#------------------------------------------------------------------------------ #$Date: 2024-06-12 05:07:36 +0300 (Wed, 12 Jun 2024) $ #$Revision: 292295 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/18/1571807.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1571807 loop_ _publ_author_name 'Shin, Jeongcheol' 'Kim, Jin' 'Choi, Jonghoon' _publ_section_title ; Triacetonitrile(1,4,7-trimethyl-1,4,7-triazacyclononane)cobalt(II) bis(tetraphenylborate) ; _journal_coeditor_code BX4029 _journal_issue 6 _journal_name_full IUCrData _journal_paper_doi 10.1107/S241431462400539X _journal_volume 9 _journal_year 2024 _chemical_formula_iupac '[Co (C2 H3 N)3 (C9 H21 N3)] (C24 H20 B)2' _chemical_formula_moiety 'C15 H30 Co N6 2+, 2(C24 H20 B -)' _chemical_formula_sum 'C63 H70 B2 Co N6' _chemical_formula_weight 991.80 _chemical_name_systematic ; Triacetonitrile(1,4,7-trimethyl-1,4,7-triazacyclononane)cobalt(II) bis(tetraphenylborate) ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90.332(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.1245(16) _cell_length_b 11.6689(10) _cell_length_c 26.067(2) _cell_measurement_reflns_used 9821 _cell_measurement_temperature 133(2) _cell_measurement_theta_max 24.65 _cell_measurement_theta_min 2.21 _cell_volume 5512.9(8) _computing_cell_refinement ; SAINT (Bruker, 2014) ; _computing_data_collection ; APEX2 (Bruker, 2014) ; _computing_data_reduction ; SAINT (Bruker, 2014) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; CIFTAB (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 133(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEXII CCD detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0958 _diffrn_reflns_av_unetI/netI 0.0525 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 112545 _diffrn_reflns_theta_full 24.757 _diffrn_reflns_theta_max 24.757 _diffrn_reflns_theta_min 1.912 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.356 _exptl_absorpt_correction_T_max 0.7451 _exptl_absorpt_correction_T_min 0.6273 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.195 _exptl_crystal_density_method 'not measured' _exptl_crystal_description platy _exptl_crystal_F_000 2108 _exptl_crystal_size_max 0.101 _exptl_crystal_size_mid 0.089 _exptl_crystal_size_min 0.051 _refine_diff_density_max 0.593 _refine_diff_density_min -0.632 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.142 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 655 _refine_ls_number_reflns 9437 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.142 _refine_ls_R_factor_all 0.0897 _refine_ls_R_factor_gt 0.0562 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0330P)^2^+3.7116P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0971 _refine_ls_wR_factor_ref 0.1069 _reflns_number_gt 6984 _reflns_number_total 9437 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file bx4029.cif _cod_data_source_block I _cod_original_cell_volume 5513.0(8) _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 1571807 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.965 _shelx_estimated_absorpt_t_max 0.982 _shelx_hkl_file ; 0 -1 0 -2.30 0.70 0 -1 0 -1.70 1.50 0 -1 0 -3.40 0.70 0 -1 0 -2.00 1.30 0 -1 0 -3.20 0.90 0 -1 0 -2.40 0.60 0 1 0 -3.70 0.60 0 1 0 -2.40 0.60 0 1 0 -2.60 0.80 0 1 0 -3.90 1.10 0 1 0 -3.10 0.80 0 -2 0 2130.59 51.99 0 -2 0 2160.18 49.10 0 -2 0 2161.68 49.80 0 -2 0 2349.56 49.50 0 -2 0 1900.41 49.90 0 -2 0 2239.78 48.40 0 2 0 2061.29 49.99 0 2 0 2190.88 48.40 0 2 0 2110.89 51.69 0 2 0 2245.18 49.30 0 2 0 2176.68 49.10 0 2 0 2186.78 49.90 0 -3 0 -0.40 2.70 0 -3 0 1.20 1.40 0 -3 0 10.10 6.60 0 -3 0 1.90 4.00 0 -3 0 0.30 3.90 0 -3 0 7.50 8.10 0 -3 0 4.60 3.80 0 -3 0 2.60 4.40 0 3 0 0.20 3.60 0 3 0 1.40 3.90 0 3 0 11.30 5.60 0 3 0 7.30 4.70 0 3 0 -1.80 2.80 0 3 0 5.10 5.90 0 -4 0 28.00 5.80 0 -4 0 44.60 11.60 0 -4 0 45.00 9.50 0 4 0 26.80 4.30 0 4 0 21.10 2.40 0 4 0 35.90 6.20 0 4 0 28.20 5.80 0 4 0 31.10 7.40 0 -5 0 4.90 8.20 0 -5 0 2.00 5.20 0 -5 0 8.90 10.50 0 5 0 1.30 4.80 0 5 0 -0.10 3.50 0 5 0 0.60 5.00 0 -6 0 135.89 17.20 0 -6 0 113.89 10.50 0 -6 0 131.39 14.00 0 6 0 120.69 7.80 0 6 0 132.29 12.40 0 6 0 127.69 9.10 0 -7 0 -0.40 7.20 0 -7 0 17.90 10.40 0 -7 0 5.10 13.60 0 7 0 3.80 6.50 0 7 0 1.60 7.30 0 7 0 -2.20 4.60 0 -8 0 73.49 16.10 0 -8 0 58.09 11.00 0 -8 0 59.09 13.60 0 8 0 47.40 7.30 0 8 0 39.60 9.40 0 8 0 50.79 11.00 0 -9 0 1.20 9.80 0 -9 0 -2.60 17.10 0 -9 0 13.00 11.40 0 9 0 3.80 6.00 0 9 0 5.00 11.20 0 9 0 0.60 8.40 0 -10 0 0.30 10.20 0 -10 0 3.40 10.90 0 -10 0 -12.50 17.80 0 10 0 -5.50 10.80 0 10 0 8.50 9.20 0 10 0 5.50 6.60 0 -11 0 -4.60 10.60 0 -11 0 -43.00 16.70 0 11 0 -9.40 6.40 0 11 0 2.00 6.70 0 -12 0 -32.90 18.10 0 -12 0 3.20 11.50 0 12 0 -5.40 6.40 0 12 0 -19.20 11.30 0 12 0 -12.30 9.00 0 -13 0 -30.30 18.90 0 -13 0 -17.60 11.60 0 13 0 3.70 7.20 0 13 0 4.30 10.50 1 13 0 22.70 9.10 1 13 0 6.20 10.70 -1 -13 0 -7.20 12.20 -1 -13 0 -12.80 20.90 1 12 0 8.90 7.40 1 12 0 -7.60 9.20 -1 -12 0 -19.30 11.90 -1 -12 0 3.00 20.50 1 11 0 2.40 11.20 1 11 0 3.00 8.90 1 11 0 5.50 6.80 -1 -11 0 3.70 10.60 -1 -11 0 19.70 20.60 1 10 0 129.49 17.10 1 10 0 152.18 13.60 1 10 0 160.88 12.20 -1 -10 0 167.98 20.20 -1 -10 0 154.08 25.70 -1 -10 0 176.08 17.30 1 9 0 57.29 13.20 1 9 0 61.29 11.00 1 9 0 61.99 8.60 -1 -9 0 69.99 16.30 -1 -9 0 62.49 12.10 -1 -9 0 61.89 20.40 1 8 0 6.30 5.80 1 8 0 5.50 8.00 1 8 0 6.20 8.70 -1 -8 0 16.70 14.00 -1 -8 0 15.70 17.20 -1 -8 0 -5.90 8.50 1 7 0 217.98 10.90 1 7 0 217.38 13.40 1 7 0 223.38 14.60 -1 -7 0 208.98 19.60 -1 -7 0 232.88 13.90 -1 -7 0 217.68 22.90 1 6 0 4.50 5.90 1 6 0 0.80 5.80 1 6 0 -1.30 4.10 -1 -6 0 19.70 13.00 -1 -6 0 1.20 6.00 -1 -6 0 4.50 10.70 1 5 0 8.10 5.10 1 5 0 8.90 5.20 1 5 0 4.80 3.90 -1 -5 0 17.40 11.00 -1 -5 0 14.30 9.20 -1 -5 0 9.90 5.50 1 4 0 58.49 7.90 1 4 0 30.20 4.60 1 4 0 40.90 5.30 1 4 0 43.80 7.50 -1 -4 0 45.30 10.10 -1 -4 0 29.70 6.00 -1 -4 0 34.90 9.60 -1 -4 0 38.80 5.60 1 3 0 1794.32 42.20 1 3 0 1792.52 42.20 1 3 0 1700.53 40.60 1 3 0 1700.73 39.50 1 3 0 1711.83 40.90 1 3 0 1719.23 40.80 -1 -3 0 1606.24 42.90 -1 -3 0 1684.43 41.90 -1 -3 0 1624.04 45.00 -1 -3 0 1688.43 42.30 -1 -3 0 1665.73 40.40 -1 -3 0 1676.63 40.60 1 2 0 768.52 19.70 1 2 0 764.12 18.70 1 2 0 765.82 21.00 1 2 0 752.82 18.50 1 2 0 738.43 18.40 1 2 0 704.53 18.30 1 2 0 734.03 17.80 -1 -2 0 724.93 17.80 -1 -2 0 736.63 18.50 -1 -2 0 747.03 20.00 -1 -2 0 699.13 18.30 -1 -2 0 719.33 21.00 -1 -2 0 717.83 18.20 -1 -2 0 749.42 18.50 1 1 0 980.30 22.40 1 1 0 1036.70 23.60 1 1 0 810.92 22.00 1 1 0 980.40 22.00 -1 -1 0 959.60 22.00 -1 -1 0 990.80 22.20 -1 -1 0 949.51 22.30 -1 -1 0 977.30 23.50 -1 -1 0 971.50 21.70 -1 -1 0 992.60 22.30 -1 -1 0 1001.50 23.20 1 0 0 0.50 0.30 1 0 0 1.90 0.50 1 0 0 -0.20 0.30 1 0 0 0.00 0.20 -1 0 0 0.50 0.40 -1 0 0 0.60 0.30 -1 0 0 0.30 0.40 -1 0 0 0.80 0.30 -1 0 0 0.00 0.30 -1 0 0 0.40 0.60 1 -1 0 1002.00 23.30 1 -1 0 929.61 22.50 1 -1 0 964.70 23.40 1 -1 0 998.20 23.30 1 -1 0 1017.10 22.50 -1 1 0 989.80 22.50 -1 1 0 981.00 22.60 -1 1 0 943.81 23.50 -1 1 0 991.20 22.00 1 -2 0 717.23 17.80 1 -2 0 728.53 17.90 1 -2 0 717.73 19.80 1 -2 0 719.13 18.00 1 -2 0 700.63 18.00 1 -2 0 734.43 17.00 1 -2 0 731.13 19.30 -1 2 0 698.13 18.00 -1 2 0 713.53 19.30 -1 2 0 702.73 20.00 -1 2 0 694.53 18.10 -1 2 0 728.23 17.10 -1 2 0 724.53 18.00 -1 2 0 688.33 17.90 1 -3 0 1678.63 41.30 1 -3 0 1720.43 40.10 1 -3 0 1669.03 43.20 1 -3 0 1716.93 39.00 1 -3 0 1698.53 38.30 1 -3 0 1661.13 40.00 -1 3 0 1700.73 41.70 -1 3 0 1728.23 38.50 -1 3 0 1676.33 39.90 -1 3 0 1557.04 43.40 -1 3 0 1466.75 40.50 -1 3 0 1660.63 39.70 -1 3 0 1650.93 39.00 1 -4 0 36.90 7.20 1 -4 0 32.40 4.10 1 -4 0 43.70 10.70 1 -4 0 43.30 6.50 -1 4 0 41.20 7.00 -1 4 0 33.60 5.90 -1 4 0 36.50 4.40 -1 4 0 39.40 4.80 -1 4 0 42.90 8.10 1 -5 0 9.60 2.80 1 -5 0 8.50 5.60 1 -5 0 5.60 6.00 1 -5 0 -0.80 9.40 -1 5 0 6.70 5.70 -1 5 0 5.00 6.90 -1 5 0 10.30 4.00 -1 5 0 9.10 3.70 1 -6 0 3.80 6.20 1 -6 0 14.10 11.80 1 -6 0 2.90 6.90 -1 6 0 9.00 6.00 -1 6 0 4.70 2.60 -1 6 0 3.00 4.00 -1 6 0 0.20 4.30 -1 6 0 6.90 6.80 1 -7 0 237.88 14.20 1 -7 0 216.98 14.50 1 -7 0 236.58 21.60 -1 7 0 205.08 13.20 -1 7 0 202.58 10.40 -1 7 0 228.38 7.80 -1 7 0 202.28 10.00 -1 7 0 229.68 15.60 1 -8 0 -0.20 15.10 1 -8 0 1.70 8.70 1 -8 0 0.70 8.70 -1 8 0 5.50 9.20 -1 8 0 1.10 5.30 -1 8 0 5.40 6.30 1 -9 0 70.29 12.30 1 -9 0 76.69 19.40 1 -9 0 65.39 12.10 -1 9 0 55.19 10.90 -1 9 0 62.69 8.50 -1 9 0 68.99 14.80 1 -10 0 184.58 16.50 1 -10 0 158.48 17.00 1 -10 0 191.38 25.40 -1 10 0 147.59 18.80 -1 10 0 153.98 15.60 -1 10 0 163.18 11.90 1 -11 0 -0.80 10.50 1 -11 0 -14.40 16.50 -1 11 0 7.00 9.60 -1 11 0 -13.80 13.30 -1 11 0 11.30 7.60 1 -12 0 -13.80 18.20 1 -12 0 -13.20 11.20 -1 12 0 5.00 10.00 -1 12 0 6.30 7.80 -1 12 0 -20.80 11.70 1 -13 0 9.70 13.30 1 -13 0 5.30 20.20 1 -13 0 12.80 7.70 -1 13 0 3.70 7.10 -1 13 0 13.00 10.90 2 13 0 4.30 8.80 2 13 0 -12.50 9.80 -2 -13 0 -11.00 11.90 -2 -13 0 -38.30 19.80 2 12 0 34.70 11.60 2 12 0 36.40 9.00 -2 -12 0 33.00 12.90 -2 -12 0 7.20 22.50 2 11 0 -4.30 8.80 2 11 0 1.70 6.80 -2 -11 0 -13.10 10.10 -2 -11 0 -7.10 19.70 2 10 0 213.48 20.00 2 10 0 207.68 13.50 2 10 0 236.28 17.30 -2 -10 0 247.38 18.80 -2 -10 0 217.58 24.60 -2 -10 0 233.08 29.60 2 9 0 4.40 6.60 2 9 0 -5.90 10.00 2 9 0 7.40 8.80 -2 -9 0 12.40 18.90 -2 -9 0 4.20 15.30 -2 -9 0 -3.50 10.50 2 8 0 46.40 9.60 2 8 0 48.70 7.60 2 8 0 56.79 11.30 -2 -8 0 43.60 10.20 -2 -8 0 66.79 17.40 -2 -8 0 62.19 19.60 2 7 0 56.99 8.90 2 7 0 43.60 9.10 2 7 0 42.00 6.70 -2 -7 0 48.80 15.30 -2 -7 0 63.09 17.20 -2 -7 0 51.69 9.10 2 6 0 8.40 4.70 2 6 0 18.50 6.50 2 6 0 20.10 7.10 -2 -6 0 18.40 12.70 -2 -6 0 12.70 12.00 -2 -6 0 15.60 6.50 2 5 0 567.94 17.00 2 5 0 580.14 19.10 2 5 0 566.14 18.50 2 5 0 576.34 19.00 -2 -5 0 575.14 18.80 -2 -5 0 565.84 25.00 -2 -5 0 539.25 23.40 2 4 0 484.85 15.80 2 4 0 502.35 16.00 2 4 0 482.45 14.60 2 4 0 491.75 16.20 -2 -4 0 488.75 16.20 -2 -4 0 479.85 15.00 -2 -4 0 502.25 20.50 -2 -4 0 477.25 22.20 2 3 0 2014.80 46.20 2 3 0 1919.21 45.60 2 3 0 2075.79 48.60 2 3 0 1989.20 46.80 2 3 0 1977.40 44.70 2 3 0 1975.80 46.50 -2 -3 0 1890.61 47.60 -2 -3 0 1943.31 50.89 -2 -3 0 1985.30 49.20 -2 -3 0 1956.50 46.70 -2 -3 0 1949.70 45.70 -2 -3 0 1962.40 44.90 2 2 0 15.20 2.60 2 2 0 15.30 3.00 2 2 0 18.10 2.40 2 2 0 14.60 3.50 2 2 0 16.90 2.70 2 2 0 16.00 2.60 2 2 0 19.90 3.90 -2 -2 0 19.10 4.50 -2 -2 0 16.10 2.10 -2 -2 0 18.20 4.00 -2 -2 0 14.80 2.60 -2 -2 0 15.70 2.60 -2 -2 0 21.70 3.00 -2 -2 0 17.80 2.60 2 1 0 2292.57 50.89 2 1 0 2323.87 52.59 2 1 0 2309.77 52.49 2 1 0 2283.07 50.69 2 1 0 2306.37 52.59 2 1 0 2299.37 52.49 2 1 0 2249.57 51.29 -2 -1 0 2306.97 52.59 -2 -1 0 2303.37 50.69 -2 -1 0 2191.68 52.49 -2 -1 0 2293.97 50.79 -2 -1 0 2214.48 52.39 -2 -1 0 2289.77 51.39 -2 -1 0 2347.67 52.59 2 0 0 36.80 2.70 2 0 0 34.70 3.00 2 0 0 38.60 2.20 2 0 0 33.60 1.60 2 0 0 38.70 2.30 -2 0 0 38.40 1.70 -2 0 0 34.40 2.20 -2 0 0 31.20 2.40 -2 0 0 37.40 3.10 -2 0 0 40.20 2.20 -2 0 0 38.40 2.60 -2 0 0 35.40 2.40 2 -1 0 2302.17 50.89 2 -1 0 2335.47 51.79 2 -1 0 2270.87 50.39 2 -1 0 2303.67 51.59 2 -1 0 2299.57 53.39 2 -1 0 2337.67 52.89 2 -1 0 2288.57 52.29 -2 1 0 2300.37 50.39 -2 1 0 2231.98 53.29 -2 1 0 2287.47 51.69 -2 1 0 2251.67 50.89 -2 1 0 2307.97 51.49 -2 1 0 2305.17 52.29 -2 1 0 2267.37 52.79 2 -2 0 15.50 2.60 2 -2 0 16.90 2.00 2 -2 0 18.40 3.60 2 -2 0 18.20 3.30 2 -2 0 19.00 4.30 2 -2 0 15.50 2.70 2 -2 0 14.70 1.90 2 -2 0 12.40 3.20 -2 2 0 16.40 3.10 -2 2 0 14.40 2.70 -2 2 0 13.30 2.00 -2 2 0 17.10 4.20 -2 2 0 16.70 3.40 -2 2 0 14.50 2.60 -2 2 0 17.10 3.80 2 -3 0 1960.90 49.00 2 -3 0 2006.70 44.70 2 -3 0 1963.70 47.00 2 -3 0 1952.50 46.50 2 -3 0 1967.50 45.80 -2 3 0 1952.60 48.80 -2 3 0 1926.41 46.30 -2 3 0 1982.90 44.70 -2 3 0 1934.31 47.10 -2 3 0 1920.21 46.20 2 -4 0 488.85 15.20 2 -4 0 486.25 19.90 2 -4 0 482.35 15.30 2 -4 0 482.75 16.20 -2 4 0 491.25 18.40 -2 4 0 479.85 13.70 -2 4 0 459.45 16.80 -2 4 0 471.35 15.80 -2 4 0 486.85 15.60 2 -5 0 577.44 17.30 2 -5 0 558.74 18.00 2 -5 0 580.84 18.90 -2 5 0 627.94 18.90 -2 5 0 569.64 17.80 -2 5 0 536.95 16.00 -2 5 0 554.04 21.10 -2 5 0 474.25 19.80 2 -6 0 9.10 6.60 2 -6 0 19.20 11.10 2 -6 0 13.20 5.90 2 -6 0 12.10 3.90 -2 6 0 12.80 5.30 -2 6 0 16.80 6.30 -2 6 0 12.10 4.30 -2 6 0 14.60 7.50 -2 6 0 11.20 3.60 2 -7 0 41.10 5.50 2 -7 0 57.79 9.00 2 -7 0 43.40 8.90 2 -7 0 55.99 14.20 -2 7 0 46.10 6.70 -2 7 0 47.50 11.20 -2 7 0 44.70 7.30 -2 7 0 44.50 8.30 -2 7 0 57.79 5.70 2 -8 0 65.59 16.90 2 -8 0 61.59 10.10 2 -8 0 53.19 10.70 -2 8 0 55.19 10.20 -2 8 0 55.49 12.20 -2 8 0 45.30 7.50 -2 8 0 44.20 8.40 2 -9 0 3.00 15.30 2 -9 0 1.60 9.80 2 -9 0 3.00 7.70 -2 9 0 -3.40 10.20 -2 9 0 -9.00 8.00 -2 9 0 0.10 6.40 2 -10 0 231.58 18.60 2 -10 0 224.08 26.30 -2 10 0 219.28 21.10 -2 10 0 245.18 13.40 -2 10 0 229.08 15.60 2 -11 0 -2.40 17.20 2 -11 0 2.40 6.70 2 -11 0 -12.50 10.30 -2 11 0 0.80 7.00 -2 11 0 -3.30 9.10 2 -12 0 20.80 12.40 2 -12 0 33.30 19.30 2 -12 0 24.70 7.90 -2 12 0 18.30 11.10 -2 12 0 -8.70 15.10 -2 12 0 43.80 8.80 2 -13 0 -27.90 11.50 2 -13 0 -23.30 17.70 2 -13 0 15.10 7.60 -2 13 0 -0.70 10.60 -2 13 0 2.40 7.10 3 13 0 45.50 12.90 3 13 0 38.30 9.60 -3 -13 0 -5.20 23.50 -3 -13 0 44.50 14.70 3 12 0 3.80 9.90 3 12 0 1.40 7.20 -3 -12 0 -7.20 10.70 -3 -12 0 -29.90 20.20 3 11 0 11.40 7.20 3 11 0 -5.30 9.00 -3 -11 0 -2.40 16.70 -3 -11 0 -31.80 19.40 -3 -11 0 -4.10 10.40 3 10 0 136.49 12.00 3 10 0 132.09 14.80 3 10 0 134.79 16.90 -3 -10 0 122.19 26.30 -3 -10 0 156.38 16.50 -3 -10 0 122.79 22.20 3 9 0 0.50 9.50 3 9 0 0.10 8.60 3 9 0 11.00 6.80 -3 -9 0 3.70 17.00 -3 -9 0 16.20 19.60 -3 -9 0 7.40 9.40 3 8 0 24.60 9.50 3 8 0 24.00 7.00 3 8 0 32.30 9.20 -3 -8 0 24.30 17.30 -3 -8 0 28.80 9.80 -3 -8 0 44.40 19.40 3 7 0 39.40 8.20 3 7 0 25.40 6.30 3 7 0 36.00 9.00 -3 -7 0 28.00 8.30 -3 -7 0 52.39 16.70 -3 -7 0 47.80 15.90 3 6 0 61.39 7.90 3 6 0 61.89 8.10 3 6 0 49.40 7.80 3 6 0 43.10 6.20 -3 -6 0 57.59 14.80 -3 -6 0 54.79 8.10 -3 -6 0 61.69 13.70 3 5 0 18.30 5.70 3 5 0 13.70 5.30 3 5 0 12.80 4.50 3 5 0 19.00 5.60 -3 -5 0 7.90 5.50 -3 -5 0 16.30 4.30 -3 -5 0 24.60 9.10 -3 -5 0 22.50 4.50 -3 -5 0 21.60 11.10 -3 -5 0 16.90 2.40 3 4 0 29.70 5.70 3 4 0 34.90 4.90 3 4 0 30.20 5.30 3 4 0 31.30 3.70 3 4 0 31.60 5.10 -3 -4 0 32.80 10.10 -3 -4 0 35.60 4.80 -3 -4 0 29.30 5.90 -3 -4 0 45.70 5.70 -3 -4 0 43.30 9.50 3 3 0 338.17 11.00 3 3 0 328.57 11.40 3 3 0 343.97 12.10 3 3 0 348.77 10.60 3 3 0 332.37 11.10 -3 -3 0 347.27 16.10 -3 -3 0 342.87 10.00 -3 -3 0 339.57 14.60 -3 -3 0 339.27 11.60 -3 -3 0 337.07 11.40 3 2 0 2656.73 60.89 3 2 0 2741.83 61.89 3 2 0 2745.63 63.79 3 2 0 2722.83 62.79 3 2 0 2707.73 60.99 3 2 0 2723.33 60.79 3 2 0 2890.11 64.39 -3 -2 0 2664.83 61.69 -3 -2 0 2696.73 63.99 -3 -2 0 2661.93 60.19 -3 -2 0 2632.04 62.69 -3 -2 0 2751.62 60.99 -3 -2 0 2712.83 60.89 -3 -2 0 2560.44 63.69 -3 -2 0 2674.53 64.09 3 1 0 1801.02 45.30 3 1 0 1996.80 45.50 3 1 0 1896.31 42.60 3 1 0 1911.31 43.20 3 1 0 1904.91 44.00 3 1 0 1930.91 46.10 3 1 0 1909.71 42.70 -3 -1 0 1922.01 45.70 -3 -1 0 1897.21 45.30 -3 -1 0 1898.01 46.00 -3 -1 0 1902.31 42.70 -3 -1 0 1969.40 43.20 -3 -1 0 1929.71 44.00 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12.60 -4 -9 0 89.69 23.10 -4 -9 0 63.69 20.80 4 8 0 9.30 8.60 4 8 0 11.20 8.20 4 8 0 4.80 6.20 -4 -8 0 0.30 17.50 -4 -8 0 5.40 8.70 -4 -8 0 14.80 17.50 4 7 0 139.49 12.40 4 7 0 147.39 12.00 4 7 0 145.09 12.30 4 7 0 120.99 9.70 -4 -7 0 152.28 21.00 -4 -7 0 139.39 12.50 -4 -7 0 128.49 17.80 4 6 0 126.89 10.60 4 6 0 127.29 8.80 4 6 0 136.39 10.10 4 6 0 134.19 10.30 -4 -6 0 120.69 8.00 -4 -6 0 123.99 10.70 -4 -6 0 131.69 5.60 -4 -6 0 117.49 8.40 -4 -6 0 142.29 17.60 -4 -6 0 145.59 18.80 4 5 0 24.50 5.20 4 5 0 25.30 6.00 4 5 0 12.80 4.80 4 5 0 19.70 3.70 4 5 0 18.90 5.80 -4 -5 0 23.60 5.60 -4 -5 0 18.00 3.90 -4 -5 0 16.20 5.90 -4 -5 0 30.80 9.70 -4 -5 0 28.70 9.50 4 4 0 121.39 6.70 4 4 0 128.59 6.80 4 4 0 123.39 8.30 4 4 0 125.59 8.30 4 4 0 118.49 7.10 -4 -4 0 124.69 11.40 -4 -4 0 118.19 5.80 -4 -4 0 116.59 7.90 -4 -4 0 132.89 13.10 4 3 0 208.48 9.80 4 3 0 211.08 8.70 4 3 0 213.78 9.80 4 3 0 221.78 8.80 4 3 0 210.48 6.90 -4 -3 0 223.98 12.70 -4 -3 0 224.88 6.80 -4 -3 0 226.18 10.60 -4 -3 0 218.28 8.70 -4 -3 0 231.88 13.40 4 2 0 38.50 6.00 4 2 0 38.60 4.30 4 2 0 42.30 4.40 4 2 0 40.70 6.60 4 2 0 37.90 5.10 -4 -2 0 42.20 5.90 -4 -2 0 41.60 6.60 -4 -2 0 49.50 7.10 -4 -2 0 31.10 2.80 -4 -2 0 37.00 2.30 -4 -2 0 47.30 4.30 4 1 0 183.58 6.20 4 1 0 187.38 7.80 4 1 0 189.78 5.60 4 1 0 184.78 6.60 4 1 0 184.48 9.40 4 1 0 185.48 8.80 4 1 0 190.38 9.10 -4 -1 0 186.38 5.50 -4 -1 0 188.78 6.50 -4 -1 0 200.58 7.70 -4 -1 0 185.08 9.20 -4 -1 0 192.48 8.70 -4 -1 0 188.68 6.30 -4 -1 0 183.78 9.50 4 0 0 161.58 9.10 4 0 0 148.39 7.20 4 0 0 167.48 6.70 4 0 0 159.68 6.80 4 0 0 147.49 7.40 -4 0 0 158.48 5.20 -4 0 0 149.99 6.50 -4 0 0 157.18 9.00 -4 0 0 151.58 7.30 -4 0 0 164.08 6.40 -4 0 0 169.68 7.90 -4 0 0 141.09 7.00 4 -1 0 194.58 8.70 4 -1 0 179.48 7.90 4 -1 0 180.98 8.20 4 -1 0 187.58 5.90 4 -1 0 182.98 10.00 4 -1 0 191.38 5.80 4 -1 0 176.28 8.60 -4 1 0 194.48 8.50 -4 1 0 183.28 5.70 -4 1 0 181.18 5.70 -4 1 0 188.68 7.80 -4 1 0 184.18 8.00 -4 1 0 192.38 8.80 -4 1 0 184.28 8.50 -4 1 0 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144.69 11.90 -4 7 0 142.19 12.00 -4 7 0 149.79 15.50 -4 7 0 121.89 8.30 4 -8 0 3.90 12.90 4 -8 0 13.70 9.20 4 -8 0 15.60 6.20 4 -8 0 9.10 6.10 -4 8 0 6.50 10.30 -4 8 0 12.90 6.20 -4 8 0 3.00 7.90 -4 8 0 15.20 8.60 4 -9 0 85.79 9.10 4 -9 0 82.59 13.90 4 -9 0 89.59 18.20 4 -9 0 83.59 9.90 -4 9 0 73.29 11.60 -4 9 0 76.49 8.60 -4 9 0 69.29 14.80 4 -10 0 78.49 18.20 4 -10 0 81.59 9.30 4 -10 0 59.29 12.70 -4 10 0 48.40 11.40 -4 10 0 67.89 9.10 -4 10 0 54.89 15.30 4 -11 0 9.50 15.60 4 -11 0 3.70 10.50 4 -11 0 9.50 7.00 -4 11 0 9.00 7.10 -4 11 0 -9.20 12.90 -4 11 0 8.40 9.50 4 -12 0 -12.00 10.90 4 -12 0 -4.90 6.80 4 -12 0 14.90 16.90 -4 12 0 1.80 7.20 -4 12 0 -4.30 9.80 -4 12 0 -24.10 12.90 4 -13 0 -0.20 12.50 4 -13 0 21.90 7.60 4 -13 0 31.80 18.90 -4 13 0 22.50 11.90 -4 13 0 24.40 8.10 5 13 0 6.00 7.80 5 13 0 -8.00 10.40 -5 -13 0 -13.90 11.90 5 12 0 -0.90 10.00 5 12 0 -4.00 7.30 -5 -12 0 -2.00 11.20 -5 -12 0 -40.50 21.10 5 11 0 15.20 10.20 5 11 0 21.40 8.20 -5 -11 0 17.40 11.10 -5 -11 0 13.10 22.50 -5 -11 0 -5.90 20.70 5 10 0 14.00 7.30 5 10 0 -0.10 10.00 -5 -10 0 -10.50 17.00 -5 -10 0 5.70 10.20 -5 -10 0 -8.90 20.00 5 9 0 95.69 10.50 5 9 0 107.39 13.00 5 9 0 130.09 16.20 -5 -9 0 111.59 13.70 -5 -9 0 101.69 23.50 -5 -9 0 122.89 24.30 5 8 0 24.60 7.30 5 8 0 24.80 9.00 5 8 0 20.80 8.60 5 8 0 26.20 9.20 -5 -8 0 26.00 18.50 -5 -8 0 27.70 9.60 -5 -8 0 21.90 15.70 5 7 0 35.30 8.20 5 7 0 35.40 8.80 5 7 0 36.30 7.20 5 7 0 31.10 7.60 -5 -7 0 17.90 8.40 -5 -7 0 43.90 4.20 -5 -7 0 32.40 13.50 -5 -7 0 42.90 14.60 -5 -7 0 42.60 6.80 5 6 0 3.30 5.60 5 6 0 4.40 5.00 5 6 0 6.80 6.20 5 6 0 2.40 5.10 5 6 0 -2.10 3.20 -5 -6 0 7.10 11.90 -5 -6 0 1.30 10.10 -5 -6 0 4.30 3.20 -5 -6 0 -6.30 6.10 -5 -6 0 1.90 3.40 -5 -6 0 6.40 6.30 5 5 0 451.15 17.00 5 5 0 450.25 15.20 5 5 0 439.26 15.80 5 5 0 464.85 15.00 5 5 0 445.36 13.90 -5 -5 0 439.26 22.70 -5 -5 0 431.46 16.20 -5 -5 0 437.26 13.00 -5 -5 0 434.76 20.90 -5 -5 0 452.65 17.20 5 4 0 307.77 9.10 5 4 0 292.17 12.20 5 4 0 311.67 12.70 5 4 0 316.07 12.10 5 4 0 291.67 11.20 -5 -4 0 299.17 8.70 -5 -4 0 321.67 16.20 -5 -4 0 303.47 13.10 -5 -4 0 289.67 16.60 5 3 0 639.64 17.90 5 3 0 647.24 20.50 5 3 0 646.34 17.80 5 3 0 643.34 19.20 -5 -3 0 634.84 14.80 -5 -3 0 634.74 20.80 -5 -3 0 645.64 17.70 -5 -3 0 612.14 21.60 -5 -3 0 651.73 22.60 -5 -3 0 634.14 15.00 5 2 0 13.00 6.00 5 2 0 8.10 3.80 5 2 0 9.40 4.60 5 2 0 11.70 3.10 5 2 0 11.40 5.20 5 2 0 9.60 2.00 -5 -2 0 10.10 2.00 -5 -2 0 8.40 2.20 -5 -2 0 13.10 6.00 -5 -2 0 11.10 3.00 -5 -2 0 8.50 6.30 -5 -2 0 10.80 6.30 5 1 0 148.19 4.80 5 1 0 133.79 8.00 5 1 0 148.99 6.40 5 1 0 146.29 7.90 5 1 0 150.08 6.30 -5 -1 0 150.38 6.70 -5 -1 0 151.28 6.40 -5 -1 0 147.49 4.70 -5 -1 0 143.69 10.10 -5 -1 0 155.18 9.80 5 0 0 21.00 3.20 5 0 0 18.60 4.60 5 0 0 19.70 5.30 5 0 0 22.00 3.80 -5 0 0 20.80 3.90 -5 0 0 29.20 5.70 -5 0 0 21.00 5.50 -5 0 0 23.70 3.30 5 -1 0 134.59 8.70 5 -1 0 147.19 8.50 5 -1 0 138.19 8.30 5 -1 0 145.49 5.60 5 -1 0 151.58 5.20 5 -1 0 134.49 8.10 -5 1 0 158.48 9.00 -5 1 0 147.09 5.60 -5 1 0 149.99 5.20 -5 1 0 146.99 9.00 -5 1 0 145.69 8.80 -5 1 0 152.58 10.80 5 -2 0 7.30 5.10 5 -2 0 1.60 5.50 5 -2 0 9.60 2.70 5 -2 0 9.30 4.20 5 -2 0 7.90 3.20 -5 2 0 8.30 3.60 -5 2 0 11.60 2.70 -5 2 0 7.70 4.20 -5 2 0 15.00 5.90 -5 2 0 10.30 4.80 -5 2 0 11.50 6.20 5 -3 0 641.54 16.50 5 -3 0 668.13 19.50 5 -3 0 657.33 16.70 5 -3 0 655.03 19.90 5 -3 0 618.84 21.40 -5 3 0 655.53 16.50 -5 3 0 669.43 18.20 -5 3 0 637.24 22.60 -5 3 0 663.13 19.40 -5 3 0 637.24 22.80 5 -4 0 295.67 13.00 5 -4 0 293.87 14.80 5 -4 0 308.67 11.90 5 -4 0 316.17 9.80 -5 4 0 298.87 12.00 -5 4 0 325.37 15.60 -5 4 0 305.07 12.30 -5 4 0 296.67 15.70 5 -5 0 429.16 13.40 5 -5 0 417.96 16.80 5 -5 0 447.06 15.50 5 -5 0 448.16 19.90 -5 5 0 454.05 16.10 -5 5 0 448.86 19.10 -5 5 0 431.26 20.40 -5 5 0 458.15 13.90 5 -6 0 0.50 4.00 5 -6 0 -5.50 8.70 5 -6 0 -1.80 3.90 5 -6 0 4.20 7.80 -5 6 0 1.80 4.10 -5 6 0 -2.30 6.40 -5 6 0 4.50 8.20 -5 6 0 1.90 6.40 5 -7 0 37.00 10.60 5 -7 0 40.30 12.80 5 -7 0 35.20 6.00 5 -7 0 39.60 6.80 -5 7 0 37.60 10.90 -5 7 0 52.79 9.00 -5 7 0 31.70 9.00 -5 7 0 34.80 6.30 5 -8 0 31.90 6.50 5 -8 0 25.90 6.70 5 -8 0 27.30 13.50 5 -8 0 22.00 9.80 -5 8 0 16.90 11.40 -5 8 0 14.60 9.40 -5 8 0 27.40 9.20 -5 8 0 23.90 6.60 5 -9 0 100.29 9.40 5 -9 0 117.79 20.20 5 -9 0 99.29 13.70 5 -9 0 107.79 10.00 -5 9 0 87.89 16.10 -5 9 0 104.89 9.80 -5 9 0 98.29 12.50 5 -10 0 -4.00 9.90 5 -10 0 -2.70 6.00 5 -10 0 2.10 13.60 -5 10 0 -3.60 8.70 -5 10 0 3.40 6.50 -5 10 0 -20.20 11.60 5 -11 0 15.20 6.50 5 -11 0 21.70 11.90 5 -11 0 24.50 15.20 -5 11 0 -6.70 13.40 -5 11 0 14.00 9.80 -5 11 0 21.80 7.30 5 -12 0 -2.90 5.80 5 -12 0 -2.70 12.80 5 -12 0 8.10 15.40 -5 12 0 -9.80 9.60 -5 12 0 12.20 6.80 5 -13 0 19.10 16.50 5 -13 0 -4.30 11.70 5 -13 0 -1.00 6.30 -5 13 0 5.10 7.10 -5 13 0 -8.30 9.80 -5 13 0 -25.80 14.70 6 13 0 7.00 12.30 6 13 0 11.00 8.70 -6 -13 0 -39.00 23.50 -6 -13 0 -13.70 13.60 6 12 0 1.20 9.90 6 12 0 -3.70 7.30 -6 -12 0 -23.30 23.30 -6 -12 0 3.40 11.50 6 11 0 24.90 10.90 6 11 0 20.80 8.20 -6 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80.59 16.90 -6 9 0 80.59 8.50 -6 9 0 61.59 15.30 -6 9 0 59.39 11.00 6 -10 0 36.50 7.30 6 -10 0 22.50 11.00 6 -10 0 17.70 14.00 -6 10 0 22.50 7.10 -6 10 0 13.20 9.50 -6 10 0 14.20 14.00 6 -11 0 11.60 6.30 6 -11 0 17.50 11.10 6 -11 0 34.30 15.70 -6 11 0 -10.40 13.50 -6 11 0 13.30 10.10 -6 11 0 23.30 7.10 6 -12 0 32.60 15.20 6 -12 0 1.40 6.90 6 -12 0 -2.00 11.20 -6 12 0 -4.50 10.00 -6 12 0 9.20 7.50 6 -13 0 6.50 13.60 6 -13 0 14.60 15.40 -6 13 0 15.00 10.90 7 12 0 7.80 10.10 7 12 0 44.10 10.00 -7 -12 0 30.40 13.00 -7 -12 0 -33.20 22.10 7 11 0 21.90 8.50 7 11 0 24.70 10.50 -7 -11 0 15.70 18.00 -7 -11 0 17.50 11.60 -7 -11 0 -46.10 21.30 7 10 0 -1.80 8.40 7 10 0 -4.60 6.80 7 10 0 -6.60 8.90 -7 -10 0 8.50 9.80 -7 -10 0 -15.70 18.00 -7 -10 0 -13.20 19.30 7 9 0 11.70 7.30 7 9 0 7.80 8.70 7 9 0 3.10 9.10 -7 -9 0 19.00 20.80 -7 -9 0 4.00 19.10 -7 -9 0 9.70 9.80 7 8 0 3.30 8.40 7 8 0 10.10 7.90 7 8 0 -4.60 6.40 -7 -8 0 -6.00 8.70 -7 -8 0 17.20 18.10 -7 -8 0 12.00 15.50 7 7 0 10.90 7.30 7 7 0 12.70 4.20 7 7 0 10.40 8.10 7 7 0 15.30 6.80 -7 -7 0 5.40 9.50 -7 -7 0 11.30 8.30 -7 -7 0 11.30 15.00 -7 -7 0 8.30 13.60 7 6 0 204.38 13.40 7 6 0 211.78 7.30 7 6 0 204.68 12.20 7 6 0 217.38 11.70 -7 -6 0 202.38 18.70 -7 -6 0 201.58 7.00 -7 -6 0 225.08 14.90 -7 -6 0 202.08 20.30 7 5 0 29.70 6.80 7 5 0 21.80 5.60 7 5 0 21.70 6.20 -7 -5 0 31.20 11.20 -7 -5 0 34.50 10.60 -7 -5 0 31.00 8.20 7 4 0 56.19 6.10 7 4 0 60.39 7.60 7 4 0 57.39 6.30 -7 -4 0 64.39 10.80 -7 -4 0 61.79 8.60 -7 -4 0 70.59 11.10 7 3 0 34.60 5.00 7 3 0 49.50 6.20 7 3 0 31.80 7.70 7 3 0 41.30 4.60 -7 -3 0 40.30 8.40 -7 -3 0 47.00 9.20 -7 -3 0 39.40 4.40 -7 -3 0 39.00 2.80 -7 -3 0 36.80 3.20 -7 -3 0 43.20 8.30 7 2 0 149.49 7.40 7 2 0 149.79 10.60 7 2 0 155.08 6.10 7 2 0 158.08 9.00 7 2 0 155.88 6.40 -7 -2 0 159.48 5.90 -7 -2 0 149.99 10.90 -7 -2 0 157.08 11.70 -7 -2 0 150.48 6.50 -7 -2 0 162.88 11.80 7 1 0 588.74 16.80 7 1 0 591.84 15.90 7 1 0 567.04 13.30 7 1 0 560.04 19.60 7 1 0 550.84 17.90 -7 -1 0 573.94 13.30 -7 -1 0 587.84 21.10 -7 -1 0 573.14 22.50 -7 -1 0 563.74 16.90 7 0 0 40.90 4.10 7 0 0 38.00 6.70 7 0 0 31.70 5.70 -7 0 0 41.70 8.70 -7 0 0 51.39 7.00 -7 0 0 40.70 7.20 7 -1 0 571.64 15.30 7 -1 0 592.34 14.00 7 -1 0 589.44 20.00 7 -1 0 551.14 18.20 7 -1 0 565.04 19.50 -7 1 0 582.84 14.00 -7 1 0 572.24 22.80 -7 1 0 575.94 19.60 -7 1 0 603.14 20.20 7 -2 0 154.88 6.50 7 -2 0 155.98 10.10 7 -2 0 141.59 10.10 7 -2 0 140.29 9.30 7 -2 0 145.19 6.40 -7 2 0 153.78 6.30 -7 2 0 154.78 6.60 -7 2 0 154.28 10.10 -7 2 0 155.78 12.60 -7 2 0 159.48 11.00 7 -3 0 39.20 7.70 7 -3 0 35.10 3.80 7 -3 0 35.40 6.30 7 -3 0 34.40 6.70 -7 3 0 35.20 5.90 -7 3 0 44.40 7.50 -7 3 0 33.10 8.50 -7 3 0 45.80 5.00 7 -4 0 65.19 5.40 7 -4 0 57.29 7.20 7 -4 0 46.20 9.10 7 -4 0 68.69 8.70 -7 4 0 67.79 10.30 -7 4 0 65.19 7.20 -7 4 0 69.89 10.40 7 -5 0 16.90 8.70 7 -5 0 26.10 4.20 7 -5 0 18.00 5.50 7 -5 0 27.80 7.90 -7 5 0 18.30 7.90 -7 5 0 21.80 9.20 -7 5 0 22.90 5.90 7 -6 0 185.18 14.10 7 -6 0 212.48 9.50 7 -6 0 217.08 11.80 7 -6 0 211.78 16.70 -7 6 0 202.28 16.30 -7 6 0 217.58 12.40 -7 6 0 191.28 17.30 7 -7 0 12.80 5.90 7 -7 0 15.90 9.20 7 -7 0 3.30 4.60 7 -7 0 14.20 11.30 -7 7 0 13.80 8.80 -7 7 0 4.80 7.20 -7 7 0 4.20 9.00 7 -8 0 9.90 12.10 7 -8 0 0.80 9.40 7 -8 0 6.00 5.60 7 -8 0 4.40 5.20 -7 8 0 -6.40 9.40 -7 8 0 3.10 11.60 -7 8 0 1.70 8.00 7 -9 0 7.50 10.10 7 -9 0 11.80 5.30 7 -9 0 3.10 12.60 -7 9 0 5.80 12.70 -7 9 0 3.40 8.50 -7 9 0 -18.30 10.90 7 -10 0 19.30 13.30 7 -10 0 -8.10 9.50 7 -10 0 -5.10 5.50 -7 10 0 -7.60 8.50 -7 10 0 -27.10 11.50 7 -11 0 32.10 15.10 7 -11 0 13.00 6.50 7 -11 0 14.00 11.30 -7 11 0 -18.20 13.90 -7 11 0 12.60 10.00 7 -12 0 9.10 11.80 7 -12 0 45.30 16.10 -7 12 0 -15.90 14.50 -7 12 0 19.30 11.00 8 12 0 38.40 10.10 8 12 0 16.40 10.70 -8 -12 0 -10.40 24.20 -8 -12 0 15.60 13.70 8 11 0 11.40 8.00 8 11 0 13.70 11.30 -8 -11 0 -8.10 21.00 -8 -11 0 13.20 11.50 -8 -11 0 -44.30 19.30 8 10 0 0.50 9.60 8 10 0 7.80 7.60 8 10 0 0.00 8.70 -8 -10 0 3.60 10.10 -8 -10 0 -38.00 20.30 -8 -10 0 -25.40 18.30 8 9 0 0.40 8.70 8 9 0 -3.10 6.90 8 9 0 1.70 8.10 -8 -9 0 -4.30 9.10 -8 -9 0 -8.80 16.50 -8 -9 0 30.40 19.60 8 8 0 10.10 8.80 8 8 0 -7.70 6.70 8 8 0 -0.70 7.70 -8 -8 0 4.00 15.60 -8 -8 0 -1.90 13.20 -8 -8 0 6.00 9.30 8 7 0 -4.50 7.70 8 7 0 1.10 7.80 8 7 0 5.30 6.30 -8 -7 0 14.20 13.90 -8 -7 0 -5.90 8.00 -8 -7 0 -3.80 10.00 -8 -7 0 12.20 14.80 8 6 0 98.09 9.30 8 6 0 105.29 11.10 8 6 0 95.29 10.90 -8 -6 0 101.89 16.10 -8 -6 0 103.19 13.30 -8 -6 0 119.39 17.50 8 5 0 54.69 7.40 8 5 0 38.40 7.80 8 5 0 42.60 6.60 -8 -5 0 50.89 10.60 -8 -5 0 52.69 12.20 -8 -5 0 55.79 10.00 8 4 0 14.90 5.10 8 4 0 17.30 4.80 8 4 0 22.30 8.30 8 4 0 17.60 5.40 -8 -4 0 11.00 7.10 -8 -4 0 17.20 7.20 -8 -4 0 11.70 7.20 8 3 0 3.00 4.10 8 3 0 3.10 6.50 8 3 0 5.30 3.60 8 3 0 2.80 5.10 -8 -3 0 3.20 2.30 -8 -3 0 5.60 7.60 -8 -3 0 6.20 2.40 -8 -3 0 2.40 6.40 -8 -3 0 1.90 3.00 -8 -3 0 4.90 5.90 8 2 0 393.66 12.10 8 2 0 388.46 13.20 8 2 0 402.66 15.00 8 2 0 385.36 17.00 8 2 0 384.06 10.90 -8 -2 0 389.66 10.70 -8 -2 0 392.06 18.30 -8 -2 0 384.86 19.60 -8 -2 0 378.26 12.30 -8 -2 0 376.56 17.20 8 1 0 15.40 1.20 8 1 0 17.50 4.20 8 1 0 23.80 6.50 8 1 0 19.30 5.40 8 1 0 16.70 3.90 -8 -1 0 22.20 8.00 -8 -1 0 19.30 4.60 -8 -1 0 23.10 6.20 8 0 0 694.93 21.50 8 0 0 705.53 18.70 8 0 0 696.43 23.20 -8 0 0 712.83 24.20 -8 0 0 710.53 21.80 -8 0 0 705.33 27.20 8 -1 0 22.10 2.10 8 -1 0 22.20 6.30 8 -1 0 19.60 3.80 8 -1 0 25.20 6.00 -8 1 0 19.90 2.10 -8 1 0 26.20 6.80 -8 1 0 26.00 8.40 -8 1 0 20.80 6.40 8 -2 0 376.96 15.10 8 -2 0 381.86 11.40 8 -2 0 384.96 16.10 8 -2 0 392.46 16.70 8 -2 0 389.86 11.20 -8 2 0 380.26 19.90 -8 2 0 380.66 17.20 -8 2 0 373.46 16.30 -8 2 0 385.46 11.30 8 -3 0 -5.80 5.40 8 -3 0 1.30 6.30 8 -3 0 2.20 2.90 8 -3 0 7.30 5.50 -8 3 0 -0.10 7.00 -8 3 0 4.70 3.80 -8 3 0 2.30 5.20 -8 3 0 8.00 7.10 8 -4 0 14.80 5.80 8 -4 0 18.90 7.00 8 -4 0 19.80 3.70 8 -4 0 18.50 7.90 -8 4 0 10.50 4.80 -8 4 0 11.20 5.70 -8 4 0 9.50 8.00 -8 4 0 17.50 8.60 8 -5 0 41.40 4.90 8 -5 0 48.90 9.10 8 -5 0 50.89 7.70 8 -5 0 49.60 10.40 -8 5 0 51.79 7.70 -8 5 0 46.00 7.30 -8 5 0 48.20 10.90 -8 5 0 49.70 10.70 8 -6 0 108.39 12.10 8 -6 0 82.79 13.30 8 -6 0 95.89 9.70 8 -6 0 87.99 7.10 -8 6 0 100.09 14.50 -8 6 0 101.89 10.40 -8 6 0 87.79 13.10 8 -7 0 6.50 4.60 8 -7 0 5.00 8.90 8 -7 0 6.70 10.70 8 -7 0 3.30 5.60 -8 7 0 3.70 9.00 -8 7 0 4.80 8.50 -8 7 0 -5.80 7.60 8 -8 0 1.80 9.40 8 -8 0 6.90 5.70 8 -8 0 2.90 5.10 8 -8 0 4.40 12.90 -8 8 0 7.70 12.00 -8 8 0 -2.40 10.30 -8 8 0 1.30 7.70 8 -9 0 6.80 12.00 8 -9 0 -3.00 5.00 8 -9 0 1.60 10.00 -8 9 0 2.20 8.20 -8 9 0 -10.90 12.10 8 -10 0 21.70 11.30 8 -10 0 10.40 5.70 8 -10 0 19.90 13.20 -8 10 0 3.50 8.60 -8 10 0 -24.10 12.10 8 -11 0 13.80 11.30 8 -11 0 32.00 15.80 -8 11 0 -16.30 14.00 -8 11 0 9.20 9.50 8 -12 0 11.10 13.50 8 -12 0 41.90 15.70 -8 12 0 -35.00 14.70 -8 12 0 12.10 10.50 9 12 0 7.20 10.40 9 12 0 13.20 8.50 -9 -12 0 5.60 13.00 -9 -12 0 -43.90 22.50 9 11 0 -8.60 10.00 9 11 0 -12.00 9.90 9 11 0 -6.00 7.60 -9 -11 0 -2.40 21.40 -9 -11 0 4.10 10.80 9 10 0 23.50 8.50 9 10 0 26.00 9.70 9 10 0 20.30 10.50 -9 -10 0 17.40 20.40 -9 -10 0 -27.30 20.90 -9 -10 0 22.60 11.00 9 9 0 -5.70 8.40 9 9 0 -1.60 9.00 9 9 0 2.20 7.20 -9 -9 0 10.40 18.30 -9 -9 0 -27.10 15.90 -9 -9 0 7.80 9.50 9 8 0 5.20 7.30 9 8 0 11.90 8.80 9 8 0 7.40 7.80 -9 -8 0 13.80 17.10 -9 -8 0 15.20 9.40 -9 -8 0 13.60 16.30 9 7 0 4.60 7.90 9 7 0 11.80 7.10 9 7 0 7.80 6.90 -9 -7 0 3.50 11.40 -9 -7 0 10.80 11.30 -9 -7 0 12.10 13.90 9 6 0 59.59 8.70 9 6 0 35.00 7.50 9 6 0 49.20 9.30 -9 -6 0 69.19 15.40 -9 -6 0 52.49 12.00 -9 -6 0 49.60 15.20 9 5 0 217.68 13.60 9 5 0 225.48 11.90 9 5 0 236.08 11.90 -9 -5 0 242.08 19.10 -9 -5 0 244.48 17.10 -9 -5 0 229.28 18.90 9 4 0 16.30 5.60 9 4 0 20.60 5.20 9 4 0 24.80 7.80 9 4 0 14.10 6.50 -9 -4 0 22.50 10.10 -9 -4 0 21.50 8.60 -9 -4 0 21.20 8.10 9 3 0 164.58 13.10 9 3 0 149.29 9.70 9 3 0 145.69 8.70 9 3 0 142.69 6.30 9 3 0 151.98 7.40 -9 -3 0 150.58 13.30 -9 -3 0 148.69 6.40 -9 -3 0 144.09 6.90 -9 -3 0 165.28 14.40 -9 -3 0 156.08 13.70 -9 -3 0 146.89 6.70 9 2 0 380.16 13.40 9 2 0 372.96 10.40 9 2 0 383.96 17.60 9 2 0 377.76 15.20 9 2 0 363.26 12.30 -9 -2 0 389.96 13.10 -9 -2 0 373.06 10.20 -9 -2 0 376.46 17.80 -9 -2 0 361.36 19.60 -9 -2 0 384.36 19.10 9 1 0 193.38 12.50 9 1 0 181.78 10.80 9 1 0 180.88 8.30 -9 -1 0 179.88 13.30 -9 -1 0 196.98 10.00 -9 -1 0 179.38 14.80 9 0 0 497.05 14.50 9 0 0 487.05 19.20 9 0 0 471.85 17.40 -9 0 0 478.85 23.10 -9 0 0 483.45 20.10 -9 0 0 481.35 18.00 9 -1 0 185.38 7.90 9 -1 0 176.68 11.00 9 -1 0 189.08 5.20 9 -1 0 189.58 12.20 9 -1 0 193.48 5.20 -9 1 0 180.18 11.90 -9 1 0 188.48 15.40 -9 1 0 180.78 5.20 -9 1 0 190.18 12.50 9 -2 0 358.16 16.50 9 -2 0 355.26 16.80 9 -2 0 382.46 15.70 9 -2 0 388.16 11.90 9 -2 0 375.06 11.00 -9 2 0 369.86 11.10 -9 2 0 401.96 21.40 -9 2 0 391.96 16.90 -9 2 0 379.56 17.90 9 -3 0 148.19 12.10 9 -3 0 157.98 7.00 9 -3 0 131.29 10.90 9 -3 0 148.39 10.70 -9 3 0 153.98 14.90 -9 3 0 148.49 10.70 -9 3 0 143.89 7.70 -9 3 0 137.59 13.20 9 -4 0 18.70 6.60 9 -4 0 14.70 9.10 9 -4 0 13.20 4.00 9 -4 0 20.50 7.70 -9 4 0 21.40 5.40 -9 4 0 21.90 9.40 -9 4 0 28.50 7.10 -9 4 0 23.30 9.20 9 -5 0 226.38 13.20 9 -5 0 217.68 16.40 9 -5 0 222.18 14.70 9 -5 0 222.28 9.30 -9 5 0 231.38 16.50 -9 5 0 236.48 12.20 -9 5 0 233.38 18.00 -9 5 0 219.78 12.50 9 -6 0 39.80 12.80 9 -6 0 64.29 8.80 9 -6 0 51.89 5.80 9 -6 0 51.59 10.60 -9 6 0 44.40 8.40 -9 6 0 49.99 8.00 -9 6 0 51.89 11.30 -9 6 0 57.59 12.70 9 -7 0 11.90 6.50 9 -7 0 12.80 5.10 9 -7 0 5.00 10.60 9 -7 0 25.00 10.00 -9 7 0 8.90 7.30 -9 7 0 5.50 10.10 -9 7 0 7.60 11.40 9 -8 0 12.00 5.30 9 -8 0 15.90 6.60 9 -8 0 14.10 11.60 9 -8 0 4.70 9.90 -9 8 0 6.90 8.00 -9 8 0 -5.10 11.50 -9 8 0 -4.30 12.20 9 -9 0 0.40 5.20 9 -9 0 5.60 11.10 9 -9 0 2.90 9.70 -9 9 0 -20.00 12.10 -9 9 0 -6.80 7.80 9 -10 0 46.00 13.90 9 -10 0 20.90 11.00 -9 10 0 -11.10 13.50 -9 10 0 21.00 9.70 9 -11 0 -1.80 10.80 9 -11 0 18.40 13.00 -9 11 0 -19.10 10.40 -9 11 0 -3.10 8.90 9 -12 0 31.60 13.80 9 -12 0 0.20 11.30 -9 12 0 -1.40 9.40 10 12 0 15.50 8.80 10 12 0 8.40 11.40 -10 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-10 -4 0 86.19 13.50 10 3 0 167.28 7.40 10 3 0 171.68 9.70 10 3 0 187.88 14.30 10 3 0 160.68 11.60 10 3 0 168.18 7.60 -10 -3 0 171.88 8.10 -10 -3 0 188.48 16.00 -10 -3 0 165.98 14.40 -10 -3 0 169.48 7.20 -10 -3 0 164.58 16.40 -10 -3 0 173.08 7.50 10 2 0 52.49 7.90 10 2 0 52.89 3.80 10 2 0 56.19 6.60 10 2 0 64.49 10.00 10 2 0 60.59 5.70 -10 -2 0 55.39 6.90 -10 -2 0 53.89 3.30 -10 -2 0 52.79 10.80 -10 -2 0 51.19 11.10 -10 -2 0 43.40 9.30 10 1 0 240.48 14.30 10 1 0 235.78 10.20 10 1 0 233.58 12.60 -10 -1 0 222.28 17.20 -10 -1 0 231.18 15.40 -10 -1 0 227.78 11.80 10 0 0 732.53 23.80 10 0 0 732.23 20.30 10 0 0 719.63 25.70 -10 0 0 738.73 27.00 -10 0 0 772.02 24.80 -10 0 0 721.53 30.40 10 -1 0 215.28 12.50 10 -1 0 246.68 9.40 10 -1 0 229.28 14.00 -10 1 0 228.38 17.70 -10 1 0 231.58 14.30 -10 1 0 238.68 13.90 10 -2 0 56.99 8.40 10 -2 0 50.99 4.50 10 -2 0 58.69 5.60 10 -2 0 53.19 9.30 -10 2 0 55.19 4.50 -10 2 0 57.79 9.00 -10 2 0 66.79 9.90 -10 2 0 57.79 12.00 10 -3 0 174.08 7.90 10 -3 0 163.68 12.40 10 -3 0 167.18 13.70 10 -3 0 179.78 12.40 -10 3 0 176.08 8.40 -10 3 0 178.78 12.30 -10 3 0 186.68 15.20 -10 3 0 165.78 16.50 10 -4 0 79.69 6.70 10 -4 0 102.49 12.80 10 -4 0 83.49 10.70 10 -4 0 86.49 10.60 -10 4 0 86.29 9.70 -10 4 0 93.29 14.40 -10 4 0 80.69 12.80 -10 4 0 77.79 7.60 10 -5 0 257.47 16.20 10 -5 0 256.27 10.70 10 -5 0 267.67 15.10 10 -5 0 277.77 18.30 -10 5 0 284.17 20.70 -10 5 0 258.77 12.90 -10 5 0 274.07 14.60 -10 5 0 290.37 20.90 10 -6 0 28.60 7.70 10 -6 0 28.50 5.20 10 -6 0 12.00 9.30 10 -6 0 6.20 9.80 -10 6 0 22.70 12.70 -10 6 0 31.70 12.60 -10 6 0 20.60 7.80 -10 6 0 29.90 7.90 10 -7 0 -1.10 8.90 10 -7 0 5.40 10.70 10 -7 0 8.10 5.10 10 -7 0 9.30 6.40 -10 7 0 7.70 6.70 -10 7 0 2.20 10.30 -10 7 0 -4.70 6.80 -10 7 0 10.70 12.40 10 -8 0 26.50 6.00 10 -8 0 28.30 12.10 10 -8 0 29.20 11.00 -10 8 0 14.10 13.50 -10 8 0 14.20 8.40 -10 8 0 10.70 13.40 10 -9 0 15.50 11.10 10 -9 0 -0.50 9.70 -10 9 0 -2.40 7.70 -10 9 0 -24.20 12.60 10 -10 0 26.60 12.60 10 -10 0 -0.20 10.50 -10 10 0 -17.70 13.90 -10 10 0 7.60 9.90 10 -11 0 19.40 11.70 10 -11 0 42.70 15.20 -10 11 0 1.50 10.40 -10 11 0 -30.50 13.90 10 -12 0 38.00 14.20 10 -12 0 6.70 11.70 -10 12 0 2.00 9.60 11 11 0 15.40 8.60 11 11 0 10.70 9.30 11 11 0 -1.40 10.90 -11 -11 0 -17.00 21.60 -11 -11 0 10.40 11.30 11 10 0 -9.60 9.10 11 10 0 1.80 7.50 11 10 0 3.10 8.50 -11 -10 0 0.90 10.30 -11 -10 0 -11.70 19.30 11 9 0 12.90 7.90 11 9 0 9.90 9.00 11 9 0 -2.50 8.90 -11 -9 0 16.70 10.20 -11 -9 0 2.80 17.90 -11 -9 0 -7.80 16.70 11 8 0 -5.60 7.30 11 8 0 -5.90 7.80 11 8 0 3.10 7.00 -11 -8 0 -3.90 15.70 -11 -8 0 8.60 10.30 -11 -8 0 -14.90 14.70 11 7 0 24.20 7.90 11 7 0 29.10 9.40 11 7 0 34.10 8.40 -11 -7 0 37.70 16.60 -11 -7 0 12.50 13.20 -11 -7 0 35.10 16.40 11 6 0 2.80 8.00 11 6 0 5.20 7.00 11 6 0 -1.40 6.30 -11 -6 0 12.10 13.70 -11 -6 0 -10.20 10.80 -11 -6 0 1.30 12.70 11 5 0 19.20 7.60 11 5 0 17.50 8.40 11 5 0 29.70 6.30 -11 -5 0 34.40 12.90 -11 -5 0 28.80 12.70 -11 -5 0 32.80 13.90 11 4 0 47.00 6.20 11 4 0 52.49 11.70 11 4 0 42.50 8.90 11 4 0 44.70 7.30 -11 -4 0 53.59 12.70 -11 -4 0 55.79 13.60 -11 -4 0 52.99 12.40 11 3 0 2.60 3.70 11 3 0 -3.20 7.90 11 3 0 0.50 5.10 11 3 0 2.00 3.20 11 3 0 -1.50 6.40 -11 -3 0 4.90 3.10 -11 -3 0 8.70 10.70 -11 -3 0 7.70 9.10 -11 -3 0 2.90 2.70 -11 -3 0 6.10 9.90 -11 -3 0 -0.40 4.30 11 2 0 194.08 9.90 11 2 0 174.78 12.30 11 2 0 184.48 14.30 11 2 0 171.68 5.40 -11 -2 0 179.78 5.20 -11 -2 0 187.48 10.90 -11 -2 0 166.48 13.90 -11 -2 0 198.28 17.30 11 1 0 43.00 9.20 11 1 0 45.60 6.30 11 1 0 42.50 8.10 -11 -1 0 49.60 7.60 -11 -1 0 46.00 11.90 -11 -1 0 43.90 9.10 11 0 0 12.20 4.20 11 0 0 16.60 7.60 11 0 0 13.40 6.90 -11 0 0 22.20 7.40 -11 0 0 19.90 8.50 -11 0 0 25.40 10.60 11 -1 0 34.80 5.20 11 -1 0 44.00 8.30 11 -1 0 41.30 9.10 -11 1 0 41.30 11.90 -11 1 0 39.40 9.20 -11 1 0 43.30 9.50 11 -2 0 193.68 9.10 11 -2 0 198.88 6.80 11 -2 0 171.58 12.80 11 -2 0 163.08 13.60 -11 2 0 183.98 16.30 -11 2 0 198.28 14.00 -11 2 0 198.08 16.40 -11 2 0 184.38 6.70 11 -3 0 -17.10 7.90 11 -3 0 -1.60 4.10 11 -3 0 -0.40 7.30 -11 3 0 5.80 10.10 -11 3 0 -2.20 3.70 -11 3 0 6.90 7.60 -11 3 0 2.90 8.60 11 -4 0 49.30 9.80 11 -4 0 31.00 9.40 11 -4 0 51.09 11.30 11 -4 0 36.90 5.50 -11 4 0 41.20 6.30 -11 4 0 43.00 12.90 -11 4 0 34.90 11.40 -11 4 0 43.40 9.40 11 -5 0 35.80 8.80 11 -5 0 23.80 5.00 11 -5 0 18.10 10.20 11 -5 0 33.80 9.70 -11 5 0 26.90 6.80 -11 5 0 32.50 12.70 -11 5 0 31.30 12.10 -11 5 0 29.10 8.70 11 -6 0 -2.10 6.40 11 -6 0 -3.70 8.80 11 -6 0 -3.20 4.60 11 -6 0 -5.50 9.30 -11 6 0 2.00 8.90 -11 6 0 3.70 11.20 -11 6 0 -5.70 6.60 -11 6 0 -2.80 6.60 11 -7 0 21.10 10.40 11 -7 0 24.10 7.60 11 -7 0 22.00 5.60 11 -7 0 26.70 11.80 -11 7 0 32.50 8.80 -11 7 0 12.80 14.20 -11 7 0 33.90 13.90 -11 7 0 37.80 8.60 11 -8 0 4.20 11.70 11 -8 0 -7.60 8.80 -11 8 0 0.10 7.90 -11 8 0 -12.10 11.90 11 -9 0 7.20 10.30 11 -9 0 13.00 11.30 -11 9 0 3.50 8.70 -11 9 0 -16.00 13.10 11 -10 0 -4.40 11.50 11 -10 0 11.40 11.20 -11 10 0 -12.50 8.60 -11 10 0 -23.80 13.90 11 -11 0 45.20 13.80 11 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-12 4 0 60.69 6.70 -12 4 0 57.59 10.00 -12 4 0 54.39 14.60 12 -5 0 13.40 9.20 12 -5 0 16.60 5.10 12 -5 0 16.40 8.10 12 -5 0 19.60 10.50 -12 5 0 21.90 10.10 -12 5 0 18.70 6.50 -12 5 0 18.30 8.50 -12 5 0 11.70 12.50 12 -6 0 1.80 6.90 12 -6 0 7.20 11.50 12 -6 0 4.50 9.40 12 -6 0 -0.70 4.40 -12 6 0 -2.50 12.00 -12 6 0 -0.10 7.20 -12 6 0 -8.20 11.30 -12 6 0 2.40 6.60 12 -7 0 24.70 8.20 12 -7 0 18.40 10.80 12 -7 0 28.90 10.50 -12 7 0 16.70 8.00 -12 7 0 -7.50 12.30 -12 7 0 20.80 8.30 -12 7 0 9.90 13.40 12 -8 0 17.80 11.20 12 -8 0 9.90 9.90 -12 8 0 1.90 7.10 -12 8 0 -9.70 12.80 12 -9 0 13.80 10.50 12 -9 0 21.40 11.60 -12 9 0 3.50 7.70 -12 9 0 -30.00 12.30 12 -10 0 35.90 12.60 12 -10 0 17.10 10.90 -12 10 0 5.00 9.40 -12 10 0 -30.90 14.20 12 -11 0 20.40 11.40 12 -11 0 48.50 14.00 -12 11 0 10.90 9.50 13 10 0 33.60 13.10 13 10 0 34.90 9.60 -13 -10 0 -30.20 20.40 -13 -10 0 29.00 12.00 -13 -10 0 16.20 20.70 13 9 0 4.80 7.90 13 9 0 5.10 9.90 -13 -9 0 -23.90 16.40 -13 -9 0 -24.30 17.40 -13 -9 0 6.50 10.20 13 8 0 26.90 8.60 13 8 0 27.70 10.10 -13 -8 0 2.80 17.00 -13 -8 0 15.10 17.40 13 7 0 55.49 11.40 13 7 0 52.19 9.30 -13 -7 0 56.79 17.80 -13 -7 0 67.19 19.00 13 6 0 155.08 12.30 13 6 0 151.38 14.60 -13 -6 0 164.58 21.20 -13 -6 0 140.59 20.80 -13 -6 0 126.69 20.70 13 5 0 33.50 10.00 13 5 0 44.10 13.30 13 5 0 49.60 8.40 -13 -5 0 51.59 15.20 -13 -5 0 36.00 16.10 -13 -5 0 43.50 13.50 13 4 0 66.79 11.00 13 4 0 68.59 13.90 13 4 0 60.29 8.30 -13 -4 0 74.99 14.80 -13 -4 0 73.19 16.90 -13 -4 0 59.39 15.40 13 3 0 98.29 14.20 13 3 0 101.39 10.90 13 3 0 77.59 8.60 -13 -3 0 75.29 9.30 -13 -3 0 85.19 14.60 -13 -3 0 106.19 17.30 -13 -3 0 89.89 15.60 13 2 0 44.50 7.10 13 2 0 55.09 10.30 13 2 0 47.50 9.70 -13 -2 0 56.59 13.30 -13 -2 0 54.29 12.00 -13 -2 0 48.00 8.70 -13 -2 0 51.79 14.30 13 1 0 21.10 6.30 13 1 0 21.60 9.50 13 1 0 8.60 6.70 -13 -1 0 26.80 8.70 -13 -1 0 28.80 12.90 -13 -1 0 28.10 11.00 13 0 0 471.75 16.20 13 0 0 469.85 22.60 13 0 0 434.06 20.10 -13 0 0 456.75 21.30 -13 0 0 493.05 28.70 -13 0 0 469.55 24.20 13 -1 0 24.10 5.70 13 -1 0 21.50 8.40 13 -1 0 24.60 9.70 -13 1 0 23.70 9.30 -13 1 0 20.50 9.80 -13 1 0 26.40 11.10 13 -2 0 45.60 12.00 13 -2 0 47.50 6.40 13 -2 0 35.70 9.50 -13 2 0 54.09 15.10 -13 2 0 40.30 10.60 -13 2 0 46.60 11.50 13 -3 0 83.89 13.10 13 -3 0 83.49 11.90 13 -3 0 95.69 8.10 -13 3 0 85.49 12.40 -13 3 0 79.49 6.80 -13 3 0 65.89 13.20 -13 3 0 97.09 17.80 13 -4 0 74.09 13.30 13 -4 0 61.99 6.60 13 -4 0 63.39 11.40 -13 4 0 62.89 11.90 -13 4 0 66.09 16.40 -13 4 0 66.69 6.80 -13 4 0 56.29 14.00 13 -5 0 46.70 12.60 13 -5 0 55.09 11.50 13 -5 0 42.70 6.20 -13 5 0 45.20 13.90 -13 5 0 48.10 15.80 -13 5 0 50.29 10.80 -13 5 0 31.90 6.70 13 -6 0 147.29 12.90 13 -6 0 163.88 15.90 13 -6 0 160.58 17.70 -13 6 0 162.38 11.30 -13 6 0 158.68 14.30 -13 6 0 137.69 20.50 -13 6 0 134.49 19.20 13 -7 0 59.69 12.20 13 -7 0 88.89 15.90 13 -7 0 64.89 12.30 -13 7 0 61.39 9.60 -13 7 0 28.30 17.40 -13 7 0 43.40 13.60 13 -8 0 50.79 12.70 13 -8 0 26.30 10.60 -13 8 0 19.20 8.40 -13 8 0 -7.50 13.70 13 -9 0 6.80 10.00 13 -9 0 23.20 11.20 -13 9 0 -1.50 8.20 -13 9 0 -31.90 13.20 13 -10 0 54.49 13.40 13 -10 0 35.70 12.00 -13 10 0 32.20 11.00 14 10 0 -1.40 10.00 14 10 0 15.80 9.80 -14 -10 0 23.00 11.20 -14 -10 0 -2.20 20.00 -14 -10 0 -52.39 20.30 14 9 0 22.70 11.10 14 9 0 38.20 10.40 -14 -9 0 -6.60 17.80 -14 -9 0 -0.10 20.60 -14 -9 0 36.50 12.10 14 8 0 12.20 9.10 14 8 0 1.00 9.10 -14 -8 0 -4.40 16.80 -14 -8 0 -7.30 16.70 14 7 0 -0.50 6.80 14 7 0 8.00 8.90 -14 -7 0 14.30 15.30 -14 -7 0 3.60 16.00 14 6 0 1.30 6.70 14 6 0 10.10 8.60 -14 -6 0 -2.10 12.70 -14 -6 0 9.40 15.00 14 5 0 6.80 10.90 14 5 0 -5.60 7.90 14 5 0 2.40 7.20 -14 -5 0 -3.60 12.00 -14 -5 0 1.60 10.50 -14 -5 0 -13.30 12.20 14 4 0 45.10 12.80 14 4 0 45.60 10.40 14 4 0 59.19 9.30 -14 -4 0 56.09 17.50 -14 -4 0 71.39 16.40 -14 -4 0 40.10 13.90 14 3 0 19.30 7.60 14 3 0 29.50 11.40 14 3 0 23.00 9.20 -14 -3 0 35.30 14.00 -14 -3 0 30.30 14.30 -14 -3 0 33.40 12.80 14 2 0 -2.70 8.90 14 2 0 4.40 5.80 14 2 0 -3.30 7.70 -14 -2 0 -3.90 7.10 -14 -2 0 10.30 12.50 -14 -2 0 -4.00 9.70 -14 -2 0 11.50 11.50 14 1 0 50.49 12.50 14 1 0 37.80 9.80 14 1 0 43.90 7.40 -14 -1 0 42.10 10.10 -14 -1 0 59.29 15.70 -14 -1 0 55.39 13.40 14 0 0 4.20 5.50 14 0 0 -0.10 8.60 14 0 0 2.70 8.20 -14 0 0 4.00 12.50 -14 0 0 6.10 10.20 -14 0 0 13.10 9.40 14 -1 0 40.60 11.20 14 -1 0 49.90 10.60 14 -1 0 37.40 6.40 -14 1 0 46.30 12.10 -14 1 0 45.70 15.20 -14 1 0 43.50 11.90 14 -2 0 -0.70 4.80 14 -2 0 3.70 9.20 14 -2 0 -0.30 7.90 -14 2 0 17.50 13.50 -14 2 0 0.50 9.80 -14 2 0 7.40 11.30 14 -3 0 28.30 6.00 14 -3 0 38.00 11.60 14 -3 0 26.30 9.80 -14 3 0 22.90 11.70 -14 3 0 25.40 10.10 -14 3 0 30.50 14.70 14 -4 0 46.60 6.60 14 -4 0 67.99 13.40 14 -4 0 54.79 11.50 -14 4 0 47.40 13.90 -14 4 0 56.69 16.70 -14 4 0 53.79 11.00 14 -5 0 17.30 10.60 14 -5 0 8.10 9.00 -14 5 0 -5.60 7.00 -14 5 0 -12.70 12.30 -14 5 0 -9.70 11.30 14 -6 0 8.50 9.50 14 -6 0 24.10 11.10 -14 6 0 -20.30 12.50 -14 6 0 3.40 8.10 -14 6 0 -19.20 11.90 14 -7 0 25.20 10.50 14 -7 0 22.90 11.10 -14 7 0 -13.50 13.00 -14 7 0 -23.40 13.30 14 -8 0 40.30 12.50 14 -8 0 24.20 10.70 -14 8 0 -15.30 14.10 14 -9 0 22.60 11.30 14 -9 0 61.49 13.20 -14 9 0 -6.90 15.30 14 -10 0 44.10 12.30 14 -10 0 61.29 13.70 15 9 0 5.30 10.80 15 9 0 26.30 10.10 -15 -9 0 -37.40 18.80 -15 -9 0 16.00 10.80 -15 -9 0 -13.30 17.40 15 8 0 34.60 9.80 15 8 0 24.90 10.80 -15 -8 0 14.90 18.30 -15 -8 0 4.30 19.00 15 7 0 6.40 9.10 15 7 0 -0.50 7.10 -15 -7 0 -15.00 13.70 -15 -7 0 -20.10 11.10 15 6 0 74.79 10.10 15 6 0 69.39 12.30 -15 -6 0 53.29 18.10 -15 -6 0 60.89 17.20 -15 -6 0 18.20 16.90 15 5 0 10.60 11.50 15 5 0 8.80 8.70 15 5 0 10.10 6.70 -15 -5 0 12.40 14.80 -15 -5 0 -10.80 13.80 -15 -5 0 8.70 13.30 15 4 0 48.50 8.30 15 4 0 45.90 10.70 15 4 0 54.29 13.50 -15 -4 0 43.50 13.20 -15 -4 0 48.60 14.30 -15 -4 0 56.09 17.20 15 3 0 13.00 6.70 15 3 0 16.90 8.90 15 3 0 15.70 11.00 -15 -3 0 17.70 14.30 -15 -3 0 19.90 13.10 -15 -3 0 22.30 12.40 15 2 0 21.10 7.30 15 2 0 29.40 9.70 15 2 0 31.20 11.40 -15 -2 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-6 2 195.18 11.80 -5 -6 2 220.88 15.90 5 5 -2 6.00 5.70 5 5 -2 6.40 5.50 5 5 -2 1.50 4.50 5 5 -2 3.70 4.20 5 5 -2 3.60 4.00 -5 -5 2 7.30 7.10 -5 -5 2 5.40 9.50 -5 -5 2 -0.30 4.50 -5 -5 2 9.40 4.50 -5 -5 2 2.80 5.90 -5 -5 2 6.60 3.80 5 4 -2 28.80 5.40 5 4 -2 28.10 4.10 5 4 -2 24.90 4.90 5 4 -2 22.20 4.70 5 4 -2 22.50 5.50 -5 -4 2 27.90 5.30 -5 -4 2 27.40 5.00 -5 -4 2 31.40 7.50 -5 -4 2 31.20 8.70 -5 -4 2 28.00 5.60 5 3 -2 58.59 5.30 5 3 -2 64.69 6.90 5 3 -2 49.80 4.50 5 3 -2 67.19 8.70 5 3 -2 62.69 5.90 5 3 -2 58.19 6.30 -5 -3 2 54.89 8.60 -5 -3 2 51.89 7.10 -5 -3 2 62.09 8.30 -5 -3 2 55.99 6.00 -5 -3 2 54.79 6.10 -5 -3 2 57.29 4.80 5 2 -2 375.76 15.00 5 2 -2 367.86 10.80 5 2 -2 372.66 11.30 5 2 -2 366.06 12.80 -5 -2 2 382.96 11.00 -5 -2 2 345.97 14.80 -5 -2 2 369.56 15.20 -5 -2 2 370.96 11.60 -5 -2 2 352.96 15.10 -5 -2 2 361.96 11.30 5 1 -2 1868.11 46.70 5 1 -2 1878.71 41.80 5 1 -2 1894.51 42.70 5 1 -2 1727.13 46.70 5 1 -2 1905.21 44.50 5 1 -2 1892.11 44.30 -5 -1 2 1923.21 42.80 -5 -1 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27.60 10.30 11 -9 -10 24.40 9.00 11 -9 -10 25.70 13.70 -11 9 10 -4.00 8.30 -11 9 10 1.80 9.80 -11 9 10 -1.80 12.20 11 -10 -10 88.89 18.10 -11 10 10 57.29 12.10 -11 10 10 55.39 17.50 12 10 -10 -6.80 10.70 12 10 -10 17.30 9.60 -12 -10 10 -24.60 17.30 -12 -10 10 -29.90 12.50 -12 -10 10 12.00 11.40 12 9 -10 17.80 8.20 12 9 -10 -1.20 10.60 -12 -9 10 34.40 12.20 -12 -9 10 -6.20 12.50 -12 -9 10 -3.90 15.70 12 8 -10 2.00 9.80 12 8 -10 9.60 7.60 -12 -8 10 -7.30 10.80 -12 -8 10 -11.10 13.50 -12 -8 10 12.00 10.00 12 7 -10 -1.80 6.60 12 7 -10 7.70 9.40 -12 -7 10 -13.90 12.00 -12 -7 10 0.40 8.90 -12 -7 10 3.10 10.50 -12 -7 10 -4.10 9.00 12 6 -10 22.40 7.20 12 6 -10 18.20 11.00 12 6 -10 16.50 9.30 12 6 -10 16.60 12.30 -12 -6 10 21.40 9.90 -12 -6 10 18.70 13.00 -12 -6 10 6.40 10.20 -12 -6 10 16.10 6.70 12 5 -10 -1.00 10.90 12 5 -10 14.70 6.10 12 5 -10 10.20 6.20 12 5 -10 15.70 8.80 -12 -5 10 9.10 5.80 -12 -5 10 13.50 12.00 -12 -5 10 10.30 6.70 -12 -5 10 16.20 10.20 -12 -5 10 8.70 10.40 12 4 -10 32.00 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10 -7.80 12.30 12 -10 -10 43.90 14.50 -12 10 10 -14.10 13.90 -12 10 10 -13.50 8.30 13 9 -10 -2.60 11.60 13 9 -10 14.90 9.00 -13 -9 10 -4.70 16.00 -13 -9 10 -19.00 11.70 -13 -9 10 -7.90 9.80 13 8 -10 15.10 7.80 13 8 -10 0.30 9.70 -13 -8 10 -17.10 11.20 -13 -8 10 19.70 10.90 -13 -8 10 3.60 14.70 13 7 -10 33.70 12.10 13 7 -10 35.20 8.30 -13 -7 10 26.80 15.10 -13 -7 10 22.10 12.90 -13 -7 10 36.10 11.10 13 6 -10 22.20 13.30 13 6 -10 26.00 7.40 13 6 -10 17.40 9.60 -13 -6 10 27.80 12.10 -13 -6 10 31.30 14.20 -13 -6 10 18.10 11.30 13 5 -10 5.00 6.60 13 5 -10 5.50 8.30 13 5 -10 24.40 12.10 -13 -5 10 9.90 9.50 -13 -5 10 9.70 11.40 -13 -5 10 8.10 10.60 13 4 -10 3.10 6.10 13 4 -10 4.80 10.70 13 4 -10 5.80 8.00 -13 -4 10 8.90 10.40 -13 -4 10 6.40 6.60 -13 -4 10 1.50 10.50 -13 -4 10 1.90 9.20 13 3 -10 296.17 20.00 13 3 -10 288.57 18.40 13 3 -10 298.37 13.10 -13 -3 10 299.97 23.40 -13 -3 10 311.97 22.10 13 2 -10 284.67 21.60 13 2 -10 291.87 16.90 13 2 -10 279.77 11.80 13 2 -10 271.37 20.60 -13 -2 10 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13.70 -6 3 -21 32.30 22.60 6 -3 21 35.80 8.40 6 -3 21 35.30 8.60 6 -3 21 25.70 8.60 -6 2 -21 16.20 11.80 -6 2 -21 6.10 21.10 -6 2 -21 30.20 11.00 6 -2 21 16.40 7.90 6 -2 21 13.60 7.70 6 -2 21 14.60 6.70 -6 1 -21 34.40 12.20 -6 1 -21 27.50 21.90 -6 1 -21 39.50 13.10 6 -1 21 25.50 8.20 6 -1 21 16.60 7.80 6 -1 21 25.10 6.90 -6 0 -21 1.60 9.90 -6 0 -21 -5.70 19.70 -6 0 -21 -2.70 12.60 6 0 21 8.90 7.50 6 0 21 8.90 7.20 -6 -1 -21 39.80 16.10 -6 -1 -21 22.20 17.60 -6 -1 -21 27.10 11.10 6 1 21 23.40 10.30 6 1 21 26.40 8.20 6 1 21 34.90 9.50 -6 -2 -21 14.50 9.60 -6 -2 -21 20.80 20.70 -6 -2 -21 27.50 16.70 6 2 21 5.00 7.20 6 2 21 9.40 8.50 6 2 21 2.50 8.00 -6 -3 -21 45.40 20.60 -6 -3 -21 23.50 17.90 -6 -3 -21 43.80 11.50 6 3 21 33.30 8.60 6 3 21 36.20 9.10 6 3 21 35.80 10.70 -6 -4 -21 119.99 23.40 -6 -4 -21 119.39 23.70 6 4 21 99.09 12.70 6 4 21 104.89 13.90 6 4 21 109.99 11.60 -6 -5 -21 31.50 19.60 -6 -5 -21 38.90 17.60 6 5 21 17.10 7.80 6 5 21 15.30 9.10 6 5 21 29.50 8.60 -6 -6 -21 18.20 14.80 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9.70 2 -5 21 45.60 10.10 -2 4 -21 25.80 10.90 -2 4 -21 38.40 19.40 2 -4 21 41.10 9.40 2 -4 21 18.80 8.50 2 -4 21 32.30 8.20 -2 3 -21 12.60 16.40 -2 3 -21 3.00 11.30 -2 3 -21 12.60 7.70 2 -3 21 6.70 7.50 2 -3 21 4.20 6.90 2 -3 21 5.10 7.10 -2 2 -21 25.20 10.30 -2 2 -21 10.50 11.70 -2 2 -21 6.80 16.50 2 -2 21 12.40 7.20 2 -2 21 12.30 7.70 2 -2 21 13.10 6.40 -2 1 -21 38.50 12.40 -2 1 -21 46.70 18.40 -2 1 -21 31.20 12.50 2 -1 21 50.49 9.30 2 -1 21 27.50 8.60 2 -1 21 38.40 11.00 -2 0 -21 2.30 15.60 -2 0 -21 -6.60 9.60 -2 0 -21 5.30 10.50 2 0 21 1.30 6.30 2 0 21 -3.50 6.80 2 0 21 -3.80 9.30 -2 -1 -21 34.30 13.50 -2 -1 -21 39.90 12.00 -2 -1 -21 40.20 18.10 2 1 21 47.40 8.90 2 1 21 40.70 9.30 2 1 21 42.50 11.90 -2 -2 -21 17.30 16.60 -2 -2 -21 18.50 13.70 -2 -2 -21 5.90 10.00 2 2 21 17.40 8.40 2 2 21 22.60 7.90 2 2 21 11.00 9.30 -2 -3 -21 5.70 14.10 -2 -3 -21 1.80 14.90 2 3 21 7.70 7.80 2 3 21 5.00 7.90 2 3 21 0.70 6.20 -2 -4 -21 47.80 17.00 -2 -4 -21 28.80 15.60 -2 -4 -21 35.40 9.90 2 4 21 30.80 9.20 2 4 21 29.30 8.00 2 4 21 28.80 10.40 -2 -5 -21 49.99 16.30 -2 -5 -21 49.20 12.10 -2 -5 -21 39.10 16.80 2 5 21 33.30 9.90 2 5 21 49.20 10.80 2 5 21 42.90 8.30 -2 -6 -21 142.09 20.10 -2 -6 -21 123.29 21.80 -2 -6 -21 140.59 18.10 2 6 21 94.49 13.50 2 6 21 102.19 10.80 2 6 21 125.49 15.20 -2 -7 -21 34.80 12.70 -2 -7 -21 21.70 14.20 -2 -7 -21 31.90 16.90 2 7 21 6.90 7.70 2 7 21 13.10 6.60 2 7 21 7.60 7.60 -2 -8 -21 32.90 17.70 -2 -8 -21 65.49 14.60 -2 -8 -21 37.60 16.30 2 8 21 11.20 9.90 2 8 21 24.20 9.90 2 8 21 23.70 7.90 -2 -9 -21 32.20 17.20 -2 -9 -21 12.30 14.50 2 9 21 5.10 10.70 2 9 21 7.20 6.60 -1 10 -21 85.89 14.70 1 -10 21 41.80 12.00 -1 9 -21 26.50 14.50 -1 9 -21 22.40 10.50 1 -9 21 14.20 8.50 1 -9 21 -11.80 12.10 1 -9 21 13.70 9.60 -1 8 -21 56.89 12.40 -1 8 -21 61.29 17.80 -1 8 -21 56.89 16.30 1 -8 21 13.80 11.90 1 -8 21 26.50 10.10 1 -8 21 32.50 9.40 -1 7 -21 147.99 21.40 -1 7 -21 200.58 21.30 -1 7 -21 149.29 16.20 1 -7 21 160.18 15.30 1 -7 21 136.99 15.70 1 -7 21 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95.79 12.10 -8 4 -22 94.49 17.90 -8 4 -22 101.79 28.70 8 -4 22 71.19 11.20 8 -4 22 85.99 12.00 8 -4 22 92.69 11.80 -8 3 -22 20.50 13.10 -8 3 -22 45.20 24.60 8 -3 22 23.90 8.10 8 -3 22 20.10 8.30 8 -3 22 18.90 8.00 -8 2 -22 31.30 24.20 -8 2 -22 27.20 12.50 8 -2 22 27.00 7.80 8 -2 22 24.90 8.50 8 -2 22 29.10 8.80 -8 1 -22 13.80 13.50 -8 1 -22 20.30 11.80 -8 1 -22 2.70 21.80 8 -1 22 4.80 7.80 8 -1 22 0.90 6.50 -8 0 -22 25.40 14.70 -8 0 -22 23.90 11.10 -8 0 -22 10.10 23.10 8 0 22 21.40 8.40 8 0 22 20.00 7.90 -8 -1 -22 4.00 15.20 -8 -1 -22 6.60 9.40 -8 -1 -22 4.70 21.80 8 1 22 8.10 7.30 8 1 22 14.20 7.90 8 1 22 -0.50 8.80 -8 -2 -22 23.70 9.70 -8 -2 -22 24.80 22.20 -8 -2 -22 16.60 17.80 8 2 22 16.80 8.10 8 2 22 14.60 9.30 8 2 22 25.50 8.70 -8 -3 -22 39.60 10.70 -8 -3 -22 20.50 19.00 -8 -3 -22 31.60 21.80 8 3 22 11.50 8.10 8 3 22 16.60 8.30 8 3 22 21.00 9.60 -8 -4 -22 93.89 24.90 -8 -4 -22 92.69 24.10 8 4 22 82.09 12.30 8 4 22 77.79 11.10 -8 -5 -22 120.09 24.60 -8 -5 -22 85.79 24.90 8 5 22 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-2.60 11.40 2 -2 29 -0.30 8.40 -2 1 -29 52.59 13.00 -2 1 -29 40.70 13.80 -2 1 -29 63.69 19.10 2 -1 29 30.60 10.00 2 -1 29 38.50 9.40 2 -1 29 20.30 13.10 -2 0 -29 36.10 17.70 -2 0 -29 32.30 11.70 -2 0 -29 26.70 11.00 2 0 29 0.10 7.20 2 0 29 9.40 11.10 2 0 29 5.60 7.80 -2 -1 -29 50.79 13.40 -2 -1 -29 54.69 19.20 -2 -1 -29 62.39 15.10 2 1 29 19.30 12.20 2 1 29 21.30 9.50 2 1 29 23.50 8.30 -2 -2 -29 32.50 16.90 -2 -2 -29 39.20 15.00 2 2 29 10.50 8.70 2 2 29 0.10 7.80 2 2 29 13.20 10.40 -2 -3 -29 39.40 16.10 -2 -3 -29 25.00 14.10 2 3 29 -5.30 6.50 2 3 29 14.50 10.20 2 3 29 3.00 9.20 -2 -4 -29 60.09 18.30 -2 -4 -29 35.70 16.00 2 4 29 15.40 10.20 2 4 29 30.60 11.40 -1 4 -29 22.00 13.20 -1 4 -29 55.09 17.90 1 -4 29 -7.50 12.80 1 -4 29 -4.20 8.70 1 -4 29 11.30 9.00 -1 3 -29 41.90 17.40 -1 3 -29 34.90 12.80 1 -3 29 10.90 8.00 1 -3 29 3.90 10.10 1 -3 29 26.80 10.00 -1 2 -29 85.29 21.50 -1 2 -29 53.89 14.90 1 -2 29 27.50 9.80 1 -2 29 21.50 8.30 1 -2 29 18.70 13.40 -1 1 -29 37.80 13.10 -1 1 -29 33.10 10.40 -1 1 -29 39.30 17.40 1 -1 29 18.60 8.00 1 -1 29 5.70 11.00 1 -1 29 8.20 8.60 -1 0 -29 42.60 12.00 -1 0 -29 31.40 12.00 -1 0 -29 28.70 16.10 1 0 29 6.60 7.90 1 0 29 9.60 11.20 1 0 29 -1.20 6.90 -1 -1 -29 29.60 15.70 -1 -1 -29 41.70 12.90 1 1 29 4.40 8.50 1 1 29 18.10 11.80 1 1 29 9.00 8.00 -1 -2 -29 57.59 18.70 -1 -2 -29 50.89 14.70 1 2 29 22.40 7.90 1 2 29 27.10 10.10 1 2 29 27.40 12.00 -1 -3 -29 45.30 17.30 -1 -3 -29 20.10 14.00 1 3 29 18.60 7.70 1 3 29 19.50 11.00 1 3 29 14.10 9.80 -1 -4 -29 29.30 14.70 -1 -4 -29 50.99 16.40 1 4 29 0.10 8.80 1 4 29 16.90 10.40 0 4 -29 54.39 15.10 0 4 -29 76.49 19.00 0 -4 29 7.60 8.20 0 -4 29 27.50 9.80 0 -4 29 11.60 13.90 0 3 -29 27.70 13.30 0 3 -29 53.79 17.30 0 -3 29 1.30 12.10 0 -3 29 10.60 8.70 0 -3 29 -6.80 7.10 0 2 -29 58.39 15.60 0 -2 29 33.70 10.10 0 -2 29 14.20 12.60 0 -2 29 18.80 8.00 0 1 -29 46.60 17.90 0 1 -29 42.40 11.10 0 1 -29 38.30 13.30 0 -1 29 18.40 9.20 0 -1 29 11.40 12.00 0 -1 29 10.80 7.70 0 0 -29 41.60 12.90 0 0 -29 27.00 14.90 0 0 29 1.80 6.70 0 0 29 -1.40 5.80 0 0 29 6.10 11.20 0 -1 -29 48.40 17.50 0 -1 -29 59.89 13.90 0 1 29 20.90 11.60 0 1 29 21.80 8.70 0 1 29 19.10 9.30 0 -2 -29 58.39 14.90 0 -2 -29 43.40 15.20 0 2 29 20.70 8.50 0 2 29 36.70 12.30 0 2 29 28.60 10.20 0 -3 -29 33.50 13.50 0 -3 -29 44.90 16.30 0 3 29 14.30 10.10 0 3 29 10.90 9.00 0 -4 -29 57.09 16.70 0 4 29 6.00 9.50 0 4 29 26.80 11.70 1 4 -29 52.59 16.50 1 4 -29 38.00 13.40 -1 -4 29 3.40 7.70 -1 -4 29 3.90 12.40 -1 -4 29 8.20 8.80 1 3 -29 49.90 14.70 1 3 -29 70.49 18.20 -1 -3 29 40.10 10.30 -1 -3 29 34.70 8.80 -1 -3 29 21.90 13.80 1 2 -29 29.00 12.70 1 2 -29 38.00 15.10 -1 -2 29 -3.40 11.20 -1 -2 29 -0.80 7.00 -1 -2 29 14.50 8.70 1 1 -29 27.90 15.30 1 1 -29 27.30 12.30 -1 -1 29 11.30 8.20 -1 -1 29 4.00 7.00 -1 -1 29 3.00 11.60 1 0 -29 35.10 11.70 1 0 -29 49.10 16.70 -1 0 29 -8.20 7.20 -1 0 29 8.20 8.20 -1 0 29 8.90 11.10 1 -1 -29 29.30 15.10 1 -1 -29 25.90 11.40 -1 1 29 6.40 9.90 -1 1 29 9.30 8.40 -1 1 29 2.40 10.80 1 -2 -29 35.20 12.60 1 -2 -29 33.20 15.40 -1 2 29 1.00 8.20 -1 2 29 15.00 10.80 1 -3 -29 78.19 18.50 1 -3 -29 68.29 16.20 -1 3 29 47.60 13.40 -1 3 29 28.90 10.70 1 -4 -29 69.09 17.50 1 -4 -29 48.10 14.80 -1 4 29 -0.30 9.40 -1 4 29 19.50 10.60 2 4 -29 85.79 17.40 -2 -4 29 71.69 12.70 -2 -4 29 52.59 16.70 -2 -4 29 67.39 10.80 2 3 -29 46.40 14.60 2 3 -29 31.90 13.00 -2 -3 29 13.20 8.50 -2 -3 29 -6.80 11.10 -2 -3 29 -11.80 7.20 2 2 -29 31.30 10.10 2 2 -29 26.40 12.30 2 2 -29 41.20 15.20 -2 -2 29 6.30 7.10 -2 -2 29 11.10 8.20 -2 -2 29 1.80 11.50 2 1 -29 29.70 10.80 2 1 -29 35.90 12.80 2 1 -29 39.90 15.60 -2 -1 29 3.20 11.30 -2 -1 29 10.60 8.40 -2 -1 29 -5.70 6.90 2 0 -29 41.60 11.80 2 0 -29 35.80 15.40 -2 0 29 8.20 8.30 -2 0 29 10.60 10.90 2 -1 -29 30.50 15.10 2 -1 -29 28.30 12.00 -2 1 29 2.00 7.90 -2 1 29 12.20 10.80 2 -2 -29 36.30 15.50 2 -2 -29 32.50 12.30 -2 2 29 3.30 8.40 -2 2 29 7.60 10.20 2 -3 -29 43.30 15.80 2 -3 -29 30.40 12.90 -2 3 29 11.40 9.10 -2 3 29 17.60 10.50 2 -4 -29 110.09 19.20 -2 4 29 82.69 16.10 -2 4 29 65.29 12.80 -3 -4 29 2.80 8.20 3 3 -29 45.40 14.00 -3 -3 29 33.90 10.30 -3 -3 29 21.20 8.80 -3 -3 29 14.20 12.90 3 2 -29 100.69 21.00 3 2 -29 66.39 15.70 -3 -2 29 62.59 11.90 -3 -2 29 46.50 15.10 -3 -2 29 34.40 8.90 3 1 -29 54.29 16.70 3 1 -29 34.10 10.70 -3 -1 29 10.90 8.60 -3 -1 29 6.20 11.40 3 0 -29 38.30 15.20 -3 0 29 17.80 11.60 -3 0 29 2.10 7.80 3 -1 -29 31.40 11.70 3 -1 -29 42.10 15.50 -3 1 29 -5.70 7.90 -3 1 29 9.10 10.40 3 -2 -29 83.09 16.80 3 -2 -29 90.59 20.30 -3 2 29 57.59 12.00 -3 2 29 48.00 13.90 3 -3 -29 49.20 14.60 3 -3 -29 66.29 18.20 -3 3 29 22.10 10.00 -3 3 29 18.40 9.60 -3 4 29 8.50 10.00 4 3 -29 41.80 13.70 -4 -3 29 17.90 9.10 -4 -3 29 9.90 12.30 -4 -3 29 -4.70 7.50 4 2 -29 47.80 15.50 4 2 -29 52.89 12.70 4 2 -29 46.40 13.10 -4 -2 29 17.80 12.90 -4 -2 29 15.30 8.70 4 1 -29 133.09 22.00 4 1 -29 148.99 18.30 4 0 -29 37.60 15.20 4 0 -29 28.70 11.50 -4 0 29 4.50 8.10 -4 0 29 11.40 10.80 4 -1 -29 72.69 15.20 -4 1 29 51.29 14.60 -4 1 29 49.50 11.20 4 -2 -29 66.19 18.10 4 -2 -29 44.00 13.50 -4 2 29 9.10 8.90 -4 2 29 14.30 10.90 4 -3 -29 67.59 18.00 4 -3 -29 38.00 13.90 -4 3 29 12.70 9.50 -4 3 29 7.60 10.40 5 3 -29 56.29 14.20 -5 -3 29 22.50 9.50 5 2 -29 49.60 11.90 5 2 -29 62.99 16.80 -5 -2 29 30.40 13.20 -5 -2 29 11.70 8.70 5 1 -29 55.79 16.50 5 1 -29 38.60 11.60 -5 -1 29 16.80 11.70 -5 -1 29 16.10 9.70 5 0 -29 48.60 16.40 5 0 -29 38.30 11.90 -5 0 29 3.30 8.10 -5 0 29 14.80 11.40 5 -1 -29 48.50 16.40 5 -1 -29 52.39 13.70 -5 1 29 17.10 9.00 -5 1 29 9.40 10.30 5 -2 -29 49.60 13.30 5 -2 -29 54.59 16.90 -5 2 29 1.40 8.50 -5 2 29 12.60 10.90 5 -3 -29 51.19 14.30 5 -3 -29 63.99 17.20 -5 3 29 -11.70 16.40 -5 3 29 19.80 9.80 6 2 -29 60.09 16.80 -6 -2 29 23.00 9.70 -6 -2 29 19.30 12.10 6 1 -29 47.50 15.70 6 1 -29 40.50 11.70 -6 -1 29 7.20 7.90 -6 -1 29 8.10 10.70 -6 -1 29 -24.30 13.20 6 0 -29 39.10 15.40 -6 0 29 9.50 11.50 -6 0 29 3.30 8.00 -6 0 29 -24.30 13.90 6 -1 -29 41.00 12.40 6 -1 -29 44.10 15.10 -6 1 29 6.90 8.50 -6 1 29 -20.50 13.60 -6 1 29 6.50 10.30 6 -2 -29 66.39 17.70 6 -2 -29 55.09 14.30 -6 2 29 8.20 14.40 -6 2 29 26.60 10.30 -7 0 29 10.70 8.40 -4 0 -30 39.80 13.00 -4 0 -30 68.59 22.00 -4 0 -30 40.90 13.50 4 0 30 18.30 9.20 4 1 30 33.20 10.70 -3 1 -30 55.79 20.20 -3 1 -30 42.60 13.20 3 -1 30 15.10 9.10 3 -1 30 4.10 8.30 3 -1 30 0.40 10.90 -3 0 -30 109.39 18.10 -3 0 -30 109.89 24.00 -3 0 -30 68.89 15.50 3 0 30 67.09 12.30 3 0 30 53.49 11.20 3 0 30 61.39 16.00 -3 -1 -30 51.89 18.90 -3 -1 -30 54.19 15.20 3 1 30 9.60 8.90 3 1 30 13.10 9.00 3 1 30 2.20 10.40 -2 2 -30 68.29 20.50 -2 2 -30 55.19 15.40 2 -2 30 29.50 14.80 2 -2 30 22.20 8.90 2 -2 30 33.10 10.10 -2 1 -30 59.09 19.10 -2 1 -30 37.00 13.40 2 -1 30 22.00 9.40 2 -1 30 5.20 12.00 2 -1 30 0.40 7.80 -2 0 -30 68.19 14.50 -2 0 -30 62.99 14.30 -2 0 -30 88.29 21.80 2 0 30 44.60 9.70 2 0 30 27.10 13.00 2 0 30 29.20 9.90 -2 -1 -30 58.99 19.20 -2 -1 -30 50.39 12.90 -2 -1 -30 34.60 14.10 2 1 30 9.60 7.80 2 1 30 10.20 8.80 -2 -2 -30 69.59 20.00 -2 -2 -30 59.29 16.30 2 2 30 32.00 10.90 2 2 30 42.70 13.20 -1 2 -30 36.20 13.40 -1 2 -30 57.69 18.50 1 -2 30 14.50 9.30 1 -2 30 15.90 12.90 1 -2 30 11.30 9.00 -1 1 -30 27.40 11.80 -1 1 -30 36.60 11.30 -1 1 -30 39.00 17.10 1 -1 30 12.80 8.90 1 -1 30 3.20 11.20 1 -1 30 2.10 7.80 -1 0 -30 49.20 17.30 -1 0 -30 34.40 12.70 -1 0 -30 44.00 12.40 1 0 30 10.00 8.60 -1 -1 -30 43.90 13.80 -1 -1 -30 45.60 17.20 1 1 30 12.00 8.80 1 1 30 10.90 11.00 1 1 30 1.00 7.70 -1 -2 -30 41.90 16.40 -1 -2 -30 33.00 13.80 1 2 30 12.60 9.40 1 2 30 3.60 7.90 1 2 30 14.50 10.80 0 2 -30 47.30 17.10 0 2 -30 35.00 13.20 0 -2 30 2.00 11.40 0 -2 30 -4.40 8.10 0 -2 30 12.70 8.70 0 1 -30 33.50 12.40 0 1 -30 42.90 11.50 0 1 -30 50.59 17.90 0 -1 30 9.60 12.20 0 -1 30 6.90 7.50 0 -1 30 8.50 8.30 0 0 -30 51.19 17.60 0 0 -30 81.69 15.60 0 0 -30 69.19 14.90 0 0 30 30.30 13.30 0 0 30 38.10 10.40 0 0 30 22.80 8.80 0 -1 -30 36.00 16.30 0 -1 -30 42.80 12.40 0 1 30 -3.30 7.50 0 1 30 13.40 11.20 0 1 30 14.30 9.00 0 -2 -30 35.60 13.00 0 -2 -30 38.50 15.30 0 2 30 8.10 10.30 0 2 30 3.60 8.60 1 2 -30 92.89 20.60 1 2 -30 76.69 17.00 -1 -2 30 51.29 16.20 -1 -2 30 23.20 9.40 -1 -2 30 56.69 11.60 1 1 -30 96.39 18.20 -1 -1 30 86.49 13.30 -1 -1 30 66.09 17.00 -1 -1 30 53.29 10.20 1 0 -30 144.79 23.40 1 0 -30 136.79 17.10 -1 0 30 65.39 16.60 -1 0 30 89.69 13.80 -1 0 30 75.39 11.20 1 -1 -30 138.29 23.10 1 -1 -30 90.99 16.50 -1 1 30 68.89 12.90 -1 1 30 74.19 16.40 1 -2 -30 101.39 17.70 -1 2 30 64.99 15.50 -1 2 30 47.40 11.80 2 2 -30 46.00 16.10 2 2 -30 31.80 12.50 -2 -2 30 9.00 8.20 -2 -2 30 6.00 12.20 -2 -2 30 6.10 8.30 2 1 -30 59.39 14.70 2 1 -30 69.59 13.40 2 1 -30 76.89 19.30 -2 -1 30 27.60 13.90 -2 -1 30 27.60 9.80 2 0 -30 65.79 17.80 2 0 -30 39.20 11.90 -2 0 30 18.80 12.10 -2 0 30 21.90 9.40 2 -1 -30 78.49 19.00 2 -1 -30 64.79 14.80 -2 1 30 36.90 13.20 -2 1 30 32.90 10.40 2 -2 -30 35.10 12.50 2 -2 -30 46.80 15.40 -2 2 30 -0.90 8.60 -2 2 30 17.10 11.40 3 2 -30 62.29 17.70 -3 -2 30 10.10 9.00 3 1 -30 88.19 19.70 -3 -1 30 38.50 14.20 -3 -1 30 38.30 10.70 3 0 -30 61.49 13.80 3 0 -30 86.19 20.00 -3 0 30 40.40 14.40 -3 0 30 30.20 10.00 3 -1 -30 83.09 16.40 3 -1 -30 52.69 15.70 -3 1 30 36.00 13.20 -3 1 30 34.00 10.80 3 -2 -30 29.50 12.70 -3 2 30 7.30 9.20 4 1 -30 179.88 24.90 4 1 -30 160.78 17.60 4 0 -30 149.69 23.40 4 0 -30 153.38 17.90 -4 0 30 90.39 14.30 -4 0 30 90.79 18.10 4 -1 -30 160.28 23.90 4 -1 -30 144.79 18.40 -4 1 30 88.29 14.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 51757 _shelx_res_file ; TITL cjh01-1_a.res in P2(1)/c cjh01-1_a.res created by SHELXL-2018/3 at 13:15:36 on 31-May-2024 REM Old TITL cjh01-1 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.144, Rweak 0.021, Alpha 0.057 REM 0.659 for 519 systematic absences, Orientation as input REM Formula found by SHELXT: C62 B2 N7 Co CELL 0.71073 18.1245 11.6689 26.0675 90.000 90.332 90.000 ZERR 4.000 0.0016 0.0010 0.0023 0.000 0.002 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H B N CO UNIT 252 280 8 24 4 ACTA TEMP -140 SIZE 0.051 0.089 0.101 L.S. 10 BOND $H LIST 4 FMAP 2 PLAN 20 OMIT 1 0 0 OMIT 0 0 2 HTAB WGHT 0.033000 3.711600 FVAR 0.24534 CO1 5 0.260793 0.217942 0.371977 11.00000 0.02078 0.02259 = 0.02047 0.00164 0.00212 0.00069 N1 4 0.365902 0.277372 0.345764 11.00000 0.02338 0.02753 = 0.03596 -0.00215 0.00510 -0.00432 N2 4 0.326894 0.104190 0.417301 11.00000 0.03242 0.04127 = 0.03554 0.00764 -0.00326 0.00507 N3 4 0.276758 0.090520 0.314022 11.00000 0.03443 0.02596 = 0.02885 -0.00401 0.00364 -0.00309 N4 4 0.250608 0.340996 0.431826 11.00000 0.04026 0.03920 = 0.03261 -0.00779 0.00731 -0.00252 N5 4 0.202705 0.328044 0.322820 11.00000 0.03126 0.03695 = 0.02912 0.00845 0.00886 0.00766 N6 4 0.159606 0.147539 0.401185 11.00000 0.02642 0.03898 = 0.02530 0.00623 0.00294 -0.00384 C1 1 0.375951 0.402538 0.349689 11.00000 0.04792 0.03533 = 0.06701 -0.00894 0.01625 -0.02042 AFIX 137 H1A 2 0.422038 0.424526 0.332853 11.00000 -1.50000 H1B 2 0.378075 0.424796 0.385918 11.00000 -1.50000 H1C 2 0.334415 0.441435 0.332902 11.00000 -1.50000 AFIX 0 C10 1 0.238345 0.403780 0.463615 11.00000 0.04103 0.04004 = 0.03163 -0.00512 0.00418 -0.00550 C2 1 0.424965 0.217162 0.375250 11.00000 0.02189 0.05735 = 0.05421 -0.00759 -0.00460 -0.00130 AFIX 23 H2A 2 0.465850 0.271200 0.382424 11.00000 -1.20000 H2B 2 0.444754 0.153452 0.354361 11.00000 -1.20000 AFIX 0 C11 1 0.221966 0.483716 0.504800 11.00000 0.09046 0.06165 = 0.04741 -0.02938 0.01545 -0.00563 AFIX 137 H11A 2 0.219402 0.561709 0.490959 11.00000 -1.50000 H11B 2 0.260938 0.479669 0.530955 11.00000 -1.50000 H11C 2 0.174521 0.463643 0.520243 11.00000 -1.50000 AFIX 0 C12 1 0.171027 0.383877 0.294503 11.00000 0.03087 0.03257 = 0.02432 0.00395 0.00844 0.00350 C13 1 0.131067 0.452434 0.257341 11.00000 0.04623 0.03993 = 0.02630 0.00885 0.00081 0.00969 AFIX 137 H13A 2 0.089775 0.490987 0.274242 11.00000 -1.50000 H13B 2 0.112109 0.402832 0.229941 11.00000 -1.50000 H13C 2 0.164259 0.509904 0.242679 11.00000 -1.50000 AFIX 0 C14 1 0.113753 0.117184 0.427391 11.00000 0.03002 0.03252 = 0.02500 0.00034 -0.00160 -0.00109 C15 1 0.056839 0.078140 0.462404 11.00000 0.03916 0.05245 = 0.03082 0.00345 0.01173 -0.01116 AFIX 137 H15A 2 0.013637 0.128266 0.459471 11.00000 -1.50000 H15B 2 0.075843 0.080410 0.497662 11.00000 -1.50000 H15C 2 0.042689 -0.000565 0.453668 11.00000 -1.50000 AFIX 0 C16 1 0.007285 0.830086 0.370252 11.00000 0.03255 0.03331 = 0.02341 -0.01014 -0.00183 0.00177 C17 1 -0.063564 0.824879 0.391563 11.00000 0.04038 0.04353 = 0.03578 -0.01130 0.00463 0.00698 AFIX 43 H17 2 -0.079004 0.755634 0.407378 11.00000 -1.20000 AFIX 0 C18 1 -0.112189 0.917568 0.390399 11.00000 0.04087 0.07238 = 0.04097 -0.02718 -0.00319 0.02206 AFIX 43 H18 2 -0.159485 0.910873 0.405629 11.00000 -1.20000 AFIX 0 C19 1 -0.091791 1.018874 0.367205 11.00000 0.06731 0.05055 = 0.04575 -0.02534 -0.02146 0.03166 AFIX 43 H19 2 -0.124900 1.081956 0.366144 11.00000 -1.20000 AFIX 0 C20 1 -0.023309 1.027429 0.345744 11.00000 0.06404 0.03177 = 0.05060 -0.01046 -0.01927 0.01280 AFIX 43 H20 2 -0.008721 1.096751 0.329605 11.00000 -1.20000 AFIX 0 C21 1 0.025051 0.934823 0.347493 11.00000 0.03971 0.03135 = 0.03949 -0.00865 -0.00677 0.00424 AFIX 43 H21 2 0.072390 0.943247 0.332497 11.00000 -1.20000 AFIX 0 C22 1 0.025759 0.599184 0.362428 11.00000 0.01942 0.03080 = 0.02236 -0.00106 0.00783 0.00288 C23 1 0.055530 0.495539 0.379906 11.00000 0.02386 0.03509 = 0.02524 0.00309 0.00566 0.00166 AFIX 43 H23 2 0.096128 0.498067 0.403093 11.00000 -1.20000 AFIX 0 C24 1 0.028596 0.389289 0.364993 11.00000 0.03212 0.02825 = 0.03186 0.00579 0.00917 0.00276 AFIX 43 H24 2 0.050531 0.321261 0.378052 11.00000 -1.20000 AFIX 0 C25 1 -0.029936 0.382537 0.331261 11.00000 0.03407 0.02788 = 0.04115 -0.00240 0.00682 -0.00111 AFIX 43 H25 2 -0.048891 0.310153 0.320958 11.00000 -1.20000 AFIX 0 C26 1 -0.060531 0.482080 0.312717 11.00000 0.02843 0.03664 = 0.04188 -0.00366 -0.00670 0.00060 AFIX 43 H26 2 -0.100747 0.478443 0.289238 11.00000 -1.20000 AFIX 0 C27 1 -0.033187 0.588006 0.327993 11.00000 0.03009 0.02694 = 0.03434 0.00135 0.00233 0.00373 AFIX 43 H27 2 -0.055402 0.655411 0.314519 11.00000 -1.20000 AFIX 0 C28 1 0.092378 0.726500 0.436501 11.00000 0.03487 0.02921 = 0.03084 -0.00584 0.00228 0.00854 C29 1 0.149784 0.797026 0.453215 11.00000 0.05844 0.02974 = 0.03127 0.00003 -0.00787 0.00189 AFIX 43 H29 2 0.175407 0.841343 0.428474 11.00000 -1.20000 AFIX 0 C30 1 0.171369 0.805625 0.504450 11.00000 0.07457 0.03372 = 0.04036 -0.00651 -0.01869 0.00569 AFIX 43 H30 2 0.210939 0.854754 0.513967 11.00000 -1.20000 AFIX 0 C31 1 0.135415 0.743098 0.541055 11.00000 0.09510 0.04559 = 0.02289 -0.01196 -0.00651 0.01926 AFIX 43 H31 2 0.150092 0.747998 0.576031 11.00000 -1.20000 AFIX 0 C32 1 0.077876 0.673171 0.526690 11.00000 0.07559 0.06320 = 0.02786 -0.00548 0.02003 0.00837 AFIX 43 H32 2 0.052427 0.629733 0.551826 11.00000 -1.20000 AFIX 0 C33 1 0.056954 0.665972 0.475589 11.00000 0.04836 0.05454 = 0.02969 -0.00876 0.01554 0.00124 AFIX 43 H33 2 0.016674 0.617682 0.466679 11.00000 -1.20000 AFIX 0 C34 1 0.133622 0.726967 0.335691 11.00000 0.02559 0.01838 = 0.02999 -0.00181 -0.00030 -0.00217 C35 1 0.123180 0.759064 0.284310 11.00000 0.02614 0.02994 = 0.03232 -0.00061 0.00213 0.00188 AFIX 43 H35 2 0.075907 0.785862 0.273925 11.00000 -1.20000 AFIX 0 C36 1 0.178513 0.753529 0.248028 11.00000 0.03570 0.03650 = 0.03246 0.00088 0.00761 -0.00214 AFIX 43 H36 2 0.168751 0.776946 0.213751 11.00000 -1.20000 AFIX 0 C37 1 0.247632 0.714254 0.261368 11.00000 0.02855 0.03319 = 0.04736 -0.01075 0.01442 -0.00578 AFIX 43 H37 2 0.285910 0.711189 0.236663 11.00000 -1.20000 AFIX 0 C38 1 0.260384 0.679419 0.311215 11.00000 0.02470 0.02782 = 0.05309 -0.00908 0.00071 0.00102 AFIX 43 H38 2 0.307613 0.651257 0.320943 11.00000 -1.20000 AFIX 0 C39 1 0.204501 0.685426 0.347072 11.00000 0.03173 0.02418 = 0.03573 -0.00035 -0.00173 -0.00074 AFIX 43 H39 2 0.214621 0.660199 0.381041 11.00000 -1.20000 AFIX 0 C40 1 0.512576 0.752032 0.319199 11.00000 0.02087 0.02123 = 0.02249 0.00094 0.00779 -0.00072 C41 1 0.493225 0.650467 0.293793 11.00000 0.02804 0.02182 = 0.02709 0.00274 0.00439 -0.00020 AFIX 43 H41 2 0.507706 0.579698 0.308791 11.00000 -1.20000 AFIX 0 C42 1 0.454184 0.647667 0.248062 11.00000 0.02577 0.02690 = 0.02578 -0.00467 0.00390 -0.00320 AFIX 43 H42 2 0.442318 0.576246 0.232589 11.00000 -1.20000 AFIX 0 C43 1 0.432401 0.748962 0.224840 11.00000 0.02171 0.03349 = 0.01947 -0.00106 0.00291 0.00037 AFIX 43 H43 2 0.407080 0.748123 0.192831 11.00000 -1.20000 AFIX 0 C44 1 0.448187 0.850912 0.249087 11.00000 0.02624 0.02367 = 0.02640 0.00227 0.00363 0.00528 AFIX 43 H44 2 0.432404 0.921059 0.234134 11.00000 -1.20000 AFIX 0 C45 1 0.486878 0.852258 0.295098 11.00000 0.02696 0.02325 = 0.02603 -0.00201 0.00431 0.00181 AFIX 43 H45 2 0.496444 0.923995 0.311034 11.00000 -1.20000 AFIX 0 C46 1 0.498710 0.711239 0.419397 11.00000 0.03544 0.01485 = 0.02365 -0.00326 0.00547 0.00041 C47 1 0.522917 0.669972 0.466872 11.00000 0.04275 0.02850 = 0.02330 -0.00189 0.00286 -0.00083 AFIX 43 H47 2 0.574506 0.662922 0.472701 11.00000 -1.20000 AFIX 0 C48 1 0.475635 0.638972 0.505682 11.00000 0.06432 0.03005 = 0.02222 0.00069 0.00520 -0.00043 AFIX 43 H48 2 0.494909 0.610553 0.537172 11.00000 -1.20000 AFIX 0 C49 1 0.400534 0.649093 0.498923 11.00000 0.06084 0.03520 = 0.02845 -0.00050 0.02103 -0.00845 AFIX 43 H49 2 0.367657 0.628399 0.525620 11.00000 -1.20000 AFIX 0 C50 1 0.373897 0.689663 0.452879 11.00000 0.03848 0.04563 = 0.03934 0.00007 0.01452 -0.00417 AFIX 43 H50 2 0.322223 0.697581 0.447692 11.00000 -1.20000 AFIX 0 C51 1 0.422188 0.719015 0.414041 11.00000 0.03806 0.02970 = 0.02901 0.00271 0.00577 0.00091 AFIX 43 H51 2 0.402379 0.745589 0.382387 11.00000 -1.20000 AFIX 0 C52 1 0.626011 0.660614 0.372504 11.00000 0.03463 0.02749 = 0.01316 0.00039 0.00163 0.00268 C53 1 0.700634 0.689693 0.367367 11.00000 0.03651 0.03682 = 0.03367 0.00130 0.00214 0.00219 AFIX 43 H53 2 0.713522 0.768607 0.367493 11.00000 -1.20000 AFIX 0 C54 1 0.756553 0.610023 0.362126 11.00000 0.03366 0.05826 = 0.04190 0.00152 0.00356 0.01054 AFIX 43 H54 2 0.806155 0.635014 0.358631 11.00000 -1.20000 AFIX 0 C55 1 0.740650 0.494428 0.361949 11.00000 0.04740 0.05560 = 0.03115 -0.00259 -0.00040 0.02612 AFIX 43 H55 2 0.778641 0.439427 0.357178 11.00000 -1.20000 AFIX 0 C56 1 0.668827 0.460343 0.368803 11.00000 0.05775 0.03172 = 0.02254 0.00020 -0.00637 0.01310 AFIX 43 H56 2 0.656977 0.381066 0.369708 11.00000 -1.20000 AFIX 0 C57 1 0.613332 0.541997 0.374431 11.00000 0.03773 0.03141 = 0.01990 0.00192 -0.00114 0.00229 AFIX 43 H57 2 0.564322 0.516009 0.379859 11.00000 -1.20000 AFIX 0 C58 1 0.585645 0.883393 0.386955 11.00000 0.02803 0.02494 = 0.02146 0.00407 -0.00516 0.00119 C59 1 0.634585 0.939861 0.354325 11.00000 0.03659 0.03233 = 0.02869 0.00612 -0.00411 -0.00261 AFIX 43 H59 2 0.650183 0.901700 0.324077 11.00000 -1.20000 AFIX 0 C60 1 0.661607 1.049814 0.364149 11.00000 0.04086 0.03661 = 0.04443 0.01914 -0.00888 -0.00968 AFIX 43 H60 2 0.696074 1.083950 0.341477 11.00000 -1.20000 AFIX 0 C61 1 0.638016 1.108630 0.406929 11.00000 0.05195 0.02296 = 0.04668 0.00548 -0.02308 -0.00476 AFIX 43 H61 2 0.656582 1.183091 0.414112 11.00000 -1.20000 AFIX 0 C62 1 0.587639 1.058960 0.438992 11.00000 0.04723 0.02530 = 0.03438 -0.00244 -0.01541 0.00557 AFIX 43 H62 2 0.569907 1.099913 0.467905 11.00000 -1.20000 AFIX 0 C63 1 0.562446 0.948227 0.429114 11.00000 0.03358 0.02466 = 0.02729 0.00377 -0.00692 0.00099 AFIX 43 H63 2 0.527914 0.915169 0.452055 11.00000 -1.20000 AFIX 0 B1 3 0.064705 0.722083 0.376331 11.00000 0.02651 0.02711 = 0.02739 -0.00142 0.00153 0.00286 B2 3 0.556858 0.752503 0.374812 11.00000 0.02949 0.01830 = 0.02440 0.00068 0.00268 -0.00048 C3 1 0.395921 0.170302 0.425237 11.00000 0.02699 0.07205 = 0.04186 0.00134 -0.01106 0.00504 AFIX 23 H3A 2 0.433697 0.120075 0.441105 11.00000 -1.20000 H3B 2 0.386375 0.234537 0.449104 11.00000 -1.20000 AFIX 0 C4 1 0.295288 0.074554 0.467690 11.00000 0.05033 0.07302 = 0.03808 0.02767 -0.00788 0.01022 AFIX 137 H4A 2 0.331093 0.029267 0.487397 11.00000 -1.50000 H4B 2 0.250094 0.029752 0.462629 11.00000 -1.50000 H4C 2 0.283707 0.144979 0.486477 11.00000 -1.50000 AFIX 0 C5 1 0.340490 -0.002582 0.386911 11.00000 0.05832 0.03347 = 0.06106 0.01349 0.00416 0.01584 AFIX 23 H5A 2 0.337486 -0.069866 0.409939 11.00000 -1.20000 H5B 2 0.390920 0.000031 0.372569 11.00000 -1.20000 AFIX 0 C6 1 0.285762 -0.016349 0.343950 11.00000 0.06630 0.02456 = 0.04849 -0.00166 0.01222 -0.00045 AFIX 23 H6A 2 0.302433 -0.078417 0.320865 11.00000 -1.20000 H6B 2 0.237452 -0.039030 0.358283 11.00000 -1.20000 AFIX 0 C7 1 0.213414 0.077113 0.278412 11.00000 0.04563 0.05928 = 0.03362 -0.01491 -0.00161 -0.01641 AFIX 137 H7A 2 0.220658 0.008683 0.257235 11.00000 -1.50000 H7B 2 0.209788 0.144769 0.256266 11.00000 -1.50000 H7C 2 0.167867 0.069012 0.298162 11.00000 -1.50000 AFIX 0 C8 1 0.344298 0.119521 0.284109 11.00000 0.03332 0.03514 = 0.03051 -0.00772 0.00881 0.00336 AFIX 23 H8A 2 0.335250 0.103584 0.247305 11.00000 -1.20000 H8B 2 0.385719 0.070483 0.295726 11.00000 -1.20000 AFIX 0 C9 1 0.365144 0.243761 0.290736 11.00000 0.02642 0.03892 = 0.03247 0.00175 0.01500 -0.00051 AFIX 23 H9A 2 0.414619 0.256903 0.275954 11.00000 -1.20000 H9B 2 0.329423 0.292381 0.271835 11.00000 -1.20000 CONF MERG 2 AFIX 0 HKLF 4 REM cjh01-1_a.res in P2(1)/c REM wR2 = 0.1069, GooF = S = 1.142, Restrained GooF = 1.142 for all data REM R1 = 0.0562 for 6984 Fo > 4sig(Fo) and 0.0897 for all 9437 data REM 655 parameters refined using 0 restraints END WGHT 0.0330 3.7117 REM Instructions for potential hydrogen bonds HTAB C9 N5 REM Highest difference peak 0.593, deepest hole -0.632, 1-sigma level 0.051 Q1 1 0.2598 0.2081 0.4109 11.00000 0.05 0.59 Q2 1 0.2606 0.2059 0.3326 11.00000 0.05 0.47 Q3 1 0.2235 0.2616 0.3993 11.00000 0.05 0.39 Q4 1 0.2230 0.1827 0.3985 11.00000 0.05 0.39 Q5 1 0.3099 0.2469 0.3527 11.00000 0.05 0.39 Q6 1 0.2751 0.2661 0.3411 11.00000 0.05 0.38 Q7 1 0.3092 0.2024 0.3524 11.00000 0.05 0.35 Q8 1 0.2736 0.1779 0.3379 11.00000 0.05 0.33 Q9 1 0.2615 0.1018 0.3490 11.00000 0.05 0.33 Q10 1 0.2595 0.3414 0.3973 11.00000 0.05 0.33 Q11 1 0.2094 0.3128 0.3597 11.00000 0.05 0.30 Q12 1 0.1032 0.7242 0.3613 11.00000 0.05 0.29 Q13 1 0.1586 0.4383 0.2241 11.00000 0.05 0.29 Q14 1 0.2707 0.3469 0.3565 11.00000 0.05 0.28 Q15 1 0.1164 0.7120 0.3104 11.00000 0.05 0.23 Q16 1 0.3019 0.1062 0.3787 11.00000 0.05 0.23 Q17 1 0.2051 0.4465 0.5374 11.00000 0.05 0.22 Q18 1 0.1541 0.7968 0.2705 11.00000 0.05 0.22 Q19 1 0.0880 0.7033 0.4052 11.00000 0.05 0.21 Q20 1 0.5257 0.7404 0.3982 11.00000 0.05 0.21 ; _shelx_res_checksum 11019 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co Co1 0.26079(2) 0.21794(3) 0.37198(2) 0.02127(11) Uani d 1 . . N N1 0.36590(12) 0.2774(2) 0.34576(9) 0.0289(6) Uani d 1 . . N N2 0.32689(13) 0.1042(2) 0.41730(9) 0.0364(6) Uani d 1 . . N N3 0.27676(13) 0.09052(19) 0.31402(8) 0.0297(6) Uani d 1 . . N N4 0.25061(14) 0.3410(2) 0.43183(9) 0.0373(6) Uani d 1 . . N N5 0.20270(13) 0.3280(2) 0.32282(9) 0.0324(6) Uani d 1 . . N N6 0.15961(13) 0.1475(2) 0.40119(9) 0.0302(6) Uani d 1 . . C C1 0.37595(19) 0.4025(3) 0.34969(14) 0.0500(9) Uani d 1 . . H H1A 0.422038 0.424526 0.332853 0.075 Uiso calc 1 . . H H1B 0.378075 0.424796 0.385918 0.075 Uiso calc 1 . . H H1C 0.334415 0.441435 0.332902 0.075 Uiso calc 1 . . C C10 0.23835(17) 0.4038(3) 0.46362(12) 0.0376(8) Uani d 1 . . C C2 0.42496(16) 0.2172(3) 0.37525(12) 0.0445(8) Uani d 1 . . H H2A 0.465850 0.271200 0.382424 0.053 Uiso calc 1 . . H H2B 0.444754 0.153452 0.354361 0.053 Uiso calc 1 . . C C11 0.2220(2) 0.4837(3) 0.50480(13) 0.0664(12) Uani d 1 . . H H11A 0.219402 0.561709 0.490959 0.100 Uiso calc 1 . . H H11B 0.260938 0.479669 0.530955 0.100 Uiso calc 1 . . H H11C 0.174521 0.463643 0.520243 0.100 Uiso calc 1 . . C C12 0.17103(16) 0.3839(3) 0.29450(11) 0.0292(7) Uani d 1 . . C C13 0.13107(17) 0.4524(3) 0.25734(11) 0.0375(8) Uani d 1 . . H H13A 0.089775 0.490987 0.274242 0.056 Uiso calc 1 . . H H13B 0.112109 0.402832 0.229941 0.056 Uiso calc 1 . . H H13C 0.164259 0.509904 0.242679 0.056 Uiso calc 1 . . C C14 0.11375(16) 0.1172(3) 0.42739(11) 0.0292(7) Uani d 1 . . C C15 0.05684(17) 0.0781(3) 0.46240(11) 0.0408(8) Uani d 1 . . H H15A 0.013637 0.128266 0.459471 0.061 Uiso calc 1 . . H H15B 0.075843 0.080410 0.497662 0.061 Uiso calc 1 . . H H15C 0.042689 -0.000565 0.453668 0.061 Uiso calc 1 . . C C16 0.00729(16) 0.8301(3) 0.37025(10) 0.0298(7) Uani d 1 . . C C17 -0.06356(17) 0.8249(3) 0.39156(11) 0.0399(8) Uani d 1 . . H H17 -0.079004 0.755634 0.407378 0.048 Uiso calc 1 . . C C18 -0.11219(19) 0.9176(3) 0.39040(13) 0.0514(10) Uani d 1 . . H H18 -0.159485 0.910873 0.405629 0.062 Uiso calc 1 . . C C19 -0.0918(2) 1.0189(3) 0.36720(13) 0.0546(11) Uani d 1 . . H H19 -0.124900 1.081956 0.366144 0.066 Uiso calc 1 . . C C20 -0.0233(2) 1.0274(3) 0.34574(13) 0.0489(9) Uani d 1 . . H H20 -0.008721 1.096751 0.329605 0.059 Uiso calc 1 . . C C21 0.02505(17) 0.9348(3) 0.34749(11) 0.0369(8) Uani d 1 . . H H21 0.072390 0.943247 0.332497 0.044 Uiso calc 1 . . C C22 0.02576(14) 0.5992(2) 0.36243(10) 0.0242(6) Uani d 1 . . C C23 0.05553(15) 0.4955(2) 0.37991(10) 0.0280(7) Uani d 1 . . H H23 0.096128 0.498067 0.403093 0.034 Uiso calc 1 . . C C24 0.02860(16) 0.3893(3) 0.36499(11) 0.0307(7) Uani d 1 . . H H24 0.050531 0.321261 0.378052 0.037 Uiso calc 1 . . C C25 -0.02994(16) 0.3825(3) 0.33126(11) 0.0343(7) Uani d 1 . . H H25 -0.048891 0.310153 0.320958 0.041 Uiso calc 1 . . C C26 -0.06053(16) 0.4821(3) 0.31272(12) 0.0357(7) Uani d 1 . . H H26 -0.100747 0.478443 0.289238 0.043 Uiso calc 1 . . C C27 -0.03319(15) 0.5880(2) 0.32799(11) 0.0304(7) Uani d 1 . . H H27 -0.055402 0.655411 0.314519 0.037 Uiso calc 1 . . C C28 0.09238(16) 0.7265(3) 0.43650(10) 0.0316(7) Uani d 1 . . C C29 0.14978(18) 0.7970(3) 0.45322(11) 0.0398(8) Uani d 1 . . H H29 0.175407 0.841343 0.428474 0.048 Uiso calc 1 . . C C30 0.1714(2) 0.8056(3) 0.50445(12) 0.0496(9) Uani d 1 . . H H30 0.210939 0.854754 0.513967 0.060 Uiso calc 1 . . C C31 0.1354(2) 0.7431(3) 0.54106(12) 0.0546(10) Uani d 1 . . H H31 0.150092 0.747998 0.576031 0.065 Uiso calc 1 . . C C32 0.0779(2) 0.6732(3) 0.52669(12) 0.0555(10) Uani d 1 . . H H32 0.052427 0.629733 0.551826 0.067 Uiso calc 1 . . C C33 0.05695(18) 0.6660(3) 0.47559(11) 0.0441(9) Uani d 1 . . H H33 0.016674 0.617682 0.466679 0.053 Uiso calc 1 . . C C34 0.13362(14) 0.7270(2) 0.33569(10) 0.0247(6) Uani d 1 . . C C35 0.12318(15) 0.7591(2) 0.28431(10) 0.0295(7) Uani d 1 . . H H35 0.075907 0.785862 0.273925 0.035 Uiso calc 1 . . C C36 0.17851(16) 0.7535(2) 0.24803(11) 0.0349(8) Uani d 1 . . H H36 0.168751 0.776946 0.213751 0.042 Uiso calc 1 . . C C37 0.24763(16) 0.7143(3) 0.26137(12) 0.0363(8) Uani d 1 . . H H37 0.285910 0.711189 0.236663 0.044 Uiso calc 1 . . C C38 0.26038(16) 0.6794(2) 0.31121(12) 0.0352(8) Uani d 1 . . H H38 0.307613 0.651257 0.320943 0.042 Uiso calc 1 . . C C39 0.20450(15) 0.6854(2) 0.34707(11) 0.0306(7) Uani d 1 . . H H39 0.214621 0.660199 0.381041 0.037 Uiso calc 1 . . C C40 0.51258(14) 0.7520(2) 0.31920(10) 0.0215(6) Uani d 1 . . C C41 0.49323(14) 0.6505(2) 0.29379(10) 0.0256(6) Uani d 1 . . H H41 0.507706 0.579698 0.308791 0.031 Uiso calc 1 . . C C42 0.45418(14) 0.6477(2) 0.24806(10) 0.0261(7) Uani d 1 . . H H42 0.442318 0.576246 0.232589 0.031 Uiso calc 1 . . C C43 0.43240(14) 0.7490(2) 0.22484(10) 0.0249(7) Uani d 1 . . H H43 0.407080 0.748123 0.192831 0.030 Uiso calc 1 . . C C44 0.44819(14) 0.8509(2) 0.24909(10) 0.0254(6) Uani d 1 . . H H44 0.432404 0.921059 0.234134 0.031 Uiso calc 1 . . C C45 0.48688(14) 0.8523(2) 0.29510(10) 0.0254(6) Uani d 1 . . H H45 0.496444 0.923995 0.311034 0.030 Uiso calc 1 . . C C46 0.49871(15) 0.7112(2) 0.41940(10) 0.0246(6) Uani d 1 . . C C47 0.52292(17) 0.6700(2) 0.46687(10) 0.0315(7) Uani d 1 . . H H47 0.574506 0.662922 0.472701 0.038 Uiso calc 1 . . C C48 0.47564(19) 0.6390(3) 0.50568(11) 0.0388(8) Uani d 1 . . H H48 0.494909 0.610553 0.537172 0.047 Uiso calc 1 . . C C49 0.40053(19) 0.6491(3) 0.49892(11) 0.0414(8) Uani d 1 . . H H49 0.367657 0.628399 0.525620 0.050 Uiso calc 1 . . C C50 0.37390(18) 0.6897(3) 0.45288(12) 0.0411(8) Uani d 1 . . H H50 0.322223 0.697581 0.447692 0.049 Uiso calc 1 . . C C51 0.42219(16) 0.7190(2) 0.41404(11) 0.0322(7) Uani d 1 . . H H51 0.402379 0.745589 0.382387 0.039 Uiso calc 1 . . C C52 0.62601(15) 0.6606(2) 0.37250(9) 0.0251(6) Uani d 1 . . C C53 0.70063(16) 0.6897(3) 0.36737(11) 0.0357(8) Uani d 1 . . H H53 0.713522 0.768607 0.367493 0.043 Uiso calc 1 . . C C54 0.75655(18) 0.6100(3) 0.36213(12) 0.0446(9) Uani d 1 . . H H54 0.806155 0.635014 0.358631 0.054 Uiso calc 1 . . C C55 0.74065(19) 0.4944(3) 0.36195(11) 0.0447(9) Uani d 1 . . H H55 0.778641 0.439427 0.357178 0.054 Uiso calc 1 . . C C56 0.66883(18) 0.4603(3) 0.36880(10) 0.0374(8) Uani d 1 . . H H56 0.656977 0.381066 0.369708 0.045 Uiso calc 1 . . C C57 0.61333(16) 0.5420(2) 0.37443(10) 0.0297(7) Uani d 1 . . H H57 0.564322 0.516009 0.379859 0.036 Uiso calc 1 . . C C58 0.58565(15) 0.8834(2) 0.38696(10) 0.0248(6) Uani d 1 . . C C59 0.63458(16) 0.9399(3) 0.35433(11) 0.0326(7) Uani d 1 . . H H59 0.650183 0.901700 0.324077 0.039 Uiso calc 1 . . C C60 0.66161(17) 1.0498(3) 0.36415(12) 0.0407(8) Uani d 1 . . H H60 0.696074 1.083950 0.341477 0.049 Uiso calc 1 . . C C61 0.63802(18) 1.1086(3) 0.40693(12) 0.0406(8) Uani d 1 . . H H61 0.656582 1.183091 0.414112 0.049 Uiso calc 1 . . C C62 0.58764(17) 1.0590(3) 0.43899(11) 0.0357(8) Uani d 1 . . H H62 0.569907 1.099913 0.467905 0.043 Uiso calc 1 . . C C63 0.56245(15) 0.9482(2) 0.42911(10) 0.0285(7) Uani d 1 . . H H63 0.527914 0.915169 0.452055 0.034 Uiso calc 1 . . B B1 0.06470(17) 0.7221(3) 0.37633(12) 0.0270(7) Uani d 1 . . B B2 0.55686(17) 0.7525(3) 0.37481(12) 0.0241(7) Uani d 1 . . C C3 0.39592(16) 0.1703(3) 0.42524(12) 0.0470(9) Uani d 1 . . H H3A 0.433697 0.120075 0.441105 0.056 Uiso calc 1 . . H H3B 0.386375 0.234537 0.449104 0.056 Uiso calc 1 . . C C4 0.29529(19) 0.0746(3) 0.46769(12) 0.0538(10) Uani d 1 . . H H4A 0.331093 0.029267 0.487397 0.081 Uiso calc 1 . . H H4B 0.250094 0.029752 0.462629 0.081 Uiso calc 1 . . H H4C 0.283707 0.144979 0.486477 0.081 Uiso calc 1 . . C C5 0.3405(2) -0.0026(3) 0.38691(13) 0.0509(9) Uani d 1 . . H H5A 0.337486 -0.069866 0.409939 0.061 Uiso calc 1 . . H H5B 0.390920 0.000031 0.372569 0.061 Uiso calc 1 . . C C6 0.2858(2) -0.0163(3) 0.34395(13) 0.0464(9) Uani d 1 . . H H6A 0.302433 -0.078417 0.320865 0.056 Uiso calc 1 . . H H6B 0.237452 -0.039030 0.358283 0.056 Uiso calc 1 . . C C7 0.21341(17) 0.0771(3) 0.27841(12) 0.0462(9) Uani d 1 . . H H7A 0.220658 0.008683 0.257235 0.069 Uiso calc 1 . . H H7B 0.209788 0.144769 0.256266 0.069 Uiso calc 1 . . H H7C 0.167867 0.069012 0.298162 0.069 Uiso calc 1 . . C C8 0.34430(16) 0.1195(2) 0.28411(11) 0.0330(7) Uani d 1 . . H H8A 0.335250 0.103584 0.247305 0.040 Uiso calc 1 . . H H8B 0.385719 0.070483 0.295726 0.040 Uiso calc 1 . . C C9 0.36514(16) 0.2438(2) 0.29074(11) 0.0325(7) Uani d 1 . . H H9A 0.414619 0.256903 0.275954 0.039 Uiso calc 1 . . H H9B 0.329423 0.292381 0.271835 0.039 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Co1 0.0208(2) 0.0226(2) 0.02047(19) 0.00069(17) 0.00212(14) 0.00164(17) N1 0.0234(13) 0.0275(13) 0.0360(14) -0.0043(11) 0.0051(10) -0.0021(12) N2 0.0324(15) 0.0413(16) 0.0355(15) 0.0051(13) -0.0033(12) 0.0076(12) N3 0.0344(14) 0.0260(14) 0.0288(13) -0.0031(11) 0.0036(11) -0.0040(11) N4 0.0403(16) 0.0392(16) 0.0326(15) -0.0025(13) 0.0073(12) -0.0078(13) N5 0.0313(15) 0.0370(15) 0.0291(14) 0.0077(12) 0.0089(12) 0.0084(12) N6 0.0264(14) 0.0390(15) 0.0253(13) -0.0038(12) 0.0029(11) 0.0062(11) C1 0.048(2) 0.035(2) 0.067(2) -0.0204(17) 0.0163(18) -0.0089(18) C10 0.041(2) 0.040(2) 0.0316(18) -0.0055(16) 0.0042(15) -0.0051(16) C2 0.0219(17) 0.057(2) 0.054(2) -0.0013(17) -0.0046(15) -0.0076(18) C11 0.090(3) 0.062(3) 0.047(2) -0.006(2) 0.015(2) -0.029(2) C12 0.0309(17) 0.0326(18) 0.0243(16) 0.0035(14) 0.0084(13) 0.0040(14) C13 0.046(2) 0.0399(19) 0.0263(16) 0.0097(16) 0.0008(14) 0.0089(14) C14 0.0300(17) 0.0325(18) 0.0250(16) -0.0011(14) -0.0016(14) 0.0003(13) C15 0.0392(19) 0.052(2) 0.0308(17) -0.0112(16) 0.0117(14) 0.0035(15) C16 0.0325(18) 0.0333(18) 0.0234(15) 0.0018(14) -0.0018(13) -0.0101(13) C17 0.040(2) 0.044(2) 0.0358(18) 0.0070(16) 0.0046(15) -0.0113(15) C18 0.041(2) 0.072(3) 0.041(2) 0.022(2) -0.0032(16) -0.027(2) C19 0.067(3) 0.051(3) 0.046(2) 0.032(2) -0.021(2) -0.0253(19) C20 0.064(3) 0.032(2) 0.051(2) 0.0128(18) -0.0193(19) -0.0105(16) C21 0.0397(19) 0.0313(18) 0.0395(18) 0.0042(15) -0.0068(15) -0.0086(15) C22 0.0194(15) 0.0308(17) 0.0224(15) 0.0029(13) 0.0078(12) -0.0011(12) C23 0.0239(16) 0.0351(18) 0.0252(16) 0.0017(14) 0.0057(12) 0.0031(13) C24 0.0321(18) 0.0283(17) 0.0319(17) 0.0028(14) 0.0092(14) 0.0058(13) C25 0.0341(18) 0.0279(18) 0.0412(19) -0.0011(15) 0.0068(15) -0.0024(14) C26 0.0284(17) 0.0366(19) 0.0419(19) 0.0006(15) -0.0067(14) -0.0037(15) C27 0.0301(17) 0.0269(17) 0.0343(17) 0.0037(14) 0.0023(14) 0.0014(13) C28 0.0349(17) 0.0292(17) 0.0308(16) 0.0085(15) 0.0023(13) -0.0058(14) C29 0.058(2) 0.0297(18) 0.0313(17) 0.0019(16) -0.0079(15) 0.0000(14) C30 0.075(3) 0.034(2) 0.040(2) 0.0057(18) -0.0187(18) -0.0065(16) C31 0.095(3) 0.046(2) 0.0229(18) 0.019(2) -0.0065(19) -0.0120(16) C32 0.076(3) 0.063(3) 0.0279(19) 0.008(2) 0.0200(18) -0.0055(18) C33 0.048(2) 0.055(2) 0.0297(18) 0.0012(17) 0.0155(15) -0.0088(16) C34 0.0256(16) 0.0184(15) 0.0300(16) -0.0022(13) -0.0003(12) -0.0018(13) C35 0.0261(16) 0.0299(17) 0.0323(17) 0.0019(13) 0.0021(13) -0.0006(13) C36 0.0357(18) 0.0365(19) 0.0325(17) -0.0021(15) 0.0076(14) 0.0009(14) C37 0.0286(17) 0.0332(18) 0.047(2) -0.0058(15) 0.0144(14) -0.0107(16) C38 0.0247(17) 0.0278(17) 0.053(2) 0.0010(13) 0.0007(15) -0.0091(15) C39 0.0317(18) 0.0242(16) 0.0357(17) -0.0007(13) -0.0017(14) -0.0003(13) C40 0.0209(14) 0.0212(15) 0.0225(14) -0.0007(12) 0.0078(11) 0.0009(11) C41 0.0280(16) 0.0218(16) 0.0271(16) -0.0002(13) 0.0044(13) 0.0027(12) C42 0.0258(16) 0.0269(17) 0.0258(16) -0.0032(13) 0.0039(12) -0.0047(13) C43 0.0217(15) 0.0335(18) 0.0195(14) 0.0004(13) 0.0029(11) -0.0011(12) C44 0.0262(16) 0.0237(16) 0.0264(16) 0.0053(13) 0.0036(12) 0.0023(13) C45 0.0270(16) 0.0233(16) 0.0260(16) 0.0018(13) 0.0043(13) -0.0020(12) C46 0.0354(17) 0.0149(14) 0.0237(15) 0.0004(13) 0.0055(12) -0.0033(12) C47 0.0427(19) 0.0285(17) 0.0233(16) -0.0008(14) 0.0029(14) -0.0019(13) C48 0.064(2) 0.0301(18) 0.0222(16) -0.0004(17) 0.0052(15) 0.0007(13) C49 0.061(2) 0.0352(19) 0.0285(18) -0.0084(17) 0.0210(16) -0.0005(14) C50 0.0385(19) 0.046(2) 0.0393(19) -0.0042(16) 0.0145(15) 0.0001(16) C51 0.0381(18) 0.0297(17) 0.0290(16) 0.0009(15) 0.0058(13) 0.0027(14) C52 0.0346(17) 0.0275(16) 0.0132(13) 0.0027(13) 0.0016(12) 0.0004(12) C53 0.0365(19) 0.0368(19) 0.0337(17) 0.0022(15) 0.0021(14) 0.0013(14) C54 0.0337(19) 0.058(2) 0.042(2) 0.0105(18) 0.0036(15) 0.0015(17) C55 0.047(2) 0.056(2) 0.0312(18) 0.0261(19) -0.0004(16) -0.0026(16) C56 0.058(2) 0.0317(18) 0.0225(16) 0.0131(17) -0.0064(15) 0.0002(13) C57 0.0377(18) 0.0314(18) 0.0199(15) 0.0023(15) -0.0011(13) 0.0019(13) C58 0.0280(16) 0.0249(16) 0.0215(15) 0.0012(13) -0.0052(12) 0.0041(12) C59 0.0366(18) 0.0323(18) 0.0287(16) -0.0026(15) -0.0041(14) 0.0061(14) C60 0.041(2) 0.037(2) 0.044(2) -0.0097(16) -0.0089(16) 0.0191(16) C61 0.052(2) 0.0230(17) 0.047(2) -0.0048(16) -0.0231(17) 0.0055(15) C62 0.047(2) 0.0253(17) 0.0344(18) 0.0056(15) -0.0154(15) -0.0024(14) C63 0.0336(17) 0.0247(16) 0.0273(16) 0.0010(14) -0.0069(13) 0.0038(13) B1 0.0265(18) 0.0271(18) 0.0274(17) 0.0029(16) 0.0015(14) -0.0014(15) B2 0.0295(18) 0.0183(17) 0.0244(17) -0.0005(14) 0.0027(14) 0.0007(13) C3 0.0270(18) 0.072(3) 0.042(2) 0.0050(17) -0.0111(15) 0.0013(18) C4 0.050(2) 0.073(3) 0.038(2) 0.010(2) -0.0079(16) 0.0277(19) C5 0.058(2) 0.033(2) 0.061(2) 0.0158(17) 0.0042(19) 0.0135(17) C6 0.066(2) 0.0246(18) 0.048(2) -0.0005(17) 0.0122(18) -0.0017(15) C7 0.046(2) 0.059(2) 0.0336(18) -0.0164(18) -0.0016(16) -0.0149(17) C8 0.0333(17) 0.0351(18) 0.0305(17) 0.0034(14) 0.0088(13) -0.0077(14) C9 0.0264(16) 0.0389(19) 0.0325(17) -0.0005(14) 0.0150(13) 0.0017(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N5 Co1 N4 . . 89.38(10) ? N4 Co1 N2 . . 93.69(10) ? N5 Co1 N3 . . 93.66(9) ? N5 Co1 N1 . . 92.93(9) ? N4 Co1 N1 . . 95.53(9) ? N1 Co1 N2 . . 83.16(9) y N1 Co1 N3 . . 82.86(9) y N2 Co1 N3 . . 83.18(9) y N1 Co1 N6 . . 175.58(9) y N2 Co1 N5 . . 175.23(9) y N3 Co1 N4 . . 176.62(10) y N5 Co1 N6 . . 91.39(9) ? N4 Co1 N6 . . 85.44(9) ? N2 Co1 N6 . . 92.49(9) ? N3 Co1 N6 . . 95.94(9) ? C1 N1 C9 . . 109.2(2) ? C1 N1 C2 . . 110.1(2) ? C9 N1 C2 . . 112.1(2) ? C1 N1 Co1 . . 114.07(18) ? C9 N1 Co1 . . 102.65(16) ? C2 N1 Co1 . . 108.68(17) ? C4 N2 C3 . . 109.2(2) ? C4 N2 C5 . . 110.0(3) ? C3 N2 C5 . . 111.4(2) ? C4 N2 Co1 . . 114.68(19) ? C3 N2 Co1 . . 102.92(18) ? C5 N2 Co1 . . 108.51(18) ? C6 N3 C7 . . 108.9(2) ? C6 N3 C8 . . 112.2(2) ? C7 N3 C8 . . 109.4(2) ? C6 N3 Co1 . . 103.20(17) ? C7 N3 Co1 . . 114.11(18) ? C8 N3 Co1 . . 109.00(16) ? C10 N4 Co1 . . 173.5(3) ? C12 N5 Co1 . . 176.8(2) ? C14 N6 Co1 . . 163.7(2) ? N1 C1 H1A . . 109.5 ? N1 C1 H1B . . 109.5 ? H1A C1 H1B . . 109.5 ? N1 C1 H1C . . 109.5 ? H1A C1 H1C . . 109.5 ? H1B C1 H1C . . 109.5 ? N4 C10 C11 . . 179.4(4) ? N1 C2 C3 . . 111.3(2) ? N1 C2 H2A . . 109.4 ? C3 C2 H2A . . 109.4 ? N1 C2 H2B . . 109.4 ? C3 C2 H2B . . 109.4 ? H2A C2 H2B . . 108.0 ? C10 C11 H11A . . 109.5 ? C10 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C10 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? N5 C12 C13 . . 178.3(3) ? C12 C13 H13A . . 109.5 ? C12 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? C12 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? N6 C14 C15 . . 178.0(3) ? C14 C15 H15A . . 109.5 ? C14 C15 H15B . . 109.5 ? H15A C15 H15B . . 109.5 ? C14 C15 H15C . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? C21 C16 C17 . . 114.8(3) ? C21 C16 B1 . . 124.4(3) ? C17 C16 B1 . . 120.6(3) ? C18 C17 C16 . . 122.5(3) ? C18 C17 H17 . . 118.8 ? C16 C17 H17 . . 118.8 ? C19 C18 C17 . . 120.2(3) ? C19 C18 H18 . . 119.9 ? C17 C18 H18 . . 119.9 ? C20 C19 C18 . . 119.2(3) ? C20 C19 H19 . . 120.4 ? C18 C19 H19 . . 120.4 ? C19 C20 C21 . . 120.2(3) ? C19 C20 H20 . . 119.9 ? C21 C20 H20 . . 119.9 ? C20 C21 C16 . . 123.1(3) ? C20 C21 H21 . . 118.4 ? C16 C21 H21 . . 118.4 ? C27 C22 C23 . . 114.9(3) ? C27 C22 B1 . . 123.4(3) ? C23 C22 B1 . . 121.3(2) ? C24 C23 C22 . . 123.1(3) ? C24 C23 H23 . . 118.4 ? C22 C23 H23 . . 118.4 ? C25 C24 C23 . . 119.9(3) ? C25 C24 H24 . . 120.0 ? C23 C24 H24 . . 120.0 ? C26 C25 C24 . . 119.0(3) ? C26 C25 H25 . . 120.5 ? C24 C25 H25 . . 120.5 ? C25 C26 C27 . . 120.6(3) ? C25 C26 H26 . . 119.7 ? C27 C26 H26 . . 119.7 ? C26 C27 C22 . . 122.5(3) ? C26 C27 H27 . . 118.7 ? C22 C27 H27 . . 118.7 ? C29 C28 C33 . . 114.5(3) ? C29 C28 B1 . . 122.6(3) ? C33 C28 B1 . . 122.7(3) ? C30 C29 C28 . . 123.2(3) ? C30 C29 H29 . . 118.4 ? C28 C29 H29 . . 118.4 ? C31 C30 C29 . . 119.8(3) ? C31 C30 H30 . . 120.1 ? C29 C30 H30 . . 120.1 ? C30 C31 C32 . . 119.3(3) ? C30 C31 H31 . . 120.3 ? C32 C31 H31 . . 120.3 ? C31 C32 C33 . . 120.1(3) ? C31 C32 H32 . . 120.0 ? C33 C32 H32 . . 120.0 ? C32 C33 C28 . . 123.1(3) ? C32 C33 H33 . . 118.5 ? C28 C33 H33 . . 118.5 ? C35 C34 C39 . . 114.4(2) ? C35 C34 B1 . . 121.7(2) ? C39 C34 B1 . . 123.4(2) ? C36 C35 C34 . . 123.1(3) ? C36 C35 H35 . . 118.5 ? C34 C35 H35 . . 118.5 ? C37 C36 C35 . . 120.3(3) ? C37 C36 H36 . . 119.8 ? C35 C36 H36 . . 119.8 ? C36 C37 C38 . . 118.9(3) ? C36 C37 H37 . . 120.6 ? C38 C37 H37 . . 120.6 ? C37 C38 C39 . . 120.1(3) ? C37 C38 H38 . . 119.9 ? C39 C38 H38 . . 119.9 ? C38 C39 C34 . . 123.2(3) ? C38 C39 H39 . . 118.4 ? C34 C39 H39 . . 118.4 ? C41 C40 C45 . . 114.3(2) ? C41 C40 B2 . . 122.4(2) ? C45 C40 B2 . . 123.2(2) ? C42 C41 C40 . . 123.6(3) ? C42 C41 H41 . . 118.2 ? C40 C41 H41 . . 118.2 ? C41 C42 C43 . . 120.0(3) ? C41 C42 H42 . . 120.0 ? C43 C42 H42 . . 120.0 ? C44 C43 C42 . . 118.6(3) ? C44 C43 H43 . . 120.7 ? C42 C43 H43 . . 120.7 ? C43 C44 C45 . . 120.7(3) ? C43 C44 H44 . . 119.7 ? C45 C44 H44 . . 119.7 ? C44 C45 C40 . . 122.8(3) ? C44 C45 H45 . . 118.6 ? C40 C45 H45 . . 118.6 ? C51 C46 C47 . . 114.7(2) ? C51 C46 B2 . . 123.4(2) ? C47 C46 B2 . . 121.8(2) ? C48 C47 C46 . . 123.2(3) ? C48 C47 H47 . . 118.4 ? C46 C47 H47 . . 118.4 ? C49 C48 C47 . . 120.1(3) ? C49 C48 H48 . . 119.9 ? C47 C48 H48 . . 119.9 ? C50 C49 C48 . . 118.9(3) ? C50 C49 H49 . . 120.6 ? C48 C49 H49 . . 120.6 ? C49 C50 C51 . . 120.2(3) ? C49 C50 H50 . . 119.9 ? C51 C50 H50 . . 119.9 ? C50 C51 C46 . . 122.8(3) ? C50 C51 H51 . . 118.6 ? C46 C51 H51 . . 118.6 ? C53 C52 C57 . . 113.6(3) ? C53 C52 B2 . . 125.4(3) ? C57 C52 B2 . . 121.0(2) ? C54 C53 C52 . . 123.7(3) ? C54 C53 H53 . . 118.1 ? C52 C53 H53 . . 118.1 ? C55 C54 C53 . . 120.3(3) ? C55 C54 H54 . . 119.8 ? C53 C54 H54 . . 119.8 ? C56 C55 C54 . . 118.7(3) ? C56 C55 H55 . . 120.6 ? C54 C55 H55 . . 120.6 ? C55 C56 C57 . . 120.0(3) ? C55 C56 H56 . . 120.0 ? C57 C56 H56 . . 120.0 ? C56 C57 C52 . . 123.5(3) ? C56 C57 H57 . . 118.3 ? C52 C57 H57 . . 118.3 ? C59 C58 C63 . . 114.7(3) ? C59 C58 B2 . . 121.5(2) ? C63 C58 B2 . . 123.8(2) ? C60 C59 C58 . . 123.0(3) ? C60 C59 H59 . . 118.5 ? C58 C59 H59 . . 118.5 ? C61 C60 C59 . . 119.7(3) ? C61 C60 H60 . . 120.2 ? C59 C60 H60 . . 120.2 ? C62 C61 C60 . . 119.6(3) ? C62 C61 H61 . . 120.2 ? C60 C61 H61 . . 120.2 ? C61 C62 C63 . . 119.9(3) ? C61 C62 H62 . . 120.1 ? C63 C62 H62 . . 120.1 ? C62 C63 C58 . . 123.1(3) ? C62 C63 H63 . . 118.5 ? C58 C63 H63 . . 118.5 ? C22 B1 C16 . . 112.3(2) ? C22 B1 C34 . . 102.5(2) ? C16 B1 C34 . . 113.3(2) ? C22 B1 C28 . . 111.5(2) ? C16 B1 C28 . . 104.9(2) ? C34 B1 C28 . . 112.6(2) ? C58 B2 C46 . . 109.9(2) ? C58 B2 C52 . . 111.7(2) ? C46 B2 C52 . . 109.0(2) ? C58 B2 C40 . . 108.9(2) ? C46 B2 C40 . . 108.0(2) ? C52 B2 C40 . . 109.3(2) ? N2 C3 C2 . . 111.5(3) ? N2 C3 H3A . . 109.3 ? C2 C3 H3A . . 109.3 ? N2 C3 H3B . . 109.3 ? C2 C3 H3B . . 109.3 ? H3A C3 H3B . . 108.0 ? N2 C4 H4A . . 109.5 ? N2 C4 H4B . . 109.5 ? H4A C4 H4B . . 109.5 ? N2 C4 H4C . . 109.5 ? H4A C4 H4C . . 109.5 ? H4B C4 H4C . . 109.5 ? N2 C5 C6 . . 112.0(3) ? N2 C5 H5A . . 109.2 ? C6 C5 H5A . . 109.2 ? N2 C5 H5B . . 109.2 ? C6 C5 H5B . . 109.2 ? H5A C5 H5B . . 107.9 ? N3 C6 C5 . . 111.9(3) ? N3 C6 H6A . . 109.2 ? C5 C6 H6A . . 109.2 ? N3 C6 H6B . . 109.2 ? C5 C6 H6B . . 109.2 ? H6A C6 H6B . . 107.9 ? N3 C7 H7A . . 109.5 ? N3 C7 H7B . . 109.5 ? H7A C7 H7B . . 109.5 ? N3 C7 H7C . . 109.5 ? H7A C7 H7C . . 109.5 ? H7B C7 H7C . . 109.5 ? N3 C8 C9 . . 111.3(2) ? N3 C8 H8A . . 109.4 ? C9 C8 H8A . . 109.4 ? N3 C8 H8B . . 109.4 ? C9 C8 H8B . . 109.4 ? H8A C8 H8B . . 108.0 ? N1 C9 C8 . . 111.4(2) ? N1 C9 H9A . . 109.3 ? C8 C9 H9A . . 109.3 ? N1 C9 H9B . . 109.3 ? C8 C9 H9B . . 109.3 ? H9A C9 H9B . . 108.0 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Co1 N1 . 2.143(2) y Co1 N2 . 2.139(2) y Co1 N3 . 2.141(2) y Co1 N4 . 2.129(3) y Co1 N5 . 2.094(3) y Co1 N6 . 2.153(2) y N1 C1 . 1.475(4) ? N1 C9 . 1.487(3) ? N1 C2 . 1.490(4) ? N2 C4 . 1.477(4) ? N2 C3 . 1.483(4) ? N2 C5 . 1.498(4) ? N3 C6 . 1.479(4) ? N3 C7 . 1.480(4) ? N3 C8 . 1.494(3) ? N4 C10 . 1.129(4) ? N5 C12 . 1.138(3) ? N6 C14 . 1.135(3) ? C1 H1A . 0.9800 ? C1 H1B . 0.9800 ? C1 H1C . 0.9800 ? C10 C11 . 1.454(4) ? C2 C3 . 1.511(4) ? C2 H2A . 0.9900 ? C2 H2B . 0.9900 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 C13 . 1.447(4) ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? C14 C15 . 1.455(4) ? C15 H15A . 0.9800 ? C15 H15B . 0.9800 ? C15 H15C . 0.9800 ? C16 C21 . 1.397(4) ? C16 C17 . 1.403(4) ? C16 B1 . 1.642(4) ? C17 C18 . 1.395(4) ? C17 H17 . 0.9500 ? C18 C19 . 1.379(5) ? C18 H18 . 0.9500 ? C19 C20 . 1.368(5) ? C19 H19 . 0.9500 ? C20 C21 . 1.392(4) ? C20 H20 . 0.9500 ? C21 H21 . 0.9500 ? C22 C27 . 1.398(4) ? C22 C23 . 1.399(4) ? C22 B1 . 1.638(4) ? C23 C24 . 1.387(4) ? C23 H23 . 0.9500 ? C24 C25 . 1.376(4) ? C24 H24 . 0.9500 ? C25 C26 . 1.374(4) ? C25 H25 . 0.9500 ? C26 C27 . 1.389(4) ? C26 H26 . 0.9500 ? C27 H27 . 0.9500 ? C28 C29 . 1.394(4) ? C28 C33 . 1.399(4) ? C28 B1 . 1.645(4) ? C29 C30 . 1.393(4) ? C29 H29 . 0.9500 ? C30 C31 . 1.369(5) ? C30 H30 . 0.9500 ? C31 C32 . 1.374(5) ? C31 H31 . 0.9500 ? C32 C33 . 1.385(4) ? C32 H32 . 0.9500 ? C33 H33 . 0.9500 ? C34 C35 . 1.403(4) ? C34 C39 . 1.403(4) ? C34 B1 . 1.643(4) ? C35 C36 . 1.384(4) ? C35 H35 . 0.9500 ? C36 C37 . 1.377(4) ? C36 H36 . 0.9500 ? C37 C38 . 1.380(4) ? C37 H37 . 0.9500 ? C38 C39 . 1.384(4) ? C38 H38 . 0.9500 ? C39 H39 . 0.9500 ? C40 C41 . 1.401(4) ? C40 C45 . 1.406(4) ? C40 B2 . 1.653(4) ? C41 C42 . 1.383(4) ? C41 H41 . 0.9500 ? C42 C43 . 1.384(4) ? C42 H42 . 0.9500 ? C43 C44 . 1.376(4) ? C43 H43 . 0.9500 ? C44 C45 . 1.386(4) ? C44 H44 . 0.9500 ? C45 H45 . 0.9500 ? C46 C51 . 1.396(4) ? C46 C47 . 1.396(4) ? C46 B2 . 1.645(4) ? C47 C48 . 1.378(4) ? C47 H47 . 0.9500 ? C48 C49 . 1.377(4) ? C48 H48 . 0.9500 ? C49 C50 . 1.375(4) ? C49 H49 . 0.9500 ? C50 C51 . 1.385(4) ? C50 H50 . 0.9500 ? C51 H51 . 0.9500 ? C52 C53 . 1.402(4) ? C52 C57 . 1.404(4) ? C52 B2 . 1.651(4) ? C53 C54 . 1.383(4) ? C53 H53 . 0.9500 ? C54 C55 . 1.379(5) ? C54 H54 . 0.9500 ? C55 C56 . 1.374(4) ? C55 H55 . 0.9500 ? C56 C57 . 1.394(4) ? C56 H56 . 0.9500 ? C57 H57 . 0.9500 ? C58 C59 . 1.398(4) ? C58 C63 . 1.401(4) ? C58 B2 . 1.644(4) ? C59 C60 . 1.396(4) ? C59 H59 . 0.9500 ? C60 C61 . 1.379(4) ? C60 H60 . 0.9500 ? C61 C62 . 1.370(4) ? C61 H61 . 0.9500 ? C62 C63 . 1.394(4) ? C62 H62 . 0.9500 ? C63 H63 . 0.9500 ? C3 H3A . 0.9900 ? C3 H3B . 0.9900 ? C4 H4A . 0.9800 ? C4 H4B . 0.9800 ? C4 H4C . 0.9800 ? C5 C6 . 1.500(5) ? C5 H5A . 0.9900 ? C5 H5B . 0.9900 ? C6 H6A . 0.9900 ? C6 H6B . 0.9900 ? C7 H7A . 0.9800 ? C7 H7B . 0.9800 ? C7 H7C . 0.9800 ? C8 C9 . 1.508(4) ? C8 H8A . 0.9900 ? C8 H8B . 0.9900 ? C9 H9A . 0.9900 ? C9 H9B . 0.9900 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C1 N1 C2 C3 . . . . 104.4(3) ? C9 N1 C2 C3 . . . . -133.9(3) ? Co1 N1 C2 C3 . . . . -21.2(3) ? C21 C16 C17 C18 . . . . -0.5(4) ? B1 C16 C17 C18 . . . . 175.4(3) ? C16 C17 C18 C19 . . . . 0.8(5) ? C17 C18 C19 C20 . . . . -0.4(5) ? C18 C19 C20 C21 . . . . -0.1(5) ? C19 C20 C21 C16 . . . . 0.4(5) ? C17 C16 C21 C20 . . . . -0.1(4) ? B1 C16 C21 C20 . . . . -175.8(3) ? C27 C22 C23 C24 . . . . -0.7(4) ? B1 C22 C23 C24 . . . . -173.5(2) ? C22 C23 C24 C25 . . . . 0.3(4) ? C23 C24 C25 C26 . . . . 0.3(4) ? C24 C25 C26 C27 . . . . -0.4(4) ? C25 C26 C27 C22 . . . . -0.1(4) ? C23 C22 C27 C26 . . . . 0.6(4) ? B1 C22 C27 C26 . . . . 173.2(3) ? C33 C28 C29 C30 . . . . 1.1(5) ? B1 C28 C29 C30 . . . . 176.8(3) ? C28 C29 C30 C31 . . . . -0.2(5) ? C29 C30 C31 C32 . . . . -0.5(5) ? C30 C31 C32 C33 . . . . 0.3(5) ? C31 C32 C33 C28 . . . . 0.7(5) ? C29 C28 C33 C32 . . . . -1.3(5) ? B1 C28 C33 C32 . . . . -177.1(3) ? C39 C34 C35 C36 . . . . -1.8(4) ? B1 C34 C35 C36 . . . . -173.6(3) ? C34 C35 C36 C37 . . . . 0.6(4) ? C35 C36 C37 C38 . . . . 0.7(4) ? C36 C37 C38 C39 . . . . -0.7(4) ? C37 C38 C39 C34 . . . . -0.6(4) ? C35 C34 C39 C38 . . . . 1.8(4) ? B1 C34 C39 C38 . . . . 173.5(3) ? C45 C40 C41 C42 . . . . 1.9(4) ? B2 C40 C41 C42 . . . . 177.9(2) ? C40 C41 C42 C43 . . . . 0.3(4) ? C41 C42 C43 C44 . . . . -2.2(4) ? C42 C43 C44 C45 . . . . 1.8(4) ? C43 C44 C45 C40 . . . . 0.6(4) ? C41 C40 C45 C44 . . . . -2.4(4) ? B2 C40 C45 C44 . . . . -178.4(2) ? C51 C46 C47 C48 . . . . 0.1(4) ? B2 C46 C47 C48 . . . . 177.4(3) ? C46 C47 C48 C49 . . . . -0.7(5) ? C47 C48 C49 C50 . . . . 0.5(5) ? C48 C49 C50 C51 . . . . 0.4(5) ? C49 C50 C51 C46 . . . . -1.1(5) ? C47 C46 C51 C50 . . . . 0.8(4) ? B2 C46 C51 C50 . . . . -176.5(3) ? C57 C52 C53 C54 . . . . 3.0(4) ? B2 C52 C53 C54 . . . . -175.5(3) ? C52 C53 C54 C55 . . . . -0.3(5) ? C53 C54 C55 C56 . . . . -2.2(5) ? C54 C55 C56 C57 . . . . 1.7(4) ? C55 C56 C57 C52 . . . . 1.3(4) ? C53 C52 C57 C56 . . . . -3.5(4) ? B2 C52 C57 C56 . . . . 175.0(2) ? C63 C58 C59 C60 . . . . 3.3(4) ? B2 C58 C59 C60 . . . . -178.3(3) ? C58 C59 C60 C61 . . . . -2.1(5) ? C59 C60 C61 C62 . . . . -0.8(5) ? C60 C61 C62 C63 . . . . 2.1(4) ? C61 C62 C63 C58 . . . . -0.7(4) ? C59 C58 C63 C62 . . . . -2.0(4) ? B2 C58 C63 C62 . . . . 179.7(3) ? C27 C22 B1 C16 . . . . 28.2(3) ? C23 C22 B1 C16 . . . . -159.6(2) ? C27 C22 B1 C34 . . . . -93.6(3) ? C23 C22 B1 C34 . . . . 78.6(3) ? C27 C22 B1 C28 . . . . 145.7(2) ? C23 C22 B1 C28 . . . . -42.2(3) ? C21 C16 B1 C22 . . . . -137.0(3) ? C17 C16 B1 C22 . . . . 47.6(3) ? C21 C16 B1 C34 . . . . -21.5(4) ? C17 C16 B1 C34 . . . . 163.0(3) ? C21 C16 B1 C28 . . . . 101.7(3) ? C17 C16 B1 C28 . . . . -73.7(3) ? C35 C34 B1 C22 . . . . 79.8(3) ? C39 C34 B1 C22 . . . . -91.3(3) ? C35 C34 B1 C16 . . . . -41.3(4) ? C39 C34 B1 C16 . . . . 147.6(3) ? C35 C34 B1 C28 . . . . -160.2(3) ? C39 C34 B1 C28 . . . . 28.7(4) ? C29 C28 B1 C22 . . . . 154.6(3) ? C33 C28 B1 C22 . . . . -30.0(4) ? C29 C28 B1 C16 . . . . -83.6(3) ? C33 C28 B1 C16 . . . . 91.8(3) ? C29 C28 B1 C34 . . . . 40.0(4) ? C33 C28 B1 C34 . . . . -144.6(3) ? C59 C58 B2 C46 . . . . -178.8(2) ? C63 C58 B2 C46 . . . . -0.6(4) ? C59 C58 B2 C52 . . . . 60.2(3) ? C63 C58 B2 C52 . . . . -121.6(3) ? C59 C58 B2 C40 . . . . -60.7(3) ? C63 C58 B2 C40 . . . . 117.5(3) ? C51 C46 B2 C58 . . . . 96.3(3) ? C47 C46 B2 C58 . . . . -80.8(3) ? C51 C46 B2 C52 . . . . -141.0(3) ? C47 C46 B2 C52 . . . . 41.9(3) ? C51 C46 B2 C40 . . . . -22.4(3) ? C47 C46 B2 C40 . . . . 160.5(2) ? C53 C52 B2 C58 . . . . -16.4(4) ? C57 C52 B2 C58 . . . . 165.2(2) ? C53 C52 B2 C46 . . . . -137.9(3) ? C57 C52 B2 C46 . . . . 43.6(3) ? C53 C52 B2 C40 . . . . 104.2(3) ? C57 C52 B2 C40 . . . . -74.2(3) ? C41 C40 B2 C58 . . . . 168.1(2) ? C45 C40 B2 C58 . . . . -16.3(3) ? C41 C40 B2 C46 . . . . -72.7(3) ? C45 C40 B2 C46 . . . . 102.9(3) ? C41 C40 B2 C52 . . . . 45.7(3) ? C45 C40 B2 C52 . . . . -138.6(2) ? C4 N2 C3 C2 . . . . -172.0(3) ? C5 N2 C3 C2 . . . . 66.3(3) ? Co1 N2 C3 C2 . . . . -49.8(3) ? N1 C2 C3 N2 . . . . 49.6(4) ? C4 N2 C5 C6 . . . . 106.9(3) ? C3 N2 C5 C6 . . . . -131.9(3) ? Co1 N2 C5 C6 . . . . -19.3(3) ? C7 N3 C6 C5 . . . . -170.4(3) ? C8 N3 C6 C5 . . . . 68.4(3) ? Co1 N3 C6 C5 . . . . -48.8(3) ? N2 C5 C6 N3 . . . . 47.6(4) ? C6 N3 C8 C9 . . . . -132.8(3) ? C7 N3 C8 C9 . . . . 106.2(3) ? Co1 N3 C8 C9 . . . . -19.1(3) ? C1 N1 C9 C8 . . . . -171.9(2) ? C2 N1 C9 C8 . . . . 65.9(3) ? Co1 N1 C9 C8 . . . . -50.6(2) ? N3 C8 C9 N1 . . . . 48.6(3) ?