#------------------------------------------------------------------------------ #$Date: 2024-08-05 20:53:54 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293732 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/18/1571899.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571899 loop_ _publ_author_name 'Fan, Chang-Chun' 'Liu, Cheng-Dong' 'Liang, Bei-Dou' 'Ju, Tong-Yu' 'Wang, Wei' 'Jin, Ming-Liang' 'Chai, Chao-Yang' 'Zhang, Wen' _publ_section_title ; Chiral three-dimensional organic-inorganic lead iodide hybrid semiconductors. ; _journal_issue 29 _journal_name_full 'Chemical science' _journal_page_first 11374 _journal_page_last 11381 _journal_paper_doi 10.1039/d4sc00954a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'I6 Pb2, C7 H11 N2' _chemical_formula_sum 'C7 H11 I6 N2 Pb2' _chemical_formula_weight 1298.96 _space_group_crystal_system orthorhombic _space_group_IT_number 20 _space_group_name_Hall 'C 2c 2' _space_group_name_H-M_alt 'C 2 2 21' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary iterative _audit_creation_date 2024-01-05 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2024-01-05 deposited with the CCDC. 2024-06-13 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 12.9621(7) _cell_length_b 18.7875(13) _cell_length_c 17.6666(9) _cell_measurement_reflns_used 3248 _cell_measurement_temperature 298.53(10) _cell_measurement_theta_max 30.6130 _cell_measurement_theta_min 3.9010 _cell_volume 4302.3(4) _computing_cell_refinement 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_environment air _diffrn_ambient_temperature 298.53(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.808 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -23.00 53.00 0.50 2.00 -- -7.05 38.00 0.00 152 2 \w -35.00 -3.00 0.50 2.00 -- -7.05 87.00 134.00 64 3 \w -18.00 14.00 0.50 2.00 -- -7.05 -99.00-120.00 64 4 \w -9.00 18.00 0.50 2.00 -- -7.05 -99.00-150.00 54 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0116812000 _diffrn_orient_matrix_UB_12 -0.0368952000 _diffrn_orient_matrix_UB_13 0.0005537000 _diffrn_orient_matrix_UB_21 -0.0476403000 _diffrn_orient_matrix_UB_22 0.0069374000 _diffrn_orient_matrix_UB_23 -0.0183189000 _diffrn_orient_matrix_UB_31 0.0242479000 _diffrn_orient_matrix_UB_32 -0.0041222000 _diffrn_orient_matrix_UB_33 -0.0357085000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0252 _diffrn_reflns_av_unetI/netI 0.0380 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.808 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 11819 _diffrn_reflns_point_group_measured_fraction_full 0.982 _diffrn_reflns_point_group_measured_fraction_max 0.759 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.652 _diffrn_reflns_theta_min 1.909 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 24.230 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.71819 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.84a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'metallic reddish red' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier reddish _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 4.011 _exptl_crystal_description block _exptl_crystal_F_000 4392 _exptl_crystal_size_max 0.03 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.02 _refine_diff_density_max 1.955 _refine_diff_density_min -2.707 _refine_diff_density_rms 0.293 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.41(2) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.075 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 176 _refine_ls_number_reflns 5064 _refine_ls_number_restraints 374 _refine_ls_restrained_S_all 1.053 _refine_ls_R_factor_all 0.0791 _refine_ls_R_factor_gt 0.0424 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0414P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0952 _refine_ls_wR_factor_ref 0.1058 _reflns_Friedel_coverage 0.716 _reflns_Friedel_fraction_full 0.958 _reflns_Friedel_fraction_max 0.700 _reflns_number_gt 3198 _reflns_number_total 5064 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc00954a2.cif _cod_data_source_block 3S-298K _cod_depositor_comments 'Adding full bibliography for 1571897--1571906.cif.' _cod_database_code 1571899 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C1 H1 N1 I1 Pb1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.643 _shelx_estimated_absorpt_t_min 0.530 _reflns_odcompleteness_completeness 99.80 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.58546 0.41454 2. Restrained distances N1B-C2 = N1A-C2 1.47 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints N2 \\sim H2 \\sim C2 \\sim H2A \\sim C3 \\sim C4 \\sim H4 \\sim C5 \\sim H5 \\sim C6 \\sim H6 \\sim C7 \\sim H7 \\sim N1A \\sim H1AA \\sim H1AB \\sim H1AC \\sim C1A \\sim H1AD \\sim H1AE \\sim H1AF \\sim N1B \\sim H1BA \\sim H1BB \\sim C1B \\sim H1BC \\sim H1BD \\sim H1BE: within 1.7A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 1.7A Uanis(N1A) \\sim Ueq, Uanis(C1B) \\sim Ueq, Uanis(N1B) \\sim Ueq, Uanis(C1A) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 4. Rigid body (RIGU) restrains N2, H2, C2, C3, C4, H4, C5, H5, C6, H6, C7, H7, N1A, C1A, N1B, C1B with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C7, C3, C4, C5, C6, N2, C2, N1B, C1A, N1A, C1B with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Fixed Sof: H2A(0.5) N1A(0.5) H1AA(0.5) H1AB(0.5) H1AC(0.5) C1A(0.5) H1AD(0.5) H1AE(0.5) H1AF(0.5) N1B(0.5) H1BA(0.5) H1BB(0.5) C1B(0.5) H1BC(0.5) H1BD(0.5) H1BE(0.5) 6.a Riding coordinates: N1A(H1AA,H1AB,H1AC), C1A(H1AD,H1AE,H1AF), C1B(H1BC,H1BD,H1BE) 6.b Ternary CH refined with riding coordinates: C2(H2A) 6.c Aromatic/amide H refined with riding coordinates: N2(H2), C4(H4), C5(H5), C6(H6), C7(H7) 6.d X=CH2 refined with riding coordinates: N1B(H1BA,H1BB) ; _shelx_res_file ; TITL fcc-121-01-1_a.res in C222(1) fcc-121-01-1.res created by SHELXL-2018/3 at 14:38:14 on 05-Jan-2024 CELL 0.71073 12.9621 18.7875 17.6666 90 90 90 ZERR 8 0.0007 0.0013 0.0009 0 0 0 LATT -7 SYMM -X,-Y,0.5+Z SYMM -X,+Y,0.5-Z SYMM +X,-Y,-Z SFAC C H I N Pb UNIT 56 88 48 16 16 DFIX 1.47 N1B C2 N1A C2 SIMU 0.04 0.08 1.7 N2 H2 C2 H2a C3 C4 H4 C5 H5 C6 H6 C7 H7 N1A H1Aa H1Ab = H1AC C1A H1AD H1AE H1AF N1B H1BA H1BB C1B H1BC H1BD H1BE RIGU N2 H2 C2 C3 C4 H4 C5 H5 C6 H6 C7 H7 N1A > C1B ISOR 0.01 0.02 N1A C1B N1B C1A RIGU C7 C3 C4 C5 C6 N2 C2 N1B C1A N1A C1B L.S. 50 PLAN 1 SIZE 0.03 0.03 0.02 TEMP 5.53 CONF BOND LIST 4 MORE -1 BOND $H fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 REM REM REM WGHT 0.041400 BASF 0.41454 FVAR 0.03484 PB1 5 0.503664 0.875400 1.119648 11.00000 0.03521 0.03272 = 0.02604 -0.00066 0.00202 0.00067 PB2 5 0.501255 0.625010 0.878572 11.00000 0.03811 0.03018 = 0.02551 0.00011 -0.00080 -0.00321 I1 3 0.500000 0.755638 1.250000 10.50000 0.02667 0.03417 = 0.03170 0.00000 0.00316 0.00000 I2 3 0.500000 0.990427 1.250000 10.50000 0.03847 0.03166 = 0.02986 0.00000 -0.00054 0.00000 I3 3 0.530339 1.000000 1.000000 10.50000 0.06149 0.05067 = 0.04254 0.02136 0.00000 0.00000 I4 3 0.500000 0.502759 0.750000 10.50000 0.04045 0.02828 = 0.02918 0.00000 0.00208 0.00000 I5 3 0.476236 0.500000 1.000000 10.50000 0.10124 0.05725 = 0.04180 0.02736 0.00000 0.00000 I6 3 0.500000 0.742648 0.750000 10.50000 0.04290 0.03011 = 0.02948 0.00000 -0.00007 0.00000 I7 3 0.751604 0.865659 1.127226 11.00000 0.02507 0.04663 = 0.05707 0.00973 -0.00600 0.00201 I8 3 0.751349 0.608342 0.889666 11.00000 0.02882 0.07598 = 0.06757 -0.00500 -0.00274 0.00390 I9 3 0.490862 0.745435 1.002275 11.00000 0.11784 0.06733 = 0.04882 -0.03535 0.00747 -0.02804 N2 4 0.744331 0.939153 0.852862 11.00000 0.09616 0.07156 = 0.08194 -0.02438 -0.00786 0.02962 AFIX 43 H2 2 0.734808 0.979246 0.875290 11.00000 -1.20000 AFIX 0 C2 1 0.746895 0.854035 0.657836 11.00000 0.08582 0.12295 = 0.04737 0.00045 -0.00766 0.01558 PART 1 AFIX 13 H2A 2 0.749507 0.803493 0.644252 10.50000 -1.20000 AFIX 0 PART 0 C3 1 0.748301 0.867147 0.743044 11.00000 0.02207 0.06383 = 0.03885 -0.00400 -0.00231 0.00181 C4 1 0.750946 0.809307 0.786101 11.00000 0.04221 0.05205 = 0.07402 -0.00588 -0.01471 -0.02146 AFIX 43 H4 2 0.748149 0.765066 0.762575 11.00000 -1.20000 AFIX 0 C5 1 0.757588 0.811466 0.863470 11.00000 0.05188 0.07532 = 0.06596 0.04212 0.00999 0.00299 AFIX 43 H5 2 0.763719 0.770996 0.893448 11.00000 -1.20000 AFIX 0 C6 1 0.754346 0.878310 0.891973 11.00000 0.06379 0.10278 = 0.05971 0.00553 -0.04424 0.02600 AFIX 43 H6 2 0.759627 0.882521 0.944281 11.00000 -1.20000 AFIX 0 C7 1 0.749955 0.934507 0.775735 11.00000 0.02658 0.05292 = 0.07282 0.00032 0.00989 -0.01165 AFIX 43 H7 2 0.754749 0.975208 0.745981 11.00000 -1.20000 AFIX 0 PART 1 N1A 4 0.821201 0.897552 0.616536 10.50000 0.08489 0.10559 = 0.05899 -0.00478 0.00897 0.02186 AFIX 3 H1AA 2 0.830971 0.879242 0.570626 10.50000 -1.20000 H1AB 2 0.880681 0.897722 0.641706 10.50000 -1.20000 H1AC 2 0.797871 0.941922 0.612266 10.50000 -1.20000 AFIX 0 C1A 1 0.657351 0.891957 0.625053 10.50000 0.06357 0.04277 = 0.02295 -0.00187 -0.01395 -0.03194 AFIX 3 H1AD 2 0.596411 0.880657 0.653503 10.50000 -1.50000 H1AE 2 0.648111 0.877597 0.573353 10.50000 -1.50000 H1AF 2 0.669521 0.942317 0.627103 10.50000 -1.50000 AFIX 0 PART 2 N1B 4 0.655269 0.859127 0.615055 10.50000 0.09930 0.09758 = 0.04253 0.01441 -0.02319 -0.01412 AFIX 93 H1BA 2 0.657703 0.872887 0.568661 10.50000 -1.20000 H1BB 2 0.596990 0.848470 0.635373 10.50000 -1.20000 AFIX 0 C1B 1 0.852108 0.871929 0.625753 10.50000 0.08981 0.07101 = 0.02448 -0.01362 0.00659 0.03153 AFIX 3 H1BC 2 0.866858 0.921569 0.632893 10.50000 -1.50000 H1BD 2 0.852288 0.861139 0.572643 10.50000 -1.50000 H1BE 2 0.903728 0.843899 0.650833 10.50000 -1.50000 AFIX 0 HKLF 4 REM fcc-121-01-1_a.res in C222(1) REM wR2 = 0.1058, GooF = S = 1.075, Restrained GooF = 1.053 for all data REM R1 = 0.0424 for 3198 Fo > 4sig(Fo) and 0.0791 for all 5064 data REM 176 parameters refined using 374 restraints END WGHT 0.0414 0.0000 REM Highest difference peak 1.955, deepest hole -2.707, 1-sigma level 0.293 Q1 1 0.7603 0.9064 1.1015 11.00000 0.05 1.96 ; _shelx_res_checksum 17689 _shelx_hkl_file ; 0 0 2 1.30 0.23 0 0 -2 1.01 0.20 0 0 3 -0.03 0.23 0 0 -3 -0.12 0.23 0 0 4 355.32 8.04 0 0 -4 344.03 8.03 0 0 5 -0.10 0.55 0 0 -5 -0.05 0.48 0 0 -6 178.84 4.84 0 0 6 183.94 4.85 0 0 7 0.39 0.64 0 0 -7 -0.27 0.63 0 0 8 7339.02 153.28 0 0 -8 7253.99 153.36 0 0 9 -0.98 0.88 0 0 9 -0.24 0.73 0 0 10 101.48 3.34 0 0 10 86.38 3.33 0 0 11 -0.24 1.14 0 0 11 1.67 1.08 0 0 12 34.47 2.11 0 0 12 34.32 2.20 0 0 13 0.46 1.24 0 0 13 -0.12 1.24 0 0 14 181.36 5.60 0 0 14 174.89 5.91 0 0 15 0.31 1.58 0 0 15 1.99 1.62 0 0 16 1423.54 31.68 0 0 16 1406.29 32.24 0 0 17 -0.11 1.54 0 0 18 39.80 2.65 0 0 19 0.86 1.62 0 0 20 3.29 1.72 0 0 21 0.92 1.82 0 0 22 70.17 3.78 0 0 22 75.30 3.85 0 -2 0 1.51 0.21 0 -2 1 1453.51 30.63 0 -2 2 0.44 0.18 0 -2 3 2028.47 42.55 0 -2 3 2023.58 42.48 0 -2 -4 0.44 0.32 0 -2 4 0.40 0.23 0 -2 5 971.46 21.65 0 2 -5 1026.49 21.97 0 -2 5 1021.99 21.81 0 2 -5 1015.53 21.79 0 -2 -5 1010.43 21.51 0 -2 5 1012.02 21.28 0 -2 6 1.30 0.74 0 2 -6 0.18 0.66 0 2 -6 0.84 0.54 0 2 6 0.92 0.57 0 -2 -6 1.21 0.38 0 -2 7 1867.33 39.70 0 2 7 1816.44 39.90 0 2 -7 1862.77 39.99 0 -2 -7 1864.11 39.17 0 -2 8 1.28 0.78 0 2 8 -0.28 0.71 0 2 -8 0.46 0.69 0 -2 -8 0.77 0.38 0 -2 -9 380.26 8.35 0 2 9 358.52 9.33 0 2 -9 375.33 9.46 0 -2 9 373.15 9.13 0 2 -10 0.78 0.84 0 2 10 1.61 0.90 0 -2 -10 1.58 0.42 0 -2 10 1.12 1.08 0 -2 11 887.87 19.86 0 2 11 900.43 20.16 0 2 -11 875.02 20.31 0 -2 -11 864.27 18.58 0 2 12 1.37 1.16 0 2 -12 0.11 1.00 0 -2 12 0.44 1.21 0 2 13 125.39 4.53 0 2 -13 126.59 4.63 0 -2 13 124.20 4.37 0 -2 14 0.80 1.55 0 2 14 0.47 1.26 0 2 -14 -0.13 1.18 0 2 15 587.51 14.81 0 -2 15 600.73 14.55 0 2 15 597.72 14.49 0 -2 16 0.56 1.56 0 2 16 -0.66 1.61 0 2 16 1.19 1.38 0 2 17 34.06 2.49 0 -2 17 37.75 2.63 0 -2 17 35.56 2.46 0 2 18 -0.24 1.55 0 -2 18 -0.57 1.59 0 2 19 172.91 6.01 0 -2 19 186.02 6.01 0 2 20 -0.13 1.81 0 -2 20 -0.12 1.68 0 2 21 9.37 2.10 0 -2 21 5.07 1.85 0 2 22 -1.08 1.92 0 -2 22 -0.92 2.01 0 -4 0 409.79 9.33 0 -4 -1 0.75 0.40 0 -4 1 1.13 0.44 0 -4 2 14.93 0.88 0 -4 3 5.37 0.60 0 -4 -4 9056.70 194.99 0 -4 4 9083.30 194.79 0 4 -5 -0.19 0.50 0 4 -5 1.46 0.76 0 -4 5 0.37 0.42 0 -4 -5 0.42 0.52 0 -4 6 93.44 2.77 0 4 -6 97.56 2.99 0 -4 -6 95.47 2.85 0 -4 6 94.99 2.61 0 -4 7 1.32 0.41 0 -4 -7 1.29 0.57 0 -4 7 1.47 0.77 0 4 -7 2.07 0.68 0 4 -7 2.47 0.79 0 -4 8 112.03 3.29 0 4 -8 108.17 3.66 0 4 -8 108.70 3.44 0 -4 -8 106.22 3.19 0 -4 8 110.10 2.84 0 4 -9 1.04 0.84 0 -4 -9 1.47 0.61 0 -4 9 2.24 0.91 0 4 -9 2.59 0.85 0 -4 9 2.00 0.43 0 -4 10 167.56 4.64 0 -4 10 157.05 3.77 0 4 10 161.17 4.90 0 4 -10 158.79 5.05 0 -4 -10 162.11 4.31 0 4 11 2.59 1.10 0 -4 11 1.38 1.12 0 4 -11 1.63 1.04 0 -4 -11 2.58 0.71 0 -4 -12 2939.70 62.43 0 4 12 2957.39 63.58 0 4 -12 2938.25 63.89 0 -4 12 2983.78 63.08 0 4 13 4.40 1.37 0 4 -13 3.33 1.29 0 -4 -13 2.72 0.69 0 -4 13 1.62 1.37 0 -4 14 71.94 3.17 0 4 -14 73.09 3.51 0 4 14 75.52 3.47 0 -4 -14 72.31 2.25 0 4 -15 -0.43 1.27 0 4 15 0.52 1.30 0 -4 -15 0.25 0.44 0 -4 15 -1.47 1.60 0 4 -16 18.28 2.09 0 4 16 16.94 1.97 0 4 -17 -0.80 1.57 0 -4 17 0.88 1.63 0 -4 18 98.37 4.14 0 4 18 108.35 4.32 0 4 -18 99.71 4.60 0 4 19 -1.94 1.87 0 -4 19 -2.74 1.85 0 4 20 489.45 12.71 0 -4 20 476.89 12.49 0 4 21 1.23 1.87 0 -4 21 -0.51 1.98 0 4 22 20.15 2.55 0 -6 0 4.47 0.76 0 -6 -1 1061.36 24.07 0 -6 1 1131.49 24.04 0 -6 2 0.76 0.56 0 -6 3 2054.41 43.92 0 -6 4 5.24 0.72 0 -6 -4 5.57 0.88 0 6 -5 1054.16 23.15 0 -6 -5 1067.96 23.57 0 -6 5 1084.24 23.31 0 6 -6 9.89 0.95 0 -6 6 11.74 0.93 0 -6 -6 13.24 1.15 0 6 -7 775.84 17.25 0 6 -7 802.12 17.78 0 -6 -7 783.76 17.75 0 -6 7 785.39 17.36 0 -6 8 0.05 0.58 0 -6 -8 0.22 0.72 0 6 -8 1.04 1.03 0 6 -9 328.15 8.52 0 6 -9 317.40 8.23 0 -6 -9 319.33 8.09 0 -6 9 323.35 7.65 0 6 -10 6.86 1.32 0 -6 -10 8.21 1.09 0 -6 10 8.38 1.37 0 6 -10 6.92 1.24 0 -6 10 5.65 0.76 0 -6 11 1188.36 26.14 0 -6 11 1188.16 25.46 0 6 -11 1194.89 26.87 0 6 -11 1169.53 26.43 0 -6 -11 1168.40 26.11 0 -6 -12 1.09 0.89 0 -6 12 0.59 0.59 0 6 -12 -1.33 1.35 0 -6 12 2.42 1.45 0 6 -12 0.36 1.09 0 6 12 -0.96 1.20 0 -6 13 141.37 4.60 0 -6 -13 135.88 4.21 0 6 -13 148.92 5.22 0 6 13 143.68 4.97 0 -6 13 137.09 3.42 0 6 14 4.92 1.50 0 -6 14 7.14 1.86 0 6 -14 5.99 1.51 0 -6 -14 4.50 1.01 0 -6 -15 204.93 5.48 0 6 15 206.19 6.65 0 6 -15 203.70 6.81 0 -6 15 197.21 6.19 0 -6 16 4.55 1.85 0 -6 -16 2.91 0.90 0 6 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1.99 -2 8 14 50.51 2.87 2 8 -14 42.59 2.87 -2 -8 -14 43.89 2.38 -2 -8 -13 10.92 1.48 2 8 -13 6.06 1.75 2 8 -13 6.82 1.57 2 -8 13 8.46 1.14 2 8 -12 40.07 2.66 -2 -8 -12 36.79 2.20 2 8 -12 38.01 2.66 2 8 -11 2.09 1.58 -2 -8 -11 3.32 1.13 2 -8 11 1.24 0.97 2 8 -10 9.56 1.75 -2 -8 -10 8.19 1.30 2 -8 10 8.69 1.17 2 8 -9 0.97 1.10 2 -8 9 2.72 0.98 2 -8 8 1879.54 40.57 2 8 -8 1876.79 40.51 2 8 -8 1846.70 40.89 2 8 -7 1.88 1.21 2 8 -7 1.83 1.18 -2 8 7 2.39 0.99 2 -8 7 3.13 0.97 2 -8 6 18.83 1.50 -2 8 6 18.94 1.50 2 8 -6 21.37 1.75 -2 8 5 3.39 0.99 2 -8 5 1.40 0.94 2 8 -5 4.57 1.25 -2 8 4 252.20 6.90 2 -8 4 250.46 6.88 2 -8 3 5.84 1.05 -2 8 3 5.35 1.04 2 -8 2 3.95 0.93 -2 8 2 5.07 1.06 2 -8 1 0.19 0.77 -2 8 1 1.86 0.97 2 -8 0 2879.55 61.80 2 -8 -1 0.97 0.87 -2 8 -3 7.17 1.12 -2 8 -4 254.82 6.96 2 -8 -4 259.27 7.23 -2 8 -5 3.12 1.05 2 -8 -5 1.35 0.96 2 -8 -6 17.81 1.64 -2 8 -6 20.23 1.48 -2 8 -6 19.11 1.13 -2 8 -7 2.23 0.92 2 -8 -7 1.39 0.95 -2 8 -7 0.57 0.60 2 -8 -8 1850.68 40.17 -2 8 -8 1805.64 39.56 2 -8 -9 2.39 1.11 -2 -8 9 3.76 0.92 -2 -8 10 10.07 1.09 -2 8 -10 8.21 1.46 2 -8 -10 6.97 1.34 -2 -8 11 3.44 0.86 -2 8 -11 2.41 1.34 -2 8 -11 4.12 1.44 2 -8 -11 2.18 1.24 -2 8 -12 40.54 2.69 -2 8 -12 38.44 2.33 -2 -8 12 39.82 1.82 2 -8 -12 38.84 2.36 -2 8 -13 6.44 1.52 -2 8 -13 11.91 1.76 2 -8 -13 13.71 1.60 -2 -8 13 7.17 0.98 2 -8 -14 42.05 2.47 -2 8 -14 42.26 2.48 2 8 14 49.84 2.86 -2 8 -14 46.51 2.87 -2 -8 14 47.40 1.87 2 -8 -15 1.25 1.18 -2 -8 15 0.33 0.66 -2 8 -15 0.16 1.39 -2 -8 16 560.35 12.31 -2 8 -16 598.54 15.19 2 -8 -16 599.35 13.91 -2 8 -17 1.98 1.79 2 -8 -17 2.59 1.26 -2 8 -18 14.41 2.33 2 -8 -18 15.37 1.54 -2 8 -19 -1.36 1.85 -2 8 -20 2.63 2.01 -2 -10 -19 22.64 1.94 2 10 -19 21.46 2.80 -2 -10 -18 0.43 1.25 2 10 -18 0.98 1.92 2 10 -17 8.82 2.14 -2 -10 -17 8.75 1.48 2 10 -16 3.54 1.90 -2 -10 -16 1.02 1.37 2 10 -15 363.25 10.52 -2 -10 -15 348.75 9.67 2 -10 15 368.01 8.99 -2 -10 -14 2.34 1.34 2 -10 14 3.02 1.14 2 10 -14 3.52 1.96 -2 -10 -13 16.00 1.77 2 -10 13 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84.48 2.58 -2 -10 9 89.90 3.34 2 -10 -10 6.97 1.70 -2 -10 10 8.19 1.25 -2 10 -11 45.10 2.60 -2 -10 11 42.66 2.16 2 -10 -11 38.25 2.61 -2 -10 12 1.62 1.05 -2 10 -12 2.88 1.56 2 -10 -12 0.13 1.27 -2 10 -12 0.83 1.40 -2 -10 13 10.98 1.29 -2 10 -13 14.71 2.02 2 -10 -13 14.87 1.92 -2 10 -13 13.78 1.82 -2 -10 14 5.37 1.08 -2 10 -14 4.88 1.67 -2 10 -14 6.37 1.77 2 -10 -14 4.82 1.47 2 -10 -15 347.59 9.80 -2 10 -15 355.34 10.42 -2 10 -15 353.79 9.64 -2 -10 15 365.70 8.79 -2 10 -16 2.32 1.72 -2 -10 16 2.48 0.92 2 -10 -16 0.51 1.42 -2 10 -17 6.99 2.12 2 -10 -17 6.09 1.58 -2 10 -18 0.79 1.86 2 -10 -18 -0.81 1.40 2 -10 -19 25.13 2.11 -2 10 -19 25.22 2.92 -2 -12 -19 -0.13 1.56 -2 -12 -18 39.71 2.80 2 12 -18 43.09 3.44 -2 -12 -17 2.58 1.64 2 12 -17 4.26 1.96 2 -12 16 6.48 1.44 -2 -12 -16 3.44 1.58 2 12 -16 6.91 2.07 2 -12 15 0.10 1.22 2 12 -15 0.54 1.77 -2 -12 -15 1.12 1.53 2 12 -14 24.54 2.62 2 12 -14 28.03 2.68 -2 -12 -14 26.33 2.29 2 -12 14 22.18 1.98 -2 -12 -13 2.41 1.50 2 -12 13 5.17 1.40 2 12 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7.13 1.89 2 -14 10 6.21 1.71 2 14 -10 6.87 2.14 2 14 -9 16.80 2.20 -2 -14 -9 17.97 2.23 2 -14 9 15.27 1.92 2 14 -9 17.93 2.40 2 14 -8 2.05 1.74 2 -14 8 0.14 1.33 -2 -14 -8 0.81 1.46 -2 -14 -7 44.48 3.01 2 14 -7 44.75 3.02 2 -14 7 38.29 2.74 2 -14 6 1.76 1.42 -2 -14 -6 2.24 1.55 -2 -14 -5 168.43 6.05 2 -14 5 156.66 5.81 2 -14 4 1.06 1.50 2 -14 3 434.77 11.92 2 -14 2 3.61 1.66 -2 -14 -1 42.82 2.87 2 -14 1 42.12 2.90 2 -14 0 0.16 1.33 -2 -14 0 1.08 1.41 -2 -14 1 45.81 2.96 2 -14 -1 44.00 3.01 -2 -14 2 4.23 1.49 -2 -14 3 433.29 11.81 -2 -14 4 2.64 1.42 -2 -14 5 166.65 6.00 2 -14 -5 181.72 6.55 -2 -14 6 0.57 1.37 2 -14 -6 1.39 1.62 -2 -14 7 40.48 2.69 2 -14 -7 38.39 2.99 2 -14 -8 2.65 1.62 -2 -14 8 -0.40 1.29 -2 14 -8 3.63 1.47 -2 -14 9 17.57 1.95 2 -14 -9 18.34 2.35 -2 14 -9 15.44 1.60 2 -14 -10 8.21 2.04 -2 -14 10 8.94 1.70 -2 14 -10 6.41 1.20 -2 -14 11 396.14 10.56 2 -14 -11 385.13 11.37 -2 14 -12 1.61 2.01 2 -14 -12 1.07 1.75 -2 -14 12 3.45 1.50 -2 -14 13 27.02 2.20 2 -14 -13 24.26 2.70 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10 -5 288.04 7.91 4 10 -5 275.68 7.93 -4 10 5 273.27 7.99 4 -10 5 267.30 8.03 4 -10 4 2.62 1.27 -4 10 4 2.16 1.26 -4 10 3 343.17 9.72 4 -10 3 364.70 9.85 4 -10 2 2.96 1.23 -4 10 2 5.35 1.47 -4 10 1 876.24 21.08 4 -10 1 897.00 21.18 4 -10 0 1.24 1.24 4 -10 -1 872.88 20.94 -4 10 -2 3.55 1.40 -4 10 -3 346.23 9.68 4 -10 -4 0.58 1.41 -4 10 -4 1.54 1.35 -4 10 -5 278.77 8.13 4 -10 -5 281.80 8.49 4 -10 -6 11.96 1.79 -4 10 -6 7.70 1.63 -4 10 -7 929.18 19.75 -4 10 -7 910.69 21.63 4 -10 -7 929.71 22.25 -4 10 -8 0.11 1.20 4 -10 -8 -0.76 1.52 -4 10 -9 253.20 7.43 4 -10 -9 261.13 8.09 4 -10 -10 10.37 1.96 -4 10 -10 10.98 1.59 4 -10 -11 163.37 6.06 -4 10 -11 173.14 5.25 -4 10 -11 170.21 5.37 -4 10 -12 0.18 1.29 -4 10 -12 1.47 1.20 -4 10 -12 2.75 1.57 4 -10 -12 0.45 1.51 -4 10 -13 66.69 3.02 -4 10 -13 68.49 3.68 -4 -10 13 68.95 2.90 4 -10 -13 72.49 3.69 4 -10 -14 3.70 1.69 -4 10 -14 2.93 1.49 -4 10 -14 7.94 1.93 -4 -10 14 3.65 1.14 -4 10 -15 383.72 9.90 -4 10 -15 389.73 11.11 -4 -10 15 390.67 9.57 4 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9 61.21 3.05 5 7 -9 65.41 3.25 5 -7 8 23.09 2.07 -5 7 8 22.03 1.96 5 7 -8 25.11 2.13 5 7 -7 102.42 4.07 5 7 -7 100.09 3.94 5 -7 7 100.40 3.99 -5 7 7 97.68 3.95 5 7 -6 13.33 1.85 -5 7 6 13.80 1.63 5 7 -6 13.88 1.80 5 -7 6 11.36 1.56 5 7 -5 -0.20 1.18 5 7 -5 0.93 1.35 -5 7 5 0.93 1.10 5 -7 5 2.52 1.27 -5 7 4 12.94 1.66 5 -7 4 8.94 1.51 5 7 -4 12.91 1.62 5 -7 3 2.12 1.13 -5 7 3 1.57 1.06 5 7 -3 2.13 1.18 5 -7 2 14.75 1.72 5 7 -2 15.26 1.59 -5 7 2 16.51 1.76 5 -7 1 124.50 4.70 -5 7 1 120.94 4.61 5 -7 0 0.79 1.06 -5 7 0 3.38 1.33 5 -7 -1 124.74 4.80 -5 7 -3 2.13 1.19 5 -7 -4 11.55 1.65 -5 7 -4 9.15 1.52 5 -7 -5 -0.83 1.27 -5 7 -5 1.34 1.19 -5 7 -5 -0.14 0.43 -5 7 -6 11.57 1.61 5 -7 -6 11.00 1.71 5 -7 -7 104.05 4.33 -5 7 -7 95.18 3.98 5 -7 -8 25.19 2.26 -5 7 -8 23.63 1.99 -5 7 -9 72.74 3.12 -5 7 -9 63.33 3.04 5 -7 -9 66.09 3.43 -5 7 -10 1.02 1.19 -5 7 -10 1.86 1.02 -5 7 -10 3.55 1.29 5 -7 -10 0.41 1.50 -5 7 -11 3.51 1.21 -5 7 -11 2.38 1.02 -5 7 -11 1.95 1.30 5 -7 -11 2.58 1.54 5 -7 -12 11.77 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2 2 4.98 1.24 6 2 -2 6.40 0.46 -6 2 2 5.34 1.10 -6 2 1 149.20 4.58 6 2 -1 157.48 4.76 -6 -2 -1 160.12 4.35 -6 2 1 170.47 5.31 6 2 -1 161.10 3.59 6 2 0 7.95 1.29 -6 2 0 7.35 1.08 -6 -2 0 10.06 1.09 -6 2 0 8.30 1.32 -6 2 -1 158.15 4.55 6 2 1 168.04 4.85 -6 -2 1 158.41 4.64 -6 2 -2 11.07 0.62 6 2 2 8.93 0.53 -6 -2 2 9.64 1.28 -6 2 -2 11.55 1.26 6 2 2 13.23 1.51 -6 -2 3 37.21 2.14 6 2 3 36.41 1.31 -6 2 -3 41.36 2.41 -6 -2 4 4.57 1.48 -6 2 -4 4.62 0.66 6 2 4 3.74 0.60 -6 2 -4 3.99 1.18 -6 -2 5 50.62 2.71 6 2 5 51.47 1.85 -6 2 -5 48.78 1.89 -6 2 -5 48.71 2.60 -6 2 -6 1.55 1.10 -6 -2 6 1.85 1.37 6 2 6 1.56 0.63 -6 2 -6 2.05 0.71 -6 -2 7 128.91 4.90 -6 -2 7 144.56 5.09 -6 2 -7 141.05 4.18 6 2 7 141.85 4.12 -6 2 -7 142.92 4.85 -6 -2 8 0.79 1.39 -6 2 -8 3.89 1.27 -6 -2 8 -0.39 1.75 6 2 8 3.35 0.93 -6 2 -8 3.19 0.96 -6 -2 9 78.57 3.78 -6 -2 9 68.09 3.60 -6 2 -9 76.24 3.26 6 2 9 72.74 2.83 -6 2 -9 71.52 2.91 -6 -2 9 69.86 3.14 -6 -2 10 7.90 2.02 -6 -2 10 7.06 1.41 -6 2 -10 6.71 1.45 -6 -2 10 3.21 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2.13 6 6 -8 1.26 1.50 6 6 -8 1.82 1.01 -6 6 8 2.46 1.32 6 6 -7 43.80 2.07 -6 6 7 40.73 2.54 6 6 -7 45.19 2.65 6 6 -7 41.16 2.59 6 6 -6 8.94 1.71 6 -6 6 13.28 1.81 -6 6 6 12.34 1.70 6 -6 5 101.67 4.14 -6 6 5 104.97 4.10 6 6 -4 4.61 1.38 6 -6 4 6.03 1.51 -6 6 4 7.11 1.46 6 6 -3 204.27 6.27 -6 6 3 209.87 6.59 6 6 -3 202.40 6.04 6 -6 3 210.87 6.65 6 6 -2 2.17 1.15 6 6 -2 6.24 1.66 6 -6 2 2.73 1.26 -6 6 2 4.55 1.36 -6 6 1 28.49 2.19 6 6 -1 25.88 1.84 6 -6 1 25.12 2.20 6 6 -1 31.69 2.28 6 -6 0 0.85 1.15 6 6 0 2.57 1.11 -6 6 0 0.80 1.18 6 -6 -1 21.99 2.11 6 6 1 28.46 1.74 6 6 2 1.88 0.96 -6 6 -3 201.48 6.49 -6 6 -3 198.07 4.95 -6 6 -4 4.43 0.73 -6 6 -4 4.94 1.45 6 -6 -4 4.75 1.52 6 -6 -5 102.78 4.43 -6 6 -5 100.92 4.18 -6 6 -6 17.96 1.98 6 -6 -6 15.77 2.05 -6 6 -7 48.49 2.25 -6 6 -7 48.70 2.85 6 -6 -7 47.64 3.01 6 -6 -8 3.53 1.61 -6 6 -8 4.04 1.18 -6 6 -8 1.11 1.37 -6 6 -9 26.04 1.85 -6 6 -9 22.94 2.06 6 -6 -9 24.76 2.40 -6 6 -10 4.15 1.40 6 -6 -10 4.62 1.63 -6 6 -10 3.02 0.84 -6 6 -10 3.71 1.30 6 6 10 2.45 1.01 -6 6 -11 219.33 5.34 -6 -6 11 213.77 7.61 6 -6 -11 219.35 7.08 6 6 11 217.52 6.44 -6 6 -11 227.24 6.73 -6 6 -11 224.63 6.64 6 6 12 -0.22 1.25 -6 6 -12 0.12 1.28 -6 6 -12 0.21 1.16 -6 -6 12 1.23 2.39 -6 6 -13 27.28 2.24 6 6 13 21.03 2.05 -6 6 -13 22.14 1.85 -6 -6 13 25.67 3.18 -6 6 -14 6.08 1.31 6 6 14 5.90 1.51 -6 6 -14 6.33 1.66 -6 6 -15 60.26 2.63 -6 -6 15 62.94 4.33 -6 6 -15 57.76 3.33 6 6 15 55.45 3.14 -6 -6 15 56.32 2.65 -6 6 -16 3.07 1.10 -6 6 -16 3.93 1.74 -6 -6 16 3.90 1.17 -6 -6 16 3.24 2.96 -6 6 -17 5.10 1.99 -6 6 -17 5.72 1.08 -6 -6 17 4.58 2.95 -6 6 -18 -0.17 1.84 -6 -6 18 3.19 2.97 -6 -6 19 137.70 6.50 -6 -6 20 2.87 3.39 -6 -6 21 8.27 3.47 -6 -6 22 6.09 3.70 6 8 -20 0.19 2.10 6 8 -19 0.92 2.01 -6 -8 -19 0.98 1.36 6 8 -18 1.95 1.84 -6 -8 -18 4.95 1.40 6 8 -17 1.70 1.78 -6 8 16 339.35 8.93 6 8 -16 323.19 9.85 -6 8 15 1.28 1.31 6 8 -15 -0.31 1.48 -6 8 14 73.57 3.24 -6 8 14 69.18 3.49 6 8 -14 65.35 3.48 -6 8 13 8.08 1.61 -6 8 13 6.05 1.52 6 8 -13 10.44 1.80 6 8 -12 9.40 1.55 -6 8 12 7.45 1.59 6 8 -11 3.94 1.40 -6 8 11 5.41 1.57 6 8 -10 2.14 1.25 -6 8 10 1.48 1.42 -6 8 9 1.52 1.41 6 -8 9 1.30 1.55 6 8 -9 1.98 1.17 6 8 -9 0.25 1.67 6 8 -8 943.47 21.98 6 8 -8 930.74 21.74 6 -8 8 920.15 21.94 -6 8 8 921.63 21.85 -6 8 7 0.79 1.42 6 8 -7 -0.83 1.80 6 8 -7 0.12 1.69 6 -8 7 0.81 1.40 6 8 -6 68.52 3.48 6 8 -6 71.44 3.45 6 -8 6 72.61 3.58 -6 8 6 76.09 3.55 6 8 -5 5.96 1.90 -6 8 5 6.53 1.65 6 -8 5 7.01 1.65 6 8 -5 4.96 1.66 6 -8 4 57.64 3.22 -6 8 4 50.39 3.03 6 8 -4 54.14 2.85 6 8 -3 6.60 1.59 -6 8 3 7.47 1.64 6 -8 3 8.12 1.58 -6 8 2 43.32 2.74 6 -8 2 43.97 2.83 6 8 -2 44.08 2.51 -6 8 1 1.45 1.28 6 -8 1 2.59 1.36 6 8 -1 1.20 1.26 6 -8 0 1354.95 31.46 6 8 0 1369.80 30.20 6 -8 -1 -0.31 1.31 -6 8 -2 40.72 2.76 -6 8 -3 10.42 1.76 6 -8 -4 57.08 3.38 -6 8 -4 51.98 3.11 -6 8 -5 3.28 0.65 -6 8 -5 6.89 1.64 6 -8 -5 5.37 1.72 6 -8 -6 69.71 3.74 -6 8 -6 70.57 3.58 6 -8 -7 2.94 1.67 -6 8 -7 2.87 1.53 -6 8 -8 957.13 22.58 6 -8 -8 960.78 23.16 -6 8 -9 2.70 1.47 6 -8 -9 3.58 1.77 -6 8 -9 4.30 1.39 -6 8 -10 2.09 1.39 -6 8 -10 1.98 1.43 6 -8 -10 1.29 1.67 -6 8 -11 4.75 1.49 6 -8 -11 3.78 1.78 -6 8 -11 7.74 1.55 -6 8 -11 4.79 1.10 6 -8 -12 5.12 1.73 -6 8 -12 6.40 1.07 -6 8 -12 8.60 1.60 6 8 12 5.34 1.36 -6 8 -12 7.12 1.49 6 -8 -13 10.39 1.94 -6 8 -13 6.99 1.11 -6 8 -13 12.88 1.92 -6 8 -13 12.64 1.68 6 8 13 8.94 1.71 -6 8 -14 67.12 3.62 6 8 14 70.77 3.42 6 -8 -14 68.07 3.67 -6 8 -14 68.80 3.03 -6 8 -15 1.11 1.57 -6 8 -15 -0.18 1.12 -6 8 -16 338.70 9.98 -6 8 -16 322.76 8.44 -6 8 -17 1.92 1.77 -6 8 -18 0.91 1.95 -6 8 -19 -0.94 2.07 -6 8 -20 -0.19 2.29 6 10 -19 22.28 2.86 -6 -10 -18 1.88 1.41 6 10 -18 2.09 1.89 6 10 -17 12.19 2.28 -6 -10 -17 9.74 1.86 6 10 -16 0.34 1.72 6 10 -15 195.47 6.94 -6 10 15 203.07 6.37 6 10 -14 1.83 1.69 -6 10 14 1.48 1.47 6 10 -13 3.97 1.55 -6 10 13 5.08 1.58 6 -10 12 1.91 1.57 6 10 -12 3.47 1.48 -6 10 12 2.04 1.39 6 10 -11 30.60 2.87 6 10 -11 37.63 2.56 -6 10 11 31.11 2.51 6 -10 11 39.83 2.71 -6 10 10 8.45 1.83 6 10 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10 -11 36.29 2.62 -6 10 -11 31.18 2.42 6 -10 -11 35.36 2.99 -6 10 -12 2.56 1.40 6 -10 -12 2.81 1.76 -6 10 -12 3.46 1.61 -6 10 -12 4.30 1.34 6 -10 -13 2.92 1.81 -6 10 -13 4.26 1.36 -6 10 -13 4.32 1.64 -6 10 -13 4.23 1.37 -6 10 -14 1.28 1.25 -6 10 -14 2.81 1.66 -6 10 -14 1.11 1.27 6 -10 -14 3.37 1.78 6 -10 -15 203.80 7.04 -6 10 -15 214.25 7.19 -6 10 -15 201.59 6.07 -6 10 -15 191.94 5.58 6 -10 -16 1.14 1.91 -6 10 -16 -0.35 1.75 -6 10 -17 5.59 2.08 -6 10 -18 1.77 2.15 -6 10 -19 21.94 2.92 -6 -12 -18 45.66 3.04 6 12 -18 48.41 3.61 -6 -12 -17 1.79 1.79 6 12 -17 4.35 2.13 -6 -12 -16 2.15 1.64 6 12 -16 4.15 1.91 6 12 -15 4.04 1.84 6 12 -14 4.05 1.86 -6 12 13 2.10 1.61 6 12 -13 2.53 1.72 6 -12 13 3.98 1.82 6 12 -12 407.46 11.30 6 -12 12 418.87 11.41 -6 12 12 405.23 11.21 -6 12 11 1.60 1.64 6 -12 11 -0.47 1.79 6 12 -11 -2.57 2.01 6 12 -10 72.43 3.81 6 -12 10 76.17 3.95 -6 12 10 70.43 3.66 6 -12 9 2.59 1.65 -6 12 9 5.79 1.68 6 12 -9 4.10 2.07 -6 12 8 5.03 1.69 6 12 -8 5.77 1.97 6 -12 8 7.08 1.74 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6.80 2.10 -6 12 -14 4.23 1.50 6 -12 -14 3.64 2.04 -6 12 -15 0.83 1.47 -6 12 -15 3.69 2.09 6 -12 -15 -0.75 1.95 -6 -12 15 0.92 1.39 -6 12 -16 0.56 2.00 6 -12 -16 3.10 2.03 -6 12 -17 2.76 2.25 6 -12 -17 5.18 2.10 -6 12 -18 47.05 3.86 6 -12 -18 44.13 3.44 -6 -14 -18 -0.17 1.88 6 14 -17 1.58 2.08 -6 -14 -17 0.85 1.81 -6 -14 -16 3.28 2.03 6 14 -16 2.79 2.05 -6 -14 -15 16.36 2.36 6 -14 15 19.54 2.52 6 14 -15 17.89 2.50 -6 -14 -14 2.16 1.95 6 14 -14 3.89 2.13 6 -14 14 1.91 1.80 6 -14 13 23.34 2.58 6 14 -13 25.35 2.68 6 -14 12 1.87 1.80 6 -14 11 261.92 8.47 6 14 -10 1.21 2.22 6 -14 10 2.46 1.86 6 14 -9 8.04 2.27 6 -14 9 5.54 1.96 -6 14 9 4.76 1.88 6 14 -8 2.18 2.08 -6 14 8 0.67 1.74 6 -14 8 3.45 1.84 6 14 -7 40.57 3.32 6 -14 7 35.22 2.92 6 14 -6 4.48 2.35 -6 14 6 2.23 1.76 6 -14 6 6.35 1.98 6 14 -6 4.95 1.98 6 14 -5 122.50 5.07 6 14 -5 118.54 5.33 -6 14 5 120.37 5.23 6 -14 5 116.70 5.35 6 14 -4 4.14 2.34 6 -14 4 -0.19 1.78 -6 14 4 0.36 1.72 6 14 -4 1.59 1.89 -6 14 3 261.69 8.65 6 -14 3 269.02 8.95 6 -14 2 1.20 1.66 -6 14 2 1.10 1.66 -6 14 1 30.79 2.93 6 -14 1 25.95 2.83 6 -14 0 1.64 1.83 6 -14 -1 25.77 2.77 -6 14 -2 4.32 1.96 -6 14 -3 262.23 8.71 6 -14 -4 0.65 1.85 -6 14 -4 -0.74 1.81 -6 14 -5 120.23 5.33 6 -14 -5 115.69 5.61 6 -14 -6 6.82 2.29 -6 14 -6 5.09 1.92 -6 14 -7 30.21 2.74 6 -14 -7 35.15 3.30 6 -14 -8 0.22 1.95 -6 14 -8 1.01 1.64 -6 14 -9 4.26 1.71 6 -14 -9 5.28 2.27 -6 14 -10 3.94 1.87 6 -14 -10 3.73 2.18 6 -14 -11 253.93 8.80 -6 14 -11 234.13 7.65 -6 14 -12 1.19 1.58 6 -14 -12 -2.60 2.41 6 -14 -13 19.29 2.86 -6 14 -13 17.37 2.11 -6 -14 14 3.14 1.67 -6 14 -14 6.79 2.13 6 -14 -14 4.65 2.20 -6 14 -14 6.28 1.76 -6 14 -15 20.38 2.78 6 -14 -15 16.41 2.79 -6 -14 15 19.46 2.16 -6 14 -16 2.93 2.11 6 -14 -16 2.89 2.35 6 -14 -17 -0.40 2.16 6 -14 -18 1.57 2.32 -6 -16 -17 2.46 2.24 -6 -16 -16 118.79 5.49 6 16 -15 2.16 2.13 -6 -16 -15 0.40 2.20 6 16 -14 40.60 3.40 6 -16 14 39.48 3.30 -6 -16 -14 37.54 3.31 6 16 -13 6.36 2.08 -6 -16 -13 4.42 2.13 6 -16 13 3.67 2.20 -6 -16 -12 5.71 2.17 6 -16 12 6.03 2.26 6 -16 11 -1.33 2.07 6 -16 10 5.03 2.05 6 -16 9 -0.39 2.01 6 -16 8 339.82 10.59 6 -16 7 -0.20 1.81 6 -16 6 41.17 3.41 6 -16 5 3.36 1.95 6 -16 4 15.37 2.56 6 -16 3 1.29 1.87 6 -16 2 6.76 2.23 6 -16 1 2.21 2.03 6 -16 0 468.33 13.74 6 -16 -1 0.23 1.88 6 -16 -2 3.46 2.10 6 -16 -5 3.09 2.14 6 -16 -6 40.64 3.67 6 -16 -7 -2.42 2.34 -6 16 -8 332.14 7.83 6 -16 -8 393.28 11.70 6 -16 -9 2.93 2.27 6 -16 -10 0.97 2.24 6 -16 -11 -0.72 2.24 6 -16 -12 8.81 2.64 -6 -16 12 6.80 2.01 6 -16 -13 5.68 2.63 -6 -16 13 5.09 1.97 -6 16 -14 39.67 3.50 6 -16 -14 48.19 4.15 -6 -16 14 42.39 3.13 6 -16 -15 0.23 2.36 -6 16 -15 1.47 2.52 6 -16 -16 121.59 6.05 6 -16 -17 1.79 2.62 -6 -18 -17 6.84 2.56 -6 -18 -16 1.71 2.35 -6 -18 -15 113.37 5.58 -6 -18 -14 1.54 2.23 6 -18 13 -1.61 2.37 -6 -18 -13 0.45 2.32 6 -18 12 2.25 2.23 -6 -18 -12 4.47 2.38 6 -18 11 19.35 2.94 -6 -18 -11 18.67 2.96 6 -18 10 -0.85 2.14 -6 -18 -10 1.82 2.15 -6 -18 -9 37.92 3.61 6 -18 9 44.10 3.77 6 -18 8 -1.09 2.26 6 -18 7 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-8 8 -7 4.71 1.89 8 -8 -7 4.90 2.04 -8 8 -8 1271.98 28.29 -8 8 -8 1253.28 29.56 8 -8 -8 1259.09 30.15 -8 8 -9 6.69 1.47 -8 8 -9 4.63 1.63 8 -8 -9 4.89 2.02 8 8 10 1.03 1.11 8 -8 -10 1.35 1.87 -8 8 -10 2.86 1.34 8 8 11 2.37 1.25 -8 8 -11 3.36 1.41 -8 8 -11 1.93 1.45 -8 8 -11 3.68 0.90 -8 8 -12 53.17 1.80 -8 8 -12 54.82 3.17 8 8 12 47.41 2.69 -8 8 -12 52.26 2.96 -8 8 -13 4.40 1.61 8 8 13 6.68 1.50 -8 8 -13 4.57 1.63 -8 8 -14 112.37 4.53 -8 8 -14 112.87 4.72 8 8 14 111.30 4.49 -8 8 -15 1.87 1.73 -8 8 -15 5.76 1.69 -8 8 -16 334.56 9.17 -8 8 -16 328.56 9.87 -8 8 -17 3.71 1.88 -8 8 -18 -0.70 1.95 -8 8 -19 -0.18 2.03 8 10 -18 -0.18 1.98 8 10 -17 18.34 2.40 8 10 -16 2.18 1.92 -8 10 15 191.52 6.37 8 10 -15 185.40 6.64 -8 10 14 7.67 1.87 8 10 -14 9.15 1.93 -8 10 13 27.42 2.57 8 10 -13 33.16 2.58 8 10 -12 0.52 1.35 -8 10 12 0.91 1.65 -8 10 11 107.57 4.70 8 10 -11 106.54 4.28 8 10 -10 9.57 1.60 -8 10 10 6.68 1.90 8 10 -9 156.31 5.21 8 10 -9 162.44 5.97 -8 10 9 155.59 5.95 -8 10 8 3.44 1.89 8 -10 8 3.90 1.91 8 10 -8 3.07 1.89 8 10 -8 -0.88 2.01 8 10 -7 467.08 12.65 8 10 -7 473.37 12.67 8 -10 7 474.87 13.12 -8 10 7 460.78 12.86 8 10 -6 19.18 2.65 8 10 -6 18.10 2.44 8 -10 6 17.08 2.46 -8 10 6 17.93 2.31 8 -10 5 125.43 5.52 -8 10 5 134.81 5.53 8 10 -5 126.03 5.01 -8 10 4 7.45 2.00 8 -10 4 4.51 1.94 8 10 -4 7.67 1.96 8 10 -3 199.03 6.41 8 -10 3 193.90 7.22 -8 10 3 188.00 7.01 8 10 -2 8.94 2.00 8 10 -2 9.56 2.50 -8 10 2 8.75 2.08 8 -10 2 8.80 2.12 -8 10 1 476.33 13.14 8 -10 1 460.08 13.26 8 10 -1 465.44 12.56 8 10 -1 450.66 11.87 8 10 0 3.56 1.82 8 -10 0 3.86 2.00 8 10 1 473.27 11.97 8 -10 -1 469.58 13.59 -8 10 -2 7.37 2.11 8 10 2 10.89 1.88 -8 10 -3 191.01 7.19 8 10 3 190.59 5.98 -8 10 -3 198.48 5.42 8 -10 -4 5.70 2.14 -8 10 -4 8.42 2.08 -8 10 -4 6.98 1.11 -8 10 -5 136.21 5.75 8 -10 -5 126.50 5.85 -8 10 -5 131.27 3.69 8 -10 -6 13.28 2.43 -8 10 -6 10.00 2.21 8 -10 -7 458.38 13.41 -8 10 -7 462.78 12.92 8 -10 -8 3.13 2.09 -8 10 -8 2.08 1.79 -8 10 -9 166.22 5.46 -8 10 -9 156.58 6.10 8 -10 -9 159.72 6.60 -8 10 -10 5.20 1.73 -8 10 -10 8.27 1.78 8 -10 -10 5.35 2.14 -8 10 -11 123.36 4.74 -8 10 -11 107.80 4.85 8 -10 -11 119.34 5.55 -8 10 -12 1.96 1.16 8 -10 -12 -0.20 2.09 -8 10 -12 0.30 1.65 -8 10 -12 3.41 1.55 8 10 12 -0.11 1.27 -8 10 -13 27.61 1.65 8 -10 -13 28.26 3.07 -8 10 -13 31.54 2.56 -8 10 -13 26.56 2.54 -8 10 -14 7.41 2.03 -8 10 -14 5.88 1.09 -8 10 -14 6.84 1.87 -8 10 -15 203.82 7.05 -8 10 -15 197.47 6.51 -8 10 -16 2.97 1.94 -8 10 -17 19.97 2.62 -8 10 -18 3.54 2.04 8 12 -17 4.40 2.26 8 12 -16 12.18 2.28 8 12 -15 -1.17 1.78 8 12 -14 1.26 1.76 8 12 -13 7.19 1.81 8 12 -12 379.65 10.62 8 -12 11 2.91 1.92 8 12 -11 2.36 1.58 8 12 -10 65.18 3.24 8 -12 10 53.91 3.72 -8 12 9 2.41 1.94 8 -12 9 4.08 2.08 8 -12 8 67.54 4.00 -8 12 8 66.32 3.92 8 -12 7 5.37 2.08 -8 12 7 0.18 1.75 -8 12 6 10.29 2.18 8 12 -6 15.48 2.31 8 -12 6 11.76 2.23 8 12 -6 13.33 2.44 -8 12 5 1.89 1.79 8 12 -5 3.42 2.21 8 12 -5 2.06 1.85 8 -12 5 4.61 2.09 8 12 -4 864.54 21.44 8 12 -4 874.31 21.03 8 -12 4 878.22 22.20 -8 12 4 883.84 21.90 -8 12 3 3.08 1.99 8 -12 3 2.29 2.03 8 12 -3 4.11 1.99 8 12 -2 53.55 3.20 8 -12 2 55.44 3.81 -8 12 2 46.94 3.48 -8 12 1 6.34 2.19 8 -12 1 4.94 2.12 8 12 -1 4.09 1.86 8 -12 0 120.82 5.65 8 12 0 114.53 4.61 8 12 1 5.74 1.83 8 -12 -1 3.07 2.19 -8 12 -2 49.49 3.59 -8 12 -3 0.60 1.85 -8 12 -4 881.24 22.10 8 -12 -4 867.32 22.49 -8 12 -5 2.36 1.95 8 -12 -5 0.91 2.13 -8 12 -5 0.67 0.90 -8 12 -6 10.35 1.01 8 -12 -6 12.37 2.58 8 -12 -7 3.66 2.17 -8 12 -7 4.22 1.95 -8 12 -8 76.77 4.22 8 -12 -8 69.13 4.51 8 -12 -9 3.85 2.21 -8 12 -9 3.22 1.90 -8 12 -10 62.59 3.86 8 -12 -10 59.36 4.17 8 -12 -11 0.66 2.17 -8 12 -11 3.40 1.78 -8 12 -11 -0.17 1.78 -8 12 -12 410.45 11.11 -8 12 -12 377.99 11.06 8 -12 -12 375.00 11.88 -8 12 -13 3.83 1.81 -8 12 -13 6.31 1.53 -8 12 -13 5.88 2.04 8 -12 -13 4.73 2.49 -8 12 -14 0.17 1.71 -8 12 -14 1.16 1.70 8 -12 -14 1.28 2.06 8 -12 -15 0.63 2.25 -8 12 -15 1.06 1.98 -8 12 -16 19.97 2.77 -8 12 -17 4.23 2.25 -8 -14 -17 4.29 2.18 8 14 -16 -0.55 1.95 8 14 -15 23.95 2.71 8 14 -14 0.33 1.84 8 14 -13 46.54 3.27 8 14 -12 4.71 1.95 8 -14 12 2.12 2.00 8 -14 11 210.51 7.59 8 14 -11 201.27 6.88 8 -14 10 11.83 2.49 8 -14 9 24.04 2.94 8 -14 8 0.61 2.01 8 -14 7 54.41 3.92 8 -14 6 7.88 2.30 8 -14 5 186.91 7.35 8 -14 4 2.84 2.19 8 -14 3 296.47 9.96 8 -14 2 7.01 2.24 8 14 -2 8.72 2.21 8 14 -1 50.77 3.36 8 -14 1 48.48 3.82 8 14 0 5.04 2.13 8 -14 0 3.03 2.08 8 -14 -1 47.22 3.78 8 -14 -4 0.24 1.96 8 -14 -5 183.71 7.64 -8 14 -6 2.48 0.90 8 -14 -6 2.71 2.41 8 -14 -7 48.37 3.96 8 -14 -8 -0.25 2.26 8 -14 -9 29.52 3.34 8 -14 -10 6.11 2.56 8 -14 -11 191.02 7.88 -8 14 -12 5.11 2.27 8 -14 -12 2.62 2.33 -8 14 -13 51.84 3.57 8 -14 -13 48.28 4.05 -8 14 -14 2.74 2.25 8 -14 -14 1.15 2.49 -8 14 -15 24.30 2.91 8 -14 -15 22.25 3.25 -8 14 -16 1.58 2.15 8 -14 -16 -0.23 2.49 -8 -16 -17 3.05 2.44 -8 -16 -16 98.82 5.15 -8 -16 -15 0.64 2.26 8 16 -14 22.34 2.85 8 -16 13 3.05 2.25 8 16 -13 4.40 2.05 8 -16 12 22.79 3.03 8 16 -12 20.06 2.64 8 -16 11 -0.21 2.19 8 -16 10 1.91 2.14 8 -16 9 5.45 2.38 8 -16 8 292.89 9.90 8 -16 7 4.73 2.41 8 -16 6 28.91 3.13 8 -16 5 5.55 2.30 8 -16 4 43.40 3.71 8 -16 3 4.07 2.30 8 -16 2 21.19 3.07 8 -16 1 0.74 2.27 8 -16 0 430.35 13.38 8 -16 -1 -0.25 2.24 8 -16 -4 39.97 3.81 8 -16 -5 2.91 2.39 8 -16 -6 36.64 3.82 8 -16 -7 1.06 2.44 -8 16 -7 -0.52 0.86 8 -16 -8 303.64 10.74 8 -16 -9 6.35 2.92 8 -16 -10 3.42 2.70 8 -16 -11 2.37 2.52 8 -16 -12 24.97 3.69 -8 16 -13 2.32 2.28 8 -16 -13 4.36 3.10 -8 16 -14 20.61 3.10 8 -16 -14 25.87 3.69 8 -16 -15 0.49 2.67 8 -16 -16 95.10 5.57 8 -16 -17 1.67 2.70 8 -18 13 7.34 2.80 8 -18 12 1.54 2.40 8 -18 11 9.90 2.74 8 -18 10 1.61 2.54 8 -18 9 59.60 4.43 8 -18 8 -1.91 2.68 8 -18 7 123.28 6.13 8 -18 6 0.74 2.36 8 -18 5 10.22 2.70 8 -18 4 1.02 2.44 8 -18 3 12.92 2.85 8 -18 2 -0.26 2.48 8 -18 1 114.84 6.14 8 -18 0 -0.27 2.40 8 -18 -1 108.71 6.02 8 -18 -2 -1.39 2.50 8 -18 -4 -2.26 2.53 8 -18 -5 15.11 3.24 8 -18 -6 0.86 2.41 8 -18 -7 120.12 6.58 8 -18 -8 -0.29 2.74 8 -18 -9 59.23 4.79 8 -18 -10 0.57 2.73 8 -18 -11 8.74 3.02 8 -18 -12 0.84 2.95 -8 -18 13 3.50 2.36 8 -20 9 2.01 2.81 8 -20 8 18.03 3.42 8 -20 7 0.78 2.64 8 -20 6 1.05 2.71 8 -20 5 3.49 2.80 8 -20 4 134.66 6.86 8 -20 3 3.33 2.82 8 -20 2 4.51 2.66 8 -20 1 2.00 2.76 8 -20 0 24.11 3.58 8 -20 -1 0.59 2.75 8 -20 -2 13.12 3.23 8 -20 -4 131.24 6.97 -8 -20 10 11.51 2.83 -9 1 18 4.84 2.69 -9 1 18 2.10 2.89 -9 -1 -17 1.56 1.56 -9 1 17 1.72 2.55 -9 1 17 2.05 2.66 -9 -1 -16 1.13 1.41 -9 1 16 3.13 2.40 -9 1 16 1.33 2.67 -9 1 15 16.40 2.92 -9 -1 -15 21.78 2.22 -9 1 15 20.28 2.12 -9 1 15 15.08 3.09 -9 1 14 5.17 2.39 -9 -1 -14 8.12 1.80 -9 1 14 5.27 1.72 9 -1 14 6.69 1.29 -9 1 14 1.04 2.49 -9 1 13 4.43 2.32 -9 -1 -13 8.96 1.76 -9 1 13 7.27 1.67 9 -1 13 7.08 1.27 -9 1 13 5.45 2.60 9 -1 12 3.09 1.15 -9 1 12 -0.19 2.39 -9 1 12 3.17 2.01 -9 1 12 3.03 1.55 -9 -1 -12 3.12 1.52 9 -1 11 -0.06 1.14 -9 1 11 1.13 2.37 -9 -1 -11 0.58 1.59 -9 1 11 1.47 1.34 9 -1 10 4.76 1.28 -9 1 10 3.62 2.17 -9 1 10 2.86 1.52 -9 -1 -10 6.72 1.73 9 -1 9 4.50 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10 37.38 2.21 -10 0 10 36.85 2.95 -10 0 -10 33.86 2.89 10 0 11 1.46 1.35 -10 0 11 -0.21 2.36 -10 0 -11 1.76 1.58 -10 0 11 2.70 1.67 10 0 12 5.34 1.44 -10 0 12 3.90 2.71 -10 0 -12 4.26 1.88 -10 0 12 2.95 1.74 10 0 13 3.65 1.46 -10 0 13 2.02 2.67 -10 0 -13 2.62 1.72 -10 0 13 2.71 1.76 -10 0 13 0.21 2.36 -10 0 14 70.49 4.85 -10 0 14 78.50 3.94 -10 0 14 78.91 4.71 -10 0 -14 79.19 3.94 -10 0 15 -0.22 2.50 -10 0 15 -3.33 2.97 -10 0 -15 0.14 1.68 -10 0 15 1.58 1.69 -10 0 16 142.82 6.97 -10 0 16 146.51 6.68 -10 0 -16 155.89 5.58 -10 0 17 -0.23 2.62 -10 0 17 -0.50 3.04 -10 2 17 6.03 2.63 -10 2 17 5.57 3.00 -10 2 16 -0.24 2.94 -10 -2 -16 2.45 1.72 -10 2 16 -1.31 2.47 -10 2 15 66.73 3.55 -10 2 15 67.41 4.44 -10 -2 -15 63.56 3.49 -10 2 14 1.25 2.28 -10 -2 -14 2.13 1.67 -10 2 14 2.52 1.73 -10 2 14 -0.67 2.59 -10 2 13 8.70 2.44 -10 -2 -13 13.53 2.28 -10 2 13 10.57 2.01 -10 2 13 9.48 2.76 10 -2 12 1.51 0.86 -10 2 12 -0.62 2.47 -10 -2 -12 5.68 2.00 -10 2 12 2.56 1.84 -10 -2 -11 38.21 3.05 -10 2 11 38.06 2.95 10 -2 11 36.41 1.72 -10 2 10 5.41 1.82 10 -2 10 4.23 1.03 10 -2 9 32.08 1.75 -10 2 9 35.66 3.09 -10 2 9 31.86 2.73 -10 2 8 3.93 2.22 -10 2 8 3.99 1.80 -10 2 8 4.95 2.00 -10 2 7 56.17 3.77 -10 2 7 61.12 3.70 -10 2 7 65.60 3.71 -10 2 6 6.83 1.96 -10 2 6 3.68 2.24 -10 2 5 23.73 2.59 -10 2 5 19.61 2.69 -10 2 4 6.38 2.01 -10 2 4 5.71 2.27 -10 2 3 14.71 2.29 -10 2 3 15.72 2.41 -10 2 2 6.37 1.91 10 2 -2 4.82 1.69 -10 -2 -1 55.77 2.73 -10 2 1 50.67 2.94 -10 2 1 50.95 3.41 -10 2 1 49.56 3.18 10 2 -1 51.92 2.98 -10 2 0 14.01 2.37 10 2 0 10.45 1.90 -10 -2 0 11.53 1.70 -10 2 0 8.26 1.67 -10 2 0 12.89 2.26 -10 2 -1 50.40 2.66 -10 -2 1 52.93 2.92 10 2 1 59.07 2.99 -10 2 -2 8.86 1.46 10 2 2 10.34 1.94 -10 -2 2 10.20 1.98 -10 2 -3 18.86 1.64 -10 -2 3 21.20 2.28 -10 2 -3 25.11 2.68 10 2 3 22.60 2.22 -10 -2 4 8.57 2.46 10 2 4 3.69 1.64 -10 2 -4 5.51 1.14 -10 -2 4 4.91 1.95 -10 2 -4 5.44 1.95 10 2 5 18.48 2.17 -10 -2 5 19.90 2.78 -10 2 -5 15.67 1.23 -10 -2 5 19.09 2.46 -10 2 -5 16.65 2.36 10 2 6 5.31 1.92 -10 2 -6 2.79 1.91 -10 -2 6 6.52 2.08 -10 -2 6 2.25 2.13 -10 -2 7 54.42 3.64 10 2 7 59.24 3.05 -10 -2 7 54.43 3.55 -10 2 -7 49.49 3.42 10 2 8 6.01 1.84 -10 2 -8 5.65 1.94 -10 -2 8 6.74 2.01 -10 -2 8 4.45 2.12 -10 -2 9 33.57 3.41 10 2 9 37.92 2.61 -10 -2 9 38.66 3.37 -10 -2 9 33.57 2.98 -10 2 -9 32.49 2.92 -10 2 -10 8.24 1.99 -10 -2 10 6.52 1.89 -10 -2 10 12.54 3.06 10 2 10 12.66 2.11 10 2 11 45.10 2.83 -10 -2 11 46.72 4.00 -10 -2 11 42.50 3.21 -10 2 -11 41.63 3.10 -10 -2 12 5.06 2.90 10 2 12 7.56 1.87 -10 2 -12 3.31 1.70 -10 -2 12 2.42 1.73 -10 -2 13 10.66 3.25 -10 -2 13 12.46 2.75 -10 -2 13 9.28 1.97 -10 2 -13 11.05 2.06 -10 -2 14 3.17 2.99 -10 -2 14 2.06 1.76 -10 2 -14 1.49 1.55 -10 -2 14 1.30 2.37 -10 2 -15 58.93 3.42 -10 -2 15 58.11 4.68 -10 -2 15 65.26 4.59 -10 -2 16 2.04 2.65 -10 2 -16 -0.55 1.65 -10 -2 16 0.77 3.19 -10 -2 17 10.30 2.88 -10 -2 17 3.66 3.35 -10 4 17 2.91 2.54 -10 4 17 0.24 2.87 -10 4 16 2.60 2.49 -10 -4 -16 5.03 1.80 -10 4 16 0.69 2.62 -10 -4 -15 2.09 1.90 -10 4 15 -1.26 2.41 -10 4 15 2.35 1.62 -10 4 15 1.74 1.70 -10 4 15 0.67 2.49 -10 4 14 11.05 2.58 -10 4 14 9.12 2.71 -10 4 14 13.38 2.06 -10 4 14 12.55 1.88 -10 4 13 0.84 2.34 -10 4 13 1.21 1.45 -10 4 13 0.16 1.62 -10 4 12 243.70 7.90 -10 4 12 243.11 7.00 -10 4 11 0.57 1.24 -10 4 11 -1.15 1.70 -10 4 10 93.42 3.40 -10 4 10 86.40 4.30 -10 4 9 0.71 2.05 -10 4 9 3.28 1.09 -10 4 9 4.43 1.87 -10 4 8 15.19 1.30 -10 4 8 18.96 2.43 -10 4 7 3.00 0.91 -10 4 7 1.30 2.13 -10 4 7 1.78 1.73 -10 4 6 68.53 3.86 -10 4 6 71.10 2.49 -10 4 6 76.66 4.14 -10 4 5 -0.04 0.66 -10 4 5 1.98 1.92 -10 4 4 332.59 9.66 10 4 -4 340.86 9.57 -10 4 4 333.24 7.71 -10 4 4 340.02 10.29 -10 4 3 -0.53 1.96 -10 4 3 1.02 0.51 10 4 -3 -1.16 1.85 -10 4 3 -1.09 1.85 10 4 -2 105.14 4.43 -10 4 2 98.18 4.29 -10 4 2 106.08 2.55 -10 4 2 108.78 4.99 -10 4 1 4.23 1.85 -10 4 1 4.63 1.93 10 4 -1 1.12 1.97 10 4 0 49.02 3.05 -10 4 0 50.00 2.98 -10 4 0 48.49 3.40 -10 4 -1 2.82 1.90 10 4 1 0.61 1.87 -10 4 -2 107.57 2.63 10 4 2 107.12 4.48 -10 4 -2 104.73 4.14 -10 4 -3 0.74 1.92 10 4 3 2.69 2.02 10 4 3 1.85 0.47 -10 4 -3 1.12 0.50 -10 -4 4 325.58 9.50 10 4 4 347.24 9.30 10 4 4 314.62 7.37 -10 4 -4 335.34 7.60 -10 4 -4 323.41 10.08 -10 -4 5 2.29 2.04 -10 4 -5 0.73 1.82 10 4 5 3.24 2.06 10 4 5 0.68 0.61 -10 4 -5 -0.44 0.73 -10 -4 6 74.57 4.03 -10 4 -6 67.22 2.38 10 4 6 76.85 3.76 10 4 6 69.83 2.36 -10 4 -6 75.37 2.58 -10 4 -6 73.73 4.08 -10 4 -7 3.90 0.77 -10 -4 7 3.43 2.26 -10 4 -7 3.98 0.93 10 4 7 7.01 2.20 10 4 7 4.73 0.95 -10 4 -7 4.10 1.97 10 4 8 13.43 1.28 -10 -4 8 14.62 2.98 10 4 8 17.50 2.37 -10 4 -8 11.69 1.27 -10 -4 8 13.75 2.48 -10 4 -8 9.18 2.09 -10 -4 9 6.45 2.50 10 4 9 6.94 1.18 -10 4 -9 3.47 1.97 10 4 10 86.20 3.31 -10 -4 10 84.77 5.10 -10 4 -10 87.19 4.39 -10 -4 10 88.87 4.64 -10 -4 11 3.39 2.93 10 4 11 1.40 1.28 -10 4 -11 -0.67 1.78 -10 -4 11 0.93 1.75 10 4 12 226.80 6.67 -10 4 -12 228.30 7.59 -10 -4 12 231.40 7.91 -10 -4 12 238.15 8.94 -10 -4 13 1.97 2.51 -10 4 -13 0.78 1.69 -10 -4 13 0.73 3.09 10 4 13 1.20 1.37 -10 -4 13 2.28 1.79 -10 -4 14 11.69 2.94 -10 4 -14 12.77 2.07 -10 -4 14 14.96 3.46 10 4 14 11.95 1.77 -10 -4 14 12.22 2.08 -10 -4 15 6.93 3.43 -10 -4 15 1.15 2.66 10 4 15 2.58 1.63 -10 4 -15 2.60 1.67 -10 -4 16 6.56 3.36 -10 -4 16 6.14 2.86 -10 4 -16 3.47 1.62 -10 -4 17 3.48 3.51 -10 -4 17 3.84 2.94 -10 6 16 2.60 2.69 -10 6 15 34.06 3.65 -10 6 14 7.40 1.80 -10 6 14 6.48 1.92 -10 6 13 15.10 2.27 -10 6 13 19.05 1.97 10 6 -12 0.42 1.17 -10 6 12 2.12 1.75 -10 6 12 2.40 1.33 -10 6 11 92.86 3.59 10 6 -11 87.07 3.50 -10 6 11 97.32 4.53 10 6 -10 1.64 1.04 -10 6 10 1.26 1.11 -10 6 10 3.23 1.79 -10 6 10 1.54 2.17 10 6 -9 11.57 1.31 -10 6 9 10.02 1.31 -10 6 9 11.13 2.36 -10 6 9 8.86 2.03 -10 6 8 1.21 1.92 -10 6 8 3.48 1.00 10 6 -8 2.67 0.94 -10 6 8 3.50 1.79 -10 6 7 25.25 1.54 10 6 -7 23.99 1.53 -10 6 7 25.82 2.68 -10 6 7 21.08 2.57 -10 6 6 8.38 1.00 10 6 -6 9.24 1.97 -10 6 6 6.09 2.08 10 6 -6 9.32 1.09 -10 6 6 8.01 2.03 -10 6 5 44.18 3.28 10 6 -5 43.50 1.82 -10 6 5 40.96 2.97 10 6 -5 47.39 3.15 10 6 -4 9.19 0.91 -10 6 4 10.27 2.25 10 6 -4 3.76 1.96 -10 6 4 9.20 2.00 -10 6 3 74.84 3.73 10 6 -3 76.43 3.97 10 6 -3 79.99 2.42 -10 6 2 1.72 1.93 10 6 -2 2.65 1.99 10 6 -2 6.33 0.73 -10 6 2 4.76 1.91 -10 6 1 13.75 2.07 10 6 -1 16.17 2.46 -10 6 1 18.08 2.51 10 6 0 0.69 2.00 -10 6 0 0.66 1.73 -10 6 0 1.17 1.94 -10 6 -1 7.88 1.86 10 6 1 7.30 2.32 -10 6 -2 3.76 1.78 10 6 2 5.22 2.27 -10 6 -2 3.32 1.98 -10 6 -3 83.13 2.60 -10 6 -3 84.44 4.52 -10 6 -3 79.79 3.45 10 6 3 79.74 4.13 10 6 4 12.50 2.44 -10 6 -4 10.17 1.07 10 6 4 8.29 0.85 -10 6 -4 10.64 2.29 -10 6 -5 46.13 1.97 -10 6 -5 43.23 3.33 10 6 5 50.21 3.34 10 6 5 45.24 1.82 10 6 6 13.52 1.18 -10 6 -6 16.09 1.32 -10 6 -6 16.43 2.52 -10 6 -7 29.37 1.76 10 6 7 28.23 1.64 -10 6 -7 26.13 2.84 10 6 8 4.50 1.10 -10 6 -8 4.59 1.16 -10 6 -8 2.02 1.77 -10 6 -9 9.52 2.25 10 6 9 6.80 1.27 -10 6 -9 7.25 1.36 -10 6 -9 6.20 0.57 -10 6 -10 -0.10 1.15 10 6 10 0.72 1.04 -10 6 -10 0.70 1.75 -10 6 -11 85.08 3.58 10 6 11 82.53 3.35 -10 6 -11 86.71 4.35 10 6 12 1.02 1.22 -10 6 -12 -0.16 1.78 -10 6 -12 0.94 1.37 -10 -6 13 14.64 2.40 10 6 13 15.25 1.77 -10 6 -13 14.16 2.25 -10 6 -13 13.76 1.82 -10 6 -14 5.39 1.90 10 6 14 6.50 1.67 -10 -6 14 6.55 2.13 -10 -6 15 42.66 4.66 -10 6 -15 32.71 2.73 -10 -6 16 9.21 4.00 -10 -6 17 9.38 4.21 10 8 -15 -2.04 1.63 10 8 -14 51.61 3.04 10 8 -13 6.19 1.56 -10 8 13 6.53 1.67 10 8 -12 5.70 1.48 -10 8 12 10.03 1.71 -10 8 11 1.76 1.31 -10 8 11 1.72 1.77 10 8 -11 2.32 1.28 -10 8 10 14.60 2.22 -10 8 10 17.04 1.70 10 8 -10 14.27 1.60 -10 8 9 -0.18 1.06 -10 8 9 1.79 1.89 10 8 -9 1.23 1.15 -10 8 8 249.77 8.36 10 8 -8 247.82 6.80 10 8 -7 1.23 0.95 -10 8 7 2.04 1.81 10 8 -6 81.88 2.94 -10 8 6 76.80 4.25 10 8 -6 74.13 4.03 10 8 -5 0.60 2.08 10 8 -5 3.79 0.98 -10 8 5 1.72 1.90 -10 8 4 5.05 1.92 -10 8 4 7.34 1.92 10 8 -4 3.65 2.00 -10 8 3 1.32 1.72 10 8 -3 1.65 2.07 10 8 -3 2.25 1.74 -10 8 3 2.16 1.87 -10 8 2 68.37 4.19 10 8 -2 69.76 3.53 -10 8 2 67.41 3.39 10 8 -2 69.10 3.94 -10 8 1 -0.80 1.67 10 8 -1 -0.72 1.72 -10 8 1 1.20 1.90 10 8 -1 2.88 2.25 -10 8 0 328.96 9.08 10 8 0 333.18 9.94 10 8 0 354.37 9.36 10 8 1 -0.67 1.53 10 8 1 2.55 2.31 -10 8 -1 -0.10 1.54 10 8 2 76.30 3.31 10 8 2 75.40 4.05 -10 8 -2 68.90 3.14 10 8 3 6.72 2.54 -10 8 -3 5.18 1.64 -10 8 -3 3.23 1.97 10 8 3 2.69 1.51 -10 8 -4 9.27 1.65 10 8 4 10.65 2.59 10 8 4 5.99 1.55 -10 8 -4 7.45 2.16 10 8 5 3.33 1.40 -10 8 -5 5.21 2.03 -10 8 -6 86.20 3.15 -10 8 -6 86.14 4.63 10 8 6 79.88 3.17 10 8 7 -0.30 1.15 -10 8 -7 3.26 1.17 -10 8 -7 0.98 1.84 -10 8 -8 255.92 7.12 10 8 8 252.83 6.89 10 8 8 264.11 6.76 -10 8 -8 273.94 8.84 -10 8 -9 3.17 1.94 -10 8 -9 3.27 1.36 10 8 9 0.95 0.98 10 8 9 1.07 1.07 -10 8 -10 16.17 2.43 -10 8 -10 15.71 1.75 10 8 10 13.33 1.48 10 8 10 14.32 1.26 10 8 11 1.75 1.28 -10 8 -11 2.25 1.37 -10 8 -11 3.53 1.85 -10 8 -12 4.35 1.60 10 8 12 4.48 1.40 -10 8 -12 3.07 1.83 10 8 13 4.97 1.63 -10 8 -13 7.09 1.99 -10 8 -13 5.73 1.66 -10 8 -14 58.86 3.54 -10 8 -14 59.78 3.33 -10 8 -15 0.30 1.76 -10 8 -15 -1.22 1.73 -10 8 -16 98.43 4.53 10 10 -18 4.38 1.95 10 10 -17 4.60 1.87 10 10 -16 -0.31 1.72 10 10 -15 78.46 3.91 10 10 -14 0.14 1.58 10 10 -13 2.30 1.65 10 10 -12 4.30 1.59 -10 10 12 3.13 1.52 10 10 -11 22.50 2.06 -10 10 11 22.41 2.10 10 10 -10 8.40 1.50 10 10 -9 33.20 2.22 10 10 -8 4.05 1.37 10 10 -7 123.45 4.19 10 10 -5 6.36 2.10 10 10 -4 2.05 1.94 10 10 -3 15.61 2.25 10 10 -2 3.28 1.83 10 10 -2 8.58 2.37 10 -10 2 8.35 2.37 -10 10 2 6.69 2.24 10 10 -1 84.02 4.49 -10 10 1 84.07 3.81 -10 10 1 82.60 4.66 10 -10 1 90.89 5.09 10 10 -1 84.81 4.06 10 10 0 9.62 2.65 -10 10 0 2.67 1.55 10 10 0 5.77 1.77 10 -10 0 7.17 2.33 -10 10 -1 87.36 3.56 10 10 1 86.69 4.57 10 -10 -1 89.89 5.16 10 10 1 85.40 3.92 10 10 2 11.91 2.73 -10 10 -2 6.63 1.62 -10 10 -2 9.45 2.37 10 10 2 11.61 2.00 -10 10 -3 21.98 1.91 10 10 3 17.61 1.95 -10 10 -3 21.91 2.76 10 -10 -4 3.71 2.33 10 10 4 1.15 1.53 -10 10 -4 2.78 1.98 -10 10 -4 3.50 1.41 10 -10 -5 3.47 2.25 10 10 5 3.88 1.59 -10 10 -5 5.92 2.31 -10 10 -5 8.09 1.39 10 -10 -6 1.98 2.27 10 10 6 2.08 1.47 -10 10 -6 2.71 2.10 -10 10 -7 130.27 4.46 10 -10 -7 139.30 6.38 -10 10 -7 125.74 5.78 10 10 7 120.86 4.25 10 10 8 1.74 1.41 -10 10 -8 3.70 1.46 -10 10 -8 3.80 2.13 -10 10 -9 39.23 2.52 -10 10 -9 41.22 3.49 10 10 9 33.63 2.10 -10 10 -10 15.18 1.84 -10 10 -10 9.29 2.33 10 10 10 12.52 1.62 10 10 11 22.05 1.95 -10 10 -11 25.62 2.23 -10 10 -12 4.28 0.93 10 10 12 0.45 1.42 -10 10 -12 4.10 1.71 -10 10 -13 0.14 1.61 -10 10 -14 1.22 1.76 -10 10 -15 84.19 4.29 -10 10 -16 -0.66 1.86 -10 10 -17 6.30 2.21 -10 10 -18 2.28 2.22 10 12 -17 2.36 1.93 10 12 -16 0.16 2.02 10 12 -15 0.16 1.76 10 12 -14 0.45 1.70 10 12 -13 0.43 1.64 10 12 -12 134.30 5.06 10 12 -11 2.14 1.54 10 12 -10 67.50 3.33 10 12 -9 6.62 1.64 10 12 -8 10.96 1.67 10 -12 6 16.59 2.75 10 -12 5 4.16 2.38 10 -12 4 267.49 9.45 10 -12 3 1.66 2.22 10 12 -2 55.23 3.47 10 -12 2 57.83 4.24 10 12 -1 1.70 2.03 10 -12 1 3.41 2.22 10 12 0 10.89 2.20 10 -12 0 5.94 2.33 10 12 1 3.54 1.82 -10 12 -1 0.87 1.54 10 -12 -1 1.50 2.13 -10 12 -2 55.01 2.81 10 12 2 60.19 3.33 -10 12 -3 -1.64 1.51 10 12 3 1.22 1.72 -10 12 -4 247.64 6.74 10 -12 -4 231.60 9.19 -10 12 -5 3.45 1.28 10 12 5 2.70 1.71 10 -12 -5 2.57 2.46 10 12 6 16.96 2.02 10 -12 -6 19.30 3.02 10 12 7 3.51 1.60 10 -12 -7 6.16 2.55 10 12 8 7.10 1.70 10 -12 -8 4.11 2.52 -10 12 -9 8.17 1.86 10 -12 -9 6.15 2.71 10 -12 -10 66.40 4.70 -10 12 -10 66.76 3.50 -10 12 -11 3.97 1.82 -10 12 -12 144.88 5.51 -10 12 -13 3.89 1.95 -10 12 -14 0.16 1.98 -10 12 -15 0.51 2.12 -10 12 -16 3.41 2.21 10 14 -15 15.36 2.44 10 14 -14 1.92 1.91 10 14 -13 15.16 2.41 10 14 -12 2.61 1.79 10 14 -11 104.14 4.51 10 14 -10 1.77 1.71 10 -14 8 1.16 2.33 10 -14 7 19.20 2.96 10 -14 6 4.02 2.33 10 -14 5 59.72 4.35 10 -14 4 2.45 2.33 10 -14 3 105.65 5.66 10 -14 2 2.02 2.36 10 -14 1 15.91 3.03 10 -14 0 2.34 2.41 10 -14 -1 14.82 3.00 10 14 2 3.47 2.12 10 14 3 100.28 4.50 -10 14 -3 117.68 4.09 10 14 4 -0.13 1.83 -10 14 -4 -1.03 1.49 10 -14 -4 -2.17 2.49 -10 14 -5 63.76 2.57 10 14 5 54.32 3.26 10 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168.02 4.34 -12 6 4 2.15 2.27 -12 6 4 2.55 0.66 -12 6 3 281.78 8.82 -12 6 3 284.10 6.40 -12 6 2 18.86 2.56 12 6 -1 156.31 5.89 -12 6 1 153.39 5.81 -12 6 0 10.86 2.26 12 6 0 5.15 2.17 12 6 1 156.81 5.98 -12 6 -1 163.99 5.72 12 6 2 11.96 2.54 -12 6 -2 12.83 0.62 -12 6 -3 286.19 6.51 12 6 3 289.77 8.84 12 6 4 1.20 2.21 12 6 4 2.19 0.57 -12 6 -4 2.22 0.69 12 6 5 170.34 4.33 -12 6 -5 179.58 4.57 12 6 5 183.48 6.49 12 6 6 9.72 2.68 12 6 6 11.51 1.00 -12 6 -6 6.68 1.29 -12 6 -6 9.34 1.07 12 6 7 152.69 4.24 -12 6 -7 145.98 4.21 -12 6 -7 160.10 4.46 12 6 7 158.75 6.01 12 6 8 4.97 2.44 12 6 8 3.48 1.01 -12 6 -8 2.97 0.82 12 6 9 41.33 3.31 12 6 9 43.83 2.13 12 6 10 15.67 2.94 12 6 10 6.84 1.37 12 6 11 171.88 6.36 12 6 11 172.55 5.25 12 6 12 3.25 1.46 -12 8 13 5.09 2.86 -12 8 12 31.79 3.66 -12 8 11 1.80 2.60 12 8 -11 0.93 1.17 -12 8 10 2.38 2.44 12 8 -10 5.02 1.24 -12 8 9 3.09 2.46 12 8 -9 4.95 1.18 -12 8 8 380.49 11.37 12 8 -8 363.57 9.08 -12 8 7 1.69 2.43 12 8 -7 3.57 0.98 -12 8 6 83.03 4.64 -12 8 6 88.33 2.96 12 8 -6 77.62 2.75 -12 8 5 6.00 0.99 12 8 -5 5.14 0.89 -12 8 4 116.45 5.23 12 8 -4 119.27 3.35 -12 8 3 4.72 2.22 12 8 -3 5.99 0.79 -12 8 2 37.44 3.10 12 8 -2 39.54 1.48 -12 8 1 2.70 2.13 12 8 -1 4.68 0.71 -12 8 0 577.20 14.68 -12 8 -1 5.98 2.04 -12 8 -2 39.23 1.68 -12 8 -2 41.73 2.92 -12 8 -3 6.57 1.00 12 8 3 5.15 0.73 12 8 4 127.36 3.54 -12 8 -4 131.34 3.79 -12 8 -5 6.93 1.10 12 8 5 3.77 0.89 -12 8 -6 88.79 3.15 12 8 6 84.18 2.89 -12 8 -7 4.04 1.17 12 8 7 2.66 1.04 12 8 8 367.82 9.36 -12 8 -8 400.90 9.77 12 8 9 4.42 1.21 -12 8 -9 4.82 1.41 -12 8 -9 2.32 0.85 -12 8 -10 5.98 1.46 12 8 10 3.91 1.32 -12 8 -11 0.43 1.42 12 8 11 1.28 1.34 -12 8 -12 41.07 2.66 12 10 -14 6.29 1.76 12 10 -13 8.30 1.73 -12 10 12 -0.72 2.78 12 10 -12 -0.11 1.42 -12 10 11 46.10 4.20 12 10 -11 48.49 2.68 -12 10 10 0.67 2.60 12 10 -10 4.24 1.34 -12 10 9 66.99 4.48 12 10 -9 67.18 2.95 -12 10 8 0.20 2.47 12 10 -8 3.03 1.21 -12 10 7 171.77 6.68 12 10 -7 150.22 4.71 -12 10 6 11.47 2.60 12 10 -6 12.34 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-4 1.83 1.57 -15 5 -5 4.59 1.51 -15 7 8 -0.69 2.81 -15 7 8 6.60 3.54 -15 7 7 -1.12 2.63 -15 7 7 3.54 3.40 -15 7 6 4.79 3.32 -15 7 5 3.75 3.15 -15 7 4 3.37 3.06 -15 7 3 6.84 3.19 -15 7 2 8.11 3.05 -15 7 1 -0.68 2.10 -15 7 1 3.34 2.92 -15 7 0 -1.91 2.16 -15 7 -1 1.62 1.94 -15 7 -2 3.50 2.02 -15 7 -3 2.20 1.88 -15 7 -4 -0.33 1.61 -15 7 -5 -1.11 1.60 -15 9 7 -0.93 3.33 -15 9 6 5.39 3.30 -15 9 5 7.17 3.17 -15 9 4 -0.21 2.89 -15 9 3 5.48 3.12 -15 9 2 9.46 3.12 -15 9 1 9.31 2.96 -15 9 0 4.04 2.92 -15 11 6 2.67 3.19 -15 11 5 -3.02 3.18 -15 11 4 -2.08 2.78 -15 11 3 0.20 3.18 -15 11 2 5.46 3.00 -15 11 1 6.10 2.91 -15 11 0 5.36 3.02 -15 11 -1 9.37 2.98 -15 13 5 -1.97 3.33 -15 13 4 -2.29 3.15 -15 13 3 2.22 3.04 -15 13 2 0.97 3.13 -15 13 1 2.80 3.03 -15 15 4 -5.36 3.53 -16 0 1 8.14 2.33 -16 0 2 28.60 3.11 -16 0 3 7.23 2.70 -16 0 4 78.59 4.74 -16 0 5 4.90 2.67 -16 0 6 52.09 4.37 -16 0 7 3.16 2.91 -16 0 8 172.52 7.55 -16 2 8 -0.47 2.99 -16 2 7 91.52 5.53 -16 2 6 6.95 3.01 -16 2 5 42.22 3.85 -16 2 4 0.98 2.54 -16 2 3 94.75 4.98 -16 2 2 8.72 2.51 -16 2 1 75.84 4.12 -16 2 0 0.43 2.09 -16 2 -1 76.43 3.81 -16 2 -2 13.95 2.25 -16 -2 6 14.72 3.36 -16 -2 7 83.00 5.35 -16 -2 8 2.65 3.16 -16 4 7 -0.23 3.10 -16 4 6 5.51 2.98 -16 4 6 12.99 3.83 -16 4 5 1.90 2.62 -16 4 5 11.47 3.73 -16 4 4 201.24 7.72 -16 4 3 3.23 2.60 -16 4 2 30.54 3.29 -16 4 1 3.12 2.21 -16 4 0 81.24 4.17 -16 4 -1 6.43 2.05 -16 4 -2 33.01 2.74 -16 4 -3 3.68 1.75 -16 6 7 59.08 4.69 -16 6 6 4.47 2.95 -16 6 6 11.52 3.81 -16 6 5 42.07 4.06 -16 6 5 60.36 5.01 -16 6 4 -0.82 2.82 -16 6 4 3.60 3.56 -16 6 3 81.46 4.81 -16 6 3 97.51 5.71 -16 6 2 3.68 2.49 -16 6 1 45.86 3.61 -16 6 0 -0.48 2.22 -16 6 -1 46.80 3.32 -16 6 -2 5.85 2.02 -16 6 -3 83.67 3.83 -16 8 5 -0.65 2.79 -16 8 5 9.05 3.63 -16 8 4 33.85 3.71 -16 8 4 47.38 4.54 -16 8 3 1.79 2.56 -16 8 3 8.99 3.40 -16 8 2 8.49 2.60 -16 8 2 17.79 3.64 -16 8 1 0.89 2.43 -16 8 0 153.04 6.08 -16 8 -1 0.15 2.22 -16 8 -2 12.25 2.36 -16 10 5 13.78 3.92 -16 10 4 4.05 3.63 -16 10 3 37.69 4.24 -16 10 2 6.35 3.34 -16 10 1 62.10 4.69 -16 12 4 80.22 5.47 -16 12 3 0.22 3.32 -16 12 2 18.29 3.72 -17 1 6 4.42 3.08 -17 1 5 -0.42 2.92 -17 1 4 3.77 2.72 -17 1 3 2.05 2.67 -17 1 2 4.19 2.67 -17 1 1 3.39 2.38 -17 -1 6 0.90 2.92 -17 3 5 1.71 2.92 -17 3 4 2.82 3.00 -17 3 3 4.55 2.69 -17 3 2 3.01 2.54 -17 3 1 1.63 2.39 -17 3 0 2.84 2.23 -17 3 -1 3.55 2.11 -17 5 5 0.44 2.91 -17 5 4 0.21 2.69 -17 5 3 1.77 2.63 -17 5 2 4.77 2.69 -17 5 1 -1.87 2.44 -17 5 0 -0.78 2.18 -17 7 4 0.21 3.00 -17 7 3 1.21 2.78 -17 7 2 -0.57 2.71 -17 7 1 2.49 2.53 -17 7 0 -0.16 2.61 -17 9 3 -2.48 3.12 -17 9 3 2.04 3.65 -17 9 2 7.45 2.82 -17 9 1 -0.18 2.62 -18 2 4 0.81 2.91 -18 2 3 -0.95 2.66 -18 2 2 1.79 2.78 -18 4 3 3.30 2.95 0 0 0 0.00 0.00 TITL FCC-121-01-1 in C222(1) REM C222(1) (#20 in standard setting) CELL 0.71073 12.962052 18.787490 17.666625 90.0000 90.0000 90.0000 ZERR 60.00 0.000746 0.001310 0.000947 0.0000 0.0000 0.0000 LATT -7 SYMM -x,-y, z+1/2 SYMM -x, y,-z+1/2 SYMM x,-y,-z SFAC C H N I Pb UNIT 60.00 60.00 60.00 60.00 60.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' 0 0 2 1.30 0.23 0 0 -2 1.01 0.20 0 0 3 -0.03 0.23 0 0 -3 -0.12 0.23 0 0 4 355.32 8.04 0 0 -4 344.03 8.03 0 0 5 -0.10 0.55 0 0 -5 -0.05 0.48 0 0 -6 178.84 4.84 0 0 6 183.94 4.85 0 0 7 0.39 0.64 0 0 -7 -0.27 0.63 0 0 8 7339.02 153.28 0 0 -8 7253.99 153.36 0 0 9 -0.98 0.88 0 0 9 -0.24 0.73 0 0 10 101.48 3.34 0 0 10 86.38 3.33 0 0 11 -0.24 1.14 0 0 11 1.67 1.08 0 0 12 34.47 2.11 0 0 12 34.32 2.20 0 0 13 0.46 1.24 0 0 13 -0.12 1.24 0 0 14 181.36 5.60 0 0 14 174.89 5.91 0 0 15 0.31 1.58 0 0 15 1.99 1.62 0 0 16 1423.54 31.68 0 0 16 1406.29 32.24 0 0 17 -0.11 1.54 0 0 18 39.80 2.65 0 0 19 0.86 1.62 0 0 20 3.29 1.72 0 0 21 0.92 1.82 0 0 22 70.17 3.78 0 0 22 75.30 3.85 0 -2 0 1.51 0.21 0 -2 1 1453.51 30.63 0 -2 2 0.44 0.18 0 -2 3 2028.47 42.55 0 -2 3 2023.58 42.48 0 -2 -4 0.44 0.32 0 -2 4 0.40 0.23 0 -2 5 971.46 21.65 0 2 -5 1026.49 21.97 0 -2 5 1021.99 21.81 0 2 -5 1015.53 21.79 0 -2 -5 1010.43 21.51 0 -2 5 1012.02 21.28 0 -2 6 1.30 0.74 0 2 -6 0.18 0.66 0 2 -6 0.84 0.54 0 2 6 0.92 0.57 0 -2 -6 1.21 0.38 0 -2 7 1867.33 39.70 0 2 7 1816.44 39.90 0 2 -7 1862.77 39.99 0 -2 -7 1864.11 39.17 0 -2 8 1.28 0.78 0 2 8 -0.28 0.71 0 2 -8 0.46 0.69 0 -2 -8 0.77 0.38 0 -2 -9 380.26 8.35 0 2 9 358.52 9.33 0 2 -9 375.33 9.46 0 -2 9 373.15 9.13 0 2 -10 0.78 0.84 0 2 10 1.61 0.90 0 -2 -10 1.58 0.42 0 -2 10 1.12 1.08 0 -2 11 887.87 19.86 0 2 11 900.43 20.16 0 2 -11 875.02 20.31 0 -2 -11 864.27 18.58 0 2 12 1.37 1.16 0 2 -12 0.11 1.00 0 -2 12 0.44 1.21 0 2 13 125.39 4.53 0 2 -13 126.59 4.63 0 -2 13 124.20 4.37 0 -2 14 0.80 1.55 0 2 14 0.47 1.26 0 2 -14 -0.13 1.18 0 2 15 587.51 14.81 0 -2 15 600.73 14.55 0 2 15 597.72 14.49 0 -2 16 0.56 1.56 0 2 16 -0.66 1.61 0 2 16 1.19 1.38 0 2 17 34.06 2.49 0 -2 17 37.75 2.63 0 -2 17 35.56 2.46 0 2 18 -0.24 1.55 0 -2 18 -0.57 1.59 0 2 19 172.91 6.01 0 -2 19 186.02 6.01 0 2 20 -0.13 1.81 0 -2 20 -0.12 1.68 0 2 21 9.37 2.10 0 -2 21 5.07 1.85 0 2 22 -1.08 1.92 0 -2 22 -0.92 2.01 0 -4 0 409.79 9.33 0 -4 -1 0.75 0.40 0 -4 1 1.13 0.44 0 -4 2 14.93 0.88 0 -4 3 5.37 0.60 0 -4 -4 9056.70 194.99 0 -4 4 9083.30 194.79 0 4 -5 -0.19 0.50 0 4 -5 1.46 0.76 0 -4 5 0.37 0.42 0 -4 -5 0.42 0.52 0 -4 6 93.44 2.77 0 4 -6 97.56 2.99 0 -4 -6 95.47 2.85 0 -4 6 94.99 2.61 0 -4 7 1.32 0.41 0 -4 -7 1.29 0.57 0 -4 7 1.47 0.77 0 4 -7 2.07 0.68 0 4 -7 2.47 0.79 0 -4 8 112.03 3.29 0 4 -8 108.17 3.66 0 4 -8 108.70 3.44 0 -4 -8 106.22 3.19 0 -4 8 110.10 2.84 0 4 -9 1.04 0.84 0 -4 -9 1.47 0.61 0 -4 9 2.24 0.91 0 4 -9 2.59 0.85 0 -4 9 2.00 0.43 0 -4 10 167.56 4.64 0 -4 10 157.05 3.77 0 4 10 161.17 4.90 0 4 -10 158.79 5.05 0 -4 -10 162.11 4.31 0 4 11 2.59 1.10 0 -4 11 1.38 1.12 0 4 -11 1.63 1.04 0 -4 -11 2.58 0.71 0 -4 -12 2939.70 62.43 0 4 12 2957.39 63.58 0 4 -12 2938.25 63.89 0 -4 12 2983.78 63.08 0 4 13 4.40 1.37 0 4 -13 3.33 1.29 0 -4 -13 2.72 0.69 0 -4 13 1.62 1.37 0 -4 14 71.94 3.17 0 4 -14 73.09 3.51 0 4 14 75.52 3.47 0 -4 -14 72.31 2.25 0 4 -15 -0.43 1.27 0 4 15 0.52 1.30 0 -4 -15 0.25 0.44 0 -4 15 -1.47 1.60 0 4 -16 18.28 2.09 0 4 16 16.94 1.97 0 4 -17 -0.80 1.57 0 -4 17 0.88 1.63 0 -4 18 98.37 4.14 0 4 18 108.35 4.32 0 4 -18 99.71 4.60 0 4 19 -1.94 1.87 0 -4 19 -2.74 1.85 0 4 20 489.45 12.71 0 -4 20 476.89 12.49 0 4 21 1.23 1.87 0 -4 21 -0.51 1.98 0 4 22 20.15 2.55 0 -6 0 4.47 0.76 0 -6 -1 1061.36 24.07 0 -6 1 1131.49 24.04 0 -6 2 0.76 0.56 0 -6 3 2054.41 43.92 0 -6 4 5.24 0.72 0 -6 -4 5.57 0.88 0 6 -5 1054.16 23.15 0 -6 -5 1067.96 23.57 0 -6 5 1084.24 23.31 0 6 -6 9.89 0.95 0 -6 6 11.74 0.93 0 -6 -6 13.24 1.15 0 6 -7 775.84 17.25 0 6 -7 802.12 17.78 0 -6 -7 783.76 17.75 0 -6 7 785.39 17.36 0 -6 8 0.05 0.58 0 -6 -8 0.22 0.72 0 6 -8 1.04 1.03 0 6 -9 328.15 8.52 0 6 -9 317.40 8.23 0 -6 -9 319.33 8.09 0 -6 9 323.35 7.65 0 6 -10 6.86 1.32 0 -6 -10 8.21 1.09 0 -6 10 8.38 1.37 0 6 -10 6.92 1.24 0 -6 10 5.65 0.76 0 -6 11 1188.36 26.14 0 -6 11 1188.16 25.46 0 6 -11 1194.89 26.87 0 6 -11 1169.53 26.43 0 -6 -11 1168.40 26.11 0 -6 -12 1.09 0.89 0 -6 12 0.59 0.59 0 6 -12 -1.33 1.35 0 -6 12 2.42 1.45 0 6 -12 0.36 1.09 0 6 12 -0.96 1.20 0 -6 13 141.37 4.60 0 -6 -13 135.88 4.21 0 6 -13 148.92 5.22 0 6 13 143.68 4.97 0 -6 13 137.09 3.42 0 6 14 4.92 1.50 0 -6 14 7.14 1.86 0 6 -14 5.99 1.51 0 -6 -14 4.50 1.01 0 -6 -15 204.93 5.48 0 6 15 206.19 6.65 0 6 -15 203.70 6.81 0 -6 15 197.21 6.19 0 -6 16 4.55 1.85 0 -6 -16 2.91 0.90 0 6 -16 2.62 1.51 0 -6 -17 31.24 1.47 0 6 -17 27.48 2.59 0 -6 18 3.21 1.85 0 6 -18 0.71 1.59 0 6 -19 290.65 9.17 0 -6 19 280.63 8.22 0 6 -20 -0.76 1.82 0 -6 20 3.29 2.00 0 6 21 7.24 2.16 0 6 22 -2.09 2.17 0 -8 0 6690.78 140.84 0 -8 1 0.98 0.76 0 -8 -1 1.53 0.81 0 -8 2 10.57 1.09 0 -8 3 3.69 0.81 0 -8 -4 94.55 3.42 0 -8 4 97.05 3.27 0 -8 -5 1.61 0.87 0 -8 5 0.89 0.76 0 -8 -6 86.11 3.25 0 -8 6 87.10 3.03 0 8 -6 84.69 2.88 0 8 -7 9.16 1.15 0 -8 7 9.90 1.09 0 -8 -7 7.23 1.18 0 8 -8 4022.62 85.46 0 8 -8 4063.87 84.79 0 -8 -8 3968.86 85.59 0 -8 8 4005.56 85.09 0 8 -9 6.33 1.48 0 -8 -9 5.74 1.15 0 -8 9 6.36 1.01 0 8 -10 43.57 2.52 0 -8 -10 46.93 2.39 0 -8 10 45.46 2.02 0 -8 -11 0.10 1.08 0 8 -11 0.41 1.40 0 8 -11 1.00 1.27 0 -8 11 -0.06 0.77 0 8 -12 17.12 1.94 0 8 -12 17.79 1.99 0 -8 -12 16.13 1.58 0 -8 12 17.00 1.26 0 8 -13 4.98 1.63 0 8 -13 6.96 1.58 0 -8 13 4.43 0.92 0 -8 -13 6.12 1.36 0 8 -14 102.90 4.08 0 8 -14 104.21 4.43 0 8 14 110.40 4.38 0 -8 -14 103.35 3.81 0 -8 14 107.65 3.14 0 -8 -15 1.76 1.14 0 8 -15 1.44 1.63 0 -8 15 0.68 0.63 0 8 -16 992.50 23.57 0 -8 -16 956.86 21.93 0 8 -17 2.16 1.74 0 -8 -17 5.47 1.25 0 8 -18 27.85 2.83 0 -8 -18 27.26 1.73 0 -8 -19 -0.53 0.96 0 8 -19 -0.59 1.90 0 8 -20 1.82 1.95 0 -10 0 5.91 1.14 0 -10 1 1090.77 24.66 0 -10 -1 1084.25 24.71 0 -10 2 5.62 1.10 0 -10 3 406.66 10.35 0 -10 -4 0.89 0.99 0 -10 4 0.20 0.86 0 -10 5 351.45 9.13 0 -10 -5 349.55 9.40 0 -10 6 4.64 1.19 0 -10 -6 5.42 1.17 0 -10 -7 1196.69 27.10 0 -10 7 1191.54 26.58 0 10 -7 1181.55 26.22 0 10 -8 1.04 1.15 0 -10 -8 0.47 1.26 0 -10 8 0.27 1.00 0 10 -9 287.21 7.94 0 -10 9 285.14 7.59 0 -10 -9 285.13 8.09 0 10 -9 274.08 7.17 0 10 -10 18.07 1.96 0 -10 -10 15.28 1.87 0 -10 10 15.83 1.52 0 10 -10 14.54 1.42 0 10 -11 183.33 5.89 0 -10 11 179.02 5.29 0 -10 -11 180.92 5.88 0 -10 -12 0.12 1.16 0 10 -12 1.88 1.66 0 10 -12 3.45 1.60 0 -10 12 1.14 1.00 0 10 -13 99.20 4.39 0 10 -13 88.87 3.95 0 -10 -13 98.67 3.94 0 -10 13 93.09 3.31 0 10 -14 1.02 1.66 0 10 -14 3.90 1.71 0 -10 -14 3.69 1.45 0 -10 14 3.62 1.06 0 10 -15 491.14 13.32 0 10 -15 482.89 12.74 0 -10 -15 481.24 12.50 0 -10 15 503.62 11.60 0 -10 -16 -0.12 1.17 0 10 -16 0.88 1.66 0 -10 16 0.32 0.85 0 10 -17 31.40 2.93 0 -10 -17 26.20 2.12 0 -10 -18 3.33 1.38 0 10 -18 0.99 1.74 0 -10 -19 41.14 2.48 0 10 -19 47.91 3.62 0 -12 0 60.96 3.07 0 -12 1 0.13 1.05 0 -12 -1 2.34 1.24 0 -12 2 11.24 1.56 0 -12 3 2.34 1.18 0 -12 4 2932.30 63.47 0 -12 5 1.19 1.15 0 -12 -5 1.38 1.35 0 -12 -6 5.45 1.49 0 -12 6 5.47 1.41 0 12 -7 1.57 1.57 0 -12 7 2.05 1.21 0 -12 -7 0.28 1.34 0 -12 -8 29.66 2.40 0 -12 8 27.61 2.07 0 12 -8 29.95 2.17 0 12 -9 1.84 1.36 0 -12 -9 3.29 1.52 0 -12 9 3.42 1.29 0 12 -10 34.85 2.68 0 -12 10 35.58 2.28 0 -12 -10 39.42 2.73 0 12 -10 31.65 2.00 0 -12 -11 1.88 1.47 0 -12 11 2.51 1.15 0 12 -11 2.25 1.65 0 12 -11 1.45 1.17 0 12 -12 1156.25 26.76 0 -12 -12 1158.44 27.00 0 -12 12 1163.23 26.19 0 -12 -13 7.91 1.77 0 -12 13 7.99 1.45 0 12 -13 9.61 2.08 0 -12 14 20.31 1.78 0 12 -14 20.59 2.44 0 -12 -14 20.03 2.16 0 12 -14 19.13 2.39 0 12 -15 0.86 1.76 0 12 -15 1.27 1.75 0 -12 15 -0.27 1.18 0 -12 -15 2.14 1.53 0 12 -16 5.68 1.98 0 -12 -16 4.93 1.72 0 12 -16 8.61 2.08 0 12 -17 4.84 2.07 0 -12 -17 1.94 1.63 0 12 -18 31.09 3.19 0 -12 -18 29.30 2.47 0 -12 -19 1.69 1.68 0 -14 0 0.15 1.32 0 -14 1 105.45 4.48 0 -14 -1 97.41 4.42 0 -14 2 0.60 1.40 0 -14 3 687.77 17.17 0 -14 4 2.46 1.49 0 -14 5 363.48 10.29 0 -14 -5 378.86 10.77 0 -14 6 7.95 1.71 0 -14 -6 8.01 1.90 0 -14 -7 73.04 3.90 0 -14 7 76.75 3.67 0 14 -8 4.34 1.78 0 -14 8 2.17 1.36 0 -14 -8 1.50 1.66 0 -14 9 82.33 3.76 0 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976.21 21.92 -4 6 -11 962.08 21.42 4 -6 -12 1.10 1.22 -4 6 -12 -0.35 1.03 -4 6 -12 2.51 0.93 -4 -6 12 4.57 2.27 -4 6 -12 2.96 1.34 4 6 12 -0.22 1.16 -4 -6 13 139.60 5.64 -4 6 -13 133.78 4.00 4 6 13 135.00 4.82 -4 6 -13 136.50 5.03 4 -6 -13 133.34 4.67 -4 6 -14 3.16 0.86 4 6 14 3.42 1.44 -4 -6 14 4.92 2.45 -4 6 -14 4.72 1.49 4 -6 -14 2.78 1.23 -4 -6 15 186.73 4.76 -4 -6 15 189.89 6.91 -4 6 -15 181.90 6.44 4 6 15 196.52 6.39 -4 -6 15 193.53 4.97 -4 -6 16 1.02 0.57 -4 -6 16 0.68 0.65 -4 6 -16 0.16 1.60 -4 -6 17 34.32 3.47 -4 6 -17 21.30 2.48 -4 6 -18 2.63 1.78 -4 -6 18 3.27 2.43 -4 6 -19 246.13 8.24 -4 -6 19 244.31 8.48 -4 -6 20 5.07 2.73 -4 -6 21 13.16 3.39 -4 -6 22 4.45 3.13 4 8 -20 3.74 2.07 -4 -8 -19 0.08 1.18 4 8 -19 -0.57 1.91 -4 -8 -18 11.73 1.52 4 8 -18 9.86 2.08 -4 -8 -17 5.46 1.34 4 8 -17 4.28 1.96 4 8 -16 688.46 17.75 -4 -8 -16 703.90 16.50 4 8 -15 3.63 1.65 -4 -8 -15 2.51 1.18 4 8 -14 126.69 4.94 -4 8 14 115.21 4.60 4 8 -13 7.63 1.55 -4 8 13 6.87 1.34 4 8 -12 23.38 2.09 4 -8 12 23.46 1.85 -4 8 12 19.60 1.75 4 8 -12 22.87 2.38 4 -8 11 4.75 1.31 4 8 -11 0.52 1.73 4 8 -11 3.70 1.43 -4 8 11 3.11 1.19 -4 8 10 11.01 1.49 4 8 -10 14.94 1.78 4 8 -10 10.51 1.91 4 -8 10 14.47 1.59 -4 8 9 5.97 1.33 4 8 -9 5.74 1.73 4 -8 9 5.43 1.31 4 8 -9 3.69 1.46 4 8 -8 2885.68 61.08 4 -8 8 2844.24 61.18 -4 8 8 2775.81 61.09 4 8 -7 7.96 1.68 -4 8 7 9.24 1.48 4 -8 7 8.39 1.44 4 8 -6 107.16 4.14 4 8 -6 118.61 4.22 4 -8 6 119.50 4.27 -4 8 6 112.45 4.18 4 8 -5 7.05 1.62 -4 8 5 6.09 1.35 4 -8 5 5.47 1.28 4 8 -5 7.18 1.53 4 8 -4 118.48 4.19 4 -8 4 114.53 4.28 4 8 -4 113.22 4.03 -4 8 4 117.93 4.34 4 -8 3 8.80 1.44 -4 8 3 9.97 1.53 -4 8 2 4.03 1.22 4 -8 2 2.71 1.12 -4 8 1 2.55 1.18 4 -8 1 0.72 1.06 4 -8 0 4511.95 96.29 4 -8 -1 2.23 1.18 -4 8 -3 6.93 1.37 4 -8 -4 116.41 4.46 -4 8 -4 114.24 4.31 -4 8 -5 5.53 1.33 4 -8 -5 6.23 1.41 -4 8 -6 114.60 4.23 4 -8 -6 114.50 4.45 4 -8 -7 10.45 1.70 -4 8 -7 9.81 1.51 -4 8 -8 2837.73 60.61 4 -8 -8 2780.14 61.21 4 -8 -9 3.87 1.45 -4 8 -9 4.39 1.28 -4 8 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1.51 4 12 -11 2.87 1.85 4 12 -10 46.43 3.18 4 -12 10 51.43 3.01 4 12 -10 52.87 3.05 4 12 -9 2.38 1.94 4 12 -9 4.21 1.91 -4 12 9 6.07 1.62 4 -12 9 2.68 1.54 4 -12 8 36.14 2.59 4 12 -8 37.73 2.87 -4 12 8 37.76 2.69 4 -12 7 3.99 1.52 -4 12 7 3.93 1.60 4 12 -7 4.35 2.07 4 -12 6 1.16 1.45 -4 12 6 1.66 1.55 4 12 -6 4.16 2.05 4 -12 5 2.49 1.50 -4 12 5 3.93 1.67 4 12 -5 5.57 2.25 -4 12 4 1975.43 44.36 4 -12 4 2015.38 44.53 -4 12 3 3.85 1.56 4 -12 3 4.66 1.61 -4 12 2 18.60 2.04 4 -12 2 24.00 2.25 -4 12 1 4.61 1.59 4 -12 1 4.84 1.55 4 -12 0 78.55 3.94 4 -12 -1 1.12 1.42 -4 12 -2 19.28 2.10 -4 12 -3 1.57 1.48 -4 12 -4 1995.13 43.30 4 -12 -4 1875.53 43.64 -4 12 -5 1.96 1.54 4 -12 -5 1.01 1.48 4 -12 -6 0.17 1.52 -4 12 -6 1.24 1.41 4 -12 -7 2.90 1.68 -4 12 -7 5.05 1.60 4 -12 -8 40.74 3.03 -4 12 -8 39.46 2.75 -4 12 -8 42.29 1.56 4 -12 -9 5.03 1.80 -4 12 -9 4.01 1.43 -4 12 -10 50.01 2.84 4 -12 -10 51.50 3.36 4 -12 -11 2.25 1.81 4 -12 -12 876.82 21.45 -4 12 -12 864.21 20.19 -4 -12 12 864.85 20.25 -4 12 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208.97 8.05 4 -18 -2 3.01 2.20 -4 -18 2 2.72 2.02 -4 -18 3 27.34 2.90 -4 -18 4 -2.04 1.97 -4 -18 5 31.10 3.06 4 -18 -5 30.59 3.24 4 -18 -6 1.20 2.16 -4 -18 6 2.56 1.95 -4 -18 7 255.16 8.75 4 -18 -7 277.94 9.66 4 -18 -8 2.91 2.29 -4 -18 8 1.72 1.97 4 -18 -9 83.83 5.01 -4 18 -9 93.34 3.29 -4 -18 9 79.81 4.43 4 -18 -10 0.73 2.19 -4 18 -10 2.00 1.15 -4 -18 10 2.67 1.92 4 -18 -11 11.94 2.77 -4 -18 11 7.72 1.94 4 -18 -12 0.73 2.33 -4 -18 12 0.86 1.80 4 -18 -13 7.98 2.80 -4 -18 13 8.45 2.24 4 -18 -14 0.48 2.70 -4 -18 14 -0.33 1.86 4 -18 -15 150.25 6.92 4 -18 -16 0.47 2.62 4 -18 -17 12.26 3.04 -4 -20 -14 3.06 2.44 4 -20 13 1.43 2.35 -4 -20 -13 -1.43 2.55 -4 -20 -12 156.76 7.03 4 -20 12 162.08 6.72 4 -20 11 0.64 2.23 -4 -20 -11 1.68 2.42 4 -20 10 9.87 2.58 -4 -20 -10 5.48 2.39 4 -20 9 1.31 2.22 -4 -20 -9 5.93 2.53 4 -20 8 16.00 2.82 -4 -20 -8 19.22 2.91 4 -20 7 0.68 2.18 -4 -20 -7 2.16 2.23 4 -20 6 0.68 2.19 -4 -20 -6 -0.48 2.27 4 -20 5 3.72 2.29 -4 -20 -5 -0.97 2.21 4 -20 4 292.22 10.10 4 -20 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180.86 5.22 -8 4 8 182.90 5.22 -8 4 8 194.20 6.39 -8 4 7 8.00 1.71 -8 4 7 5.14 1.90 8 4 -7 6.88 1.02 -8 4 7 8.65 1.07 -8 4 6 7.18 1.72 -8 4 6 8.56 1.81 8 4 -6 6.48 0.95 -8 4 6 8.19 0.94 -8 4 5 3.68 1.57 8 4 -5 4.61 0.77 -8 4 5 6.24 0.78 -8 4 5 4.83 1.65 8 4 -5 3.37 1.55 8 4 -4 2714.80 58.25 -8 4 4 2692.25 58.27 8 4 -4 2672.70 56.73 -8 4 4 2698.16 59.01 -8 4 3 3.73 1.49 -8 4 3 4.65 1.63 8 4 -3 5.44 0.65 8 4 -3 3.18 1.68 8 4 -2 133.53 3.32 -8 4 2 126.64 4.49 8 4 -2 138.71 4.85 -8 4 2 133.90 5.24 -8 4 1 17.82 2.10 -8 4 1 15.55 1.78 8 4 -1 16.06 1.97 -8 4 0 408.44 10.36 8 4 0 433.78 10.91 -8 4 0 411.33 11.54 -8 4 -1 15.25 1.67 8 4 1 20.77 2.25 -8 4 -2 132.01 4.25 8 4 2 136.58 4.78 8 4 3 6.92 2.02 -8 4 -3 8.22 1.43 -8 4 -3 4.16 1.76 -8 4 -3 3.79 0.71 -8 -4 3 4.70 1.60 -8 -4 4 2622.68 59.05 -8 4 -4 2800.38 57.61 8 4 4 2701.28 57.48 -8 4 -4 2687.87 59.80 -8 -4 5 6.62 1.80 8 4 5 4.33 0.74 -8 4 -5 6.33 0.93 -8 4 -5 4.42 1.59 -8 -4 6 10.29 2.09 8 4 6 7.42 0.94 -8 -4 6 12.46 2.59 -8 4 -6 7.09 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102.25 5.86 -8 -4 19 4.77 2.90 -8 -4 19 4.16 3.55 -8 -4 20 164.72 7.74 8 6 -16 0.29 1.46 8 6 -15 117.41 4.75 -8 6 15 126.35 4.69 -8 6 14 3.64 1.54 8 6 -14 0.53 1.37 -8 6 14 3.92 1.47 -8 6 13 82.65 3.79 8 6 -13 81.96 3.65 -8 6 13 82.52 3.55 8 6 -12 3.70 1.31 -8 6 12 2.27 1.55 -8 6 12 5.17 1.50 -8 6 11 472.05 12.45 8 6 -11 462.62 11.93 -8 6 11 483.60 11.83 -8 6 10 23.67 2.28 -8 6 10 20.44 1.77 8 6 -10 21.09 1.77 -8 6 9 105.79 4.59 8 6 -9 112.32 3.93 -8 6 9 116.17 3.82 8 6 -8 4.63 1.08 -8 6 8 5.38 1.75 -8 6 7 366.38 10.45 8 6 -7 372.20 9.12 -8 6 6 11.70 2.06 8 6 -6 12.48 1.23 8 6 -5 415.61 10.09 -8 6 5 444.94 11.90 8 6 -5 440.01 11.38 8 6 -4 -0.25 1.89 8 6 -4 0.92 1.51 -8 6 4 2.97 1.65 -8 6 3 803.70 20.03 8 6 -3 823.48 19.41 8 6 -3 811.27 19.15 -8 6 2 24.41 2.50 8 6 -2 27.92 2.53 8 6 -2 24.25 2.17 -8 6 1 426.61 11.95 8 6 -1 445.86 10.98 8 6 -1 437.73 11.42 -8 6 1 414.42 10.75 -8 6 0 14.36 1.52 8 6 0 14.00 1.79 -8 6 0 19.43 2.28 8 6 0 17.45 2.32 -8 6 -1 423.59 10.61 8 6 1 437.02 11.51 8 6 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1.58 8 8 0 1946.81 42.05 8 -8 0 1895.80 43.76 8 8 0 1901.56 42.67 -8 8 -1 1.71 1.21 8 -8 -1 6.12 2.02 8 8 1 3.92 1.58 -8 8 -2 35.27 2.88 8 8 2 39.65 2.37 -8 8 -2 38.58 2.03 -8 8 -3 7.52 1.24 -8 8 -3 10.58 2.08 8 8 3 10.99 1.69 -8 8 -4 183.38 6.85 8 8 4 188.30 5.50 8 -8 -4 198.59 7.23 -8 8 -4 189.02 5.07 -8 8 -5 12.30 1.24 8 8 5 7.98 1.42 8 -8 -5 11.83 2.30 -8 8 -5 8.32 2.11 -8 8 -6 140.12 5.78 8 8 6 146.31 4.48 8 -8 -6 146.92 6.09 8 8 7 7.21 1.43 -8 8 -7 4.71 1.89 8 -8 -7 4.90 2.04 -8 8 -8 1271.98 28.29 -8 8 -8 1253.28 29.56 8 -8 -8 1259.09 30.15 -8 8 -9 6.69 1.47 -8 8 -9 4.63 1.63 8 -8 -9 4.89 2.02 8 8 10 1.03 1.11 8 -8 -10 1.35 1.87 -8 8 -10 2.86 1.34 8 8 11 2.37 1.25 -8 8 -11 3.36 1.41 -8 8 -11 1.93 1.45 -8 8 -11 3.68 0.90 -8 8 -12 53.17 1.80 -8 8 -12 54.82 3.17 8 8 12 47.41 2.69 -8 8 -12 52.26 2.96 -8 8 -13 4.40 1.61 8 8 13 6.68 1.50 -8 8 -13 4.57 1.63 -8 8 -14 112.37 4.53 -8 8 -14 112.87 4.72 8 8 14 111.30 4.49 -8 8 -15 1.87 1.73 -8 8 -15 5.76 1.69 -8 8 -16 334.56 9.17 -8 8 -16 328.56 9.87 -8 8 -17 3.71 1.88 -8 8 -18 -0.70 1.95 -8 8 -19 -0.18 2.03 8 10 -18 -0.18 1.98 8 10 -17 18.34 2.40 8 10 -16 2.18 1.92 -8 10 15 191.52 6.37 8 10 -15 185.40 6.64 -8 10 14 7.67 1.87 8 10 -14 9.15 1.93 -8 10 13 27.42 2.57 8 10 -13 33.16 2.58 8 10 -12 0.52 1.35 -8 10 12 0.91 1.65 -8 10 11 107.57 4.70 8 10 -11 106.54 4.28 8 10 -10 9.57 1.60 -8 10 10 6.68 1.90 8 10 -9 156.31 5.21 8 10 -9 162.44 5.97 -8 10 9 155.59 5.95 -8 10 8 3.44 1.89 8 -10 8 3.90 1.91 8 10 -8 3.07 1.89 8 10 -8 -0.88 2.01 8 10 -7 467.08 12.65 8 10 -7 473.37 12.67 8 -10 7 474.87 13.12 -8 10 7 460.78 12.86 8 10 -6 19.18 2.65 8 10 -6 18.10 2.44 8 -10 6 17.08 2.46 -8 10 6 17.93 2.31 8 -10 5 125.43 5.52 -8 10 5 134.81 5.53 8 10 -5 126.03 5.01 -8 10 4 7.45 2.00 8 -10 4 4.51 1.94 8 10 -4 7.67 1.96 8 10 -3 199.03 6.41 8 -10 3 193.90 7.22 -8 10 3 188.00 7.01 8 10 -2 8.94 2.00 8 10 -2 9.56 2.50 -8 10 2 8.75 2.08 8 -10 2 8.80 2.12 -8 10 1 476.33 13.14 8 -10 1 460.08 13.26 8 10 -1 465.44 12.56 8 10 -1 450.66 11.87 8 10 0 3.56 1.82 8 -10 0 3.86 2.00 8 10 1 473.27 11.97 8 -10 -1 469.58 13.59 -8 10 -2 7.37 2.11 8 10 2 10.89 1.88 -8 10 -3 191.01 7.19 8 10 3 190.59 5.98 -8 10 -3 198.48 5.42 8 -10 -4 5.70 2.14 -8 10 -4 8.42 2.08 -8 10 -4 6.98 1.11 -8 10 -5 136.21 5.75 8 -10 -5 126.50 5.85 -8 10 -5 131.27 3.69 8 -10 -6 13.28 2.43 -8 10 -6 10.00 2.21 8 -10 -7 458.38 13.41 -8 10 -7 462.78 12.92 8 -10 -8 3.13 2.09 -8 10 -8 2.08 1.79 -8 10 -9 166.22 5.46 -8 10 -9 156.58 6.10 8 -10 -9 159.72 6.60 -8 10 -10 5.20 1.73 -8 10 -10 8.27 1.78 8 -10 -10 5.35 2.14 -8 10 -11 123.36 4.74 -8 10 -11 107.80 4.85 8 -10 -11 119.34 5.55 -8 10 -12 1.96 1.16 8 -10 -12 -0.20 2.09 -8 10 -12 0.30 1.65 -8 10 -12 3.41 1.55 8 10 12 -0.11 1.27 -8 10 -13 27.61 1.65 8 -10 -13 28.26 3.07 -8 10 -13 31.54 2.56 -8 10 -13 26.56 2.54 -8 10 -14 7.41 2.03 -8 10 -14 5.88 1.09 -8 10 -14 6.84 1.87 -8 10 -15 203.82 7.05 -8 10 -15 197.47 6.51 -8 10 -16 2.97 1.94 -8 10 -17 19.97 2.62 -8 10 -18 3.54 2.04 8 12 -17 4.40 2.26 8 12 -16 12.18 2.28 8 12 -15 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4 46.03 3.26 -10 0 5 3.88 2.24 -10 0 -5 2.54 1.92 -10 0 5 3.61 1.88 -10 0 5 1.37 1.94 10 0 5 -0.35 1.52 -10 0 6 88.47 4.44 10 0 6 87.61 3.46 -10 0 6 88.63 4.61 -10 0 -6 98.43 4.62 -10 0 6 91.36 4.52 10 0 7 -1.27 1.63 -10 0 7 0.17 1.68 -10 0 -7 2.01 1.82 -10 0 7 -1.86 2.02 10 0 8 287.06 7.52 -10 0 8 270.68 8.93 -10 0 -8 282.15 8.82 -10 0 8 267.25 8.79 10 0 9 -0.08 1.38 -10 0 9 1.05 1.75 -10 0 -9 0.82 1.61 -10 0 9 0.18 2.11 -10 0 10 32.77 3.37 10 0 10 37.38 2.21 -10 0 10 36.85 2.95 -10 0 -10 33.86 2.89 10 0 11 1.46 1.35 -10 0 11 -0.21 2.36 -10 0 -11 1.76 1.58 -10 0 11 2.70 1.67 10 0 12 5.34 1.44 -10 0 12 3.90 2.71 -10 0 -12 4.26 1.88 -10 0 12 2.95 1.74 10 0 13 3.65 1.46 -10 0 13 2.02 2.67 -10 0 -13 2.62 1.72 -10 0 13 2.71 1.76 -10 0 13 0.21 2.36 -10 0 14 70.49 4.85 -10 0 14 78.50 3.94 -10 0 14 78.91 4.71 -10 0 -14 79.19 3.94 -10 0 15 -0.22 2.50 -10 0 15 -3.33 2.97 -10 0 -15 0.14 1.68 -10 0 15 1.58 1.69 -10 0 16 142.82 6.97 -10 0 16 146.51 6.68 -10 0 -16 155.89 5.58 -10 0 17 -0.23 2.62 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1.90 -10 -2 0 11.53 1.70 -10 2 0 8.26 1.67 -10 2 0 12.89 2.26 -10 2 -1 50.40 2.66 -10 -2 1 52.93 2.92 10 2 1 59.07 2.99 -10 2 -2 8.86 1.46 10 2 2 10.34 1.94 -10 -2 2 10.20 1.98 -10 2 -3 18.86 1.64 -10 -2 3 21.20 2.28 -10 2 -3 25.11 2.68 10 2 3 22.60 2.22 -10 -2 4 8.57 2.46 10 2 4 3.69 1.64 -10 2 -4 5.51 1.14 -10 -2 4 4.91 1.95 -10 2 -4 5.44 1.95 10 2 5 18.48 2.17 -10 -2 5 19.90 2.78 -10 2 -5 15.67 1.23 -10 -2 5 19.09 2.46 -10 2 -5 16.65 2.36 10 2 6 5.31 1.92 -10 2 -6 2.79 1.91 -10 -2 6 6.52 2.08 -10 -2 6 2.25 2.13 -10 -2 7 54.42 3.64 10 2 7 59.24 3.05 -10 -2 7 54.43 3.55 -10 2 -7 49.49 3.42 10 2 8 6.01 1.84 -10 2 -8 5.65 1.94 -10 -2 8 6.74 2.01 -10 -2 8 4.45 2.12 -10 -2 9 33.57 3.41 10 2 9 37.92 2.61 -10 -2 9 38.66 3.37 -10 -2 9 33.57 2.98 -10 2 -9 32.49 2.92 -10 2 -10 8.24 1.99 -10 -2 10 6.52 1.89 -10 -2 10 12.54 3.06 10 2 10 12.66 2.11 10 2 11 45.10 2.83 -10 -2 11 46.72 4.00 -10 -2 11 42.50 3.21 -10 2 -11 41.63 3.10 -10 -2 12 5.06 2.90 10 2 12 7.56 1.87 -10 2 -12 3.31 1.70 -10 -2 12 2.42 1.73 -10 -2 13 10.66 3.25 -10 -2 13 12.46 2.75 -10 -2 13 9.28 1.97 -10 2 -13 11.05 2.06 -10 -2 14 3.17 2.99 -10 -2 14 2.06 1.76 -10 2 -14 1.49 1.55 -10 -2 14 1.30 2.37 -10 2 -15 58.93 3.42 -10 -2 15 58.11 4.68 -10 -2 15 65.26 4.59 -10 -2 16 2.04 2.65 -10 2 -16 -0.55 1.65 -10 -2 16 0.77 3.19 -10 -2 17 10.30 2.88 -10 -2 17 3.66 3.35 -10 4 17 2.91 2.54 -10 4 17 0.24 2.87 -10 4 16 2.60 2.49 -10 -4 -16 5.03 1.80 -10 4 16 0.69 2.62 -10 -4 -15 2.09 1.90 -10 4 15 -1.26 2.41 -10 4 15 2.35 1.62 -10 4 15 1.74 1.70 -10 4 15 0.67 2.49 -10 4 14 11.05 2.58 -10 4 14 9.12 2.71 -10 4 14 13.38 2.06 -10 4 14 12.55 1.88 -10 4 13 0.84 2.34 -10 4 13 1.21 1.45 -10 4 13 0.16 1.62 -10 4 12 243.70 7.90 -10 4 12 243.11 7.00 -10 4 11 0.57 1.24 -10 4 11 -1.15 1.70 -10 4 10 93.42 3.40 -10 4 10 86.40 4.30 -10 4 9 0.71 2.05 -10 4 9 3.28 1.09 -10 4 9 4.43 1.87 -10 4 8 15.19 1.30 -10 4 8 18.96 2.43 -10 4 7 3.00 0.91 -10 4 7 1.30 2.13 -10 4 7 1.78 1.73 -10 4 6 68.53 3.86 -10 4 6 71.10 2.49 -10 4 6 76.66 4.14 -10 4 5 -0.04 0.66 -10 4 5 1.98 1.92 -10 4 4 332.59 9.66 10 4 -4 340.86 9.57 -10 4 4 333.24 7.71 -10 4 4 340.02 10.29 -10 4 3 -0.53 1.96 -10 4 3 1.02 0.51 10 4 -3 -1.16 1.85 -10 4 3 -1.09 1.85 10 4 -2 105.14 4.43 -10 4 2 98.18 4.29 -10 4 2 106.08 2.55 -10 4 2 108.78 4.99 -10 4 1 4.23 1.85 -10 4 1 4.63 1.93 10 4 -1 1.12 1.97 10 4 0 49.02 3.05 -10 4 0 50.00 2.98 -10 4 0 48.49 3.40 -10 4 -1 2.82 1.90 10 4 1 0.61 1.87 -10 4 -2 107.57 2.63 10 4 2 107.12 4.48 -10 4 -2 104.73 4.14 -10 4 -3 0.74 1.92 10 4 3 2.69 2.02 10 4 3 1.85 0.47 -10 4 -3 1.12 0.50 -10 -4 4 325.58 9.50 10 4 4 347.24 9.30 10 4 4 314.62 7.37 -10 4 -4 335.34 7.60 -10 4 -4 323.41 10.08 -10 -4 5 2.29 2.04 -10 4 -5 0.73 1.82 10 4 5 3.24 2.06 10 4 5 0.68 0.61 -10 4 -5 -0.44 0.73 -10 -4 6 74.57 4.03 -10 4 -6 67.22 2.38 10 4 6 76.85 3.76 10 4 6 69.83 2.36 -10 4 -6 75.37 2.58 -10 4 -6 73.73 4.08 -10 4 -7 3.90 0.77 -10 -4 7 3.43 2.26 -10 4 -7 3.98 0.93 10 4 7 7.01 2.20 10 4 7 4.73 0.95 -10 4 -7 4.10 1.97 10 4 8 13.43 1.28 -10 -4 8 14.62 2.98 10 4 8 17.50 2.37 -10 4 -8 11.69 1.27 -10 -4 8 13.75 2.48 -10 4 -8 9.18 2.09 -10 -4 9 6.45 2.50 10 4 9 6.94 1.18 -10 4 -9 3.47 1.97 10 4 10 86.20 3.31 -10 -4 10 84.77 5.10 -10 4 -10 87.19 4.39 -10 -4 10 88.87 4.64 -10 -4 11 3.39 2.93 10 4 11 1.40 1.28 -10 4 -11 -0.67 1.78 -10 -4 11 0.93 1.75 10 4 12 226.80 6.67 -10 4 -12 228.30 7.59 -10 -4 12 231.40 7.91 -10 -4 12 238.15 8.94 -10 -4 13 1.97 2.51 -10 4 -13 0.78 1.69 -10 -4 13 0.73 3.09 10 4 13 1.20 1.37 -10 -4 13 2.28 1.79 -10 -4 14 11.69 2.94 -10 4 -14 12.77 2.07 -10 -4 14 14.96 3.46 10 4 14 11.95 1.77 -10 -4 14 12.22 2.08 -10 -4 15 6.93 3.43 -10 -4 15 1.15 2.66 10 4 15 2.58 1.63 -10 4 -15 2.60 1.67 -10 -4 16 6.56 3.36 -10 -4 16 6.14 2.86 -10 4 -16 3.47 1.62 -10 -4 17 3.48 3.51 -10 -4 17 3.84 2.94 -10 6 16 2.60 2.69 -10 6 15 34.06 3.65 -10 6 14 7.40 1.80 -10 6 14 6.48 1.92 -10 6 13 15.10 2.27 -10 6 13 19.05 1.97 10 6 -12 0.42 1.17 -10 6 12 2.12 1.75 -10 6 12 2.40 1.33 -10 6 11 92.86 3.59 10 6 -11 87.07 3.50 -10 6 11 97.32 4.53 10 6 -10 1.64 1.04 -10 6 10 1.26 1.11 -10 6 10 3.23 1.79 -10 6 10 1.54 2.17 10 6 -9 11.57 1.31 -10 6 9 10.02 1.31 -10 6 9 11.13 2.36 -10 6 9 8.86 2.03 -10 6 8 1.21 1.92 -10 6 8 3.48 1.00 10 6 -8 2.67 0.94 -10 6 8 3.50 1.79 -10 6 7 25.25 1.54 10 6 -7 23.99 1.53 -10 6 7 25.82 2.68 -10 6 7 21.08 2.57 -10 6 6 8.38 1.00 10 6 -6 9.24 1.97 -10 6 6 6.09 2.08 10 6 -6 9.32 1.09 -10 6 6 8.01 2.03 -10 6 5 44.18 3.28 10 6 -5 43.50 1.82 -10 6 5 40.96 2.97 10 6 -5 47.39 3.15 10 6 -4 9.19 0.91 -10 6 4 10.27 2.25 10 6 -4 3.76 1.96 -10 6 4 9.20 2.00 -10 6 3 74.84 3.73 10 6 -3 76.43 3.97 10 6 -3 79.99 2.42 -10 6 2 1.72 1.93 10 6 -2 2.65 1.99 10 6 -2 6.33 0.73 -10 6 2 4.76 1.91 -10 6 1 13.75 2.07 10 6 -1 16.17 2.46 -10 6 1 18.08 2.51 10 6 0 0.69 2.00 -10 6 0 0.66 1.73 -10 6 0 1.17 1.94 -10 6 -1 7.88 1.86 10 6 1 7.30 2.32 -10 6 -2 3.76 1.78 10 6 2 5.22 2.27 -10 6 -2 3.32 1.98 -10 6 -3 83.13 2.60 -10 6 -3 84.44 4.52 -10 6 -3 79.79 3.45 10 6 3 79.74 4.13 10 6 4 12.50 2.44 -10 6 -4 10.17 1.07 10 6 4 8.29 0.85 -10 6 -4 10.64 2.29 -10 6 -5 46.13 1.97 -10 6 -5 43.23 3.33 10 6 5 50.21 3.34 10 6 5 45.24 1.82 10 6 6 13.52 1.18 -10 6 -6 16.09 1.32 -10 6 -6 16.43 2.52 -10 6 -7 29.37 1.76 10 6 7 28.23 1.64 -10 6 -7 26.13 2.84 10 6 8 4.50 1.10 -10 6 -8 4.59 1.16 -10 6 -8 2.02 1.77 -10 6 -9 9.52 2.25 10 6 9 6.80 1.27 -10 6 -9 7.25 1.36 -10 6 -9 6.20 0.57 -10 6 -10 -0.10 1.15 10 6 10 0.72 1.04 -10 6 -10 0.70 1.75 -10 6 -11 85.08 3.58 10 6 11 82.53 3.35 -10 6 -11 86.71 4.35 10 6 12 1.02 1.22 -10 6 -12 -0.16 1.78 -10 6 -12 0.94 1.37 -10 -6 13 14.64 2.40 10 6 13 15.25 1.77 -10 6 -13 14.16 2.25 -10 6 -13 13.76 1.82 -10 6 -14 5.39 1.90 10 6 14 6.50 1.67 -10 -6 14 6.55 2.13 -10 -6 15 42.66 4.66 -10 6 -15 32.71 2.73 -10 -6 16 9.21 4.00 -10 -6 17 9.38 4.21 10 8 -15 -2.04 1.63 10 8 -14 51.61 3.04 10 8 -13 6.19 1.56 -10 8 13 6.53 1.67 10 8 -12 5.70 1.48 -10 8 12 10.03 1.71 -10 8 11 1.76 1.31 -10 8 11 1.72 1.77 10 8 -11 2.32 1.28 -10 8 10 14.60 2.22 -10 8 10 17.04 1.70 10 8 -10 14.27 1.60 -10 8 9 -0.18 1.06 -10 8 9 1.79 1.89 10 8 -9 1.23 1.15 -10 8 8 249.77 8.36 10 8 -8 247.82 6.80 10 8 -7 1.23 0.95 -10 8 7 2.04 1.81 10 8 -6 81.88 2.94 -10 8 6 76.80 4.25 10 8 -6 74.13 4.03 10 8 -5 0.60 2.08 10 8 -5 3.79 0.98 -10 8 5 1.72 1.90 -10 8 4 5.05 1.92 -10 8 4 7.34 1.92 10 8 -4 3.65 2.00 -10 8 3 1.32 1.72 10 8 -3 1.65 2.07 10 8 -3 2.25 1.74 -10 8 3 2.16 1.87 -10 8 2 68.37 4.19 10 8 -2 69.76 3.53 -10 8 2 67.41 3.39 10 8 -2 69.10 3.94 -10 8 1 -0.80 1.67 10 8 -1 -0.72 1.72 -10 8 1 1.20 1.90 10 8 -1 2.88 2.25 -10 8 0 328.96 9.08 10 8 0 333.18 9.94 10 8 0 354.37 9.36 10 8 1 -0.67 1.53 10 8 1 2.55 2.31 -10 8 -1 -0.10 1.54 10 8 2 76.30 3.31 10 8 2 75.40 4.05 -10 8 -2 68.90 3.14 10 8 3 6.72 2.54 -10 8 -3 5.18 1.64 -10 8 -3 3.23 1.97 10 8 3 2.69 1.51 -10 8 -4 9.27 1.65 10 8 4 10.65 2.59 10 8 4 5.99 1.55 -10 8 -4 7.45 2.16 10 8 5 3.33 1.40 -10 8 -5 5.21 2.03 -10 8 -6 86.20 3.15 -10 8 -6 86.14 4.63 10 8 6 79.88 3.17 10 8 7 -0.30 1.15 -10 8 -7 3.26 1.17 -10 8 -7 0.98 1.84 -10 8 -8 255.92 7.12 10 8 8 252.83 6.89 10 8 8 264.11 6.76 -10 8 -8 273.94 8.84 -10 8 -9 3.17 1.94 -10 8 -9 3.27 1.36 10 8 9 0.95 0.98 10 8 9 1.07 1.07 -10 8 -10 16.17 2.43 -10 8 -10 15.71 1.75 10 8 10 13.33 1.48 10 8 10 14.32 1.26 10 8 11 1.75 1.28 -10 8 -11 2.25 1.37 -10 8 -11 3.53 1.85 -10 8 -12 4.35 1.60 10 8 12 4.48 1.40 -10 8 -12 3.07 1.83 10 8 13 4.97 1.63 -10 8 -13 7.09 1.99 -10 8 -13 5.73 1.66 -10 8 -14 58.86 3.54 -10 8 -14 59.78 3.33 -10 8 -15 0.30 1.76 -10 8 -15 -1.22 1.73 -10 8 -16 98.43 4.53 10 10 -18 4.38 1.95 10 10 -17 4.60 1.87 10 10 -16 -0.31 1.72 10 10 -15 78.46 3.91 10 10 -14 0.14 1.58 10 10 -13 2.30 1.65 10 10 -12 4.30 1.59 -10 10 12 3.13 1.52 10 10 -11 22.50 2.06 -10 10 11 22.41 2.10 10 10 -10 8.40 1.50 10 10 -9 33.20 2.22 10 10 -8 4.05 1.37 10 10 -7 123.45 4.19 10 10 -5 6.36 2.10 10 10 -4 2.05 1.94 10 10 -3 15.61 2.25 10 10 -2 3.28 1.83 10 10 -2 8.58 2.37 10 -10 2 8.35 2.37 -10 10 2 6.69 2.24 10 10 -1 84.02 4.49 -10 10 1 84.07 3.81 -10 10 1 82.60 4.66 10 -10 1 90.89 5.09 10 10 -1 84.81 4.06 10 10 0 9.62 2.65 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2.36 1.93 10 12 -16 0.16 2.02 10 12 -15 0.16 1.76 10 12 -14 0.45 1.70 10 12 -13 0.43 1.64 10 12 -12 134.30 5.06 10 12 -11 2.14 1.54 10 12 -10 67.50 3.33 10 12 -9 6.62 1.64 10 12 -8 10.96 1.67 10 -12 6 16.59 2.75 10 -12 5 4.16 2.38 10 -12 4 267.49 9.45 10 -12 3 1.66 2.22 10 12 -2 55.23 3.47 10 -12 2 57.83 4.24 10 12 -1 1.70 2.03 10 -12 1 3.41 2.22 10 12 0 10.89 2.20 10 -12 0 5.94 2.33 10 12 1 3.54 1.82 -10 12 -1 0.87 1.54 10 -12 -1 1.50 2.13 -10 12 -2 55.01 2.81 10 12 2 60.19 3.33 -10 12 -3 -1.64 1.51 10 12 3 1.22 1.72 -10 12 -4 247.64 6.74 10 -12 -4 231.60 9.19 -10 12 -5 3.45 1.28 10 12 5 2.70 1.71 10 -12 -5 2.57 2.46 10 12 6 16.96 2.02 10 -12 -6 19.30 3.02 10 12 7 3.51 1.60 10 -12 -7 6.16 2.55 10 12 8 7.10 1.70 10 -12 -8 4.11 2.52 -10 12 -9 8.17 1.86 10 -12 -9 6.15 2.71 10 -12 -10 66.40 4.70 -10 12 -10 66.76 3.50 -10 12 -11 3.97 1.82 -10 12 -12 144.88 5.51 -10 12 -13 3.89 1.95 -10 12 -14 0.16 1.98 -10 12 -15 0.51 2.12 -10 12 -16 3.41 2.21 10 14 -15 15.36 2.44 10 14 -14 1.92 1.91 10 14 -13 15.16 2.41 10 14 -12 2.61 1.79 10 14 -11 104.14 4.51 10 14 -10 1.77 1.71 10 -14 8 1.16 2.33 10 -14 7 19.20 2.96 10 -14 6 4.02 2.33 10 -14 5 59.72 4.35 10 -14 4 2.45 2.33 10 -14 3 105.65 5.66 10 -14 2 2.02 2.36 10 -14 1 15.91 3.03 10 -14 0 2.34 2.41 10 -14 -1 14.82 3.00 10 14 2 3.47 2.12 10 14 3 100.28 4.50 -10 14 -3 117.68 4.09 10 14 4 -0.13 1.83 -10 14 -4 -1.03 1.49 10 -14 -4 -2.17 2.49 -10 14 -5 63.76 2.57 10 14 5 54.32 3.26 10 -14 -5 58.76 4.63 -10 14 -6 9.52 1.24 10 14 6 9.79 2.05 10 -14 -6 6.53 2.74 10 14 7 17.71 2.27 10 -14 -7 18.20 3.12 10 -14 -8 0.27 2.54 10 -14 -9 -1.35 2.47 -10 14 -10 4.56 2.05 10 -14 -10 3.20 2.64 10 -14 -11 98.80 5.92 -10 14 -11 109.55 4.87 -10 14 -12 3.65 2.11 10 -14 -12 2.11 2.74 -10 14 -13 12.76 2.54 10 -14 -13 8.08 3.02 -10 14 -14 2.80 2.10 -10 14 -15 12.20 2.67 10 16 -14 32.42 3.06 10 16 -13 2.59 1.96 10 16 -12 7.20 2.24 10 16 -11 3.08 2.12 10 -16 10 0.71 2.52 10 -16 9 5.06 2.76 10 -16 8 115.33 5.94 10 -16 7 1.72 2.51 10 -16 6 37.73 3.73 10 -16 5 3.05 2.47 10 -16 4 19.65 3.17 10 -16 3 3.17 2.54 10 -16 2 14.23 3.03 10 -16 1 1.37 2.53 10 -16 0 152.93 7.31 10 -16 -1 -1.69 2.53 -10 16 -4 19.80 1.92 10 -16 -4 16.23 3.12 -10 16 -5 1.69 1.41 10 -16 -5 1.75 2.67 10 -16 -6 39.81 4.23 10 -16 -7 2.32 2.55 10 -16 -8 122.32 6.60 10 -16 -9 2.01 2.94 10 -16 -10 -0.28 2.84 10 -16 -11 0.28 2.77 -10 16 -11 1.93 2.01 10 -16 -12 4.17 2.78 -10 16 -12 9.00 2.64 -10 16 -13 6.23 2.44 10 18 -11 15.01 2.61 10 -18 9 32.21 3.69 10 -18 8 0.77 2.65 10 -18 7 87.97 5.41 10 -18 6 1.85 2.68 10 -18 5 0.54 2.57 10 -18 4 3.04 2.72 10 -18 3 9.01 2.94 10 -18 2 0.86 2.65 10 -18 1 77.06 5.40 10 -18 0 1.78 2.62 10 -18 -1 75.41 5.38 10 -18 -2 5.17 2.96 10 -18 -4 0.62 2.79 -11 1 16 1.62 2.83 -11 1 16 0.26 3.25 -11 1 15 -0.23 2.51 -11 -1 -15 -0.81 1.84 -11 1 15 1.25 2.93 -11 1 14 -3.41 3.06 -11 -1 -14 1.84 1.75 -11 1 14 1.18 1.82 -11 1 13 3.32 2.98 -11 -1 -13 2.05 1.74 -11 1 13 -0.53 1.96 -11 1 12 0.92 2.73 -11 -1 -12 3.49 1.95 -11 1 12 1.46 1.64 -11 -1 -11 14.72 2.35 -11 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8.81 2.74 -13 3 10 2.39 2.94 -13 3 10 -1.76 2.50 -13 3 9 0.93 2.76 -13 3 9 1.71 2.36 -13 3 8 0.45 2.76 -13 3 8 4.77 2.37 -13 3 7 3.65 2.79 -13 3 7 0.60 2.23 -13 3 6 0.42 2.66 -13 3 6 -1.73 2.41 -13 3 5 6.70 2.70 -13 3 5 8.48 2.42 -13 3 4 6.18 2.70 -13 3 4 1.76 2.11 -13 3 3 16.33 2.91 -13 3 3 7.64 2.23 -13 3 2 4.33 2.53 -13 3 2 0.31 1.98 -13 3 1 1.02 1.93 13 3 0 -1.46 2.18 -13 3 0 -0.13 1.73 13 3 1 -0.84 1.95 -13 3 -1 1.09 1.55 13 3 2 -0.28 1.95 -13 3 -2 0.87 1.50 13 3 3 12.31 2.19 -13 3 -3 11.20 1.71 13 3 4 1.44 2.06 -13 -3 4 5.14 2.23 -13 3 -4 3.68 1.31 13 3 5 3.49 1.95 -13 3 -5 6.65 1.26 -13 -3 5 8.41 2.40 13 3 6 -0.13 2.12 -13 -3 6 2.12 2.40 13 3 7 -0.77 1.99 -13 -3 7 3.86 2.34 13 3 8 2.90 1.89 -13 -3 8 3.83 2.64 13 3 9 -1.60 2.04 -13 -3 9 2.44 2.57 -13 -3 10 2.76 2.57 -13 -3 11 8.56 3.05 -13 -3 12 10.03 3.90 -13 -3 12 7.07 3.13 -13 -3 13 6.24 3.06 -13 5 12 -0.75 2.89 -13 5 12 0.92 2.66 -13 5 11 2.40 2.76 -13 5 11 6.23 2.64 -13 5 10 4.87 2.93 -13 5 10 9.77 2.67 -13 5 9 4.24 2.71 -13 5 9 3.18 2.40 -13 5 8 -3.46 2.84 -13 5 7 -0.83 2.49 -13 5 6 15.16 3.10 -13 5 5 -0.58 2.45 -13 5 4 2.77 2.49 -13 5 3 4.98 2.53 -13 5 2 16.04 2.87 -13 5 1 5.79 2.62 -13 5 0 5.10 2.29 -13 5 -1 2.33 1.67 -13 5 -2 10.78 1.95 13 5 3 0.15 2.27 -13 5 -3 -0.63 1.43 13 5 4 -0.89 2.27 -13 5 -4 0.09 1.40 13 5 5 0.14 2.22 -13 5 -5 1.17 1.23 13 5 6 6.52 2.32 -13 5 -6 7.86 1.28 13 5 7 -0.14 2.23 -13 5 -7 0.45 0.92 13 5 8 0.58 2.18 13 5 9 3.73 2.38 13 5 10 6.73 2.36 -13 7 11 -2.37 3.05 -13 7 10 -2.98 3.08 -13 7 9 7.31 2.90 -13 7 8 -0.21 2.76 -13 7 7 11.55 2.87 -13 7 6 -1.17 2.49 -13 7 5 3.36 2.49 -13 7 4 2.34 2.45 -13 7 3 6.56 2.55 -13 7 2 1.33 2.36 -13 7 1 15.99 2.66 -13 7 0 4.51 2.35 -13 7 -1 17.49 2.68 -13 7 -6 0.54 1.21 13 7 6 2.15 0.74 -13 7 -7 12.96 1.40 13 7 7 13.99 1.15 13 7 8 3.17 1.04 -13 7 -8 4.20 1.01 -13 9 11 -0.24 3.02 -13 9 10 2.96 2.80 -13 9 9 -2.62 2.93 13 9 -9 1.34 1.07 -13 9 8 -3.34 2.84 13 9 -8 -0.61 1.03 -13 9 7 0.20 2.53 13 9 -7 2.32 1.00 13 9 -6 14.38 1.17 -13 9 6 16.60 2.93 13 9 -5 4.42 0.89 -13 9 5 -0.75 2.43 13 9 -4 -0.16 0.71 -13 9 4 -2.52 2.42 13 9 -3 1.01 0.64 -13 9 3 -0.17 2.15 13 9 -2 20.52 1.02 -13 9 2 20.72 2.79 13 9 -1 3.62 0.63 -13 9 1 2.97 2.23 -13 9 0 0.75 2.16 -13 9 -1 4.52 2.26 -13 9 -2 30.19 2.83 13 9 2 21.07 1.01 13 9 3 0.21 0.64 13 9 4 -0.13 0.69 13 9 5 3.22 0.86 13 9 6 13.63 1.19 -13 11 10 1.64 3.01 13 11 -9 1.73 1.28 -13 11 9 1.12 2.71 13 11 -8 0.76 1.17 -13 11 8 2.36 2.53 13 11 -7 3.11 1.19 -13 11 7 4.08 2.56 13 11 -6 0.79 1.05 -13 11 6 -1.36 2.51 -13 11 5 14.87 2.86 13 11 -5 15.97 1.40 13 11 -4 2.17 1.01 -13 11 4 -2.13 2.40 -13 11 3 10.41 2.47 13 11 -3 16.08 1.33 -13 11 2 -0.66 2.39 -13 11 1 2.79 2.19 -13 11 0 2.22 2.06 -13 11 -1 6.77 2.23 -13 11 -2 3.54 2.12 -13 11 -3 19.13 2.49 -13 13 8 -1.76 2.84 -13 13 7 -0.42 2.76 -13 13 6 7.89 2.76 13 13 -6 11.67 1.64 13 13 -5 4.41 1.32 -13 13 5 -1.16 2.35 -13 13 4 -1.09 2.45 -13 13 3 -0.17 2.29 -13 13 2 16.64 2.72 -13 13 1 -0.16 2.31 -13 13 0 -2.09 2.24 -13 13 -1 2.39 2.18 -13 13 -2 19.20 2.69 -13 13 -3 4.60 2.20 -13 13 -4 8.54 2.23 -13 15 7 3.09 3.20 -13 15 6 -0.84 2.98 -13 15 5 1.79 2.78 -13 15 4 1.72 2.74 -13 15 3 2.54 2.43 -13 15 2 1.02 2.42 -13 15 1 9.46 2.56 -13 15 0 -0.15 2.28 -13 15 -1 11.71 2.43 -13 17 5 -2.31 3.08 -13 17 4 -2.00 2.95 -13 17 3 -1.50 2.96 -13 17 2 10.62 2.80 -13 17 1 -1.01 2.49 -14 0 0 42.47 2.89 -14 0 1 1.14 1.82 -14 0 -1 0.84 1.75 -14 0 2 39.93 3.12 -14 0 3 2.18 2.23 -14 0 4 7.35 2.46 -14 0 5 -0.19 2.29 -14 0 6 42.52 3.69 -14 0 6 40.18 4.16 -14 0 7 1.69 2.44 -14 0 7 5.41 3.24 -14 0 8 48.66 4.10 -14 0 8 66.21 4.91 -14 0 9 1.36 2.81 -14 0 9 6.39 3.49 -14 0 10 21.29 3.44 -14 0 10 26.39 4.32 -14 0 11 1.68 2.88 -14 0 11 6.00 3.54 -14 2 11 13.60 3.27 -14 2 11 14.06 3.93 -14 2 10 -0.47 2.86 -14 2 10 7.01 3.45 -14 2 9 5.42 2.77 -14 2 9 13.77 3.54 -14 2 8 0.88 2.59 -14 2 8 5.77 3.21 -14 2 7 10.56 2.72 -14 2 7 16.73 3.40 -14 2 6 1.62 2.44 -14 2 6 3.75 3.08 -14 2 5 6.00 2.40 -14 2 5 4.69 3.07 -14 2 4 0.18 2.37 -14 2 4 3.88 2.86 -14 2 3 1.56 2.17 -14 2 2 0.97 2.06 -14 2 1 10.55 2.29 -14 2 0 4.87 1.94 -14 2 -1 15.91 2.13 -14 2 -2 6.26 1.70 -14 -2 2 5.93 2.25 -14 2 -3 5.31 1.52 -14 -2 3 5.53 2.04 -14 -2 4 5.37 2.54 -14 2 -4 4.07 1.45 14 2 4 -0.14 1.96 14 2 5 1.97 1.80 -14 -2 5 3.42 2.34 14 2 6 -0.13 1.86 -14 -2 6 2.01 2.51 -14 -2 7 12.67 2.94 14 2 7 10.54 2.09 -14 -2 8 1.55 2.39 -14 -2 9 9.41 3.12 -14 -2 10 5.40 3.64 -14 -2 10 4.51 2.99 -14 -2 11 8.79 3.21 -14 4 11 -1.18 2.81 -14 4 11 1.05 3.33 -14 4 10 33.01 3.65 -14 4 10 42.14 4.45 -14 4 9 -0.22 2.61 -14 4 9 2.94 3.19 -14 4 8 2.83 2.55 -14 4 8 10.87 3.35 -14 4 7 -1.26 2.64 -14 4 7 3.44 3.22 -14 4 6 34.30 3.40 -14 4 6 33.53 3.85 -14 4 5 0.19 2.22 -14 4 5 2.51 2.83 -14 4 4 68.44 4.20 -14 4 4 67.21 4.47 -14 4 3 -0.88 2.17 -14 4 3 7.48 2.82 -14 4 2 50.62 3.49 -14 4 2 53.91 4.08 -14 4 1 0.16 1.97 -14 4 0 7.77 2.13 -14 4 -1 0.39 1.72 -14 4 -2 47.60 2.91 -14 4 -3 0.73 1.41 -14 4 -4 62.99 2.91 -14 4 -5 1.65 1.31 -14 -4 11 5.63 3.29 -14 6 10 1.15 2.65 -14 6 10 4.20 3.27 -14 6 9 3.36 2.77 -14 6 9 4.76 3.17 -14 6 8 -0.46 2.89 -14 6 7 5.75 2.81 -14 6 6 2.14 2.78 -14 6 5 18.15 3.14 -14 6 4 3.60 2.72 -14 6 3 19.91 3.27 -14 6 2 7.37 2.53 -14 6 1 8.51 2.70 -14 6 0 6.43 2.68 -14 6 -1 2.22 1.86 -14 6 -2 1.14 1.65 -14 6 -3 15.85 1.97 -14 6 -4 1.93 1.50 -14 6 -5 11.87 1.62 -14 6 -6 6.55 1.38 -14 6 -7 10.15 1.23 -14 8 9 -1.90 3.11 -14 8 8 48.29 4.28 -14 8 7 2.17 2.81 -14 8 6 39.29 3.78 -14 8 5 -1.61 2.79 -14 8 4 1.17 2.64 -14 8 3 1.13 2.45 -14 8 2 39.65 3.55 -14 8 1 3.43 2.44 -14 8 0 79.59 4.42 -14 8 -1 1.85 2.44 -14 8 -6 32.87 2.18 -14 10 9 7.21 3.09 -14 10 8 0.23 3.12 -14 10 7 32.42 3.79 -14 10 6 3.37 2.96 -14 10 5 2.83 2.54 -14 10 4 -0.77 2.71 -14 10 3 6.30 2.66 -14 10 2 1.07 2.42 -14 10 1 24.35 3.10 -14 10 0 4.72 2.42 -14 10 -1 25.67 3.03 -14 10 -2 8.66 2.62 -14 12 7 -2.16 3.22 -14 12 6 9.99 2.99 -14 12 5 -2.63 2.99 -14 12 4 54.45 4.14 -14 12 3 -1.69 2.77 -14 12 2 25.80 3.25 -14 12 1 1.88 2.41 -14 12 0 9.15 2.71 -14 12 -1 3.83 2.46 -14 12 -2 29.32 3.07 -14 14 6 0.64 3.08 -14 14 5 15.41 3.20 -14 14 4 -0.98 3.00 -14 14 3 32.33 3.63 -14 14 2 1.10 2.77 -14 14 1 -0.34 2.87 -14 14 0 0.49 2.56 -14 16 5 -2.92 3.17 -14 16 4 6.62 2.98 -14 16 3 -3.26 3.18 -14 16 2 3.51 2.88 -15 1 10 0.73 2.76 -15 1 9 1.41 2.96 -15 1 9 5.86 3.51 -15 1 8 1.36 2.83 -15 1 8 2.31 3.18 -15 1 7 0.88 2.54 -15 1 7 10.80 3.65 -15 1 6 1.05 2.46 -15 1 5 3.39 2.51 -15 1 4 -0.56 2.29 -15 1 3 0.18 2.08 -15 1 2 2.46 2.17 -15 1 1 1.80 1.97 -15 1 0 2.20 1.93 -15 1 -1 2.64 1.73 -15 -1 2 1.46 2.16 -15 -1 3 2.09 2.36 -15 -1 4 4.65 2.49 -15 -1 5 5.73 2.52 -15 -1 6 1.25 2.52 -15 -1 7 2.41 2.57 -15 -1 8 1.37 2.61 -15 -1 9 8.30 3.08 -15 -1 10 1.22 2.85 -15 3 9 -1.65 2.81 -15 3 9 2.35 3.66 -15 3 8 4.56 2.76 -15 3 8 12.49 3.67 -15 3 7 -1.10 2.60 -15 3 7 6.02 3.37 -15 3 6 2.54 2.52 -15 3 6 8.15 3.23 -15 3 5 -1.22 2.60 -15 3 5 5.17 3.07 -15 3 4 -0.77 2.41 -15 3 4 9.22 3.29 -15 3 3 2.00 2.32 -15 3 2 2.73 2.19 -15 3 1 0.95 2.01 -15 3 0 0.29 1.87 -15 3 -1 3.38 1.80 -15 3 -2 2.93 1.74 -15 3 -3 2.98 1.62 -15 3 -4 2.25 1.47 -15 -3 7 6.08 3.01 -15 -3 8 5.41 3.00 -15 -3 9 4.16 3.45 -15 5 9 6.13 3.19 -15 5 8 0.69 2.86 -15 5 8 6.00 3.45 -15 5 7 0.44 2.55 -15 5 7 2.15 2.97 -15 5 6 -0.43 2.40 -15 5 6 0.92 3.10 -15 5 5 1.84 2.44 -15 5 5 3.51 3.18 -15 5 4 -2.15 2.34 -15 5 4 6.13 3.21 -15 5 3 -1.68 2.41 -15 5 3 2.86 2.84 -15 5 2 2.11 2.25 -15 5 2 9.95 3.16 -15 5 1 -0.49 2.04 -15 5 0 -0.31 2.00 -15 5 -1 1.66 1.79 -15 5 -2 2.14 1.74 -15 5 -3 0.89 1.63 -15 5 -4 1.83 1.57 -15 5 -5 4.59 1.51 -15 7 8 -0.69 2.81 -15 7 8 6.60 3.54 -15 7 7 -1.12 2.63 -15 7 7 3.54 3.40 -15 7 6 4.79 3.32 -15 7 5 3.75 3.15 -15 7 4 3.37 3.06 -15 7 3 6.84 3.19 -15 7 2 8.11 3.05 -15 7 1 -0.68 2.10 -15 7 1 3.34 2.92 -15 7 0 -1.91 2.16 -15 7 -1 1.62 1.94 -15 7 -2 3.50 2.02 -15 7 -3 2.20 1.88 -15 7 -4 -0.33 1.61 -15 7 -5 -1.11 1.60 -15 9 7 -0.93 3.33 -15 9 6 5.39 3.30 -15 9 5 7.17 3.17 -15 9 4 -0.21 2.89 -15 9 3 5.48 3.12 -15 9 2 9.46 3.12 -15 9 1 9.31 2.96 -15 9 0 4.04 2.92 -15 11 6 2.67 3.19 -15 11 5 -3.02 3.18 -15 11 4 -2.08 2.78 -15 11 3 0.20 3.18 -15 11 2 5.46 3.00 -15 11 1 6.10 2.91 -15 11 0 5.36 3.02 -15 11 -1 9.37 2.98 -15 13 5 -1.97 3.33 -15 13 4 -2.29 3.15 -15 13 3 2.22 3.04 -15 13 2 0.97 3.13 -15 13 1 2.80 3.03 -15 15 4 -5.36 3.53 -16 0 1 8.14 2.33 -16 0 2 28.60 3.11 -16 0 3 7.23 2.70 -16 0 4 78.59 4.74 -16 0 5 4.90 2.67 -16 0 6 52.09 4.37 -16 0 7 3.16 2.91 -16 0 8 172.52 7.55 -16 2 8 -0.47 2.99 -16 2 7 91.52 5.53 -16 2 6 6.95 3.01 -16 2 5 42.22 3.85 -16 2 4 0.98 2.54 -16 2 3 94.75 4.98 -16 2 2 8.72 2.51 -16 2 1 75.84 4.12 -16 2 0 0.43 2.09 -16 2 -1 76.43 3.81 -16 2 -2 13.95 2.25 -16 -2 6 14.72 3.36 -16 -2 7 83.00 5.35 -16 -2 8 2.65 3.16 -16 4 7 -0.23 3.10 -16 4 6 5.51 2.98 -16 4 6 12.99 3.83 -16 4 5 1.90 2.62 -16 4 5 11.47 3.73 -16 4 4 201.24 7.72 -16 4 3 3.23 2.60 -16 4 2 30.54 3.29 -16 4 1 3.12 2.21 -16 4 0 81.24 4.17 -16 4 -1 6.43 2.05 -16 4 -2 33.01 2.74 -16 4 -3 3.68 1.75 -16 6 7 59.08 4.69 -16 6 6 4.47 2.95 -16 6 6 11.52 3.81 -16 6 5 42.07 4.06 -16 6 5 60.36 5.01 -16 6 4 -0.82 2.82 -16 6 4 3.60 3.56 -16 6 3 81.46 4.81 -16 6 3 97.51 5.71 -16 6 2 3.68 2.49 -16 6 1 45.86 3.61 -16 6 0 -0.48 2.22 -16 6 -1 46.80 3.32 -16 6 -2 5.85 2.02 -16 6 -3 83.67 3.83 -16 8 5 -0.65 2.79 -16 8 5 9.05 3.63 -16 8 4 33.85 3.71 -16 8 4 47.38 4.54 -16 8 3 1.79 2.56 -16 8 3 8.99 3.40 -16 8 2 8.49 2.60 -16 8 2 17.79 3.64 -16 8 1 0.89 2.43 -16 8 0 153.04 6.08 -16 8 -1 0.15 2.22 -16 8 -2 12.25 2.36 -16 10 5 13.78 3.92 -16 10 4 4.05 3.63 -16 10 3 37.69 4.24 -16 10 2 6.35 3.34 -16 10 1 62.10 4.69 -16 12 4 80.22 5.47 -16 12 3 0.22 3.32 -16 12 2 18.29 3.72 -17 1 6 4.42 3.08 -17 1 5 -0.42 2.92 -17 1 4 3.77 2.72 -17 1 3 2.05 2.67 -17 1 2 4.19 2.67 -17 1 1 3.39 2.38 -17 -1 6 0.90 2.92 -17 3 5 1.71 2.92 -17 3 4 2.82 3.00 -17 3 3 4.55 2.69 -17 3 2 3.01 2.54 -17 3 1 1.63 2.39 -17 3 0 2.84 2.23 -17 3 -1 3.55 2.11 -17 5 5 0.44 2.91 -17 5 4 0.21 2.69 -17 5 3 1.77 2.63 -17 5 2 4.77 2.69 -17 5 1 -1.87 2.44 -17 5 0 -0.78 2.18 -17 7 4 0.21 3.00 -17 7 3 1.21 2.78 -17 7 2 -0.57 2.71 -17 7 1 2.49 2.53 -17 7 0 -0.16 2.61 -17 9 3 -2.48 3.12 -17 9 3 2.04 3.65 -17 9 2 7.45 2.82 -17 9 1 -0.18 2.62 -18 2 4 0.81 2.91 -18 2 3 -0.95 2.66 -18 2 2 1.79 2.78 -18 4 3 3.30 2.95 0 0 0 0.00 0.00 TITL FCC-121-01-1 in C222(1) REM C222(1) (#20 in standard setting) CELL 0.71073 12.962052 18.787490 17.666625 90.0000 90.0000 90.0000 ZERR 60.00 0.000746 0.001310 0.000947 0.0000 0.0000 0.0000 LATT -7 SYMM -x,-y, z+1/2 SYMM -x, y,-z+1/2 SYMM x,-y,-z SFAC C H N I Pb UNIT 60.00 60.00 60.00 60.00 60.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 75365 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.378 _oxdiff_exptl_absorpt_empirical_full_min 0.732 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.50366(5) 0.87540(4) 1.11965(4) 0.0313(2) Uani 1 1 d . . . . . Pb2 Pb 0.50125(5) 0.62501(4) 0.87857(4) 0.0313(2) Uani 1 1 d . . . . . I1 I 0.500000 0.75564(12) 1.250000 0.0308(5) Uani 1 2 d S T P . . I2 I 0.500000 0.99043(13) 1.250000 0.0333(5) Uani 1 2 d S T P . . I3 I 0.5303(2) 1.000000 1.000000 0.0516(7) Uani 1 2 d S T P . . I4 I 0.500000 0.50276(13) 0.750000 0.0326(5) Uani 1 2 d S T P . . I5 I 0.4762(3) 0.500000 1.000000 0.0668(9) Uani 1 2 d S T P . . I6 I 0.500000 0.74265(13) 0.750000 0.0342(6) Uani 1 2 d S T P . . I7 I 0.75160(14) 0.86566(7) 1.12723(5) 0.0429(3) Uani 1 1 d . . . . . I8 I 0.75135(15) 0.60834(7) 0.88967(6) 0.0575(4) Uani 1 1 d . . . . . I9 I 0.4909(3) 0.74543(15) 1.00227(14) 0.0780(6) Uani 1 1 d . . . . . N2 N 0.744(2) 0.9392(10) 0.8529(8) 0.083(5) Uani 1 1 d . U . . . H2 H 0.734808 0.979246 0.875290 0.100 Uiso 1 1 calc R U . . . C2 C 0.747(2) 0.8540(13) 0.6578(9) 0.085(6) Uani 1 1 d D U . . . H2A H 0.749507 0.803493 0.644252 0.102 Uiso 0.5 1 calc R U P A 1 C3 C 0.748(2) 0.8671(9) 0.7430(6) 0.042(3) Uani 1 1 d . U . . . C4 C 0.751(2) 0.8093(9) 0.7861(8) 0.056(4) Uani 1 1 d . U . . . H4 H 0.748149 0.765066 0.762575 0.067 Uiso 1 1 calc R U . . . C5 C 0.758(2) 0.8115(11) 0.8635(9) 0.064(5) Uani 1 1 d . U . . . H5 H 0.763719 0.770996 0.893448 0.077 Uiso 1 1 calc R U . . . C6 C 0.7543(19) 0.8783(12) 0.8920(11) 0.075(5) Uani 1 1 d . U . . . H6 H 0.759627 0.882521 0.944281 0.091 Uiso 1 1 calc R U . . . C7 C 0.750(2) 0.9345(9) 0.7757(9) 0.051(3) Uani 1 1 d . U . . . H7 H 0.754749 0.975208 0.745981 0.061 Uiso 1 1 calc R U . . . N1A N 0.821(3) 0.898(2) 0.617(2) 0.083(10) Uani 0.5 1 d D U P B 1 H1AA H 0.830971 0.879242 0.570626 0.100 Uiso 0.5 1 d R U P B 1 H1AB H 0.880681 0.897722 0.641706 0.100 Uiso 0.5 1 d R U P B 1 H1AC H 0.797871 0.941922 0.612266 0.100 Uiso 0.5 1 d R U P B 1 C1A C 0.657(3) 0.892(2) 0.625(2) 0.043(8) Uani 0.5 1 d . U P B 1 H1AD H 0.596411 0.880657 0.653503 0.065 Uiso 0.5 1 d R U P B 1 H1AE H 0.648111 0.877597 0.573353 0.065 Uiso 0.5 1 d R U P B 1 H1AF H 0.669521 0.942317 0.627103 0.065 Uiso 0.5 1 d R U P B 1 N1B N 0.655(3) 0.859(2) 0.615(2) 0.080(10) Uani 0.5 1 d D U P B 2 H1BA H 0.657703 0.872887 0.568661 0.096 Uiso 0.5 1 calc R U P B 2 H1BB H 0.596990 0.848470 0.635373 0.096 Uiso 0.5 1 calc R U P B 2 C1B C 0.852(3) 0.872(3) 0.626(3) 0.062(9) Uani 0.5 1 d . U P B 2 H1BC H 0.866858 0.921569 0.632893 0.093 Uiso 0.5 1 d R U P B 2 H1BD H 0.852288 0.861139 0.572643 0.093 Uiso 0.5 1 d R U P B 2 H1BE H 0.903728 0.843899 0.650833 0.093 Uiso 0.5 1 d R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.0352(5) 0.0327(4) 0.0260(4) -0.0007(3) 0.0020(3) 0.0007(8) Pb2 0.0381(5) 0.0302(4) 0.0255(4) 0.0001(3) -0.0008(3) -0.0032(8) I1 0.0267(13) 0.0342(13) 0.0317(10) 0.000 0.0032(10) 0.000 I2 0.0385(12) 0.0317(12) 0.0299(10) 0.000 -0.0005(11) 0.000 I3 0.0615(16) 0.0507(16) 0.0425(12) 0.0214(10) 0.000 0.000 I4 0.0405(12) 0.0283(11) 0.0292(10) 0.000 0.0021(11) 0.000 I5 0.101(2) 0.0573(18) 0.0418(13) 0.0274(12) 0.000 0.000 I6 0.0429(16) 0.0301(13) 0.0295(10) 0.000 -0.0001(11) 0.000 I7 0.0251(5) 0.0466(7) 0.0571(6) 0.0097(4) -0.0060(8) 0.0020(10) I8 0.0288(5) 0.0760(11) 0.0676(7) -0.0050(6) -0.0027(9) 0.0039(11) I9 0.1178(16) 0.0673(12) 0.0488(8) -0.0354(7) 0.0075(7) -0.0280(10) N2 0.096(12) 0.072(10) 0.082(8) -0.024(7) -0.008(13) 0.030(13) C2 0.086(9) 0.123(16) 0.047(7) 0.000(8) -0.008(9) 0.016(14) C3 0.022(6) 0.064(9) 0.039(5) -0.004(5) -0.002(6) 0.002(11) C4 0.042(8) 0.052(9) 0.074(7) -0.006(6) -0.015(11) -0.021(12) C5 0.052(11) 0.075(10) 0.066(7) 0.042(7) 0.010(11) 0.003(13) C6 0.064(11) 0.103(12) 0.060(9) 0.006(7) -0.044(10) 0.026(14) C7 0.027(7) 0.053(9) 0.073(7) 0.000(6) 0.010(12) -0.012(12) N1A 0.085(14) 0.11(2) 0.059(15) -0.005(15) 0.009(14) 0.022(15) C1A 0.064(12) 0.043(17) 0.023(13) -0.002(13) -0.014(11) -0.032(13) N1B 0.099(13) 0.10(2) 0.043(15) 0.014(17) -0.023(12) -0.014(17) C1B 0.090(13) 0.07(2) 0.024(14) -0.014(16) 0.007(12) 0.032(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag I1 Pb1 I7 86.86(3) . . ? I1 Pb1 I8 94.94(3) . 8_467 ? I2 Pb1 I1 87.50(4) . . ? I2 Pb1 I3 89.00(4) . . ? I2 Pb1 I7 91.35(3) . . ? I2 Pb1 I8 87.59(3) . 8_467 ? I2 Pb1 I9 172.48(6) . . ? I3 Pb1 I1 173.51(5) . . ? I3 Pb1 I7 87.76(6) . . ? I3 Pb1 I8 90.37(6) . 8_467 ? I3 Pb1 I9 97.85(5) . . ? I7 Pb1 I8 177.87(5) . 8_467 ? I9 Pb1 I1 85.97(5) . . ? I9 Pb1 I7 92.02(7) . . ? I9 Pb1 I8 89.25(7) . 8_467 ? I4 Pb2 I7 90.64(3) . 8_467 ? I4 Pb2 I8 88.80(3) . . ? I5 Pb2 I4 87.08(4) . . ? I5 Pb2 I7 87.69(6) . 8_467 ? I5 Pb2 I8 89.43(7) . . ? I6 Pb2 I4 89.53(4) . . ? I6 Pb2 I5 173.02(6) . . ? I6 Pb2 I7 86.25(3) . 8_467 ? I6 Pb2 I8 96.61(3) . . ? I7 Pb2 I8 177.08(4) 8_467 . ? I9 Pb2 I4 177.18(7) . . ? I9 Pb2 I5 93.31(5) . . ? I9 Pb2 I6 89.78(6) . . ? I9 Pb2 I7 86.58(7) . 8_467 ? I9 Pb2 I8 94.00(7) . . ? Pb1 I1 Pb1 91.34(6) 3_657 . ? Pb1 I2 Pb1 93.65(6) . 3_657 ? Pb1 I3 Pb1 167.49(10) . 4_577 ? Pb2 I4 Pb2 89.37(6) 3_656 . ? Pb2 I5 Pb2 168.36(12) 4_567 . ? Pb2 I6 Pb2 91.57(6) . 3_656 ? Pb1 I7 Pb2 172.38(4) . 8_567 ? Pb2 I8 Pb1 167.45(5) . 8_567 ? Pb2 I9 Pb1 173.46(11) . . ? C6 N2 H2 121.5 . . ? C6 N2 C7 117.0(18) . . ? C7 N2 H2 121.5 . . ? C3 C2 H2A 113.4 . . ? N1A C2 H2A 113.4 . . ? N1A C2 C3 113(3) . . ? N1A C2 C1A 93(3) . . ? C1A C2 H2A 113.4 . . ? C1A C2 C3 109(3) . . ? N1B C2 C3 122(3) . . ? N1B C2 C1B 123(3) . . ? C1B C2 C3 109(3) . . ? C4 C3 C2 115.7(17) . . ? C4 C3 C7 120.4(14) . . ? C7 C3 C2 123.8(17) . . ? C3 C4 H4 118.3 . . ? C3 C4 C5 123.3(17) . . ? C5 C4 H4 118.3 . . ? C4 C5 H5 123.3 . . ? C6 C5 C4 113.4(17) . . ? C6 C5 H5 123.3 . . ? N2 C6 C5 127.0(18) . . ? N2 C6 H6 116.5 . . ? C5 C6 H6 116.5 . . ? N2 C7 C3 118.1(16) . . ? N2 C7 H7 121.0 . . ? C3 C7 H7 121.0 . . ? C2 N1A H1AA 109.5 . . ? C2 N1A H1AB 108.9 . . ? C2 N1A H1AC 110.1 . . ? H1AA N1A H1AB 109.5 . . ? H1AA N1A H1AC 109.5 . . ? H1AB N1A H1AC 109.5 . . ? C2 C1A H1AD 109.5 . . ? C2 C1A H1AE 109.6 . . ? C2 C1A H1AF 109.3 . . ? H1AD C1A H1AE 109.5 . . ? H1AD C1A H1AF 109.5 . . ? H1AE C1A H1AF 109.5 . . ? C2 N1B H1BA 120.0 . . ? C2 N1B H1BB 120.0 . . ? H1BA N1B H1BB 120.0 . . ? C2 C1B H1BC 110.2 . . ? C2 C1B H1BD 108.7 . . ? C2 C1B H1BE 109.5 . . ? H1BC C1B H1BD 109.5 . . ? H1BC C1B H1BE 109.5 . . ? H1BD C1B H1BE 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 I1 3.2200(19) . ? Pb1 I2 3.1584(19) . ? Pb1 I3 3.1729(9) . ? Pb1 I7 3.222(2) . ? Pb1 I8 3.289(2) 8_467 ? Pb1 I9 3.208(2) . ? Pb2 I4 3.230(2) . ? Pb2 I5 3.1974(9) . ? Pb2 I6 3.1693(19) . ? Pb2 I7 3.242(2) 8_467 ? Pb2 I8 3.263(2) . ? Pb2 I9 3.148(2) . ? N2 H2 0.8600 . ? N2 C6 1.34(2) . ? N2 C7 1.367(18) . ? C2 H2A 0.9800 . ? C2 C3 1.53(2) . ? C2 N1A 1.46(2) . ? C2 C1A 1.48(5) . ? C2 N1B 1.41(2) . ? C2 C1B 1.51(6) . ? C3 C4 1.33(2) . ? C3 C7 1.39(2) . ? C4 H4 0.9300 . ? C4 C5 1.370(19) . ? C5 H5 0.9300 . ? C5 C6 1.35(3) . ? C6 H6 0.9300 . ? C7 H7 0.9300 . ? N1A H1AA 0.8901 . ? N1A H1AB 0.8900 . ? N1A H1AC 0.8900 . ? C1A H1AD 0.9600 . ? C1A H1AE 0.9599 . ? C1A H1AF 0.9599 . ? N1B H1BA 0.8600 . ? N1B H1BB 0.8600 . ? C1B H1BC 0.9603 . ? C1B H1BD 0.9599 . ? C1B H1BE 0.9599 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 C3 C4 C5 177(3) . . . . ? C2 C3 C7 N2 176(3) . . . . ? C3 C4 C5 C6 4(4) . . . . ? C4 C3 C7 N2 -6(4) . . . . ? C4 C5 C6 N2 1(4) . . . . ? C6 N2 C7 C3 10(5) . . . . ? C7 N2 C6 C5 -8(4) . . . . ? C7 C3 C4 C5 -1(4) . . . . ? N1A C2 C3 C4 -132(3) . . . . ? N1A C2 C3 C7 46(4) . . . . ? C1A C2 C3 C4 126(3) . . . . ? C1A C2 C3 C7 -56(4) . . . . ? N1B C2 C3 C4 102(3) . . . . ? N1B C2 C3 C7 -80(4) . . . . ? C1B C2 C3 C4 -106(3) . . . . ? C1B C2 C3 C7 72(4) . . . . ? loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.58546 2 0.41454