#------------------------------------------------------------------------------ #$Date: 2024-06-15 01:10:55 +0300 (Sat, 15 Jun 2024) $ #$Revision: 292399 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/18/1571888.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571888 loop_ _publ_author_name 'Zhao, Yankun' 'Yan, Hongya' 'Zhang, Yulian' 'Zhou, Tao' 'Tian, Mengxing' 'Zhang, Chongzhou' 'Yuan, Shan' 'Qiu, Hanyue' 'He, Ling' 'Zhang, Min' _publ_section_title ; Catalytic Asymmetric Intramolecular Propargylation of Cyclopropanols to Access the Cuparane Core ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC02504K _journal_year 2024 _chemical_absolute_configuration unk _chemical_formula_moiety 'C25 H35 N3 O2' _chemical_formula_sum 'C25 H35 N3 O2' _chemical_formula_weight 409.56 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2022-10-27 _audit_creation_method ; Olex2 1.5 (compiled 2021.10.07 svn.r9718050b for OlexSys, GUI svn.r6410) ; _audit_update_record ; 2023-12-22 deposited with the CCDC. 2024-06-10 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 96.520(5) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 6.5199(3) _cell_length_b 8.9739(5) _cell_length_c 19.7834(10) _cell_measurement_reflns_used 6517 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 27.5390 _cell_measurement_theta_min 3.8360 _cell_volume 1150.02(10) _computing_cell_refinement 'CrysAlisPro 1.171.41.117a (Rigaku OD, 2021)' _computing_data_collection 'CrysAlisPro 1.171.41.117a (Rigaku OD, 2021)' _computing_data_reduction 'CrysAlisPro 1.171.41.117a (Rigaku OD, 2021)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.0892 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.913 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 36.00 61.00 1.00 15.32 -- 18.74 -99.00 -30.00 25 2 \w -39.00 49.00 1.00 15.32 -- 18.74 -77.00 150.00 88 3 \w 1.00 87.00 1.00 15.32 -- 18.74 57.00-150.00 86 4 \w -3.00 84.00 1.00 15.32 -- 18.74 57.00 120.00 87 5 \w 5.00 86.00 1.00 15.32 -- 18.74 57.00 -60.00 81 6 \w -38.00 49.00 1.00 15.32 -- 18.74 -77.00 60.00 87 7 \w -11.00 19.00 1.00 15.32 -- 18.74 77.00 30.00 30 8 \w -36.00 37.00 1.00 15.32 -- 18.74 -57.00 -60.00 73 9 \w -40.00 23.00 1.00 15.32 -- -18.93 57.00 -90.00 63 10 \w -78.00 -7.00 1.00 15.32 -- -18.93 -38.00 -30.00 71 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Single source at offset/far, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0704034000 _diffrn_orient_matrix_UB_12 -0.0478892000 _diffrn_orient_matrix_UB_13 0.0141760000 _diffrn_orient_matrix_UB_21 0.0720960000 _diffrn_orient_matrix_UB_22 -0.0098760000 _diffrn_orient_matrix_UB_23 0.0293054000 _diffrn_orient_matrix_UB_31 -0.0427449000 _diffrn_orient_matrix_UB_32 0.0621151000 _diffrn_orient_matrix_UB_33 0.0155886000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0352 _diffrn_reflns_av_unetI/netI 0.0444 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.913 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 16343 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.882 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.173 _diffrn_reflns_theta_min 3.421 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.075 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.52110 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.117a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.183 _exptl_crystal_description block _exptl_crystal_F_000 444 _exptl_crystal_size_max 0.31 _exptl_crystal_size_mid 0.28 _exptl_crystal_size_min 0.25 _refine_diff_density_max 0.159 _refine_diff_density_min -0.198 _refine_diff_density_rms 0.042 _refine_ls_abs_structure_details ; Flack x determined using 1449 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.3(6) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.141 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 273 _refine_ls_number_reflns 5469 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.141 _refine_ls_R_factor_all 0.0748 _refine_ls_R_factor_gt 0.0498 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0622P)^2^+0.0916P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1328 _refine_ls_wR_factor_ref 0.1471 _reflns_Friedel_coverage 0.822 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.847 _reflns_number_gt 4023 _reflns_number_total 5469 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc02504k2.cif _cod_data_source_block 20221027-zyk-py-cy-me _cod_database_code 1571888 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C25 H35 N3 O2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.981 _shelx_estimated_absorpt_t_min 0.977 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C008(H008), C00C(H00C), C00F(H00F), C00G(H00G), C00H(H00H), C00J(H00K) 2.b Secondary CH2 refined with riding coordinates: C00K(H00L,H00M), C00L(H00N,H00O), C00M(H00P,H00Q), C00N(H00R,H00S), C00P(H00W, H00X), C00Q(H00Y,H), C00R(H00Z,HA), C00S(H00,HB), C00T(H1,HC), C00U(H2,HD) 2.c Aromatic/amide H refined with riding coordinates: C00B(H00B), C00D(H00D), C00E(H00E) 2.d Idealised Me refined as rotating group: C00I(H00A,H00I,H00J), C00O(H00T,H00U,H00V) ; _shelx_res_file ; TITL 20221027-zyk-py-cy-me_a.res in P2(1) 20221027-zyk-py-cy-me.res created by SHELXL-2018/3 at 19:07:29 on 27-Oct-2022 REM Old TITL 20221027-Zhang Min-ZYK-Py-Cy-Me_auto in P2(1) REM SHELXT solution in P2(1): R1 0.152, Rweak 0.080, Alpha 0.004 REM 3.466 for 5 systematic absences, Orientation as input REM Flack x = 0.052 ( 0.614 ) from 1545 Parsons' quotients REM Formula found by SHELXT: C25 N3 O2 CELL 0.71073 6.5199 8.9739 19.7834 90 96.52 90 ZERR 2 0.0003 0.0005 0.001 0 0.005 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 50 70 6 4 L.S. 30 PLAN 7 SIZE 0.31 0.28 0.25 CONF BOND list 4 fmap 2 53 MORE -1 BOND $H ACTA REM REM REM WGHT 0.062200 0.091600 FVAR 0.75980 O001 4 0.753417 0.383802 0.562486 11.00000 0.03700 0.06936 = 0.03890 -0.01257 0.00359 0.00373 O002 4 0.846117 0.588837 0.791606 11.00000 0.03996 0.07767 = 0.04466 -0.01744 0.00949 -0.00558 N003 3 0.595524 0.474167 0.681672 11.00000 0.03804 0.04522 = 0.03427 -0.00079 0.00639 0.00255 N004 3 0.430330 0.371640 0.507879 11.00000 0.04067 0.06556 = 0.03496 -0.00270 0.00711 -0.00915 N005 3 0.571640 0.623529 0.849211 11.00000 0.03850 0.08325 = 0.03800 -0.01160 0.00284 0.00641 C006 1 0.642974 0.573108 0.797037 11.00000 0.03702 0.05333 = 0.03485 0.00112 0.00588 0.00608 C007 1 0.546264 0.392745 0.562820 11.00000 0.03590 0.04321 = 0.03619 -0.00146 0.00501 -0.00106 C008 1 0.785921 0.351489 0.491553 11.00000 0.04250 0.04793 = 0.03849 -0.00743 0.01086 -0.00500 AFIX 13 H008 2 0.859816 0.434550 0.473131 11.00000 -1.20000 AFIX 0 C009 1 0.464801 0.428865 0.628179 11.00000 0.03915 0.04118 = 0.03396 0.00290 0.00357 0.00134 C00A 1 0.510018 0.507726 0.738591 11.00000 0.03877 0.04169 = 0.03645 0.00215 0.00511 0.00402 C00B 1 0.252645 0.416476 0.629894 11.00000 0.03710 0.05576 = 0.03881 -0.00110 0.00134 -0.00226 AFIX 43 H00B 2 0.167948 0.387551 0.591107 11.00000 -1.20000 AFIX 0 C00C 1 0.564542 0.342460 0.454379 11.00000 0.03952 0.05055 = 0.03812 -0.00954 0.00700 -0.00740 AFIX 13 H00C 2 0.539680 0.240456 0.437742 11.00000 -1.20000 AFIX 0 C00D 1 0.168687 0.447002 0.688888 11.00000 0.03821 0.06252 = 0.04394 0.00047 0.00611 -0.00292 AFIX 43 H00D 2 0.027629 0.437413 0.691204 11.00000 -1.20000 AFIX 0 C00E 1 0.300762 0.492597 0.744944 11.00000 0.04301 0.05530 = 0.03893 -0.00129 0.01119 0.00223 AFIX 43 H00E 2 0.250293 0.512730 0.786106 11.00000 -1.20000 AFIX 0 C00F 1 0.518675 0.449568 0.394762 11.00000 0.04239 0.05008 = 0.03577 -0.00851 0.00814 -0.00345 AFIX 13 H00F 2 0.543000 0.551018 0.412187 11.00000 -1.20000 AFIX 0 C00G 1 0.936245 0.658704 0.854806 11.00000 0.04171 0.05268 = 0.04275 -0.00622 0.00185 0.00344 AFIX 13 H00G 2 1.021643 0.585710 0.881995 11.00000 -1.20000 AFIX 0 C00H 1 0.744632 0.696982 0.891180 11.00000 0.04536 0.05112 = 0.03860 -0.00657 0.00349 0.00805 AFIX 13 H00H 2 0.722705 0.804877 0.887715 11.00000 -1.20000 AFIX 0 C00I 1 0.910310 0.211229 0.488989 11.00000 0.04732 0.05890 = 0.07824 -0.02248 0.00706 0.00386 AFIX 137 H00A 2 1.039709 0.222719 0.516904 11.00000 -1.50000 H00I 2 0.935233 0.191977 0.442891 11.00000 -1.50000 H00J 2 0.835527 0.129301 0.505531 11.00000 -1.50000 AFIX 0 C00J 1 0.758138 0.654626 0.966444 11.00000 0.04688 0.05417 = 0.04162 -0.00568 0.00216 0.00269 AFIX 13 H00K 2 0.793141 0.548594 0.970790 11.00000 -1.20000 AFIX 0 C00K 1 0.661142 0.423923 0.339515 11.00000 0.05016 0.06378 = 0.04505 -0.00760 0.01428 -0.00265 AFIX 23 H00L 2 0.803550 0.435631 0.359042 11.00000 -1.20000 H00M 2 0.643699 0.322740 0.322589 11.00000 -1.20000 AFIX 0 C00L 1 0.615439 0.532680 0.280605 11.00000 0.06726 0.08108 = 0.04301 0.00050 0.02026 -0.00939 AFIX 23 H00N 2 0.647359 0.633149 0.296559 11.00000 -1.20000 H00O 2 0.703206 0.509672 0.245558 11.00000 -1.20000 AFIX 0 C00M 1 0.293276 0.440033 0.363427 11.00000 0.04436 0.07798 = 0.04031 -0.00589 0.00779 -0.00469 AFIX 23 H00P 2 0.264261 0.339855 0.346567 11.00000 -1.20000 H00Q 2 0.203409 0.460470 0.398173 11.00000 -1.20000 AFIX 0 C00N 1 0.928807 0.744110 1.008023 11.00000 0.06561 0.06736 = 0.04477 -0.00103 -0.00477 -0.00421 AFIX 23 H00R 2 1.060770 0.719407 0.992676 11.00000 -1.20000 H00S 2 0.904405 0.849601 1.000009 11.00000 -1.20000 AFIX 0 C00O 1 1.068008 0.788904 0.838992 11.00000 0.04928 0.06398 = 0.07640 -0.00815 0.01005 -0.00378 AFIX 137 H00T 2 1.175977 0.755046 0.813553 11.00000 -1.50000 H00U 2 1.127731 0.833863 0.880679 11.00000 -1.50000 H00V 2 0.984420 0.860908 0.812651 11.00000 -1.50000 AFIX 0 C00P 1 0.551702 0.679229 0.994638 11.00000 0.05585 0.08808 = 0.04336 -0.00659 0.01037 0.00294 AFIX 23 H00W 2 0.508243 0.781643 0.986422 11.00000 -1.20000 H00X 2 0.448131 0.615029 0.970616 11.00000 -1.20000 AFIX 0 C00Q 1 0.248500 0.550283 0.305550 11.00000 0.05400 0.09644 = 0.04801 0.00101 -0.00009 0.00568 AFIX 23 H00Y 2 0.266493 0.650940 0.323094 11.00000 -1.20000 H 2 0.106208 0.539407 0.285768 11.00000 -1.20000 AFIX 0 C00R 1 0.732440 0.738333 1.110066 11.00000 0.12483 0.08144 = 0.03572 -0.00490 0.00736 -0.00166 AFIX 23 H00Z 2 0.696930 0.843195 1.106226 11.00000 -1.20000 HA 2 0.742254 0.711099 1.157773 11.00000 -1.20000 AFIX 0 C00S 1 0.564611 0.647046 1.070372 11.00000 0.08904 0.09361 = 0.04778 0.00331 0.02039 -0.00014 AFIX 23 H00 2 0.432958 0.669677 1.086431 11.00000 -1.20000 HB 2 0.592640 0.541931 1.078228 11.00000 -1.20000 AFIX 0 C00T 1 0.938577 0.713058 1.083905 11.00000 0.09796 0.07455 = 0.05055 0.00329 -0.01404 -0.01168 AFIX 23 H1 2 0.981440 0.610716 1.092720 11.00000 -1.20000 HC 2 1.041085 0.777598 1.108245 11.00000 -1.20000 AFIX 0 C00U 1 0.391906 0.525268 0.250577 11.00000 0.07690 0.09397 = 0.04093 0.00060 0.00598 0.00356 AFIX 23 H2 2 0.363845 0.428539 0.229667 11.00000 -1.20000 HD 2 0.365730 0.600681 0.215533 11.00000 -1.20000 AFIX 0 HKLF 4 REM 20221027-zyk-py-cy-me_a.res in P2(1) REM wR2 = 0.1471, GooF = S = 1.141, Restrained GooF = 1.141 for all data REM R1 = 0.0498 for 4023 Fo > 4sig(Fo) and 0.0748 for all 5469 data REM 273 parameters refined using 1 restraints END WGHT 0.0622 0.0916 REM Highest difference peak 0.159, deepest hole -0.198, 1-sigma level 0.042 Q1 1 0.4941 0.1672 0.3978 11.00000 0.05 0.16 Q2 1 0.7710 0.4635 0.6836 11.00000 0.05 0.15 Q3 1 0.5971 0.2043 0.4547 11.00000 0.05 0.15 Q4 1 0.1701 0.7920 0.3359 11.00000 0.05 0.14 Q5 1 0.3999 0.7177 0.2376 11.00000 0.05 0.14 Q6 1 0.2461 0.1747 0.3949 11.00000 0.05 0.14 Q7 1 0.5005 0.3627 0.4819 11.00000 0.05 0.14 ; _shelx_res_checksum 60079 _shelx_hkl_file ; 0 -11 0 0.97 1.56 0 -11 1 5.72 2.91 0 -11 -1 2.44 2.29 0 -11 2 0.97 1.77 0 -11 -2 1.67 2.31 0 -11 -3 0.89 1.47 0 -11 3 -2.75 2.36 0 -11 -4 0.29 1.47 0 -11 4 4.21 2.82 0 -11 5 6.36 3.21 0 -11 -5 2.89 2.44 0 -11 6 -5.60 2.97 0 -11 -6 0.30 1.64 0 -11 7 10.82 4.22 0 -11 -7 17.31 5.05 0 -11 -8 2.23 2.46 0 -10 0 1.39 1.84 0 -10 1 0.98 1.18 0 -10 -1 2.96 2.44 0 -10 2 5.76 2.94 0 -10 -2 4.38 2.78 0 -10 -3 5.75 2.71 0 -10 3 6.53 2.96 0 -10 4 9.13 3.56 0 -10 -4 3.40 2.11 0 -10 5 2.94 2.22 0 -10 -5 3.06 2.20 0 -10 -6 2.51 2.01 0 -10 6 8.25 3.19 0 -10 -7 1.56 3.23 0 -10 7 3.17 2.67 0 -10 -8 7.41 3.08 0 -10 8 6.79 3.03 0 -10 -9 3.87 2.65 0 -10 9 0.70 1.90 0 -10 -10 5.52 2.85 0 -10 10 8.30 3.25 0 -10 -11 5.04 2.74 0 -10 11 11.80 4.09 0 -10 -12 -2.84 2.07 0 -10 -13 4.80 2.81 0 -9 0 3.40 2.43 0 -9 -1 17.55 4.29 0 -9 1 15.38 3.88 0 -9 -2 31.84 5.73 0 -9 2 35.53 5.67 0 -9 3 7.04 2.46 0 -9 -3 7.82 3.21 0 -9 -4 9.22 3.15 0 -9 4 11.50 3.33 0 -9 5 23.32 4.83 0 -9 -5 17.81 4.29 0 -9 6 21.03 4.66 0 -9 -6 23.67 5.07 0 -9 7 -0.64 2.10 0 -9 -7 1.34 1.71 0 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2.04 0 -8 12 25.44 4.91 0 -8 -12 31.52 4.22 0 -8 13 8.06 3.13 0 -8 -13 3.05 1.57 0 -8 14 7.80 3.41 0 -8 -14 4.08 1.77 0 -8 15 3.14 2.29 0 -8 -15 1.74 1.09 0 -8 16 8.76 3.69 0 -8 -16 5.63 2.06 0 -8 17 2.58 2.45 0 -8 -17 2.60 1.69 0 -8 -18 0.46 1.07 0 -8 -19 -1.16 1.68 0 -8 19 -0.11 1.32 0 -7 0 12.35 2.99 0 -7 0 6.90 1.01 0 -7 -1 13.08 3.12 0 -7 1 10.48 2.79 0 -7 -1 12.70 1.86 0 -7 -1 12.44 1.46 0 -7 1 11.73 1.19 0 -7 -2 3.51 2.29 0 -7 2 0.74 2.26 0 -7 -2 5.57 1.40 0 -7 -3 165.10 7.38 0 -7 3 164.33 10.51 0 -7 -3 166.71 10.97 0 -7 -4 43.45 3.76 0 -7 4 49.88 5.88 0 -7 -4 51.29 6.15 0 -7 -5 8.40 1.79 0 -7 -5 8.43 2.40 0 -7 5 13.18 3.59 0 -7 -5 6.99 1.32 0 -7 -6 9.61 1.88 0 -7 6 10.06 2.40 0 -7 -6 4.71 1.88 0 -7 -6 8.89 1.52 0 -7 -7 96.98 6.21 0 -7 7 86.18 8.03 0 -7 -7 118.28 9.38 0 -7 8 53.70 6.25 0 -7 -8 64.33 3.61 0 -7 -8 51.11 4.48 0 -7 -9 21.04 3.00 0 -7 9 24.04 4.26 0 -7 -10 7.29 1.90 0 -7 10 6.17 2.74 0 -7 11 58.14 6.95 0 -7 -11 48.46 4.81 0 -7 -12 28.28 3.76 0 -7 12 38.73 5.82 0 -7 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3.17 0 2 5 47.59 2.24 0 2 -5 49.53 3.48 0 2 5 51.62 2.47 0 2 6 310.53 9.35 0 2 6 303.05 7.46 0 2 -6 296.26 9.02 0 2 6 317.41 7.32 0 2 -6 321.92 10.13 0 2 6 318.16 7.41 0 2 7 84.95 3.54 0 2 7 90.28 4.88 0 2 7 84.65 3.43 0 2 -7 81.37 4.54 0 2 8 60.13 4.14 0 2 8 58.68 3.08 0 2 8 63.08 3.00 0 2 -8 62.36 4.11 0 2 9 87.53 5.19 0 2 -9 90.83 5.25 0 2 9 99.90 3.94 0 2 10 130.39 6.66 0 2 -10 133.39 6.64 0 2 10 144.16 4.96 0 2 -10 138.71 4.80 0 2 11 46.23 4.02 0 2 -11 51.43 4.25 0 2 11 54.10 2.97 0 2 -11 50.06 2.88 0 2 12 66.16 5.00 0 2 -12 71.40 5.14 0 2 12 75.84 3.65 0 2 -12 68.01 3.57 0 2 -13 21.32 2.99 0 2 13 15.27 2.55 0 2 13 19.15 1.84 0 2 -13 18.28 1.93 0 2 -14 28.32 3.49 0 2 -14 30.20 2.57 0 2 14 26.18 3.37 0 2 14 31.73 2.44 0 2 -15 135.15 5.89 0 2 -15 145.53 8.14 0 2 15 148.77 5.62 0 2 15 130.00 8.04 0 2 -16 172.76 7.02 0 2 -16 173.72 9.10 0 2 16 175.11 6.29 0 2 16 152.18 9.06 0 2 -17 46.28 3.68 0 2 -17 47.57 4.85 0 2 17 51.18 3.27 0 2 17 36.97 4.64 0 2 18 81.04 7.04 0 2 -18 98.34 7.06 0 2 -18 87.73 5.24 0 2 -19 17.43 2.45 0 2 -19 18.68 3.21 0 2 19 16.93 3.36 0 2 -20 3.66 1.30 0 2 -20 5.38 1.87 0 2 20 2.06 1.31 0 2 -21 6.24 1.66 0 2 -21 7.04 2.10 0 2 21 6.38 2.07 0 2 22 9.44 2.81 0 2 -22 10.97 2.20 0 2 23 3.15 1.79 0 2 -23 2.61 1.24 0 2 24 -0.50 1.41 0 2 -24 0.53 1.00 0 2 -25 -1.51 1.13 0 3 0 0.11 0.15 0 3 0 0.05 0.55 0 3 0 -0.06 0.54 0 3 0 0.10 0.68 0 3 -1 9.45 0.73 0 3 -1 9.77 1.52 0 3 1 12.34 1.65 0 3 -1 10.55 1.03 0 3 1 11.30 0.84 0 3 -1 11.60 1.51 0 3 1 11.20 1.41 0 3 -1 10.38 1.62 0 3 -1 10.23 0.82 0 3 -2 868.16 13.44 0 3 -2 861.54 15.44 0 3 -2 862.12 17.81 0 3 2 869.03 14.19 0 3 -2 870.49 19.29 0 3 -2 856.47 16.80 0 3 2 866.77 16.40 0 3 -2 848.99 14.28 0 3 -3 212.47 5.87 0 3 -3 215.28 7.37 0 3 3 222.08 7.96 0 3 -3 208.20 8.12 0 3 3 200.00 4.92 0 3 -3 201.05 4.00 0 3 3 202.40 6.18 0 3 -3 212.06 6.68 0 3 4 220.67 5.34 0 3 -4 209.62 7.50 0 3 -4 200.28 6.07 0 3 4 215.04 6.36 0 3 -4 218.13 7.02 0 3 4 214.07 8.01 0 3 5 119.60 3.88 0 3 -5 111.71 4.41 0 3 -5 118.28 5.56 0 3 5 112.24 4.47 0 3 -5 117.91 5.23 0 3 5 118.80 5.95 0 3 -6 559.53 14.41 0 3 -6 601.30 12.95 0 3 6 571.77 12.46 0 3 6 586.98 15.51 0 3 -7 50.68 3.91 0 3 7 50.97 3.00 0 3 7 56.98 4.32 0 3 7 54.93 3.14 0 3 -8 300.28 10.26 0 3 8 294.36 8.13 0 3 8 283.97 10.50 0 3 8 284.66 8.32 0 3 -9 73.69 5.02 0 3 9 81.58 4.00 0 3 9 84.98 5.66 0 3 -10 84.63 3.53 0 3 -10 90.98 5.67 0 3 10 85.61 4.16 0 3 10 81.55 5.63 0 3 -11 73.22 3.43 0 3 -11 75.88 5.34 0 3 11 73.06 3.89 0 3 11 70.20 5.49 0 3 -12 25.00 2.14 0 3 -12 33.85 3.91 0 3 12 25.49 2.42 0 3 12 34.12 4.10 0 3 -13 30.17 2.40 0 3 -13 33.37 3.79 0 3 13 29.48 2.56 0 3 13 29.02 3.77 0 3 -14 84.23 4.32 0 3 -14 95.83 6.56 0 3 14 88.71 4.60 0 3 14 87.35 6.64 0 3 -15 115.15 5.31 0 3 -15 118.44 7.54 0 3 15 125.33 5.57 0 3 15 114.41 7.95 0 3 -16 87.16 4.76 0 3 -16 97.01 6.97 0 3 16 95.18 4.87 0 3 16 78.27 6.83 0 3 -17 65.57 4.28 0 3 17 69.75 6.57 0 3 -17 74.05 6.13 0 3 17 70.33 4.20 0 3 -18 14.83 2.15 0 3 18 19.65 3.83 0 3 -18 18.59 3.24 0 3 -19 29.94 3.12 0 3 -19 24.37 3.67 0 3 19 29.25 4.58 0 3 -20 30.96 3.32 0 3 -20 30.84 4.20 0 3 20 34.50 5.01 0 3 -21 24.87 3.10 0 3 -21 26.87 4.00 0 3 21 31.43 5.02 0 3 22 9.04 2.83 0 3 -22 3.91 1.41 0 3 23 5.15 2.44 0 3 -23 2.17 1.04 0 3 -24 2.66 1.32 0 3 -25 1.94 1.32 0 4 0 647.50 14.93 0 4 0 640.46 15.81 0 4 1 250.03 8.38 0 4 -1 233.65 8.43 0 4 -1 228.67 5.99 0 4 1 233.60 5.23 0 4 1 229.01 7.54 0 4 -1 229.42 7.63 0 4 -1 229.35 5.02 0 4 -2 994.64 21.14 0 4 -2 950.74 17.55 0 4 2 971.62 16.15 0 4 -2 988.53 19.83 0 4 2 998.45 19.42 0 4 -2 957.97 15.85 0 4 -3 1045.92 15.90 0 4 -3 1063.50 22.30 0 4 -3 992.60 19.05 0 4 3 1053.77 17.43 0 4 -3 1043.90 20.97 0 4 3 1039.52 20.37 0 4 -3 1028.07 17.16 0 4 -4 563.27 9.05 0 4 -4 549.31 12.44 0 4 -4 575.18 15.11 0 4 4 560.56 10.91 0 4 4 563.68 13.17 0 4 -4 579.37 14.15 0 4 -4 543.46 10.81 0 4 5 102.24 6.25 0 4 5 97.88 4.71 0 4 -5 102.31 5.36 0 4 -5 97.28 4.55 0 4 -5 115.49 6.13 0 4 6 95.64 6.20 0 4 -6 100.64 5.45 0 4 6 98.92 4.77 0 4 -6 112.48 6.20 0 4 -6 96.61 4.70 0 4 7 56.85 4.90 0 4 7 56.28 3.56 0 4 -7 67.26 4.80 0 4 -7 59.46 3.75 0 4 8 194.51 9.39 0 4 -8 205.25 8.91 0 4 -8 190.52 7.33 0 4 8 180.39 6.76 0 4 -9 3.81 1.40 0 4 -9 4.55 1.27 0 4 9 1.55 1.15 0 4 9 4.85 1.17 0 4 10 38.49 4.21 0 4 -10 39.17 4.04 0 4 -10 43.44 3.71 0 4 10 37.82 3.08 0 4 11 34.46 4.08 0 4 -11 35.51 2.28 0 4 -11 34.66 3.95 0 4 -11 41.26 3.72 0 4 11 34.59 2.95 0 4 12 57.20 5.42 0 4 -12 64.67 5.38 0 4 12 57.48 3.94 0 4 -12 54.29 3.02 0 4 -13 29.15 3.80 0 4 -13 27.41 2.24 0 4 13 24.61 3.86 0 4 13 25.93 2.72 0 4 -14 184.49 6.48 0 4 -14 196.18 9.99 0 4 14 183.55 7.44 0 4 14 186.15 10.52 0 4 -15 62.80 3.75 0 4 -15 59.91 5.58 0 4 15 61.06 4.21 0 4 15 56.90 5.95 0 4 -16 25.75 2.51 0 4 -16 27.25 3.89 0 4 16 30.38 2.96 0 4 16 29.39 4.48 0 4 -17 35.81 3.07 0 4 17 33.91 4.91 0 4 -17 34.47 4.41 0 4 17 32.29 3.08 0 4 18 2.00 1.62 0 4 -18 1.95 1.44 0 4 -18 4.72 1.24 0 4 19 26.27 4.54 0 4 -19 21.97 3.61 0 4 -19 21.02 2.55 0 4 -20 8.19 2.35 0 4 20 11.68 3.27 0 4 -20 7.58 2.38 0 4 -20 9.66 1.85 0 4 -21 1.32 1.14 0 4 -21 5.37 1.48 0 4 -21 2.88 1.73 0 4 21 6.09 2.59 0 4 -22 4.65 1.46 0 4 -22 5.41 2.25 0 4 22 3.70 2.24 0 4 -23 2.68 1.20 0 4 23 3.66 2.22 0 4 -23 2.68 1.66 0 4 -24 4.50 2.22 0 5 0 0.48 0.33 0 5 0 3.26 1.38 0 5 0 1.99 1.44 0 5 1 146.41 4.07 0 5 -1 157.77 3.96 0 5 -1 139.92 6.53 0 5 1 145.07 6.55 0 5 -1 157.69 7.49 0 5 -2 11.95 2.27 0 5 -2 8.36 1.14 0 5 2 10.22 1.00 0 5 -2 9.60 0.83 0 5 2 11.73 2.07 0 5 -2 8.30 1.85 0 5 -3 79.60 3.90 0 5 3 85.59 3.20 0 5 -3 86.24 5.18 0 5 3 88.43 4.98 0 5 -3 80.35 2.76 0 5 -3 89.36 5.69 0 5 -4 395.27 10.50 0 5 4 408.88 11.77 0 5 -4 413.23 12.53 0 5 -4 409.51 8.39 0 5 -4 410.90 7.65 0 5 -4 426.85 13.53 0 5 -5 18.43 2.18 0 5 5 18.94 2.57 0 5 -5 14.70 2.56 0 5 -5 13.42 1.34 0 5 -6 185.39 8.68 0 5 -6 166.75 6.77 0 5 -6 169.68 7.94 0 5 6 173.59 7.18 0 5 6 155.00 8.64 0 5 -7 32.18 3.66 0 5 7 28.41 3.68 0 5 7 30.76 2.99 0 5 -7 27.43 3.36 0 5 -7 29.02 2.81 0 5 8 38.97 4.57 0 5 8 42.33 3.49 0 5 -8 38.53 3.40 0 5 -8 42.91 4.33 0 5 9 50.29 5.20 0 5 -9 62.01 4.47 0 5 -9 57.92 5.12 0 5 9 52.47 3.96 0 5 -10 14.90 2.29 0 5 -10 14.06 1.32 0 5 -10 13.69 2.70 0 5 10 13.55 2.76 0 5 10 14.72 2.18 0 5 -11 12.94 2.26 0 5 -11 14.00 1.38 0 5 -11 13.83 2.73 0 5 11 6.46 2.20 0 5 11 10.34 1.87 0 5 -12 4.01 1.46 0 5 -12 2.21 1.39 0 5 12 5.40 1.38 0 5 -12 4.33 0.87 0 5 -13 107.68 4.44 0 5 -13 112.52 7.80 0 5 -13 124.15 7.38 0 5 13 103.94 5.93 0 5 13 117.05 8.63 0 5 -14 105.06 4.58 0 5 14 121.56 9.00 0 5 -14 117.80 8.09 0 5 -14 110.40 7.30 0 5 14 115.44 6.32 0 5 -15 20.14 3.31 0 5 -15 14.43 2.96 0 5 -15 16.71 1.88 0 5 15 17.46 3.55 0 5 15 16.03 2.40 0 5 -16 2.66 1.32 0 5 16 1.10 0.82 0 5 -16 1.74 0.72 0 5 16 -0.19 1.51 0 5 -16 1.68 1.27 0 5 -17 -0.08 0.95 0 5 17 1.84 0.96 0 5 -17 2.37 0.90 0 5 17 2.36 1.53 0 5 -17 1.34 1.27 0 5 -18 9.07 1.58 0 5 -18 10.35 2.62 0 5 -18 9.73 2.52 0 5 18 6.37 2.49 0 5 -19 8.38 2.40 0 5 -19 4.60 1.72 0 5 19 6.55 2.59 0 5 -20 17.34 3.54 0 5 -20 12.63 2.98 0 5 20 10.81 3.20 0 5 -21 7.80 2.53 0 5 -21 3.36 1.82 0 5 21 6.66 2.58 0 5 22 6.36 2.61 0 5 -22 3.74 2.14 0 5 -23 4.56 2.16 0 6 0 44.21 4.01 0 6 0 36.01 1.83 0 6 0 50.92 4.58 0 6 1 65.31 4.68 0 6 -1 61.13 4.69 0 6 -1 57.05 2.17 0 6 1 56.93 2.45 0 6 -1 59.81 4.91 0 6 2 132.57 6.86 0 6 -2 130.82 6.98 0 6 -2 130.33 3.42 0 6 2 129.43 4.09 0 6 -2 139.00 7.68 0 6 -3 241.73 7.18 0 6 -3 236.74 9.69 0 6 3 238.79 9.39 0 6 -4 334.90 12.54 0 6 -4 303.22 11.39 0 6 4 313.42 10.85 0 6 -4 307.14 6.29 0 6 -4 292.86 9.01 0 6 -5 191.53 9.41 0 6 -5 168.84 4.34 0 6 5 185.82 8.06 0 6 -5 167.06 8.46 0 6 -5 173.84 4.58 0 6 -5 172.78 6.82 0 6 -6 118.50 7.43 0 6 6 123.45 6.71 0 6 -6 116.63 3.96 0 6 -6 131.05 6.18 0 6 -7 57.56 5.23 0 6 -7 46.04 2.56 0 6 -7 52.17 3.96 0 6 -7 45.96 2.63 0 6 -7 50.03 4.85 0 6 7 45.43 4.01 0 6 -8 15.67 2.26 0 6 -8 15.10 2.83 0 6 8 12.70 2.82 0 6 8 14.42 2.33 0 6 -9 81.92 6.52 0 6 -9 63.57 2.54 0 6 9 84.07 7.27 0 6 -9 78.30 5.28 0 6 9 74.22 5.21 0 6 -10 60.00 5.62 0 6 -10 58.06 2.57 0 6 10 60.94 6.30 0 6 -10 59.52 4.76 0 6 10 55.51 4.53 0 6 -11 33.79 3.78 0 6 -11 37.22 4.49 0 6 -11 37.42 2.14 0 6 11 34.11 4.72 0 6 11 36.48 3.69 0 6 -12 71.95 6.50 0 6 -12 63.18 3.01 0 6 12 68.50 7.04 0 6 12 57.65 4.75 0 6 -12 67.52 5.49 0 6 13 71.07 7.25 0 6 13 66.70 5.09 0 6 -13 67.20 5.70 0 6 -13 72.18 6.61 0 6 14 40.45 5.51 0 6 -14 40.58 4.93 0 6 -14 40.41 4.57 0 6 14 39.61 3.97 0 6 -15 13.99 2.88 0 6 15 13.55 3.35 0 6 15 13.79 2.38 0 6 -15 15.55 3.15 0 6 -16 14.26 3.00 0 6 16 12.60 3.26 0 6 16 12.13 2.24 0 6 -16 11.02 2.78 0 6 -17 2.25 1.49 0 6 17 0.80 1.31 0 6 17 1.19 0.83 0 6 -17 -0.15 0.94 0 6 18 10.96 3.26 0 6 -18 10.04 2.75 0 6 -18 12.25 2.98 0 6 19 6.44 2.78 0 6 -19 7.57 2.44 0 6 -19 4.82 1.99 0 6 20 -0.03 1.62 0 6 -20 5.14 2.18 0 6 -20 2.38 1.55 0 6 -21 3.21 1.64 0 6 -21 3.50 1.92 0 6 -22 2.89 2.14 0 6 -23 0.88 1.36 0 7 0 11.20 2.40 0 7 1 11.61 2.26 0 7 -1 11.26 2.38 0 7 -1 15.36 2.75 0 7 -2 4.13 1.47 0 7 2 4.36 1.79 0 7 -2 2.06 1.30 0 7 -3 166.79 9.25 0 7 -3 146.52 8.31 0 7 3 174.13 8.62 0 7 -4 55.23 5.80 0 7 -4 52.98 5.10 0 7 4 56.84 4.85 0 7 -4 49.12 3.27 0 7 5 11.30 2.33 0 7 -5 9.39 2.54 0 7 -5 10.30 2.86 0 7 -5 7.68 1.40 0 7 6 8.23 2.02 0 7 -6 6.44 1.85 0 7 -6 3.67 1.81 0 7 -6 6.76 1.41 0 7 7 82.21 5.98 0 7 -7 82.38 6.89 0 7 -7 79.39 5.10 0 7 -8 56.56 5.66 0 7 -8 57.27 5.64 0 7 8 55.02 4.80 0 7 -8 54.38 4.33 0 7 -9 28.12 4.08 0 7 9 27.07 3.44 0 7 -9 26.06 3.15 0 7 -10 6.12 1.62 0 7 10 8.84 2.17 0 7 -10 11.37 2.98 0 7 11 51.91 6.40 0 7 -11 53.35 4.82 0 7 -11 64.71 6.47 0 7 11 56.02 4.96 0 7 12 35.54 5.33 0 7 -12 36.11 4.14 0 7 12 35.07 4.00 0 7 -12 34.64 4.77 0 7 -13 27.68 3.73 0 7 -13 25.81 4.16 0 7 13 23.28 4.55 0 7 13 27.38 3.58 0 7 14 6.74 1.86 0 7 -14 5.55 2.16 0 7 14 4.98 2.29 0 7 -14 5.05 1.73 0 7 15 3.86 1.36 0 7 -15 4.02 1.78 0 7 15 1.28 1.23 0 7 -15 5.05 1.73 0 7 16 1.84 1.14 0 7 -16 2.68 1.55 0 7 16 3.06 1.98 0 7 -16 0.29 0.92 0 7 17 6.64 2.68 0 7 -17 2.35 1.52 0 7 17 5.75 1.69 0 7 18 -1.18 1.59 0 7 -18 -0.66 1.27 0 7 19 3.99 2.45 0 7 -19 6.67 2.50 0 7 -20 3.29 1.81 0 7 -21 4.60 2.12 0 8 0 6.23 2.09 0 8 1 6.95 1.99 0 8 -1 8.82 2.28 0 8 -2 7.71 2.40 0 8 2 5.31 1.90 0 8 -2 6.33 2.09 0 8 -3 39.11 4.77 0 8 -3 28.07 4.04 0 8 3 34.89 4.34 0 8 -4 117.92 8.31 0 8 4 100.26 7.16 0 8 -4 99.57 7.61 0 8 -5 18.98 3.54 0 8 -5 19.49 3.55 0 8 5 19.30 3.19 0 8 -6 16.54 3.28 0 8 -6 10.38 2.61 0 8 6 15.24 2.92 0 8 -7 52.97 5.80 0 8 -7 43.78 5.27 0 8 7 53.37 5.13 0 8 -8 39.52 5.16 0 8 8 25.95 3.77 0 8 -8 31.45 4.65 0 8 -9 11.55 3.03 0 8 9 7.31 1.96 0 8 -10 78.35 7.30 0 8 10 76.31 6.33 0 8 -11 9.83 2.79 0 8 11 9.23 2.38 0 8 -12 30.51 4.74 0 8 12 21.55 3.46 0 8 -13 4.58 2.03 0 8 13 2.67 1.50 0 8 -14 2.62 1.45 0 8 14 5.59 1.98 0 8 15 -1.40 1.91 0 8 -15 3.72 1.88 0 8 15 4.82 1.77 0 8 16 2.05 1.87 0 8 -16 6.61 2.37 0 8 16 3.27 1.55 0 8 17 0.10 1.39 0 8 -17 1.28 1.29 0 8 17 3.17 1.62 0 8 -18 0.95 1.22 0 8 -19 1.38 1.32 0 8 -20 2.66 1.85 0 9 0 0.80 1.05 0 9 1 14.21 3.07 0 9 -1 16.03 3.21 0 9 2 32.53 4.45 0 9 -2 27.72 4.22 0 9 -3 4.48 2.02 0 9 3 6.72 2.18 0 9 -4 15.17 3.44 0 9 -4 10.90 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3.14 1 3 -19 9.54 2.64 -1 3 18 27.01 4.32 1 3 -18 23.34 3.87 1 3 -18 22.95 3.01 1 3 -18 22.14 2.64 -1 3 17 94.44 7.48 1 3 -17 83.01 4.92 1 3 -17 86.92 6.93 1 3 -17 88.91 5.91 -1 3 16 5.28 1.05 1 3 -16 4.00 1.37 -1 3 16 5.96 2.31 1 3 -16 4.13 1.84 -1 3 15 1.02 0.54 1 3 -15 2.67 1.56 1 3 -15 0.00 0.94 1 3 -14 11.09 2.34 1 3 -14 12.99 2.18 -1 3 14 12.53 2.55 -1 3 14 10.84 1.37 -1 3 13 49.28 4.78 1 3 -13 38.67 2.39 1 3 -13 44.07 3.81 1 3 -13 49.33 4.60 -1 3 13 42.60 2.80 -1 3 12 198.26 9.32 1 3 -12 207.01 8.41 1 3 -12 214.34 9.44 -1 3 12 198.37 6.40 1 3 -12 179.16 5.44 1 3 -11 15.59 2.26 1 3 -11 18.70 2.77 -1 3 11 20.63 2.98 -1 3 11 18.40 1.82 -1 3 10 55.34 4.56 -1 3 10 57.99 3.22 1 3 -10 67.28 4.82 1 3 -10 57.02 4.03 -1 3 9 166.73 7.74 1 3 -9 186.45 7.94 -1 3 9 154.36 5.51 1 3 -9 161.86 6.26 1 3 -9 155.43 6.68 -1 3 8 193.42 8.16 1 3 -8 197.05 8.15 -1 3 8 184.38 6.09 1 3 -8 197.65 6.68 1 3 -8 187.50 7.26 -1 3 7 168.86 7.34 1 3 -7 176.63 7.38 1 3 -7 177.29 6.01 -1 3 7 164.94 5.69 1 3 -7 172.48 5.93 1 3 -7 168.59 6.73 1 3 -6 37.16 2.95 1 3 -6 39.38 2.53 1 3 -6 37.74 3.23 -1 3 6 35.80 3.23 -1 3 6 37.05 2.56 1 3 -6 35.98 2.46 -1 3 6 39.82 2.57 1 3 -5 34.61 2.82 1 3 -5 37.53 2.37 1 3 -5 36.85 3.13 -1 3 5 39.58 3.23 -1 3 5 38.06 2.54 1 3 -5 40.33 2.52 -1 3 5 39.76 2.51 -1 3 4 20.82 1.89 1 3 -4 22.35 2.21 1 3 -4 24.78 1.81 1 3 -4 20.59 2.27 -1 3 4 24.38 2.46 -1 3 4 22.60 2.02 1 3 -4 24.38 1.91 -1 3 4 23.48 1.92 -1 3 3 44.32 2.82 1 3 -3 43.25 2.31 1 3 -3 40.02 2.96 -1 3 3 45.57 2.29 1 3 -3 45.91 3.27 -1 3 3 42.72 3.18 1 3 -3 44.27 2.57 -1 3 3 43.67 2.87 -1 3 3 46.24 2.63 -1 3 2 203.20 5.93 1 3 -2 196.35 7.02 1 3 -2 194.59 5.95 -1 3 2 201.66 6.71 1 3 -2 197.13 7.96 1 3 -2 203.40 6.71 1 3 -2 198.56 5.29 -1 3 2 190.39 6.49 -1 3 2 200.51 5.33 1 3 -1 23.53 2.20 1 3 -1 26.82 2.73 1 3 -1 27.74 2.11 -1 3 1 28.68 2.51 1 3 -1 28.43 2.24 -1 3 1 26.49 1.76 -1 3 1 28.35 2.43 -1 3 0 966.32 19.48 -1 3 0 967.12 17.16 -1 3 0 945.21 19.28 -1 3 0 962.98 19.56 1 3 0 973.80 18.13 1 3 0 976.51 18.52 -1 3 -1 73.62 4.19 -1 3 -1 71.20 4.09 -1 3 -1 67.04 3.11 -1 3 -1 65.89 4.03 1 3 1 72.59 3.56 1 3 1 70.45 3.52 -1 3 -2 284.03 9.17 1 3 2 287.37 7.98 1 3 2 305.06 7.99 -1 3 -2 303.80 9.33 -1 3 -3 63.98 4.13 -1 3 -3 60.82 4.11 1 3 3 65.08 3.44 1 3 3 62.44 3.23 -1 3 -4 92.30 5.20 1 3 4 83.63 5.13 -1 3 -4 85.08 4.94 1 3 4 92.32 4.23 -1 3 -4 85.23 2.49 -1 3 -5 832.51 19.33 -1 3 -5 783.07 13.42 1 3 5 820.52 19.49 1 3 5 782.62 13.44 -1 3 -6 173.90 7.86 1 3 6 163.33 6.07 -1 3 -6 160.46 4.30 1 3 6 155.54 7.46 1 3 6 157.39 4.32 -1 3 -7 401.16 12.90 1 3 7 370.52 12.39 1 3 7 368.80 8.08 -1 3 -7 382.82 8.13 1 3 7 371.49 10.11 -1 3 -8 9.27 2.28 1 3 8 8.76 1.05 -1 3 -8 11.56 1.22 1 3 8 9.25 1.97 1 3 8 9.03 1.56 -1 3 -9 242.66 10.40 1 3 9 230.35 9.95 1 3 9 225.31 6.48 -1 3 -9 251.09 6.74 1 3 9 236.94 7.90 -1 3 -10 17.69 1.70 -1 3 -10 19.90 3.18 1 3 10 15.90 1.63 1 3 10 16.51 2.78 1 3 10 17.83 2.08 -1 3 -11 5.26 1.87 1 3 11 7.86 2.15 1 3 11 4.26 1.11 -1 3 -11 3.80 0.88 -1 3 -12 8.00 2.33 1 3 12 6.98 2.10 1 3 12 3.36 1.03 -1 3 -12 6.03 1.15 -1 3 -13 8.82 2.47 1 3 13 8.67 1.57 1 3 13 11.37 2.53 -1 3 -13 10.03 1.52 -1 3 -14 80.94 6.75 1 3 14 76.65 4.73 -1 3 -14 74.35 4.41 1 3 14 67.05 6.07 -1 3 -15 89.59 7.22 1 3 15 87.00 5.13 -1 3 -15 94.37 5.22 1 3 15 99.16 7.52 -1 3 -16 35.61 4.66 1 3 16 40.44 4.93 -1 3 -16 42.44 3.67 1 3 16 39.14 3.44 -1 3 -17 7.70 2.32 1 3 17 7.93 1.65 1 3 17 5.02 2.02 -1 3 -17 8.04 1.71 -1 3 -18 56.29 6.13 1 3 18 57.60 4.29 1 3 18 42.95 5.47 -1 3 -18 55.02 4.51 1 3 19 44.93 5.68 -1 3 -19 47.98 4.37 -1 3 -19 50.50 5.92 1 3 20 35.55 5.27 -1 3 -20 39.05 4.09 -1 3 -20 39.35 5.34 1 3 21 34.89 5.39 -1 3 -21 31.33 4.84 -1 3 -21 34.27 3.97 1 3 22 8.49 2.74 -1 3 -22 6.81 2.38 -1 3 -22 9.91 2.22 1 3 23 6.26 2.48 -1 3 -23 6.78 1.97 -1 3 -24 6.48 2.01 1 4 -24 5.48 2.56 1 4 -24 3.06 1.31 -1 4 23 5.13 2.23 1 4 -23 1.93 1.53 1 4 -23 5.24 1.59 -1 4 22 0.62 1.22 1 4 -22 1.68 1.32 1 4 -22 2.05 0.94 -1 4 21 2.93 1.80 1 4 -21 2.62 1.87 1 4 -21 3.49 1.22 -1 4 20 3.03 1.77 1 4 -20 2.32 1.50 1 4 -20 2.00 0.90 1 4 -19 2.36 1.21 1 4 -19 3.52 1.14 1 4 -19 2.27 1.53 -1 4 19 5.21 2.26 1 4 -18 25.19 2.73 -1 4 18 28.38 4.53 1 4 -18 32.39 4.56 1 4 -18 28.05 3.60 -1 4 17 38.12 5.03 1 4 -17 28.95 3.63 1 4 -17 33.68 4.51 1 4 -17 35.13 3.14 1 4 -16 29.55 4.16 1 4 -16 27.12 3.46 -1 4 16 29.09 2.70 -1 4 16 25.36 4.05 1 4 -15 17.94 3.19 1 4 -15 20.61 2.95 -1 4 15 27.82 4.05 -1 4 15 22.49 2.35 -1 4 14 34.12 4.42 1 4 -14 26.39 3.34 1 4 -14 27.52 3.81 -1 4 14 31.28 2.78 -1 4 13 58.17 5.58 1 4 -13 56.96 5.22 -1 4 13 58.64 3.83 1 4 -13 55.54 4.71 1 4 -12 26.73 3.46 1 4 -12 24.80 3.14 -1 4 12 20.91 3.39 -1 4 12 25.55 2.52 1 4 -11 32.98 3.54 1 4 -11 28.96 3.57 -1 4 11 28.17 2.58 -1 4 11 31.32 3.85 1 4 -10 32.07 3.32 1 4 -10 31.79 3.56 -1 4 10 29.37 2.62 -1 4 10 27.62 3.50 1 4 -9 36.94 3.50 1 4 -9 35.61 3.60 -1 4 9 32.87 2.80 1 4 -9 34.02 3.13 -1 4 9 28.71 3.53 1 4 -8 74.78 4.90 -1 4 8 72.96 5.42 1 4 -8 76.41 5.15 -1 4 8 76.17 4.22 1 4 -8 71.00 4.34 1 4 -7 5.24 0.99 1 4 -7 6.08 1.49 1 4 -7 6.19 1.37 -1 4 7 4.72 1.20 -1 4 7 4.32 1.26 1 4 -7 3.89 1.41 1 4 -6 230.86 6.88 1 4 -6 239.47 8.95 -1 4 6 264.03 7.54 -1 4 6 233.40 9.54 1 4 -6 234.21 7.82 -1 4 6 229.70 7.81 1 4 -6 238.58 9.02 1 4 -5 172.53 7.37 1 4 -5 161.91 5.32 -1 4 5 180.83 5.87 -1 4 5 151.64 7.44 -1 4 5 148.41 6.18 1 4 -5 169.93 6.34 1 4 -5 168.18 7.22 1 4 -4 185.46 7.43 1 4 -4 188.71 7.56 1 4 -4 159.31 5.13 -1 4 4 175.11 6.69 -1 4 4 185.08 5.88 -1 4 4 161.03 7.43 1 4 -4 184.89 6.51 -1 4 4 165.77 6.57 1 4 -4 177.56 6.63 1 4 -3 102.47 5.33 -1 4 3 109.37 4.36 1 4 -3 106.85 5.49 1 4 -3 99.29 3.61 -1 4 3 103.84 5.11 -1 4 3 108.96 5.23 1 4 -3 104.99 4.75 1 4 -3 105.70 4.92 1 4 -2 237.34 8.13 -1 4 2 247.19 6.83 -1 4 2 228.71 8.03 -1 4 2 220.89 5.65 1 4 -2 227.30 5.48 -1 4 2 221.83 7.98 1 4 -2 230.77 7.47 1 4 -2 235.85 7.53 1 4 -1 184.73 7.02 -1 4 1 198.80 5.97 -1 4 1 188.48 5.07 -1 4 1 199.57 7.52 1 4 -1 194.83 6.70 -1 4 1 199.45 7.61 1 4 -1 196.24 6.63 -1 4 0 93.31 3.87 1 4 0 91.34 4.45 -1 4 0 93.84 5.34 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91.68 7.29 1 4 14 75.41 6.87 -1 4 -14 86.53 4.69 1 4 14 79.73 5.14 -1 4 -15 5.54 1.29 1 4 15 7.12 1.61 1 4 15 4.08 1.82 -1 4 -15 4.52 1.82 -1 4 -16 9.93 1.74 1 4 16 8.53 1.76 1 4 16 6.61 2.17 -1 4 -16 7.10 2.34 -1 4 -17 10.44 1.89 1 4 17 5.46 2.32 -1 4 -17 7.79 2.49 1 4 17 6.97 1.64 -1 4 -18 17.02 3.52 1 4 18 15.52 3.47 1 4 18 15.39 2.38 -1 4 -18 19.51 2.61 -1 4 -19 21.72 4.09 1 4 19 12.11 3.25 -1 4 -19 17.03 2.56 1 4 20 5.80 2.36 -1 4 -20 5.28 2.20 -1 4 -20 5.20 1.52 -1 4 -21 7.66 2.57 1 4 21 5.44 2.31 -1 4 -22 1.86 1.63 1 4 22 2.14 1.68 1 5 -23 10.06 3.22 -1 5 22 8.93 3.16 1 5 -22 9.36 3.01 -1 5 21 4.81 2.36 1 5 -21 5.43 2.33 -1 5 20 5.28 2.31 1 5 -20 8.16 2.72 1 5 -20 5.82 1.44 1 5 -19 9.58 2.21 -1 5 19 12.01 3.35 1 5 -19 10.79 2.87 1 5 -19 9.29 1.69 1 5 -18 6.82 1.92 -1 5 18 12.48 3.26 1 5 -18 5.56 2.12 1 5 -18 10.41 1.73 1 5 -17 7.33 2.01 1 5 -17 7.50 1.44 -1 5 17 10.76 2.99 1 5 -17 7.73 2.37 1 5 -16 31.95 4.01 -1 5 16 32.08 4.81 1 5 -16 29.41 4.35 -1 5 16 32.31 3.22 -1 5 15 13.78 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1 5 -4 9.13 1.78 1 5 -4 7.90 0.97 1 5 -4 8.03 1.75 -1 5 4 8.81 1.33 1 5 -4 7.69 1.58 -1 5 4 7.03 1.53 1 5 -4 9.95 1.52 -1 5 3 0.65 0.84 1 5 -3 0.50 0.49 1 5 -3 0.21 0.18 1 5 -3 -1.43 0.95 1 5 -3 -0.35 0.86 -1 5 3 -0.31 1.00 -1 5 3 0.55 0.62 -1 5 2 59.08 3.18 1 5 -2 56.05 3.96 -1 5 2 56.43 4.25 1 5 -2 56.43 3.88 -1 5 2 60.69 4.40 1 5 -2 58.39 3.54 -1 5 1 145.85 3.96 -1 5 1 156.08 7.31 -1 5 1 147.80 7.16 1 5 -1 143.71 6.35 -1 5 1 156.49 5.32 1 5 -1 150.29 5.79 -1 5 0 31.58 1.71 -1 5 0 35.31 3.47 1 5 0 29.91 2.82 -1 5 0 32.70 3.40 -1 5 0 33.73 2.30 1 5 0 32.21 2.49 -1 5 -1 49.77 2.42 -1 5 -1 61.30 4.63 1 5 1 51.91 3.20 -1 5 -1 57.18 3.00 1 5 1 47.65 3.61 -1 5 -1 52.49 4.34 -1 5 -2 5.11 0.99 1 5 2 4.12 1.22 -1 5 -2 4.06 1.69 -1 5 -2 8.35 2.08 -1 5 -2 3.85 0.75 -1 5 -3 241.41 10.05 -1 5 -3 223.34 5.23 1 5 3 235.36 8.47 -1 5 -3 212.25 9.35 -1 5 -3 227.16 6.74 -1 5 -4 253.60 6.53 -1 5 -4 290.63 11.13 1 5 4 263.36 9.17 -1 5 -5 40.60 2.48 -1 5 -5 49.50 4.67 1 5 5 43.80 3.56 -1 5 -6 50.07 2.95 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34.98 2.61 -2 0 -4 33.51 2.87 -2 0 -4 36.35 2.26 2 0 4 36.18 3.18 -2 0 -4 40.44 3.19 -2 0 -5 0.69 0.77 -2 0 -5 0.03 0.61 2 0 5 -0.41 0.68 -2 0 -6 2.86 1.09 2 0 6 1.01 1.48 -2 0 -6 2.58 0.93 2 0 6 2.14 0.76 2 0 7 403.81 10.47 -2 0 -7 391.80 11.41 2 0 7 405.89 11.95 -2 0 -7 415.43 11.76 2 0 8 53.88 3.55 -2 0 -8 46.94 3.64 2 0 8 54.53 4.16 2 0 9 214.05 7.90 -2 0 -9 200.41 8.07 2 0 9 203.90 8.33 -2 0 -10 6.27 1.50 2 0 10 7.20 2.01 2 0 10 7.93 1.68 -2 0 -11 -0.62 1.02 2 0 11 1.44 1.73 2 0 11 0.08 0.98 2 0 12 76.78 5.35 -2 0 -12 77.11 5.29 2 0 12 85.86 5.69 2 0 13 429.36 14.17 -2 0 -13 455.62 14.21 2 0 13 433.48 13.76 2 0 14 125.40 7.51 -2 0 -14 135.94 7.52 2 0 14 132.06 7.10 2 0 15 83.02 6.33 2 0 15 93.18 6.06 -2 0 -15 88.13 6.23 2 0 16 3.46 1.70 2 0 16 4.74 1.87 -2 0 -16 3.95 1.70 2 0 17 10.84 2.52 2 0 17 16.94 2.71 -2 0 -17 13.38 2.61 2 0 18 1.52 1.03 2 0 18 2.07 1.12 -2 0 -18 4.27 1.70 -2 0 -19 10.19 2.51 2 0 19 8.20 2.42 -2 0 -20 12.10 2.73 2 0 20 5.85 2.04 -2 0 -21 13.33 3.03 2 0 21 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24.88 -2 1 8 1159.88 22.13 -2 1 8 1080.01 20.73 -2 1 8 1072.06 22.01 -2 1 8 1046.66 18.27 2 1 -7 505.22 8.93 -2 1 7 518.42 12.03 -2 1 7 549.26 12.92 2 1 -7 527.62 14.66 2 1 -7 483.44 12.97 -2 1 7 518.81 12.43 -2 1 7 490.83 10.28 2 1 -6 25.02 1.43 -2 1 6 23.33 2.36 2 1 -6 25.35 2.81 2 1 -6 24.45 2.36 -2 1 6 31.86 2.56 -2 1 6 24.18 1.84 2 1 -5 1265.57 21.01 -2 1 5 1274.32 19.71 -2 1 5 1325.59 23.63 2 1 -5 1260.36 25.98 -2 1 5 1350.85 24.61 2 1 -5 1302.43 25.13 2 1 -5 1251.20 23.68 -2 1 5 1291.07 22.39 -2 1 5 1283.69 22.33 -2 1 4 290.08 8.30 2 1 -4 276.39 9.62 -2 1 4 277.33 6.47 2 1 -4 297.67 9.24 -2 1 4 310.47 9.06 2 1 -4 283.41 8.17 -2 1 4 274.77 6.93 2 1 -4 301.59 7.54 2 1 -4 277.15 6.82 -2 1 4 288.49 7.81 2 1 -3 462.47 12.10 -2 1 3 461.54 11.84 2 1 -3 429.50 10.48 -2 1 3 443.08 8.85 2 1 -3 478.30 10.04 2 1 -3 449.64 12.56 -2 1 3 475.65 11.25 -2 1 3 450.27 10.79 2 1 -2 110.32 4.38 -2 1 2 122.09 5.07 2 1 -2 113.49 5.67 2 1 -2 124.70 5.51 -2 1 2 119.30 5.44 2 1 -2 120.71 4.27 -2 1 2 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5 3.76 0.93 2 3 -5 4.70 0.94 -2 3 4 16.71 1.93 2 3 -4 15.81 1.95 -2 3 4 16.61 1.91 -2 3 4 15.34 1.72 2 3 -4 17.39 1.73 2 3 -4 19.49 2.65 -2 3 3 75.67 4.01 2 3 -3 84.41 3.94 2 3 -3 81.21 4.34 -2 3 3 81.70 4.38 -2 3 3 78.33 4.06 2 3 -3 79.17 5.25 -2 3 2 108.52 5.18 2 3 -2 113.23 5.16 2 3 -2 122.01 4.89 2 3 -2 108.45 6.08 -2 3 2 111.55 5.06 -2 3 2 106.48 3.52 -2 3 1 44.10 3.26 2 3 -1 44.87 2.96 -2 3 1 41.93 2.16 2 3 -1 45.38 3.82 -2 3 1 48.44 3.44 -2 3 0 25.66 2.52 -2 3 0 25.88 1.75 -2 3 0 27.24 2.73 -2 3 0 23.93 2.10 2 3 0 25.92 2.32 -2 3 -1 50.61 3.29 -2 3 -1 52.50 3.69 2 3 1 48.49 3.27 -2 3 -1 55.82 4.06 -2 3 -1 51.09 2.61 -2 3 -2 136.02 5.79 -2 3 -2 136.44 6.23 2 3 2 135.96 5.76 -2 3 -2 136.23 4.72 -2 3 -2 131.36 6.60 2 3 3 39.68 3.13 -2 3 -3 41.88 3.81 -2 3 -3 35.94 2.99 -2 3 -4 201.75 8.90 -2 3 -4 174.98 7.33 2 3 4 192.46 7.32 -2 3 -4 187.56 5.80 -2 3 -5 309.81 11.65 2 3 5 293.57 9.51 -2 3 -5 286.72 7.92 2 3 5 264.80 10.25 -2 3 -6 73.95 5.76 2 3 6 65.64 5.00 -2 3 -6 69.18 3.62 2 3 6 72.56 4.54 -2 3 -7 12.24 1.60 -2 3 -7 13.99 2.90 2 3 7 9.57 2.10 2 3 7 11.96 2.01 -2 3 -8 4.63 1.10 2 3 8 3.68 0.92 -2 3 -8 5.69 2.05 2 3 8 4.66 1.52 -2 3 -9 19.31 3.42 -2 3 -9 15.99 1.97 2 3 9 13.40 2.53 2 3 9 14.93 2.26 -2 3 -10 52.03 5.42 2 3 10 44.46 3.83 -2 3 -10 42.30 3.27 2 3 10 44.54 4.55 -2 3 -11 92.42 7.28 2 3 11 85.10 5.31 -2 3 -11 78.31 4.69 2 3 11 71.91 5.96 -2 3 -12 70.67 6.61 2 3 12 58.55 5.60 -2 3 -12 59.09 4.22 2 3 12 60.58 4.60 -2 3 -13 1.93 1.01 -2 3 -13 4.47 2.32 2 3 13 1.56 1.35 2 3 13 3.34 1.41 -2 3 -14 6.85 1.62 2 3 14 6.13 2.04 2 3 14 6.34 1.65 -2 3 -15 12.88 2.24 -2 3 -15 12.98 3.28 2 3 15 11.87 2.81 2 3 15 9.95 2.04 -2 3 -16 10.22 2.13 -2 3 -16 10.48 2.94 2 3 16 7.82 2.52 2 3 16 9.10 1.87 -2 3 -17 2.05 1.13 -2 3 -17 2.12 1.72 2 3 17 2.39 1.60 2 3 17 0.73 0.84 -2 3 -18 7.25 1.87 -2 3 -18 11.11 3.06 2 3 18 10.39 2.91 2 3 18 11.22 2.21 -2 3 -19 4.54 1.53 -2 3 -19 3.39 1.94 2 3 19 2.40 1.62 2 3 19 2.87 1.16 2 3 20 18.68 4.01 -2 3 -20 20.00 4.15 -2 3 -20 20.59 3.33 2 3 21 15.06 3.81 -2 3 -21 9.93 2.99 -2 3 -21 14.55 2.90 2 3 22 11.42 3.42 -2 3 -22 10.82 3.26 -2 3 -22 10.26 2.55 2 3 23 12.07 3.51 -2 3 -23 5.80 2.62 -2 3 -24 1.24 1.70 2 4 -25 1.26 1.07 2 4 -24 1.34 1.09 2 4 -23 4.29 1.48 2 4 -23 2.60 2.08 -2 4 23 5.95 2.46 2 4 -22 4.85 1.52 2 4 -22 5.43 2.37 -2 4 22 3.72 2.03 2 4 -21 12.66 2.30 -2 4 21 13.60 3.42 2 4 -21 11.83 3.26 -2 4 20 16.19 3.71 2 4 -20 14.60 3.60 -2 4 19 5.89 2.12 2 4 -19 10.70 2.90 -2 4 18 0.94 1.44 2 4 -18 2.02 1.94 2 4 -17 34.04 3.45 2 4 -17 33.60 5.01 -2 4 17 36.71 4.89 2 4 -16 10.15 1.92 -2 4 16 14.10 2.99 2 4 -16 10.65 2.92 2 4 -15 13.36 2.19 -2 4 15 16.35 3.16 2 4 -15 12.88 2.95 -2 4 15 11.41 1.77 2 4 -14 2.40 1.06 -2 4 14 5.70 1.32 -2 4 14 5.53 2.05 2 4 -14 1.43 1.25 2 4 -13 61.27 4.54 2 4 -13 69.43 6.44 -2 4 13 63.42 4.16 -2 4 13 63.47 5.70 2 4 -12 45.02 3.86 2 4 -12 45.71 5.05 2 4 -12 47.32 3.71 -2 4 12 40.54 3.34 -2 4 12 38.99 4.44 2 4 -11 91.18 5.51 -2 4 11 97.22 6.66 2 4 -11 93.92 6.99 -2 4 11 87.77 4.98 2 4 -11 108.29 5.47 2 4 -10 63.69 4.57 -2 4 10 68.97 4.30 -2 4 10 60.19 5.08 2 4 -10 70.59 5.95 2 4 -10 75.07 4.33 -2 4 10 62.21 4.25 2 4 -9 2.24 1.03 -2 4 9 3.25 1.19 -2 4 9 3.67 1.28 2 4 -9 2.31 0.95 -2 4 9 2.57 1.16 2 4 -9 2.77 1.42 2 4 -8 39.27 4.31 2 4 -8 42.30 3.06 -2 4 8 38.29 3.32 -2 4 8 40.83 3.23 -2 4 8 40.38 3.94 2 4 -7 118.45 7.19 -2 4 7 107.75 6.31 2 4 -7 115.75 5.12 -2 4 7 103.99 5.68 -2 4 7 122.95 5.61 -2 4 6 71.94 3.89 -2 4 6 63.33 3.80 2 4 -6 66.66 4.18 2 4 -6 69.58 5.40 -2 4 6 60.38 4.51 2 4 -6 65.34 3.74 -2 4 6 66.11 4.51 -2 4 6 64.22 4.02 -2 4 5 42.92 3.20 -2 4 5 45.98 3.09 2 4 -5 40.24 3.16 2 4 -5 38.35 3.93 -2 4 5 41.29 3.62 2 4 -5 37.82 2.85 -2 4 5 46.65 3.79 -2 4 5 44.75 3.29 2 4 -4 9.55 1.49 -2 4 4 7.97 1.48 -2 4 4 10.79 1.50 -2 4 4 9.11 1.54 2 4 -4 8.36 1.40 2 4 -4 8.78 1.89 2 4 -3 43.56 4.02 -2 4 3 45.59 3.15 2 4 -3 42.89 3.07 -2 4 3 46.05 3.47 2 4 -3 46.37 3.21 2 4 -2 89.85 5.75 -2 4 2 102.43 5.36 -2 4 2 97.13 4.78 2 4 -2 97.92 4.83 2 4 -1 119.72 6.66 -2 4 1 139.43 6.52 -2 4 1 131.33 5.77 2 4 -1 130.35 5.71 -2 4 0 19.69 2.58 -2 4 0 14.51 1.94 2 4 0 13.91 1.89 -2 4 0 15.62 1.98 -2 4 -1 0.09 0.93 -2 4 -1 -0.06 0.23 -2 4 -1 0.46 0.64 -2 4 -1 0.12 0.43 2 4 1 0.40 0.63 2 4 2 15.63 2.09 -2 4 -2 14.96 1.25 -2 4 -2 13.84 1.96 -2 4 -2 17.85 2.63 2 4 3 74.28 4.53 -2 4 -3 81.56 5.55 -2 4 -3 78.70 4.84 2 4 4 188.89 7.50 -2 4 -4 198.89 9.13 2 4 5 120.09 5.93 -2 4 -5 122.75 7.36 -2 4 -6 24.26 3.47 2 4 6 20.12 2.45 -2 4 -6 21.09 1.76 -2 4 -7 48.33 4.82 2 4 7 43.15 3.63 -2 4 -7 41.62 2.66 2 4 7 40.06 1.68 2 4 7 38.36 4.28 -2 4 -8 72.94 6.11 2 4 8 68.01 4.63 -2 4 -8 69.72 3.71 2 4 8 68.88 5.88 2 4 8 68.14 2.63 -2 4 -9 66.66 6.02 2 4 9 66.95 4.64 -2 4 -9 67.17 3.81 2 4 9 60.06 2.72 2 4 9 61.90 5.71 -2 4 -10 80.56 6.63 2 4 10 66.88 3.12 2 4 10 74.84 6.42 -2 4 -10 82.43 4.46 2 4 10 73.84 4.99 -2 4 -11 5.07 1.16 2 4 11 3.20 1.68 -2 4 -11 7.20 2.34 2 4 11 6.52 1.58 -2 4 -12 15.61 3.21 2 4 12 15.91 3.14 2 4 12 16.95 2.52 -2 4 -12 16.27 2.15 -2 4 -13 20.29 3.76 -2 4 -13 23.50 2.66 2 4 13 18.44 3.50 2 4 13 21.97 2.89 -2 4 -14 51.51 5.80 2 4 14 47.75 5.64 -2 4 -14 49.95 4.04 2 4 14 49.02 4.36 -2 4 -15 7.76 1.73 -2 4 -15 9.51 2.78 2 4 15 4.50 2.06 2 4 15 7.66 1.80 -2 4 -16 3.24 1.27 -2 4 -16 3.90 2.37 2 4 16 2.92 1.68 2 4 16 0.97 0.85 -2 4 -17 2.42 1.11 -2 4 -17 2.76 1.99 2 4 17 2.17 1.69 2 4 17 0.08 0.76 -2 4 -18 1.80 0.99 2 4 18 -0.53 1.49 2 4 18 1.13 0.98 -2 4 -18 1.33 1.64 2 4 19 1.04 1.37 2 4 19 1.89 1.11 -2 4 -19 1.24 1.74 -2 4 -20 5.76 2.31 2 4 20 6.67 2.60 -2 4 -21 0.00 1.45 2 4 21 1.85 1.66 -2 4 -22 1.40 1.93 2 4 22 1.98 1.86 -2 4 -23 18.17 4.28 -2 4 -24 0.85 1.53 2 5 -23 0.00 1.47 -2 5 22 19.33 4.49 2 5 -22 21.13 4.70 2 5 -22 18.48 2.74 -2 5 21 7.00 2.75 2 5 -21 10.82 3.35 2 5 -21 15.06 2.45 2 5 -20 5.20 2.35 -2 5 20 7.95 2.79 2 5 -19 7.26 2.69 -2 5 19 4.26 2.28 2 5 -18 6.23 2.41 -2 5 18 2.61 1.63 2 5 -17 4.50 2.26 -2 5 17 2.71 1.71 2 5 -17 1.23 0.88 -2 5 16 50.14 5.87 2 5 -16 56.30 6.39 2 5 -16 45.39 4.37 2 5 -15 6.95 2.38 -2 5 15 6.57 2.36 -2 5 15 5.11 1.35 2 5 -15 8.02 1.90 2 5 -14 4.47 2.10 -2 5 14 1.69 1.09 -2 5 14 3.44 1.23 2 5 -14 1.39 0.96 2 5 -13 18.23 2.78 2 5 -13 20.22 3.61 -2 5 13 15.61 3.08 -2 5 13 17.76 2.51 -2 5 12 152.97 9.34 2 5 -12 152.49 9.57 2 5 -12 149.68 7.86 2 5 -12 156.00 7.70 -2 5 12 132.67 6.98 -2 5 11 117.79 7.97 2 5 -11 128.09 8.52 2 5 -11 111.31 6.83 -2 5 11 115.17 6.44 2 5 -11 122.98 6.53 -2 5 10 105.89 7.35 2 5 -10 104.34 7.47 2 5 -10 105.96 5.86 -2 5 10 97.19 5.86 2 5 -10 105.35 6.51 -2 5 9 17.14 2.93 -2 5 9 13.21 2.26 2 5 -9 13.64 2.07 -2 5 9 16.78 2.23 2 5 -9 11.86 2.64 -2 5 8 9.30 2.17 2 5 -8 11.33 1.87 -2 5 8 12.18 1.87 -2 5 8 9.93 1.99 2 5 -8 10.56 2.26 -2 5 7 12.85 2.35 -2 5 7 14.52 2.01 2 5 -7 11.23 2.41 -2 5 7 14.41 2.53 2 5 -7 13.68 1.98 2 5 -6 66.51 5.48 -2 5 6 55.54 4.80 -2 5 6 70.53 4.28 2 5 -6 64.01 4.24 -2 5 6 70.04 5.02 -2 5 6 63.51 4.31 2 5 -6 62.45 4.06 2 5 -5 83.76 6.11 -2 5 5 86.17 4.74 -2 5 5 80.52 5.56 2 5 -5 86.35 4.95 -2 5 5 88.99 4.30 2 5 -5 75.17 4.31 -2 5 5 89.22 5.27 2 5 -4 29.20 3.57 -2 5 4 27.69 2.65 2 5 -4 27.24 2.74 -2 5 4 34.04 3.65 -2 5 4 31.07 3.13 -2 5 4 29.12 2.39 2 5 -4 25.08 2.34 2 5 -3 27.44 3.37 -2 5 3 29.47 3.13 -2 5 3 29.08 2.41 -2 5 3 27.89 2.65 2 5 -3 30.00 2.87 -2 5 2 3.49 0.93 -2 5 2 3.17 1.03 2 5 -2 5.08 1.37 2 5 -2 2.77 1.26 -2 5 2 5.98 1.50 2 5 -1 42.66 3.52 -2 5 1 42.60 3.11 -2 5 1 41.89 3.83 2 5 0 20.01 2.42 -2 5 0 21.36 2.89 -2 5 0 21.35 2.23 -2 5 -1 24.71 3.10 2 5 1 23.76 2.70 -2 5 -1 23.92 2.49 -2 5 -2 68.63 5.28 2 5 2 69.19 4.66 -2 5 -2 63.64 4.23 -2 5 -3 56.80 2.30 -2 5 -3 74.58 5.65 2 5 3 70.11 4.65 -2 5 -3 57.24 4.07 -2 5 -4 161.43 8.56 2 5 4 147.50 7.01 -2 5 -4 141.30 6.82 2 5 5 22.99 2.82 -2 5 -5 17.57 3.06 2 5 6 32.99 3.28 -2 5 -6 27.03 3.75 -2 5 -7 46.89 4.96 2 5 7 42.24 3.84 -2 5 -8 4.47 2.04 2 5 8 -0.32 1.09 2 5 8 3.02 1.42 -2 5 -8 1.31 0.46 -2 5 -9 3.08 1.93 2 5 9 3.99 1.44 2 5 9 4.58 2.05 -2 5 -9 3.31 0.78 -2 5 -10 48.60 5.37 2 5 10 34.05 4.71 -2 5 -10 44.20 3.00 2 5 10 44.86 4.09 -2 5 -11 5.48 1.21 2 5 11 3.09 1.74 -2 5 -11 4.98 2.14 2 5 11 5.68 1.67 -2 5 -12 32.12 4.64 2 5 12 24.77 4.14 2 5 12 29.24 3.48 2 5 13 38.83 5.45 -2 5 -13 47.94 5.75 2 5 13 42.71 4.20 2 5 14 12.65 3.26 2 5 14 15.42 2.56 -2 5 -14 16.72 3.62 2 5 15 0.70 1.29 2 5 15 -0.51 0.99 -2 5 -15 2.23 1.85 2 5 16 -1.33 1.33 2 5 16 0.41 0.71 -2 5 -16 -0.74 1.62 2 5 17 -2.13 2.22 2 5 17 0.14 0.82 -2 5 -17 0.60 1.30 2 5 18 4.57 2.09 2 5 18 6.23 1.81 -2 5 -18 6.93 2.68 2 5 19 0.42 1.40 2 5 19 0.96 0.93 -2 5 -19 0.14 1.16 -2 5 -20 14.50 3.79 2 5 20 9.69 3.16 -2 5 -21 3.32 2.03 2 5 21 0.37 1.12 -2 5 -22 14.86 3.84 2 6 -22 3.05 2.01 2 6 -21 5.67 2.51 -2 6 21 2.84 1.95 2 6 -20 3.01 2.03 -2 6 20 -1.52 1.85 2 6 -19 -0.08 1.14 -2 6 19 2.00 1.64 2 6 -18 7.17 1.93 2 6 -18 9.32 2.99 -2 6 18 8.60 2.94 2 6 -17 2.36 1.14 2 6 -17 4.73 2.12 -2 6 17 2.44 1.54 2 6 -16 3.06 1.46 -2 6 16 2.26 1.44 2 6 -16 5.89 2.35 -2 6 15 10.15 2.07 2 6 -15 12.24 2.51 -2 6 15 9.16 2.50 2 6 -15 10.76 2.87 -2 6 14 15.39 2.59 2 6 -14 14.73 2.76 -2 6 14 20.83 3.86 2 6 -14 18.50 3.66 -2 6 13 3.22 1.27 2 6 -13 4.79 1.67 2 6 -13 2.38 1.21 -2 6 13 3.67 1.98 2 6 -13 6.51 2.30 2 6 -12 1.78 1.10 -2 6 12 0.87 0.86 2 6 -12 1.78 1.14 -2 6 12 0.12 1.24 -2 6 11 14.00 2.54 2 6 -11 12.85 2.41 2 6 -11 14.92 2.76 -2 6 11 14.70 3.19 2 6 -11 12.73 2.83 -2 6 10 15.67 3.19 2 6 -10 13.99 2.81 -2 6 10 13.44 2.40 2 6 -10 16.66 2.64 -2 6 9 14.11 2.87 2 6 -9 11.43 2.51 2 6 -9 14.35 2.39 -2 6 9 15.23 2.67 2 6 -8 20.08 3.27 -2 6 8 21.48 3.46 2 6 -8 20.09 2.75 -2 6 8 20.32 3.07 -2 6 8 22.77 2.55 2 6 -7 2.81 1.49 -2 6 7 4.97 1.87 2 6 -7 2.84 1.19 -2 6 7 5.39 1.38 2 6 -6 21.09 3.25 -2 6 6 20.01 2.98 2 6 -6 16.69 2.38 -2 6 6 22.63 2.49 -2 6 5 37.81 3.72 2 6 -5 38.04 2.88 2 6 -5 38.16 4.23 2 6 -5 40.81 3.70 -2 6 5 36.91 4.06 -2 6 5 42.96 3.33 -2 6 4 130.22 7.14 -2 6 4 134.17 5.10 2 6 -4 129.33 7.78 -2 6 4 126.32 7.56 2 6 -4 122.31 6.50 -2 6 4 125.55 5.90 -2 6 3 6.36 2.22 -2 6 3 2.96 1.07 2 6 -3 1.96 1.12 -2 6 3 2.81 0.84 -2 6 3 3.17 1.39 2 6 -3 2.10 0.97 -2 6 2 4.50 1.12 2 6 -2 1.90 0.77 -2 6 2 3.25 0.81 -2 6 2 4.31 1.46 -2 6 1 2.00 0.64 -2 6 1 2.40 0.87 2 6 -1 2.14 0.96 -2 6 1 1.66 1.17 2 6 0 18.95 2.61 -2 6 0 18.03 2.12 -2 6 0 17.58 2.87 -2 6 0 20.79 2.14 2 6 1 11.85 2.19 -2 6 -1 14.44 2.73 -2 6 -1 11.94 1.66 -2 6 -2 56.10 3.81 2 6 2 60.99 4.68 -2 6 -2 58.90 5.24 -2 6 -3 17.87 2.22 -2 6 -3 17.81 2.97 2 6 3 21.86 2.91 -2 6 -4 28.87 2.95 2 6 4 30.62 3.37 -2 6 -4 33.06 4.14 -2 6 -5 47.54 3.92 -2 6 -5 44.55 2.23 -2 6 -5 49.95 5.21 2 6 5 44.46 4.17 -2 6 -6 33.27 2.19 -2 6 -6 35.85 4.49 2 6 6 37.94 3.86 -2 6 -7 59.75 5.89 -2 6 -7 53.11 3.10 2 6 7 63.66 4.98 -2 6 -8 16.29 3.26 2 6 8 17.38 2.70 -2 6 -9 1.52 1.58 2 6 9 1.42 1.00 -2 6 -10 1.73 1.73 2 6 10 4.06 1.54 2 6 11 8.05 2.48 -2 6 -11 15.48 3.36 2 6 11 11.26 2.31 2 6 12 9.03 2.95 -2 6 -12 14.01 3.36 2 6 12 10.43 2.26 2 6 13 11.63 3.28 -2 6 -13 13.97 3.35 2 6 13 15.51 2.71 2 6 14 2.94 2.14 -2 6 -14 1.58 1.56 2 6 14 -0.45 0.87 2 6 15 4.57 2.48 -2 6 -15 3.72 2.15 2 6 15 3.98 1.60 2 6 16 1.83 1.54 -2 6 -16 1.69 1.65 2 6 16 1.24 0.97 2 6 17 -0.71 1.35 -2 6 -17 2.02 1.58 2 6 17 1.95 1.25 2 6 18 0.43 1.52 -2 6 -18 -1.38 1.52 2 6 18 -0.52 0.70 2 6 19 8.83 3.14 -2 6 -19 9.38 3.00 2 6 19 7.15 2.05 -2 6 -20 4.53 2.28 2 7 -21 2.30 1.90 2 7 -20 -1.15 1.44 2 7 -19 0.79 1.23 -2 7 19 2.08 1.63 2 7 -18 11.20 2.56 2 7 -18 12.91 3.53 -2 7 18 12.56 3.64 2 7 -17 1.88 1.28 2 7 -17 5.20 2.26 -2 7 17 3.11 1.84 2 7 -16 5.12 1.68 -2 7 16 3.14 1.67 2 7 -16 2.52 1.73 2 7 -15 1.16 1.12 -2 7 15 1.25 1.57 2 7 -15 3.42 1.78 -2 7 15 1.46 1.15 2 7 -14 16.31 3.10 -2 7 14 13.21 2.54 -2 7 14 19.31 3.99 2 7 -14 17.56 3.69 -2 7 13 33.51 5.09 2 7 -13 36.41 5.01 2 7 -13 38.66 4.67 -2 7 13 33.02 4.05 2 7 -13 33.07 4.32 2 7 -12 21.42 3.79 -2 7 12 21.99 4.06 2 7 -12 24.11 3.60 -2 7 12 22.20 3.42 2 7 -11 35.86 4.78 -2 7 11 37.42 4.33 2 7 -11 34.90 4.23 -2 7 11 32.59 4.81 2 7 -10 14.92 3.07 2 7 -10 11.16 2.45 -2 7 10 10.32 2.49 2 7 -9 1.24 1.28 2 7 -9 0.66 1.08 -2 7 9 0.36 1.02 2 7 -8 12.95 2.75 -2 7 8 11.16 2.48 2 7 -8 13.95 2.48 2 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3.89 -4 4 10 37.67 3.92 4 4 -10 38.65 3.08 -4 4 9 20.98 2.04 -4 4 9 19.66 2.95 4 4 -9 23.13 4.10 -4 4 9 21.89 2.92 -4 4 9 22.72 3.08 4 4 -9 21.93 2.39 -4 4 8 86.65 4.57 -4 4 8 86.93 6.11 4 4 -8 101.02 8.31 -4 4 8 83.37 5.57 -4 4 8 85.30 6.03 4 4 -8 83.51 4.84 -4 4 7 37.55 3.56 4 4 -7 42.42 5.34 4 4 -7 43.33 3.56 -4 4 7 44.21 4.35 -4 4 7 41.13 3.30 -4 4 6 2.38 0.93 4 4 -6 1.45 1.32 -4 4 6 2.22 0.87 -4 4 6 2.34 1.17 4 4 -6 2.76 1.07 -4 4 5 19.68 3.02 -4 4 5 19.17 2.49 4 4 -5 20.01 3.69 4 4 -5 18.78 2.43 -4 4 4 51.34 4.94 4 4 -4 48.35 3.98 4 4 -4 57.74 6.11 -4 4 4 56.18 4.43 -4 4 3 4.45 1.53 4 4 -3 7.70 1.71 4 4 -3 7.58 2.43 -4 4 3 7.11 1.71 4 4 -2 47.96 4.09 -4 4 2 53.67 4.61 4 4 -2 54.37 5.71 -4 4 2 46.98 4.68 4 4 -1 38.50 3.72 -4 4 1 39.29 4.22 -4 4 1 39.35 4.40 4 4 0 100.27 6.16 -4 4 0 104.14 6.97 -4 4 0 94.37 6.98 -4 4 -1 67.26 5.82 -4 4 -1 66.49 5.86 4 4 1 66.87 5.09 -4 4 -1 62.00 3.70 -4 4 -2 34.08 4.27 4 4 2 32.25 3.68 -4 4 -2 23.75 3.60 4 4 3 8.62 2.18 -4 4 -3 10.92 2.66 -4 4 -3 5.24 1.87 4 4 3 8.29 0.84 -4 4 -4 32.34 4.56 4 4 4 25.54 3.48 -4 4 -5 265.92 13.10 4 4 5 248.86 10.89 -4 4 -5 238.83 12.12 -4 4 -6 97.04 7.99 4 4 6 93.15 6.62 -4 4 -6 79.53 7.01 4 4 7 5.09 1.77 -4 4 -7 3.68 2.23 4 4 8 2.83 1.39 -4 4 -8 4.12 2.34 -4 4 -9 7.86 1.79 4 4 9 5.64 1.91 -4 4 -9 12.05 3.44 -4 4 -10 7.90 1.94 4 4 10 6.89 2.13 -4 4 -10 5.32 2.61 4 4 11 25.17 3.74 -4 4 -11 20.53 4.19 4 4 11 22.59 3.78 -4 4 -11 21.98 3.21 4 4 12 16.95 3.39 -4 4 -12 13.72 3.81 4 4 12 12.74 2.78 4 4 13 13.69 3.11 -4 4 -13 13.63 3.69 4 4 13 17.41 3.10 4 4 14 5.94 2.36 -4 4 -14 8.81 3.18 4 4 14 6.02 2.06 4 4 15 10.89 3.04 -4 4 -15 10.53 3.31 4 4 15 12.41 2.79 4 4 16 3.83 1.93 -4 4 -16 0.65 2.08 4 4 16 4.64 1.81 4 4 17 17.68 3.94 -4 4 -17 18.22 4.39 4 4 17 22.17 3.69 4 4 18 -0.04 1.13 -4 4 -18 5.13 2.72 4 4 18 3.84 1.74 4 4 19 5.07 1.91 4 4 19 7.06 2.71 4 4 20 4.65 1.98 4 4 20 5.69 2.59 -4 5 21 0.74 1.21 4 5 -20 8.62 3.47 -4 5 20 7.81 2.73 4 5 -19 8.60 3.29 -4 5 19 5.42 2.14 4 5 -18 4.74 2.61 -4 5 18 2.00 1.52 4 5 -17 8.52 3.16 -4 5 17 5.58 2.13 4 5 -16 12.93 3.63 -4 5 16 11.06 2.82 -4 5 15 11.75 2.34 -4 5 15 14.05 3.14 4 5 -15 12.76 3.61 -4 5 14 37.54 4.85 4 5 -14 48.25 6.56 -4 5 14 43.09 4.27 -4 5 13 1.30 1.15 -4 5 13 -0.58 0.90 4 5 -13 -0.02 1.23 4 5 -12 29.98 5.01 -4 5 12 29.00 3.55 -4 5 12 26.62 3.90 -4 5 11 24.59 3.25 -4 5 11 25.85 3.67 4 5 -11 24.26 4.48 4 5 -11 22.42 2.59 -4 5 10 7.08 1.92 -4 5 10 6.24 1.91 4 5 -10 6.71 2.43 -4 5 10 6.97 1.83 4 5 -10 4.29 1.23 -4 5 9 0.80 0.65 -4 5 9 2.18 1.03 -4 5 9 1.39 0.90 4 5 -9 1.34 0.84 -4 5 9 1.99 1.23 4 5 -9 -0.30 1.70 -4 5 8 29.66 2.96 -4 5 8 25.33 3.30 -4 5 8 28.70 3.57 -4 5 8 24.77 3.29 4 5 -8 25.95 4.37 4 5 -8 27.24 3.01 -4 5 7 53.35 4.14 -4 5 7 54.45 4.82 4 5 -7 49.31 5.91 4 5 -7 45.66 3.93 -4 5 7 52.62 4.80 -4 5 6 18.56 2.58 -4 5 6 21.10 3.00 4 5 -6 18.37 3.57 4 5 -6 20.72 2.70 -4 5 5 1.89 1.14 4 5 -5 1.98 1.56 -4 5 5 3.04 1.31 4 5 -5 4.20 1.37 -4 5 4 32.87 3.86 -4 5 4 35.78 3.74 4 5 -4 30.47 4.60 4 5 -4 40.42 3.79 -4 5 3 17.25 2.65 -4 5 3 18.78 2.97 4 5 -3 19.08 3.79 4 5 -3 19.40 2.76 4 5 -2 89.27 5.79 -4 5 2 79.20 6.11 -4 5 2 83.23 6.09 -4 5 1 19.82 3.11 4 5 -1 20.53 2.80 -4 5 1 20.93 3.23 -4 5 0 1.05 1.39 4 5 0 -1.95 1.67 -4 5 0 -1.32 1.48 4 5 1 59.27 4.94 -4 5 -1 63.79 5.71 -4 5 -1 62.01 5.68 4 5 2 44.64 4.34 -4 5 -2 53.05 5.39 -4 5 -2 41.29 4.75 4 5 3 117.08 7.20 -4 5 -3 109.75 7.83 -4 5 -3 128.98 8.70 -4 5 -4 24.30 3.73 -4 5 -4 34.16 4.71 4 5 4 27.70 3.63 4 5 5 38.41 4.20 -4 5 -5 35.08 4.58 -4 5 -5 42.51 5.21 -4 5 -6 22.61 3.74 4 5 6 25.63 3.53 -4 5 -6 22.76 3.96 -4 5 -7 18.73 3.61 -4 5 -7 13.29 3.33 4 5 7 13.70 2.76 -4 5 -8 35.84 5.02 -4 5 -8 30.07 4.76 4 5 8 33.10 4.03 -4 5 -9 4.08 2.31 4 5 9 2.92 1.33 -4 5 -10 14.70 3.54 4 5 10 13.15 2.57 -4 5 -11 19.66 4.24 4 5 11 13.93 2.89 -4 5 -12 2.32 2.03 4 5 12 2.38 1.39 -4 5 -13 18.67 4.23 4 5 13 13.23 2.71 4 5 14 2.19 1.54 -4 5 -14 0.91 1.79 4 5 14 3.01 1.72 4 5 15 0.06 1.18 -4 5 -15 -0.49 1.47 4 5 15 2.94 1.38 4 5 16 5.00 2.29 -4 5 -16 6.39 2.87 4 5 16 3.79 1.62 4 5 17 4.27 2.16 -4 5 -17 3.43 2.52 4 5 17 3.08 1.79 4 5 18 5.19 1.96 4 5 18 1.75 1.63 4 5 19 3.88 1.88 4 5 19 1.85 1.64 -4 6 20 -0.22 1.24 -4 6 19 2.31 1.70 4 6 -19 7.06 3.05 -4 6 18 -2.68 1.73 4 6 -18 0.29 1.23 -4 6 17 16.47 3.68 4 6 -17 17.78 4.32 -4 6 16 2.81 1.68 4 6 -16 2.94 1.98 4 6 -15 29.65 5.42 -4 6 15 30.39 4.74 -4 6 14 3.55 1.45 -4 6 14 2.11 1.52 4 6 -14 4.12 2.14 -4 6 13 36.42 3.97 4 6 -13 29.50 5.21 -4 6 13 32.49 4.70 -4 6 12 0.55 0.97 4 6 -12 0.19 1.36 -4 6 12 1.48 1.29 -4 6 11 10.81 2.16 4 6 -11 7.95 1.70 4 6 -11 5.79 2.54 -4 6 11 8.92 2.41 -4 6 10 9.66 2.08 4 6 -10 6.68 1.56 -4 6 10 7.35 2.18 4 6 -10 6.76 2.41 -4 6 9 38.76 3.90 4 6 -9 40.88 5.80 4 6 -9 41.78 3.96 -4 6 9 44.71 4.39 4 6 -8 16.65 3.70 -4 6 8 19.00 2.60 -4 6 8 17.46 2.63 -4 6 8 19.04 2.98 4 6 -8 16.33 2.47 -4 6 7 33.07 3.59 -4 6 7 31.41 3.52 4 6 -7 30.54 4.81 4 6 -7 30.06 3.42 -4 6 7 36.91 4.06 4 6 -6 7.09 2.30 -4 6 6 7.17 1.85 -4 6 6 10.75 2.18 -4 6 6 8.38 2.04 4 6 -6 9.68 2.02 -4 6 5 33.24 3.78 -4 6 5 29.42 3.49 -4 6 5 29.98 3.67 4 6 -5 32.86 4.84 4 6 -5 32.81 3.69 -4 6 4 21.13 3.11 4 6 -4 19.08 3.79 -4 6 4 18.08 2.84 4 6 -4 16.62 2.70 -4 6 3 16.39 2.74 4 6 -3 20.14 2.93 -4 6 3 17.85 2.99 -4 6 2 8.08 2.00 4 6 -2 6.47 1.84 -4 6 2 8.58 2.22 -4 6 1 8.96 2.14 4 6 -1 13.96 2.51 -4 6 1 12.03 2.66 -4 6 0 6.87 1.80 4 6 0 9.38 2.18 -4 6 0 6.91 2.13 4 6 1 21.18 3.14 -4 6 -1 22.76 3.72 -4 6 -1 18.85 3.17 -4 6 -2 24.16 3.57 -4 6 -2 18.59 3.47 4 6 2 25.36 3.47 -4 6 -3 43.15 4.88 -4 6 -3 44.39 5.18 4 6 3 42.42 4.54 4 6 4 77.53 6.12 -4 6 -4 68.44 6.27 -4 6 -4 84.90 7.35 -4 6 -5 1.65 1.23 4 6 5 3.66 1.75 -4 6 -5 3.04 1.77 -4 6 -6 18.46 3.41 4 6 6 23.95 3.53 -4 6 -6 20.94 3.83 -4 6 -7 20.52 3.70 4 6 7 19.91 3.17 -4 6 -7 20.12 3.98 -4 6 -8 17.95 3.52 4 6 8 23.15 3.56 -4 6 -8 24.71 4.41 -4 6 -9 15.08 3.40 4 6 9 11.34 2.45 -4 6 -9 13.30 3.39 4 6 10 -0.99 1.50 -4 6 -10 -2.20 1.86 4 6 11 -0.15 1.03 -4 6 -11 0.71 1.89 4 6 12 14.10 2.87 -4 6 -12 13.13 3.60 4 6 13 5.76 2.05 -4 6 -13 6.54 2.76 4 6 14 5.25 2.00 -4 6 -14 1.22 1.46 4 6 15 6.85 2.23 -4 6 -15 4.61 2.51 4 6 16 12.67 2.91 4 6 17 4.45 1.97 -4 7 19 5.42 2.71 4 7 -18 -2.38 1.88 -4 7 18 0.26 1.13 4 7 -17 0.38 1.12 -4 7 17 1.01 1.25 4 7 -16 10.28 3.58 -4 7 16 13.48 3.42 4 7 -15 8.81 3.09 -4 7 15 4.18 1.89 4 7 -14 10.77 3.34 -4 7 14 10.88 2.91 -4 7 13 7.56 2.01 4 7 -13 7.31 2.74 -4 7 13 3.29 1.73 4 7 -12 11.70 3.34 -4 7 12 9.38 2.13 4 7 -11 17.12 3.90 -4 7 11 18.49 2.90 4 7 -11 14.18 2.54 4 7 -10 7.15 2.43 -4 7 10 12.62 2.43 4 7 -10 8.55 1.99 4 7 -9 1.52 1.56 -4 7 9 3.02 1.27 4 7 -9 2.19 1.19 4 7 -8 2.45 1.92 -4 7 8 0.74 0.73 -4 7 8 2.98 1.16 -4 7 8 1.61 1.09 4 7 -8 1.44 1.05 4 7 -7 1.13 1.25 -4 7 7 3.37 1.19 -4 7 7 1.64 1.06 -4 7 7 3.30 1.29 4 7 -7 2.39 1.21 4 7 -6 3.45 1.87 -4 7 6 2.77 1.07 -4 7 6 1.12 0.98 -4 7 6 1.60 1.13 4 7 -6 1.83 0.99 -4 7 5 28.93 3.79 -4 7 5 26.99 3.21 4 7 -5 25.06 4.32 -4 7 5 29.92 3.70 4 7 -5 23.67 3.32 -4 7 4 5.59 1.82 4 7 -4 4.77 1.60 -4 7 4 3.16 1.13 -4 7 4 6.27 1.91 -4 7 3 23.43 3.25 4 7 -3 18.61 3.02 -4 7 3 20.22 2.90 -4 7 3 16.90 3.03 -4 7 2 -0.35 0.95 -4 7 2 0.86 1.22 4 7 -2 0.93 1.06 -4 7 1 47.34 4.54 -4 7 1 37.42 4.68 4 7 -1 45.01 4.80 -4 7 0 17.46 3.33 4 7 0 20.06 3.29 -4 7 0 20.07 3.00 -4 7 -1 9.12 2.44 4 7 1 9.75 2.40 -4 7 -1 8.36 2.02 -4 7 -2 23.28 3.84 4 7 2 19.10 3.26 -4 7 -2 20.10 3.14 -4 7 -3 21.29 3.82 4 7 3 21.94 3.47 -4 7 -3 14.46 2.78 -4 7 -4 2.26 1.66 4 7 4 4.11 1.68 -4 7 -4 3.59 1.60 -4 7 -5 25.63 3.80 -4 7 -5 31.24 4.89 4 7 5 26.98 3.89 -4 7 -6 2.03 1.24 4 7 6 2.48 1.47 -4 7 -6 4.49 1.90 -4 7 -7 6.47 2.02 4 7 7 10.52 2.49 -4 7 -8 10.00 2.59 4 7 8 15.95 3.06 -4 7 -8 16.76 3.75 -4 7 -9 8.37 2.46 4 7 9 7.67 2.32 -4 7 -9 5.05 2.35 4 7 10 4.70 1.84 -4 7 -10 10.12 3.20 4 7 11 4.37 1.81 -4 7 -11 2.90 2.04 4 7 12 -0.85 1.14 -4 7 -12 0.71 1.16 4 7 13 1.02 1.05 -4 7 -13 2.23 1.77 4 7 14 0.39 1.01 4 8 -17 0.87 1.42 -4 8 17 3.07 1.88 4 8 -16 3.56 2.20 -4 8 16 2.44 1.71 4 8 -15 6.03 2.64 4 8 -14 1.02 1.62 4 8 -13 2.27 1.73 -4 8 12 17.64 2.93 4 8 -12 16.95 4.02 -4 8 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23.01 3.60 5 5 -6 15.36 3.77 -5 5 6 21.87 2.96 5 5 -6 25.91 3.21 5 5 -5 23.76 4.44 -5 5 5 32.54 3.71 5 5 -5 24.34 3.19 -5 5 5 28.82 4.01 -5 5 4 1.55 1.22 5 5 -4 3.52 2.12 -5 5 4 4.59 1.61 5 5 -4 7.74 1.92 -5 5 3 4.04 1.61 5 5 -3 2.92 1.09 -5 5 2 14.33 2.75 5 5 -2 10.09 2.15 -5 5 2 11.99 2.85 -5 5 1 45.25 4.97 5 5 -1 37.20 4.19 -5 5 1 43.71 5.28 -5 5 0 38.86 4.77 5 5 0 38.19 4.30 -5 5 0 35.83 4.80 -5 5 -1 53.73 5.78 5 5 1 62.22 5.53 -5 5 -1 54.00 5.99 -5 5 -2 46.95 5.53 -5 5 -2 41.86 5.34 5 5 2 49.61 4.99 -5 5 -3 13.23 3.26 5 5 3 14.24 2.89 -5 5 -3 11.02 2.89 -5 5 -4 4.36 2.24 5 5 4 1.90 1.36 -5 5 -4 1.46 1.12 -5 5 -5 6.07 2.42 5 5 5 3.49 1.37 -5 5 -5 7.55 2.54 -5 5 -6 14.78 3.52 5 5 6 17.77 3.21 -5 5 -6 20.84 4.01 -5 5 -7 19.29 4.09 5 5 7 12.96 2.87 -5 5 -7 18.26 3.94 -5 5 -8 15.26 3.70 5 5 8 14.09 2.98 -5 5 -8 14.72 3.58 -5 5 -9 14.38 3.67 5 5 9 12.88 2.93 -5 5 -9 15.94 3.76 -5 5 -10 29.62 5.22 5 5 10 26.97 4.12 -5 5 -10 25.75 4.78 -5 5 -11 23.79 4.74 5 5 11 30.70 4.43 -5 5 -11 30.11 5.34 -5 5 -12 6.14 2.93 5 5 12 7.82 2.30 -5 5 -13 4.70 2.39 5 5 13 1.62 1.30 -5 5 -14 2.37 1.85 5 5 14 2.20 1.36 5 5 15 1.05 1.14 5 6 -17 2.76 2.43 -5 6 16 0.66 0.92 5 6 -16 -1.45 1.74 -5 6 15 5.61 1.93 5 6 -15 4.63 2.46 -5 6 14 7.91 2.12 5 6 -14 0.00 2.26 -5 6 13 11.63 2.51 5 6 -13 4.75 2.26 -5 6 12 6.28 1.97 5 6 -12 6.12 2.49 -5 6 11 20.92 3.28 -5 6 11 24.20 3.57 5 6 -11 16.73 3.98 -5 6 10 1.54 1.17 -5 6 10 -0.55 1.29 5 6 -10 -0.28 0.92 5 6 -10 1.34 1.65 -5 6 9 23.37 3.48 5 6 -9 19.27 2.79 -5 6 9 24.85 3.64 5 6 -9 18.04 4.09 -5 6 8 16.80 3.02 -5 6 8 15.89 3.02 5 6 -8 17.35 2.75 5 6 -8 19.80 4.42 -5 6 7 25.53 3.71 5 6 -7 32.70 3.77 -5 6 7 32.97 4.23 5 6 -7 28.80 5.02 5 6 -6 73.79 8.00 5 6 -6 74.38 5.79 -5 6 6 74.26 5.78 -5 6 6 72.20 6.24 -5 6 5 14.13 2.81 5 6 -5 15.58 3.73 5 6 -5 15.41 2.70 -5 6 5 18.69 2.96 -5 6 4 3.89 1.53 5 6 -4 5.68 1.66 -5 6 4 5.36 1.83 -5 6 3 0.53 1.05 -5 6 3 1.10 1.29 5 6 -3 2.07 1.28 -5 6 2 35.13 4.40 5 6 -2 35.23 4.16 -5 6 2 31.56 4.35 -5 6 1 2.89 1.59 5 6 -1 2.36 1.51 -5 6 1 3.02 1.57 -5 6 0 3.43 1.65 -5 6 0 4.56 1.86 5 6 0 4.29 1.72 -5 6 -1 27.25 4.25 -5 6 -1 29.75 4.40 5 6 1 35.83 4.35 -5 6 -2 6.58 2.36 5 6 2 7.13 2.24 -5 6 -2 1.63 1.14 -5 6 -3 8.83 2.80 5 6 3 7.80 2.04 -5 6 -3 8.78 2.52 -5 6 -4 5.60 2.39 5 6 4 2.41 1.18 -5 6 -4 4.77 1.95 -5 6 -5 4.83 2.37 5 6 5 3.40 1.61 -5 6 -5 4.00 2.05 -5 6 -6 3.20 2.14 5 6 6 1.95 1.30 -5 6 -6 7.06 2.28 -5 6 -7 0.70 1.14 5 6 7 3.56 1.78 -5 6 -7 0.81 1.10 -5 6 -8 6.61 2.72 5 6 8 4.53 1.77 -5 6 -8 1.52 1.22 -5 6 -9 2.46 1.82 5 6 9 0.06 0.82 -5 6 -9 3.07 2.04 5 6 10 0.40 1.01 -5 6 -10 1.68 1.46 -5 6 -11 22.19 4.78 5 6 11 15.39 3.28 -5 6 -11 11.89 3.38 -5 6 -12 14.91 4.17 -5 6 -12 8.49 3.07 5 6 12 5.56 2.31 -5 6 -13 10.62 3.35 5 6 13 4.49 1.83 5 7 -16 3.72 2.47 5 7 -15 -0.16 1.66 5 7 -14 5.01 2.62 -5 7 13 2.65 1.49 5 7 -13 2.89 2.20 -5 7 12 4.53 1.76 5 7 -12 5.77 2.63 -5 7 11 4.46 1.78 5 7 -11 0.55 1.17 5 7 -10 10.48 3.34 -5 7 10 10.82 2.43 -5 7 10 10.28 2.30 5 7 -9 2.41 1.86 -5 7 9 7.88 2.12 5 7 -9 8.05 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3.01 1.74 7 -2 -9 1.82 1.45 7 -2 -9 1.86 1.36 -7 -2 9 0.07 1.38 7 -2 -9 1.63 1.53 7 -2 -8 -0.52 1.15 7 -2 -8 -0.02 1.00 -7 -2 8 -1.58 1.62 7 -2 -8 -0.62 1.21 7 -2 -7 6.74 2.44 7 -2 -7 6.83 2.23 -7 -2 7 6.77 2.50 7 -2 -7 5.48 2.08 7 -2 -6 11.87 3.14 -7 -2 6 10.29 3.10 7 -2 -6 12.54 3.03 7 -2 -5 1.40 1.95 -7 -2 5 -1.20 1.69 7 -2 -5 -2.30 2.03 7 -2 -4 11.90 3.16 -7 -2 4 6.70 2.57 7 -2 -3 1.36 1.57 -7 -2 3 -1.02 2.00 7 -2 -2 18.76 4.02 -7 -2 2 14.33 3.72 7 -2 -1 20.61 4.23 -7 -2 1 19.17 4.21 7 -2 0 4.76 2.63 -7 -2 0 -1.33 2.20 7 -2 1 5.48 2.48 -7 -2 -1 3.17 2.03 7 -2 2 9.46 3.41 -7 -2 -2 6.94 2.81 7 -2 3 2.20 2.50 -7 -2 -3 1.50 1.40 7 -2 4 3.54 2.27 -7 -2 -4 -0.66 1.94 7 -2 5 8.55 3.30 -7 -2 -5 2.13 1.74 7 -2 6 6.81 3.17 -7 -2 -6 5.34 2.52 7 -2 7 4.33 2.59 -7 -2 -7 0.30 1.31 7 -2 8 4.23 2.51 -7 -2 -8 0.17 1.10 7 -2 9 2.51 2.53 -7 -2 -9 1.23 1.97 -7 -2 -10 1.05 1.63 7 -1 -17 0.77 1.52 7 -1 -16 0.13 1.36 -7 -1 16 1.61 1.14 -7 -1 15 6.12 2.32 -7 -1 15 3.51 1.53 7 -1 -15 3.61 2.30 7 -1 -14 2.93 1.64 -7 -1 14 3.64 1.93 -7 -1 14 -0.04 1.12 7 -1 -14 3.61 2.41 7 -1 -13 24.84 5.23 7 -1 -13 17.59 3.34 -7 -1 13 22.73 4.12 7 -1 -12 16.26 4.19 7 -1 -12 17.64 3.40 -7 -1 12 13.80 3.41 7 -1 -11 -1.10 1.78 7 -1 -11 1.26 1.34 -7 -1 11 -1.11 1.50 7 -1 -10 1.25 1.32 7 -1 -10 2.60 1.41 7 -1 -10 3.35 1.53 -7 -1 10 2.96 1.67 7 -1 -9 0.36 1.57 7 -1 -9 -0.89 1.31 -7 -1 9 1.15 1.37 7 -1 -9 -0.95 1.33 7 -1 -8 1.11 1.60 7 -1 -8 0.18 1.14 -7 -1 8 1.38 1.30 7 -1 -8 3.19 1.58 7 -1 -7 3.26 1.68 7 -1 -7 2.87 1.45 -7 -1 7 4.59 2.32 7 -1 -7 2.61 1.43 7 -1 -6 3.82 1.95 7 -1 -6 -1.12 1.41 -7 -1 6 -0.35 1.45 7 -1 -6 -1.70 1.53 7 -1 -5 14.45 3.26 -7 -1 5 8.49 2.84 7 -1 -5 9.51 2.55 7 -1 -4 5.43 2.30 -7 -1 4 6.83 2.56 7 -1 -4 4.17 1.75 7 -1 -3 1.30 1.62 -7 -1 3 0.05 1.56 7 -1 -3 -1.98 1.51 7 -1 -2 -0.86 1.74 -7 -1 2 -0.17 1.44 7 -1 -1 1.91 2.04 -7 -1 1 1.12 1.39 7 -1 0 -1.20 1.79 -7 -1 0 -1.91 2.29 7 -1 1 7.31 2.81 -7 -1 -1 7.23 2.74 7 -1 2 1.03 2.02 -7 -1 -2 1.35 1.60 7 -1 3 3.28 2.57 -7 -1 -3 4.09 2.35 7 -1 4 7.22 2.80 -7 -1 -4 1.71 1.65 7 -1 5 3.13 2.34 -7 -1 -5 2.76 2.19 7 -1 6 4.08 2.35 -7 -1 -6 3.04 2.05 7 -1 7 2.60 2.56 -7 -1 -7 -0.23 1.33 7 -1 8 13.14 3.88 -7 -1 -8 2.15 1.90 7 -1 9 1.30 1.75 -7 -1 -9 0.01 1.40 7 -1 10 6.66 3.19 -7 -1 -10 0.16 1.49 -7 0 19 7.60 2.19 -7 0 18 1.30 1.30 -7 0 17 -0.18 0.83 7 0 -16 2.11 2.20 -7 0 16 3.18 1.56 -7 0 15 6.32 2.26 7 0 -15 9.25 3.41 -7 0 15 5.20 1.88 -7 0 14 3.84 2.17 -7 0 14 3.40 1.64 7 0 -14 5.70 3.02 7 0 -13 2.07 2.15 7 0 -13 2.14 1.64 -7 0 13 -0.67 1.56 7 0 -12 1.39 1.51 7 0 -12 3.49 1.87 -7 0 12 -1.46 1.32 7 0 -11 5.30 2.55 7 0 -11 2.11 1.22 -7 0 11 2.97 1.88 7 0 -10 15.58 3.99 7 0 -10 19.82 3.40 -7 0 10 20.66 4.05 7 0 -9 29.03 5.33 -7 0 9 21.72 4.23 7 0 -9 27.11 3.95 7 0 -8 1.79 1.47 7 0 -8 -0.32 1.33 -7 0 8 0.38 1.52 7 0 -8 2.27 1.44 7 0 -7 6.72 2.67 7 0 -7 4.98 1.78 -7 0 7 8.00 2.65 7 0 -7 8.13 2.37 7 0 -6 -0.78 1.75 7 0 -6 0.54 1.24 -7 0 6 0.06 1.29 7 0 -6 1.33 0.97 7 0 -5 0.97 1.55 -7 0 5 1.04 1.57 7 0 -5 0.26 0.98 7 0 -4 10.51 2.72 -7 0 4 15.82 3.78 7 0 -4 12.56 2.81 7 0 -3 1.15 1.71 -7 0 3 -2.38 2.43 7 0 -3 1.38 1.13 7 0 -2 4.60 2.11 -7 0 2 4.84 2.16 7 0 -2 1.96 1.42 7 0 -1 25.48 4.25 -7 0 1 19.76 4.30 7 0 0 -0.94 2.04 -7 0 0 -6.01 2.65 7 0 1 7.83 2.75 -7 0 -1 7.80 2.96 7 0 2 1.76 1.58 -7 0 -2 1.28 1.46 7 0 3 2.28 2.20 -7 0 -3 3.66 2.08 7 0 4 4.51 2.60 -7 0 -4 6.11 2.61 7 0 5 -0.10 1.31 -7 0 -5 -1.15 1.17 7 0 6 1.87 1.66 -7 0 -6 0.93 1.55 7 0 7 4.95 2.23 -7 0 -7 5.79 2.62 7 0 8 1.62 1.63 -7 0 -8 2.56 2.21 7 0 9 -0.16 1.39 -7 0 -9 -1.33 1.80 7 0 10 1.76 1.81 -7 0 -10 -0.38 1.83 -7 1 17 0.22 0.84 -7 1 16 0.28 0.78 7 1 -15 6.66 3.07 -7 1 15 3.28 1.65 -7 1 14 1.85 1.71 7 1 -14 4.33 2.69 -7 1 14 0.27 1.02 7 1 -13 21.76 5.02 -7 1 13 22.20 4.11 7 1 -12 22.82 5.09 -7 1 12 16.88 3.61 7 1 -11 -1.80 1.92 7 1 -11 0.99 1.13 -7 1 11 1.53 1.62 7 1 -10 3.93 2.39 7 1 -10 1.07 1.25 -7 1 10 1.58 1.71 7 1 -9 0.19 1.58 -7 1 9 -1.46 1.76 7 1 -9 1.32 1.19 7 1 -8 1.06 1.28 -7 1 8 1.09 1.16 7 1 -8 4.15 1.64 7 1 -7 5.49 2.78 -7 1 7 4.66 2.17 7 1 -7 6.18 1.86 7 1 -6 -0.11 1.53 -7 1 6 1.04 1.27 7 1 -6 0.92 1.08 -7 1 5 10.27 3.15 7 1 -5 8.64 2.17 7 1 -4 2.57 1.57 -7 1 4 5.61 2.52 7 1 -4 4.61 1.72 -7 1 3 0.63 0.99 7 1 -3 0.52 0.69 7 1 -2 -0.91 2.06 -7 1 2 0.02 1.52 7 1 -2 -0.22 1.11 7 1 -1 3.16 1.65 -7 1 1 6.53 2.74 7 1 -1 3.67 1.51 7 1 0 -1.32 1.89 -7 1 0 1.00 1.64 7 1 0 -0.88 1.14 7 1 1 2.73 1.84 -7 1 -1 6.01 2.78 7 1 2 -0.53 1.59 -7 1 -2 1.14 1.79 7 1 3 2.94 2.28 -7 1 -3 6.55 2.74 7 1 4 1.28 1.37 -7 1 -4 1.70 1.29 7 1 5 2.06 1.70 -7 1 -5 -1.23 1.68 7 1 6 1.73 1.82 -7 1 -6 4.39 2.31 7 1 7 -1.73 2.29 -7 1 -7 -0.70 1.29 7 1 8 2.51 1.97 -7 1 -8 4.75 2.41 7 1 9 1.31 1.74 -7 1 -9 5.99 2.86 7 1 10 0.37 1.83 -7 1 -10 0.89 1.47 -7 2 16 -0.55 0.82 -7 2 15 -1.19 1.38 -7 2 14 1.76 1.38 7 2 -14 -0.30 1.29 -7 2 14 0.30 1.01 -7 2 13 4.38 1.84 7 2 -13 2.88 2.06 -7 2 13 1.97 1.44 -7 2 12 22.31 4.13 7 2 -12 22.54 5.17 -7 2 11 2.11 1.49 7 2 -11 3.24 2.28 -7 2 10 2.95 1.63 7 2 -10 7.24 2.93 7 2 -9 0.02 1.41 -7 2 9 1.66 1.81 7 2 -8 0.97 1.11 7 2 -8 -1.47 1.92 -7 2 8 0.66 1.11 7 2 -8 2.64 1.27 7 2 -7 5.25 1.84 7 2 -7 4.44 2.17 -7 2 7 2.53 1.47 7 2 -7 6.13 1.79 7 2 -6 12.65 2.65 7 2 -6 10.55 3.23 -7 2 6 13.07 3.43 7 2 -6 13.56 2.53 -7 2 5 0.31 1.38 7 2 -5 0.93 0.87 7 2 -5 1.94 1.50 -7 2 4 9.46 3.04 7 2 -4 7.90 1.95 7 2 -4 11.96 2.85 -7 2 3 -1.08 1.45 7 2 -3 0.78 0.76 7 2 -3 2.78 1.74 -7 2 2 19.61 4.21 7 2 -2 15.47 2.71 -7 2 1 16.35 3.91 7 2 -1 15.82 2.69 -7 2 0 1.85 1.39 7 2 0 4.86 1.58 7 2 1 4.93 2.11 -7 2 -1 4.32 2.36 7 2 2 5.57 2.03 -7 2 -2 5.61 2.24 7 2 3 -1.00 1.75 -7 2 -3 2.71 1.84 7 2 4 1.83 1.52 -7 2 -4 2.23 1.95 7 2 5 4.77 2.43 -7 2 -5 4.17 2.59 7 2 6 4.35 2.00 -7 2 -6 2.40 1.83 7 2 7 2.38 1.88 -7 2 -7 2.06 1.83 7 2 8 -0.67 1.66 -7 2 -8 0.74 1.18 7 2 9 -0.51 1.51 -7 2 -9 -2.72 2.13 7 2 10 0.22 1.18 -7 3 14 10.84 2.78 -7 3 13 10.14 2.87 7 3 -13 13.75 4.14 -7 3 13 10.21 2.69 -7 3 12 1.42 1.17 7 3 -12 0.20 1.96 -7 3 12 -0.90 1.62 -7 3 11 0.44 0.98 7 3 -11 4.44 2.69 -7 3 10 6.32 2.38 7 3 -10 5.02 2.70 7 3 -9 -1.65 1.79 -7 3 9 -0.42 1.37 7 3 -8 6.73 2.98 -7 3 8 4.91 2.19 -7 3 7 0.44 1.33 7 3 -7 1.41 1.65 7 3 -7 1.41 0.97 -7 3 6 2.62 2.02 7 3 -6 2.37 1.78 7 3 -6 3.29 1.36 7 3 -5 0.03 1.04 -7 3 5 0.61 1.13 7 3 -4 3.22 1.60 -7 3 4 4.89 2.11 7 3 -3 1.43 1.43 -7 3 3 0.54 1.16 7 3 -2 20.69 3.67 -7 3 2 20.79 4.30 -7 3 2 22.13 3.82 7 3 -1 1.44 1.39 -7 3 1 -0.64 1.17 -7 3 1 0.89 1.30 7 3 0 3.71 2.00 -7 3 0 1.52 1.59 -7 3 0 3.78 1.93 7 3 1 1.06 0.98 -7 3 -1 3.83 2.02 -7 3 -1 1.36 1.73 7 3 2 2.02 1.76 -7 3 -2 2.82 2.05 7 3 3 1.27 1.51 -7 3 -3 -1.64 1.91 7 3 4 5.26 2.21 -7 3 -4 3.16 1.95 7 3 5 9.01 2.79 -7 3 -5 11.57 3.52 7 3 6 9.40 2.99 -7 3 -6 10.01 3.32 7 3 7 3.28 2.01 -7 3 -7 -0.61 1.52 7 3 8 3.13 2.31 -7 3 -8 -0.61 1.69 -7 3 -9 4.40 2.38 -7 4 13 2.72 1.68 -7 4 12 3.80 1.98 -7 4 11 -0.94 1.26 7 4 -11 2.64 1.93 -7 4 11 0.32 1.23 -7 4 10 2.72 1.66 7 4 -10 -1.12 1.53 -7 4 9 3.26 1.76 7 4 -9 6.76 2.88 7 4 -8 0.19 1.31 -7 4 8 -3.86 2.04 -7 4 7 -1.05 1.22 7 4 -7 0.82 1.28 7 4 -7 -1.00 0.96 7 4 -6 -0.30 0.92 -7 4 6 0.24 1.14 7 4 -5 -0.76 1.24 -7 4 5 2.96 2.09 7 4 -4 4.81 1.73 -7 4 4 1.70 1.42 7 4 -3 7.39 2.05 -7 4 3 6.05 2.28 7 4 -2 1.06 1.16 -7 4 2 0.71 1.40 -7 4 2 0.16 1.03 7 4 -1 3.93 1.66 -7 4 1 3.69 1.80 -7 4 1 3.18 1.85 7 4 0 7.87 2.33 -7 4 0 5.85 2.43 -7 4 0 4.32 2.07 7 4 1 6.45 2.30 -7 4 -1 8.67 2.95 -7 4 -1 8.29 2.73 7 4 2 3.96 1.86 -7 4 -2 5.09 2.66 -7 4 -2 6.03 2.60 7 4 3 3.98 2.05 -7 4 -3 -0.57 1.50 -7 4 -3 2.19 1.68 7 4 4 5.46 2.30 -7 4 -4 3.98 2.25 -7 4 -4 3.78 2.14 7 4 5 3.19 1.72 -7 4 -5 3.29 2.03 -7 4 -5 2.69 2.17 7 4 6 0.95 1.24 -7 4 -6 1.38 1.53 -7 4 -6 3.09 1.92 -7 4 -7 3.55 2.29 -7 4 -7 2.88 2.19 -7 4 -8 -1.48 1.75 -7 4 -8 1.57 2.04 -7 5 11 2.07 1.56 -7 5 10 1.77 1.45 -7 5 9 -0.12 1.13 7 5 -9 -0.41 1.46 7 5 -8 4.55 2.57 -7 5 8 0.51 1.04 7 5 -7 -0.70 0.99 -7 5 7 0.29 1.00 7 5 -6 0.97 1.19 -7 5 6 2.30 1.85 7 5 -5 3.51 1.48 -7 5 5 1.86 1.52 7 5 -4 -0.81 1.08 -7 5 4 -0.72 1.37 7 5 -3 -0.48 1.32 -7 5 3 -1.34 1.70 7 5 -2 4.57 1.82 -7 5 2 4.58 1.98 7 5 -1 0.66 1.06 -7 5 1 -0.63 1.53 -7 5 1 0.59 1.04 7 5 0 2.38 1.44 -7 5 0 2.51 2.03 -7 5 0 2.56 1.66 7 5 1 0.39 1.14 -7 5 -1 0.53 1.29 -7 5 -1 4.21 1.99 7 5 2 2.33 1.47 -7 5 -2 0.19 1.10 -7 5 -2 1.21 1.47 7 5 3 4.70 2.11 -7 5 -3 5.23 2.26 -7 5 -3 3.87 2.12 7 5 4 8.34 2.64 -7 5 -4 10.28 3.49 -7 5 -4 4.93 2.53 -7 5 -5 0.13 1.21 -7 5 -5 -1.03 1.61 -7 5 -6 0.28 1.39 -7 5 -6 5.05 2.80 -7 5 -7 0.42 1.49 -7 5 -7 -1.68 1.71 -7 6 10 -0.79 1.10 -7 6 9 2.93 1.70 -7 6 8 -0.08 1.06 -7 6 7 4.18 2.01 7 6 -6 2.14 1.21 -7 6 6 0.01 1.08 7 6 -5 0.16 0.91 -7 6 5 -0.25 1.05 7 6 -4 -0.34 0.77 -7 6 4 0.72 1.07 7 6 -3 -0.10 0.92 -7 6 3 0.07 1.06 7 6 -2 0.67 1.12 -7 6 2 -1.57 1.49 7 6 -1 2.63 1.55 -7 6 1 -1.16 1.41 7 6 0 0.56 0.99 -7 6 0 2.40 1.65 -7 6 0 0.34 0.94 7 6 1 -1.96 1.50 -7 6 -1 0.39 1.27 -7 6 -1 1.02 1.37 -7 6 -2 6.02 2.49 -7 6 -2 5.68 2.42 -7 6 -3 -0.84 1.33 -7 6 -3 0.61 1.44 -7 6 -4 1.83 1.68 -7 6 -4 3.06 2.13 -7 6 -5 -1.06 1.49 -7 6 -5 3.37 2.30 -7 6 -6 1.32 1.89 -7 7 9 -2.41 1.51 -7 7 8 1.09 1.23 -7 7 7 -0.18 0.79 7 7 -6 1.58 1.41 -7 7 6 0.27 0.91 7 7 -5 3.41 1.62 -7 7 5 1.69 1.38 7 7 -4 1.16 1.42 -7 7 4 -0.34 1.08 7 7 -3 -0.57 0.99 -7 7 3 0.76 1.14 -7 7 2 -1.60 1.38 -7 7 1 0.18 0.85 -7 7 -1 2.40 1.82 -7 7 -2 1.49 1.76 8 -5 -6 6.15 2.70 8 -5 -5 0.77 1.51 -8 -5 5 1.16 1.26 -8 -5 4 2.48 1.88 -8 -5 3 1.63 1.50 -8 -5 2 0.41 1.36 -8 -5 1 1.33 1.54 -8 -4 7 2.57 1.68 8 -4 -6 -1.27 1.67 -8 -4 6 0.05 1.14 8 -4 -5 2.46 2.16 -8 -4 5 6.13 2.61 8 -4 -4 1.21 2.11 -8 -4 4 1.39 1.42 8 -4 -3 2.05 2.16 -8 -4 3 -3.28 2.12 8 -4 -2 1.54 2.20 -8 -4 2 0.61 1.35 -8 -4 1 -0.88 1.43 -8 -4 0 -0.06 1.40 -8 -4 -1 2.91 2.04 8 -3 -7 -2.16 1.95 -8 -3 7 0.05 1.16 8 -3 -6 3.12 2.02 -8 -3 6 0.71 1.26 8 -3 -5 3.06 2.07 -8 -3 5 2.86 1.84 8 -3 -4 3.77 2.48 -8 -3 4 2.29 2.15 8 -3 -4 3.24 2.06 8 -3 -3 6.65 3.00 -8 -3 3 2.44 1.72 8 -3 -2 1.17 2.02 -8 -3 2 -0.23 1.49 8 -3 -1 -0.62 1.55 -8 -3 1 1.62 1.72 8 -3 0 3.15 2.49 -8 -3 0 4.83 2.43 -8 -3 -1 -0.53 2.01 8 -2 -13 7.45 3.19 8 -2 -12 -3.53 2.23 8 -2 -11 0.32 1.21 8 -2 -10 6.12 2.81 8 -2 -9 5.38 2.44 8 -2 -8 0.05 1.00 -8 -2 8 -1.69 1.79 8 -2 -8 0.00 1.08 8 -2 -7 4.04 2.07 -8 -2 7 3.32 1.98 8 -2 -7 3.67 2.14 8 -2 -6 14.75 3.55 -8 -2 6 8.75 3.02 8 -2 -6 11.38 3.34 8 -2 -5 0.52 1.65 -8 -2 5 2.37 1.68 8 -2 -5 1.01 1.19 8 -2 -4 0.83 1.70 -8 -2 4 1.68 1.38 8 -2 -4 4.16 2.14 8 -2 -3 0.21 1.22 -8 -2 3 2.77 1.92 8 -2 -3 0.05 1.22 8 -2 -2 12.40 3.59 -8 -2 2 9.25 3.38 8 -2 -1 5.09 2.86 -8 -2 1 1.59 1.32 8 -2 0 6.50 2.94 -8 -2 0 4.82 2.43 8 -2 1 1.65 1.83 -8 -2 -1 -1.62 2.16 -8 -2 -2 -2.38 2.24 8 -1 -12 16.72 4.67 8 -1 -11 8.99 3.69 8 -1 -10 1.17 1.91 8 -1 -10 1.84 1.57 8 -1 -9 2.13 1.90 8 -1 -9 0.01 0.91 8 -1 -9 3.39 1.72 8 -1 -8 2.65 1.62 -8 -1 8 3.84 2.16 8 -1 -8 1.63 1.17 8 -1 -7 -1.54 1.59 -8 -1 7 -0.31 1.20 8 -1 -7 0.84 1.48 8 -1 -6 1.45 1.58 -8 -1 6 0.97 1.52 8 -1 -6 3.08 2.00 8 -1 -5 5.98 2.44 -8 -1 5 8.69 2.97 8 -1 -5 8.72 2.76 8 -1 -4 3.55 1.98 -8 -1 4 4.90 2.55 8 -1 -4 2.22 1.66 8 -1 -3 4.87 2.35 -8 -1 3 3.36 2.19 8 -1 -3 4.42 2.24 8 -1 -2 0.34 1.90 -8 -1 2 -1.61 2.09 8 -1 -2 -0.22 1.21 8 -1 -1 1.39 1.65 -8 -1 1 2.28 2.04 8 -1 0 12.43 3.60 -8 -1 0 11.21 3.69 8 -1 1 6.57 3.08 -8 -1 -1 9.02 3.24 8 -1 2 2.98 2.19 -8 -1 -2 -1.28 1.56 8 0 -11 0.45 1.05 8 0 -11 6.80 2.36 8 0 -10 0.00 1.61 8 0 -10 1.77 1.45 8 0 -9 5.75 2.65 8 0 -9 3.77 1.90 8 0 -8 14.37 4.02 8 0 -8 9.08 2.62 -8 0 7 1.95 1.77 8 0 -7 0.27 0.84 8 0 -6 -0.29 1.59 -8 0 6 3.98 2.19 8 0 -6 3.51 1.60 8 0 -5 7.33 2.59 -8 0 5 5.23 2.36 8 0 -5 6.68 2.24 8 0 -4 0.00 1.19 -8 0 4 0.85 1.56 8 0 -4 0.31 1.25 8 0 -3 15.75 3.59 -8 0 3 19.29 4.51 8 0 -3 15.06 3.38 8 0 -2 9.44 2.92 -8 0 2 13.81 3.75 8 0 -2 15.53 3.41 8 0 -1 0.70 1.48 -8 0 1 0.31 1.76 8 0 -1 0.71 1.18 8 0 0 1.14 1.57 -8 0 0 1.69 1.91 8 0 0 0.04 1.08 8 0 1 2.09 2.30 -8 0 -1 1.39 1.58 8 0 2 2.18 1.86 -8 0 -2 -2.89 2.55 8 1 -11 11.63 2.81 8 1 -10 2.50 1.49 8 1 -9 -1.78 1.82 8 1 -9 1.63 1.24 8 1 -8 1.05 1.71 8 1 -8 3.94 1.85 -8 1 7 -0.71 1.35 8 1 -7 2.11 1.49 -8 1 6 -0.10 1.34 8 1 -6 2.86 1.47 -8 1 5 10.41 3.26 8 1 -5 10.08 2.59 -8 1 4 8.00 3.04 8 1 -4 3.33 1.62 -8 1 3 3.74 2.43 8 1 -3 7.18 2.24 8 1 -2 -3.25 1.92 -8 1 2 -2.18 1.86 8 1 -2 1.71 1.55 8 1 -1 1.69 1.56 -8 1 1 0.14 1.86 8 1 0 6.97 2.57 -8 1 0 5.37 2.59 8 1 1 10.57 3.31 -8 1 -1 9.77 3.47 8 1 2 1.38 1.42 8 2 -8 0.56 0.90 8 2 -7 2.44 1.51 8 2 -6 10.66 2.71 8 2 -5 2.44 1.70 -8 2 5 0.02 1.00 8 2 -4 4.10 1.89 -8 2 4 1.99 2.09 8 2 -3 4.76 2.19 -8 2 3 2.23 1.96 8 2 -2 14.97 3.45 -8 2 2 4.89 2.38 8 2 -1 8.59 2.99 -8 2 1 -0.70 2.01 8 2 0 12.52 3.33 -8 2 0 2.07 1.96 8 3 -5 3.07 1.72 8 3 -4 2.44 1.63 8 3 -3 1.97 1.69 8 3 -2 1.97 1.69 8 3 -1 0.68 1.32 8 3 0 4.11 2.30 -8 3 -1 8.17 2.92 8 3 1 6.54 2.47 -8 3 -2 16.93 4.39 -8 3 -3 3.93 2.46 -8 3 -4 1.52 2.10 -8 3 -5 3.10 2.35 8 4 -5 4.87 1.87 8 4 -4 0.73 1.24 8 4 -3 0.48 1.06 8 4 -2 1.34 1.47 8 4 -1 2.67 1.73 -8 4 -2 12.55 3.77 -8 4 -3 7.34 2.99 -8 4 -4 2.60 2.22 8 5 -4 0.54 1.12 0 0 0 0.00 0.00 TITL 20221027-Zhang Min-ZYK-Py-Cy-Me_auto in P2(1) REM P2(1) (#4 in standard setting) CELL 0.71073 6.519919 8.973876 19.783360 90.0000 96.5201 90.0000 ZERR 2.00 0.000350 0.000529 0.001007 0.0000 0.0047 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 50.00 70.00 6.00 4.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 37046 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.444 _oxdiff_exptl_absorpt_empirical_full_min 0.503 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.7534(3) 0.3838(3) 0.56249(11) 0.0485(6) Uani 1 1 d . . . . . O002 O 0.8461(4) 0.5888(3) 0.79161(12) 0.0537(7) Uani 1 1 d . . . . . N003 N 0.5955(4) 0.4742(3) 0.68167(13) 0.0390(6) Uani 1 1 d . . . . . N004 N 0.4303(4) 0.3716(4) 0.50788(14) 0.0468(7) Uani 1 1 d . . . . . N005 N 0.5716(4) 0.6235(4) 0.84921(14) 0.0534(8) Uani 1 1 d . . . . . C006 C 0.6430(5) 0.5731(4) 0.79704(16) 0.0416(8) Uani 1 1 d . . . . . C007 C 0.5463(5) 0.3927(4) 0.56282(16) 0.0384(7) Uani 1 1 d . . . . . C008 C 0.7859(5) 0.3515(4) 0.49155(16) 0.0425(8) Uani 1 1 d . . . . . H008 H 0.859816 0.434550 0.473131 0.051 Uiso 1 1 calc R U . . . C009 C 0.4648(5) 0.4289(3) 0.62818(15) 0.0381(7) Uani 1 1 d . . . . . C00A C 0.5100(5) 0.5077(4) 0.73859(16) 0.0389(7) Uani 1 1 d . . . . . C00B C 0.2526(5) 0.4165(4) 0.62989(17) 0.0441(8) Uani 1 1 d . . . . . H00B H 0.167948 0.387551 0.591107 0.053 Uiso 1 1 calc R U . . . C00C C 0.5645(5) 0.3425(4) 0.45438(16) 0.0425(8) Uani 1 1 d . . . . . H00C H 0.539680 0.240456 0.437742 0.051 Uiso 1 1 calc R U . . . C00D C 0.1687(5) 0.4470(4) 0.68889(17) 0.0481(8) Uani 1 1 d . . . . . H00D H 0.027629 0.437413 0.691204 0.058 Uiso 1 1 calc R U . . . C00E C 0.3008(5) 0.4926(4) 0.74494(17) 0.0452(8) Uani 1 1 d . . . . . H00E H 0.250293 0.512730 0.786106 0.054 Uiso 1 1 calc R U . . . C00F C 0.5187(5) 0.4496(4) 0.39476(16) 0.0425(7) Uani 1 1 d . . . . . H00F H 0.543000 0.551018 0.412187 0.051 Uiso 1 1 calc R U . . . C00G C 0.9362(5) 0.6587(4) 0.85481(17) 0.0459(8) Uani 1 1 d . . . . . H00G H 1.021643 0.585710 0.881995 0.055 Uiso 1 1 calc R U . . . C00H C 0.7446(5) 0.6970(4) 0.89118(16) 0.0451(8) Uani 1 1 d . . . . . H00H H 0.722705 0.804877 0.887715 0.054 Uiso 1 1 calc R U . . . C00I C 0.9103(6) 0.2112(5) 0.4890(2) 0.0615(11) Uani 1 1 d . . . . . H00A H 1.039709 0.222719 0.516904 0.092 Uiso 1 1 calc R U . . . H00I H 0.935233 0.191977 0.442891 0.092 Uiso 1 1 calc R U . . . H00J H 0.835527 0.129301 0.505531 0.092 Uiso 1 1 calc R U . . . C00J C 0.7581(5) 0.6546(4) 0.96644(17) 0.0478(8) Uani 1 1 d . . . . . H00K H 0.793141 0.548594 0.970790 0.057 Uiso 1 1 calc R U . . . C00K C 0.6611(6) 0.4239(5) 0.33952(19) 0.0523(9) Uani 1 1 d . . . . . H00L H 0.803550 0.435631 0.359042 0.063 Uiso 1 1 calc R U . . . H00M H 0.643699 0.322740 0.322589 0.063 Uiso 1 1 calc R U . . . C00L C 0.6154(6) 0.5327(5) 0.28060(19) 0.0627(11) Uani 1 1 d . . . . . H00N H 0.647359 0.633149 0.296559 0.075 Uiso 1 1 calc R U . . . H00O H 0.703206 0.509672 0.245558 0.075 Uiso 1 1 calc R U . . . C00M C 0.2933(5) 0.4400(5) 0.36343(18) 0.0540(9) Uani 1 1 d . . . . . H00P H 0.264261 0.339855 0.346567 0.065 Uiso 1 1 calc R U . . . H00Q H 0.203409 0.460470 0.398173 0.065 Uiso 1 1 calc R U . . . C00N C 0.9288(7) 0.7441(5) 1.00802(18) 0.0601(10) Uani 1 1 d . . . . . H00R H 1.060770 0.719407 0.992676 0.072 Uiso 1 1 calc R U . . . H00S H 0.904405 0.849601 1.000009 0.072 Uiso 1 1 calc R U . . . C00O C 1.0680(6) 0.7889(5) 0.8390(2) 0.0630(11) Uani 1 1 d . . . . . H00T H 1.175977 0.755046 0.813553 0.094 Uiso 1 1 calc R U . . . H00U H 1.127731 0.833863 0.880679 0.094 Uiso 1 1 calc R U . . . H00V H 0.984420 0.860908 0.812651 0.094 Uiso 1 1 calc R U . . . C00P C 0.5517(6) 0.6792(6) 0.99464(18) 0.0621(11) Uani 1 1 d . . . . . H00W H 0.508243 0.781643 0.986422 0.074 Uiso 1 1 calc R U . . . H00X H 0.448131 0.615029 0.970616 0.074 Uiso 1 1 calc R U . . . C00Q C 0.2485(6) 0.5503(6) 0.3056(2) 0.0666(12) Uani 1 1 d . . . . . H00Y H 0.266493 0.650940 0.323094 0.080 Uiso 1 1 calc R U . . . H H 0.106208 0.539407 0.285768 0.080 Uiso 1 1 calc R U . . . C00R C 0.7324(9) 0.7383(6) 1.1101(2) 0.0808(15) Uani 1 1 d . . . . . H00Z H 0.696930 0.843195 1.106226 0.097 Uiso 1 1 calc R U . . . HA H 0.742254 0.711099 1.157773 0.097 Uiso 1 1 calc R U . . . C00S C 0.5646(8) 0.6470(6) 1.0704(2) 0.0758(13) Uani 1 1 d . . . . . H00 H 0.432958 0.669677 1.086431 0.091 Uiso 1 1 calc R U . . . HB H 0.592640 0.541931 1.078228 0.091 Uiso 1 1 calc R U . . . C00T C 0.9386(8) 0.7131(6) 1.0839(2) 0.0761(14) Uani 1 1 d . . . . . H1 H 0.981440 0.610716 1.092720 0.091 Uiso 1 1 calc R U . . . HC H 1.041085 0.777598 1.108245 0.091 Uiso 1 1 calc R U . . . C00U C 0.3919(7) 0.5253(6) 0.2506(2) 0.0707(12) Uani 1 1 d . . . . . H2 H 0.363845 0.428539 0.229667 0.085 Uiso 1 1 calc R U . . . HD H 0.365730 0.600681 0.215533 0.085 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0370(12) 0.0694(16) 0.0389(12) -0.0126(11) 0.0036(9) 0.0037(11) O002 0.0400(14) 0.0777(18) 0.0447(14) -0.0174(13) 0.0095(11) -0.0056(12) N003 0.0380(14) 0.0452(15) 0.0343(13) -0.0008(11) 0.0064(11) 0.0026(11) N004 0.0407(15) 0.066(2) 0.0350(14) -0.0027(13) 0.0071(12) -0.0091(14) N005 0.0385(16) 0.083(2) 0.0380(15) -0.0116(15) 0.0028(12) 0.0064(15) C006 0.0370(18) 0.053(2) 0.0349(16) 0.0011(14) 0.0059(13) 0.0061(14) C007 0.0359(16) 0.0432(17) 0.0362(16) -0.0015(13) 0.0050(13) -0.0011(13) C008 0.0425(18) 0.0479(19) 0.0385(17) -0.0074(15) 0.0109(14) -0.0050(15) C009 0.0392(17) 0.0412(17) 0.0340(15) 0.0029(13) 0.0036(13) 0.0013(13) C00A 0.0388(16) 0.0417(18) 0.0365(16) 0.0022(13) 0.0051(13) 0.0040(13) C00B 0.0371(17) 0.056(2) 0.0388(17) -0.0011(15) 0.0013(13) -0.0023(15) C00C 0.0395(18) 0.0506(19) 0.0381(17) -0.0095(15) 0.0070(14) -0.0074(15) C00D 0.0382(18) 0.063(2) 0.0439(18) 0.0005(17) 0.0061(14) -0.0029(16) C00E 0.0430(19) 0.055(2) 0.0389(18) -0.0013(15) 0.0112(14) 0.0022(15) C00F 0.0424(18) 0.050(2) 0.0358(16) -0.0085(14) 0.0081(13) -0.0034(14) C00G 0.0417(18) 0.053(2) 0.0428(18) -0.0062(16) 0.0018(14) 0.0034(15) C00H 0.0454(19) 0.051(2) 0.0386(17) -0.0066(15) 0.0035(14) 0.0080(15) C00I 0.047(2) 0.059(2) 0.078(3) -0.022(2) 0.0071(19) 0.0039(17) C00J 0.047(2) 0.054(2) 0.0416(18) -0.0057(16) 0.0022(15) 0.0027(16) C00K 0.050(2) 0.064(2) 0.0450(19) -0.0076(17) 0.0143(16) -0.0027(17) C00L 0.067(3) 0.081(3) 0.043(2) 0.0005(19) 0.0203(19) -0.009(2) C00M 0.044(2) 0.078(3) 0.0403(18) -0.0059(19) 0.0078(15) -0.0047(18) C00N 0.066(3) 0.067(3) 0.045(2) -0.0010(18) -0.0048(18) -0.0042(19) C00O 0.049(2) 0.064(3) 0.076(3) -0.008(2) 0.010(2) -0.0038(19) C00P 0.056(3) 0.088(3) 0.043(2) -0.007(2) 0.0104(17) 0.003(2) C00Q 0.054(2) 0.096(3) 0.048(2) 0.001(2) -0.0001(18) 0.006(2) C00R 0.125(5) 0.081(3) 0.036(2) -0.005(2) 0.007(2) -0.002(3) C00S 0.089(3) 0.094(3) 0.048(2) 0.003(2) 0.020(2) 0.000(3) C00T 0.098(4) 0.075(3) 0.051(2) 0.003(2) -0.014(2) -0.012(3) C00U 0.077(3) 0.094(3) 0.041(2) 0.001(2) 0.006(2) 0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C007 O001 C008 105.6(2) . . ? C006 O002 C00G 106.3(2) . . ? C009 N003 C00A 116.1(3) . . ? C007 N004 C00C 107.4(3) . . ? C006 N005 C00H 106.9(3) . . ? O002 C006 C00A 118.1(3) . . ? N005 C006 O002 118.9(3) . . ? N005 C006 C00A 122.8(3) . . ? O001 C007 C009 118.2(3) . . ? N004 C007 O001 119.1(3) . . ? N004 C007 C009 122.8(3) . . ? O001 C008 H008 109.6 . . ? O001 C008 C00C 103.7(2) . . ? O001 C008 C00I 109.5(3) . . ? C00C C008 H008 109.6 . . ? C00I C008 H008 109.6 . . ? C00I C008 C00C 114.8(3) . . ? N003 C009 C007 119.5(3) . . ? N003 C009 C00B 123.2(3) . . ? C00B C009 C007 117.2(3) . . ? N003 C00A C006 118.6(3) . . ? N003 C00A C00E 123.9(3) . . ? C00E C00A C006 117.4(3) . . ? C009 C00B H00B 120.1 . . ? C00D C00B C009 119.9(3) . . ? C00D C00B H00B 120.1 . . ? N004 C00C C008 104.4(3) . . ? N004 C00C H00C 108.6 . . ? N004 C00C C00F 111.3(3) . . ? C008 C00C H00C 108.6 . . ? C00F C00C C008 115.2(3) . . ? C00F C00C H00C 108.6 . . ? C00B C00D H00D 121.1 . . ? C00B C00D C00E 117.9(3) . . ? C00E C00D H00D 121.1 . . ? C00A C00E H00E 120.6 . . ? C00D C00E C00A 118.9(3) . . ? C00D C00E H00E 120.6 . . ? C00C C00F H00F 107.7 . . ? C00C C00F C00K 112.1(3) . . ? C00C C00F C00M 111.9(3) . . ? C00K C00F H00F 107.7 . . ? C00K C00F C00M 109.6(3) . . ? C00M C00F H00F 107.7 . . ? O002 C00G H00G 109.3 . . ? O002 C00G C00H 103.0(3) . . ? O002 C00G C00O 109.8(3) . . ? C00H C00G H00G 109.3 . . ? C00O C00G H00G 109.3 . . ? C00O C00G C00H 115.7(3) . . ? N005 C00H C00G 104.1(3) . . ? N005 C00H H00H 107.8 . . ? N005 C00H C00J 113.1(3) . . ? C00G C00H H00H 107.8 . . ? C00J C00H C00G 115.9(3) . . ? C00J C00H H00H 107.8 . . ? C008 C00I H00A 109.5 . . ? C008 C00I H00I 109.5 . . ? C008 C00I H00J 109.5 . . ? H00A C00I H00I 109.5 . . ? H00A C00I H00J 109.5 . . ? H00I C00I H00J 109.5 . . ? C00H C00J H00K 108.3 . . ? C00H C00J C00N 110.5(3) . . ? C00H C00J C00P 111.3(3) . . ? C00N C00J H00K 108.3 . . ? C00P C00J H00K 108.3 . . ? C00P C00J C00N 110.1(3) . . ? C00F C00K H00L 109.3 . . ? C00F C00K H00M 109.3 . . ? H00L C00K H00M 108.0 . . ? C00L C00K C00F 111.6(3) . . ? C00L C00K H00L 109.3 . . ? C00L C00K H00M 109.3 . . ? C00K C00L H00N 109.3 . . ? C00K C00L H00O 109.3 . . ? H00N C00L H00O 108.0 . . ? C00U C00L C00K 111.6(3) . . ? C00U C00L H00N 109.3 . . ? C00U C00L H00O 109.3 . . ? C00F C00M H00P 109.4 . . ? C00F C00M H00Q 109.4 . . ? H00P C00M H00Q 108.0 . . ? C00Q C00M C00F 111.3(3) . . ? C00Q C00M H00P 109.4 . . ? C00Q C00M H00Q 109.4 . . ? C00J C00N H00R 109.1 . . ? C00J C00N H00S 109.1 . . ? H00R C00N H00S 107.9 . . ? C00T C00N C00J 112.3(3) . . ? C00T C00N H00R 109.1 . . ? C00T C00N H00S 109.1 . . ? C00G C00O H00T 109.5 . . ? C00G C00O H00U 109.5 . . ? C00G C00O H00V 109.5 . . ? H00T C00O H00U 109.5 . . ? H00T C00O H00V 109.5 . . ? H00U C00O H00V 109.5 . . ? C00J C00P H00W 109.1 . . ? C00J C00P H00X 109.1 . . ? H00W C00P H00X 107.9 . . ? C00S C00P C00J 112.3(3) . . ? C00S C00P H00W 109.1 . . ? C00S C00P H00X 109.1 . . ? C00M C00Q H00Y 109.4 . . ? C00M C00Q H 109.4 . . ? C00M C00Q C00U 111.1(4) . . ? H00Y C00Q H 108.0 . . ? C00U C00Q H00Y 109.4 . . ? C00U C00Q H 109.4 . . ? H00Z C00R HA 108.0 . . ? C00S C00R H00Z 109.4 . . ? C00S C00R HA 109.4 . . ? C00T C00R H00Z 109.4 . . ? C00T C00R HA 109.4 . . ? C00T C00R C00S 111.1(4) . . ? C00P C00S H00 109.3 . . ? C00P C00S HB 109.3 . . ? C00R C00S C00P 111.4(4) . . ? C00R C00S H00 109.3 . . ? C00R C00S HB 109.3 . . ? H00 C00S HB 108.0 . . ? C00N C00T H1 109.3 . . ? C00N C00T HC 109.3 . . ? C00R C00T C00N 111.8(4) . . ? C00R C00T H1 109.3 . . ? C00R C00T HC 109.3 . . ? H1 C00T HC 107.9 . . ? C00L C00U C00Q 110.7(3) . . ? C00L C00U H2 109.5 . . ? C00L C00U HD 109.5 . . ? C00Q C00U H2 109.5 . . ? C00Q C00U HD 109.5 . . ? H2 C00U HD 108.1 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C007 1.354(4) . ? O001 C008 1.472(4) . ? O002 C006 1.348(4) . ? O002 C00G 1.461(4) . ? N003 C009 1.344(4) . ? N003 C00A 1.346(4) . ? N004 C007 1.266(4) . ? N004 C00C 1.471(4) . ? N005 C006 1.263(4) . ? N005 C00H 1.478(4) . ? C006 C00A 1.485(5) . ? C007 C009 1.488(4) . ? C008 H008 0.9800 . ? C008 C00C 1.546(5) . ? C008 C00I 1.501(5) . ? C009 C00B 1.392(4) . ? C00A C00E 1.391(5) . ? C00B H00B 0.9300 . ? C00B C00D 1.372(4) . ? C00C H00C 0.9800 . ? C00C C00F 1.525(5) . ? C00D H00D 0.9300 . ? C00D C00E 1.386(5) . ? C00E H00E 0.9300 . ? C00F H00F 0.9800 . ? C00F C00K 1.530(4) . ? C00F C00M 1.531(5) . ? C00G H00G 0.9800 . ? C00G C00H 1.549(5) . ? C00G C00O 1.504(5) . ? C00H H00H 0.9800 . ? C00H C00J 1.530(5) . ? C00I H00A 0.9600 . ? C00I H00I 0.9600 . ? C00I H00J 0.9600 . ? C00J H00K 0.9800 . ? C00J C00N 1.534(5) . ? C00J C00P 1.530(5) . ? C00K H00L 0.9700 . ? C00K H00M 0.9700 . ? C00K C00L 1.523(5) . ? C00L H00N 0.9700 . ? C00L H00O 0.9700 . ? C00L C00U 1.512(6) . ? C00M H00P 0.9700 . ? C00M H00Q 0.9700 . ? C00M C00Q 1.516(6) . ? C00N H00R 0.9700 . ? C00N H00S 0.9700 . ? C00N C00T 1.521(5) . ? C00O H00T 0.9600 . ? C00O H00U 0.9600 . ? C00O H00V 0.9600 . ? C00P H00W 0.9700 . ? C00P H00X 0.9700 . ? C00P C00S 1.519(5) . ? C00Q H00Y 0.9700 . ? C00Q H 0.9700 . ? C00Q C00U 1.529(6) . ? C00R H00Z 0.9700 . ? C00R HA 0.9700 . ? C00R C00S 1.513(7) . ? C00R C00T 1.511(7) . ? C00S H00 0.9700 . ? C00S HB 0.9700 . ? C00T H1 0.9700 . ? C00T HC 0.9700 . ? C00U H2 0.9700 . ? C00U HD 0.9700 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O001 C007 C009 N003 10.4(4) . . . . ? O001 C007 C009 C00B -171.0(3) . . . . ? O001 C008 C00C N004 0.4(3) . . . . ? O001 C008 C00C C00F 122.8(3) . . . . ? O002 C006 C00A N003 -3.3(5) . . . . ? O002 C006 C00A C00E -179.8(3) . . . . ? O002 C00G C00H N005 8.4(4) . . . . ? O002 C00G C00H C00J 133.3(3) . . . . ? N003 C009 C00B C00D -2.0(5) . . . . ? N003 C00A C00E C00D -3.1(5) . . . . ? N004 C007 C009 N003 -168.9(3) . . . . ? N004 C007 C009 C00B 9.7(5) . . . . ? N004 C00C C00F C00K 178.3(3) . . . . ? N004 C00C C00F C00M -58.1(3) . . . . ? N005 C006 C00A N003 171.7(3) . . . . ? N005 C006 C00A C00E -4.8(5) . . . . ? N005 C00H C00J C00N -175.3(3) . . . . ? N005 C00H C00J C00P -52.6(4) . . . . ? C006 O002 C00G C00H -7.1(3) . . . . ? C006 O002 C00G C00O -131.0(3) . . . . ? C006 N005 C00H C00G -6.9(4) . . . . ? C006 N005 C00H C00J -133.6(3) . . . . ? C006 C00A C00E C00D 173.2(3) . . . . ? C007 O001 C008 C00C -0.7(3) . . . . ? C007 O001 C008 C00I -123.7(3) . . . . ? C007 N004 C00C C008 0.1(4) . . . . ? C007 N004 C00C C00F -124.8(3) . . . . ? C007 C009 C00B C00D 179.4(3) . . . . ? C008 O001 C007 N004 0.9(4) . . . . ? C008 O001 C007 C009 -178.4(3) . . . . ? C008 C00C C00F C00K 59.8(4) . . . . ? C008 C00C C00F C00M -176.7(3) . . . . ? C009 N003 C00A C006 -173.8(3) . . . . ? C009 N003 C00A C00E 2.5(5) . . . . ? C009 C00B C00D C00E 1.3(5) . . . . ? C00A N003 C009 C007 178.7(3) . . . . ? C00A N003 C009 C00B 0.1(4) . . . . ? C00B C00D C00E C00A 1.1(5) . . . . ? C00C N004 C007 O001 -0.7(4) . . . . ? C00C N004 C007 C009 178.7(3) . . . . ? C00C C00F C00K C00L -179.4(3) . . . . ? C00C C00F C00M C00Q 178.4(3) . . . . ? C00F C00K C00L C00U -55.9(4) . . . . ? C00F C00M C00Q C00U 57.2(5) . . . . ? C00G O002 C006 N005 3.3(4) . . . . ? C00G O002 C006 C00A 178.5(3) . . . . ? C00G C00H C00J C00N 64.6(4) . . . . ? C00G C00H C00J C00P -172.8(3) . . . . ? C00H N005 C006 O002 2.6(4) . . . . ? C00H N005 C006 C00A -172.3(3) . . . . ? C00H C00J C00N C00T 176.2(3) . . . . ? C00H C00J C00P C00S -176.5(4) . . . . ? C00I C008 C00C N004 119.8(3) . . . . ? C00I C008 C00C C00F -117.8(3) . . . . ? C00J C00N C00T C00R -54.5(5) . . . . ? C00J C00P C00S C00R 55.7(6) . . . . ? C00K C00F C00M C00Q -56.7(4) . . . . ? C00K C00L C00U C00Q 55.0(5) . . . . ? C00M C00F C00K C00L 55.8(4) . . . . ? C00M C00Q C00U C00L -55.8(5) . . . . ? C00N C00J C00P C00S -53.6(5) . . . . ? C00O C00G C00H N005 128.3(3) . . . . ? C00O C00G C00H C00J -106.8(4) . . . . ? C00P C00J C00N C00T 52.9(5) . . . . ? C00S C00R C00T C00N 55.3(5) . . . . ? C00T C00R C00S C00P -55.8(6) . . . . ?