#------------------------------------------------------------------------------ #$Date: 2024-08-05 20:56:12 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293737 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571799.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571799 loop_ _publ_author_name 'Liu, Yang' 'Xu, Ling' 'Jin, Xiaorong' 'Yin, Bangshao' 'Rao, Yutao' 'Zhou, Mingbo' 'Song, Jianxin' 'Osuka, Atsuhiro' _publ_section_title ; The unprecedented strong paratropic ring current of a bis-PdII complex of 5,10,23-trimesityl [28]heptaphyrin(1.1.0.0.1.0.0). ; _journal_issue 29 _journal_name_full 'Chemical science' _journal_page_first 11402 _journal_page_last 11407 _journal_paper_doi 10.1039/d4sc01909a _journal_volume 15 _journal_year 2024 _chemical_absolute_configuration ad _chemical_formula_moiety '2(C58 H50 B F2 N7)' _chemical_formula_sum 'C116 H100 B2 F4 N14' _chemical_formula_weight 1787.71 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2022-12-16 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-02-01 deposited with the CCDC. 2024-06-05 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 105.272(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 11.9268(3) _cell_length_b 27.7816(9) _cell_length_c 16.3663(5) _cell_measurement_reflns_used 3951 _cell_measurement_temperature 100.0(9) _cell_measurement_theta_max 70.8390 _cell_measurement_theta_min 2.7930 _cell_volume 5231.4(3) _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.0(9) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 8.0697 _diffrn_detector_type EosS2 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -37.00 32.00 1.00 5.00 -- -34.73 57.00 0.00 69 2 \w 63.00 102.00 1.00 5.00 -- 34.73 38.00 120.00 39 3 \w -31.00 39.00 1.00 5.00 -- 34.73 -57.00-150.00 70 4 \w 13.00 66.00 1.00 5.00 -- 34.73 -99.00 90.00 53 5 \w 36.00 63.00 1.00 5.00 -- 34.73-125.00 0.00 27 6 \w 24.00 57.00 1.00 5.00 -- 34.73-125.00-150.00 33 7 \w 76.00 104.00 1.00 5.00 -- 34.73 38.00 -90.00 28 8 \w 69.00 103.00 1.00 20.00 -- 105.25 -94.00-180.00 34 9 \w 36.00 88.00 1.00 20.00 -- 105.25 -94.00 150.00 52 10 \w 148.00 176.00 1.00 20.00 -- 105.25 15.00-150.00 28 11 \w 42.00 119.00 1.00 20.00 -- 105.25 -45.00 150.00 77 12 \w 88.00 174.00 1.00 20.00 -- 105.25 45.00 -90.00 86 13 \w 115.00 165.00 1.00 20.00 -- 105.25 61.00 0.00 50 14 \w 46.00 119.00 1.00 20.00 -- 105.25 -45.00 -90.00 73 15 \w 60.00 107.00 1.00 20.00 -- 105.25 -45.00 0.00 47 16 \w 74.00 124.00 1.00 20.00 -- 105.25 15.00-150.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, EosS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0560109000 _diffrn_orient_matrix_UB_12 -0.0421405000 _diffrn_orient_matrix_UB_13 0.0362441000 _diffrn_orient_matrix_UB_21 -0.0489451000 _diffrn_orient_matrix_UB_22 -0.0200988000 _diffrn_orient_matrix_UB_23 -0.0901023000 _diffrn_orient_matrix_UB_31 0.1113259000 _diffrn_orient_matrix_UB_32 -0.0298994000 _diffrn_orient_matrix_UB_33 0.0094220000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0479 _diffrn_reflns_av_unetI/netI 0.1002 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 32 _diffrn_reflns_limit_k_min -33 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 19567 _diffrn_reflns_point_group_measured_fraction_full 0.729 _diffrn_reflns_point_group_measured_fraction_max 0.729 _diffrn_reflns_theta_full 66.601 _diffrn_reflns_theta_max 66.601 _diffrn_reflns_theta_min 2.799 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.573 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.83273 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour violet _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.135 _exptl_crystal_description plate _exptl_crystal_F_000 1880 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.531 _refine_diff_density_min -0.275 _refine_diff_density_rms 0.057 _refine_ls_abs_structure_details ; Flack x determined using 2240 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.9(2) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.023 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1243 _refine_ls_number_reflns 13478 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.023 _refine_ls_R_factor_all 0.0894 _refine_ls_R_factor_gt 0.0656 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0770P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1563 _refine_ls_wR_factor_ref 0.1724 _reflns_Friedel_coverage 0.426 _reflns_Friedel_fraction_full 0.446 _reflns_Friedel_fraction_max 0.446 _reflns_number_gt 10045 _reflns_number_total 13478 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc01909a2.cif _cod_data_source_block exp_2740_sq _cod_depositor_comments 'Adding full bibliography for 1571798--1571800.cif.' _cod_database_code 1571799 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula 'C50 H100 N7 B1 F2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.972 _shelx_estimated_absorpt_t_min 0.945 _reflns_odcompleteness_completeness 99.93 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.49 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: N2(H2), N4(H4), N6(H6), C3(H3), C4(H4A), C7(H7), C8(H8), C11(H11), C12(H12), C16(H16), C17(H17), C21(H21), C22(H22), C25(H25), C26(H26), C29(H29), C30(H30), C34(H34), C36(H36), C42(H42), C44(H44), C51(H51), C53(H53), N1AA(H1AA), N3AA(H3AA), N5AA(H5AA), C61(H61), C62(H62), C65(H65), C66(H66), C69(H69), C70(H70), C74(H74), C75(H75), C79(H79), C80(H80), C83(H83), C84(H84), C87(H87), C88(H88), C92(H92), C94(H94), C101(H101), C103(H103), C109(H109), C112(H112) 2.b Idealised Me refined as rotating group: C37(H37A,H37B,H37C), C38(H38A,H38B,H38C), C39(H39A,H39B,H39C), C46(H46A,H46B, H46C), C47(H47A,H47B,H47C), C48(H48A,H48B,H48C), C55(H55A,H55B,H55C), C56(H56A, H56B,H56C), C57(H57A,H57B,H57C), C95(H95A,H95B,H95C), C96(H96A,H96B,H96C), C97(H97A,H97B,H97C), C104(H10A,H10B,H10C), C105(H10D,H10E,H10F), C106(H10G, H10H,H10I), C111(H11A,H11B,H11C), C114(H11D,H11E,H11F), C115(H11G,H11H,H11I) ; _shelx_res_file ; TITL exp_2740_a.res in P2(1) exp_2740_sq.res created by SHELXL-2016/6 at 11:52:14 on 16-Dec-2022 REM Old TITL exp_2740_a.res in P2(1) REM SHELXT solution in P2(1) REM R1 0.150, Rweak 0.033, Alpha 0.004, Orientation as input REM Flack x = 0.413 ( 0.022 ) from Parsons' quotients REM Formula found by SHELXT: C121 B4 N17 F6 Cl3 CELL 1.54184 11.9268 27.7816 16.3663 90 105.272 90 ZERR 2 0.0003 0.0009 0.0005 0 0.003 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H B F N UNIT 232 200 4 8 28 L.S. 5 0 164 PLAN 20 SIZE 0.1 0.1 0.05 TEMP-173 BOND $H ABIN fmap 2 53 acta SHEL 999 0.84 REM REM REM WGHT 0.077000 FVAR 0.32241 F1 4 0.256043 0.468935 0.448751 11.00000 0.01996 0.04473 = 0.02702 -0.00297 0.00354 0.00214 F2 4 0.383434 0.406854 0.474029 11.00000 0.03648 0.02698 = 0.03041 0.00152 0.01277 -0.00749 N1 5 0.443676 0.481201 0.548703 11.00000 0.02199 0.02424 = 0.02650 0.00674 0.00566 0.00033 N2 5 0.250533 0.421667 0.605328 11.00000 0.02830 0.03169 = 0.02503 -0.00094 0.00816 -0.00632 AFIX 43 H2 2 0.216182 0.428958 0.552315 11.00000 -1.20000 AFIX 0 N3 5 0.008509 0.371137 0.568422 11.00000 0.02021 0.03154 = 0.02764 -0.00428 0.00416 -0.00557 N4 5 -0.197263 0.362519 0.392357 11.00000 0.02110 0.03615 = 0.02135 0.00124 0.00663 0.00029 AFIX 43 H4 2 -0.122259 0.360480 0.396812 11.00000 -1.20000 AFIX 0 N5 5 -0.055967 0.378286 0.262035 11.00000 0.01926 0.03210 = 0.01875 0.00394 0.00689 -0.00382 N6 5 0.199319 0.415768 0.290331 11.00000 0.01270 0.02580 = 0.02778 -0.00054 0.00772 0.00486 AFIX 43 H6 2 0.177198 0.426533 0.334203 11.00000 -1.20000 AFIX 0 N7 5 0.423878 0.474349 0.394433 11.00000 0.02421 0.02826 = 0.02373 -0.00263 0.00754 0.00115 C1 1 0.577742 0.523515 0.483728 11.00000 0.01992 0.03074 = 0.03123 0.00399 0.00508 0.00466 C2 1 0.521380 0.504109 0.405147 11.00000 0.02329 0.02109 = 0.03707 -0.00563 0.00778 -0.00237 C3 1 0.548980 0.508450 0.328416 11.00000 0.01483 0.02570 = 0.03188 0.00388 0.00468 -0.00669 AFIX 43 H3 2 0.610776 0.527032 0.318205 11.00000 -1.20000 AFIX 0 C4 1 0.469954 0.480693 0.268598 11.00000 0.02129 0.03147 = 0.02201 0.00208 0.00321 -0.00070 AFIX 43 H4A 2 0.468005 0.476579 0.210616 11.00000 -1.20000 AFIX 0 C5 1 0.393783 0.460046 0.311586 11.00000 0.01221 0.02642 = 0.02360 0.00093 0.00092 0.00041 C6 1 0.302924 0.426429 0.271536 11.00000 0.01461 0.02946 = 0.02699 -0.00081 0.00513 0.00279 C7 1 0.307875 0.401061 0.199927 11.00000 0.01728 0.03551 = 0.02893 -0.00502 0.01120 0.00396 AFIX 43 H7 2 0.370214 0.401156 0.173831 11.00000 -1.20000 AFIX 0 C8 1 0.204034 0.375227 0.173038 11.00000 0.02551 0.03058 = 0.02702 -0.01161 0.00864 0.00022 AFIX 43 H8 2 0.183548 0.354461 0.125296 11.00000 -1.20000 AFIX 0 C9 1 0.136073 0.385078 0.227906 11.00000 0.02011 0.03472 = 0.02268 -0.00765 0.00748 -0.00059 C10 1 0.015833 0.372317 0.211829 11.00000 0.02259 0.02588 = 0.02721 0.00681 0.00670 0.00623 C11 1 -0.048667 0.356936 0.127521 11.00000 0.02193 0.02614 = 0.02242 0.00309 0.00478 0.00003 AFIX 43 H11 2 -0.016552 0.349066 0.081906 11.00000 -1.20000 AFIX 0 C12 1 -0.163796 0.355868 0.125889 11.00000 0.01348 0.03800 = 0.02638 -0.00087 0.00424 -0.00516 AFIX 43 H12 2 -0.227652 0.348063 0.079301 11.00000 -1.20000 AFIX 0 C13 1 -0.167113 0.369220 0.210597 11.00000 0.02490 0.02599 = 0.02822 0.00117 0.00732 0.00202 C14 1 -0.268933 0.370608 0.234442 11.00000 0.02070 0.02969 = 0.02507 0.00273 0.00734 -0.00305 C15 1 -0.283967 0.372042 0.317179 11.00000 0.03254 0.02430 = 0.02589 0.00627 0.00290 0.00693 C16 1 -0.389306 0.374779 0.339956 11.00000 0.01579 0.02722 = 0.02904 -0.00251 0.00256 -0.00079 AFIX 43 H16 2 -0.463071 0.381902 0.302690 11.00000 -1.20000 AFIX 0 C17 1 -0.367902 0.365401 0.425484 11.00000 0.02614 0.02582 = 0.02727 -0.00165 0.00838 -0.00558 AFIX 43 H17 2 -0.424464 0.364832 0.456903 11.00000 -1.20000 AFIX 0 C18 1 -0.249097 0.356888 0.458075 11.00000 0.02492 0.02387 = 0.02354 -0.00479 0.00698 -0.00741 C19 1 -0.192870 0.340280 0.542388 11.00000 0.03414 0.01429 = 0.02894 -0.00365 0.00857 -0.00525 C20 1 -0.081143 0.342581 0.586512 11.00000 0.03137 0.01603 = 0.02601 0.00969 0.00881 0.00403 C21 1 -0.035550 0.317829 0.666175 11.00000 0.04116 0.04086 = 0.02671 0.00501 0.01302 -0.00799 AFIX 43 H21 2 -0.077360 0.296701 0.693066 11.00000 -1.20000 AFIX 0 C22 1 0.076244 0.330188 0.694918 11.00000 0.02010 0.05441 = 0.03144 0.01155 0.00213 0.00314 AFIX 43 H22 2 0.129814 0.319051 0.745122 11.00000 -1.20000 AFIX 0 C23 1 0.098979 0.363921 0.634087 11.00000 0.02664 0.03166 = 0.03435 -0.00526 0.00643 0.00203 C24 1 0.209976 0.389224 0.654169 11.00000 0.03326 0.04095 = 0.02847 0.00291 0.00898 -0.00660 C25 1 0.289054 0.388294 0.733075 11.00000 0.04296 0.09326 = 0.03145 0.01021 0.00575 -0.03228 AFIX 43 H25 2 0.282817 0.369093 0.779710 11.00000 -1.20000 AFIX 0 C26 1 0.378443 0.419819 0.732925 11.00000 0.05211 0.09338 = 0.02483 -0.00299 0.00691 -0.02628 AFIX 43 H26 2 0.444465 0.425963 0.778860 11.00000 -1.20000 AFIX 0 C27 1 0.353964 0.440992 0.652894 11.00000 0.02459 0.04709 = 0.02113 -0.00184 -0.00062 -0.00554 C28 1 0.430167 0.474691 0.627783 11.00000 0.01961 0.04670 = 0.02103 -0.00584 -0.00115 -0.00203 C29 1 0.515035 0.503171 0.684810 11.00000 0.02911 0.05016 = 0.02873 -0.01129 0.00913 -0.00996 AFIX 43 H29 2 0.524055 0.505880 0.744057 11.00000 -1.20000 AFIX 0 C30 1 0.580666 0.525723 0.640652 11.00000 0.02631 0.03164 = 0.03284 -0.00263 0.00368 -0.00647 AFIX 43 H30 2 0.644732 0.546470 0.662980 11.00000 -1.20000 AFIX 0 C31 1 0.535406 0.512434 0.554345 11.00000 0.02604 0.02893 = 0.02660 -0.00114 0.00185 -0.00449 C32 1 0.682515 0.554630 0.492319 11.00000 0.02314 0.03443 = 0.02355 0.00395 0.00388 0.00212 C33 1 0.673611 0.604562 0.499212 11.00000 0.02246 0.03118 = 0.02566 -0.00083 0.00730 -0.00248 C34 1 0.771681 0.633067 0.502652 11.00000 0.02075 0.02565 = 0.02608 0.00314 0.00508 0.00255 AFIX 43 H34 2 0.766837 0.667002 0.507999 11.00000 -1.20000 AFIX 0 C35 1 0.877129 0.612036 0.498285 11.00000 0.03297 0.04177 = 0.02135 0.00073 0.00831 -0.01325 C36 1 0.882700 0.563418 0.490675 11.00000 0.02509 0.03429 = 0.02793 0.00460 0.00492 -0.00314 AFIX 43 H36 2 0.953718 0.549437 0.486601 11.00000 -1.20000 AFIX 0 C37 1 0.802353 0.480351 0.482350 11.00000 0.03157 0.02322 = 0.04318 0.00093 0.01124 -0.00231 AFIX 137 H37A 2 0.771302 0.470224 0.423347 11.00000 -1.50000 H37B 2 0.759321 0.464239 0.517934 11.00000 -1.50000 H37C 2 0.884744 0.471644 0.501650 11.00000 -1.50000 AFIX 0 C38 1 0.560159 0.628823 0.498926 11.00000 0.02549 0.01726 = 0.03269 0.00146 0.00713 0.00893 AFIX 137 H38A 2 0.572530 0.663607 0.506153 11.00000 -1.50000 H38B 2 0.531443 0.616129 0.545507 11.00000 -1.50000 H38C 2 0.502903 0.622473 0.444934 11.00000 -1.50000 AFIX 0 C39 1 0.977266 0.644373 0.495941 11.00000 0.02597 0.03356 = 0.03158 0.00164 0.00911 -0.00514 AFIX 137 H39A 2 1.050600 0.627627 0.520955 11.00000 -1.50000 H39B 2 0.973414 0.673742 0.528259 11.00000 -1.50000 H39C 2 0.973074 0.652834 0.437080 11.00000 -1.50000 AFIX 0 C40 1 -0.378695 0.370196 0.165673 11.00000 0.02545 0.04293 = 0.02985 0.00060 0.01636 0.00189 C41 1 -0.451412 0.329720 0.147439 11.00000 0.02004 0.04650 = 0.03684 -0.02133 0.01383 -0.01291 C42 1 -0.554379 0.331337 0.081163 11.00000 0.01840 0.08233 = 0.03228 -0.02077 0.01003 -0.01504 AFIX 43 H42 2 -0.603475 0.303861 0.070067 11.00000 -1.20000 AFIX 0 C43 1 -0.586124 0.373047 0.030810 11.00000 0.02479 0.09914 = 0.01587 0.00159 0.00316 -0.00754 C44 1 -0.514043 0.412589 0.049084 11.00000 0.02556 0.10480 = 0.02010 -0.00429 0.00702 0.01117 AFIX 43 H44 2 -0.534656 0.440915 0.016020 11.00000 -1.20000 AFIX 0 C45 1 -0.410988 0.412377 0.115069 11.00000 0.02209 0.05891 = 0.02719 -0.00086 0.00753 0.00540 C46 1 -0.336540 0.455890 0.129138 11.00000 0.03922 0.05255 = 0.03444 0.01622 0.00869 0.00308 AFIX 137 H46A 2 -0.311506 0.463053 0.189872 11.00000 -1.50000 H46B 2 -0.380686 0.483218 0.098975 11.00000 -1.50000 H46C 2 -0.268183 0.450181 0.107875 11.00000 -1.50000 AFIX 0 C47 1 -0.697220 0.374334 -0.037490 11.00000 0.02243 0.20571 = 0.02688 -0.00481 -0.00053 -0.01182 AFIX 137 H47A 2 -0.759498 0.386711 -0.014412 11.00000 -1.50000 H47B 2 -0.716937 0.341748 -0.059539 11.00000 -1.50000 H47C 2 -0.688196 0.395389 -0.083380 11.00000 -1.50000 AFIX 0 C48 1 -0.421921 0.284607 0.198037 11.00000 0.03856 0.04505 = 0.06701 -0.01778 0.02212 -0.01430 AFIX 137 H48A 2 -0.339371 0.277197 0.206171 11.00000 -1.50000 H48B 2 -0.469127 0.258012 0.167853 11.00000 -1.50000 H48C 2 -0.437897 0.288984 0.253315 11.00000 -1.50000 AFIX 0 C49 1 -0.278920 0.314937 0.581581 11.00000 0.02837 0.04011 = 0.02361 0.00451 -0.00007 -0.00397 C50 1 -0.334353 0.339566 0.632698 11.00000 0.03177 0.05178 = 0.02700 -0.00358 0.00582 -0.01962 C51 1 -0.416442 0.314436 0.663006 11.00000 0.05105 0.06221 = 0.02223 0.00193 0.01219 -0.02595 AFIX 43 H51 2 -0.457155 0.331353 0.696731 11.00000 -1.20000 AFIX 0 C52 1 -0.441625 0.266472 0.646690 11.00000 0.06250 0.06917 = 0.03200 -0.00169 0.01468 -0.03982 C53 1 -0.383314 0.242641 0.594192 11.00000 0.06459 0.05358 = 0.04942 -0.00568 0.01690 -0.02892 AFIX 43 H53 2 -0.400711 0.209748 0.580745 11.00000 -1.20000 AFIX 0 C54 1 -0.301415 0.265356 0.561345 11.00000 0.04520 0.03331 = 0.03575 0.00833 0.00276 -0.02214 C55 1 -0.244060 0.238505 0.505142 11.00000 0.05722 0.03009 = 0.05380 -0.00525 0.01472 0.00309 AFIX 137 H55A 2 -0.247850 0.257499 0.454027 11.00000 -1.50000 H55B 2 -0.283871 0.207702 0.489243 11.00000 -1.50000 H55C 2 -0.162579 0.232582 0.535039 11.00000 -1.50000 AFIX 0 C56 1 -0.312743 0.391781 0.653169 11.00000 0.04047 0.05173 = 0.04190 -0.00294 0.02008 -0.00483 AFIX 137 H56A 2 -0.271363 0.395328 0.713103 11.00000 -1.50000 H56B 2 -0.387140 0.408871 0.641805 11.00000 -1.50000 H56C 2 -0.265567 0.405354 0.618011 11.00000 -1.50000 AFIX 0 C57 1 -0.529983 0.239407 0.681681 11.00000 0.07731 0.10463 = 0.07805 -0.00366 0.03604 -0.05716 AFIX 137 H57A 2 -0.491410 0.226317 0.737629 11.00000 -1.50000 H57B 2 -0.563449 0.213005 0.643265 11.00000 -1.50000 H57C 2 -0.591918 0.261492 0.686655 11.00000 -1.50000 AFIX 0 C58 1 0.789706 0.533539 0.488617 11.00000 0.02134 0.02389 = 0.03362 0.00296 0.00509 -0.00352 B1 3 0.373804 0.455606 0.466183 11.00000 0.02445 0.02601 = 0.02445 -0.00672 0.00614 -0.00290 F3 4 0.189945 0.570513 0.925102 11.00000 0.03036 0.03666 = 0.02802 0.00140 0.00651 -0.00295 F4 4 0.313871 0.507858 0.944260 11.00000 0.02220 0.04764 = 0.02649 0.00169 0.00484 -0.00134 N0AA 5 0.127912 0.497045 0.845485 11.00000 0.01967 0.04805 = 0.02351 -0.00634 0.00436 -0.00956 N1AA 5 0.319881 0.559523 0.788797 11.00000 0.01745 0.04803 = 0.02411 0.00008 0.00561 -0.00372 AFIX 43 H1AA 2 0.356018 0.551225 0.840980 11.00000 -1.20000 AFIX 0 N2AA 5 0.561147 0.609341 0.825946 11.00000 0.01786 0.04110 = 0.02617 0.00382 0.00724 -0.00046 N3AA 5 0.767659 0.616079 1.002158 11.00000 0.01806 0.04752 = 0.02776 0.00817 0.00321 -0.00681 AFIX 43 H3AA 2 0.693570 0.620918 0.998462 11.00000 -1.20000 AFIX 0 N4AA 5 0.622026 0.598007 1.132585 11.00000 0.02534 0.03451 = 0.02528 0.00137 0.00587 0.00182 N5AA 5 0.371002 0.560595 1.107046 11.00000 0.02315 0.03093 = 0.01345 0.00039 -0.00102 -0.00370 AFIX 43 H5AA 2 0.393989 0.550670 1.063021 11.00000 -1.20000 AFIX 0 N6AA 5 0.146879 0.501800 1.000101 11.00000 0.01508 0.02601 = 0.02824 0.00317 0.00092 -0.00913 C59 1 -0.005430 0.452940 0.908207 11.00000 0.02905 0.03067 = 0.03119 0.00264 0.00180 -0.00718 C60 1 0.033551 0.466390 0.837581 11.00000 0.02056 0.03908 = 0.03406 0.00217 0.00362 -0.00890 C61 1 -0.010746 0.455160 0.750946 11.00000 0.03160 0.04949 = 0.03600 -0.01423 0.00925 -0.01568 AFIX 43 H61 2 -0.073862 0.434104 0.727740 11.00000 -1.20000 AFIX 0 C62 1 0.052787 0.479800 0.706029 11.00000 0.03045 0.04336 = 0.03443 -0.00766 0.00762 -0.00952 AFIX 43 H62 2 0.040987 0.479709 0.646314 11.00000 -1.20000 AFIX 0 C63 1 0.139992 0.505579 0.766354 11.00000 0.03193 0.03181 = 0.03146 -0.00843 0.00473 -0.00867 C64 1 0.214814 0.540332 0.741111 11.00000 0.01477 0.05666 = 0.02990 -0.00615 0.00692 -0.01406 C65 1 0.189297 0.563053 0.663452 11.00000 0.02081 0.06363 = 0.02432 0.00493 -0.00350 -0.01566 AFIX 43 H65 2 0.122781 0.557105 0.617809 11.00000 -1.20000 AFIX 0 C66 1 0.275915 0.595783 0.662779 11.00000 0.03288 0.05759 = 0.02656 0.00433 0.00652 -0.01064 AFIX 43 H66 2 0.279276 0.616300 0.617048 11.00000 -1.20000 AFIX 0 C67 1 0.357714 0.593397 0.741207 11.00000 0.02501 0.05166 = 0.02257 0.00596 0.00425 -0.01030 C68 1 0.467498 0.617688 0.759992 11.00000 0.02480 0.04792 = 0.02008 0.00170 0.01237 -0.00547 C69 1 0.494245 0.653680 0.701406 11.00000 0.03726 0.03695 = 0.02256 0.00848 0.00539 -0.00654 AFIX 43 H69 2 0.441485 0.666982 0.652758 11.00000 -1.20000 AFIX 0 C70 1 0.606047 0.663724 0.730024 11.00000 0.03453 0.03611 = 0.03174 0.00822 0.01310 0.00032 AFIX 43 H70 2 0.649596 0.684710 0.704282 11.00000 -1.20000 AFIX 0 C71 1 0.649967 0.637007 0.807510 11.00000 0.02601 0.04196 = 0.02744 -0.00055 0.00991 -0.01172 C72 1 0.765067 0.638867 0.852558 11.00000 0.02077 0.03239 = 0.02737 0.00254 0.00697 -0.00487 C73 1 0.817867 0.619144 0.936260 11.00000 0.02419 0.02917 = 0.02673 -0.00011 0.00880 -0.00250 C74 1 0.934737 0.606773 0.967294 11.00000 0.02379 0.03158 = 0.02575 -0.00214 0.00924 -0.00142 AFIX 43 H74 2 0.990415 0.605065 0.935217 11.00000 -1.20000 AFIX 0 C75 1 0.955154 0.597493 1.052431 11.00000 0.02649 0.02619 = 0.02956 0.00132 0.00439 0.00220 AFIX 43 H75 2 1.027418 0.588119 1.089441 11.00000 -1.20000 AFIX 0 C76 1 0.850843 0.604256 1.075216 11.00000 0.01331 0.03352 = 0.02766 -0.00325 0.00535 -0.00556 C77 1 0.836604 0.605212 1.158697 11.00000 0.02774 0.02990 = 0.02764 0.00174 0.00216 -0.00383 C78 1 0.734871 0.608104 1.182033 11.00000 0.02356 0.04115 = 0.01875 0.00119 0.00096 -0.00670 C79 1 0.727175 0.622086 1.267024 11.00000 0.04522 0.03920 = 0.01255 -0.00419 -0.00312 -0.01136 AFIX 43 H79 2 0.790704 0.630697 1.313293 11.00000 -1.20000 AFIX 0 C80 1 0.617029 0.620636 1.268082 11.00000 0.02901 0.03149 = 0.02612 -0.00046 0.00917 -0.00837 AFIX 43 H80 2 0.585959 0.628287 1.314306 11.00000 -1.20000 AFIX 0 C81 1 0.552825 0.604911 1.183917 11.00000 0.02569 0.02284 = 0.02602 0.00099 0.00582 0.00058 C82 1 0.433102 0.591116 1.169865 11.00000 0.02793 0.01571 = 0.02638 0.00475 0.00659 -0.00095 C83 1 0.364847 0.598616 1.224981 11.00000 0.02590 0.04045 = 0.02508 0.00288 0.00958 -0.00035 AFIX 43 H83 2 0.384716 0.618584 1.273799 11.00000 -1.20000 AFIX 0 C84 1 0.264327 0.572845 1.198351 11.00000 0.02208 0.04084 = 0.02476 0.00098 0.00873 0.00190 AFIX 43 H84 2 0.203033 0.571866 1.225441 11.00000 -1.20000 AFIX 0 C85 1 0.266931 0.548137 1.124423 11.00000 0.01978 0.02665 = 0.02215 0.00760 0.00550 -0.00414 C86 1 0.177823 0.515215 1.081636 11.00000 0.02334 0.02998 = 0.02216 0.00077 0.00370 0.00167 C87 1 0.101664 0.493595 1.124951 11.00000 0.02717 0.03524 = 0.02429 0.00491 0.00240 -0.00883 AFIX 43 H87 2 0.105104 0.497059 1.183308 11.00000 -1.20000 AFIX 0 C88 1 0.021895 0.466661 1.066284 11.00000 0.03220 0.03075 = 0.02599 0.01195 0.00416 -0.00392 AFIX 43 H88 2 -0.040209 0.448369 1.076703 11.00000 -1.20000 AFIX 0 C89 1 0.050157 0.471402 0.986449 11.00000 0.02488 0.04315 = 0.03014 0.01642 0.00645 -0.00305 C90 1 0.948277 0.602885 1.230474 11.00000 0.02037 0.04430 = 0.02757 -0.00259 0.00422 -0.00600 C91 1 1.017728 0.643932 1.250272 11.00000 0.02979 0.05110 = 0.02943 0.00778 0.00869 0.00571 C92 1 1.119920 0.640134 1.318178 11.00000 0.02258 0.04947 = 0.02993 -0.00900 0.01067 -0.01010 AFIX 43 H92 2 1.168783 0.667475 1.333500 11.00000 -1.20000 AFIX 0 C93 1 1.150017 0.597715 1.362465 11.00000 0.01940 0.05418 = 0.02304 -0.00946 0.01093 0.00218 C94 1 1.078153 0.558507 1.340776 11.00000 0.02246 0.04958 = 0.02289 0.01051 0.00718 0.00043 AFIX 43 H94 2 1.099014 0.529238 1.370969 11.00000 -1.20000 AFIX 0 C95 1 0.898919 0.516098 1.255018 11.00000 0.02503 0.04689 = 0.05147 0.01242 0.00873 -0.00260 AFIX 137 H95A 2 0.942834 0.488123 1.282876 11.00000 -1.50000 H95B 2 0.875522 0.510911 1.193628 11.00000 -1.50000 H95C 2 0.829555 0.520435 1.275666 11.00000 -1.50000 AFIX 0 C96 1 0.987987 0.691585 1.206521 11.00000 0.04773 0.03932 = 0.04680 -0.01107 -0.00701 -0.00658 AFIX 137 H96A 2 0.935575 0.709371 1.232742 11.00000 -1.50000 H96B 2 0.949699 0.686227 1.146462 11.00000 -1.50000 H96C 2 1.059289 0.710239 1.211822 11.00000 -1.50000 AFIX 0 C97 1 1.261413 0.593539 1.429985 11.00000 0.02976 0.05245 = 0.04016 -0.00873 0.00323 0.00242 AFIX 137 H97A 2 1.321679 0.580354 1.405643 11.00000 -1.50000 H97B 2 1.250469 0.572084 1.474788 11.00000 -1.50000 H97C 2 1.285254 0.625436 1.453872 11.00000 -1.50000 AFIX 0 C98 1 0.973891 0.560339 1.274792 11.00000 0.02253 0.04534 = 0.03413 0.00586 0.01057 -0.00864 C99 1 0.848615 0.663280 0.813711 11.00000 0.02227 0.03375 = 0.02188 0.00228 0.00563 -0.00456 C100 1 0.876821 0.711528 0.832394 11.00000 0.04776 0.03157 = 0.04017 0.00247 0.02177 0.00472 C101 1 0.951617 0.734814 0.793741 11.00000 0.04398 0.02646 = 0.05675 0.00293 0.02259 -0.00672 AFIX 43 H101 2 0.965162 0.768259 0.803789 11.00000 -1.20000 AFIX 0 C102 1 1.006747 0.711768 0.741801 11.00000 0.02668 0.03485 = 0.04046 0.00915 0.00340 -0.00423 C103 1 0.982479 0.663085 0.725881 11.00000 0.03082 0.04994 = 0.02924 -0.00008 0.01020 -0.00849 AFIX 43 H103 2 1.021397 0.646169 0.690969 11.00000 -1.20000 AFIX 0 C104 1 0.880555 0.586427 0.739837 11.00000 0.04666 0.03687 = 0.03355 -0.01152 0.01626 -0.01141 AFIX 137 H10A 2 0.941954 0.567127 0.777099 11.00000 -1.50000 H10B 2 0.879476 0.580315 0.680661 11.00000 -1.50000 H10C 2 0.805212 0.577611 0.748957 11.00000 -1.50000 AFIX 0 C105 1 0.820800 0.738295 0.892171 11.00000 0.11490 0.04547 = 0.08904 -0.01214 0.07564 -0.01615 AFIX 137 H10D 2 0.736239 0.738486 0.868765 11.00000 -1.50000 H10E 2 0.849621 0.771482 0.898953 11.00000 -1.50000 H10F 2 0.840348 0.722212 0.947413 11.00000 -1.50000 AFIX 0 C106 1 1.093589 0.736633 0.704290 11.00000 0.04673 0.05410 = 0.04030 -0.00298 0.01636 -0.01896 AFIX 137 H10G 2 1.060253 0.766793 0.677514 11.00000 -1.50000 H10H 2 1.112897 0.715698 0.661753 11.00000 -1.50000 H10I 2 1.164207 0.743611 0.749160 11.00000 -1.50000 AFIX 0 C107 1 -0.111928 0.423337 0.899725 11.00000 0.02419 0.03952 = 0.02189 -0.00681 0.00045 -0.01011 C108 1 -0.217543 0.445430 0.902170 11.00000 0.03167 0.03962 = 0.02413 -0.00695 0.00522 -0.01162 C109 1 -0.314421 0.415454 0.898485 11.00000 0.02130 0.04553 = 0.03217 0.00214 -0.00008 -0.00035 AFIX 43 H109 2 -0.386350 0.429864 0.899309 11.00000 -1.20000 AFIX 0 C110 1 -0.308234 0.365973 0.893729 11.00000 0.02822 0.03609 = 0.02252 0.00001 0.00798 0.00098 C111 1 -0.412487 0.334648 0.892392 11.00000 0.03472 0.04072 = 0.03788 -0.00415 0.01401 -0.00778 AFIX 137 H11A 2 -0.399236 0.302188 0.873422 11.00000 -1.50000 H11B 2 -0.481826 0.348474 0.853420 11.00000 -1.50000 H11C 2 -0.423921 0.332992 0.949468 11.00000 -1.50000 AFIX 0 C112 1 -0.202653 0.345211 0.889416 11.00000 0.02908 0.03413 = 0.02273 -0.00112 0.00785 -0.01277 AFIX 43 H112 2 -0.197623 0.311295 0.883870 11.00000 -1.20000 AFIX 0 C113 1 -0.106303 0.373246 0.893098 11.00000 0.03124 0.02996 = 0.02590 0.00057 -0.00008 0.00088 C114 1 0.007181 0.348989 0.896815 11.00000 0.03497 0.06085 = 0.03608 -0.00732 0.00890 -0.01064 AFIX 137 H11D 2 0.045872 0.365592 0.858949 11.00000 -1.50000 H11E 2 -0.006999 0.315365 0.878978 11.00000 -1.50000 H11F 2 0.056872 0.350150 0.954946 11.00000 -1.50000 AFIX 0 C115 1 -0.230537 0.498701 0.906792 11.00000 0.02681 0.04714 = 0.05306 0.00005 0.00720 -0.00018 AFIX 137 H11G 2 -0.181554 0.510533 0.960875 11.00000 -1.50000 H11H 2 -0.311959 0.506624 0.902484 11.00000 -1.50000 H11I 2 -0.206633 0.513935 0.860055 11.00000 -1.50000 AFIX 0 C116 1 0.903367 0.638401 0.759265 11.00000 0.02135 0.03579 = 0.02919 0.00034 -0.00097 -0.00740 B2 3 0.198681 0.520287 0.928808 11.00000 0.01916 0.03273 = 0.02742 0.00525 0.00348 -0.00642 HKLF 4 REM exp_2740_a.res in P2(1) REM R1 = 0.0656 for 10045 Fo > 4sig(Fo) and 0.0894 for all 13478 data REM 1243 parameters refined using 1 restraints END WGHT 0.0770 0.0000 REM Highest difference peak 0.531, deepest hole -0.275, 1-sigma level 0.057 Q1 1 0.6023 0.7643 0.5779 11.00000 0.05 0.53 Q2 1 -0.2412 0.2404 0.0601 11.00000 0.05 0.42 Q3 1 0.8398 0.7686 0.4967 11.00000 0.05 0.34 Q4 1 0.3024 0.2597 0.8212 11.00000 0.05 0.32 Q5 1 0.0464 0.4218 0.4242 11.00000 0.05 0.30 Q6 1 0.5182 0.6774 0.9592 11.00000 0.05 0.29 Q7 1 1.0332 0.7185 1.1852 11.00000 0.05 0.25 Q8 1 -0.7629 0.2587 -0.0912 11.00000 0.05 0.24 Q9 1 0.2822 0.2960 0.3826 11.00000 0.05 0.23 Q10 1 1.2917 0.5376 1.3584 11.00000 0.05 0.23 Q11 1 0.6153 0.5801 1.0821 11.00000 0.05 0.23 Q12 1 0.7626 0.4968 0.6332 11.00000 0.05 0.22 Q13 1 0.9688 0.5557 1.0795 11.00000 0.05 0.22 Q14 1 0.8268 0.4216 0.5178 11.00000 0.05 0.22 Q15 1 0.3140 0.2845 0.4383 11.00000 0.05 0.21 Q16 1 0.2593 0.6630 1.0380 11.00000 0.05 0.21 Q17 1 0.0857 0.5581 0.9740 11.00000 0.05 0.21 Q18 1 0.4147 0.5210 0.5376 11.00000 0.05 0.21 Q19 1 0.2588 0.6812 0.9988 11.00000 0.05 0.21 Q20 1 0.9755 0.5986 0.6764 11.00000 0.05 0.21 ; _shelx_res_checksum 96597 _shelx_hkl_file ; 0 0 1 56.07 3.22 0 0 1 56.52 3.18 0 0 2 47.51 5.02 0 0 2 46.81 4.42 0 0 3 1115.11 26.33 0 0 3 1151.34 29.43 0 0 -3 1154.72 29.09 0 0 4 263.59 16.11 0 0 4 290.70 14.98 0 0 -5 2457.51 57.57 0 0 5 2510.81 57.72 0 0 5 2476.32 52.46 0 0 -6 24.48 8.35 0 0 6 15.24 7.40 0 0 7 278.92 22.25 0 0 -7 275.06 22.55 0 0 8 116.26 15.78 0 0 9 27.93 9.59 0 0 10 -0.95 6.29 0 0 11 -2.98 8.67 0 0 12 237.71 29.38 0 0 -12 247.77 16.33 0 0 -13 429.14 22.01 0 0 -14 2.64 5.84 0 0 -15 -4.79 4.51 0 0 -16 2.34 4.99 0 0 -17 10.96 4.87 0 0 -18 53.77 7.48 0 0 -19 1.45 2.91 0 1 1 150.69 5.04 0 -1 1 162.74 6.19 0 1 2 122.58 6.43 0 -1 2 128.52 7.81 0 1 -2 124.43 7.49 0 -1 2 130.22 7.34 0 -1 3 632.29 21.33 0 1 -3 633.42 20.77 0 1 3 610.82 17.91 0 -1 3 622.90 19.45 0 1 -4 2349.77 49.69 0 -1 4 2378.45 47.10 0 -1 4 2393.33 50.98 0 1 4 2412.93 50.84 0 -1 -5 997.97 35.32 0 1 5 1049.93 35.77 0 -1 5 1023.08 32.41 0 -1 5 1051.96 35.78 0 1 -5 1059.86 35.75 0 -1 -6 647.96 31.32 0 -1 6 654.19 30.90 0 1 6 645.64 30.73 0 1 -6 647.46 30.85 0 -1 6 616.55 27.87 0 -1 7 249.41 21.32 0 1 7 232.78 20.48 0 -1 7 248.29 19.27 0 -1 -7 235.36 20.75 0 -1 8 290.82 24.64 0 1 8 250.53 22.51 0 1 9 7.39 7.28 0 -1 9 1.36 5.62 0 -1 10 30.81 11.86 0 1 10 34.04 10.97 0 -1 11 157.80 22.81 0 1 11 152.74 23.04 0 1 12 302.91 33.32 0 1 12 263.21 15.64 0 -1 -12 253.67 16.26 0 1 -12 283.75 17.20 0 -1 -13 26.77 6.70 0 1 -13 20.29 6.39 0 -1 -14 150.40 13.92 0 1 -14 166.68 14.49 0 1 -15 3.46 4.87 0 -1 -15 3.75 5.28 0 1 -16 25.45 7.25 0 -1 -16 17.61 5.79 0 -1 -17 19.28 5.46 0 1 -17 22.82 6.29 0 1 -18 3.69 4.03 0 -1 -18 7.40 3.83 0 -1 -19 55.74 6.02 0 1 -19 61.67 6.14 0 -2 0 2448.79 30.53 0 -2 1 1168.82 21.48 0 2 1 1095.16 18.41 0 -2 2 152.05 9.06 0 2 2 165.46 7.42 0 -2 2 144.99 8.53 0 -2 3 237.62 13.61 0 -2 -3 235.45 12.96 0 -2 3 244.50 12.95 0 2 3 236.98 10.84 0 -2 4 4825.30 75.35 0 2 4 4639.43 68.48 0 -2 4 4673.83 78.25 0 -2 5 375.30 19.77 0 -2 5 362.43 21.23 0 -2 -5 370.01 21.40 0 2 -6 845.46 21.20 0 -2 6 917.55 34.49 0 2 6 858.13 36.16 0 -2 6 886.10 36.39 0 -2 -6 878.14 37.11 0 -2 -7 321.57 24.76 0 -2 7 301.98 23.37 0 2 7 311.09 23.38 0 -2 7 303.35 21.64 0 -2 8 105.36 16.07 0 -2 -8 100.33 15.50 0 2 8 82.79 13.96 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7 25.29 5.09 6 -5 8 107.33 10.16 6 5 8 102.41 10.96 6 -5 9 138.06 11.39 6 5 9 109.48 11.24 -6 -5 -10 34.08 6.83 6 -5 10 29.33 5.66 6 5 10 14.28 5.88 -6 -5 -11 55.02 8.81 6 -5 11 57.23 7.72 6 5 11 33.36 6.55 -6 -5 -12 30.63 6.86 6 -5 12 37.61 6.69 6 5 12 28.26 6.40 -6 -5 -13 0.33 3.96 6 5 13 2.44 3.73 -6 -5 -14 -0.29 3.40 6 5 14 3.03 3.21 -6 -5 -15 10.84 3.06 6 -6 -19 6.15 3.62 6 6 -18 -0.37 4.58 6 -6 -18 10.09 4.78 6 6 -17 27.47 7.53 6 -6 -17 16.47 5.57 6 6 -16 85.71 10.82 6 -6 -16 76.15 9.45 6 -6 -16 88.57 9.61 6 6 -15 -4.79 6.04 6 -6 -15 -1.40 5.18 6 -6 -15 0.83 4.30 6 6 -14 23.93 8.10 6 -6 -14 11.47 5.87 6 -6 -14 16.22 5.50 6 -6 -13 39.93 7.51 6 6 -13 20.16 7.23 6 -6 -13 35.05 7.93 6 6 -12 49.28 9.92 6 -6 -12 51.30 8.54 6 -6 -12 43.02 7.71 6 6 -11 194.08 15.63 6 -6 -11 168.68 13.39 6 -6 -11 180.91 13.39 6 -6 -10 51.08 14.93 6 -6 -9 141.80 20.89 6 -6 -9 149.13 23.45 6 -6 -8 189.17 23.49 6 -6 -8 196.78 24.86 6 -6 -7 26.05 9.47 6 -6 -7 42.71 12.70 6 -6 -6 70.97 15.58 6 -6 -6 73.15 15.51 6 6 -5 344.94 29.48 6 -6 -5 328.31 28.91 6 -6 -5 347.84 30.64 6 6 -4 33.52 10.92 6 -6 -4 37.39 11.50 6 -6 -3 21.05 9.75 6 6 -3 20.07 8.29 6 6 -3 10.88 7.00 6 6 -2 115.68 16.61 6 6 -2 111.94 17.10 6 6 -1 365.09 30.03 6 6 -1 360.39 26.86 6 6 0 99.02 13.65 6 6 0 96.04 16.00 6 6 1 39.19 10.77 6 6 2 83.70 16.47 6 6 3 59.43 14.53 6 -6 3 49.52 15.68 6 6 4 80.40 16.41 6 -6 4 65.59 17.32 6 6 5 244.80 28.73 6 -6 5 243.10 30.09 6 6 6 19.07 5.10 6 -6 6 27.65 6.02 6 6 6 30.06 10.56 6 6 6 11.73 4.33 6 -6 6 32.25 15.00 6 6 7 27.15 6.68 6 6 7 47.96 7.88 6 -6 7 51.21 8.60 6 -6 7 37.92 5.96 6 6 8 84.22 10.05 6 -6 8 96.10 9.37 6 -6 9 78.59 8.77 6 6 9 58.85 8.49 -6 -6 -10 73.74 9.99 6 -6 10 76.71 8.73 6 6 10 47.02 7.71 -6 -6 -11 79.31 10.11 6 -6 11 74.45 8.53 6 6 11 59.61 8.58 -6 -6 -12 2.19 4.84 6 6 12 2.18 4.12 -6 -6 -13 0.83 3.94 6 6 13 3.81 3.82 -6 -6 -14 1.14 3.29 6 6 14 -2.33 3.20 -6 -6 -15 8.22 2.93 6 -7 -19 4.38 2.92 6 7 -18 -6.16 4.34 6 -7 -18 -4.17 3.75 6 7 -17 17.16 6.47 6 -7 -17 4.85 4.42 6 7 -16 53.40 9.37 6 -7 -16 48.20 8.29 6 -7 -16 42.65 7.46 6 7 -15 38.06 8.38 6 -7 -15 23.98 6.72 6 -7 -15 24.77 6.49 6 7 -14 42.42 8.41 6 -7 -14 45.77 7.83 6 -7 -14 58.88 8.65 6 7 -13 -5.98 6.51 6 -7 -13 8.06 5.44 6 -7 -13 -0.20 3.90 6 7 -12 62.34 10.76 6 -7 -12 63.99 8.79 6 -7 -12 62.45 8.55 6 7 -11 6.33 7.10 6 -7 -11 -1.41 4.55 6 -7 -11 10.07 4.70 6 -7 -10 -3.55 7.49 6 7 -10 6.66 5.26 6 -7 -9 248.90 26.95 6 -7 -9 230.70 29.02 6 -7 -8 44.24 14.71 6 -7 -8 33.23 11.80 6 -7 -7 52.25 13.38 6 -7 -7 15.22 8.36 6 -7 -6 121.07 18.52 6 -7 -6 100.93 18.13 6 7 -5 185.92 22.35 6 -7 -5 165.70 21.99 6 7 -4 82.00 15.72 6 -7 -4 96.86 17.45 6 7 -3 160.25 20.47 6 7 -3 167.95 20.85 6 -7 -3 175.02 21.89 6 7 -2 386.10 32.08 6 7 -2 439.02 31.69 6 7 -1 7.10 5.50 6 7 -1 3.18 6.23 6 7 0 661.70 42.45 6 7 1 115.34 18.73 6 7 2 78.96 16.31 6 7 3 4.24 6.19 6 -7 3 5.82 9.52 6 7 4 264.09 29.80 6 -7 4 297.76 32.46 6 7 5 -7.61 8.35 6 -7 5 15.68 11.42 6 7 6 24.04 5.22 6 7 6 34.73 13.51 6 7 6 25.95 6.88 6 -7 6 41.56 8.05 6 -7 6 21.40 13.02 6 7 7 84.37 9.35 6 7 7 123.09 11.87 6 -7 8 63.34 7.80 6 7 8 47.14 7.76 6 -7 9 72.29 7.87 6 7 9 61.61 9.07 -6 -7 -10 114.23 12.55 6 -7 10 101.23 9.38 -6 -7 -11 14.62 5.52 6 -7 11 12.76 4.67 6 7 11 18.58 5.72 -6 -7 -12 7.49 5.30 6 7 12 2.99 4.65 -6 -7 -13 -3.88 4.54 6 7 13 0.30 3.39 -6 -7 -14 -1.77 3.03 -6 -7 -15 22.75 3.82 -6 -8 19 3.49 2.80 6 -8 -18 3.98 3.44 6 8 -17 15.03 5.40 6 -8 -17 23.05 5.66 6 8 -16 22.27 6.28 6 -8 -16 23.45 6.21 6 -8 -16 34.93 6.62 6 8 -15 2.10 6.05 6 -8 -15 4.99 5.46 6 -8 -15 10.34 4.69 6 8 -14 9.47 7.44 6 -8 -14 7.67 4.92 6 -8 -14 8.99 4.53 6 8 -13 25.54 8.27 6 -8 -13 29.30 6.57 6 -8 -13 24.28 6.52 6 8 -12 4.60 6.02 6 -8 -12 4.27 5.21 6 -8 -12 16.25 5.81 6 8 -11 50.22 8.51 6 -8 -11 64.79 8.34 6 -8 -10 22.27 12.20 6 8 -10 16.82 6.51 6 -8 -10 13.13 4.43 6 -8 -9 13.52 11.51 6 -8 -8 52.84 14.82 6 -8 -7 13.77 9.23 6 -8 -6 206.03 26.12 6 8 -5 98.35 17.43 6 -8 -5 80.85 15.90 6 8 -4 34.07 10.67 6 -8 -4 38.93 13.21 6 8 -3 107.27 18.43 6 -8 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15.01 6 -9 -11 142.05 12.45 6 9 -10 187.83 14.99 6 -9 -10 214.24 14.48 6 -9 -10 223.43 29.14 6 -9 -9 20.13 10.71 6 -9 -8 25.87 12.77 -6 -9 7 37.37 10.40 6 -9 -7 47.90 14.37 6 -9 -6 105.72 19.75 6 -9 -5 55.44 14.02 6 9 -4 112.52 18.97 6 -9 -4 68.52 15.95 6 9 -3 60.08 15.04 6 -9 -3 62.75 14.85 6 -9 -2 81.12 16.13 6 9 -2 83.01 14.76 6 9 -2 89.04 17.26 6 9 -1 537.75 39.85 6 9 0 85.94 17.31 6 9 1 206.72 26.05 6 9 2 5.64 7.66 6 -9 3 12.45 12.45 6 9 3 11.35 10.16 6 9 4 38.19 13.27 6 -9 4 17.72 11.08 6 9 5 127.77 11.92 6 9 5 129.83 22.34 6 -9 5 125.35 11.12 6 9 5 117.76 10.83 6 -9 5 92.27 21.08 6 9 6 71.09 9.61 6 9 6 63.91 8.85 6 -9 6 84.44 10.40 6 9 7 48.78 7.80 6 9 7 70.42 9.63 6 9 8 210.26 14.97 6 9 9 7.50 5.32 -6 -9 -10 15.82 6.44 6 9 10 19.21 6.03 -6 -9 -11 64.59 9.58 6 9 11 47.90 7.87 -6 -9 -12 10.06 5.25 6 9 12 4.43 4.31 -6 -9 -13 19.15 5.05 6 9 13 15.88 4.11 -6 -9 -14 10.03 3.83 -6 -10 18 3.81 3.14 6 -10 -17 1.44 2.89 6 -10 -16 2.88 3.67 6 10 -16 -0.60 5.78 6 10 -15 10.50 6.47 6 -10 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42.88 6.50 -6 -10 -12 16.30 5.50 6 10 12 12.41 4.32 -6 -10 -13 5.51 3.52 6 10 13 11.39 4.04 -6 -10 -14 14.42 3.84 6 -11 -18 9.25 2.84 -6 -11 18 19.95 4.09 6 -11 -17 4.22 2.99 -6 -11 17 5.23 3.63 6 -11 -16 16.29 5.34 6 11 -15 7.66 5.36 6 -11 -15 7.77 4.48 6 11 -14 0.56 5.21 6 -11 -14 -1.65 4.03 6 11 -13 60.00 9.75 6 -11 -13 75.18 9.65 6 11 -12 46.14 8.95 6 -11 -12 50.19 7.91 6 11 -11 8.59 5.37 6 -11 -11 11.56 4.63 6 11 -10 22.48 7.06 6 -11 -10 31.17 7.11 6 -11 -9 5.53 9.51 6 11 -9 -3.91 5.58 6 -11 -9 -0.76 3.71 6 -11 -8 8.18 8.86 6 -11 -7 8.68 10.40 -6 -11 7 7.12 6.00 6 -11 -6 86.88 19.31 -6 -11 6 97.86 17.31 6 -11 -5 103.04 18.85 6 11 -4 24.97 11.80 6 -11 -4 33.11 10.82 6 11 -3 221.53 27.81 6 -11 -3 222.74 27.00 6 11 -2 86.50 17.55 6 -11 -2 103.93 17.97 6 11 -1 392.97 36.95 6 -11 -1 330.98 31.20 6 11 0 -5.36 9.01 6 11 1 98.94 20.26 6 11 2 179.75 26.02 6 11 3 6.24 8.17 6 11 4 10.23 4.44 6 -11 4 5.76 5.30 6 -11 4 18.28 9.90 6 11 5 7.99 4.73 6 11 5 -0.86 5.48 6 -11 5 8.32 5.76 6 11 6 5.90 4.65 6 11 6 5.11 4.82 -6 -11 -6 0.04 5.66 6 11 7 50.45 8.63 6 11 7 46.15 7.35 -6 -11 -7 34.90 9.07 6 11 8 -3.09 4.84 6 11 8 -3.78 4.80 -6 -11 -8 1.46 5.31 6 11 9 142.14 11.87 -6 -11 -9 120.29 13.49 -6 -11 -10 27.22 7.36 6 11 10 24.44 6.21 -6 -11 -11 29.86 6.54 6 11 11 27.41 5.63 -6 -11 -12 3.48 4.10 6 11 12 13.45 4.19 -6 -11 -13 3.45 3.82 6 11 13 5.49 2.72 6 -11 14 2.38 3.29 -6 -11 -14 7.56 3.38 -6 -12 18 36.21 4.83 6 -12 -17 15.19 3.78 -6 -12 17 19.89 4.97 6 -12 -17 20.99 4.65 -6 -12 16 3.46 3.92 6 -12 -16 10.32 4.53 6 -12 -15 16.25 4.92 6 -12 -14 38.29 7.33 6 12 -13 73.97 11.00 6 -12 -13 74.61 9.72 6 12 -12 10.75 5.29 6 -12 -12 19.75 6.30 6 12 -11 42.79 8.57 6 -12 -11 35.00 6.99 6 -12 -10 2.27 4.41 6 -12 -9 94.50 9.65 6 -12 -8 115.57 22.99 -6 -12 8 143.54 12.23 6 -12 -7 3.81 6.72 -6 -12 7 10.76 8.51 6 -12 -6 43.91 13.85 -6 -12 6 39.33 11.77 6 -12 -5 128.01 22.28 6 12 -4 42.84 14.80 6 -12 -4 24.52 9.61 6 12 -3 193.42 26.71 6 -12 -3 162.16 23.22 6 12 -2 68.02 16.58 6 -12 -2 83.24 16.00 6 -12 -1 80.11 16.50 6 12 -1 60.44 15.97 6 12 0 87.12 19.05 6 12 1 20.44 11.61 6 12 2 85.24 19.81 6 12 3 3.54 7.59 6 12 4 151.97 13.06 6 -12 4 176.42 12.97 6 12 4 160.73 12.48 6 12 4 125.07 22.96 6 -12 4 171.23 26.63 6 12 5 48.71 7.47 6 12 5 51.46 8.63 6 -12 5 48.32 8.02 6 12 6 170.05 14.04 6 12 6 156.74 12.38 -6 -12 -6 139.07 15.01 6 12 7 18.34 6.52 6 12 7 17.51 6.05 -6 -12 -7 5.22 6.23 6 12 8 0.45 3.91 6 12 8 8.21 5.46 -6 -12 -8 9.75 5.62 6 12 9 52.04 7.83 -6 -12 -9 31.55 8.15 -6 -12 -10 36.74 8.22 6 12 10 24.79 5.43 -6 -12 -11 14.06 5.03 6 12 11 17.45 4.92 -6 -12 -12 4.93 3.71 6 12 12 7.41 3.20 6 -12 13 1.82 3.88 -6 -12 -13 5.63 3.61 6 12 13 -1.49 2.67 -6 -12 -14 -1.03 2.74 -6 -13 18 16.86 3.46 -6 -13 17 19.96 4.52 6 -13 -17 9.63 3.27 6 -13 -16 0.53 3.36 -6 -13 16 7.64 4.42 -6 -13 15 11.46 5.54 6 -13 -15 8.66 4.58 -6 -13 14 4.12 5.17 6 -13 -14 7.69 5.05 6 -13 -13 42.01 7.64 6 -13 -12 21.04 5.75 6 -13 -11 1.85 3.73 -6 -13 10 4.59 5.14 6 -13 -10 -2.41 3.57 -6 -13 9 20.62 6.14 6 -13 -9 14.47 4.80 -6 -13 8 17.41 5.97 6 -13 -8 13.96 4.55 6 -13 -7 106.63 21.53 -6 -13 7 95.10 10.62 -6 -13 7 128.35 24.13 6 -13 -6 84.91 19.42 -6 -13 6 86.71 16.81 6 -13 -5 143.18 23.79 6 13 -4 23.01 13.39 6 -13 -4 24.45 10.56 6 13 -3 124.19 22.77 6 -13 -3 147.50 23.49 6 13 -2 91.23 19.69 6 -13 -2 87.71 17.47 6 -13 -1 36.36 11.43 6 13 -1 48.53 15.13 6 13 0 2.50 9.26 6 13 1 82.04 19.95 6 13 2 23.57 11.92 6 13 3 39.03 6.72 6 13 3 50.11 8.39 6 -13 3 44.64 7.19 6 13 3 36.04 13.12 6 13 4 9.79 4.73 6 13 4 12.31 4.69 6 13 5 64.15 9.66 6 13 5 64.53 8.33 6 13 6 124.13 12.39 6 13 6 161.91 12.66 -6 -13 -6 152.84 15.98 6 13 7 38.74 7.56 6 13 7 68.73 8.66 -6 -13 -7 51.68 11.32 6 13 8 57.38 8.72 -6 -13 -8 75.50 11.17 6 13 9 29.43 6.12 -6 -13 -9 18.44 6.99 -6 -13 -10 10.59 5.81 6 13 10 5.52 4.25 -6 -13 -11 8.08 4.56 6 13 11 15.51 3.86 -6 -13 -12 7.44 4.56 6 13 12 7.29 3.03 6 -13 13 5.58 4.07 -6 -13 -13 16.20 4.05 -6 -14 17 -1.17 2.96 6 -14 -17 0.98 2.30 6 -14 -16 20.31 4.96 -6 -14 16 19.70 5.22 -6 -14 15 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48.00 8.45 7 -11 -9 43.42 6.66 7 -11 -8 11.68 5.71 -7 -11 8 25.17 6.64 7 11 -7 23.51 13.39 7 -11 -7 11.88 8.12 -7 -11 7 11.87 5.72 7 11 -6 108.49 21.24 7 -11 -6 130.83 24.31 7 11 -5 5.83 9.97 7 -11 -5 26.43 11.73 7 11 -4 184.96 26.83 7 -11 -4 155.76 24.33 7 11 -4 199.57 26.18 7 11 -3 2.19 7.55 7 11 -2 25.11 13.48 7 11 -1 132.43 23.09 7 11 0 6.08 8.99 7 11 1 14.92 10.12 7 11 2 10.85 4.63 7 -11 2 16.92 5.77 7 11 2 15.93 5.55 7 11 2 13.65 12.37 7 11 3 145.31 13.59 7 -11 3 151.88 12.45 7 11 3 140.61 12.17 7 11 4 53.27 8.72 7 -11 4 45.95 8.29 7 11 4 49.62 8.14 7 11 5 90.34 11.11 7 -11 5 117.37 11.72 7 11 5 110.22 11.31 7 11 6 136.97 13.22 7 11 6 110.44 10.96 7 11 7 3.09 4.40 7 11 7 2.42 4.44 7 11 8 8.36 4.40 7 11 9 -3.13 4.51 -7 -11 -10 6.01 5.15 7 11 10 6.12 3.52 -7 -11 -11 4.36 4.77 7 11 11 -2.06 3.14 -7 -11 -12 18.56 4.75 7 11 12 17.31 3.82 -7 -11 -13 -3.34 2.38 -7 -12 18 5.37 2.90 7 -12 -17 10.34 3.43 -7 -12 17 4.74 3.74 7 -12 -16 19.36 4.54 7 -12 -16 12.17 4.19 -7 -12 16 12.27 5.22 7 -12 -15 8.79 4.46 -7 -12 15 0.35 4.40 7 -12 -15 11.18 4.54 -7 -12 14 67.44 9.64 7 -12 -14 66.58 8.65 7 -12 -14 72.89 8.79 -7 -12 13 20.86 7.07 7 -12 -13 18.57 5.41 -7 -12 12 64.32 9.80 7 -12 -12 82.07 9.54 7 -12 -11 182.07 13.68 -7 -12 11 207.13 15.66 7 -12 -11 197.80 14.03 7 -12 -10 1.93 4.68 -7 -12 10 3.32 5.35 7 -12 -10 -2.04 3.72 7 -12 -9 66.74 8.45 -7 -12 9 64.85 9.49 7 -12 -9 60.70 8.15 7 -12 -8 104.02 10.45 -7 -12 8 107.99 11.24 7 12 -7 14.87 12.55 7 -12 -7 8.37 4.06 -7 -12 7 10.08 5.49 7 12 -6 11.66 9.50 7 -12 -6 2.55 8.85 -7 -12 6 -0.72 7.68 -7 -12 6 6.89 4.95 7 12 -5 24.88 12.97 7 -12 -5 33.62 12.35 7 12 -4 17.76 8.21 7 -12 -4 9.96 8.80 7 -12 -3 7.69 9.07 7 12 -3 -4.92 8.36 7 12 -2 19.62 9.75 7 12 -1 124.58 23.65 7 12 0 60.06 15.72 7 12 1 19.91 6.14 7 -12 1 25.91 5.86 7 12 1 31.49 6.43 7 12 1 31.90 14.57 7 12 2 13.92 5.39 7 -12 2 10.23 5.06 7 12 2 10.69 5.22 7 12 3 35.93 8.14 7 -12 3 27.09 6.55 7 12 3 25.76 6.32 7 12 4 7.53 6.45 7 -12 4 16.73 6.13 7 12 4 14.73 5.24 7 12 5 45.13 8.52 7 -12 5 50.79 8.65 7 12 5 39.35 7.01 7 12 6 351.91 20.47 7 12 6 370.12 19.46 7 12 7 34.12 7.25 7 12 7 44.69 7.45 7 12 8 6.37 3.89 7 12 9 14.78 4.32 -7 -12 -10 40.37 7.58 7 12 10 25.23 5.30 -7 -12 -11 23.75 5.67 7 12 11 18.29 4.43 -7 -12 -12 30.63 5.17 7 12 12 26.68 4.34 -7 -12 -13 12.23 3.08 -7 -13 17 18.76 4.20 7 -13 -16 -1.52 3.10 -7 -13 16 4.30 3.64 7 -13 -16 2.76 2.65 7 -13 -15 5.45 4.00 -7 -13 15 -1.65 4.59 7 -13 -15 0.78 3.54 7 -13 -14 -3.83 4.75 -7 -13 14 -1.72 4.86 7 -13 -14 -1.55 3.71 7 -13 -13 0.84 4.37 -7 -13 13 6.66 5.99 7 -13 -13 6.59 4.74 7 -13 -12 19.24 6.08 -7 -13 12 1.60 5.56 7 -13 -12 19.72 5.74 7 -13 -11 5.12 4.84 -7 -13 11 7.11 5.46 7 -13 -11 4.72 4.19 7 -13 -10 3.03 4.71 -7 -13 10 0.50 5.03 7 -13 -10 0.60 3.38 7 -13 -9 5.82 4.81 -7 -13 9 -0.88 5.11 7 -13 -9 5.90 3.59 7 -13 -8 35.64 6.79 -7 -13 8 47.50 8.77 7 -13 -7 67.33 8.34 -7 -13 7 54.45 8.44 7 13 -6 -10.12 8.31 -7 -13 6 9.84 4.48 7 13 -5 120.52 23.84 7 -13 -5 128.98 24.08 -7 -13 5 128.78 11.31 7 13 -4 73.18 16.56 7 -13 -4 95.61 20.06 -7 -13 4 90.88 9.62 7 -13 -3 17.15 11.31 7 13 -3 31.69 13.68 7 13 -2 64.59 8.91 7 13 -2 62.78 18.11 7 13 -1 15.21 6.10 -7 -13 1 9.66 4.27 7 13 -1 -2.61 10.58 7 13 0 12.50 4.99 7 -13 0 17.36 5.17 -7 -13 0 22.31 6.20 7 13 0 13.03 11.10 7 13 1 48.83 8.13 7 -13 1 58.92 7.95 7 13 1 39.64 7.49 7 13 2 6.25 4.45 7 -13 2 7.95 4.65 7 13 2 10.36 4.47 7 13 3 6.01 5.52 7 -13 3 7.13 4.85 7 13 3 4.76 3.98 7 13 4 44.58 8.43 7 -13 4 32.23 7.17 7 13 4 41.27 7.54 7 13 5 48.57 8.51 7 13 5 56.23 8.44 7 13 6 40.83 8.50 7 13 6 50.37 7.55 -7 -13 -6 39.59 9.01 7 13 7 31.25 6.59 7 13 7 40.88 7.08 -7 -13 -7 38.29 8.60 7 13 8 0.72 4.00 7 13 9 2.29 3.99 -7 -13 -10 23.90 5.73 7 13 10 19.37 4.52 -7 -13 -11 13.53 4.78 7 13 11 5.19 3.33 -7 -13 -12 8.24 3.06 7 13 12 13.27 3.04 -7 -14 17 18.67 4.13 7 -14 -16 19.94 4.32 -7 -14 16 20.55 4.87 -7 -14 15 3.08 4.71 7 -14 -15 6.80 3.74 -7 -14 14 52.52 8.65 7 -14 -14 53.48 7.11 -7 -14 13 26.65 7.44 7 -14 -13 8.30 4.42 -7 -14 12 4.06 5.12 7 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5.13 7 15 7 3.95 3.59 -7 -15 -7 7.28 6.14 7 15 8 128.61 10.20 -7 -15 -8 104.32 11.87 7 15 9 61.88 7.07 -7 -15 -9 44.57 7.80 -7 -15 -10 30.96 5.64 7 15 10 20.65 4.13 -7 -15 -11 1.93 3.33 -7 -15 -12 16.90 3.63 -7 -16 16 1.95 3.04 7 -16 -16 1.61 2.15 -7 -16 15 1.62 3.85 7 -16 -15 10.79 3.95 -7 -16 14 66.35 8.50 7 -16 -14 71.00 7.64 -7 -16 13 10.24 5.53 7 -16 -13 12.96 4.75 -7 -16 12 57.55 9.12 7 -16 -12 48.24 7.35 -7 -16 11 164.04 14.46 7 -16 -11 142.93 12.03 -7 -16 10 6.96 6.15 7 -16 -10 1.07 3.56 -7 -16 9 98.58 11.79 7 -16 -9 81.36 8.94 -7 -16 8 46.54 8.91 -7 -16 7 143.97 13.45 -7 -16 6 10.15 5.51 -7 -16 5 6.01 5.38 -7 -16 4 177.75 13.89 7 16 -3 17.11 6.59 -7 -16 3 11.95 5.11 -7 -16 2 1.48 5.46 7 16 -2 0.15 4.33 7 16 -1 80.91 10.73 -7 -16 1 86.19 10.29 -7 -16 0 68.75 9.16 7 16 0 74.80 10.34 7 16 0 84.44 9.43 7 16 1 38.44 8.16 7 -16 1 34.22 6.55 7 16 1 38.90 6.98 7 16 2 10.09 5.46 7 -16 2 9.21 5.12 7 16 2 9.56 4.93 7 16 3 36.79 7.07 7 16 3 26.45 7.19 7 16 4 199.71 16.31 7 16 4 249.56 15.43 7 16 5 -5.46 5.14 7 16 5 3.40 3.58 7 16 6 6.16 4.77 7 16 6 5.30 4.01 -7 -16 -6 1.81 5.63 7 16 7 13.28 5.12 7 16 7 23.00 5.32 -7 -16 -7 16.98 6.72 7 16 8 88.10 8.26 -7 -16 -8 83.91 10.75 7 16 9 -3.11 2.98 -7 -16 -9 3.47 4.27 -7 -16 -10 20.94 4.97 -7 -16 -11 41.28 5.44 -7 -17 16 6.82 2.90 7 -17 -16 12.36 3.10 -7 -17 15 10.42 4.36 7 -17 -15 9.70 3.28 -7 -17 14 26.19 5.72 7 -17 -14 19.57 4.26 -7 -17 13 6.95 4.91 7 -17 -13 4.28 3.22 -7 -17 12 20.07 6.67 7 -17 -12 13.77 3.93 -7 -17 11 4.46 5.04 7 -17 -11 13.75 5.20 -7 -17 10 4.65 5.45 7 -17 -10 -2.21 3.68 -7 -17 9 15.67 6.79 7 -17 -9 13.59 5.40 -7 -17 8 145.86 13.26 -7 -17 7 221.52 16.19 -7 -17 6 13.76 5.98 -7 -17 5 14.93 6.38 -7 -17 4 48.91 8.39 7 17 -3 50.48 9.18 -7 -17 3 45.18 8.02 7 17 -2 48.87 9.05 -7 -17 2 47.71 8.01 7 17 -1 4.97 4.96 -7 -17 1 5.38 4.82 7 17 0 26.59 7.09 -7 -17 0 25.13 6.61 7 17 0 41.13 7.46 7 17 1 184.39 15.80 7 17 1 216.23 14.61 7 17 2 -3.38 5.41 7 17 2 2.05 3.95 7 17 3 27.09 7.26 7 17 3 38.43 6.63 7 17 4 76.73 10.08 7 17 4 70.56 8.72 7 17 5 -3.24 4.53 7 17 5 2.47 4.16 -7 -17 -5 -2.73 5.41 7 17 6 16.51 6.10 7 17 6 21.62 5.35 -7 -17 -6 22.66 7.98 7 17 7 13.94 4.76 7 17 7 11.78 3.97 -7 -17 -7 11.81 6.11 -7 -17 -8 5.07 4.41 -7 -17 -9 114.22 9.69 -7 -17 -9 88.98 10.24 -7 -17 -10 11.68 3.60 -7 -17 -11 28.69 4.19 -7 -18 16 26.70 3.99 7 -18 -16 30.92 3.82 -7 -18 15 6.22 3.56 7 -18 -15 1.51 2.28 -7 -18 14 41.73 6.24 7 -18 -14 33.14 4.87 -7 -18 13 8.41 4.86 7 -18 -13 11.37 3.84 -7 -18 12 9.72 5.69 7 -18 -12 4.05 3.64 -7 -18 11 10.27 5.83 7 -18 -11 10.85 4.27 -7 -18 10 8.06 6.10 7 -18 -10 4.78 3.41 -7 -18 9 53.91 8.91 7 -18 -9 52.95 7.67 -7 -18 8 52.46 8.51 -7 -18 7 71.86 10.13 -7 -18 6 11.71 6.57 -7 -18 5 43.05 7.81 -7 -18 4 11.81 5.27 7 18 -3 98.54 11.90 -7 -18 3 88.84 10.87 7 18 -2 40.02 8.40 -7 -18 2 45.72 8.45 7 18 -1 15.46 7.00 -7 -18 1 11.31 5.87 7 18 -1 10.50 4.56 7 18 0 99.01 12.24 7 18 0 99.09 10.18 7 18 1 14.26 6.16 7 18 1 26.61 6.19 7 18 2 68.96 10.37 7 18 2 76.99 9.02 7 18 3 50.06 8.79 7 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3.26 3.42 -7 -19 -8 7.72 4.43 -7 -19 -9 4.30 2.87 -7 -19 -10 17.10 3.37 7 -20 -15 2.14 1.80 -7 -20 15 0.25 2.25 -7 -20 14 38.46 5.40 7 -20 -14 34.99 4.49 -7 -20 13 8.80 3.76 7 -20 -13 10.30 3.58 -7 -20 12 88.32 9.44 7 -20 -12 70.67 7.28 -7 -20 11 20.01 5.75 7 -20 -11 26.00 4.69 -7 -20 10 -2.85 4.73 7 -20 -10 7.14 3.70 -7 -20 9 24.91 6.76 7 -20 -9 12.40 4.08 -7 -20 8 7.90 5.25 -7 -20 7 64.10 9.96 -7 -20 6 12.99 6.02 -7 -20 5 6.79 5.71 7 20 -4 6.82 6.14 -7 -20 4 7.52 5.40 7 20 -3 57.60 10.10 -7 -20 3 64.83 10.03 7 20 -2 13.63 6.24 -7 -20 2 23.59 6.41 7 20 -1 24.20 6.41 -7 -20 1 30.46 6.67 7 20 0 74.76 10.49 7 20 1 165.68 15.19 7 20 2 7.54 5.07 7 20 3 14.48 5.58 7 20 4 15.05 6.42 7 20 5 5.52 4.74 -7 -20 -5 10.44 6.47 7 20 6 21.81 5.38 -7 -20 -6 18.33 7.06 7 20 7 7.28 3.77 -7 -20 -7 -2.30 3.51 -7 -20 -7 3.75 4.27 -7 -20 -8 7.32 3.14 -7 -20 -8 2.35 4.00 -7 -20 -9 12.94 3.49 -7 -21 14 1.08 2.70 7 -21 -14 0.68 1.85 -7 -21 13 2.29 3.15 7 -21 -13 4.13 2.37 7 -21 -12 121.83 8.83 -7 -21 12 118.30 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12 1.74 2.66 8 -7 -18 1.16 3.13 -8 -7 18 1.13 2.90 8 -7 -17 22.64 5.38 -8 -7 17 26.00 5.49 8 -7 -16 14.83 4.96 8 7 -16 6.97 4.91 8 -7 -15 36.14 6.97 8 -7 -14 5.13 5.78 8 -7 -14 2.80 4.08 8 -7 -13 38.61 6.53 8 -7 -12 42.39 6.74 8 -7 -11 34.72 6.62 8 -7 -10 12.80 6.18 8 -7 -10 17.85 4.83 8 -7 -9 15.45 5.87 8 -7 -8 87.59 10.52 -8 -7 8 80.19 9.17 8 -7 -7 7.31 4.47 8 7 -7 2.47 7.92 8 7 -6 372.02 38.37 8 7 -5 15.77 11.73 8 7 -5 -1.24 7.37 8 7 -4 40.47 14.50 8 7 -4 18.19 10.25 8 7 -3 161.10 23.00 8 7 -3 162.93 24.32 8 7 -2 79.96 18.96 8 7 -1 22.54 11.01 8 7 0 12.40 10.38 8 -7 1 10.87 5.39 8 7 1 6.16 3.81 8 -7 1 7.84 4.89 8 7 1 1.63 7.34 8 7 1 0.45 3.45 8 7 2 111.02 11.40 8 -7 2 117.67 11.17 8 7 3 17.14 5.53 8 -7 3 9.61 5.02 8 7 3 2.24 4.49 8 7 4 74.19 10.02 8 -7 4 70.31 10.03 8 7 4 40.57 7.42 8 7 5 229.08 16.79 8 -7 5 229.62 16.32 8 -7 6 -1.70 5.50 8 7 6 -1.08 4.37 8 7 7 6.97 4.78 8 7 8 11.90 4.92 8 7 9 10.30 5.01 -8 -7 -10 -1.77 4.21 8 7 10 2.79 4.11 -8 -7 -11 71.64 7.84 8 7 11 49.80 6.56 -8 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49.58 7.75 -8 -8 -10 25.67 5.54 8 8 10 22.03 5.45 -8 -8 -11 12.68 4.15 8 8 11 16.36 4.48 -8 -8 -12 44.47 5.70 8 8 12 47.97 5.33 8 -9 -18 7.51 2.66 -8 -9 18 6.22 3.17 8 -9 -17 4.61 3.79 -8 -9 17 -2.40 3.48 8 -9 -16 12.97 4.51 -8 -9 16 16.70 5.15 8 -9 -15 54.22 7.93 -8 -9 15 62.29 8.34 8 -9 -15 64.69 7.70 8 -9 -14 23.09 6.74 8 -9 -14 30.73 6.18 8 -9 -13 0.67 5.47 8 -9 -13 9.46 3.70 8 -9 -12 21.99 7.14 8 -9 -12 29.34 5.83 8 -9 -11 52.96 9.20 8 -9 -11 40.17 6.60 -8 -9 11 47.80 7.92 8 -9 -10 35.51 7.56 -8 -9 10 40.32 7.41 8 -9 -10 37.50 6.41 8 -9 -9 21.43 6.50 -8 -9 9 18.53 6.06 8 -9 -8 33.78 7.69 -8 -9 8 26.02 6.49 8 -9 -7 40.33 7.44 -8 -9 7 43.75 7.46 8 -9 -6 64.52 8.85 -8 -9 6 46.26 7.30 8 9 -6 62.06 18.31 8 9 -6 68.18 18.68 8 -9 -5 12.73 4.68 8 9 -5 16.70 11.03 8 9 -5 20.02 11.33 8 9 -4 7.94 9.37 8 9 -4 0.19 8.13 8 9 -3 2.19 7.31 8 9 -2 123.71 21.80 8 -9 -1 215.13 14.02 8 9 -1 189.33 27.35 8 -9 -1 215.55 14.07 8 9 0 137.74 12.24 8 -9 0 148.17 12.03 8 9 0 133.18 23.91 8 -9 0 148.03 11.81 8 -9 1 43.61 7.34 8 9 1 45.85 7.69 8 -9 1 40.47 7.61 8 9 1 39.51 7.45 8 9 2 29.26 7.44 8 -9 2 24.66 6.99 8 9 2 23.20 6.65 8 9 3 106.38 11.63 8 -9 3 92.45 10.69 8 9 3 83.66 10.10 8 9 4 128.81 13.20 8 -9 4 142.10 13.27 8 9 4 106.20 11.30 8 9 5 6.92 4.63 8 -9 5 10.62 5.72 8 9 5 12.22 5.54 8 9 6 12.99 5.91 8 9 6 9.93 5.13 8 9 7 18.12 5.57 8 9 8 47.77 7.92 8 9 9 62.32 7.90 -8 -9 -10 26.06 5.81 8 9 10 14.88 4.87 -8 -9 -11 0.16 3.41 8 9 11 3.75 3.47 -8 -9 -12 14.82 3.90 8 9 12 18.07 3.24 -8 -10 18 6.73 3.06 8 -10 -17 7.12 3.10 -8 -10 17 1.58 3.43 8 -10 -16 -0.75 3.58 -8 -10 16 -0.80 3.86 8 -10 -15 75.07 8.62 -8 -10 15 71.46 8.91 8 -10 -15 69.62 7.61 8 -10 -14 29.75 6.88 -8 -10 14 38.19 7.68 8 -10 -14 32.02 6.14 8 -10 -13 33.23 6.69 -8 -10 13 42.96 8.08 8 -10 -13 47.17 6.73 8 -10 -12 2.38 4.96 -8 -10 12 8.55 5.74 8 -10 -12 -0.76 3.53 8 -10 -11 20.89 6.67 -8 -10 11 22.00 6.82 8 -10 -11 15.95 4.48 8 -10 -10 32.57 6.78 -8 -10 10 37.22 8.28 8 -10 -10 30.29 6.22 8 -10 -9 40.31 7.66 -8 -10 9 41.43 8.37 8 -10 -8 200.12 14.43 -8 -10 8 182.70 13.95 8 -10 -7 7.38 4.63 -8 -10 7 1.33 4.45 8 -10 -6 52.17 7.97 -8 -10 6 58.49 8.09 8 10 -6 48.66 15.52 8 10 -6 31.35 12.83 8 -10 -5 9.45 5.34 -8 -10 5 5.02 4.83 8 10 -5 0.87 9.57 8 10 -5 10.58 6.74 8 -10 -4 83.43 8.88 8 10 -4 78.12 17.74 8 -10 -3 0.86 4.09 8 10 -3 2.04 8.38 8 -10 -2 32.58 6.48 8 10 -2 44.72 7.31 8 10 -2 39.64 14.89 8 -10 -1 82.08 9.36 8 10 -1 82.76 9.84 8 -10 -1 82.79 9.39 8 10 -1 76.73 19.29 8 -10 0 17.73 5.06 8 10 0 11.99 4.35 8 -10 0 9.54 4.09 8 -10 1 49.18 7.85 8 10 1 54.97 8.92 8 -10 1 43.38 7.43 8 10 1 59.91 8.94 8 10 2 22.23 7.04 8 -10 2 26.20 5.89 8 10 2 25.71 6.86 8 10 3 61.97 9.59 8 -10 3 59.37 8.59 8 10 3 80.13 10.26 8 10 4 30.05 6.92 8 10 4 37.79 7.14 8 -10 4 44.54 8.24 8 10 5 116.57 12.22 8 -10 5 108.65 12.16 8 10 5 98.32 10.63 8 10 6 32.18 7.52 8 10 6 26.39 6.72 8 10 7 9.60 4.90 8 10 8 104.94 10.28 8 10 9 43.31 6.55 -8 -10 -10 -3.41 4.26 8 10 10 4.86 3.58 -8 -10 -11 17.39 4.58 8 10 11 20.13 4.43 -8 -10 -12 12.80 3.58 8 10 12 3.55 2.30 8 -11 -17 19.05 3.63 -8 -11 17 28.09 4.94 8 -11 -16 -2.66 3.14 -8 -11 16 2.72 3.85 8 -11 -15 14.38 5.07 -8 -11 15 20.01 6.07 8 -11 -15 13.64 4.13 8 -11 -14 29.41 6.56 -8 -11 14 33.19 7.09 8 -11 -14 25.98 5.48 8 -11 -13 47.65 7.78 -8 -11 13 46.03 8.40 8 -11 -13 55.41 7.21 8 -11 -12 20.00 6.67 8 -11 -12 5.37 4.12 -8 -11 12 11.63 5.65 8 -11 -11 10.78 5.74 -8 -11 11 15.56 6.27 8 -11 -11 19.82 5.21 8 -11 -10 19.64 6.59 -8 -11 10 10.72 5.32 8 -11 -10 12.69 4.26 8 -11 -9 5.32 5.38 -8 -11 9 0.57 4.79 -8 -11 8 141.70 12.62 8 -11 -8 137.74 12.30 8 -11 -7 3.53 4.24 -8 -11 7 3.10 4.63 -8 -11 6 9.87 5.38 8 -11 -6 5.11 5.05 8 -11 -5 28.12 6.49 8 11 -5 43.89 7.43 -8 -11 5 28.07 6.62 8 -11 -4 -2.39 4.88 8 11 -4 -3.13 3.95 -8 -11 4 0.96 4.03 8 11 -4 10.86 10.54 8 -11 -3 19.34 5.54 8 11 -3 19.40 6.41 -8 -11 3 40.15 9.68 8 11 -3 18.23 11.24 8 -11 -2 94.44 9.44 8 11 -2 93.38 10.54 8 -11 -2 93.89 9.87 -8 -11 2 91.44 9.39 8 -11 -1 27.38 6.12 8 11 -1 30.99 8.17 8 -11 -1 28.97 6.18 -8 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8 -12 -10 6.75 3.73 -8 -12 9 326.79 19.48 8 -12 -9 330.99 18.09 -8 -12 8 182.62 14.25 8 -12 -8 161.91 12.90 8 -12 -7 35.87 6.37 -8 -12 7 34.18 7.28 8 -12 -6 14.13 4.82 -8 -12 6 6.68 4.77 8 -12 -5 64.02 7.84 8 12 -5 71.35 9.50 -8 -12 5 72.55 9.36 8 -12 -4 2.94 4.00 8 12 -4 3.93 3.87 -8 -12 4 -0.02 4.69 8 -12 -3 12.55 4.96 8 12 -3 7.70 5.15 8 -12 -3 18.66 4.87 -8 -12 3 13.41 5.00 8 12 -2 121.37 11.97 8 -12 -2 130.09 11.07 -8 -12 2 107.25 10.19 8 -12 -2 123.74 10.74 8 -12 -1 73.63 8.24 8 12 -1 79.13 9.80 8 -12 -1 92.09 9.69 -8 -12 1 81.12 9.20 8 -12 0 40.41 6.66 8 12 0 35.44 7.34 8 -12 0 31.40 6.68 -8 -12 0 34.14 6.91 8 12 0 36.13 7.77 8 12 1 1.07 4.77 8 -12 1 12.10 6.01 8 12 1 4.91 4.84 8 12 2 18.66 6.31 8 -12 2 14.56 5.44 8 12 2 21.82 5.95 8 12 3 126.53 12.79 8 -12 3 124.54 12.11 8 12 3 114.73 11.66 8 12 4 49.81 8.91 8 -12 4 51.12 8.78 8 12 4 55.91 8.48 8 12 5 23.99 7.76 8 12 5 16.64 5.58 8 12 6 11.28 5.02 8 12 6 -2.42 5.17 8 12 7 36.16 6.55 8 12 8 11.53 4.31 -8 -12 -9 21.33 5.99 8 12 9 20.69 4.85 -8 -12 -10 47.77 6.77 8 12 10 34.11 5.22 -8 -12 -11 22.35 4.43 8 12 11 30.04 4.24 -8 -13 17 13.17 3.24 8 -13 -16 6.87 3.03 -8 -13 16 9.06 4.60 8 -13 -15 25.99 4.84 -8 -13 15 25.23 6.28 8 -13 -15 26.61 4.66 8 -13 -14 14.28 4.41 -8 -13 14 26.61 6.82 8 -13 -14 12.97 4.20 8 -13 -13 20.58 5.50 -8 -13 13 6.21 5.16 8 -13 -13 20.80 5.17 8 -13 -12 202.49 13.53 -8 -13 12 211.97 15.53 8 -13 -12 186.88 12.87 8 -13 -11 8.72 4.57 -8 -13 11 5.53 5.10 8 -13 -11 4.13 3.73 8 -13 -10 12.99 5.24 -8 -13 10 12.22 5.85 -8 -13 9 118.17 12.43 8 -13 -9 111.46 10.99 8 -13 -8 49.02 7.64 -8 -13 8 57.03 9.06 8 -13 -7 23.63 5.82 -8 -13 7 14.89 5.71 -8 -13 6 70.39 9.43 8 -13 -6 91.03 9.70 8 13 -6 87.82 10.36 8 -13 -5 8.56 4.81 8 13 -5 7.12 4.20 -8 -13 5 12.56 5.99 8 -13 -4 50.38 7.79 8 13 -4 64.81 9.16 -8 -13 4 53.60 8.22 8 13 -3 123.62 12.27 -8 -13 3 134.74 11.92 8 -13 -3 128.48 10.65 8 -13 -2 20.66 5.38 8 13 -2 17.97 6.89 8 -13 -2 2.71 4.27 -8 -13 2 19.46 5.90 8 -13 -1 14.21 4.98 8 13 -1 17.12 6.39 8 -13 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9.71 -8 -14 8 80.67 10.38 8 -14 -7 34.87 6.72 8 14 -7 32.83 6.47 -8 -14 7 35.73 8.11 8 14 -6 284.38 18.06 -8 -14 6 292.27 18.33 8 -14 -6 264.48 15.53 8 14 -5 22.73 6.26 -8 -14 5 30.07 6.68 8 14 -4 115.90 12.13 -8 -14 4 122.10 11.63 -8 -14 3 11.73 5.60 8 14 -3 10.56 5.38 8 -14 -2 28.95 6.20 8 14 -2 25.68 7.03 -8 -14 2 24.97 6.79 8 -14 -1 62.74 8.04 8 14 -1 59.00 9.46 8 -14 -1 68.31 8.52 -8 -14 1 55.81 8.61 8 14 0 172.01 14.55 8 -14 0 181.78 13.50 8 14 0 171.18 13.66 8 14 1 294.95 19.30 8 -14 1 274.84 16.48 8 14 1 298.76 17.71 8 14 2 37.15 7.99 8 -14 2 33.20 7.04 8 14 2 35.40 6.75 8 14 3 28.10 7.82 8 -14 3 33.64 7.39 8 14 3 15.97 5.55 8 14 4 19.04 6.35 8 14 4 18.20 5.85 8 14 5 16.33 6.41 8 14 5 12.72 5.61 8 14 6 15.57 5.65 8 14 6 26.35 6.05 8 14 7 7.27 4.47 8 14 8 24.46 4.78 -8 -14 -9 14.96 4.55 8 14 9 15.07 4.11 -8 -14 -10 23.32 4.73 8 14 10 28.56 4.18 -8 -14 -11 13.87 3.35 -8 -15 16 13.78 3.81 -8 -15 15 2.67 3.67 8 -15 -15 2.23 2.55 -8 -15 14 5.73 4.33 8 -15 -14 2.03 2.98 -8 -15 13 24.52 6.55 8 -15 -13 14.95 4.45 -8 -15 12 10.15 5.56 8 -15 -12 8.43 3.61 -8 -15 11 16.70 6.55 8 -15 -11 16.42 4.97 -8 -15 10 46.83 8.44 -8 -15 9 18.24 6.74 -8 -15 8 0.17 5.21 8 15 -7 19.09 5.82 -8 -15 7 16.18 5.97 8 15 -6 298.96 18.68 -8 -15 6 311.37 18.81 8 15 -5 44.81 8.36 -8 -15 5 29.46 7.07 -8 -15 4 1.91 4.58 8 15 -4 3.35 4.47 8 15 -3 88.52 10.75 -8 -15 3 94.37 10.74 8 15 -2 211.01 16.32 -8 -15 2 186.24 14.21 8 15 -1 250.53 17.85 8 -15 -1 243.55 14.63 -8 -15 1 221.54 15.18 8 15 0 2.81 5.23 8 -15 0 10.58 4.70 8 15 0 3.71 4.09 8 15 1 58.05 8.99 8 -15 1 57.27 8.16 8 15 1 55.16 8.71 8 15 2 209.32 16.37 8 -15 2 217.13 14.90 8 15 2 213.22 14.98 8 15 3 23.54 7.02 8 -15 3 10.97 6.38 8 15 3 24.66 6.26 8 15 4 55.99 8.97 8 15 4 77.23 8.81 8 15 5 19.72 6.37 8 15 5 30.17 6.31 -8 -15 -5 29.16 7.90 8 15 6 5.78 5.06 8 15 6 3.50 3.78 8 15 7 23.95 5.20 8 15 8 -3.43 3.12 -8 -15 -9 16.17 4.60 8 15 9 10.86 3.13 -8 -15 -10 -1.51 2.94 8 15 10 -1.55 2.13 -8 -16 16 9.33 3.34 -8 -16 15 5.33 3.83 8 -16 -15 7.42 2.68 -8 -16 14 25.89 5.53 8 -16 -14 28.98 4.74 -8 -16 13 -1.07 4.62 8 -16 -13 -5.59 3.27 -8 -16 12 4.38 5.05 8 -16 -12 18.08 4.31 -8 -16 11 9.90 5.80 8 -16 -11 6.32 3.85 -8 -16 10 208.46 15.64 -8 -16 9 5.76 5.20 8 16 -8 20.28 6.23 -8 -16 8 16.46 6.73 8 16 -7 11.34 5.08 -8 -16 7 18.03 6.35 8 16 -6 31.72 7.80 -8 -16 6 36.50 8.29 8 16 -5 5.00 5.23 -8 -16 5 12.97 6.36 8 16 -4 69.34 10.21 -8 -16 4 73.54 9.85 8 16 -3 3.30 4.62 -8 -16 3 12.02 5.40 8 16 -2 7.39 5.51 -8 -16 2 14.52 6.32 8 16 -1 25.48 6.70 -8 -16 1 23.21 6.07 8 16 -1 31.33 6.44 8 16 0 12.56 6.30 8 -16 0 19.60 5.58 8 16 0 14.80 5.40 8 16 1 35.01 7.58 8 -16 1 48.11 7.66 8 16 1 39.93 7.08 8 16 2 92.72 11.28 8 -16 2 113.69 10.93 8 16 2 123.39 11.46 8 16 3 57.32 9.41 8 16 3 99.10 10.46 8 16 4 4.40 4.87 8 16 4 5.79 3.64 8 16 5 52.16 8.60 8 16 5 59.61 7.44 -8 -16 -5 65.01 9.65 8 16 6 23.63 6.44 8 16 6 19.11 5.50 -8 -16 -6 19.71 6.69 8 16 7 10.43 4.65 -8 -16 -8 14.17 4.64 8 16 8 5.05 3.08 -8 -16 -9 15.94 4.52 8 16 9 9.45 2.98 -8 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26.20 4.06 9 -6 -18 11.95 3.33 9 -6 -17 6.29 3.51 -9 -6 17 7.55 3.61 9 6 -16 12.49 4.27 9 -6 -16 10.96 4.72 -9 -6 16 11.29 3.88 9 6 -15 1.93 3.96 9 -6 -15 6.98 5.00 -9 -6 15 -6.91 4.86 9 6 -14 6.14 4.44 9 -6 -14 5.37 5.06 -9 -6 14 11.06 5.04 9 6 -13 4.18 4.65 9 -6 -13 -0.18 5.21 -9 -6 13 10.77 5.21 9 6 -12 73.67 9.53 9 -6 -12 63.30 10.19 -9 -6 12 66.66 8.93 9 6 -11 20.03 6.05 9 -6 -11 34.20 8.13 -9 -6 11 31.95 7.29 9 6 -10 186.62 13.73 9 -6 -10 180.36 14.72 -9 -6 10 196.67 14.23 9 6 -9 2.70 4.26 9 -6 -9 0.23 5.31 -9 -6 9 16.18 5.42 9 6 -8 48.76 7.75 9 -6 -8 61.15 8.98 9 6 -7 10.91 5.27 9 -6 -7 13.55 5.36 9 -6 -6 16.49 5.85 9 -6 -5 58.86 8.49 9 6 -4 95.89 20.33 9 -6 -4 123.62 11.71 9 6 -3 123.25 21.76 9 -6 -3 131.20 11.77 9 -6 -2 48.90 8.48 9 6 -2 40.50 6.80 9 6 -2 56.70 15.79 9 -6 -1 17.98 5.73 9 6 -1 23.00 5.55 9 6 0 151.37 12.57 9 -6 0 183.39 14.26 9 6 0 140.76 12.44 9 -6 0 168.54 13.54 9 6 1 92.17 10.38 9 -6 1 108.90 11.05 9 6 1 77.90 9.75 9 -6 1 111.04 11.31 9 6 2 50.60 8.50 9 6 2 47.48 7.79 9 6 3 35.14 7.30 9 -6 3 27.70 6.75 9 6 3 30.58 7.22 9 6 4 76.00 10.50 9 -6 4 84.98 10.72 9 6 4 47.78 7.82 9 -6 5 30.46 6.89 9 6 5 22.71 6.35 9 -6 6 59.27 9.42 9 6 6 32.30 6.65 9 6 7 23.31 6.16 9 6 8 42.36 6.89 -9 -6 -9 7.09 4.77 9 6 9 4.31 3.64 -9 -6 -10 1.70 3.27 9 6 10 -1.36 2.88 -9 -6 -11 3.40 2.71 9 6 11 3.16 2.63 9 -7 -17 1.27 3.37 -9 -7 17 -2.16 2.93 9 -7 -16 24.95 5.83 -9 -7 16 20.86 4.95 9 -7 -15 20.69 5.91 -9 -7 15 19.85 5.05 9 7 -14 5.10 3.98 9 -7 -14 3.85 5.92 -9 -7 14 6.96 4.63 9 7 -13 28.66 6.27 9 -7 -13 42.29 8.22 -9 -7 13 40.02 7.38 9 7 -12 31.92 6.25 9 -7 -12 42.87 8.42 -9 -7 12 36.21 7.02 9 -7 -12 41.35 6.50 9 -7 -11 11.62 6.19 -9 -7 11 17.91 6.28 9 -7 -10 254.78 17.10 -9 -7 10 233.26 15.44 9 -7 -9 40.78 8.13 -9 -7 9 22.47 5.38 9 -7 -8 70.28 9.32 -9 -7 8 58.13 8.16 9 -7 -7 9.69 6.16 9 -7 -6 7.65 4.92 9 -7 -5 49.70 8.02 9 -7 -4 22.82 6.15 9 -7 -3 95.54 10.12 9 -7 -2 61.82 8.67 9 7 -2 49.70 7.40 9 -7 -1 0.75 4.39 9 7 -1 0.92 4.24 9 -7 0 81.82 10.02 9 7 0 66.48 9.49 9 -7 0 70.78 9.50 9 7 0 53.49 8.26 9 7 1 8.64 5.21 9 -7 1 7.22 5.30 9 7 1 2.84 4.10 9 7 2 75.56 10.37 9 -7 2 96.68 11.19 9 7 2 75.74 10.01 9 7 3 48.36 8.53 9 -7 3 47.58 8.64 9 7 3 37.32 6.92 9 7 4 54.20 8.29 9 7 4 84.77 10.62 9 -7 4 86.28 10.98 9 -7 5 -0.46 5.63 9 7 5 -5.17 4.23 9 7 6 5.12 4.11 9 7 7 3.86 4.56 9 7 8 31.21 6.51 -9 -7 -9 17.50 5.38 9 7 9 4.41 4.10 -9 -7 -10 5.64 3.68 9 7 10 0.30 2.88 -9 -7 -11 9.43 3.11 9 7 11 13.47 3.47 9 -8 -17 -1.72 3.04 -9 -8 17 1.53 2.79 9 -8 -16 66.26 7.39 -9 -8 16 74.26 7.55 9 -8 -15 12.24 5.18 -9 -8 15 7.74 4.66 9 -8 -14 29.75 7.12 -9 -8 14 15.58 5.16 9 -8 -13 68.33 9.48 -9 -8 13 71.47 9.17 9 -8 -12 14.33 6.07 -9 -8 12 11.55 5.66 9 -8 -12 13.44 4.58 9 -8 -11 25.36 7.38 -9 -8 11 28.86 6.94 9 -8 -10 46.46 8.35 -9 -8 10 45.33 8.14 9 -8 -9 147.78 13.00 -9 -8 9 132.68 12.05 9 -8 -8 -1.56 4.86 -9 -8 8 0.76 4.24 9 -8 -7 18.98 6.00 -9 -8 7 15.88 5.40 9 -8 -6 49.17 9.15 9 -8 -5 6.92 4.37 9 -8 -4 13.30 5.55 9 8 -3 147.43 12.30 9 -8 -3 150.72 12.83 9 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13.54 5.85 -9 -9 7 15.62 5.34 9 -9 -6 27.72 6.78 -9 -9 6 36.31 7.01 9 -9 -5 41.63 7.46 9 -9 -4 18.63 6.01 9 -9 -3 48.62 7.70 9 9 -3 47.32 7.75 9 -9 -2 81.84 9.53 9 9 -2 78.64 9.72 9 9 -1 94.31 10.50 9 -9 -1 101.66 10.96 9 -9 -1 114.02 11.52 9 -9 0 11.34 5.78 9 9 0 3.92 4.30 9 -9 0 10.54 5.34 9 9 0 -0.56 4.95 9 9 1 166.90 14.18 9 -9 1 165.88 13.54 9 9 1 155.80 13.48 9 9 2 61.74 9.21 9 -9 2 65.66 9.31 9 9 2 45.26 7.56 9 9 3 1.74 4.75 9 -9 3 6.55 5.59 9 9 3 6.46 5.07 9 9 4 126.67 13.47 9 -9 4 104.59 11.84 9 9 4 87.55 10.18 9 9 5 -3.29 4.87 9 -9 5 1.04 5.65 9 9 5 -0.59 4.53 9 9 6 15.76 6.21 9 9 7 42.68 7.03 9 9 8 1.35 4.01 -9 -9 -9 13.43 4.36 9 9 9 5.84 3.42 -9 -9 -10 7.52 3.79 9 9 10 3.54 3.30 -9 -9 -11 40.54 4.70 9 9 11 38.20 4.33 9 -10 -17 2.63 2.33 -9 -10 17 -3.91 2.97 9 -10 -16 7.65 3.71 -9 -10 16 4.91 3.60 9 -10 -15 14.47 5.15 -9 -10 15 7.88 4.34 9 -10 -14 9.45 4.50 -9 -10 14 3.65 5.18 9 -10 -13 22.56 6.18 -9 -10 13 30.67 6.42 9 -10 -13 29.86 5.05 9 -10 -12 13.28 5.44 -9 -10 12 4.74 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7.90 2.95 -9 -11 17 -1.05 2.51 9 -11 -16 35.67 4.76 -9 -11 16 38.47 5.76 9 -11 -15 3.83 3.75 -9 -11 15 -1.45 3.96 9 -11 -14 1.19 3.77 -9 -11 14 11.81 5.22 9 -11 -13 11.10 4.98 -9 -11 13 17.21 6.42 9 -11 -13 15.67 4.33 9 -11 -12 19.40 5.65 -9 -11 12 19.46 6.56 9 -11 -12 21.49 4.65 9 -11 -11 34.65 7.41 -9 -11 11 38.55 8.22 9 -11 -10 59.88 8.60 -9 -11 10 57.07 9.14 9 -11 -9 14.74 5.97 -9 -11 9 12.20 5.69 -9 -11 8 161.34 13.77 9 -11 -8 162.58 13.02 9 -11 -7 76.33 9.60 -9 -11 7 64.97 8.82 9 -11 -6 47.52 7.55 -9 -11 6 49.36 8.09 9 -11 -5 93.62 10.46 -9 -11 5 91.68 10.22 9 -11 -4 26.62 6.44 9 11 -4 21.27 5.93 -9 -11 4 19.09 5.22 9 -11 -3 23.95 6.37 9 11 -3 35.33 7.70 9 -11 -3 30.77 7.11 9 -11 -2 30.11 6.14 9 11 -2 29.51 6.84 9 -11 -2 36.57 7.69 9 11 -1 174.35 14.87 9 -11 -1 195.29 14.20 9 11 -1 169.93 14.00 9 -11 -1 169.11 13.41 9 -11 0 11.02 5.14 9 11 0 9.87 4.55 9 -11 0 13.92 5.80 9 11 0 18.98 6.27 9 11 1 236.07 17.13 9 -11 1 257.50 16.64 9 11 1 246.70 16.55 9 11 2 53.11 8.84 9 -11 2 59.20 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4.73 9 23 -1 20.80 5.45 9 23 0 -3.95 4.45 9 23 1 10.52 4.01 9 23 2 3.69 3.69 -9 -23 -2 -2.90 3.64 9 23 3 23.52 4.46 -9 -23 -3 16.91 4.35 9 23 4 1.97 2.52 -9 -24 10 10.41 3.07 -9 -24 9 4.51 2.93 9 24 -8 2.12 2.80 -9 -24 8 11.46 3.70 9 24 -7 7.17 3.30 9 24 -6 20.93 5.02 9 24 -5 11.53 4.38 9 24 -4 14.26 4.48 9 24 -3 -2.32 3.55 9 24 -2 7.81 4.21 9 24 -1 4.19 3.29 9 24 0 0.60 3.32 9 24 1 21.22 4.58 -9 -24 -1 22.06 5.10 9 24 2 41.29 5.63 -9 -24 -2 31.04 5.67 9 24 3 5.74 2.73 -9 -24 -3 3.22 3.32 9 25 -7 29.84 4.49 9 25 -6 13.92 3.86 9 25 -5 25.32 5.22 9 25 -4 2.31 3.31 9 25 -3 3.00 3.48 9 25 -2 2.11 3.00 9 25 -1 17.89 4.45 9 25 0 22.08 4.64 9 25 1 9.76 3.49 -9 -25 -1 7.25 4.16 9 25 2 89.68 6.83 -9 -25 -2 103.02 8.31 9 26 -6 4.62 2.76 9 26 -5 1.76 2.53 9 26 -4 -2.01 2.89 9 26 -3 23.92 4.67 9 26 -2 -4.67 3.37 9 26 -1 3.49 2.58 9 26 0 4.71 2.64 -9 -26 0 16.80 4.61 9 27 -3 15.20 3.44 10 0 -17 1.65 3.15 10 0 -16 6.35 3.60 10 0 -15 3.49 4.41 10 0 -14 -3.48 4.48 10 0 -13 2.02 4.83 10 0 -12 24.66 7.48 10 0 -11 21.83 6.51 10 0 -10 13.91 5.86 10 0 -9 30.98 7.67 10 0 -8 4.92 5.45 10 0 -7 42.96 8.22 10 0 -6 108.74 11.65 10 0 -5 473.60 22.75 10 0 -4 23.59 6.97 10 0 -3 6.90 5.99 10 0 -3 3.25 3.87 10 0 -2 3.65 5.01 10 0 -2 22.12 5.45 10 0 -1 49.27 8.02 10 0 -1 38.94 6.96 10 0 0 16.91 5.87 10 0 0 15.82 5.11 10 0 1 78.32 9.87 10 0 1 66.02 8.59 10 0 2 4.38 4.66 10 0 2 7.24 3.61 10 0 3 204.78 17.23 10 0 3 223.72 14.36 10 0 4 34.84 7.55 10 0 4 53.83 7.97 10 0 5 11.23 4.90 10 0 5 20.77 5.36 10 0 6 76.50 8.09 10 0 7 12.71 3.99 10 0 8 1.67 3.14 10 0 9 1.91 2.86 10 0 10 9.91 2.81 10 1 -17 3.25 3.21 10 -1 -17 -4.92 2.98 10 1 -16 2.09 3.87 10 -1 -16 -1.01 3.61 10 1 -15 18.86 5.63 10 -1 -15 16.20 5.30 10 1 -14 39.08 6.98 10 -1 -14 43.92 7.95 10 1 -13 22.10 6.56 10 -1 -13 16.91 6.77 10 1 -12 74.40 9.79 10 -1 -12 79.76 10.39 10 1 -11 151.61 13.35 10 -1 -11 176.90 14.75 10 1 -10 37.51 8.04 10 -1 -10 53.64 9.53 10 1 -9 16.24 6.07 10 -1 -9 7.38 5.65 10 1 -8 269.89 17.59 10 -1 -8 276.46 17.89 10 1 -7 6.75 6.08 10 -1 -7 2.81 5.25 10 1 -6 20.41 6.04 10 -1 -6 38.57 8.18 10 1 -5 554.99 24.20 10 -1 -5 493.18 23.15 10 1 -4 8.01 5.39 10 -1 -4 10.39 5.36 10 1 -3 162.07 12.41 10 1 -3 167.71 13.28 10 -1 -3 149.06 12.80 10 1 -2 69.71 9.19 10 -1 -2 57.65 8.70 10 1 -2 56.11 7.66 10 1 -1 88.91 10.22 10 -1 -1 85.09 9.83 10 -1 -1 103.10 10.05 10 1 -1 79.91 8.89 10 1 0 78.07 10.08 10 -1 0 67.08 8.83 10 -1 0 73.20 9.84 10 -1 0 54.00 7.61 10 1 0 59.75 8.48 10 -1 1 7.99 5.75 10 1 1 0.40 4.60 10 -1 1 3.28 3.46 10 1 1 4.37 4.25 10 -1 2 206.07 15.18 10 -1 2 180.26 12.65 10 1 2 192.67 13.67 10 -1 3 74.09 9.41 10 1 3 68.00 9.40 10 -1 3 99.52 9.68 10 1 3 94.95 9.87 10 -1 4 45.29 7.66 10 1 4 47.40 7.49 10 -1 4 65.66 8.24 10 1 4 78.01 9.05 10 1 5 134.74 11.36 10 -1 5 136.73 10.99 10 1 5 144.33 11.48 10 -1 6 35.32 6.42 10 1 6 38.83 6.49 10 -1 7 87.36 8.08 10 1 7 95.73 8.82 10 -1 8 23.46 4.68 10 1 8 24.45 5.06 10 -1 9 4.50 3.04 10 1 9 8.38 3.37 10 -1 10 45.91 4.40 10 1 10 46.37 4.70 10 2 -17 7.76 3.17 10 -2 -17 9.01 3.55 10 2 -16 11.46 4.25 10 -2 -16 8.23 3.91 10 2 -15 25.60 6.06 10 -2 -15 25.62 6.00 10 2 -14 32.28 6.80 10 -2 -14 25.08 6.11 10 2 -13 73.45 9.10 10 -2 -13 57.20 8.32 10 2 -12 10.04 5.42 10 -2 -12 15.39 6.51 10 2 -11 140.54 12.53 10 -2 -11 164.86 14.46 10 -2 -10 119.09 12.20 10 2 -10 114.35 12.00 10 2 -9 171.70 14.07 10 -2 -9 192.52 15.43 10 2 -8 141.69 12.66 10 -2 -8 161.34 13.93 10 2 -7 493.74 23.16 10 -2 -7 549.83 24.72 10 2 -6 172.92 14.30 10 -2 -6 174.52 14.01 10 2 -5 215.59 15.34 10 -2 -5 231.03 16.15 10 2 -4 5.34 4.70 10 -2 -4 1.13 4.58 10 2 -3 17.67 5.71 10 -2 -3 15.02 5.80 10 2 -2 14.67 5.49 10 -2 -2 18.17 5.80 10 2 -2 18.63 5.21 10 2 -1 113.29 11.00 10 2 -1 108.85 11.68 10 -2 -1 103.92 11.59 10 -2 0 198.18 15.43 10 2 0 213.88 14.58 10 -2 0 171.80 14.11 10 -2 1 77.29 10.18 10 2 1 53.95 8.68 10 2 1 82.08 9.35 10 -2 2 6.66 4.96 10 2 2 10.73 5.04 10 -2 2 13.65 4.29 10 2 2 6.15 3.86 10 -2 3 29.59 7.00 10 2 3 23.83 6.95 10 -2 3 26.50 5.29 10 2 3 33.83 6.60 10 -2 4 52.94 8.88 10 2 4 58.69 7.48 10 -2 4 73.06 7.96 10 2 4 56.20 8.02 10 2 5 53.09 7.40 10 -2 5 50.18 7.79 10 -2 5 64.60 7.68 10 2 5 67.69 8.57 10 -2 6 21.69 5.40 10 2 6 17.25 5.01 10 -2 7 5.25 3.60 10 2 7 8.64 4.14 10 -2 8 5.40 2.78 10 2 8 8.22 3.62 10 -2 9 4.94 2.87 10 2 9 4.31 3.00 10 2 10 7.17 2.54 10 3 -17 4.10 3.08 10 -3 -17 -1.03 2.87 10 3 -16 73.30 7.29 10 -3 -16 44.81 6.62 10 3 -15 16.71 4.67 10 -3 -15 16.98 5.20 10 3 -14 41.11 7.10 10 -3 -14 42.58 7.70 10 3 -13 25.91 6.74 10 -3 -13 25.87 6.93 10 3 -12 147.88 12.65 10 -3 -12 154.14 13.80 10 3 -11 101.89 10.81 10 -3 -11 105.38 11.97 10 -3 -10 75.73 10.02 10 3 -10 104.87 13.26 10 3 -9 154.51 13.34 10 -3 -9 159.28 13.87 10 3 -8 11.22 5.52 10 -3 -8 17.01 6.28 10 3 -7 403.14 20.45 10 -3 -7 461.65 22.66 10 3 -6 343.81 18.93 10 -3 -6 371.01 20.47 10 3 -5 -0.57 4.34 10 -3 -5 0.41 5.31 10 3 -4 16.86 5.88 10 -3 -4 23.26 7.00 10 3 -3 14.53 5.64 10 -3 -3 26.21 7.00 10 3 -2 -0.89 4.27 10 -3 -2 3.19 5.44 10 3 -2 2.56 4.47 10 3 -1 261.38 16.30 10 3 -1 248.56 15.93 10 -3 0 61.86 9.41 10 3 0 67.94 9.14 10 -3 0 81.26 10.33 10 3 0 74.91 9.35 10 -3 1 40.60 8.29 10 3 1 27.79 6.77 10 3 1 35.82 7.17 10 -3 2 33.78 7.66 10 3 2 25.95 6.19 10 3 2 28.05 6.03 10 -3 3 15.41 6.45 10 3 3 12.91 5.62 10 3 3 8.98 4.36 10 -3 4 40.89 7.07 10 3 4 39.25 7.05 10 -3 4 35.73 5.99 10 3 4 41.12 7.41 10 -3 5 19.91 6.09 10 -3 5 29.29 5.41 10 3 5 36.59 6.86 10 -3 6 210.46 12.24 10 3 6 176.55 12.46 10 -3 7 30.24 4.86 10 3 7 18.34 5.40 -10 -3 -8 4.68 3.54 10 -3 8 11.53 3.12 10 3 8 15.13 4.68 10 -3 9 12.96 3.03 10 3 9 14.70 3.75 10 3 10 8.28 2.91 10 4 -17 3.27 2.62 10 -4 -17 0.10 2.85 10 4 -16 6.65 3.60 10 -4 -16 0.82 3.63 10 4 -15 14.06 4.69 -10 -4 15 7.77 3.15 10 4 -14 11.69 5.97 10 -4 -14 27.05 7.03 10 4 -13 1.63 4.59 10 -4 -13 8.52 5.86 10 4 -12 5.13 4.65 10 -4 -12 14.77 6.02 10 4 -11 32.10 6.47 10 -4 -11 39.84 8.51 10 4 -10 11.52 4.69 10 -4 -10 10.69 6.36 10 4 -9 129.07 11.86 10 -4 -9 164.88 14.16 10 4 -8 13.66 6.54 10 -4 -8 4.72 5.27 10 4 -7 37.74 6.52 10 -4 -7 42.52 7.50 10 4 -6 -2.95 4.87 10 -4 -6 -2.19 5.21 10 4 -5 41.18 7.37 10 -4 -5 34.20 7.08 10 4 -4 20.96 6.11 10 -4 -4 15.50 6.45 10 4 -3 6.53 4.42 10 -4 -3 14.45 6.11 10 4 -2 171.81 13.48 10 4 -2 181.01 13.48 10 -4 -2 165.03 13.48 10 4 -1 366.89 18.96 10 4 -1 403.69 20.42 10 4 -1 384.95 19.64 10 -4 -1 376.43 20.29 10 -4 0 14.21 5.84 10 4 0 10.66 4.44 10 -4 0 16.94 5.77 10 4 0 23.59 6.54 10 4 1 322.96 18.77 10 -4 1 355.40 20.36 10 4 1 306.12 17.79 10 4 1 365.18 19.58 10 -4 2 95.19 11.23 10 4 2 76.36 8.96 10 4 2 106.73 10.88 10 -4 3 176.99 14.22 10 4 3 148.81 12.73 10 -4 4 8.54 5.55 10 4 4 11.95 4.86 10 -4 5 115.95 11.43 10 4 5 105.70 10.08 10 4 6 31.47 6.32 10 4 7 30.03 5.80 -10 -4 -8 7.02 3.57 10 4 8 -1.63 3.49 -10 -4 -9 12.88 3.63 10 4 9 7.35 3.28 10 4 10 3.64 2.36 10 -5 -17 -2.66 2.79 10 5 -16 39.86 5.14 10 -5 -16 49.11 6.17 -10 -5 16 41.12 5.26 10 5 -15 21.08 4.48 10 -5 -15 16.97 5.43 -10 -5 15 9.07 4.04 10 5 -14 16.87 5.23 10 -5 -14 26.04 6.39 -10 -5 14 26.34 4.98 10 5 -13 -0.04 3.99 10 -5 -13 -3.47 5.60 10 5 -12 19.43 5.70 10 -5 -12 28.27 7.79 10 5 -11 9.27 5.67 10 -5 -11 0.78 5.31 10 5 -10 29.49 6.80 10 -5 -10 32.54 7.41 10 5 -9 27.28 6.78 10 -5 -9 9.32 5.04 10 5 -8 73.46 8.97 10 -5 -8 97.09 11.45 10 5 -7 1.41 4.30 10 -5 -7 -3.24 4.96 10 5 -6 83.29 9.50 10 -5 -6 94.29 10.83 10 5 -5 53.40 8.29 10 -5 -5 46.88 7.99 10 5 -4 117.00 10.95 10 -5 -4 129.59 12.40 10 5 -3 7.30 4.87 10 -5 -3 -1.17 4.85 10 -5 -2 81.14 10.06 10 5 -2 78.17 9.66 10 5 -2 93.69 10.18 10 5 -1 106.08 10.85 10 -5 -1 136.86 12.79 10 5 -1 124.25 11.90 10 5 -1 116.37 10.34 10 -5 -1 114.67 11.91 10 -5 0 24.96 6.44 10 5 0 17.19 5.37 10 -5 0 30.04 7.09 10 5 0 28.02 6.79 10 5 1 106.07 11.46 10 5 1 116.63 11.13 10 -5 1 106.28 11.64 10 5 1 124.18 11.80 10 -5 2 80.82 10.33 10 5 2 84.18 10.28 10 -5 3 110.67 11.47 10 5 3 107.56 11.28 10 -5 4 15.09 6.28 10 5 4 7.85 4.33 10 -5 5 24.46 7.15 10 5 5 23.42 5.75 10 5 6 4.85 3.76 10 5 7 4.12 3.97 -10 -5 -8 1.41 3.71 10 5 8 1.44 3.05 -10 -5 -9 5.34 3.09 10 5 9 8.02 3.44 10 5 10 1.92 2.07 10 -6 -17 3.62 2.53 10 -6 -16 13.18 4.26 -10 -6 16 0.89 2.75 10 6 -15 7.91 4.24 10 -6 -15 6.44 4.08 -10 -6 15 5.68 3.82 10 6 -14 53.34 6.94 10 -6 -14 51.04 7.50 -10 -6 14 54.26 7.22 10 6 -13 55.30 7.35 10 -6 -13 73.23 9.50 -10 -6 13 61.31 7.79 10 6 -12 3.79 3.90 10 -6 -12 10.99 5.69 -10 -6 12 16.34 5.24 10 6 -11 44.85 7.51 10 -6 -11 49.80 8.48 10 6 -10 17.40 5.92 10 -6 -10 22.36 6.87 10 6 -9 75.00 9.07 10 -6 -9 62.17 9.42 10 6 -8 -0.15 4.15 10 -6 -8 -3.95 6.38 10 6 -7 65.69 8.67 10 -6 -7 64.71 9.27 10 6 -6 156.00 12.43 10 -6 -6 177.44 14.11 10 -6 -5 4.64 5.24 10 -6 -4 17.24 6.30 10 -6 -3 13.37 6.55 10 6 -2 6.59 4.92 10 6 -2 11.84 4.76 10 -6 -1 11.25 6.39 10 6 -1 13.73 4.97 10 -6 -1 19.47 6.64 10 6 -1 14.79 5.82 10 6 0 222.52 15.40 10 -6 0 262.30 17.54 10 6 0 256.90 16.76 10 -6 0 265.40 17.32 10 6 1 9.47 4.83 10 -6 1 1.25 5.13 10 6 1 12.84 5.50 10 6 2 30.86 7.30 10 -6 2 35.81 7.74 10 6 2 31.39 7.37 10 -6 3 0.96 4.98 10 6 3 -0.16 3.99 10 -6 4 5.84 5.26 10 6 4 8.56 5.07 10 -6 5 10.53 5.58 10 6 5 12.58 5.12 10 6 6 20.77 5.94 10 6 7 54.02 7.05 -10 -6 -8 5.02 3.34 10 6 8 10.53 4.11 -10 -6 -9 11.55 3.95 10 6 9 2.68 2.66 10 6 10 11.31 2.99 10 -7 -17 14.74 3.40 10 -7 -16 23.11 4.73 -10 -7 16 22.40 4.61 10 -7 -15 19.78 4.85 -10 -7 15 26.75 4.85 10 -7 -14 51.09 7.67 -10 -7 14 66.26 7.75 10 -7 -13 26.20 6.57 -10 -7 13 23.61 4.77 10 -7 -12 26.30 6.85 -10 -7 12 31.36 5.95 10 -7 -11 14.25 6.68 -10 -7 11 15.66 5.06 10 -7 -10 -8.84 5.68 10 -7 -9 128.18 12.63 10 -7 -8 13.60 5.54 10 -7 -7 11.69 5.77 10 -7 -6 32.08 7.58 10 -7 -5 57.37 9.30 10 -7 -4 225.80 15.96 10 -7 -3 5.45 5.10 10 7 -2 133.74 11.90 10 7 -2 145.48 12.94 10 -7 -2 158.97 13.54 10 -7 -1 -1.95 4.92 10 7 -1 3.30 3.83 10 -7 -1 7.32 5.71 10 7 -1 2.29 4.49 10 7 0 404.66 21.40 10 -7 0 407.98 21.52 10 7 0 392.14 20.63 10 7 1 -2.93 4.94 10 -7 1 -1.21 5.09 10 7 1 2.85 4.10 10 7 2 12.03 5.83 10 -7 2 5.12 6.04 10 7 2 4.50 5.24 10 -7 3 56.74 9.24 10 7 3 39.55 7.34 10 -7 4 49.49 8.38 10 7 4 24.75 5.74 10 -7 5 31.63 7.66 10 7 5 13.59 4.73 10 7 6 0.32 3.87 10 7 7 2.87 3.69 -10 -7 -8 17.80 4.67 10 7 8 17.16 4.50 -10 -7 -9 10.64 3.75 10 7 9 8.01 2.92 10 7 10 11.37 2.83 10 -8 -16 5.40 2.86 -10 -8 16 11.84 3.56 10 -8 -15 3.68 3.39 -10 -8 15 17.68 4.33 -10 -8 14 101.61 9.27 10 -8 -14 106.58 9.91 10 -8 -13 20.81 5.98 -10 -8 13 16.31 5.54 10 -8 -12 2.82 5.14 -10 -8 12 -1.72 3.89 10 -8 -11 9.55 5.94 -10 -8 11 10.05 4.45 10 -8 -10 37.26 7.64 -10 -8 10 36.11 6.59 10 -8 -9 0.03 5.12 10 -8 -8 9.44 6.33 10 -8 -7 7.15 4.84 10 -8 -6 6.22 6.06 10 -8 -5 11.01 6.49 10 -8 -4 337.43 19.20 10 -8 -3 35.99 7.41 10 -8 -2 49.46 8.00 10 8 -2 37.91 6.71 10 -8 -2 56.68 9.06 10 8 -2 31.93 7.72 10 -8 -1 50.66 8.41 10 8 -1 48.32 8.33 10 -8 -1 48.30 8.67 10 8 -1 35.90 7.25 10 8 0 269.22 17.65 10 -8 0 278.15 17.80 10 8 1 159.61 13.96 10 -8 1 169.99 14.01 10 8 1 136.29 12.22 10 8 2 6.68 5.09 10 -8 2 2.39 5.23 10 8 2 12.24 5.45 10 8 3 48.86 8.05 10 -8 3 44.08 8.11 10 8 3 38.90 7.14 10 -8 4 30.87 7.35 10 8 4 34.55 7.11 10 8 5 21.92 5.64 10 8 6 5.09 3.64 10 8 7 20.35 4.81 -10 -8 -8 13.66 4.25 10 8 8 12.94 3.99 -10 -8 -9 17.54 4.26 10 8 9 9.93 3.38 10 -9 -16 11.11 3.55 -10 -9 16 14.95 3.85 10 -9 -15 53.11 6.39 -10 -9 15 41.66 5.78 10 -9 -14 22.13 5.85 -10 -9 14 17.02 5.07 10 -9 -13 9.91 4.88 -10 -9 13 0.26 3.88 10 -9 -12 34.97 6.91 -10 -9 12 24.48 5.68 10 -9 -11 40.54 7.33 -10 -9 11 28.51 5.86 10 -9 -10 21.10 6.07 -10 -9 10 22.09 5.80 10 -9 -9 6.12 4.86 -10 -9 9 9.41 4.59 10 -9 -8 6.85 5.69 10 -9 -7 39.85 7.71 10 -9 -6 45.11 7.99 10 -9 -5 117.85 11.67 10 -9 -4 77.71 10.02 10 -9 -3 9.32 6.10 10 9 -3 10.16 4.91 10 -9 -3 3.86 4.79 10 9 -2 160.63 13.30 10 -9 -2 163.14 13.64 10 9 -2 147.66 13.27 10 -9 -2 177.94 14.09 10 -9 -1 31.72 6.55 10 9 -1 30.12 6.49 10 -9 -1 38.01 8.04 10 9 -1 32.91 7.65 10 9 0 113.94 11.85 10 -9 0 117.84 11.55 10 9 0 110.00 11.62 10 9 1 58.39 9.37 10 -9 1 52.00 9.03 10 9 1 54.57 8.31 10 9 2 2.77 4.47 10 -9 2 0.25 5.09 10 9 2 2.70 4.70 10 9 3 75.62 9.93 10 -9 3 65.96 9.41 10 9 3 69.39 9.48 10 -9 4 35.76 7.35 10 9 4 30.73 7.13 10 9 5 10.01 5.21 10 9 6 63.41 7.95 10 9 7 5.40 3.65 -10 -9 -8 24.06 4.78 10 9 8 17.43 3.85 -10 -9 -9 19.33 4.26 10 9 9 18.26 3.87 10 -10 -16 11.01 3.13 -10 -10 16 8.61 3.10 10 -10 -15 62.28 6.36 -10 -10 15 54.62 6.31 10 -10 -14 2.90 3.58 -10 -10 14 5.56 3.95 10 -10 -13 6.34 4.17 -10 -10 13 -2.11 3.76 10 -10 -12 3.87 4.15 -10 -10 12 9.21 4.21 10 -10 -11 36.21 7.43 -10 -10 11 33.47 6.37 10 -10 -10 19.85 6.00 -10 -10 10 16.25 5.60 10 -10 -9 -0.89 4.85 -10 -10 9 1.10 4.25 10 -10 -8 11.32 5.46 -10 -10 8 9.56 4.26 10 -10 -7 44.58 8.21 10 -10 -6 64.75 9.30 10 -10 -5 187.21 14.09 10 -10 -4 92.06 10.56 10 -10 -4 102.56 10.61 10 -10 -3 51.73 8.28 10 10 -3 45.31 7.62 10 -10 -3 48.57 8.10 10 -10 -2 34.99 7.37 10 10 -2 39.11 6.93 10 -10 -2 26.98 6.36 10 10 -2 40.42 7.62 10 -10 -1 14.69 6.44 10 10 -1 7.86 5.00 10 -10 -1 -0.21 4.50 10 10 -1 -2.15 4.27 10 10 0 72.01 9.74 10 -10 0 75.82 9.83 10 10 0 74.68 9.98 10 10 1 -5.62 5.23 10 -10 1 8.30 6.17 10 10 1 -1.65 4.58 10 10 2 12.15 5.74 10 -10 2 2.96 5.72 10 10 2 7.46 5.29 10 10 3 5.47 4.97 10 -10 3 10.33 5.71 10 10 3 13.09 5.04 10 -10 4 36.68 7.65 10 10 4 33.29 6.26 10 10 5 -0.90 4.09 10 10 6 17.30 4.36 10 10 7 -1.69 3.52 -10 -10 -8 7.91 3.84 10 10 8 7.70 3.28 -10 -10 -9 -3.05 2.76 10 10 9 4.18 2.62 -10 -11 16 13.07 3.13 10 -11 -15 24.03 4.33 -10 -11 15 23.51 4.48 10 -11 -14 4.79 3.62 -10 -11 14 6.22 3.82 10 -11 -13 27.11 5.57 -10 -11 13 21.57 5.54 10 -11 -12 53.33 7.58 -10 -11 12 47.71 7.38 10 -11 -11 81.04 9.21 -10 -11 11 64.61 7.98 10 -11 -10 10.44 4.92 -10 -11 10 2.30 4.06 -10 -11 9 127.61 11.41 10 -11 -9 108.65 10.93 10 -11 -8 77.57 9.47 -10 -11 8 60.05 8.08 -10 -11 7 223.66 14.71 10 -11 -7 221.62 15.13 10 -11 -6 289.46 17.30 10 -11 -5 88.43 10.10 10 -11 -5 102.18 10.62 10 -11 -4 11.52 5.87 10 11 -4 7.91 4.97 10 -11 -4 6.81 4.60 10 11 -3 114.08 11.70 10 -11 -3 144.11 12.61 10 -11 -3 111.84 11.14 10 -11 -2 93.89 10.40 10 11 -2 90.19 11.07 10 -11 -2 75.43 9.40 10 11 -2 79.45 9.95 10 -11 -1 14.53 5.77 10 11 -1 1.11 4.40 10 -11 -1 7.17 4.82 10 11 -1 -0.62 4.51 10 11 0 18.33 6.64 10 -11 0 18.86 5.95 10 11 0 20.16 6.59 10 11 1 -1.46 4.56 10 -11 1 2.35 4.48 10 11 1 9.98 5.49 10 11 2 208.96 15.75 10 -11 2 184.29 14.10 10 11 2 175.78 13.92 10 11 3 74.43 9.53 10 -11 3 72.23 9.90 10 11 3 74.21 9.42 10 11 4 28.73 6.43 10 11 5 4.43 3.83 10 11 6 14.08 4.35 10 11 7 12.19 3.60 -10 -11 -8 8.04 3.17 10 11 8 2.63 2.77 -10 -11 -9 9.99 3.03 10 11 9 2.94 2.54 10 -12 -15 -3.21 2.77 -10 -12 15 -0.02 2.88 10 -12 -14 8.43 3.36 -10 -12 14 -3.76 3.70 10 -12 -13 14.53 4.22 -10 -12 13 15.51 5.17 10 -12 -12 30.21 5.71 -10 -12 12 26.76 5.89 10 -12 -11 44.61 7.16 -10 -12 11 27.74 5.85 10 -12 -10 11.76 5.22 -10 -12 10 11.22 6.03 10 -12 -9 9.61 4.95 -10 -12 9 12.32 4.99 10 -12 -8 -0.73 4.68 -10 -12 8 2.07 4.03 10 -12 -7 27.83 6.44 -10 -12 7 27.23 6.72 -10 -12 6 113.40 10.57 10 -12 -6 119.01 11.71 10 -12 -5 99.03 10.35 10 -12 -5 111.30 10.44 10 -12 -4 74.95 9.43 10 12 -4 77.04 9.70 10 -12 -4 69.20 8.55 10 -12 -3 16.31 5.91 10 12 -3 9.88 5.03 10 -12 -3 17.94 5.72 10 -12 -2 37.58 7.03 10 12 -2 24.12 6.19 10 -12 -2 22.55 6.06 10 12 -2 27.36 6.84 10 12 -1 16.49 6.34 10 -12 -1 21.16 6.36 10 12 -1 16.74 5.74 10 12 0 8.47 5.24 10 -12 0 24.81 6.48 10 12 0 14.20 5.56 10 12 1 25.39 7.30 10 -12 1 19.68 6.15 10 12 1 31.98 6.89 10 12 2 1.15 4.57 10 -12 2 13.27 5.67 10 12 2 15.03 6.15 10 12 3 36.83 8.24 10 -12 3 30.61 7.28 10 12 3 30.75 7.03 10 12 4 1.09 4.44 10 12 4 9.15 4.66 10 12 5 22.54 4.90 10 12 6 14.04 4.42 10 12 7 62.42 6.41 -10 -12 -8 14.34 3.90 10 12 8 8.29 2.98 -10 -13 15 5.25 2.75 10 -13 -14 -2.61 2.55 -10 -13 14 6.33 3.58 -10 -13 13 75.67 7.74 10 -13 -13 91.03 7.85 10 -13 -12 -1.05 3.30 -10 -13 12 -3.22 3.80 10 -13 -11 9.14 4.70 -10 -13 11 -4.85 4.99 10 -13 -10 5.98 4.67 -10 -13 10 11.61 5.66 10 -13 -9 11.76 4.95 -10 -13 9 11.57 5.41 10 -13 -8 8.49 4.69 -10 -13 8 10.46 5.46 -10 -13 7 116.59 10.99 10 -13 -7 121.47 11.19 10 -13 -6 20.68 6.08 -10 -13 6 18.15 5.80 10 -13 -5 10.94 4.77 10 13 -5 4.34 4.02 -10 -13 5 4.97 4.26 10 -13 -4 -3.48 3.76 10 13 -4 6.05 4.84 10 -13 -4 4.03 3.96 10 -13 -3 5.81 4.29 10 13 -3 5.37 5.12 10 -13 -3 2.89 3.89 10 -13 -2 12.78 5.01 10 13 -2 20.77 6.47 10 -13 -2 18.73 5.26 10 13 -2 23.51 6.36 10 13 -1 38.91 7.74 10 -13 -1 48.53 7.87 10 13 -1 37.55 7.78 10 13 0 80.07 10.51 10 -13 0 78.01 9.22 10 13 0 75.01 9.46 10 13 1 2.48 5.40 10 -13 1 -1.96 4.57 10 13 1 1.25 4.20 10 13 2 -1.33 4.89 10 -13 2 2.93 5.16 10 13 2 2.51 4.16 10 13 3 40.54 7.92 10 -13 3 43.14 8.03 10 13 3 41.31 7.12 10 13 4 8.35 4.80 10 13 4 12.22 4.80 10 13 5 18.73 4.77 10 13 6 65.52 6.93 10 13 7 26.43 4.96 -10 -13 -8 6.73 2.99 10 13 8 4.52 2.20 -10 -14 15 13.44 3.11 -10 -14 14 11.30 3.89 10 -14 -13 24.06 4.31 -10 -14 13 32.36 5.66 10 -14 -12 -1.11 3.76 -10 -14 12 -4.53 4.31 10 -14 -11 8.01 3.83 -10 -14 11 11.86 5.07 10 -14 -10 -1.09 3.53 -10 -14 10 12.37 5.09 10 -14 -9 2.76 4.21 -10 -14 9 10.28 5.26 10 -14 -8 2.21 4.15 -10 -14 8 -1.38 4.02 10 -14 -7 31.73 5.81 -10 -14 7 23.17 6.40 10 -14 -6 40.43 6.99 -10 -14 6 40.89 7.60 10 -14 -5 19.15 5.43 10 14 -5 8.41 3.79 -10 -14 5 18.43 5.49 10 -14 -4 -2.90 4.21 10 14 -4 4.34 5.22 -10 -14 4 4.35 3.91 10 -14 -3 50.15 7.59 10 14 -3 63.71 9.48 10 -14 -3 48.19 7.43 10 14 -3 54.87 8.63 10 14 -2 14.42 6.12 10 -14 -2 21.69 5.95 10 14 -2 11.82 5.69 10 14 -1 77.32 10.62 10 -14 -1 77.01 8.82 10 14 -1 72.46 9.67 10 14 0 48.21 8.72 10 -14 0 42.12 7.34 10 14 0 40.39 7.38 10 14 1 74.95 10.11 10 -14 1 100.38 10.11 10 14 1 92.82 10.15 10 14 2 7.08 5.46 10 -14 2 4.18 4.64 10 14 2 12.70 5.13 10 14 3 40.95 7.83 10 14 3 46.30 7.09 10 14 4 2.49 4.24 10 14 4 6.28 4.04 10 14 5 11.09 3.95 10 14 6 10.14 3.79 -10 -14 -7 -4.15 3.13 10 14 7 -0.40 2.33 -10 -14 -8 8.50 3.05 -10 -15 14 5.28 3.20 -10 -15 13 9.19 4.03 -10 -15 12 -0.46 3.63 10 -15 -11 1.63 2.76 -10 -15 11 2.75 4.25 10 -15 -10 12.89 4.50 -10 -15 10 11.06 4.98 10 -15 -9 25.06 5.12 -10 -15 9 29.55 6.61 10 -15 -8 49.32 6.88 -10 -15 8 44.01 7.33 10 -15 -7 3.11 3.59 -10 -15 7 2.37 4.32 10 -15 -6 12.90 4.49 -10 -15 6 -4.54 4.77 10 -15 -5 22.40 5.27 10 15 -5 29.84 6.27 -10 -15 5 18.29 5.30 10 15 -4 126.64 12.22 -10 -15 4 122.49 11.19 10 -15 -4 152.84 11.67 10 -15 -3 17.79 4.48 10 15 -3 17.17 6.09 -10 -15 3 13.16 5.04 10 15 -3 14.02 5.64 10 15 -2 5.83 4.31 10 -15 -2 12.08 4.12 10 15 -2 11.62 4.76 10 15 -1 65.17 9.43 10 -15 -1 81.52 8.64 10 15 -1 68.96 9.18 10 15 0 36.66 7.77 10 -15 0 38.73 6.65 10 15 0 32.06 6.50 10 15 1 49.32 8.25 10 -15 1 49.19 7.39 10 15 1 59.67 8.02 10 15 2 3.66 4.55 10 15 2 8.50 4.38 10 15 3 0.16 4.78 10 15 3 6.52 4.54 10 15 4 8.99 4.91 10 15 4 10.79 4.16 10 15 5 14.73 4.30 10 15 6 6.74 3.25 -10 -15 -7 -2.02 2.60 10 15 7 3.14 2.14 -10 -16 14 9.78 3.09 -10 -16 13 17.93 4.29 -10 -16 12 14.87 4.06 -10 -16 11 0.98 3.69 -10 -16 10 10.80 4.63 -10 -16 9 19.43 5.11 -10 -16 8 70.68 8.89 -10 -16 7 3.40 4.44 10 16 -6 -0.28 3.47 -10 -16 6 7.17 5.23 10 16 -5 64.35 8.55 -10 -16 5 72.53 8.84 10 16 -4 97.17 10.90 -10 -16 4 98.36 9.88 10 16 -3 17.50 6.05 10 16 -3 18.77 5.39 10 16 -2 -1.42 4.29 10 16 -2 2.46 4.05 10 16 -1 9.14 5.55 10 -16 -1 1.76 3.56 10 16 -1 -0.78 4.05 10 16 0 35.02 7.24 10 -16 0 50.45 7.32 10 16 0 50.96 7.20 10 16 1 -0.35 4.56 10 16 1 -0.23 3.74 10 16 2 9.75 5.28 10 16 2 16.87 4.62 10 16 3 6.90 4.47 10 16 3 4.19 3.21 10 16 4 8.14 5.05 10 16 4 11.49 3.96 10 16 5 15.62 3.89 10 16 6 32.13 4.26 -10 -16 -7 -0.39 2.34 -10 -17 13 -0.25 2.67 -10 -17 12 24.61 4.63 -10 -17 11 -4.33 3.96 -10 -17 10 69.83 8.09 -10 -17 9 8.52 4.85 -10 -17 8 -3.08 4.18 -10 -17 7 2.17 4.09 10 17 -6 7.99 4.74 -10 -17 6 6.69 3.93 10 17 -5 14.03 5.25 -10 -17 5 9.22 3.96 10 17 -4 47.74 7.69 -10 -17 4 48.20 7.30 10 17 -4 57.02 7.97 10 17 -3 46.45 8.09 10 17 -3 61.06 7.92 10 17 -2 10.40 5.45 10 17 -2 1.20 4.19 10 17 -1 -1.67 4.41 10 17 -1 -4.60 3.89 10 17 0 37.94 7.33 10 17 0 42.99 6.70 10 17 1 9.29 5.09 10 17 1 9.12 4.17 10 17 2 10.37 4.94 10 17 2 9.78 4.28 10 17 3 0.41 3.79 10 17 3 6.16 3.66 10 17 4 4.99 4.12 10 17 4 6.15 3.09 10 17 5 1.59 2.44 -10 -17 -6 4.66 2.82 10 17 6 3.22 2.34 -10 -18 13 8.39 2.81 -10 -18 12 3.62 2.87 -10 -18 11 -1.92 3.47 -10 -18 10 29.09 5.78 -10 -18 9 -0.05 3.53 -10 -18 8 11.35 4.56 -10 -18 7 126.29 10.85 10 18 -6 24.93 5.83 -10 -18 6 18.89 5.84 10 18 -5 5.64 4.22 -10 -18 5 3.56 3.60 10 18 -4 12.16 4.12 10 18 -4 7.66 4.26 10 18 -3 3.08 4.02 10 18 -3 3.33 3.94 10 18 -2 13.66 5.59 10 18 -2 12.08 4.67 10 18 -1 32.16 6.67 10 18 -1 31.40 6.09 10 18 0 13.19 5.32 10 18 0 11.47 4.24 10 18 1 64.65 8.59 10 18 1 74.10 7.83 10 18 2 15.73 5.48 10 18 2 19.34 4.19 10 18 3 10.29 4.46 10 18 3 13.02 3.59 10 18 4 13.49 3.58 10 18 5 4.60 2.46 -10 -19 12 12.20 3.34 -10 -19 11 4.91 3.28 -10 -19 10 -1.56 3.14 -10 -19 9 9.37 4.10 -10 -19 8 11.49 4.05 10 19 -7 5.98 3.80 -10 -19 7 3.97 3.90 10 19 -6 12.93 4.50 -10 -19 6 3.91 3.94 10 19 -5 0.26 4.25 -10 -19 5 -3.57 4.41 10 19 -5 -1.16 3.91 10 19 -4 28.19 6.44 10 19 -4 29.14 5.62 10 19 -3 33.68 7.10 10 19 -3 38.94 5.85 10 19 -2 2.70 4.42 10 19 -2 1.39 3.36 10 19 -1 34.32 6.65 10 19 -1 41.80 5.93 10 19 0 19.05 5.57 10 19 0 28.07 5.15 10 19 1 47.79 7.17 10 19 1 43.87 5.80 10 19 2 11.67 4.55 10 19 2 5.51 3.22 10 19 3 14.44 4.67 10 19 3 10.18 3.49 10 19 4 2.85 1.95 -10 -20 12 7.54 2.70 -10 -20 11 2.65 2.71 -10 -20 10 5.53 3.27 -10 -20 9 51.61 6.39 -10 -20 8 19.62 5.06 10 20 -7 4.14 3.03 -10 -20 7 6.71 4.59 10 20 -6 7.46 4.13 -10 -20 6 4.04 3.62 10 20 -6 3.51 3.23 10 20 -5 10.84 4.64 10 20 -5 8.93 3.66 10 20 -4 7.26 4.16 10 20 -4 6.57 3.66 10 20 -3 9.25 4.62 10 20 -3 5.71 3.32 10 20 -2 5.48 4.63 10 20 -2 0.00 2.95 10 20 -1 105.98 9.97 10 20 -1 108.78 8.78 10 20 0 28.38 6.04 10 20 0 30.77 4.54 10 20 1 -2.53 3.92 10 20 1 -0.97 2.75 -10 -20 -1 4.06 4.99 10 20 2 0.24 3.43 10 20 2 -2.44 2.34 10 20 3 21.54 4.69 -10 -21 11 4.27 2.64 -10 -21 10 8.98 3.15 -10 -21 9 2.42 2.86 -10 -21 8 42.62 5.98 10 21 -8 46.42 5.55 10 21 -7 24.06 4.56 -10 -21 7 21.58 4.77 10 21 -7 20.40 4.14 10 21 -6 5.75 3.67 10 21 -6 23.36 4.86 10 21 -5 61.76 7.42 10 21 -5 50.34 6.14 10 21 -4 3.51 3.89 10 21 -4 12.71 3.34 10 21 -3 7.81 4.36 10 21 -3 12.31 3.74 10 21 -2 14.03 4.80 10 21 -2 17.88 4.24 10 21 -1 6.81 4.20 10 21 -1 9.11 2.71 10 21 0 5.59 3.61 10 21 0 -4.66 2.84 10 21 1 13.16 4.29 -10 -21 -1 13.87 4.60 10 21 2 11.92 4.01 10 21 3 -3.65 3.03 -10 -22 10 15.59 3.14 -10 -22 9 -4.24 2.99 -10 -22 8 28.98 4.64 10 22 -8 25.76 3.83 10 22 -7 4.16 2.89 10 22 -7 6.83 2.98 10 22 -6 11.30 3.73 10 22 -6 13.00 3.49 10 22 -5 49.04 6.50 10 22 -5 55.72 5.52 10 22 -4 4.28 3.77 10 22 -4 12.12 3.19 10 22 -3 14.21 4.46 10 22 -2 9.46 3.85 10 22 -1 3.24 3.65 10 22 0 10.24 3.54 10 22 1 4.91 3.33 -10 -22 -1 8.37 4.44 10 22 2 3.32 2.53 10 23 -6 9.61 3.14 10 23 -5 32.71 5.19 10 23 -4 5.23 3.27 10 23 -3 24.34 4.82 10 23 -2 4.92 3.44 10 23 -1 13.11 3.88 10 23 0 11.52 3.37 -10 -23 0 6.91 3.66 10 23 1 5.87 2.80 10 24 -5 4.79 2.35 10 24 -4 -1.16 2.62 10 24 -3 1.36 2.68 10 24 -2 -2.91 2.54 10 24 -1 16.78 3.59 10 24 0 17.89 3.57 11 0 -16 4.59 2.63 11 0 -15 -0.88 3.39 11 0 -14 15.93 5.23 11 0 -13 -4.07 4.33 11 0 -12 4.02 4.53 11 0 -11 121.40 11.33 11 0 -10 12.90 5.82 11 0 -9 5.34 5.66 11 0 -8 66.79 9.25 11 0 -7 -4.98 5.09 11 0 -6 268.56 17.38 11 0 -5 45.13 8.35 11 0 -4 2.80 4.52 11 0 -3 26.69 6.82 11 0 -2 6.74 4.62 11 0 -2 11.18 4.32 11 0 -1 -2.70 4.65 11 0 -1 1.74 4.66 11 0 -1 3.54 4.00 11 0 0 2.91 4.60 11 0 0 -0.36 3.79 11 0 1 57.78 8.74 11 0 1 68.93 8.39 11 0 2 99.70 10.67 11 0 2 123.77 10.43 11 0 3 6.74 5.11 11 0 3 8.16 3.57 11 0 4 50.82 7.35 11 0 4 52.73 6.72 11 0 5 50.88 6.52 11 0 6 -1.92 2.55 11 0 7 25.30 4.06 11 0 8 -3.75 2.38 11 1 -16 3.32 2.84 11 -1 -16 -7.38 3.51 11 1 -15 12.59 4.13 11 -1 -15 13.55 4.11 11 1 -14 0.11 4.02 11 -1 -14 4.93 4.02 11 1 -13 60.36 8.07 11 -1 -13 58.80 7.81 11 1 -12 7.62 5.23 11 -1 -12 9.79 5.19 11 1 -11 27.26 7.02 11 -1 -11 23.02 6.09 11 1 -10 35.91 7.47 11 -1 -10 53.19 8.51 11 1 -9 32.28 7.35 11 -1 -9 25.82 6.90 11 1 -8 52.03 8.77 11 -1 -8 41.47 7.88 11 1 -7 20.68 6.43 11 -1 -7 30.01 7.27 11 1 -6 18.43 6.73 11 -1 -6 9.10 5.60 11 1 -5 38.86 7.60 11 -1 -5 32.45 7.15 11 1 -4 16.13 5.82 11 -1 -4 27.88 7.19 11 1 -4 27.05 5.64 11 1 -3 0.38 4.36 11 -1 -3 11.09 5.47 11 1 -3 4.82 3.42 11 1 -2 149.30 12.01 11 1 -2 149.50 12.67 11 -1 -2 143.38 13.08 11 -1 -1 4.56 5.16 11 -1 -1 6.51 5.06 11 1 -1 14.10 5.15 11 -1 0 10.51 6.07 11 1 0 11.22 4.69 11 1 0 10.55 4.74 11 -1 1 201.75 15.20 11 1 1 170.60 13.79 11 -1 1 186.16 12.28 11 1 1 202.00 13.54 11 -1 2 5.80 4.89 11 1 2 4.89 4.94 11 -1 2 5.62 4.01 11 1 2 14.01 5.26 11 -1 3 12.22 5.40 11 1 3 13.18 4.94 11 -1 3 11.32 3.66 11 1 3 12.98 4.23 11 1 4 70.62 8.42 11 -1 4 66.89 8.25 11 -1 4 90.67 8.30 11 1 4 94.75 8.97 11 -1 5 25.34 5.02 11 1 5 31.36 5.23 11 -1 6 1.24 2.56 11 1 6 1.02 2.78 11 -1 7 0.08 2.27 11 1 7 9.46 3.35 11 1 8 13.44 2.87 11 2 -16 -1.45 2.76 11 -2 -16 2.05 2.85 11 2 -15 17.34 4.15 11 -2 -15 21.88 4.87 11 2 -14 1.90 3.80 11 -2 -14 5.95 4.60 11 2 -13 20.53 5.79 11 -2 -13 12.23 5.39 11 2 -12 2.62 4.45 11 -2 -12 -4.66 5.25 11 2 -11 92.70 10.07 11 -2 -11 98.32 11.27 11 2 -10 18.88 5.48 11 -2 -10 21.82 7.22 11 2 -9 55.11 8.88 11 -2 -9 55.28 8.79 11 2 -8 68.93 10.01 11 -2 -8 70.03 9.67 11 2 -7 20.88 6.66 11 -2 -7 18.62 6.70 11 2 -6 29.88 7.54 11 -2 -6 19.33 6.07 11 2 -5 34.90 7.64 11 -2 -5 23.69 6.52 11 2 -4 6.10 5.75 11 -2 -4 0.66 4.67 11 2 -4 9.41 4.78 11 2 -3 44.99 8.13 11 -2 -3 35.93 7.70 11 2 -3 21.76 5.45 11 2 -2 166.36 12.76 11 2 -2 164.66 12.99 11 -2 -2 164.54 13.65 11 -2 -1 7.94 5.48 11 -2 -1 4.90 5.96 11 2 -1 0.87 4.26 11 -2 0 17.23 6.55 11 2 0 17.39 5.67 11 2 0 11.91 4.68 11 -2 1 225.82 15.86 11 2 1 213.83 14.03 11 -2 2 1.77 4.50 11 2 2 5.91 4.41 11 2 2 5.97 4.00 11 -2 3 2.93 4.12 11 2 3 11.18 4.90 11 2 3 -0.69 3.91 11 2 4 63.81 7.98 11 -2 4 51.97 7.55 11 -2 4 58.18 6.63 11 2 4 59.90 7.57 11 -2 5 -0.47 2.99 11 2 5 3.07 3.63 11 -2 6 27.00 4.35 11 2 6 32.50 5.30 11 2 7 7.06 3.48 11 2 8 14.64 3.28 11 3 -16 2.81 2.74 11 -3 -16 -1.69 3.00 11 3 -15 4.18 3.52 11 -3 -15 5.87 3.79 11 3 -14 11.73 4.59 11 -3 -14 14.72 4.92 11 3 -13 36.84 6.16 11 -3 -13 49.48 7.32 11 3 -12 9.28 4.65 11 -3 -12 1.43 5.45 11 3 -11 29.93 7.28 11 -3 -11 27.71 6.94 11 3 -10 23.50 6.11 11 -3 -10 21.78 7.47 11 3 -9 33.27 6.95 11 -3 -9 25.35 6.50 11 3 -8 44.86 7.93 11 -3 -8 40.89 8.24 11 3 -7 10.41 5.45 11 -3 -7 14.07 6.69 11 3 -6 6.30 4.64 11 -3 -6 4.95 5.25 11 3 -5 278.35 17.22 11 -3 -5 280.49 17.76 11 3 -4 86.23 10.06 11 -3 -4 89.32 10.65 11 3 -4 85.30 9.66 11 3 -3 49.06 8.15 11 -3 -3 50.35 8.84 11 3 -3 48.63 7.46 11 3 -2 3.05 4.31 11 -3 -2 7.27 5.73 11 3 -2 6.27 4.39 11 -3 -1 5.14 4.80 11 -3 -1 14.32 6.40 11 3 -1 9.43 4.97 11 -3 0 32.20 7.70 11 3 0 29.09 6.92 11 3 0 38.00 7.13 11 -3 1 119.47 12.24 11 3 1 90.10 9.94 11 3 1 95.15 10.01 11 -3 2 26.84 6.34 11 3 2 27.21 6.56 11 3 2 18.80 5.04 11 -3 3 4.13 4.26 11 3 3 18.35 5.71 11 3 3 15.40 4.99 11 -3 4 72.77 8.50 11 3 4 73.22 8.43 11 3 5 21.80 4.99 11 3 6 0.21 2.90 11 3 7 22.03 4.28 11 3 8 0.53 2.12 11 -4 -16 1.50 2.67 11 4 -15 8.87 3.62 11 -4 -15 10.57 4.10 11 4 -14 14.56 4.35 11 -4 -14 5.99 4.04 11 4 -13 30.63 5.70 11 -4 -13 27.58 6.41 11 4 -12 13.29 5.35 11 -4 -12 1.45 4.48 11 4 -11 18.75 5.76 11 -4 -11 3.87 5.16 11 4 -10 88.78 9.71 11 -4 -10 93.70 10.64 11 4 -9 13.41 5.57 11 -4 -9 -0.29 6.33 11 4 -8 117.84 11.09 11 -4 -8 121.43 12.28 11 4 -7 43.38 7.70 11 -4 -7 38.46 8.49 11 4 -6 55.24 8.46 11 -4 -6 59.09 8.90 11 4 -5 106.76 10.92 11 -4 -5 125.70 12.69 11 4 -4 246.98 16.10 11 4 -4 235.27 15.48 11 -4 -4 287.01 18.01 11 4 -3 34.11 6.75 11 -4 -3 51.03 8.90 11 4 -3 44.63 7.43 11 4 -2 -2.13 4.19 11 -4 -2 4.52 5.13 11 -4 -2 -2.12 5.27 11 4 -2 0.33 3.90 11 -4 -1 8.83 5.69 11 -4 -1 3.47 5.27 11 4 -1 16.68 5.67 11 -4 0 53.18 9.18 11 4 0 39.02 7.38 11 4 0 29.76 6.64 11 -4 1 133.68 12.81 11 4 1 109.37 10.73 11 4 1 111.96 10.95 11 4 2 100.28 9.96 11 -4 2 107.23 11.07 11 4 2 112.53 10.42 11 -4 3 4.35 4.80 11 4 3 4.21 3.81 11 -4 4 4.88 4.70 11 4 4 6.96 3.99 11 4 5 16.18 4.56 11 4 6 -2.50 3.04 -11 -4 -7 8.83 3.47 11 4 7 10.79 3.77 11 4 8 7.77 2.48 11 -5 -16 16.46 3.97 11 -5 -15 -4.39 3.80 11 5 -14 24.10 4.86 11 -5 -14 28.36 5.78 11 5 -13 7.84 4.14 11 -5 -13 2.28 4.22 11 5 -12 24.81 5.03 11 -5 -12 36.34 7.42 11 5 -11 80.37 8.62 11 -5 -11 86.41 10.32 11 5 -10 46.08 7.27 11 -5 -10 56.25 9.95 11 5 -9 17.67 5.62 11 -5 -9 18.78 6.42 11 5 -8 74.08 9.12 11 -5 -8 86.32 10.74 11 5 -7 1.80 4.48 11 -5 -7 3.77 5.08 11 5 -6 212.82 14.52 11 -5 -6 233.13 16.64 11 5 -5 11.49 4.78 11 -5 -5 13.73 5.27 11 5 -4 324.94 17.85 11 -5 -4 338.68 19.75 11 5 -3 -1.82 4.22 11 -5 -3 -2.02 5.40 11 5 -3 4.69 3.92 11 -5 -2 71.59 9.36 11 -5 -2 59.03 9.35 11 5 -2 61.87 8.63 11 -5 -1 145.45 12.88 11 5 -1 115.20 11.08 11 -5 -1 132.38 12.58 11 -5 0 94.21 11.41 11 5 0 87.03 9.46 11 5 0 102.45 10.66 11 -5 1 83.06 10.35 11 5 1 74.77 8.93 11 5 1 63.04 8.41 11 -5 2 28.90 7.17 11 5 2 33.61 6.62 11 -5 3 2.54 4.62 11 5 3 2.13 4.77 11 -5 4 4.86 5.18 11 5 4 10.51 4.62 11 5 5 1.05 3.33 11 5 6 0.55 2.93 -11 -5 -7 16.11 3.60 11 5 7 24.10 4.38 11 5 8 2.23 2.15 11 -6 -16 -1.53 2.69 11 -6 -15 25.21 4.64 11 -6 -14 32.04 5.88 11 -6 -13 25.66 6.10 11 -6 -12 14.47 5.68 11 6 -11 17.99 4.77 11 -6 -11 15.85 5.51 11 6 -10 46.42 6.88 11 -6 -10 37.67 7.18 11 6 -9 53.73 7.33 11 -6 -9 48.89 8.89 11 6 -8 12.22 4.90 11 -6 -8 11.94 5.77 11 -6 -7 83.72 10.30 11 -6 -6 137.18 12.76 11 -6 -5 3.88 5.59 11 -6 -4 269.56 17.28 11 6 -3 95.47 10.52 11 -6 -3 127.82 12.55 11 -6 -2 94.15 10.99 11 -6 -2 91.34 10.81 11 6 -2 74.04 9.61 11 -6 -1 21.95 6.13 11 6 -1 34.54 6.60 11 -6 -1 24.39 6.76 11 6 -1 29.99 6.76 11 -6 0 9.62 5.90 11 6 0 11.00 5.24 11 6 0 15.39 5.98 11 -6 1 60.10 9.18 11 6 1 61.03 8.51 11 -6 2 32.99 7.18 11 6 2 36.00 7.03 11 -6 3 15.72 5.97 11 6 3 17.38 5.29 11 -6 4 -0.91 4.65 11 6 4 10.95 5.01 11 6 5 15.53 4.55 11 6 6 9.30 3.35 -11 -6 -7 15.35 3.73 11 6 7 16.64 3.73 11 6 8 -0.41 2.01 11 -7 -16 24.91 3.96 11 -7 -15 26.50 4.66 11 -7 -14 9.26 3.56 11 -7 -13 16.38 5.08 11 -7 -12 20.04 6.59 11 -7 -11 55.46 9.02 11 -7 -10 9.05 5.23 11 -7 -9 12.42 6.07 11 -7 -8 4.94 5.34 11 -7 -7 6.21 5.80 11 -7 -6 31.81 7.52 11 -7 -5 4.12 4.78 11 -7 -4 92.90 11.11 11 -7 -3 23.31 6.35 11 -7 -3 31.17 7.40 11 7 -3 28.04 6.91 11 -7 -2 7.75 5.32 11 -7 -2 -0.52 5.41 11 7 -2 2.68 4.53 11 7 -1 65.22 8.64 11 -7 -1 62.44 9.78 11 7 -1 43.98 7.37 11 7 -1 56.29 8.09 11 7 0 13.82 5.63 11 -7 0 17.51 7.08 11 7 0 19.02 6.02 11 -7 1 61.46 8.82 11 7 1 63.24 8.77 11 -7 2 9.21 5.30 11 7 2 10.49 4.80 11 -7 3 36.59 7.30 11 7 3 31.80 6.33 11 -7 4 41.90 7.74 11 7 4 28.40 5.81 11 7 5 11.59 4.14 11 7 6 1.95 2.88 -11 -7 -7 11.54 3.31 11 7 7 16.30 3.95 11 7 8 7.60 2.72 11 -8 -15 12.69 3.66 11 -8 -14 14.61 4.50 11 -8 -13 42.85 6.66 11 -8 -12 2.28 4.03 11 -8 -11 17.44 5.74 11 -8 -10 13.15 5.33 11 -8 -9 4.31 5.31 11 -8 -8 99.62 10.92 11 -8 -7 4.45 5.88 11 -8 -6 49.00 8.86 11 -8 -5 16.12 6.44 11 -8 -4 7.53 5.38 11 -8 -4 11.60 6.05 11 -8 -3 129.19 12.28 11 8 -3 101.42 10.98 11 -8 -3 126.57 12.07 11 -8 -2 0.80 5.23 11 8 -2 0.95 3.77 11 -8 -2 11.03 6.01 11 8 -2 8.07 5.16 11 8 -1 54.85 8.27 11 -8 -1 51.87 8.75 11 8 -1 48.53 7.75 11 8 0 103.99 11.00 11 -8 0 116.63 11.76 11 8 0 103.80 10.76 11 -8 1 38.90 7.71 11 8 1 20.76 5.61 11 -8 2 67.07 8.87 11 8 2 72.21 9.01 11 -8 3 5.19 4.84 11 8 3 -0.52 4.08 11 -8 4 38.62 7.58 11 8 4 20.35 5.27 11 8 5 3.96 3.18 11 8 6 2.10 3.09 -11 -8 -7 10.62 3.83 11 8 7 0.24 2.60 11 8 8 6.16 2.39 11 -9 -15 -1.68 2.65 11 -9 -14 -3.54 3.17 11 -9 -13 28.38 5.35 11 -9 -12 9.74 4.72 11 -9 -11 79.03 9.22 11 -9 -10 5.96 5.16 11 -9 -9 23.60 6.16 11 -9 -8 35.27 7.41 11 -9 -7 52.45 8.74 11 -9 -6 5.01 4.62 11 -9 -5 20.05 6.02 11 -9 -5 19.06 5.56 11 -9 -4 46.78 8.03 11 -9 -4 56.53 9.00 11 -9 -3 15.53 6.20 11 -9 -3 19.48 6.28 11 9 -3 15.39 6.06 11 -9 -2 19.11 6.61 11 9 -2 15.57 5.32 11 -9 -2 22.12 6.50 11 9 -2 13.42 5.56 11 9 -1 9.44 5.22 11 -9 -1 15.94 5.78 11 9 -1 12.73 5.56 11 9 0 54.06 8.52 11 -9 0 54.12 8.42 11 9 0 40.64 7.40 11 9 1 32.33 6.71 11 -9 1 24.03 6.59 11 9 1 23.74 5.63 11 -9 2 21.31 6.32 11 9 2 17.11 5.94 11 -9 3 13.55 5.78 11 9 3 14.24 4.60 11 9 4 91.68 9.12 11 9 5 6.59 3.39 11 9 6 5.06 3.27 -11 -9 -7 3.26 2.67 11 9 7 2.48 2.75 11 -10 -15 4.53 2.54 11 -10 -14 -1.30 3.09 11 -10 -13 14.34 4.57 11 -10 -12 5.25 4.24 11 -10 -11 0.64 4.01 11 -10 -10 26.86 6.00 11 -10 -9 106.33 10.23 11 -10 -8 19.08 5.87 11 -10 -7 182.21 13.74 11 -10 -6 11.09 5.92 11 -10 -6 11.66 5.38 11 -10 -5 19.56 5.79 11 -10 -5 13.67 5.47 11 -10 -4 -1.74 5.20 11 -10 -4 0.64 4.17 11 -10 -3 86.44 9.91 11 10 -3 75.17 8.73 11 -10 -3 86.14 10.14 11 10 -3 93.80 10.67 11 -10 -2 91.26 10.38 11 10 -2 95.92 9.97 11 -10 -2 101.01 10.50 11 10 -2 62.85 8.66 11 10 -1 11.82 4.89 11 -10 -1 20.76 6.01 11 10 -1 22.55 6.13 11 10 0 3.16 4.02 11 -10 0 2.21 4.35 11 10 0 0.44 4.33 11 10 1 22.89 6.36 11 -10 1 12.47 5.42 11 10 1 13.03 5.61 11 -10 2 -3.48 4.76 11 10 2 8.70 4.82 11 -10 3 2.91 4.93 11 10 3 6.34 4.21 11 10 4 5.26 3.67 11 10 5 32.68 5.37 11 10 6 -2.21 3.12 -11 -10 -7 2.66 2.62 11 10 7 4.37 2.69 11 -11 -14 -4.81 3.19 -11 -11 14 7.33 2.79 11 -11 -13 9.51 3.18 -11 -11 13 17.28 3.79 11 -11 -12 5.13 3.70 -11 -11 12 7.55 3.44 11 -11 -11 13.58 4.95 -11 -11 11 11.58 4.53 11 -11 -10 0.43 3.91 11 -11 -9 25.34 5.93 11 -11 -8 4.41 4.68 11 -11 -7 18.58 6.12 11 -11 -7 25.21 5.59 11 -11 -6 22.16 5.73 11 -11 -6 27.43 5.64 11 -11 -5 41.00 7.24 11 -11 -5 28.43 6.28 11 -11 -4 9.12 4.89 11 -11 -4 13.75 5.51 11 11 -4 18.95 5.92 11 -11 -3 5.48 4.52 11 11 -3 -2.95 4.75 11 -11 -3 3.32 4.13 11 11 -3 3.35 4.56 11 11 -2 12.26 4.38 11 -11 -2 23.28 5.78 11 11 -2 16.55 4.95 11 11 -1 12.01 4.81 11 -11 -1 12.73 6.19 11 11 -1 26.26 6.86 11 11 0 25.66 6.29 11 -11 0 22.72 5.77 11 11 0 22.87 6.66 11 11 1 19.50 5.22 11 -11 1 30.18 6.55 11 11 1 20.96 5.82 11 -11 2 19.14 5.31 11 11 2 45.63 6.95 11 11 3 5.50 4.06 11 11 4 18.04 4.58 11 11 5 24.78 4.94 11 11 6 3.56 2.77 -11 -11 -7 11.63 3.21 11 11 7 5.51 2.15 11 -12 -14 0.81 2.31 11 -12 -13 3.17 2.66 -11 -12 13 0.46 2.74 11 -12 -12 2.20 2.94 -11 -12 12 4.06 3.47 11 -12 -11 8.56 4.37 -11 -12 11 -3.33 3.27 11 -12 -10 8.69 4.09 -11 -12 10 10.09 4.72 11 -12 -9 7.10 4.31 11 -12 -8 71.43 8.61 11 -12 -7 3.10 4.81 11 -12 -6 3.56 4.37 11 -12 -6 -1.11 3.59 11 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9.26 11 -13 -2 60.92 7.99 11 13 -2 60.37 8.50 11 13 -1 3.36 4.08 11 -13 -1 5.94 4.09 11 13 -1 1.34 4.36 11 13 0 14.63 5.25 11 -13 0 11.25 4.72 11 13 0 19.57 5.62 11 13 1 3.27 4.48 11 -13 1 -1.18 4.51 11 13 1 7.79 5.08 11 13 2 15.10 5.49 11 13 2 15.13 4.87 11 13 3 34.83 5.91 11 13 4 -0.24 2.96 11 13 5 43.29 5.38 11 13 6 22.45 3.57 -11 -14 13 -2.46 2.83 11 -14 -12 58.71 5.66 -11 -14 12 64.28 6.23 11 -14 -11 5.11 3.11 -11 -14 11 17.06 4.38 11 -14 -10 11.44 3.68 -11 -14 10 11.78 4.18 11 -14 -9 59.29 6.92 -11 -14 9 55.94 6.69 11 -14 -8 11.76 4.52 -11 -14 8 3.70 3.27 11 -14 -7 42.12 6.30 11 -14 -6 0.81 3.60 11 -14 -5 22.85 5.24 11 -14 -4 22.74 5.76 11 14 -4 17.75 4.77 11 -14 -4 18.02 4.76 11 14 -4 20.79 6.03 11 14 -3 49.22 7.60 11 -14 -3 44.66 6.58 11 14 -3 44.15 7.85 11 14 -2 14.99 6.17 11 -14 -2 8.37 4.25 11 14 -2 10.35 4.84 11 14 -1 13.28 5.19 11 -14 -1 5.81 3.85 11 14 -1 -2.08 3.91 11 14 0 12.14 4.93 11 -14 0 6.06 4.03 11 14 0 10.72 4.92 11 14 1 35.60 7.01 11 -14 1 24.49 5.75 11 14 1 25.10 5.48 11 14 2 0.88 3.63 11 14 2 -2.46 3.40 11 14 3 43.47 5.69 11 14 4 2.38 3.09 11 14 5 11.39 3.18 -11 -14 -6 12.73 3.23 -11 -15 12 5.46 2.84 -11 -15 11 6.36 3.20 11 -15 -10 29.77 4.61 -11 -15 10 30.85 5.53 11 -15 -9 14.52 3.83 -11 -15 9 12.73 4.19 11 -15 -8 24.10 4.93 -11 -15 8 18.39 4.83 11 -15 -7 47.25 6.43 -11 -15 7 29.67 5.50 11 -15 -6 13.74 4.37 11 -15 -5 36.86 6.03 11 15 -5 22.99 5.82 11 15 -4 16.83 4.42 11 15 -4 17.87 5.04 11 15 -3 10.54 4.68 11 -15 -3 11.67 4.15 11 15 -3 13.68 5.21 11 15 -2 0.81 4.07 11 -15 -2 4.66 3.23 11 15 -2 2.61 3.91 11 15 -1 20.25 5.48 11 -15 -1 31.03 5.80 11 15 -1 25.28 5.58 11 15 0 -2.78 3.88 11 -15 0 3.49 3.78 11 15 0 5.06 4.15 11 15 1 0.90 3.72 11 15 1 9.93 4.30 11 15 2 11.77 4.21 11 15 2 23.88 5.24 11 15 3 19.32 4.61 11 15 4 9.90 3.08 11 15 5 10.48 2.86 -11 -16 12 -1.48 2.21 -11 -16 11 1.86 2.71 -11 -16 10 55.30 6.07 -11 -16 9 2.75 2.89 -11 -16 8 5.65 3.65 -11 -16 7 9.89 3.87 -11 -16 6 10.78 4.02 11 16 -5 12.22 3.79 11 16 -5 15.95 5.15 11 16 -4 26.05 5.66 11 16 -4 27.71 5.95 11 16 -3 28.18 6.16 11 16 -3 31.19 5.96 11 16 -2 7.79 4.70 11 16 -2 0.85 3.85 11 16 -1 2.75 4.03 11 -16 -1 2.58 3.95 11 16 -1 7.30 3.94 11 16 0 11.17 4.57 11 16 0 8.44 4.01 11 16 1 10.46 4.49 11 16 1 18.10 4.48 11 16 2 50.42 6.65 11 16 2 63.54 6.44 11 16 3 9.96 3.02 11 16 4 18.27 3.70 -11 -17 11 6.59 2.72 -11 -17 10 21.86 4.26 -11 -17 9 5.58 3.14 -11 -17 8 20.11 4.03 -11 -17 7 9.29 3.54 11 17 -6 24.32 5.53 11 17 -5 84.70 8.36 11 17 -5 89.19 8.65 11 17 -4 109.93 9.69 11 17 -4 130.96 10.60 11 17 -3 17.98 4.97 11 17 -3 24.90 5.61 11 17 -2 43.28 6.66 11 17 -2 47.89 6.52 11 17 -1 12.98 4.46 11 17 -1 12.58 4.16 11 17 0 5.83 3.75 11 17 0 -1.43 3.09 11 17 1 28.96 5.87 11 17 1 44.96 5.68 11 17 2 22.12 5.17 11 17 2 18.10 4.01 11 17 3 23.49 3.73 -11 -18 11 23.23 3.55 -11 -18 10 5.46 2.90 -11 -18 9 7.61 3.20 -11 -18 8 13.67 3.74 -11 -18 7 39.84 5.46 11 18 -7 58.98 7.12 11 18 -6 35.98 5.54 11 18 -5 76.29 7.54 11 18 -5 76.20 8.03 11 18 -4 78.37 7.98 11 18 -4 80.07 7.84 11 18 -3 38.12 5.88 11 18 -3 41.49 6.03 11 18 -2 1.55 3.24 11 18 -2 4.07 3.19 11 18 -1 8.83 4.33 11 18 -1 11.66 3.75 11 18 0 6.35 3.77 11 18 0 0.37 2.81 11 18 1 12.19 4.03 11 18 1 7.19 3.01 11 18 2 3.01 2.27 -11 -19 10 1.17 2.09 -11 -19 9 1.40 2.30 11 19 -9 -2.16 2.94 -11 -19 8 14.85 3.53 11 19 -8 8.04 3.50 11 19 -7 31.30 5.07 11 19 -6 15.68 4.26 11 19 -5 34.20 5.29 11 19 -5 40.66 5.37 11 19 -4 0.68 3.27 11 19 -4 -2.09 3.26 11 19 -3 22.72 4.79 11 19 -3 19.68 4.48 11 19 -2 59.62 6.99 11 19 -2 54.96 6.00 11 19 -1 2.69 3.23 11 19 -1 3.86 3.03 11 19 0 22.61 4.80 11 19 0 17.33 3.58 11 19 1 3.76 3.21 11 19 1 4.18 2.67 11 20 -9 14.00 3.00 11 20 -8 0.90 2.28 11 20 -7 42.38 4.95 11 20 -6 13.09 3.34 11 20 -5 8.38 3.33 11 20 -5 5.72 2.96 11 20 -4 4.13 3.10 11 20 -4 5.76 2.76 11 20 -3 11.70 3.93 11 20 -3 1.98 2.61 11 20 -2 -0.60 2.97 11 20 -2 -3.22 2.77 11 20 -1 4.06 2.85 11 20 -1 2.59 2.30 11 20 0 10.90 3.82 11 20 0 5.98 2.39 11 20 1 10.15 3.43 11 21 -7 6.44 2.36 11 21 -6 8.45 3.03 11 21 -5 11.73 3.18 11 21 -5 9.64 2.91 11 21 -4 4.20 2.75 11 21 -4 6.20 2.48 11 21 -3 6.77 3.21 11 21 -3 3.11 2.24 11 21 -2 18.89 4.23 11 21 -2 20.20 3.07 11 21 -1 10.43 3.22 11 21 0 3.16 2.73 11 22 -2 -1.03 2.32 12 0 -15 14.67 3.31 12 0 -14 10.46 3.62 12 0 -13 12.62 4.63 12 0 -12 127.75 10.47 12 0 -11 1.07 3.90 12 0 -10 21.13 5.62 12 0 -9 0.94 4.90 12 0 -8 10.22 5.58 12 0 -7 55.08 8.07 12 0 -6 -6.09 4.65 12 0 -5 18.33 6.12 12 0 -4 25.58 6.82 12 0 -3 6.86 4.99 12 0 -2 273.24 17.07 12 0 -1 11.64 6.34 12 0 0 20.95 6.60 12 0 1 1.88 3.99 12 0 1 -0.56 2.91 12 0 2 7.51 4.14 12 0 2 10.68 3.51 12 0 3 4.05 3.80 12 0 3 -8.18 3.39 12 0 4 9.70 3.12 12 0 5 8.41 2.79 12 1 -15 16.58 3.61 12 -1 -15 8.81 3.09 12 1 -14 8.51 3.32 12 -1 -14 17.21 4.09 12 1 -13 12.30 4.32 12 -1 -13 3.22 3.58 12 1 -12 8.84 3.81 12 -1 -12 12.86 5.02 12 1 -11 31.01 6.04 12 -1 -11 39.48 7.56 12 1 -10 10.76 5.59 12 -1 -10 6.66 4.66 12 1 -9 -1.42 4.22 12 -1 -9 9.28 5.36 12 1 -8 24.85 6.34 12 -1 -8 -0.82 4.55 12 1 -7 34.42 7.30 12 -1 -7 28.13 6.94 12 1 -6 2.87 5.29 12 -1 -6 -2.32 4.71 12 1 -5 31.55 6.44 12 -1 -5 38.41 7.52 12 -1 -4 89.75 10.38 12 1 -4 104.44 11.40 12 1 -3 8.06 4.72 12 -1 -3 5.94 4.86 12 1 -3 4.46 3.50 12 -1 -2 12.88 6.35 12 1 -2 13.90 6.00 12 1 -2 17.02 4.79 12 -1 -1 14.92 6.30 12 1 -1 13.49 4.58 12 1 -1 12.73 3.45 12 -1 0 32.95 7.01 12 1 0 37.05 6.87 12 1 0 33.00 5.41 12 -1 1 3.37 4.47 12 1 1 6.21 4.28 12 1 1 3.10 3.27 12 -1 2 53.05 7.12 12 1 2 45.89 6.90 12 1 2 62.08 6.61 12 1 3 3.92 4.04 12 -1 3 11.90 4.51 12 1 3 1.81 2.93 12 1 4 139.78 8.88 12 1 5 16.07 3.62 12 -2 -15 -1.33 2.52 12 2 -14 29.94 4.74 12 -2 -14 23.56 4.44 12 2 -13 11.78 4.05 12 -2 -13 -3.78 3.98 12 2 -12 14.26 4.78 12 -2 -12 13.88 5.22 12 2 -11 14.80 4.59 12 -2 -11 15.03 5.33 12 2 -10 6.69 4.24 12 -2 -10 5.34 4.58 12 2 -9 16.42 5.48 12 -2 -9 29.15 7.11 12 2 -8 36.90 6.95 12 -2 -8 35.59 7.00 12 2 -7 24.94 6.20 12 -2 -7 14.23 5.16 12 2 -7 22.79 5.10 12 2 -6 47.94 7.32 12 -2 -6 36.13 7.64 12 2 -6 46.51 6.94 12 2 -5 126.64 10.55 12 2 -5 116.93 11.14 12 -2 -5 121.09 11.89 12 2 -4 198.18 12.98 12 2 -4 174.58 13.20 12 -2 -4 171.38 13.98 12 2 -3 6.24 4.55 12 -2 -3 7.30 4.74 12 -2 -3 0.59 5.53 12 2 -3 4.28 3.56 12 -2 -2 8.82 5.93 12 2 -2 17.09 6.08 12 2 -2 17.46 4.99 12 -2 -1 21.73 6.59 12 2 -1 15.50 5.64 12 2 -1 16.74 4.75 12 -2 0 43.74 7.76 12 2 0 32.50 6.54 12 2 0 44.27 6.64 12 -2 1 -0.79 4.91 12 2 1 6.45 4.33 12 -2 2 25.65 5.84 12 2 2 15.64 4.17 12 2 2 14.17 4.09 12 2 3 3.63 3.53 12 -2 3 3.72 4.35 12 2 3 0.53 2.98 12 2 4 11.18 3.45 12 2 5 11.75 3.47 12 2 6 11.79 2.82 12 -3 -15 -1.24 2.57 12 3 -14 23.45 4.28 12 -3 -14 22.69 4.74 12 3 -13 0.12 3.31 12 -3 -13 8.58 4.06 12 3 -12 6.51 3.99 12 -3 -12 5.06 4.66 12 3 -11 4.27 3.64 12 -3 -11 9.78 5.04 12 3 -10 69.69 8.30 12 -3 -10 51.57 7.47 12 3 -9 35.41 6.69 12 -3 -9 33.06 7.26 12 3 -8 87.75 9.74 12 -3 -8 71.36 9.40 12 3 -7 -0.18 3.89 12 -3 -7 -0.37 5.01 12 3 -6 5.96 4.06 12 -3 -6 4.74 5.07 12 3 -6 4.06 3.58 12 3 -5 13.95 5.39 12 -3 -5 13.71 5.39 12 3 -5 12.49 4.55 12 3 -4 66.26 8.38 12 -3 -4 77.79 10.25 12 3 -4 62.19 7.86 12 -3 -3 64.56 8.61 12 -3 -3 71.38 9.57 12 3 -3 64.56 7.85 12 -3 -2 152.77 13.15 12 3 -2 137.13 12.01 12 3 -2 146.78 11.40 12 3 -1 86.76 9.72 12 3 -1 104.81 9.54 12 -3 0 3.33 4.82 12 3 0 -0.25 3.85 12 3 0 1.13 3.58 12 -3 1 46.64 7.48 12 3 1 31.02 5.56 12 3 1 30.42 5.28 12 -3 2 14.27 4.60 12 3 2 9.29 3.38 12 3 2 14.45 4.47 12 -3 3 -1.52 3.60 12 3 3 -0.34 2.99 12 3 4 25.99 4.34 12 3 5 0.61 2.60 12 3 6 22.11 3.47 12 -4 -15 2.52 2.73 12 4 -14 9.04 3.18 12 -4 -14 9.75 3.70 12 4 -13 15.02 3.67 12 -4 -13 6.58 3.42 12 4 -12 3.91 3.22 12 -4 -12 -2.08 3.90 12 4 -11 12.22 4.21 12 -4 -11 18.96 5.33 12 4 -10 8.56 4.43 12 -4 -10 17.21 5.82 12 4 -9 0.39 3.89 12 -4 -9 1.10 4.78 12 4 -8 65.20 8.31 12 -4 -8 60.55 9.10 12 4 -7 19.86 5.32 12 -4 -7 8.00 5.29 12 4 -6 55.24 7.78 12 -4 -6 64.64 9.20 12 4 -6 77.81 8.78 12 4 -5 86.45 8.93 12 -4 -5 75.96 9.77 12 4 -5 68.18 8.34 12 4 -4 8.02 4.03 12 -4 -4 10.22 5.40 12 4 -4 3.37 4.08 12 -4 -3 44.73 7.75 12 -4 -3 54.86 10.22 12 4 -3 35.43 6.44 12 -4 -2 6.83 4.68 12 4 -2 3.00 4.47 12 4 -2 1.15 3.82 12 -4 -1 9.78 5.66 12 4 -1 -0.66 3.99 12 4 -1 12.42 4.98 12 -4 0 17.88 5.97 12 4 0 10.86 5.06 12 4 0 9.25 3.67 12 -4 1 31.19 6.41 12 4 1 26.06 5.38 12 4 1 28.95 5.57 12 -4 2 5.95 4.98 12 4 2 10.63 4.07 12 -4 3 8.93 4.12 12 4 3 1.49 3.11 12 4 4 25.78 4.57 12 4 5 -2.58 2.72 12 4 6 24.46 3.34 12 -5 -15 8.86 2.90 12 -5 -14 72.03 6.77 12 -5 -13 13.72 4.22 12 5 -12 24.00 4.72 12 -5 -12 9.85 4.13 12 5 -11 -5.03 3.53 12 -5 -11 -2.07 4.23 12 5 -10 40.87 6.05 12 -5 -10 36.50 6.86 12 5 -9 8.59 4.29 12 -5 -9 12.98 5.02 12 5 -8 33.59 6.16 12 -5 -8 43.02 8.04 12 5 -7 21.53 4.84 12 -5 -7 9.98 5.40 12 5 -6 4.17 4.09 12 -5 -6 2.52 4.72 12 5 -6 0.48 3.87 12 5 -5 44.37 6.62 12 -5 -5 38.95 7.93 12 5 -5 50.19 7.70 12 5 -4 11.43 4.98 12 -5 -4 18.05 5.74 12 -5 -4 17.50 6.21 12 5 -4 14.91 5.06 12 -5 -3 50.17 8.42 12 -5 -3 54.11 8.61 12 -5 -2 4.67 5.24 12 5 -2 -9.25 4.87 12 5 -2 0.99 3.82 12 -5 -1 18.48 6.11 12 5 -1 10.18 4.47 12 5 -1 26.43 6.10 12 -5 0 17.00 5.69 12 5 0 15.30 4.68 12 5 0 12.52 4.95 12 -5 1 2.43 4.49 12 5 1 1.44 3.28 12 -5 2 4.96 4.52 12 5 2 5.08 3.67 12 -5 3 56.54 7.61 12 5 3 51.32 6.40 12 5 4 91.51 7.71 12 5 5 14.57 3.71 12 5 6 15.77 3.04 12 -6 -15 15.01 3.22 12 -6 -14 19.86 3.86 12 -6 -13 13.04 4.11 12 -6 -12 3.68 3.71 12 -6 -11 8.73 4.45 12 -6 -10 7.02 4.86 12 -6 -9 41.50 7.28 12 -6 -8 0.21 4.85 12 -6 -7 6.67 4.95 12 -6 -6 20.34 6.62 12 6 -6 33.01 6.67 12 -6 -5 57.57 8.71 12 6 -5 39.11 6.88 12 -6 -4 28.23 6.90 12 -6 -4 21.42 6.26 12 6 -4 30.01 6.00 12 -6 -3 16.09 5.41 12 -6 -3 21.91 6.48 12 6 -3 12.75 4.97 12 -6 -2 90.23 10.45 12 6 -2 64.00 8.27 12 6 -2 76.05 8.66 12 -6 -1 3.92 5.30 12 6 -1 -8.19 4.27 12 6 -1 -3.66 3.95 12 -6 0 11.78 5.45 12 6 0 9.04 4.20 12 -6 1 8.57 5.05 12 6 1 8.89 4.37 12 -6 2 0.05 4.36 12 6 2 -0.59 3.45 12 -6 3 -3.10 4.30 12 6 3 5.73 3.71 12 6 4 8.22 3.38 12 6 5 30.68 4.37 12 6 6 21.03 3.31 12 -7 -14 7.75 3.50 12 -7 -13 2.55 3.28 12 -7 -12 3.87 3.49 12 -7 -11 9.42 4.87 12 -7 -10 1.70 4.50 12 -7 -9 25.48 6.68 12 -7 -8 2.34 4.69 12 -7 -7 20.81 6.15 12 -7 -6 6.92 4.71 12 7 -6 5.62 4.29 12 -7 -5 91.77 10.09 12 -7 -5 66.65 8.77 12 7 -5 86.17 9.52 12 -7 -4 87.86 9.74 12 -7 -4 81.39 9.76 12 7 -4 67.93 8.70 12 -7 -3 6.82 4.60 12 -7 -3 6.22 5.49 12 7 -3 4.11 3.88 12 -7 -2 41.25 8.65 12 7 -2 33.24 5.86 12 7 -2 28.56 5.93 12 -7 -1 3.61 4.94 12 7 -1 5.08 4.11 12 -7 0 11.67 5.19 12 7 0 3.90 3.78 12 -7 1 29.22 6.31 12 7 1 33.17 5.78 12 -7 2 11.21 4.83 12 7 2 9.41 4.18 12 -7 3 0.13 4.55 12 7 3 0.38 3.22 12 7 4 34.02 4.98 12 7 5 42.57 4.92 12 7 6 15.93 3.05 12 -8 -14 -1.81 2.32 12 -8 -13 -2.29 3.18 12 -8 -12 11.07 4.12 12 -8 -11 -4.31 4.47 12 -8 -10 5.02 4.64 12 -8 -9 -0.98 4.10 12 -8 -8 5.15 5.07 12 -8 -7 34.31 6.52 12 -8 -6 7.75 6.04 12 -8 -6 11.59 5.35 12 8 -6 2.47 4.18 12 -8 -5 25.96 7.08 12 -8 -5 22.55 5.94 12 8 -5 11.95 4.92 12 -8 -4 95.15 10.58 12 -8 -4 90.20 9.87 12 -8 -3 53.98 8.06 12 -8 -3 41.55 7.54 12 8 -3 32.88 6.60 12 -8 -2 180.34 13.53 12 8 -2 127.20 11.19 12 -8 -1 31.79 6.66 12 8 -1 16.75 4.83 12 -8 0 2.86 4.08 12 8 0 -0.47 3.52 12 -8 1 13.99 5.25 12 8 1 10.46 4.03 12 -8 2 14.09 5.03 12 8 2 13.91 4.20 12 8 3 2.89 2.87 12 8 4 20.20 4.12 12 8 5 19.85 3.66 12 -9 -14 7.53 2.91 12 -9 -13 7.09 3.31 12 -9 -12 9.20 4.14 12 -9 -11 5.92 3.86 12 -9 -10 34.03 6.17 12 -9 -9 11.00 4.42 12 -9 -9 5.68 3.54 12 -9 -8 13.56 4.85 12 -9 -8 11.31 4.15 12 -9 -7 139.93 10.94 12 -9 -7 139.54 11.60 12 -9 -6 3.28 4.14 12 -9 -6 7.68 4.17 12 9 -6 4.03 3.94 12 -9 -5 7.06 4.10 12 -9 -5 6.77 4.43 12 9 -5 0.43 4.08 12 -9 -4 9.02 4.64 12 -9 -4 9.22 5.17 12 9 -4 1.98 3.80 12 -9 -3 9.19 4.73 12 9 -3 12.58 4.82 12 -9 -2 33.62 6.34 12 9 -2 33.64 6.85 12 -9 -1 40.08 7.29 12 9 -1 34.70 6.43 12 -9 0 34.46 6.38 12 9 0 29.18 5.78 12 -9 1 17.15 4.80 12 9 1 7.96 3.96 12 -9 2 7.91 4.46 12 9 2 -1.23 3.19 12 9 3 31.50 5.20 12 9 4 3.86 2.68 12 9 5 2.84 2.37 12 -10 -13 2.47 2.50 12 -10 -12 7.44 3.78 12 -10 -11 7.25 3.74 12 -10 -10 19.93 5.10 12 -10 -9 39.18 6.44 12 -10 -8 31.85 6.14 12 -10 -8 37.78 5.84 12 -10 -7 4.58 4.10 12 -10 -7 -0.11 3.28 12 -10 -6 7.25 4.61 12 -10 -6 10.10 4.90 12 10 -6 11.27 4.84 12 -10 -5 4.28 4.02 12 -10 -5 0.13 4.08 12 10 -5 1.67 3.90 12 -10 -4 9.07 4.50 12 10 -4 5.83 4.31 12 -10 -3 54.36 7.84 12 10 -3 54.19 7.85 12 -10 -2 9.18 4.55 12 10 -2 13.18 5.19 12 -10 -1 29.91 6.01 12 10 -1 28.89 5.83 12 -10 0 32.70 6.28 12 10 0 24.05 5.39 12 -10 1 3.88 3.94 12 10 1 1.75 3.58 12 -10 2 16.53 5.45 12 10 2 10.22 3.98 12 10 3 14.06 3.82 12 10 4 0.56 2.43 12 10 5 12.90 3.00 12 -11 -13 12.05 3.24 12 -11 -12 5.51 3.08 12 -11 -11 14.58 3.51 12 -11 -10 79.34 7.97 12 -11 -9 6.27 3.88 12 -11 -8 25.27 5.18 12 -11 -7 -0.59 3.68 12 -11 -7 11.21 4.02 12 -11 -6 18.09 5.19 12 -11 -6 16.96 4.22 12 11 -6 19.51 5.58 12 -11 -5 11.26 4.89 12 -11 -5 13.12 4.81 12 11 -5 13.66 4.74 12 -11 -4 21.95 5.71 12 -11 -4 13.17 4.46 12 11 -4 16.60 4.79 12 -11 -3 13.85 4.94 12 11 -3 0.78 4.18 12 11 -2 1.65 3.10 12 -11 -2 10.21 4.58 12 11 -2 0.95 3.94 12 -11 -1 11.41 4.55 12 11 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13 -9 -2 1.73 3.19 13 9 -2 5.31 2.88 13 -9 -1 2.43 3.52 13 9 -1 1.96 2.94 13 -9 0 29.69 4.84 13 9 0 20.45 4.12 13 9 1 2.35 2.60 13 9 2 2.39 2.19 13 -10 -11 18.74 3.68 13 10 -11 18.29 3.38 13 -10 -10 2.15 2.75 13 10 -10 2.59 2.55 13 -10 -9 1.80 2.91 13 10 -9 3.86 2.85 13 -10 -8 16.55 3.59 13 10 -8 12.77 3.77 13 -10 -7 1.60 3.04 13 -10 -7 3.58 2.81 13 10 -7 2.70 3.23 13 -10 -6 5.75 3.90 13 -10 -6 6.86 3.25 13 10 -6 0.74 2.96 13 -10 -5 9.81 4.13 13 10 -5 2.66 3.07 13 -10 -4 19.48 4.50 13 10 -4 10.81 3.51 13 -10 -3 31.26 4.87 13 10 -3 28.92 5.11 13 -10 -2 26.12 4.57 13 10 -2 26.01 4.78 13 -10 -1 11.41 3.57 13 10 -1 17.87 4.19 13 -10 0 1.81 3.59 13 10 0 4.11 2.91 13 10 1 11.45 2.93 13 10 2 0.09 2.03 13 -11 -10 23.07 4.00 13 11 -10 15.12 3.41 13 -11 -9 14.31 3.49 13 11 -9 13.95 3.72 13 -11 -8 24.68 4.87 13 11 -8 16.65 4.04 13 -11 -7 16.61 4.75 13 -11 -7 10.44 2.93 13 11 -7 8.33 3.76 13 -11 -6 19.21 3.82 13 11 -6 13.94 4.05 13 -11 -5 2.13 2.83 13 11 -5 1.92 3.03 13 -11 -4 0.19 2.85 13 11 -4 5.11 3.80 13 -11 -3 2.88 2.98 13 11 -3 13.62 3.75 13 -11 -2 2.67 2.98 13 11 -2 1.56 3.06 13 -11 -1 -3.24 3.65 13 11 -1 4.31 3.13 13 11 0 31.43 4.60 13 11 1 36.04 4.44 13 12 -10 9.51 3.00 13 -12 -9 38.79 4.50 13 12 -9 25.66 4.29 13 -12 -8 10.43 3.32 13 12 -8 6.66 3.29 13 12 -7 8.28 3.55 13 -12 -6 4.78 2.60 13 12 -6 2.90 3.07 13 -12 -5 2.53 2.32 13 12 -5 2.90 2.89 13 -12 -4 16.94 3.70 13 12 -4 11.72 3.48 13 -12 -3 6.92 3.11 13 12 -3 6.59 2.96 13 -12 -2 4.28 3.13 13 12 -2 4.74 3.15 13 -12 -1 3.28 3.04 13 12 -1 1.77 2.56 13 12 0 19.26 3.47 13 12 1 5.16 2.47 13 13 -9 2.66 2.57 13 13 -8 5.81 2.67 13 13 -7 0.22 2.69 13 13 -6 -0.24 2.56 13 13 -5 21.45 4.27 13 -13 -4 23.99 3.69 13 13 -4 30.84 4.68 13 -13 -3 27.80 4.12 13 13 -3 16.31 3.38 13 13 -2 5.58 2.95 13 13 -1 7.38 2.63 13 13 0 3.58 2.15 13 14 -8 31.31 4.24 13 14 -7 8.60 3.44 13 14 -6 2.22 2.64 13 14 -5 8.46 3.15 13 14 -4 8.24 3.16 13 14 -3 8.36 2.92 13 14 -2 31.41 4.67 13 14 -1 12.44 2.82 13 15 -7 18.57 3.47 13 15 -6 14.90 3.24 13 15 -5 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-5 -6 14.36 3.68 14 5 -6 17.33 3.66 14 -5 -5 1.76 2.74 14 5 -5 1.56 2.87 14 -5 -4 -1.75 2.90 14 5 -4 6.96 3.21 14 -5 -3 7.86 3.58 14 5 -3 5.32 2.66 14 -5 -2 27.85 4.39 14 -5 -1 33.62 4.47 14 -6 -9 35.13 4.62 14 -6 -8 55.96 5.29 14 6 -8 45.16 5.12 14 -6 -7 23.68 4.05 14 6 -7 14.07 3.58 14 -6 -6 -1.08 2.68 14 6 -6 1.75 2.48 14 -6 -5 8.69 3.18 14 6 -5 7.86 2.89 14 -6 -4 18.49 4.05 14 6 -4 15.61 3.33 14 6 -4 21.26 3.59 14 -6 -3 28.21 4.41 14 6 -3 24.09 3.59 14 -6 -2 56.86 5.58 14 -6 -1 34.91 4.36 14 -7 -9 5.03 2.68 14 -7 -7 -0.49 2.70 14 7 -7 7.42 2.82 14 -7 -6 64.95 6.00 14 7 -6 50.49 4.91 14 7 -6 52.70 4.81 14 -7 -5 0.20 2.69 14 7 -5 6.08 2.66 14 -7 -4 8.32 3.06 14 7 -4 8.42 2.54 14 -7 -3 14.27 3.48 14 -7 -2 11.09 3.29 14 -7 -1 10.93 3.06 14 -8 -6 9.94 3.01 14 -8 -5 12.67 3.16 14 8 -5 6.58 2.35 14 -8 -4 -4.43 2.67 14 8 -4 4.46 2.27 14 -8 -3 11.67 3.23 14 -8 -2 10.42 3.05 14 -9 -4 15.09 3.20 0 0 0 0.00 0.00 TITL exp_2740 in P2(1)/m REM P2(1)/m (#11 in standard setting) CELL 1.54184 11.926828 27.781641 16.366307 90.0000 105.2719 90.0000 ZERR 5.00 0.000326 0.000913 0.000509 0.0000 0.0031 0.0000 LATT 1 SYMM -x, y+1/2,-z SFAC C H B N F UNIT 250.00 500.00 5.00 35.00 10.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 44907 _shelx_fab_file ; 1 33 0 2.19 -1.46 2 33 0 -0.56 2.90 0 32 0 -3.02 -4.16 1 32 0 0.42 -3.38 2 32 0 0.27 3.10 3 32 0 0.88 3.18 1 31 0 -6.51 2.58 2 31 0 -1.05 -5.16 3 31 0 -1.42 -2.74 4 31 0 -0.19 2.16 5 31 0 1.32 3.50 0 30 0 6.05 2.10 1 30 0 -1.53 2.72 2 30 0 -1.58 -4.68 3 30 0 -1.56 -6.17 6 30 0 -0.80 -1.26 1 29 0 11.13 -4.31 2 29 0 1.39 7.62 3 29 0 -0.63 2.23 4 29 0 -3.59 -0.94 7 29 0 -3.20 3.44 0 28 0 -8.89 -0.73 1 28 0 1.53 -6.32 2 28 0 2.22 2.26 3 28 0 4.18 3.24 4 28 0 10.17 -5.40 8 28 0 2.53 0.60 1 27 0 -16.42 8.00 2 27 0 -2.29 -9.86 3 27 0 -0.84 -2.17 4 27 0 4.65 -1.94 0 26 0 13.24 -6.90 1 26 0 3.29 3.83 2 26 0 0.85 -1.04 3 26 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6 17 0.92 -0.50 4 7 17 0.67 0.13 -10 8 17 -0.91 0.97 -10 9 17 -1.26 0.47 3 11 17 2.32 0.74 -9 12 17 -1.73 -1.42 -8 15 17 0.28 -1.18 1 15 17 -1.02 0.53 -7 16 17 0.26 -1.89 -2 16 17 -2.34 -0.25 -1 16 17 0.86 0.20 0 16 17 -0.09 0.41 -2 17 17 0.50 -1.44 -1 17 17 0.41 1.60 0 17 17 -0.28 -0.93 -5 18 17 -0.93 -0.97 -4 18 17 0.05 1.02 -3 18 17 1.61 -0.88 -2 18 17 1.32 -0.12 -1 18 17 0.06 0.03 -10 0 18 0.34 -0.04 3 0 18 0.43 -0.14 -10 1 18 -1.36 -0.83 3 1 18 0.04 0.19 -10 2 18 -0.13 -0.96 3 2 18 -0.08 -0.89 3 3 18 0.75 -0.56 -9 7 18 0.74 1.54 -9 8 18 2.14 -0.14 2 8 18 -0.01 -0.76 2 9 18 -0.59 -0.07 -8 11 18 1.39 -0.47 1 11 18 -0.46 1.10 0 12 18 -0.81 0.26 -7 13 18 0.98 0.48 -3 13 18 0.23 -0.72 -2 13 18 2.23 0.11 -1 13 18 -1.84 0.04 0 13 18 0.15 -0.98 -6 14 18 -2.05 -1.75 -5 14 18 1.63 -0.32 -4 14 18 -2.36 0.16 -3 14 18 0.86 0.92 -2 14 18 1.23 0.80 -1 14 18 -0.22 -1.03 -5 15 18 0.36 1.02 -4 15 18 -0.19 -0.94 -3 15 18 -0.67 1.51 -2 15 18 -1.34 -0.93 1 0 19 0.81 0.04 1 1 19 -0.88 -0.18 1 2 19 0.08 0.19 1 3 19 -0.26 -0.25 1 4 19 -0.14 -1.20 -8 5 19 -0.08 0.21 -8 6 19 0.74 -1.07 -7 8 19 -0.81 -1.78 0 8 19 0.31 1.01 -7 9 19 0.48 -0.46 -1 9 19 -0.03 0.05 -6 10 19 0.40 0.10 -5 10 19 -1.25 -0.23 -4 10 19 -0.19 0.93 -3 10 19 1.42 -1.36 -2 10 19 -0.02 1.83 -1 10 19 0.46 1.24 -5 11 19 0.05 1.85 -4 11 19 -0.56 -1.34 -3 11 19 -1.43 -0.51 -2 11 19 -1.08 0.37 -4 12 19 0.03 0.00 -3 12 19 -0.69 0.94 -6 0 20 1.88 -0.10 -2 0 20 -0.18 -0.07 -6 1 20 0.65 -0.85 -2 1 20 1.20 -1.09 -6 2 20 -2.42 -0.32 -2 2 20 -0.29 1.28 -6 3 20 -0.42 0.08 -5 3 20 -0.28 0.20 -2 3 20 -1.64 0.71 -5 4 20 -0.94 2.14 -4 4 20 0.05 -1.05 -3 4 20 0.69 -0.68 -2 4 20 -0.69 -1.43 -5 5 20 -0.46 -0.70 -4 5 20 -0.33 0.46 -3 5 20 0.27 1.88 -4 6 20 -0.14 0.80 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 81119) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 -0.564 0.240 0.755 554 145 ' ' 2 0.564 0.740 0.245 554 145 ' ' _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL exp_2740 P 1 21 1 R = 0.24 CELL 11.9268 27.7816 16.3663 90.00 105.27 90.00 SPGR P21 # Solvent Accessible Volume = 1110 # Electrons Found in S.A.V. = 291 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.395 0.264 0.418 ! 19.00 eA-3 C102 0.839 0.775 0.491 ! 18.18 eA-3 C103 0.265 0.710 0.138 ! 16.07 eA-3 C104 0.761 0.240 0.062 ! 13.33 eA-3 C105 0.531 0.677 0.974 ! 10.68 eA-3 C106 0.951 0.920 0.575 ! 8.74 eA-3 C107 0.308 0.259 0.834 ! 7.54 eA-3 C108 0.513 0.562 0.968 ! 5.55 eA-3 C109 0.753 0.759 0.099 ! 5.38 eA-3 C110 0.731 0.807 0.608 ! 4.65 eA-3 C111 0.237 0.316 0.463 ! 4.42 eA-3 C112 0.074 0.727 0.018 ! 3.82 eA-3 C113 0.374 0.224 0.914 ! 3.37 eA-3 C114 0.549 0.716 0.056 ! 3.28 eA-3 C115 0.192 0.680 0.067 ! 3.17 eA-3 C116 0.808 0.179 0.942 ! 3.16 eA-3 C117 0.170 0.695 0.969 ! 2.54 eA-3 C118 0.367 0.662 0.949 ! 2.46 eA-3 C119 0.715 0.180 0.120 ! 2.07 eA-3 Q120 0.421 0.703 0.892 ! 1.80 eA-3 C121 0.358 0.301 0.330 ! 1.63 eA-3 C122 0.674 0.736 0.553 ! 1.44 eA-3 C123 0.315 0.320 0.336 ! 1.41 eA-3 Q124 0.658 0.179 0.861 ! 1.27 eA-3 Q125 0.608 0.720 0.599 ! 1.25 eA-3 C126 0.545 0.193 0.017 ! 1.22 eA-3 Q127 0.310 0.676 0.186 ! 1.21 eA-3 C128 0.818 0.736 0.331 ! 1.16 eA-3 Q129 0.620 0.500 0.966 ! 1.15 eA-3 Q130 0.406 0.334 0.361 ! 1.10 eA-3 Q131 0.295 0.624 0.968 ! 1.07 eA-3 Q132 0.423 0.234 0.460 ! 1.05 eA-3 C133 0.285 0.220 0.818 ! 1.04 eA-3 C134 0.298 0.272 0.433 ! 1.04 eA-3 Q135 0.820 0.198 0.851 ! 1.03 eA-3 Q136 0.456 0.076 0.078 ! 1.02 eA-3 Q137 0.719 0.163 0.874 ! 1.02 eA-3 C138 0.722 0.763 0.519 ! 1.01 eA-3 Q139 0.824 0.727 0.523 ! 0.99 eA-3 Q140 0.970 0.929 0.635 ! 0.97 eA-3 Q141 0.752 0.278 0.069 ! 0.95 eA-3 C142 0.300 0.668 0.007 ! 0.95 eA-3 Q143 0.955 0.214 0.895 ! 0.93 eA-3 Q144 0.157 0.416 0.465 ! 0.92 eA-3 Q145 0.795 0.845 0.495 ! 0.89 eA-3 Q146 0.343 0.335 0.402 ! 0.89 eA-3 C147 0.658 0.774 0.106 ! 0.88 eA-3 Q148 0.175 0.250 0.107 ! 0.87 eA-3 Q149 0.481 0.031 0.124 ! 0.86 eA-3 Q150 0.032 0.199 0.791 ! 0.86 eA-3 Q151 0.016 0.504 0.519 ! 0.85 eA-3 Q152 0.703 0.134 0.970 ! 0.85 eA-3 Q153 0.905 0.736 0.512 ! 0.84 eA-3 Q154 0.784 0.225 0.763 ! 0.84 eA-3 C155 0.815 0.206 0.090 ! 0.83 eA-3 Q156 0.687 0.766 0.758 ! 0.83 eA-3 Q157 0.405 0.293 0.854 ! 0.83 eA-3 Q158 0.153 0.318 0.561 ! 0.82 eA-3 C159 0.702 0.218 0.973 ! 0.82 eA-3 Q160 0.078 0.758 0.076 ! 0.82 eA-3 Q161 0.823 0.229 0.846 ! 0.81 eA-3 Q162 0.982 0.861 0.544 ! 0.80 eA-3 Q163 0.091 0.394 0.362 ! 0.80 eA-3 C164 0.062 0.299 0.438 ! 0.80 eA-3 Q165 0.465 0.687 0.082 ! 0.78 eA-3 C166 0.827 0.226 0.903 ! 0.78 eA-3 Q167 0.330 0.805 0.921 ! 0.77 eA-3 Q168 0.733 0.847 0.605 ! 0.77 eA-3 C169 0.236 0.740 0.031 ! 0.77 eA-3 Q170 0.111 0.726 0.119 ! 0.77 eA-3 Q171 0.764 0.708 0.065 ! 0.76 eA-3 Q172 0.636 0.766 0.987 ! 0.76 eA-3 Q173 0.985 0.493 0.394 ! 0.75 eA-3 Q174 0.015 0.213 0.640 ! 0.75 eA-3 Q175 0.325 0.286 0.938 ! 0.75 eA-3 Q176 0.119 0.226 0.772 ! 0.75 eA-3 Q177 0.950 0.274 0.968 ! 0.74 eA-3 Q178 0.215 0.317 0.298 ! 0.73 eA-3 C179 0.675 0.753 0.035 ! 0.73 eA-3 Q180 0.105 0.372 0.451 ! 0.73 eA-3 Q181 0.265 0.286 0.661 ! 0.73 eA-3 Q182 0.365 0.407 0.166 ! 0.72 eA-3 Q183 0.286 0.189 0.962 ! 0.72 eA-3 Q184 0.393 0.804 0.118 ! 0.72 eA-3 Q185 0.077 0.274 0.325 ! 0.70 eA-3 Q186 0.890 0.147 0.024 ! 0.70 eA-3 Q187 0.725 0.246 0.126 ! 0.70 eA-3 Q188 0.688 0.880 0.050 ! 0.70 eA-3 Q189 0.448 0.969 0.059 ! 0.69 eA-3 C190 0.785 0.805 0.473 ! 0.69 eA-3 Q191 0.748 0.720 0.984 ! 0.69 eA-3 Q192 0.764 0.727 0.186 ! 0.69 eA-3 Q193 0.446 0.761 0.358 ! 0.69 eA-3 Q194 0.907 0.836 0.512 ! 0.69 eA-3 Q195 0.674 0.734 0.953 ! 0.69 eA-3 Q196 0.912 0.005 0.455 ! 0.68 eA-3 Q197 0.776 0.772 0.354 ! 0.68 eA-3 Q198 0.264 0.275 0.591 ! 0.68 eA-3 Q199 0.262 0.747 0.565 ! 0.68 eA-3 ) ; _shelx_fab_checksum 73459 _platon_squeeze_void_probe_radius 1.20 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.484 _oxdiff_exptl_absorpt_empirical_full_min 0.822 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group F1 F 0.2560(3) 0.46893(17) 0.4488(2) 0.0311(9) Uani 1 1 d . . . . . F2 F 0.3834(3) 0.40685(15) 0.4740(2) 0.0305(9) Uani 1 1 d . . . . . N1 N 0.4437(4) 0.4812(2) 0.5487(3) 0.0244(12) Uani 1 1 d . . . . . N2 N 0.2505(5) 0.4217(2) 0.6053(4) 0.0281(13) Uani 1 1 d . . . . . H2 H 0.216182 0.428958 0.552315 0.034 Uiso 1 1 calc R . . . . N3 N 0.0085(4) 0.3711(2) 0.5684(4) 0.0269(12) Uani 1 1 d . . . . . N4 N -0.1973(5) 0.3625(2) 0.3924(3) 0.0260(13) Uani 1 1 d . . . . . H4 H -0.122259 0.360480 0.396812 0.031 Uiso 1 1 calc R . . . . N5 N -0.0560(4) 0.3783(2) 0.2620(3) 0.0230(12) Uani 1 1 d . . . . . N6 N 0.1993(4) 0.4158(2) 0.2903(3) 0.0216(12) Uani 1 1 d . . . . . H6 H 0.177198 0.426533 0.334203 0.026 Uiso 1 1 calc R . . . . N7 N 0.4239(4) 0.4743(2) 0.3944(3) 0.0252(12) Uani 1 1 d . . . . . C1 C 0.5777(5) 0.5235(3) 0.4837(5) 0.0276(15) Uani 1 1 d . . . . . C2 C 0.5214(6) 0.5041(3) 0.4051(5) 0.0272(15) Uani 1 1 d . . . . . C3 C 0.5490(5) 0.5085(3) 0.3284(4) 0.0244(14) Uani 1 1 d . . . . . H3 H 0.610776 0.527032 0.318205 0.029 Uiso 1 1 calc R . . . . C4 C 0.4700(5) 0.4807(3) 0.2686(4) 0.0254(14) Uani 1 1 d . . . . . H4A H 0.468005 0.476579 0.210616 0.030 Uiso 1 1 calc R . . . . C5 C 0.3938(5) 0.4600(3) 0.3116(4) 0.0215(13) Uani 1 1 d . . . . . C6 C 0.3029(5) 0.4264(3) 0.2715(4) 0.0238(14) Uani 1 1 d . . . . . C7 C 0.3079(5) 0.4011(3) 0.1999(4) 0.0263(15) Uani 1 1 d . . . . . H7 H 0.370214 0.401156 0.173831 0.032 Uiso 1 1 calc R . . . . C8 C 0.2040(6) 0.3752(3) 0.1730(4) 0.0274(16) Uani 1 1 d . . . . . H8 H 0.183548 0.354461 0.125296 0.033 Uiso 1 1 calc R . . . . C9 C 0.1361(5) 0.3851(3) 0.2279(4) 0.0255(15) Uani 1 1 d . . . . . C10 C 0.0158(5) 0.3723(3) 0.2118(4) 0.0252(14) Uani 1 1 d . . . . . C11 C -0.0487(5) 0.3569(3) 0.1275(4) 0.0237(14) Uani 1 1 d . . . . . H11 H -0.016552 0.349066 0.081906 0.028 Uiso 1 1 calc R . . . . C12 C -0.1638(5) 0.3559(3) 0.1259(4) 0.0261(16) Uani 1 1 d . . . . . H12 H -0.227652 0.348063 0.079301 0.031 Uiso 1 1 calc R . . . . C13 C -0.1671(6) 0.3692(3) 0.2106(4) 0.0263(14) Uani 1 1 d . . . . . C14 C -0.2689(5) 0.3706(3) 0.2344(4) 0.0249(14) Uani 1 1 d . . . . . C15 C -0.2840(6) 0.3720(3) 0.3172(4) 0.0285(15) Uani 1 1 d . . . . . C16 C -0.3893(5) 0.3748(3) 0.3400(4) 0.0246(14) Uani 1 1 d . . . . . H16 H -0.463071 0.381902 0.302690 0.030 Uiso 1 1 calc R . . . . C17 C -0.3679(6) 0.3654(3) 0.4255(4) 0.0262(15) Uani 1 1 d . . . . . H17 H -0.424464 0.364832 0.456903 0.031 Uiso 1 1 calc R . . . . C18 C -0.2491(6) 0.3569(3) 0.4581(4) 0.0240(14) Uani 1 1 d . . . . . C19 C -0.1929(6) 0.3403(2) 0.5424(4) 0.0257(14) Uani 1 1 d . . . . . C20 C -0.0811(6) 0.3426(2) 0.5865(4) 0.0242(14) Uani 1 1 d . . . . . C21 C -0.0356(7) 0.3178(3) 0.6662(5) 0.0355(17) Uani 1 1 d . . . . . H21 H -0.077360 0.296701 0.693066 0.043 Uiso 1 1 calc R . . . . C22 C 0.0762(6) 0.3302(3) 0.6949(5) 0.0362(18) Uani 1 1 d . . . . . H22 H 0.129814 0.319051 0.745122 0.043 Uiso 1 1 calc R . . . . C23 C 0.0990(6) 0.3639(3) 0.6341(5) 0.0312(16) Uani 1 1 d . . . . . C24 C 0.2100(6) 0.3892(3) 0.6542(5) 0.0341(17) Uani 1 1 d . . . . . C25 C 0.2891(7) 0.3883(4) 0.7331(5) 0.057(3) Uani 1 1 d . . . . . H25 H 0.282817 0.369093 0.779710 0.068 Uiso 1 1 calc R . . . . C26 C 0.3784(8) 0.4198(4) 0.7329(5) 0.057(3) Uani 1 1 d . . . . . H26 H 0.444465 0.425963 0.778860 0.069 Uiso 1 1 calc R . . . . C27 C 0.3540(6) 0.4410(3) 0.6529(4) 0.0322(17) Uani 1 1 d . . . . . C28 C 0.4302(5) 0.4747(3) 0.6278(4) 0.0303(16) Uani 1 1 d . . . . . C29 C 0.5150(6) 0.5032(3) 0.6848(5) 0.0357(18) Uani 1 1 d . . . . . H29 H 0.524055 0.505880 0.744057 0.043 Uiso 1 1 calc R . . . . C30 C 0.5807(6) 0.5257(3) 0.6407(5) 0.0310(16) Uani 1 1 d . . . . . H30 H 0.644732 0.546470 0.662980 0.037 Uiso 1 1 calc R . . . . C31 C 0.5354(6) 0.5124(3) 0.5543(4) 0.0281(15) Uani 1 1 d . . . . . C32 C 0.6825(6) 0.5546(3) 0.4923(4) 0.0275(15) Uani 1 1 d . . . . . C33 C 0.6736(6) 0.6046(3) 0.4992(4) 0.0263(15) Uani 1 1 d . . . . . C34 C 0.7717(5) 0.6331(3) 0.5027(4) 0.0244(14) Uani 1 1 d . . . . . H34 H 0.766837 0.667002 0.507999 0.029 Uiso 1 1 calc R . . . . C35 C 0.8771(6) 0.6120(3) 0.4983(4) 0.0318(17) Uani 1 1 d . . . . . C36 C 0.8827(6) 0.5634(3) 0.4907(4) 0.0295(16) Uani 1 1 d . . . . . H36 H 0.953718 0.549437 0.486601 0.035 Uiso 1 1 calc R . . . . C37 C 0.8024(6) 0.4804(3) 0.4823(5) 0.0324(16) Uani 1 1 d . . . . . H37A H 0.771302 0.470224 0.423347 0.049 Uiso 1 1 calc GR . . . . H37B H 0.759321 0.464239 0.517934 0.049 Uiso 1 1 calc GR . . . . H37C H 0.884744 0.471644 0.501650 0.049 Uiso 1 1 calc GR . . . . C38 C 0.5602(6) 0.6288(3) 0.4989(4) 0.0252(15) Uani 1 1 d . . . . . H38A H 0.572530 0.663607 0.506153 0.038 Uiso 1 1 calc GR . . . . H38B H 0.531443 0.616129 0.545507 0.038 Uiso 1 1 calc GR . . . . H38C H 0.502903 0.622473 0.444934 0.038 Uiso 1 1 calc GR . . . . C39 C 0.9773(6) 0.6444(3) 0.4959(5) 0.0301(16) Uani 1 1 d . . . . . H39A H 1.050600 0.627627 0.520955 0.045 Uiso 1 1 calc GR . . . . H39B H 0.973414 0.673742 0.528259 0.045 Uiso 1 1 calc GR . . . . H39C H 0.973074 0.652834 0.437080 0.045 Uiso 1 1 calc GR . . . . C40 C -0.3787(6) 0.3702(3) 0.1657(5) 0.0310(16) Uani 1 1 d . . . . . C41 C -0.4514(6) 0.3297(3) 0.1474(5) 0.0333(18) Uani 1 1 d . . . . . C42 C -0.5544(6) 0.3313(4) 0.0812(5) 0.044(2) Uani 1 1 d . . . . . H42 H -0.603475 0.303861 0.070067 0.052 Uiso 1 1 calc R . . . . C43 C -0.5861(6) 0.3730(4) 0.0308(4) 0.047(2) Uani 1 1 d . . . . . C44 C -0.5140(6) 0.4126(4) 0.0491(5) 0.050(3) Uani 1 1 d . . . . . H44 H -0.534656 0.440915 0.016020 0.060 Uiso 1 1 calc R . . . . C45 C -0.4110(6) 0.4124(4) 0.1151(5) 0.0359(19) Uani 1 1 d . . . . . C46 C -0.3365(7) 0.4559(3) 0.1291(5) 0.042(2) Uani 1 1 d . . . . . H46A H -0.311506 0.463053 0.189872 0.063 Uiso 1 1 calc GR . . . . H46B H -0.380686 0.483218 0.098975 0.063 Uiso 1 1 calc GR . . . . H46C H -0.268183 0.450181 0.107875 0.063 Uiso 1 1 calc GR . . . . C47 C -0.6972(7) 0.3743(6) -0.0375(5) 0.086(5) Uani 1 1 d . . . . . H47A H -0.759498 0.386711 -0.014412 0.129 Uiso 1 1 calc GR . . . . H47B H -0.716937 0.341748 -0.059539 0.129 Uiso 1 1 calc GR . . . . H47C H -0.688196 0.395389 -0.083380 0.129 Uiso 1 1 calc GR . . . . C48 C -0.4219(7) 0.2846(3) 0.1980(6) 0.049(2) Uani 1 1 d . . . . . H48A H -0.339371 0.277197 0.206171 0.073 Uiso 1 1 calc GR . . . . H48B H -0.469127 0.258012 0.167853 0.073 Uiso 1 1 calc GR . . . . H48C H -0.437897 0.288984 0.253315 0.073 Uiso 1 1 calc GR . . . . C49 C -0.2789(6) 0.3149(3) 0.5816(4) 0.0320(17) Uani 1 1 d . . . . . C50 C -0.3344(7) 0.3396(3) 0.6327(5) 0.0372(19) Uani 1 1 d . . . . . C51 C -0.4164(7) 0.3144(4) 0.6630(5) 0.045(2) Uani 1 1 d . . . . . H51 H -0.457155 0.331353 0.696731 0.054 Uiso 1 1 calc R . . . . C52 C -0.4416(8) 0.2665(4) 0.6467(5) 0.054(3) Uani 1 1 d . . . . . C53 C -0.3833(8) 0.2426(4) 0.5942(6) 0.056(3) Uani 1 1 d . . . . . H53 H -0.400711 0.209748 0.580745 0.067 Uiso 1 1 calc R . . . . C54 C -0.3014(7) 0.2654(3) 0.5613(5) 0.0396(19) Uani 1 1 d . . . . . C55 C -0.2441(8) 0.2385(3) 0.5051(6) 0.047(2) Uani 1 1 d . . . . . H55A H -0.247850 0.257499 0.454027 0.071 Uiso 1 1 calc GR . . . . H55B H -0.283871 0.207702 0.489243 0.071 Uiso 1 1 calc GR . . . . H55C H -0.162579 0.232582 0.535039 0.071 Uiso 1 1 calc GR . . . . C56 C -0.3127(7) 0.3918(3) 0.6532(5) 0.043(2) Uani 1 1 d . . . . . H56A H -0.271363 0.395328 0.713103 0.064 Uiso 1 1 calc GR . . . . H56B H -0.387140 0.408871 0.641805 0.064 Uiso 1 1 calc GR . . . . H56C H -0.265567 0.405354 0.618011 0.064 Uiso 1 1 calc GR . . . . C57 C -0.5300(10) 0.2394(5) 0.6817(7) 0.084(4) Uani 1 1 d . . . . . H57A H -0.491410 0.226317 0.737629 0.126 Uiso 1 1 calc GR . . . . H57B H -0.563449 0.213005 0.643265 0.126 Uiso 1 1 calc GR . . . . H57C H -0.591918 0.261492 0.686655 0.126 Uiso 1 1 calc GR . . . . C58 C 0.7897(6) 0.5335(3) 0.4886(5) 0.0267(15) Uani 1 1 d . . . . . B1 B 0.3738(6) 0.4556(3) 0.4662(5) 0.0250(16) Uani 1 1 d . . . . . F3 F 0.1899(3) 0.57051(16) 0.9251(3) 0.0319(9) Uani 1 1 d . . . . . F4 F 0.3139(3) 0.50786(17) 0.9443(2) 0.0324(9) Uani 1 1 d . . . . . N0AA N 0.1279(5) 0.4970(3) 0.8455(4) 0.0307(14) Uani 1 1 d . . . . . N1AA N 0.3199(5) 0.5595(3) 0.7888(4) 0.0298(14) Uani 1 1 d . . . . . H1AA H 0.356018 0.551225 0.840980 0.036 Uiso 1 1 calc R . . . . N2AA N 0.5611(4) 0.6093(2) 0.8259(3) 0.0281(13) Uani 1 1 d . . . . . N3AA N 0.7677(5) 0.6161(3) 1.0022(4) 0.0316(15) Uani 1 1 d . . . . . H3AA H 0.693570 0.620918 0.998462 0.038 Uiso 1 1 calc R . . . . N4AA N 0.6220(5) 0.5980(2) 1.1326(4) 0.0285(13) Uani 1 1 d . . . . . N5AA N 0.3710(4) 0.5606(2) 1.1070(3) 0.0236(12) Uani 1 1 d . . . . . H5AA H 0.393989 0.550670 1.063021 0.028 Uiso 1 1 calc R . . . . N6AA N 0.1469(4) 0.5018(2) 1.0001(3) 0.0240(12) Uani 1 1 d . . . . . C59 C -0.0054(6) 0.4529(3) 0.9082(5) 0.0315(16) Uani 1 1 d . . . . . C60 C 0.0336(6) 0.4664(3) 0.8376(5) 0.0319(16) Uani 1 1 d . . . . . C61 C -0.0107(7) 0.4552(3) 0.7509(5) 0.0390(19) Uani 1 1 d . . . . . H61 H -0.073862 0.434104 0.727740 0.047 Uiso 1 1 calc R . . . . C62 C 0.0528(6) 0.4798(3) 0.7060(5) 0.0363(18) Uani 1 1 d . . . . . H62 H 0.040987 0.479709 0.646314 0.044 Uiso 1 1 calc R . . . . C63 C 0.1400(6) 0.5056(3) 0.7664(5) 0.0324(16) Uani 1 1 d . . . . . C64 C 0.2148(5) 0.5403(3) 0.7411(5) 0.0336(18) Uani 1 1 d . . . . . C65 C 0.1893(6) 0.5631(3) 0.6635(4) 0.038(2) Uani 1 1 d . . . . . H65 H 0.122781 0.557105 0.617809 0.046 Uiso 1 1 calc R . . . . C66 C 0.2759(6) 0.5958(3) 0.6628(5) 0.0393(19) Uani 1 1 d . . . . . H66 H 0.279276 0.616300 0.617048 0.047 Uiso 1 1 calc R . . . . C67 C 0.3577(6) 0.5934(3) 0.7412(4) 0.0335(18) Uani 1 1 d . . . . . C68 C 0.4675(6) 0.6177(3) 0.7600(4) 0.0297(16) Uani 1 1 d . . . . . C69 C 0.4942(6) 0.6537(3) 0.7014(4) 0.0327(17) Uani 1 1 d . . . . . H69 H 0.441485 0.666982 0.652758 0.039 Uiso 1 1 calc R . . . . C70 C 0.6060(6) 0.6637(3) 0.7300(5) 0.0333(17) Uani 1 1 d . . . . . H70 H 0.649596 0.684710 0.704282 0.040 Uiso 1 1 calc R . . . . C71 C 0.6500(6) 0.6370(3) 0.8075(4) 0.0313(17) Uani 1 1 d . . . . . C72 C 0.7651(5) 0.6389(3) 0.8526(4) 0.0267(15) Uani 1 1 d . . . . . C73 C 0.8179(6) 0.6191(3) 0.9363(4) 0.0263(15) Uani 1 1 d . . . . . C74 C 0.9347(6) 0.6068(3) 0.9673(4) 0.0265(15) Uani 1 1 d . . . . . H74 H 0.990415 0.605065 0.935217 0.032 Uiso 1 1 calc R . . . . C75 C 0.9552(6) 0.5975(3) 1.0524(4) 0.0280(15) Uani 1 1 d . . . . . H75 H 1.027418 0.588119 1.089441 0.034 Uiso 1 1 calc R . . . . C76 C 0.8508(5) 0.6043(3) 1.0752(4) 0.0248(14) Uani 1 1 d . . . . . C77 C 0.8366(6) 0.6052(3) 1.1587(4) 0.0294(16) Uani 1 1 d . . . . . C78 C 0.7349(6) 0.6081(3) 1.1820(4) 0.0287(16) Uani 1 1 d . . . . . C79 C 0.7272(7) 0.6221(3) 1.2670(4) 0.0343(18) Uani 1 1 d . . . . . H79 H 0.790704 0.630697 1.313293 0.041 Uiso 1 1 calc R . . . . C80 C 0.6170(6) 0.6206(3) 1.2681(4) 0.0285(15) Uani 1 1 d . . . . . H80 H 0.585959 0.628287 1.314306 0.034 Uiso 1 1 calc R . . . . C81 C 0.5528(6) 0.6049(3) 1.1839(4) 0.0250(14) Uani 1 1 d . . . . . C82 C 0.4331(6) 0.5911(2) 1.1699(4) 0.0234(14) Uani 1 1 d . . . . . C83 C 0.3648(6) 0.5986(3) 1.2250(4) 0.0299(16) Uani 1 1 d . . . . . H83 H 0.384716 0.618584 1.273799 0.036 Uiso 1 1 calc R . . . . C84 C 0.2643(5) 0.5728(3) 1.1984(4) 0.0287(16) Uani 1 1 d . . . . . H84 H 0.203033 0.571866 1.225441 0.034 Uiso 1 1 calc R . . . . C85 C 0.2669(5) 0.5481(3) 1.1244(4) 0.0229(14) Uani 1 1 d . . . . . C86 C 0.1778(5) 0.5152(3) 1.0816(4) 0.0256(15) Uani 1 1 d . . . . . C87 C 0.1017(6) 0.4936(3) 1.1250(4) 0.0297(16) Uani 1 1 d . . . . . H87 H 0.105104 0.497059 1.183308 0.036 Uiso 1 1 calc R . . . . C88 C 0.0219(6) 0.4667(3) 1.0663(4) 0.0303(16) Uani 1 1 d . . . . . H88 H -0.040209 0.448369 1.076703 0.036 Uiso 1 1 calc R . . . . C89 C 0.0502(6) 0.4714(3) 0.9864(5) 0.0329(17) Uani 1 1 d . . . . . C90 C 0.9483(5) 0.6029(3) 1.2305(4) 0.0311(16) Uani 1 1 d . . . . . C91 C 1.0177(6) 0.6439(3) 1.2503(5) 0.0366(18) Uani 1 1 d . . . . . C92 C 1.1199(6) 0.6401(3) 1.3182(5) 0.0333(17) Uani 1 1 d . . . . . H92 H 1.168783 0.667475 1.333500 0.040 Uiso 1 1 calc R . . . . C93 C 1.1500(5) 0.5977(3) 1.3625(4) 0.0312(17) Uani 1 1 d . . . . . C94 C 1.0782(6) 0.5585(3) 1.3408(4) 0.0314(17) Uani 1 1 d . . . . . H94 H 1.099014 0.529238 1.370969 0.038 Uiso 1 1 calc R . . . . C95 C 0.8989(6) 0.5161(3) 1.2550(5) 0.041(2) Uani 1 1 d . . . . . H95A H 0.942834 0.488123 1.282876 0.062 Uiso 1 1 calc GR . . . . H95B H 0.875522 0.510911 1.193628 0.062 Uiso 1 1 calc GR . . . . H95C H 0.829555 0.520435 1.275666 0.062 Uiso 1 1 calc GR . . . . C96 C 0.9880(8) 0.6916(3) 1.2065(5) 0.048(2) Uani 1 1 d . . . . . H96A H 0.935575 0.709371 1.232742 0.072 Uiso 1 1 calc GR . . . . H96B H 0.949699 0.686227 1.146462 0.072 Uiso 1 1 calc GR . . . . H96C H 1.059289 0.710239 1.211822 0.072 Uiso 1 1 calc GR . . . . C97 C 1.2614(6) 0.5935(4) 1.4300(5) 0.042(2) Uani 1 1 d . . . . . H97A H 1.321679 0.580354 1.405643 0.063 Uiso 1 1 calc GR . . . . H97B H 1.250469 0.572084 1.474788 0.063 Uiso 1 1 calc GR . . . . H97C H 1.285254 0.625436 1.453872 0.063 Uiso 1 1 calc GR . . . . C98 C 0.9739(6) 0.5603(3) 1.2748(5) 0.0334(17) Uani 1 1 d . . . . . C99 C 0.8486(5) 0.6633(3) 0.8137(4) 0.0260(15) Uani 1 1 d . . . . . C100 C 0.8768(7) 0.7115(3) 0.8324(5) 0.0379(18) Uani 1 1 d . . . . . C101 C 0.9516(7) 0.7348(3) 0.7937(5) 0.0406(19) Uani 1 1 d . . . . . H101 H 0.965162 0.768259 0.803789 0.049 Uiso 1 1 calc R . . . . C102 C 1.0067(6) 0.7118(3) 0.7418(5) 0.0350(17) Uani 1 1 d . . . . . C103 C 0.9825(6) 0.6631(3) 0.7259(5) 0.0362(18) Uani 1 1 d . . . . . H103 H 1.021397 0.646169 0.690969 0.043 Uiso 1 1 calc R . . . . C104 C 0.8806(7) 0.5864(3) 0.7398(5) 0.0379(18) Uani 1 1 d . . . . . H10A H 0.941954 0.567127 0.777099 0.057 Uiso 1 1 calc GR . . . . H10B H 0.879476 0.580315 0.680661 0.057 Uiso 1 1 calc GR . . . . H10C H 0.805212 0.577611 0.748957 0.057 Uiso 1 1 calc GR . . . . C105 C 0.8208(11) 0.7383(4) 0.8922(7) 0.074(4) Uani 1 1 d . . . . . H10D H 0.736239 0.738486 0.868765 0.111 Uiso 1 1 calc GR . . . . H10E H 0.849621 0.771482 0.898953 0.111 Uiso 1 1 calc GR . . . . H10F H 0.840348 0.722212 0.947413 0.111 Uiso 1 1 calc GR . . . . C106 C 1.0936(7) 0.7366(4) 0.7043(5) 0.046(2) Uani 1 1 d . . . . . H10G H 1.060253 0.766793 0.677514 0.069 Uiso 1 1 calc GR . . . . H10H H 1.112897 0.715698 0.661753 0.069 Uiso 1 1 calc GR . . . . H10I H 1.164207 0.743611 0.749160 0.069 Uiso 1 1 calc GR . . . . C107 C -0.1119(6) 0.4233(3) 0.8997(4) 0.0296(16) Uani 1 1 d . . . . . C108 C -0.2175(6) 0.4454(3) 0.9022(4) 0.0322(17) Uani 1 1 d . . . . . C109 C -0.3144(6) 0.4155(3) 0.8985(5) 0.0343(18) Uani 1 1 d . . . . . H109 H -0.386350 0.429864 0.899309 0.041 Uiso 1 1 calc R . . . . C110 C -0.3082(6) 0.3660(3) 0.8937(4) 0.0287(15) Uani 1 1 d . . . . . C111 C -0.4125(6) 0.3346(3) 0.8924(5) 0.0369(18) Uani 1 1 d . . . . . H11A H -0.399236 0.302188 0.873422 0.055 Uiso 1 1 calc GR . . . . H11B H -0.481826 0.348474 0.853420 0.055 Uiso 1 1 calc GR . . . . H11C H -0.423921 0.332992 0.949468 0.055 Uiso 1 1 calc GR . . . . C112 C -0.2027(6) 0.3452(3) 0.8894(4) 0.0285(16) Uani 1 1 d . . . . . H112 H -0.197623 0.311295 0.883870 0.034 Uiso 1 1 calc R . . . . C113 C -0.1063(6) 0.3732(3) 0.8931(4) 0.0305(16) Uani 1 1 d . . . . . C114 C 0.0072(7) 0.3490(4) 0.8968(5) 0.044(2) Uani 1 1 d . . . . . H11D H 0.045872 0.365592 0.858949 0.066 Uiso 1 1 calc GR . . . . H11E H -0.006999 0.315365 0.878978 0.066 Uiso 1 1 calc GR . . . . H11F H 0.056872 0.350150 0.954946 0.066 Uiso 1 1 calc GR . . . . C115 C -0.2305(6) 0.4987(3) 0.9068(6) 0.043(2) Uani 1 1 d . . . . . H11G H -0.181554 0.510533 0.960875 0.064 Uiso 1 1 calc GR . . . . H11H H -0.311959 0.506624 0.902484 0.064 Uiso 1 1 calc GR . . . . H11I H -0.206633 0.513935 0.860055 0.064 Uiso 1 1 calc GR . . . . C116 C 0.9034(6) 0.6384(3) 0.7593(5) 0.0302(16) Uani 1 1 d . . . . . B2 B 0.1987(6) 0.5203(3) 0.9288(5) 0.0269(17) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F1 0.0200(18) 0.045(3) 0.027(2) -0.0030(19) 0.0035(15) 0.0021(18) F2 0.036(2) 0.027(2) 0.030(2) 0.0015(18) 0.0128(17) -0.0075(18) N1 0.022(3) 0.024(3) 0.026(3) 0.007(3) 0.006(2) 0.000(2) N2 0.028(3) 0.032(3) 0.025(3) -0.001(3) 0.008(2) -0.006(3) N3 0.020(3) 0.032(3) 0.028(3) -0.004(3) 0.004(2) -0.006(2) N4 0.021(3) 0.036(4) 0.021(3) 0.001(3) 0.007(2) 0.000(2) N5 0.019(2) 0.032(3) 0.019(3) 0.004(2) 0.007(2) -0.004(2) N6 0.013(2) 0.026(3) 0.028(3) -0.001(2) 0.008(2) 0.005(2) N7 0.024(3) 0.028(3) 0.024(3) -0.003(3) 0.008(2) 0.001(2) C1 0.020(3) 0.031(4) 0.031(4) 0.004(3) 0.005(3) 0.005(3) C2 0.023(3) 0.021(4) 0.037(4) -0.006(3) 0.008(3) -0.002(3) C3 0.015(3) 0.026(4) 0.032(3) 0.004(3) 0.005(2) -0.007(3) C4 0.021(3) 0.031(4) 0.022(3) 0.002(3) 0.003(3) -0.001(3) C5 0.012(3) 0.026(4) 0.024(3) 0.001(3) 0.001(2) 0.000(3) C6 0.015(3) 0.029(4) 0.027(3) -0.001(3) 0.005(3) 0.003(3) C7 0.017(3) 0.036(4) 0.029(3) -0.005(3) 0.011(3) 0.004(3) C8 0.026(3) 0.031(4) 0.027(3) -0.012(3) 0.009(3) 0.000(3) C9 0.020(3) 0.035(4) 0.023(3) -0.008(3) 0.007(3) -0.001(3) C10 0.023(3) 0.026(4) 0.027(3) 0.007(3) 0.007(3) 0.006(3) C11 0.022(3) 0.026(4) 0.022(3) 0.003(3) 0.005(3) 0.000(3) C12 0.013(3) 0.038(4) 0.026(3) -0.001(3) 0.004(3) -0.005(3) C13 0.025(3) 0.026(4) 0.028(3) 0.001(3) 0.007(3) 0.002(3) C14 0.021(3) 0.030(4) 0.025(3) 0.003(3) 0.007(3) -0.003(3) C15 0.033(4) 0.024(4) 0.026(4) 0.006(3) 0.003(3) 0.007(3) C16 0.016(3) 0.027(4) 0.029(3) -0.003(3) 0.003(2) -0.001(3) C17 0.026(3) 0.026(4) 0.027(3) -0.002(3) 0.008(3) -0.006(3) C18 0.025(3) 0.024(4) 0.024(3) -0.005(3) 0.007(3) -0.007(3) C19 0.034(4) 0.014(3) 0.029(3) -0.004(3) 0.009(3) -0.005(3) C20 0.031(3) 0.016(3) 0.026(3) 0.010(3) 0.009(3) 0.004(3) C21 0.041(4) 0.041(5) 0.027(4) 0.005(3) 0.013(3) -0.008(4) C22 0.020(3) 0.054(5) 0.031(4) 0.012(4) 0.002(3) 0.003(3) C23 0.027(3) 0.032(4) 0.034(4) -0.005(3) 0.006(3) 0.002(3) C24 0.033(4) 0.041(5) 0.028(4) 0.003(3) 0.009(3) -0.007(3) C25 0.043(4) 0.093(8) 0.031(4) 0.010(5) 0.006(4) -0.032(5) C26 0.052(5) 0.093(9) 0.025(4) -0.003(5) 0.007(4) -0.026(5) C27 0.025(3) 0.047(5) 0.021(3) -0.002(3) -0.001(3) -0.006(3) C28 0.020(3) 0.047(5) 0.021(3) -0.006(3) -0.001(3) -0.002(3) C29 0.029(3) 0.050(5) 0.029(4) -0.011(4) 0.009(3) -0.010(4) C30 0.026(3) 0.032(4) 0.033(4) -0.003(3) 0.004(3) -0.006(3) C31 0.026(3) 0.029(4) 0.027(3) -0.001(3) 0.002(3) -0.004(3) C32 0.023(3) 0.034(4) 0.024(3) 0.004(3) 0.004(3) 0.002(3) C33 0.022(3) 0.031(4) 0.026(3) -0.001(3) 0.007(3) -0.002(3) C34 0.021(3) 0.026(4) 0.026(3) 0.003(3) 0.005(3) 0.003(3) C35 0.033(4) 0.042(5) 0.021(3) 0.001(3) 0.008(3) -0.013(3) C36 0.025(3) 0.034(4) 0.028(4) 0.005(3) 0.005(3) -0.003(3) C37 0.032(3) 0.023(4) 0.043(4) 0.001(3) 0.011(3) -0.002(3) C38 0.025(3) 0.017(3) 0.033(4) 0.001(3) 0.007(3) 0.009(3) C39 0.026(3) 0.034(4) 0.032(4) 0.002(3) 0.009(3) -0.005(3) C40 0.025(3) 0.043(5) 0.030(4) 0.001(3) 0.016(3) 0.002(3) C41 0.020(3) 0.047(5) 0.037(4) -0.021(4) 0.014(3) -0.013(3) C42 0.018(3) 0.082(7) 0.032(4) -0.021(5) 0.010(3) -0.015(4) C43 0.025(3) 0.099(8) 0.016(3) 0.002(4) 0.003(3) -0.008(4) C44 0.026(4) 0.105(9) 0.020(4) -0.004(4) 0.007(3) 0.011(5) C45 0.022(3) 0.059(6) 0.027(4) -0.001(4) 0.008(3) 0.005(4) C46 0.039(4) 0.053(6) 0.034(4) 0.016(4) 0.009(3) 0.003(4) C47 0.022(4) 0.206(16) 0.027(4) -0.005(7) -0.001(3) -0.012(6) C48 0.039(4) 0.045(5) 0.067(6) -0.018(5) 0.022(4) -0.014(4) C49 0.028(3) 0.040(5) 0.024(3) 0.005(3) 0.000(3) -0.004(3) C50 0.032(4) 0.052(5) 0.027(4) -0.004(4) 0.006(3) -0.020(4) C51 0.051(5) 0.062(6) 0.022(4) 0.002(4) 0.012(3) -0.026(4) C52 0.063(6) 0.069(7) 0.032(4) -0.002(5) 0.015(4) -0.040(5) C53 0.065(6) 0.054(6) 0.049(5) -0.006(5) 0.017(4) -0.029(5) C54 0.045(4) 0.033(4) 0.036(4) 0.008(4) 0.003(3) -0.022(4) C55 0.057(5) 0.030(4) 0.054(5) -0.005(4) 0.015(4) 0.003(4) C56 0.040(4) 0.052(6) 0.042(5) -0.003(4) 0.020(4) -0.005(4) C57 0.077(7) 0.105(10) 0.078(8) -0.004(7) 0.036(6) -0.057(8) C58 0.021(3) 0.024(4) 0.034(4) 0.003(3) 0.005(3) -0.004(3) B1 0.024(4) 0.026(4) 0.024(4) -0.007(3) 0.006(3) -0.003(3) F3 0.030(2) 0.037(3) 0.028(2) 0.0014(19) 0.0065(16) -0.0029(18) F4 0.0222(18) 0.048(3) 0.0265(19) 0.002(2) 0.0048(15) -0.0013(19) N0AA 0.020(3) 0.048(4) 0.024(3) -0.006(3) 0.004(2) -0.010(3) N1AA 0.017(2) 0.048(4) 0.024(3) 0.000(3) 0.006(2) -0.004(3) N2AA 0.018(2) 0.041(4) 0.026(3) 0.004(3) 0.007(2) 0.000(3) N3AA 0.018(3) 0.048(4) 0.028(3) 0.008(3) 0.003(2) -0.007(3) N4AA 0.025(3) 0.035(4) 0.025(3) 0.001(3) 0.006(2) 0.002(3) N5AA 0.023(3) 0.031(3) 0.013(2) 0.000(2) -0.001(2) -0.004(2) N6AA 0.015(2) 0.026(3) 0.028(3) 0.003(3) 0.001(2) -0.009(2) C59 0.029(3) 0.031(4) 0.031(4) 0.003(3) 0.002(3) -0.007(3) C60 0.021(3) 0.039(4) 0.034(4) 0.002(3) 0.004(3) -0.009(3) C61 0.032(4) 0.049(5) 0.036(4) -0.014(4) 0.009(3) -0.016(4) C62 0.030(4) 0.043(5) 0.034(4) -0.008(4) 0.008(3) -0.010(3) C63 0.032(4) 0.032(4) 0.031(4) -0.008(3) 0.005(3) -0.009(3) C64 0.015(3) 0.057(5) 0.030(4) -0.006(4) 0.007(3) -0.014(3) C65 0.021(3) 0.064(6) 0.024(4) 0.005(4) -0.003(3) -0.016(4) C66 0.033(4) 0.058(6) 0.027(4) 0.004(4) 0.007(3) -0.011(4) C67 0.025(3) 0.052(5) 0.023(3) 0.006(3) 0.004(3) -0.010(3) C68 0.025(3) 0.048(5) 0.020(3) 0.002(3) 0.012(3) -0.005(3) C69 0.037(4) 0.037(4) 0.023(3) 0.008(3) 0.005(3) -0.007(3) C70 0.035(4) 0.036(4) 0.032(4) 0.008(3) 0.013(3) 0.000(3) C71 0.026(3) 0.042(5) 0.027(4) -0.001(3) 0.010(3) -0.012(3) C72 0.021(3) 0.032(4) 0.027(3) 0.003(3) 0.007(3) -0.005(3) C73 0.024(3) 0.029(4) 0.027(3) 0.000(3) 0.009(3) -0.002(3) C74 0.024(3) 0.032(4) 0.026(3) -0.002(3) 0.009(3) -0.001(3) C75 0.026(3) 0.026(4) 0.030(4) 0.001(3) 0.004(3) 0.002(3) C76 0.013(3) 0.034(4) 0.028(3) -0.003(3) 0.005(2) -0.006(3) C77 0.028(3) 0.030(4) 0.028(4) 0.002(3) 0.002(3) -0.004(3) C78 0.024(3) 0.041(4) 0.019(3) 0.001(3) 0.001(3) -0.007(3) C79 0.045(4) 0.039(5) 0.013(3) -0.004(3) -0.003(3) -0.011(4) C80 0.029(3) 0.031(4) 0.026(4) 0.000(3) 0.009(3) -0.008(3) C81 0.026(3) 0.023(4) 0.026(3) 0.001(3) 0.006(3) 0.001(3) C82 0.028(3) 0.016(3) 0.026(3) 0.005(3) 0.007(3) -0.001(3) C83 0.026(3) 0.040(5) 0.025(3) 0.003(3) 0.010(3) 0.000(3) C84 0.022(3) 0.041(4) 0.025(3) 0.001(3) 0.009(3) 0.002(3) C85 0.020(3) 0.027(4) 0.022(3) 0.008(3) 0.005(3) -0.004(3) C86 0.023(3) 0.030(4) 0.022(3) 0.001(3) 0.004(3) 0.002(3) C87 0.027(3) 0.035(4) 0.024(4) 0.005(3) 0.002(3) -0.009(3) C88 0.032(4) 0.031(4) 0.026(3) 0.012(3) 0.004(3) -0.004(3) C89 0.025(3) 0.043(5) 0.030(4) 0.016(4) 0.006(3) -0.003(3) C90 0.020(3) 0.044(5) 0.028(3) -0.003(3) 0.004(3) -0.006(3) C91 0.030(4) 0.051(5) 0.029(4) 0.008(4) 0.009(3) 0.006(4) C92 0.023(3) 0.049(5) 0.030(4) -0.009(4) 0.011(3) -0.010(3) C93 0.019(3) 0.054(5) 0.023(3) -0.009(3) 0.011(3) 0.002(3) C94 0.022(3) 0.050(5) 0.023(3) 0.011(3) 0.007(3) 0.000(3) C95 0.025(3) 0.047(5) 0.051(5) 0.012(4) 0.009(3) -0.003(3) C96 0.048(5) 0.039(5) 0.047(5) -0.011(4) -0.007(4) -0.007(4) C97 0.030(4) 0.052(5) 0.040(4) -0.009(4) 0.003(3) 0.002(4) C98 0.023(3) 0.045(5) 0.034(4) 0.006(4) 0.011(3) -0.009(3) C99 0.022(3) 0.034(4) 0.022(3) 0.002(3) 0.006(3) -0.005(3) C100 0.048(4) 0.032(4) 0.040(4) 0.002(4) 0.022(4) 0.005(4) C101 0.044(4) 0.026(4) 0.057(5) 0.003(4) 0.023(4) -0.007(4) C102 0.027(3) 0.035(4) 0.040(4) 0.009(4) 0.003(3) -0.004(3) C103 0.031(4) 0.050(5) 0.029(4) 0.000(4) 0.010(3) -0.008(3) C104 0.047(4) 0.037(5) 0.034(4) -0.012(4) 0.016(3) -0.011(4) C105 0.115(9) 0.045(6) 0.089(8) -0.012(6) 0.076(8) -0.016(6) C106 0.047(4) 0.054(6) 0.040(4) -0.003(4) 0.016(4) -0.019(4) C107 0.024(3) 0.040(4) 0.022(3) -0.007(3) 0.000(3) -0.010(3) C108 0.032(4) 0.040(4) 0.024(4) -0.007(3) 0.005(3) -0.012(3) C109 0.021(3) 0.046(5) 0.032(4) 0.002(4) 0.000(3) 0.000(3) C110 0.028(3) 0.036(4) 0.023(3) 0.000(3) 0.008(3) 0.001(3) C111 0.035(4) 0.041(5) 0.038(4) -0.004(4) 0.014(3) -0.008(3) C112 0.029(3) 0.034(4) 0.023(3) -0.001(3) 0.008(3) -0.013(3) C113 0.031(3) 0.030(4) 0.026(4) 0.001(3) 0.000(3) 0.001(3) C114 0.035(4) 0.061(6) 0.036(4) -0.007(4) 0.009(3) -0.011(4) C115 0.027(4) 0.047(5) 0.053(5) 0.000(4) 0.007(3) 0.000(4) C116 0.021(3) 0.036(4) 0.029(4) 0.000(3) -0.001(3) -0.007(3) B2 0.019(3) 0.033(5) 0.027(4) 0.005(4) 0.003(3) -0.006(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C28 N1 C31 108.1(6) . . ? C28 N1 B1 126.5(6) . . ? C31 N1 B1 125.3(6) . . ? C24 N2 H2 125.5 . . ? C24 N2 C27 109.0(6) . . ? C27 N2 H2 125.5 . . ? C23 N3 C20 104.1(6) . . ? C15 N4 H4 125.5 . . ? C18 N4 H4 125.5 . . ? C18 N4 C15 109.0(6) . . ? C10 N5 C13 105.4(5) . . ? C6 N6 H6 125.9 . . ? C6 N6 C9 108.2(5) . . ? C9 N6 H6 125.9 . . ? C2 N7 B1 125.4(6) . . ? C5 N7 C2 106.8(5) . . ? C5 N7 B1 127.2(6) . . ? C2 C1 C31 118.8(6) . . ? C2 C1 C32 119.9(6) . . ? C31 C1 C32 121.3(6) . . ? C1 C2 N7 121.8(6) . . ? C3 C2 N7 109.0(6) . . ? C3 C2 C1 129.1(6) . . ? C2 C3 H3 126.0 . . ? C2 C3 C4 108.0(6) . . ? C4 C3 H3 126.0 . . ? C3 C4 H4A 126.9 . . ? C3 C4 C5 106.2(6) . . ? C5 C4 H4A 126.9 . . ? N7 C5 C4 110.0(6) . . ? N7 C5 C6 127.3(6) . . ? C4 C5 C6 122.7(6) . . ? N6 C6 C5 130.0(6) . . ? N6 C6 C7 108.7(6) . . ? C7 C6 C5 121.2(6) . . ? C6 C7 H7 126.4 . . ? C6 C7 C8 107.2(6) . . ? C8 C7 H7 126.4 . . ? C7 C8 H8 125.8 . . ? C9 C8 C7 108.4(6) . . ? C9 C8 H8 125.8 . . ? N6 C9 C10 127.6(6) . . ? C8 C9 N6 107.5(6) . . ? C8 C9 C10 124.1(6) . . ? N5 C10 C9 128.7(6) . . ? N5 C10 C11 110.7(6) . . ? C9 C10 C11 120.0(6) . . ? C10 C11 H11 126.2 . . ? C12 C11 C10 107.6(6) . . ? C12 C11 H11 126.2 . . ? C11 C12 H12 127.6 . . ? C11 C12 C13 104.9(6) . . ? C13 C12 H12 127.6 . . ? N5 C13 C12 111.3(6) . . ? C14 C13 N5 126.6(6) . . ? C14 C13 C12 122.0(6) . . ? C13 C14 C15 128.3(6) . . ? C13 C14 C40 117.0(6) . . ? C15 C14 C40 114.7(6) . . ? N4 C15 C14 125.7(6) . . ? C16 C15 N4 106.3(6) . . ? C16 C15 C14 127.2(6) . . ? C15 C16 H16 125.7 . . ? C17 C16 C15 108.7(6) . . ? C17 C16 H16 125.7 . . ? C16 C17 H17 125.7 . . ? C16 C17 C18 108.5(6) . . ? C18 C17 H17 125.7 . . ? N4 C18 C17 107.5(6) . . ? N4 C18 C19 126.1(6) . . ? C17 C18 C19 126.1(6) . . ? C18 C19 C49 110.9(6) . . ? C20 C19 C18 130.3(7) . . ? C20 C19 C49 118.8(6) . . ? N3 C20 C21 109.1(6) . . ? C19 C20 N3 127.5(6) . . ? C19 C20 C21 123.2(7) . . ? C20 C21 H21 126.3 . . ? C22 C21 C20 107.4(7) . . ? C22 C21 H21 126.3 . . ? C21 C22 H22 127.0 . . ? C21 C22 C23 106.0(6) . . ? C23 C22 H22 127.0 . . ? N3 C23 C22 113.4(6) . . ? N3 C23 C24 127.5(7) . . ? C22 C23 C24 118.8(6) . . ? N2 C24 C23 128.5(7) . . ? N2 C24 C25 107.3(7) . . ? C25 C24 C23 123.8(7) . . ? C24 C25 H25 125.6 . . ? C26 C25 C24 108.9(8) . . ? C26 C25 H25 125.6 . . ? C25 C26 H26 126.3 . . ? C25 C26 C27 107.4(7) . . ? C27 C26 H26 126.3 . . ? N2 C27 C26 107.5(7) . . ? N2 C27 C28 129.0(6) . . ? C26 C27 C28 123.4(7) . . ? N1 C28 C27 127.0(6) . . ? N1 C28 C29 108.0(7) . . ? C29 C28 C27 124.7(7) . . ? C28 C29 H29 125.7 . . ? C30 C29 C28 108.6(7) . . ? C30 C29 H29 125.7 . . ? C29 C30 H30 126.6 . . ? C29 C30 C31 106.8(6) . . ? C31 C30 H30 126.6 . . ? N1 C31 C1 122.0(6) . . ? N1 C31 C30 108.5(6) . . ? C1 C31 C30 129.2(6) . . ? C33 C32 C1 120.1(6) . . ? C33 C32 C58 120.0(7) . . ? C58 C32 C1 119.7(7) . . ? C32 C33 C34 118.9(6) . . ? C32 C33 C38 122.0(6) . . ? C34 C33 C38 119.0(7) . . ? C33 C34 H34 119.6 . . ? C33 C34 C35 120.8(7) . . ? C35 C34 H34 119.6 . . ? C34 C35 C39 118.7(7) . . ? C36 C35 C34 118.9(7) . . ? C36 C35 C39 122.2(7) . . ? C35 C36 H36 118.6 . . ? C35 C36 C58 122.8(7) . . ? C58 C36 H36 118.6 . . ? H37A C37 H37B 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C58 C37 H37A 109.5 . . ? C58 C37 H37B 109.5 . . ? C58 C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C35 C39 H39A 109.5 . . ? C35 C39 H39B 109.5 . . ? C35 C39 H39C 109.5 . . ? H39A C39 H39B 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C41 C40 C14 122.6(7) . . ? C41 C40 C45 118.5(7) . . ? C45 C40 C14 118.9(7) . . ? C40 C41 C42 120.2(8) . . ? C40 C41 C48 120.9(7) . . ? C42 C41 C48 119.0(8) . . ? C41 C42 H42 119.3 . . ? C41 C42 C43 121.3(8) . . ? C43 C42 H42 119.3 . . ? C42 C43 C47 120.3(10) . . ? C44 C43 C42 118.1(7) . . ? C44 C43 C47 121.6(11) . . ? C43 C44 H44 118.9 . . ? C43 C44 C45 122.2(10) . . ? C45 C44 H44 118.9 . . ? C40 C45 C46 121.4(7) . . ? C44 C45 C40 119.8(9) . . ? C44 C45 C46 118.9(9) . . ? C45 C46 H46A 109.5 . . ? C45 C46 H46B 109.5 . . ? C45 C46 H46C 109.5 . . ? H46A C46 H46B 109.5 . . ? H46A C46 H46C 109.5 . . ? H46B C46 H46C 109.5 . . ? C43 C47 H47A 109.5 . . ? C43 C47 H47B 109.5 . . ? C43 C47 H47C 109.5 . . ? H47A C47 H47B 109.5 . . ? H47A C47 H47C 109.5 . . ? H47B C47 H47C 109.5 . . ? C41 C48 H48A 109.5 . . ? C41 C48 H48B 109.5 . . ? C41 C48 H48C 109.5 . . ? H48A C48 H48B 109.5 . . ? H48A C48 H48C 109.5 . . ? H48B C48 H48C 109.5 . . ? C50 C49 C19 120.8(7) . . ? C50 C49 C54 122.0(7) . . ? C54 C49 C19 117.2(7) . . ? C49 C50 C51 117.5(8) . . ? C49 C50 C56 122.4(7) . . ? C51 C50 C56 120.1(8) . . ? C50 C51 H51 118.2 . . ? C52 C51 C50 123.6(9) . . ? C52 C51 H51 118.2 . . ? C51 C52 C53 117.2(8) . . ? C51 C52 C57 122.8(10) . . ? C53 C52 C57 120.0(10) . . ? C52 C53 H53 118.8 . . ? C54 C53 C52 122.4(9) . . ? C54 C53 H53 118.8 . . ? C49 C54 C55 122.7(7) . . ? C53 C54 C49 117.3(9) . . ? C53 C54 C55 119.9(8) . . ? C54 C55 H55A 109.5 . . ? C54 C55 H55B 109.5 . . ? C54 C55 H55C 109.5 . . ? H55A C55 H55B 109.5 . . ? H55A C55 H55C 109.5 . . ? H55B C55 H55C 109.5 . . ? C50 C56 H56A 109.5 . . ? C50 C56 H56B 109.5 . . ? C50 C56 H56C 109.5 . . ? H56A C56 H56B 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? C52 C57 H57A 109.5 . . ? C52 C57 H57B 109.5 . . ? C52 C57 H57C 109.5 . . ? H57A C57 H57B 109.5 . . ? H57A C57 H57C 109.5 . . ? H57B C57 H57C 109.5 . . ? C32 C58 C37 121.3(7) . . ? C36 C58 C32 118.5(7) . . ? C36 C58 C37 120.2(7) . . ? F1 B1 N1 109.4(6) . . ? F1 B1 N7 108.8(6) . . ? F2 B1 F1 109.6(6) . . ? F2 B1 N1 111.0(6) . . ? F2 B1 N7 111.6(6) . . ? N7 B1 N1 106.3(6) . . ? C60 N0AA B2 125.4(6) . . ? C63 N0AA C60 107.7(6) . . ? C63 N0AA B2 126.7(6) . . ? C64 N1AA H1AA 125.5 . . ? C67 N1AA H1AA 125.5 . . ? C67 N1AA C64 109.0(6) . . ? C68 N2AA C71 104.2(6) . . ? C73 N3AA H3AA 125.2 . . ? C73 N3AA C76 109.6(5) . . ? C76 N3AA H3AA 125.2 . . ? C81 N4AA C78 105.4(6) . . ? C82 N5AA H5AA 125.3 . . ? C82 N5AA C85 109.4(6) . . ? C85 N5AA H5AA 125.3 . . ? C86 N6AA C89 109.0(6) . . ? C86 N6AA B2 126.8(6) . . ? C89 N6AA B2 123.8(6) . . ? C60 C59 C107 122.0(6) . . ? C89 C59 C60 118.9(7) . . ? C89 C59 C107 118.9(7) . . ? N0AA C60 C59 121.4(6) . . ? N0AA C60 C61 108.0(6) . . ? C59 C60 C61 130.5(7) . . ? C60 C61 H61 125.8 . . ? C62 C61 C60 108.4(7) . . ? C62 C61 H61 125.8 . . ? C61 C62 H62 126.7 . . ? C61 C62 C63 106.6(7) . . ? C63 C62 H62 126.7 . . ? N0AA C63 C62 109.3(7) . . ? N0AA C63 C64 128.0(7) . . ? C62 C63 C64 122.0(7) . . ? N1AA C64 C63 128.7(7) . . ? C65 C64 N1AA 106.7(6) . . ? C65 C64 C63 124.4(6) . . ? C64 C65 H65 125.5 . . ? C66 C65 C64 109.0(6) . . ? C66 C65 H65 125.5 . . ? C65 C66 H66 126.1 . . ? C65 C66 C67 107.8(7) . . ? C67 C66 H66 126.1 . . ? N1AA C67 C66 107.5(6) . . ? N1AA C67 C68 128.3(6) . . ? C66 C67 C68 123.6(7) . . ? N2AA C68 C67 127.3(7) . . ? N2AA C68 C69 111.1(6) . . ? C67 C68 C69 121.4(6) . . ? C68 C69 H69 126.8 . . ? C70 C69 C68 106.4(6) . . ? C70 C69 H69 126.8 . . ? C69 C70 H70 126.2 . . ? C69 C70 C71 107.6(7) . . ? C71 C70 H70 126.2 . . ? N2AA C71 C70 110.5(6) . . ? C72 C71 N2AA 127.4(7) . . ? C72 C71 C70 122.1(7) . . ? C71 C72 C73 127.8(6) . . ? C71 C72 C99 118.4(6) . . ? C73 C72 C99 113.8(6) . . ? N3AA C73 C72 126.5(6) . . ? N3AA C73 C74 107.5(6) . . ? C74 C73 C72 125.3(6) . . ? C73 C74 H74 126.0 . . ? C75 C74 C73 108.0(6) . . ? C75 C74 H74 126.0 . . ? C74 C75 H75 125.9 . . ? C74 C75 C76 108.2(6) . . ? C76 C75 H75 125.9 . . ? N3AA C76 C75 106.7(6) . . ? N3AA C76 C77 126.1(6) . . ? C75 C76 C77 126.7(6) . . ? C76 C77 C90 116.0(6) . . ? C78 C77 C76 127.6(6) . . ? C78 C77 C90 116.5(6) . . ? N4AA C78 C79 108.0(6) . . ? C77 C78 N4AA 127.9(6) . . ? C77 C78 C79 124.1(6) . . ? C78 C79 H79 125.8 . . ? C80 C79 C78 108.4(6) . . ? C80 C79 H79 125.8 . . ? C79 C80 H80 127.0 . . ? C79 C80 C81 105.9(6) . . ? C81 C80 H80 127.0 . . ? N4AA C81 C80 112.3(6) . . ? N4AA C81 C82 127.8(6) . . ? C82 C81 C80 119.0(6) . . ? N5AA C82 C81 126.6(6) . . ? C83 C82 N5AA 106.6(6) . . ? C83 C82 C81 125.9(6) . . ? C82 C83 H83 125.3 . . ? C84 C83 C82 109.4(7) . . ? C84 C83 H83 125.3 . . ? C83 C84 H84 125.8 . . ? C83 C84 C85 108.4(6) . . ? C85 C84 H84 125.8 . . ? N5AA C85 C84 106.2(6) . . ? N5AA C85 C86 130.2(6) . . ? C84 C85 C86 123.5(6) . . ? N6AA C86 C85 129.5(6) . . ? N6AA C86 C87 109.5(6) . . ? C87 C86 C85 120.9(6) . . ? C86 C87 H87 126.4 . . ? C88 C87 C86 107.2(6) . . ? C88 C87 H87 126.4 . . ? C87 C88 H88 126.3 . . ? C87 C88 C89 107.4(7) . . ? C89 C88 H88 126.3 . . ? N6AA C89 C88 106.9(6) . . ? C59 C89 N6AA 123.2(6) . . ? C59 C89 C88 129.8(7) . . ? C91 C90 C77 119.2(7) . . ? C98 C90 C77 117.9(7) . . ? C98 C90 C91 122.9(6) . . ? C90 C91 C92 117.1(8) . . ? C90 C91 C96 123.9(7) . . ? C92 C91 C96 119.0(8) . . ? C91 C92 H92 119.2 . . ? C93 C92 C91 121.7(7) . . ? C93 C92 H92 119.2 . . ? C92 C93 C97 120.9(8) . . ? C94 C93 C92 118.9(6) . . ? C94 C93 C97 120.2(8) . . ? C93 C94 H94 119.0 . . ? C93 C94 C98 122.1(8) . . ? C98 C94 H94 119.0 . . ? H95A C95 H95B 109.5 . . ? H95A C95 H95C 109.5 . . ? H95B C95 H95C 109.5 . . ? C98 C95 H95A 109.5 . . ? C98 C95 H95B 109.5 . . ? C98 C95 H95C 109.5 . . ? C91 C96 H96A 109.5 . . ? C91 C96 H96B 109.5 . . ? C91 C96 H96C 109.5 . . ? H96A C96 H96B 109.5 . . ? H96A C96 H96C 109.5 . . ? H96B C96 H96C 109.5 . . ? C93 C97 H97A 109.5 . . ? C93 C97 H97B 109.5 . . ? C93 C97 H97C 109.5 . . ? H97A C97 H97B 109.5 . . ? H97A C97 H97C 109.5 . . ? H97B C97 H97C 109.5 . . ? C90 C98 C94 117.4(7) . . ? C90 C98 C95 123.4(7) . . ? C94 C98 C95 119.2(7) . . ? C100 C99 C72 119.8(7) . . ? C100 C99 C116 118.8(7) . . ? C116 C99 C72 121.4(7) . . ? C99 C100 C105 119.4(7) . . ? C101 C100 C99 119.8(7) . . ? C101 C100 C105 120.8(8) . . ? C100 C101 H101 118.6 . . ? C102 C101 C100 122.7(8) . . ? C102 C101 H101 118.6 . . ? C101 C102 C103 117.5(7) . . ? C101 C102 C106 122.4(8) . . ? C103 C102 C106 120.1(8) . . ? C102 C103 H103 118.8 . . ? C116 C103 C102 122.3(8) . . ? C116 C103 H103 118.8 . . ? H10A C104 H10B 109.5 . . ? H10A C104 H10C 109.5 . . ? H10B C104 H10C 109.5 . . ? C116 C104 H10A 109.5 . . ? C116 C104 H10B 109.5 . . ? C116 C104 H10C 109.5 . . ? C100 C105 H10D 109.5 . . ? C100 C105 H10E 109.5 . . ? C100 C105 H10F 109.5 . . ? H10D C105 H10E 109.5 . . ? H10D C105 H10F 109.5 . . ? H10E C105 H10F 109.5 . . ? C102 C106 H10G 109.5 . . ? C102 C106 H10H 109.5 . . ? C102 C106 H10I 109.5 . . ? H10G C106 H10H 109.5 . . ? H10G C106 H10I 109.5 . . ? H10H C106 H10I 109.5 . . ? C108 C107 C59 120.2(7) . . ? C113 C107 C59 120.0(7) . . ? C113 C107 C108 119.8(7) . . ? C107 C108 C109 117.9(8) . . ? C107 C108 C115 122.6(7) . . ? C109 C108 C115 119.5(7) . . ? C108 C109 H109 118.8 . . ? C110 C109 C108 122.3(7) . . ? C110 C109 H109 118.8 . . ? C109 C110 C111 121.2(7) . . ? C109 C110 C112 118.3(7) . . ? C112 C110 C111 120.5(7) . . ? C110 C111 H11A 109.5 . . ? C110 C111 H11B 109.5 . . ? C110 C111 H11C 109.5 . . ? H11A C111 H11B 109.5 . . ? H11A C111 H11C 109.5 . . ? H11B C111 H11C 109.5 . . ? C110 C112 H112 119.5 . . ? C113 C112 C110 121.0(7) . . ? C113 C112 H112 119.5 . . ? C107 C113 C114 120.4(7) . . ? C112 C113 C107 120.7(7) . . ? C112 C113 C114 118.8(7) . . ? C113 C114 H11D 109.5 . . ? C113 C114 H11E 109.5 . . ? C113 C114 H11F 109.5 . . ? H11D C114 H11E 109.5 . . ? H11D C114 H11F 109.5 . . ? H11E C114 H11F 109.5 . . ? C108 C115 H11G 109.5 . . ? C108 C115 H11H 109.5 . . ? C108 C115 H11I 109.5 . . ? H11G C115 H11H 109.5 . . ? H11G C115 H11I 109.5 . . ? H11H C115 H11I 109.5 . . ? C99 C116 C104 121.3(7) . . ? C103 C116 C99 118.7(7) . . ? C103 C116 C104 120.0(7) . . ? F3 B2 N0AA 111.2(6) . . ? F3 B2 N6AA 108.9(6) . . ? F4 B2 F3 108.5(6) . . ? F4 B2 N0AA 110.2(6) . . ? F4 B2 N6AA 110.9(6) . . ? N0AA B2 N6AA 107.1(5) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag F1 B1 1.407(8) . ? F2 B1 1.362(10) . ? N1 C28 1.358(9) . ? N1 C31 1.380(9) . ? N1 B1 1.559(9) . ? N2 H2 0.8800 . ? N2 C24 1.374(10) . ? N2 C27 1.382(9) . ? N3 C20 1.424(9) . ? N3 C23 1.322(9) . ? N4 H4 0.8800 . ? N4 C15 1.408(9) . ? N4 C18 1.383(8) . ? N5 C10 1.344(8) . ? N5 C13 1.393(8) . ? N6 H6 0.8800 . ? N6 C6 1.382(8) . ? N6 C9 1.391(9) . ? N7 C2 1.400(9) . ? N7 C5 1.367(9) . ? N7 B1 1.542(9) . ? C1 C2 1.393(10) . ? C1 C31 1.412(10) . ? C1 C32 1.495(10) . ? C2 C3 1.385(10) . ? C3 H3 0.9500 . ? C3 C4 1.398(9) . ? C4 H4A 0.9500 . ? C4 C5 1.409(9) . ? C5 C6 1.450(9) . ? C6 C7 1.382(9) . ? C7 H7 0.9500 . ? C7 C8 1.398(10) . ? C8 H8 0.9500 . ? C8 C9 1.386(9) . ? C9 C10 1.433(9) . ? C10 C11 1.456(9) . ? C11 H11 0.9500 . ? C11 C12 1.367(9) . ? C12 H12 0.9500 . ? C12 C13 1.446(10) . ? C13 C14 1.370(9) . ? C14 C15 1.413(10) . ? C14 C40 1.485(9) . ? C15 C16 1.404(9) . ? C16 H16 0.9500 . ? C16 C17 1.380(10) . ? C17 H17 0.9500 . ? C17 C18 1.396(10) . ? C18 C19 1.442(10) . ? C19 C20 1.340(10) . ? C19 C49 1.519(10) . ? C20 C21 1.447(10) . ? C21 H21 0.9500 . ? C21 C22 1.337(10) . ? C22 H22 0.9500 . ? C22 C23 1.444(11) . ? C23 C24 1.458(10) . ? C24 C25 1.384(11) . ? C25 H25 0.9500 . ? C25 C26 1.380(13) . ? C26 H26 0.9500 . ? C26 C27 1.395(12) . ? C27 C28 1.438(11) . ? C28 C29 1.423(10) . ? C29 H29 0.9500 . ? C29 C30 1.351(11) . ? C30 H30 0.9500 . ? C30 C31 1.422(10) . ? C32 C33 1.398(11) . ? C32 C58 1.422(10) . ? C33 C34 1.401(9) . ? C33 C38 1.511(9) . ? C34 H34 0.9500 . ? C34 C35 1.406(10) . ? C35 C36 1.360(12) . ? C35 C39 1.503(10) . ? C36 H36 0.9500 . ? C36 C58 1.379(10) . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C37 C58 1.492(10) . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 C41 1.403(11) . ? C40 C45 1.428(12) . ? C41 C42 1.409(10) . ? C41 C48 1.492(13) . ? C42 H42 0.9500 . ? C42 C43 1.415(14) . ? C43 C44 1.378(15) . ? C43 C47 1.492(10) . ? C44 H44 0.9500 . ? C44 C45 1.406(10) . ? C45 C46 1.482(12) . ? C46 H46A 0.9800 . ? C46 H46B 0.9800 . ? C46 H46C 0.9800 . ? C47 H47A 0.9800 . ? C47 H47B 0.9800 . ? C47 H47C 0.9800 . ? C48 H48A 0.9800 . ? C48 H48B 0.9800 . ? C48 H48C 0.9800 . ? C49 C50 1.377(12) . ? C49 C54 1.426(12) . ? C50 C51 1.396(11) . ? C50 C56 1.496(13) . ? C51 H51 0.9500 . ? C51 C52 1.377(14) . ? C52 C53 1.405(14) . ? C52 C57 1.524(11) . ? C53 H53 0.9500 . ? C53 C54 1.385(11) . ? C54 C55 1.484(12) . ? C55 H55A 0.9800 . ? C55 H55B 0.9800 . ? C55 H55C 0.9800 . ? C56 H56A 0.9800 . ? C56 H56B 0.9800 . ? C56 H56C 0.9800 . ? C57 H57A 0.9800 . ? C57 H57B 0.9800 . ? C57 H57C 0.9800 . ? F3 B2 1.399(10) . ? F4 B2 1.374(8) . ? N0AA C60 1.390(9) . ? N0AA C63 1.361(10) . ? N0AA B2 1.544(9) . ? N1AA H1AA 0.8800 . ? N1AA C64 1.396(9) . ? N1AA C67 1.371(9) . ? N2AA C68 1.353(9) . ? N2AA C71 1.404(9) . ? N3AA H3AA 0.8800 . ? N3AA C73 1.367(9) . ? N3AA C76 1.377(9) . ? N4AA C78 1.404(8) . ? N4AA C81 1.338(9) . ? N5AA H5AA 0.8800 . ? N5AA C82 1.387(9) . ? N5AA C85 1.388(8) . ? N6AA C86 1.340(9) . ? N6AA C89 1.399(9) . ? N6AA B2 1.545(9) . ? C59 C60 1.405(11) . ? C59 C89 1.377(11) . ? C59 C107 1.489(10) . ? C60 C61 1.411(11) . ? C61 H61 0.9500 . ? C61 C62 1.370(11) . ? C62 H62 0.9500 . ? C62 C63 1.424(10) . ? C63 C64 1.447(10) . ? C64 C65 1.379(11) . ? C65 H65 0.9500 . ? C65 C66 1.378(11) . ? C66 H66 0.9500 . ? C66 C67 1.394(10) . ? C67 C68 1.433(10) . ? C68 C69 1.477(10) . ? C69 H69 0.9500 . ? C69 C70 1.321(10) . ? C70 H70 0.9500 . ? C70 C71 1.443(11) . ? C71 C72 1.378(10) . ? C72 C73 1.456(10) . ? C72 C99 1.480(9) . ? C73 C74 1.395(9) . ? C74 H74 0.9500 . ? C74 C75 1.374(10) . ? C75 H75 0.9500 . ? C75 C76 1.402(9) . ? C76 C77 1.421(10) . ? C77 C78 1.367(10) . ? C77 C90 1.528(9) . ? C78 C79 1.470(10) . ? C79 H79 0.9500 . ? C79 C80 1.319(10) . ? C80 H80 0.9500 . ? C80 C81 1.456(9) . ? C81 C82 1.437(9) . ? C82 C83 1.381(9) . ? C83 H83 0.9500 . ? C83 C84 1.366(10) . ? C84 H84 0.9500 . ? C84 C85 1.399(10) . ? C85 C86 1.437(10) . ? C86 C87 1.424(9) . ? C87 H87 0.9500 . ? C87 C88 1.380(10) . ? C88 H88 0.9500 . ? C88 C89 1.439(10) . ? C90 C91 1.396(12) . ? C90 C98 1.378(12) . ? C91 C92 1.421(10) . ? C91 C96 1.502(12) . ? C92 H92 0.9500 . ? C92 C93 1.381(12) . ? C93 C94 1.374(11) . ? C93 C97 1.492(10) . ? C94 H94 0.9500 . ? C94 C98 1.417(10) . ? C95 H95A 0.9800 . ? C95 H95B 0.9800 . ? C95 H95C 0.9800 . ? C95 C98 1.504(11) . ? C96 H96A 0.9800 . ? C96 H96B 0.9800 . ? C96 H96C 0.9800 . ? C97 H97A 0.9800 . ? C97 H97B 0.9800 . ? C97 H97C 0.9800 . ? C99 C100 1.396(11) . ? C99 C116 1.416(10) . ? C100 C101 1.383(11) . ? C100 C105 1.517(12) . ? C101 H101 0.9500 . ? C101 C102 1.364(12) . ? C102 C103 1.393(12) . ? C102 C106 1.504(10) . ? C103 H103 0.9500 . ? C103 C116 1.389(10) . ? C104 H10A 0.9800 . ? C104 H10B 0.9800 . ? C104 H10C 0.9800 . ? C104 C116 1.488(11) . ? C105 H10D 0.9800 . ? C105 H10E 0.9800 . ? C105 H10F 0.9800 . ? C106 H10G 0.9800 . ? C106 H10H 0.9800 . ? C106 H10I 0.9800 . ? C107 C108 1.411(11) . ? C107 C113 1.399(11) . ? C108 C109 1.413(11) . ? C108 C115 1.492(12) . ? C109 H109 0.9500 . ? C109 C110 1.380(12) . ? C110 C111 1.513(10) . ? C110 C112 1.404(10) . ? C111 H11A 0.9800 . ? C111 H11B 0.9800 . ? C111 H11C 0.9800 . ? C112 H112 0.9500 . ? C112 C113 1.376(10) . ? C113 C114 1.499(11) . ? C114 H11D 0.9800 . ? C114 H11E 0.9800 . ? C114 H11F 0.9800 . ? C115 H11G 0.9800 . ? C115 H11H 0.9800 . ? C115 H11I 0.9800 . ? loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 -0.564 0.240 0.755 554 145 ' ' 2 0.564 0.740 0.245 554 145 ' '