#------------------------------------------------------------------------------ #$Date: 2024-08-05 21:05:39 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293762 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571789.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571789 loop_ _publ_author_name 'Jiang, Qing' 'Tang, Hui' 'Peng, Yuchen' 'Hu, Zhenni' 'Zeng, Wangdong' _publ_section_title ; Helical polycyclic hydrocarbons with open-shell singlet ground states and ambipolar redox behaviors. ; _journal_issue 27 _journal_name_full 'Chemical science' _journal_page_first 10519 _journal_page_last 10528 _journal_paper_doi 10.1039/d4sc02116a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C48 H24 Cl4' _chemical_formula_sum 'C48 H24 Cl4' _chemical_formula_weight 742.47 _space_group_crystal_system orthorhombic _space_group_IT_number 60 _space_group_name_Hall '-P 2n 2ab' _space_group_name_H-M_alt 'P b c n' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2019-06-04 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-03-20 deposited with the CCDC. 2024-05-29 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 30.8986(17) _cell_length_b 10.7331(6) _cell_length_c 22.0999(13) _cell_measurement_reflns_used 9922 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 66.57 _cell_measurement_theta_min 2.86 _cell_volume 7329.2(7) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 100.03 _diffrn_measured_fraction_theta_full 0.949 _diffrn_measured_fraction_theta_max 0.949 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.1510 _diffrn_reflns_av_unetI/netI 0.0914 _diffrn_reflns_Laue_measured_fraction_full 0.949 _diffrn_reflns_Laue_measured_fraction_max 0.949 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -36 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 46283 _diffrn_reflns_point_group_measured_fraction_full 0.949 _diffrn_reflns_point_group_measured_fraction_max 0.949 _diffrn_reflns_theta_full 66.915 _diffrn_reflns_theta_max 66.915 _diffrn_reflns_theta_min 2.860 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 3.197 _exptl_absorpt_correction_T_max 0.7528 _exptl_absorpt_correction_T_min 0.5898 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1956 before and 0.1096 after correction. The Ratio of minimum to maximum transmission is 0.7835. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'dark black' _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 1.346 _exptl_crystal_description plank _exptl_crystal_F_000 3040 _exptl_crystal_size_max 0.652 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.07 _refine_diff_density_max 0.782 _refine_diff_density_min -0.718 _refine_diff_density_rms 0.146 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.182 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 469 _refine_ls_number_reflns 6202 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.182 _refine_ls_R_factor_all 0.1275 _refine_ls_R_factor_gt 0.1051 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2838 _refine_ls_wR_factor_ref 0.3090 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4568 _reflns_number_total 6202 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL jq13o3_a.res in Pbcn jq13o3.res created by SHELXL-2017/1 at 23:27:29 on 04-Jun-2019 REM Old TITL JQ13O3 in Pbcn REM SHELXT solution in Pbcn REM R1 0.226, Rweak 0.006, Alpha 0.031, Orientation as input REM Formula found by SHELXT: C49 Cl4 CELL 1.54178 30.8986 10.7331 22.0999 90 90 90 ZERR 8 0.0017 0.0006 0.0013 0 0 0 LATT 1 SYMM 0.5-X,0.5-Y,0.5+Z SYMM -X,+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Cl UNIT 384 192 32 L.S. 10 PLAN 20 SIZE 0.07 0.17 0.652 TEMP -173.12 BOND $H LIST 6 fmap 2 ABIN ACTA OMIT 2 0 4 OMIT 0 0 2 OMIT 3 3 11 OMIT 6 1 13 OMIT 2 3 13 OMIT 17 9 9 OMIT 2 11 11 OMIT 15 10 8 OMIT 15 9 10 OMIT 10 5 11 OMIT 9 5 11 OMIT 3 11 11 OMIT 15 9 8 OMIT 1 10 12 OMIT 14 11 7 OMIT 20 10 6 OMIT 18 8 7 OMIT 15 6 10 OMIT 16 8 10 OMIT 18 8 8 OMIT 24 9 6 OMIT 20 8 8 OMIT 17 10 8 OMIT 1 10 16 OMIT 17 10 7 OMIT 2 1 6 OMIT 3 9 17 OMIT 21 8 9 OMIT 2 7 6 OMIT 5 10 12 OMIT 5 1 15 OMIT 8 11 12 OMIT 0 4 12 OMIT 18 1 6 OMIT 12 7 10 OMIT 14 8 8 OMIT 11 5 11 OMIT 1 10 7 OMIT 10 7 11 OMIT 5 3 15 OMIT 11 11 10 OMIT 7 5 15 OMIT 0 2 12 OMIT 2 8 0 OMIT 19 9 9 OMIT 17 10 6 OMIT 11 7 9 OMIT 4 8 20 OMIT 17 8 11 OMIT 14 8 10 OMIT 4 10 14 OMIT 1 10 15 OMIT 21 9 6 OMIT 2 9 18 OMIT 12 7 11 OMIT 23 8 6 OMIT 13 7 9 OMIT 3 10 6 OMIT 6 11 11 OMIT 8 6 10 OMIT 13 9 9 OMIT 1 9 4 OMIT 4 2 6 OMIT 24 7 10 OMIT 17 7 9 OMIT 9 7 11 OMIT 12 2 11 OMIT 7 4 16 OMIT 17 8 8 OMIT 10 5 13 OMIT 16 7 12 OMIT 2 5 7 OMIT 22 9 8 OMIT 30 7 2 OMIT 12 3 12 OMIT 8 6 15 OMIT 15 11 7 OMIT 2 4 9 OMIT 15 8 10 OMIT 11 9 8 OMIT 10 5 12 OMIT 9 4 16 OMIT 24 0 2 OMIT 31 6 1 OMIT 17 7 12 OMIT 7 5 22 OMIT 3 10 3 OMIT 12 5 13 OMIT 13 8 11 OMIT 13 10 9 OMIT 5 10 2 OMIT 12 8 9 OMIT 20 10 4 OMIT 6 7 12 OMIT 7 7 12 OMIT 18 10 6 OMIT 20 9 5 OMIT 9 1 15 OMIT 12 6 11 OMIT 31 6 4 REM REM REM WGHT 0.200000 FVAR 0.24667 CL4 3 0.348267 0.245312 0.422301 11.00000 0.03566 0.02588 = 0.03493 0.00463 0.00442 -0.00465 CL3 3 0.362541 0.705158 0.321940 11.00000 0.03042 0.03109 = 0.04335 0.01478 0.00472 0.00021 CL2 3 0.507975 0.555255 0.597128 11.00000 0.02537 0.05319 = 0.04496 0.01421 -0.00205 0.01158 CL1 3 0.450422 0.923857 0.449708 11.00000 0.02199 0.05622 = 0.08875 0.04362 0.01688 0.01171 C16 1 0.401393 0.688418 0.534005 11.00000 0.00541 0.02039 = 0.02178 0.00066 -0.00088 0.00318 C20 1 0.314954 0.631884 0.509467 11.00000 0.00972 0.01644 = 0.02230 -0.00233 0.00016 -0.00027 C14 1 0.388567 0.774365 0.629354 11.00000 0.01207 0.01897 = 0.02416 -0.00245 -0.00035 -0.00358 C22 1 0.331229 0.526699 0.419047 11.00000 0.01221 0.02211 = 0.02009 0.00569 0.00182 0.00214 C24 1 0.275323 0.580136 0.484917 11.00000 0.00804 0.01329 = 0.02150 -0.00222 -0.00316 0.00327 C17 1 0.368315 0.709610 0.579267 11.00000 0.01114 0.01044 = 0.01848 -0.00022 -0.00049 0.00073 C21 1 0.325507 0.682296 0.565324 11.00000 0.01002 0.01719 = 0.02221 0.00206 0.00111 -0.00258 AFIX 43 H21 2 0.303387 0.698214 0.594162 11.00000 -1.20000 AFIX 0 C19 1 0.348947 0.599830 0.467093 11.00000 0.01351 0.01867 = 0.01813 -0.00251 0.00133 -0.00314 C23 1 0.286969 0.509175 0.431845 11.00000 0.01477 0.02049 = 0.01844 0.00479 -0.00265 -0.00218 C28 1 0.231242 0.580674 0.505170 11.00000 0.01156 0.01582 = 0.02016 0.00732 -0.00180 -0.00291 C15 1 0.440780 0.741536 0.555627 11.00000 0.00831 0.02331 = 0.02764 0.00668 -0.00073 0.00037 C43 1 0.357546 0.472862 0.370281 11.00000 0.01393 0.02581 = 0.01930 0.00154 -0.00530 -0.00238 C6 1 0.331606 0.794639 0.712562 11.00000 0.01882 0.02329 = 0.01773 0.00399 -0.00253 0.00334 C2 1 0.270870 0.655103 0.727140 11.00000 0.02191 0.03597 = 0.01993 0.00203 0.00068 -0.00342 AFIX 43 H2 2 0.256817 0.578416 0.718498 11.00000 -1.20000 AFIX 0 C10 1 0.372886 0.827953 0.683866 11.00000 0.01703 0.02571 = 0.01896 0.00158 -0.00521 0.00350 C32 1 0.213772 0.661239 0.550787 11.00000 0.00472 0.02389 = 0.02527 0.01048 -0.00089 -0.00019 C13 1 0.432989 0.797630 0.611428 11.00000 0.01215 0.01737 = 0.02948 0.00487 -0.00300 -0.00266 C18 1 0.391754 0.632855 0.478548 11.00000 0.01073 0.01506 = 0.02647 0.00191 0.00383 0.00232 AFIX 43 H18 2 0.413770 0.617972 0.449425 11.00000 -1.20000 AFIX 0 C1 1 0.310586 0.681371 0.701564 11.00000 0.02030 0.02507 = 0.01602 0.00101 0.00024 0.00570 AFIX 43 H1 2 0.323910 0.621424 0.676006 11.00000 -1.20000 AFIX 0 C36 1 0.231996 0.778973 0.566458 11.00000 0.01064 0.03024 = 0.02077 0.00777 0.00283 0.00538 AFIX 43 H36 2 0.256509 0.808143 0.544721 11.00000 -1.20000 AFIX 0 C25 1 0.257138 0.428666 0.403061 11.00000 0.02349 0.02440 = 0.01938 0.00244 -0.00873 -0.00451 AFIX 43 H25 2 0.264661 0.385005 0.367178 11.00000 -1.20000 AFIX 0 C35 1 0.215342 0.851089 0.611695 11.00000 0.01585 0.02846 = 0.02960 0.00582 -0.00033 0.00378 AFIX 43 H35 2 0.228492 0.928747 0.621043 11.00000 -1.20000 AFIX 0 C44 1 0.375190 0.547450 0.324185 11.00000 0.01687 0.02159 = 0.02564 0.00873 -0.00256 -0.00138 C27 1 0.203935 0.490160 0.478981 11.00000 0.01054 0.02606 = 0.03068 0.00933 -0.00476 -0.00146 C31 1 0.173470 0.629720 0.579360 11.00000 0.01023 0.02954 = 0.02868 0.01348 -0.00029 0.00214 C26 1 0.217044 0.415836 0.428705 11.00000 0.01878 0.03315 = 0.02404 0.00568 -0.00982 -0.00974 AFIX 43 H26 2 0.197502 0.356045 0.412641 11.00000 -1.20000 AFIX 0 C48 1 0.368871 0.347009 0.368235 11.00000 0.01873 0.03068 = 0.02519 -0.00326 -0.00168 -0.00532 C5 1 0.314467 0.874025 0.757340 11.00000 0.02700 0.03230 = 0.02399 0.00745 0.00126 0.00654 C37 1 0.482230 0.739150 0.521961 11.00000 0.00830 0.03982 = 0.03286 -0.00355 -0.00046 -0.00522 C11 1 0.442803 0.939498 0.693596 11.00000 0.02424 0.02143 = 0.03747 0.00444 -0.00911 -0.01322 AFIX 43 H11 2 0.460282 0.998066 0.714610 11.00000 -1.20000 AFIX 0 C3 1 0.251524 0.740889 0.765477 11.00000 0.02373 0.03841 = 0.02716 0.01070 0.00533 0.00798 AFIX 43 H3 2 0.223181 0.725705 0.780414 11.00000 -1.20000 AFIX 0 C12 1 0.459838 0.875532 0.646309 11.00000 0.01708 0.02941 = 0.02729 0.00429 -0.00472 -0.00181 AFIX 43 H12 2 0.489701 0.883265 0.636796 11.00000 -1.20000 AFIX 0 C33 1 0.158547 0.702745 0.627985 11.00000 0.01229 0.03829 = 0.03387 0.01081 0.00495 0.00785 AFIX 43 H33 2 0.133752 0.675975 0.649826 11.00000 -1.20000 AFIX 0 C9 1 0.398965 0.920351 0.712411 11.00000 0.02830 0.01868 = 0.02627 0.00371 -0.00198 -0.00274 C8 1 0.381213 0.994291 0.759998 11.00000 0.04373 0.02371 = 0.02397 -0.00241 -0.00381 -0.00841 AFIX 43 H8 2 0.398484 1.056812 0.778511 11.00000 -1.20000 AFIX 0 C30 1 0.148858 0.529766 0.555303 11.00000 0.01075 0.02618 = 0.04499 0.01372 0.00045 0.00126 AFIX 43 H30 2 0.122749 0.505520 0.574710 11.00000 -1.20000 AFIX 0 C29 1 0.161976 0.468900 0.505424 11.00000 0.00747 0.01935 = 0.04896 0.01483 -0.00501 -0.00463 AFIX 43 H29 2 0.143049 0.410230 0.487101 11.00000 -1.20000 AFIX 0 C34 1 0.178606 0.811141 0.644841 11.00000 0.01373 0.04387 = 0.03346 0.01004 0.00740 0.00867 AFIX 43 H34 2 0.168116 0.858540 0.678050 11.00000 -1.20000 AFIX 0 C45 1 0.402717 0.500456 0.280319 11.00000 0.02178 0.04693 = 0.02048 0.00827 0.00093 -0.00640 AFIX 43 H45 2 0.413631 0.553567 0.249502 11.00000 -1.20000 AFIX 0 C47 1 0.397592 0.298323 0.325612 11.00000 0.02373 0.02819 = 0.03660 -0.00475 0.00390 -0.00224 AFIX 43 H47 2 0.405653 0.212940 0.326749 11.00000 -1.20000 AFIX 0 C42 1 0.515947 0.659029 0.538542 11.00000 0.01330 0.03556 = 0.03794 -0.00599 -0.00299 -0.00278 C46 1 0.414162 0.377237 0.281480 11.00000 0.02657 0.04805 = 0.02912 -0.00720 0.00553 -0.00227 AFIX 43 H46 2 0.433562 0.345482 0.251912 11.00000 -1.20000 AFIX 0 C7 1 0.339924 0.976309 0.779115 11.00000 0.04501 0.02917 = 0.02546 -0.00529 0.00332 0.01036 AFIX 43 H7 2 0.327654 1.032635 0.807492 11.00000 -1.20000 AFIX 0 C4 1 0.272815 0.846729 0.781896 11.00000 0.03470 0.03249 = 0.02580 0.00542 0.00601 0.01512 AFIX 43 H4 2 0.259868 0.902695 0.809849 11.00000 -1.20000 AFIX 0 C41 1 0.554974 0.657628 0.507618 11.00000 0.01190 0.03376 = 0.05824 0.00253 0.00241 -0.00127 AFIX 43 H41 2 0.577157 0.601281 0.519322 11.00000 -1.20000 AFIX 0 C38 1 0.490322 0.818377 0.473526 11.00000 0.01173 0.03705 = 0.05645 0.01367 0.00597 0.00291 C40 1 0.561462 0.736704 0.460670 11.00000 0.01429 0.04704 = 0.07527 0.00292 0.01946 -0.00254 AFIX 43 H40 2 0.588521 0.736354 0.440261 11.00000 -1.20000 AFIX 0 C39 1 0.529310 0.818087 0.441907 11.00000 0.01715 0.07416 = 0.07700 0.02814 0.02216 0.00115 AFIX 43 H39 2 0.533747 0.872124 0.408431 11.00000 -1.20000 AFIX 0 HKLF 4 REM jq13o3_a.res in Pbcn REM R1 = 0.1051 for 4568 Fo > 4sig(Fo) and 0.1275 for all 6202 data REM 469 parameters refined using 0 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 0.782, deepest hole -0.718, 1-sigma level 0.146 Q1 1 0.3286 0.6891 0.2956 11.00000 0.05 0.70 Q2 1 0.3106 0.5756 0.4343 11.00000 0.05 0.69 Q3 1 0.3517 0.2952 0.3645 11.00000 0.05 0.65 Q4 1 0.3683 0.4803 0.3729 11.00000 0.05 0.64 Q5 1 0.3069 0.4774 0.4284 11.00000 0.05 0.61 Q6 1 0.3782 0.3010 0.4324 11.00000 0.05 0.60 Q7 1 0.5259 0.6129 0.5907 11.00000 0.05 0.60 Q8 1 0.4878 0.9349 0.4877 11.00000 0.05 0.57 Q9 1 0.3310 0.3119 0.4251 11.00000 0.05 0.55 Q10 1 0.4729 0.8574 0.4537 11.00000 0.05 0.55 Q11 1 0.3432 0.7348 0.5602 11.00000 0.05 0.55 Q12 1 0.3632 0.7539 0.2610 11.00000 0.05 0.54 Q13 1 0.5332 0.5019 0.6010 11.00000 0.05 0.53 Q14 1 0.3834 0.6460 0.3218 11.00000 0.05 0.53 Q15 1 0.6060 0.8489 0.4515 11.00000 0.05 0.52 Q16 1 0.4104 0.7421 0.6187 11.00000 0.05 0.52 Q17 1 0.2489 0.6342 0.4989 11.00000 0.05 0.52 Q18 1 0.4019 0.3720 0.2927 11.00000 0.05 0.51 Q19 1 0.3794 0.2017 0.4331 11.00000 0.05 0.51 Q20 1 0.4495 0.8568 0.3904 11.00000 0.05 0.50 REM The information below was added by Olex2. REM REM R1 = 0.1051 for 4568 Fo > 4sig(Fo) and 0.1275 for all 50385 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.78, deepest hole -0.72 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1275 REM R1_gt = 0.1051 REM wR_ref = 0.3090 REM GOOF = 1.182 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 50385 REM Reflections_gt = 4568 REM Parameters = n/a REM Hole = -0.72 REM Peak = 0.78 REM Flack = n/a ; _cod_data_source_file d4sc02116a2.cif _cod_data_source_block jq13o3 _cod_depositor_comments 'Adding full bibliography for 1571789--1571792.cif.' _cod_database_code 1571789 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.807 _shelx_estimated_absorpt_t_min 0.230 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C21(H21), C2(H2), C18(H18), C1(H1), C36(H36), C25(H25), C35(H35), C26(H26), C11(H11), C3(H3), C12(H12), C33(H33), C8(H8), C30(H30), C29(H29), C34(H34), C45(H45), C47(H47), C46(H46), C7(H7), C4(H4), C41(H41), C40(H40), C39(H39) ; _shelx_fab_file ; 0 0 6 20.3147 -0.1936 0 0 10 27.0562 -0.4477 0 0 12 -6.6125 -0.5570 0 0 14 -3.2123 0.7551 0 0 16 8.4380 -0.2320 0 0 18 -6.4869 -0.1809 0 2 0 -81.2579 0.8494 0 2 1 -14.1224 0.2372 0 2 2 65.7811 -0.5126 0 2 3 2.8798 -0.3666 0 2 4 -22.4877 -0.2973 0 2 5 -1.0694 -0.1961 0 2 6 -19.4842 0.8133 0 2 7 3.6323 0.7330 0 2 8 29.2866 -0.6414 0 2 9 3.9275 -0.2626 0 2 10 -15.3354 0.1283 0 2 11 -13.8449 -0.2096 0 2 13 13.9671 0.2568 0 2 14 11.5712 -0.6354 0 2 15 -6.8270 -0.3773 0 2 16 -1.2104 0.3884 0 2 17 1.7223 0.2071 0 2 18 -6.3411 0.2064 0 2 19 -0.5328 0.2600 0 2 20 1.8798 -0.4686 0 2 21 -0.1525 -0.2860 0 4 0 28.3319 -0.4407 0 4 1 6.1257 -0.8692 0 4 2 -24.4038 0.1919 0 4 3 -2.8627 -0.0771 0 4 4 10.0680 0.1442 0 4 5 -2.1301 0.4981 0 4 6 11.5183 -0.3561 0 4 7 3.3816 -0.5996 0 4 8 -17.4790 0.3543 0 4 9 -4.9654 0.6121 0 4 10 -1.7186 -0.0090 0 4 11 10.4838 0.0655 0 4 13 -12.7716 -0.7523 0 4 14 -12.7850 0.3273 0 4 15 8.4434 0.5346 0 4 16 7.3525 -0.0636 0 4 17 0.0724 -0.0111 0 4 18 -2.7306 -0.1239 0 4 19 -6.6071 -0.2405 0 4 20 -2.8721 0.2580 0 4 24 1.5844 -0.1243 0 6 0 -15.8711 -0.0895 0 6 1 -0.1280 0.7083 0 6 2 9.8132 0.1117 0 6 3 6.4660 -0.3794 0 6 4 1.4712 -0.0542 0 6 5 -8.2589 -0.5525 0 6 6 -7.3529 -0.1228 0 6 7 2.0195 0.9584 0 6 8 6.6578 0.1543 0 6 9 2.6135 -0.3589 0 6 10 -2.3720 -0.0554 0 6 11 -5.1578 -0.2169 0 6 12 -3.1484 0.0318 0 6 13 9.4484 0.4416 0 6 14 3.4992 0.0389 0 6 15 -7.4393 -0.5376 0 6 16 1.0238 -0.1821 0 6 17 0.1501 0.1581 0 6 18 -1.8110 0.1242 0 6 19 2.0284 0.4470 0 6 20 0.1311 0.0399 0 6 21 -0.7141 -0.4533 0 6 22 -0.6628 -0.0348 0 6 23 0.6703 0.0564 0 8 0 7.5127 0.5593 0 8 1 -3.6931 -0.5700 0 8 2 -3.7880 -0.3036 0 8 3 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7 1.9788 0.2222 29 2 8 2.3104 0.4577 29 2 9 -3.1623 -0.2659 29 2 10 -5.2967 -0.3326 29 2 11 2.0246 -0.0464 29 2 12 3.7304 0.1852 29 2 13 -0.4149 0.2465 29 2 14 -0.2070 -0.0726 29 2 15 -0.2934 -0.0985 29 3 0 3.0552 -0.1455 29 3 1 2.1943 -0.2910 29 3 2 -0.9710 0.1513 29 3 3 1.5200 -0.1808 29 3 4 -0.3100 0.0647 29 3 5 -3.5318 0.4090 29 3 6 -1.0972 -0.2330 29 3 7 1.7650 -0.0896 29 3 8 0.3585 0.1282 29 3 9 0.5578 -0.2103 29 3 10 0.6983 -0.0027 29 3 11 -1.8886 0.1978 29 3 12 0.2017 -0.0068 29 3 13 2.2096 -0.2260 29 3 14 -0.0493 0.0900 29 4 1 -3.3805 1.4252 29 4 2 -3.9735 -0.2449 29 4 3 6.5147 -1.0064 29 4 4 5.5789 0.2760 29 4 5 -4.5588 0.1668 29 4 6 -2.3086 -0.1163 29 4 7 0.6824 0.1981 29 4 8 -1.8398 -0.1406 29 4 9 2.9933 -0.2009 29 4 10 2.7325 0.0974 29 4 11 -3.8357 0.2559 29 4 12 -2.5482 0.0772 29 4 13 2.2144 -0.0899 29 4 14 2.3369 -0.0557 29 5 0 -3.1054 0.0916 29 5 1 1.2495 -0.1392 29 5 2 2.0299 0.3807 29 5 3 -3.0414 -0.1106 29 5 4 0.1281 -0.3467 29 5 5 3.6226 0.2421 29 5 6 -0.7761 -0.2040 29 5 7 -1.5335 -0.1599 29 5 8 -0.5818 0.3934 29 5 9 -1.5610 0.0488 29 5 10 1.1118 -0.0215 29 5 11 2.4771 0.0882 29 5 12 -0.1063 -0.1148 29 6 1 2.1741 0.9553 29 6 2 0.4375 0.3342 29 6 3 -5.1119 -0.2595 29 6 4 -1.3269 -0.1126 29 6 5 4.2469 -0.1593 29 6 6 1.3877 -0.1505 29 6 7 -0.7568 0.0209 29 6 8 1.4800 0.0532 29 6 9 -1.7962 0.0693 29 6 10 -3.5117 0.0919 29 7 0 -0.7504 0.1218 29 7 1 0.0438 0.1875 29 7 2 -0.5457 0.1022 29 7 3 2.9947 -0.0690 29 7 4 1.9038 -0.3115 29 7 5 -2.0367 0.0372 29 7 6 -1.0452 0.2032 29 7 7 -1.1410 0.0877 30 0 0 3.9612 -0.0534 30 0 2 -0.9305 0.1726 30 0 4 -2.6105 -0.2076 30 0 6 2.8339 0.0010 30 0 8 -2.7220 0.0173 30 0 10 1.0444 0.1061 30 0 12 2.4524 -0.1165 30 0 14 -3.4049 0.2323 30 1 1 -3.3789 0.5236 30 1 2 1.5617 -0.2516 30 1 3 8.0166 -0.1416 30 1 4 -1.3820 -0.1495 30 1 5 -7.4359 0.0793 30 1 6 -0.6345 0.0050 30 1 7 2.1029 -0.1000 30 1 8 1.8420 0.2584 30 1 9 3.0322 -0.0394 30 1 10 -1.4933 -0.0722 30 1 11 -3.7624 -0.0293 30 1 12 0.7905 -0.2236 30 1 13 1.6985 0.2910 30 1 14 -0.0610 0.1308 30 1 15 0.0488 -0.2378 30 2 0 1.9035 0.2209 30 2 1 3.1809 -0.0370 30 2 2 -0.6116 0.0944 30 2 3 -0.6050 0.2578 30 2 4 1.4128 -0.1699 30 2 5 -0.9682 0.0046 30 2 6 -4.4647 -0.1901 30 2 7 1.1721 -0.0669 30 2 8 2.8526 0.3511 30 2 9 -0.9597 0.0113 30 2 10 0.8718 -0.1216 30 2 11 -0.2396 -0.0327 30 2 12 -1.8201 0.1108 30 2 13 1.1903 -0.0297 30 2 14 1.7558 -0.3200 30 3 1 2.2257 0.7249 30 3 2 -4.8342 -0.0020 30 3 3 -5.3571 -0.6912 30 3 4 5.1374 -0.0263 30 3 5 4.3095 0.2489 30 3 6 -1.6407 -0.1011 30 3 7 -0.2553 0.2332 30 3 8 -1.7445 0.1160 30 3 9 -2.3234 -0.4193 30 3 10 2.4717 -0.1701 30 3 11 2.5373 0.3430 30 3 12 -1.3184 0.2186 30 3 13 -1.3889 -0.1328 30 4 0 2.6421 -0.3335 30 4 1 -1.6649 0.1260 30 4 2 0.1614 0.0339 30 4 3 0.4570 0.1908 30 4 4 -3.2402 0.1018 30 4 5 0.6857 -0.1797 30 4 6 2.5025 -0.1162 30 4 7 -0.4167 -0.0592 30 4 8 -1.0029 -0.0313 30 4 9 -0.5419 0.1228 30 4 10 -0.6387 0.1752 30 4 11 0.5096 0.0696 30 4 12 1.8440 -0.0865 30 5 1 -0.8566 0.5238 30 5 2 5.1663 -0.4466 30 5 3 2.6166 -0.1464 30 5 4 -6.1771 0.3197 30 5 5 -3.3045 0.0453 30 5 6 3.5206 -0.0690 30 5 7 0.8222 -0.1815 30 5 8 0.4160 -0.0953 30 5 9 2.6035 0.0352 30 5 10 -2.4992 0.0607 30 5 11 -2.8590 0.1873 30 6 0 -0.8401 -0.5451 30 6 1 3.2378 0.0582 30 6 2 -1.4603 -0.0099 30 6 3 -0.6368 -0.1039 30 6 4 4.4614 0.1766 30 6 5 -0.2984 -0.1791 30 6 6 -2.7866 -0.1528 30 6 7 -0.2209 0.3780 30 6 8 -1.0613 0.1355 30 6 9 -0.0234 -0.0541 30 7 1 -0.8430 0.5168 30 7 3 1.2294 -0.1303 30 7 4 3.7229 -0.3361 30 7 5 -0.4400 -0.1076 31 0 2 -5.9825 -0.0250 31 0 4 6.5193 -0.1828 31 0 6 -4.0513 0.1255 31 0 8 0.7550 0.2304 31 0 10 1.8264 -0.1744 31 0 12 -1.5648 -0.2259 31 0 14 0.3565 0.2142 31 1 0 1.2248 -0.4515 31 1 1 -1.1418 -0.0412 31 1 2 0.0967 -0.0390 31 1 3 -0.5022 -0.1436 31 1 4 -0.2368 -0.0210 31 1 5 3.5987 0.3565 31 1 6 -2.0553 0.0306 31 1 7 -4.7742 -0.2908 31 1 8 1.8544 0.0658 31 1 9 2.3655 0.0583 31 1 10 0.0734 0.0229 31 1 11 0.7989 0.0384 31 1 12 -0.3218 -0.0898 31 1 13 -2.1805 0.1486 31 1 14 0.1087 0.1227 31 2 1 1.8443 0.3832 31 2 2 3.1684 -0.0369 31 2 3 -3.5587 -0.3450 31 2 4 -5.4167 -0.1647 31 2 5 1.6493 0.1907 31 2 6 2.8335 -0.1545 31 2 7 1.0690 0.1345 31 2 8 1.7575 0.4039 31 2 9 -1.6494 -0.2610 31 2 10 -3.0116 -0.2902 31 2 11 0.6946 0.0193 31 2 12 1.8018 0.2071 31 2 13 0.2349 0.1985 31 3 0 5.3636 -0.2575 31 3 1 2.8594 -0.0417 31 3 2 -2.4071 0.3237 31 3 3 0.3614 -0.4621 31 3 4 -0.9011 -0.0951 31 3 5 -2.9600 0.2057 31 3 6 0.6681 -0.1881 31 3 7 3.0251 0.2804 31 3 8 -0.5785 0.2227 31 3 9 -1.0943 -0.3501 31 3 10 0.3375 -0.1217 31 3 11 -0.7794 0.2290 31 3 12 0.8645 0.0489 31 4 1 -2.6116 1.0258 31 4 2 -1.2527 -0.4535 31 4 3 5.8325 -0.6836 31 4 4 2.2805 0.2240 31 4 5 -4.8694 0.2185 31 4 6 -2.4121 0.0987 31 4 7 0.9059 0.0613 31 4 8 0.7550 -0.1300 31 4 9 1.9784 -0.2482 31 4 10 1.4746 0.0133 31 4 11 -1.4580 0.2928 31 5 0 -4.2750 0.2105 31 5 1 0.5838 0.0732 31 5 2 2.3920 0.0657 31 5 3 -2.6969 -0.3939 31 5 4 1.2366 -0.2241 31 5 5 3.8867 0.1882 31 5 6 -2.0149 -0.1509 31 5 7 -1.7919 0.0037 31 5 8 -0.2187 0.3838 31 5 9 -0.9297 0.0802 31 6 2 0.4702 0.1568 31 6 3 -5.3264 -0.0142 31 6 5 3.5914 -0.2882 31 6 6 1.1452 0.0050 31 6 7 -1.2787 0.0942 32 0 0 5.8136 0.0424 32 0 2 -2.9966 0.1576 32 0 4 -2.2319 -0.3335 32 0 6 5.0262 0.1087 32 0 8 -4.4351 0.0413 32 0 10 1.5523 0.0571 32 0 12 1.5775 -0.1475 32 1 1 -1.5739 0.6434 32 1 2 -1.0904 -0.5515 32 1 3 3.7680 -0.2902 32 1 4 -0.6029 -0.3276 32 1 5 -3.5567 0.1277 32 1 6 0.2652 0.2354 32 1 7 1.2160 0.0261 32 1 8 1.2951 0.3642 32 1 9 1.0054 -0.2389 32 1 10 -0.3394 -0.2751 32 1 11 -1.4162 0.0709 32 1 12 -0.3558 -0.1306 32 2 0 -0.4754 0.1085 32 2 1 3.5918 -0.0695 32 2 2 0.3348 0.2184 32 2 3 -0.9489 0.2174 32 2 4 1.6880 -0.0572 32 2 5 -1.2398 -0.0862 32 2 6 -4.4759 -0.4113 32 2 7 1.7852 -0.0374 32 2 8 3.5526 0.5264 32 2 9 -0.8814 0.1784 32 2 10 -0.4942 -0.2366 32 2 11 -0.4046 -0.1505 32 2 12 -0.5329 0.0965 32 3 1 0.6521 0.8119 32 3 2 -4.6263 -0.0989 32 3 3 -1.7385 -0.6720 32 3 4 3.8542 0.0281 32 3 5 1.9582 0.1525 32 3 6 -1.1510 0.0183 32 3 7 -0.9615 0.3064 32 3 8 -0.5071 0.1304 32 3 9 -0.5830 -0.3468 32 3 10 1.0925 -0.2559 32 3 11 1.3911 0.2330 32 4 0 3.0184 -0.2863 32 4 1 -3.0871 0.5526 32 4 2 -0.8235 -0.0879 32 4 3 -0.0382 -0.2203 32 4 4 -2.5035 0.1001 32 4 5 2.2345 -0.2324 32 4 6 3.2218 0.0653 32 4 7 -1.2669 0.1549 32 4 8 -1.7319 -0.1628 32 4 9 -0.2025 0.0464 32 4 10 -0.2920 0.1673 32 5 1 0.4110 0.3687 32 5 2 4.8728 -0.2508 32 5 3 0.6217 -0.1924 32 5 4 -5.8885 0.3240 32 5 5 -2.5262 0.1313 32 5 6 2.3776 -0.1404 32 5 7 1.3535 -0.0413 32 5 8 0.7486 0.0008 32 6 0 -0.1632 -0.4369 32 6 1 3.2172 0.0623 32 6 2 -1.2504 -0.1709 32 6 3 -0.7378 -0.1023 32 6 4 3.1698 0.1991 33 0 2 -3.7319 0.1082 33 0 4 2.3023 -0.4200 33 0 6 -1.1514 0.2693 33 0 8 1.4300 0.3352 33 0 10 0.1515 -0.4084 33 1 0 -0.6418 -0.3380 33 1 1 -2.7786 -0.0994 33 1 2 0.0643 0.0813 33 1 3 -0.2359 -0.2139 33 1 4 0.9365 -0.0597 33 1 5 4.1534 0.4884 33 1 6 -1.5477 0.0376 33 1 7 -5.2810 -0.3920 33 1 8 1.2288 -0.0051 33 1 9 2.8820 0.1794 33 1 10 -0.1287 0.1144 33 1 11 -0.0257 0.0138 33 2 1 1.0434 0.0317 33 2 2 -0.7362 -0.1708 33 2 3 -1.9665 -0.3363 33 2 4 -1.4447 -0.1079 33 2 5 0.9032 0.3418 33 2 6 1.4851 -0.0101 33 2 7 0.5879 0.1114 33 2 8 0.7364 0.1893 33 2 9 -0.6576 -0.2528 33 2 10 -0.9747 -0.1514 33 3 0 5.1033 -0.3755 33 3 1 2.9659 0.1851 33 3 2 -2.9495 0.4033 33 3 3 -0.3186 -0.5234 33 3 4 -0.8848 -0.0764 33 3 5 -2.6645 -0.0249 33 3 6 2.3158 -0.1471 33 3 7 3.3046 0.5013 33 3 8 -1.0785 0.2236 33 3 9 -1.3742 -0.3875 33 3 10 -0.4559 -0.2540 33 4 1 -1.9983 0.4299 33 4 2 0.4197 -0.4677 33 4 3 4.4473 -0.5031 33 4 4 0.0871 0.1142 33 4 5 -3.1575 0.3490 33 4 6 -1.7993 0.2322 33 4 7 -0.0163 0.0524 33 4 8 1.7306 -0.0621 33 5 0 -3.8331 0.3499 33 5 1 0.1677 0.2233 33 5 2 1.9271 -0.2402 33 5 3 -1.9408 -0.4745 33 5 4 1.1209 -0.0336 33 5 5 2.8846 0.1222 34 0 0 4.1520 0.0474 34 0 2 -3.0054 0.1539 34 0 4 -1.0782 -0.3740 34 0 6 5.0142 0.2241 34 0 8 -4.2325 -0.0064 34 0 10 1.2042 0.0074 34 1 1 -0.0567 0.8689 34 1 2 -1.8464 -0.5405 34 1 3 0.2161 -0.4761 34 1 4 0.4032 -0.5207 34 1 5 -0.5517 0.1107 34 1 6 0.0647 0.3829 34 1 7 0.8241 0.2578 34 1 8 0.7446 0.3351 34 1 9 -0.3392 -0.4081 34 2 0 -2.6300 0.0062 34 2 1 3.2395 -0.0585 34 2 2 0.6202 0.1609 34 2 3 -0.9001 0.0707 34 2 4 2.6097 0.1711 34 2 5 -1.3825 -0.0143 34 2 6 -3.8689 -0.4445 34 2 7 1.6686 -0.0525 34 2 8 3.0458 0.4308 34 2 9 -0.4264 0.2454 34 3 1 -0.5117 0.5670 34 3 2 -3.4956 -0.1684 34 3 3 0.7236 -0.5953 34 3 4 2.5309 0.1205 34 3 5 0.2698 0.1269 34 3 6 -0.0698 0.0020 34 3 7 -0.7906 0.3408 34 3 8 -0.7690 0.1127 34 4 0 2.4031 -0.1864 34 4 1 -3.0560 0.6109 34 4 2 -1.3228 -0.1367 34 4 3 0.0696 -0.3159 34 4 4 -1.5143 0.0874 34 4 5 2.1065 -0.1651 34 4 6 3.1536 0.1918 35 0 2 -0.3633 0.2421 35 0 4 -0.5872 -0.4739 35 0 6 -0.2089 0.2513 35 0 8 1.8041 0.3112 35 1 0 -1.9509 -0.1552 35 1 1 -2.4369 -0.0345 35 1 2 0.0916 0.1214 35 1 3 -0.4094 -0.3596 35 1 4 1.6655 -0.0824 35 1 5 3.5000 0.5525 35 1 6 -0.9821 0.1076 35 1 7 -3.9629 -0.2944 35 2 1 0.4418 -0.1257 35 2 2 -1.7741 -0.3353 35 2 3 -0.8170 -0.3735 35 2 4 0.9054 0.0207 35 2 5 0.0828 0.4594 35 2 6 0.2608 0.0227 35 2 7 0.8737 0.0674 35 3 0 3.2730 -0.3048 35 3 1 2.4591 0.1336 35 3 2 -2.5921 0.1896 35 3 3 -0.2783 -0.2930 35 3 4 0.0479 0.0677 35 3 5 -2.0988 -0.0875 35 4 1 -1.1226 -0.0159 36 0 0 1.7026 0.0856 36 0 2 -1.7993 0.1309 36 0 4 -0.2359 -0.3844 36 1 1 0.7167 0.9560 36 1 2 -0.7516 -0.3822 36 1 3 -1.5248 -0.5570 36 1 4 0.6628 -0.4861 36 1 5 0.7317 0.1166 36 2 0 -2.5757 0.0006 36 2 1 2.1655 0.0018 36 2 2 0.2433 -0.0654 36 2 3 -0.8219 -0.1395 0 0 0 0.0 0.0 ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl4 Cl 0.34827(4) 0.24531(12) 0.42230(6) 0.0322(4) Uani 1 1 d . . . . . Cl3 Cl 0.36254(4) 0.70516(13) 0.32194(6) 0.0350(4) Uani 1 1 d . . . . . Cl2 Cl 0.50798(4) 0.55526(14) 0.59713(7) 0.0412(4) Uani 1 1 d . . . . . Cl1 Cl 0.45042(4) 0.92386(16) 0.44971(8) 0.0557(5) Uani 1 1 d . . . . . C16 C 0.40139(11) 0.6884(4) 0.5340(2) 0.0159(9) Uani 1 1 d . . . . . C20 C 0.31495(11) 0.6319(4) 0.5095(2) 0.0162(9) Uani 1 1 d . . . . . C14 C 0.38857(12) 0.7744(4) 0.6294(2) 0.0184(10) Uani 1 1 d . . . . . C22 C 0.33123(12) 0.5267(4) 0.4190(2) 0.0181(10) Uani 1 1 d . . . . . C24 C 0.27532(11) 0.5801(4) 0.48492(19) 0.0143(9) Uani 1 1 d . . . . . C17 C 0.36831(12) 0.7096(4) 0.57927(19) 0.0134(9) Uani 1 1 d . . . . . C21 C 0.32551(12) 0.6823(4) 0.5653(2) 0.0165(9) Uani 1 1 d . . . . . H21 H 0.303387 0.698214 0.594162 0.020 Uiso 1 1 calc R . . . . C19 C 0.34895(12) 0.5998(4) 0.46709(19) 0.0168(9) Uani 1 1 d . . . . . C23 C 0.28697(12) 0.5092(4) 0.43184(19) 0.0179(10) Uani 1 1 d . . . . . C28 C 0.23124(11) 0.5807(4) 0.50517(19) 0.0158(9) Uani 1 1 d . . . . . C15 C 0.44078(12) 0.7415(4) 0.5556(2) 0.0198(10) Uani 1 1 d . . . . . C43 C 0.35755(12) 0.4729(4) 0.3703(2) 0.0197(10) Uani 1 1 d . . . . . C6 C 0.33161(13) 0.7946(4) 0.7126(2) 0.0199(10) Uani 1 1 d . . . . . C2 C 0.27087(13) 0.6551(5) 0.7271(2) 0.0259(11) Uani 1 1 d . . . . . H2 H 0.256817 0.578416 0.718498 0.031 Uiso 1 1 calc R . . . . C10 C 0.37289(13) 0.8280(5) 0.6839(2) 0.0206(10) Uani 1 1 d . . . . . C32 C 0.21377(11) 0.6612(4) 0.5508(2) 0.0180(10) Uani 1 1 d . . . . . C13 C 0.43299(12) 0.7976(4) 0.6114(2) 0.0197(10) Uani 1 1 d . . . . . C18 C 0.39175(11) 0.6329(4) 0.4785(2) 0.0174(9) Uani 1 1 d . . . . . H18 H 0.413770 0.617972 0.449425 0.021 Uiso 1 1 calc R . . . . C1 C 0.31059(13) 0.6814(5) 0.7016(2) 0.0205(10) Uani 1 1 d . . . . . H1 H 0.323910 0.621424 0.676006 0.025 Uiso 1 1 calc R . . . . C36 C 0.23200(12) 0.7790(5) 0.5665(2) 0.0206(10) Uani 1 1 d . . . . . H36 H 0.256509 0.808143 0.544721 0.025 Uiso 1 1 calc R . . . . C25 C 0.25714(13) 0.4287(5) 0.4031(2) 0.0224(10) Uani 1 1 d . . . . . H25 H 0.264661 0.385005 0.367178 0.027 Uiso 1 1 calc R . . . . C35 C 0.21534(13) 0.8511(5) 0.6117(2) 0.0246(11) Uani 1 1 d . . . . . H35 H 0.228492 0.928747 0.621043 0.030 Uiso 1 1 calc R . . . . C44 C 0.37519(12) 0.5475(5) 0.3242(2) 0.0214(10) Uani 1 1 d . . . . . C27 C 0.20393(12) 0.4902(5) 0.4790(2) 0.0224(10) Uani 1 1 d . . . . . C31 C 0.17347(12) 0.6297(5) 0.5794(2) 0.0228(11) Uani 1 1 d . . . . . C26 C 0.21704(13) 0.4158(5) 0.4287(2) 0.0253(11) Uani 1 1 d . . . . . H26 H 0.197502 0.356045 0.412641 0.030 Uiso 1 1 calc R . . . . C48 C 0.36887(13) 0.3470(5) 0.3682(2) 0.0249(11) Uani 1 1 d . . . . . C5 C 0.31447(14) 0.8740(5) 0.7573(2) 0.0278(11) Uani 1 1 d . . . . . C37 C 0.48223(12) 0.7391(5) 0.5220(2) 0.0270(12) Uani 1 1 d . . . . . C11 C 0.44280(14) 0.9395(5) 0.6936(2) 0.0277(11) Uani 1 1 d . . . . . H11 H 0.460282 0.998066 0.714610 0.033 Uiso 1 1 calc R . . . . C3 C 0.25152(14) 0.7409(5) 0.7655(2) 0.0298(12) Uani 1 1 d . . . . . H3 H 0.223181 0.725705 0.780414 0.036 Uiso 1 1 calc R . . . . C12 C 0.45984(13) 0.8755(5) 0.6463(2) 0.0246(11) Uani 1 1 d . . . . . H12 H 0.489701 0.883265 0.636796 0.030 Uiso 1 1 calc R . . . . C33 C 0.15855(13) 0.7027(5) 0.6280(2) 0.0282(12) Uani 1 1 d . . . . . H33 H 0.133752 0.675975 0.649826 0.034 Uiso 1 1 calc R . . . . C9 C 0.39896(14) 0.9204(5) 0.7124(2) 0.0244(11) Uani 1 1 d . . . . . C8 C 0.38121(16) 0.9943(5) 0.7600(2) 0.0305(12) Uani 1 1 d . . . . . H8 H 0.398484 1.056812 0.778511 0.037 Uiso 1 1 calc R . . . . C30 C 0.14886(13) 0.5298(5) 0.5553(2) 0.0273(12) Uani 1 1 d . . . . . H30 H 0.122749 0.505520 0.574710 0.033 Uiso 1 1 calc R . . . . C29 C 0.16198(12) 0.4689(4) 0.5054(2) 0.0253(11) Uani 1 1 d . . . . . H29 H 0.143049 0.410230 0.487101 0.030 Uiso 1 1 calc R . . . . C34 C 0.17861(13) 0.8111(5) 0.6448(2) 0.0304(12) Uani 1 1 d . . . . . H34 H 0.168116 0.858540 0.678050 0.036 Uiso 1 1 calc R . . . . C45 C 0.40272(14) 0.5005(6) 0.2803(2) 0.0297(12) Uani 1 1 d . . . . . H45 H 0.413631 0.553567 0.249502 0.036 Uiso 1 1 calc R . . . . C47 C 0.39759(14) 0.2983(5) 0.3256(2) 0.0295(12) Uani 1 1 d . . . . . H47 H 0.405653 0.212940 0.326749 0.035 Uiso 1 1 calc R . . . . C42 C 0.51595(13) 0.6590(5) 0.5385(2) 0.0289(12) Uani 1 1 d . . . . . C46 C 0.41416(15) 0.3772(6) 0.2815(2) 0.0346(13) Uani 1 1 d . . . . . H46 H 0.433562 0.345482 0.251912 0.041 Uiso 1 1 calc R . . . . C7 C 0.33992(16) 0.9763(5) 0.7791(2) 0.0332(12) Uani 1 1 d . . . . . H7 H 0.327654 1.032635 0.807492 0.040 Uiso 1 1 calc R . . . . C4 C 0.27281(15) 0.8467(5) 0.7819(2) 0.0310(12) Uani 1 1 d . . . . . H4 H 0.259868 0.902695 0.809849 0.037 Uiso 1 1 calc R . . . . C41 C 0.55497(14) 0.6576(5) 0.5076(3) 0.0346(13) Uani 1 1 d . . . . . H41 H 0.577157 0.601281 0.519322 0.042 Uiso 1 1 calc R . . . . C38 C 0.49032(13) 0.8184(5) 0.4735(3) 0.0351(14) Uani 1 1 d . . . . . C40 C 0.56146(15) 0.7367(6) 0.4607(3) 0.0455(17) Uani 1 1 d . . . . . H40 H 0.588521 0.736354 0.440261 0.055 Uiso 1 1 calc R . . . . C39 C 0.52931(15) 0.8181(7) 0.4419(3) 0.056(2) Uani 1 1 d . . . . . H39 H 0.533747 0.872124 0.408431 0.067 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl4 0.0357(6) 0.0259(8) 0.0349(8) 0.0046(6) 0.0044(5) -0.0047(5) Cl3 0.0304(6) 0.0311(8) 0.0434(8) 0.0148(6) 0.0047(5) 0.0002(5) Cl2 0.0254(6) 0.0532(10) 0.0450(8) 0.0142(7) -0.0021(5) 0.0116(5) Cl1 0.0220(6) 0.0562(11) 0.0887(12) 0.0436(10) 0.0169(6) 0.0117(6) C16 0.0054(16) 0.020(2) 0.022(2) 0.001(2) -0.0009(14) 0.0032(16) C20 0.0097(17) 0.016(2) 0.022(2) -0.002(2) 0.0002(14) -0.0003(16) C14 0.0121(17) 0.019(2) 0.024(2) -0.002(2) -0.0003(16) -0.0036(16) C22 0.0122(18) 0.022(3) 0.020(2) 0.006(2) 0.0018(15) 0.0021(17) C24 0.0080(17) 0.013(2) 0.021(2) -0.0022(19) -0.0032(14) 0.0033(15) C17 0.0111(17) 0.010(2) 0.018(2) -0.0002(18) -0.0005(14) 0.0007(16) C21 0.0100(17) 0.017(2) 0.022(2) 0.002(2) 0.0011(15) -0.0026(16) C19 0.0135(17) 0.019(2) 0.018(2) -0.003(2) 0.0013(15) -0.0031(16) C23 0.0148(19) 0.020(3) 0.018(2) 0.005(2) -0.0026(15) -0.0022(17) C28 0.0116(17) 0.016(2) 0.020(2) 0.0073(19) -0.0018(14) -0.0029(16) C15 0.0083(17) 0.023(3) 0.028(3) 0.007(2) -0.0007(16) 0.0004(16) C43 0.0139(17) 0.026(3) 0.019(2) 0.002(2) -0.0053(15) -0.0024(17) C6 0.0188(19) 0.023(3) 0.018(2) 0.004(2) -0.0025(15) 0.0033(18) C2 0.022(2) 0.036(3) 0.020(2) 0.002(2) 0.0007(17) -0.003(2) C10 0.0170(18) 0.026(3) 0.019(2) 0.002(2) -0.0052(15) 0.0035(18) C32 0.0047(16) 0.024(3) 0.025(2) 0.010(2) -0.0009(14) -0.0002(16) C13 0.0121(17) 0.017(2) 0.029(3) 0.005(2) -0.0030(16) -0.0027(16) C18 0.0107(17) 0.015(2) 0.026(2) 0.002(2) 0.0038(15) 0.0023(16) C1 0.0203(19) 0.025(3) 0.016(2) 0.001(2) 0.0002(16) 0.0057(18) C36 0.0106(17) 0.030(3) 0.021(2) 0.008(2) 0.0028(15) 0.0054(17) C25 0.023(2) 0.024(3) 0.019(2) 0.002(2) -0.0087(16) -0.0045(19) C35 0.0159(19) 0.028(3) 0.030(3) 0.006(2) -0.0003(16) 0.0038(18) C44 0.0169(19) 0.022(3) 0.026(2) 0.009(2) -0.0026(16) -0.0014(18) C27 0.0105(18) 0.026(3) 0.031(3) 0.009(2) -0.0048(16) -0.0015(17) C31 0.0102(17) 0.030(3) 0.029(3) 0.013(2) -0.0003(16) 0.0021(18) C26 0.0188(19) 0.033(3) 0.024(2) 0.006(2) -0.0098(16) -0.010(2) C48 0.0187(19) 0.031(3) 0.025(3) -0.003(2) -0.0017(16) -0.0053(19) C5 0.027(2) 0.032(3) 0.024(3) 0.007(2) 0.0013(17) 0.007(2) C37 0.0083(18) 0.040(3) 0.033(3) -0.004(2) -0.0005(17) -0.0052(18) C11 0.024(2) 0.021(3) 0.037(3) 0.004(2) -0.0091(19) -0.0132(19) C3 0.024(2) 0.038(3) 0.027(3) 0.011(2) 0.0053(18) 0.008(2) C12 0.0171(19) 0.029(3) 0.027(2) 0.004(2) -0.0047(17) -0.0018(19) C33 0.0123(18) 0.038(3) 0.034(3) 0.011(2) 0.0049(17) 0.008(2) C9 0.028(2) 0.019(3) 0.026(3) 0.004(2) -0.0020(17) -0.0027(19) C8 0.044(3) 0.024(3) 0.024(3) -0.002(2) -0.004(2) -0.008(2) C30 0.0107(18) 0.026(3) 0.045(3) 0.014(3) 0.0005(18) 0.0013(18) C29 0.0075(17) 0.019(3) 0.049(3) 0.015(2) -0.0050(18) -0.0046(17) C34 0.0137(19) 0.044(3) 0.033(3) 0.010(3) 0.0074(17) 0.009(2) C45 0.022(2) 0.047(4) 0.020(2) 0.008(2) 0.0009(17) -0.006(2) C47 0.024(2) 0.028(3) 0.037(3) -0.005(2) 0.0039(19) -0.002(2) C42 0.0133(18) 0.036(3) 0.038(3) -0.006(3) -0.0030(18) -0.0028(19) C46 0.027(2) 0.048(4) 0.029(3) -0.007(3) 0.0055(19) -0.002(2) C7 0.045(3) 0.029(3) 0.025(3) -0.005(2) 0.003(2) 0.010(2) C4 0.035(2) 0.032(3) 0.026(3) 0.005(2) 0.0060(19) 0.015(2) C41 0.0119(19) 0.034(3) 0.058(4) 0.003(3) 0.0024(19) -0.0013(19) C38 0.0117(19) 0.037(3) 0.056(4) 0.014(3) 0.006(2) 0.0029(19) C40 0.014(2) 0.047(4) 0.075(5) 0.003(3) 0.019(2) -0.003(2) C39 0.017(2) 0.074(5) 0.077(5) 0.028(4) 0.022(3) 0.001(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C15 C16 C17 107.9(4) . . ? C18 C16 C17 121.6(3) . . ? C18 C16 C15 130.3(4) . . ? C21 C20 C24 132.9(4) . . ? C21 C20 C19 119.8(3) . . ? C19 C20 C24 106.2(3) . . ? C17 C14 C13 106.4(4) . . ? C10 C14 C17 134.0(4) . . ? C10 C14 C13 119.0(4) . . ? C19 C22 C43 123.3(3) . . ? C23 C22 C19 107.2(4) . . ? C23 C22 C43 129.2(4) . . ? C23 C24 C20 107.2(3) . . ? C28 C24 C20 133.2(4) . . ? C28 C24 C23 119.5(4) . . ? C16 C17 C14 107.3(3) . . ? C21 C17 C16 119.1(4) . . ? C21 C17 C14 133.0(4) . . ? C20 C21 C17 120.2(4) . . ? C20 C21 H21 119.9 . . ? C17 C21 H21 119.9 . . ? C22 C19 C20 109.4(3) . . ? C18 C19 C20 120.7(4) . . ? C18 C19 C22 129.7(4) . . ? C22 C23 C24 109.5(4) . . ? C22 C23 C25 128.6(4) . . ? C25 C23 C24 121.7(4) . . ? C24 C28 C32 125.4(4) . . ? C27 C28 C24 115.9(4) . . ? C27 C28 C32 118.6(4) . . ? C16 C15 C37 124.2(4) . . ? C13 C15 C16 108.8(4) . . ? C13 C15 C37 127.0(4) . . ? C44 C43 C22 121.5(4) . . ? C48 C43 C22 122.9(4) . . ? C48 C43 C44 115.5(4) . . ? C1 C6 C10 122.7(4) . . ? C1 C6 C5 118.2(4) . . ? C5 C6 C10 118.8(4) . . ? C1 C2 H2 120.1 . . ? C1 C2 C3 119.9(5) . . ? C3 C2 H2 120.1 . . ? C14 C10 C6 124.3(4) . . ? C14 C10 C9 117.7(4) . . ? C9 C10 C6 118.0(4) . . ? C28 C32 C31 119.6(4) . . ? C36 C32 C28 123.8(3) . . ? C36 C32 C31 116.4(4) . . ? C15 C13 C14 109.3(4) . . ? C15 C13 C12 129.8(4) . . ? C12 C13 C14 120.7(4) . . ? C16 C18 H18 120.9 . . ? C19 C18 C16 118.1(4) . . ? C19 C18 H18 120.9 . . ? C6 C1 H1 119.4 . . ? C2 C1 C6 121.3(4) . . ? C2 C1 H1 119.4 . . ? C32 C36 H36 118.9 . . ? C35 C36 C32 122.1(4) . . ? C35 C36 H36 118.9 . . ? C23 C25 H25 121.1 . . ? C26 C25 C23 117.7(4) . . ? C26 C25 H25 121.1 . . ? C36 C35 H35 119.7 . . ? C36 C35 C34 120.6(5) . . ? C34 C35 H35 119.7 . . ? C43 C44 Cl3 119.2(4) . . ? C45 C44 Cl3 118.2(4) . . ? C45 C44 C43 122.6(5) . . ? C28 C27 C26 122.3(4) . . ? C28 C27 C29 118.7(4) . . ? C26 C27 C29 118.9(4) . . ? C33 C31 C32 119.2(4) . . ? C33 C31 C30 122.1(4) . . ? C30 C31 C32 118.6(4) . . ? C25 C26 C27 121.5(4) . . ? C25 C26 H26 119.2 . . ? C27 C26 H26 119.2 . . ? C43 C48 Cl4 119.6(4) . . ? C47 C48 Cl4 117.5(4) . . ? C47 C48 C43 122.9(5) . . ? C6 C5 C7 119.5(4) . . ? C6 C5 C4 118.8(5) . . ? C4 C5 C7 121.6(5) . . ? C42 C37 C15 121.5(5) . . ? C38 C37 C15 122.1(4) . . ? C38 C37 C42 116.3(4) . . ? C12 C11 H11 119.4 . . ? C12 C11 C9 121.2(4) . . ? C9 C11 H11 119.4 . . ? C2 C3 H3 119.7 . . ? C4 C3 C2 120.6(4) . . ? C4 C3 H3 119.7 . . ? C13 C12 H12 120.2 . . ? C11 C12 C13 119.6(4) . . ? C11 C12 H12 120.2 . . ? C31 C33 H33 118.9 . . ? C34 C33 C31 122.2(4) . . ? C34 C33 H33 118.9 . . ? C10 C9 C11 120.4(4) . . ? C10 C9 C8 119.7(4) . . ? C8 C9 C11 119.9(4) . . ? C9 C8 H8 119.6 . . ? C7 C8 C9 120.8(5) . . ? C7 C8 H8 119.6 . . ? C31 C30 H30 119.6 . . ? C29 C30 C31 120.9(4) . . ? C29 C30 H30 119.6 . . ? C27 C29 H29 119.1 . . ? C30 C29 C27 121.8(4) . . ? C30 C29 H29 119.1 . . ? C35 C34 H34 120.7 . . ? C33 C34 C35 118.6(5) . . ? C33 C34 H34 120.7 . . ? C44 C45 H45 120.1 . . ? C46 C45 C44 119.8(5) . . ? C46 C45 H45 120.1 . . ? C48 C47 H47 120.7 . . ? C46 C47 C48 118.7(5) . . ? C46 C47 H47 120.7 . . ? C37 C42 Cl2 119.1(4) . . ? C41 C42 Cl2 119.2(4) . . ? C41 C42 C37 121.7(5) . . ? C45 C46 C47 120.4(5) . . ? C45 C46 H46 119.8 . . ? C47 C46 H46 119.8 . . ? C5 C7 H7 119.3 . . ? C8 C7 C5 121.3(5) . . ? C8 C7 H7 119.3 . . ? C5 C4 H4 119.8 . . ? C3 C4 C5 120.4(5) . . ? C3 C4 H4 119.8 . . ? C42 C41 H41 120.0 . . ? C40 C41 C42 120.0(5) . . ? C40 C41 H41 120.0 . . ? C37 C38 Cl1 120.0(3) . . ? C37 C38 C39 122.7(5) . . ? C39 C38 Cl1 117.3(5) . . ? C41 C40 H40 119.4 . . ? C41 C40 C39 121.2(5) . . ? C39 C40 H40 119.4 . . ? C38 C39 H39 120.9 . . ? C40 C39 C38 118.1(6) . . ? C40 C39 H39 120.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl4 C48 1.739(5) . ? Cl3 C44 1.738(5) . ? Cl2 C42 1.726(6) . ? Cl1 C38 1.755(5) . ? C16 C17 1.448(5) . ? C16 C15 1.426(5) . ? C16 C18 1.395(6) . ? C20 C24 1.450(5) . ? C20 C21 1.387(6) . ? C20 C19 1.449(5) . ? C14 C17 1.449(6) . ? C14 C10 1.420(6) . ? C14 C13 1.450(5) . ? C22 C19 1.429(6) . ? C22 C23 1.409(5) . ? C22 C43 1.469(6) . ? C24 C23 1.444(6) . ? C24 C28 1.434(5) . ? C17 C21 1.389(5) . ? C21 H21 0.9500 . ? C19 C18 1.393(5) . ? C23 C25 1.415(6) . ? C28 C32 1.434(6) . ? C28 C27 1.411(6) . ? C15 C13 1.393(7) . ? C15 C37 1.481(5) . ? C43 C44 1.406(6) . ? C43 C48 1.396(7) . ? C6 C10 1.469(6) . ? C6 C1 1.400(7) . ? C6 C5 1.409(7) . ? C2 H2 0.9500 . ? C2 C1 1.380(6) . ? C2 C3 1.387(7) . ? C10 C9 1.425(7) . ? C32 C36 1.426(7) . ? C32 C31 1.437(5) . ? C13 C12 1.408(6) . ? C18 H18 0.9500 . ? C1 H1 0.9500 . ? C36 H36 0.9500 . ? C36 C35 1.365(7) . ? C25 H25 0.9500 . ? C25 C26 1.369(6) . ? C35 H35 0.9500 . ? C35 C34 1.417(6) . ? C44 C45 1.385(7) . ? C27 C26 1.427(7) . ? C27 C29 1.440(5) . ? C31 C33 1.408(7) . ? C31 C30 1.418(7) . ? C26 H26 0.9500 . ? C48 C47 1.396(7) . ? C5 C7 1.434(8) . ? C5 C4 1.427(6) . ? C37 C42 1.400(7) . ? C37 C38 1.390(8) . ? C11 H11 0.9500 . ? C11 C12 1.357(7) . ? C11 C9 1.432(6) . ? C3 H3 0.9500 . ? C3 C4 1.362(8) . ? C12 H12 0.9500 . ? C33 H33 0.9500 . ? C33 C34 1.370(8) . ? C9 C8 1.427(7) . ? C8 H8 0.9500 . ? C8 C7 1.358(7) . ? C30 H30 0.9500 . ? C30 C29 1.344(7) . ? C29 H29 0.9500 . ? C34 H34 0.9500 . ? C45 H45 0.9500 . ? C45 C46 1.369(8) . ? C47 H47 0.9500 . ? C47 C46 1.390(7) . ? C42 C41 1.386(6) . ? C46 H46 0.9500 . ? C7 H7 0.9500 . ? C4 H4 0.9500 . ? C41 H41 0.9500 . ? C41 C40 1.355(8) . ? C38 C39 1.393(6) . ? C40 H40 0.9500 . ? C40 C39 1.386(8) . ? C39 H39 0.9500 . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 1 0 0 4.2 0 -1 0 1.1 3.9 0 2 0 5889.11 638.64 0 -2 0 5593.74 637.64 0 -3 0 -6.3 10.3 0 3 0 -2.1 8.9 0 4 0 1241.28 142.29 0 -5 0 -1.3 8.5 0 5 0 -4.6 5.1 0 6 0 28.4 9.3 0 -6 0 5.1 18.6 0 -8 0 114.19 33.1 0 -8 0 94.39 12.3 0 -9 0 -4 2 0 10 0 13.5 5.1 0 1 -1 -0.2 2.5 0 -1 -1 1.4 4.8 0 1 -1 -0.6 3.6 0 -1 1 -1.4 3.4 0 1 1 2.6 4.4 0 -1 1 -1.1 2.5 0 2 -1 52.79 10.1 0 2 1 51.09 13.4 0 -2 -1 60.09 14.8 0 -2 1 39.4 11.5 0 2 -1 51.89 13 0 3 -1 -4.7 9.1 0 3 -1 -0.7 5.3 0 -3 -1 3.8 10.5 0 3 1 7.8 10.1 0 -3 1 1.6 9.5 0 -4 1 212.48 36.2 0 4 -1 194.88 28.1 0 -4 -1 232.58 37.6 0 4 -1 215.18 43.8 0 -5 1 6.7 11.8 0 -5 -1 2.7 12.6 0 -5 1 -0.7 1.3 0 5 1 2.9 6.9 0 5 -1 0.2 4.6 0 -6 1 194.48 24.2 0 -6 1 225.88 41.5 0 6 -1 251.37 29.2 0 6 1 189.78 30.4 0 -7 1 -4.1 8.9 0 -7 -1 1.6 10.5 0 -7 -1 1.1 1.8 0 -7 1 0 1.4 0 8 -1 30.6 7 0 -8 1 84.39 34.3 0 8 -1 16 6.2 0 -9 -1 -0.4 1.9 0 9 1 -4.4 4.5 0 9 -1 -5.2 3.8 0 10 -1 65.49 12 0 0 -2 749.33 82.89 0 -1 2 0.1 3.3 0 1 -2 -0.6 3.1 0 -1 2 0.2 0.2 0 -1 2 0.7 3.4 0 -1 -2 3.2 5.9 0 1 -2 1.7 4 0 1 2 0.3 4.7 0 1 2 -1.7 2.8 0 -1 -2 0.6 0.5 0 -2 2 114.19 19 0 2 -2 151.88 25.1 0 -2 2 136.29 15 0 -2 2 144.79 23 0 -2 -2 142.89 27.2 0 2 2 134.99 25.9 0 3 -2 0.6 8.7 0 -3 2 -0.5 8.7 0 3 2 2.2 9.2 0 3 -2 0 5 0 -3 -2 -7.7 10 0 -4 -2 36.1 16.5 0 -4 2 44.1 15.2 0 4 -2 42.9 9.9 0 -4 2 37.9 5.1 0 4 -2 40.8 24 0 -5 2 -0.5 9.3 0 -5 -2 -1.8 12.6 0 5 2 -1 6.6 0 5 -2 -2.3 4.2 0 -5 2 -1.1 1.2 0 -6 2 801.42 110.89 0 -6 2 797.02 92.29 0 -6 -2 943.21 113.59 0 -7 2 -1.6 1.3 0 -7 -2 -0.6 1.8 0 -7 -2 -8.2 10.4 0 7 -2 1.5 1.9 0 -8 2 -8.4 15.9 0 -8 -2 13.8 3.4 0 -8 2 11.5 2.7 0 10 -2 68.99 12.4 0 11 -2 -3.8 3.9 0 0 -3 5 5.5 0 0 3 0.4 4.4 0 0 -3 0.1 0.7 0 -1 -3 -0.1 0.7 0 -1 3 -0.8 4.1 0 1 -3 0.2 4.6 0 -1 3 0.3 0.3 0 1 3 0.5 5.6 0 1 -3 -2.4 4.4 0 1 -3 0.2 0.3 0 -1 -3 -0.5 5.2 0 1 3 -1 5.9 0 -1 -3 5.3 7 0 -2 3 8940.91 1058.89 0 -2 3 9803.52 1055.09 0 -2 -3 9569.34 1061.49 0 2 3 9582.44 1061.19 0 -2 3 9999 1058.89 0 2 -3 9522.05 1060.29 0 3 -3 -2.4 8.4 0 3 3 -2.4 5.5 0 -3 -3 2.7 11.7 0 -3 3 -0.3 0.7 0 3 3 7.1 10.3 0 3 -3 -3.9 4.7 0 -3 3 -5.2 7.3 0 -4 3 938.61 108.19 0 -4 -3 947.61 112.49 0 -4 3 841.12 99.19 0 -5 -3 13.7 15.2 0 -5 3 -3.7 8 0 5 3 0.3 7.4 0 5 -3 0 5 0 -5 3 -0.1 1 0 6 -3 1373.16 156.08 0 -7 3 -2.4 1.2 0 -7 3 -0.8 9.8 0 -7 -3 0.3 2 0 -7 -3 10.5 13.8 0 7 -3 -0.8 1.9 0 -8 3 54.09 7.3 0 -8 -3 48.7 8.1 0 11 -3 -1.3 3.9 0 -1 -4 3.3 8.8 0 -1 -4 -0.7 1 0 -1 -4 2.9 8.6 0 1 4 -1.7 8 0 1 4 -4.6 6.6 0 -1 4 -2.3 5.7 0 1 -4 1.5 5.4 0 1 -4 2.5 7.4 0 2 4 1001.8 116.29 0 -2 -4 1005 109.29 0 2 -4 986.2 115.19 0 -2 -4 983.9 117.29 0 -2 4 956.6 108.99 0 -2 4 998.3 113.99 0 3 4 -2 6 0 3 -4 0.9 5.6 0 -3 4 -0.7 6.6 0 -3 -4 7.5 11.9 0 3 -4 -1.5 8.3 0 3 4 -2.7 9.4 0 -3 4 -0.6 6.1 0 -3 4 0.1 0.5 0 -4 4 354.16 40 0 -4 -4 354.66 54.49 0 -4 4 377.46 49.6 0 5 -4 -0.3 4.6 0 -5 -4 1.6 13.5 0 -5 4 -0.5 8.7 0 5 4 1.5 7.8 0 -5 4 -0.2 0.8 0 -6 -4 89.19 28.1 0 -6 4 123.19 14.1 0 -6 4 128.09 34.5 0 9 -4 21.1 11.3 0 10 -4 4.2 4.8 0 -10 -4 0.3 3.2 0 11 -4 -4.9 3.4 0 12 4 300.87 65.09 0 0 -5 2.8 9.5 0 0 5 -7.7 7.1 0 -1 -5 2.1 10.5 0 -1 -5 1.7 9.9 0 1 -5 -3.6 5.3 0 -1 5 -2 6.4 0 1 -5 -0.5 1.3 0 1 5 -1.8 7.3 0 1 -5 -0.4 8.2 0 -1 -5 -1.3 1.1 0 -2 5 6090.69 652.53 0 -2 -5 5490.15 654.43 0 2 -5 5748.82 652.53 0 -2 -5 6085.49 647.04 0 2 5 5890.31 653.63 0 3 5 5.1 7.3 0 -3 5 3.5 6.8 0 3 -5 -4.9 7.9 0 -3 -5 -2.8 12.4 0 -3 5 0.8 0.5 0 3 -5 -1.8 5.5 0 3 5 -0.4 9.7 0 4 -5 1590.44 180.68 0 -5 5 -1.7 0.7 0 5 -5 0.3 5.5 0 -5 5 -2.8 9 0 -5 -5 -3 13.1 0 -6 5 371.56 40.9 0 -6 -5 350.26 62.59 0 -6 5 355.76 55.19 0 -7 -5 -5.6 15.2 0 7 -5 1.3 2.3 0 8 -5 1.2 3.3 0 -8 -5 15 4 0 9 -5 4.8 7.8 0 11 -5 1 4.3 0 12 5 8.2 25.2 0 0 6 4757.42 529.85 0 1 -6 2.7 6.2 0 -1 -6 5.6 10.6 0 1 6 2.2 7.2 0 -1 -6 3.5 9.5 0 -1 6 -3.2 5.6 0 1 -6 0.2 7.9 0 1 -6 -0.1 1.5 0 -1 -6 -0.3 1.2 0 2 6 301.27 43.7 0 -2 6 310.87 42 0 -2 -6 301.67 47.4 0 2 -6 293.57 42.2 0 -2 -6 342.67 35.6 0 -3 6 -0.9 5.9 0 3 -6 -6.1 9.3 0 3 -6 2.3 6.4 0 -3 -6 -5.5 11.6 0 3 6 -10.4 8.1 0 3 6 -2.9 5.7 0 -4 6 692.93 86.59 0 5 -6 -0.6 1.9 0 5 -6 0.6 5.4 0 -5 -6 -0.5 12.2 0 6 -6 155.78 23.2 0 7 -6 -2.2 1.9 0 -9 -6 -2.2 2.9 0 9 -6 9 6.5 0 11 -6 0.5 3.4 0 0 7 2 6.2 0 0 -7 0 1.4 0 0 -7 2.2 8 0 0 -7 5.8 9.5 0 1 -7 -1.7 1.7 0 1 -7 5 9.9 0 -1 -7 2.5 9.5 0 -1 -7 -3.8 9 0 -1 -7 0 1.1 0 -1 7 2.6 6.7 0 1 7 2.8 5.9 0 -2 7 80.09 16.4 0 -2 -7 61.99 7.3 0 2 -7 51.99 13.7 0 -2 -7 34.2 15.8 0 3 -7 -17.8 9 0 -3 7 -5.7 7 0 3 -7 -0.5 1.8 0 3 7 0.3 10.8 0 -3 -7 -0.5 12.8 0 3 -7 2.3 8.2 0 -4 -7 617.14 76.99 0 -4 7 448.66 65.69 0 -5 -7 -13.3 11.5 0 5 -7 2.4 7 0 5 -7 -0.6 2 0 6 -7 130.39 17.8 0 -6 -7 97.89 31.9 0 -7 -7 18.2 16.7 0 9 -7 10.6 6.4 0 -9 -7 -0.9 3.1 0 10 -7 -1.7 3.9 0 11 7 -0.2 25.2 0 11 -7 -0.3 3.9 0 12 7 -13.1 33 0 12 -7 -3.4 3.1 0 1 -8 0.4 1.7 0 1 -8 5.6 10.3 0 -1 8 0.6 6 0 -1 -8 -0.2 8.5 0 -1 -8 -0.6 1.2 0 -1 -8 1.5 10.3 0 1 -8 -6.8 5.2 0 -2 -8 2031.9 216.08 0 -2 -8 1878.31 226.58 0 -2 8 1975 224.78 0 2 -8 1906.21 223.48 0 -3 -8 -0.1 1.2 0 -3 -8 -4.1 12.6 0 3 -8 -0.2 1.9 0 3 -8 2.3 9 0 -3 8 -3.5 7.4 0 -4 -8 1179.58 148.89 0 -5 -8 8.1 17 0 5 -8 7.2 8.6 0 -6 -8 165.58 41.1 0 -7 -8 -15.6 17.1 0 7 -8 0.2 2.2 0 -9 -8 -0.8 2.7 0 9 -8 4.8 5.1 0 10 8 28.5 30.6 0 10 -8 10.2 6.7 0 11 8 -3 25.4 0 11 -8 -0.8 4.1 0 12 8 9.2 24.4 0 12 -8 3.5 3.1 0 0 -9 0.3 10.5 0 0 -9 -1.2 8.2 0 0 -9 -0.9 1.5 0 1 -9 -3.6 9.6 0 1 -9 -0.1 1.6 0 -1 -9 -1.8 9.5 0 -1 -9 0.2 1.5 0 -1 -9 5.5 11 0 2 -9 -2.5 9.4 0 -2 -9 6.5 1.7 0 -2 -9 -7.2 11.4 0 2 -9 32.7 13.1 0 2 -9 -0.1 2.2 0 -3 -9 0.3 1.3 0 -3 -9 1.7 14.8 0 3 -9 -6.2 8.3 0 3 -9 -0.5 2.1 0 -4 -9 581.64 84.79 0 5 -9 0.1 3.2 0 -5 -9 6.1 15.7 0 5 -9 -3.1 8.4 0 5 -9 -0.8 2.1 0 -6 -9 619.24 89.79 0 6 -9 516.25 64.69 0 6 -9 601.54 96.79 0 7 -9 -0.1 4.9 0 7 -9 -1.7 23.8 0 7 -9 -2.4 2.9 0 -8 -9 111.99 18.2 0 10 9 -15.8 26.3 0 10 -9 -1.3 4.9 0 11 9 51.79 28.4 0 0 -10 366.86 50.79 0 -1 -10 0.6 1.8 0 1 -10 -0.2 2 0 -1 -10 1.9 10.2 0 1 -10 0.1 12.9 0 1 -10 -1.2 6.9 0 -1 -10 2.1 12.2 0 2 -10 460.35 62.39 0 -2 -10 473.05 67.09 0 -3 -10 8.4 14.8 0 3 -10 -1.9 2 0 3 -10 -10.3 12 0 3 -10 -0.1 10.2 0 -3 -10 -1.7 1.3 0 4 -10 -0.6 2.2 0 -4 -10 5.3 16.7 0 -5 -10 -18.1 14.3 0 5 -10 -1.8 3.7 0 -5 -10 -41.9 29.9 0 5 -10 -7.6 9.6 0 -6 -10 -18.7 18.8 0 6 -10 12.5 5.4 0 6 10 46.8 30.5 0 7 -10 -10.6 25.4 0 7 -10 -1.4 2.5 0 8 -10 387.86 94.19 0 -8 -10 216.38 28.4 0 9 -10 13.3 10.4 0 9 10 -15 53.99 0 -9 -10 -3.4 3 0 10 10 83.59 36.6 0 11 -10 -2.9 3.5 0 0 -11 -1.9 8.8 0 0 -11 -0.3 2.1 0 0 -11 -8 12.2 0 -1 -11 -3 10.6 0 1 -11 -1.3 1.9 0 1 -11 4.9 12 0 -1 -11 -0.2 1.7 0 1 -11 3.8 8.3 0 -2 -11 98.09 12 0 -2 -11 105.79 26 0 2 -11 105.69 23 0 3 -11 -1.6 1.8 0 3 -11 -0.6 8.9 0 -3 -11 -1.6 1.3 0 -3 -11 0.5 12.1 0 -4 -11 0.4 15.3 0 4 -11 1.1 11 0 4 -11 0.9 2.3 0 4 -11 -0.1 3.5 0 5 -11 -2 2.3 0 -5 -11 -10.7 18 0 5 11 -20.7 22.5 0 5 -11 2.8 3.8 0 5 -11 -9.4 11.4 0 6 -11 44 10.7 0 6 -11 44.6 28.4 0 -6 -11 50.59 24.9 0 7 -11 -34.7 27.1 0 7 -11 -2.4 5.2 0 7 -11 -1.5 3.3 0 -8 -11 152.18 20.8 0 8 -11 172.48 45.7 0 9 11 -42.2 26.9 0 -9 -11 0.9 2.9 0 11 -11 -1.5 3.5 0 0 -12 0.4 9.1 0 0 -12 46.8 20.1 0 -1 -12 -0.2 1.6 0 -1 -12 -1.4 10.4 0 1 -12 -8 9.2 0 1 -12 6.3 9.2 0 1 -12 -1.3 2.1 0 1 -12 -10 11.7 0 2 -12 35.8 17 0 -2 -12 21.1 3.9 0 -2 -12 21 15.1 0 3 -12 1.9 13.5 0 -3 -12 -3.9 13.5 0 3 -12 -1.4 2.2 0 4 -12 1748.63 206.58 0 5 -12 -4.2 15 0 5 -12 -2.2 1.9 0 5 -12 -0.5 3.5 0 6 -12 239.88 68.99 0 -6 -12 449.56 78.69 0 6 -12 303.37 38.5 0 7 -12 -2.3 3.8 0 7 -12 2.3 4.9 0 -7 -12 4.7 3.7 0 7 -12 8.2 27.8 0 -8 -12 131.59 18 0 8 -12 117.79 42.4 0 11 -12 -3.3 2.9 0 0 -13 1.5 2.2 0 0 -13 7.8 17.1 0 -1 -13 1.2 1.9 0 1 -13 7.2 17.3 0 1 -13 6.1 9.9 0 -1 -13 -16.6 8.8 0 1 -13 36.4 20.3 0 2 -13 217.98 24.5 0 -2 -13 154.48 36.9 0 -2 -13 184.58 23.6 0 2 -13 274.27 37.9 0 -3 -13 -11.4 14.8 0 3 -13 -1 2.3 0 3 -13 -0.7 1.3 0 3 -13 -5.5 11.8 0 3 -13 1.9 3.9 0 -4 -13 92.69 30.3 0 4 -13 88.89 14.4 0 5 -13 -0.1 4.2 0 5 -13 -15.7 16.7 0 5 13 33.3 31.7 0 5 -13 -1.1 2.4 0 6 -13 22.9 34.6 0 6 -13 53.29 11.5 0 7 -13 -9.3 25.4 0 7 -13 3 3.7 0 -7 -13 0.9 3.2 0 -8 -13 3 3.6 0 8 -13 7.8 4.3 0 11 -13 11.5 20.1 0 0 -14 370.16 43.4 0 0 -14 376.26 42.2 0 -1 -14 1.4 2.2 0 1 -14 0.5 12.5 0 -1 -14 -22.5 10.8 0 1 -14 1.1 2.9 0 1 -14 0.5 1.5 0 -1 -14 -3 1.4 0 2 -14 18.8 4.8 0 -2 -14 -4 15.2 0 2 -14 6.5 3.5 0 -2 -14 8.6 3 0 2 -14 55.99 23.1 0 -2 -14 9.3 2.6 0 2 -14 -4.8 11.4 0 3 -14 -3 2 0 3 -14 4.9 13.7 0 3 -14 0 1.8 0 -3 -14 -1.2 1.4 0 3 -14 -1.9 3.4 0 -3 -14 4 20.2 0 -4 -14 25.1 4.2 0 -4 -14 62.29 26.4 0 4 -14 37.9 9.2 0 -5 -14 33.1 27.9 0 5 -14 1 4.9 0 6 -14 -28.6 25.6 0 6 -14 26.3 8.6 0 7 -14 1 2.8 0 7 -14 -27 23.8 0 -7 -14 -1.4 3 0 8 -14 240.78 29.9 0 8 -14 216.68 55.39 0 10 -14 -1.2 4.6 0 0 -15 1.4 2.6 0 0 -15 -0.4 1.6 0 1 -15 -1.4 1.6 0 -1 -15 -1.8 1.7 0 -1 -15 1.6 15.9 0 1 -15 7.5 6.5 0 1 -15 1.1 2.6 0 -1 -15 1 2.2 0 2 -15 3.3 3.2 0 -2 -15 8.2 3.2 0 -2 -15 11 18.4 0 2 -15 12.3 2.7 0 -2 -15 11.2 2.5 0 2 -15 21.4 8.7 0 -3 -15 8.5 22.5 0 3 -15 -2.3 2.6 0 3 -15 -1.2 3.8 0 -3 -15 -0.5 1.4 0 4 -15 163.48 21.7 0 -4 -15 138.09 16.8 0 5 -15 -3.4 2.8 0 5 -15 4.4 5.6 0 6 -15 5.2 5.7 0 6 -15 4.6 3.6 0 -6 -15 4.7 3.4 0 6 -15 -34.1 26 0 -7 -15 6.6 3.5 0 7 -15 5.7 3.4 0 7 -15 14.9 25.6 0 8 -15 -15.1 20.3 0 10 -15 3.5 4.3 0 0 -16 83.19 10.6 0 1 -16 0.3 1.9 0 -1 -16 -2.8 2.4 0 -1 -16 2.8 1.9 0 1 -16 0.3 2.8 0 1 -16 12.4 6.5 0 2 -16 234.38 31.3 0 2 -16 258.67 28.8 0 -2 -16 248.98 28.6 0 3 -16 5.5 4.5 0 -3 -16 -0.8 1.6 0 3 -16 0.4 3.6 0 -4 -16 26.6 4.8 0 4 -16 38.4 9 0 5 -16 0 5.2 0 -5 -16 1.6 2.8 0 5 -16 -0.2 3.5 0 6 -16 -9.7 21.7 0 -6 -16 0.2 2.9 0 6 -16 6.9 3.4 0 6 -16 3.9 4.8 0 7 -16 9.5 3.4 0 -7 -16 2 2.7 0 7 -16 -24.1 18.7 0 8 -16 14 22.4 0 10 -16 13.9 5 0 0 -17 0.6 2.9 0 0 -17 -1.1 1.9 0 -1 -17 -2 2.2 0 1 -17 -0.1 2.1 0 1 -17 -2.9 3.9 0 -1 -17 -0.2 2 0 1 -17 -0.4 3 0 2 -17 45.9 9.7 0 -2 -17 63.69 8.1 0 2 -17 67.59 12.3 0 3 -17 2.5 3.5 0 -3 -17 2.7 2 0 3 -17 -0.2 5.2 0 4 -17 106.09 16.3 0 5 -17 0.6 5.3 0 5 -17 -1.5 3.7 0 -5 -17 -1.3 2.8 0 6 -17 31.9 7.5 0 -6 -17 58.19 9.1 0 6 -17 46.1 33.5 0 7 -17 -7.1 21.8 0 8 -17 -18.4 17.8 0 0 -18 -5.3 2.9 0 0 -18 1.6 2.2 0 -1 -18 0.7 2.4 0 1 -18 -4.5 5.1 0 1 -18 2.8 3.3 0 -1 -18 -12.9 5.7 0 -2 -18 82.99 10.6 0 2 -18 86.29 13 0 2 -18 77.29 14.3 0 3 -18 -2.5 4.8 0 3 -18 2.9 3.8 0 -3 -18 -4 2.9 0 4 -18 53.59 10.7 0 -4 -18 32.6 6.5 0 4 -18 24.9 7.2 0 -5 -18 -1.5 2.6 0 5 -18 3.1 3.2 0 5 -18 5 5.3 0 6 -18 -10.5 21.3 0 6 -18 4.7 3.2 0 7 -18 24.7 22.6 0 8 -18 70.29 25.1 0 0 -19 -6 3.5 0 1 -19 3.1 5.7 0 2 -19 0 3.5 0 2 -19 -1.4 5 0 -3 -19 -0.7 2.7 0 3 -19 -3.8 3 0 3 -19 1 5.2 0 4 -19 17.7 7 0 4 -19 13.5 5 0 -4 -19 13.3 3.7 0 -5 -19 -6 3.9 0 5 -19 -1.9 3.1 0 6 -19 351.46 71.19 0 7 -19 -1.6 21.2 0 2 -20 578.94 67.59 0 2 -20 589.64 68.29 0 3 -20 -0.7 3.7 0 3 -20 -0.3 5.1 0 4 -20 544.35 55.29 0 4 -20 387.76 53.49 0 6 -20 34 24.3 0 7 -20 0.6 16.1 0 2 -21 -7.3 4.3 0 2 -21 -1.3 4 0 5 -21 5.2 20 0 6 -21 27.6 21.6 0 5 -22 8.1 19.1 0 6 -22 -9 12.7 0 7 -22 28 22.6 0 5 -23 -7.6 15.3 0 6 -23 -6.4 11 0 4 -24 42.4 24.5 0 5 -24 -18.7 10.4 1 1 0 76.19 12.6 -1 -1 0 89.99 12.7 -1 1 0 71.99 13.1 1 -1 0 70.19 13 1 2 0 -3.1 8.1 -1 -2 0 -0.9 8.2 1 -2 0 4.9 8.8 -1 2 0 0.9 8.9 -1 3 0 867.61 106.59 1 3 0 856.31 105.99 -1 -3 0 909.61 104.99 1 -3 0 868.51 105.19 1 -4 0 -6.4 9.6 1 4 0 -1.7 6.7 -1 -4 0 -4.5 8.9 -1 4 0 -1.3 5.2 -1 -5 0 370.46 47.2 1 5 0 390.36 53.19 -1 -5 0 541.85 63.09 1 -5 0 475.85 62.09 -1 5 0 428.16 51.19 -1 -6 0 -0.3 13.5 1 6 0 11 7.7 -1 6 0 -3.6 5.5 -1 -6 0 0.1 1.4 -1 6 0 3.3 4.3 1 -6 0 6.1 16.8 1 -7 0 16.7 3.2 1 -7 0 0.3 10.1 -1 -7 0 13.4 3.1 -1 -7 0 37.1 14.6 -1 -8 0 10.3 18.5 -1 10 0 2.4 4.1 -1 0 1 0.4 1.5 -1 0 1 -0.1 0.2 -1 0 -1 -0.1 0.3 -1 0 -1 0 0.2 1 0 -1 0.2 1.6 1 -1 1 694.33 82.29 -1 1 1 749.92 83.39 1 -1 1 787.42 80.89 1 1 -1 768.12 82.69 -1 -1 -1 724.13 80.19 -1 -1 -1 703.43 82.69 1 1 -1 666.83 81.99 -1 -1 1 654.43 79.99 1 -1 -1 763.22 83.59 -1 -1 1 778.32 82.29 -1 1 -1 709.33 82.59 1 1 1 714.53 82.89 -1 2 1 724.13 82.19 -1 -2 -1 672.13 80.69 1 2 -1 711.73 81.29 1 2 -1 570.14 77.79 1 -2 1 690.23 80.49 -1 2 -1 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1 -7 29.4 45 -35 1 -7 46.7 6.4 -35 -1 7 98.59 40.6 -35 1 -7 45 7.7 -35 -1 7 87.19 37.1 -35 2 7 49.2 31 -35 -2 -7 32.3 5.8 -35 2 7 24.6 5.1 -35 -2 7 19.6 31.2 -35 0 8 321.07 65.09 -35 0 8 323.37 61.49 -35 0 8 196.58 26.3 -35 0 -8 239.98 25.8 -35 0 -8 222.18 27.1 -36 0 0 51.29 32.7 -36 0 0 26.5 4.5 -36 0 0 32.4 40.6 -36 -1 0 -12 25.7 -36 1 0 -13.7 33.1 -36 1 0 -11 24.3 -36 -1 0 -0.8 1.7 -36 -1 0 4.3 27 -36 -2 0 -6.5 26 -36 -2 0 2.5 2 -36 -2 0 4.7 2.3 -36 2 0 0.4 23 -36 2 0 -10.7 25.7 -36 -2 0 -22.6 24.9 -36 0 1 -1.6 1.6 -36 0 1 -2.9 23.8 -36 0 1 -7.6 24.8 -36 0 -1 7.2 23.7 -36 0 -1 0.3 1.6 -36 0 -1 13.4 26.5 -36 -1 -1 67.99 9.2 -36 -1 -1 110.49 42.8 -36 1 1 75.89 36 -36 1 1 112.09 33.3 -36 -1 -1 52.19 6.8 -36 1 -1 32.8 6.2 -36 1 -1 59.89 28.5 -36 -1 1 49.3 6.8 -36 -1 1 96.89 42.4 -36 1 -1 79.49 33.8 -36 -1 1 136.09 48.6 -36 2 1 0.8 25.7 -36 -2 -1 1 2.1 -36 2 1 4.7 35 -36 -2 -1 1 2 -36 -2 -1 4.6 27.3 -36 2 -1 38.5 28.5 -36 -2 1 14.3 25.8 -36 -2 1 3.1 1.9 -36 -2 1 1.9 28.4 -36 2 -1 29.8 26.1 -36 0 -2 102.29 12.5 -36 0 2 94.29 12.6 -36 0 -2 176.88 48.5 -36 0 2 149.39 41.2 -36 0 2 172.08 49.4 -36 -1 -2 83.39 10 -36 -1 -2 84.09 10.1 -36 1 2 130.79 42.4 -36 1 2 108.59 34.5 -36 -1 -2 149.69 45.2 -36 -1 2 122.29 42.7 -36 -1 2 112.19 36.4 -36 -1 2 69.29 9.8 -36 1 -2 68.99 9.5 -36 1 -2 138.39 51.79 -36 -2 -2 167.08 46 -36 2 2 157.88 38.6 -36 -2 -2 107.89 13 -36 2 2 165.48 41.2 -36 2 2 104.89 12.9 -36 -2 -2 107.69 13.1 -36 -2 2 119.69 42.8 -36 -2 2 143.29 44 -36 -2 2 86.79 12.7 -36 0 -3 0 25.9 -36 0 3 -10.6 26.8 -36 0 -3 10 4.9 -36 0 -3 -0.2 1.6 -36 0 3 -1.5 1.8 -36 0 3 30 30.9 -36 1 3 83.09 33.7 -36 -1 -3 41.9 5.5 -36 1 3 55.59 32.2 -36 -1 -3 70.79 35.2 -36 -1 -3 41.7 5.8 -36 1 -3 27.5 4.9 -36 1 -3 64.09 31.4 -36 -1 3 34.6 32.8 -36 -1 3 37 30 -36 -1 3 30.4 5.3 -36 -2 -3 -7.7 23.9 -36 -2 -3 4.3 2.5 -36 2 3 -19.8 22.9 -36 -2 -3 5.9 2.3 -36 2 3 -7.6 23.3 -36 2 3 9.7 2.9 -36 -2 3 0.6 24.4 -36 -2 3 3.5 2 -36 -2 3 34.8 29.7 -36 0 4 -4.4 26.3 -36 0 -4 12.7 24.1 -36 0 4 -0.8 28 -36 0 4 1.3 1.7 -36 0 -4 3.1 1.8 -36 0 -4 9.4 2.7 -36 1 4 128.99 38.5 -36 1 4 125.19 40.3 -36 1 4 76.09 10.1 -36 -1 -4 78.19 10.3 -36 -1 -4 86.89 9.9 -36 -1 4 113.79 38.4 -36 -1 4 62.59 9.7 -36 1 -4 81.49 9.4 -36 1 -4 72.99 30.1 -36 -1 4 134.59 42.2 -36 0 -5 1.7 1.8 -36 0 -5 2.3 2.3 -36 0 -5 -9 25.2 -36 0 5 -0.8 23.9 -36 0 5 -0.4 26.5 -36 0 5 -3.5 1.5 -36 -1 -5 39.1 25.6 -36 -1 -5 18.5 4 -36 1 5 11.7 3.5 -36 1 5 43.9 32.3 -36 1 5 12.9 26.9 -36 -1 -5 18.1 3.2 -36 1 -5 16 2.7 -36 -1 5 35.1 31.6 -36 -1 5 12.2 3.6 -36 -1 5 10.2 27.9 loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.187 0.250 166.3 36.5 ? 2 0.000 -0.187 0.750 166.3 36.7 ? 3 0.500 0.313 0.750 166.3 36.7 ? 4 0.500 0.687 0.250 166.3 36.5 ?