#------------------------------------------------------------------------------ #$Date: 2024-06-13 01:13:08 +0300 (Thu, 13 Jun 2024) $ #$Revision: 292319 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/18/1571809.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571809 loop_ _publ_author_name 'Nu\~nez Bahena, Erick' 'Hosseini, Kimia' 'Curto, Sheila Galv\'an' 'Schafer, Laurel L.' _publ_section_title ; Understanding mechanism driven regioselectivity in zirconium-catalysed hydroaminoalkylation: homoallylic amines from conjugated dienes ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC00636D _journal_year 2024 _chemical_formula_moiety 'C42 H59 N5 O2 Zr' _chemical_formula_sum 'C42 H59 N5 O2 Zr' _chemical_formula_weight 757.16 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2021-07-13 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6226) ; _audit_update_record ; 2024-05-25 deposited with the CCDC. 2024-05-29 downloaded from the CCDC. ; _cell_angle_alpha 79.490(2) _cell_angle_beta 72.182(2) _cell_angle_gamma 67.933(2) _cell_formula_units_Z 2 _cell_length_a 10.6003(6) _cell_length_b 13.7655(7) _cell_length_c 15.6971(8) _cell_measurement_reflns_used 9783 _cell_measurement_temperature 100 _cell_measurement_theta_max 30.54 _cell_measurement_theta_min 2.18 _cell_volume 2014.97(19) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 100 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0484 _diffrn_reflns_av_unetI/netI 0.0425 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 59696 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.568 _diffrn_reflns_theta_min 1.601 _diffrn_source_current 30.0 _diffrn_source_power 1.35 _diffrn_source_voltage 45.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.313 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.7222 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0512 before and 0.0486 after correction. The Ratio of minimum to maximum transmission is 0.9680. The \l/2 correction factor is Not present. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.248 _exptl_crystal_description prism _exptl_crystal_F_000 804 _exptl_crystal_size_max 0.118 _exptl_crystal_size_mid 0.114 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.472 _refine_diff_density_min -0.355 _refine_diff_density_rms 0.067 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.012 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 469 _refine_ls_number_reflns 12351 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.012 _refine_ls_R_factor_all 0.0449 _refine_ls_R_factor_gt 0.0324 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0303P)^2^+0.7671P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0691 _refine_ls_wR_factor_ref 0.0736 _reflns_Friedel_coverage 0.000 _reflns_number_gt 10307 _reflns_number_total 12351 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc00636d2.cif _cod_data_source_block ls926 _cod_database_code 1571809 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.975 _shelx_estimated_absorpt_t_min 0.964 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C4(H4), C1(H1), C34(H34), C31(H31), C37(H37), C40(H40) 2.b Secondary CH2 refined with riding coordinates: C27(H27A,H27B), C26(H26A,H26B), C2(H2A,H2B) 2.c Aromatic/amide H refined with riding coordinates: C10(H10), C13(H13), C23(H23), C11(H11), C17(H17), C9(H9), C19(H19), C20(H20), C7(H7), C8(H8), C21(H21), C22(H22), C14(H14), C16(H16), C15(H15) 2.d Idealised Me refined as rotating group: C39(H39A,H39B,H39C), C36(H36A,H36B,H36C), C42(H42A,H42B,H42C), C38(H38A,H38B, H38C), C33(H33A,H33B,H33C), C32(H32A,H32B,H32C), C30(H30A,H30B,H30C), C29(H29A, H29B,H29C), C41(H41A,H41B,H41C), C35(H35A,H35B,H35C) ; _shelx_res_file ; TITL ls926_a.res in P-1 ls926.res created by SHELXL-2018/3 at 10:23:34 on 13-Jul-2021 REM Old TITL ls926 in P-1 REM SHELXT solution in P-1: R1 0.074, Rweak 0.007, Alpha 0.018 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C42 N5 O2 Zr CELL 0.71073 10.6003 13.7655 15.6971 79.49 72.182 67.933 ZERR 2 0.0006 0.0007 0.0008 0.002 0.002 0.002 LATT 1 SFAC C H N O Zr UNIT 84 118 10 4 2 L.S. 99 PLAN 20 SIZE 0.08 0.114 0.118 TEMP -173.15 CONF BOND list 4 fmap 2 53 MORE -1 BOND $H ACTA REM REM REM WGHT 0.030300 0.767100 FVAR 0.49459 ZR1 5 0.432444 0.791384 0.716910 11.00000 0.00704 0.00798 = 0.00937 0.00018 -0.00125 -0.00211 O2 4 0.273037 0.950704 0.733980 11.00000 0.00920 0.00952 = 0.01738 0.00062 -0.00138 -0.00305 O1 4 0.640585 0.661121 0.702319 11.00000 0.00884 0.00981 = 0.01521 0.00024 -0.00189 -0.00291 N3 3 0.218258 0.813404 0.802896 11.00000 0.00940 0.00850 = 0.01306 0.00071 -0.00060 -0.00148 N2 3 0.444697 0.631322 0.772709 11.00000 0.00897 0.00915 = 0.01182 0.00029 -0.00111 -0.00225 N1 3 0.431747 0.791833 0.581528 11.00000 0.01168 0.01229 = 0.01058 0.00086 -0.00302 -0.00619 N5 3 0.037565 0.985800 0.797254 11.00000 0.00840 0.00831 = 0.01663 -0.00187 -0.00236 -0.00130 N4 3 0.661049 0.487208 0.723654 11.00000 0.00743 0.00968 = 0.01511 -0.00230 -0.00170 -0.00136 C12 1 0.578668 0.768029 0.423494 11.00000 0.01316 0.01937 = 0.01412 -0.00503 -0.00183 -0.00826 C4 1 0.625238 0.866563 0.689178 11.00000 0.01082 0.01198 = 0.01354 -0.00167 -0.00096 -0.00682 AFIX 13 H4 2 0.724320 0.816094 0.678042 11.00000 -1.20000 AFIX 0 C25 1 0.171032 0.916542 0.779829 11.00000 0.01017 0.01055 = 0.00955 -0.00150 -0.00271 -0.00234 C18 1 0.305845 0.787708 0.571036 11.00000 0.01157 0.01252 = 0.01127 -0.00400 -0.00234 -0.00337 C3 1 0.569043 0.903327 0.616670 11.00000 0.01270 0.01175 = 0.01164 -0.00049 -0.00169 -0.00677 C27 1 0.142331 0.748490 0.863976 11.00000 0.00973 0.01141 = 0.01306 0.00079 -0.00041 -0.00283 AFIX 23 H27A 2 0.095487 0.724145 0.830667 11.00000 -1.20000 H27B 2 0.068272 0.791314 0.911784 11.00000 -1.20000 AFIX 0 C24 1 0.582376 0.589693 0.734304 11.00000 0.01009 0.01032 = 0.00954 0.00018 -0.00376 -0.00202 C1 1 0.515015 0.837287 0.501616 11.00000 0.01382 0.01162 = 0.01016 -0.00102 -0.00298 -0.00472 AFIX 13 H1 2 0.451048 0.906684 0.482086 11.00000 -1.20000 AFIX 0 C34 1 0.597826 0.409120 0.719723 11.00000 0.01183 0.01172 = 0.01764 -0.00347 -0.00221 -0.00322 AFIX 13 H34 2 0.493665 0.446046 0.731160 11.00000 -1.20000 AFIX 0 C31 1 0.817012 0.452341 0.700555 11.00000 0.00723 0.01309 = 0.01997 -0.00261 -0.00262 0.00063 AFIX 13 H31 2 0.850846 0.374210 0.699097 11.00000 -1.20000 AFIX 0 C10 1 0.573602 0.820593 1.018903 11.00000 0.02416 0.02656 = 0.01124 -0.00192 -0.00148 -0.01037 AFIX 43 H10 2 0.518196 0.844931 1.076102 11.00000 -1.20000 AFIX 0 C26 1 0.352448 0.579596 0.835337 11.00000 0.01057 0.01016 = 0.01307 0.00128 -0.00121 -0.00312 AFIX 23 H26A 2 0.409784 0.515967 0.865150 11.00000 -1.20000 H26B 2 0.304021 0.557030 0.801881 11.00000 -1.20000 AFIX 0 C13 1 0.644353 0.660552 0.438096 11.00000 0.01813 0.02099 = 0.02714 -0.00699 -0.00721 -0.00250 AFIX 43 H13 2 0.643291 0.629816 0.497524 11.00000 -1.20000 AFIX 0 C23 1 0.226429 0.860198 0.514845 11.00000 0.01722 0.01549 = 0.01561 0.00002 -0.00679 -0.00518 AFIX 43 H23 2 0.260503 0.912876 0.478405 11.00000 -1.20000 AFIX 0 C5 1 0.546217 0.880321 0.780003 11.00000 0.01088 0.01092 = 0.01272 -0.00162 -0.00237 -0.00286 C11 1 0.525477 0.866077 0.943291 11.00000 0.01373 0.01962 = 0.01302 -0.00286 -0.00054 -0.00647 AFIX 43 H11 2 0.437115 0.921460 0.949656 11.00000 -1.20000 AFIX 0 C17 1 0.579948 0.811175 0.336040 11.00000 0.02906 0.02714 = 0.01422 -0.00311 -0.00293 -0.01903 AFIX 43 H17 2 0.533493 0.884404 0.325389 11.00000 -1.20000 AFIX 0 C9 1 0.702602 0.739510 1.011407 11.00000 0.02776 0.02779 = 0.01443 0.00250 -0.01003 -0.01050 AFIX 43 H9 2 0.735516 0.707779 1.063180 11.00000 -1.20000 AFIX 0 C37 1 -0.087760 0.954687 0.813682 11.00000 0.00910 0.01216 = 0.01683 -0.00042 -0.00236 -0.00320 AFIX 13 H37 2 -0.053781 0.876341 0.814054 11.00000 -1.20000 AFIX 0 C19 1 0.251994 0.709630 0.621184 11.00000 0.01596 0.01558 = 0.01651 0.00117 -0.00612 -0.00661 AFIX 43 H19 2 0.304976 0.657220 0.657510 11.00000 -1.20000 AFIX 0 C40 1 0.014350 1.100258 0.788285 11.00000 0.01083 0.00880 = 0.02385 -0.00237 -0.00353 -0.00056 AFIX 13 H40 2 -0.090066 1.136561 0.806941 11.00000 -1.20000 AFIX 0 C28 1 0.241449 0.652301 0.907134 11.00000 0.01052 0.01180 = 0.01144 0.00086 -0.00037 -0.00282 C39 1 -0.160181 0.999622 0.737739 11.00000 0.01790 0.01910 = 0.02335 -0.00063 -0.00907 -0.00723 AFIX 137 H39A 2 -0.194878 1.076587 0.735416 11.00000 -1.50000 H39B 2 -0.239571 0.974880 0.748439 11.00000 -1.50000 H39C 2 -0.092618 0.976263 0.680575 11.00000 -1.50000 AFIX 0 C36 1 0.622598 0.319462 0.792645 11.00000 0.01988 0.01170 = 0.03271 0.00279 -0.00685 -0.00434 AFIX 137 H36A 2 0.724158 0.283848 0.785217 11.00000 -1.50000 H36B 2 0.580220 0.269181 0.787799 11.00000 -1.50000 H36C 2 0.579330 0.347765 0.851761 11.00000 -1.50000 AFIX 0 C20 1 0.123088 0.707292 0.618882 11.00000 0.01732 0.02120 = 0.02274 -0.00390 -0.00295 -0.01044 AFIX 43 H20 2 0.087813 0.655168 0.655293 11.00000 -1.20000 AFIX 0 C6 1 0.604165 0.832331 0.857236 11.00000 0.01262 0.01371 = 0.01192 -0.00058 -0.00237 -0.00699 C2 1 0.632113 0.856248 0.527598 11.00000 0.01417 0.01558 = 0.01026 -0.00115 -0.00118 -0.00754 AFIX 23 H2A 2 0.710029 0.789034 0.531932 11.00000 -1.20000 H2B 2 0.670298 0.904758 0.481554 11.00000 -1.20000 AFIX 0 C42 1 0.064614 1.144675 0.692359 11.00000 0.02031 0.01499 = 0.02837 0.00595 -0.00876 -0.00519 AFIX 137 H42A 2 0.167891 1.117934 0.673353 11.00000 -1.50000 H42B 2 0.030899 1.221603 0.690327 11.00000 -1.50000 H42C 2 0.027234 1.122927 0.651982 11.00000 -1.50000 AFIX 0 C38 1 -0.189119 0.984252 0.905105 11.00000 0.01316 0.02474 = 0.01904 -0.00347 0.00012 -0.00672 AFIX 137 H38A 2 -0.139203 0.952410 0.952002 11.00000 -1.50000 H38B 2 -0.267479 0.958470 0.915411 11.00000 -1.50000 H38C 2 -0.225884 1.060896 0.906720 11.00000 -1.50000 AFIX 0 C33 1 0.866340 0.472518 0.774967 11.00000 0.01427 0.02644 = 0.02808 -0.00520 -0.01022 -0.00135 AFIX 137 H33A 2 0.836741 0.548439 0.779026 11.00000 -1.50000 H33B 2 0.969367 0.442007 0.761587 11.00000 -1.50000 H33C 2 0.824674 0.440100 0.832204 11.00000 -1.50000 AFIX 0 C7 1 0.735127 0.751378 0.851193 11.00000 0.01518 0.01852 = 0.01234 -0.00269 -0.00273 -0.00506 AFIX 43 H7 2 0.792190 0.727551 0.794122 11.00000 -1.20000 AFIX 0 C32 1 0.886226 0.493842 0.607962 11.00000 0.01287 0.02512 = 0.02400 -0.00253 0.00173 -0.00339 AFIX 137 H32A 2 0.847261 0.482765 0.562873 11.00000 -1.50000 H32B 2 0.988210 0.456231 0.593452 11.00000 -1.50000 H32C 2 0.867581 0.569138 0.608198 11.00000 -1.50000 AFIX 0 C8 1 0.782645 0.705567 0.927187 11.00000 0.01751 0.02076 = 0.02079 0.00009 -0.00873 -0.00460 AFIX 43 H8 2 0.871037 0.650307 0.921459 11.00000 -1.20000 AFIX 0 C30 1 0.311428 0.686043 0.962886 11.00000 0.01926 0.01937 = 0.01404 -0.00233 -0.00338 -0.00488 AFIX 137 H30A 2 0.369508 0.726131 0.923816 11.00000 -1.50000 H30B 2 0.371011 0.623575 0.991214 11.00000 -1.50000 H30C 2 0.238633 0.730058 1.009371 11.00000 -1.50000 AFIX 0 C29 1 0.151838 0.588354 0.968365 11.00000 0.01487 0.01603 = 0.01603 0.00392 0.00000 -0.00397 AFIX 137 H29A 2 0.075720 0.632983 1.013137 11.00000 -1.50000 H29B 2 0.211309 0.528144 0.998834 11.00000 -1.50000 H29C 2 0.111344 0.563156 0.932169 11.00000 -1.50000 AFIX 0 C21 1 0.045409 0.780165 0.564050 11.00000 0.01168 0.02589 = 0.02343 -0.00948 -0.00447 -0.00472 AFIX 43 H21 2 -0.042427 0.778359 0.562210 11.00000 -1.20000 AFIX 0 C41 1 0.073856 1.127611 0.854106 11.00000 0.02230 0.02110 = 0.02899 -0.01199 -0.00324 -0.00678 AFIX 137 H41A 2 0.033047 1.102895 0.915206 11.00000 -1.50000 H41B 2 0.050192 1.203987 0.850569 11.00000 -1.50000 H41C 2 0.176562 1.093528 0.838833 11.00000 -1.50000 AFIX 0 C22 1 0.099071 0.855799 0.511927 11.00000 0.01761 0.02114 = 0.02070 -0.00443 -0.01012 -0.00111 AFIX 43 H22 2 0.047588 0.905614 0.473438 11.00000 -1.20000 AFIX 0 C14 1 0.711841 0.597521 0.366024 11.00000 0.01896 0.02674 = 0.04662 -0.02043 -0.00685 -0.00081 AFIX 43 H14 2 0.756064 0.523930 0.376477 11.00000 -1.20000 AFIX 0 C35 1 0.650947 0.368358 0.626227 11.00000 0.02187 0.02797 = 0.02770 -0.01498 0.00051 -0.00965 AFIX 137 H35A 2 0.632414 0.427843 0.581264 11.00000 -1.50000 H35B 2 0.601868 0.321512 0.623874 11.00000 -1.50000 H35C 2 0.752568 0.329621 0.613686 11.00000 -1.50000 AFIX 0 C16 1 0.648382 0.748457 0.263994 11.00000 0.03288 0.04664 = 0.01619 -0.01100 0.00208 -0.02790 AFIX 43 H16 2 0.649510 0.778924 0.204490 11.00000 -1.20000 AFIX 0 C15 1 0.714601 0.641912 0.279171 11.00000 0.01889 0.05240 = 0.03261 -0.02852 0.00485 -0.01642 AFIX 43 H15 2 0.762108 0.598969 0.230051 11.00000 -1.20000 AFIX 0 H3 2 0.479558 0.959830 0.621709 11.00000 0.01929 H5 2 0.464103 0.941821 0.791255 11.00000 0.01159 HKLF 4 REM ls926_a.res in P-1 REM wR2 = 0.0736, GooF = S = 1.012, Restrained GooF = 1.012 for all data REM R1 = 0.0324 for 10307 Fo > 4sig(Fo) and 0.0449 for all 12351 data REM 469 parameters refined using 0 restraints END WGHT 0.0303 0.7669 REM Highest difference peak 0.472, deepest hole -0.355, 1-sigma level 0.067 Q1 1 0.6995 0.7010 0.2828 11.00000 0.05 0.47 Q2 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141.89 18.80 -9 7 0 133.09 19.70 -9 7 0 193.08 21.10 8 -7 0 160.18 15.40 8 -7 0 143.09 19.50 8 -7 0 137.39 18.90 -8 7 0 171.08 19.50 -8 7 0 126.29 17.90 -8 7 0 141.19 17.30 7 -7 0 485.85 27.20 7 -7 0 453.25 20.80 7 -7 0 447.86 25.60 -7 7 0 486.65 25.80 -7 7 0 489.75 25.40 -7 7 0 528.55 26.90 6 -7 0 336.77 17.00 6 -7 0 398.06 22.40 6 -7 0 342.37 22.30 -6 7 0 357.36 21.20 -6 7 0 363.96 21.90 -6 7 0 374.16 21.20 5 -7 0 343.57 20.20 5 -7 0 326.17 20.80 5 -7 0 338.97 15.50 -5 7 0 347.97 20.00 -5 7 0 368.46 20.00 -5 7 0 364.86 19.50 4 -7 0 -3.50 6.20 4 -7 0 1.40 4.30 4 -7 0 3.50 6.60 4 -7 0 14.10 7.70 -4 7 0 0.90 6.00 -4 7 0 -3.50 6.10 -4 7 0 1.40 5.60 3 -7 0 -3.30 5.80 3 -7 0 -3.60 5.40 3 -7 0 -0.10 5.30 3 -7 0 2.50 3.70 -3 7 0 -1.30 4.60 -3 7 0 -7.80 5.30 -3 7 0 0.70 6.10 2 -7 0 16.60 6.40 2 -7 0 21.70 6.20 2 -7 0 15.40 6.20 2 -7 0 19.20 4.30 -2 7 0 12.60 5.00 -2 7 0 24.20 6.70 -2 7 0 16.80 6.70 1 -7 0 183.28 8.40 1 -7 0 188.48 11.90 1 -7 0 174.48 12.90 1 -7 0 166.88 12.10 -1 7 0 170.88 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26.20 9.70 5 -8 9 28.40 9.60 -6 8 -9 69.19 11.90 6 -8 9 66.39 14.50 6 -8 9 60.69 11.80 6 -8 9 76.79 13.30 6 -8 9 71.79 13.10 7 -8 9 44.10 12.70 7 -8 9 16.60 10.80 7 -8 9 39.10 10.50 7 -8 9 27.70 13.10 8 -8 9 91.09 15.40 8 -8 9 86.19 13.60 8 -8 9 67.79 14.30 8 -8 9 52.79 15.40 9 -8 9 66.79 16.60 9 -8 9 117.19 18.60 9 -8 9 63.79 15.00 11 7 -9 319.47 28.80 -11 -7 9 268.27 24.70 -11 -7 9 276.17 25.60 10 7 -9 111.79 18.50 -10 -7 9 111.39 18.00 -10 -7 9 98.19 15.80 9 7 -9 174.88 22.30 -9 -7 9 171.48 19.60 -9 -7 9 146.09 19.70 8 7 -9 191.68 21.10 -8 -7 9 189.58 16.60 -8 -7 9 147.99 19.00 -8 -7 9 148.89 18.10 7 7 -9 45.90 12.20 -7 -7 9 42.70 10.20 -7 -7 9 43.20 11.00 -7 -7 9 47.30 8.20 6 7 -9 12.20 9.10 6 7 -9 7.50 6.90 -6 -7 9 3.60 7.50 -6 -7 9 9.20 5.00 -6 -7 9 3.10 8.10 5 7 -9 109.89 16.00 5 7 -9 79.29 12.20 -5 -7 9 92.29 13.50 -5 -7 9 109.19 9.10 -5 -7 9 127.39 16.20 4 7 -9 120.79 15.40 4 7 -9 98.09 11.80 -4 -7 9 105.69 16.50 -4 -7 9 115.99 13.60 3 7 -9 31.80 9.10 3 7 -9 28.50 7.20 -3 -7 9 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15.00 5 4 -9 60.99 9.00 -5 -4 9 74.99 11.70 -5 -4 9 64.39 11.30 -5 -4 9 77.19 10.30 4 4 -9 199.88 16.60 4 4 -9 202.08 13.00 -4 -4 9 213.28 14.10 -4 -4 9 200.88 11.80 -4 -4 9 219.88 16.60 3 4 -9 952.50 26.10 3 4 -9 940.31 31.90 -3 -4 9 931.71 23.50 -3 -4 9 919.51 31.60 -3 -4 9 883.81 26.90 2 4 -9 436.56 20.50 2 4 -9 420.56 15.20 -2 -4 9 409.26 15.90 -2 -4 9 428.66 12.60 -2 -4 9 399.86 10.70 -2 -4 9 406.56 20.10 -2 -4 9 425.26 16.50 1 4 -9 70.39 10.60 -1 -4 9 75.09 4.70 -1 -4 9 50.29 8.70 -1 -4 9 88.09 8.80 -1 -4 9 75.59 7.80 0 4 -9 14.20 6.90 0 4 -9 12.40 4.30 0 -4 9 7.50 4.20 0 -4 9 15.10 6.90 0 -4 9 19.10 7.00 0 -4 9 10.10 4.80 -1 4 -9 153.38 9.10 -1 4 -9 124.39 12.70 1 -4 9 141.49 9.20 1 -4 9 109.89 12.50 1 -4 9 135.39 12.40 1 -4 9 132.69 9.70 -2 4 -9 249.28 11.70 2 -4 9 247.68 12.70 2 -4 9 244.68 15.00 2 -4 9 248.48 15.80 2 -4 9 255.97 8.00 2 -4 9 245.18 11.90 -3 4 -9 451.25 16.70 3 -4 9 497.45 21.60 3 -4 9 447.26 19.10 3 -4 9 470.55 13.60 3 -4 9 489.05 18.20 -4 4 -9 787.32 24.00 4 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9 31.10 11.70 9 3 -9 36.80 12.90 -9 -3 9 43.40 11.50 -9 -3 9 63.19 12.60 -9 -3 9 64.89 13.70 8 3 -9 54.89 13.20 -8 -3 9 71.59 12.00 -8 -3 9 63.29 11.60 -8 -3 9 68.99 13.50 7 3 -9 34.10 11.10 -7 -3 9 41.50 9.80 -7 -3 9 53.29 10.20 -7 -3 9 63.79 12.00 6 3 -9 353.06 18.20 6 3 -9 333.67 22.40 -6 -3 9 343.57 18.80 -6 -3 9 290.67 20.30 -6 -3 9 369.26 19.60 5 3 -9 478.25 19.60 5 3 -9 491.75 25.00 -5 -3 9 551.14 20.90 -5 -3 9 511.15 21.50 -5 -3 9 542.15 25.10 4 3 -9 199.68 12.50 4 3 -9 218.78 17.00 -4 -3 9 230.08 14.00 -4 -3 9 237.68 12.90 -4 -3 9 228.18 17.10 3 3 -9 9.00 7.00 3 3 -9 12.40 4.80 -3 -3 9 6.40 4.30 -3 -3 9 4.60 4.20 -3 -3 9 1.00 6.50 -3 -3 9 6.90 5.10 2 3 -9 381.96 14.00 2 3 -9 427.86 19.80 -2 -3 9 383.26 15.10 -2 -3 9 391.36 9.80 -2 -3 9 385.46 19.10 -2 -3 9 402.56 14.90 -2 -3 9 389.46 13.10 1 3 -9 746.83 19.70 1 3 -9 786.42 26.80 -1 -3 9 739.23 18.20 -1 -3 9 765.22 18.30 -1 -3 9 778.62 21.30 -1 -3 9 732.73 25.90 -1 -3 9 800.02 21.20 0 3 -9 485.75 14.30 0 3 -9 447.86 20.00 0 -3 9 454.45 15.20 0 -3 9 479.45 15.20 0 -3 9 498.05 20.00 0 -3 9 477.25 12.20 -1 3 -9 204.48 14.00 -1 3 -9 218.28 9.50 1 -3 9 227.38 7.50 1 -3 9 251.77 14.80 1 -3 9 221.88 14.50 1 -3 9 215.38 10.60 1 -3 9 219.78 7.60 1 -3 9 216.78 10.00 -2 3 -9 228.48 14.70 -2 3 -9 236.58 10.10 2 -3 9 216.08 10.90 2 -3 9 224.68 14.70 2 -3 9 212.18 8.00 2 -3 9 204.48 10.10 2 -3 9 190.98 13.20 -3 3 -9 452.95 15.20 3 -3 9 472.35 18.40 3 -3 9 451.65 16.50 3 -3 9 457.95 20.30 3 -3 9 455.65 16.00 3 -3 9 471.35 14.50 -4 3 -9 253.67 12.50 4 -3 9 257.07 12.90 4 -3 9 246.18 13.40 4 -3 9 265.87 16.50 4 -3 9 258.97 13.90 4 -3 9 264.87 16.10 -5 3 -9 4.10 4.70 5 -3 9 4.90 5.40 5 -3 9 10.10 7.30 5 -3 9 8.40 5.30 5 -3 9 -5.10 6.00 -6 3 -9 14.40 6.20 6 -3 9 16.30 6.90 6 -3 9 11.60 7.60 6 -3 9 12.00 7.80 6 -3 9 15.70 5.80 -7 3 -9 13.30 6.90 -7 3 -9 -0.70 5.90 7 -3 9 9.10 7.20 7 -3 9 19.00 8.60 7 -3 9 13.60 9.30 7 -3 9 9.80 5.70 -8 3 -9 448.76 21.60 -8 3 -9 469.55 22.10 8 -3 9 471.85 23.40 8 -3 9 410.86 23.60 8 -3 9 403.46 24.40 8 -3 9 429.46 17.90 -9 3 -9 375.86 21.90 -9 3 -9 401.36 21.90 9 -3 9 395.46 23.70 9 -3 9 428.06 26.80 9 -3 9 434.96 25.70 -10 3 -9 140.39 17.00 10 -3 9 112.09 17.50 10 -3 9 78.99 16.30 10 -3 9 90.29 15.70 -11 3 -9 104.29 15.00 11 -3 9 121.69 17.20 11 -3 9 102.69 17.40 11 -3 9 118.99 18.70 11 -3 9 108.19 16.60 -12 3 -9 -9.10 8.60 12 -3 9 -1.50 8.70 12 -3 9 0.40 12.00 12 -3 9 -11.60 9.20 12 -3 9 15.40 12.50 11 2 -9 83.49 17.70 -11 -2 9 109.29 17.30 -11 -2 9 81.89 15.60 -11 -2 9 57.99 15.10 10 2 -9 112.39 18.70 -10 -2 9 124.89 19.00 -10 -2 9 120.09 18.40 -10 -2 9 156.48 19.90 9 2 -9 350.26 26.90 -9 -2 9 358.76 24.30 -9 -2 9 352.46 24.10 -9 -2 9 396.06 25.40 8 2 -9 22.70 11.10 -8 -2 9 12.60 8.70 -8 -2 9 10.40 9.40 -8 -2 9 13.80 8.50 7 2 -9 39.40 11.80 -7 -2 9 61.19 11.00 -7 -2 9 36.90 9.90 -7 -2 9 53.69 11.10 6 2 -9 -5.20 5.50 6 2 -9 -0.20 7.70 -6 -2 9 0.00 7.20 -6 -2 9 2.20 6.90 -6 -2 9 12.20 7.00 5 2 -9 320.37 20.80 5 2 -9 328.37 16.20 -5 -2 9 319.97 17.20 -5 -2 9 307.97 19.60 -5 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114.99 13.20 3 -8 10 120.09 16.80 3 -8 10 133.39 15.10 3 -8 10 116.79 15.60 -4 8 -10 205.48 17.90 4 -8 10 191.78 18.40 4 -8 10 154.18 16.60 4 -8 10 198.58 17.90 4 -8 10 195.78 20.30 5 -8 10 153.58 19.40 5 -8 10 141.79 16.90 5 -8 10 141.49 17.90 5 -8 10 144.09 16.60 6 -8 10 165.28 17.80 6 -8 10 186.78 22.10 6 -8 10 173.58 18.80 6 -8 10 184.48 19.40 7 -8 10 185.88 20.40 7 -8 10 189.38 19.00 7 -8 10 196.98 20.70 7 -8 10 175.68 22.20 8 -8 10 -8.80 9.10 8 -8 10 -0.60 11.60 8 -8 10 2.00 10.10 9 -8 10 4.00 10.80 9 -8 10 -5.40 10.10 9 -8 10 0.70 12.20 10 7 -10 123.29 19.90 -10 -7 10 104.39 16.90 -10 -7 10 84.09 15.70 9 7 -10 20.80 11.60 -9 -7 10 -9.50 8.30 -9 -7 10 -7.60 8.70 8 7 -10 16.10 10.90 -8 -7 10 15.80 10.30 -8 -7 10 -5.40 8.20 7 7 -10 121.99 18.70 -7 -7 10 105.29 14.60 -7 -7 10 114.49 17.60 6 7 -10 252.27 21.90 -6 -7 10 249.28 18.50 5 7 -10 226.68 19.30 -5 -7 10 211.28 17.00 -5 -7 10 191.98 19.70 4 7 -10 221.08 16.20 4 7 -10 191.28 17.70 -4 -7 10 160.18 18.40 -4 -7 10 183.08 15.70 3 7 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16.30 8 -7 10 66.89 16.10 8 -7 10 66.19 13.60 9 -7 10 161.08 21.30 9 -7 10 143.69 22.40 9 -7 10 223.38 22.50 10 -7 10 66.99 17.70 10 -7 10 32.60 13.50 10 -7 10 48.60 14.50 10 6 -10 79.79 17.00 -10 -6 10 74.29 15.20 -10 -6 10 124.89 19.40 9 6 -10 132.09 21.80 -9 -6 10 91.19 16.00 -9 -6 10 94.09 15.10 8 6 -10 798.02 37.40 -8 -6 10 786.22 29.90 -8 -6 10 799.92 33.60 -8 -6 10 784.02 35.90 7 6 -10 398.86 25.90 -7 -6 10 381.86 18.80 -7 -6 10 398.46 25.50 -7 -6 10 375.06 22.90 6 6 -10 37.30 11.10 -6 -6 10 12.40 8.10 -6 -6 10 17.90 9.50 -6 -6 10 30.40 7.10 5 6 -10 1.50 8.30 -5 -6 10 1.70 6.60 -5 -6 10 9.30 5.00 -5 -6 10 16.50 8.90 4 6 -10 163.68 13.10 4 6 -10 135.19 16.50 -4 -6 10 164.98 9.30 -4 -6 10 176.68 17.40 -4 -6 10 164.78 14.20 3 6 -10 151.28 15.80 3 6 -10 150.18 11.80 -3 -6 10 131.19 15.70 -3 -6 10 159.08 13.40 2 6 -10 299.67 14.40 2 6 -10 315.57 19.60 -2 -6 10 283.47 15.80 -2 -6 10 313.57 20.50 1 6 -10 407.36 16.80 1 6 -10 400.86 21.60 -1 -6 10 400.36 17.90 -1 -6 10 389.56 21.50 -1 -6 10 385.16 21.00 0 6 -10 10.60 5.50 0 6 -10 23.70 8.50 0 -6 10 8.10 5.80 0 -6 10 40.80 9.40 0 -6 10 11.40 7.50 -1 6 -10 225.38 17.30 -1 6 -10 249.78 13.60 1 -6 10 256.47 17.70 1 -6 10 242.48 17.50 1 -6 10 244.78 14.70 -2 6 -10 74.29 9.60 2 -6 10 82.89 12.90 2 -6 10 58.49 9.00 2 -6 10 52.69 10.50 -3 6 -10 33.80 7.20 3 -6 10 36.60 8.30 3 -6 10 34.60 8.90 3 -6 10 28.10 9.10 -4 6 -10 267.87 15.90 4 -6 10 251.97 16.80 4 -6 10 329.07 21.00 4 -6 10 276.37 18.90 4 -6 10 260.77 17.60 -5 6 -10 317.07 17.80 5 -6 10 349.37 19.70 5 -6 10 308.67 19.20 5 -6 10 314.77 21.10 5 -6 10 306.97 21.60 -6 6 -10 155.78 16.00 6 -6 10 156.38 15.60 6 -6 10 167.18 19.50 6 -6 10 151.78 17.30 6 -6 10 168.88 16.80 7 -6 10 219.88 17.40 7 -6 10 209.98 21.60 7 -6 10 225.68 19.40 7 -6 10 247.78 19.80 -8 6 -10 15.40 7.50 8 -6 10 31.40 9.40 8 -6 10 5.50 11.00 8 -6 10 25.10 10.10 8 -6 10 21.50 11.00 -9 6 -10 -4.10 7.00 9 -6 10 -0.90 11.70 9 -6 10 -3.60 9.40 9 -6 10 6.30 10.70 10 -6 10 86.99 17.50 10 -6 10 121.19 18.40 10 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4.10 0 -5 10 -2.80 5.60 0 -5 10 10.80 7.10 0 -5 10 -10.60 4.50 0 -5 10 4.30 6.60 -1 5 -10 5.10 6.50 -1 5 -10 2.20 4.10 1 -5 10 -5.20 4.60 1 -5 10 -5.00 6.00 1 -5 10 -1.00 6.00 -2 5 -10 344.97 14.80 2 -5 10 327.87 19.20 2 -5 10 338.37 16.10 2 -5 10 332.27 18.40 -3 5 -10 203.98 12.40 3 -5 10 203.68 16.60 3 -5 10 211.48 15.70 3 -5 10 195.88 13.70 -4 5 -10 119.79 11.30 4 -5 10 112.89 13.40 4 -5 10 148.79 15.90 4 -5 10 123.99 12.40 4 -5 10 135.99 14.40 -5 5 -10 9.80 5.90 5 -5 10 6.30 6.70 5 -5 10 10.60 6.90 5 -5 10 7.40 8.30 5 -5 10 20.30 8.40 -6 5 -10 10.40 6.70 6 -5 10 8.70 9.40 6 -5 10 8.70 8.40 6 -5 10 4.10 7.00 6 -5 10 3.40 6.70 7 -5 10 276.87 17.20 7 -5 10 264.07 20.50 7 -5 10 247.88 19.10 7 -5 10 266.97 22.00 8 -5 10 1.90 8.30 8 -5 10 7.50 7.00 8 -5 10 2.40 9.10 8 -5 10 -2.20 10.00 -9 5 -10 95.89 14.80 9 -5 10 105.39 16.00 9 -5 10 78.89 14.00 9 -5 10 81.59 16.20 -10 5 -10 45.10 11.00 10 -5 10 34.40 14.00 10 -5 10 38.10 13.30 10 -5 10 40.60 12.00 -11 5 -10 21.30 10.30 11 -5 10 14.00 11.90 11 -5 10 11.20 13.00 11 -5 10 1.90 11.40 10 4 -10 4.40 11.90 -10 -4 10 27.80 10.80 -10 -4 10 11.50 10.50 -10 -4 10 3.10 10.50 9 4 -10 370.56 28.70 -9 -4 10 428.56 26.20 -9 -4 10 384.76 26.20 -9 -4 10 362.86 23.30 8 4 -10 437.56 28.30 -8 -4 10 419.66 24.80 -8 -4 10 406.26 26.70 -8 -4 10 412.76 22.70 7 4 -10 205.88 20.60 -7 -4 10 171.58 18.70 -7 -4 10 206.68 18.10 -7 -4 10 173.28 15.70 6 4 -10 68.79 13.70 -6 -4 10 63.99 10.60 -6 -4 10 60.79 12.40 -6 -4 10 47.10 8.90 5 4 -10 45.50 11.30 5 4 -10 55.09 11.80 -5 -4 10 52.19 9.20 -5 -4 10 36.90 9.90 -5 -4 10 53.69 8.30 4 4 -10 35.50 6.80 4 4 -10 28.10 9.80 -4 -4 10 43.20 6.80 -4 -4 10 40.90 9.40 -4 -4 10 40.40 8.00 3 4 -10 23.40 5.70 3 4 -10 15.40 8.30 -3 -4 10 12.10 7.40 -3 -4 10 17.90 4.80 -3 -4 10 7.90 5.50 2 4 -10 381.86 20.90 2 4 -10 371.76 14.40 -2 -4 10 387.66 12.30 -2 -4 10 396.76 20.60 -2 -4 10 356.46 15.80 -2 -4 10 344.67 13.40 1 4 -10 731.43 20.30 1 4 -10 760.82 27.80 -1 -4 10 704.13 16.30 -1 -4 10 661.73 21.30 -1 -4 10 699.73 21.20 -1 -4 10 693.23 26.70 0 4 -10 105.99 8.20 0 4 -10 106.59 12.60 0 -4 10 111.99 12.70 0 -4 10 129.19 13.30 0 -4 10 98.99 8.60 0 -4 10 109.39 9.40 -1 4 -10 87.19 7.70 -1 4 -10 83.49 12.50 1 -4 10 81.49 8.90 1 -4 10 74.49 7.90 1 -4 10 128.49 13.00 1 -4 10 84.79 11.90 -2 4 -10 334.37 13.30 2 -4 10 339.07 18.60 2 -4 10 331.87 17.30 2 -4 10 357.76 15.10 2 -4 10 317.37 13.60 2 -4 10 329.37 9.50 -3 4 -10 166.48 10.50 3 -4 10 184.68 12.10 3 -4 10 173.58 15.20 3 -4 10 185.68 12.20 3 -4 10 173.68 13.80 -4 4 -10 25.60 5.90 4 -4 10 15.90 6.80 4 -4 10 27.40 6.90 4 -4 10 31.70 8.40 4 -4 10 36.00 9.50 -5 4 -10 102.89 10.60 5 -4 10 138.49 12.70 5 -4 10 123.89 12.30 5 -4 10 158.28 15.80 5 -4 10 142.99 14.70 -6 4 -10 142.29 12.70 6 -4 10 110.09 13.70 6 -4 10 119.29 14.90 6 -4 10 101.49 14.30 6 -4 10 103.69 12.40 -7 4 -10 242.68 16.30 7 -4 10 238.38 17.80 7 -4 10 246.08 15.40 7 -4 10 212.38 18.80 7 -4 10 215.98 20.30 8 -4 10 558.04 26.40 8 -4 10 525.45 21.50 8 -4 10 511.25 26.80 8 -4 10 534.65 29.10 9 -4 10 10.40 9.10 9 -4 10 -7.40 9.00 9 -4 10 0.40 10.80 -10 4 -10 12.10 8.40 10 -4 10 -20.90 8.80 10 -4 10 -9.60 8.20 10 -4 10 -4.30 9.30 -11 4 -10 9.70 9.60 11 -4 10 6.50 10.80 11 -4 10 9.00 11.70 11 -4 10 13.30 12.60 12 -4 10 23.20 14.10 12 -4 10 6.20 11.10 12 -4 10 -10.70 10.50 12 -4 10 -13.60 11.20 10 3 -10 112.49 19.60 -10 -3 10 110.09 17.30 -10 -3 10 94.69 15.60 -10 -3 10 141.59 19.60 9 3 -10 17.90 12.70 -9 -3 10 10.00 10.30 -9 -3 10 -0.30 8.50 -9 -3 10 16.40 9.20 8 3 -10 -10.10 9.60 -8 -3 10 -1.00 8.90 -8 -3 10 -5.70 7.40 -8 -3 10 -8.20 7.50 7 3 -10 14.70 10.40 -7 -3 10 4.60 8.90 -7 -3 10 3.50 8.10 -7 -3 10 1.20 7.40 6 3 -10 -4.80 7.70 -6 -3 10 5.60 8.20 -6 -3 10 -7.40 6.10 -6 -3 10 2.20 6.60 5 3 -10 -3.00 6.40 5 3 -10 9.10 8.50 -5 -3 10 13.80 6.90 -5 -3 10 3.70 6.10 -5 -3 10 -3.30 7.20 4 3 -10 261.77 19.40 4 3 -10 295.27 14.50 -4 -3 10 279.77 19.30 -4 -3 10 285.77 15.60 -4 -3 10 282.27 14.60 3 3 -10 289.47 18.90 3 3 -10 296.07 13.30 -3 -3 10 300.77 18.80 -3 -3 10 306.87 13.40 -3 -3 10 285.37 14.50 2 3 -10 226.88 16.70 2 3 -10 221.38 10.60 -2 -3 10 201.58 11.40 -2 -3 10 238.78 10.50 -2 -3 10 209.08 11.70 -2 -3 10 203.28 7.00 -2 -3 10 259.07 17.10 -2 -3 10 230.28 7.40 1 3 -10 250.47 16.70 -1 -3 10 271.17 10.10 -1 -3 10 261.97 9.70 -1 -3 10 261.17 11.70 -1 -3 10 275.77 16.90 -1 -3 10 247.28 11.90 0 3 -10 20.20 4.00 0 3 -10 16.10 7.20 0 -3 10 26.50 7.40 0 -3 10 18.20 3.40 0 -3 10 22.40 4.40 0 -3 10 15.40 4.60 -1 3 -10 1.00 5.30 -1 3 -10 4.90 3.30 1 -3 10 1.50 3.50 1 -3 10 1.80 2.40 1 -3 10 -1.60 2.40 1 -3 10 -2.10 3.70 1 -3 10 2.40 5.70 1 -3 10 2.00 5.60 -2 3 -10 72.59 6.70 -2 3 -10 103.09 12.30 2 -3 10 81.19 7.20 2 -3 10 75.19 8.00 2 -3 10 81.19 5.60 2 -3 10 87.89 10.70 2 -3 10 82.49 11.80 -3 3 -10 264.17 11.40 3 -3 10 238.58 16.00 3 -3 10 281.17 15.20 3 -3 10 260.47 12.70 -4 3 -10 511.85 17.40 4 -3 10 521.75 18.90 4 -3 10 491.15 22.20 4 -3 10 507.65 18.30 4 -3 10 559.94 20.40 4 -3 10 527.45 23.00 -5 3 -10 401.76 16.40 5 -3 10 385.56 20.40 5 -3 10 410.46 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6 13 10 307.97 21.60 6 13 10 320.57 21.00 6 13 10 331.27 19.10 7 13 10 62.39 12.40 7 13 10 53.39 12.50 7 13 10 77.59 11.50 8 13 10 73.99 13.80 8 13 10 66.29 11.00 8 13 10 55.19 9.30 8 13 10 65.99 13.10 9 13 10 30.90 8.80 9 13 10 14.60 10.10 9 13 10 32.50 9.70 9 13 10 14.30 9.60 10 13 10 4.00 10.10 10 13 10 -2.10 9.10 10 13 10 21.80 8.00 10 13 10 21.50 9.30 11 13 10 58.49 12.00 11 13 10 16.40 11.40 11 13 10 16.00 10.00 11 13 10 25.00 10.50 12 13 10 19.60 10.50 12 13 10 26.90 12.00 12 13 10 32.20 11.20 12 13 10 37.20 14.00 13 13 10 -1.50 9.40 13 13 10 0.50 11.30 13 13 10 11.30 10.40 13 13 10 2.40 9.60 14 13 10 41.00 13.50 14 13 10 6.80 10.20 14 13 10 22.40 13.60 14 13 10 27.90 12.60 -3 14 10 54.89 14.60 -3 14 10 65.79 13.90 -3 14 10 74.39 15.30 -2 14 10 58.19 14.30 -2 14 10 44.60 12.10 -2 14 10 83.69 16.20 -1 14 10 37.00 12.20 -1 14 10 -2.40 9.70 -1 14 10 5.30 9.50 0 14 10 6.10 9.60 0 14 10 -1.60 9.10 0 14 10 -5.60 7.20 1 14 10 16.30 9.70 1 14 10 23.20 10.80 1 14 10 29.70 9.60 2 14 10 33.50 8.90 2 14 10 50.59 10.50 2 14 10 31.60 11.80 2 14 10 20.40 9.80 3 14 10 121.19 17.90 3 14 10 152.88 17.50 3 14 10 121.09 15.20 3 14 10 128.99 15.10 4 14 10 210.28 17.20 4 14 10 212.98 19.80 4 14 10 186.58 18.90 4 14 10 186.28 17.20 5 14 10 412.96 24.80 5 14 10 373.76 22.50 5 14 10 367.46 21.20 6 14 10 6.50 9.30 6 14 10 28.40 10.70 7 14 10 45.30 10.20 7 14 10 68.49 13.60 7 14 10 45.30 12.50 8 14 10 4.40 7.40 8 14 10 0.60 9.50 8 14 10 11.90 10.70 9 14 10 223.28 18.90 9 14 10 220.08 21.00 9 14 10 191.48 16.90 9 14 10 196.78 20.50 10 14 10 249.58 22.50 10 14 10 283.97 24.40 10 14 10 296.87 21.70 10 14 10 249.38 19.10 11 14 10 62.29 12.50 11 14 10 61.69 14.60 11 14 10 63.69 13.60 11 14 10 62.89 13.20 12 14 10 19.10 12.90 12 14 10 34.30 12.10 12 14 10 34.00 11.50 12 14 10 31.20 11.50 13 14 10 1.20 11.60 13 14 10 7.50 10.40 13 14 10 6.90 10.60 13 14 10 -12.50 9.30 -2 15 10 -12.10 8.70 -2 15 10 1.30 10.60 -2 15 10 -4.50 9.20 -1 15 10 60.49 13.00 -1 15 10 54.79 13.80 -1 15 10 67.39 14.70 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14.90 3 17 10 116.79 17.70 3 17 10 131.49 20.80 3 17 10 123.89 19.50 3 17 10 131.89 17.40 4 17 10 3.90 9.30 4 17 10 -9.50 7.60 4 17 10 19.40 10.20 4 17 10 10.70 10.70 5 17 10 67.39 13.80 5 17 10 65.89 14.50 5 17 10 55.89 13.00 5 17 10 59.19 12.60 6 17 10 35.30 11.70 6 17 10 34.20 11.20 6 17 10 53.29 13.10 6 17 10 34.20 11.90 7 17 10 106.39 15.60 7 17 10 138.69 19.20 7 17 10 93.79 16.60 8 17 10 39.30 12.90 8 17 10 56.99 13.80 9 17 10 85.09 16.30 9 17 10 127.59 17.10 9 17 10 119.29 18.00 10 17 10 236.98 24.00 10 17 10 215.48 21.80 10 17 10 221.08 23.50 11 17 10 145.79 20.80 11 17 10 160.58 21.50 11 17 10 168.28 22.50 3 18 10 30.20 11.00 3 18 10 31.50 12.80 3 18 10 25.60 12.00 4 18 10 116.09 18.00 4 18 10 162.98 19.60 4 18 10 144.49 21.00 4 18 10 151.78 21.20 5 18 10 55.99 13.60 5 18 10 49.00 13.30 5 18 10 45.20 13.90 5 18 10 49.60 12.60 6 18 10 182.58 21.70 6 18 10 162.28 20.10 6 18 10 167.68 20.60 6 18 10 179.68 22.50 7 18 10 68.69 15.30 7 18 10 70.39 14.80 7 18 10 41.50 13.50 7 18 10 83.49 15.00 8 18 10 14.60 11.70 8 18 10 8.90 10.80 8 18 10 4.60 10.10 9 18 10 12.80 10.60 9 18 10 21.10 11.20 9 18 10 6.70 11.40 10 18 10 5.30 11.10 10 18 10 0.90 10.70 10 18 10 11.20 10.90 -3 -15 11 2.80 10.70 -3 -15 11 -5.70 11.90 -3 -15 11 -7.80 10.20 -2 -15 11 -4.40 10.40 -2 -15 11 17.40 12.20 -2 -15 11 -4.00 12.00 -1 -15 11 83.19 17.70 -1 -15 11 77.99 15.50 -1 -15 11 89.69 17.10 -5 -14 11 90.49 16.50 -5 -14 11 113.39 20.00 -5 -14 11 92.79 16.30 -4 -14 11 171.98 22.00 -4 -14 11 169.18 22.20 -4 -14 11 235.18 26.00 -3 -14 11 26.90 12.70 -3 -14 11 48.70 14.90 -3 -14 11 72.79 15.30 -2 -14 11 44.20 13.40 -2 -14 11 47.90 15.50 -2 -14 11 21.00 12.20 -1 -14 11 95.49 17.00 -1 -14 11 130.39 21.00 -1 -14 11 143.29 23.20 0 -14 11 14.50 11.50 0 -14 11 -1.00 11.60 0 -14 11 2.70 11.50 1 -14 11 -2.70 10.60 1 -14 11 9.60 12.30 1 -14 11 -0.30 9.60 2 -14 11 -2.20 11.10 2 -14 11 9.30 10.50 2 -14 11 15.90 13.10 2 -14 11 17.70 11.70 7 13 -11 55.99 14.60 -7 -13 11 52.49 14.80 -7 -13 11 56.79 15.60 -7 -13 11 45.70 13.20 6 13 -11 282.37 24.60 -6 -13 11 344.47 28.10 -6 -13 11 275.07 25.30 -6 -13 11 378.46 27.10 5 13 -11 -2.30 9.40 -5 -13 11 31.70 12.40 -5 -13 11 23.40 11.70 -5 -13 11 17.00 13.00 4 13 -11 13.40 10.60 -4 -13 11 15.40 11.10 -4 -13 11 19.60 11.00 -4 -13 11 16.70 12.80 3 13 -11 71.09 13.90 -3 -13 11 72.09 16.30 -3 -13 11 44.40 13.50 -3 -13 11 67.29 14.30 -2 -13 11 -8.00 10.60 -2 -13 11 -2.70 9.10 -2 -13 11 -6.50 8.60 -1 -13 11 10.60 12.50 -1 -13 11 5.80 10.50 -1 -13 11 11.40 10.30 0 -13 11 173.88 21.80 0 -13 11 186.58 23.20 0 -13 11 216.98 21.40 1 -13 11 262.27 23.20 1 -13 11 290.57 26.00 1 -13 11 233.68 23.50 2 -13 11 11.30 12.60 2 -13 11 27.20 11.80 2 -13 11 45.70 13.30 2 -13 11 39.20 13.70 3 -13 11 58.59 16.00 3 -13 11 52.09 15.20 3 -13 11 47.10 13.50 3 -13 11 52.19 14.40 4 -13 11 -0.80 10.10 4 -13 11 4.30 10.20 4 -13 11 7.70 11.50 4 -13 11 -2.60 12.10 8 12 -11 29.70 12.50 -8 -12 11 27.30 12.20 -8 -12 11 26.50 13.60 -8 -12 11 42.80 13.30 7 12 -11 193.78 22.50 -7 -12 11 182.58 22.90 -7 -12 11 223.28 24.80 -7 -12 11 184.78 21.70 6 12 -11 0.30 9.50 -6 -12 11 16.00 12.00 -6 -12 11 13.40 10.40 -6 -12 11 4.30 10.50 5 12 -11 20.00 11.00 -5 -12 11 7.60 11.30 -5 -12 11 3.00 10.20 -5 -12 11 3.30 9.40 4 12 -11 38.20 11.60 -4 -12 11 14.90 10.10 -4 -12 11 19.90 11.90 -4 -12 11 21.10 10.50 3 12 -11 84.19 14.70 -3 -12 11 95.39 14.60 -3 -12 11 107.39 16.70 -3 -12 11 86.39 15.70 2 12 -11 91.79 14.60 -2 -12 11 61.19 12.90 -2 -12 11 66.49 14.40 -2 -12 11 55.99 14.00 -1 -12 11 14.70 10.10 -1 -12 11 24.70 10.30 -1 -12 11 31.50 13.10 0 -12 11 14.10 11.50 0 -12 11 36.90 12.50 0 -12 11 21.90 10.60 1 -12 11 -3.30 10.00 1 -12 11 9.80 9.70 1 -12 11 -5.90 9.60 2 -12 11 10.00 11.30 2 -12 11 11.80 10.50 2 -12 11 62.49 14.50 3 -12 11 -5.20 10.60 3 -12 11 -2.60 10.50 3 -12 11 -1.10 9.40 3 -12 11 21.10 11.20 4 -12 11 42.80 14.60 4 -12 11 59.59 14.70 4 -12 11 48.30 13.30 4 -12 11 76.39 15.30 5 -12 11 24.50 12.20 5 -12 11 4.00 10.70 5 -12 11 43.20 15.70 5 -12 11 34.00 12.90 8 11 -11 12.80 11.40 -8 -11 11 5.80 12.00 -8 -11 11 16.60 11.60 7 11 -11 116.69 17.70 -7 -11 11 91.69 16.60 -7 -11 11 80.79 16.30 -7 -11 11 99.69 16.30 6 11 -11 244.38 23.20 -6 -11 11 271.47 25.50 -6 -11 11 279.07 22.70 -6 -11 11 349.17 25.60 5 11 -11 56.19 12.90 -5 -11 11 46.50 11.50 -5 -11 11 39.50 12.80 -5 -11 11 62.49 14.60 4 11 -11 103.19 15.70 -4 -11 11 59.59 14.10 -4 -11 11 75.79 13.50 -4 -11 11 73.79 14.10 3 11 -11 43.70 11.70 -3 -11 11 34.90 12.30 -3 -11 11 48.90 12.80 -3 -11 11 26.70 10.70 2 11 -11 21.10 9.90 -2 -11 11 11.60 9.60 -2 -11 11 14.20 10.80 -2 -11 11 5.10 8.30 -1 -11 11 4.30 10.10 -1 -11 11 -2.40 8.00 -1 -11 11 4.80 9.50 0 -11 11 32.60 11.70 0 -11 11 21.30 9.90 0 -11 11 12.40 11.20 1 -11 11 -1.00 9.50 1 -11 11 -8.90 8.00 1 -11 11 1.20 10.30 2 -11 11 36.60 13.00 2 -11 11 23.90 11.10 2 -11 11 29.00 10.60 3 -11 11 188.68 20.70 3 -11 11 200.88 20.40 3 -11 11 216.08 22.80 3 -11 11 218.88 22.80 4 -11 11 201.38 21.10 4 -11 11 212.08 22.90 4 -11 11 218.38 21.40 4 -11 11 214.98 23.50 5 -11 11 35.90 12.40 5 -11 11 12.50 12.40 5 -11 11 8.70 10.90 5 -11 11 26.00 11.50 6 -11 11 10.60 10.40 6 -11 11 10.90 11.30 6 -11 11 -3.20 12.30 9 10 -11 32.20 13.30 -9 -10 11 19.70 11.40 -9 -10 11 14.70 13.20 8 10 -11 75.89 16.20 -8 -10 11 82.09 16.80 -8 -10 11 88.69 15.60 7 10 -11 89.49 16.30 -7 -10 11 117.49 17.70 -7 -10 11 74.59 14.00 6 10 -11 252.67 23.00 -6 -10 11 235.18 20.70 -6 -10 11 220.28 22.80 5 10 -11 180.38 20.50 -5 -10 11 207.78 22.60 -5 -10 11 191.28 18.90 -5 -10 11 242.48 21.20 4 10 -11 8.90 9.40 -4 -10 11 15.50 9.90 -4 -10 11 25.40 9.20 -4 -10 11 -4.70 9.10 3 10 -11 35.40 10.90 -3 -10 11 16.60 10.50 -3 -10 11 11.60 8.70 -3 -10 11 6.90 9.30 2 10 -11 140.89 17.70 -2 -10 11 130.79 18.70 -2 -10 11 123.99 18.40 -2 -10 11 150.08 17.00 1 10 -11 321.07 22.10 -1 -10 11 305.27 20.80 -1 -10 11 309.47 23.20 -1 -10 11 315.47 23.80 0 -10 11 322.77 21.10 0 -10 11 306.97 24.40 0 -10 11 358.36 24.00 1 -10 11 43.30 10.90 1 -10 11 68.79 13.80 1 -10 11 53.69 12.60 2 -10 11 85.79 13.80 2 -10 11 124.69 18.40 2 -10 11 108.39 17.50 3 -10 11 47.00 11.90 3 -10 11 71.59 14.30 3 -10 11 75.39 14.30 3 -10 11 57.49 11.70 4 -10 11 55.59 11.80 4 -10 11 45.80 13.80 4 -10 11 73.79 13.80 4 -10 11 56.59 13.80 5 -10 11 1.80 9.60 5 -10 11 24.60 11.50 5 -10 11 7.00 9.30 5 -10 11 25.90 13.00 6 -10 11 6.70 10.90 6 -10 11 2.20 11.80 6 -10 11 24.10 11.10 6 -10 11 6.50 10.30 7 -10 11 82.89 16.10 7 -10 11 90.09 16.40 7 -10 11 84.39 15.00 7 -10 11 145.49 23.40 9 9 -11 21.90 12.90 -9 -9 11 33.30 12.50 -9 -9 11 26.90 12.90 8 9 -11 -12.60 9.70 -8 -9 11 -18.60 9.00 -8 -9 11 -7.60 8.20 7 9 -11 47.10 13.40 -7 -9 11 39.50 11.70 -7 -9 11 25.70 12.20 6 9 -11 72.89 14.20 -6 -9 11 111.59 16.50 -6 -9 11 83.49 15.60 5 9 -11 5.70 9.00 -5 -9 11 -7.20 7.60 -5 -9 11 2.80 10.00 4 9 -11 52.19 12.20 -4 -9 11 27.50 10.90 -4 -9 11 48.50 10.60 -4 -9 11 48.50 13.10 3 9 -11 76.99 13.50 -3 -9 11 82.79 13.80 -3 -9 11 100.89 16.20 -3 -9 11 92.29 14.30 2 9 -11 65.89 12.70 -2 -9 11 64.39 10.80 -2 -9 11 45.70 11.80 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5 -10 12 179.58 20.30 5 -10 12 125.09 18.80 5 -10 12 139.79 21.90 6 -10 12 -2.60 9.90 6 -10 12 -6.00 10.20 6 -10 12 11.60 11.10 6 -10 12 18.40 13.50 7 -10 12 5.50 11.10 7 -10 12 -11.20 12.30 7 -10 12 8.00 10.30 8 9 -12 86.49 17.00 -8 -9 12 108.19 16.70 -8 -9 12 93.39 17.60 7 9 -12 280.27 25.50 -7 -9 12 260.37 25.00 -7 -9 12 238.48 21.90 6 9 -12 17.40 11.00 -6 -9 12 14.00 9.50 -6 -9 12 13.20 11.90 5 9 -12 -3.00 9.80 -5 -9 12 21.20 11.90 -5 -9 12 23.60 9.70 4 9 -12 48.90 12.90 -4 -9 12 50.19 12.90 -4 -9 12 23.20 11.40 -4 -9 12 22.70 9.50 3 9 -12 14.90 9.90 -3 -9 12 23.80 11.40 -3 -9 12 18.00 8.50 -3 -9 12 7.80 9.30 2 9 -12 43.40 11.50 -2 -9 12 62.09 13.80 -2 -9 12 68.29 11.50 -2 -9 12 49.80 12.20 1 9 -12 522.35 28.00 -1 -9 12 552.64 28.90 -1 -9 12 529.75 28.90 -1 -9 12 494.25 24.40 0 -9 12 372.96 25.30 0 -9 12 416.96 22.30 0 -9 12 407.76 25.60 1 -9 12 308.17 23.30 1 -9 12 293.47 19.70 1 -9 12 265.67 22.00 2 -9 12 172.78 19.80 2 -9 12 206.68 21.10 2 -9 12 167.68 17.00 3 -9 12 13.20 8.60 3 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158.08 19.00 5 -6 12 210.78 17.50 6 -6 12 59.79 13.40 6 -6 12 58.99 11.30 6 -6 12 72.79 14.10 6 -6 12 48.30 10.80 7 -6 12 52.29 14.30 7 -6 12 63.79 11.50 7 -6 12 70.29 12.50 7 -6 12 61.79 14.10 8 -6 12 14.40 11.10 8 -6 12 8.10 11.90 8 -6 12 18.90 10.40 9 -6 12 9.30 12.40 9 -6 12 6.20 11.60 9 -6 12 12.80 10.00 10 -6 12 70.99 15.60 10 -6 12 88.69 17.90 10 -6 12 82.69 16.50 9 5 -12 -7.60 10.80 -9 -5 12 11.90 11.40 8 5 -12 0.30 10.30 -8 -5 12 -8.80 9.40 -8 -5 12 -1.40 8.20 7 5 -12 25.00 12.40 -7 -5 12 36.50 10.20 6 5 -12 88.59 16.00 -6 -5 12 74.39 14.50 -6 -5 12 70.49 11.70 5 5 -12 117.69 17.00 -5 -5 12 143.49 15.00 -5 -5 12 141.79 18.20 4 5 -12 25.00 10.30 -4 -5 12 3.00 6.50 -4 -5 12 4.80 8.60 3 5 -12 34.80 11.10 -3 -5 12 51.39 11.70 -3 -5 12 47.80 8.50 2 5 -12 31.50 10.50 -2 -5 12 18.80 6.60 -2 -5 12 19.70 8.80 1 5 -12 242.58 19.30 -1 -5 12 206.88 18.00 -1 -5 12 244.78 14.10 -1 -5 12 201.08 18.30 0 5 -12 113.19 15.00 0 -5 12 100.89 15.20 0 -5 12 111.19 15.80 0 -5 12 114.29 11.00 -1 5 -12 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32.90 12.00 -6 -4 12 36.80 11.30 -6 -4 12 24.40 8.60 -6 -4 12 37.80 9.60 5 4 -12 15.70 10.70 -5 -4 12 1.40 6.30 -5 -4 12 29.00 8.50 -5 -4 12 31.90 11.00 4 4 -12 211.78 19.70 -4 -4 12 212.08 15.20 -4 -4 12 202.08 19.40 -4 -4 12 202.48 13.10 3 4 -12 271.07 21.00 -3 -4 12 270.07 12.90 -3 -4 12 253.47 20.10 -3 -4 12 280.37 15.50 2 4 -12 278.17 20.50 -2 -4 12 279.57 20.10 -2 -4 12 307.27 11.80 -2 -4 12 272.17 14.70 1 4 -12 8.60 8.10 -1 -4 12 0.10 7.00 -1 -4 12 10.70 5.40 -1 -4 12 3.10 3.20 0 4 -12 77.49 11.90 0 -4 12 99.09 5.80 0 -4 12 83.29 9.50 0 -4 12 103.89 14.30 0 -4 12 98.69 13.60 -1 4 -12 29.70 9.60 1 -4 12 9.50 8.00 1 -4 12 22.20 6.00 1 -4 12 18.60 8.30 -2 4 -12 4.80 7.30 2 -4 12 -6.80 6.20 2 -4 12 -5.80 6.30 2 -4 12 -0.80 4.80 2 -4 12 -1.30 2.40 3 -4 12 7.30 7.90 3 -4 12 25.60 6.40 3 -4 12 28.90 8.20 4 -4 12 256.47 19.10 4 -4 12 256.27 18.80 4 -4 12 255.57 14.80 4 -4 12 233.98 16.40 5 -4 12 16.00 9.30 5 -4 12 19.60 7.60 5 -4 12 23.40 9.50 5 -4 12 26.00 7.40 6 -4 12 74.19 10.80 6 -4 12 72.49 13.10 6 -4 12 97.49 15.50 6 -4 12 68.09 10.20 7 -4 12 132.09 17.30 7 -4 12 92.49 12.80 7 -4 12 143.59 18.50 7 -4 12 145.69 15.60 8 -4 12 97.89 15.30 8 -4 12 98.59 15.60 8 -4 12 78.89 14.50 9 -4 12 212.68 19.50 9 -4 12 194.68 22.90 9 -4 12 191.08 21.00 10 -4 12 37.60 14.50 10 -4 12 59.69 13.40 10 -4 12 49.10 14.10 11 -4 12 106.89 18.70 11 -4 12 143.59 20.40 11 -4 12 107.59 17.70 9 3 -12 35.50 14.10 -9 -3 12 19.40 11.40 -9 -3 12 37.00 11.60 -9 -3 12 28.40 11.50 8 3 -12 9.10 11.20 -8 -3 12 6.30 9.00 -8 -3 12 8.40 9.60 -8 -3 12 -1.50 9.80 7 3 -12 17.30 12.20 -7 -3 12 1.30 7.90 -7 -3 12 8.10 8.60 -7 -3 12 -3.30 9.30 6 3 -12 231.58 21.80 -6 -3 12 201.28 20.70 -6 -3 12 202.08 17.20 -6 -3 12 203.88 16.80 5 3 -12 252.47 22.20 -5 -3 12 287.77 22.10 -5 -3 12 262.57 16.70 -5 -3 12 278.17 17.50 4 3 -12 428.16 25.00 -4 -3 12 459.85 25.40 -4 -3 12 451.15 19.80 -4 -3 12 402.76 18.30 3 3 -12 271.67 20.50 -3 -3 12 263.97 14.90 -3 -3 12 251.87 13.30 -3 -3 12 249.58 19.60 2 3 -12 569.84 26.90 -2 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51.19 14.20 11 -3 12 51.39 14.20 11 -3 12 38.40 12.80 12 -3 12 28.40 14.30 12 -3 12 64.89 17.10 12 -3 12 50.39 14.20 12 -3 12 32.00 13.00 9 2 -12 8.50 11.60 -9 -2 12 9.80 10.60 -9 -2 12 12.30 10.30 -9 -2 12 11.20 10.80 8 2 -12 72.09 16.70 -8 -2 12 74.69 14.10 -8 -2 12 79.99 13.90 -8 -2 12 111.99 17.70 7 2 -12 68.99 14.70 -7 -2 12 85.39 13.50 -7 -2 12 68.19 12.00 -7 -2 12 89.29 15.50 6 2 -12 49.99 13.00 -6 -2 12 44.00 10.00 -6 -2 12 58.39 10.90 -6 -2 12 75.59 14.60 5 2 -12 10.00 9.10 -5 -2 12 6.90 7.30 -5 -2 12 5.10 9.10 -5 -2 12 16.10 7.20 4 2 -12 34.60 11.00 -4 -2 12 20.50 6.90 -4 -2 12 17.80 8.90 -4 -2 12 31.70 7.50 3 2 -12 66.69 12.30 -3 -2 12 64.79 11.90 -3 -2 12 75.59 9.80 -3 -2 12 48.40 7.60 2 2 -12 76.39 11.60 -2 -2 12 66.59 5.40 -2 -2 12 53.89 10.70 -2 -2 12 68.49 8.70 -2 -2 12 75.49 8.90 1 2 -12 22.70 8.70 -1 -2 12 14.90 4.90 -1 -2 12 28.90 5.40 -1 -2 12 34.10 8.90 0 2 -12 138.19 15.00 0 -2 12 114.79 8.20 0 -2 12 127.29 9.80 0 -2 12 138.49 14.90 0 -2 12 107.29 8.30 -1 2 -12 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229.18 27.20 8 -8 13 233.18 23.00 8 -8 13 218.78 24.20 8 7 -13 20.40 13.50 -8 -7 13 22.60 10.50 -8 -7 13 12.20 11.90 7 7 -13 45.80 14.40 -7 -7 13 43.70 13.90 -7 -7 13 50.99 12.00 6 7 -13 19.00 11.30 -6 -7 13 1.90 8.10 -6 -7 13 3.20 10.60 5 7 -13 188.58 22.30 -5 -7 13 177.98 17.20 -5 -7 13 189.98 22.40 4 7 -13 169.88 19.70 -4 -7 13 138.99 20.20 -4 -7 13 132.99 15.50 3 7 -13 92.69 15.10 -3 -7 13 105.29 15.40 -3 -7 13 63.79 14.20 -3 -7 13 133.99 14.30 2 7 -13 51.89 12.10 -2 -7 13 90.89 15.20 -2 -7 13 37.50 11.70 -2 -7 13 69.89 11.10 1 7 -13 145.09 17.80 -1 -7 13 132.69 13.90 -1 -7 13 118.69 17.50 -1 -7 13 116.79 17.20 0 7 -13 72.99 13.50 0 -7 13 95.59 12.70 0 -7 13 80.49 14.00 0 -7 13 56.89 12.50 1 -7 13 40.00 11.20 1 -7 13 33.00 10.60 1 -7 13 26.00 8.30 2 -7 13 369.06 24.50 2 -7 13 347.87 19.60 2 -7 13 400.86 23.90 3 -7 13 186.58 15.80 3 -7 13 206.88 19.10 3 -7 13 162.78 19.00 4 -7 13 154.68 15.70 4 -7 13 171.48 19.90 4 -7 13 166.68 20.70 4 -7 13 162.98 18.60 5 -7 13 27.70 11.70 5 -7 13 33.50 12.20 5 -7 13 59.29 12.00 5 -7 13 55.09 11.00 6 -7 13 52.09 14.10 6 -7 13 36.30 10.70 6 -7 13 30.80 12.10 6 -7 13 44.90 11.50 7 -7 13 7.10 10.90 7 -7 13 9.30 10.10 7 -7 13 -2.10 8.40 7 -7 13 15.10 13.00 8 -7 13 -3.80 8.60 8 -7 13 -20.30 9.70 8 -7 13 27.90 13.80 9 -7 13 48.10 15.00 9 -7 13 52.09 16.50 9 -7 13 67.59 14.30 8 6 -13 36.70 14.40 -8 -6 13 20.80 10.50 -8 -6 13 15.10 12.40 7 6 -13 56.59 15.00 -7 -6 13 43.20 13.00 -7 -6 13 62.89 12.40 6 6 -13 120.99 20.20 -6 -6 13 113.19 16.00 -6 -6 13 65.89 13.80 5 6 -13 170.48 21.00 -5 -6 13 144.29 15.90 -5 -6 13 193.58 21.50 4 6 -13 25.20 11.20 -4 -6 13 15.90 9.70 -4 -6 13 26.40 8.40 3 6 -13 -1.00 9.40 -3 -6 13 -8.60 5.90 -3 -6 13 -14.80 7.70 2 6 -13 33.20 10.80 -2 -6 13 27.50 7.40 -2 -6 13 39.00 12.50 -2 -6 13 43.10 11.10 1 6 -13 26.80 10.20 -1 -6 13 37.20 8.10 -1 -6 13 27.60 10.60 -1 -6 13 30.10 10.60 0 6 -13 308.97 22.20 0 -6 13 291.37 21.50 0 -6 13 276.27 16.20 0 -6 13 259.27 21.20 -1 6 -13 203.28 18.80 1 -6 13 165.88 13.90 1 -6 13 165.48 17.90 1 -6 13 180.48 17.70 2 -6 13 57.29 12.20 2 -6 13 60.49 11.80 2 -6 13 82.49 11.80 3 -6 13 13.40 7.20 3 -6 13 6.20 8.70 3 -6 13 -5.30 7.80 4 -6 13 70.59 13.00 4 -6 13 110.09 15.70 4 -6 13 88.89 13.10 4 -6 13 138.29 17.30 5 -6 13 -5.90 8.60 5 -6 13 -4.50 8.20 5 -6 13 -2.10 6.90 5 -6 13 0.70 7.70 6 -6 13 17.20 8.50 6 -6 13 6.90 8.30 6 -6 13 1.80 10.00 6 -6 13 2.50 9.60 7 -6 13 84.09 15.10 7 -6 13 84.09 15.80 7 -6 13 84.59 12.90 7 -6 13 115.49 16.50 8 -6 13 327.67 25.80 8 -6 13 333.87 23.80 8 -6 13 302.47 26.80 9 -6 13 66.49 15.50 9 -6 13 68.19 16.30 10 -6 13 120.19 17.30 10 -6 13 115.09 20.40 10 -6 13 106.99 18.30 9 5 -13 103.89 19.80 8 5 -13 -16.10 10.00 -8 -5 13 -12.90 9.30 -8 -5 13 -8.70 8.70 7 5 -13 61.99 15.60 -7 -5 13 72.39 15.50 -7 -5 13 56.99 12.30 6 5 -13 142.99 21.30 -6 -5 13 195.98 22.60 -6 -5 13 220.78 18.10 5 5 -13 -3.90 9.40 -5 -5 13 0.80 6.60 -5 -5 13 6.20 9.70 4 5 -13 45.50 12.20 -4 -5 13 46.00 9.40 -4 -5 13 36.10 11.60 3 5 -13 379.96 24.90 -3 -5 13 355.36 24.20 -3 -5 13 412.46 19.50 2 5 -13 85.89 14.40 -2 -5 13 74.19 13.20 -2 -5 13 53.29 8.80 1 5 -13 169.38 18.30 -1 -5 13 190.18 18.00 -1 -5 13 148.59 17.60 -1 -5 13 173.28 12.90 0 5 -13 813.82 32.90 0 -5 13 818.52 32.60 0 -5 13 732.33 31.60 0 -5 13 797.32 25.50 -1 5 -13 22.20 9.40 1 -5 13 27.30 9.20 1 -5 13 17.90 6.40 1 -5 13 30.70 9.50 2 -5 13 4.00 5.60 2 -5 13 -8.20 6.90 2 -5 13 22.40 9.00 3 -5 13 46.10 12.20 3 -5 13 49.60 10.40 3 -5 13 59.19 9.00 4 -5 13 127.39 17.60 4 -5 13 122.69 16.50 4 -5 13 105.49 12.60 4 -5 13 126.49 15.20 5 -5 13 157.58 17.90 5 -5 13 140.49 15.90 5 -5 13 162.28 14.80 5 -5 13 138.09 18.00 6 -5 13 140.89 19.00 6 -5 13 150.38 15.70 6 -5 13 128.59 14.90 6 -5 13 120.99 18.60 7 -5 13 240.68 22.30 7 -5 13 187.68 20.20 7 -5 13 198.38 18.00 7 -5 13 218.98 17.60 8 -5 13 79.79 13.50 8 -5 13 57.29 14.50 8 -5 13 64.99 14.70 9 -5 13 2.90 10.80 9 -5 13 -1.40 11.30 9 -5 13 2.90 8.90 10 -5 13 -3.90 10.80 10 -5 13 5.70 9.60 10 -5 13 -9.00 12.00 9 4 -13 8.10 12.30 -9 -4 13 2.20 11.10 -9 -4 13 6.70 9.60 8 4 -13 9.20 11.40 -8 -4 13 1.10 8.80 -8 -4 13 2.70 10.10 7 4 -13 67.19 16.10 -7 -4 13 104.39 16.00 -7 -4 13 77.89 15.30 6 4 -13 221.78 23.60 -6 -4 13 183.98 22.20 -6 -4 13 206.28 18.00 5 4 -13 120.69 18.50 -5 -4 13 121.39 14.00 -5 -4 13 124.19 18.70 4 4 -13 68.79 13.70 -4 -4 13 86.49 11.80 -4 -4 13 74.49 14.00 3 4 -13 86.49 14.20 -3 -4 13 76.99 10.00 -3 -4 13 89.39 14.80 2 4 -13 -6.60 7.90 -2 -4 13 4.90 8.40 -2 -4 13 11.60 5.90 1 4 -13 46.60 10.60 -1 -4 13 48.70 11.40 -1 -4 13 59.49 9.30 0 4 -13 -3.90 7.70 0 -4 13 12.40 8.60 0 -4 13 12.00 8.40 0 -4 13 4.20 4.90 -1 4 -13 206.28 18.60 1 -4 13 180.18 17.40 1 -4 13 173.58 17.30 1 -4 13 178.68 11.80 -2 4 -13 20.40 9.00 2 -4 13 15.00 5.80 2 -4 13 3.10 7.80 2 -4 13 22.80 8.70 3 -4 13 530.45 26.40 3 -4 13 539.55 19.80 3 -4 13 500.15 23.50 4 -4 13 452.95 22.10 4 -4 13 451.55 18.90 4 -4 13 436.46 23.90 4 -4 13 389.16 23.90 5 -4 13 104.89 13.90 5 -4 13 115.69 17.40 5 -4 13 98.49 14.60 5 -4 13 118.29 12.70 6 -4 13 34.30 12.20 6 -4 13 47.00 12.50 6 -4 13 26.90 8.20 6 -4 13 27.50 8.10 7 -4 13 146.79 15.50 7 -4 13 142.59 18.90 7 -4 13 151.88 15.00 7 -4 13 112.69 16.50 8 -4 13 2.70 9.20 8 -4 13 -7.20 7.20 8 -4 13 -2.70 9.90 9 -4 13 72.59 16.30 9 -4 13 44.70 13.10 9 -4 13 45.10 11.50 10 -4 13 30.80 13.00 10 -4 13 43.60 14.40 10 -4 13 20.50 10.50 11 -4 13 14.00 13.30 11 -4 13 12.40 12.60 11 -4 13 23.50 11.80 9 3 -13 89.89 18.30 -9 -3 13 91.29 15.80 -9 -3 13 84.39 16.40 8 3 -13 83.49 17.00 -8 -3 13 74.89 13.60 -8 -3 13 47.70 14.00 -8 -3 13 63.59 18.50 7 3 -13 283.77 26.00 -7 -3 13 252.47 23.70 -7 -3 13 278.27 20.50 -7 -3 13 248.58 20.00 6 3 -13 118.59 20.10 -6 -3 13 138.89 20.20 -6 -3 13 100.79 14.50 -6 -3 13 116.39 15.30 5 3 -13 81.49 15.20 -5 -3 13 57.19 10.10 -5 -3 13 62.49 10.30 -5 -3 13 71.79 14.50 4 3 -13 1.70 8.60 -4 -3 13 -1.80 5.80 -4 -3 13 -5.80 5.50 -4 -3 13 -5.90 8.10 3 3 -13 62.99 12.80 -3 -3 13 48.70 7.40 -3 -3 13 54.69 11.50 -3 -3 13 34.00 7.20 2 3 -13 90.69 15.10 -2 -3 13 113.09 10.70 -2 -3 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14 2.30 7.90 -2 -10 14 0.60 10.00 1 10 -14 52.59 14.00 -1 -10 14 66.99 12.50 -1 -10 14 73.49 16.00 -1 -10 14 58.49 15.00 0 -10 14 48.40 11.50 0 -10 14 54.29 14.10 0 -10 14 44.30 13.80 1 -10 14 57.69 14.70 1 -10 14 52.59 14.50 1 -10 14 33.40 10.70 2 -10 14 143.29 21.80 2 -10 14 88.09 15.80 2 -10 14 129.49 17.80 3 -10 14 28.50 11.10 3 -10 14 49.40 14.80 3 -10 14 23.00 11.60 3 -10 14 27.40 12.50 4 -10 14 16.00 12.10 4 -10 14 23.80 12.30 4 -10 14 25.90 12.00 4 -10 14 12.70 10.40 5 -10 14 13.10 10.70 5 -10 14 20.20 12.30 5 -10 14 18.90 13.70 5 -10 14 1.80 10.90 6 -10 14 35.60 15.00 6 -10 14 23.00 12.10 6 -10 14 24.00 13.50 7 9 -14 130.79 20.80 -7 -9 14 143.69 22.80 -7 -9 14 179.48 20.50 6 9 -14 33.60 13.10 -6 -9 14 37.70 11.90 -6 -9 14 47.20 14.70 5 9 -14 -0.50 10.80 -5 -9 14 -5.50 10.90 -5 -9 14 4.60 8.50 -5 -9 14 3.70 10.60 4 9 -14 18.50 11.80 -4 -9 14 32.80 10.30 -4 -9 14 46.00 13.70 -4 -9 14 48.90 14.30 3 9 -14 -0.90 9.40 -3 -9 14 2.90 8.20 -3 -9 14 20.30 11.10 -3 -9 14 5.70 10.90 2 9 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34.50 12.30 -3 -8 14 51.49 10.80 -3 -8 14 46.30 13.90 -3 -8 14 47.80 13.40 2 8 -14 28.20 11.40 -2 -8 14 27.30 11.80 -2 -8 14 27.90 9.00 -2 -8 14 17.90 10.70 1 8 -14 -3.60 8.70 -1 -8 14 13.80 10.50 -1 -8 14 -2.20 9.40 -1 -8 14 1.90 7.00 0 8 -14 61.19 13.30 0 -8 14 44.80 12.30 0 -8 14 38.10 9.50 0 -8 14 48.00 13.20 1 -8 14 178.78 16.00 1 -8 14 174.98 21.10 1 -8 14 147.09 19.90 2 -8 14 148.29 16.00 2 -8 14 155.48 19.80 2 -8 14 153.28 20.20 3 -8 14 42.30 13.40 3 -8 14 55.89 12.90 3 -8 14 38.60 9.70 4 -8 14 226.18 21.90 4 -8 14 199.58 21.10 4 -8 14 204.48 18.40 4 -8 14 178.08 23.20 5 -8 14 56.19 12.70 5 -8 14 17.20 9.80 5 -8 14 27.00 12.90 5 -8 14 36.30 12.70 6 -8 14 16.50 13.00 6 -8 14 54.79 14.80 6 -8 14 24.30 11.20 6 -8 14 37.40 11.70 7 -8 14 67.39 13.80 7 -8 14 96.79 18.90 8 -8 14 42.40 13.00 8 -8 14 53.09 15.20 8 -8 14 37.10 16.20 7 7 -14 120.29 19.80 -7 -7 14 91.99 15.00 -7 -7 14 89.79 17.30 6 7 -14 71.69 16.40 -6 -7 14 84.09 16.40 -6 -7 14 69.09 13.00 5 7 -14 43.90 13.70 -5 -7 14 13.20 11.90 -5 -7 14 25.60 9.50 4 7 -14 22.20 12.00 -4 -7 14 20.50 8.40 -4 -7 14 7.50 11.10 3 7 -14 5.10 9.80 -3 -7 14 -4.00 9.70 -3 -7 14 -4.60 6.50 -3 -7 14 17.20 10.80 2 7 -14 9.00 9.80 -2 -7 14 1.10 9.50 -2 -7 14 1.10 9.80 -2 -7 14 4.30 7.10 1 7 -14 88.99 15.10 -1 -7 14 112.59 17.60 -1 -7 14 120.19 19.10 -1 -7 14 96.09 13.20 0 7 -14 482.85 28.10 0 -7 14 509.95 22.30 0 -7 14 459.15 27.50 0 -7 14 462.35 27.10 1 -7 14 234.18 21.10 1 -7 14 247.88 16.90 1 -7 14 264.97 22.10 2 -7 14 185.98 20.30 2 -7 14 178.18 15.40 2 -7 14 149.09 18.40 3 -7 14 1.00 9.70 3 -7 14 29.90 8.80 3 -7 14 30.50 10.90 4 -7 14 18.20 7.90 4 -7 14 -0.70 9.20 4 -7 14 -9.50 8.60 4 -7 14 11.40 9.60 5 -7 14 171.48 20.30 5 -7 14 185.78 19.30 5 -7 14 177.98 17.50 5 -7 14 147.39 20.60 6 -7 14 28.90 12.30 6 -7 14 8.50 9.00 6 -7 14 46.20 14.20 6 -7 14 13.40 10.10 7 -7 14 302.67 23.00 7 -7 14 298.07 25.20 7 -7 14 290.37 26.80 8 -7 14 247.48 26.60 8 -7 14 263.07 23.00 8 -7 14 271.87 25.70 8 6 -14 1.30 12.00 -8 -6 14 5.90 9.60 -8 -6 14 27.60 13.90 7 6 -14 17.10 11.90 -7 -6 14 5.40 8.40 -7 -6 14 11.80 11.90 6 6 -14 5.00 11.20 -6 -6 14 3.30 11.40 -6 -6 14 14.10 8.40 5 6 -14 167.38 22.00 -5 -6 14 133.49 16.00 -5 -6 14 147.49 20.50 4 6 -14 123.49 19.60 -4 -6 14 97.39 15.70 -4 -6 14 109.09 14.20 3 6 -14 123.99 19.30 -3 -6 14 128.09 14.10 -3 -6 14 149.79 19.60 2 6 -14 36.00 11.60 -2 -6 14 25.60 11.00 -2 -6 14 24.60 11.00 -2 -6 14 35.70 8.50 1 6 -14 84.69 14.60 -1 -6 14 60.09 12.80 -1 -6 14 105.89 12.50 -1 -6 14 124.89 18.20 0 6 -14 33.80 11.20 0 -6 14 21.00 7.40 0 -6 14 25.00 10.00 0 -6 14 24.00 10.80 -1 6 -14 97.29 16.30 1 -6 14 78.59 11.90 1 -6 14 73.59 13.20 1 -6 14 76.19 14.50 2 -6 14 114.79 17.20 2 -6 14 106.69 17.10 2 -6 14 80.29 11.90 3 -6 14 237.28 16.20 3 -6 14 252.67 20.60 3 -6 14 199.88 20.30 4 -6 14 91.79 13.90 4 -6 14 87.59 14.60 4 -6 14 103.19 13.60 4 -6 14 110.49 15.90 5 -6 14 276.57 19.00 5 -6 14 298.87 23.20 5 -6 14 271.57 20.80 5 -6 14 274.47 23.40 6 -6 14 150.28 19.90 6 -6 14 161.88 16.90 6 -6 14 141.29 17.30 6 -6 14 130.29 20.10 7 -6 14 234.08 22.60 7 -6 14 215.48 24.50 7 -6 14 277.07 20.60 8 -6 14 6.60 9.50 8 -6 14 6.50 11.80 8 -6 14 8.00 11.00 9 -6 14 93.79 18.00 9 -6 14 61.99 15.80 9 -6 14 99.49 15.80 8 5 -14 104.59 20.20 -8 -5 14 98.29 19.00 -8 -5 14 122.19 17.90 7 5 -14 114.59 18.90 -7 -5 14 165.08 22.20 -7 -5 14 137.39 17.50 6 5 -14 156.58 22.40 -6 -5 14 139.59 16.10 -6 -5 14 157.08 21.60 5 5 -14 52.49 13.90 -5 -5 14 75.49 11.60 -5 -5 14 51.19 13.70 4 5 -14 48.50 13.40 -4 -5 14 41.70 9.50 -4 -5 14 30.70 12.20 3 5 -14 25.30 11.10 -3 -5 14 9.80 10.00 -3 -5 14 28.00 8.00 2 5 -14 114.19 17.50 -2 -5 14 105.79 15.70 -2 -5 14 116.79 12.20 1 5 -14 77.19 14.20 -1 -5 14 58.49 12.00 -1 -5 14 70.49 11.00 -1 -5 14 71.09 13.60 0 5 -14 142.39 18.10 0 -5 14 146.49 17.90 0 -5 14 185.88 13.20 0 -5 14 172.18 18.80 -1 5 -14 389.66 24.60 1 -5 14 489.65 26.70 1 -5 14 414.06 24.30 1 -5 14 429.16 18.70 2 -5 14 193.18 19.10 2 -5 14 164.58 17.90 2 -5 14 168.78 13.10 3 -5 14 20.20 6.80 3 -5 14 26.30 9.80 3 -5 14 23.60 10.30 4 -5 14 33.80 10.00 4 -5 14 -9.90 8.00 4 -5 14 12.90 9.40 4 -5 14 16.30 7.10 5 -5 14 2.20 6.30 5 -5 14 0.30 9.20 5 -5 14 9.70 9.70 5 -5 14 8.40 8.20 6 -5 14 140.39 19.10 6 -5 14 130.69 15.30 6 -5 14 177.48 20.40 6 -5 14 121.49 15.70 7 -5 14 2.90 7.70 7 -5 14 22.30 12.00 7 -5 14 -2.80 10.40 8 -5 14 82.49 15.40 8 -5 14 71.29 15.60 8 -5 14 87.39 13.80 9 -5 14 132.79 18.10 9 -5 14 88.79 17.90 9 -5 14 106.09 18.30 10 -5 14 -0.40 13.70 10 -5 14 38.70 14.60 10 -5 14 17.30 11.20 8 4 -14 33.90 15.00 -8 -4 14 55.69 15.40 -8 -4 14 32.30 11.20 7 4 -14 77.69 16.90 -7 -4 14 94.19 14.10 -7 -4 14 47.30 13.60 6 4 -14 27.50 12.70 -6 -4 14 20.80 8.70 -6 -4 14 29.40 11.80 5 4 -14 -2.20 9.80 -5 -4 14 25.00 11.00 -5 -4 14 30.50 8.70 4 4 -14 -1.10 10.00 -4 -4 14 5.70 6.50 -4 -4 14 7.50 9.40 3 4 -14 60.69 13.20 -3 -4 14 115.89 17.60 -3 -4 14 84.39 11.80 2 4 -14 140.59 17.90 -2 -4 14 155.38 18.40 -2 -4 14 140.59 12.30 1 4 -14 310.07 22.40 -1 -4 14 320.07 22.30 -1 -4 14 257.77 14.60 0 4 -14 309.67 22.20 0 -4 14 302.97 21.60 0 -4 14 315.17 15.00 0 -4 14 342.17 22.00 -1 4 -14 12.10 8.80 1 -4 14 3.50 8.50 1 -4 14 12.20 5.60 1 -4 14 16.70 9.30 -2 4 -14 94.89 16.10 2 -4 14 87.19 10.10 2 -4 14 95.19 14.40 2 -4 14 92.79 14.50 3 -4 14 13.30 5.90 3 -4 14 0.20 6.90 3 -4 14 -4.80 7.60 4 -4 14 21.60 9.60 4 -4 14 19.80 6.60 4 -4 14 20.20 10.00 4 -4 14 24.50 8.50 5 -4 14 284.57 16.60 5 -4 14 263.47 22.00 5 -4 14 309.67 22.60 5 -4 14 277.87 18.80 6 -4 14 262.37 17.50 6 -4 14 243.18 22.00 6 -4 14 272.47 18.40 6 -4 14 246.38 21.40 7 -4 14 126.39 19.20 7 -4 14 126.79 19.10 7 -4 14 120.89 14.90 7 -4 14 109.29 17.10 8 -4 14 136.59 21.10 8 -4 14 118.29 18.40 8 -4 14 146.69 16.50 9 -4 14 -3.60 10.90 9 -4 14 0.50 8.90 9 -4 14 6.20 11.90 10 -4 14 21.20 12.70 10 -4 14 16.90 13.30 10 -4 14 22.60 10.60 8 3 -14 18.00 12.40 -8 -3 14 19.70 9.90 -8 -3 14 24.30 13.00 7 3 -14 37.70 14.60 -7 -3 14 30.30 10.00 -7 -3 14 23.90 11.70 6 3 -14 327.17 26.30 -6 -3 14 311.77 25.50 -6 -3 14 251.87 18.80 5 3 -14 55.89 14.00 -5 -3 14 56.79 13.50 -5 -3 14 52.59 10.10 4 3 -14 159.78 19.50 -4 -3 14 138.89 13.70 -4 -3 14 131.09 18.60 3 3 -14 49.40 12.50 -3 -3 14 37.40 7.90 -3 -3 14 53.59 12.80 2 3 -14 -0.90 8.00 -2 -3 14 2.00 5.30 -2 -3 14 8.00 8.60 1 3 -14 0.80 8.20 -1 -3 14 2.20 4.70 -1 -3 14 9.30 8.90 0 3 -14 173.88 18.20 0 -3 14 237.08 19.20 0 -3 14 231.08 18.90 0 -3 14 218.58 12.00 -1 3 -14 91.19 14.40 1 -3 14 107.59 15.30 1 -3 14 108.59 9.40 1 -3 14 110.69 16.10 -2 3 -14 83.29 13.40 2 -3 14 111.79 15.60 2 -3 14 107.29 15.00 2 -3 14 100.89 9.30 3 -3 14 271.97 13.50 3 -3 14 287.67 20.90 3 -3 14 271.17 18.00 4 -3 14 412.56 17.40 4 -3 14 407.26 23.80 4 -3 14 453.65 24.80 4 -3 14 482.25 22.60 5 -3 14 171.58 13.10 5 -3 14 130.99 17.60 5 -3 14 166.68 17.90 5 -3 14 160.98 14.90 6 -3 14 2.50 8.50 6 -3 14 9.30 6.40 6 -3 14 -4.70 6.50 6 -3 14 8.20 9.20 7 -3 14 63.99 14.00 7 -3 14 55.69 10.00 7 -3 14 63.39 13.10 7 -3 14 59.99 10.10 8 -3 14 73.99 11.80 8 -3 14 62.69 13.80 8 -3 14 61.39 14.40 9 -3 14 36.00 13.40 9 -3 14 38.00 10.20 9 -3 14 10.50 11.80 10 -3 14 114.09 18.70 10 -3 14 162.88 18.70 10 -3 14 140.89 22.10 11 -3 14 32.20 13.80 11 -3 14 38.20 12.20 11 -3 14 39.60 16.10 8 2 -14 96.79 17.70 -8 -2 14 80.69 17.10 -8 -2 14 101.59 15.30 7 2 -14 43.20 14.00 -7 -2 14 48.90 11.20 -7 -2 14 51.49 12.20 -7 -2 14 37.20 13.20 6 2 -14 217.48 23.90 -6 -2 14 168.38 17.60 -6 -2 14 191.48 21.70 -6 -2 14 178.38 16.90 5 2 -14 5.10 9.90 -5 -2 14 6.90 7.00 -5 -2 14 4.20 7.40 -5 -2 14 -4.00 9.20 4 2 -14 -5.20 8.70 -4 -2 14 -2.40 5.60 -4 -2 14 4.50 9.70 -4 -2 14 4.00 6.60 3 2 -14 34.50 11.20 -3 -2 14 5.50 9.50 -3 -2 14 24.70 6.80 -3 -2 14 19.20 6.60 2 2 -14 19.60 9.90 -2 -2 14 32.90 6.70 -2 -2 14 17.70 9.80 -2 -2 14 29.50 6.30 1 2 -14 499.75 26.30 -1 -2 14 483.95 17.70 -1 -2 14 518.15 26.00 -1 -2 14 458.65 16.60 0 2 -14 921.21 35.90 0 -2 14 1002.00 25.10 0 -2 14 1020.60 36.40 0 -2 14 1005.50 26.40 -1 2 -14 40.70 10.90 1 -2 14 46.20 10.60 1 -2 14 33.20 10.20 1 -2 14 46.70 6.40 1 -2 14 49.00 6.90 -2 2 -14 125.89 16.30 2 -2 14 98.09 8.10 2 -2 14 83.79 8.30 2 -2 14 82.29 12.50 2 -2 14 103.89 13.90 3 -2 14 78.89 8.20 3 -2 14 117.79 13.90 3 -2 14 91.19 14.70 4 -2 14 -12.60 6.80 4 -2 14 4.60 6.10 4 -2 14 -1.20 7.30 4 -2 14 -0.80 4.30 5 -2 14 41.90 10.70 5 -2 14 48.00 9.30 5 -2 14 59.29 12.40 5 -2 14 81.29 9.90 6 -2 14 492.85 26.00 6 -2 14 474.45 26.30 6 -2 14 481.75 19.90 6 -2 14 509.45 21.30 7 -2 14 95.09 12.30 7 -2 14 116.19 12.80 7 -2 14 125.59 17.10 7 -2 14 114.79 17.10 8 -2 14 6.10 9.80 8 -2 14 31.00 11.30 8 -2 14 24.60 8.50 9 -2 14 73.59 15.10 9 -2 14 104.49 16.80 9 -2 14 87.49 13.10 10 -2 14 17.00 12.10 10 -2 14 26.00 12.50 10 -2 14 9.90 9.00 11 -2 14 5.10 9.40 11 -2 14 -7.30 10.60 11 -2 14 -10.30 11.30 8 1 -14 95.39 18.40 -8 -1 14 74.29 13.70 -8 -1 14 42.90 15.30 -8 -1 14 35.60 12.30 7 1 -14 23.60 12.70 -7 -1 14 2.70 8.40 -7 -1 14 29.50 12.30 -7 -1 14 0.10 10.00 6 1 -14 19.10 11.40 -6 -1 14 1.40 9.80 -6 -1 14 6.80 7.90 -6 -1 14 0.70 8.60 5 1 -14 191.18 21.80 -5 -1 14 168.68 15.10 -5 -1 14 174.98 16.90 -5 -1 14 168.08 20.50 4 1 -14 222.38 21.70 -4 -1 14 222.08 21.50 -4 -1 14 195.18 14.50 -4 -1 14 209.58 15.90 3 1 -14 329.77 23.80 -3 -1 14 287.97 15.10 -3 -1 14 268.47 22.00 -3 -1 14 275.17 16.70 2 1 -14 174.38 18.10 -2 -1 14 158.78 17.90 -2 -1 14 152.98 10.70 -2 -1 14 166.38 12.70 1 1 -14 115.89 16.00 -1 -1 14 106.39 8.80 -1 -1 14 99.59 8.90 -1 -1 14 94.79 10.10 -1 -1 14 109.99 15.50 0 1 -14 13.40 8.90 0 -1 14 -1.50 3.40 0 -1 14 -3.80 4.20 0 -1 14 -3.90 4.00 0 -1 14 1.00 7.60 -1 1 -14 53.99 11.90 1 -1 14 68.09 6.20 1 -1 14 96.79 14.60 1 -1 14 71.09 8.70 1 -1 14 55.99 11.00 -2 1 -14 546.15 26.00 2 -1 14 498.55 24.50 2 -1 14 470.15 13.90 2 -1 14 478.95 17.40 2 -1 14 540.05 23.60 -3 1 -14 347.47 21.60 3 -1 14 354.26 21.20 3 -1 14 362.06 12.30 3 -1 14 396.86 19.80 4 -1 14 379.66 22.40 4 -1 14 419.26 14.40 4 -1 14 391.26 21.90 4 -1 14 401.26 19.70 5 -1 14 282.27 19.60 5 -1 14 245.18 19.00 5 -1 14 248.68 15.50 5 -1 14 244.88 12.60 6 -1 14 27.10 10.00 6 -1 14 42.50 7.90 6 -1 14 44.40 10.60 6 -1 14 48.80 7.60 7 -1 14 13.10 6.50 7 -1 14 14.80 9.20 7 -1 14 24.70 10.00 7 -1 14 6.00 6.20 8 -1 14 3.20 6.60 8 -1 14 7.60 9.80 8 -1 14 2.40 9.60 9 -1 14 96.09 14.10 9 -1 14 79.09 14.70 9 -1 14 79.89 14.80 10 -1 14 417.36 23.60 10 -1 14 435.36 28.20 10 -1 14 417.36 28.30 11 -1 14 126.79 19.70 11 -1 14 167.78 18.40 11 -1 14 139.19 22.50 11 -1 14 202.58 22.90 12 -1 14 124.99 19.30 12 -1 14 136.19 20.10 12 -1 14 161.38 23.90 12 -1 14 139.79 20.30 8 0 -14 72.69 17.50 -8 0 14 102.89 18.60 -8 0 14 111.99 15.70 -8 0 14 104.59 17.10 7 0 -14 156.98 21.70 -7 0 14 193.18 22.60 -7 0 14 157.28 17.20 -7 0 14 145.99 19.50 6 0 -14 55.69 14.80 -6 0 14 73.59 11.60 -6 0 14 35.90 11.20 -6 0 14 66.59 14.20 5 0 -14 89.99 15.80 -5 0 14 118.49 18.80 -5 0 14 89.49 12.80 -5 0 14 103.79 15.80 4 0 -14 3.90 9.20 -4 0 14 4.60 6.10 -4 0 14 10.80 10.50 -4 0 14 5.30 7.40 3 0 -14 11.40 9.10 -3 0 14 5.20 8.90 -3 0 14 7.30 5.50 -3 0 14 10.20 6.80 2 0 -14 81.29 13.40 -2 0 14 98.69 9.20 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16.60 9 0 20 49.99 14.80 9 0 20 70.99 16.80 2 -1 -20 17.00 12.50 -2 1 20 20.70 13.00 1 -1 -20 -0.60 10.60 -1 1 20 3.50 10.90 0 -1 -20 237.28 24.90 0 1 20 186.38 23.10 -1 -1 -20 47.40 13.60 1 1 20 50.99 13.80 1 1 20 50.79 13.50 -2 -1 -20 94.19 16.60 2 1 20 123.59 18.40 2 1 20 103.19 16.20 -3 -1 -20 85.29 15.50 3 1 20 64.19 13.50 3 1 20 47.90 13.30 3 1 20 55.59 13.20 4 1 20 6.00 8.50 4 1 20 18.90 11.40 4 1 20 25.90 11.10 5 1 20 11.70 10.20 5 1 20 2.70 10.00 5 1 20 -5.60 8.30 6 1 20 12.40 10.00 6 1 20 0.30 9.90 7 1 20 19.20 10.90 7 1 20 37.90 13.40 8 1 20 3.20 10.90 8 1 20 33.90 12.80 9 1 20 8.90 11.40 9 1 20 11.40 12.20 9 1 20 9.50 12.80 2 -2 -20 170.58 24.00 -2 2 20 201.38 26.00 1 -2 -20 134.79 21.10 -1 2 20 130.59 21.20 0 -2 -20 118.19 19.90 0 2 20 96.29 16.80 -1 -2 -20 2.60 10.60 1 2 20 10.10 10.40 1 2 20 9.80 9.80 -2 -2 -20 29.10 12.00 2 2 20 3.40 9.70 2 2 20 38.50 10.00 2 2 20 13.40 9.70 -3 -2 -20 44.20 13.10 3 2 20 42.70 11.50 3 2 20 52.39 12.90 3 2 20 48.60 12.10 3 2 20 55.09 13.20 4 2 20 7.30 9.30 4 2 20 34.60 10.10 4 2 20 24.70 10.90 4 2 20 32.80 10.80 5 2 20 151.08 19.10 5 2 20 180.18 20.30 5 2 20 151.08 16.90 6 2 20 200.28 21.30 6 2 20 198.28 21.20 6 2 20 213.58 20.70 7 2 20 56.79 13.40 7 2 20 74.49 14.00 7 2 20 57.79 14.60 8 2 20 228.88 22.00 8 2 20 216.38 23.60 8 2 20 209.98 22.80 9 2 20 196.68 23.10 9 2 20 140.09 20.60 9 2 20 112.39 18.80 2 -3 -20 32.80 13.70 -2 3 20 37.70 14.30 1 -3 -20 -6.90 9.60 -1 3 20 12.90 11.70 0 -3 -20 50.69 13.90 0 3 20 60.09 14.60 -1 -3 -20 53.99 13.90 1 3 20 62.49 14.30 1 3 20 48.90 13.30 -2 -3 -20 16.10 11.40 2 3 20 31.90 9.90 2 3 20 32.20 11.50 2 3 20 35.80 9.70 2 3 20 42.50 11.70 -3 -3 -20 71.29 14.70 3 3 20 65.69 12.50 3 3 20 77.99 12.20 3 3 20 86.69 14.40 3 3 20 77.49 11.90 3 3 20 75.89 13.60 3 3 20 77.19 12.70 4 3 20 60.59 12.50 4 3 20 49.90 11.90 4 3 20 69.89 11.90 4 3 20 68.09 11.60 4 3 20 76.39 13.30 4 3 20 56.59 12.00 5 3 20 229.68 20.90 5 3 20 260.47 20.50 5 3 20 234.88 20.70 5 3 20 244.68 18.60 5 3 20 235.58 21.50 6 3 20 34.00 12.20 6 3 20 64.19 13.30 6 3 20 47.70 12.10 7 3 20 1.90 8.70 7 3 20 -7.90 9.60 7 3 20 11.40 10.50 8 3 20 3.30 9.20 8 3 20 4.40 10.20 8 3 20 2.00 10.90 9 3 20 11.00 12.10 9 3 20 -13.10 14.10 9 3 20 2.20 11.10 10 3 20 4.90 11.40 10 3 20 23.50 13.60 1 -4 -20 -1.70 9.90 -1 4 20 24.20 10.50 -1 4 20 23.90 12.50 0 -4 -20 59.29 14.70 0 4 20 56.89 14.30 0 4 20 65.89 12.80 -1 -4 -20 91.79 16.60 1 4 20 97.29 16.50 1 4 20 92.59 14.10 2 4 20 112.89 15.20 2 4 20 115.69 16.80 2 4 20 105.59 16.30 2 4 20 90.69 14.60 -3 -4 -20 50.89 13.40 3 4 20 39.90 10.70 3 4 20 35.80 11.30 3 4 20 41.40 10.30 3 4 20 31.50 9.40 3 4 20 41.40 11.40 3 4 20 36.80 10.60 4 4 20 -3.40 8.00 4 4 20 -0.40 7.40 4 4 20 11.80 8.40 4 4 20 10.50 7.90 4 4 20 11.80 8.50 4 4 20 2.70 8.50 5 4 20 0.00 8.60 5 4 20 0.80 7.70 5 4 20 -13.80 7.00 5 4 20 6.10 8.70 5 4 20 -5.30 7.00 5 4 20 -16.00 7.20 6 4 20 17.40 10.40 6 4 20 45.20 12.30 6 4 20 32.80 10.70 7 4 20 33.70 10.90 7 4 20 36.20 12.30 7 4 20 57.59 13.40 8 4 20 14.20 11.60 8 4 20 -0.70 9.60 9 4 20 47.70 14.00 9 4 20 11.10 11.70 10 4 20 11.90 11.80 10 4 20 11.40 11.30 1 -5 -20 125.69 20.30 -1 5 20 101.29 18.40 -1 5 20 142.59 19.50 0 -5 -20 -3.30 9.80 0 5 20 -6.40 9.80 0 5 20 18.90 9.90 -1 -5 -20 -2.60 9.70 1 5 20 5.60 8.30 1 5 20 2.90 9.70 -2 -5 -20 -4.40 9.60 2 5 20 3.80 8.60 2 5 20 9.40 8.70 -3 -5 -20 43.00 12.60 3 5 20 30.10 10.60 3 5 20 50.59 11.40 3 5 20 53.39 14.40 3 5 20 30.70 9.40 3 5 20 33.40 9.70 3 5 20 45.30 10.80 4 5 20 124.39 16.20 4 5 20 106.49 15.80 4 5 20 146.59 17.60 4 5 20 104.59 14.60 4 5 20 135.29 16.50 4 5 20 131.59 17.60 5 5 20 112.39 17.10 5 5 20 103.59 14.70 5 5 20 138.39 16.80 5 5 20 121.19 17.30 5 5 20 127.09 17.50 5 5 20 109.49 16.00 6 5 20 320.57 22.00 6 5 20 319.37 23.50 6 5 20 302.17 23.50 6 5 20 316.27 23.10 7 5 20 57.39 13.40 8 5 20 26.90 11.30 8 5 20 18.60 11.80 9 5 20 17.30 11.90 9 5 20 30.10 12.70 10 5 20 143.49 22.60 10 5 20 150.58 21.40 1 -6 -20 0.50 10.10 -1 6 20 -7.80 8.70 0 -6 -20 252.47 23.60 0 6 20 220.58 22.00 -1 -6 -20 252.77 23.20 1 6 20 236.08 21.70 -2 -6 -20 396.46 26.70 2 6 20 413.56 27.10 2 6 20 413.86 25.50 -3 -6 -20 86.59 15.10 3 6 20 80.39 13.80 3 6 20 96.49 15.30 3 6 20 83.49 14.10 3 6 20 87.29 13.90 4 6 20 7.70 8.80 4 6 20 7.70 8.80 4 6 20 -2.70 9.80 4 6 20 21.30 8.90 4 6 20 9.80 8.40 4 6 20 13.30 9.70 5 6 20 20.70 10.30 5 6 20 23.40 9.50 5 6 20 19.50 9.80 5 6 20 20.20 10.10 5 6 20 32.50 11.30 6 6 20 18.90 9.50 6 6 20 21.10 10.70 6 6 20 12.50 10.60 7 6 20 -2.40 8.70 7 6 20 13.70 10.40 7 6 20 1.00 8.80 8 6 20 29.40 11.60 8 6 20 41.10 13.00 9 6 20 57.89 14.50 9 6 20 21.00 11.90 10 6 20 14.40 12.40 10 6 20 23.00 12.80 0 -7 -20 88.99 15.90 0 7 20 145.69 20.00 -1 -7 -20 45.10 13.10 1 7 20 47.50 13.20 -2 -7 -20 28.20 12.10 2 7 20 25.40 11.50 2 7 20 29.50 13.30 -3 -7 -20 2.60 9.70 3 7 20 10.60 8.50 3 7 20 -0.10 8.70 4 7 20 45.60 11.30 4 7 20 11.30 9.30 4 7 20 17.80 9.30 4 7 20 19.30 9.70 5 7 20 107.39 16.10 5 7 20 144.49 18.10 5 7 20 126.09 17.20 5 7 20 134.19 18.00 6 7 20 27.00 11.20 6 7 20 -0.80 8.60 6 7 20 9.00 8.30 6 7 20 7.80 9.00 7 7 20 92.89 15.70 7 7 20 69.09 13.10 7 7 20 88.09 15.30 8 7 20 101.29 15.80 8 7 20 92.89 16.00 8 7 20 78.19 14.80 9 7 20 11.40 11.20 9 7 20 2.50 9.70 9 7 20 9.40 10.30 10 7 20 73.59 16.40 10 7 20 27.80 12.70 1 8 20 149.79 20.80 -2 -8 -20 196.68 22.30 2 8 20 216.38 19.70 2 8 20 145.89 20.00 -3 -8 -20 5.50 9.40 3 8 20 12.70 9.40 3 8 20 22.40 10.70 4 8 20 5.80 9.40 4 8 20 6.50 9.40 5 8 20 13.70 12.10 5 8 20 18.20 10.40 5 8 20 21.80 11.30 5 8 20 27.80 10.70 6 8 20 -4.60 8.80 6 8 20 0.60 9.40 6 8 20 -2.60 8.90 7 8 20 0.20 9.20 7 8 20 1.70 10.10 8 8 20 33.20 11.20 8 8 20 27.60 12.90 8 8 20 51.29 14.40 9 8 20 168.68 22.20 9 8 20 150.38 20.20 9 8 20 229.68 23.70 10 8 20 320.67 26.80 10 8 20 264.87 25.40 10 8 20 287.77 24.60 1 9 20 24.60 12.20 2 9 20 26.20 11.70 2 9 20 48.50 12.30 3 9 20 1.30 9.90 3 9 20 5.70 9.20 4 9 20 1.40 9.50 4 9 20 29.30 11.70 5 9 20 19.50 10.00 5 9 20 23.50 10.80 5 9 20 26.30 11.90 6 9 20 76.19 13.90 6 9 20 51.69 13.70 6 9 20 79.19 15.10 7 9 20 141.39 19.20 7 9 20 220.48 22.60 8 9 20 146.69 20.70 8 9 20 147.59 20.50 9 9 20 24.00 12.30 9 9 20 17.60 11.70 10 9 20 12.50 11.30 10 9 20 2.70 11.10 10 9 20 6.90 11.30 2 10 20 9.50 10.70 2 10 20 21.20 11.40 3 10 20 23.70 11.50 3 10 20 18.60 10.90 4 10 20 59.59 13.70 4 10 20 47.40 13.60 5 10 20 83.59 15.90 5 10 20 75.69 14.80 6 10 20 41.70 12.40 6 10 20 42.40 13.70 6 10 20 35.90 12.30 7 10 20 -7.80 8.90 7 10 20 19.10 11.10 8 10 20 14.50 11.50 8 10 20 36.10 13.10 9 10 20 140.79 20.30 9 10 20 104.29 18.10 4 11 20 4.20 10.70 4 11 20 6.90 10.90 5 11 20 67.59 14.80 5 11 20 56.79 14.60 6 11 20 6.70 9.30 6 11 20 2.90 10.70 6 11 20 -6.60 9.40 7 11 20 100.59 15.80 7 11 20 92.19 16.10 7 11 20 109.49 17.80 8 11 20 97.69 16.60 8 11 20 74.39 15.70 -1 3 -21 43.60 14.20 1 -3 21 43.10 14.50 2 -3 21 6.80 10.50 2 -3 21 -14.10 9.90 3 -3 21 62.79 16.10 3 -3 21 88.09 17.60 3 -3 21 79.59 15.70 4 -3 21 24.80 12.80 4 -3 21 30.40 12.50 4 -3 21 47.50 15.40 0 2 -21 142.99 23.30 -1 2 -21 163.58 23.80 1 -2 21 158.58 23.50 1 -2 21 161.78 22.00 -2 2 -21 42.60 14.20 2 -2 21 35.90 13.20 2 -2 21 27.00 13.40 3 -2 21 1.70 10.50 3 -2 21 -8.40 9.10 3 -2 21 14.90 11.90 4 -2 21 26.30 13.50 4 -2 21 18.90 11.30 4 -2 21 17.50 13.10 5 -2 21 27.30 13.00 5 -2 21 29.60 14.10 0 1 -21 15.00 12.60 0 -1 21 -2.20 11.00 0 -1 21 -6.00 10.90 -1 1 -21 2.80 10.80 1 -1 21 -1.40 11.60 1 -1 21 17.10 12.30 -2 1 -21 41.90 14.60 2 -1 21 45.20 13.10 2 -1 21 74.89 16.20 3 -1 21 43.70 14.00 3 -1 21 21.50 11.90 3 -1 21 40.00 13.70 4 -1 21 96.99 17.00 4 -1 21 95.29 17.00 4 -1 21 114.99 18.50 5 -1 21 66.19 14.90 5 -1 21 62.49 15.90 6 -1 21 19.50 13.50 6 -1 21 42.50 14.40 0 0 -21 153.18 22.90 0 0 21 192.28 25.00 0 0 21 155.18 22.90 -1 0 -21 119.09 19.40 1 0 21 123.49 18.80 1 0 21 147.89 21.20 -2 0 -21 43.30 14.20 2 0 21 50.99 13.70 2 0 21 60.09 15.30 3 0 21 22.40 11.40 3 0 21 19.10 10.30 3 0 21 21.60 12.10 4 0 21 46.90 13.50 4 0 21 47.30 13.80 4 0 21 29.80 11.60 5 0 21 -8.00 10.30 5 0 21 6.90 10.60 6 0 21 44.70 14.30 6 0 21 51.99 14.90 7 0 21 57.49 14.60 7 0 21 66.79 16.20 0 -1 -21 66.19 15.90 0 1 21 51.09 15.30 0 1 21 69.39 15.70 -1 -1 -21 8.50 12.40 1 1 21 -4.70 10.50 1 1 21 6.90 10.60 -2 -1 -21 -4.00 9.50 2 1 21 6.60 10.60 2 1 21 13.60 10.90 3 1 21 38.30 12.10 3 1 21 16.00 10.80 3 1 21 19.60 10.70 4 1 21 123.49 19.90 4 1 21 132.19 18.00 4 1 21 164.28 21.00 5 1 21 245.68 23.50 5 1 21 221.08 23.10 6 1 21 113.09 17.50 6 1 21 74.79 15.60 7 1 21 150.98 20.90 7 1 21 130.29 19.10 8 1 21 115.59 17.80 8 1 21 147.89 22.90 8 1 21 155.78 22.20 0 -2 -21 132.69 22.50 0 2 21 135.29 19.90 -1 -2 -21 51.49 15.20 1 2 21 44.90 13.40 1 2 21 44.90 13.10 -2 -2 -21 90.89 17.30 2 2 21 88.59 16.10 2 2 21 95.69 15.80 -3 -2 -21 159.58 22.20 3 2 21 179.58 19.80 3 2 21 262.87 22.60 3 2 21 156.38 19.70 3 2 21 211.88 19.60 4 2 21 44.00 12.00 4 2 21 49.70 12.70 4 2 21 65.69 13.50 4 2 21 52.59 12.70 5 2 21 20.30 11.00 5 2 21 -3.50 8.90 5 2 21 -8.90 8.40 6 2 21 4.50 10.30 6 2 21 12.60 10.40 6 2 21 1.40 10.30 7 2 21 40.00 13.30 7 2 21 54.39 13.40 7 2 21 29.40 12.90 8 2 21 33.00 12.40 8 2 21 41.00 13.60 8 2 21 18.10 12.40 0 -3 -21 86.69 17.30 0 3 21 64.59 16.10 -1 -3 -21 3.00 10.50 1 3 21 -1.40 9.40 1 3 21 9.10 10.20 -2 -3 -21 1.10 10.40 2 3 21 7.80 8.30 2 3 21 8.80 9.00 2 3 21 2.30 9.60 -3 -3 -21 1.40 9.90 3 3 21 12.00 9.90 3 3 21 11.00 8.90 3 3 21 23.50 10.50 3 3 21 4.70 8.50 4 3 21 26.60 9.70 4 3 21 16.30 10.30 4 3 21 22.90 10.60 4 3 21 44.10 12.00 4 3 21 27.50 10.60 5 3 21 22.70 11.60 5 3 21 7.20 9.70 5 3 21 20.90 9.60 5 3 21 28.40 11.50 6 3 21 123.49 17.80 6 3 21 107.59 16.90 6 3 21 109.69 17.40 7 3 21 103.59 17.20 7 3 21 117.29 17.90 7 3 21 145.39 19.30 8 3 21 148.29 20.90 8 3 21 116.29 19.00 8 3 21 145.19 21.20 9 3 21 37.40 13.80 9 3 21 15.00 12.90 0 -4 -21 45.70 14.50 0 4 21 52.19 14.50 -1 -4 -21 -1.80 10.70 1 4 21 17.80 12.00 -2 -4 -21 57.99 14.90 2 4 21 55.79 13.30 2 4 21 47.30 12.00 2 4 21 53.09 17.80 -3 -4 -21 143.79 20.70 3 4 21 118.49 18.00 3 4 21 124.29 16.80 3 4 21 131.79 19.00 3 4 21 151.48 18.50 4 4 21 198.68 19.40 4 4 21 176.68 19.10 4 4 21 179.38 17.90 4 4 21 170.58 19.80 4 4 21 180.68 19.00 4 4 21 203.58 20.30 5 4 21 168.18 19.40 5 4 21 175.68 19.40 5 4 21 172.48 18.60 5 4 21 180.98 18.80 5 4 21 196.38 20.60 6 4 21 39.80 12.20 6 4 21 41.30 11.40 6 4 21 9.40 10.30 6 4 21 28.20 10.80 6 4 21 13.30 9.90 7 4 21 16.70 11.10 7 4 21 2.20 10.30 8 4 21 12.50 11.60 8 4 21 2.00 10.60 9 4 21 141.89 22.30 9 4 21 144.79 21.10 -1 -5 -21 69.39 15.50 1 5 21 52.59 13.90 1 5 21 48.30 12.40 -2 -5 -21 -10.80 9.50 2 5 21 15.30 9.90 2 5 21 12.60 8.70 2 5 21 18.50 10.90 -3 -5 -21 12.30 10.70 3 5 21 -0.10 8.30 3 5 21 5.80 7.90 3 5 21 11.80 10.00 4 5 21 0.30 8.40 4 5 21 13.30 9.80 4 5 21 15.00 8.60 4 5 21 11.30 8.40 4 5 21 10.00 9.40 4 5 21 17.20 9.20 5 5 21 -0.90 8.30 5 5 21 0.10 8.60 5 5 21 3.80 8.70 5 5 21 7.60 8.50 5 5 21 7.60 8.60 6 5 21 -2.00 8.90 6 5 21 17.40 10.80 6 5 21 5.00 8.00 6 5 21 -1.30 8.80 7 5 21 45.20 13.00 7 5 21 72.09 14.90 7 5 21 36.30 12.40 8 5 21 54.79 14.80 8 5 21 52.59 14.30 9 5 21 33.20 13.90 9 5 21 48.60 15.00 -1 -6 -21 6.70 10.60 1 6 21 1.90 9.60 1 6 21 17.60 10.10 -2 -6 -21 34.90 13.00 2 6 21 17.00 10.50 2 6 21 16.00 9.80 -3 -6 -21 48.40 12.90 3 6 21 56.99 12.50 3 6 21 49.80 12.20 3 6 21 54.49 12.60 4 6 21 148.09 17.30 4 6 21 140.09 18.70 4 6 21 157.88 17.70 5 6 21 100.59 14.70 5 6 21 109.69 17.40 5 6 21 70.49 13.70 5 6 21 65.39 15.80 6 6 21 52.39 11.90 6 6 21 61.89 13.90 6 6 21 54.09 12.30 6 6 21 53.49 13.20 7 6 21 36.10 12.10 7 6 21 37.30 12.30 7 6 21 40.70 13.20 8 6 21 8.30 10.70 8 6 21 3.40 10.60 8 6 21 -4.70 8.90 9 6 21 0.80 10.80 9 6 21 5.70 11.20 -2 -7 -21 109.79 17.10 2 7 21 80.29 14.90 -3 -7 -21 43.10 12.60 3 7 21 69.59 14.20 3 7 21 38.00 13.70 3 7 21 53.19 12.80 4 7 21 48.80 12.50 4 7 21 46.10 11.80 4 7 21 56.59 12.90 5 7 21 52.19 12.30 5 7 21 30.50 11.30 5 7 21 31.60 11.50 6 7 21 -11.30 8.20 6 7 21 -10.70 8.10 6 7 21 9.90 10.20 7 7 21 56.99 14.00 7 7 21 55.29 13.50 7 7 21 72.49 13.70 8 7 21 113.09 16.80 8 7 21 77.49 15.70 8 7 21 75.39 15.30 9 7 21 230.38 24.40 9 7 21 198.08 22.30 9 7 21 195.38 22.60 2 8 21 13.50 11.50 3 8 21 10.80 9.80 3 8 21 16.00 10.80 4 8 21 29.40 11.30 4 8 21 34.70 12.00 4 8 21 12.80 10.70 5 8 21 144.69 19.90 5 8 21 111.89 16.60 6 8 21 110.69 16.80 6 8 21 86.59 15.10 6 8 21 80.09 14.40 7 8 21 23.80 12.00 7 8 21 30.10 12.00 8 8 21 31.60 13.20 8 8 21 64.19 15.20 9 8 21 38.70 13.80 9 8 21 34.10 12.40 9 8 21 17.20 12.10 4 9 21 160.78 20.40 4 9 21 159.08 21.40 5 9 21 72.69 14.70 5 9 21 89.49 15.90 6 9 21 -2.80 9.10 6 9 21 -4.20 9.50 6 9 21 6.80 10.60 7 9 21 17.50 12.00 7 9 21 16.50 11.70 7 9 21 9.70 10.50 8 9 21 107.69 17.40 8 9 21 97.59 16.80 5 10 21 25.00 12.20 5 10 21 40.60 13.40 6 10 21 37.00 13.00 6 10 21 26.10 17.90 6 10 21 17.00 11.90 7 10 21 70.99 15.10 7 10 21 101.49 17.00 7 10 21 59.69 14.30 3 0 22 48.90 13.90 3 0 22 33.70 12.30 3 0 22 15.90 12.50 4 0 22 184.08 23.20 4 0 22 189.18 22.30 4 0 22 200.58 23.00 -2 -1 -22 246.98 26.10 2 1 22 191.58 23.00 2 1 22 166.08 22.70 3 1 22 17.60 10.90 3 1 22 34.20 11.70 3 1 22 43.30 13.80 4 1 22 68.39 15.40 4 1 22 72.99 14.90 4 1 22 40.30 12.30 5 1 22 28.00 13.10 5 1 22 26.60 13.00 -2 -2 -22 -3.50 10.00 2 2 22 2.10 10.80 2 2 22 0.70 8.70 2 2 22 5.70 10.60 3 2 22 43.20 12.40 3 2 22 30.80 12.20 3 2 22 32.20 12.40 4 2 22 95.79 16.00 4 2 22 97.29 16.20 4 2 22 72.29 15.30 4 2 22 96.99 15.70 5 2 22 183.98 21.30 5 2 22 172.28 22.20 5 2 22 147.29 20.80 6 2 22 23.80 12.00 6 2 22 41.50 13.20 6 2 22 13.40 11.60 -2 -3 -22 3.30 11.10 2 3 22 27.00 11.90 2 3 22 15.20 10.60 2 3 22 21.50 10.20 3 3 22 142.09 19.70 3 3 22 135.99 19.90 3 3 22 127.49 18.10 4 3 22 83.19 15.10 4 3 22 98.09 15.80 4 3 22 70.79 14.00 4 3 22 64.69 14.40 5 3 22 2.00 9.80 5 3 22 9.00 10.70 5 3 22 4.20 9.80 5 3 22 -13.20 7.40 6 3 22 9.90 10.80 6 3 22 16.10 10.10 6 3 22 12.40 11.10 6 3 22 10.30 10.20 7 3 22 52.69 16.60 7 3 22 29.80 13.40 7 3 22 14.90 12.40 -2 -4 -22 6.90 11.30 2 4 22 8.20 9.80 3 4 22 -2.60 8.70 3 4 22 1.60 8.90 4 4 22 79.99 14.80 4 4 22 71.89 17.50 4 4 22 77.69 14.10 4 4 22 73.19 14.30 5 4 22 23.80 10.00 5 4 22 35.00 11.70 5 4 22 43.30 12.70 5 4 22 45.40 13.40 6 4 22 2.20 8.90 6 4 22 14.10 11.00 6 4 22 20.90 11.10 7 4 22 116.09 17.60 7 4 22 124.89 19.90 -3 -5 -22 20.70 11.50 3 5 22 23.80 11.60 3 5 22 37.40 11.90 4 5 22 151.18 24.80 4 5 22 137.19 19.30 5 5 22 167.78 20.10 5 5 22 130.19 18.20 5 5 22 240.88 20.70 6 5 22 108.09 16.70 6 5 22 81.39 14.80 6 5 22 109.19 16.70 7 5 22 16.00 10.80 7 5 22 25.00 12.00 7 5 22 5.10 10.10 4 6 22 17.10 10.00 4 6 22 2.10 10.00 5 6 22 24.50 10.80 5 6 22 38.10 11.80 5 6 22 9.70 8.80 6 6 22 84.09 14.30 6 6 22 95.79 15.90 6 6 22 78.69 15.00 7 6 22 48.00 14.10 7 6 22 62.29 12.40 7 6 22 98.79 17.20 7 6 22 59.39 14.10 5 7 22 173.18 19.80 5 7 22 164.48 19.40 6 7 22 73.79 14.60 6 7 22 99.19 15.80 6 7 22 58.59 14.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 59222 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zr1 Zr 0.43244(2) 0.79138(2) 0.71691(2) 0.00860(4) Uani 1 1 d . . . . . O2 O 0.27304(10) 0.95070(7) 0.73398(7) 0.01280(19) Uani 1 1 d . . . . . O1 O 0.64059(10) 0.66112(7) 0.70232(7) 0.01183(19) Uani 1 1 d . . . . . N3 N 0.21826(12) 0.81340(9) 0.80290(8) 0.0116(2) Uani 1 1 d . . . . . N2 N 0.44470(12) 0.63132(9) 0.77271(8) 0.0108(2) Uani 1 1 d . . . . . N1 N 0.43175(12) 0.79183(9) 0.58153(8) 0.0111(2) Uani 1 1 d . . . . . N5 N 0.03757(12) 0.98580(9) 0.79725(8) 0.0117(2) Uani 1 1 d . . . . . N4 N 0.66105(12) 0.48721(9) 0.72365(8) 0.0113(2) Uani 1 1 d . . . . . C12 C 0.57867(15) 0.76803(11) 0.42349(10) 0.0146(3) Uani 1 1 d . . . . . C4 C 0.62524(14) 0.86656(10) 0.68918(9) 0.0117(2) Uani 1 1 d . . . . . H4 H 0.724320 0.816094 0.678042 0.014 Uiso 1 1 calc R U . . . C25 C 0.17103(14) 0.91654(10) 0.77983(9) 0.0103(2) Uani 1 1 d . . . . . C18 C 0.30585(14) 0.78771(10) 0.57104(9) 0.0117(2) Uani 1 1 d . . . . . C3 C 0.56904(14) 0.90333(10) 0.61667(9) 0.0117(2) Uani 1 1 d . . . . . C27 C 0.14233(14) 0.74849(10) 0.86398(9) 0.0125(3) Uani 1 1 d . . . . . H27A H 0.095487 0.724145 0.830667 0.015 Uiso 1 1 calc R U . . . H27B H 0.068272 0.791314 0.911784 0.015 Uiso 1 1 calc R U . . . C24 C 0.58238(14) 0.58969(10) 0.73430(9) 0.0103(2) Uani 1 1 d . . . . . C1 C 0.51501(14) 0.83729(10) 0.50162(9) 0.0118(2) Uani 1 1 d . . . . . H1 H 0.451048 0.906684 0.482086 0.014 Uiso 1 1 calc R U . . . C34 C 0.59783(15) 0.40912(11) 0.71972(10) 0.0140(3) Uani 1 1 d . . . . . H34 H 0.493665 0.446046 0.731160 0.017 Uiso 1 1 calc R U . . . C31 C 0.81701(14) 0.45234(11) 0.70055(10) 0.0147(3) Uani 1 1 d . . . . . H31 H 0.850846 0.374210 0.699097 0.018 Uiso 1 1 calc R U . . . C10 C 0.57360(17) 0.82059(13) 1.01890(10) 0.0208(3) Uani 1 1 d . . . . . H10 H 0.518196 0.844931 1.076102 0.025 Uiso 1 1 calc R U . . . C26 C 0.35245(14) 0.57960(10) 0.83534(9) 0.0121(3) Uani 1 1 d . . . . . H26A H 0.409784 0.515967 0.865150 0.015 Uiso 1 1 calc R U . . . H26B H 0.304021 0.557030 0.801881 0.015 Uiso 1 1 calc R U . . . C13 C 0.64435(16) 0.66055(12) 0.43810(12) 0.0223(3) Uani 1 1 d . . . . . H13 H 0.643291 0.629816 0.497524 0.027 Uiso 1 1 calc R U . . . C23 C 0.22643(15) 0.86020(11) 0.51484(10) 0.0158(3) Uani 1 1 d . . . . . H23 H 0.260503 0.912876 0.478405 0.019 Uiso 1 1 calc R U . . . C5 C 0.54622(14) 0.88032(10) 0.78000(9) 0.0118(2) Uani 1 1 d . . . . . C11 C 0.52548(15) 0.86608(12) 0.94329(10) 0.0157(3) Uani 1 1 d . . . . . H11 H 0.437115 0.921460 0.949656 0.019 Uiso 1 1 calc R U . . . C17 C 0.57995(18) 0.81117(13) 0.33604(10) 0.0211(3) Uani 1 1 d . . . . . H17 H 0.533493 0.884404 0.325389 0.025 Uiso 1 1 calc R U . . . C9 C 0.70260(18) 0.73951(13) 1.01141(10) 0.0225(3) Uani 1 1 d . . . . . H9 H 0.735516 0.707779 1.063180 0.027 Uiso 1 1 calc R U . . . C37 C -0.08776(14) 0.95469(11) 0.81368(10) 0.0132(3) Uani 1 1 d . . . . . H37 H -0.053781 0.876341 0.814054 0.016 Uiso 1 1 calc R U . . . C19 C 0.25199(15) 0.70963(11) 0.62118(10) 0.0155(3) Uani 1 1 d . . . . . H19 H 0.304976 0.657220 0.657510 0.019 Uiso 1 1 calc R U . . . C40 C 0.01435(15) 1.10026(10) 0.78829(10) 0.0154(3) Uani 1 1 d . . . . . H40 H -0.090066 1.136561 0.806941 0.019 Uiso 1 1 calc R U . . . C28 C 0.24145(14) 0.65230(10) 0.90713(9) 0.0124(3) Uani 1 1 d . . . . . C39 C -0.16018(16) 0.99962(12) 0.73774(11) 0.0191(3) Uani 1 1 d . . . . . H39A H -0.194878 1.076587 0.735416 0.029 Uiso 1 1 calc R U . . . H39B H -0.239571 0.974880 0.748439 0.029 Uiso 1 1 calc R U . . . H39C H -0.092618 0.976263 0.680575 0.029 Uiso 1 1 calc R U . . . C36 C 0.62260(17) 0.31946(11) 0.79264(12) 0.0224(3) Uani 1 1 d . . . . . H36A H 0.724158 0.283848 0.785217 0.034 Uiso 1 1 calc R U . . . H36B H 0.580220 0.269181 0.787799 0.034 Uiso 1 1 calc R U . . . H36C H 0.579330 0.347765 0.851761 0.034 Uiso 1 1 calc R U . . . C20 C 0.12309(16) 0.70729(12) 0.61888(11) 0.0195(3) Uani 1 1 d . . . . . H20 H 0.087813 0.655168 0.655293 0.023 Uiso 1 1 calc R U . . . C6 C 0.60417(14) 0.83233(11) 0.85724(9) 0.0123(3) Uani 1 1 d . . . . . C2 C 0.63211(15) 0.85625(11) 0.52760(9) 0.0130(3) Uani 1 1 d . . . . . H2A H 0.710029 0.789034 0.531932 0.016 Uiso 1 1 calc R U . . . H2B H 0.670298 0.904758 0.481554 0.016 Uiso 1 1 calc R U . . . C42 C 0.06461(17) 1.14468(12) 0.69236(11) 0.0220(3) Uani 1 1 d . . . . . H42A H 0.167891 1.117934 0.673353 0.033 Uiso 1 1 calc R U . . . H42B H 0.030899 1.221603 0.690327 0.033 Uiso 1 1 calc R U . . . H42C H 0.027234 1.122927 0.651982 0.033 Uiso 1 1 calc R U . . . C38 C -0.18912(15) 0.98425(12) 0.90511(10) 0.0197(3) Uani 1 1 d . . . . . H38A H -0.139203 0.952410 0.952002 0.030 Uiso 1 1 calc R U . . . H38B H -0.267479 0.958470 0.915411 0.030 Uiso 1 1 calc R U . . . H38C H -0.225884 1.060896 0.906720 0.030 Uiso 1 1 calc R U . . . C33 C 0.86634(16) 0.47252(13) 0.77497(11) 0.0231(3) Uani 1 1 d . . . . . H33A H 0.836741 0.548439 0.779026 0.035 Uiso 1 1 calc R U . . . H33B H 0.969367 0.442007 0.761587 0.035 Uiso 1 1 calc R U . . . H33C H 0.824674 0.440100 0.832204 0.035 Uiso 1 1 calc R U . . . C7 C 0.73513(15) 0.75138(11) 0.85119(10) 0.0156(3) Uani 1 1 d . . . . . H7 H 0.792190 0.727551 0.794122 0.019 Uiso 1 1 calc R U . . . C32 C 0.88623(16) 0.49384(13) 0.60796(11) 0.0231(3) Uani 1 1 d . . . . . H32A H 0.847261 0.482765 0.562873 0.035 Uiso 1 1 calc R U . . . H32B H 0.988210 0.456231 0.593452 0.035 Uiso 1 1 calc R U . . . H32C H 0.867581 0.569138 0.608198 0.035 Uiso 1 1 calc R U . . . C8 C 0.78264(16) 0.70557(12) 0.92719(10) 0.0196(3) Uani 1 1 d . . . . . H8 H 0.871037 0.650307 0.921459 0.024 Uiso 1 1 calc R U . . . C30 C 0.31143(16) 0.68604(12) 0.96289(10) 0.0182(3) Uani 1 1 d . . . . . H30A H 0.369508 0.726131 0.923816 0.027 Uiso 1 1 calc R U . . . H30B H 0.371011 0.623575 0.991214 0.027 Uiso 1 1 calc R U . . . H30C H 0.238633 0.730058 1.009371 0.027 Uiso 1 1 calc R U . . . C29 C 0.15184(15) 0.58835(11) 0.96837(10) 0.0177(3) Uani 1 1 d . . . . . H29A H 0.075720 0.632983 1.013137 0.027 Uiso 1 1 calc R U . . . H29B H 0.211309 0.528144 0.998834 0.027 Uiso 1 1 calc R U . . . H29C H 0.111344 0.563156 0.932169 0.027 Uiso 1 1 calc R U . . . C21 C 0.04541(15) 0.78016(12) 0.56405(11) 0.0198(3) Uani 1 1 d . . . . . H21 H -0.042427 0.778359 0.562210 0.024 Uiso 1 1 calc R U . . . C41 C 0.07386(17) 1.12761(13) 0.85411(12) 0.0238(3) Uani 1 1 d . . . . . H41A H 0.033047 1.102895 0.915206 0.036 Uiso 1 1 calc R U . . . H41B H 0.050192 1.203987 0.850569 0.036 Uiso 1 1 calc R U . . . H41C H 0.176562 1.093528 0.838833 0.036 Uiso 1 1 calc R U . . . C22 C 0.09907(16) 0.85580(12) 0.51193(11) 0.0199(3) Uani 1 1 d . . . . . H22 H 0.047588 0.905614 0.473438 0.024 Uiso 1 1 calc R U . . . C14 C 0.71184(18) 0.59752(14) 0.36602(14) 0.0309(4) Uani 1 1 d . . . . . H14 H 0.756064 0.523930 0.376477 0.037 Uiso 1 1 calc R U . . . C35 C 0.65095(18) 0.36836(13) 0.62623(11) 0.0254(3) Uani 1 1 d . . . . . H35A H 0.632414 0.427843 0.581264 0.038 Uiso 1 1 calc R U . . . H35B H 0.601868 0.321512 0.623874 0.038 Uiso 1 1 calc R U . . . H35C H 0.752568 0.329621 0.613686 0.038 Uiso 1 1 calc R U . . . C16 C 0.64838(19) 0.74846(15) 0.26399(11) 0.0284(4) Uani 1 1 d . . . . . H16 H 0.649510 0.778924 0.204490 0.034 Uiso 1 1 calc R U . . . C15 C 0.71460(18) 0.64191(16) 0.27917(13) 0.0326(4) Uani 1 1 d . . . . . H15 H 0.762108 0.598969 0.230051 0.039 Uiso 1 1 calc R U . . . H3 H 0.4796(19) 0.9598(14) 0.6217(12) 0.019(4) Uiso 1 1 d . . . . . H5 H 0.4641(17) 0.9418(13) 0.7913(11) 0.012(4) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zr1 0.00704(6) 0.00798(6) 0.00937(6) 0.00018(4) -0.00125(4) -0.00211(4) O2 0.0092(4) 0.0095(4) 0.0174(5) 0.0006(4) -0.0014(4) -0.0030(3) O1 0.0088(4) 0.0098(4) 0.0152(5) 0.0002(4) -0.0019(4) -0.0029(3) N3 0.0094(5) 0.0085(5) 0.0131(5) 0.0007(4) -0.0006(4) -0.0015(4) N2 0.0090(5) 0.0092(5) 0.0118(5) 0.0003(4) -0.0011(4) -0.0023(4) N1 0.0117(5) 0.0123(5) 0.0106(5) 0.0009(4) -0.0030(4) -0.0062(4) N5 0.0084(5) 0.0083(5) 0.0166(6) -0.0019(4) -0.0024(4) -0.0013(4) N4 0.0074(5) 0.0097(5) 0.0151(6) -0.0023(4) -0.0017(4) -0.0014(4) C12 0.0132(6) 0.0194(7) 0.0141(7) -0.0050(5) -0.0018(5) -0.0083(5) C4 0.0108(6) 0.0120(6) 0.0135(6) -0.0017(5) -0.0010(5) -0.0068(5) C25 0.0102(6) 0.0105(6) 0.0096(6) -0.0015(5) -0.0027(5) -0.0023(5) C18 0.0116(6) 0.0125(6) 0.0113(6) -0.0040(5) -0.0023(5) -0.0034(5) C3 0.0127(6) 0.0117(6) 0.0116(6) -0.0005(5) -0.0017(5) -0.0068(5) C27 0.0097(6) 0.0114(6) 0.0131(6) 0.0008(5) -0.0004(5) -0.0028(5) C24 0.0101(6) 0.0103(6) 0.0095(6) 0.0002(5) -0.0038(5) -0.0020(5) C1 0.0138(6) 0.0116(6) 0.0102(6) -0.0010(5) -0.0030(5) -0.0047(5) C34 0.0118(6) 0.0117(6) 0.0176(7) -0.0035(5) -0.0022(5) -0.0032(5) C31 0.0072(6) 0.0131(6) 0.0200(7) -0.0026(5) -0.0026(5) 0.0006(5) C10 0.0242(8) 0.0266(8) 0.0112(7) -0.0019(6) -0.0015(6) -0.0104(6) C26 0.0106(6) 0.0102(6) 0.0131(6) 0.0013(5) -0.0012(5) -0.0031(5) C13 0.0181(7) 0.0210(7) 0.0271(8) -0.0070(6) -0.0072(6) -0.0025(6) C23 0.0172(7) 0.0155(6) 0.0156(7) 0.0000(5) -0.0068(6) -0.0052(5) C5 0.0109(6) 0.0109(6) 0.0127(6) -0.0016(5) -0.0024(5) -0.0029(5) C11 0.0137(6) 0.0196(7) 0.0130(7) -0.0029(5) -0.0005(5) -0.0065(5) C17 0.0291(8) 0.0271(8) 0.0142(7) -0.0031(6) -0.0029(6) -0.0190(7) C9 0.0278(8) 0.0278(8) 0.0144(7) 0.0025(6) -0.0100(6) -0.0105(7) C37 0.0091(6) 0.0122(6) 0.0168(7) -0.0004(5) -0.0024(5) -0.0032(5) C19 0.0160(7) 0.0156(6) 0.0165(7) 0.0012(5) -0.0061(6) -0.0066(5) C40 0.0108(6) 0.0088(6) 0.0239(8) -0.0024(5) -0.0035(5) -0.0006(5) C28 0.0105(6) 0.0118(6) 0.0114(6) 0.0009(5) -0.0004(5) -0.0028(5) C39 0.0179(7) 0.0191(7) 0.0234(8) -0.0006(6) -0.0091(6) -0.0072(6) C36 0.0199(7) 0.0117(6) 0.0327(9) 0.0028(6) -0.0068(7) -0.0043(6) C20 0.0173(7) 0.0212(7) 0.0227(8) -0.0039(6) -0.0030(6) -0.0104(6) C6 0.0126(6) 0.0137(6) 0.0119(6) -0.0006(5) -0.0024(5) -0.0070(5) C2 0.0142(6) 0.0156(6) 0.0103(6) -0.0012(5) -0.0012(5) -0.0075(5) C42 0.0203(7) 0.0150(7) 0.0284(8) 0.0060(6) -0.0088(7) -0.0052(6) C38 0.0132(7) 0.0247(8) 0.0190(7) -0.0035(6) 0.0001(6) -0.0067(6) C33 0.0143(7) 0.0264(8) 0.0281(9) -0.0052(7) -0.0102(6) -0.0013(6) C7 0.0152(7) 0.0185(7) 0.0123(6) -0.0027(5) -0.0027(5) -0.0051(5) C32 0.0129(7) 0.0251(8) 0.0240(8) -0.0025(6) 0.0017(6) -0.0034(6) C8 0.0175(7) 0.0208(7) 0.0208(8) 0.0001(6) -0.0087(6) -0.0046(6) C30 0.0193(7) 0.0194(7) 0.0140(7) -0.0023(6) -0.0034(6) -0.0049(6) C29 0.0149(7) 0.0160(7) 0.0160(7) 0.0039(5) 0.0000(5) -0.0040(5) C21 0.0117(6) 0.0259(8) 0.0234(8) -0.0095(6) -0.0045(6) -0.0047(6) C41 0.0223(8) 0.0211(7) 0.0290(9) -0.0120(7) -0.0032(7) -0.0068(6) C22 0.0176(7) 0.0211(7) 0.0207(8) -0.0044(6) -0.0101(6) -0.0011(6) C14 0.0190(8) 0.0267(9) 0.0466(11) -0.0204(8) -0.0068(8) -0.0008(7) C35 0.0219(8) 0.0280(8) 0.0277(9) -0.0150(7) 0.0005(7) -0.0096(7) C16 0.0329(9) 0.0466(11) 0.0162(8) -0.0110(7) 0.0021(7) -0.0279(8) C15 0.0189(8) 0.0524(12) 0.0326(10) -0.0285(9) 0.0048(7) -0.0164(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zr Zr -2.9673 0.5597 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Zr1 O1 159.93(4) . . ? O2 Zr1 C4 90.05(4) . . ? O2 Zr1 C25 29.40(4) . . ? O2 Zr1 C3 78.57(4) . . ? O2 Zr1 C24 165.89(4) . . ? O2 Zr1 C5 77.73(4) . . ? O1 Zr1 C4 70.29(4) . . ? O1 Zr1 C25 163.56(4) . . ? O1 Zr1 C3 86.13(4) . . ? O1 Zr1 C24 29.39(4) . . ? O1 Zr1 C5 83.31(4) . . ? N3 Zr1 O2 59.43(4) . . ? N3 Zr1 O1 134.84(4) . . ? N3 Zr1 C4 139.31(4) . . ? N3 Zr1 C25 30.33(4) . . ? N3 Zr1 C3 137.97(4) . . ? N3 Zr1 C24 107.38(4) . . ? N3 Zr1 C5 108.87(4) . . ? N2 Zr1 O2 136.51(4) . . ? N2 Zr1 O1 59.14(4) . . ? N2 Zr1 N3 77.20(4) . . ? N2 Zr1 C4 125.15(4) . . ? N2 Zr1 C25 107.49(4) . . ? N2 Zr1 C3 144.80(4) . . ? N2 Zr1 C24 30.25(4) . . ? N2 Zr1 C5 116.70(4) . . ? N1 Zr1 O2 93.72(4) . . ? N1 Zr1 O1 93.25(4) . . ? N1 Zr1 N3 108.71(4) . . ? N1 Zr1 N2 103.68(4) . . ? N1 Zr1 C4 98.73(4) . . ? N1 Zr1 C25 99.69(4) . . ? N1 Zr1 C3 70.31(4) . . ? N1 Zr1 C24 95.67(4) . . ? N1 Zr1 C5 129.42(4) . . ? C4 Zr1 C25 117.13(4) . . ? C4 Zr1 C3 31.66(4) . . ? C4 Zr1 C24 98.89(4) . . ? C25 Zr1 C24 137.70(4) . . ? C3 Zr1 C25 107.70(4) . . ? C3 Zr1 C24 114.57(4) . . ? C5 Zr1 C4 32.97(4) . . ? C5 Zr1 C25 96.03(4) . . ? C5 Zr1 C3 59.12(4) . . ? C5 Zr1 C24 104.03(4) . . ? C25 O2 Zr1 94.00(8) . . ? C24 O1 Zr1 92.89(7) . . ? C25 N3 Zr1 93.60(8) . . ? C25 N3 C27 128.98(11) . . ? C27 N3 Zr1 137.42(8) . . ? C24 N2 Zr1 94.04(8) . . ? C24 N2 C26 128.13(11) . . ? C26 N2 Zr1 137.57(8) . . ? C18 N1 Zr1 114.45(8) . . ? C18 N1 C1 114.72(11) . . ? C1 N1 Zr1 125.92(8) . . ? C25 N5 C37 123.11(11) . . ? C25 N5 C40 119.17(11) . . ? C37 N5 C40 117.24(10) . . ? C24 N4 C34 121.67(11) . . ? C24 N4 C31 120.61(11) . . ? C31 N4 C34 116.98(11) . . ? C13 C12 C1 119.95(13) . . ? C13 C12 C17 118.88(14) . . ? C17 C12 C1 121.06(13) . . ? Zr1 C4 H4 117.3 . . ? C3 C4 Zr1 74.39(8) . . ? C3 C4 H4 117.3 . . ? C3 C4 C5 124.52(13) . . ? C5 C4 Zr1 72.74(8) . . ? C5 C4 H4 117.3 . . ? O2 C25 Zr1 56.60(6) . . ? O2 C25 N3 111.90(11) . . ? O2 C25 N5 118.55(12) . . ? N3 C25 Zr1 56.07(7) . . ? N3 C25 N5 129.55(12) . . ? N5 C25 Zr1 170.27(10) . . ? C23 C18 N1 123.85(12) . . ? C19 C18 N1 119.33(12) . . ? C19 C18 C23 116.78(13) . . ? Zr1 C3 H3 86.8(10) . . ? C4 C3 Zr1 73.95(8) . . ? C4 C3 C2 124.40(13) . . ? C4 C3 H3 120.6(10) . . ? C2 C3 Zr1 106.21(8) . . ? C2 C3 H3 114.8(10) . . ? N3 C27 H27A 109.3 . . ? N3 C27 H27B 109.3 . . ? N3 C27 C28 111.80(11) . . ? H27A C27 H27B 107.9 . . ? C28 C27 H27A 109.3 . . ? C28 C27 H27B 109.3 . . ? O1 C24 Zr1 57.72(6) . . ? O1 C24 N2 112.12(11) . . ? O1 C24 N4 119.61(12) . . ? N2 C24 Zr1 55.70(7) . . ? N2 C24 N4 128.23(12) . . ? N4 C24 Zr1 167.27(10) . . ? N1 C1 C12 112.69(11) . . ? N1 C1 H1 108.3 . . ? N1 C1 C2 109.11(11) . . ? C12 C1 H1 108.3 . . ? C12 C1 C2 110.05(11) . . ? C2 C1 H1 108.3 . . ? N4 C34 H34 107.4 . . ? N4 C34 C36 111.64(12) . . ? N4 C34 C35 111.03(12) . . ? C36 C34 H34 107.4 . . ? C36 C34 C35 111.70(13) . . ? C35 C34 H34 107.4 . . ? N4 C31 H31 105.9 . . ? N4 C31 C33 110.73(12) . . ? N4 C31 C32 115.11(12) . . ? C33 C31 H31 105.9 . . ? C33 C31 C32 112.46(13) . . ? C32 C31 H31 105.9 . . ? C11 C10 H10 119.9 . . ? C11 C10 C9 120.28(14) . . ? C9 C10 H10 119.9 . . ? N2 C26 H26A 109.2 . . ? N2 C26 H26B 109.2 . . ? N2 C26 C28 111.92(11) . . ? H26A C26 H26B 107.9 . . ? C28 C26 H26A 109.2 . . ? C28 C26 H26B 109.2 . . ? C12 C13 H13 119.8 . . ? C12 C13 C14 120.32(16) . . ? C14 C13 H13 119.8 . . ? C18 C23 H23 119.5 . . ? C22 C23 C18 120.98(14) . . ? C22 C23 H23 119.5 . . ? Zr1 C5 H5 93.3(10) . . ? C4 C5 Zr1 74.29(8) . . ? C4 C5 C6 124.16(12) . . ? C4 C5 H5 116.9(10) . . ? C6 C5 Zr1 121.39(9) . . ? C6 C5 H5 115.1(10) . . ? C10 C11 H11 119.1 . . ? C10 C11 C6 121.72(14) . . ? C6 C11 H11 119.1 . . ? C12 C17 H17 119.6 . . ? C16 C17 C12 120.83(16) . . ? C16 C17 H17 119.6 . . ? C10 C9 H9 120.5 . . ? C8 C9 C10 119.05(14) . . ? C8 C9 H9 120.5 . . ? N5 C37 H37 107.3 . . ? N5 C37 C39 110.98(11) . . ? N5 C37 C38 111.64(12) . . ? C39 C37 H37 107.3 . . ? C38 C37 H37 107.3 . . ? C38 C37 C39 112.07(12) . . ? C18 C19 H19 119.2 . . ? C20 C19 C18 121.59(13) . . ? C20 C19 H19 119.2 . . ? N5 C40 H40 106.2 . . ? N5 C40 C42 114.53(12) . . ? N5 C40 C41 111.01(12) . . ? C42 C40 H40 106.2 . . ? C41 C40 H40 106.2 . . ? C41 C40 C42 112.13(13) . . ? C26 C28 C27 110.91(11) . . ? C30 C28 C27 111.20(11) . . ? C30 C28 C26 111.11(11) . . ? C30 C28 C29 109.36(12) . . ? C29 C28 C27 107.55(11) . . ? C29 C28 C26 106.51(11) . . ? C37 C39 H39A 109.5 . . ? C37 C39 H39B 109.5 . . ? C37 C39 H39C 109.5 . . ? H39A C39 H39B 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C34 C36 H36A 109.5 . . ? C34 C36 H36B 109.5 . . ? C34 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C19 C20 H20 119.6 . . ? C21 C20 C19 120.77(14) . . ? C21 C20 H20 119.6 . . ? C11 C6 C5 119.56(13) . . ? C7 C6 C5 123.48(12) . . ? C7 C6 C11 116.95(13) . . ? C3 C2 C1 107.86(11) . . ? C3 C2 H2A 110.1 . . ? C3 C2 H2B 110.1 . . ? C1 C2 H2A 110.1 . . ? C1 C2 H2B 110.1 . . ? H2A C2 H2B 108.4 . . ? C40 C42 H42A 109.5 . . ? C40 C42 H42B 109.5 . . ? C40 C42 H42C 109.5 . . ? H42A C42 H42B 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? C37 C38 H38A 109.5 . . ? C37 C38 H38B 109.5 . . ? C37 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C31 C33 H33A 109.5 . . ? C31 C33 H33B 109.5 . . ? C31 C33 H33C 109.5 . . ? H33A C33 H33B 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C6 C7 H7 119.4 . . ? C8 C7 C6 121.16(13) . . ? C8 C7 H7 119.4 . . ? C31 C32 H32A 109.5 . . ? C31 C32 H32B 109.5 . . ? C31 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C9 C8 C7 120.83(14) . . ? C9 C8 H8 119.6 . . ? C7 C8 H8 119.6 . . ? C28 C30 H30A 109.5 . . ? C28 C30 H30B 109.5 . . ? C28 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C28 C29 H29A 109.5 . . ? C28 C29 H29B 109.5 . . ? C28 C29 H29C 109.5 . . ? H29A C29 H29B 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C20 C21 H21 120.8 . . ? C20 C21 C22 118.41(14) . . ? C22 C21 H21 120.8 . . ? C40 C41 H41A 109.5 . . ? C40 C41 H41B 109.5 . . ? C40 C41 H41C 109.5 . . ? H41A C41 H41B 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? C23 C22 H22 119.3 . . ? C21 C22 C23 121.40(14) . . ? C21 C22 H22 119.3 . . ? C13 C14 H14 119.9 . . ? C15 C14 C13 120.14(17) . . ? C15 C14 H14 119.9 . . ? C34 C35 H35A 109.5 . . ? C34 C35 H35B 109.5 . . ? C34 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C17 C16 H16 120.1 . . ? C15 C16 C17 119.82(17) . . ? C15 C16 H16 120.1 . . ? C14 C15 H15 120.0 . . ? C16 C15 C14 120.00(16) . . ? C16 C15 H15 120.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zr1 O2 2.2112(9) . ? Zr1 O1 2.2369(9) . ? Zr1 N3 2.1966(11) . ? Zr1 N2 2.1885(11) . ? Zr1 N1 2.1262(12) . ? Zr1 C4 2.5134(13) . ? Zr1 C25 2.6422(13) . ? Zr1 C3 2.5189(13) . ? Zr1 C24 2.6424(13) . ? Zr1 C5 2.4934(14) . ? O2 C25 1.3002(16) . ? O1 C24 1.2984(16) . ? N3 C25 1.3367(16) . ? N3 C27 1.4564(17) . ? N2 C24 1.3345(17) . ? N2 C26 1.4523(17) . ? N1 C18 1.4165(17) . ? N1 C1 1.4816(17) . ? N5 C25 1.3528(17) . ? N5 C37 1.4807(17) . ? N5 C40 1.4872(17) . ? N4 C24 1.3529(16) . ? N4 C34 1.4830(17) . ? N4 C31 1.4817(17) . ? C12 C1 1.5181(19) . ? C12 C13 1.388(2) . ? C12 C17 1.391(2) . ? C4 H4 1.0000 . ? C4 C3 1.3728(19) . ? C4 C5 1.4208(19) . ? C18 C23 1.4087(19) . ? C18 C19 1.4064(19) . ? C3 C2 1.5016(19) . ? C3 H3 0.966(18) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C27 C28 1.5424(19) . ? C1 H1 1.0000 . ? C1 C2 1.5386(19) . ? C34 H34 1.0000 . ? C34 C36 1.526(2) . ? C34 C35 1.531(2) . ? C31 H31 1.0000 . ? C31 C33 1.522(2) . ? C31 C32 1.529(2) . ? C10 H10 0.9500 . ? C10 C11 1.386(2) . ? C10 C9 1.390(2) . ? C26 H26A 0.9900 . ? C26 H26B 0.9900 . ? C26 C28 1.5399(19) . ? C13 H13 0.9500 . ? C13 C14 1.393(2) . ? C23 H23 0.9500 . ? C23 C22 1.389(2) . ? C5 C6 1.4636(19) . ? C5 H5 0.955(16) . ? C11 H11 0.9500 . ? C11 C6 1.4087(19) . ? C17 H17 0.9500 . ? C17 C16 1.391(2) . ? C9 H9 0.9500 . ? C9 C8 1.388(2) . ? C37 H37 1.0000 . ? C37 C39 1.526(2) . ? C37 C38 1.523(2) . ? C19 H19 0.9500 . ? C19 C20 1.390(2) . ? C40 H40 1.0000 . ? C40 C42 1.531(2) . ? C40 C41 1.525(2) . ? C28 C30 1.529(2) . ? C28 C29 1.5368(19) . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C20 H20 0.9500 . ? C20 C21 1.387(2) . ? C6 C7 1.4048(19) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C42 H42A 0.9800 . ? C42 H42B 0.9800 . ? C42 H42C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C7 H7 0.9500 . ? C7 C8 1.389(2) . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C8 H8 0.9500 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C21 H21 0.9500 . ? C21 C22 1.388(2) . ? C41 H41A 0.9800 . ? C41 H41B 0.9800 . ? C41 H41C 0.9800 . ? C22 H22 0.9500 . ? C14 H14 0.9500 . ? C14 C15 1.385(3) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C16 H16 0.9500 . ? C16 C15 1.379(3) . ? C15 H15 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Zr1 O2 C25 N3 9.74(11) . . . . ? Zr1 O2 C25 N5 -170.16(11) . . . . ? Zr1 O1 C24 N2 -12.55(11) . . . . ? Zr1 O1 C24 N4 165.48(11) . . . . ? Zr1 N3 C25 O2 -9.81(11) . . . . ? Zr1 N3 C25 N5 170.09(13) . . . . ? Zr1 N3 C27 C28 28.26(19) . . . . ? Zr1 N2 C24 O1 12.85(11) . . . . ? Zr1 N2 C24 N4 -164.97(13) . . . . ? Zr1 N2 C26 C28 -29.27(19) . . . . ? Zr1 N1 C18 C23 126.69(12) . . . . ? Zr1 N1 C18 C19 -51.02(15) . . . . ? Zr1 N1 C1 C12 138.31(10) . . . . ? Zr1 N1 C1 C2 15.76(15) . . . . ? Zr1 C4 C3 C2 -98.91(12) . . . . ? Zr1 C4 C5 C6 117.59(13) . . . . ? Zr1 C3 C2 C1 47.94(12) . . . . ? Zr1 C5 C6 C11 -100.07(13) . . . . ? Zr1 C5 C6 C7 78.58(15) . . . . ? N3 C27 C28 C26 -62.73(15) . . . . ? N3 C27 C28 C30 61.46(15) . . . . ? N3 C27 C28 C29 -178.83(11) . . . . ? N2 C26 C28 C27 63.27(15) . . . . ? N2 C26 C28 C30 -60.96(15) . . . . ? N2 C26 C28 C29 -179.98(11) . . . . ? N1 C18 C23 C22 -175.82(13) . . . . ? N1 C18 C19 C20 174.71(13) . . . . ? N1 C1 C2 C3 -43.20(14) . . . . ? C12 C1 C2 C3 -167.33(11) . . . . ? C12 C13 C14 C15 0.4(2) . . . . ? C12 C17 C16 C15 0.7(2) . . . . ? C4 C3 C2 C1 129.32(14) . . . . ? C4 C5 C6 C11 168.16(13) . . . . ? C4 C5 C6 C7 -13.2(2) . . . . ? C25 N3 C27 C28 -152.28(13) . . . . ? C25 N5 C37 C39 -112.50(14) . . . . ? C25 N5 C37 C38 121.70(14) . . . . ? C25 N5 C40 C42 65.93(17) . . . . ? C25 N5 C40 C41 -62.30(17) . . . . ? C18 N1 C1 C12 -68.03(15) . . . . ? C18 N1 C1 C2 169.42(11) . . . . ? C18 C23 C22 C21 0.0(2) . . . . ? C18 C19 C20 C21 2.4(2) . . . . ? C3 C4 C5 Zr1 56.24(12) . . . . ? C3 C4 C5 C6 173.82(13) . . . . ? C27 N3 C25 Zr1 -179.64(16) . . . . ? C27 N3 C25 O2 170.56(13) . . . . ? C27 N3 C25 N5 -9.6(2) . . . . ? C24 N2 C26 C28 143.27(13) . . . . ? C24 N4 C34 C36 -121.99(14) . . . . ? C24 N4 C34 C35 112.65(14) . . . . ? C24 N4 C31 C33 63.10(17) . . . . ? C24 N4 C31 C32 -65.84(17) . . . . ? C1 N1 C18 C23 -30.06(18) . . . . ? C1 N1 C18 C19 152.23(12) . . . . ? C1 C12 C13 C14 -175.38(14) . . . . ? C1 C12 C17 C16 174.75(14) . . . . ? C34 N4 C24 Zr1 -77.8(5) . . . . ? C34 N4 C24 O1 -152.01(12) . . . . ? C34 N4 C24 N2 25.7(2) . . . . ? C34 N4 C31 C33 -126.59(13) . . . . ? C34 N4 C31 C32 104.47(15) . . . . ? C31 N4 C24 Zr1 92.1(4) . . . . ? C31 N4 C24 O1 17.84(19) . . . . ? C31 N4 C24 N2 -164.48(13) . . . . ? C31 N4 C34 C36 67.81(15) . . . . ? C31 N4 C34 C35 -57.55(16) . . . . ? C10 C11 C6 C5 177.74(13) . . . . ? C10 C11 C6 C7 -1.0(2) . . . . ? C10 C9 C8 C7 -0.2(2) . . . . ? C26 N2 C24 Zr1 -174.96(16) . . . . ? C26 N2 C24 O1 -162.11(13) . . . . ? C26 N2 C24 N4 20.1(2) . . . . ? C13 C12 C1 N1 -45.00(18) . . . . ? C13 C12 C1 C2 77.03(16) . . . . ? C13 C12 C17 C16 -1.4(2) . . . . ? C13 C14 C15 C16 -1.1(3) . . . . ? C23 C18 C19 C20 -3.2(2) . . . . ? C5 C4 C3 Zr1 -55.52(12) . . . . ? C5 C4 C3 C2 -154.43(13) . . . . ? C5 C6 C7 C8 -177.31(13) . . . . ? C11 C10 C9 C8 0.5(2) . . . . ? C11 C6 C7 C8 1.4(2) . . . . ? C17 C12 C1 N1 138.88(14) . . . . ? C17 C12 C1 C2 -99.09(16) . . . . ? C17 C12 C13 C14 0.8(2) . . . . ? C17 C16 C15 C14 0.5(3) . . . . ? C9 C10 C11 C6 0.1(2) . . . . ? C37 N5 C25 O2 154.02(12) . . . . ? C37 N5 C25 N3 -25.9(2) . . . . ? C37 N5 C40 C42 -106.40(14) . . . . ? C37 N5 C40 C41 125.36(13) . . . . ? C19 C18 C23 C22 1.9(2) . . . . ? C19 C20 C21 C22 -0.3(2) . . . . ? C40 N5 C25 O2 -17.85(19) . . . . ? C40 N5 C25 N3 162.27(14) . . . . ? C40 N5 C37 C39 59.50(16) . . . . ? C40 N5 C37 C38 -66.30(16) . . . . ? C20 C21 C22 C23 -0.9(2) . . . . ? C6 C7 C8 C9 -0.8(2) . . . . ?