#------------------------------------------------------------------------------ #$Date: 2024-06-13 01:14:14 +0300 (Thu, 13 Jun 2024) $ #$Revision: 292322 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/18/1571815.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571815 loop_ _publ_author_name 'Guo, Weiwei' 'Huang, Jianhao' 'Ishihara, Kazuaki' _publ_section_title ; Chiral \p--Cu(II)-catalyzed site-, exo/endo-, and enantioselective dearomative (3+2) cycloadditions of isoquinolinium ylides with enamides, dienamides, and a trienamide ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC02946A _journal_year 2024 _chemical_absolute_configuration ad _chemical_formula_moiety 'C25 H19 Br N6 O' _chemical_formula_sum 'C25 H19 Br N6 O' _chemical_formula_weight 499.37 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-07-21 _audit_creation_method ; Olex2 1.2-ac3 (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _audit_update_record ; 2024-01-17 deposited with the CCDC. 2024-06-06 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 103.686(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.2893(3) _cell_length_b 14.1630(4) _cell_length_c 10.0325(3) _cell_measurement_reflns_used 7952 _cell_measurement_temperature 123.15 _cell_measurement_theta_max 30.7380 _cell_measurement_theta_min 2.1200 _cell_volume 1144.39(6) _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 123.15 _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.893 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -105.00 75.00 0.50 5.00 -- -15.00 45.00 0.00 360 2 \w -105.00 75.00 0.50 5.00 -- -15.00 45.00 90.00 360 ; _diffrn_measurement_device 'abstract diffractometer' _diffrn_measurement_device_type 'dtrek-CrysAlisPro-abstract goniometer imported rigaku-d*trek images' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0488917000 _diffrn_orient_matrix_UB_12 0.0068484000 _diffrn_orient_matrix_UB_13 0.0675495000 _diffrn_orient_matrix_UB_21 -0.0694509000 _diffrn_orient_matrix_UB_22 0.0201735000 _diffrn_orient_matrix_UB_23 0.0192957000 _diffrn_orient_matrix_UB_31 -0.0235822000 _diffrn_orient_matrix_UB_32 -0.0453214000 _diffrn_orient_matrix_UB_33 0.0187664000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0154 _diffrn_reflns_av_unetI/netI 0.0194 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.893 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 9917 _diffrn_reflns_point_group_measured_fraction_full 0.928 _diffrn_reflns_point_group_measured_fraction_max 0.772 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.815 _diffrn_reflns_theta_min 2.089 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 1.826 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.75042 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.449 _exptl_crystal_description block _exptl_crystal_F_000 508 _exptl_crystal_size_max 0.8 _exptl_crystal_size_mid 0.5 _exptl_crystal_size_min 0.3 _refine_diff_density_max 0.349 _refine_diff_density_min -0.751 _refine_diff_density_rms 0.054 _refine_ls_abs_structure_details ; Flack x determined using 2000 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.011(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.075 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 300 _refine_ls_number_reflns 5540 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.075 _refine_ls_R_factor_all 0.0265 _refine_ls_R_factor_gt 0.0246 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0462P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0650 _refine_ls_wR_factor_ref 0.0655 _reflns_Friedel_coverage 0.667 _reflns_Friedel_fraction_full 0.852 _reflns_Friedel_fraction_max 0.641 _reflns_number_gt 5185 _reflns_number_total 5540 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc02946a2.cif _cod_data_source_block 20230721- _cod_database_code 1571815 _shelx_shelxl_version_number 2018/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 89.33 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 30.75 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C00E(H00E), C00G(H00G), C00O(H00O) 2.b Aromatic/amide H refined with riding coordinates: C008(H008), C00B(H00B), C00D(H00D), C00H(H00H), C00I(H00I), C00Q(H00Q), C00R(H00R), C00T(H00T), C00V(H00V), C00X(H00X) 2.c Idealised Me refined as rotating group: C00U(H00A,H00C,H00F), C00W(H00J,H00K,H00L) ; _shelx_res_file ; TITL 20230721-_a.res in P2(1) 20230721-.res created by SHELXL-2018/1 at 14:07:04 on 21-Jul-2023 REM Old TITL 20230721-_a.res in P2(1) REM SHELXT solution in P2(1) REM R1 0.144, Rweak 0.040, Alpha 0.004, Orientation as input REM Flack x = 0.064 ( 0.004 ) from Parsons' quotients REM Formula found by SHELXT: Br C25 N6 O CELL 0.71073 8.2893 14.163 10.0325 90 103.686 90 ZERR 2 0.0003 0.0004 0.0003 0 0.003 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC Br C N O H UNIT 2 50 12 2 38 L.S. 10 PLAN 20 TEMP 123.15 list 4 fmap 2 acta REM REM REM WGHT 0.046200 FVAR 0.87491 BR01 1 0.459698 0.714430 0.642307 11.00000 0.06781 0.01825 = 0.02881 -0.01056 0.01288 -0.00411 N002 3 0.456547 0.400791 0.134874 11.00000 0.02409 0.01845 = 0.01395 -0.00058 0.00747 0.00202 N003 3 0.100884 0.535418 0.589246 11.00000 0.02197 0.02381 = 0.01420 0.00162 0.00379 0.00213 N004 3 0.400594 0.433867 0.247049 11.00000 0.01720 0.01554 = 0.01265 -0.00234 0.00478 -0.00118 N005 3 0.050358 0.598796 0.482280 11.00000 0.01935 0.01846 = 0.01457 -0.00124 0.00279 0.00360 O006 4 0.042911 0.630605 0.259849 11.00000 0.06528 0.04167 = 0.02025 0.01151 0.01485 0.03564 C007 2 0.178789 0.333777 0.065492 11.00000 0.02157 0.01948 = 0.01105 -0.00129 0.00244 0.00077 C008 2 0.347191 0.351318 0.050438 11.00000 0.02554 0.01948 = 0.01433 -0.00378 0.00732 0.00098 AFIX 43 H008 5 0.377686 0.325106 -0.024991 11.00000 -1.20000 AFIX 0 N009 3 0.543127 0.646969 0.159694 11.00000 0.06505 0.03068 = 0.02649 0.00100 0.01648 -0.01641 C00A 2 0.116150 0.391600 0.155728 11.00000 0.02145 0.01734 = 0.01207 -0.00053 0.00133 0.00206 C00B 2 0.079429 0.263511 -0.009212 11.00000 0.02766 0.02305 = 0.01789 -0.00458 0.00137 -0.00060 AFIX 43 H00B 5 0.119971 0.225733 -0.069767 11.00000 -1.20000 AFIX 0 N00C 3 0.791665 0.428186 0.437922 11.00000 0.02370 0.04545 = 0.02759 -0.00876 0.00533 -0.00147 C00D 2 -0.042378 0.377252 0.172369 11.00000 0.02150 0.03064 = 0.02046 -0.00350 0.00449 0.00375 AFIX 43 H00D 5 -0.083488 0.415050 0.232572 11.00000 -1.20000 AFIX 0 C00E 2 0.229280 0.470303 0.221097 11.00000 0.02147 0.01507 = 0.01121 -0.00044 0.00428 0.00390 AFIX 13 H00E 5 0.216828 0.524165 0.158162 11.00000 -1.20000 AFIX 0 C00F 2 0.506093 0.507415 0.324246 11.00000 0.02375 0.01652 = 0.01245 -0.00163 0.00618 -0.00536 C00G 2 0.222982 0.504520 0.363991 11.00000 0.02161 0.01406 = 0.01121 0.00032 0.00374 0.00287 AFIX 13 H00G 5 0.199520 0.451539 0.419346 11.00000 -1.20000 AFIX 0 C00H 2 -0.066680 0.648224 0.643216 11.00000 0.02656 0.03447 = 0.02463 -0.01011 0.00869 0.00640 AFIX 43 H00H 5 -0.127683 0.681693 0.694237 11.00000 -1.20000 AFIX 0 C00I 2 0.566641 0.559056 0.815816 11.00000 0.03431 0.04257 = 0.01439 -0.00565 0.00248 -0.01035 AFIX 43 H00I 5 0.588189 0.605162 0.883726 11.00000 -1.20000 AFIX 0 C00J 2 0.096205 0.582755 0.359872 11.00000 0.02852 0.01926 = 0.01527 0.00027 0.00433 0.00796 C00K 2 0.504352 0.584299 0.679758 11.00000 0.02535 0.02203 = 0.01524 -0.00267 0.00476 -0.00356 C00L 2 -0.051765 0.669213 0.514093 11.00000 0.01956 0.02085 = 0.02363 -0.00829 0.00273 0.00299 C00M 2 0.533116 0.586241 0.233273 11.00000 0.03752 0.02111 = 0.01866 -0.00333 0.01086 -0.00865 C00N 2 0.669542 0.465179 0.390330 11.00000 0.02259 0.02574 = 0.01781 -0.00655 0.00773 -0.00765 C00O 2 0.402148 0.544643 0.426667 11.00000 0.02385 0.01180 = 0.01085 -0.00068 0.00492 0.00066 AFIX 13 H00O 5 0.397311 0.613693 0.420764 11.00000 -1.20000 AFIX 0 C00P 2 0.470744 0.517370 0.575161 11.00000 0.01844 0.01660 = 0.01205 -0.00078 0.00394 -0.00192 C00Q 2 0.596397 0.465536 0.849851 11.00000 0.02930 0.05225 = 0.01633 0.01099 0.00043 -0.00518 AFIX 43 H00Q 5 0.639491 0.448339 0.940779 11.00000 -1.20000 AFIX 0 C00R 2 -0.081326 0.250198 0.007434 11.00000 0.02724 0.02951 = 0.02552 -0.00431 -0.00070 -0.00506 AFIX 43 H00R 5 -0.148711 0.203801 -0.042840 11.00000 -1.20000 AFIX 0 C00S 2 0.028751 0.565452 0.685009 11.00000 0.02561 0.03439 = 0.01817 -0.00188 0.00595 0.00303 C00T 2 -0.141033 0.306098 0.098963 11.00000 0.01918 0.03262 = 0.02978 -0.00062 0.00196 -0.00196 AFIX 43 H00T 5 -0.247396 0.295978 0.111306 11.00000 -1.20000 AFIX 0 C00U 2 0.053165 0.513369 0.816949 11.00000 0.05643 0.05916 = 0.02507 0.00611 0.02066 0.01263 AFIX 137 H00A 5 -0.051304 0.488453 0.826285 11.00000 -1.50000 H00C 5 0.096650 0.555574 0.891690 11.00000 -1.50000 H00F 5 0.129914 0.462449 0.818064 11.00000 -1.50000 AFIX 0 C00V 2 0.562105 0.396957 0.748530 11.00000 0.02726 0.03285 = 0.02638 0.01545 0.00543 0.00385 AFIX 43 H00V 5 0.581191 0.333654 0.771551 11.00000 -1.20000 AFIX 0 C00W 2 -0.116007 0.750848 0.423655 11.00000 0.03327 0.02199 = 0.03126 -0.00468 0.00240 0.01083 AFIX 137 H00J 5 -0.024766 0.789520 0.413018 11.00000 -1.50000 H00K 5 -0.189403 0.787503 0.464142 11.00000 -1.50000 H00L 5 -0.175291 0.728179 0.335468 11.00000 -1.50000 AFIX 0 C00X 2 0.499536 0.422673 0.613272 11.00000 0.02432 0.01937 = 0.01988 0.00379 0.00703 -0.00051 AFIX 43 H00X 5 0.476070 0.376068 0.546159 11.00000 -1.20000 AFIX 0 HKLF 4 REM 20230721-_a.res in P2(1) REM R1 = 0.0246 for 5185 Fo > 4sig(Fo) and 0.0265 for all 5540 data REM 300 parameters refined using 1 restraints END WGHT 0.0462 0.0000 REM Highest difference peak 0.349, deepest hole -0.751, 1-sigma level 0.054 Q1 1 0.3811 0.7177 0.5963 11.00000 0.05 0.35 Q2 1 0.4807 0.5466 0.6230 11.00000 0.05 0.22 Q3 1 0.1617 0.3629 0.1203 11.00000 0.05 0.22 Q4 1 0.5198 0.7130 0.6084 11.00000 0.05 0.22 Q5 1 -0.0255 0.5571 0.8557 11.00000 0.05 0.21 Q6 1 0.4589 0.6862 0.6901 11.00000 0.05 0.20 Q7 1 0.5086 0.4694 0.5957 11.00000 0.05 0.19 Q8 1 0.1262 0.3079 0.0154 11.00000 0.05 0.19 Q9 1 0.0309 0.4465 0.8038 11.00000 0.05 0.18 Q10 1 -0.0916 0.2701 0.0594 11.00000 0.05 0.18 Q11 1 0.6876 0.7059 0.1201 11.00000 0.05 0.18 Q12 1 0.1632 0.4260 0.1915 11.00000 0.05 0.18 Q13 1 0.6293 0.6432 0.1197 11.00000 0.05 0.18 Q14 1 0.4016 0.7565 0.6704 11.00000 0.05 0.17 Q15 1 0.7235 0.5982 0.9148 11.00000 0.05 0.17 Q16 1 0.2377 0.4857 0.2956 11.00000 0.05 0.17 Q17 1 0.5228 0.6554 0.9425 11.00000 0.05 0.16 Q18 1 0.1855 0.5533 0.8782 11.00000 0.05 0.16 Q19 1 0.2369 0.5390 0.8964 11.00000 0.05 0.16 Q20 1 0.4928 0.5716 0.7458 11.00000 0.05 0.16 ; _shelx_res_checksum 48083 _shelx_hkl_file ; 0 -17 6 167.84 5.83 0 -17 7 35.55 4.72 0 -16 5 25.97 4.16 0 -16 6 168.15 5.68 0 -16 7 204.89 6.10 0 -15 4 39.57 3.93 0 -15 5 105.57 4.66 0 -15 6 96.83 4.91 0 -15 7 42.35 4.36 0 -14 4 425.84 6.68 0 -14 5 3.66 3.38 0 -14 6 161.65 5.37 0 -14 7 536.81 8.16 0 -14 8 44.31 4.24 0 -14 9 12.81 4.29 0 -13 3 56.20 3.52 0 -13 4 163.92 4.57 0 -13 5 387.00 6.62 0 -13 6 318.67 6.00 0 -13 7 12.47 3.48 0 -13 8 239.01 5.65 0 -13 9 216.27 6.12 0 -13 10 38.82 4.75 0 -12 -2 362.92 3.92 0 -12 2 336.64 5.23 0 -12 3 78.16 3.32 0 -12 4 898.40 9.19 0 -12 5 64.23 3.40 0 -12 6 46.50 3.72 0 -12 7 68.27 3.86 0 -12 8 106.14 4.40 0 -12 9 17.23 4.03 0 -12 10 93.27 5.03 0 -11 -1 603.95 5.29 0 -11 2 607.81 6.81 0 -11 -2 617.06 5.16 0 -11 -3 496.71 4.18 0 -11 3 554.78 6.50 0 -11 4 83.83 3.27 0 -11 5 1402.10 11.78 0 -11 6 385.00 6.05 0 -11 7 37.48 3.52 0 -11 8 132.77 4.60 0 -11 9 244.73 5.67 0 -11 10 54.54 4.53 0 -11 11 14.23 4.21 0 -10 -1 683.37 5.46 0 -10 -2 247.85 2.90 0 -10 2 237.30 4.11 0 -10 -3 580.89 4.66 0 -10 3 572.34 6.55 0 -10 -4 932.39 6.44 0 -10 4 942.87 8.59 0 -10 5 248.50 4.64 0 -10 6 443.56 6.05 0 -10 7 534.32 6.95 0 -10 8 207.46 5.07 0 -10 10 215.94 5.44 0 -10 11 117.03 5.28 0 -9 0 0.57 1.27 0 -9 1 408.30 4.81 0 -9 -1 455.69 4.05 0 -9 -2 810.63 5.73 0 -9 2 766.63 7.14 0 -9 3 211.26 3.68 0 -9 -3 219.69 2.56 0 -9 -4 316.71 3.15 0 -9 4 296.78 4.46 0 -9 5 358.17 5.04 0 -9 -5 354.97 3.55 0 -9 6 667.42 7.21 0 -9 7 162.95 4.12 0 -9 8 85.37 3.79 0 -9 10 12.39 3.64 0 -9 11 156.97 5.29 0 -9 12 182.37 5.86 0 -8 0 458.57 4.03 0 -8 1 495.57 5.13 0 -8 -1 487.87 4.07 0 -8 -2 84.37 1.63 0 -8 2 82.27 2.36 0 -8 -3 1541.67 11.12 0 -8 -3 1616.29 9.34 0 -8 -4 332.91 3.14 0 -8 4 338.03 4.38 0 -8 -5 61.26 1.69 0 -8 5 62.85 2.65 0 -8 6 216.02 4.08 0 -8 -6 212.91 2.99 0 -8 7 1862.19 13.56 0 -8 8 117.00 3.92 0 -8 9 30.80 3.44 0 -8 10 126.96 4.69 0 -8 11 36.80 4.20 0 -8 12 110.86 5.29 0 -7 0 0.90 0.96 0 -7 1 2365.94 14.03 0 -7 -1 2232.50 12.54 0 -7 -2 1862.15 10.55 0 -7 -2 1851.64 12.05 0 -7 -3 122.48 2.67 0 -7 3 126.34 2.54 0 -7 -3 130.87 1.87 0 -7 4 939.89 7.67 0 -7 -4 961.44 6.30 0 -7 5 2345.64 15.29 0 -7 -5 2348.57 13.62 0 -7 6 943.79 8.34 0 -7 -6 962.00 7.13 0 -7 -7 187.14 3.12 0 -7 7 190.75 4.09 0 -7 8 188.20 4.55 0 -7 9 175.67 4.64 0 -7 10 134.34 4.60 0 -7 11 5.39 3.94 0 -7 12 14.72 4.36 0 -7 13 41.91 5.04 0 -6 0 2538.14 14.07 0 -6 1 1032.85 7.22 0 -6 -1 897.69 5.91 0 -6 2 35.98 1.47 0 -6 -2 37.78 1.01 0 -6 3 1024.85 7.53 0 -6 -3 1005.47 6.34 0 -6 -4 2004.12 11.34 0 -6 4 1935.89 12.52 0 -6 5 257.12 3.74 0 -6 -5 235.23 2.81 0 -6 -6 534.68 4.87 0 -6 6 513.73 5.77 0 -6 7 351.92 5.03 0 -6 -7 365.47 4.36 0 -6 8 205.15 4.43 0 -6 9 59.37 3.45 0 -6 10 173.03 4.65 0 -6 11 76.42 4.36 0 -6 12 1.41 4.06 0 -6 13 161.36 6.00 0 -5 0 1.00 0.60 0 -5 1 2984.65 16.69 0 -5 -1 2935.22 16.75 0 -5 -2 932.33 5.59 0 -5 -2 917.19 6.66 0 -5 -3 756.20 4.95 0 -5 3 746.25 5.75 0 -5 4 595.42 5.55 0 -5 4 601.53 5.25 0 -5 -5 613.17 4.93 0 -5 5 600.60 5.76 0 -5 -6 162.27 2.62 0 -5 6 170.46 3.26 0 -5 7 95.77 3.36 0 -5 7 101.67 2.97 0 -5 8 34.24 2.67 0 -5 -8 40.03 2.35 0 -5 8 34.96 2.87 0 -5 9 732.13 7.93 0 -5 9 805.82 8.56 0 -5 10 58.62 3.50 0 -5 11 97.86 4.28 0 -5 12 114.83 4.81 0 -5 13 55.73 4.96 0 -4 0 1267.12 7.78 0 -4 0 1314.40 7.43 0 -4 -1 1890.62 10.99 0 -4 -1 1904.48 10.16 0 -4 1 1899.78 10.82 0 -4 -2 1038.93 5.92 0 -4 2 1032.10 6.60 0 -4 3 2471.90 14.11 0 -4 -3 2469.15 13.24 0 -4 4 1524.05 9.98 0 -4 -4 1533.50 9.13 0 -4 -5 1282.10 8.29 0 -4 5 1258.11 8.88 0 -4 -5 1253.18 9.21 0 -4 -6 243.47 3.20 0 -4 6 234.79 3.57 0 -4 7 323.12 4.78 0 -4 -7 320.08 4.08 0 -4 8 840.71 8.13 0 -4 8 855.97 8.31 0 -4 -8 837.07 7.43 0 -4 9 191.91 4.63 0 -4 9 225.91 5.02 0 -4 10 461.72 6.78 0 -4 10 445.18 6.45 0 -4 11 169.58 5.06 0 -4 12 33.09 4.18 0 -4 13 7.42 3.87 0 -3 0 0.58 0.44 0 -3 0 1.09 0.50 0 -3 -1 49.72 0.71 0 -3 -1 51.23 1.09 0 -3 2 9991.39 50.07 0 -3 2 9999.00 49.88 0 -3 3 24.95 1.08 0 -3 -3 14.45 0.79 0 -3 -4 1033.37 6.62 0 -3 4 1009.06 7.13 0 -3 -5 972.66 6.74 0 -3 -5 981.32 7.64 0 -3 6 1130.65 8.72 0 -3 -6 1140.84 8.13 0 -3 7 232.75 3.93 0 -3 -7 236.66 3.59 0 -3 8 1343.27 10.68 0 -3 8 1313.45 10.49 0 -3 9 1036.09 9.58 0 -3 9 1104.54 9.88 0 -3 10 222.68 4.87 0 -3 10 260.69 5.36 0 -3 11 9.74 3.39 0 -3 11 8.45 3.39 0 -3 12 153.41 5.17 0 -3 13 79.63 4.95 0 -2 0 1885.39 9.98 0 -2 0 1908.90 9.72 0 -2 1 5605.78 28.02 0 -2 2 2372.89 13.01 0 -2 -2 2448.24 12.61 0 -2 -3 4002.10 21.06 0 -2 3 4159.61 21.52 0 -2 -4 99.15 1.95 0 -2 4 95.29 1.93 0 -2 5 164.44 2.73 0 -2 -5 163.41 2.75 0 -2 -6 1254.23 8.80 0 -2 -6 1205.02 9.11 0 -2 6 1194.46 9.03 0 -2 6 1258.14 9.14 0 -2 7 1045.44 8.54 0 -2 -7 1040.99 8.12 0 -2 8 451.41 5.60 0 -2 8 417.27 5.33 0 -2 9 59.82 2.87 0 -2 9 71.98 3.31 0 -2 10 75.23 3.76 0 -2 10 69.30 3.77 0 -2 11 469.03 7.37 0 -2 11 469.84 6.95 0 -2 12 32.39 4.08 0 -2 12 33.17 3.96 0 -2 13 98.34 5.21 0 -1 -1 3144.88 15.06 0 -1 1 2822.51 15.30 0 -1 2 1077.11 6.45 0 -1 -2 1183.16 6.43 0 -1 -3 1680.43 9.47 0 -1 -3 1675.39 9.83 0 -1 3 1658.78 9.63 0 -1 -4 1094.81 7.22 0 -1 4 1079.11 7.36 0 -1 4 1104.34 7.40 0 -1 5 2565.49 14.98 0 -1 5 2577.28 15.22 0 -1 -6 637.23 5.94 0 -1 6 653.05 5.87 0 -1 6 643.09 5.88 0 -1 7 131.06 3.04 0 -1 -7 126.68 2.97 0 -1 8 428.04 5.52 0 -1 8 434.07 5.47 0 -1 9 294.11 4.83 0 -1 10 68.56 3.62 0 -1 10 70.05 3.69 0 -1 11 39.78 3.81 0 -1 11 31.27 3.36 0 -1 12 100.69 4.59 0 -1 12 93.14 4.68 0 -1 13 87.63 5.31 0 0 1 7.33 0.32 0 0 -1 2271.13 3.51 0 0 2 594.34 3.92 0 0 -2 607.68 3.89 0 0 3 864.60 5.83 0 0 -3 857.35 5.84 0 0 4 2817.13 15.73 0 0 -4 2848.19 15.99 0 0 -5 1426.32 9.30 0 0 -5 1358.91 9.23 0 0 5 1388.67 9.04 0 0 5 1320.30 9.11 0 0 -6 514.45 5.24 0 0 6 512.88 5.03 0 0 -6 499.99 4.97 0 0 7 392.12 4.93 0 0 7 405.46 4.72 0 0 8 412.64 5.16 0 0 8 388.55 5.37 0 0 9 0.46 2.43 0 0 9 2.05 2.56 0 0 10 526.40 6.45 0 0 10 528.52 7.03 0 0 11 47.34 3.81 0 0 11 47.09 3.75 0 0 12 147.22 4.98 0 0 12 134.85 5.05 0 0 13 7.66 3.65 0 1 1 3055.97 15.21 0 1 2 952.54 5.50 0 1 -2 965.53 5.72 0 1 2 956.77 5.82 0 1 -3 1800.17 10.19 0 1 3 1807.95 9.88 0 1 4 1095.79 7.14 0 1 -4 1107.91 7.44 0 1 5 2536.08 15.22 0 1 -5 2555.08 15.19 0 1 -5 2600.77 15.21 0 1 5 2490.88 14.67 0 1 -6 681.09 6.05 0 1 6 677.47 5.75 0 1 -6 667.05 5.99 0 1 6 673.85 6.14 0 1 7 133.04 2.82 0 1 7 127.51 3.18 0 1 8 497.25 5.55 0 1 8 497.15 6.16 0 1 9 437.02 5.99 0 1 9 463.24 5.83 0 1 10 71.74 3.88 0 1 10 70.66 3.43 0 1 11 46.81 3.67 0 1 11 55.77 3.51 0 1 12 67.65 4.27 0 1 12 74.69 4.33 0 1 13 116.95 5.47 0 1 13 116.91 4.70 0 2 0 1697.02 8.93 0 2 1 5388.15 26.81 0 2 -1 5492.87 27.23 0 2 -2 2297.46 12.37 0 2 2 2304.56 12.04 0 2 3 4019.81 21.55 0 2 3 4064.15 20.86 0 2 -3 4046.40 21.31 0 2 -3 4013.96 21.51 0 2 4 77.17 1.75 0 2 -4 81.21 1.80 0 2 4 80.11 1.52 0 2 5 194.99 3.01 0 2 -5 186.38 2.85 0 2 5 188.69 2.56 0 2 -5 184.75 2.96 0 2 -6 1146.51 8.59 0 2 6 1160.62 8.87 0 2 -6 1170.16 8.92 0 2 6 1166.59 8.17 0 2 7 1001.47 7.78 0 2 7 971.55 8.36 0 2 8 488.22 6.10 0 2 8 454.48 5.29 0 2 9 62.94 3.41 0 2 9 61.00 2.97 0 2 10 108.96 4.25 0 2 10 102.38 3.52 0 2 11 466.22 6.36 0 2 11 460.94 7.19 0 2 12 43.95 3.89 0 2 12 40.37 4.15 0 2 -13 93.68 5.34 0 2 13 91.66 4.73 0 3 0 0.47 0.41 0 3 1 59.29 0.80 0 3 -1 58.38 1.03 0 3 -2 9831.06 49.13 0 3 3 49.83 1.02 0 3 -3 51.69 1.34 0 3 4 1016.91 7.31 0 3 -4 1015.59 7.07 0 3 4 1029.42 6.52 0 3 5 902.55 6.33 0 3 5 884.51 7.07 0 3 -5 892.31 6.87 0 3 -5 898.83 7.12 0 3 6 1088.56 8.78 0 3 6 1079.87 7.71 0 3 7 220.77 3.28 0 3 7 216.60 3.89 0 3 8 1273.97 10.39 0 3 8 1211.13 9.16 0 3 9 1077.83 8.81 0 3 9 1089.84 10.06 0 3 10 312.88 5.20 0 3 10 279.97 5.43 0 3 11 16.36 3.88 0 3 -12 168.26 5.92 0 3 12 164.04 4.64 0 3 12 158.09 5.45 0 3 -13 98.58 5.78 0 3 13 73.92 4.84 0 4 0 1286.28 7.43 0 4 0 1284.98 7.81 0 4 1 1919.39 10.31 0 4 -1 1940.46 10.86 0 4 -1 1921.82 10.74 0 4 -1 1916.59 10.95 0 4 -2 914.97 6.55 0 4 -2 915.40 6.21 0 4 3 2630.97 14.26 0 4 -3 2822.90 15.11 0 4 -4 1736.16 10.54 0 4 4 1695.41 9.80 0 4 -5 1384.81 9.33 0 4 5 1390.96 8.71 0 4 -6 238.67 3.60 0 4 6 239.92 3.09 0 4 7 291.22 3.75 0 4 7 282.51 4.49 0 4 8 739.71 6.52 0 4 8 713.01 7.52 0 4 9 218.30 3.98 0 4 9 216.80 4.72 0 4 10 351.52 6.37 0 4 10 347.05 5.13 0 4 11 182.41 5.37 0 4 -11 196.65 5.80 0 4 11 185.24 4.51 0 4 -12 31.89 4.66 0 4 12 26.78 3.61 0 4 12 24.64 4.45 0 4 13 20.08 4.81 0 5 0 0.51 0.78 0 5 0 0.57 0.65 0 5 0 0.90 0.78 0 5 -1 2908.36 16.14 0 5 -1 2999.59 15.92 0 5 1 2840.11 16.53 0 5 -1 3050.90 16.25 0 5 1 2959.39 15.61 0 5 2 1119.47 6.48 0 5 -2 1095.78 7.14 0 5 -3 592.72 5.39 0 5 -3 597.48 5.04 0 5 -4 648.28 5.34 0 5 4 619.98 4.53 0 5 5 556.71 5.63 0 5 -5 555.76 5.13 0 5 6 151.48 2.51 0 5 6 147.40 3.32 0 5 7 107.41 2.41 0 5 7 103.04 3.12 0 5 8 41.66 2.29 0 5 8 38.15 2.92 0 5 9 702.79 8.28 0 5 9 679.42 6.57 0 5 10 46.58 2.93 0 5 -10 51.63 4.16 0 5 10 43.81 3.79 0 5 11 98.03 3.78 0 5 11 91.27 4.72 0 5 12 130.79 5.46 0 5 -12 134.63 5.67 0 6 0 2705.93 15.00 0 6 0 2733.09 15.67 0 6 0 2717.29 15.44 0 6 1 977.38 7.02 0 6 -1 968.53 6.77 0 6 -1 1029.36 6.95 0 6 -1 940.26 6.39 0 6 1 993.69 7.20 0 6 1 989.10 6.31 0 6 -2 57.54 1.61 0 6 -2 49.51 1.65 0 6 2 57.80 1.18 0 6 -2 51.45 1.52 0 6 -3 1031.84 7.46 0 6 3 1043.94 6.47 0 6 -4 1864.24 12.12 0 6 4 1835.22 10.64 0 6 -4 1817.58 11.51 0 6 -4 1877.63 12.66 0 6 5 251.80 2.87 0 6 5 247.37 3.88 0 6 -6 545.13 5.54 0 6 6 538.16 4.76 0 6 -7 222.64 4.66 0 6 7 215.57 4.27 0 6 7 220.57 3.10 0 6 8 310.57 5.30 0 6 8 320.77 4.14 0 6 9 78.60 3.88 0 6 9 77.07 2.77 0 6 10 171.39 3.79 0 6 10 172.78 5.20 0 6 -11 87.40 4.85 0 6 11 79.03 4.74 0 6 -12 3.09 4.78 0 6 12 1.01 4.37 0 7 0 1.45 1.22 0 7 0 0.38 1.04 0 7 0 0.24 1.14 0 7 1 2072.60 12.08 0 7 -1 2078.78 12.70 0 7 1 2084.78 13.00 0 7 -1 2108.02 12.81 0 7 -2 1583.73 10.05 0 7 2 1522.28 10.62 0 7 -2 1577.87 10.19 0 7 2 1593.42 9.31 0 7 -2 1518.18 10.46 0 7 -3 99.74 2.30 0 7 -3 94.73 2.54 0 7 3 93.96 1.57 0 7 -4 954.53 8.28 0 7 -4 948.42 7.69 0 7 -5 2647.69 15.74 0 7 -5 2668.88 17.08 0 7 6 826.89 8.02 0 7 6 859.77 6.37 0 7 7 213.76 4.46 0 7 7 192.31 2.91 0 7 8 122.19 3.97 0 7 -8 122.36 4.41 0 7 8 132.01 2.88 0 7 9 213.69 3.75 0 7 -9 212.72 5.32 0 7 9 210.55 5.24 0 7 -10 121.24 5.29 0 7 10 119.35 4.86 0 7 -11 15.70 4.60 0 7 11 16.03 4.14 0 7 12 28.38 4.86 0 7 -12 30.05 5.19 0 8 0 539.32 5.38 0 8 0 540.85 4.77 0 8 -1 364.47 3.92 0 8 -1 379.46 4.06 0 8 1 374.93 4.47 0 8 1 368.69 4.25 0 8 1 359.97 3.56 0 8 -1 380.44 3.77 0 8 2 80.59 2.35 0 8 -2 81.15 2.11 0 8 -2 79.76 2.05 0 8 2 79.62 2.29 0 8 -2 72.62 2.16 0 8 3 1474.85 11.08 0 8 3 1554.13 9.34 0 8 -3 1529.75 11.14 0 8 -3 1593.31 10.55 0 8 -3 1617.31 10.58 0 8 -4 332.34 4.12 0 8 -4 313.89 4.64 0 8 5 93.02 1.94 0 8 -5 101.34 3.32 0 8 6 302.19 3.32 0 8 -6 306.13 5.21 0 8 7 1973.37 12.02 0 8 7 1923.18 14.59 0 8 8 137.17 2.86 0 8 8 137.95 4.26 0 8 9 30.29 2.45 0 8 9 29.84 3.80 0 8 -10 167.85 5.76 0 8 10 153.63 5.06 0 8 11 65.84 4.87 0 8 -11 74.26 5.38 0 8 12 94.66 5.62 0 9 0 0.30 1.45 0 9 0 0.63 1.38 0 9 -1 342.41 4.15 0 9 -1 351.33 4.20 0 9 -1 346.88 3.75 0 9 1 362.19 4.37 0 9 1 357.44 4.62 0 9 1 356.61 3.73 0 9 -2 871.17 7.41 0 9 2 845.69 6.16 0 9 2 854.70 7.29 0 9 2 884.93 7.73 0 9 -2 890.82 6.92 0 9 -2 863.51 6.94 0 9 -3 240.71 3.52 0 9 -3 211.52 3.60 0 9 3 236.84 2.74 0 9 -3 255.06 3.67 0 9 3 218.95 3.86 0 9 4 276.58 2.94 0 9 -4 267.99 4.49 0 9 -5 181.25 4.17 0 9 5 185.80 2.58 0 9 -6 955.68 9.55 0 9 6 906.44 6.57 0 9 -7 184.96 5.14 0 9 7 175.52 2.95 0 9 8 95.17 4.17 0 9 8 87.00 2.42 0 9 -8 93.41 4.65 0 9 9 92.06 4.36 0 9 10 30.96 4.26 0 9 11 171.57 5.86 0 9 -11 207.09 6.77 0 10 0 924.82 8.29 0 10 0 887.34 7.15 0 10 1 666.92 6.78 0 10 -1 672.06 5.68 0 10 1 677.39 5.70 0 10 -1 709.00 6.53 0 10 -1 665.19 6.19 0 10 -1 703.27 6.88 0 10 2 213.25 3.95 0 10 -2 210.27 3.40 0 10 -2 213.49 3.71 0 10 2 223.97 2.97 0 10 3 640.99 6.91 0 10 3 647.70 5.19 0 10 4 853.69 6.14 0 10 4 846.46 8.26 0 10 -5 301.67 5.27 0 10 5 300.09 3.31 0 10 6 329.50 3.53 0 10 -6 359.14 6.13 0 10 7 460.82 4.43 0 10 -7 482.30 7.12 0 10 -8 165.70 5.31 0 10 8 151.22 4.65 0 10 9 67.64 4.51 0 10 -9 68.28 4.84 0 10 10 227.91 6.00 0 10 11 128.19 5.73 0 11 0 0.46 1.68 0 11 0 2.71 1.44 0 11 0 0.40 2.14 0 11 -1 560.69 6.41 0 11 -1 563.07 5.88 0 11 1 595.36 5.46 0 11 -1 566.73 5.32 0 11 1 599.11 6.80 0 11 2 615.22 6.89 0 11 -2 627.03 6.54 0 11 -2 607.81 5.84 0 11 3 526.72 4.68 0 11 3 513.40 6.41 0 11 -3 517.08 6.32 0 11 4 136.01 3.90 0 11 4 134.20 2.33 0 11 -4 130.39 3.86 0 11 5 1327.00 11.59 0 11 5 1337.47 8.49 0 11 6 350.52 3.67 0 11 -6 366.58 6.38 0 11 -7 24.96 3.72 0 11 -8 219.92 6.05 0 11 8 182.54 5.43 0 11 -9 352.84 7.44 0 11 -10 67.23 5.47 0 11 10 59.70 4.88 0 12 0 337.52 5.42 0 12 0 326.60 3.99 0 12 -1 87.63 2.56 0 12 -1 94.32 3.38 0 12 1 87.64 3.44 0 12 -1 95.70 3.01 0 12 1 89.37 2.51 0 12 2 372.74 4.17 0 12 -2 363.60 5.09 0 12 3 73.01 3.29 0 12 -3 68.55 3.18 0 12 3 73.97 2.15 0 12 4 894.80 9.10 0 12 -4 906.66 9.21 0 12 4 922.47 6.73 0 12 -5 43.30 3.58 0 12 5 45.08 3.58 0 12 -6 82.19 4.06 0 12 6 88.32 4.09 0 12 -7 78.90 4.48 0 12 -8 137.27 5.45 0 12 -9 8.80 4.70 0 12 9 8.04 4.26 0 12 10 109.44 5.46 0 12 -10 123.06 6.13 0 13 0 0.28 1.82 0 13 0 0.52 1.98 0 13 0 0.60 2.79 0 13 -1 442.28 6.46 0 13 1 417.94 4.80 0 13 -1 417.60 5.39 0 13 1 396.86 4.37 0 13 1 424.07 6.16 0 13 -2 754.56 7.68 0 13 2 798.87 6.73 0 13 -2 873.61 9.13 0 13 2 826.10 8.89 0 13 -3 78.58 3.53 0 13 3 72.29 2.32 0 13 3 72.57 3.65 0 13 -4 143.56 4.53 0 13 4 141.85 4.22 0 13 5 413.94 6.84 0 13 -5 387.56 6.70 0 13 -6 294.54 6.34 0 13 6 275.29 5.85 0 13 -7 16.05 4.38 0 13 -8 252.85 6.59 0 13 -9 178.17 6.21 0 14 0 410.99 5.34 0 14 0 453.92 6.92 0 14 -1 383.68 5.54 0 14 1 387.76 6.57 0 14 -1 385.12 6.26 0 14 -2 225.26 5.16 0 14 2 235.96 5.23 0 14 2 227.01 3.69 0 14 -2 229.96 4.86 0 14 -3 847.74 9.03 0 14 3 928.02 10.01 0 14 -4 444.32 6.98 0 14 4 442.63 6.88 0 14 -5 3.65 3.73 0 14 5 2.34 3.57 0 14 -6 192.53 5.74 0 14 6 187.36 5.32 0 14 -7 582.73 8.93 0 14 7 535.27 8.33 0 14 -8 52.26 5.16 0 14 -9 18.81 5.10 0 15 0 3.11 3.42 0 15 0 0.79 2.62 0 15 1 165.39 3.94 0 15 -1 164.56 5.05 0 15 1 171.08 5.14 0 15 2 604.36 8.33 0 15 -2 592.99 7.46 0 15 -2 584.59 8.05 0 15 3 139.75 4.85 0 15 -3 149.77 4.99 0 15 -3 145.89 4.50 0 15 4 47.18 3.98 0 15 -4 44.11 3.86 0 15 5 62.04 4.64 0 15 -5 59.53 4.29 0 15 -6 92.20 5.25 0 15 6 80.02 4.71 0 15 7 49.86 4.71 0 15 -7 50.45 5.21 0 15 8 83.87 5.64 0 16 0 612.08 8.46 0 16 0 615.81 7.15 0 16 -1 160.71 4.28 0 16 -1 177.69 5.44 0 16 1 165.51 5.32 0 16 -2 111.11 4.28 0 16 2 111.83 4.85 0 16 -2 114.63 4.97 0 16 -3 171.82 5.40 0 16 -3 170.75 5.21 0 16 3 170.65 5.49 0 16 4 324.67 6.85 0 16 -4 331.55 6.72 0 16 5 21.21 4.64 0 16 -5 22.09 4.10 0 16 6 138.50 5.52 0 16 -7 224.26 6.55 0 16 7 225.02 6.54 0 17 0 1.20 4.05 0 17 -1 209.48 6.11 0 17 1 210.22 5.93 0 17 -2 369.16 6.53 0 17 -2 357.96 7.05 0 17 2 361.78 7.19 0 17 -3 139.40 5.53 0 17 3 128.45 5.53 0 17 -3 129.59 5.03 0 17 4 89.63 5.12 0 17 -4 79.34 5.16 0 17 -5 379.91 7.46 0 17 -5 392.98 7.54 0 17 6 180.05 6.15 0 17 -6 178.77 6.10 0 17 -7 29.97 5.62 0 18 0 143.08 5.75 0 18 1 100.60 5.24 0 18 -1 106.90 5.34 0 18 2 2.28 4.28 0 18 -2 2.71 4.37 0 18 3 81.49 5.41 0 18 -3 76.45 5.22 0 18 4 103.22 5.62 0 18 -4 97.03 5.22 0 18 -4 97.92 5.46 0 18 -5 13.05 4.55 0 18 -5 9.93 4.85 0 18 -6 84.85 5.71 0 18 -6 73.72 5.14 0 19 0 2.59 4.57 0 19 1 129.41 5.94 0 19 -1 129.52 6.13 0 19 2 106.22 5.53 0 19 -2 107.01 5.71 0 19 -4 58.01 5.57 1 -17 5 182.87 6.36 1 -17 6 57.80 5.28 -1 -16 6 139.69 4.92 1 -16 4 214.14 6.15 1 -16 5 214.96 6.20 1 -16 6 33.86 4.67 1 -16 7 60.02 5.28 -1 -15 7 14.97 3.70 -1 -15 6 37.66 4.09 -1 -15 5 229.97 5.18 1 -15 3 385.73 6.92 1 -15 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173.19 4.36 1 3 9 111.34 3.24 1 3 9 107.74 4.01 -1 3 -9 120.40 4.28 -1 3 -10 112.32 4.33 1 3 10 109.99 4.67 1 3 10 106.65 3.67 1 3 11 80.03 4.62 1 3 12 23.56 4.28 -1 3 -12 25.52 4.46 -1 3 -13 50.15 5.25 -1 4 13 35.92 4.62 -1 4 12 7.40 3.78 -1 4 12 7.78 3.55 -1 4 11 113.94 4.69 -1 4 11 110.02 3.88 -1 4 10 590.45 7.53 -1 4 10 588.32 6.70 -1 4 9 1.96 2.72 -1 4 9 2.78 2.32 -1 4 8 530.82 5.59 -1 4 8 547.10 6.38 1 4 -7 880.44 7.40 -1 4 7 863.26 7.10 -1 4 6 778.75 6.27 1 4 -6 782.11 6.41 -1 4 6 788.83 6.98 -1 4 5 42.54 1.58 1 4 -5 45.31 1.69 -1 4 5 43.70 1.89 1 4 -4 1804.27 11.62 -1 4 4 1806.81 11.49 -1 4 3 4288.37 23.05 1 4 -3 4311.63 22.20 -1 4 3 4309.11 22.56 -1 4 2 1521.70 8.87 -1 4 2 1504.64 9.22 1 4 -1 1567.12 8.72 1 4 -1 1567.26 8.72 -1 4 1 1518.09 9.40 -1 4 1 1541.81 9.37 -1 4 1 1591.66 9.13 1 4 0 3382.89 17.24 1 4 0 3359.33 17.15 -1 4 0 3418.64 18.24 -1 4 -1 4377.61 23.80 1 4 1 4573.49 23.52 -1 4 -2 169.60 2.19 1 4 2 168.87 2.25 1 4 3 80.38 1.06 -1 4 -3 80.06 1.83 -1 4 -4 2519.35 15.12 1 4 4 2571.97 13.77 -1 4 -5 127.73 2.95 -1 4 -5 136.04 2.85 1 4 5 129.14 1.96 -1 4 -5 134.26 2.79 1 4 6 103.56 2.08 1 4 6 99.06 3.08 1 4 7 1030.87 9.28 -1 4 -7 1041.63 9.48 1 4 8 429.04 6.06 -1 4 -8 460.72 6.44 -1 4 -9 58.85 3.74 1 4 9 61.06 3.68 1 4 9 59.90 2.87 1 4 10 139.30 4.86 1 4 10 139.84 3.74 1 4 11 204.12 5.98 -1 4 -11 211.77 5.84 -1 4 -12 30.40 5.09 1 5 -13 183.49 6.58 -1 5 12 212.48 5.95 -1 5 12 215.83 5.01 -1 5 11 125.94 3.64 -1 5 11 136.39 4.91 -1 5 10 121.83 3.69 -1 5 10 122.50 4.48 -1 5 9 622.50 6.40 -1 5 9 568.05 7.05 -1 5 8 286.74 4.17 -1 5 8 261.12 4.59 -1 5 7 37.66 2.09 1 5 -7 37.86 2.20 -1 5 7 36.92 2.50 -1 5 6 457.02 5.31 -1 5 6 462.19 4.66 -1 5 5 2201.33 14.22 -1 5 5 2325.13 13.59 1 5 -5 2232.34 14.33 1 5 -5 2293.02 13.45 -1 5 4 787.38 5.96 1 5 -4 777.84 6.42 1 5 -4 861.70 6.03 -1 5 4 840.58 6.80 1 5 -3 37.78 1.43 -1 5 3 39.44 1.56 1 5 -3 40.52 1.21 -1 5 3 39.82 1.31 -1 5 2 1506.46 9.03 1 5 -2 1509.60 8.74 1 5 -1 1471.53 8.75 1 5 -1 1457.86 8.56 1 5 -1 1488.66 8.67 1 5 0 1093.29 6.94 -1 5 0 1098.83 7.00 1 5 0 997.78 5.85 1 5 0 1004.04 5.99 1 5 0 1062.96 6.73 1 5 1 288.78 2.99 -1 5 -1 284.45 3.11 1 5 1 285.06 1.93 1 5 2 327.42 2.05 -1 5 -2 333.46 3.48 1 5 3 1399.01 7.43 -1 5 -3 1436.58 9.31 1 5 4 793.12 4.90 -1 5 -4 688.07 5.81 -1 5 -5 550.84 5.51 -1 5 -5 522.53 5.28 -1 5 -5 523.76 5.95 1 5 5 541.19 4.13 -1 5 -6 563.06 6.52 1 5 6 531.97 4.47 -1 5 -7 280.76 5.13 1 5 7 269.53 3.40 1 5 8 487.95 6.77 -1 5 -8 505.54 7.06 1 5 9 289.53 4.30 1 5 9 297.20 5.77 1 5 10 272.04 4.51 1 5 10 268.03 5.91 -1 5 -10 284.16 6.21 1 5 11 13.89 4.18 -1 5 -11 18.67 4.46 -1 5 -12 101.16 5.66 1 5 12 91.36 5.14 -1 6 13 237.03 6.46 -1 6 12 34.87 4.51 1 6 -12 37.36 4.91 -1 6 11 171.96 4.32 -1 6 11 169.18 5.33 -1 6 10 226.06 4.42 -1 6 10 216.64 5.08 -1 6 9 287.75 4.39 -1 6 9 281.85 5.30 -1 6 8 165.84 3.97 -1 6 8 168.81 3.28 -1 6 7 929.46 8.57 -1 6 7 926.15 7.37 -1 6 6 181.64 3.64 -1 6 6 184.36 2.91 -1 6 5 103.20 2.70 1 6 -5 109.18 2.34 -1 6 5 102.53 2.16 1 6 -5 104.26 2.68 1 6 -4 189.99 3.10 -1 6 4 184.80 2.58 -1 6 4 181.21 3.02 -1 6 3 923.23 7.25 1 6 -3 950.01 6.47 -1 6 3 896.97 6.47 1 6 -3 870.21 6.62 1 6 -2 1640.15 9.79 -1 6 2 1679.92 10.02 1 6 -1 538.35 4.27 1 6 -1 520.54 4.22 1 6 -1 565.63 4.59 -1 6 1 550.43 4.56 1 6 -1 524.02 3.98 1 6 0 2209.79 12.75 1 6 0 2245.43 12.01 -1 6 0 2134.73 12.96 1 6 0 2179.11 13.01 1 6 0 2167.88 11.78 -1 6 -1 1858.99 11.25 1 6 1 1824.85 11.18 1 6 1 1815.05 9.63 -1 6 -1 1860.67 11.52 1 6 2 350.82 3.81 -1 6 -2 348.61 4.00 1 6 2 340.20 2.26 -1 6 -3 2471.54 14.49 1 6 3 2422.80 12.32 1 6 3 2243.31 14.38 -1 6 -3 2226.15 14.83 -1 6 -3 2397.35 14.30 1 6 4 467.99 3.28 1 6 4 460.61 5.07 1 6 5 35.15 1.22 -1 6 -5 38.96 2.13 1 6 6 237.63 2.78 -1 6 -6 265.83 4.83 1 6 7 890.31 6.68 -1 6 -7 986.99 9.62 1 6 8 634.91 7.68 1 6 8 643.33 5.77 1 6 9 81.06 4.40 1 6 9 79.90 2.72 -1 6 -9 89.83 4.67 -1 6 -10 194.48 5.57 1 6 10 174.36 5.47 1 6 11 198.21 6.01 -1 6 -11 221.07 6.59 -1 6 -12 33.06 5.09 1 6 12 33.14 5.00 -1 7 12 53.63 4.76 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1629.93 12.41 1 7 5 1741.19 9.68 1 7 6 1254.27 7.81 -1 7 -7 275.18 5.44 1 7 8 117.36 2.59 1 7 8 116.61 4.33 -1 7 -9 284.02 6.31 1 7 9 259.00 5.82 -1 7 -10 199.56 6.04 1 7 10 180.05 5.56 -1 7 -11 28.50 4.79 1 7 11 21.22 4.31 -1 7 -12 123.96 6.01 -1 8 12 54.66 5.03 1 8 -12 56.51 5.25 -1 8 11 171.16 5.62 1 8 -11 188.38 6.26 -1 8 10 209.70 4.14 -1 8 10 206.37 5.38 -1 8 9 95.62 4.16 -1 8 9 95.35 3.11 -1 8 8 128.09 3.10 -1 8 8 126.48 4.13 -1 8 7 795.45 6.66 -1 8 7 806.57 8.32 -1 8 6 343.59 5.11 -1 8 6 351.01 4.11 1 8 -5 154.68 3.59 -1 8 5 139.93 3.46 -1 8 5 131.77 2.41 1 8 -5 152.45 2.87 1 8 -4 681.31 5.75 1 8 -4 673.65 6.12 -1 8 4 671.04 6.77 1 8 -3 1176.77 8.53 1 8 -3 1172.55 9.02 -1 8 3 1180.71 8.20 1 8 -2 770.20 6.32 1 8 -2 773.76 5.97 1 8 -1 246.43 3.01 -1 8 1 241.25 3.43 1 8 -1 253.60 2.90 -1 8 1 254.65 3.29 1 8 -1 266.05 3.25 1 8 -1 271.10 3.53 1 8 0 1655.87 10.00 -1 8 0 1676.31 11.12 -1 8 0 1683.92 11.23 1 8 0 1697.27 9.91 1 8 0 1753.62 11.41 1 8 0 1722.43 11.08 1 8 1 474.60 4.91 1 8 1 507.55 3.75 1 8 1 437.06 3.35 1 8 1 459.88 4.68 -1 8 -1 443.94 4.52 -1 8 -1 479.48 4.98 -1 8 -2 88.59 2.46 -1 8 -2 92.70 2.27 1 8 2 88.43 2.56 1 8 2 85.85 1.26 1 8 3 1283.72 9.70 -1 8 -3 1361.65 9.43 -1 8 -3 1245.55 9.91 -1 8 -3 1339.42 9.42 1 8 3 1234.97 6.99 1 8 4 645.16 6.58 1 8 4 649.26 4.11 -1 8 -5 878.48 8.62 1 8 5 896.88 8.40 1 8 6 245.75 2.60 1 8 7 289.96 3.17 -1 8 -8 208.14 5.57 1 8 9 24.83 3.54 -1 8 -9 28.95 4.20 1 8 10 42.60 4.60 -1 8 -10 45.39 4.82 1 8 11 121.65 5.51 -1 8 -11 115.39 5.94 -1 9 11 261.96 6.48 -1 9 10 69.65 4.34 -1 9 9 406.60 6.74 -1 9 9 439.52 5.31 -1 9 8 384.27 4.67 -1 9 8 385.86 6.20 -1 9 7 496.55 5.20 -1 9 7 484.19 6.59 -1 9 6 1.60 2.35 -1 9 6 2.11 1.79 1 9 -6 1.64 2.69 1 9 -5 901.72 7.32 1 9 -5 891.60 8.44 -1 9 5 886.05 8.54 1 9 -4 291.11 4.51 -1 9 4 290.63 3.49 1 9 -3 129.70 3.00 1 9 -3 128.77 2.70 -1 9 3 123.49 2.41 1 9 -2 1335.52 9.53 1 9 -2 1354.20 9.11 -1 9 2 1330.08 9.31 -1 9 1 2146.94 13.40 -1 9 1 2115.42 13.78 -1 9 1 2175.75 14.58 1 9 -1 2079.73 13.16 1 9 -1 2188.33 13.09 1 9 -1 2104.81 12.63 1 9 -1 2124.93 13.78 -1 9 0 199.67 3.27 1 9 0 198.59 3.37 -1 9 0 203.77 3.53 1 9 0 199.04 3.19 -1 9 0 193.96 3.17 1 9 0 183.74 2.54 1 9 0 188.45 2.41 -1 9 -1 637.17 5.97 1 9 1 650.81 6.24 1 9 1 624.57 5.85 -1 9 -1 631.11 6.15 1 9 1 610.42 4.42 -1 9 -2 1293.98 10.08 1 9 2 1280.26 7.52 -1 9 -2 1298.16 9.51 1 9 3 247.76 2.16 1 9 3 256.61 4.23 -1 9 -3 248.73 4.35 1 9 4 69.31 2.78 1 9 4 74.19 1.18 -1 9 -4 72.62 3.16 1 9 5 752.89 7.77 -1 9 -5 754.11 8.10 1 9 6 603.78 4.35 -1 9 -6 631.97 7.94 -1 9 -9 484.31 8.23 -1 9 -10 112.85 5.58 1 9 10 105.79 5.34 1 9 11 26.14 4.75 -1 9 -11 27.28 5.16 -1 10 11 112.20 5.55 -1 10 10 59.16 4.64 1 10 -10 62.57 4.99 -1 10 9 189.71 5.55 1 10 -9 211.94 5.85 -1 10 8 106.63 4.52 -1 10 8 99.20 2.88 -1 10 7 233.65 3.58 -1 10 7 225.66 4.90 1 10 -6 452.45 6.47 -1 10 6 464.16 6.60 -1 10 5 24.72 1.83 1 10 -5 29.27 2.89 -1 10 5 31.11 2.78 1 10 -4 822.10 7.95 -1 10 4 821.68 6.72 1 10 -3 1523.31 11.37 -1 10 3 1515.23 10.33 1 10 -2 18.90 2.07 1 10 -2 17.56 1.73 -1 10 2 22.03 2.39 1 10 -2 17.57 2.07 1 10 -2 17.87 1.75 -1 10 2 19.27 1.85 1 10 -1 329.15 4.10 1 10 -1 319.00 3.60 -1 10 1 328.47 4.80 -1 10 1 323.92 4.19 1 10 0 1499.29 10.68 -1 10 0 1558.30 11.04 -1 10 0 1629.64 12.09 1 10 0 1542.45 11.25 1 10 0 1453.00 9.39 1 10 0 1546.82 9.89 1 10 1 1050.26 7.01 1 10 1 1032.15 6.79 1 10 1 1056.22 8.83 -1 10 -2 195.09 3.85 1 10 2 191.29 3.74 1 10 2 189.69 2.13 1 10 3 1244.27 10.39 -1 10 -3 1232.23 10.64 1 10 4 533.77 6.62 -1 10 -4 512.72 6.65 1 10 5 270.50 4.99 -1 10 -5 261.00 5.21 1 10 6 209.37 4.70 -1 10 -6 191.00 4.82 -1 10 -7 315.63 5.90 1 10 7 315.46 6.02 1 10 10 81.80 4.97 -1 10 -10 87.92 5.49 -1 11 11 5.50 4.65 -1 11 10 68.96 4.82 1 11 -10 73.81 5.29 1 11 -9 351.84 7.49 -1 11 9 303.76 6.54 1 11 -8 343.21 7.01 -1 11 8 296.31 6.04 -1 11 7 58.41 2.44 1 11 -7 62.70 3.92 -1 11 7 59.94 4.01 -1 11 6 358.68 5.96 -1 11 6 354.18 4.20 1 11 -5 597.99 7.23 -1 11 5 593.35 5.60 -1 11 4 255.24 3.58 1 11 -4 242.85 4.60 -1 11 3 82.40 2.44 1 11 -3 74.28 2.81 -1 11 2 731.03 7.77 1 11 -2 742.83 6.40 1 11 -2 738.15 7.31 1 11 -2 748.33 7.05 -1 11 2 748.61 6.63 1 11 -1 406.81 5.33 1 11 -1 413.63 4.52 -1 11 1 420.16 4.88 -1 11 0 255.71 4.03 1 11 0 260.02 3.38 1 11 0 246.20 4.13 1 11 0 241.03 3.01 -1 11 -1 181.05 3.79 1 11 1 175.98 2.39 1 11 1 183.68 2.67 1 11 2 500.06 4.04 1 11 2 504.48 6.15 1 11 3 297.96 4.94 -1 11 -3 306.67 5.15 1 11 3 306.97 2.68 1 11 4 108.28 3.56 -1 11 -4 115.59 4.39 -1 11 -5 371.02 6.29 1 11 5 421.57 6.22 1 11 6 42.20 3.51 -1 11 -6 38.04 3.74 1 11 7 19.55 3.55 -1 11 -7 22.66 3.92 -1 11 -8 179.85 5.72 1 12 -10 291.05 7.39 -1 12 10 264.92 6.46 1 12 -9 64.23 5.22 -1 12 9 62.71 4.67 1 12 -8 122.90 5.12 -1 12 8 111.23 4.70 1 12 -7 372.01 6.91 -1 12 7 336.05 6.36 1 12 -6 768.67 8.96 -1 12 6 688.07 6.14 1 12 -5 59.80 3.59 -1 12 5 61.19 2.42 -1 12 4 38.88 2.17 1 12 -4 36.64 2.96 -1 12 3 635.79 6.03 -1 12 3 653.53 7.65 -1 12 2 12.53 2.08 1 12 -2 13.22 2.52 -1 12 2 9.90 2.60 1 12 -2 11.43 1.80 1 12 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892.35 8.28 4 7 -3 161.63 2.73 -4 7 3 167.38 3.24 4 7 -3 160.20 1.86 4 7 -3 160.53 1.87 -4 7 3 164.35 3.66 4 7 -2 153.80 2.03 -4 7 2 154.69 3.50 -4 7 2 150.72 3.05 4 7 -1 886.66 6.07 -4 7 1 905.72 7.59 -4 7 1 912.14 8.54 4 7 0 106.97 2.28 4 7 0 105.67 1.47 4 7 1 486.98 4.87 4 7 2 1123.33 8.69 -4 7 -3 539.47 6.85 4 7 3 551.35 6.09 -4 7 -4 3.60 2.87 4 7 4 10.52 2.57 4 7 5 325.58 5.56 -4 7 -5 310.44 5.86 4 7 6 146.39 4.53 -4 7 -6 141.40 4.67 4 7 7 79.36 4.41 -4 7 -7 76.82 4.53 4 7 8 8.17 3.78 -4 7 -8 5.32 4.19 4 7 9 48.11 5.03 -4 7 -9 48.50 5.02 4 7 10 78.07 5.31 -4 8 13 29.76 4.76 -4 8 12 158.51 5.63 -4 8 12 157.68 5.47 -4 8 11 2.84 3.53 -4 8 11 1.68 3.60 -4 8 10 27.69 3.63 -4 8 10 28.48 3.57 -4 8 9 588.75 7.54 -4 8 9 558.26 7.03 -4 8 8 77.47 3.56 -4 8 8 79.80 3.61 -4 8 7 155.40 3.99 -4 8 7 159.47 4.05 -4 8 6 331.27 5.14 -4 8 6 344.68 5.26 -4 8 5 152.86 3.82 4 8 -5 162.16 2.27 4 8 -5 158.06 2.10 -4 8 5 149.82 3.72 4 8 -4 34.53 1.31 4 8 -4 31.42 2.10 -4 8 4 34.57 2.64 4 8 -4 33.14 1.38 -4 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37.95 1.64 -4 9 2 34.81 2.71 -4 9 2 34.13 2.87 4 9 -2 36.65 1.72 4 9 -1 111.52 2.38 4 9 -1 109.86 1.95 4 9 -1 109.99 2.38 -4 9 1 108.19 3.57 4 9 0 174.74 3.04 4 9 0 172.36 1.81 -4 9 0 177.65 4.27 4 9 0 166.79 1.78 4 9 1 40.89 2.27 -4 9 -1 44.12 3.20 4 9 2 356.01 4.89 -4 9 -2 288.76 5.37 4 9 3 378.16 5.33 4 9 4 806.65 8.24 4 9 5 60.20 3.62 -4 9 -5 57.22 4.10 4 9 6 190.77 5.13 -4 9 -6 183.54 5.58 4 9 7 57.78 4.35 -4 9 -7 64.47 4.76 4 9 8 5.32 4.08 -4 9 -8 6.00 4.45 4 9 9 14.88 4.72 -4 9 -9 13.40 4.85 -4 10 12 40.92 4.73 -4 10 11 78.65 4.75 -4 10 11 79.43 4.53 -4 10 10 98.65 4.83 -4 10 10 97.11 4.23 -4 10 9 19.68 3.48 -4 10 9 20.65 3.63 -4 10 8 85.65 3.66 -4 10 8 83.04 4.05 -4 10 7 20.01 3.02 -4 10 7 16.68 3.25 -4 10 6 240.97 4.81 4 10 -6 246.27 3.45 -4 10 6 232.79 4.93 -4 10 5 113.82 3.77 4 10 -5 115.23 2.58 -4 10 5 117.55 3.99 -4 10 4 195.93 4.51 -4 10 4 196.83 4.41 4 10 -3 646.69 6.03 4 10 -3 701.07 5.68 -4 10 3 669.58 7.83 4 10 -3 686.62 5.79 -4 10 3 644.82 7.54 4 10 -2 319.82 3.69 4 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144.41 3.75 -5 4 6 149.08 3.03 -5 4 6 149.66 2.88 -5 4 5 393.55 4.29 -5 4 5 401.63 4.41 -5 4 4 223.43 3.15 -5 4 4 227.55 3.37 -5 4 3 372.48 4.22 -5 4 3 361.65 3.95 -5 4 2 205.07 3.04 -5 4 2 201.69 3.84 -5 4 1 119.00 2.48 5 4 -1 115.60 1.74 5 4 -1 115.79 2.19 -5 4 1 118.81 3.19 -5 4 0 61.06 2.10 5 4 0 57.66 1.57 -5 4 0 62.84 2.79 5 4 1 185.12 3.01 5 4 1 180.16 2.33 -5 4 -1 179.24 3.79 -5 4 -1 186.64 3.19 5 4 2 896.47 7.37 5 4 2 868.18 5.98 5 4 3 57.21 2.62 -5 4 -3 62.60 3.08 5 4 4 100.26 3.33 -5 4 -4 96.45 3.63 5 4 5 252.39 4.86 -5 4 -5 262.14 5.32 -5 4 -6 12.73 3.31 5 4 6 12.23 3.30 5 4 7 70.06 4.03 -5 4 -7 66.87 3.80 5 4 8 42.60 4.30 -5 4 -8 39.32 4.11 5 4 9 76.48 4.94 -5 4 -9 69.59 4.62 -5 4 -10 48.89 4.93 5 4 10 48.67 5.11 -5 5 13 11.60 4.29 -5 5 11 328.40 6.22 -5 5 11 337.42 5.71 -5 5 10 60.21 3.34 -5 5 10 63.25 4.05 -5 5 9 67.50 3.03 -5 5 9 66.42 3.82 -5 5 8 41.81 2.60 -5 5 8 39.02 3.09 -5 5 7 208.15 4.41 -5 5 7 206.32 3.76 -5 5 6 230.34 4.59 -5 5 6 237.55 3.95 -5 5 6 233.15 3.78 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440.25 6.05 5 7 -2 310.66 2.87 -5 7 2 316.18 5.23 5 7 -2 329.52 2.93 5 7 -2 330.25 3.79 5 7 -1 263.01 3.07 5 7 -1 274.14 3.03 5 7 0 731.48 6.01 5 7 0 703.07 4.91 5 7 1 74.08 2.57 -5 7 -1 68.85 3.38 5 7 2 112.09 3.09 -5 7 -2 102.89 3.61 5 7 3 533.96 6.31 -5 7 -3 535.46 7.40 5 7 4 356.86 5.56 -5 7 -4 358.16 6.39 5 7 5 15.06 3.38 -5 7 -5 14.47 4.00 5 7 6 121.24 4.53 -5 7 -6 125.59 5.25 5 7 7 84.90 4.78 -5 7 -7 79.50 4.84 -5 7 -8 19.65 4.53 5 7 8 18.78 4.30 -5 7 -9 1.94 4.31 5 7 9 1.02 4.53 -5 8 12 107.41 5.00 -5 8 11 0.94 3.75 -5 8 10 93.01 4.32 -5 8 10 94.41 4.52 -5 8 9 460.10 6.54 -5 8 9 494.89 7.29 -5 8 8 124.25 4.38 -5 8 8 130.68 4.17 -5 8 7 347.83 5.90 -5 8 7 343.90 5.33 -5 8 6 265.39 5.23 -5 8 6 261.33 4.83 -5 8 5 236.21 4.83 -5 8 5 253.66 4.76 -5 8 4 289.41 4.81 5 8 -4 277.81 2.16 -5 8 4 281.01 5.19 5 8 -3 282.02 3.89 5 8 -3 274.80 2.58 5 8 -3 264.09 2.47 -5 8 3 274.95 4.71 -5 8 3 274.62 5.08 5 8 -2 591.49 5.32 5 8 -2 563.92 4.49 5 8 -2 557.31 4.39 -5 8 2 582.48 7.31 5 8 -1 48.95 1.82 5 8 -1 43.18 1.65 -5 8 1 48.82 3.26 5 8 -1 49.60 1.68 5 8 0 96.49 2.44 5 8 0 93.79 1.51 5 8 1 567.83 5.74 5 8 2 117.34 3.27 -5 8 -2 118.16 4.04 5 8 3 48.25 3.14 -5 8 -3 50.40 3.90 5 8 4 398.82 5.96 -5 8 -4 407.57 6.98 5 8 5 73.66 4.02 -5 8 -5 80.19 4.48 5 8 6 47.61 4.24 -5 8 -6 49.44 4.49 5 8 7 38.04 4.42 5 8 8 140.68 5.72 -5 8 -8 126.21 5.94 5 8 9 92.92 5.48 -5 8 -9 92.76 5.86 -5 9 12 102.22 5.13 -5 9 11 22.49 4.26 -5 9 11 27.16 4.14 -5 9 10 38.15 3.93 -5 9 10 36.55 4.14 -5 9 9 58.35 3.99 -5 9 9 56.18 3.87 -5 9 8 225.29 5.20 -5 9 8 232.31 5.10 -5 9 7 591.69 7.59 -5 9 7 542.84 6.85 -5 9 6 207.96 4.92 -5 9 6 193.23 4.59 -5 9 5 201.05 4.78 -5 9 5 206.87 4.66 5 9 -4 426.87 3.42 -5 9 4 437.98 6.43 5 9 -3 343.89 4.35 -5 9 3 344.83 5.48 -5 9 3 350.81 5.89 5 9 -2 153.35 2.69 5 9 -2 161.24 2.55 5 9 -2 154.79 2.39 -5 9 2 153.35 4.28 5 9 -1 180.14 2.95 5 9 -1 171.40 2.81 5 9 -1 174.54 2.42 5 9 0 767.21 6.62 -5 9 0 745.48 8.65 5 9 1 295.38 4.34 5 9 2 12.21 2.63 5 9 3 61.42 3.13 5 9 4 75.35 3.92 -5 9 -4 71.74 4.61 5 9 5 27.22 3.58 -5 9 -5 26.07 4.13 5 9 6 151.96 4.97 -5 9 -6 157.08 5.91 5 9 7 99.14 5.02 -5 9 -7 99.45 5.67 5 9 8 27.33 4.67 -5 9 -8 26.40 5.24 -5 10 12 99.48 5.21 -5 10 11 92.31 4.80 -5 10 10 30.39 4.15 -5 10 10 27.42 3.83 -5 10 9 48.81 3.96 -5 10 9 47.94 3.97 -5 10 8 207.14 5.14 -5 10 8 207.29 5.25 -5 10 7 8.89 3.10 -5 10 7 13.54 3.26 -5 10 6 337.66 5.82 -5 10 6 340.11 5.93 -5 10 5 284.75 5.83 -5 10 5 268.93 5.57 -5 10 4 100.18 4.08 -5 10 4 92.10 3.84 5 10 -3 166.31 2.60 -5 10 3 170.89 4.63 -5 10 3 166.22 4.81 5 10 -2 821.42 6.46 -5 10 2 803.16 8.88 5 10 -1 54.30 2.31 -5 10 1 53.88 3.56 5 10 0 62.87 2.53 -5 10 0 58.89 3.75 5 10 1 246.87 4.16 -5 10 -1 238.57 5.58 5 10 2 219.45 4.27 5 10 3 84.84 3.72 5 10 4 53.50 3.61 -5 10 -4 48.72 4.22 5 10 5 88.96 4.46 -5 10 -5 89.10 5.12 5 10 6 45.88 4.28 -5 10 -6 48.77 5.00 5 10 7 10.81 4.28 -5 10 -7 12.13 4.80 5 10 8 29.51 4.74 -5 10 -8 28.95 5.55 -5 11 11 306.45 7.09 -5 11 10 109.53 5.12 -5 11 10 109.57 4.67 -5 11 9 16.65 3.98 -5 11 9 16.40 3.86 -5 11 8 131.11 4.50 -5 11 8 143.66 5.12 -5 11 7 66.47 4.08 -5 11 7 59.08 4.01 -5 11 6 138.99 4.63 -5 11 6 135.21 4.62 -5 11 5 45.45 3.79 -5 11 5 42.06 3.93 -5 11 4 4.86 3.30 -5 11 4 2.90 3.35 5 11 -3 208.03 3.03 -5 11 3 220.55 5.35 -5 11 3 225.13 5.45 -5 11 2 2.79 3.26 5 11 -2 1.34 1.82 -5 11 2 2.83 3.18 5 11 -1 832.67 7.15 -5 11 1 763.19 9.29 5 11 0 241.98 4.15 -5 11 0 230.03 5.48 5 11 1 20.93 2.64 -5 11 -1 22.99 3.87 5 11 2 200.91 4.39 -5 11 -2 180.61 5.33 5 11 3 229.26 4.77 5 11 4 66.87 3.75 5 11 5 21.70 3.64 -5 11 -5 20.56 4.70 5 11 6 115.63 5.03 -5 11 -6 106.47 5.76 5 11 7 106.27 5.58 -5 11 -7 100.01 6.13 5 11 8 62.67 5.51 -5 12 10 254.18 6.55 -5 12 10 252.47 6.10 -5 12 9 47.84 4.27 -5 12 9 50.81 4.05 -5 12 8 34.30 3.79 -5 12 8 37.74 4.33 -5 12 7 5.99 3.88 -5 12 7 4.77 3.56 -5 12 6 12.27 3.70 -5 12 6 14.13 3.48 -5 12 5 517.63 7.70 -5 12 5 508.67 7.62 -5 12 4 1.17 3.38 -5 12 4 1.03 3.68 5 12 -3 72.23 2.77 -5 12 3 69.36 4.24 -5 12 3 70.15 4.35 5 12 -2 285.62 4.18 -5 12 2 285.33 6.28 -5 12 2 271.84 6.00 5 12 -1 35.99 2.53 -5 12 1 35.08 3.99 5 12 0 21.93 2.63 -5 12 0 21.38 3.54 5 12 1 58.70 3.42 -5 12 -1 52.99 4.40 5 12 2 188.85 4.50 -5 12 -2 197.52 6.20 5 12 3 39.39 3.61 -5 12 -3 42.77 4.22 5 12 4 34.61 3.82 5 12 5 151.22 5.12 5 12 6 23.37 4.51 -5 12 -6 20.58 5.27 5 12 7 103.48 5.41 -5 13 9 63.70 4.79 -5 13 9 68.17 4.57 -5 13 8 183.70 5.36 -5 13 8 197.74 6.03 -5 13 7 120.20 5.01 -5 13 7 122.49 5.32 -5 13 6 15.02 4.13 -5 13 6 12.39 3.83 -5 13 5 61.95 4.46 5 13 -5 58.64 3.61 -5 13 5 59.66 4.49 -5 13 4 176.73 5.49 -5 13 4 176.42 5.30 -5 13 3 71.20 4.62 -5 13 3 66.79 4.48 -5 13 2 7.79 3.62 -5 13 2 7.07 3.53 5 13 -1 86.90 3.23 -5 13 1 88.10 4.79 -5 13 1 89.36 4.80 5 13 0 131.46 3.92 -5 13 0 116.38 4.99 5 13 1 18.31 3.02 -5 13 -1 19.68 4.28 5 13 2 121.04 4.26 -5 13 -2 127.33 5.67 5 13 3 234.98 5.35 -5 13 -3 226.81 6.77 5 13 4 24.89 4.09 -5 13 -4 24.03 4.66 5 13 5 8.89 4.14 -5 13 -5 5.93 4.71 5 13 6 100.95 5.38 5 13 7 40.62 5.37 5 14 -9 121.23 6.04 -5 14 8 49.52 4.38 5 14 -8 51.79 4.97 -5 14 8 48.52 4.97 -5 14 7 85.67 4.86 5 14 -7 91.98 4.77 -5 14 7 76.65 4.85 -5 14 6 93.52 4.74 5 14 -6 105.75 4.37 -5 14 5 123.84 5.10 -5 14 5 121.79 5.40 -5 14 4 100.41 4.86 -5 14 4 101.26 4.91 -5 14 3 142.51 5.74 -5 14 3 137.04 5.40 -5 14 2 201.75 6.14 -5 14 2 198.32 5.94 -5 14 1 120.47 5.34 -5 14 1 124.15 5.39 5 14 0 53.72 3.25 -5 14 0 49.65 4.66 5 14 1 279.06 5.30 -5 14 -1 255.38 6.88 5 14 2 32.71 3.84 -5 14 -2 29.04 4.94 5 14 3 11.85 3.57 -5 14 -3 9.98 4.50 5 14 4 63.05 4.58 -5 14 -4 53.16 5.37 5 14 5 -0.04 4.40 -5 14 -5 -1.48 5.58 5 14 6 15.01 4.86 -5 15 7 148.56 5.54 -5 15 7 153.74 5.96 -5 15 6 13.70 4.92 -5 15 6 9.99 4.19 -5 15 5 20.32 4.49 -5 15 5 26.19 4.69 -5 15 4 171.43 6.16 -5 15 4 167.94 5.76 -5 15 3 145.84 6.01 -5 15 3 132.13 5.45 -5 15 2 38.88 4.81 -5 15 2 39.13 4.53 -5 15 1 65.29 5.48 -5 15 1 56.79 5.02 -5 15 0 81.55 5.41 -5 15 0 84.71 5.73 -5 15 -1 56.42 4.95 5 15 2 5.22 3.71 -5 15 -2 9.36 5.00 5 15 3 95.06 4.77 -5 15 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1.19 4.26 -7 10 9 20.11 4.53 -7 10 8 170.13 5.78 -7 10 8 169.56 5.02 -7 10 7 26.07 4.41 -7 10 7 28.19 3.73 -7 10 6 124.59 5.28 -7 10 6 123.63 4.55 -7 10 5 37.30 4.69 -7 10 5 37.99 3.86 -7 10 4 2.67 3.96 -7 10 4 2.64 3.45 -7 10 3 9.40 3.85 -7 10 3 12.90 3.70 -7 10 2 196.12 5.77 -7 10 -1 142.51 5.76 7 10 2 96.56 3.72 -7 10 -2 94.56 5.28 -7 10 -3 43.80 5.04 7 10 4 55.69 4.44 -7 10 -4 47.02 5.46 7 10 5 9.33 4.18 -7 10 -5 5.23 5.16 7 10 6 13.23 4.42 -7 11 9 0.73 3.95 -7 11 9 -0.76 4.36 -7 11 8 91.40 5.21 -7 11 8 92.06 4.89 -7 11 7 155.92 5.82 -7 11 7 155.45 5.18 -7 11 6 54.91 4.71 -7 11 6 58.41 4.45 -7 11 5 11.31 4.39 -7 11 5 8.75 3.61 -7 11 4 8.71 4.16 -7 11 3 159.04 5.19 -7 11 3 149.63 5.46 -7 11 2 6.08 3.97 -7 11 2 6.87 3.79 -7 11 1 12.09 4.31 -7 11 -2 66.15 5.40 -7 11 -3 63.75 5.34 7 11 4 41.83 4.46 -7 11 -4 34.20 5.24 7 11 5 0.94 4.10 7 11 6 78.56 5.13 -7 12 9 21.92 4.96 -7 12 9 23.04 4.55 -7 12 8 17.94 4.06 -7 12 8 19.64 4.74 -7 12 7 43.80 4.83 -7 12 7 42.22 4.48 -7 12 6 11.49 4.04 -7 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46.50 5.60 8 -13 0 19.52 5.20 8 -13 1 6.77 5.15 8 -12 -1 105.04 5.42 8 -12 0 14.59 4.70 8 -12 2 205.47 7.43 8 -11 -1 55.70 4.74 8 -11 0 6.11 4.60 8 -11 1 40.97 5.48 8 -11 2 11.38 4.84 8 -11 3 144.31 6.48 -8 -10 9 6.88 3.97 -8 -10 8 91.08 4.36 8 -10 -1 60.14 4.59 8 -10 0 10.26 4.67 8 -10 1 126.66 5.80 8 -10 2 63.07 5.23 8 -10 3 41.66 4.98 8 -10 4 60.45 5.97 -8 -9 10 127.41 5.54 -8 -9 9 13.17 4.53 -8 -9 8 18.86 4.01 -8 -9 7 72.85 4.28 -8 -9 6 87.13 3.80 8 -9 -2 36.55 3.97 8 -9 -1 6.90 3.83 8 -9 2 17.08 4.27 8 -9 3 12.92 4.45 8 -9 4 102.55 5.82 -8 -8 10 53.34 4.67 -8 -8 8 40.76 3.95 -8 -8 7 10.14 3.41 -8 -8 6 31.79 3.47 -8 -8 5 180.57 4.33 -8 -8 4 140.62 3.97 8 -8 -2 19.23 3.51 8 -8 -1 131.13 4.83 8 -8 0 3.69 3.86 8 -8 1 0.14 3.80 8 -8 2 19.31 4.28 8 -8 3 3.39 4.54 8 -8 4 28.79 5.00 8 -8 5 59.12 5.32 -8 -7 9 7.72 3.71 -8 -7 8 61.43 4.10 -8 -7 7 116.99 4.39 -8 -7 6 127.61 4.34 -8 -7 5 2.63 3.09 -8 -7 4 124.41 3.65 -8 -7 3 38.26 2.79 8 -7 -2 13.35 3.38 8 -7 -1 6.21 3.71 8 -7 0 53.24 4.01 8 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-8 11 7 12.11 4.70 -8 11 6 33.55 4.22 -8 11 5 7.97 4.85 -8 11 5 11.15 4.21 -8 11 4 20.14 4.91 -8 11 3 47.37 4.63 -8 11 3 46.75 5.42 -8 11 2 13.39 4.66 -8 11 2 9.80 4.37 -8 11 -1 17.19 5.02 -8 11 -2 12.47 5.78 -8 12 7 15.05 4.61 -8 12 7 17.50 5.22 -8 12 6 50.04 5.15 -8 12 6 55.00 4.91 -8 12 5 154.24 6.80 -8 12 5 141.92 5.33 -8 12 4 141.61 5.94 -8 12 4 131.74 6.06 -8 12 3 10.42 4.77 -8 12 3 14.42 4.73 -8 12 2 39.16 4.80 -8 12 2 37.57 5.10 -8 13 7 12.16 4.56 -8 13 6 23.06 4.89 -8 13 5 10.41 5.44 -8 13 5 9.37 4.86 -8 13 4 12.38 5.03 -8 13 4 17.11 4.53 -8 13 3 80.85 5.78 -8 13 3 75.39 5.90 -8 13 2 36.35 5.00 -8 13 2 39.03 5.74 -8 13 1 13.55 5.54 -8 13 1 12.72 4.74 -8 14 4 19.63 5.31 -8 14 3 15.93 5.36 -8 14 2 19.42 5.36 9 -12 -1 11.26 4.68 9 -11 -1 28.14 5.24 9 -11 0 20.48 5.19 9 -11 1 83.14 6.08 9 -10 -1 10.07 4.62 9 -10 0 11.26 4.85 9 -10 1 10.36 5.22 9 -10 2 35.64 5.50 9 -9 -2 41.27 4.36 9 -9 -1 7.72 4.20 9 -9 0 26.98 4.58 9 -9 1 21.09 4.93 9 -9 2 18.14 5.01 -9 -8 9 15.07 4.29 -9 -8 8 32.42 4.13 -9 -8 7 57.34 4.27 9 -8 -2 8.29 3.59 9 -8 -1 61.78 4.70 9 -8 0 17.68 4.69 9 -8 1 22.67 4.59 9 -8 2 5.08 4.45 9 -8 3 41.62 5.07 -9 -7 9 37.90 4.79 -9 -7 7 25.03 4.29 -9 -7 6 178.51 5.03 -9 -7 5 16.23 3.30 9 -7 -2 51.75 4.04 9 -7 -1 43.79 4.63 9 -7 0 7.08 3.92 9 -7 1 26.72 4.36 9 -7 2 25.78 4.43 9 -7 3 4.45 4.70 9 -7 4 2.60 5.31 -9 -6 9 0.81 4.40 -9 -6 8 68.67 4.60 -9 -6 7 42.32 4.13 -9 -6 6 7.26 3.41 -9 -6 5 11.10 3.06 -9 -6 4 7.16 2.99 9 -6 -2 49.12 3.82 9 -6 -1 17.75 3.90 9 -6 0 44.44 4.06 9 -6 1 9.84 4.11 9 -6 2 55.71 4.81 9 -6 3 70.56 5.27 9 -6 4 7.55 4.56 -9 -5 10 5.55 4.50 -9 -5 9 12.40 4.43 -9 -5 8 1.40 3.94 -9 -5 7 22.18 4.01 -9 -5 6 32.66 3.76 -9 -5 4 13.94 2.98 -9 -5 3 172.13 4.36 9 -5 -2 91.93 3.85 9 -5 -1 37.04 3.63 9 -5 0 6.57 3.47 9 -5 1 48.32 4.22 9 -5 3 22.25 4.54 9 -5 4 71.55 5.31 9 -5 5 76.26 5.79 -9 -4 10 3.88 4.58 -9 -4 9 7.75 4.33 -9 -4 8 20.65 4.08 -9 -4 7 72.85 4.38 -9 -4 6 8.51 3.53 -9 -4 5 23.54 3.43 -9 -4 4 35.93 3.70 -9 -4 3 18.38 3.07 -9 -4 2 30.95 3.04 9 -4 -2 30.02 3.09 9 -4 -1 108.02 3.92 9 -4 0 44.75 3.75 9 -4 1 43.01 3.75 9 -4 2 8.09 4.02 9 -4 3 27.24 4.00 9 -4 4 4.39 4.46 9 -4 5 18.71 4.67 -9 -3 10 146.53 5.95 -9 -3 9 55.25 4.62 -9 -3 8 11.33 3.82 -9 -3 7 59.51 4.22 -9 -3 6 81.13 4.26 -9 -3 5 4.14 3.24 -9 -3 4 13.74 3.14 -9 -3 3 100.29 4.00 -9 -3 2 4.66 3.09 9 -3 -2 6.08 2.79 -9 -3 1 5.37 2.92 9 -3 -1 2.23 2.94 9 -3 0 32.69 3.28 9 -3 1 51.24 4.17 9 -3 2 6.22 3.68 9 -3 3 102.47 4.91 9 -3 5 9.15 4.97 -9 -2 10 12.19 4.61 -9 -2 9 22.08 4.28 -9 -2 8 3.18 3.68 -9 -2 7 50.82 4.22 -9 -2 6 25.39 4.30 -9 -2 5 120.85 4.48 -9 -2 4 41.66 3.59 -9 -2 2 6.22 3.04 -9 -2 1 4.27 3.10 9 -2 -1 3.07 2.55 -9 -2 0 15.00 2.86 9 -2 0 18.58 2.98 9 -2 1 41.25 3.68 9 -2 2 57.78 3.85 9 -2 3 50.45 4.19 9 -2 4 12.88 4.51 9 -2 5 30.42 4.86 9 -2 6 6.97 5.11 -9 -1 10 -0.49 4.26 -9 -1 9 35.72 4.63 -9 -1 8 7.57 4.02 -9 -1 7 45.59 4.25 -9 -1 6 19.07 3.60 -9 -1 5 83.86 4.25 -9 -1 4 25.44 3.63 -9 -1 3 85.02 4.13 -9 -1 2 14.53 3.18 -9 -1 1 19.04 3.21 -9 -1 0 31.86 3.57 9 -1 0 30.15 2.98 -9 -1 -1 5.14 3.14 9 -1 1 5.35 3.04 9 -1 2 0.31 2.96 9 -1 3 5.93 3.81 9 -1 4 7.69 4.20 9 -1 5 34.33 5.16 9 -1 6 23.54 5.34 -9 0 10 13.56 4.49 -9 0 9 1.47 4.38 -9 0 8 111.92 5.24 -9 0 7 0.02 3.52 -9 0 6 52.67 4.18 -9 0 5 289.70 5.85 -9 0 4 136.45 4.73 -9 0 3 1.36 3.22 -9 0 2 9.87 3.34 -9 0 1 127.63 4.34 -9 0 0 10.87 3.37 9 0 0 10.78 2.82 9 0 1 89.50 3.64 9 0 2 40.92 3.54 -9 0 -2 39.61 3.79 9 0 3 3.28 3.62 9 0 4 29.14 4.18 9 0 5 11.42 4.21 9 0 6 6.58 4.79 -9 1 10 0.56 4.32 -9 1 9 51.45 5.06 -9 1 8 10.17 4.70 -9 1 7 57.54 4.40 -9 1 6 26.97 3.97 -9 1 5 96.72 4.47 -9 1 4 29.86 3.84 -9 1 3 107.04 4.49 -9 1 2 19.62 3.52 -9 1 1 19.56 3.67 -9 1 0 24.83 3.79 -9 1 -1 12.53 3.51 9 1 1 11.99 3.03 -9 1 -2 1.65 3.53 9 1 2 -0.88 3.20 -9 1 -3 4.15 4.00 9 1 3 4.06 3.75 9 1 4 3.63 4.26 9 1 5 39.31 5.03 -9 2 10 11.20 4.63 -9 2 8 6.24 3.77 -9 2 7 35.81 4.29 -9 2 6 19.18 4.01 -9 2 5 96.65 4.70 -9 2 4 37.60 4.12 -9 2 3 0.62 3.44 -9 2 2 4.24 3.65 -9 2 1 7.09 3.79 -9 2 -1 38.75 4.18 9 2 2 53.03 3.72 -9 2 -2 49.47 4.33 9 2 3 49.12 4.31 -9 2 -3 43.93 4.02 9 2 4 14.02 4.15 -9 2 -4 11.63 4.38 9 2 5 32.89 4.69 9 2 6 7.53 4.62 -9 3 9 65.42 5.58 -9 3 8 15.09 4.33 -9 3 7 45.20 4.52 -9 3 6 65.61 4.50 -9 3 5 4.15 3.69 -9 3 4 8.30 3.64 -9 3 3 69.95 4.43 -9 3 2 5.08 3.88 -9 3 1 3.28 3.53 -9 3 0 43.82 3.97 -9 3 -1 37.37 4.41 -9 3 -2 8.23 4.12 9 3 3 103.41 4.59 -9 3 -3 116.08 5.40 9 3 4 157.50 5.16 -9 3 -4 176.77 5.74 9 3 6 12.59 4.60 -9 4 8 36.84 4.58 -9 4 7 95.37 5.32 -9 4 6 10.87 4.12 -9 4 5 29.23 4.29 -9 4 4 25.98 3.92 -9 4 3 20.48 4.40 -9 4 2 36.33 4.28 -9 4 1 143.16 5.28 -9 4 0 48.63 4.60 -9 4 -1 40.94 4.52 -9 4 -2 1.33 3.99 -9 4 -3 38.30 4.77 -9 4 -4 2.83 4.72 -9 4 -5 17.49 5.16 9 4 6 20.90 5.18 -9 5 7 15.77 4.09 -9 5 6 50.50 4.87 -9 5 5 50.87 4.71 -9 5 4 23.65 4.25 -9 5 3 182.63 5.78 -9 5 2 94.55 5.07 -9 5 1 35.11 4.33 -9 5 0 1.32 4.32 -9 5 -2 3.74 4.46 -9 5 -3 19.81 4.74 -9 5 -5 75.44 5.72 -9 6 9 0.38 4.49 -9 6 6 8.35 4.49 -9 6 3 11.52 4.36 -9 6 2 45.38 4.81 -9 6 1 13.82 4.19 -9 6 0 47.85 4.56 -9 6 -1 9.90 4.41 -9 6 -2 59.40 5.22 -9 6 -3 54.43 5.38 -9 6 -4 8.46 5.32 -9 6 -5 5.50 5.25 -9 7 8 39.14 5.03 -9 7 5 16.14 4.24 -9 7 4 48.14 5.22 -9 7 3 5.38 4.35 -9 7 3 4.69 3.35 -9 7 2 34.42 4.70 -9 7 1 35.88 4.74 -9 7 -1 23.74 4.81 -9 7 -2 26.54 5.08 -9 7 -3 4.14 4.86 -9 7 -4 7.17 5.85 -9 8 8 47.81 5.63 -9 8 7 64.05 5.41 -9 8 4 29.67 5.23 -9 8 3 26.67 3.78 -9 8 3 25.11 4.63 -9 8 2 13.98 4.78 -9 8 1 56.67 5.38 -9 8 0 20.94 5.14 -9 8 -1 19.22 5.12 -9 8 -2 7.81 5.10 -9 9 7 11.44 5.08 -9 9 6 5.42 4.84 -9 9 3 16.86 4.93 -9 9 3 18.45 3.90 -9 9 2 48.78 5.22 -9 9 1 9.15 4.68 -9 9 0 22.22 5.30 -9 9 -1 32.91 5.19 -9 9 -2 19.10 5.54 -9 10 6 21.85 4.90 -9 10 5 12.05 5.00 -9 10 4 51.60 4.71 -9 10 3 7.94 4.37 -9 10 2 27.12 4.99 -9 10 1 19.66 5.49 -9 10 0 3.98 5.11 -9 10 -1 10.49 5.30 -9 11 4 24.66 5.53 -9 11 4 25.28 4.81 -9 11 3 67.73 5.18 -9 11 3 54.53 5.92 -9 11 2 59.62 5.03 -9 12 4 5.19 4.77 -9 12 3 45.63 5.32 -9 12 2 2.96 4.75 10 -10 -1 45.27 5.50 10 -10 0 27.40 5.07 10 -9 0 1.67 4.92 10 -9 1 2.12 5.23 10 -8 0 17.31 4.90 10 -8 1 10.09 5.06 10 -8 2 15.62 5.35 10 -7 0 17.18 4.90 10 -7 1 18.13 4.65 10 -7 2 8.80 4.87 -10 -6 8 2.85 4.55 -10 -6 7 9.56 3.92 10 -6 2 46.18 5.28 10 -6 3 35.03 5.39 -10 -5 8 10.29 4.56 -10 -5 7 54.41 4.70 -10 -5 6 3.51 3.64 10 -5 1 2.11 4.20 10 -5 2 15.22 4.63 10 -5 3 5.76 4.87 -10 -4 9 -0.63 4.35 -10 -4 8 25.79 4.38 -10 -4 7 51.54 4.49 -10 -4 6 33.23 4.07 -10 -4 5 23.05 3.70 -10 -4 4 124.74 4.73 10 -4 2 18.63 4.67 10 -4 3 21.28 4.68 10 -4 4 5.37 5.24 -10 -3 9 53.38 5.39 -10 -3 8 10.44 4.16 -10 -3 7 72.84 4.66 -10 -3 6 19.15 4.15 -10 -3 5 61.86 4.76 -10 -3 4 1.51 3.64 -10 -3 3 17.17 3.67 10 -3 3 30.58 4.58 -10 -2 9 2.88 4.55 -10 -2 8 26.04 4.40 -10 -2 7 17.16 4.18 -10 -2 6 3.33 4.33 -10 -2 5 4.14 3.83 -10 -2 4 104.53 4.73 -10 -2 3 45.04 3.83 -10 -2 2 2.86 3.46 -10 -1 9 11.18 4.73 -10 -1 8 33.37 4.71 -10 -1 6 44.73 4.28 -10 -1 5 21.83 3.87 -10 -1 4 3.90 3.75 -10 -1 3 59.10 4.06 -10 -1 2 0.03 3.55 -10 -1 1 2.75 3.58 -10 0 9 94.14 5.50 -10 0 8 25.09 4.80 -10 0 7 72.21 4.68 -10 0 6 3.84 3.72 -10 0 5 15.40 4.05 -10 0 4 20.01 4.07 -10 0 3 2.23 3.69 -10 0 2 -0.44 3.66 -10 0 1 2.29 3.68 -10 0 0 3.05 3.91 -10 1 8 29.71 4.88 -10 1 7 29.46 4.53 -10 1 6 55.84 4.63 -10 1 5 33.87 4.38 -10 1 4 1.25 4.06 -10 1 3 78.61 4.87 -10 1 2 2.58 3.86 -10 1 1 3.02 3.73 -10 1 0 1.65 3.96 -10 1 -1 26.45 3.99 -10 2 8 15.59 4.34 -10 2 7 14.53 4.29 -10 2 6 2.22 4.26 -10 2 5 12.78 4.45 -10 2 4 128.31 5.48 -10 2 3 48.89 4.45 -10 2 2 3.28 4.20 -10 2 1 36.65 4.33 -10 2 0 62.95 4.60 -10 2 -1 70.32 4.90 -10 2 -2 11.53 4.12 -10 3 8 13.74 4.84 -10 3 7 58.55 4.92 -10 3 6 12.48 4.60 -10 3 5 44.82 4.84 -10 3 4 0.95 4.29 -10 3 3 17.78 4.25 -10 3 2 53.14 4.74 -10 3 1 7.57 4.21 -10 3 0 31.30 4.50 -10 3 -1 46.29 4.58 -10 3 -2 9.38 4.57 -10 4 8 25.42 5.09 -10 4 7 56.87 5.00 -10 4 6 30.47 4.74 -10 4 5 21.25 4.76 -10 4 4 110.79 5.31 -10 4 2 3.81 4.56 -10 4 1 62.40 4.92 -10 4 -1 7.73 4.57 -10 4 -2 24.62 4.71 -10 4 -3 24.57 4.98 -10 5 7 61.70 5.51 -10 5 6 -0.32 4.78 -10 5 5 39.15 5.01 -10 5 4 0.88 4.37 -10 5 3 9.23 4.59 -10 5 2 5.83 4.79 -10 5 1 12.17 4.59 -10 5 0 23.01 4.61 -10 5 -1 -0.38 4.81 -10 6 6 8.50 4.99 -10 6 5 42.23 5.31 -10 6 4 8.36 4.56 -10 6 3 17.64 5.27 -10 6 2 42.65 5.01 -10 6 1 4.88 4.88 -10 6 0 32.57 5.07 -10 6 -1 23.12 5.11 -10 7 6 67.56 5.75 -10 7 5 26.46 5.05 -10 7 4 44.59 5.47 -10 7 3 12.31 4.87 -10 7 2 13.22 5.11 -10 7 1 2.57 5.10 -10 7 0 17.07 5.25 -10 7 -1 15.08 5.12 -10 8 4 8.08 5.06 -10 8 3 52.58 5.86 -10 8 2 17.16 5.34 -10 8 1 47.75 5.58 -11 -3 7 3.69 4.21 -11 -3 6 27.69 4.77 -11 -3 5 52.61 4.89 -11 -2 7 3.66 4.45 -11 -2 5 138.19 5.26 -11 -2 4 10.39 3.96 -11 -1 7 9.29 5.00 -11 -1 6 10.77 4.50 -11 -1 5 32.82 4.43 -11 -1 4 51.72 4.45 -11 0 5 2.11 4.18 -11 0 3 10.67 4.47 -11 0 2 67.51 4.93 -11 1 6 14.04 4.94 -11 1 5 44.19 4.95 -11 1 4 51.66 4.80 -11 1 3 37.00 4.55 -11 1 2 31.82 4.87 -11 1 1 3.24 4.15 -11 2 6 3.65 4.51 -11 2 5 144.32 6.02 -11 2 4 6.95 5.13 -11 2 3 20.85 4.87 -11 2 2 17.62 4.74 -11 2 1 3.72 4.36 -11 2 0 56.98 5.50 -11 3 5 41.19 5.34 -11 3 4 14.25 4.97 -11 3 3 39.62 4.77 -11 3 2 28.47 5.01 -11 3 1 31.20 5.65 -11 3 0 1.37 4.97 -11 4 4 35.69 5.32 -11 4 3 2.14 4.96 -11 4 2 16.65 5.03 -11 4 0 11.55 4.88 -11 4 -1 0.88 5.20 -11 5 2 7.31 5.67 0 0 0 0.00 0.00 TITL 20230721- in P2(1) REM P2(1) (#4 in standard setting) CELL 0.71073 8.289261 14.163029 10.032473 90.0000 103.6857 90.0000 ZERR 5.00 0.000274 0.000355 0.000269 0.0000 0.0031 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 55.00 50.00 5.00 5.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 47333 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.292 _oxdiff_exptl_absorpt_empirical_full_min 0.784 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br01 Br 0.45970(3) 0.71443(2) 0.64231(2) 0.03805(8) Uani 1 1 d . . . . . N002 N 0.4565(2) 0.40079(14) 0.13487(15) 0.0183(3) Uani 1 1 d . . . . . N003 N 0.1009(2) 0.53542(13) 0.58925(17) 0.0201(3) Uani 1 1 d . . . . . N004 N 0.40059(19) 0.43387(11) 0.24705(16) 0.0149(3) Uani 1 1 d . . . . . N005 N 0.0504(2) 0.59880(12) 0.48228(16) 0.0177(3) Uani 1 1 d . . . . . O006 O 0.0429(3) 0.63061(14) 0.25985(17) 0.0416(5) Uani 1 1 d . . . . . C007 C 0.1788(2) 0.33378(15) 0.06549(18) 0.0176(4) Uani 1 1 d . . . . . C008 C 0.3472(2) 0.35132(15) 0.05044(19) 0.0193(4) Uani 1 1 d . . . . . H008 H 0.377686 0.325106 -0.024991 0.023 Uiso 1 1 calc R . . . . N009 N 0.5431(3) 0.64697(17) 0.1597(2) 0.0398(5) Uani 1 1 d . . . . . C00A C 0.1162(2) 0.39160(14) 0.15573(18) 0.0174(4) Uani 1 1 d . . . . . C00B C 0.0794(3) 0.26351(16) -0.0092(2) 0.0235(4) Uani 1 1 d . . . . . H00B H 0.119971 0.225733 -0.069767 0.028 Uiso 1 1 calc R . . . . N00C N 0.7917(2) 0.42819(16) 0.4379(2) 0.0324(5) Uani 1 1 d . . . . . C00D C -0.0424(2) 0.37725(18) 0.1724(2) 0.0243(4) Uani 1 1 d . . . . . H00D H -0.083488 0.415050 0.232572 0.029 Uiso 1 1 calc R . . . . C00E C 0.2293(2) 0.47030(14) 0.22110(18) 0.0158(3) Uani 1 1 d . . . . . H00E H 0.216828 0.524165 0.158162 0.019 Uiso 1 1 calc R . . . . C00F C 0.5061(2) 0.50742(15) 0.3242(2) 0.0173(4) Uani 1 1 d . . . . . C00G C 0.2230(2) 0.50452(13) 0.36399(18) 0.0156(3) Uani 1 1 d . . . . . H00G H 0.199520 0.451539 0.419346 0.019 Uiso 1 1 calc R . . . . C00H C -0.0667(3) 0.64822(19) 0.6432(2) 0.0281(5) Uani 1 1 d . . . . . H00H H -0.127683 0.681693 0.694237 0.034 Uiso 1 1 calc R . . . . C00I C 0.5666(3) 0.5591(2) 0.8158(2) 0.0310(5) Uani 1 1 d . . . . . H00I H 0.588189 0.605162 0.883726 0.037 Uiso 1 1 calc R . . . . C00J C 0.0962(3) 0.58275(16) 0.35987(19) 0.0212(4) Uani 1 1 d . . . . . C00K C 0.5044(3) 0.58430(16) 0.6798(2) 0.0209(4) Uani 1 1 d . . . . . C00L C -0.0518(2) 0.66921(16) 0.5141(2) 0.0217(4) Uani 1 1 d . . . . . C00M C 0.5331(3) 0.58624(16) 0.2333(2) 0.0251(4) Uani 1 1 d . . . . . C00N C 0.6695(2) 0.46518(16) 0.3903(2) 0.0216(4) Uani 1 1 d . . . . . C00O C 0.4021(2) 0.54464(13) 0.42667(18) 0.0154(3) Uani 1 1 d . . . . . H00O H 0.397311 0.613693 0.420764 0.018 Uiso 1 1 calc R . . . . C00P C 0.4707(2) 0.51737(14) 0.57516(18) 0.0156(3) Uani 1 1 d . . . . . C00Q C 0.5964(3) 0.4655(2) 0.8499(2) 0.0335(5) Uani 1 1 d . . . . . H00Q H 0.639491 0.448339 0.940779 0.040 Uiso 1 1 calc R . . . . C00R C -0.0813(3) 0.25020(18) 0.0074(2) 0.0286(5) Uani 1 1 d . . . . . H00R H -0.148711 0.203801 -0.042840 0.034 Uiso 1 1 calc R . . . . C00S C 0.0288(3) 0.56545(17) 0.6850(2) 0.0259(5) Uani 1 1 d . . . . . C00T C -0.1410(3) 0.30610(18) 0.0990(2) 0.0278(5) Uani 1 1 d . . . . . H00T H -0.247396 0.295978 0.111306 0.033 Uiso 1 1 calc R . . . . C00U C 0.0532(4) 0.5134(3) 0.8169(3) 0.0450(7) Uani 1 1 d . . . . . H00A H -0.051304 0.488453 0.826285 0.068 Uiso 1 1 calc GR . . . . H00C H 0.096650 0.555574 0.891690 0.068 Uiso 1 1 calc GR . . . . H00F H 0.129914 0.462449 0.818064 0.068 Uiso 1 1 calc GR . . . . C00V C 0.5621(3) 0.39696(18) 0.7485(2) 0.0290(5) Uani 1 1 d . . . . . H00V H 0.581191 0.333654 0.771551 0.035 Uiso 1 1 calc R . . . . C00W C -0.1160(3) 0.75085(17) 0.4237(2) 0.0297(5) Uani 1 1 d . . . . . H00J H -0.024766 0.789520 0.413018 0.045 Uiso 1 1 calc GR . . . . H00K H -0.189403 0.787503 0.464142 0.045 Uiso 1 1 calc GR . . . . H00L H -0.175291 0.728179 0.335468 0.045 Uiso 1 1 calc GR . . . . C00X C 0.4995(3) 0.42267(15) 0.6133(2) 0.0209(4) Uani 1 1 d . . . . . H00X H 0.476070 0.376068 0.546159 0.025 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br01 0.06781(17) 0.01825(11) 0.02881(11) -0.01056(9) 0.01288(10) -0.00411(11) N002 0.0241(8) 0.0184(9) 0.0140(8) -0.0006(6) 0.0075(6) 0.0020(6) N003 0.0220(8) 0.0238(9) 0.0142(7) 0.0016(6) 0.0038(6) 0.0021(7) N004 0.0172(7) 0.0155(8) 0.0126(7) -0.0023(6) 0.0048(6) -0.0012(6) N005 0.0193(7) 0.0185(8) 0.0146(7) -0.0012(6) 0.0028(6) 0.0036(6) O006 0.0653(12) 0.0417(11) 0.0202(8) 0.0115(7) 0.0148(8) 0.0356(10) C007 0.0216(9) 0.0195(9) 0.0110(7) -0.0013(7) 0.0024(6) 0.0008(7) C008 0.0255(9) 0.0195(10) 0.0143(8) -0.0038(7) 0.0073(7) 0.0010(7) N009 0.0651(15) 0.0307(12) 0.0265(10) 0.0010(8) 0.0165(10) -0.0164(11) C00A 0.0215(9) 0.0173(9) 0.0121(8) -0.0005(7) 0.0013(7) 0.0021(7) C00B 0.0277(10) 0.0230(11) 0.0179(8) -0.0046(8) 0.0014(8) -0.0006(8) N00C 0.0237(9) 0.0455(13) 0.0276(9) -0.0088(9) 0.0053(7) -0.0015(9) C00D 0.0215(10) 0.0306(13) 0.0205(9) -0.0035(9) 0.0045(8) 0.0037(8) C00E 0.0215(9) 0.0151(9) 0.0112(7) -0.0004(6) 0.0043(6) 0.0039(7) C00F 0.0238(9) 0.0165(9) 0.0125(7) -0.0016(7) 0.0062(7) -0.0054(7) C00G 0.0216(9) 0.0141(9) 0.0112(7) 0.0003(6) 0.0037(6) 0.0029(7) C00H 0.0266(11) 0.0345(14) 0.0246(10) -0.0101(9) 0.0087(8) 0.0064(9) C00I 0.0343(12) 0.0426(15) 0.0144(9) -0.0056(9) 0.0025(8) -0.0103(10) C00J 0.0285(10) 0.0193(10) 0.0153(8) 0.0003(7) 0.0043(7) 0.0080(8) C00K 0.0253(9) 0.0220(10) 0.0152(8) -0.0027(7) 0.0048(7) -0.0036(8) C00L 0.0196(9) 0.0209(10) 0.0236(10) -0.0083(8) 0.0027(7) 0.0030(8) C00M 0.0375(12) 0.0211(10) 0.0187(9) -0.0033(8) 0.0109(8) -0.0087(9) C00N 0.0226(10) 0.0257(11) 0.0178(9) -0.0065(8) 0.0077(7) -0.0077(8) C00O 0.0238(9) 0.0118(8) 0.0109(7) -0.0007(6) 0.0049(7) 0.0007(7) C00P 0.0184(8) 0.0166(9) 0.0120(7) -0.0008(7) 0.0039(6) -0.0019(7) C00Q 0.0293(11) 0.0522(16) 0.0163(9) 0.0110(10) 0.0004(8) -0.0052(11) C00R 0.0272(11) 0.0295(11) 0.0255(10) -0.0043(9) -0.0007(8) -0.0051(9) C00S 0.0256(10) 0.0344(13) 0.0182(9) -0.0019(8) 0.0059(8) 0.0030(9) C00T 0.0192(9) 0.0326(13) 0.0298(11) -0.0006(9) 0.0020(8) -0.0020(9) C00U 0.0564(17) 0.059(2) 0.0251(11) 0.0061(13) 0.0207(11) 0.0126(15) C00V 0.0273(10) 0.0329(13) 0.0264(10) 0.0154(9) 0.0054(8) 0.0039(9) C00W 0.0333(12) 0.0220(10) 0.0313(11) -0.0047(9) 0.0024(9) 0.0108(9) C00X 0.0243(10) 0.0194(10) 0.0199(9) 0.0038(8) 0.0070(8) -0.0005(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C008 N002 N004 113.30(15) . . ? C00S N003 N005 104.45(17) . . ? N002 N004 C00E 117.70(14) . . ? N002 N004 C00F 113.32(15) . . ? C00F N004 C00E 105.96(15) . . ? N003 N005 C00J 118.91(16) . . ? N003 N005 C00L 112.02(16) . . ? C00J N005 C00L 128.94(17) . . ? C00A C007 C008 118.33(18) . . ? C00B C007 C008 121.61(18) . . ? C00B C007 C00A 120.05(18) . . ? N002 C008 C007 124.36(17) . . ? C007 C00A C00E 115.14(17) . . ? C00D C00A C007 119.96(19) . . ? C00D C00A C00E 124.79(18) . . ? C007 C00B C00R 119.51(19) . . ? C00A C00D C00T 120.0(2) . . ? N004 C00E C00A 107.02(15) . . ? N004 C00E C00G 101.00(13) . . ? C00A C00E C00G 119.26(16) . . ? N004 C00F C00M 111.55(16) . . ? N004 C00F C00N 108.55(17) . . ? N004 C00F C00O 103.47(14) . . ? C00M C00F C00O 109.40(17) . . ? C00N C00F C00M 108.73(17) . . ? C00N C00F C00O 115.10(16) . . ? C00E C00G C00O 104.54(14) . . ? C00J C00G C00E 112.51(14) . . ? C00J C00G C00O 109.15(16) . . ? C00L C00H C00S 106.92(18) . . ? C00Q C00I C00K 119.7(2) . . ? N005 C00J C00G 115.31(16) . . ? O006 C00J N005 121.46(19) . . ? O006 C00J C00G 123.18(18) . . ? C00I C00K Br01 117.03(17) . . ? C00I C00K C00P 121.8(2) . . ? C00P C00K Br01 121.10(15) . . ? N005 C00L C00W 124.45(19) . . ? C00H C00L N005 104.97(19) . . ? C00H C00L C00W 130.5(2) . . ? N009 C00M C00F 175.6(3) . . ? N00C C00N C00F 176.3(2) . . ? C00G C00O C00F 103.17(14) . . ? C00P C00O C00F 114.79(16) . . ? C00P C00O C00G 113.57(15) . . ? C00K C00P C00O 121.98(18) . . ? C00K C00P C00X 117.11(18) . . ? C00X C00P C00O 120.90(17) . . ? C00I C00Q C00V 119.9(2) . . ? C00T C00R C00B 120.1(2) . . ? N003 C00S C00H 111.62(19) . . ? N003 C00S C00U 120.0(2) . . ? C00H C00S C00U 128.4(2) . . ? C00R C00T C00D 120.3(2) . . ? C00X C00V C00Q 120.0(2) . . ? C00V C00X C00P 121.4(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br01 C00K 1.900(2) . ? N002 N004 1.396(2) . ? N002 C008 1.291(3) . ? N003 N005 1.386(2) . ? N003 C00S 1.317(3) . ? N004 C00E 1.475(2) . ? N004 C00F 1.459(3) . ? N005 C00J 1.387(2) . ? N005 C00L 1.393(3) . ? O006 C00J 1.205(3) . ? C007 C008 1.460(3) . ? C007 C00A 1.408(3) . ? C007 C00B 1.392(3) . ? N009 C00M 1.149(3) . ? C00A C00D 1.378(3) . ? C00A C00E 1.504(3) . ? C00B C00R 1.394(3) . ? N00C C00N 1.140(3) . ? C00D C00T 1.393(3) . ? C00E C00G 1.526(2) . ? C00F C00M 1.492(3) . ? C00F C00N 1.486(3) . ? C00F C00O 1.580(3) . ? C00G C00J 1.521(3) . ? C00G C00O 1.575(3) . ? C00H C00L 1.363(3) . ? C00H C00S 1.421(3) . ? C00I C00K 1.387(3) . ? C00I C00Q 1.375(4) . ? C00K C00P 1.392(3) . ? C00L C00W 1.488(3) . ? C00O C00P 1.514(2) . ? C00P C00X 1.400(3) . ? C00Q C00V 1.386(4) . ? C00R C00T 1.389(3) . ? C00S C00U 1.487(3) . ? C00V C00X 1.382(3) . ?