.79 2 4 -10 2073.49 105.89 -2 -4 10 2093.69 106.29 -2 -4 10 1943.11 113.99 1 4 -10 111.49 6.20 -1 -4 10 85.09 17.20 -1 -4 10 108.59 7.40 -1 -4 10 102.19 5.90 -1 -4 10 77.49 10.80 0 4 -10 60.59 4.20 0 -4 10 61.89 4.00 0 -4 10 69.39 5.60 0 -4 10 62.19 7.50 0 -4 10 34.20 16.20 -1 4 -10 59.09 4.00 1 -4 10 54.29 33.80 1 -4 10 57.69 3.80 1 -4 10 57.19 5.20 1 -4 10 52.59 7.10 1 -4 10 27.80 16.70 -2 4 -10 13.90 2.00 2 -4 10 14.40 18.60 2 -4 10 10.20 1.70 2 -4 10 8.50 2.80 -3 4 -10 308.27 16.20 3 -4 10 271.67 16.50 3 -4 10 319.17 16.20 -4 4 -10 52.79 4.00 4 -4 10 50.29 3.90 4 -4 10 46.40 59.19 4 -4 10 47.10 4.90 -5 4 -10 74.19 4.90 5 -4 10 64.99 5.60 5 -4 10 62.89 4.70 -6 4 -10 -0.30 1.90 6 -4 10 0.70 2.70 6 -4 10 1.10 1.80 -7 4 -10 17.50 2.60 7 -4 10 14.90 3.00 -8 4 -10 3.60 2.30 8 -4 10 1.00 2.20 8 -4 10 4.80 1.90 -9 4 -10 4.10 2.30 9 -4 10 0.40 2.00 9 -4 10 3.40 2.50 -10 4 -10 46.00 4.40 10 -4 10 61.99 4.90 -11 4 -10 7.10 2.20 11 -4 10 18.10 3.20 -12 4 -10 -0.40 1.70 12 -4 10 1.60 2.70 13 -4 10 -0.80 2.90 14 -4 10 3.90 3.60 19 3 -10 -1.50 8.90 18 3 -10 -3.30 7.70 -17 -3 10 36.30 17.40 16 3 -10 3.00 7.60 -16 -3 10 2.30 13.50 15 3 -10 1.10 8.60 -15 -3 10 2.00 14.60 14 3 -10 1.30 8.00 -14 -3 10 4.20 3.60 -14 -3 10 8.70 12.60 13 3 -10 38.20 11.10 -13 -3 10 51.29 14.20 -13 -3 10 58.39 5.90 12 3 -10 0.70 8.40 -12 -3 10 1.50 3.40 -12 -3 10 19.90 11.10 11 3 -10 0.40 7.80 -11 -3 10 0.00 3.30 -11 -3 10 2.60 9.60 10 3 -10 -0.20 7.80 -10 -3 10 1.70 3.30 9 3 -10 30.90 9.00 -9 -3 10 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129.09 7.40 -4 -7 14 115.19 9.30 -4 -7 14 89.69 14.20 3 7 -14 182.08 9.90 -3 -7 14 169.48 9.60 -3 -7 14 138.49 17.40 -3 -7 14 172.38 11.70 2 7 -14 40.20 3.90 -2 -7 14 40.10 3.50 -2 -7 14 45.50 10.70 -2 -7 14 27.60 5.20 1 7 -14 3.60 2.10 -1 -7 14 -3.90 4.00 -1 -7 14 -1.20 1.90 0 7 -14 64.09 4.70 0 -7 14 55.79 4.60 0 -7 14 56.39 6.20 -1 7 -14 63.99 4.90 1 -7 14 49.30 6.10 1 -7 14 62.89 4.80 -2 7 -14 0.00 2.10 2 -7 14 -3.30 3.80 2 -7 14 0.60 2.10 -3 7 -14 2.50 2.30 3 -7 14 1.40 2.50 3 -7 14 0.30 2.30 3 -7 14 -0.70 2.60 -4 7 -14 8.00 2.50 4 -7 14 12.70 2.50 -5 7 -14 13.50 2.90 5 -7 14 17.10 2.90 -6 7 -14 2.70 2.40 6 -7 14 2.00 2.50 -7 7 -14 11.80 2.60 7 -7 14 8.40 2.80 -8 7 -14 5.60 2.40 8 -7 14 -1.40 2.40 -9 7 -14 -1.60 2.20 9 -7 14 -0.30 2.40 -10 7 -14 0.40 2.40 10 -7 14 0.60 2.90 -11 7 -14 0.00 2.30 11 -7 14 0.50 3.40 12 -7 14 0.40 3.60 18 6 -14 3.70 10.10 17 6 -14 9.40 11.80 16 6 -14 5.00 9.00 -16 -6 14 -9.30 14.40 -16 -6 14 6.70 3.10 15 6 -14 5.80 9.40 -15 -6 14 6.50 13.40 14 6 -14 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11.90 4.30 -2 6 -14 42.30 4.20 2 -6 14 46.10 5.10 2 -6 14 44.00 4.00 -3 6 -14 26.70 3.20 3 -6 14 21.20 4.30 3 -6 14 30.90 3.20 -4 6 -14 90.49 6.50 4 -6 14 101.29 6.50 -5 6 -14 95.19 6.60 5 -6 14 99.79 6.60 -6 6 -14 0.40 2.30 6 -6 14 -3.00 2.90 6 -6 14 1.90 2.50 -7 6 -14 -0.20 2.20 7 -6 14 1.30 2.30 -8 6 -14 20.20 2.90 -9 6 -14 2.40 2.30 9 -6 14 -1.50 2.70 -10 6 -14 24.90 3.30 10 -6 14 36.00 4.10 11 -6 14 -2.20 3.70 12 -6 14 1.10 3.80 18 5 -14 2.30 11.70 -17 -5 14 23.60 21.60 16 5 -14 8.00 9.80 -16 -5 14 10.50 13.80 -16 -5 14 -0.40 2.90 15 5 -14 10.30 9.40 -15 -5 14 -4.10 15.10 -15 -5 14 5.50 4.00 14 5 -14 1.60 9.00 -14 -5 14 11.90 4.60 -14 -5 14 -7.00 11.80 13 5 -14 14.00 10.40 -13 -5 14 21.10 13.00 12 5 -14 5.50 10.10 -12 -5 14 3.10 4.60 -12 -5 14 -17.40 11.40 11 5 -14 223.68 23.10 -11 -5 14 315.77 26.90 -11 -5 14 279.17 16.40 10 5 -14 -2.30 9.00 -10 -5 14 2.60 4.30 -10 -5 14 1.20 11.60 9 5 -14 26.70 10.30 -9 -5 14 13.20 11.50 -9 -5 14 4.70 4.10 8 5 -14 169.08 17.40 -8 -5 14 185.58 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2.70 -1 -12 15 1.00 5.00 0 12 -15 23.60 3.40 0 -12 15 23.60 5.80 0 -12 15 33.50 3.70 -1 12 -15 72.09 5.50 1 -12 15 50.09 7.20 1 -12 15 58.39 5.50 -2 12 -15 51.29 5.00 2 -12 15 34.40 6.40 2 -12 15 53.69 5.30 -3 12 -15 40.30 4.80 3 -12 15 30.40 3.90 -4 12 -15 0.10 2.90 4 -12 15 -1.60 2.70 -5 12 -15 38.30 4.40 5 -12 15 40.60 4.50 -6 12 -15 0.70 2.90 6 -12 15 2.40 3.10 -7 12 -15 13.70 3.50 7 -12 15 17.70 3.70 -8 12 -15 16.70 4.00 8 -12 15 26.20 4.30 -9 12 -15 -1.70 3.50 9 -12 15 1.40 3.80 -10 12 -15 0.30 3.70 10 -12 15 -1.30 3.90 15 11 -15 4.30 11.60 -15 -11 15 4.30 3.20 14 11 -15 -2.00 8.20 -14 -11 15 7.90 3.90 -14 -11 15 -16.50 14.50 13 11 -15 2.10 7.80 -13 -11 15 5.20 4.00 -13 -11 15 1.00 16.20 12 11 -15 1.80 8.70 -12 -11 15 4.60 4.30 11 11 -15 3.80 9.10 -11 -11 15 -2.80 4.20 10 11 -15 2.20 7.10 -10 -11 15 10.00 4.80 9 11 -15 6.50 8.70 -9 -11 15 11.60 5.10 8 11 -15 5.40 8.60 -8 -11 15 1.80 4.90 7 11 -15 7.90 9.20 -7 -11 15 4.70 5.20 6 11 -15 10.90 10.20 -6 -11 15 15.20 5.20 -5 -11 15 54.59 6.90 4 11 -15 21.10 2.90 -4 -11 15 21.10 5.50 3 11 -15 52.99 4.50 -3 -11 15 49.00 6.70 2 11 -15 47.20 4.40 -2 -11 15 39.70 6.40 1 11 -15 7.10 2.70 -1 -11 15 2.40 4.90 -1 -11 15 0.90 12.90 0 11 -15 119.49 7.80 0 -11 15 111.09 10.10 0 -11 15 134.19 8.10 -1 11 -15 40.50 4.60 1 -11 15 44.30 4.40 1 -11 15 32.80 6.10 -2 11 -15 39.80 4.70 2 -11 15 35.00 6.20 2 -11 15 49.00 4.60 -3 11 -15 9.80 3.00 3 -11 15 8.40 3.00 -4 11 -15 2.80 2.80 4 -11 15 3.50 2.70 -5 11 -15 -1.90 2.70 5 -11 15 -0.30 2.80 -6 11 -15 -0.90 2.80 6 -11 15 0.70 2.80 -7 11 -15 -0.30 2.80 7 -11 15 0.50 3.00 -8 11 -15 3.00 3.00 8 -11 15 6.40 3.40 -9 11 -15 7.30 3.50 9 -11 15 2.90 3.50 -10 11 -15 1.70 3.60 10 -11 15 4.10 4.00 16 10 -15 -2.70 12.50 15 10 -15 -1.40 9.90 -15 -10 15 3.60 3.20 14 10 -15 3.10 9.60 -14 -10 15 -13.30 17.80 -14 -10 15 -5.30 3.40 13 10 -15 -0.30 8.40 -13 -10 15 -1.60 3.80 -13 -10 15 -8.60 13.60 12 10 -15 3.30 9.60 -12 -10 15 -2.40 4.10 11 10 -15 -1.20 6.80 -11 -10 15 2.10 4.30 10 10 -15 -0.30 7.80 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-15 7.50 2.90 6 -9 15 5.70 2.80 -7 9 -15 1.20 2.60 7 -9 15 1.50 2.60 8 -9 15 18.80 3.10 -9 9 -15 -1.30 2.60 9 -9 15 -1.80 2.90 -10 9 -15 12.50 3.40 10 -9 15 9.50 3.60 -11 9 -15 -1.90 2.90 11 -9 15 4.20 3.70 17 8 -15 -1.30 10.20 16 8 -15 4.30 11.10 15 8 -15 -1.50 8.90 -15 -8 15 -13.40 16.60 -15 -8 15 -5.50 3.70 14 8 -15 4.10 9.70 -14 -8 15 3.20 3.90 -14 -8 15 -1.20 12.60 13 8 -15 2.00 10.10 -13 -8 15 21.70 13.40 12 8 -15 1.60 10.30 -12 -8 15 -1.40 11.70 -12 -8 15 11.90 4.60 11 8 -15 71.39 13.80 -11 -8 15 66.49 15.60 10 8 -15 4.90 10.80 -10 -8 15 4.40 4.70 9 8 -15 -0.80 9.30 -9 -8 15 -0.50 4.60 8 8 -15 -2.10 10.20 -8 -8 15 -6.40 4.30 7 8 -15 24.90 11.60 -7 -8 15 24.90 5.20 6 8 -15 14.30 10.90 -6 -8 15 31.00 5.30 5 8 -15 11.20 10.60 -5 -8 15 13.00 4.80 -5 -8 15 20.20 12.30 4 8 -15 14.10 2.50 -4 -8 15 15.20 11.50 -4 -8 15 11.90 2.20 -4 -8 15 10.80 4.90 3 8 -15 0.00 2.10 -3 -8 15 2.30 10.80 -3 -8 15 1.90 4.60 -3 -8 15 -1.00 1.90 2 8 -15 258.77 13.90 -2 -8 15 229.98 15.50 -2 -8 15 253.07 13.80 1 8 -15 8.40 2.30 -1 -8 15 -2.20 9.60 -1 -8 15 14.80 5.00 -1 -8 15 8.30 2.40 0 -8 15 214.28 14.60 0 -8 15 239.68 12.90 -1 8 -15 45.10 4.30 1 -8 15 43.40 4.30 1 -8 15 31.60 5.90 2 -8 15 132.19 8.20 -4 8 -15 3.50 2.60 4 -8 15 3.70 2.70 -5 8 -15 12.00 2.90 5 -8 15 6.90 2.50 -6 8 -15 20.50 3.00 6 -8 15 20.00 3.20 -7 8 -15 5.00 2.60 7 -8 15 4.60 2.90 -8 8 -15 17.60 3.00 8 -8 15 27.20 3.70 -9 8 -15 12.40 3.00 9 -8 15 10.30 3.30 -10 8 -15 1.10 2.80 10 -8 15 -0.70 3.80 11 -8 15 6.20 3.90 17 7 -15 2.80 10.90 16 7 -15 1.00 10.80 -16 -7 15 0.00 2.90 -16 -7 15 10.80 16.10 15 7 -15 1.10 9.20 -15 -7 15 1.10 15.00 -15 -7 15 6.90 4.10 14 7 -15 0.50 8.30 -14 -7 15 -1.70 3.90 -14 -7 15 -2.40 11.80 13 7 -15 0.20 9.50 -13 -7 15 4.80 4.50 -13 -7 15 0.60 11.50 12 7 -15 7.60 11.50 -12 -7 15 15.50 12.70 -11 -7 15 21.50 15.20 -11 -7 15 30.40 5.50 10 7 -15 8.70 10.60 -10 -7 15 42.80 14.90 -10 -7 15 29.80 5.40 9 7 -15 -6.80 9.80 -9 -7 15 -1.30 12.30 -9 -7 15 0.70 4.40 8 7 -15 1.30 10.20 -8 -7 15 14.10 4.90 -8 -7 15 -15.90 11.80 7 7 -15 -0.90 1.10 7 7 -15 6.60 10.00 -7 -7 15 0.80 4.30 -7 -7 15 1.60 11.20 6 7 -15 87.89 15.10 -6 -7 15 93.99 8.60 -6 -7 15 105.39 16.90 5 7 -15 0.30 9.10 -5 -7 15 1.00 4.40 -5 -7 15 6.10 11.10 4 7 -15 345.37 17.60 -4 -7 15 311.57 19.10 -4 -7 15 293.17 25.30 -4 -7 15 324.07 17.30 3 7 -15 2.30 2.10 -3 -7 15 1.50 4.50 -3 -7 15 0.50 1.70 -3 -7 15 -6.50 9.90 2 7 -15 63.59 4.80 -2 -7 15 66.29 4.40 -2 -7 15 37.40 11.50 -2 -7 15 54.99 6.50 1 7 -15 13.00 2.50 -1 -7 15 -1.40 8.40 -1 -7 15 6.70 4.80 -1 -7 15 10.00 2.20 0 7 -15 36.60 4.00 0 -7 15 36.80 3.40 -1 7 -15 13.60 2.60 1 -7 15 13.20 2.40 1 -7 15 17.40 4.90 -2 7 -15 12.10 2.70 2 -7 15 8.80 2.50 -3 7 -15 1.30 2.40 3 -7 15 -1.20 2.20 3 -7 15 -0.80 2.20 -4 7 -15 5.50 2.60 4 -7 15 8.40 2.60 4 -7 15 8.90 2.50 -5 7 -15 2.20 2.40 5 -7 15 13.10 2.60 -6 7 -15 3.70 2.50 6 -7 15 7.10 2.80 -7 7 -15 1.00 2.40 7 -7 15 0.20 2.40 -8 7 -15 19.70 3.00 8 -7 15 18.30 3.00 -9 7 -15 8.50 2.80 9 -7 15 4.40 3.10 -10 7 -15 5.20 2.70 10 -7 15 0.50 3.70 11 -7 15 -1.10 3.50 18 6 -15 5.30 10.40 17 6 -15 2.10 12.30 16 6 -15 5.90 10.00 -16 -6 15 5.80 3.50 -16 -6 15 24.10 14.00 -15 -6 15 0.20 14.90 -15 -6 15 -0.20 3.80 14 6 -15 10.10 11.00 -14 -6 15 15.30 13.90 13 6 -15 8.60 9.90 -13 -6 15 2.10 4.40 -13 -6 15 4.40 11.70 12 6 -15 13.30 10.30 -12 -6 15 6.80 13.90 -12 -6 15 20.30 5.00 11 6 -15 44.00 12.70 -11 -6 15 67.39 7.60 -11 -6 15 88.69 17.60 10 6 -15 9.60 10.90 -10 -6 15 9.10 12.70 -10 -6 15 7.40 4.70 9 6 -15 9.50 10.90 -9 -6 15 41.20 13.40 -9 -6 15 30.90 5.10 8 6 -15 151.88 17.20 -8 -6 15 171.68 21.00 -8 -6 15 187.18 11.90 7 6 -15 31.00 2.90 7 6 -15 20.80 11.20 -7 -6 15 27.80 5.20 -7 -6 15 26.60 13.00 6 6 -15 43.30 11.80 -6 -6 15 49.99 6.00 -6 -6 15 50.49 13.30 5 6 -15 -1.60 8.20 -5 -6 15 -8.70 9.50 -5 -6 15 -1.80 4.00 4 6 -15 17.80 9.60 4 6 -15 29.50 3.50 -4 -6 15 38.60 11.40 -4 -6 15 19.70 4.80 3 6 -15 32.60 3.50 -3 -6 15 24.30 10.70 -3 -6 15 26.20 2.60 -3 -6 15 27.50 5.10 2 6 -15 3.60 2.00 -2 -6 15 2.90 1.60 -2 -6 15 17.90 9.70 -2 -6 15 6.70 4.60 1 6 -15 161.78 9.10 -1 -6 15 156.28 8.70 -1 -6 15 132.39 11.00 0 6 -15 -0.60 2.00 0 -6 15 0.40 1.80 0 -6 15 -0.40 4.30 -1 6 -15 1.30 2.10 1 -6 15 -3.10 4.00 1 -6 15 0.90 2.00 -2 6 -15 -0.30 2.00 2 -6 15 -0.40 2.10 2 -6 15 1.80 2.50 -3 6 -15 5.60 2.30 3 -6 15 5.50 2.30 3 -6 15 3.80 3.60 -4 6 -15 0.10 2.20 4 -6 15 -1.10 2.30 4 -6 15 2.60 2.40 -5 6 -15 35.10 3.60 5 -6 15 25.00 3.20 -6 6 -15 -2.60 2.20 6 -6 15 -1.20 2.40 -7 6 -15 1.30 2.40 7 -6 15 2.40 2.30 -8 6 -15 5.90 2.50 8 -6 15 4.90 2.80 -9 6 -15 32.00 3.80 9 -6 15 35.50 4.00 10 -6 15 2.40 3.30 11 -6 15 7.40 3.80 18 5 -15 -2.20 11.90 17 5 -15 -1.60 10.10 16 5 -15 27.30 11.10 -16 -5 15 4.50 14.70 -16 -5 15 25.30 4.70 15 5 -15 1.20 8.90 -15 -5 15 8.20 14.60 -15 -5 15 -1.10 4.10 14 5 -15 -1.00 8.10 -14 -5 15 2.60 4.50 -14 -5 15 -8.10 15.20 13 5 -15 1.70 8.70 -13 -5 15 8.00 4.70 -13 -5 15 -7.80 14.20 12 5 -15 -2.90 9.50 -12 -5 15 11.90 4.90 -12 -5 15 17.90 13.90 11 5 -15 27.50 11.80 -11 -5 15 32.90 5.50 -11 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0.0167 16 1 6 -0.1519 -0.0091 16 2 0 -1.3401 -0.0293 16 2 1 -0.7836 -0.0535 16 2 2 -0.1311 0.0119 16 2 3 0.0337 0.0096 16 2 4 0.1191 -0.0344 16 2 5 0.0884 -0.0207 16 3 0 -0.1614 -0.0045 16 3 1 0.4512 0.0375 16 3 2 -0.1106 -0.0018 16 3 3 -0.0055 -0.0069 16 3 4 0.1706 0.0261 16 3 5 -0.3345 0.0141 16 4 0 -0.1560 0.0376 16 4 1 0.5948 -0.0178 16 4 2 0.0699 -0.0111 16 4 3 -0.5143 0.0013 16 4 4 0.3863 -0.0194 16 5 0 0.3443 -0.0541 16 5 1 0.7630 -0.0048 16 5 2 0.5931 0.0133 16 5 3 0.3958 0.0080 16 6 0 0.6993 0.0607 16 6 1 -1.1819 0.0263 16 6 2 -0.4423 -0.0152 16 7 0 -2.0073 -0.0620 16 7 1 0.0582 -0.0342 16 8 0 1.7537 0.0530 17 -13 0 -0.1086 0.0077 17 -12 0 0.4781 -0.0082 17 -12 1 0.7432 -0.0038 17 -12 2 1.0502 -0.0090 17 -11 0 -0.6294 -0.0031 17 -11 1 -0.1750 0.0146 17 -11 2 -0.9991 0.0109 17 -10 0 0.9973 0.0191 17 -10 1 -0.1697 -0.0284 17 -10 2 -0.4623 -0.0141 17 -10 3 0.1442 -0.0105 17 -10 4 -0.3039 -0.0180 17 -9 0 -0.3618 -0.0539 17 -9 1 -0.6225 0.0167 17 -9 2 0.7084 0.0283 17 -9 3 0.5668 0.0203 17 -9 4 0.1894 0.0141 17 -9 5 -0.2175 0.0001 17 -8 1 0.5548 -0.0073 17 -8 2 0.2919 -0.0347 17 -8 3 0.0019 -0.0133 17 -8 4 -0.2602 -0.0112 17 -8 5 0.0157 -0.0039 17 -7 0 1.0390 -0.0995 17 -7 1 0.5254 -0.0030 17 -7 2 0.0246 0.0332 17 -7 3 -0.3010 0.0041 17 -7 4 0.0273 0.0053 17 -7 5 0.0861 0.0088 17 -7 6 -0.8593 -0.0097 17 -6 0 0.6602 0.1115 17 -6 1 -0.1064 0.0172 17 -6 2 -0.7131 -0.0448 17 -6 3 -0.2385 -0.0027 17 -6 4 0.2426 0.0133 17 -6 5 -0.1036 -0.0020 17 -6 6 -0.1117 0.0038 17 -5 0 -1.2782 -0.1159 17 -5 1 -0.8344 -0.0336 17 -5 2 0.1329 0.0511 17 -5 3 0.0431 0.0089 17 -5 4 -0.4102 -0.0266 17 -5 5 -0.2236 -0.0098 17 -5 6 -0.0898 -0.0014 17 -4 0 0.3927 0.1024 17 -4 1 -0.0480 0.0513 17 -4 2 -0.1792 -0.0477 17 -4 3 0.3008 -0.0201 17 -4 4 0.4406 0.0251 17 -4 5 0.4432 0.0128 17 -4 6 0.9745 0.0031 17 -3 0 -0.2443 -0.0726 17 -3 1 0.2669 -0.0580 17 -3 2 1.1533 0.0375 17 -3 3 0.8514 0.0298 17 -3 4 0.1023 -0.0123 17 -3 5 -0.2085 -0.0074 17 -3 6 -0.8649 0.0001 17 -2 0 0.6652 0.0369 17 -2 1 0.4178 0.0568 17 -2 2 -0.9689 -0.0215 17 -2 3 -1.0809 -0.0312 17 -2 4 -0.3219 0.0030 17 -2 5 -0.3904 -0.0029 17 -1 0 0.2212 -0.0092 17 -1 1 0.2507 -0.0485 17 -1 2 -0.1902 0.0029 17 -1 3 -0.0278 0.0146 17 -1 4 0.2472 -0.0052 17 -1 5 0.5109 0.0096 17 0 0 0.7745 -0.0153 17 0 1 -0.5803 0.0350 17 0 2 -0.6237 0.0128 17 0 3 -0.0998 0.0078 17 0 4 0.1203 0.0185 17 0 5 -0.0229 -0.0001 17 1 0 -2.7548 0.0400 17 1 1 -0.1945 -0.0218 17 1 2 1.1121 -0.0170 17 1 3 0.2393 -0.0170 17 1 4 -0.1349 -0.0308 17 2 0 1.1756 -0.0603 17 2 1 1.1316 0.0085 17 2 2 0.1889 0.0148 17 2 3 -0.1533 0.0128 17 3 0 0.4116 0.0758 17 3 1 -0.3014 0.0071 17 3 2 0.0432 -0.0200 17 3 3 -0.1065 -0.0095 17 4 0 -0.0716 -0.0864 17 4 1 -0.6856 -0.0201 17 4 2 -0.2333 0.0287 17 5 0 0.0148 0.0822 17 5 1 -0.4518 0.0315 17 6 0 -0.7630 -0.0711 18 -6 0 -0.5230 -0.0690 18 -6 2 0.6427 0.0339 18 -6 3 0.2521 -0.0038 18 -5 0 0.6552 0.0590 18 -5 1 0.3871 0.0310 18 -5 2 -0.2781 -0.0349 18 -5 3 -0.1154 -0.0063 18 -4 0 -0.2519 -0.0289 18 -4 1 0.0890 -0.0405 18 -4 2 0.3092 0.0222 18 -4 3 0.0056 0.0134 18 -3 0 -0.0099 -0.0118 18 -3 1 0.0327 0.0342 18 -3 2 -0.8572 -0.0081 18 -3 3 -0.8516 -0.0163 18 -2 0 0.0368 0.0449 18 -2 1 0.0518 -0.0217 18 -2 2 0.5948 -0.0061 18 -2 3 0.7957 0.0115 18 -1 0 0.1679 -0.0618 18 -1 1 -0.6650 0.0114 18 -1 2 -0.0689 0.0214 18 -1 3 0.0306 0.0072 18 0 0 -1.7227 0.0755 18 0 1 0.1740 -0.0010 18 0 2 0.7544 -0.0326 18 1 0 2.2474 -0.0889 18 1 1 0.6308 -0.0091 18 1 2 -0.6744 0.0328 18 2 0 -0.1706 0.0911 18 2 1 -0.7220 0.0165 18 3 0 -0.7343 -0.0855 19 -4 0 0.3499 -0.0255 19 -3 0 0.1945 0.0577 19 -2 0 -0.2408 -0.0741 19 -1 0 -0.6864 0.0760 0 0 0 0.0 0.0 ; _shelx_fab_checksum 82362 _olex2_submission_special_instructions 'No special instructions were received' _site XU loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn01 Zn 0.20278(6) 0.45434(6) 0.33184(5) 0.0559(3) Uani 1 1 d . . . . . Cl1 Cl 0.35525(12) 0.45682(13) 0.37595(11) 0.0790(6) Uani 1 1 d . . . . . Si1 Si 0.17251(14) 0.25452(12) 0.63846(11) 0.0661(5) Uani 1 1 d . . . . . Si2 Si 0.27857(17) 0.84072(13) 0.68433(12) 0.0784(6) Uani 1 1 d . U . . . Si3 Si 0.30934(19) 0.66368(16) 0.05083(13) 0.0898(8) Uani 1 1 d . U . . . Si4 Si 0.2172(9) 0.0828(7) 0.0021(7) 0.116(3) Uani 0.512(7) 1 d D U P A 2 C1 C 0.6429(9) 0.5543(8) 0.4195(14) 0.056(3) Uani 0.644(7) 1 d D U P B 1 H1A H 0.624642 0.504789 0.374911 0.084 Uiso 0.644(7) 1 d R U P B 1 H1B H 0.680362 0.544169 0.465231 0.084 Uiso 0.644(7) 1 d R U P B 1 H1C H 0.676192 0.595349 0.408211 0.084 Uiso 0.644(7) 1 d R U P B 1 N1 N 0.1642(3) 0.4839(3) 0.4295(3) 0.0525(13) Uani 1 1 d . . . . . N2 N 0.1615(4) 0.3319(3) 0.3140(3) 0.0563(13) Uani 1 1 d . . . . . N3 N 0.2074(4) 0.5763(3) 0.3359(3) 0.0568(13) Uani 1 1 d . . . . . N4 N 0.1782(3) 0.4231(3) 0.2127(3) 0.0550(13) Uani 1 1 d . . . . . C2 C 0.1635(4) 0.2702(4) 0.2535(4) 0.0549(16) Uani 1 1 d . . . . . C3 C 0.1535(4) 0.3473(4) 0.1607(3) 0.0564(16) Uani 1 1 d . . . . . C4 C 0.1160(4) 0.4745(4) 0.5304(4) 0.0563(16) Uani 1 1 d . . . . . C5 C 0.1316(4) 0.5572(4) 0.5377(3) 0.0539(16) Uani 1 1 d . . . . . C6 C 0.1647(4) 0.5604(4) 0.4747(4) 0.0558(16) Uani 1 1 d . . . . . C7 C 0.1503(4) 0.2164(4) 0.3458(4) 0.0569(16) Uani 1 1 d . . . . . C8 C 0.1246(5) 0.3504(4) 0.0816(4) 0.0575(16) Uani 1 1 d . . . . . C9 C 0.2323(4) 0.6044(4) 0.2838(4) 0.0561(16) Uani 1 1 d . . . . . C10 C 0.1408(4) 0.4314(4) 0.4640(3) 0.0502(15) Uani 1 1 d . . . . . C11 C 0.1526(4) 0.3022(4) 0.3714(4) 0.0549(16) Uani 1 1 d . . . . . C12 C 0.0787(5) 0.4509(4) 0.5789(4) 0.0593(17) Uani 1 1 d . . . . . H12 H 0.065149 0.395739 0.572413 0.071 Uiso 1 1 calc R U . . . C13 C 0.1606(4) 0.2767(4) 0.1809(4) 0.0566(16) Uani 1 1 d . . . . . C14 C 0.0755(4) 0.5905(4) 0.6445(4) 0.0576(16) Uani 1 1 d . . . . . C15 C 0.0612(4) 0.5085(4) 0.6375(4) 0.0573(16) Uani 1 1 d . . . . . C16 C 0.1456(4) 0.3500(4) 0.4419(3) 0.0546(16) Uani 1 1 d . . . . . C17 C 0.1988(5) 0.6311(4) 0.4654(4) 0.0576(17) Uani 1 1 d . . . . . C18 C 0.2196(5) 0.7021(4) 0.5321(4) 0.0627(18) Uani 1 1 d . . . . . C19 C 0.2193(5) 0.6382(4) 0.4005(4) 0.0589(17) Uani 1 1 d . . . . . C20 C 0.1601(5) 0.1957(4) 0.2712(4) 0.0582(17) Uani 1 1 d . . . . . C21 C 0.1093(5) 0.6133(4) 0.5922(4) 0.0606(17) Uani 1 1 d . . . . . H21 H 0.116615 0.667785 0.594653 0.073 Uiso 1 1 calc R U . . . C22 C 0.1504(4) 0.3125(4) 0.5000(4) 0.0571(16) Uani 1 1 d . . . . . C23 C 0.1400(4) 0.4318(4) 0.0894(3) 0.0548(16) Uani 1 1 d . . . . . C24 C 0.0503(5) 0.3167(4) -0.0552(4) 0.0657(19) Uani 1 1 d . . . . . C25 C 0.2170(4) 0.5570(4) 0.2067(4) 0.0562(16) Uani 1 1 d . . . . . C26 C 0.0635(5) 0.3997(4) -0.0471(4) 0.0610(17) Uani 1 1 d . . . . . C27 C 0.1097(5) 0.4565(4) 0.0251(4) 0.0604(17) Uani 1 1 d . . . . . H27 H 0.120489 0.511613 0.030409 0.072 Uiso 1 1 calc R U . . . C28 C 0.1394(5) 0.1571(4) 0.3776(4) 0.0654(18) Uani 1 1 d . . . . . H28 H 0.130209 0.170038 0.426421 0.078 Uiso 1 1 calc R U . . . C29 C 0.1785(4) 0.4758(4) 0.1717(4) 0.0550(16) Uani 1 1 d . . . . . C30 C 0.2567(5) 0.7131(4) 0.3934(4) 0.0570(16) Uani 1 1 d . . . . . C31 C 0.2659(5) 0.6900(4) 0.3184(4) 0.0633(18) Uani 1 1 d . . . . . C32 C 0.1419(5) 0.0781(4) 0.3377(4) 0.0636(18) Uani 1 1 d . . . . . C33 C 0.0277(5) 0.4218(5) -0.1137(4) 0.0652(18) Uani 1 1 d . . . . . H33 H 0.037372 0.476632 -0.109527 0.078 Uiso 1 1 calc R U . . . C34 C 0.0250(5) 0.6235(5) 0.7555(4) 0.070(2) Uani 1 1 d . . . . . H34 H 0.014532 0.662484 0.796681 0.083 Uiso 1 1 calc R U . . . C35 C 0.0253(4) 0.4876(5) 0.6908(4) 0.0626(18) Uani 1 1 d . . . . . H35 H 0.011735 0.432732 0.685492 0.075 Uiso 1 1 calc R U . . . C36 C 0.0808(5) 0.2933(4) 0.0109(4) 0.0664(19) Uani 1 1 d . . . . . H36 H 0.071128 0.238402 0.006586 0.080 Uiso 1 1 calc R U . . . C37 C 0.2819(5) 0.7908(4) 0.4405(4) 0.070(2) Uani 1 1 d . . . . . H37 H 0.273354 0.805926 0.489584 0.084 Uiso 1 1 calc R U . . . C38 C 0.0548(5) 0.6474(5) 0.7038(4) 0.0676(19) Uani 1 1 d . . . . . H38 H 0.061637 0.702233 0.707567 0.081 Uiso 1 1 calc R U . . . C39 C 0.1607(5) 0.2851(4) 0.5529(4) 0.0638(18) Uani 1 1 d . . . . . C40 C 0.1568(5) 0.0584(4) 0.2657(4) 0.0626(18) Uani 1 1 d . . . . . C41 C 0.2442(5) 0.5941(4) 0.1564(4) 0.0645(18) Uani 1 1 d . . . . . C42 C -0.0202(5) 0.3666(4) -0.1834(4) 0.071(2) Uani 1 1 d . . . . . H42 H -0.044839 0.383088 -0.226989 0.085 Uiso 1 1 calc R U . . . C43 C 0.1627(5) 0.1189(4) 0.2321(4) 0.0634(18) Uani 1 1 d . . . . . H43 H 0.168566 0.105819 0.182015 0.076 Uiso 1 1 calc R U . . . C44 C 0.0100(5) 0.5439(5) 0.7487(4) 0.0656(19) Uani 1 1 d . . . . . H44 H -0.011131 0.528341 0.784833 0.079 Uiso 1 1 calc R U . . . C45 C 0.1726(5) 0.2104(4) 0.1234(4) 0.0657(18) Uani 1 1 d . . . . . C46 C 0.1947(6) 0.3493(5) 0.7224(4) 0.076(2) Uani 1 1 d . . . . . H46 H 0.141768 0.375428 0.709768 0.092 Uiso 1 1 calc R U . . . C47 C 0.3343(6) 0.8253(5) 0.3438(4) 0.080(2) Uani 1 1 d . . . . . C48 C 0.2432(6) 0.7597(5) 0.5909(4) 0.073(2) Uani 1 1 d . . . . . C49 C 0.0643(5) 0.1917(4) 0.6213(4) 0.073(2) Uani 1 1 d . . . . . H49 H 0.068877 0.179418 0.670053 0.087 Uiso 1 1 calc R U . . . C50 C 0.3037(6) 0.7460(4) 0.2944(4) 0.075(2) Uani 1 1 d . . . . . H50 H 0.308989 0.730605 0.244111 0.090 Uiso 1 1 calc R U . . . C51 C 0.3207(6) 0.8494(4) 0.4169(4) 0.077(2) Uani 1 1 d . . . . . C52 C 0.0009(6) 0.2610(5) -0.1290(4) 0.081(2) Uani 1 1 d . . . . . H52 H -0.008406 0.205580 -0.135341 0.098 Uiso 1 1 calc R U . . . C53 C 0.6159(10) 0.7970(5) 0.5610(7) 0.070(3) Uani 0.644(7) 1 d D U P B 1 H53A H 0.556984 0.806363 0.535360 0.105 Uiso 0.644(7) 1 calc R U P B 1 H53B H 0.661240 0.834250 0.556963 0.105 Uiso 0.644(7) 1 calc R U P B 1 H53C H 0.623826 0.805649 0.615798 0.105 Uiso 0.644(7) 1 calc R U P B 1 C54 C 0.1628(6) -0.0217(5) 0.2288(4) 0.077(2) Uani 1 1 d . . . . . H54 H 0.172896 -0.035424 0.180399 0.092 Uiso 1 1 calc R U . . . C55 C -0.0119(6) 0.2363(5) 0.6066(5) 0.083(2) Uani 1 1 d . . . . . H55A H -0.000482 0.285436 0.650748 0.124 Uiso 1 1 calc R U . . . H55B H -0.066723 0.202383 0.600024 0.124 Uiso 1 1 calc R U . . . H55C H -0.017999 0.250004 0.559435 0.124 Uiso 1 1 calc R U . . . N5 N 0.5420(4) 0.6526(3) 0.4719(3) 0.1096(17) Uani 1 1 d D U . . . C56 C 0.2699(5) 0.6218(5) 0.1141(4) 0.074(2) Uani 1 1 d . . . . . C57 C 0.1318(6) 0.0159(4) 0.3692(5) 0.081(2) Uani 1 1 d . . . . . H57 H 0.120792 0.027761 0.417190 0.097 Uiso 1 1 calc R U . . . C58 C 0.1883(6) 0.1589(5) 0.0750(4) 0.080(2) Uani 1 1 d D . . . . C59 C -0.0332(6) 0.2851(5) -0.1907(4) 0.082(2) Uani 1 1 d . . . . . H59 H -0.066400 0.246519 -0.239542 0.099 Uiso 1 1 calc R U . . . C60 C 0.0424(6) 0.1118(5) 0.5561(5) 0.087(2) Uani 1 1 d . . . . . H60A H 0.034988 0.121435 0.506780 0.130 Uiso 1 1 calc R U . . . H60B H -0.012712 0.080943 0.552986 0.130 Uiso 1 1 calc R U . . . H60C H 0.090652 0.081762 0.566378 0.130 Uiso 1 1 calc R U . . . C61 C 0.1377(6) -0.0611(5) 0.3310(5) 0.084(2) Uani 1 1 d . . . . . H61 H 0.130342 -0.102318 0.352227 0.100 Uiso 1 1 calc R U . . . C62 C 0.2701(6) 0.2013(5) 0.6537(5) 0.077(2) Uani 1 1 d . . . . . H62 H 0.324081 0.244057 0.676450 0.093 Uiso 1 1 calc R U . . . C63 C 0.1546(6) -0.0785(5) 0.2606(5) 0.087(3) Uani 1 1 d . . . . . H63 H 0.160353 -0.131496 0.235111 0.104 Uiso 1 1 calc R U . . . C64 C 0.2022(6) 0.3370(6) 0.7999(4) 0.095(3) Uani 1 1 d . . . . . H64A H 0.149774 0.300203 0.793618 0.143 Uiso 1 1 calc R U . . . H64B H 0.206387 0.388607 0.838878 0.143 Uiso 1 1 calc R U . . . H64C H 0.255403 0.314398 0.816719 0.143 Uiso 1 1 calc R U . . . C65 C 0.2788(6) 0.1444(6) 0.5800(5) 0.095(3) Uani 1 1 d . . . . . H65A H 0.229969 0.098601 0.557463 0.142 Uiso 1 1 calc R U . . . H65B H 0.335368 0.125459 0.592577 0.142 Uiso 1 1 calc R U . . . H65C H 0.276772 0.172665 0.542629 0.142 Uiso 1 1 calc R U . . . C66 C 0.3500(7) 0.9300(5) 0.4655(5) 0.097(3) Uani 1 1 d . . . . . H66 H 0.342512 0.946032 0.515001 0.117 Uiso 1 1 calc R U . . . C67 C 0.3752(8) 0.8852(6) 0.3233(6) 0.114(4) Uani 1 1 d . . . . . H67 H 0.384161 0.870827 0.274378 0.137 Uiso 1 1 calc R U . . . C68 C 0.1919(7) 0.9040(5) 0.6828(6) 0.101(3) Uani 1 1 d . U . . . H68 H 0.215264 0.951756 0.731023 0.121 Uiso 1 1 calc R U . . . C69 C 0.2736(8) 0.4093(6) 0.7314(6) 0.120(4) Uani 1 1 d . . . . . H69A H 0.328617 0.390664 0.752005 0.181 Uiso 1 1 calc R U . . . H69B H 0.273417 0.461557 0.767244 0.181 Uiso 1 1 calc R U . . . H69C H 0.269605 0.414123 0.680755 0.181 Uiso 1 1 calc R U . . . C70 C 0.3889(8) 0.9850(6) 0.4426(6) 0.123(4) Uani 1 1 d . . . . . H70 H 0.407080 1.039170 0.475609 0.147 Uiso 1 1 calc R U . . . C71 C 0.2749(8) 0.1590(6) 0.7136(5) 0.110(3) Uani 1 1 d . . . . . H71A H 0.279155 0.198258 0.763323 0.165 Uiso 1 1 calc R U . . . H71B H 0.327156 0.133147 0.720110 0.165 Uiso 1 1 calc R U . . . H71C H 0.221409 0.118405 0.695733 0.165 Uiso 1 1 calc R U . . . C72 C 0.3832(8) 0.9024(6) 0.6921(7) 0.128(3) Uani 1 1 d . U . . . H72 H 0.361989 0.922003 0.647094 0.153 Uiso 1 1 calc R U . . . C73 C 0.2868(8) 0.7905(6) 0.7580(5) 0.102(3) Uani 1 1 d . U . . . H73 H 0.224528 0.765593 0.748060 0.122 Uiso 1 1 calc R U . . . C74 C 0.4023(9) 0.9625(6) 0.3710(6) 0.131(5) Uani 1 1 d . . . . . H74 H 0.430149 1.001058 0.355602 0.157 Uiso 1 1 calc R U . . . C75 C 0.4147(8) 0.9809(6) 0.7593(7) 0.141(5) Uani 1 1 d . U . . . H75A H 0.367308 1.012675 0.756406 0.211 Uiso 1 1 calc R U . . . H75B H 0.466845 1.010731 0.756294 0.211 Uiso 1 1 calc R U . . . H75C H 0.430275 0.969795 0.808413 0.211 Uiso 1 1 calc R U . . . C76 C 0.3368(9) 0.7227(7) 0.7514(6) 0.132(4) Uani 1 1 d . U . . . H76A H 0.314733 0.685689 0.697901 0.198 Uiso 1 1 calc R U . . . H76B H 0.328482 0.694385 0.786518 0.198 Uiso 1 1 calc R U . . . H76C H 0.399905 0.743568 0.765326 0.198 Uiso 1 1 calc R U . . . C77 C 0.2207(9) 0.7268(7) 0.0159(6) 0.122(3) Uani 1 1 d . U . . . H77 H 0.240625 0.752256 -0.018146 0.146 Uiso 1 1 calc R U . . . C78 C 0.1334(8) 0.6674(7) -0.0344(6) 0.124(4) Uani 1 1 d . U . . . H78A H 0.109590 0.645200 -0.001390 0.186 Uiso 1 1 calc R U . . . H78B H 0.144845 0.623936 -0.073822 0.186 Uiso 1 1 calc R U . . . H78C H 0.090271 0.695485 -0.059817 0.186 Uiso 1 1 calc R U . . . C79 C 0.1046(7) 0.8642(6) 0.6826(8) 0.134(4) Uani 1 1 d . U . . . H79A H 0.075619 0.821441 0.632888 0.201 Uiso 1 1 calc R U . . . H79B H 0.066079 0.904043 0.690049 0.201 Uiso 1 1 calc R U . . . H79C H 0.115614 0.841554 0.724806 0.201 Uiso 1 1 calc R U . . . C80 C 0.1763(9) 0.9353(6) 0.6136(7) 0.145(5) Uani 1 1 d . U . . . H80A H 0.231667 0.966623 0.617882 0.217 Uiso 1 1 calc R U . . . H80B H 0.130923 0.969163 0.613914 0.217 Uiso 1 1 calc R U . . . H80C H 0.156391 0.889849 0.565138 0.217 Uiso 1 1 calc R U . . . C81 C 0.5610(6) 0.5701(4) 0.4392(7) 0.102(2) Uani 0.644(7) 1 d D U P B 1 H81A H 0.558177 0.542089 0.476522 0.122 Uiso 0.644(7) 1 calc R U P B 1 H81B H 0.510492 0.542305 0.391246 0.122 Uiso 0.644(7) 1 calc R U P B 1 C82 C 0.4092(9) 0.7392(7) 0.1117(6) 0.136(3) Uani 1 1 d D U . . . H82 H 0.396408 0.773041 0.157991 0.164 Uiso 1 1 calc R U . . . C83 C 0.3102(10) 0.5837(8) -0.0329(7) 0.139(3) Uani 1 1 d . U . . . H83 H 0.247007 0.555976 -0.058388 0.167 Uiso 1 1 calc R U . . . C84 C 0.3173(10) 0.8487(8) 0.8413(6) 0.155(5) Uani 1 1 d . U . . . H84A H 0.380606 0.870162 0.857460 0.232 Uiso 1 1 calc R U . . . H84B H 0.306917 0.820466 0.875859 0.232 Uiso 1 1 calc R U . . . H84C H 0.283813 0.892780 0.843776 0.232 Uiso 1 1 calc R U . . . C85 C 0.5044(6) 0.6407(8) 0.5332(6) 0.112(3) Uani 0.644(7) 1 d D U P B 1 H85A H 0.499166 0.582889 0.526583 0.134 Uiso 0.644(7) 1 calc R U P B 1 H85B H 0.550770 0.668928 0.583895 0.134 Uiso 0.644(7) 1 calc R U P B 1 C86 C 0.3622(10) 0.5170(9) -0.0105(8) 0.171(6) Uani 1 1 d . U . . . H86A H 0.423209 0.541756 0.022736 0.256 Uiso 1 1 calc R U . . . H86B H 0.362838 0.476465 -0.057830 0.256 Uiso 1 1 calc R U . . . H86C H 0.332779 0.491739 0.017280 0.256 Uiso 1 1 calc R U . . . C87 C 0.4393(10) 0.7952(8) 0.0725(7) 0.172(6) Uani 1 1 d D U . . . H87A H 0.472363 0.768076 0.039892 0.258 Uiso 1 1 calc R U . . . H87B H 0.477340 0.843882 0.112331 0.258 Uiso 1 1 calc R U . . . H87C H 0.387255 0.809414 0.040408 0.258 Uiso 1 1 calc R U . . . C88 C 0.2145(12) 0.7937(8) 0.0847(8) 0.173(5) Uani 1 1 d . U . . . H88A H 0.178253 0.830154 0.065702 0.259 Uiso 1 1 calc R U . . . H88B H 0.273982 0.823307 0.117407 0.259 Uiso 1 1 calc R U . . . H88C H 0.187086 0.770492 0.115103 0.259 Uiso 1 1 calc R U . . . C89 C 0.4733(7) 0.6771(9) 0.4167(7) 0.122(2) Uani 0.644(7) 1 d D U P B 1 H89A H 0.419878 0.634860 0.388420 0.146 Uiso 0.644(7) 1 calc R U P B 1 H89B H 0.456293 0.727755 0.442198 0.146 Uiso 0.644(7) 1 calc R U P B 1 C90 C 0.4529(10) 0.8626(8) 0.6742(9) 0.183(6) Uani 1 1 d . U . . . H90A H 0.485148 0.846373 0.717971 0.274 Uiso 1 1 calc R U . . . H90B H 0.493775 0.899129 0.664491 0.274 Uiso 1 1 calc R U . . . H90C H 0.427243 0.815063 0.627845 0.274 Uiso 1 1 calc R U . . . C91 C 0.4203(7) 0.6634(9) 0.5416(8) 0.066(3) Uani 0.644(7) 1 d D U P B 1 H91A H 0.378345 0.657107 0.490448 0.100 Uiso 0.644(7) 1 calc R U P B 1 H91B H 0.431389 0.719301 0.575040 0.100 Uiso 0.644(7) 1 calc R U P B 1 H91C H 0.395383 0.628775 0.564883 0.100 Uiso 0.644(7) 1 calc R U P B 1 C92 C 0.6243(6) 0.7119(5) 0.5222(7) 0.107(2) Uani 0.644(7) 1 d D U P B 1 H92A H 0.662750 0.713704 0.490305 0.128 Uiso 0.644(7) 1 calc R U P B 1 H92B H 0.655954 0.691066 0.563455 0.128 Uiso 0.644(7) 1 calc R U P B 1 C93 C 0.4895(17) 0.6314(19) 0.3166(9) 0.106(4) Uani 0.356(7) 1 d D U P B 2 H93A H 0.450921 0.582741 0.277054 0.159 Uiso 0.356(7) 1 d R U P B 2 H93B H 0.551311 0.628361 0.320404 0.159 Uiso 0.356(7) 1 d R U P B 2 H93C H 0.473511 0.678201 0.301984 0.159 Uiso 0.356(7) 1 d R U P B 2 C94 C 0.4839(9) 0.6951(9) 0.1408(8) 0.202(7) Uani 1 1 d D U . . . H94A H 0.541310 0.729948 0.157027 0.302 Uiso 1 1 d R U . . . H94B H 0.481010 0.646268 0.098817 0.302 Uiso 1 1 d R U . . . H94C H 0.476890 0.680878 0.184837 0.302 Uiso 1 1 d R U . . . C95 C 0.3148(18) 0.0284(15) 0.1128(12) 0.137(6) Uani 0.512(7) 1 d D U P A 2 H95A H 0.256315 0.030767 0.118670 0.205 Uiso 0.512(7) 1 calc R U P A 2 H95B H 0.359433 0.069009 0.157281 0.205 Uiso 0.512(7) 1 calc R U P A 2 H95C H 0.329175 -0.024795 0.110122 0.205 Uiso 0.512(7) 1 calc R U P A 2 C96 C 0.1232(13) -0.0013(13) -0.0385(13) 0.154(5) Uani 0.512(7) 1 d D U P A 2 H96 H 0.133874 -0.036559 -0.085324 0.185 Uiso 0.512(7) 1 calc R U P A 2 C97 C 0.2522(18) 0.2088(10) -0.0570(12) 0.146(6) Uani 0.512(7) 1 d D U P A 2 H97A H 0.208407 0.240843 -0.043982 0.219 Uiso 0.512(7) 1 calc R U P A 2 H97B H 0.261998 0.215384 -0.103391 0.219 Uiso 0.512(7) 1 calc R U P A 2 H97C H 0.308137 0.226850 -0.013603 0.219 Uiso 0.512(7) 1 calc R U P A 2 C98 C 0.3854(17) 0.0054(17) 0.0099(13) 0.185(8) Uani 0.512(7) 1 d D U P A 2 H98A H 0.359858 -0.049563 -0.024895 0.278 Uiso 0.512(7) 1 calc R U P A 2 H98B H 0.434182 0.004486 0.054626 0.278 Uiso 0.512(7) 1 calc R U P A 2 H98C H 0.407827 0.036099 -0.017892 0.278 Uiso 0.512(7) 1 calc R U P A 2 C99 C 0.124(2) -0.0549(16) 0.0108(16) 0.203(9) Uani 0.512(7) 1 d D U P A 2 H99A H 0.160348 -0.095328 -0.000646 0.305 Uiso 0.512(7) 1 calc R U P A 2 H99B H 0.062809 -0.081609 -0.001010 0.305 Uiso 0.512(7) 1 calc R U P A 2 H99C H 0.147545 -0.022458 0.065852 0.305 Uiso 0.512(7) 1 calc R U P A 2 C100 C 0.0294(17) 0.0143(18) -0.0709(16) 0.200(9) Uani 0.512(7) 1 d D U P A 2 H10A H -0.011980 -0.036856 -0.096476 0.300 Uiso 0.512(7) 1 calc R U P A 2 H10B H 0.027997 0.042071 -0.108496 0.300 Uiso 0.512(7) 1 calc R U P A 2 H10C H 0.012155 0.047509 -0.028363 0.300 Uiso 0.512(7) 1 calc R U P A 2 C101 C 0.3141(13) 0.0445(14) 0.0380(12) 0.154(4) Uani 0.512(7) 1 d D U P A 2 H101 H 0.352552 0.098523 0.065598 0.184 Uiso 0.512(7) 1 calc R U P A 2 C102 C 0.158(2) 0.0819(14) -0.1567(9) 0.200(9) Uani 0.512(7) 1 d D U P A 2 H10D H 0.171732 0.028934 -0.178080 0.300 Uiso 0.512(7) 1 calc R U P A 2 H10E H 0.167281 0.115437 -0.187304 0.300 Uiso 0.512(7) 1 calc R U P A 2 H10F H 0.095974 0.076247 -0.158547 0.300 Uiso 0.512(7) 1 calc R U P A 2 C103 C 0.2182(14) 0.1209(10) -0.0728(8) 0.143(4) Uani 0.512(7) 1 d D U P A 2 H103 H 0.272531 0.100937 -0.080675 0.171 Uiso 0.512(7) 1 calc R U P A 2 C104 C 0.3312(14) 0.6189(9) -0.0947(8) 0.218(7) Uani 1 1 d . U . . . H10G H 0.278345 0.635722 -0.122475 0.327 Uiso 1 1 calc R U . . . H10H H 0.348702 0.577552 -0.131700 0.327 Uiso 1 1 calc R U . . . H10I H 0.379696 0.665019 -0.067945 0.327 Uiso 1 1 calc R U . . . Si5 Si 0.2365(10) 0.0931(8) 0.0106(8) 0.122(3) Uani 0.488(7) 1 d D U P A 1 C105 C 0.3428(17) 0.0834(19) 0.1542(10) 0.166(8) Uani 0.488(7) 1 d D U P A 1 H10J H 0.401955 0.115830 0.183122 0.249 Uiso 0.488(7) 1 calc R U P A 1 H10K H 0.337156 0.036152 0.170295 0.249 Uiso 0.488(7) 1 calc R U P A 1 H10L H 0.297923 0.115219 0.164782 0.249 Uiso 0.488(7) 1 calc R U P A 1 C106 C 0.1625(13) 0.0087(11) -0.0666(12) 0.143(4) Uani 0.488(7) 1 d D U P A 1 H106 H 0.198220 -0.004532 -0.102222 0.171 Uiso 0.488(7) 1 calc R U P A 1 C107 C 0.315(2) 0.2442(10) -0.0114(15) 0.167(8) Uani 0.488(7) 1 d D U P A 1 H10M H 0.270945 0.271160 0.007648 0.250 Uiso 0.488(7) 1 calc R U P A 1 H10N H 0.317392 0.256400 -0.057645 0.250 Uiso 0.488(7) 1 calc R U P A 1 H10O H 0.373251 0.262974 0.029029 0.250 Uiso 0.488(7) 1 calc R U P A 1 C108 C 0.4142(13) 0.088(2) 0.0551(15) 0.202(8) Uani 0.488(7) 1 d D U P A 1 H10P H 0.398870 0.095839 0.004602 0.304 Uiso 0.488(7) 1 calc R U P A 1 H10Q H 0.453768 0.048343 0.056468 0.304 Uiso 0.488(7) 1 calc R U P A 1 H10R H 0.444036 0.138540 0.096243 0.304 Uiso 0.488(7) 1 calc R U P A 1 C109 C 0.125(2) -0.0753(12) -0.0711(18) 0.179(8) Uani 0.488(7) 1 d D U P A 1 H10S H 0.168194 -0.092255 -0.032990 0.269 Uiso 0.488(7) 1 d R U P A 1 H10T H 0.114374 -0.113085 -0.123230 0.269 Uiso 0.488(7) 1 d R U P A 1 H10U H 0.069784 -0.074035 -0.059600 0.269 Uiso 0.488(7) 1 d R U P A 1 C110 C 0.089(2) 0.0426(15) -0.1132(16) 0.175(7) Uani 0.488(7) 1 d D U P A 1 H11A H 0.045762 0.052881 -0.086346 0.263 Uiso 0.488(7) 1 d R U P A 1 H11B H 0.060312 0.004021 -0.165456 0.263 Uiso 0.488(7) 1 d R U P A 1 H11C H 0.114572 0.092811 -0.116956 0.263 Uiso 0.488(7) 1 d R U P A 1 C111 C 0.3294(13) 0.0567(14) 0.0676(10) 0.155(5) Uani 0.488(7) 1 d D U P A 1 H111 H 0.317882 -0.003117 0.047018 0.187 Uiso 0.488(7) 1 calc R U P A 1 C112 C 0.309(2) 0.1097(13) -0.1051(13) 0.164(7) Uani 0.488(7) 1 d D U P A 1 H11D H 0.359436 0.082984 -0.091322 0.247 Uiso 0.488(7) 1 calc R U P A 1 H11E H 0.322967 0.147964 -0.129790 0.247 Uiso 0.488(7) 1 calc R U P A 1 H11F H 0.256887 0.069709 -0.141140 0.247 Uiso 0.488(7) 1 calc R U P A 1 C113 C 0.2891(16) 0.1542(11) -0.0318(11) 0.143(5) Uani 0.488(7) 1 d D U P A 1 H113 H 0.349084 0.151514 0.001456 0.171 Uiso 0.488(7) 1 calc R U P A 1 C114 C 0.4973(11) 0.6114(9) 0.5135(10) 0.107(2) Uani 0.356(7) 1 d D U P B 2 H11G H 0.465347 0.558201 0.476015 0.128 Uiso 0.356(7) 1 calc R U P B 2 H11H H 0.544523 0.601681 0.554911 0.128 Uiso 0.356(7) 1 calc R U P B 2 C115 C 0.4788(10) 0.6267(12) 0.3903(5) 0.115(3) Uani 0.356(7) 1 d D U P B 2 H11I H 0.456582 0.569297 0.378496 0.138 Uiso 0.356(7) 1 calc R U P B 2 H11J H 0.428235 0.654115 0.394824 0.138 Uiso 0.356(7) 1 calc R U P B 2 C116 C 0.4332(17) 0.6500(18) 0.5498(17) 0.071(3) Uani 0.356(7) 1 d D U P B 2 H11K H 0.376295 0.617225 0.513792 0.106 Uiso 0.356(7) 1 d R U P B 2 H11L H 0.433645 0.705755 0.551652 0.106 Uiso 0.356(7) 1 d R U P B 2 H11M H 0.441365 0.646805 0.601712 0.106 Uiso 0.356(7) 1 d R U P B 2 C117 C 0.6303(6) 0.6316(10) 0.4725(11) 0.100(2) Uani 0.356(7) 1 d D U P B 2 H11N H 0.664859 0.638750 0.527005 0.120 Uiso 0.356(7) 1 calc R U P B 2 H11O H 0.660496 0.672100 0.457563 0.120 Uiso 0.356(7) 1 calc R U P B 2 C118 C 0.616(2) 0.7860(9) 0.5861(11) 0.091(4) Uani 0.356(7) 1 d D U P B 2 H11P H 0.672774 0.766868 0.590577 0.136 Uiso 0.356(7) 1 calc R U P B 2 H11Q H 0.593583 0.776704 0.625780 0.136 Uiso 0.356(7) 1 calc R U P B 2 H11R H 0.625534 0.843373 0.593479 0.136 Uiso 0.356(7) 1 calc R U P B 2 C119 C 0.5510(12) 0.7416(5) 0.5074(9) 0.109(3) Uani 0.356(7) 1 d D U P B 2 H11S H 0.564927 0.766172 0.470882 0.131 Uiso 0.356(7) 1 calc R U P B 2 H11T H 0.491908 0.752472 0.509175 0.131 Uiso 0.356(7) 1 calc R U P B 2 C120 C 0.5242(11) 0.6871(11) 0.3664(10) 0.118(4) Uani 0.644(7) 1 d D U P B 1 H12A H 0.502450 0.637459 0.322003 0.177 Uiso 0.644(7) 1 d R U P B 1 H12B H 0.589020 0.695929 0.386893 0.177 Uiso 0.644(7) 1 d R U P B 1 H12C H 0.505340 0.732159 0.349853 0.177 Uiso 0.644(7) 1 d R U P B 1 C121 C 0.6386(17) 0.5502(15) 0.423(3) 0.069(4) Uani 0.356(7) 1 d D U P B 2 H12D H 0.619882 0.547731 0.369019 0.104 Uiso 0.356(7) 1 d R U P B 2 H12E H 0.609102 0.501951 0.427529 0.104 Uiso 0.356(7) 1 d R U P B 2 H12F H 0.702912 0.553361 0.442569 0.104 Uiso 0.356(7) 1 d R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn01 0.0626(6) 0.0572(6) 0.0453(5) 0.0181(4) 0.0135(4) 0.0077(4) Cl1 0.0613(11) 0.0985(15) 0.0731(12) 0.0353(11) 0.0101(9) 0.0117(10) Si1 0.0800(14) 0.0650(12) 0.0534(11) 0.0257(9) 0.0160(10) 0.0118(10) Si2 0.0970(16) 0.0644(13) 0.0571(12) 0.0073(10) 0.0151(11) 0.0083(11) Si3 0.1139(19) 0.0930(17) 0.0546(12) 0.0213(11) 0.0294(12) -0.0200(14) Si4 0.180(6) 0.114(4) 0.076(3) 0.030(3) 0.064(4) 0.073(4) C1 0.051(4) 0.066(4) 0.047(4) 0.032(4) 0.006(3) -0.016(4) N1 0.062(3) 0.049(3) 0.045(3) 0.018(2) 0.015(2) 0.005(2) N2 0.061(3) 0.061(3) 0.043(3) 0.017(3) 0.010(2) 0.012(3) N3 0.062(3) 0.058(3) 0.043(3) 0.015(3) 0.012(2) 0.002(3) N4 0.060(3) 0.056(3) 0.044(3) 0.013(2) 0.013(2) 0.012(3) C2 0.063(4) 0.048(4) 0.052(4) 0.016(3) 0.017(3) 0.012(3) C3 0.065(4) 0.060(4) 0.043(3) 0.014(3) 0.016(3) 0.017(3) C4 0.059(4) 0.061(4) 0.046(3) 0.019(3) 0.012(3) 0.013(3) C5 0.058(4) 0.060(4) 0.042(3) 0.018(3) 0.014(3) 0.007(3) C6 0.060(4) 0.053(4) 0.049(3) 0.015(3) 0.013(3) 0.007(3) C7 0.065(4) 0.053(4) 0.052(4) 0.019(3) 0.016(3) 0.010(3) C8 0.068(4) 0.055(4) 0.047(3) 0.017(3) 0.014(3) 0.008(3) C9 0.063(4) 0.052(4) 0.048(3) 0.020(3) 0.010(3) 0.000(3) C10 0.055(4) 0.048(4) 0.044(3) 0.015(3) 0.011(3) 0.005(3) C11 0.061(4) 0.048(4) 0.054(4) 0.020(3) 0.014(3) 0.007(3) C12 0.068(4) 0.059(4) 0.050(4) 0.021(3) 0.016(3) 0.009(3) C13 0.064(4) 0.055(4) 0.052(4) 0.020(3) 0.018(3) 0.015(3) C14 0.058(4) 0.067(4) 0.046(3) 0.020(3) 0.014(3) 0.012(3) C15 0.058(4) 0.063(4) 0.048(4) 0.020(3) 0.012(3) 0.009(3) C16 0.060(4) 0.054(4) 0.046(3) 0.015(3) 0.013(3) 0.005(3) C17 0.073(4) 0.050(4) 0.045(3) 0.017(3) 0.013(3) 0.006(3) C18 0.078(5) 0.060(4) 0.047(4) 0.019(3) 0.017(3) 0.007(4) C19 0.067(4) 0.058(4) 0.048(4) 0.020(3) 0.012(3) 0.006(3) C20 0.068(4) 0.055(4) 0.049(4) 0.019(3) 0.013(3) 0.013(3) C21 0.075(5) 0.052(4) 0.049(4) 0.014(3) 0.015(3) 0.009(3) C22 0.064(4) 0.056(4) 0.048(4) 0.019(3) 0.013(3) 0.008(3) C23 0.057(4) 0.063(4) 0.043(3) 0.018(3) 0.013(3) 0.011(3) C24 0.079(5) 0.063(5) 0.048(4) 0.017(3) 0.013(3) 0.011(4) C25 0.062(4) 0.058(4) 0.048(3) 0.023(3) 0.015(3) 0.007(3) C26 0.070(4) 0.063(4) 0.046(4) 0.018(3) 0.015(3) 0.011(3) C27 0.069(4) 0.058(4) 0.052(4) 0.018(3) 0.017(3) 0.009(3) C28 0.082(5) 0.059(4) 0.055(4) 0.022(3) 0.022(4) 0.008(4) C29 0.060(4) 0.060(4) 0.047(3) 0.022(3) 0.018(3) 0.009(3) C30 0.068(4) 0.048(4) 0.050(4) 0.019(3) 0.014(3) 0.000(3) C31 0.070(4) 0.059(4) 0.055(4) 0.022(3) 0.011(3) 0.002(3) C32 0.077(5) 0.054(4) 0.053(4) 0.021(3) 0.010(3) 0.002(3) C33 0.076(5) 0.070(5) 0.048(4) 0.023(3) 0.014(3) 0.015(4) C34 0.071(5) 0.085(6) 0.053(4) 0.021(4) 0.019(3) 0.022(4) C35 0.062(4) 0.073(5) 0.054(4) 0.027(4) 0.016(3) 0.012(4) C36 0.088(5) 0.055(4) 0.049(4) 0.017(3) 0.015(4) 0.011(4) C37 0.087(5) 0.060(5) 0.057(4) 0.021(3) 0.020(4) 0.000(4) C38 0.078(5) 0.067(5) 0.056(4) 0.018(4) 0.021(4) 0.018(4) C39 0.078(5) 0.053(4) 0.055(4) 0.016(3) 0.017(3) 0.012(3) C40 0.079(5) 0.052(4) 0.051(4) 0.016(3) 0.018(3) 0.005(3) C41 0.082(5) 0.061(4) 0.045(4) 0.014(3) 0.019(3) 0.002(4) C42 0.088(5) 0.068(5) 0.047(4) 0.018(3) 0.008(4) 0.009(4) C43 0.089(5) 0.053(4) 0.048(4) 0.016(3) 0.022(3) 0.011(4) C44 0.076(5) 0.077(5) 0.046(4) 0.025(4) 0.018(3) 0.017(4) C45 0.088(5) 0.063(5) 0.055(4) 0.027(4) 0.027(4) 0.021(4) C46 0.084(5) 0.089(6) 0.052(4) 0.020(4) 0.018(4) 0.018(4) C47 0.102(6) 0.071(5) 0.057(4) 0.017(4) 0.025(4) -0.015(4) C48 0.095(6) 0.060(5) 0.058(4) 0.019(4) 0.019(4) 0.005(4) C49 0.091(6) 0.066(5) 0.061(4) 0.026(4) 0.022(4) 0.008(4) C50 0.104(6) 0.060(5) 0.048(4) 0.009(3) 0.021(4) -0.009(4) C51 0.095(6) 0.057(5) 0.067(5) 0.018(4) 0.018(4) -0.006(4) C52 0.126(7) 0.060(5) 0.049(4) 0.019(3) 0.018(4) 0.005(4) C53 0.065(5) 0.057(5) 0.112(6) 0.049(4) 0.042(5) 0.019(4) C54 0.108(6) 0.061(5) 0.059(4) 0.017(4) 0.028(4) 0.011(4) C55 0.086(6) 0.078(6) 0.080(5) 0.025(4) 0.024(4) 0.005(4) N5 0.093(3) 0.103(3) 0.111(3) 0.036(3) 0.006(3) -0.001(3) C56 0.091(6) 0.073(5) 0.052(4) 0.019(4) 0.022(4) -0.002(4) C57 0.121(7) 0.050(4) 0.070(5) 0.020(4) 0.032(5) 0.001(4) C58 0.119(7) 0.077(5) 0.059(4) 0.030(4) 0.038(5) 0.043(5) C59 0.107(6) 0.074(5) 0.046(4) 0.015(4) 0.004(4) -0.001(5) C60 0.084(6) 0.074(5) 0.088(6) 0.024(5) 0.014(5) 0.001(4) C61 0.123(7) 0.051(5) 0.079(5) 0.023(4) 0.037(5) 0.005(4) C62 0.089(6) 0.071(5) 0.074(5) 0.036(4) 0.018(4) 0.014(4) C63 0.133(8) 0.054(5) 0.072(5) 0.017(4) 0.036(5) 0.012(5) C64 0.113(7) 0.121(8) 0.052(4) 0.034(5) 0.024(4) 0.018(6) C65 0.104(7) 0.096(7) 0.094(6) 0.040(5) 0.035(5) 0.031(5) C66 0.152(9) 0.059(5) 0.070(5) 0.011(4) 0.039(6) -0.012(5) C67 0.169(10) 0.074(6) 0.090(7) 0.017(5) 0.051(7) -0.025(6) C68 0.111(6) 0.062(4) 0.097(5) 0.008(4) 0.005(5) 0.012(4) C69 0.153(10) 0.094(7) 0.087(7) 0.004(6) 0.039(7) -0.033(7) C70 0.204(12) 0.065(6) 0.090(7) 0.014(5) 0.063(8) -0.037(7) C71 0.155(9) 0.097(7) 0.080(6) 0.047(5) 0.021(6) 0.036(7) C72 0.119(6) 0.087(6) 0.122(6) -0.019(5) 0.020(5) -0.005(5) C73 0.131(6) 0.100(5) 0.067(4) 0.018(4) 0.027(4) 0.033(5) C74 0.212(13) 0.077(7) 0.093(7) 0.017(6) 0.063(8) -0.040(7) C75 0.115(8) 0.085(7) 0.146(9) -0.026(6) 0.000(7) 0.002(6) C76 0.169(10) 0.138(9) 0.097(7) 0.055(7) 0.033(7) 0.054(8) C77 0.167(7) 0.115(6) 0.082(5) 0.039(5) 0.037(5) 0.003(6) C78 0.133(9) 0.147(9) 0.085(6) 0.041(6) 0.023(6) 0.017(7) C79 0.097(7) 0.091(7) 0.173(10) 0.008(7) 0.019(7) 0.023(6) C80 0.176(10) 0.081(7) 0.133(9) 0.033(6) -0.014(8) 0.031(7) C81 0.088(3) 0.096(3) 0.100(4) 0.033(3) 0.006(3) -0.004(3) C82 0.155(7) 0.139(7) 0.095(6) 0.031(5) 0.039(5) -0.049(6) C83 0.188(7) 0.125(7) 0.090(5) 0.021(5) 0.052(6) -0.018(6) C84 0.229(12) 0.146(10) 0.068(6) 0.019(6) 0.030(7) 0.044(9) C85 0.102(4) 0.099(4) 0.106(4) 0.029(4) 0.004(4) -0.006(4) C86 0.189(12) 0.154(11) 0.132(10) 0.009(9) 0.029(9) 0.059(9) C87 0.199(12) 0.161(11) 0.142(10) 0.048(8) 0.063(9) -0.063(9) C88 0.274(14) 0.120(9) 0.127(9) 0.030(8) 0.080(10) 0.041(10) C89 0.100(4) 0.110(4) 0.124(4) 0.026(4) 0.008(4) 0.002(4) C90 0.161(11) 0.133(10) 0.205(12) -0.038(9) 0.098(10) -0.035(9) C91 0.066(5) 0.063(5) 0.063(5) 0.046(4) -0.007(4) -0.013(4) C92 0.087(4) 0.101(4) 0.114(4) 0.034(4) 0.013(3) 0.000(3) C93 0.090(6) 0.115(7) 0.108(7) 0.035(6) 0.032(6) -0.004(6) C94 0.167(12) 0.254(15) 0.133(10) 0.078(10) -0.012(9) -0.066(11) C95 0.166(11) 0.141(12) 0.117(11) 0.023(10) 0.071(10) 0.087(10) C96 0.196(8) 0.140(7) 0.109(7) 0.009(6) 0.049(7) 0.060(7) C97 0.200(13) 0.150(12) 0.106(11) 0.033(10) 0.082(10) 0.046(11) C98 0.189(12) 0.166(12) 0.147(12) -0.014(11) 0.028(11) 0.091(11) C99 0.237(16) 0.153(14) 0.156(14) 0.003(13) 0.024(14) 0.022(14) C100 0.216(16) 0.184(14) 0.141(14) 0.007(13) 0.022(14) 0.034(14) C101 0.186(7) 0.148(6) 0.115(6) 0.016(6) 0.049(6) 0.068(6) C102 0.238(15) 0.188(14) 0.142(13) 0.040(13) 0.034(13) 0.034(14) C103 0.196(7) 0.145(6) 0.095(6) 0.026(6) 0.066(6) 0.054(6) C104 0.346(16) 0.172(12) 0.125(10) 0.009(9) 0.128(11) -0.052(12) Si5 0.174(6) 0.122(4) 0.081(4) 0.022(3) 0.062(4) 0.071(4) C105 0.177(14) 0.165(15) 0.125(13) 0.014(12) 0.027(13) 0.077(13) C106 0.188(8) 0.134(6) 0.100(6) 0.013(6) 0.055(6) 0.065(6) C107 0.223(16) 0.168(14) 0.110(13) 0.025(12) 0.078(12) 0.030(14) C108 0.207(13) 0.186(13) 0.163(12) 0.008(12) 0.034(12) 0.045(12) C109 0.222(13) 0.144(12) 0.151(12) 0.043(11) 0.040(12) 0.021(12) C110 0.210(12) 0.168(11) 0.121(11) 0.017(10) 0.040(11) 0.053(11) C111 0.182(8) 0.155(7) 0.113(7) 0.010(7) 0.049(7) 0.073(7) C112 0.213(14) 0.168(13) 0.120(12) 0.019(11) 0.094(11) 0.033(13) C113 0.195(9) 0.144(8) 0.097(7) 0.019(7) 0.076(7) 0.050(7) C114 0.095(4) 0.097(4) 0.103(4) 0.033(3) 0.004(3) -0.009(3) C115 0.097(4) 0.106(4) 0.116(4) 0.029(4) 0.010(4) -0.002(4) C116 0.079(4) 0.070(4) 0.067(4) 0.039(3) 0.017(3) -0.006(3) C117 0.084(4) 0.097(4) 0.101(4) 0.035(4) 0.008(3) -0.004(3) C118 0.074(6) 0.084(6) 0.116(7) 0.032(6) 0.033(6) 0.014(6) C119 0.089(4) 0.104(4) 0.117(4) 0.034(4) 0.013(4) 0.004(4) C120 0.094(6) 0.117(6) 0.134(6) 0.021(6) 0.054(5) -0.023(6) C121 0.069(6) 0.065(5) 0.065(6) 0.041(5) -0.005(5) -0.011(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3281 0.5435 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2153 0.2529 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn -2.7473 0.5279 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Zn01 Cl1 106.23(15) . . ? N1 Zn01 N2 88.8(2) . . ? N1 Zn01 N3 88.5(2) . . ? N1 Zn01 N4 153.0(2) . . ? N2 Zn01 Cl1 97.44(16) . . ? N2 Zn01 N3 164.7(2) . . ? N3 Zn01 Cl1 97.78(16) . . ? N4 Zn01 Cl1 100.78(16) . . ? N4 Zn01 N2 87.9(2) . . ? N4 Zn01 N3 87.7(2) . . ? C39 Si1 C46 106.1(3) . . ? C39 Si1 C49 107.2(3) . . ? C39 Si1 C62 108.6(4) . . ? C46 Si1 C62 110.0(4) . . ? C49 Si1 C46 110.5(4) . . ? C49 Si1 C62 114.2(4) . . ? C48 Si2 C68 107.7(4) . . ? C48 Si2 C72 107.3(4) . . ? C48 Si2 C73 105.4(4) . . ? C68 Si2 C72 108.5(5) . . ? C68 Si2 C73 111.0(5) . . ? C73 Si2 C72 116.4(6) . . ? C56 Si3 C77 105.1(5) . . ? C56 Si3 C82 107.7(4) . . ? C82 Si3 C77 103.9(6) . . ? C83 Si3 C56 109.6(5) . . ? C83 Si3 C77 108.4(6) . . ? C83 Si3 C82 121.0(6) . . ? C58 Si4 C96 105.0(10) . . ? C101 Si4 C58 115.6(10) . . ? C101 Si4 C96 107.1(9) . . ? C103 Si4 C58 107.7(9) . . ? C103 Si4 C96 106.9(8) . . ? C103 Si4 C101 113.9(9) . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C81 C1 H1A 105.7 . . ? C81 C1 H1B 102.8 . . ? C81 C1 H1C 119.5 . . ? C6 N1 Zn01 125.6(4) . . ? C10 N1 Zn01 125.9(4) . . ? C10 N1 C6 108.3(5) . . ? C2 N2 Zn01 124.9(4) . . ? C2 N2 C11 108.4(5) . . ? C11 N2 Zn01 124.4(4) . . ? C9 N3 Zn01 122.8(4) . . ? C19 N3 Zn01 124.2(4) . . ? C19 N3 C9 108.7(5) . . ? C3 N4 Zn01 126.0(4) . . ? C3 N4 C29 107.8(5) . . ? C29 N4 Zn01 126.1(4) . . ? N2 C2 C13 123.8(6) . . ? N2 C2 C20 110.6(6) . . ? C13 C2 C20 125.3(6) . . ? N4 C3 C8 109.8(6) . . ? N4 C3 C13 124.5(6) . . ? C13 C3 C8 125.6(6) . . ? C5 C4 C10 106.1(6) . . ? C12 C4 C5 119.9(6) . . ? C12 C4 C10 133.8(6) . . ? C4 C5 C6 105.8(6) . . ? C21 C5 C4 120.5(6) . . ? C21 C5 C6 133.5(6) . . ? N1 C6 C5 109.7(6) . . ? N1 C6 C17 125.0(6) . . ? C17 C6 C5 125.1(6) . . ? C20 C7 C11 106.5(6) . . ? C28 C7 C11 133.8(6) . . ? C28 C7 C20 119.6(6) . . ? C23 C8 C3 105.7(5) . . ? C36 C8 C3 132.6(6) . . ? C36 C8 C23 121.2(6) . . ? N3 C9 C25 123.1(6) . . ? N3 C9 C31 109.6(6) . . ? C25 C9 C31 126.9(6) . . ? N1 C10 C4 109.8(5) . . ? N1 C10 C16 125.1(6) . . ? C16 C10 C4 124.9(6) . . ? N2 C11 C7 109.2(6) . . ? N2 C11 C16 123.5(6) . . ? C16 C11 C7 127.3(6) . . ? C4 C12 H12 120.2 . . ? C4 C12 C15 119.5(6) . . ? C15 C12 H12 120.2 . . ? C2 C13 C3 125.5(6) . . ? C2 C13 C45 119.6(6) . . ? C3 C13 C45 114.7(6) . . ? C15 C14 C38 119.2(6) . . ? C21 C14 C15 119.1(6) . . ? C21 C14 C38 121.7(7) . . ? C12 C15 C14 120.8(6) . . ? C12 C15 C35 121.9(7) . . ? C14 C15 C35 117.3(6) . . ? C10 C16 C11 127.3(6) . . ? C10 C16 C22 116.1(6) . . ? C11 C16 C22 116.5(6) . . ? C6 C17 C18 115.2(6) . . ? C19 C17 C6 127.1(6) . . ? C19 C17 C18 117.6(6) . . ? C48 C18 C17 174.9(8) . . ? N3 C19 C17 123.8(6) . . ? N3 C19 C30 110.5(6) . . ? C17 C19 C30 125.6(6) . . ? C7 C20 C2 105.2(6) . . ? C43 C20 C2 133.9(6) . . ? C43 C20 C7 120.9(6) . . ? C5 C21 C14 120.0(6) . . ? C5 C21 H21 120.0 . . ? C14 C21 H21 120.0 . . ? C39 C22 C16 174.7(7) . . ? C8 C23 C29 106.9(5) . . ? C27 C23 C8 120.4(6) . . ? C27 C23 C29 132.2(6) . . ? C36 C24 C26 119.4(6) . . ? C36 C24 C52 122.1(7) . . ? C52 C24 C26 118.3(6) . . ? C9 C25 C41 118.1(6) . . ? C29 C25 C9 126.9(6) . . ? C29 C25 C41 115.0(6) . . ? C27 C26 C24 120.0(6) . . ? C27 C26 C33 121.9(7) . . ? C33 C26 C24 118.1(6) . . ? C23 C27 C26 119.5(6) . . ? C23 C27 H27 120.3 . . ? C26 C27 H27 120.3 . . ? C7 C28 H28 120.2 . . ? C7 C28 C32 119.6(7) . . ? C32 C28 H28 120.2 . . ? N4 C29 C23 109.1(6) . . ? N4 C29 C25 123.4(6) . . ? C25 C29 C23 127.3(6) . . ? C31 C30 C19 104.8(6) . . ? C37 C30 C19 134.7(6) . . ? C37 C30 C31 120.5(6) . . ? C30 C31 C9 106.2(6) . . ? C50 C31 C9 133.8(7) . . ? C50 C31 C30 120.0(6) . . ? C28 C32 C40 120.7(6) . . ? C28 C32 C57 121.0(7) . . ? C40 C32 C57 118.3(7) . . ? C26 C33 H33 119.1 . . ? C42 C33 C26 121.8(7) . . ? C42 C33 H33 119.1 . . ? C38 C34 H34 119.5 . . ? C38 C34 C44 120.9(7) . . ? C44 C34 H34 119.5 . . ? C15 C35 H35 119.1 . . ? C44 C35 C15 121.7(7) . . ? C44 C35 H35 119.1 . . ? C8 C36 C24 119.5(7) . . ? C8 C36 H36 120.2 . . ? C24 C36 H36 120.2 . . ? C30 C37 H37 119.8 . . ? C30 C37 C51 120.5(7) . . ? C51 C37 H37 119.8 . . ? C14 C38 H38 119.9 . . ? C34 C38 C14 120.2(7) . . ? C34 C38 H38 119.9 . . ? C22 C39 Si1 173.3(6) . . ? C32 C40 C43 118.8(6) . . ? C32 C40 C54 118.8(6) . . ? C43 C40 C54 122.3(7) . . ? C56 C41 C25 176.3(9) . . ? C33 C42 H42 120.2 . . ? C33 C42 C59 119.7(7) . . ? C59 C42 H42 120.2 . . ? C20 C43 C40 120.2(6) . . ? C20 C43 H43 119.9 . . ? C40 C43 H43 119.9 . . ? C34 C44 H44 119.8 . . ? C35 C44 C34 120.4(7) . . ? C35 C44 H44 119.8 . . ? C58 C45 C13 174.7(9) . . ? Si1 C46 H46 105.9 . . ? C64 C46 Si1 114.7(6) . . ? C64 C46 H46 105.9 . . ? C69 C46 Si1 113.3(6) . . ? C69 C46 H46 105.9 . . ? C69 C46 C64 110.5(7) . . ? C50 C47 C51 119.7(7) . . ? C50 C47 C67 123.1(8) . . ? C67 C47 C51 117.1(8) . . ? C18 C48 Si2 175.0(7) . . ? Si1 C49 H49 107.1 . . ? C55 C49 Si1 111.9(5) . . ? C55 C49 H49 107.1 . . ? C55 C49 C60 109.2(7) . . ? C60 C49 Si1 114.2(6) . . ? C60 C49 H49 107.1 . . ? C31 C50 C47 120.3(7) . . ? C31 C50 H50 119.8 . . ? C47 C50 H50 119.8 . . ? C37 C51 C47 118.9(7) . . ? C66 C51 C37 121.7(8) . . ? C66 C51 C47 119.3(7) . . ? C24 C52 H52 119.3 . . ? C59 C52 C24 121.4(7) . . ? C59 C52 H52 119.3 . . ? H53A C53 H53B 109.5 . . ? H53A C53 H53C 109.5 . . ? H53B C53 H53C 109.5 . . ? C92 C53 H53A 109.5 . . ? C92 C53 H53B 109.5 . . ? C92 C53 H53C 109.5 . . ? C40 C54 H54 119.3 . . ? C63 C54 C40 121.4(8) . . ? C63 C54 H54 119.3 . . ? C49 C55 H55A 109.5 . . ? C49 C55 H55B 109.5 . . ? C49 C55 H55C 109.5 . . ? H55A C55 H55B 109.5 . . ? H55A C55 H55C 109.5 . . ? H55B C55 H55C 109.5 . . ? C81 N5 C85 100.6(6) . . ? C89 N5 C81 114.7(7) . . ? C89 N5 C85 107.7(6) . . ? C89 N5 C92 118.4(7) . . ? C92 N5 C81 112.3(5) . . ? C92 N5 C85 100.3(6) . . ? C115 N5 C114 104.8(8) . . ? C115 N5 C119 108.6(8) . . ? C117 N5 C114 114.0(8) . . ? C117 N5 C115 110.5(8) . . ? C117 N5 C119 109.8(7) . . ? C119 N5 C114 109.0(8) . . ? C41 C56 Si3 179.6(8) . . ? C32 C57 H57 119.7 . . ? C61 C57 C32 120.7(8) . . ? C61 C57 H57 119.7 . . ? C45 C58 Si4 177.4(10) . . ? C45 C58 Si5 167.5(10) . . ? C42 C59 H59 119.6 . . ? C52 C59 C42 120.7(7) . . ? C52 C59 H59 119.6 . . ? C49 C60 H60A 109.5 . . ? C49 C60 H60B 109.5 . . ? C49 C60 H60C 109.5 . . ? H60A C60 H60B 109.5 . . ? H60A C60 H60C 109.5 . . ? H60B C60 H60C 109.5 . . ? C57 C61 H61 120.1 . . ? C57 C61 C63 119.7(8) . . ? C63 C61 H61 120.1 . . ? Si1 C62 H62 105.9 . . ? C65 C62 Si1 115.2(6) . . ? C65 C62 H62 105.9 . . ? C65 C62 C71 110.5(7) . . ? C71 C62 Si1 112.6(7) . . ? C71 C62 H62 105.9 . . ? C54 C63 C61 121.0(8) . . ? C54 C63 H63 119.5 . . ? C61 C63 H63 119.5 . . ? C46 C64 H64A 109.5 . . ? C46 C64 H64B 109.5 . . ? C46 C64 H64C 109.5 . . ? H64A C64 H64B 109.5 . . ? H64A C64 H64C 109.5 . . ? H64B C64 H64C 109.5 . . ? C62 C65 H65A 109.5 . . ? C62 C65 H65B 109.5 . . ? C62 C65 H65C 109.5 . . ? H65A C65 H65B 109.5 . . ? H65A C65 H65C 109.5 . . ? H65B C65 H65C 109.5 . . ? C51 C66 H66 119.6 . . ? C70 C66 C51 120.9(8) . . ? C70 C66 H66 119.6 . . ? C47 C67 H67 118.8 . . ? C74 C67 C47 122.4(9) . . ? C74 C67 H67 118.8 . . ? Si2 C68 H68 107.1 . . ? C79 C68 Si2 114.8(7) . . ? C79 C68 H68 107.1 . . ? C79 C68 C80 110.1(10) . . ? C80 C68 Si2 110.3(8) . . ? C80 C68 H68 107.1 . . ? C46 C69 H69A 109.5 . . ? C46 C69 H69B 109.5 . . ? C46 C69 H69C 109.5 . . ? H69A C69 H69B 109.5 . . ? H69A C69 H69C 109.5 . . ? H69B C69 H69C 109.5 . . ? C66 C70 H70 119.7 . . ? C66 C70 C74 120.5(9) . . ? C74 C70 H70 119.7 . . ? C62 C71 H71A 109.5 . . ? C62 C71 H71B 109.5 . . ? C62 C71 H71C 109.5 . . ? H71A C71 H71B 109.5 . . ? H71A C71 H71C 109.5 . . ? H71B C71 H71C 109.5 . . ? Si2 C72 H72 101.1 . . ? C75 C72 Si2 115.3(9) . . ? C75 C72 H72 101.1 . . ? C90 C72 Si2 119.0(9) . . ? C90 C72 H72 101.1 . . ? C90 C72 C75 114.8(10) . . ? Si2 C73 H73 105.0 . . ? C76 C73 Si2 115.8(7) . . ? C76 C73 H73 105.0 . . ? C76 C73 C84 111.3(9) . . ? C84 C73 Si2 113.5(8) . . ? C84 C73 H73 105.0 . . ? C67 C74 C70 119.8(9) . . ? C67 C74 H74 120.1 . . ? C70 C74 H74 120.1 . . ? C72 C75 H75A 109.5 . . ? C72 C75 H75B 109.5 . . ? C72 C75 H75C 109.5 . . ? H75A C75 H75B 109.5 . . ? H75A C75 H75C 109.5 . . ? H75B C75 H75C 109.5 . . ? C73 C76 H76A 109.5 . . ? C73 C76 H76B 109.5 . . ? C73 C76 H76C 109.5 . . ? H76A C76 H76B 109.5 . . ? H76A C76 H76C 109.5 . . ? H76B C76 H76C 109.5 . . ? Si3 C77 H77 107.8 . . ? C78 C77 Si3 107.1(8) . . ? C78 C77 H77 107.8 . . ? C88 C77 Si3 110.8(9) . . ? C88 C77 H77 107.8 . . ? C88 C77 C78 115.2(12) . . ? C77 C78 H78A 109.5 . . ? C77 C78 H78B 109.5 . . ? C77 C78 H78C 109.5 . . ? H78A C78 H78B 109.5 . . ? H78A C78 H78C 109.5 . . ? H78B C78 H78C 109.5 . . ? C68 C79 H79A 109.5 . . ? C68 C79 H79B 109.5 . . ? C68 C79 H79C 109.5 . . ? H79A C79 H79B 109.5 . . ? H79A C79 H79C 109.5 . . ? H79B C79 H79C 109.5 . . ? C68 C80 H80A 109.5 . . ? C68 C80 H80B 109.5 . . ? C68 C80 H80C 109.5 . . ? H80A C80 H80B 109.5 . . ? H80A C80 H80C 109.5 . . ? H80B C80 H80C 109.5 . . ? C1 C81 N5 124.1(6) . . ? C1 C81 H81A 106.3 . . ? C1 C81 H81B 106.3 . . ? N5 C81 H81A 106.3 . . ? N5 C81 H81B 106.3 . . ? H81A C81 H81B 106.4 . . ? Si3 C82 H82 107.6 . . ? C87 C82 Si3 115.3(8) . . ? C87 C82 H82 107.6 . . ? C87 C82 C94 110.6(12) . . ? C94 C82 Si3 107.9(8) . . ? C94 C82 H82 107.6 . . ? Si3 C83 H83 104.4 . . ? C86 C83 Si3 112.9(9) . . ? C86 C83 H83 104.4 . . ? C86 C83 C104 118.6(14) . . ? C104 C83 Si3 110.5(9) . . ? C104 C83 H83 104.4 . . ? C73 C84 H84A 109.5 . . ? C73 C84 H84B 109.5 . . ? C73 C84 H84C 109.5 . . ? H84A C84 H84B 109.5 . . ? H84A C84 H84C 109.5 . . ? H84B C84 H84C 109.5 . . ? N5 C85 H85A 106.2 . . ? N5 C85 H85B 106.2 . . ? H85A C85 H85B 106.4 . . ? C91 C85 N5 124.6(6) . . ? C91 C85 H85A 106.2 . . ? C91 C85 H85B 106.2 . . ? C83 C86 H86A 109.5 . . ? C83 C86 H86B 109.5 . . ? C83 C86 H86C 109.5 . . ? H86A C86 H86B 109.5 . . ? H86A C86 H86C 109.5 . . ? H86B C86 H86C 109.5 . . ? C82 C87 H87A 109.5 . . ? C82 C87 H87B 109.5 . . ? C82 C87 H87C 109.5 . . ? H87A C87 H87B 109.5 . . ? H87A C87 H87C 109.5 . . ? H87B C87 H87C 109.5 . . ? C77 C88 H88A 109.5 . . ? C77 C88 H88B 109.5 . . ? C77 C88 H88C 109.5 . . ? H88A C88 H88B 109.5 . . ? H88A C88 H88C 109.5 . . ? H88B C88 H88C 109.5 . . ? N5 C89 H89A 112.2 . . ? N5 C89 H89B 112.2 . . ? H89A C89 H89B 109.8 . . ? C120 C89 N5 97.9(11) . . ? C120 C89 H89A 112.2 . . ? C120 C89 H89B 112.2 . . ? C72 C90 H90A 109.5 . . ? C72 C90 H90B 109.5 . . ? C72 C90 H90C 109.5 . . ? H90A C90 H90B 109.5 . . ? H90A C90 H90C 109.5 . . ? H90B C90 H90C 109.5 . . ? C85 C91 H91A 109.5 . . ? C85 C91 H91B 109.5 . . ? C85 C91 H91C 109.5 . . ? H91A C91 H91B 109.5 . . ? H91A C91 H91C 109.5 . . ? H91B C91 H91C 109.5 . . ? C53 C92 H92A 107.7 . . ? C53 C92 H92B 107.7 . . ? N5 C92 C53 118.6(8) . . ? N5 C92 H92A 107.7 . . ? N5 C92 H92B 107.7 . . ? H92A C92 H92B 107.1 . . ? H93A C93 H93B 109.5 . . ? H93A C93 H93C 109.5 . . ? H93B C93 H93C 109.4 . . ? C115 C93 H93A 103.8 . . ? C115 C93 H93B 107.4 . . ? C115 C93 H93C 117.1 . . ? C82 C94 H94A 109.5 . . ? C82 C94 H94B 109.4 . . ? C82 C94 H94C 109.5 . . ? H94A C94 H94B 109.5 . . ? H94A C94 H94C 109.5 . . ? H94B C94 H94C 109.5 . . ? H95A C95 H95B 109.5 . . ? H95A C95 H95C 109.5 . . ? H95B C95 H95C 109.5 . . ? C101 C95 H95A 109.5 . . ? C101 C95 H95B 109.5 . . ? C101 C95 H95C 109.5 . . ? Si4 C96 H96 103.5 . . ? C99 C96 Si4 115.0(16) . . ? C99 C96 H96 103.5 . . ? C99 C96 C100 110.0(5) . . ? C100 C96 Si4 119.2(17) . . ? C100 C96 H96 103.5 . . ? H97A C97 H97B 109.5 . . ? H97A C97 H97C 109.5 . . ? H97B C97 H97C 109.5 . . ? C103 C97 H97A 109.5 . . ? C103 C97 H97B 109.5 . . ? C103 C97 H97C 109.5 . . ? H98A C98 H98B 109.5 . . ? H98A C98 H98C 109.5 . . ? H98B C98 H98C 109.5 . . ? C101 C98 H98A 109.5 . . ? C101 C98 H98B 109.5 . . ? C101 C98 H98C 109.5 . . ? C96 C99 H99A 109.5 . . ? C96 C99 H99B 109.5 . . ? C96 C99 H99C 109.5 . . ? H99A C99 H99B 109.5 . . ? H99A C99 H99C 109.5 . . ? H99B C99 H99C 109.5 . . ? C96 C100 H10A 109.5 . . ? C96 C100 H10B 109.5 . . ? C96 C100 H10C 109.5 . . ? H10A C100 H10B 109.5 . . ? H10A C100 H10C 109.5 . . ? H10B C100 H10C 109.5 . . ? Si4 C101 H101 94.4 . . ? C95 C101 Si4 109.6(13) . . ? C95 C101 H101 94.4 . . ? C98 C101 Si4 139.7(14) . . ? C98 C101 C95 108.8(5) . . ? C98 C101 H101 94.4 . . ? H10D C102 H10E 109.5 . . ? H10D C102 H10F 109.5 . . ? H10E C102 H10F 109.5 . . ? C103 C102 H10D 109.5 . . ? C103 C102 H10E 109.5 . . ? C103 C102 H10F 109.5 . . ? Si4 C103 H103 96.3 . . ? C97 C103 Si4 122.2(9) . . ? C97 C103 C102 110.4(5) . . ? C97 C103 H103 96.3 . . ? C102 C103 Si4 123.8(9) . . ? C102 C103 H103 96.3 . . ? C83 C104 H10G 109.5 . . ? C83 C104 H10H 109.5 . . ? C83 C104 H10I 109.5 . . ? H10G C104 H10H 109.5 . . ? H10G C104 H10I 109.5 . . ? H10H C104 H10I 109.5 . . ? C58 Si5 C111 110.2(10) . . ? C106 Si5 C58 117.0(11) . . ? C106 Si5 C111 108.8(8) . . ? C106 Si5 C113 108.5(9) . . ? C113 Si5 C58 107.4(9) . . ? C113 Si5 C111 104.1(9) . . ? H10J C105 H10K 109.5 . . ? H10J C105 H10L 109.5 . . ? H10K C105 H10L 109.5 . . ? C111 C105 H10J 109.5 . . ? C111 C105 H10K 109.5 . . ? C111 C105 H10L 109.5 . . ? Si5 C106 H106 100.6 . . ? C109 C106 Si5 133.4(17) . . ? C109 C106 H106 100.6 . . ? C109 C106 C110 109.6(5) . . ? C110 C106 Si5 106.4(15) . . ? C110 C106 H106 100.6 . . ? H10M C107 H10N 109.5 . . ? H10M C107 H10O 109.5 . . ? H10N C107 H10O 109.5 . . ? C113 C107 H10M 109.5 . . ? C113 C107 H10N 109.5 . . ? C113 C107 H10O 109.5 . . ? H10P C108 H10Q 109.5 . . ? H10P C108 H10R 109.5 . . ? H10Q C108 H10R 109.5 . . ? C111 C108 H10P 109.5 . . ? C111 C108 H10Q 109.5 . . ? C111 C108 H10R 109.5 . . ? C106 C109 H10S 109.4 . . ? C106 C109 H10T 110.0 . . ? C106 C109 H10U 109.1 . . ? H10S C109 H10T 109.5 . . ? H10S C109 H10U 109.5 . . ? H10T C109 H10U 109.5 . . ? C106 C110 H11A 108.4 . . ? C106 C110 H11B 110.1 . . ? C106 C110 H11C 109.9 . . ? H11A C110 H11B 109.5 . . ? H11A C110 H11C 109.5 . . ? H11B C110 H11C 109.5 . . ? Si5 C111 H111 108.6 . . ? C105 C111 Si5 113.9(15) . . ? C105 C111 C108 109.4(5) . . ? C105 C111 H111 108.6 . . ? C108 C111 Si5 107.8(14) . . ? C108 C111 H111 108.5 . . ? H11D C112 H11E 109.5 . . ? H11D C112 H11F 109.5 . . ? H11E C112 H11F 109.5 . . ? C113 C112 H11D 109.5 . . ? C113 C112 H11E 109.5 . . ? C113 C112 H11F 109.5 . . ? Si5 C113 H113 90.9 . . ? C107 C113 Si5 132.9(13) . . ? C107 C113 C112 110.4(5) . . ? C107 C113 H113 90.9 . . ? C112 C113 Si5 116.6(13) . . ? C112 C113 H113 90.9 . . ? N5 C114 H11G 107.3 . . ? N5 C114 H11H 107.3 . . ? H11G C114 H11H 106.9 . . ? C116 C114 N5 120.3(6) . . ? C116 C114 H11G 107.3 . . ? C116 C114 H11H 107.3 . . ? N5 C115 H11I 104.2 . . ? N5 C115 H11J 104.2 . . ? C93 C115 N5 132.3(12) . . ? C93 C115 H11I 104.2 . . ? C93 C115 H11J 104.2 . . ? H11I C115 H11J 105.5 . . ? C114 C116 H11K 101.7 . . ? C114 C116 H11L 113.0 . . ? C114 C116 H11M 113.5 . . ? H11K C116 H11L 109.5 . . ? H11K C116 H11M 109.4 . . ? H11L C116 H11M 109.5 . . ? N5 C117 H11N 107.1 . . ? N5 C117 H11O 107.0 . . ? N5 C117 C121 121.1(6) . . ? H11N C117 H11O 106.8 . . ? C121 C117 H11N 107.0 . . ? C121 C117 H11O 107.1 . . ? H11P C118 H11Q 109.5 . . ? H11P C118 H11R 109.5 . . ? H11Q C118 H11R 109.5 . . ? C119 C118 H11P 109.5 . . ? C119 C118 H11Q 109.5 . . ? C119 C118 H11R 109.5 . . ? N5 C119 H11S 107.1 . . ? N5 C119 H11T 107.1 . . ? C118 C119 N5 120.9(6) . . ? C118 C119 H11S 107.1 . . ? C118 C119 H11T 107.1 . . ? H11S C119 H11T 106.8 . . ? C89 C120 H12A 103.5 . . ? C89 C120 H12B 119.1 . . ? C89 C120 H12C 105.5 . . ? H12A C120 H12B 109.5 . . ? H12A C120 H12C 109.5 . . ? H12B C120 H12C 109.5 . . ? C117 C121 H12D 108.5 . . ? C117 C121 H12E 119.1 . . ? C117 C121 H12F 100.3 . . ? H12D C121 H12E 109.5 . . ? H12D C121 H12F 109.5 . . ? H12E C121 H12F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn01 Cl1 2.335(2) . ? Zn01 N1 2.072(5) . ? Zn01 N2 2.118(6) . ? Zn01 N3 2.137(6) . ? Zn01 N4 2.084(5) . ? Si1 C39 1.831(7) . ? Si1 C46 1.877(8) . ? Si1 C49 1.875(8) . ? Si1 C62 1.886(8) . ? Si2 C48 1.832(8) . ? Si2 C68 1.853(10) . ? Si2 C72 1.874(12) . ? Si2 C73 1.854(10) . ? Si3 C56 1.819(8) . ? Si3 C77 1.963(13) . ? Si3 C82 1.839(11) . ? Si3 C83 1.806(12) . ? Si4 C58 1.831(12) . ? Si4 C96 1.842(16) . ? Si4 C101 1.778(15) . ? Si4 C103 1.756(16) . ? C1 H1A 0.9798 . ? C1 H1B 0.9801 . ? C1 H1C 0.9799 . ? C1 C81 1.493(5) . ? N1 C6 1.377(8) . ? N1 C10 1.375(8) . ? N2 C2 1.351(8) . ? N2 C11 1.384(8) . ? N3 C9 1.375(8) . ? N3 C19 1.344(8) . ? N4 C3 1.364(8) . ? N4 C29 1.385(8) . ? C2 C13 1.412(9) . ? C2 C20 1.457(9) . ? C3 C8 1.463(8) . ? C3 C13 1.418(9) . ? C4 C5 1.428(9) . ? C4 C10 1.459(9) . ? C4 C12 1.379(9) . ? C5 C6 1.464(9) . ? C5 C21 1.367(9) . ? C6 C17 1.409(9) . ? C7 C11 1.450(9) . ? C7 C20 1.422(9) . ? C7 C28 1.385(9) . ? C8 C23 1.403(9) . ? C8 C36 1.370(9) . ? C9 C25 1.402(9) . ? C9 C31 1.455(9) . ? C10 C16 1.397(9) . ? C11 C16 1.409(9) . ? C12 H12 0.9500 . ? C12 C15 1.390(9) . ? C13 C45 1.426(10) . ? C14 C15 1.415(9) . ? C14 C21 1.406(9) . ? C14 C38 1.420(9) . ? C15 C35 1.428(9) . ? C16 C22 1.440(9) . ? C17 C18 1.438(9) . ? C17 C19 1.409(9) . ? C18 C48 1.213(9) . ? C19 C30 1.474(9) . ? C20 C43 1.361(9) . ? C21 H21 0.9500 . ? C22 C39 1.219(9) . ? C23 C27 1.391(9) . ? C23 C29 1.449(8) . ? C24 C26 1.429(10) . ? C24 C36 1.409(9) . ? C24 C52 1.415(10) . ? C25 C29 1.402(9) . ? C25 C41 1.454(9) . ? C26 C27 1.394(9) . ? C26 C33 1.413(9) . ? C27 H27 0.9500 . ? C28 H28 0.9500 . ? C28 C32 1.397(10) . ? C30 C31 1.425(9) . ? C30 C37 1.360(9) . ? C31 C50 1.378(10) . ? C32 C40 1.411(10) . ? C32 C57 1.424(10) . ? C33 H33 0.9500 . ? C33 C42 1.358(9) . ? C34 H34 0.9500 . ? C34 C38 1.368(10) . ? C34 C44 1.376(10) . ? C35 H35 0.9500 . ? C35 C44 1.353(10) . ? C36 H36 0.9500 . ? C37 H37 0.9500 . ? C37 C51 1.418(10) . ? C38 H38 0.9500 . ? C40 C43 1.413(9) . ? C40 C54 1.415(10) . ? C41 C56 1.209(10) . ? C42 H42 0.9500 . ? C42 C59 1.405(10) . ? C43 H43 0.9500 . ? C44 H44 0.9500 . ? C45 C58 1.195(10) . ? C46 H46 1.0000 . ? C46 C64 1.530(10) . ? C46 C69 1.523(12) . ? C47 C50 1.400(10) . ? C47 C51 1.423(11) . ? C47 C67 1.413(11) . ? C49 H49 1.0000 . ? C49 C55 1.510(11) . ? C49 C60 1.523(11) . ? C50 H50 0.9500 . ? C51 C66 1.412(11) . ? C52 H52 0.9500 . ? C52 C59 1.350(10) . ? C53 H53A 0.9800 . ? C53 H53B 0.9800 . ? C53 H53C 0.9800 . ? C53 C92 1.512(5) . ? C54 H54 0.9500 . ? C54 C63 1.337(10) . ? C55 H55A 0.9800 . ? C55 H55B 0.9800 . ? C55 H55C 0.9800 . ? N5 C81 1.506(5) . ? N5 C85 1.522(5) . ? N5 C89 1.476(5) . ? N5 C92 1.493(5) . ? N5 C114 1.507(5) . ? N5 C115 1.501(5) . ? N5 C117 1.490(5) . ? N5 C119 1.503(5) . ? C57 H57 0.9500 . ? C57 C61 1.373(11) . ? C58 Si5 1.826(13) . ? C59 H59 0.9500 . ? C60 H60A 0.9800 . ? C60 H60B 0.9800 . ? C60 H60C 0.9800 . ? C61 H61 0.9500 . ? C61 C63 1.399(11) . ? C62 H62 1.0000 . ? C62 C65 1.525(12) . ? C62 C71 1.528(11) . ? C63 H63 0.9500 . ? C64 H64A 0.9800 . ? C64 H64B 0.9800 . ? C64 H64C 0.9800 . ? C65 H65A 0.9800 . ? C65 H65B 0.9800 . ? C65 H65C 0.9800 . ? C66 H66 0.9500 . ? C66 C70 1.360(11) . ? C67 H67 0.9500 . ? C67 C74 1.360(12) . ? C68 H68 1.0000 . ? C68 C79 1.518(14) . ? C68 C80 1.539(14) . ? C69 H69A 0.9800 . ? C69 H69B 0.9800 . ? C69 H69C 0.9800 . ? C70 H70 0.9500 . ? C70 C74 1.392(13) . ? C71 H71A 0.9800 . ? C71 H71B 0.9800 . ? C71 H71C 0.9800 . ? C72 H72 1.0000 . ? C72 C75 1.519(13) . ? C72 C90 1.439(16) . ? C73 H73 1.0000 . ? C73 C76 1.492(14) . ? C73 C84 1.530(13) . ? C74 H74 0.9500 . ? C75 H75A 0.9800 . ? C75 H75B 0.9800 . ? C75 H75C 0.9800 . ? C76 H76A 0.9800 . ? C76 H76B 0.9800 . ? C76 H76C 0.9800 . ? C77 H77 1.0000 . ? C77 C78 1.546(15) . ? C77 C88 1.525(15) . ? C78 H78A 0.9800 . ? C78 H78B 0.9800 . ? C78 H78C 0.9800 . ? C79 H79A 0.9800 . ? C79 H79B 0.9800 . ? C79 H79C 0.9800 . ? C80 H80A 0.9800 . ? C80 H80B 0.9800 . ? C80 H80C 0.9800 . ? C81 H81A 0.9900 . ? C81 H81B 0.9900 . ? C82 H82 1.0000 . ? C82 C87 1.533(5) . ? C82 C94 1.538(5) . ? C83 H83 1.0000 . ? C83 C86 1.587(18) . ? C83 C104 1.590(16) . ? C84 H84A 0.9800 . ? C84 H84B 0.9800 . ? C84 H84C 0.9800 . ? C85 H85A 0.9900 . ? C85 H85B 0.9900 . ? C85 C91 1.477(5) . ? C86 H86A 0.9800 . ? C86 H86B 0.9800 . ? C86 H86C 0.9800 . ? C87 H87A 0.9800 . ? C87 H87B 0.9800 . ? C87 H87C 0.9800 . ? C88 H88A 0.9800 . ? C88 H88B 0.9800 . ? C88 H88C 0.9800 . ? C89 H89A 0.9900 . ? C89 H89B 0.9900 . ? C89 C120 1.468(14) . ? C90 H90A 0.9800 . ? C90 H90B 0.9800 . ? C90 H90C 0.9800 . ? C91 H91A 0.9800 . ? C91 H91B 0.9800 . ? C91 H91C 0.9800 . ? C92 H92A 0.9900 . ? C92 H92B 0.9900 . ? C93 H93A 0.9801 . ? C93 H93B 0.9801 . ? C93 H93C 0.9799 . ? C93 C115 1.492(5) . ? C94 H94A 0.9800 . ? C94 H94B 0.9799 . ? C94 H94C 0.9795 . ? C95 H95A 0.9800 . ? C95 H95B 0.9800 . ? C95 H95C 0.9800 . ? C95 C101 1.533(5) . ? C96 H96 1.0000 . ? C96 C99 1.522(5) . ? C96 C100 1.531(5) . ? C97 H97A 0.9800 . ? C97 H97B 0.9800 . ? C97 H97C 0.9800 . ? C97 C103 1.523(5) . ? C98 H98A 0.9800 . ? C98 H98B 0.9800 . ? C98 H98C 0.9800 . ? C98 C101 1.531(5) . ? C99 H99A 0.9800 . ? C99 H99B 0.9800 . ? C99 H99C 0.9800 . ? C100 H10A 0.9800 . ? C100 H10B 0.9800 . ? C100 H10C 0.9800 . ? C101 H101 1.0000 . ? C102 H10D 0.9800 . ? C102 H10E 0.9800 . ? C102 H10F 0.9800 . ? C102 C103 1.525(5) . ? C103 H103 1.0000 . ? C104 H10G 0.9800 . ? C104 H10H 0.9800 . ? C104 H10I 0.9800 . ? Si5 C106 1.799(17) . ? Si5 C111 1.854(18) . ? Si5 C113 1.819(17) . ? C105 H10J 0.9800 . ? C105 H10K 0.9800 . ? C105 H10L 0.9800 . ? C105 C111 1.525(5) . ? C106 H106 1.0000 . ? C106 C109 1.530(5) . ? C106 C110 1.531(5) . ? C107 H10M 0.9800 . ? C107 H10N 0.9800 . ? C107 H10O 0.9800 . ? C107 C113 1.521(5) . ? C108 H10P 0.9800 . ? C108 H10Q 0.9800 . ? C108 H10R 0.9800 . ? C108 C111 1.536(5) . ? C109 H10S 0.9799 . ? C109 H10T 0.9801 . ? C109 H10U 0.9801 . ? C110 H11A 0.9798 . ? C110 H11B 0.9801 . ? C110 H11C 0.9802 . ? C111 H111 1.0000 . ? C112 H11D 0.9800 . ? C112 H11E 0.9800 . ? C112 H11F 0.9800 . ? C112 C113 1.528(5) . ? C113 H113 1.0000 . ? C114 H11G 0.9900 . ? C114 H11H 0.9900 . ? C114 C116 1.502(5) . ? C115 H11I 0.9900 . ? C115 H11J 0.9900 . ? C116 H11K 0.9801 . ? C116 H11L 0.9799 . ? C116 H11M 0.9799 . ? C117 H11N 0.9900 . ? C117 H11O 0.9900 . ? C117 C121 1.515(4) . ? C118 H11P 0.9800 . ? C118 H11Q 0.9800 . ? C118 H11R 0.9800 . ? C118 C119 1.496(5) . ? C119 H11S 0.9900 . ? C119 H11T 0.9900 . ? C120 H12A 0.9796 . ? C120 H12B 0.9801 . ? C120 H12C 0.9800 . ? C121 H12D 0.9802 . ? C121 H12E 0.9799 . ? C121 H12F 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Zn01 N1 C6 C5 179.1(4) . . . . ? Zn01 N1 C6 C17 -5.7(9) . . . . ? Zn01 N1 C10 C4 -178.9(4) . . . . ? Zn01 N1 C10 C16 5.1(9) . . . . ? Zn01 N2 C2 C13 -25.0(9) . . . . ? Zn01 N2 C2 C20 160.6(4) . . . . ? Zn01 N2 C11 C7 -162.6(4) . . . . ? Zn01 N2 C11 C16 18.4(9) . . . . ? Zn01 N3 C9 C25 31.2(9) . . . . ? Zn01 N3 C9 C31 -155.3(5) . . . . ? Zn01 N3 C19 C17 -23.9(9) . . . . ? Zn01 N3 C19 C30 155.8(4) . . . . ? Zn01 N4 C3 C8 168.2(4) . . . . ? Zn01 N4 C3 C13 -15.6(9) . . . . ? Zn01 N4 C29 C23 -167.7(4) . . . . ? Zn01 N4 C29 C25 16.8(9) . . . . ? N1 C6 C17 C18 -160.2(6) . . . . ? N1 C6 C17 C19 15.5(11) . . . . ? N1 C10 C16 C11 -17.5(11) . . . . ? N1 C10 C16 C22 157.7(6) . . . . ? N2 C2 C13 C3 -1.3(11) . . . . ? N2 C2 C13 C45 173.2(6) . . . . ? N2 C2 C20 C7 3.6(8) . . . . ? N2 C2 C20 C43 -177.9(8) . . . . ? N2 C11 C16 C10 4.3(11) . . . . ? N2 C11 C16 C22 -170.8(6) . . . . ? N3 C9 C25 C29 -2.5(11) . . . . ? N3 C9 C25 C41 178.3(6) . . . . ? N3 C9 C31 C30 -2.3(8) . . . . ? N3 C9 C31 C50 175.4(8) . . . . ? N3 C19 C30 C31 0.1(8) . . . . ? N3 C19 C30 C37 -179.2(8) . . . . ? N4 C3 C8 C23 4.5(8) . . . . ? N4 C3 C8 C36 -167.5(8) . . . . ? N4 C3 C13 C2 23.5(11) . . . . ? N4 C3 C13 C45 -151.3(7) . . . . ? C2 N2 C11 C7 1.0(7) . . . . ? C2 N2 C11 C16 -178.0(6) . . . . ? C2 C20 C43 C40 -179.2(7) . . . . ? C3 N4 C29 C23 8.5(7) . . . . ? C3 N4 C29 C25 -167.0(6) . . . . ? C3 C8 C23 C27 -172.2(6) . . . . ? C3 C8 C23 C29 0.8(7) . . . . ? C3 C8 C36 C24 170.8(7) . . . . ? C4 C5 C6 N1 3.3(7) . . . . ? C4 C5 C6 C17 -171.9(6) . . . . ? C4 C5 C21 C14 3.7(10) . . . . ? C4 C10 C16 C11 167.1(6) . . . . ? C4 C10 C16 C22 -17.7(9) . . . . ? C4 C12 C15 C14 4.3(10) . . . . ? C4 C12 C15 C35 -178.0(6) . . . . ? C5 C4 C10 N1 -4.0(7) . . . . ? C5 C4 C10 C16 172.1(6) . . . . ? C5 C4 C12 C15 -3.6(9) . . . . ? C5 C6 C17 C18 14.3(10) . . . . ? C5 C6 C17 C19 -170.0(7) . . . . ? C6 N1 C10 C4 6.1(7) . . . . ? C6 N1 C10 C16 -170.0(6) . . . . ? C6 C5 C21 C14 177.6(7) . . . . ? C6 C17 C19 N3 1.0(12) . . . . ? C6 C17 C19 C30 -178.6(7) . . . . ? C7 C11 C16 C10 -174.4(6) . . . . ? C7 C11 C16 C22 10.4(10) . . . . ? C7 C20 C43 C40 -0.8(11) . . . . ? C7 C28 C32 C40 0.9(11) . . . . ? C7 C28 C32 C57 179.4(7) . . . . ? C8 C3 C13 C2 -160.9(7) . . . . ? C8 C3 C13 C45 24.4(10) . . . . ? C8 C23 C27 C26 0.3(11) . . . . ? C8 C23 C29 N4 -5.7(8) . . . . ? C8 C23 C29 C25 169.6(7) . . . . ? C9 N3 C19 C17 178.7(6) . . . . ? C9 N3 C19 C30 -1.6(8) . . . . ? C9 C25 C29 N4 -23.9(11) . . . . ? C9 C25 C29 C23 161.4(7) . . . . ? C9 C31 C50 C47 -176.6(8) . . . . ? C10 N1 C6 C5 -5.8(7) . . . . ? C10 N1 C6 C17 169.4(6) . . . . ? C10 C4 C5 C6 0.4(7) . . . . ? C10 C4 C5 C21 175.8(6) . . . . ? C10 C4 C12 C15 -178.5(7) . . . . ? C11 N2 C2 C13 171.6(6) . . . . ? C11 N2 C2 C20 -2.8(7) . . . . ? C11 C7 C20 C2 -2.8(7) . . . . ? C11 C7 C20 C43 178.4(6) . . . . ? C11 C7 C28 C32 -178.9(7) . . . . ? C12 C4 C5 C6 -175.8(6) . . . . ? C12 C4 C5 C21 -0.4(9) . . . . ? C12 C4 C10 N1 171.5(7) . . . . ? C12 C4 C10 C16 -12.4(11) . . . . ? C12 C15 C35 C44 178.6(7) . . . . ? C13 C2 C20 C7 -170.7(6) . . . . ? C13 C2 C20 C43 7.8(13) . . . . ? C13 C3 C8 C23 -171.7(7) . . . . ? C13 C3 C8 C36 16.3(13) . . . . ? C14 C15 C35 C44 -3.6(10) . . . . ? C15 C14 C21 C5 -3.0(10) . . . . ? C15 C14 C38 C34 2.9(10) . . . . ? C15 C35 C44 C34 3.1(11) . . . . ? C17 C19 C30 C31 179.8(7) . . . . ? C17 C19 C30 C37 0.5(13) . . . . ? C18 C17 C19 N3 176.6(6) . . . . ? C18 C17 C19 C30 -3.0(11) . . . . ? C19 N3 C9 C25 -171.1(6) . . . . ? C19 N3 C9 C31 2.4(8) . . . . ? C19 C30 C31 C9 1.3(7) . . . . ? C19 C30 C31 C50 -176.8(7) . . . . ? C19 C30 C37 C51 176.8(8) . . . . ? C20 C2 C13 C3 172.3(7) . . . . ? C20 C2 C13 C45 -13.2(11) . . . . ? C20 C7 C11 N2 1.2(7) . . . . ? C20 C7 C11 C16 -179.8(6) . . . . ? C20 C7 C28 C32 2.8(11) . . . . ? C21 C5 C6 N1 -171.3(7) . . . . ? C21 C5 C6 C17 13.6(12) . . . . ? C21 C14 C15 C12 -1.0(10) . . . . ? C21 C14 C15 C35 -178.8(6) . . . . ? C21 C14 C38 C34 -177.7(7) . . . . ? C23 C8 C36 C24 -0.3(11) . . . . ? C24 C26 C27 C23 -2.3(11) . . . . ? C24 C26 C33 C42 1.9(11) . . . . ? C24 C52 C59 C42 0.3(14) . . . . ? C25 C9 C31 C30 170.9(7) . . . . ? C25 C9 C31 C50 -11.4(14) . . . . ? C26 C24 C36 C8 -1.7(12) . . . . ? C26 C24 C52 C59 0.0(13) . . . . ? C26 C33 C42 C59 -1.5(12) . . . . ? C27 C23 C29 N4 166.1(7) . . . . ? C27 C23 C29 C25 -18.7(12) . . . . ? C27 C26 C33 C42 -177.5(7) . . . . ? C28 C7 C11 N2 -177.2(7) . . . . ? C28 C7 C11 C16 1.7(13) . . . . ? C28 C7 C20 C2 176.0(6) . . . . ? C28 C7 C20 C43 -2.9(10) . . . . ? C28 C32 C40 C43 -4.5(11) . . . . ? C28 C32 C40 C54 177.2(7) . . . . ? C28 C32 C57 C61 -177.5(8) . . . . ? C29 N4 C3 C8 -8.1(7) . . . . ? C29 N4 C3 C13 168.2(6) . . . . ? C29 C23 C27 C26 -170.5(7) . . . . ? C30 C31 C50 C47 0.9(12) . . . . ? C30 C37 C51 C47 -1.2(12) . . . . ? C30 C37 C51 C66 -177.9(8) . . . . ? C31 C9 C25 C29 -174.9(7) . . . . ? C31 C9 C25 C41 6.0(11) . . . . ? C31 C30 C37 C51 -2.4(12) . . . . ? C32 C40 C43 C20 4.4(11) . . . . ? C32 C40 C54 C63 0.1(12) . . . . ? C32 C57 C61 C63 0.5(14) . . . . ? C33 C26 C27 C23 177.0(7) . . . . ? C33 C42 C59 C52 0.4(14) . . . . ? C36 C8 C23 C27 1.0(11) . . . . ? C36 C8 C23 C29 173.9(7) . . . . ? C36 C24 C26 C27 3.0(11) . . . . ? C36 C24 C26 C33 -176.4(7) . . . . ? C36 C24 C52 C59 175.2(9) . . . . ? C37 C30 C31 C9 -179.3(7) . . . . ? C37 C30 C31 C50 2.6(11) . . . . ? C37 C51 C66 C70 178.5(10) . . . . ? C38 C14 C15 C12 178.4(6) . . . . ? C38 C14 C15 C35 0.6(9) . . . . ? C38 C14 C21 C5 177.6(6) . . . . ? C38 C34 C44 C35 0.5(11) . . . . ? C39 Si1 C46 C64 177.1(6) . . . . ? C39 Si1 C46 C69 -54.8(8) . . . . ? C39 Si1 C49 C55 -57.7(6) . . . . ? C39 Si1 C49 C60 67.0(6) . . . . ? C39 Si1 C62 C65 -40.8(7) . . . . ? C39 Si1 C62 C71 -168.7(6) . . . . ? C40 C32 C57 C61 1.0(12) . . . . ? C40 C54 C63 C61 1.5(14) . . . . ? C41 C25 C29 N4 155.3(6) . . . . ? C41 C25 C29 C23 -19.4(10) . . . . ? C43 C40 C54 C63 -178.1(8) . . . . ? C44 C34 C38 C14 -3.5(11) . . . . ? C45 C58 Si5 C106 -176(4) . . . . ? C45 C58 Si5 C111 59(4) . . . . ? C45 C58 Si5 C113 -54(4) . . . . ? C46 Si1 C49 C55 57.5(6) . . . . ? C46 Si1 C49 C60 -177.8(6) . . . . ? C46 Si1 C62 C65 -156.5(6) . . . . ? C46 Si1 C62 C71 75.6(7) . . . . ? C47 C51 C66 C70 1.8(16) . . . . ? C47 C67 C74 C70 -1(2) . . . . ? C48 Si2 C68 C79 68.4(9) . . . . ? C48 Si2 C68 C80 -56.7(8) . . . . ? C48 Si2 C72 C75 169.9(9) . . . . ? C48 Si2 C72 C90 -47.7(13) . . . . ? C48 Si2 C73 C76 48.6(10) . . . . ? C48 Si2 C73 C84 179.1(9) . . . . ? C49 Si1 C46 C64 61.3(7) . . . . ? C49 Si1 C46 C69 -170.7(7) . . . . ? C49 Si1 C62 C65 78.7(7) . . . . ? C49 Si1 C62 C71 -49.2(7) . . . . ? C50 C47 C51 C37 4.6(13) . . . . ? C50 C47 C51 C66 -178.6(9) . . . . ? C50 C47 C67 C74 178.0(11) . . . . ? C51 C47 C50 C31 -4.5(13) . . . . ? C51 C47 C67 C74 1.1(17) . . . . ? C51 C66 C70 C74 -1.4(19) . . . . ? C52 C24 C26 C27 178.3(7) . . . . ? C52 C24 C26 C33 -1.1(11) . . . . ? C52 C24 C36 C8 -176.8(8) . . . . ? C54 C40 C43 C20 -177.4(7) . . . . ? C56 Si3 C82 C87 -165.8(10) . . . . ? C56 Si3 C82 C94 70.1(9) . . . . ? C56 Si3 C83 C86 -52.5(12) . . . . ? C56 Si3 C83 C104 172.0(10) . . . . ? C57 C32 C40 C43 177.0(7) . . . . ? C57 C32 C40 C54 -1.3(11) . . . . ? C57 C61 C63 C54 -1.8(14) . . . . ? C58 Si4 C96 C99 -79.8(19) . . . . ? C58 Si4 C96 C100 54.0(19) . . . . ? C58 Si4 C101 C95 43(2) . . . . ? C58 Si4 C101 C98 -155(3) . . . . ? C58 Si4 C103 C97 37(2) . . . . ? C58 Si4 C103 C102 -119(2) . . . . ? C58 Si5 C106 C109 -83(3) . . . . ? C58 Si5 C106 C110 56(2) . . . . ? C58 Si5 C111 C105 4.0(17) . . . . ? C58 Si5 C111 C108 -117.5(16) . . . . ? C58 Si5 C113 C107 15(3) . . . . ? C58 Si5 C113 C112 -162(2) . . . . ? C62 Si1 C46 C64 -65.7(7) . . . . ? C62 Si1 C46 C69 62.4(8) . . . . ? C62 Si1 C49 C55 -177.9(5) . . . . ? C62 Si1 C49 C60 -53.3(7) . . . . ? C66 C70 C74 C67 1(2) . . . . ? C67 C47 C50 C31 178.7(9) . . . . ? C67 C47 C51 C37 -178.4(9) . . . . ? C67 C47 C51 C66 -1.6(14) . . . . ? C68 Si2 C72 C75 53.7(11) . . . . ? C68 Si2 C72 C90 -163.8(12) . . . . ? C68 Si2 C73 C76 165.0(8) . . . . ? C68 Si2 C73 C84 -64.5(10) . . . . ? C72 Si2 C68 C79 -175.7(8) . . . . ? C72 Si2 C68 C80 59.2(8) . . . . ? C72 Si2 C73 C76 -70.2(10) . . . . ? C72 Si2 C73 C84 60.3(10) . . . . ? C73 Si2 C68 C79 -46.5(9) . . . . ? C73 Si2 C68 C80 -171.6(7) . . . . ? C73 Si2 C72 C75 -72.4(11) . . . . ? C73 Si2 C72 C90 70.1(13) . . . . ? C77 Si3 C82 C87 -54.7(12) . . . . ? C77 Si3 C82 C94 -178.8(8) . . . . ? C77 Si3 C83 C86 -166.6(10) . . . . ? C77 Si3 C83 C104 57.9(12) . . . . ? C81 N5 C85 C91 -129.7(12) . . . . ? C81 N5 C89 C120 -70.7(12) . . . . ? C81 N5 C92 C53 -178.5(11) . . . . ? C82 Si3 C83 C86 73.7(11) . . . . ? C82 Si3 C83 C104 -61.8(13) . . . . ? C83 Si3 C82 C87 67.1(13) . . . . ? C83 Si3 C82 C94 -57.0(10) . . . . ? C85 N5 C81 C1 -138.0(15) . . . . ? C85 N5 C89 C120 178.3(10) . . . . ? C85 N5 C92 C53 -72.4(12) . . . . ? C89 N5 C81 C1 106.8(17) . . . . ? C89 N5 C85 C91 -9.3(15) . . . . ? C89 N5 C92 C53 44.3(14) . . . . ? C92 N5 C81 C1 -32.2(17) . . . . ? C92 N5 C85 C91 115.1(13) . . . . ? C92 N5 C89 C120 65.7(12) . . . . ? C96 Si4 C101 C95 -73(2) . . . . ? C96 Si4 C101 C98 89(3) . . . . ? C96 Si4 C103 C97 149.7(19) . . . . ? C96 Si4 C103 C102 -7(3) . . . . ? C101 Si4 C96 C99 44(2) . . . . ? C101 Si4 C96 C100 177.3(17) . . . . ? C101 Si4 C103 C97 -92(2) . . . . ? C101 Si4 C103 C102 111(2) . . . . ? C103 Si4 C96 C99 166.0(18) . . . . ? C103 Si4 C96 C100 -60(2) . . . . ? C103 Si4 C101 C95 168.8(16) . . . . ? C103 Si4 C101 C98 -29(3) . . . . ? C106 Si5 C111 C105 -125.6(17) . . . . ? C106 Si5 C111 C108 112.9(16) . . . . ? C106 Si5 C113 C107 142(3) . . . . ? C106 Si5 C113 C112 -34(2) . . . . ? C111 Si5 C106 C109 42(3) . . . . ? C111 Si5 C106 C110 -178.0(17) . . . . ? C111 Si5 C113 C107 -102(3) . . . . ? C111 Si5 C113 C112 81(2) . . . . ? C113 Si5 C106 C109 155(2) . . . . ? C113 Si5 C106 C110 -65(2) . . . . ? C113 Si5 C111 C105 118.9(16) . . . . ? C113 Si5 C111 C108 -2.6(17) . . . . ? C114 N5 C115 C93 -165(3) . . . . ? C114 N5 C117 C121 73(3) . . . . ? C114 N5 C119 C118 72(2) . . . . ? C115 N5 C114 C116 -87(2) . . . . ? C115 N5 C117 C121 -45(3) . . . . ? C115 N5 C119 C118 -174(2) . . . . ? C117 N5 C114 C116 152(2) . . . . ? C117 N5 C115 C93 -42(3) . . . . ? C117 N5 C119 C118 -53(2) . . . . ? C119 N5 C114 C116 29(2) . . . . ? C119 N5 C115 C93 78(3) . . . . ? C119 N5 C117 C121 -165(3) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.155 0.773 0.861 12.7 0.0 ? 2 0.455 0.375 0.179 169.6 44.2 ? 3 0.545 0.625 0.821 169.6 43.6 ? 4 0.475 0.151 0.725 13.8 1.1 ? 5 0.525 0.849 0.275 13.8 1.1 ? 6 0.845 0.227 0.139 12.7 0.0 ?