#------------------------------------------------------------------------------ #$Date: 2024-08-05 20:56:12 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293737 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571798.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571798 loop_ _publ_author_name 'Liu, Yang' 'Xu, Ling' 'Jin, Xiaorong' 'Yin, Bangshao' 'Rao, Yutao' 'Zhou, Mingbo' 'Song, Jianxin' 'Osuka, Atsuhiro' _publ_section_title ; The unprecedented strong paratropic ring current of a bis-PdII complex of 5,10,23-trimesityl [28]heptaphyrin(1.1.0.0.1.0.0). ; _journal_issue 29 _journal_name_full 'Chemical science' _journal_page_first 11402 _journal_page_last 11407 _journal_paper_doi 10.1039/d4sc01909a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'Cl, C H Cl3, C58 H52 N7, 2(C2 H3 N)' _chemical_formula_sum 'C63 H59 Cl4 N9' _chemical_formula_weight 1083.99 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2022-12-14 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-02-01 deposited with the CCDC. 2024-06-05 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 91.717(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.7069(7) _cell_length_b 16.7483(6) _cell_length_c 31.0611(12) _cell_measurement_reflns_used 5737 _cell_measurement_temperature 99.9(5) _cell_measurement_theta_max 71.7110 _cell_measurement_theta_min 2.9810 _cell_volume 5567.4(5) _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 99.9(5) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 8.0697 _diffrn_detector_type EosS2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -7.00 40.00 1.00 2.00 -- 34.73 -77.00 30.00 47 2 \w 26.00 88.00 1.00 2.00 -- 34.73-125.00 -30.00 62 3 \w 44.00 121.00 1.00 6.00 -- 105.88 -45.00 -90.00 77 4 \w 58.00 84.00 1.00 6.00 -- 105.88 -94.00 0.00 26 5 \w 44.00 139.00 1.00 6.00 -- 105.88 -15.00 -60.00 95 6 \w 97.00 165.00 1.00 6.00 -- 105.88 51.00 -57.00 68 7 \w 106.00 172.00 1.00 6.00 -- 105.88 61.00 -30.00 66 8 \w 108.00 175.00 1.00 6.00 -- 105.88 111.00-180.00 67 9 \w 13.00 40.00 1.00 2.00 -- 34.73 -99.00 -60.00 27 10 \w 5.00 56.00 1.00 2.00 -- 34.73 -99.00-120.00 51 11 \w -27.00 51.00 1.00 2.00 -- 34.73 -57.00 120.00 78 12 \w 41.00 127.00 1.00 6.00 -- 105.88 -30.00 150.00 86 13 \w -97.00 -25.00 1.00 2.00 -- -34.73 -38.00 -90.00 72 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, EosS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0100508000 _diffrn_orient_matrix_UB_12 -0.0367573000 _diffrn_orient_matrix_UB_13 -0.0453128000 _diffrn_orient_matrix_UB_21 0.1191527000 _diffrn_orient_matrix_UB_22 -0.0449787000 _diffrn_orient_matrix_UB_23 0.0149106000 _diffrn_orient_matrix_UB_31 -0.0803818000 _diffrn_orient_matrix_UB_32 -0.0712171000 _diffrn_orient_matrix_UB_33 0.0136607000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0505 _diffrn_reflns_av_unetI/netI 0.0711 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 36 _diffrn_reflns_limit_l_min -34 _diffrn_reflns_number 20151 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 66.593 _diffrn_reflns_theta_max 66.593 _diffrn_reflns_theta_min 2.847 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 2.315 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.41247 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour violet _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.293 _exptl_crystal_description plate _exptl_crystal_F_000 2272 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.729 _refine_diff_density_min -1.279 _refine_diff_density_rms 0.081 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.063 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 723 _refine_ls_number_reflns 9836 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.063 _refine_ls_R_factor_all 0.0916 _refine_ls_R_factor_gt 0.0729 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0816P)^2^+10.3701P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1843 _refine_ls_wR_factor_ref 0.1975 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7729 _reflns_number_total 9836 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc01909a2.cif _cod_data_source_block exp_2723 _cod_depositor_comments 'Adding full bibliography for 1571798--1571800.cif.' _cod_database_code 1571798 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula 'C100 H100 N7' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.802 _shelx_estimated_absorpt_t_min 0.655 _reflns_odcompleteness_completeness 99.97 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.49 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C60(H60) 2.b Aromatic/amide H refined with riding coordinates: N2(H2), C7(H7A), C8(H8), C48(H48), C21(H21), C13(H13), C17(H17), C3(H3), C25(H25), C12(H12), C20(H20), C46(H46), C40(H40), C16(H16), C42(H42), C34(H34), C30(H30), C29(H29), C26(H26), C36(H36), C2(H2A) 2.c Idealised Me refined as rotating group: C59(H59A,H59B,H59C), C55(H55A,H55B,H55C), C57(H57A,H57B,H57C), C51(H51A,H51B, H51C), C54(H54A,H54B,H54C), C58(H58A,H58B,H58C), C56(H56A,H56B,H56C), C53(H53A, H53B,H53C), C52(H52A,H52B,H52C), C63(H63A,H63B,H63C) ; _shelx_res_file ; TITL exp_2723_a.res in P2(1)/c exp_2723.res created by SHELXL-2016/6 at 10:13:45 on 14-Dec-2022 REM Old TITL exp_2723 in P21/c #14 REM SHELXT solution in P2(1)/c REM R1 0.204, Rweak 0.018, Alpha 0.054, Orientation as input REM Formula found by SHELXT: C63 N11 Q2 CELL 1.54184 10.7069 16.7483 31.0611 90 91.717 90 ZERR 4 0.0007 0.0006 0.0012 0 0.004 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cl N UNIT 252 236 16 36 L.S. 4 0 0 PLAN 20 SIZE 0.2 0.2 0.1 TEMP -173 BOND $H list 4 fmap 2 53 acta SHEL 999 0.84 REM REM REM WGHT 0.081600 10.370100 FVAR 0.23023 CL1 3 0.652431 0.305478 0.394807 11.00000 0.02164 0.01803 = 0.03596 -0.00444 -0.00608 0.00353 CL4 3 0.824743 0.367729 0.270588 11.00000 0.07003 0.02849 = 0.04896 0.00040 0.01929 -0.00053 CL3 3 0.662666 0.484966 0.307412 11.00000 0.05259 0.06211 = 0.05138 0.00269 0.02254 0.00804 CL2 3 0.925267 0.518907 0.300092 11.00000 0.04645 0.04633 = 0.08617 -0.01525 -0.02799 0.00888 N7 4 0.359566 0.310539 0.350165 11.00000 0.01585 0.01906 = 0.02205 0.00111 -0.00323 0.00388 N6 4 0.488456 0.461446 0.387881 11.00000 0.01878 0.01481 = 0.02405 -0.00122 -0.00001 0.00390 N2 4 0.686987 -0.014837 0.372438 11.00000 0.01962 0.01508 = 0.02204 -0.00098 -0.00057 0.00035 AFIX 43 H2 2 0.703465 -0.057711 0.357246 11.00000 -1.20000 AFIX 0 N4 4 0.959202 0.315865 0.422433 11.00000 0.01497 0.01753 = 0.02575 -0.00037 -0.00202 -0.00170 N5 4 0.784399 0.463626 0.422870 11.00000 0.02079 0.01530 = 0.02244 -0.00162 -0.00186 -0.00204 N3 4 0.955166 0.145458 0.414094 11.00000 0.01807 0.01735 = 0.02508 -0.00115 -0.00272 0.00302 N1 4 0.394089 0.141178 0.343479 11.00000 0.01931 0.01629 = 0.02471 -0.00264 -0.00123 0.00173 C6 1 0.572655 0.023839 0.372359 11.00000 0.01764 0.01671 = 0.02182 0.00126 -0.00094 0.00182 C9 1 0.771066 0.023429 0.399686 11.00000 0.01921 0.01712 = 0.02368 0.00221 0.00060 -0.00143 C31 1 0.276427 0.261268 0.329111 11.00000 0.02005 0.02000 = 0.02180 -0.00019 -0.00318 0.00355 C11 1 0.989133 0.064371 0.409532 11.00000 0.01822 0.02008 = 0.02080 -0.00162 -0.00234 0.00284 C15 1 1.063890 0.269022 0.426083 11.00000 0.01985 0.01966 = 0.01723 -0.00014 -0.00073 0.00332 C27 1 0.372650 0.456288 0.368800 11.00000 0.01870 0.02106 = 0.02148 0.00057 -0.00275 0.00091 C5 1 0.472419 0.004725 0.342199 11.00000 0.02025 0.01703 = 0.02298 -0.00178 0.00178 -0.00132 C28 1 0.315570 0.386859 0.349674 11.00000 0.02291 0.01707 = 0.02296 -0.00217 -0.00113 0.00197 C1 1 0.296685 0.176623 0.324825 11.00000 0.01856 0.02130 = 0.02425 -0.00249 -0.00283 0.00018 C50 1 0.604153 0.656817 0.437526 11.00000 0.01888 0.01327 = 0.02711 -0.00139 -0.00334 -0.00015 C38 1 0.942995 -0.077782 0.390738 11.00000 0.01675 0.01843 = 0.02590 -0.00161 -0.00392 0.00056 C32 1 0.471268 -0.076386 0.321612 11.00000 0.01902 0.01394 = 0.02663 -0.00328 -0.00482 0.00303 C10 1 0.902990 0.005672 0.400865 11.00000 0.02065 0.02040 = 0.01890 0.00071 -0.00127 0.00353 C23 1 0.617700 0.570980 0.422997 11.00000 0.02419 0.01746 = 0.01892 0.00036 0.00233 -0.00020 C43 1 0.968525 -0.098799 0.348183 11.00000 0.01996 0.01992 = 0.02454 0.00056 -0.00235 -0.00018 C47 1 0.582422 0.814970 0.466183 11.00000 0.02472 0.01419 = 0.03095 -0.00148 -0.00545 0.00018 C22 1 0.737797 0.539941 0.431157 11.00000 0.02409 0.01642 = 0.01936 0.00121 0.00100 0.00154 C7 1 0.583863 0.084369 0.403329 11.00000 0.01973 0.01339 = 0.02550 -0.00323 -0.00034 0.00337 AFIX 43 H7A 2 0.519451 0.119798 0.411494 11.00000 -1.20000 AFIX 0 C8 1 0.705439 0.083533 0.419988 11.00000 0.02289 0.01936 = 0.02373 -0.00242 -0.00138 0.00242 AFIX 43 H8 2 0.738403 0.118269 0.441674 11.00000 -1.20000 AFIX 0 C48 1 0.621730 0.797985 0.425101 11.00000 0.02658 0.01626 = 0.02869 0.00580 -0.00165 -0.00222 AFIX 43 H48 2 0.639971 0.841006 0.406373 11.00000 -1.20000 AFIX 0 C19 1 0.908060 0.460760 0.433872 11.00000 0.02161 0.02077 = 0.02026 0.00089 -0.00164 -0.00002 C24 1 0.510047 0.538762 0.403179 11.00000 0.02477 0.01779 = 0.02170 -0.00086 0.00167 0.00065 C21 1 0.839885 0.584640 0.447929 11.00000 0.02630 0.01523 = 0.03177 0.00082 -0.00336 -0.00012 AFIX 43 H21 2 0.836871 0.638778 0.456965 11.00000 -1.20000 AFIX 0 C13 1 1.170131 0.130995 0.420606 11.00000 0.01478 0.02694 = 0.02514 -0.00338 -0.00146 0.00270 AFIX 43 H13 2 1.255329 0.145551 0.424968 11.00000 -1.20000 AFIX 0 C14 1 1.061574 0.184126 0.420216 11.00000 0.02323 0.02065 = 0.01596 -0.00087 -0.00158 0.00073 C17 1 1.118292 0.395749 0.441721 11.00000 0.01898 0.02083 = 0.02850 -0.00355 -0.00188 -0.00393 AFIX 43 H17 2 1.165544 0.441679 0.449761 11.00000 -1.20000 AFIX 0 C45 1 0.565460 0.672201 0.479679 11.00000 0.02150 0.01479 = 0.02645 -0.00042 -0.00086 0.00041 C3 1 0.276028 0.050761 0.302027 11.00000 0.02177 0.02088 = 0.02796 -0.00642 -0.00722 -0.00177 AFIX 43 H3 2 0.249338 0.002560 0.288508 11.00000 -1.20000 AFIX 0 C25 1 0.399810 0.581955 0.393001 11.00000 0.02737 0.01327 = 0.03439 -0.00214 -0.00292 0.00292 AFIX 43 H25 2 0.385382 0.636378 0.399893 11.00000 -1.20000 AFIX 0 C18 1 0.990173 0.393948 0.431679 11.00000 0.02156 0.01697 = 0.02366 0.00014 -0.00013 -0.00074 C39 1 0.953436 -0.134188 0.424079 11.00000 0.02126 0.02427 = 0.02487 0.00112 -0.00417 0.00224 C12 1 1.124169 0.057280 0.413503 11.00000 0.02030 0.02016 = 0.02477 -0.00088 0.00036 0.00707 AFIX 43 H12 2 1.171296 0.009441 0.411462 11.00000 -1.20000 AFIX 0 C49 1 0.635575 0.719514 0.410152 11.00000 0.02257 0.01834 = 0.02279 0.00099 -0.00186 0.00216 C20 1 0.944396 0.536908 0.449031 11.00000 0.02279 0.02227 = 0.02774 -0.00299 -0.00206 -0.00123 AFIX 43 H20 2 1.026199 0.552403 0.458315 11.00000 -1.20000 AFIX 0 C46 1 0.555000 0.751159 0.492992 11.00000 0.02463 0.01892 = 0.02313 -0.00101 -0.00149 0.00263 AFIX 43 H46 2 0.528268 0.761866 0.521304 11.00000 -1.20000 AFIX 0 C40 1 0.992919 -0.211067 0.414306 11.00000 0.02252 0.01912 = 0.03011 0.00407 -0.00422 -0.00055 AFIX 43 H40 2 1.000812 -0.249485 0.436723 11.00000 -1.20000 AFIX 0 C41 1 1.021111 -0.233042 0.372519 11.00000 0.02004 0.02060 = 0.03467 -0.00499 -0.00144 -0.00282 C16 1 1.164675 0.318225 0.437868 11.00000 0.02057 0.02491 = 0.02511 -0.00302 -0.00427 0.00073 AFIX 43 H16 2 1.249042 0.301954 0.442412 11.00000 -1.20000 AFIX 0 C42 1 1.007154 -0.177379 0.340006 11.00000 0.02200 0.02249 = 0.02718 -0.00524 0.00196 0.00110 AFIX 43 H42 2 1.024123 -0.192586 0.311302 11.00000 -1.20000 AFIX 0 N9 4 0.221180 0.613958 0.477305 11.00000 0.03427 0.05312 = 0.04750 -0.01081 0.00151 -0.00975 C4 1 0.386207 0.061186 0.330324 11.00000 0.01876 0.01846 = 0.02206 -0.00283 -0.00242 -0.00231 C34 1 0.406045 -0.213855 0.319958 11.00000 0.02601 0.01640 = 0.03439 0.00015 -0.00548 -0.00258 AFIX 43 H34 2 0.360040 -0.256472 0.331978 11.00000 -1.20000 AFIX 0 C33 1 0.405602 -0.139226 0.340091 11.00000 0.01846 0.01883 = 0.02814 -0.00149 -0.00472 0.00332 C30 1 0.174742 0.307388 0.314961 11.00000 0.02173 0.02206 = 0.03466 -0.00053 -0.00737 0.00351 AFIX 43 H30 2 0.102621 0.288898 0.299432 11.00000 -1.20000 AFIX 0 C35 1 0.472167 -0.227320 0.282749 11.00000 0.03282 0.02112 = 0.02757 -0.00676 -0.00886 0.00479 C37 1 0.537529 -0.088517 0.283703 11.00000 0.02792 0.02029 = 0.02566 -0.00308 -0.00347 0.00228 C59 1 0.684410 0.703929 0.365975 11.00000 0.03304 0.02483 = 0.02608 0.00327 0.00182 0.00180 AFIX 137 H59A 2 0.768247 0.680639 0.368670 11.00000 -1.50000 H59B 2 0.688272 0.754282 0.349999 11.00000 -1.50000 H59C 2 0.628494 0.666722 0.350505 11.00000 -1.50000 AFIX 0 C29 1 0.198990 0.385969 0.327945 11.00000 0.02279 0.02339 = 0.03500 -0.00123 -0.00699 0.00476 AFIX 43 H29 2 0.145959 0.430697 0.322935 11.00000 -1.20000 AFIX 0 C26 1 0.316744 0.532387 0.371487 11.00000 0.02179 0.02231 = 0.03750 -0.00385 -0.00737 0.00378 AFIX 43 H26 2 0.236185 0.546777 0.360417 11.00000 -1.20000 AFIX 0 C36 1 0.537244 -0.164669 0.265300 11.00000 0.03092 0.02387 = 0.02577 -0.00338 -0.00113 0.00633 AFIX 43 H36 2 0.583191 -0.173541 0.240047 11.00000 -1.20000 AFIX 0 C2 1 0.219626 0.122114 0.298730 11.00000 0.02156 0.02360 = 0.03081 -0.00360 -0.00777 -0.00087 AFIX 43 H2A 2 0.145114 0.134568 0.282754 11.00000 -1.20000 AFIX 0 C55 1 1.067770 -0.316433 0.363550 11.00000 0.03364 0.02152 = 0.04152 -0.00331 0.00292 0.00646 AFIX 137 H55A 2 1.143415 -0.326843 0.381202 11.00000 -1.50000 H55B 2 1.086978 -0.321176 0.333005 11.00000 -1.50000 H55C 2 1.003159 -0.355329 0.370628 11.00000 -1.50000 AFIX 0 C57 1 0.536752 0.605431 0.510061 11.00000 0.03804 0.01977 = 0.02559 0.00234 0.00265 -0.00117 AFIX 137 H57A 2 0.468545 0.572870 0.497742 11.00000 -1.50000 H57B 2 0.511717 0.627696 0.537676 11.00000 -1.50000 H57C 2 0.611251 0.572134 0.514603 11.00000 -1.50000 AFIX 0 C51 1 0.332395 -0.128121 0.380264 11.00000 0.02817 0.02062 = 0.03413 -0.00311 0.00231 -0.00057 AFIX 137 H51A 2 0.375905 -0.090040 0.399397 11.00000 -1.50000 H51B 2 0.324601 -0.179509 0.395031 11.00000 -1.50000 H51C 2 0.249007 -0.107583 0.372525 11.00000 -1.50000 AFIX 0 C54 1 0.925325 -0.112297 0.469897 11.00000 0.03998 0.02976 = 0.02634 0.00076 -0.00276 0.00990 AFIX 137 H54A 2 0.995442 -0.081888 0.482577 11.00000 -1.50000 H54B 2 0.912956 -0.161055 0.486684 11.00000 -1.50000 H54C 2 0.849315 -0.079727 0.470194 11.00000 -1.50000 AFIX 0 C58 1 0.567244 0.900302 0.481337 11.00000 0.03820 0.01462 = 0.03644 -0.00227 0.00122 0.00002 AFIX 137 H58A 2 0.590624 0.937002 0.458363 11.00000 -1.50000 H58B 2 0.621307 0.909489 0.506874 11.00000 -1.50000 H58C 2 0.479983 0.909615 0.488577 11.00000 -1.50000 AFIX 0 C56 1 0.957942 -0.039811 0.312095 11.00000 0.03331 0.02887 = 0.02836 0.00589 0.00418 0.00589 AFIX 137 H56A 2 0.879681 -0.009913 0.314194 11.00000 -1.50000 H56B 2 0.958511 -0.068146 0.284497 11.00000 -1.50000 H56C 2 1.028703 -0.002731 0.313953 11.00000 -1.50000 AFIX 0 C64 1 0.226271 0.680268 0.485724 11.00000 0.02767 0.05543 = 0.02613 -0.00526 -0.00106 -0.00657 C53 1 0.605514 -0.021395 0.262324 11.00000 0.04111 0.03042 = 0.02862 -0.00332 0.00457 -0.00147 AFIX 137 H53A 2 0.548921 0.024144 0.258231 11.00000 -1.50000 H53B 2 0.634404 -0.039305 0.234283 11.00000 -1.50000 H53C 2 0.677499 -0.005302 0.280531 11.00000 -1.50000 AFIX 0 C52 1 0.475531 -0.309669 0.263066 11.00000 0.04339 0.02599 = 0.03817 -0.01110 -0.00129 0.00160 AFIX 137 H52A 2 0.409567 -0.342631 0.275152 11.00000 -1.50000 H52B 2 0.557051 -0.334241 0.269475 11.00000 -1.50000 H52C 2 0.462159 -0.305597 0.231793 11.00000 -1.50000 AFIX 0 C62 1 1.223242 0.672072 0.179778 11.00000 0.04585 0.03502 = 0.02902 0.00093 -0.00210 -0.00204 C61 1 1.155063 0.662185 0.218871 11.00000 0.03982 0.03742 = 0.04266 -0.01294 -0.00464 -0.01112 N8 4 1.100554 0.654017 0.249856 11.00000 0.07217 0.09473 = 0.05088 -0.01892 0.02470 -0.04219 C63 1 0.233405 0.763533 0.497205 11.00000 0.03733 0.04944 = 0.04003 -0.00793 0.00062 -0.00483 AFIX 137 H63A 2 0.258948 0.794676 0.472249 11.00000 -1.50000 H63B 2 0.294789 0.770656 0.520934 11.00000 -1.50000 H63C 2 0.151330 0.781900 0.506240 11.00000 -1.50000 AFIX 0 C60 1 0.813025 0.443167 0.309569 11.00000 0.07074 0.04287 = 0.02803 0.00435 -0.00218 0.01444 AFIX 13 H60 2 0.829550 0.419704 0.338792 11.00000 -1.20000 AFIX 0 H62A 2 1.271625 0.733812 0.179946 11.00000 0.07535 H62B 2 1.171870 0.666399 0.154616 11.00000 0.06339 H62C 2 1.296890 0.633308 0.178923 11.00000 0.06244 H4 2 0.889285 0.298698 0.415974 11.00000 0.01251 H7 2 0.422790 0.299103 0.361500 11.00000 0.01501 H5 2 0.749929 0.424677 0.416034 11.00000 0.03516 H6 2 0.536114 0.419513 0.389897 11.00000 0.02684 HKLF 4 REM exp_2723_a.res in P2(1)/c REM R1 = 0.0729 for 7729 Fo > 4sig(Fo) and 0.0916 for all 9836 data REM 723 parameters refined using 0 restraints END WGHT 0.0816 10.3701 REM Highest difference peak 0.729, deepest hole -1.279, 1-sigma level 0.081 Q1 1 0.8867 0.4982 0.3243 11.00000 0.05 0.73 Q2 1 0.9157 0.5183 0.3400 11.00000 0.05 0.63 Q3 1 0.6477 0.3019 0.3572 11.00000 0.05 0.52 Q4 1 0.6531 0.3025 0.4338 11.00000 0.05 0.50 Q5 1 0.2942 0.2936 0.3376 11.00000 0.05 0.39 Q6 1 0.8307 0.3752 0.3076 11.00000 0.05 0.36 Q7 1 0.9650 0.3124 0.4619 11.00000 0.05 0.35 Q8 1 0.3955 -0.2029 0.2822 11.00000 0.05 0.32 Q9 1 0.3608 0.3580 0.3407 11.00000 0.05 0.31 Q10 1 0.2350 0.2738 0.3206 11.00000 0.05 0.30 Q11 1 0.7996 0.2993 0.2744 11.00000 0.05 0.30 Q12 1 1.1277 0.3987 0.4805 11.00000 0.05 0.29 Q13 1 0.7849 0.4617 0.4599 11.00000 0.05 0.29 Q14 1 0.9324 -0.1160 0.4001 11.00000 0.05 0.29 Q15 1 0.9181 0.5174 0.2536 11.00000 0.05 0.28 Q16 1 0.4601 0.4612 0.3635 11.00000 0.05 0.28 Q17 1 0.5496 0.7865 0.4770 11.00000 0.05 0.27 Q18 1 0.6884 0.3568 0.3775 11.00000 0.05 0.26 Q19 1 0.8162 0.4264 0.2750 11.00000 0.05 0.26 Q20 1 0.6744 0.5615 0.3042 11.00000 0.05 0.25 ; _shelx_res_checksum 40212 _shelx_hkl_file ; 0 0 2 6.48 0.90 0 0 3 0.88 0.82 0 0 4 3267.64 56.99 0 0 5 8.08 2.68 0 0 6 811.16 20.57 0 0 7 31.49 4.82 0 0 8 1072.53 27.32 0 0 9 10.44 3.22 0 0 10 1472.92 36.79 0 0 11 8.52 4.52 0 0 12 1822.50 45.33 0 0 13 1.26 1.56 0 0 14 86.15 8.63 0 0 15 0.70 2.47 0 0 15 -1.95 1.89 0 0 16 33.50 6.08 0 0 16 32.71 4.81 0 0 17 3.13 2.43 0 0 17 1.16 1.31 0 0 18 150.44 13.36 0 0 19 2.29 2.23 0 0 20 189.36 16.19 0 0 21 1.25 2.09 0 0 22 2.41 3.00 0 0 23 3.39 2.77 0 0 24 80.27 7.36 0 0 24 77.79 6.73 0 0 24 83.42 12.20 0 0 25 -0.26 1.62 0 0 25 -0.74 1.60 0 0 26 64.73 6.96 0 0 26 70.38 6.73 0 0 27 1.07 1.81 0 0 27 2.13 2.31 0 0 28 28.74 4.63 0 0 28 25.09 4.02 0 0 29 -2.52 2.83 0 0 29 -1.23 1.46 0 0 30 18.26 3.59 0 0 30 23.69 4.74 0 0 31 3.93 2.50 0 0 31 0.19 1.98 0 0 32 9.35 2.35 0 0 32 3.53 2.00 0 0 33 1.96 1.79 0 0 33 6.58 2.85 0 0 34 46.24 4.81 0 0 34 46.36 5.49 0 0 35 -0.36 1.44 0 0 35 0.58 1.13 0 0 36 5.90 1.85 0 0 36 3.90 1.36 0 -1 0 0.38 0.50 0 1 -1 166.15 4.58 0 -1 1 175.26 4.78 0 -1 -1 174.56 4.96 0 -1 2 252.43 6.37 0 -1 2 264.15 7.38 0 1 2 276.25 6.25 0 1 -2 263.91 6.11 0 -1 2 280.10 6.30 0 -1 -2 275.26 6.17 0 -1 3 467.66 10.45 0 1 3 444.67 10.57 0 -1 3 467.04 10.01 0 -1 4 121.42 4.41 0 1 4 116.81 5.14 0 1 5 113.08 5.59 0 -1 5 105.03 4.49 0 1 6 12.16 2.60 0 -1 6 7.51 1.57 0 -1 7 423.69 11.91 0 1 7 429.08 14.15 0 1 8 1037.28 26.40 0 -1 8 1044.72 23.24 0 -1 9 307.79 14.19 0 -1 9 260.92 10.76 0 1 9 286.97 13.89 0 -1 10 2294.32 51.10 0 1 10 2350.51 50.31 0 -1 10 2296.57 45.27 0 1 11 326.88 15.03 0 -1 11 330.26 12.24 0 -1 11 309.76 15.17 0 -1 12 16.05 3.54 0 -1 12 12.22 2.44 0 1 12 18.71 4.13 0 -1 13 168.26 11.84 0 1 13 174.28 11.69 0 -1 13 179.48 9.31 0 -1 14 15.93 3.83 0 -1 14 18.77 3.21 0 1 14 17.74 4.00 0 -1 15 1133.31 29.81 0 1 15 1162.32 36.64 0 -1 15 1158.82 37.04 0 1 16 107.54 10.33 0 -1 16 117.81 11.01 0 -1 17 336.53 19.97 0 1 17 344.04 19.82 0 1 18 28.81 4.87 0 -1 18 30.01 6.56 0 1 18 32.67 6.55 0 1 19 2.21 2.34 0 -1 19 -1.83 2.04 0 1 20 0.25 2.24 0 -1 20 -0.85 2.85 0 -1 21 46.06 8.28 0 1 21 44.84 8.17 0 1 22 11.19 4.10 0 -1 22 8.13 4.31 0 1 23 353.95 24.37 0 -1 23 378.85 25.75 0 -1 24 11.43 5.23 0 1 24 6.76 2.32 0 -1 24 12.50 3.25 0 -1 24 11.12 3.19 0 1 24 12.76 3.15 0 1 25 36.28 5.03 0 1 25 36.73 5.07 0 -1 25 37.03 4.84 0 -1 25 34.84 4.97 0 1 26 63.51 6.52 0 -1 26 56.09 5.97 0 -1 26 62.95 6.78 0 1 26 57.57 6.52 0 1 27 16.24 3.81 0 -1 27 15.98 3.37 0 -1 27 17.62 3.37 0 1 27 18.50 3.90 0 -1 28 13.96 3.37 0 1 28 13.44 3.16 0 1 28 7.12 2.74 0 -1 28 9.87 2.75 0 -1 29 11.23 2.80 0 -1 29 8.42 2.91 0 1 29 5.11 2.29 0 1 29 8.88 2.94 0 -1 30 15.00 2.96 0 1 30 17.67 3.69 0 -1 30 22.78 4.52 0 1 30 27.21 4.84 0 -1 31 4.15 1.96 0 1 31 2.96 2.46 0 -1 31 6.65 2.94 0 1 31 1.89 2.02 0 1 32 1.59 1.70 0 -1 32 8.92 2.50 0 -1 32 6.25 3.03 0 1 32 5.68 2.65 0 1 33 97.36 7.49 0 -1 33 92.12 7.93 0 -1 33 86.96 6.60 0 1 33 103.48 8.27 0 -1 34 30.20 4.42 0 1 34 33.83 4.58 0 1 34 34.91 4.42 0 -1 35 2.81 1.70 0 1 35 5.46 2.17 0 -1 36 5.48 1.81 0 1 36 8.81 2.10 0 1 36 6.75 1.98 0 1 37 1.04 0.84 0 -2 0 641.27 16.71 0 -2 1 568.80 12.44 0 -2 -1 585.40 14.94 0 -2 2 388.11 10.27 0 -2 -2 371.75 10.58 0 -2 3 53.11 2.87 0 -2 3 52.90 3.69 0 2 3 54.51 2.43 0 -2 -3 54.34 3.31 0 -2 4 522.55 11.99 0 -2 4 511.44 14.38 0 -2 -4 487.98 11.77 0 -2 4 471.65 12.61 0 2 4 525.78 11.99 0 -2 -5 92.18 3.86 0 -2 5 85.91 4.39 0 2 5 88.94 4.72 0 -2 5 92.00 5.86 0 -2 5 83.00 4.54 0 -2 6 81.38 4.64 0 -2 -6 87.37 3.62 0 2 6 88.52 5.20 0 -2 6 80.22 4.65 0 -2 7 133.04 6.34 0 2 7 132.79 7.23 0 -2 -7 125.41 4.46 0 -2 7 126.45 6.58 0 -2 8 629.06 16.31 0 -2 8 650.20 17.45 0 2 8 645.45 18.53 0 -2 9 322.74 10.93 0 -2 9 320.51 11.78 0 -2 9 314.13 13.99 0 2 9 321.23 12.86 0 -2 10 520.02 18.86 0 2 10 511.24 17.24 0 -2 10 531.91 14.59 0 -2 11 2.50 2.57 0 2 11 0.46 1.67 0 -2 11 0.71 1.34 0 2 12 851.43 26.76 0 -2 12 823.81 22.30 0 -2 12 805.32 27.78 0 -2 13 26.51 3.68 0 2 13 30.47 4.94 0 -2 13 24.31 4.54 0 -2 14 109.18 9.98 0 2 14 118.48 9.94 0 -2 14 107.45 7.40 0 2 15 44.35 6.34 0 -2 15 36.56 6.06 0 -2 16 186.92 14.31 0 2 16 189.36 13.83 0 -2 17 94.52 10.72 0 2 17 94.13 9.96 0 2 18 137.73 12.61 0 -2 18 121.72 12.39 0 -2 19 340.65 21.83 0 2 19 389.43 22.13 0 2 20 182.54 15.53 0 -2 20 171.62 15.77 0 -2 21 13.70 4.65 0 2 21 10.64 4.47 0 -2 22 28.63 7.22 0 -2 23 18.95 6.23 0 2 24 3.84 1.85 0 -2 24 0.35 1.84 0 2 24 2.77 2.17 0 -2 25 464.60 17.56 0 2 25 514.40 19.41 0 -2 25 526.19 20.26 0 2 25 537.78 20.59 0 2 26 8.41 2.63 0 -2 26 2.87 2.11 0 2 26 5.56 2.64 0 -2 26 2.76 2.05 0 2 27 4.68 3.17 0 2 27 0.66 1.71 0 -2 27 2.30 1.59 0 -2 27 0.52 1.80 0 -2 28 139.35 9.03 0 2 28 161.00 11.03 0 2 28 152.23 10.42 0 -2 28 135.42 10.14 0 2 29 11.21 3.35 0 2 29 11.36 3.15 0 -2 29 14.24 3.42 0 2 30 28.56 4.47 0 2 30 30.71 5.01 0 -2 30 29.63 5.18 0 -2 31 14.10 3.41 0 2 31 8.32 2.79 0 2 31 14.38 3.59 0 2 32 15.92 3.33 0 -2 32 16.06 3.60 0 2 32 17.64 3.47 0 -2 33 17.27 3.49 0 2 33 16.16 3.48 0 2 33 15.69 3.41 0 2 34 17.30 3.09 0 2 34 18.51 3.49 0 -2 34 9.96 2.64 0 2 35 11.19 2.49 0 2 35 14.18 2.95 0 -2 35 9.90 2.32 0 -2 36 2.09 1.24 0 2 36 6.66 1.95 0 2 37 0.76 1.12 0 -3 0 1.07 1.49 0 -3 -1 11.73 2.47 0 -3 1 12.21 1.68 0 -3 2 323.69 9.90 0 -3 -2 300.98 11.50 0 -3 3 169.50 7.33 0 -3 -3 154.24 7.53 0 -3 4 48.30 4.22 0 -3 -4 39.93 3.58 0 -3 -5 544.17 14.53 0 -3 5 521.96 13.46 0 -3 5 537.10 16.49 0 3 5 546.21 12.38 0 -3 6 0.84 1.74 0 3 6 2.50 1.53 0 -3 -6 2.70 1.46 0 -3 6 2.25 1.16 0 -3 6 1.81 2.15 0 -3 7 734.35 17.86 0 3 7 753.47 18.75 0 -3 -7 736.43 16.61 0 -3 7 731.20 22.14 0 -3 8 480.36 17.95 0 -3 8 441.28 14.34 0 -3 -8 411.92 10.91 0 -3 8 443.16 13.39 0 3 8 460.73 14.62 0 -3 9 542.83 15.40 0 -3 9 556.28 16.20 0 3 9 538.72 16.72 0 -3 9 555.96 19.84 0 -3 10 153.13 10.50 0 3 10 147.87 8.85 0 -3 10 149.08 8.09 0 -3 10 134.46 7.51 0 -3 11 524.30 20.95 0 -3 11 507.76 16.39 0 3 11 493.88 18.26 0 -3 11 487.49 16.18 0 -3 12 111.75 9.69 0 3 12 109.85 8.51 0 -3 12 103.02 7.02 0 -3 12 114.25 7.26 0 3 13 96.51 8.35 0 -3 13 92.40 9.16 0 -3 13 80.92 6.42 0 3 14 125.26 10.04 0 -3 14 125.84 11.14 0 3 15 300.66 16.49 0 -3 15 298.75 17.95 0 -3 16 217.58 15.85 0 3 16 219.88 14.61 0 3 17 184.91 13.86 0 -3 17 164.84 14.37 0 3 18 41.69 6.98 0 -3 18 41.88 7.84 0 -3 19 45.01 8.34 0 -3 20 139.26 14.50 0 -3 21 91.40 12.09 0 -3 22 3.85 3.84 0 -3 23 42.38 8.83 0 -3 23 48.37 5.65 0 3 23 50.32 5.65 0 3 23 43.06 5.44 0 3 24 64.07 6.70 0 -3 24 60.23 6.44 0 3 24 56.41 6.31 0 3 25 318.14 15.55 0 3 25 323.68 15.07 0 -3 25 312.87 15.21 0 3 26 167.07 11.18 0 -3 26 163.99 11.03 0 3 26 162.25 10.85 0 3 27 47.81 5.90 0 3 27 38.67 5.37 0 -3 27 29.93 4.71 0 3 28 0.19 2.14 0 3 28 3.76 2.51 0 -3 28 1.82 1.63 0 -3 29 21.64 4.29 0 3 29 18.71 3.87 0 3 29 20.16 3.98 0 -3 30 45.77 5.83 0 3 30 41.77 5.36 0 3 30 43.08 5.67 0 -3 31 5.46 2.26 0 3 31 4.10 2.18 0 3 31 5.89 2.59 0 3 32 23.44 4.23 0 3 32 19.28 3.49 0 -3 32 23.41 4.15 0 3 33 1.52 1.82 0 -3 33 0.20 1.82 0 3 33 -0.79 2.20 0 -3 34 4.07 2.14 0 3 34 2.25 1.50 0 3 35 5.52 1.94 0 3 35 7.03 2.32 0 -3 35 3.31 1.86 0 3 36 76.72 5.73 0 3 37 9.53 1.95 0 -4 0 29.01 2.48 0 -4 1 68.52 4.44 0 -4 -2 222.11 11.54 0 -4 2 222.68 8.75 0 -4 -3 1613.81 37.76 0 -4 3 1673.49 34.73 0 -4 4 728.42 20.14 0 -4 -4 706.74 20.97 0 -4 -5 133.64 7.80 0 -4 5 113.44 7.44 0 -4 -6 102.83 6.53 0 -4 6 88.33 6.89 0 -4 7 301.68 13.66 0 -4 -7 292.60 11.08 0 -4 8 101.48 6.12 0 -4 8 113.64 9.39 0 4 8 105.28 5.88 0 -4 9 954.31 22.70 0 -4 9 913.04 28.75 0 4 9 913.41 22.70 0 4 10 1069.37 26.21 0 -4 10 1132.49 32.78 0 -4 11 18.43 3.09 0 -4 11 18.00 2.74 0 4 11 20.04 3.30 0 -4 11 23.99 4.81 0 4 12 244.83 12.28 0 -4 12 263.74 15.65 0 -4 13 26.54 5.53 0 4 13 25.22 4.07 0 -4 14 38.42 6.49 0 4 14 28.00 4.64 0 -4 15 28.96 6.07 0 -4 16 658.92 29.53 0 -4 17 449.39 24.55 0 -4 18 143.11 14.05 0 -4 19 140.89 14.37 0 -4 20 113.72 13.47 0 -4 21 22.89 6.15 0 -4 22 60.86 10.16 0 4 23 21.54 4.08 0 4 23 12.86 3.16 0 -4 24 48.11 5.70 0 4 24 53.42 6.26 0 4 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249.04 16.09 0 -5 14 1.84 2.39 0 -5 15 178.69 14.50 0 -5 16 26.64 6.14 0 -5 17 326.94 21.41 0 -5 18 8.57 4.07 0 -5 19 3.11 3.19 0 -5 20 1.09 2.78 0 -5 21 19.10 5.71 0 -5 22 -0.92 3.13 0 -5 23 139.65 9.52 0 5 23 149.81 10.07 0 5 23 142.34 9.91 0 -5 24 75.53 7.02 0 5 24 85.03 7.65 0 5 24 84.67 7.67 0 5 25 0.67 1.71 0 -5 25 -0.34 1.95 0 5 25 0.53 1.87 0 5 26 4.46 2.30 0 5 26 5.25 2.42 0 -5 26 4.09 2.05 0 5 27 0.71 2.26 0 5 27 1.05 1.61 0 -5 27 1.73 1.60 0 5 28 44.80 5.77 0 5 28 56.68 6.46 0 -5 28 42.58 5.43 0 5 29 3.74 2.63 0 -5 29 2.62 1.76 0 5 29 1.38 1.69 0 5 30 10.18 2.66 0 5 30 16.72 3.96 0 -5 30 19.11 3.50 0 -5 31 5.54 2.17 0 5 31 4.59 2.07 0 5 31 3.03 1.80 0 5 32 12.63 2.86 0 5 32 14.63 2.90 0 -5 32 12.88 2.65 0 -5 33 20.06 3.14 0 5 33 16.27 3.15 0 5 33 20.70 3.31 0 5 34 4.18 2.13 0 5 35 4.84 1.92 0 5 36 3.17 1.45 0 5 37 6.10 1.61 0 -6 0 1103.56 31.14 0 -6 0 984.93 23.10 0 -6 1 36.45 4.26 0 -6 1 35.98 5.68 0 -6 -1 31.87 3.01 0 -6 -1 32.62 5.59 0 -6 -2 1507.37 36.92 0 -6 2 1486.41 31.39 0 -6 -3 87.23 8.08 0 -6 3 96.86 8.55 0 -6 3 88.89 6.77 0 -6 -4 29.93 4.68 0 -6 4 32.62 4.36 0 -6 4 40.55 5.85 0 -6 5 11.37 3.00 0 -6 -5 11.46 4.06 0 -6 6 65.56 6.56 0 -6 7 8.44 3.26 0 -6 8 27.78 5.40 0 -6 9 437.50 19.83 0 -6 10 99.06 9.79 0 -6 11 11.63 3.47 0 -6 12 22.85 5.32 0 -6 13 17.24 4.75 0 -6 14 39.16 7.00 0 -6 15 111.70 11.82 0 -6 16 11.78 4.35 0 -6 17 52.42 8.41 0 -6 18 110.49 13.00 0 -6 19 8.47 4.11 0 -6 20 5.62 3.99 0 -6 21 13.27 6.02 0 6 22 14.28 3.50 0 6 23 32.55 5.03 0 -6 23 17.79 3.47 0 -6 24 47.04 5.49 0 6 24 54.98 6.30 0 -6 25 115.67 8.69 0 6 25 115.74 9.03 0 6 25 141.27 9.94 0 6 26 36.43 5.31 0 6 26 42.08 5.38 0 -6 26 37.73 5.00 0 6 27 8.24 2.66 0 6 27 11.33 3.43 0 -6 27 9.31 2.74 0 6 28 42.10 5.75 0 6 28 44.67 5.41 0 -6 28 43.59 5.25 0 6 29 134.70 9.59 0 -6 29 124.11 8.66 0 6 29 121.78 8.85 0 -6 30 20.96 3.47 0 6 30 30.91 4.29 0 6 30 34.01 5.02 0 6 31 5.73 2.25 0 6 31 6.01 2.19 0 -6 31 7.68 2.25 0 6 32 -0.39 1.07 0 -6 32 -0.25 1.26 0 6 32 -2.41 2.12 0 6 33 9.50 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2 -6 28 114.65 8.34 2 6 28 120.92 8.77 2 6 29 7.50 2.31 2 -6 29 8.63 2.36 2 6 30 19.97 4.15 2 6 30 15.16 3.12 2 -6 30 10.89 2.62 2 6 31 16.44 3.79 2 6 31 12.27 2.67 2 -6 31 14.32 2.94 2 6 32 9.42 3.07 2 -6 32 7.75 2.07 2 6 32 5.54 1.78 2 6 33 27.44 3.77 2 -6 33 22.53 2.97 2 6 34 -1.27 1.48 2 6 35 1.48 1.23 -2 7 35 0.75 1.00 -2 7 34 8.96 2.24 2 -7 -34 9.73 1.97 -2 7 33 4.07 1.75 2 -7 -33 3.32 1.56 -2 7 32 8.51 2.74 -2 7 31 39.58 4.73 -2 7 30 3.09 2.33 -2 7 29 4.68 2.31 -2 7 28 4.69 2.72 -2 7 27 28.14 4.76 -2 7 26 26.01 4.33 -2 7 25 91.19 8.11 -2 7 24 10.80 3.08 -2 7 23 118.85 9.15 -2 7 22 83.95 7.75 -2 7 21 119.95 9.07 -2 7 20 187.76 11.32 -2 -7 19 92.73 13.12 -2 -7 18 34.83 8.22 -2 -7 17 6.29 4.14 -2 -7 16 52.84 9.25 -2 -7 15 6.63 4.31 -2 -7 14 5.80 3.63 -2 -7 13 285.64 20.15 -2 -7 12 331.27 21.08 -2 -7 11 124.61 12.41 -2 -7 10 767.66 31.83 -2 -7 9 6.49 3.15 -2 -7 8 18.36 4.36 2 -7 -7 117.69 10.63 -2 -7 7 123.57 10.85 2 -7 -6 98.93 9.48 -2 -7 6 100.58 9.54 -2 -7 6 88.35 11.38 -2 -7 5 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4.41 3.60 -2 -7 -19 1.67 2.56 -2 -7 -20 13.34 4.09 -2 -7 -21 35.73 5.85 -2 -7 -22 261.29 15.43 -2 -7 -23 14.76 4.20 -2 -7 -24 11.40 3.98 -2 -7 -25 67.67 7.69 -2 -7 -26 -3.11 2.81 2 7 27 2.71 2.81 2 7 28 74.28 7.32 2 7 29 3.10 2.79 2 7 30 10.10 3.11 2 7 31 96.49 7.48 2 7 32 1.49 1.64 2 7 33 64.61 5.52 2 7 34 -1.18 1.39 2 7 35 4.77 1.49 -2 8 34 24.13 2.99 2 -8 -34 21.98 2.62 2 -8 -33 17.22 2.67 -2 8 33 17.65 2.88 2 -8 -32 33.04 4.04 -2 8 32 35.26 4.15 -2 8 31 21.50 3.54 2 -8 -31 18.67 3.30 -2 8 30 8.64 2.73 -2 8 29 7.08 2.69 -2 8 28 19.60 3.73 -2 8 27 36.39 5.19 -2 8 26 52.84 6.19 -2 8 25 -2.04 2.36 -2 8 24 17.83 3.55 -2 8 23 16.45 3.36 -2 8 22 16.18 3.39 -2 8 21 121.99 9.24 2 -8 -21 144.51 11.19 -2 8 20 29.83 4.79 2 -8 -20 40.38 6.24 2 -8 -19 3.71 3.07 -2 8 19 1.44 2.06 -2 -8 18 53.31 9.82 2 -8 -18 62.51 7.37 -2 -8 17 317.36 24.27 -2 -8 16 13.29 5.02 -2 -8 15 265.55 21.26 -2 -8 14 414.47 26.12 -2 -8 13 4.92 3.33 -2 -8 12 15.59 5.40 -2 -8 11 5.56 3.79 2 -8 -10 36.83 6.88 -2 -8 10 46.28 7.89 -2 -8 9 14.34 4.12 2 -8 -9 19.33 5.07 2 -8 -8 253.33 17.12 -2 -8 8 251.73 17.16 2 -8 -7 7.79 3.89 -2 -8 7 0.41 1.55 2 -8 -6 12.82 3.99 2 -8 -5 1.74 2.13 2 -8 -4 136.11 11.64 -2 -8 4 121.69 14.02 2 -8 -3 766.11 28.94 -2 -8 3 734.68 35.44 2 -8 -2 512.79 23.44 -2 -8 2 530.84 29.63 -2 -8 2 568.05 24.48 -2 -8 1 213.81 14.26 -2 -8 1 182.20 16.80 2 -8 -1 198.00 14.02 -2 -8 0 123.14 10.79 2 -8 0 122.55 10.90 -2 -8 0 107.44 12.88 -2 -8 -1 86.01 8.96 2 -8 1 86.20 9.19 -2 -8 -1 79.88 10.90 -2 -8 -2 14.03 4.86 2 -8 2 23.67 5.15 -2 -8 -2 25.29 4.98 2 -8 3 86.44 9.11 -2 -8 -3 64.35 7.77 -2 -8 -3 60.23 9.66 -2 -8 -4 192.38 16.74 -2 -8 -4 231.18 14.71 -2 -8 -5 521.15 22.92 2 -8 5 481.53 21.19 -2 -8 -6 81.90 10.99 -2 -8 -6 103.78 10.17 2 -8 6 111.10 10.00 -2 -8 -7 9.92 4.57 -2 -8 -7 12.00 3.96 2 -8 7 10.59 3.76 -2 -8 -8 18.79 4.38 -2 -8 -8 13.31 4.58 2 -8 8 21.76 5.05 -2 -8 -9 -0.38 1.85 2 -8 9 0.94 2.64 2 -8 10 27.52 5.75 -2 -8 -10 31.91 6.09 -2 -8 -11 103.46 11.40 2 -8 11 91.47 10.84 2 -8 12 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55.84 6.33 2 -9 -19 84.25 8.84 2 -9 -18 280.11 16.10 2 -9 -17 13.62 4.18 -2 -9 17 15.11 5.50 2 -9 -16 8.18 3.51 2 -9 -16 3.91 4.54 -2 -9 16 6.84 4.35 2 -9 -15 153.07 17.60 -2 -9 15 156.06 16.67 -2 -9 14 132.78 15.28 2 -9 -14 109.72 14.29 2 -9 -13 1.55 2.97 2 -9 -12 44.21 8.77 2 -9 -11 6.05 3.48 2 -9 -10 8.21 3.76 2 -9 -9 44.24 7.77 2 -9 -8 13.93 4.75 2 -9 -7 17.69 4.91 2 -9 -6 63.63 8.61 2 -9 -5 37.32 6.76 2 -9 -4 11.15 3.95 2 -9 -3 3.61 2.60 2 -9 -2 2.55 1.83 -2 -9 2 9.29 3.54 -2 -9 1 1.43 4.42 2 -9 -1 4.41 2.98 -2 -9 1 4.22 3.28 -2 -9 0 93.40 10.00 2 -9 0 96.05 10.38 -2 -9 0 82.31 12.30 -2 -9 -1 45.59 7.12 -2 -9 -1 32.92 8.09 2 -9 1 30.60 6.45 2 -9 2 42.49 7.09 -2 -9 -2 36.17 8.82 -2 -9 -2 59.51 8.71 2 -9 3 510.61 25.00 -2 -9 -3 545.36 25.24 2 -9 4 11.29 3.63 -2 -9 -4 15.44 6.14 -2 -9 -4 11.81 4.55 -2 -9 -5 39.59 6.57 -2 -9 -5 33.72 8.04 2 -9 5 26.86 5.15 2 -9 6 1269.76 39.80 -2 -9 -6 1307.28 41.77 2 -9 7 95.12 10.56 -2 -9 -7 104.85 11.30 -2 -9 -7 76.70 11.60 2 -9 8 413.89 22.26 -2 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2 -10 -27 63.20 6.41 -2 10 26 29.54 4.49 -2 10 25 14.50 3.31 2 -10 -24 2.74 2.80 -2 10 24 5.99 2.65 2 -10 -23 19.24 4.59 -2 10 23 25.29 4.12 2 -10 -22 3.89 2.81 2 -10 -21 53.34 6.84 2 -10 -20 18.23 4.76 2 -10 -19 25.37 5.37 2 -10 -18 38.94 6.40 2 -10 -17 18.55 5.09 2 -10 -16 5.17 3.67 -2 -10 15 248.96 14.66 2 -10 -15 225.55 14.46 2 -10 -14 100.68 14.20 -2 -10 14 103.46 9.22 2 -10 -14 107.77 9.75 2 -10 -13 11.03 4.51 2 -10 -12 2.61 3.24 2 -10 -11 123.25 14.34 2 -10 -10 38.00 7.78 2 -10 -9 13.11 4.90 2 -10 -8 5.32 3.12 2 -10 -7 42.79 7.47 2 -10 -6 1.14 2.83 2 -10 -5 37.76 7.22 2 -10 -4 117.35 12.24 2 -10 -3 141.71 13.40 2 -10 -2 464.23 24.88 2 -10 -1 106.29 11.69 -2 -10 1 98.43 11.72 -2 -10 0 11.06 4.95 2 -10 0 6.50 3.57 2 -10 1 66.35 9.22 -2 -10 -1 61.90 8.84 -2 -10 -2 198.30 15.64 2 -10 2 240.93 17.56 -2 -10 -3 156.51 14.01 -2 -10 -4 41.88 7.20 -2 -10 -5 74.64 9.75 -2 -10 -6 12.05 4.65 -2 -10 -7 110.67 12.05 -2 -10 -8 110.79 12.24 -2 -10 -9 7.42 3.87 -2 -10 -10 1.70 1.86 2 -10 10 0.38 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79.29 8.37 2 -11 -21 3.23 2.59 2 -11 -20 102.50 9.77 2 -11 -19 405.35 20.08 2 -11 -18 218.62 14.47 2 -11 -17 9.02 3.61 2 -11 -16 47.51 7.06 2 -11 -15 94.52 8.34 2 -11 -15 95.52 9.62 -2 -11 15 120.06 10.20 -2 -11 14 136.20 10.95 2 -11 -14 136.54 9.83 2 -11 -14 145.08 11.72 2 -11 -13 154.67 10.38 -2 -11 13 118.91 10.38 2 -11 -13 150.69 11.95 -2 -11 12 59.98 7.28 2 -11 -12 67.40 6.52 2 -11 -12 68.21 8.00 2 -11 -11 60.17 6.10 -2 -11 11 72.01 7.44 2 -11 -11 54.40 9.97 2 -11 -11 72.55 8.22 -2 -11 10 274.56 14.60 2 -11 -10 242.10 20.43 2 -11 -10 270.30 15.32 2 -11 -9 3.42 2.95 2 -11 -8 4.74 2.65 2 -11 -7 3.59 3.63 2 -11 -6 5.14 2.96 2 -11 -5 6.98 3.84 2 -11 -4 12.50 4.90 2 -11 -3 -1.15 1.84 2 -11 -2 107.40 12.38 2 -11 -1 40.50 7.66 2 -11 0 240.67 18.44 -2 -11 0 245.66 18.50 -2 -11 -1 7.01 4.26 2 -11 1 5.01 3.73 2 -11 2 59.40 9.41 -2 -11 -2 52.42 8.60 -2 -11 -3 26.29 6.27 -2 -11 -4 7.06 3.25 -2 -11 -5 1.76 2.06 -2 -11 -6 131.70 13.75 -2 -11 -7 150.73 14.94 -2 -11 -8 352.86 23.36 -2 -11 -9 3.11 3.25 -2 -11 -10 6.78 4.28 -2 -11 -10 3.07 3.25 -2 -11 -11 18.54 4.52 -2 -11 -11 23.88 6.58 -2 -11 -12 2.49 3.06 -2 -11 -12 3.01 3.32 -2 -11 -13 40.57 6.30 -2 -11 -14 6.34 4.03 -2 -11 -15 20.56 4.82 -2 -11 -16 55.93 7.86 -2 -11 -17 8.62 3.79 -2 -11 -18 164.05 13.12 -2 -11 -19 99.51 10.14 -2 -11 -20 24.11 5.19 2 11 21 14.12 3.43 -2 -11 -21 6.95 3.07 2 11 22 12.68 3.49 -2 -11 -22 14.20 4.08 2 11 23 286.70 13.55 -2 -11 -23 292.31 16.49 -2 -11 -24 3.34 2.88 2 11 24 1.66 1.74 -2 -11 -25 1.54 2.05 2 11 25 7.51 2.37 -2 -11 -26 1.12 2.27 2 11 26 0.08 1.42 2 11 27 25.20 3.66 -2 -11 -27 17.49 3.94 -2 -11 -28 1.09 1.83 2 11 28 2.28 1.53 -2 -11 -29 7.16 2.29 2 11 29 5.21 1.57 2 11 30 -0.78 1.37 2 -12 -30 91.51 5.60 2 -12 -29 1.58 1.37 2 -12 -28 13.08 2.72 2 -12 -27 2.85 1.71 2 -12 -26 1.46 1.64 2 -12 -26 6.16 2.67 2 -12 -25 1.37 1.76 2 -12 -25 3.55 2.47 2 -12 -24 0.97 2.05 2 -12 -24 1.47 2.33 2 -12 -23 4.96 2.58 2 -12 -23 4.53 1.89 2 -12 -22 12.96 3.84 2 -12 -22 7.69 2.76 2 -12 -21 15.45 4.08 2 -12 -21 17.58 3.65 2 -12 -20 1.10 2.03 2 -12 -20 2.63 2.77 2 -12 -19 12.00 3.60 2 -12 -19 18.06 4.84 2 -12 -18 69.74 8.43 2 -12 -18 73.57 7.59 2 -12 -18 74.12 8.68 2 -12 -17 26.09 5.54 2 -12 -17 20.52 4.87 2 -12 -17 25.55 4.55 2 -12 -16 63.01 6.82 2 -12 -16 51.35 7.22 2 -12 -16 72.17 8.39 2 -12 -15 10.21 4.56 2 -12 -15 13.63 4.23 2 -12 -15 16.98 3.68 -2 -12 15 17.41 4.47 -2 -12 14 32.67 6.01 2 -12 -14 25.21 5.06 2 -12 -14 24.23 5.09 2 -12 -14 29.77 4.68 2 -12 -13 2.08 2.67 -2 -12 13 5.11 2.76 2 -12 -13 2.14 1.70 2 -12 -13 3.31 2.49 2 -12 -12 82.98 7.61 -2 -12 12 82.84 8.64 2 -12 -12 90.34 9.04 2 -12 -12 76.94 8.73 -2 -12 11 4.57 2.88 2 -12 -11 4.43 2.27 2 -12 -11 2.75 2.41 2 -12 -11 7.74 2.65 -2 -12 10 33.58 5.20 2 -12 -10 32.06 5.51 2 -12 -10 35.56 4.71 2 -12 -10 41.34 5.89 -2 -12 9 102.54 9.13 2 -12 -9 117.20 9.64 2 -12 -9 112.92 8.25 2 -12 -9 105.06 9.63 2 -12 -8 10.35 3.65 2 -12 -8 8.88 2.39 -2 -12 8 6.76 2.75 2 -12 -8 9.31 3.44 -2 -12 8 13.11 5.26 2 -12 -7 194.21 10.78 -2 -12 7 178.66 11.60 2 -12 -7 189.85 18.07 2 -12 -7 214.41 12.62 -2 -12 7 192.65 12.92 2 -12 -7 202.89 13.14 2 -12 -6 43.98 5.54 -2 -12 6 45.81 5.96 2 -12 -6 40.81 5.84 -2 -12 6 53.52 6.95 2 -12 -6 44.44 8.79 2 -12 -5 65.99 6.66 2 -12 -5 73.53 7.73 -2 -12 5 76.01 7.46 -2 -12 5 82.29 8.20 2 -12 -5 67.74 10.59 -2 -12 4 9.92 3.05 2 -12 -4 14.78 5.08 2 -12 -3 11.55 4.88 2 -12 -2 40.63 8.12 2 -12 -1 17.49 6.06 2 -12 0 151.73 15.47 2 -12 1 215.04 18.42 -2 -12 -1 225.63 18.62 -2 -12 -2 13.47 5.18 -2 -12 -3 116.00 13.29 -2 -12 -4 -1.22 2.73 2 -12 5 9.95 3.00 -2 -12 -5 7.64 4.43 -2 -12 -6 41.73 8.29 2 -12 6 33.11 4.65 2 -12 7 391.03 16.25 -2 -12 -7 362.13 24.93 -2 -12 -7 389.53 18.44 2 -12 8 97.34 8.10 -2 -12 -8 106.83 13.59 -2 -12 -8 105.09 9.67 -2 -12 -9 7.49 3.32 2 -12 9 12.32 3.86 2 -12 10 11.27 3.19 -2 -12 -10 12.35 4.00 2 -12 11 66.81 6.72 -2 -12 -11 79.86 8.87 -2 -12 -12 73.86 8.79 -2 -12 -13 307.57 18.21 -2 -12 -14 18.81 5.04 -2 -12 -15 55.58 7.82 -2 -12 -16 1.48 3.12 -2 -12 -17 79.51 9.48 -2 -12 -18 85.56 9.65 -2 -12 -19 3.80 2.84 -2 -12 -20 5.79 2.78 -2 -12 -21 13.78 4.24 -2 -12 -22 30.09 5.79 -2 -12 -23 61.84 7.75 -2 -12 -24 40.19 6.04 -2 -12 -25 11.84 3.69 -2 -12 -26 23.94 4.19 -2 -12 -27 3.43 2.18 -2 -12 -28 1.04 1.58 -2 -12 -29 4.39 1.73 -2 -12 -29 3.85 1.57 -2 -12 -30 -0.53 0.84 2 -13 -29 2.90 1.27 2 -13 -28 5.71 1.66 2 -13 -27 -0.34 1.17 2 -13 -26 19.12 3.25 2 -13 -26 25.20 3.49 2 -13 -25 1.91 1.95 2 -13 -25 3.38 2.37 2 -13 -24 18.51 3.81 2 -13 -24 12.44 3.03 2 -13 -23 18.74 3.83 2 -13 -23 16.73 3.36 2 -13 -22 1.81 1.97 2 -13 -22 1.92 2.50 2 -13 -21 0.78 2.37 2 -13 -21 -1.84 2.35 2 -13 -20 1.93 1.87 2 -13 -20 2.64 2.59 2 -13 -19 31.07 5.60 2 -13 -19 28.42 4.62 2 -13 -18 11.03 3.91 2 -13 -18 17.06 4.10 2 -13 -18 18.49 5.21 2 -13 -17 59.69 7.74 2 -13 -17 76.25 8.49 2 -13 -17 73.88 7.44 2 -13 -16 20.22 4.97 2 -13 -16 22.24 4.97 2 -13 -16 23.00 4.33 2 -13 -15 30.34 5.64 2 -13 -15 41.76 5.64 2 -13 -15 42.96 6.67 -2 -13 14 1.59 2.50 2 -13 -14 6.45 3.13 2 -13 -14 2.15 2.48 2 -13 -14 3.33 2.07 -2 -13 13 64.26 8.07 2 -13 -13 76.85 7.41 2 -13 -13 70.04 8.21 2 -13 -13 65.63 8.29 -2 -13 12 115.55 10.18 2 -13 -12 119.50 10.50 2 -13 -12 104.51 8.48 2 -13 -12 102.26 9.89 2 -13 -11 141.58 11.42 -2 -13 11 115.92 10.37 2 -13 -11 131.43 9.37 2 -13 -11 127.37 11.33 2 -13 -10 3.53 3.19 2 -13 -10 7.40 2.86 -2 -13 10 6.05 3.43 2 -13 -10 10.84 3.65 2 -13 -9 11.61 3.76 -2 -13 9 12.19 3.86 2 -13 -9 16.99 3.58 2 -13 -9 15.51 3.65 -2 -13 8 157.96 12.51 2 -13 -8 186.42 12.21 -2 -13 8 162.13 11.68 2 -13 -8 184.65 12.87 2 -13 -8 184.44 10.67 2 -13 -7 -3.10 3.00 -2 -13 7 7.02 3.61 2 -13 -7 6.39 2.66 2 -13 -7 5.22 2.60 -2 -13 7 6.75 4.41 -2 -13 6 13.24 3.68 2 -13 -6 11.56 3.40 2 -13 -6 12.47 3.09 -2 -13 6 20.90 4.98 2 -13 -6 10.81 3.34 2 -13 -5 14.16 3.89 -2 -13 5 16.58 3.99 2 -13 -5 15.85 3.52 -2 -13 5 18.02 5.21 2 -13 -5 14.82 3.05 -2 -13 4 30.97 4.84 2 -13 -4 27.18 4.64 2 -13 -4 24.56 3.73 -2 -13 4 38.37 6.06 2 -13 -4 24.97 4.80 -2 -13 3 29.28 4.96 2 -13 -3 27.84 3.89 2 -13 -3 33.98 4.93 -2 -13 3 28.44 5.22 2 -13 -3 35.43 5.54 2 -13 -2 127.45 9.28 -2 -13 2 140.07 10.23 2 -13 -2 137.19 10.14 -2 -13 2 136.75 10.19 2 -13 -1 38.56 5.55 2 -13 -1 39.10 5.08 -2 -13 1 31.78 5.13 -2 -13 1 30.82 4.89 2 -13 0 24.34 4.20 -2 -13 0 23.38 4.66 -2 -13 0 25.17 4.47 2 -13 0 23.93 4.27 2 -13 1 25.24 4.31 -2 -13 -1 30.01 4.90 -2 -13 -1 18.56 3.68 2 -13 1 24.70 4.18 -2 -13 -2 21.05 4.40 -2 -13 -2 12.00 3.38 2 -13 2 21.57 4.12 -2 -13 -3 57.15 6.75 2 -13 3 55.18 6.15 -2 -13 -4 48.61 6.19 2 -13 4 43.12 5.35 -2 -13 -5 23.64 4.36 2 -13 5 17.11 3.45 -2 -13 -5 21.40 4.35 2 -13 6 5.75 2.43 -2 -13 -6 7.59 2.88 -2 -13 -6 7.07 2.89 2 -13 7 48.51 5.81 -2 -13 -7 41.52 5.66 -2 -13 -7 44.64 6.58 2 -13 8 4.64 2.58 -2 -13 -8 6.87 3.32 2 -13 9 18.85 3.65 -2 -13 -9 18.95 4.67 2 -13 10 -0.57 1.54 -2 -13 -10 3.33 2.58 -2 -13 -11 131.91 11.55 2 -13 11 147.39 10.30 -2 -13 -12 8.93 4.07 2 -13 12 3.53 2.31 -2 -13 -13 16.49 4.89 -2 -13 -14 20.30 5.28 -2 -13 -15 191.47 14.48 -2 -13 -16 1.20 2.78 -2 -13 -17 24.38 5.36 -2 -13 -18 42.79 6.94 -2 -13 -19 43.02 6.81 -2 -13 -20 23.49 5.51 -2 -13 -21 49.26 7.02 -2 -13 -22 9.39 3.10 -2 -13 -23 77.80 8.00 -2 -13 -24 5.28 3.11 -2 -13 -25 2.69 2.27 -2 -13 -25 -3.57 2.08 -2 -13 -26 8.29 2.82 -2 -13 -26 4.45 1.69 -2 -13 -27 89.88 6.36 -2 -13 -27 105.94 7.12 -2 -13 -28 63.06 4.95 -2 -13 -28 57.24 4.62 2 -14 -27 2.37 1.34 2 -14 -26 19.67 2.82 2 -14 -26 16.96 2.73 2 -14 -25 14.00 2.73 2 -14 -25 16.35 2.85 2 -14 -24 5.76 2.15 2 -14 -24 11.37 2.92 2 -14 -23 38.06 4.96 2 -14 -23 28.54 4.20 2 -14 -22 19.24 3.56 2 -14 -22 19.70 3.88 2 -14 -21 -2.92 1.86 2 -14 -21 -0.80 2.25 2 -14 -20 16.68 4.20 2 -14 -20 13.94 3.16 2 -14 -19 10.12 2.91 2 -14 -19 3.76 2.73 2 -14 -18 5.89 3.56 2 -14 -18 4.50 2.55 2 -14 -18 3.54 2.44 2 -14 -17 67.86 7.88 2 -14 -17 87.21 8.99 2 -14 -17 84.91 7.82 2 -14 -16 133.65 11.39 2 -14 -16 116.38 9.10 2 -14 -15 77.08 7.38 2 -14 -15 53.81 7.29 2 -14 -15 76.03 8.61 2 -14 -14 1.74 2.74 -2 -14 14 8.49 4.07 2 -14 -14 9.72 3.17 2 -14 -14 7.39 2.71 2 -14 -13 46.29 7.23 2 -14 -13 51.18 7.00 -2 -14 13 50.86 6.97 2 -14 -13 46.11 5.60 2 -14 -12 97.54 9.77 2 -14 -12 89.98 9.10 2 -14 -12 91.10 7.75 -2 -14 12 94.30 9.27 -2 -14 11 127.13 10.77 2 -14 -11 117.55 10.42 2 -14 -11 121.14 9.06 2 -14 -11 124.92 10.95 -2 -14 10 36.94 5.82 2 -14 -10 47.82 6.58 2 -14 -10 43.33 6.94 2 -14 -10 42.80 5.29 2 -14 -9 52.97 5.68 2 -14 -9 59.29 7.61 -2 -14 9 53.66 7.00 2 -14 -9 45.86 6.16 -2 -14 8 15.55 4.26 2 -14 -8 17.56 3.53 2 -14 -8 19.31 4.84 2 -14 -8 27.62 5.28 -2 -14 7 169.06 12.06 2 -14 -7 172.31 11.87 2 -14 -7 166.43 9.96 2 -14 -7 182.79 12.77 -2 -14 6 20.36 4.89 2 -14 -6 21.85 4.59 2 -14 -6 15.21 3.29 2 -14 -6 11.10 3.85 -2 -14 5 153.17 11.30 2 -14 -5 151.62 10.68 -2 -14 5 149.45 11.86 2 -14 -5 133.39 8.61 2 -14 -5 146.01 11.06 -2 -14 4 117.62 10.24 -2 -14 4 118.75 9.86 2 -14 -4 120.16 9.42 2 -14 -4 109.61 7.68 2 -14 -4 115.93 9.60 -2 -14 3 85.96 8.72 -2 -14 3 72.01 7.93 2 -14 -3 77.23 7.56 2 -14 -3 67.33 7.35 2 -14 -2 2.07 2.56 -2 -14 2 7.07 3.09 2 -14 -2 4.55 2.86 -2 -14 2 5.58 3.74 -2 -14 1 83.66 8.30 2 -14 -1 75.53 7.22 -2 -14 1 82.73 8.00 2 -14 -1 68.60 7.22 2 -14 0 4.76 2.74 -2 -14 0 0.18 2.05 -2 -14 0 1.11 2.09 2 -14 0 1.83 2.16 -2 -14 -1 8.66 3.70 2 -14 1 6.65 2.92 -2 -14 -1 2.79 2.71 -2 -14 -2 24.94 5.10 2 -14 2 29.87 4.68 -2 -14 -2 29.21 4.85 2 -14 3 49.50 5.69 -2 -14 -3 46.01 6.31 -2 -14 -3 32.82 4.69 -2 -14 -4 24.37 4.87 2 -14 4 17.96 3.71 -2 -14 -4 22.36 4.05 2 -14 5 44.45 5.39 -2 -14 -5 48.87 6.48 -2 -14 -5 43.42 5.58 -2 -14 -5 50.52 6.26 -2 -14 -6 -0.20 2.06 -2 -14 -6 1.17 2.09 2 -14 6 -0.97 1.94 -2 -14 -7 9.29 3.46 2 -14 7 16.37 3.60 -2 -14 -7 13.46 4.13 2 -14 8 77.99 7.47 -2 -14 -8 99.05 9.53 2 -14 9 1.33 2.01 -2 -14 -9 10.08 4.01 -2 -14 -10 4.29 3.55 2 -14 10 5.38 2.44 2 -14 11 15.52 3.51 -2 -14 -11 18.91 5.00 2 -14 12 7.64 3.15 -2 -14 -12 13.71 4.49 -2 -14 -13 -1.34 3.16 -2 -14 -14 47.63 7.36 -2 -14 -15 36.83 7.11 -2 -14 -16 43.83 6.85 -2 -14 -17 29.58 6.24 -2 -14 -18 0.27 3.47 -2 -14 -19 157.81 12.70 -2 -14 -20 35.56 6.12 -2 -14 -21 18.27 3.31 -2 -14 -21 33.03 5.99 -2 -14 -22 14.23 4.08 -2 -14 -22 11.13 2.71 -2 -14 -23 28.61 3.89 -2 -14 -23 50.87 6.24 -2 -14 -24 3.48 2.61 -2 -14 -24 0.67 1.34 -2 -14 -25 34.80 3.86 -2 -14 -25 52.62 5.46 -2 -14 -26 2.28 1.55 2 -15 -25 0.35 0.99 2 -15 -24 5.94 2.07 2 -15 -24 2.18 1.45 2 -15 -23 9.11 2.50 2 -15 -23 7.54 2.13 2 -15 -22 5.47 2.46 2 -15 -22 4.28 1.84 2 -15 -21 77.39 6.42 2 -15 -21 89.01 7.51 2 -15 -20 1.71 2.25 2 -15 -20 1.43 1.89 2 -15 -19 7.74 3.45 2 -15 -19 11.00 2.79 2 -15 -18 22.76 4.65 2 -15 -18 21.39 3.93 2 -15 -17 3.20 3.18 2 -15 -17 -0.72 1.73 2 -15 -17 1.26 1.94 2 -15 -16 1.72 1.97 2 -15 -16 4.24 2.67 2 -15 -16 0.21 2.79 2 -15 -15 76.69 8.23 2 -15 -15 86.11 7.37 2 -15 -15 93.13 9.26 2 -15 -14 1.37 1.83 2 -15 -14 -0.35 1.74 2 -15 -14 0.46 2.68 -2 -15 13 18.15 4.44 2 -15 -13 13.67 3.15 2 -15 -13 12.92 4.02 2 -15 -13 17.52 4.89 -2 -15 12 26.19 5.37 2 -15 -12 18.24 4.30 2 -15 -12 28.12 4.33 2 -15 -12 21.18 4.75 -2 -15 11 132.37 10.71 2 -15 -11 153.38 11.75 2 -15 -11 133.25 9.10 2 -15 -11 132.73 11.16 2 -15 -10 18.97 4.65 2 -15 -10 16.41 3.35 -2 -15 10 13.96 4.07 2 -15 -10 19.23 4.38 -2 -15 9 0.52 2.61 2 -15 -9 12.62 3.78 2 -15 -9 8.13 2.39 2 -15 -9 8.59 3.09 2 -15 -8 38.25 6.60 -2 -15 8 36.90 6.66 2 -15 -8 33.85 4.58 2 -15 -8 38.40 6.45 -2 -15 7 56.74 7.28 2 -15 -7 65.50 5.95 2 -15 -7 67.37 7.89 -2 -15 6 76.48 8.35 2 -15 -6 82.71 8.22 2 -15 -6 88.68 8.68 2 -15 -6 73.89 6.34 -2 -15 5 149.72 11.96 2 -15 -5 149.57 11.02 2 -15 -5 165.51 11.37 2 -15 -4 13.24 3.46 -2 -15 4 18.96 4.64 2 -15 -4 20.28 4.34 -2 -15 4 29.23 6.12 -2 -15 3 64.04 7.62 2 -15 -3 76.96 7.58 -2 -15 3 71.66 8.68 2 -15 -3 77.75 7.73 2 -15 -2 22.26 4.88 2 -15 -2 13.76 4.22 -2 -15 2 30.44 5.96 -2 -15 2 28.13 6.53 -2 -15 1 120.88 10.19 2 -15 -1 107.46 8.97 -2 -15 1 124.73 10.41 2 -15 -1 106.02 8.62 -2 -15 0 52.67 6.87 2 -15 0 44.14 5.81 -2 -15 0 49.31 6.62 2 -15 0 42.65 5.43 2 -15 1 7.86 2.81 -2 -15 -1 10.10 3.57 -2 -15 -1 12.02 4.10 -2 -15 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10.31 3.82 2 -16 -5 7.16 3.39 -2 -16 5 5.42 3.62 2 -16 -5 6.41 3.26 2 -16 -4 37.09 5.35 -2 -16 4 36.62 5.70 2 -16 -4 38.36 5.62 2 -16 -3 6.85 2.83 -2 -16 3 2.30 2.15 2 -16 -3 4.35 2.16 2 -16 -2 9.51 3.00 -2 -16 2 11.52 4.44 2 -16 -2 5.20 2.00 -2 -16 2 15.38 4.43 -2 -16 1 12.92 3.86 2 -16 -1 10.13 3.34 -2 -16 1 18.49 5.07 -2 -16 0 74.12 8.39 -2 -16 0 75.73 8.38 2 -16 0 76.14 7.56 -2 -16 -1 213.37 13.70 -2 -16 -1 231.17 14.40 2 -16 1 192.63 12.05 -2 -16 -2 100.19 9.49 2 -16 2 106.05 8.72 -2 -16 -2 108.30 9.68 -2 -16 -3 44.06 6.45 2 -16 3 32.81 4.80 -2 -16 -3 37.96 6.05 -2 -16 -4 5.22 2.83 2 -16 4 1.28 1.91 -2 -16 -4 4.56 2.93 -2 -16 -5 3.46 3.58 2 -16 5 1.16 2.19 -2 -16 -5 5.63 2.71 2 -16 6 -1.39 2.20 -2 -16 -6 3.97 2.98 -2 -16 -6 9.27 3.32 -2 -16 -7 -2.22 2.52 -2 -16 -7 0.35 2.06 2 -16 7 -2.56 2.03 -2 -16 -7 -3.59 3.17 -2 -16 -8 -2.03 2.97 -2 -16 -8 3.31 2.49 -2 -16 -8 3.75 3.12 2 -16 8 2.14 2.19 2 -16 9 13.52 3.16 -2 -16 -9 13.90 3.33 -2 -16 -9 11.04 3.03 -2 -16 -10 39.40 6.07 2 -16 10 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-24 38.08 4.62 3 -13 -23 14.47 3.42 3 -13 -23 14.95 3.39 3 -13 -22 19.31 4.12 3 -13 -22 18.33 3.89 3 -13 -21 36.73 5.17 3 -13 -21 55.82 6.52 3 -13 -20 8.64 3.49 3 -13 -20 6.44 3.04 3 -13 -20 2.55 2.06 3 -13 -19 5.43 2.77 3 -13 -19 10.70 3.35 3 -13 -19 4.27 2.92 3 -13 -18 43.19 6.48 3 -13 -18 36.77 6.11 3 -13 -18 41.31 5.55 3 -13 -17 110.10 10.59 3 -13 -17 124.72 9.77 3 -13 -17 133.21 11.12 3 -13 -16 10.38 4.18 3 -13 -16 9.21 3.58 3 -13 -16 12.47 3.33 3 -13 -15 8.27 3.11 3 -13 -15 12.60 3.85 3 -13 -15 8.05 3.70 3 -13 -14 20.88 4.71 3 -13 -14 17.01 3.94 3 -13 -14 21.36 4.30 3 -13 -13 6.91 2.76 3 -13 -13 9.02 3.00 3 -13 -12 5.72 2.72 -3 -13 12 9.91 3.67 3 -13 -12 10.49 3.67 3 -13 -12 7.84 2.74 -3 -13 11 4.27 2.38 3 -13 -11 -2.18 2.86 3 -13 -11 3.78 2.83 3 -13 -11 -0.54 2.38 -3 -13 10 21.99 5.00 3 -13 -10 15.53 4.79 3 -13 -10 18.92 4.21 3 -13 -10 18.11 3.67 3 -13 -9 7.69 3.83 -3 -13 9 4.14 2.88 3 -13 -9 2.34 2.35 3 -13 -9 5.64 2.40 -3 -13 8 125.40 11.28 -3 -13 8 101.70 9.76 3 -13 -8 124.97 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7.30 -4 -6 -27 100.55 8.67 -4 -6 -28 24.27 4.33 4 6 28 28.83 4.23 4 -6 28 20.98 3.46 4 6 29 32.65 4.88 4 6 29 24.62 3.65 4 -6 29 23.21 3.49 4 6 30 3.02 1.33 4 -6 30 0.27 1.16 4 6 31 27.47 4.02 4 -6 31 12.04 2.25 4 6 32 91.36 6.57 4 -6 32 70.90 4.89 4 6 33 47.36 4.38 4 6 34 1.88 1.37 -4 7 34 3.71 1.26 -4 7 33 2.02 1.26 -4 7 32 67.37 5.52 -4 7 31 2.86 1.26 -4 7 30 15.58 3.01 4 -7 -30 19.93 3.20 -4 7 29 11.07 2.70 4 -7 -29 6.72 2.28 -4 7 28 0.10 1.73 4 -7 -28 0.57 1.41 -4 7 27 0.96 1.65 4 -7 -27 -0.13 1.43 -4 7 26 10.28 3.15 4 -7 -26 12.21 3.05 -4 7 25 1.62 2.04 4 -7 -25 4.12 2.31 -4 7 24 138.49 10.18 4 -7 -24 127.69 9.59 -4 7 23 3.28 2.26 4 -7 -23 0.40 1.98 -4 7 22 5.79 2.76 4 -7 -22 1.20 1.70 -4 7 21 7.54 2.93 -4 7 20 10.60 3.11 -4 7 19 16.75 3.95 -4 7 18 3.75 2.52 -4 7 17 6.96 2.90 -4 -7 17 3.89 2.65 -4 -7 16 113.06 14.39 -4 -7 15 214.73 19.75 -4 -7 14 24.01 6.80 -4 -7 14 28.47 7.31 -4 -7 13 -0.53 3.51 -4 -7 13 -1.82 3.34 -4 -7 12 10.11 3.69 -4 -7 11 15.12 4.82 -4 -7 11 7.01 4.63 4 -7 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29 57.82 5.31 -4 -9 -29 40.58 4.67 4 9 30 2.03 1.70 4 9 31 0.17 1.18 4 -10 -30 5.37 1.73 4 -10 -29 22.34 3.17 4 -10 -28 27.20 3.70 4 -10 -27 1.51 1.47 4 -10 -26 1.86 1.86 4 -10 -25 5.59 2.29 4 -10 -24 26.42 4.63 4 -10 -23 11.21 3.15 4 -10 -22 6.75 2.86 4 -10 -21 8.03 3.46 4 -10 -21 8.58 2.96 4 -10 -20 75.75 7.68 4 -10 -20 77.09 8.16 4 -10 -19 3.73 2.59 4 -10 -19 0.44 2.24 4 -10 -18 44.67 6.56 4 -10 -18 41.62 5.66 4 -10 -17 0.32 2.56 4 -10 -17 0.15 1.76 4 -10 -16 32.19 5.75 4 -10 -16 29.54 4.90 4 -10 -15 4.24 2.78 4 -10 -15 3.55 3.21 4 -10 -14 51.64 6.13 4 -10 -14 54.59 7.09 4 -10 -13 63.66 6.71 4 -10 -13 64.22 7.83 4 -10 -12 162.18 10.48 4 -10 -12 151.14 11.65 4 -10 -11 10.91 4.34 4 -10 -11 11.00 3.47 4 -10 -11 8.96 4.90 4 -10 -10 106.13 8.23 -4 -10 10 102.07 9.17 -4 -10 10 117.44 10.67 4 -10 -10 82.21 11.62 4 -10 -10 114.60 9.87 -4 -10 9 4.47 3.01 4 -10 -9 0.75 2.04 4 -10 -9 3.97 2.04 4 -10 -9 0.14 2.74 4 -10 -8 14.66 4.97 4 -10 -7 170.33 15.61 4 -10 -6 73.12 9.92 -4 -10 5 26.80 8.77 4 -10 -5 27.87 6.19 4 -10 -4 6.69 3.89 -4 -10 4 4.96 4.89 -4 -10 3 5.25 4.55 4 -10 -3 0.42 1.89 -4 -10 2 47.35 11.19 4 -10 -2 41.98 7.40 -4 -10 1 23.49 8.06 4 -10 -1 23.21 5.72 4 -10 0 62.71 9.12 -4 -10 0 52.37 11.49 -4 -10 -1 219.46 23.25 -4 -10 -2 195.14 22.00 -4 -10 -3 46.89 11.68 -4 -10 -4 180.36 21.23 -4 -10 -5 11.07 7.51 -4 -10 -6 28.33 8.77 4 10 6 38.64 8.20 4 10 7 96.85 12.36 4 10 8 69.29 10.81 4 -10 8 47.87 8.46 -4 -10 -9 4.50 3.26 4 -10 9 11.38 5.05 4 -10 10 314.70 13.84 4 -10 10 265.39 20.83 -4 -10 -10 281.18 16.88 4 -10 11 1.19 1.48 -4 -10 -11 0.38 2.06 4 -10 12 20.97 3.53 -4 -10 -12 22.28 5.19 4 -10 13 15.05 3.09 -4 -10 -13 16.51 4.81 -4 -10 -14 113.06 11.26 4 -10 14 115.72 8.60 4 -10 15 4.21 2.14 -4 -10 -15 10.13 4.44 4 -10 16 1.98 1.80 -4 -10 -16 4.55 3.19 4 -10 17 1.83 1.53 -4 -10 -17 8.17 3.79 -4 -10 -18 52.05 7.72 -4 -10 -19 8.17 4.26 -4 -10 -20 28.06 5.68 -4 -10 -21 3.07 3.44 -4 -10 -22 63.12 8.06 -4 -10 -23 15.35 4.44 -4 -10 -24 54.52 6.76 -4 -10 -25 2.36 2.49 -4 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7.14 3.61 4 -11 -8 45.10 5.63 -4 -11 8 50.89 6.93 -4 -11 8 56.07 8.07 4 -11 -8 52.52 7.25 4 -11 -7 15.71 4.87 -4 -11 7 18.92 4.21 4 -11 -7 17.77 4.58 4 -11 -7 19.55 3.63 -4 -11 7 21.73 4.83 4 -11 -6 1.92 3.23 -4 -11 6 2.74 2.38 4 -11 -6 3.81 2.64 -4 -11 6 2.57 2.61 4 -11 -6 -0.39 2.17 -4 -11 5 140.43 10.53 4 -11 -5 118.14 13.62 4 -11 -5 138.75 9.13 -4 -11 5 142.83 10.44 4 -11 -5 144.69 10.93 4 -11 -4 9.97 3.81 -4 -11 4 7.79 3.54 4 -11 -4 1.03 1.67 -4 -11 4 9.49 3.61 4 -11 -4 5.37 3.64 4 -11 -3 97.54 7.44 -4 -11 3 100.32 8.50 4 -11 -3 98.44 11.87 4 -11 -3 98.32 8.73 4 -11 -2 14.02 4.32 4 -11 -2 9.47 3.02 4 -11 -2 7.63 3.82 -4 -11 2 13.02 3.50 -4 -11 1 105.95 17.12 4 -11 -1 144.80 10.27 -4 -11 0 45.28 11.45 -4 -11 -1 498.97 37.90 -4 -11 -2 51.53 12.93 4 -11 3 241.52 11.80 -4 -11 -3 207.46 24.40 4 -11 4 129.21 8.59 -4 -11 -4 136.40 19.94 4 -11 5 41.99 4.88 4 -11 5 33.56 4.59 4 -11 6 14.06 3.03 -4 -11 -6 22.63 4.56 4 -11 7 35.92 4.65 -4 -11 -7 44.20 6.49 -4 -11 -8 3.26 3.00 4 -11 8 1.17 1.73 4 -11 9 636.07 20.96 -4 -11 -9 624.08 25.98 4 -11 10 143.23 9.25 -4 -11 -10 124.36 11.50 -4 -11 -11 6.27 3.74 4 -11 11 2.14 1.93 4 -11 12 1.07 1.74 -4 -11 -12 0.65 2.30 -4 -11 -13 67.98 9.09 4 -11 13 74.88 6.75 -4 -11 -14 65.15 9.05 4 -11 14 61.62 6.24 -4 -11 -15 4.13 3.32 -4 -11 -16 4.94 3.12 -4 -11 -17 45.49 7.99 -4 -11 -18 117.80 11.64 -4 -11 -19 143.22 12.51 -4 -11 -20 5.31 3.66 -4 -11 -21 94.72 10.03 -4 -11 -22 36.76 6.02 -4 -11 -23 24.50 4.82 -4 -11 -24 26.22 4.76 4 11 24 26.34 3.76 -4 -11 -25 31.20 4.87 4 11 25 27.22 3.79 -4 -11 -26 6.92 2.70 4 11 26 10.00 2.48 -4 -11 -27 37.57 4.77 4 11 27 41.98 4.10 -4 -11 -28 25.39 3.68 4 11 28 33.89 3.43 -4 -11 -29 7.92 2.01 4 11 29 4.12 1.27 4 -12 -28 17.41 2.57 4 -12 -27 4.53 1.82 4 -12 -26 3.63 1.77 4 -12 -25 9.27 2.54 4 -12 -24 9.50 2.53 4 -12 -23 32.12 4.72 4 -12 -23 31.57 4.74 4 -12 -23 34.85 4.75 4 -12 -22 20.18 4.12 4 -12 -22 20.45 4.30 4 -12 -22 17.08 3.65 4 -12 -21 11.90 3.55 4 -12 -21 16.21 4.01 4 -12 -21 11.93 3.52 4 -12 -20 65.61 6.87 4 -12 -20 55.69 7.36 4 -12 -20 77.75 7.78 4 -12 -19 79.81 7.85 4 -12 -19 83.58 8.37 4 -12 -18 11.46 4.09 4 -12 -18 11.20 3.36 4 -12 -17 18.19 4.26 4 -12 -17 14.51 4.37 4 -12 -16 6.96 3.28 4 -12 -16 5.48 2.92 4 -12 -15 16.14 4.62 4 -12 -15 13.31 3.61 4 -12 -14 8.47 4.22 4 -12 -14 4.40 3.18 4 -12 -13 20.42 4.70 4 -12 -13 32.26 5.08 4 -12 -12 -2.19 2.45 4 -12 -12 2.65 1.95 4 -12 -11 25.40 4.54 4 -12 -11 21.88 4.63 4 -12 -10 2.94 3.42 -4 -12 10 2.59 3.27 4 -12 -10 2.05 2.36 4 -12 -9 4.77 3.36 -4 -12 9 2.00 2.26 4 -12 -9 2.60 2.35 -4 -12 9 6.89 4.58 4 -12 -8 3.25 3.22 -4 -12 8 3.44 2.52 4 -12 -8 1.52 1.70 4 -12 -7 6.46 3.65 -4 -12 7 6.62 3.29 4 -12 -7 5.71 2.59 -4 -12 7 11.10 4.23 -4 -12 6 3.01 2.95 4 -12 -6 9.53 3.83 4 -12 -6 4.44 2.50 -4 -12 6 2.88 3.18 -4 -12 5 68.00 7.64 4 -12 -5 64.47 6.76 4 -12 -5 62.14 6.21 -4 -12 5 70.84 7.85 4 -12 -5 69.62 7.94 4 -12 -4 56.35 7.30 4 -12 -4 41.86 5.41 -4 -12 4 52.67 7.03 4 -12 -4 57.84 6.74 -4 -12 4 51.25 6.66 4 -12 -3 13.91 4.54 -4 -12 3 10.40 3.60 4 -12 -3 10.30 3.46 4 -12 -3 9.77 3.76 -4 -12 3 7.74 3.87 4 -12 -2 79.72 7.15 -4 -12 2 65.32 7.56 4 -12 -2 72.52 7.01 -4 -12 2 72.10 7.42 4 -12 -2 88.49 8.61 4 -12 -1 442.24 17.00 -4 -12 1 431.15 19.68 4 -12 -1 444.58 17.73 -4 -12 1 469.20 18.92 4 -12 -1 455.23 19.59 -4 -12 0 14.85 4.32 4 -12 0 14.28 3.53 4 -12 0 10.35 3.36 -4 -12 0 15.51 4.84 -4 -12 -1 5.24 2.65 4 -12 1 8.57 3.19 4 -12 1 6.00 2.51 -4 -12 -2 10.73 3.65 4 -12 2 13.26 3.64 4 -12 2 12.37 3.41 4 -12 3 156.61 9.42 4 -12 3 140.64 9.22 4 -12 4 11.16 3.22 4 -12 4 9.79 3.20 4 -12 5 200.51 10.85 4 -12 5 186.16 10.71 4 -12 6 239.22 11.91 4 -12 6 229.12 11.91 -4 -12 -6 238.77 14.26 4 -12 7 5.73 2.40 -4 -12 -7 11.29 3.64 4 -12 8 95.05 7.31 -4 -12 -8 101.67 9.81 4 -12 9 7.74 2.54 -4 -12 -9 8.14 3.76 4 -12 10 58.37 5.79 -4 -12 -10 51.81 7.43 4 -12 11 31.75 4.38 -4 -12 -11 32.47 6.40 -4 -12 -12 50.03 7.71 -4 -12 -13 26.88 5.97 -4 -12 -14 1.95 2.77 -4 -12 -15 1.93 2.61 -4 -12 -16 6.10 4.20 -4 -12 -17 86.07 9.95 -4 -12 -18 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65.62 10.86 5 -7 13 0.06 2.85 5 -7 13 -0.24 2.06 5 -7 14 24.54 4.56 -5 7 -14 24.48 4.56 -5 7 -15 44.35 5.88 5 -7 15 48.86 5.89 5 -7 16 39.75 5.66 -5 7 -16 46.12 6.13 -5 7 -17 260.36 15.06 5 -7 17 251.69 13.70 5 -7 18 -0.26 1.85 -5 -7 -18 1.87 3.31 5 -7 19 0.53 2.22 -5 -7 -19 1.85 3.36 -5 -7 -20 169.47 13.54 -5 -7 -21 93.01 9.80 -5 -7 -22 27.98 5.49 -5 -7 -23 37.57 6.29 -5 -7 -24 76.08 8.51 -5 -7 -25 82.90 8.38 -5 -7 -26 7.86 3.02 -5 -7 -27 3.34 2.71 -5 -7 -28 4.19 2.11 -5 -7 -29 15.50 2.82 5 7 29 23.64 3.74 5 7 30 14.96 2.85 5 7 31 4.13 1.89 5 7 32 0.21 1.02 -5 8 32 26.34 2.68 -5 8 31 5.57 1.59 -5 8 31 5.09 1.51 -5 8 30 103.39 6.71 -5 8 29 64.28 5.65 -5 8 28 4.92 2.00 5 -8 -28 5.39 2.08 5 -8 -27 34.71 4.35 -5 8 27 27.20 4.05 -5 8 26 1.09 1.66 5 -8 -26 -0.54 1.53 -5 8 25 4.56 1.70 5 -8 -25 5.39 2.09 -5 8 24 1.86 1.88 5 -8 -24 -1.35 1.77 -5 8 23 6.10 2.31 5 -8 -23 8.61 2.52 -5 8 22 3.32 1.73 5 -8 -22 6.12 2.88 -5 8 21 31.93 4.91 5 -8 -21 29.91 4.74 -5 8 20 -1.09 1.89 5 -8 -20 0.36 1.55 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5 -9 -15 337.36 17.45 5 -9 -14 106.13 8.85 5 -9 -14 115.98 10.04 5 -9 -13 5.71 3.29 5 -9 -13 3.47 2.56 5 -9 -12 4.43 2.75 5 -9 -12 3.06 2.48 5 -9 -11 44.05 6.25 5 -9 -11 38.19 5.14 5 -9 -10 14.61 4.49 5 -9 -10 15.16 3.78 5 -9 -9 23.27 4.97 5 -9 -9 29.28 4.80 -5 -9 9 26.63 8.50 5 -9 -8 534.37 19.20 5 -9 -8 500.36 21.05 -5 -9 7 2.98 3.96 -5 -9 6 67.58 12.45 -5 -9 5 127.34 17.03 -5 -9 4 167.85 19.47 -5 -9 3 42.57 10.46 -5 -9 2 8.16 5.76 -5 -9 1 42.77 10.13 -5 -9 0 149.12 18.69 -5 -9 -1 8.22 5.17 -5 -9 -2 297.73 27.17 -5 -9 -3 105.27 16.11 -5 -9 -4 25.14 7.91 -5 -9 -5 7.14 6.12 -5 -9 -6 21.54 9.12 -5 -9 -7 30.48 9.78 5 9 7 43.91 8.43 5 -9 8 104.70 7.88 5 9 8 105.00 13.39 5 -9 9 5.44 3.04 5 -9 9 7.99 2.98 -5 -9 -9 1.73 2.21 5 -9 10 86.75 7.42 -5 -9 -10 65.28 8.23 5 -9 11 17.06 3.64 -5 -9 -11 7.86 3.32 5 -9 12 2.79 2.00 -5 -9 -12 1.12 2.34 5 -9 13 0.86 1.65 -5 -9 -13 -0.81 2.39 5 -9 14 19.45 3.76 -5 -9 -14 19.18 5.29 -5 -9 -15 45.11 7.86 5 -9 15 56.50 6.44 5 -9 16 27.53 4.60 -5 -9 -16 29.29 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86.94 8.05 5 -10 -13 97.87 9.50 5 -10 -12 30.18 5.84 5 -10 -12 25.59 4.69 5 -10 -11 55.25 6.26 5 -10 -11 49.27 6.89 5 -10 -10 48.12 7.01 5 -10 -10 42.41 5.57 5 -10 -9 4.14 3.72 5 -10 -9 5.51 2.97 -5 -10 9 14.67 4.64 5 -10 -8 17.47 4.42 5 -10 -8 20.04 4.25 -5 -10 8 23.52 5.37 5 -10 -7 280.49 13.79 -5 -10 7 311.09 15.96 5 -10 -7 278.55 15.73 5 -10 -6 1.24 2.41 5 -10 -6 0.85 2.11 -5 -10 6 4.02 3.22 5 -10 -5 64.44 6.24 -5 -10 5 76.90 7.97 -5 -10 5 72.30 13.63 -5 -10 5 74.00 7.33 5 -10 -5 65.64 7.35 5 -10 -4 47.51 5.48 -5 -10 4 34.72 5.16 -5 -10 4 30.20 9.16 5 -10 -3 107.36 8.06 -5 -10 3 102.24 16.09 5 -10 -2 28.64 4.22 -5 -10 2 26.04 8.23 -5 -10 1 183.45 21.68 5 -10 -1 223.74 11.62 5 -10 0 44.52 5.64 -5 -10 0 23.22 8.74 5 -10 1 67.12 6.53 -5 -10 -1 27.93 10.52 -5 -10 -2 220.07 24.92 5 -10 2 228.84 11.83 5 -10 3 22.85 4.08 -5 -10 -3 19.91 8.89 5 -10 4 127.97 8.76 -5 -10 -4 107.49 17.79 5 -10 5 4.91 2.72 -5 -10 -5 7.07 6.23 5 -10 6 115.80 8.49 -5 -10 -6 96.34 17.60 -5 -10 -6 108.45 9.70 5 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7.10 5 -11 0 75.62 6.77 5 -11 1 54.18 5.70 5 -11 1 45.78 5.34 5 -11 2 40.40 5.05 5 -11 2 35.67 4.65 5 -11 3 31.40 4.57 5 -11 3 24.12 3.80 5 -11 4 9.63 2.85 5 -11 5 85.39 7.16 5 -11 6 5.62 2.39 -5 -11 -6 1.20 2.15 5 -11 7 2.12 2.07 -5 -11 -7 2.40 2.29 5 -11 8 21.17 3.72 -5 -11 -8 12.42 3.98 5 -11 9 9.33 2.73 -5 -11 -9 10.69 4.32 5 -11 10 41.78 5.32 -5 -11 -10 37.13 6.61 -5 -11 -11 292.83 18.43 5 -11 11 358.76 15.50 -5 -11 -12 2.12 2.53 5 -11 12 -0.25 1.51 5 -11 13 1.98 1.72 -5 -11 -13 1.19 2.82 5 -11 14 7.15 2.83 -5 -11 -14 16.76 5.71 -5 -11 -15 48.32 7.63 5 -11 15 41.07 5.21 5 -11 16 15.30 3.08 -5 -11 -16 14.17 4.79 5 -11 17 4.35 2.19 -5 -11 -17 5.36 3.93 5 -11 18 17.44 3.25 -5 -11 -18 21.18 5.63 -5 -11 -19 1.54 3.40 -5 -11 -20 23.26 5.79 -5 -11 -21 2.42 3.21 -5 -11 -22 11.05 3.70 -5 -11 -23 30.79 5.19 -5 -11 -24 -1.87 2.49 -5 -11 -25 9.68 2.98 5 11 25 10.06 2.38 -5 -11 -26 3.81 2.10 5 11 26 7.89 2.07 -5 -11 -27 33.05 4.15 5 11 27 30.49 3.17 -5 -11 -28 11.65 2.29 5 -12 -27 23.96 2.76 5 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1.76 -6 8 24 3.95 2.17 -6 8 23 0.33 1.33 6 -8 -23 2.65 1.90 -6 8 22 9.26 2.88 6 -8 -22 18.46 3.73 -6 8 21 15.86 3.59 6 -8 -21 13.61 3.24 6 -8 -20 84.74 7.56 -6 8 20 71.42 7.41 -6 8 19 20.46 4.26 6 -8 -19 25.99 4.52 6 -8 -18 56.78 6.48 6 -8 -17 102.82 8.61 -6 8 17 90.38 8.57 6 -8 -16 32.95 5.03 -6 8 16 30.11 5.04 6 -8 -15 43.31 5.75 -6 8 15 40.56 5.72 6 -8 -14 96.65 8.33 -6 8 14 96.19 8.58 6 -8 -13 25.11 4.30 -6 8 13 24.88 4.29 6 -8 -12 231.88 12.80 -6 8 12 231.85 13.05 6 -8 -11 6.63 3.08 -6 8 11 2.27 2.18 6 -8 -10 4.91 2.74 -6 8 10 0.92 1.46 6 -8 -9 15.30 3.87 -6 8 9 14.38 3.41 6 -8 -8 47.48 5.60 -6 8 8 57.98 6.03 -6 -8 7 93.81 14.86 6 -8 -7 101.55 7.91 6 -8 -6 2.33 1.57 -6 -8 6 6.01 5.33 -6 -8 5 3.87 4.26 -6 -8 4 3.82 5.00 -6 -8 3 32.81 8.70 -6 -8 2 48.02 10.98 -6 -8 1 301.09 27.07 -6 -8 0 20.29 7.33 -6 -8 -1 8.91 6.23 -6 -8 -2 12.51 5.86 -6 -8 -3 16.08 7.51 6 -8 4 69.39 6.50 -6 -8 -4 62.62 13.34 6 -8 5 18.93 3.65 -6 -8 -5 12.70 6.00 6 -8 6 7.22 2.52 -6 -8 -6 0.83 5.35 6 -8 7 63.20 6.31 -6 -8 -7 47.61 11.67 6 -8 8 35.75 5.10 -6 -8 -8 19.37 8.87 6 -8 9 8.26 3.31 6 -8 10 144.66 9.87 6 -8 11 64.27 6.48 6 -8 12 69.53 7.07 6 -8 13 1.93 1.87 6 -8 14 13.07 3.72 6 -8 15 58.59 6.67 6 -8 16 3.18 2.72 -6 -8 -16 1.76 3.36 6 -8 17 41.09 5.72 -6 -8 -17 37.32 7.04 6 -8 18 3.87 2.40 -6 -8 -18 5.25 3.83 6 -8 19 19.03 3.85 -6 -8 -19 29.18 6.27 -6 -8 -20 150.89 12.99 -6 -8 -21 5.27 3.56 -6 -8 -22 4.96 3.14 -6 -8 -23 2.52 3.49 -6 -8 -24 1.84 2.46 -6 -8 -25 7.29 3.01 -6 -8 -26 11.96 3.17 -6 -8 -27 45.35 5.21 -6 -8 -28 1.16 1.40 6 8 28 6.66 2.18 -6 -8 -29 18.22 2.80 6 8 29 19.11 2.85 6 8 30 1.83 1.28 -6 9 29 5.69 1.36 -6 9 28 26.79 3.12 -6 9 27 1.73 1.30 6 -9 -26 2.78 1.54 -6 9 26 2.72 1.67 -6 9 25 2.19 1.55 6 -9 -25 2.04 1.71 6 -9 -24 25.92 3.76 -6 9 24 22.94 3.75 6 -9 -23 14.14 3.09 -6 9 23 17.84 3.54 6 -9 -22 0.26 1.80 -6 9 22 -0.05 1.32 6 -9 -21 15.16 3.32 -6 9 21 12.52 3.08 6 -9 -20 7.64 2.68 -6 9 20 4.33 1.97 6 -9 -19 12.08 3.34 -6 9 19 16.69 3.65 6 -9 -18 17.78 3.91 -6 9 18 13.57 3.53 6 -9 -17 23.75 4.28 -6 9 17 19.38 3.94 6 -9 -16 23.09 4.32 -6 9 16 20.51 3.87 6 -9 -15 12.77 3.23 -6 9 15 13.68 3.39 6 -9 -14 -0.70 1.63 -6 9 14 0.17 1.37 6 -9 -13 42.77 5.76 -6 9 13 35.03 5.11 6 -9 -12 368.86 16.67 -6 9 12 368.10 16.68 6 -9 -11 98.89 8.42 -6 9 11 96.88 8.12 6 -9 -10 16.67 3.57 -6 9 10 19.98 3.83 6 -9 -9 1.08 1.77 -6 9 9 9.49 2.58 6 -9 -8 12.49 2.80 -6 9 8 10.89 2.75 6 -9 -7 7.91 3.15 6 -9 -6 303.67 14.46 6 -9 -5 4.09 2.52 6 -9 -4 63.03 6.40 6 -9 -3 40.66 5.45 6 -9 -2 90.93 7.74 6 -9 -1 47.48 5.66 6 -9 0 5.82 2.47 6 -9 1 4.51 2.67 6 -9 2 33.58 5.21 6 -9 3 9.40 3.07 6 -9 4 176.81 10.57 6 -9 5 61.62 6.34 6 -9 6 284.48 13.58 -6 -9 -6 236.59 15.09 6 -9 7 3.48 2.55 6 -9 8 9.57 3.34 -6 -9 -8 0.70 2.52 6 -9 9 2.39 1.94 -6 -9 -9 0.70 2.53 6 -9 10 13.89 3.78 -6 -9 -10 18.23 5.04 6 -9 11 72.07 6.98 -6 -9 -11 71.29 9.52 6 -9 12 1.71 2.14 -6 -9 -12 -1.18 2.90 6 -9 13 8.65 2.84 -6 -9 -13 13.52 4.84 6 -9 14 8.80 2.94 -6 -9 -14 6.83 3.69 6 -9 15 1.37 2.23 -6 -9 -15 2.99 3.60 6 -9 16 -0.65 2.14 -6 -9 -16 -1.72 3.14 6 -9 17 7.74 2.74 -6 -9 -17 13.02 5.04 6 -9 18 2.29 2.15 -6 -9 -18 2.70 3.05 6 -9 19 8.35 3.04 -6 -9 -19 9.16 4.03 -6 -9 -20 54.65 7.78 -6 -9 -21 4.26 3.57 -6 -9 -22 7.45 3.71 -6 -9 -23 78.59 8.26 -6 -9 -24 10.41 3.83 -6 -9 -25 131.11 9.67 -6 -9 -26 210.21 11.57 -6 -9 -27 3.74 2.13 -6 -9 -28 17.12 3.00 6 9 28 15.71 2.54 6 9 29 21.37 2.57 6 -10 -27 14.10 2.22 6 -10 -26 9.09 2.14 -6 10 26 6.10 1.65 6 -10 -25 5.46 1.78 -6 10 25 8.27 2.04 6 -10 -24 23.66 3.44 -6 10 24 24.64 3.42 6 -10 -23 20.17 3.70 -6 10 23 20.09 3.31 6 -10 -22 1.39 1.82 -6 10 22 -0.75 1.42 6 -10 -21 12.83 3.11 -6 10 21 9.44 2.65 6 -10 -20 131.64 9.22 -6 10 20 125.71 8.95 6 -10 -19 1.51 1.87 -6 10 19 1.01 1.56 6 -10 -18 6.50 2.77 -6 10 18 1.34 1.38 6 -10 -17 4.01 2.74 -6 10 17 1.23 1.46 6 -10 -16 7.93 3.04 -6 10 16 6.01 2.25 6 -10 -15 7.30 3.01 -6 10 15 3.58 2.05 6 -10 -14 67.50 7.14 6 -10 -13 248.01 13.63 6 -10 -12 4.17 2.61 6 -10 -11 186.46 11.61 6 -10 -10 9.37 3.17 6 -10 -9 3.23 1.75 6 -10 -8 1.29 1.95 6 -10 -7 8.87 2.89 6 -10 -6 4.87 2.45 6 -10 -5 40.85 5.36 6 -10 -4 21.91 4.17 -6 -10 4 25.61 4.48 6 -10 -3 50.19 5.84 -6 -10 3 42.03 5.38 6 -10 -2 7.38 3.07 -6 -10 2 2.44 2.23 6 -10 -1 83.61 7.47 -6 -10 1 72.92 6.72 6 -10 0 94.04 7.90 6 -10 1 10.73 3.35 6 -10 1 6.33 2.32 6 -10 2 7.11 3.36 6 -10 3 95.53 7.92 6 -10 4 51.87 5.80 6 -10 5 68.00 6.70 6 -10 6 51.46 5.79 -6 -10 -6 43.96 6.34 6 -10 7 38.42 5.47 -6 -10 -7 28.04 5.80 6 -10 8 79.99 7.19 -6 -10 -8 72.64 8.73 6 -10 9 11.08 3.38 -6 -10 -9 13.63 4.52 -6 -10 -10 54.63 8.27 6 -10 10 70.66 6.81 6 -10 11 42.48 5.48 -6 -10 -11 37.70 6.72 -6 -10 -12 118.37 12.11 6 -10 12 137.77 9.62 6 -10 13 15.00 3.61 -6 -10 -13 24.52 6.24 6 -10 14 0.01 1.92 -6 -10 -14 3.89 3.73 6 -10 15 18.24 3.84 -6 -10 -15 16.80 4.86 6 -10 16 68.98 6.99 -6 -10 -16 60.67 9.41 6 -10 17 1.97 2.02 -6 -10 -17 4.91 4.37 6 -10 18 30.14 4.59 -6 -10 -18 27.04 5.88 -6 -10 -19 32.48 6.47 -6 -10 -20 3.93 3.65 -6 -10 -21 2.54 2.70 -6 -10 -22 99.78 9.63 -6 -10 -23 25.10 5.01 -6 -10 -24 6.64 2.79 -6 -10 -25 1.27 1.74 -6 -10 -26 9.46 2.65 6 10 26 14.01 2.60 6 10 27 61.33 4.47 -6 -10 -27 56.02 5.15 6 -11 -26 4.68 1.37 6 -11 -26 5.63 1.47 6 -11 -25 7.16 2.07 6 -11 -25 2.84 1.26 6 -11 -24 1.29 1.38 6 -11 -23 16.57 3.04 6 -11 -22 91.59 6.92 6 -11 -21 20.73 3.55 6 -11 -20 -0.88 1.80 6 -11 -19 0.05 1.80 6 -11 -18 23.17 4.06 6 -11 -17 31.36 4.88 6 -11 -16 8.20 2.51 6 -11 -15 97.34 8.21 6 -11 -14 -2.35 1.89 6 -11 -13 73.59 7.34 6 -11 -12 52.32 6.23 6 -11 -11 41.94 5.63 6 -11 -10 20.42 4.46 6 -11 -9 188.34 11.53 6 -11 -8 26.30 5.04 6 -11 -7 338.54 15.99 -6 -11 7 337.06 17.27 6 -11 -6 153.87 10.41 -6 -11 6 164.88 11.81 6 -11 -5 3.62 2.64 -6 -11 5 5.44 3.46 6 -11 -4 36.80 5.25 -6 -11 4 30.01 4.79 6 -11 -3 147.11 9.99 -6 -11 3 143.46 10.34 6 -11 -2 4.56 2.72 -6 -11 2 2.89 2.67 6 -11 -1 24.66 4.46 6 -11 -1 16.64 3.33 -6 -11 1 26.54 4.33 6 -11 0 8.64 3.57 6 -11 0 6.37 2.55 -6 -11 0 1.27 1.96 6 -11 1 64.61 6.66 6 -11 1 45.90 5.26 6 -11 2 114.19 8.56 6 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1.95 6 -12 -17 55.62 5.90 6 -12 -16 1.13 1.75 6 -12 -15 35.30 5.02 6 -12 -14 3.65 2.56 6 -12 -13 13.96 3.19 6 -12 -12 9.95 3.10 6 -12 -11 -0.04 2.06 6 -12 -10 193.81 11.67 6 -12 -9 189.34 11.53 6 -12 -8 10.02 3.40 6 -12 -7 26.31 4.71 -6 -12 7 28.44 5.65 -6 -12 6 30.42 5.57 6 -12 -6 27.95 4.76 6 -12 -5 18.65 4.00 6 -12 -5 16.50 3.60 -6 -12 5 23.59 5.10 6 -12 -4 8.08 2.84 6 -12 -4 10.16 3.11 -6 -12 4 13.27 4.35 6 -12 -3 1.32 1.92 6 -12 -3 4.74 2.87 -6 -12 3 9.36 4.13 6 -12 -2 29.66 5.03 6 -12 -2 28.94 4.70 -6 -12 2 25.90 5.14 6 -12 -1 13.09 4.09 6 -12 -1 1.25 1.85 -6 -12 1 13.80 3.95 6 -12 0 110.29 9.02 6 -12 0 93.93 7.81 -6 -12 0 94.93 8.40 6 -12 1 444.82 17.59 6 -12 1 387.36 16.13 -6 -12 -1 438.16 18.15 6 -12 2 26.78 5.71 6 -12 2 22.82 4.23 -6 -12 -2 27.34 6.09 6 -12 3 333.26 14.90 6 -12 4 164.32 10.26 6 -12 5 344.65 15.50 6 -12 6 133.25 9.19 6 -12 7 41.87 5.78 6 -12 8 499.61 18.44 -6 -12 -8 451.14 21.32 -6 -12 -9 66.27 8.18 6 -12 9 65.36 6.60 6 -12 10 22.85 3.94 -6 -12 -10 30.02 5.84 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1.49 6 -16 -12 0.72 1.43 6 -16 -11 39.51 4.18 6 -16 -11 40.90 4.66 6 -16 -10 7.67 2.73 6 -16 -10 7.94 2.35 6 -16 -9 43.51 4.51 6 -16 -9 38.89 4.80 6 -16 -8 32.17 3.89 6 -16 -8 28.08 4.06 6 -16 -7 11.75 2.95 6 -16 -7 9.22 2.35 6 -16 -6 27.53 3.99 6 -16 -6 25.70 3.51 6 -16 -5 11.87 2.87 6 -16 -5 11.91 2.56 6 -16 -4 4.55 1.92 6 -16 -4 3.59 1.85 6 -16 -3 13.38 2.86 6 -16 -3 15.85 3.05 6 -16 -2 21.33 3.24 6 -16 -2 19.17 3.36 6 -16 -1 18.67 3.05 6 -16 -1 18.70 3.27 -6 -16 1 27.23 4.97 6 -16 0 74.11 5.66 6 -16 0 65.56 5.48 -6 -16 0 76.76 7.27 6 -16 1 38.93 4.22 6 -16 1 37.08 4.06 6 -16 2 8.55 2.73 -6 -16 -2 13.90 3.96 6 -16 3 11.45 2.38 -6 -16 -3 18.80 3.99 6 -16 4 8.64 2.15 -6 -16 -4 13.88 3.64 6 -16 5 14.53 2.43 -6 -16 -5 14.80 3.66 6 -16 6 9.66 2.10 -6 -16 -6 17.27 4.03 6 -16 7 11.61 2.05 -6 -16 -7 16.71 3.75 -6 -16 -8 7.16 2.96 -6 -16 -9 33.09 4.66 -6 -16 -10 0.05 1.91 -6 -16 -11 80.28 7.02 -6 -16 -12 11.78 2.94 -6 -16 -13 -4.55 2.52 -6 -16 -14 15.81 3.34 -6 -16 -15 15.01 3.00 -6 -16 -16 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14.47 3.21 7 -9 -19 61.78 6.06 -7 9 19 60.35 6.47 7 -9 -18 67.56 6.47 -7 9 18 76.58 7.42 7 -9 -17 5.41 2.26 -7 9 17 2.31 1.72 7 -9 -16 21.01 3.85 -7 9 16 24.48 4.50 7 -9 -15 5.45 2.45 -7 9 15 3.72 1.91 7 -9 -14 0.56 1.69 -7 9 14 0.02 1.36 7 -9 -13 0.71 1.63 -7 9 13 7.09 2.82 7 -9 -12 135.77 9.83 -7 9 12 131.09 9.80 7 -9 -11 51.25 6.12 -7 9 11 57.05 6.35 7 -9 -10 42.35 5.83 -7 9 10 48.02 6.04 7 -9 -9 24.92 4.61 -7 9 9 26.40 4.44 7 -9 -8 1.98 2.05 -7 9 8 -0.09 1.42 7 -9 -7 15.77 3.64 -7 9 7 19.86 3.54 7 -9 -6 6.80 2.97 -7 9 6 3.73 1.49 7 -9 -5 15.34 3.49 -7 9 5 12.48 3.08 7 -9 -4 50.38 5.92 -7 9 4 47.01 5.51 7 -9 -3 4.77 2.80 -7 9 3 4.26 2.27 7 -9 -2 131.35 9.39 -7 9 2 130.27 8.83 7 -9 -1 84.09 7.47 -7 9 1 78.73 6.82 7 -9 0 16.48 3.75 -7 9 0 13.40 2.76 7 -9 1 14.43 3.32 -7 9 -1 14.03 3.09 7 -9 2 65.58 6.72 -7 9 -2 70.68 6.43 7 -9 3 20.62 4.05 7 -9 4 3.14 2.24 7 -9 5 101.05 8.38 7 -9 6 23.19 4.20 -7 -9 -6 27.57 5.26 7 -9 7 15.54 3.64 -7 -9 -7 11.00 3.30 7 -9 8 25.94 4.54 -7 -9 -8 23.14 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29.57 4.86 -8 5 -14 27.99 5.01 -8 5 -15 87.30 8.44 8 -5 15 87.04 8.13 8 -5 16 17.47 5.03 -8 5 -16 3.74 2.29 -8 5 -17 1.05 2.11 8 5 17 -1.31 1.93 8 -5 17 -0.54 1.59 -8 5 -18 5.63 3.22 8 5 18 3.43 2.57 8 -5 18 7.80 2.68 8 5 19 17.03 3.62 8 -5 19 16.20 3.24 8 5 20 1.94 1.93 8 -5 20 3.08 2.09 8 5 21 62.50 6.23 8 -5 21 42.66 5.03 8 5 22 6.32 2.51 8 -5 22 5.35 2.22 -8 -5 -22 1.24 2.55 8 5 23 10.43 2.65 8 -5 23 7.90 2.29 -8 -5 -23 10.49 3.04 -8 -5 -24 10.74 3.13 8 5 24 16.14 2.98 8 -5 24 13.67 2.61 8 5 25 9.56 2.25 8 -5 25 10.28 2.21 -8 -5 -26 8.32 2.45 8 5 26 6.70 1.96 8 -5 26 8.45 1.88 -8 -5 -27 0.59 1.30 8 -5 27 0.23 0.78 -8 6 29 0.53 0.80 -8 6 28 12.92 2.16 -8 6 27 30.48 3.37 -8 6 26 17.14 2.84 -8 6 25 1.11 1.38 -8 6 24 17.85 3.23 -8 6 23 21.11 3.70 -8 6 22 168.39 10.33 -8 6 21 3.30 2.13 -8 6 20 74.02 7.29 -8 6 19 3.24 2.33 -8 6 18 60.60 6.80 -8 6 17 54.76 6.66 -8 6 16 10.73 3.17 -8 6 15 9.80 3.63 -8 6 14 1.02 2.32 -8 6 13 6.82 3.14 -8 6 12 35.56 5.60 -8 6 11 14.68 4.04 8 -6 -10 22.27 3.95 -8 6 10 27.28 5.16 8 -6 -9 160.08 10.08 -8 6 9 181.62 12.02 8 -6 -8 60.03 6.11 -8 6 8 67.65 7.31 8 -6 -7 15.11 4.03 -8 6 7 14.19 4.22 8 -6 -6 17.50 4.03 -8 6 6 17.94 4.59 8 -6 -5 170.76 10.44 -8 6 5 156.37 10.71 8 -6 -4 21.12 3.98 -8 6 4 13.79 3.26 8 -6 -3 24.85 4.44 -8 6 3 29.32 4.53 8 -6 -2 86.82 7.67 -8 6 2 89.97 7.94 8 -6 -1 230.93 12.47 -8 6 1 238.35 12.97 8 -6 0 80.90 7.24 -8 6 0 80.47 7.54 8 -6 1 8.61 2.86 -8 6 -1 5.73 2.36 8 -6 2 109.66 8.49 -8 6 -2 114.02 8.70 8 -6 3 1.75 1.81 -8 6 -3 2.41 1.71 8 -6 4 1.41 1.89 -8 6 -4 0.12 1.37 8 -6 5 8.09 3.02 -8 6 -5 5.65 2.28 8 -6 6 27.74 4.54 -8 6 -6 29.01 4.53 8 -6 7 5.94 3.15 -8 6 -7 -0.18 1.61 8 -6 8 3.65 2.75 -8 6 -8 2.24 2.05 -8 6 -9 163.01 10.82 8 -6 9 170.13 11.22 -8 6 -10 93.52 8.33 8 -6 10 102.43 8.63 8 -6 11 14.64 4.16 -8 6 -11 13.93 3.50 -8 6 -12 122.94 9.52 8 -6 12 118.33 9.44 -8 6 -13 89.29 8.16 8 -6 13 80.98 7.99 8 -6 14 9.97 3.84 -8 6 -14 13.28 3.81 8 -6 15 0.48 2.12 -8 6 -15 -1.26 1.68 8 6 15 2.46 2.33 -8 6 -16 61.47 7.11 8 6 16 65.17 6.69 8 -6 16 64.26 6.23 8 -6 16 58.76 6.75 -8 6 -17 96.67 8.62 8 6 17 91.48 7.81 8 -6 17 93.28 7.44 -8 6 -18 23.06 4.39 8 6 18 20.96 3.96 8 -6 18 19.13 3.39 8 6 19 9.56 2.83 8 -6 19 11.63 2.94 8 6 20 21.37 3.63 8 -6 20 24.36 3.67 -8 -6 -20 22.96 5.32 8 6 21 7.98 2.26 8 -6 21 10.12 2.22 -8 -6 -21 9.18 3.00 -8 -6 -22 22.32 4.44 8 -6 22 18.81 2.92 -8 -6 -23 1.69 2.18 8 -6 23 -1.85 1.43 -8 -6 -24 21.35 3.96 8 -6 24 15.02 2.44 -8 -6 -25 13.87 3.22 8 -6 25 9.54 1.82 -8 -6 -26 1.25 1.54 -8 7 28 4.07 1.17 -8 7 27 66.41 4.69 -8 7 26 -0.81 0.86 -8 7 25 1.32 1.08 -8 7 24 21.93 3.38 -8 7 23 146.49 8.98 -8 7 22 1.51 2.19 -8 7 21 3.51 2.25 -8 7 20 2.78 2.03 -8 7 19 11.04 2.89 -8 7 18 25.05 4.53 -8 7 17 100.48 8.78 -8 7 16 58.22 6.72 -8 7 15 85.34 8.22 -8 7 14 42.96 6.21 8 -7 -13 140.56 9.44 -8 7 13 168.57 11.86 8 -7 -12 1.23 2.07 -8 7 12 2.80 2.30 8 -7 -11 3.52 1.87 -8 7 11 3.34 2.93 8 -7 -10 226.36 12.33 -8 7 10 248.01 14.00 8 -7 -9 11.62 3.28 -8 7 9 8.75 3.30 8 -7 -8 32.16 4.72 -8 7 8 39.21 6.03 8 -7 -7 77.33 7.21 -8 7 7 64.92 7.27 8 -7 -6 134.10 9.42 -8 7 6 136.98 10.03 8 -7 -5 23.80 4.31 -8 7 5 18.96 3.94 8 -7 -4 39.59 5.69 -8 7 4 40.43 5.61 8 -7 -3 145.30 9.90 -8 7 3 153.23 10.25 8 -7 -2 54.88 6.19 -8 7 2 65.49 6.65 8 -7 -1 26.33 4.95 -8 7 1 20.74 4.14 8 -7 0 263.39 13.61 -8 7 0 248.03 13.18 8 -7 1 3.48 2.72 -8 7 -1 5.22 2.22 8 -7 2 10.60 3.20 -8 7 -2 6.98 2.86 8 -7 3 48.44 5.90 -8 7 -3 42.37 5.37 8 -7 4 65.18 6.76 -8 7 -4 55.38 6.19 8 -7 5 56.29 6.31 -8 7 -5 50.10 5.83 8 -7 6 2.39 2.59 -8 7 -6 0.07 1.38 -8 7 -7 76.56 7.11 8 -7 7 80.30 7.70 8 -7 8 20.35 4.16 -8 7 -8 24.72 4.14 8 -7 9 29.19 4.75 -8 7 -9 25.11 4.18 8 -7 10 3.51 2.16 -8 7 -10 15.28 3.47 8 -7 11 5.49 2.96 -8 7 -11 7.44 2.62 8 -7 12 -0.34 1.88 -8 7 -12 6.27 2.88 -8 7 -13 70.71 7.38 8 -7 13 78.91 7.90 8 -7 14 7.88 2.62 -8 7 -14 10.01 3.34 8 -7 15 15.71 3.84 -8 7 -15 12.84 3.48 8 -7 16 26.32 4.60 -8 7 -16 28.02 4.82 -8 7 -17 102.21 8.67 8 -7 17 110.08 8.64 -8 -7 -18 50.09 7.86 -8 -7 -19 52.48 7.88 -8 -7 -20 32.44 6.07 -8 -7 -21 16.92 5.04 -8 -7 -22 2.19 2.34 -8 -7 -23 8.41 2.93 -8 -7 -24 73.11 6.82 -8 -7 -25 10.91 2.80 -8 -7 -26 24.01 3.46 -8 8 26 61.70 4.49 -8 8 25 26.01 3.14 -8 8 24 6.40 1.88 -8 8 23 35.88 4.18 -8 8 22 1.29 1.46 -8 8 21 4.31 2.12 -8 8 20 66.62 6.42 -8 8 19 3.34 2.07 -8 8 18 3.03 1.99 8 -8 -17 0.73 1.53 -8 8 17 -0.96 1.86 8 -8 -16 5.73 2.44 -8 8 16 13.91 3.55 8 -8 -15 58.22 5.86 -8 8 15 51.29 6.17 8 -8 -14 12.21 2.97 -8 8 14 11.55 3.53 8 -8 -13 63.61 6.37 -8 8 13 66.38 7.12 8 -8 -12 28.62 4.49 -8 8 12 25.08 4.76 8 -8 -11 24.50 4.36 -8 8 11 26.14 4.42 8 -8 -10 1.88 1.55 -8 8 10 2.45 2.43 8 -8 -9 3.46 2.44 -8 8 9 -0.82 1.49 8 -8 -8 29.06 4.58 -8 8 8 38.19 5.41 8 -8 -7 4.76 2.30 -8 8 7 6.36 2.62 8 -8 -6 -1.43 2.05 -8 8 6 2.79 2.39 8 -8 -5 15.52 3.53 -8 8 5 10.03 2.92 8 -8 -4 5.28 2.54 -8 8 4 5.49 2.25 8 -8 -3 5.75 2.15 -8 8 3 4.29 2.01 8 -8 -2 15.62 3.48 -8 8 2 13.13 3.36 8 -8 -1 18.21 4.00 -8 8 1 18.32 3.90 8 -8 0 112.85 8.83 -8 8 0 119.96 8.84 8 -8 1 6.38 3.18 -8 8 -1 2.50 2.76 8 -8 2 4.60 2.87 -8 8 -2 -0.26 1.38 8 -8 3 40.57 5.54 -8 8 -3 34.97 4.79 8 -8 4 9.32 3.17 -8 8 -4 9.90 2.80 8 -8 5 20.65 4.15 -8 8 -5 12.90 3.15 8 -8 6 12.48 3.53 -8 8 -6 11.69 3.02 8 -8 7 12.64 3.67 -8 8 -7 10.09 3.25 8 -8 8 13.86 3.97 -8 8 -8 13.60 3.40 -8 8 -9 73.39 6.99 8 -8 9 82.53 7.88 -8 8 -10 49.84 5.84 8 -8 10 51.72 6.26 -8 8 -11 115.25 8.94 8 -8 11 117.46 9.29 8 -8 12 20.57 4.13 -8 8 -12 20.37 4.10 -8 8 -13 62.76 6.69 8 -8 13 61.02 6.69 8 -8 14 5.27 2.87 -8 8 -14 10.28 3.25 8 -8 15 26.93 4.58 -8 8 -15 29.88 4.61 -8 -8 -15 22.65 5.97 -8 8 -16 78.44 7.31 -8 -8 -16 66.88 9.17 8 -8 16 84.05 7.45 8 -8 17 1.47 2.13 -8 -8 -17 -1.82 3.14 -8 -8 -18 -1.56 2.85 -8 -8 -19 3.69 3.20 -8 -8 -20 32.91 5.96 -8 -8 -21 19.47 4.52 -8 -8 -22 2.69 2.63 -8 -8 -23 8.97 2.99 -8 -8 -24 6.08 2.41 -8 -8 -25 1.35 1.69 -8 9 25 1.71 0.93 -8 9 24 -0.65 0.98 -8 9 23 19.13 2.77 -8 9 22 21.47 3.20 -8 9 21 35.04 4.17 -8 9 20 0.85 1.44 8 -9 -19 7.85 2.16 -8 9 19 9.00 2.51 8 -9 -18 27.56 3.73 -8 9 18 28.60 4.35 8 -9 -17 11.78 2.67 -8 9 17 13.58 3.30 8 -9 -16 37.09 4.57 -8 9 16 38.26 5.15 8 -9 -15 2.45 2.05 -8 9 15 -0.42 1.44 8 -9 -14 10.45 3.04 -8 9 14 12.97 3.42 8 -9 -13 5.51 2.15 -8 9 13 4.21 2.83 8 -9 -12 65.01 6.38 -8 9 12 64.91 6.90 8 -9 -11 4.05 2.20 -8 9 11 6.28 2.62 8 -9 -10 38.04 5.16 -8 9 10 39.44 5.39 8 -9 -9 2.79 2.37 -8 9 9 5.05 2.46 8 -9 -8 53.49 6.03 -8 9 8 56.04 6.23 8 -9 -7 8.43 2.84 -8 9 7 7.90 2.81 8 -9 -6 5.65 2.60 -8 9 6 4.64 2.37 8 -9 -5 17.21 3.93 -8 9 5 12.06 3.02 8 -9 -4 9.24 3.24 -8 9 4 6.68 3.03 8 -9 -3 116.46 8.83 -8 9 3 112.73 8.56 8 -9 -2 18.67 3.77 -8 9 2 18.37 3.54 8 -9 -1 36.95 5.28 -8 9 1 36.25 4.71 8 -9 0 3.77 2.90 -8 9 0 7.02 2.32 8 -9 1 64.95 6.59 -8 9 -1 55.68 5.89 8 -9 2 7.12 3.01 -8 9 -2 4.32 2.22 8 -9 3 3.00 2.59 -8 9 -3 1.99 1.66 8 -9 4 1.30 1.72 -8 9 -4 -0.60 1.75 8 -9 5 30.56 4.76 -8 9 -5 25.62 3.95 8 -9 6 28.10 4.60 -8 9 -6 19.42 3.55 8 -9 7 11.65 3.46 -8 9 -7 11.92 3.13 -8 -9 -7 6.55 3.36 8 -9 8 33.23 5.27 -8 9 -8 28.18 4.17 -8 -9 -8 28.95 5.78 8 -9 9 11.47 3.38 -8 9 -9 11.68 2.93 -8 -9 -9 8.01 3.57 8 -9 10 12.61 3.44 -8 9 -10 8.60 2.64 -8 -9 -10 6.05 3.49 8 -9 11 3.65 2.57 -8 9 -11 2.07 1.61 -8 -9 -11 -2.19 3.70 8 -9 12 0.19 1.97 -8 9 -12 1.01 1.79 -8 -9 -12 3.16 3.64 8 -9 13 4.06 2.28 -8 9 -13 6.19 2.31 -8 -9 -13 6.81 3.46 -8 9 -14 134.34 9.12 8 -9 14 142.63 9.63 -8 -9 -14 116.59 12.10 8 -9 15 4.28 2.23 -8 -9 -15 5.49 3.49 8 -9 16 7.86 2.99 -8 -9 -16 4.11 3.89 8 -9 17 -0.36 1.67 -8 -9 -17 4.25 3.34 -8 -9 -18 26.06 5.53 -8 -9 -19 2.42 2.73 -8 -9 -20 14.96 4.51 -8 -9 -21 4.29 3.06 -8 -9 -22 4.67 2.39 -8 -9 -23 7.34 2.75 -8 -9 -24 21.10 3.50 -8 10 23 3.47 1.20 -8 10 22 6.75 1.77 -8 10 21 3.86 1.47 8 -10 -20 8.60 1.92 -8 10 20 10.58 2.33 8 -10 -19 30.16 3.60 -8 10 19 31.55 3.86 8 -10 -18 17.07 3.13 -8 10 18 18.01 3.17 8 -10 -17 3.88 2.00 -8 10 17 0.78 1.52 8 -10 -16 21.49 3.46 -8 10 16 18.72 3.42 8 -10 -15 4.26 1.94 -8 10 15 2.13 1.55 8 -10 -14 75.42 6.59 -8 10 14 69.52 6.49 8 -10 -13 127.49 8.70 -8 10 13 119.65 8.75 8 -10 -12 52.71 5.80 -8 10 12 45.28 5.41 8 -10 -11 67.08 6.53 -8 10 11 59.07 6.12 8 -10 -10 22.41 4.04 -8 10 10 18.78 3.73 8 -10 -9 193.21 11.27 -8 10 9 199.02 11.32 8 -10 -8 122.72 8.94 -8 10 8 121.07 8.71 8 -10 -7 30.66 4.65 -8 10 7 30.98 4.55 8 -10 -6 27.36 4.52 -8 10 6 23.67 3.92 8 -10 -5 42.72 5.44 -8 10 5 46.98 5.28 8 -10 -4 11.99 3.08 -8 10 4 10.60 2.81 8 -10 -3 4.36 2.46 -8 10 3 3.89 2.01 8 -10 -2 3.40 2.16 -8 10 2 0.19 1.66 8 -10 -1 9.60 2.84 8 -10 0 20.26 3.74 8 -10 1 9.56 2.91 8 -10 2 18.75 4.23 8 -10 3 17.01 4.22 8 -10 4 37.43 5.12 8 -10 5 5.93 2.83 8 -10 6 63.92 7.08 8 -10 7 83.71 7.59 -8 -10 -8 194.08 13.80 8 -10 8 213.77 11.92 -8 -10 -9 45.94 7.01 8 -10 9 65.59 6.88 8 -10 10 6.62 3.00 -8 -10 -10 5.53 3.05 8 -10 11 19.41 4.00 -8 -10 -11 14.60 4.86 8 -10 12 129.81 9.04 -8 -10 -12 124.08 11.88 8 -10 13 1.80 2.34 -8 -10 -13 -1.27 2.54 8 -10 14 21.07 3.89 -8 -10 -14 10.80 3.95 -8 -10 -15 41.59 7.08 8 -10 15 49.00 5.46 8 -10 16 22.77 3.43 -8 -10 -16 32.99 6.30 -8 -10 -17 3.71 3.07 -8 -10 -18 2.55 2.64 -8 -10 -19 20.70 4.77 -8 -10 -20 6.89 3.29 -8 -10 -21 19.85 3.94 -8 -10 -22 4.15 2.72 -8 -10 -23 16.42 3.26 8 -11 -23 2.34 1.10 8 -11 -22 2.48 1.60 8 -11 -21 15.40 2.12 8 -11 -20 29.57 3.15 8 -11 -19 1.30 1.03 8 -11 -18 9.19 2.16 8 -11 -17 31.83 3.84 8 -11 -16 4.87 1.92 8 -11 -15 2.01 1.93 8 -11 -14 117.94 7.91 8 -11 -13 7.73 2.72 8 -11 -12 3.86 2.33 8 -11 -11 40.16 4.92 8 -11 -10 86.27 7.20 8 -11 -9 6.02 2.75 8 -11 -8 28.93 4.73 8 -11 -7 6.85 3.24 8 -11 -6 109.92 8.39 8 -11 -5 52.80 5.82 8 -11 -4 3.40 2.86 8 -11 -4 5.08 2.09 8 -11 -3 2.94 2.72 8 -11 -3 1.48 1.29 8 -11 -2 28.27 4.57 8 -11 -1 8.14 3.59 8 -11 0 14.41 3.78 8 -11 1 37.93 5.16 8 -11 2 2.38 2.00 8 -11 3 10.24 3.23 8 -11 4 34.22 5.17 8 -11 5 31.11 4.74 -8 -11 -6 126.33 8.58 8 -11 6 124.16 8.78 8 -11 7 1.16 1.89 8 -11 8 34.92 4.81 8 -11 9 8.38 3.04 -8 -11 -9 5.31 2.34 8 -11 10 3.54 2.26 -8 -11 -10 1.46 2.62 8 -11 11 -0.31 1.70 -8 -11 -11 4.54 3.32 8 -11 12 4.62 2.16 -8 -11 -12 2.27 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3.09 1.40 -11 9 -2 3.88 1.54 11 -9 3 1.53 1.35 -11 9 -3 0.97 1.21 11 -9 4 1.04 1.39 -11 9 -4 2.64 1.39 11 -9 5 0.61 1.25 -11 9 -5 3.26 1.59 11 -9 6 1.60 1.23 -11 9 -6 1.85 1.27 11 -9 7 6.84 1.76 -11 9 -7 5.96 1.70 11 -9 8 2.01 1.23 -11 9 -8 1.81 1.28 -11 10 6 17.58 2.51 -11 10 5 73.40 4.90 -11 10 4 30.19 3.24 11 -10 -4 27.93 2.97 11 -10 -3 2.03 1.17 -11 10 3 3.39 1.52 11 -10 -2 4.41 1.43 -11 10 2 2.34 1.21 -11 10 1 26.55 2.96 11 -10 -1 30.07 3.14 11 -10 0 7.93 1.85 -11 10 0 7.92 1.98 11 -10 1 2.08 1.46 -11 10 -1 2.65 2.04 11 -10 2 8.63 1.91 11 -10 3 2.44 1.37 11 -10 4 3.44 1.36 11 -10 5 3.56 1.39 11 -10 6 5.51 1.52 11 -10 7 6.74 1.55 -12 0 13 -0.48 0.99 -12 0 12 10.35 1.97 -12 0 11 0.69 1.14 -12 0 10 13.36 2.48 -12 0 9 0.55 1.11 -12 0 8 4.95 1.81 -12 0 7 -2.12 1.10 -12 0 6 12.03 2.47 -12 0 5 1.08 1.45 -12 0 4 4.32 2.10 -12 0 3 2.28 2.52 -12 0 2 33.63 4.35 -12 0 1 0.23 2.36 -12 0 0 6.51 2.24 -12 0 -1 1.46 1.47 -12 0 -2 45.41 5.10 -12 0 -3 6.69 2.70 -12 0 -4 15.78 3.11 -12 0 -5 -0.51 1.55 -12 0 -6 2.23 2.05 -12 0 -7 1.73 1.75 -12 0 -8 5.47 2.08 -12 0 -9 -0.38 1.54 -12 0 -10 6.86 2.19 -12 0 -11 3.57 2.28 12 0 13 2.83 1.58 12 0 14 224.46 9.08 -12 1 14 -0.61 0.96 -12 1 13 4.26 1.57 -12 1 12 2.23 1.23 -12 1 11 60.90 4.94 -12 1 10 7.86 2.17 -12 1 9 2.89 1.63 -12 -1 8 33.50 3.93 -12 1 8 39.95 4.43 -12 -1 7 137.65 7.98 -12 1 7 137.66 8.38 -12 -1 6 80.74 6.49 -12 1 6 91.17 7.05 -12 -1 5 50.16 5.39 -12 1 5 61.71 6.23 -12 -1 4 63.67 6.00 -12 1 4 61.02 6.15 -12 1 3 37.48 4.58 -12 -1 3 26.86 3.95 -12 -1 2 4.93 2.43 -12 1 2 3.64 2.79 -12 -1 1 4.87 1.95 -12 1 1 4.11 1.94 -12 -1 0 4.19 1.70 -12 1 0 3.70 2.01 -12 -1 -1 2.89 1.77 -12 1 -1 2.35 1.78 -12 -1 -2 2.54 2.27 -12 1 -2 0.99 2.75 -12 -1 -3 60.78 5.89 -12 1 -3 64.41 6.01 -12 -1 -4 16.45 3.51 -12 1 -4 13.79 2.89 -12 -1 -5 7.98 2.48 -12 1 -5 11.21 2.81 -12 -1 -6 51.65 5.40 -12 1 -6 66.93 6.01 -12 -1 -7 2.18 1.90 -12 1 -7 5.75 2.38 -12 -1 -8 36.93 4.61 -12 1 -8 41.51 4.80 -12 -1 -9 3.07 1.56 -12 1 -9 7.95 2.34 -12 -1 -10 3.89 1.93 -12 1 -10 6.50 2.41 -12 1 -11 6.56 2.21 12 1 12 16.42 2.70 12 -1 12 18.70 2.83 12 1 13 6.67 1.88 12 -1 13 3.55 1.47 12 1 14 2.98 1.35 12 -1 14 1.98 1.23 -12 2 15 5.14 1.27 -12 2 14 6.07 1.54 -12 2 13 8.94 1.89 -12 2 12 12.20 2.28 -12 2 11 2.64 1.48 -12 2 10 2.32 1.36 -12 2 9 2.19 1.60 -12 2 8 27.67 3.72 -12 2 7 27.72 3.95 -12 2 6 15.75 3.23 -12 2 5 1.71 2.27 -12 2 4 18.79 3.29 -12 2 3 -1.05 1.26 -12 2 2 5.51 1.56 -12 2 1 0.44 1.41 -12 2 0 1.61 1.63 -12 2 -1 2.29 1.57 -12 2 -2 2.54 1.54 -12 2 -3 3.18 2.54 -12 2 -4 33.05 4.30 -12 2 -5 5.48 2.30 -12 2 -6 5.97 2.18 -12 2 -7 5.07 2.41 -12 2 -8 67.70 5.98 -12 2 -9 1.16 1.42 -12 2 -10 25.46 3.72 -12 2 -11 2.96 1.57 -12 2 -12 7.41 2.26 12 2 12 9.14 2.20 12 -2 12 8.14 1.97 12 2 13 6.47 1.76 12 -2 13 8.41 1.84 12 -2 14 8.24 1.79 -12 3 15 1.75 0.85 -12 3 14 -0.97 0.79 -12 3 13 33.56 3.45 -12 3 12 4.31 1.57 -12 3 11 -0.24 1.03 -12 3 10 -0.69 1.14 -12 3 9 6.64 1.92 -12 3 8 -1.36 1.32 -12 3 7 6.06 1.91 -12 3 6 1.08 1.23 -12 3 5 2.73 1.61 -12 3 4 25.10 3.92 -12 3 3 16.63 3.37 -12 3 2 3.20 2.00 -12 3 1 -0.38 1.25 -12 3 0 13.24 2.94 -12 3 -1 8.51 2.55 -12 3 -2 5.40 2.13 -12 3 -3 0.40 1.48 -12 3 -4 5.89 2.40 -12 3 -5 69.90 6.07 -12 3 -6 5.48 2.16 -12 3 -7 13.67 2.95 -12 3 -8 3.78 2.01 -12 3 -9 4.61 1.93 -12 3 -10 5.24 2.15 12 3 11 48.71 4.24 12 -3 11 48.49 4.13 -12 3 -12 1.71 1.68 12 3 12 0.71 0.94 12 -3 12 0.34 0.97 12 -3 13 4.74 1.49 -12 4 14 2.71 1.09 -12 4 13 20.46 2.63 -12 4 12 -1.73 1.24 -12 4 11 9.50 2.11 -12 4 10 2.27 1.51 -12 4 9 19.06 2.88 -12 4 8 46.74 4.68 -12 4 7 2.06 2.35 -12 4 6 2.55 1.27 -12 4 5 14.28 3.08 -12 4 4 12.43 2.87 -12 4 3 9.87 2.44 -12 4 2 7.43 2.75 -12 4 1 21.41 3.55 -12 4 0 18.06 3.65 -12 4 -1 28.31 4.09 -12 4 -2 3.76 2.33 -12 4 -3 11.55 3.28 -12 4 -4 38.03 4.85 -12 4 -5 94.97 6.90 -12 4 -6 2.10 1.61 -12 4 -7 0.60 1.44 -12 4 -8 1.11 1.37 -12 4 -9 19.83 3.32 -12 4 -10 60.70 5.36 12 4 10 73.05 5.09 -12 4 -11 15.37 2.79 12 -4 11 19.40 2.43 -12 5 14 1.78 1.02 -12 5 13 8.04 1.68 -12 5 12 52.13 4.20 -12 5 11 32.87 3.57 -12 5 10 1.54 1.22 -12 5 9 3.58 1.52 -12 5 8 1.76 1.10 -12 5 7 3.11 1.38 -12 5 6 -1.01 1.38 -12 5 5 4.61 1.90 -12 5 4 0.31 1.48 -12 5 3 1.61 1.39 -12 5 2 3.34 2.04 -12 5 1 11.16 2.44 -12 5 0 -0.17 1.52 -12 5 -1 0.35 1.42 -12 5 -2 2.72 1.70 -12 5 -3 15.25 2.94 -12 5 -4 5.59 1.87 -12 5 -5 6.13 2.01 -12 5 -6 1.42 1.62 -12 5 -7 6.14 2.15 -12 5 -8 8.99 2.13 -12 5 -9 1.01 1.49 12 -5 9 0.41 0.84 -12 5 -10 0.20 1.01 -12 5 -11 4.93 1.66 -12 6 12 4.74 1.37 -12 6 11 26.16 2.95 -12 6 10 19.87 2.69 -12 6 9 38.21 3.82 -12 6 8 2.95 1.75 -12 6 7 40.04 4.04 -12 6 6 2.91 1.73 -12 6 5 -0.35 1.05 -12 6 4 0.13 1.14 -12 6 3 4.28 1.53 -12 6 2 4.30 1.66 -12 6 1 5.49 2.55 -12 6 0 53.63 4.95 -12 6 -1 2.46 1.53 -12 6 -2 8.57 2.14 -12 6 -3 1.83 1.61 -12 6 -4 0.97 1.53 -12 6 -5 4.54 1.90 -12 6 -6 29.88 3.59 -12 6 -7 5.73 1.73 -12 6 -8 10.34 2.04 -12 6 -9 1.02 1.18 -12 7 10 2.10 1.04 -12 7 9 0.99 0.88 -12 7 8 0.97 1.18 -12 7 7 -0.60 1.13 -12 7 6 4.12 1.52 -12 7 5 10.89 2.19 -12 7 4 5.06 1.93 -12 7 3 9.09 2.07 -12 7 2 4.28 1.81 -12 7 1 3.61 1.50 -12 7 0 19.39 2.93 -12 7 -1 1.47 1.43 -12 7 -2 2.85 1.54 -12 7 -3 6.20 1.73 -12 7 -4 0.16 1.11 -12 7 -5 3.59 1.57 -12 7 -6 0.18 1.17 -12 7 -7 21.05 2.69 -12 8 4 9.72 1.84 -12 8 3 3.96 1.54 -12 8 2 24.10 2.81 -12 8 1 5.13 1.73 -12 8 0 5.28 1.48 -12 8 -1 0.51 0.83 -13 2 2 3.76 1.62 -13 2 1 3.98 1.37 -13 2 0 5.15 1.78 -13 2 -1 28.94 3.23 -13 3 1 1.97 1.34 0 0 0 0.00 0.00 TITL exp_2723 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 10.706905 16.748296 31.061134 90.0000 91.7173 90.0000 ZERR 3.00 0.000662 0.000611 0.001218 0.0000 0.0045 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N UNIT 300.00 300.00 21.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 50945 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.953 _oxdiff_exptl_absorpt_empirical_full_min 0.708 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.65243(8) 0.30548(5) 0.39481(3) 0.0253(2) Uani 1 1 d . . . . . Cl4 Cl 0.82474(13) 0.36773(7) 0.27059(4) 0.0488(3) Uani 1 1 d . . . . . Cl3 Cl 0.66267(13) 0.48497(9) 0.30741(4) 0.0549(4) Uani 1 1 d . . . . . Cl2 Cl 0.92527(13) 0.51891(8) 0.30009(5) 0.0602(4) Uani 1 1 d . . . . . N7 N 0.3596(3) 0.31054(19) 0.35016(10) 0.0191(6) Uani 1 1 d . . . . . N6 N 0.4885(3) 0.46145(19) 0.38788(10) 0.0192(6) Uani 1 1 d . . . . . N2 N 0.6870(3) -0.01484(18) 0.37244(10) 0.0189(6) Uani 1 1 d . . . . . H2 H 0.703465 -0.057711 0.357246 0.023 Uiso 1 1 calc R . . . . N4 N 0.9592(3) 0.31586(19) 0.42243(10) 0.0195(6) Uani 1 1 d . . . . . N5 N 0.7844(3) 0.4636(2) 0.42287(10) 0.0196(6) Uani 1 1 d . . . . . N3 N 0.9552(3) 0.14546(18) 0.41409(10) 0.0202(6) Uani 1 1 d . . . . . N1 N 0.3941(3) 0.14118(18) 0.34348(10) 0.0201(6) Uani 1 1 d . . . . . C6 C 0.5727(3) 0.0238(2) 0.37236(11) 0.0188(7) Uani 1 1 d . . . . . C9 C 0.7711(3) 0.0234(2) 0.39969(12) 0.0200(7) Uani 1 1 d . . . . . C31 C 0.2764(3) 0.2613(2) 0.32911(12) 0.0207(8) Uani 1 1 d . . . . . C11 C 0.9891(3) 0.0644(2) 0.40953(11) 0.0198(7) Uani 1 1 d . . . . . C15 C 1.0639(3) 0.2690(2) 0.42608(11) 0.0189(7) Uani 1 1 d . . . . . C27 C 0.3726(3) 0.4563(2) 0.36880(12) 0.0205(7) Uani 1 1 d . . . . . C5 C 0.4724(3) 0.0047(2) 0.34220(12) 0.0201(7) Uani 1 1 d . . . . . C28 C 0.3156(3) 0.3869(2) 0.34967(12) 0.0210(8) Uani 1 1 d . . . . . C1 C 0.2967(3) 0.1766(2) 0.32483(12) 0.0214(8) Uani 1 1 d . . . . . C50 C 0.6042(3) 0.6568(2) 0.43753(12) 0.0198(7) Uani 1 1 d . . . . . C38 C 0.9430(3) -0.0778(2) 0.39074(12) 0.0205(7) Uani 1 1 d . . . . . C32 C 0.4713(3) -0.0764(2) 0.32161(12) 0.0200(7) Uani 1 1 d . . . . . C10 C 0.9030(3) 0.0057(2) 0.40087(11) 0.0200(7) Uani 1 1 d . . . . . C23 C 0.6177(3) 0.5710(2) 0.42300(11) 0.0202(7) Uani 1 1 d . . . . . C43 C 0.9685(3) -0.0988(2) 0.34818(12) 0.0215(8) Uani 1 1 d . . . . . C47 C 0.5824(4) 0.8150(2) 0.46618(13) 0.0234(8) Uani 1 1 d . . . . . C22 C 0.7378(3) 0.5399(2) 0.43116(11) 0.0200(7) Uani 1 1 d . . . . . C7 C 0.5839(3) 0.0844(2) 0.40333(12) 0.0196(7) Uani 1 1 d . . . . . H7A H 0.519451 0.119798 0.411494 0.023 Uiso 1 1 calc R . . . . C8 C 0.7054(3) 0.0835(2) 0.41999(12) 0.0220(8) Uani 1 1 d . . . . . H8 H 0.738403 0.118269 0.441674 0.026 Uiso 1 1 calc R . . . . C48 C 0.6217(4) 0.7980(2) 0.42510(13) 0.0239(8) Uani 1 1 d . . . . . H48 H 0.639971 0.841006 0.406373 0.029 Uiso 1 1 calc R . . . . C19 C 0.9081(3) 0.4608(2) 0.43387(11) 0.0209(7) Uani 1 1 d . . . . . C24 C 0.5100(4) 0.5388(2) 0.40318(12) 0.0214(8) Uani 1 1 d . . . . . C21 C 0.8399(4) 0.5846(2) 0.44793(13) 0.0245(8) Uani 1 1 d . . . . . H21 H 0.836871 0.638778 0.456965 0.029 Uiso 1 1 calc R . . . . C13 C 1.1701(3) 0.1310(2) 0.42061(12) 0.0223(8) Uani 1 1 d . . . . . H13 H 1.255329 0.145551 0.424968 0.027 Uiso 1 1 calc R . . . . C14 C 1.0616(3) 0.1841(2) 0.42022(11) 0.0200(7) Uani 1 1 d . . . . . C17 C 1.1183(3) 0.3957(2) 0.44172(12) 0.0228(8) Uani 1 1 d . . . . . H17 H 1.165544 0.441679 0.449761 0.027 Uiso 1 1 calc R . . . . C45 C 0.5655(3) 0.6722(2) 0.47968(12) 0.0209(8) Uani 1 1 d . . . . . C3 C 0.2760(4) 0.0508(2) 0.30203(12) 0.0237(8) Uani 1 1 d . . . . . H3 H 0.249338 0.002560 0.288508 0.028 Uiso 1 1 calc R . . . . C25 C 0.3998(4) 0.5820(2) 0.39300(13) 0.0251(8) Uani 1 1 d . . . . . H25 H 0.385382 0.636378 0.399893 0.030 Uiso 1 1 calc R . . . . C18 C 0.9902(3) 0.3939(2) 0.43168(12) 0.0207(7) Uani 1 1 d . . . . . C39 C 0.9534(4) -0.1342(2) 0.42408(12) 0.0236(8) Uani 1 1 d . . . . . C12 C 1.1242(3) 0.0573(2) 0.41350(12) 0.0218(8) Uani 1 1 d . . . . . H12 H 1.171296 0.009441 0.411462 0.026 Uiso 1 1 calc R . . . . C49 C 0.6356(3) 0.7195(2) 0.41015(12) 0.0213(8) Uani 1 1 d . . . . . C20 C 0.9444(4) 0.5369(2) 0.44903(12) 0.0243(8) Uani 1 1 d . . . . . H20 H 1.026199 0.552403 0.458315 0.029 Uiso 1 1 calc R . . . . C46 C 0.5550(4) 0.7512(2) 0.49299(12) 0.0223(8) Uani 1 1 d . . . . . H46 H 0.528268 0.761866 0.521304 0.027 Uiso 1 1 calc R . . . . C40 C 0.9929(4) -0.2111(2) 0.41431(13) 0.0240(8) Uani 1 1 d . . . . . H40 H 1.000812 -0.249485 0.436723 0.029 Uiso 1 1 calc R . . . . C41 C 1.0211(4) -0.2330(2) 0.37252(13) 0.0251(8) Uani 1 1 d . . . . . C16 C 1.1647(4) 0.3182(2) 0.43787(12) 0.0236(8) Uani 1 1 d . . . . . H16 H 1.249042 0.301954 0.442412 0.028 Uiso 1 1 calc R . . . . C42 C 1.0072(3) -0.1774(2) 0.34001(13) 0.0239(8) Uani 1 1 d . . . . . H42 H 1.024123 -0.192586 0.311302 0.029 Uiso 1 1 calc R . . . . N9 N 0.2212(4) 0.6140(3) 0.47731(14) 0.0450(10) Uani 1 1 d . . . . . C4 C 0.3862(3) 0.0612(2) 0.33032(12) 0.0198(7) Uani 1 1 d . . . . . C34 C 0.4060(4) -0.2139(2) 0.31996(13) 0.0257(8) Uani 1 1 d . . . . . H34 H 0.360040 -0.256472 0.331978 0.031 Uiso 1 1 calc R . . . . C33 C 0.4056(3) -0.1392(2) 0.34009(12) 0.0219(8) Uani 1 1 d . . . . . C30 C 0.1747(4) 0.3074(2) 0.31496(13) 0.0263(8) Uani 1 1 d . . . . . H30 H 0.102621 0.288898 0.299432 0.032 Uiso 1 1 calc R . . . . C35 C 0.4722(4) -0.2273(2) 0.28275(13) 0.0274(9) Uani 1 1 d . . . . . C37 C 0.5375(4) -0.0885(2) 0.28370(12) 0.0247(8) Uani 1 1 d . . . . . C59 C 0.6844(4) 0.7039(2) 0.36598(13) 0.0280(9) Uani 1 1 d . . . . . H59A H 0.768247 0.680639 0.368670 0.042 Uiso 1 1 calc GR . . . . H59B H 0.688272 0.754282 0.349999 0.042 Uiso 1 1 calc GR . . . . H59C H 0.628494 0.666722 0.350505 0.042 Uiso 1 1 calc GR . . . . C29 C 0.1990(4) 0.3860(2) 0.32795(13) 0.0272(9) Uani 1 1 d . . . . . H29 H 0.145959 0.430697 0.322935 0.033 Uiso 1 1 calc R . . . . C26 C 0.3167(4) 0.5324(2) 0.37149(13) 0.0274(9) Uani 1 1 d . . . . . H26 H 0.236185 0.546777 0.360417 0.033 Uiso 1 1 calc R . . . . C36 C 0.5372(4) -0.1647(2) 0.26530(13) 0.0269(8) Uani 1 1 d . . . . . H36 H 0.583191 -0.173541 0.240047 0.032 Uiso 1 1 calc R . . . . C2 C 0.2196(4) 0.1221(2) 0.29873(13) 0.0255(8) Uani 1 1 d . . . . . H2A H 0.145114 0.134568 0.282754 0.031 Uiso 1 1 calc R . . . . C55 C 1.0678(4) -0.3164(2) 0.36355(15) 0.0322(9) Uani 1 1 d . . . . . H55A H 1.143415 -0.326843 0.381202 0.048 Uiso 1 1 calc GR . . . . H55B H 1.086978 -0.321176 0.333005 0.048 Uiso 1 1 calc GR . . . . H55C H 1.003159 -0.355329 0.370628 0.048 Uiso 1 1 calc GR . . . . C57 C 0.5368(4) 0.6054(2) 0.51006(13) 0.0278(9) Uani 1 1 d . . . . . H57A H 0.468545 0.572870 0.497742 0.042 Uiso 1 1 calc GR . . . . H57B H 0.511717 0.627696 0.537676 0.042 Uiso 1 1 calc GR . . . . H57C H 0.611251 0.572134 0.514603 0.042 Uiso 1 1 calc GR . . . . C51 C 0.3324(4) -0.1281(2) 0.38026(13) 0.0276(8) Uani 1 1 d . . . . . H51A H 0.375905 -0.090040 0.399397 0.041 Uiso 1 1 calc GR . . . . H51B H 0.324601 -0.179509 0.395031 0.041 Uiso 1 1 calc GR . . . . H51C H 0.249007 -0.107583 0.372525 0.041 Uiso 1 1 calc GR . . . . C54 C 0.9253(4) -0.1123(3) 0.46990(13) 0.0321(9) Uani 1 1 d . . . . . H54A H 0.995442 -0.081888 0.482577 0.048 Uiso 1 1 calc GR . . . . H54B H 0.912956 -0.161055 0.486684 0.048 Uiso 1 1 calc GR . . . . H54C H 0.849315 -0.079727 0.470194 0.048 Uiso 1 1 calc GR . . . . C58 C 0.5672(4) 0.9003(2) 0.48134(14) 0.0298(9) Uani 1 1 d . . . . . H58A H 0.590624 0.937002 0.458363 0.045 Uiso 1 1 calc GR . . . . H58B H 0.621307 0.909489 0.506874 0.045 Uiso 1 1 calc GR . . . . H58C H 0.479983 0.909615 0.488577 0.045 Uiso 1 1 calc GR . . . . C56 C 0.9579(4) -0.0398(3) 0.31210(13) 0.0301(9) Uani 1 1 d . . . . . H56A H 0.879681 -0.009913 0.314194 0.045 Uiso 1 1 calc GR . . . . H56B H 0.958511 -0.068146 0.284497 0.045 Uiso 1 1 calc GR . . . . H56C H 1.028703 -0.002731 0.313953 0.045 Uiso 1 1 calc GR . . . . C64 C 0.2263(4) 0.6803(3) 0.48572(14) 0.0364(11) Uani 1 1 d . . . . . C53 C 0.6055(4) -0.0214(3) 0.26232(14) 0.0333(9) Uani 1 1 d . . . . . H53A H 0.548921 0.024144 0.258231 0.050 Uiso 1 1 calc GR . . . . H53B H 0.634404 -0.039305 0.234283 0.050 Uiso 1 1 calc GR . . . . H53C H 0.677499 -0.005302 0.280531 0.050 Uiso 1 1 calc GR . . . . C52 C 0.4755(4) -0.3097(3) 0.26307(15) 0.0359(10) Uani 1 1 d . . . . . H52A H 0.409567 -0.342631 0.275152 0.054 Uiso 1 1 calc GR . . . . H52B H 0.557051 -0.334241 0.269475 0.054 Uiso 1 1 calc GR . . . . H52C H 0.462159 -0.305597 0.231793 0.054 Uiso 1 1 calc GR . . . . C62 C 1.2232(5) 0.6721(3) 0.17978(15) 0.0367(10) Uani 1 1 d . . . . . C61 C 1.1551(5) 0.6622(3) 0.21887(16) 0.0401(11) Uani 1 1 d . . . . . N8 N 1.1006(5) 0.6540(4) 0.24986(16) 0.0721(17) Uani 1 1 d . . . . . C63 C 0.2334(5) 0.7635(3) 0.49720(16) 0.0423(11) Uani 1 1 d . . . . . H63A H 0.258948 0.794676 0.472249 0.063 Uiso 1 1 calc GR . . . . H63B H 0.294789 0.770656 0.520934 0.063 Uiso 1 1 calc GR . . . . H63C H 0.151330 0.781900 0.506240 0.063 Uiso 1 1 calc GR . . . . C60 C 0.8130(5) 0.4432(3) 0.30957(15) 0.0473(13) Uani 1 1 d . . . . . H60 H 0.829550 0.419704 0.338792 0.057 Uiso 1 1 calc R . . . . H62A H 1.272(6) 0.734(4) 0.180(2) 0.08(2) Uiso 1 1 d . . . . . H62B H 1.172(6) 0.666(4) 0.155(2) 0.063(18) Uiso 1 1 d . . . . . H62C H 1.297(6) 0.633(4) 0.1789(19) 0.062(18) Uiso 1 1 d . . . . . H4 H 0.889(4) 0.299(2) 0.4160(12) 0.013(10) Uiso 1 1 d . . . . . H7 H 0.423(4) 0.299(3) 0.3615(13) 0.015(10) Uiso 1 1 d . . . . . H5 H 0.750(5) 0.425(3) 0.4160(16) 0.035(14) Uiso 1 1 d . . . . . H6 H 0.536(4) 0.420(3) 0.3899(14) 0.027(12) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0216(4) 0.0180(4) 0.0360(5) -0.0044(4) -0.0061(4) 0.0035(3) Cl4 0.0700(9) 0.0285(6) 0.0490(7) 0.0004(5) 0.0193(6) -0.0005(5) Cl3 0.0526(8) 0.0621(8) 0.0514(7) 0.0027(6) 0.0225(6) 0.0080(6) Cl2 0.0465(7) 0.0463(7) 0.0862(10) -0.0152(7) -0.0280(7) 0.0089(6) N7 0.0159(15) 0.0191(16) 0.0221(15) 0.0011(13) -0.0032(12) 0.0039(12) N6 0.0188(15) 0.0148(15) 0.0241(15) -0.0012(13) 0.0000(12) 0.0039(13) N2 0.0196(15) 0.0151(14) 0.0220(15) -0.0010(12) -0.0006(12) 0.0004(12) N4 0.0150(15) 0.0175(15) 0.0257(16) -0.0004(13) -0.0020(12) -0.0017(12) N5 0.0208(16) 0.0153(16) 0.0224(15) -0.0016(13) -0.0019(12) -0.0020(13) N3 0.0181(15) 0.0174(15) 0.0251(15) -0.0012(13) -0.0027(12) 0.0030(12) N1 0.0193(15) 0.0163(15) 0.0247(15) -0.0026(13) -0.0012(12) 0.0017(12) C6 0.0176(17) 0.0167(17) 0.0218(17) 0.0013(14) -0.0009(14) 0.0018(14) C9 0.0192(18) 0.0171(18) 0.0237(18) 0.0022(15) 0.0006(14) -0.0014(14) C31 0.0200(18) 0.0200(19) 0.0218(17) -0.0002(15) -0.0032(14) 0.0035(15) C11 0.0182(18) 0.0201(18) 0.0208(17) -0.0016(15) -0.0023(14) 0.0028(14) C15 0.0199(18) 0.0197(18) 0.0172(16) -0.0001(14) -0.0007(13) 0.0033(14) C27 0.0187(18) 0.0211(18) 0.0215(17) 0.0006(15) -0.0028(14) 0.0009(15) C5 0.0203(18) 0.0170(18) 0.0230(18) -0.0018(15) 0.0018(14) -0.0013(14) C28 0.0229(18) 0.0171(18) 0.0230(18) -0.0022(15) -0.0011(14) 0.0020(15) C1 0.0186(18) 0.0213(19) 0.0242(18) -0.0025(15) -0.0028(14) 0.0002(15) C50 0.0189(18) 0.0133(17) 0.0271(18) -0.0014(15) -0.0033(14) -0.0001(14) C38 0.0168(17) 0.0184(18) 0.0259(18) -0.0016(15) -0.0039(14) 0.0006(14) C32 0.0190(18) 0.0139(17) 0.0266(18) -0.0033(15) -0.0048(14) 0.0030(14) C10 0.0207(18) 0.0204(18) 0.0189(17) 0.0007(14) -0.0013(14) 0.0035(15) C23 0.0242(19) 0.0175(18) 0.0189(17) 0.0004(14) 0.0023(14) -0.0002(14) C43 0.0200(18) 0.0199(18) 0.0245(18) 0.0006(15) -0.0024(14) -0.0002(14) C47 0.0247(19) 0.0142(18) 0.031(2) -0.0015(15) -0.0054(15) 0.0002(15) C22 0.0241(19) 0.0164(17) 0.0194(17) 0.0012(14) 0.0010(14) 0.0015(15) C7 0.0197(18) 0.0134(17) 0.0255(18) -0.0032(14) -0.0003(14) 0.0034(14) C8 0.0229(19) 0.0194(18) 0.0237(18) -0.0024(15) -0.0014(15) 0.0024(15) C48 0.0266(19) 0.0163(18) 0.0287(19) 0.0058(15) -0.0017(16) -0.0022(15) C19 0.0216(18) 0.0208(19) 0.0203(17) 0.0009(15) -0.0016(14) 0.0000(15) C24 0.0248(19) 0.0178(18) 0.0217(17) -0.0009(15) 0.0017(15) 0.0007(15) C21 0.026(2) 0.0152(18) 0.032(2) 0.0008(16) -0.0034(16) -0.0001(15) C13 0.0148(17) 0.027(2) 0.0251(18) -0.0034(16) -0.0015(14) 0.0027(15) C14 0.0232(19) 0.0206(18) 0.0160(16) -0.0009(14) -0.0016(14) 0.0007(15) C17 0.0190(18) 0.0208(19) 0.0285(19) -0.0036(16) -0.0019(15) -0.0039(15) C45 0.0215(18) 0.0148(17) 0.0264(19) -0.0004(15) -0.0009(15) 0.0004(14) C3 0.0218(19) 0.0209(19) 0.0280(19) -0.0064(16) -0.0072(15) -0.0018(15) C25 0.027(2) 0.0133(17) 0.034(2) -0.0021(16) -0.0029(16) 0.0029(15) C18 0.0216(18) 0.0170(18) 0.0237(18) 0.0001(15) -0.0001(14) -0.0007(15) C39 0.0213(19) 0.024(2) 0.0249(19) 0.0011(16) -0.0042(15) 0.0022(15) C12 0.0203(18) 0.0202(19) 0.0248(18) -0.0009(15) 0.0004(14) 0.0071(15) C49 0.0226(18) 0.0183(18) 0.0228(18) 0.0010(15) -0.0019(14) 0.0022(15) C20 0.0228(19) 0.0223(19) 0.0277(19) -0.0030(16) -0.0021(15) -0.0012(15) C46 0.0246(19) 0.0189(18) 0.0231(18) -0.0010(15) -0.0015(15) 0.0026(15) C40 0.0225(19) 0.0191(19) 0.030(2) 0.0041(16) -0.0042(15) -0.0006(15) C41 0.0200(18) 0.0206(19) 0.035(2) -0.0050(16) -0.0014(15) -0.0028(15) C16 0.0206(18) 0.025(2) 0.0251(18) -0.0030(16) -0.0043(15) 0.0007(15) C42 0.0220(19) 0.022(2) 0.0272(19) -0.0052(16) 0.0020(15) 0.0011(15) N9 0.034(2) 0.053(3) 0.047(2) -0.011(2) 0.0015(18) -0.0097(19) C4 0.0188(18) 0.0185(18) 0.0221(17) -0.0028(15) -0.0024(14) -0.0023(14) C34 0.026(2) 0.0164(18) 0.034(2) 0.0002(16) -0.0055(16) -0.0026(15) C33 0.0185(18) 0.0188(18) 0.0281(19) -0.0015(15) -0.0047(15) 0.0033(14) C30 0.0217(19) 0.0221(19) 0.035(2) -0.0005(17) -0.0074(16) 0.0035(15) C35 0.033(2) 0.021(2) 0.0276(19) -0.0068(16) -0.0089(16) 0.0048(16) C37 0.028(2) 0.0203(19) 0.0257(19) -0.0031(16) -0.0035(15) 0.0023(16) C59 0.033(2) 0.025(2) 0.026(2) 0.0033(16) 0.0018(16) 0.0018(17) C29 0.0228(19) 0.023(2) 0.035(2) -0.0012(17) -0.0070(16) 0.0048(16) C26 0.0218(19) 0.022(2) 0.037(2) -0.0039(17) -0.0074(16) 0.0038(16) C36 0.031(2) 0.024(2) 0.0258(19) -0.0034(16) -0.0011(16) 0.0063(16) C2 0.0216(19) 0.024(2) 0.031(2) -0.0036(17) -0.0078(15) -0.0009(15) C55 0.034(2) 0.022(2) 0.042(2) -0.0033(18) 0.0029(18) 0.0065(17) C57 0.038(2) 0.0198(19) 0.0256(19) 0.0023(16) 0.0027(17) -0.0012(17) C51 0.028(2) 0.0206(19) 0.034(2) -0.0031(17) 0.0023(17) -0.0006(16) C54 0.040(2) 0.030(2) 0.026(2) 0.0008(18) -0.0028(18) 0.0099(19) C58 0.038(2) 0.0146(19) 0.036(2) -0.0023(17) 0.0012(18) 0.0000(16) C56 0.033(2) 0.029(2) 0.028(2) 0.0059(18) 0.0042(17) 0.0059(18) C64 0.028(2) 0.055(3) 0.026(2) -0.005(2) -0.0011(17) -0.007(2) C53 0.041(2) 0.030(2) 0.029(2) -0.0033(18) 0.0046(18) -0.0015(19) C52 0.043(3) 0.026(2) 0.038(2) -0.0111(19) -0.001(2) 0.0016(19) C62 0.046(3) 0.035(3) 0.029(2) 0.0009(19) -0.002(2) -0.002(2) C61 0.040(3) 0.037(3) 0.043(3) -0.013(2) -0.005(2) -0.011(2) N8 0.072(4) 0.095(4) 0.051(3) -0.019(3) 0.025(3) -0.042(3) C63 0.037(3) 0.049(3) 0.040(2) -0.008(2) 0.001(2) -0.005(2) C60 0.071(4) 0.043(3) 0.028(2) 0.004(2) -0.002(2) 0.014(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C31 N7 H7 128(3) . . ? C28 N7 C31 110.0(3) . . ? C28 N7 H7 122(3) . . ? C27 N6 C24 110.3(3) . . ? C27 N6 H6 120(3) . . ? C24 N6 H6 129(3) . . ? C6 N2 H2 124.9 . . ? C9 N2 H2 124.9 . . ? C9 N2 C6 110.2(3) . . ? C15 N4 C18 109.6(3) . . ? C15 N4 H4 124(3) . . ? C18 N4 H4 127(3) . . ? C22 N5 H5 130(4) . . ? C19 N5 C22 109.7(3) . . ? C19 N5 H5 119(4) . . ? C14 N3 C11 105.2(3) . . ? C1 N1 C4 105.2(3) . . ? N2 C6 C5 122.6(3) . . ? N2 C6 C7 106.3(3) . . ? C7 C6 C5 130.9(3) . . ? N2 C9 C10 122.8(3) . . ? N2 C9 C8 106.6(3) . . ? C8 C9 C10 130.2(3) . . ? N7 C31 C1 122.7(3) . . ? N7 C31 C30 107.9(3) . . ? C30 C31 C1 129.3(4) . . ? N3 C11 C12 109.2(3) . . ? C10 C11 N3 122.4(3) . . ? C10 C11 C12 128.4(3) . . ? N4 C15 C14 123.1(3) . . ? N4 C15 C16 107.9(3) . . ? C16 C15 C14 128.9(3) . . ? N6 C27 C28 127.1(3) . . ? N6 C27 C26 107.4(3) . . ? C26 C27 C28 125.5(3) . . ? C6 C5 C32 118.4(3) . . ? C4 C5 C6 120.5(3) . . ? C4 C5 C32 121.0(3) . . ? N7 C28 C27 127.8(3) . . ? N7 C28 C29 107.3(3) . . ? C29 C28 C27 124.8(3) . . ? N1 C1 C31 121.4(3) . . ? N1 C1 C2 112.9(3) . . ? C31 C1 C2 125.6(3) . . ? C45 C50 C23 118.9(3) . . ? C49 C50 C23 120.3(3) . . ? C49 C50 C45 120.7(3) . . ? C43 C38 C10 119.8(3) . . ? C43 C38 C39 120.9(3) . . ? C39 C38 C10 119.3(3) . . ? C33 C32 C5 120.3(3) . . ? C33 C32 C37 120.5(3) . . ? C37 C32 C5 119.3(3) . . ? C9 C10 C38 118.2(3) . . ? C11 C10 C9 120.7(3) . . ? C11 C10 C38 121.1(3) . . ? C22 C23 C50 113.2(3) . . ? C24 C23 C50 114.3(3) . . ? C24 C23 C22 132.5(4) . . ? C38 C43 C42 118.2(3) . . ? C38 C43 C56 121.9(3) . . ? C42 C43 C56 120.0(3) . . ? C48 C47 C46 118.0(3) . . ? C48 C47 C58 121.2(4) . . ? C46 C47 C58 120.8(4) . . ? N5 C22 C23 129.4(3) . . ? N5 C22 C21 106.0(3) . . ? C23 C22 C21 124.4(3) . . ? C6 C7 H7A 126.0 . . ? C8 C7 C6 108.0(3) . . ? C8 C7 H7A 126.0 . . ? C9 C8 H8 125.7 . . ? C7 C8 C9 108.7(3) . . ? C7 C8 H8 125.7 . . ? C47 C48 H48 118.8 . . ? C47 C48 C49 122.4(3) . . ? C49 C48 H48 118.8 . . ? N5 C19 C18 127.8(3) . . ? N5 C19 C20 108.0(3) . . ? C20 C19 C18 124.1(3) . . ? N6 C24 C23 129.3(3) . . ? N6 C24 C25 105.7(3) . . ? C23 C24 C25 125.0(3) . . ? C22 C21 H21 125.6 . . ? C20 C21 C22 108.8(3) . . ? C20 C21 H21 125.6 . . ? C14 C13 H13 127.2 . . ? C12 C13 H13 127.2 . . ? C12 C13 C14 105.7(3) . . ? N3 C14 C15 121.1(3) . . ? N3 C14 C13 112.6(3) . . ? C15 C14 C13 126.2(3) . . ? C18 C17 H17 126.0 . . ? C16 C17 H17 126.0 . . ? C16 C17 C18 108.1(3) . . ? C50 C45 C57 121.3(3) . . ? C46 C45 C50 118.6(3) . . ? C46 C45 C57 120.1(3) . . ? C4 C3 H3 126.5 . . ? C2 C3 H3 126.5 . . ? C2 C3 C4 107.0(3) . . ? C24 C25 H25 125.6 . . ? C26 C25 C24 108.9(3) . . ? C26 C25 H25 125.6 . . ? N4 C18 C19 127.6(3) . . ? N4 C18 C17 107.2(3) . . ? C17 C18 C19 125.1(3) . . ? C38 C39 C54 121.2(4) . . ? C40 C39 C38 118.7(4) . . ? C40 C39 C54 120.1(4) . . ? C11 C12 H12 126.4 . . ? C13 C12 C11 107.3(3) . . ? C13 C12 H12 126.4 . . ? C50 C49 C48 118.2(3) . . ? C50 C49 C59 121.4(3) . . ? C48 C49 C59 120.5(3) . . ? C19 C20 H20 126.2 . . ? C21 C20 C19 107.5(3) . . ? C21 C20 H20 126.2 . . ? C47 C46 H46 118.9 . . ? C45 C46 C47 122.1(4) . . ? C45 C46 H46 118.9 . . ? C39 C40 H40 119.2 . . ? C41 C40 C39 121.6(4) . . ? C41 C40 H40 119.2 . . ? C40 C41 C55 119.9(4) . . ? C42 C41 C40 118.9(4) . . ? C42 C41 C55 121.2(4) . . ? C15 C16 H16 126.4 . . ? C17 C16 C15 107.3(3) . . ? C17 C16 H16 126.4 . . ? C43 C42 H42 119.1 . . ? C41 C42 C43 121.8(4) . . ? C41 C42 H42 119.1 . . ? N1 C4 C3 109.3(3) . . ? C5 C4 N1 123.3(3) . . ? C5 C4 C3 127.4(3) . . ? C33 C34 H34 119.2 . . ? C35 C34 H34 119.2 . . ? C35 C34 C33 121.7(4) . . ? C32 C33 C51 121.9(3) . . ? C34 C33 C32 118.7(4) . . ? C34 C33 C51 119.4(4) . . ? C31 C30 H30 126.5 . . ? C31 C30 C29 107.1(3) . . ? C29 C30 H30 126.5 . . ? C34 C35 C52 120.2(4) . . ? C36 C35 C34 118.6(4) . . ? C36 C35 C52 121.2(4) . . ? C32 C37 C53 121.6(3) . . ? C36 C37 C32 118.6(4) . . ? C36 C37 C53 119.8(4) . . ? C49 C59 H59A 109.5 . . ? C49 C59 H59B 109.5 . . ? C49 C59 H59C 109.5 . . ? H59A C59 H59B 109.5 . . ? H59A C59 H59C 109.5 . . ? H59B C59 H59C 109.5 . . ? C28 C29 H29 126.2 . . ? C30 C29 C28 107.7(3) . . ? C30 C29 H29 126.2 . . ? C27 C26 H26 126.1 . . ? C25 C26 C27 107.7(3) . . ? C25 C26 H26 126.1 . . ? C35 C36 C37 121.9(4) . . ? C35 C36 H36 119.1 . . ? C37 C36 H36 119.1 . . ? C1 C2 H2A 127.2 . . ? C3 C2 C1 105.6(3) . . ? C3 C2 H2A 127.2 . . ? C41 C55 H55A 109.5 . . ? C41 C55 H55B 109.5 . . ? C41 C55 H55C 109.5 . . ? H55A C55 H55B 109.5 . . ? H55A C55 H55C 109.5 . . ? H55B C55 H55C 109.5 . . ? C45 C57 H57A 109.5 . . ? C45 C57 H57B 109.5 . . ? C45 C57 H57C 109.5 . . ? H57A C57 H57B 109.5 . . ? H57A C57 H57C 109.5 . . ? H57B C57 H57C 109.5 . . ? C33 C51 H51A 109.5 . . ? C33 C51 H51B 109.5 . . ? C33 C51 H51C 109.5 . . ? H51A C51 H51B 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C39 C54 H54A 109.5 . . ? C39 C54 H54B 109.5 . . ? C39 C54 H54C 109.5 . . ? H54A C54 H54B 109.5 . . ? H54A C54 H54C 109.5 . . ? H54B C54 H54C 109.5 . . ? C47 C58 H58A 109.5 . . ? C47 C58 H58B 109.5 . . ? C47 C58 H58C 109.5 . . ? H58A C58 H58B 109.5 . . ? H58A C58 H58C 109.5 . . ? H58B C58 H58C 109.5 . . ? C43 C56 H56A 109.5 . . ? C43 C56 H56B 109.5 . . ? C43 C56 H56C 109.5 . . ? H56A C56 H56B 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? N9 C64 C63 178.9(5) . . ? C37 C53 H53A 109.5 . . ? C37 C53 H53B 109.5 . . ? C37 C53 H53C 109.5 . . ? H53A C53 H53B 109.5 . . ? H53A C53 H53C 109.5 . . ? H53B C53 H53C 109.5 . . ? C35 C52 H52A 109.5 . . ? C35 C52 H52B 109.5 . . ? C35 C52 H52C 109.5 . . ? H52A C52 H52B 109.5 . . ? H52A C52 H52C 109.5 . . ? H52B C52 H52C 109.5 . . ? C61 C62 H62A 110(3) . . ? C61 C62 H62B 113(4) . . ? C61 C62 H62C 111(3) . . ? H62A C62 H62B 110(5) . . ? H62A C62 H62C 103(5) . . ? H62B C62 H62C 110(5) . . ? N8 C61 C62 179.7(6) . . ? C64 C63 H63A 109.5 . . ? C64 C63 H63B 109.5 . . ? C64 C63 H63C 109.5 . . ? H63A C63 H63B 109.5 . . ? H63A C63 H63C 109.5 . . ? H63B C63 H63C 109.5 . . ? Cl4 C60 Cl2 109.7(3) . . ? Cl4 C60 H60 109.2 . . ? Cl3 C60 Cl4 110.2(3) . . ? Cl3 C60 Cl2 109.4(3) . . ? Cl3 C60 H60 109.2 . . ? Cl2 C60 H60 109.2 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl4 C60 1.757(5) . ? Cl3 C60 1.755(6) . ? Cl2 C60 1.778(6) . ? N7 C31 1.366(5) . ? N7 C28 1.362(5) . ? N7 H7 0.78(4) . ? N6 C27 1.361(5) . ? N6 C24 1.396(5) . ? N6 H6 0.87(5) . ? N2 H2 0.8800 . ? N2 C6 1.385(5) . ? N2 C9 1.375(5) . ? N4 C15 1.370(5) . ? N4 C18 1.377(5) . ? N4 H4 0.82(4) . ? N5 C22 1.399(5) . ? N5 C19 1.358(5) . ? N5 H5 0.78(5) . ? N3 C11 1.414(5) . ? N3 C14 1.319(5) . ? N1 C1 1.319(5) . ? N1 C4 1.402(5) . ? C6 C5 1.439(5) . ? C6 C7 1.400(5) . ? C9 C10 1.443(5) . ? C9 C8 1.390(5) . ? C31 C1 1.441(5) . ? C31 C30 1.395(5) . ? C11 C10 1.369(5) . ? C11 C12 1.452(5) . ? C15 C14 1.434(5) . ? C15 C16 1.398(5) . ? C27 C28 1.434(5) . ? C27 C26 1.412(5) . ? C5 C32 1.501(5) . ? C5 C4 1.365(5) . ? C28 C29 1.401(5) . ? C1 C2 1.460(5) . ? C50 C23 1.515(5) . ? C50 C45 1.409(5) . ? C50 C49 1.399(5) . ? C38 C10 1.498(5) . ? C38 C43 1.403(5) . ? C38 C39 1.404(5) . ? C32 C33 1.398(5) . ? C32 C37 1.408(5) . ? C23 C22 1.403(5) . ? C23 C24 1.399(5) . ? C43 C42 1.405(5) . ? C43 C56 1.496(5) . ? C47 C48 1.385(6) . ? C47 C46 1.392(5) . ? C47 C58 1.515(5) . ? C22 C21 1.412(5) . ? C7 H7A 0.9500 . ? C7 C8 1.386(5) . ? C8 H8 0.9500 . ? C48 H48 0.9500 . ? C48 C49 1.403(5) . ? C19 C18 1.426(5) . ? C19 C20 1.410(5) . ? C24 C25 1.412(5) . ? C21 H21 0.9500 . ? C21 C20 1.375(5) . ? C13 H13 0.9500 . ? C13 C14 1.464(5) . ? C13 C12 1.345(6) . ? C17 H17 0.9500 . ? C17 C18 1.398(5) . ? C17 C16 1.397(5) . ? C45 C46 1.391(5) . ? C45 C57 1.501(5) . ? C3 H3 0.9500 . ? C3 C4 1.460(5) . ? C3 C2 1.341(6) . ? C25 H25 0.9500 . ? C25 C26 1.375(6) . ? C39 C40 1.392(6) . ? C39 C54 1.509(5) . ? C12 H12 0.9500 . ? C49 C59 1.506(5) . ? C20 H20 0.9500 . ? C46 H46 0.9500 . ? C40 H40 0.9500 . ? C40 C41 1.391(6) . ? C41 C42 1.379(6) . ? C41 C55 1.512(5) . ? C16 H16 0.9500 . ? C42 H42 0.9500 . ? N9 C64 1.142(7) . ? C34 H34 0.9500 . ? C34 C33 1.398(5) . ? C34 C35 1.392(6) . ? C33 C51 1.505(5) . ? C30 H30 0.9500 . ? C30 C29 1.399(6) . ? C35 C36 1.379(6) . ? C35 C52 1.510(5) . ? C37 C36 1.398(5) . ? C37 C53 1.505(6) . ? C59 H59A 0.9800 . ? C59 H59B 0.9800 . ? C59 H59C 0.9800 . ? C29 H29 0.9500 . ? C26 H26 0.9500 . ? C36 H36 0.9500 . ? C2 H2A 0.9500 . ? C55 H55A 0.9800 . ? C55 H55B 0.9800 . ? C55 H55C 0.9800 . ? C57 H57A 0.9800 . ? C57 H57B 0.9800 . ? C57 H57C 0.9800 . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C54 H54A 0.9800 . ? C54 H54B 0.9800 . ? C54 H54C 0.9800 . ? C58 H58A 0.9800 . ? C58 H58B 0.9800 . ? C58 H58C 0.9800 . ? C56 H56A 0.9800 . ? C56 H56B 0.9800 . ? C56 H56C 0.9800 . ? C64 C63 1.441(7) . ? C53 H53A 0.9800 . ? C53 H53B 0.9800 . ? C53 H53C 0.9800 . ? C52 H52A 0.9800 . ? C52 H52B 0.9800 . ? C52 H52C 0.9800 . ? C62 C61 1.445(7) . ? C62 H62A 1.16(7) . ? C62 H62B 0.95(6) . ? C62 H62C 1.02(6) . ? C61 N8 1.149(7) . ? C63 H63A 0.9800 . ? C63 H63B 0.9800 . ? C63 H63C 0.9800 . ? C60 H60 1.0000 . ?