#------------------------------------------------------------------------------ #$Date: 2024-06-15 01:13:38 +0300 (Sat, 15 Jun 2024) $ #$Revision: 292406 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/19/1571905.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571905 loop_ _publ_author_name 'Fan, Chang-Chun' 'Liu, Cheng-Dong' 'Liang, Bei-Dou' 'Ju, Tong-Yu' 'Wang, Wei' 'Jin, Ming-Liang' 'Chai, Chao-Yang' 'Zhang, Wen' _publ_section_title ; Chiral Three-Dimensional Organic-Inorganic Lead Iodide Hybrid Semiconductor ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC00954A _journal_year 2024 _chemical_formula_moiety 'I6 Pb2, 0.5(C14 H24 N4)' _chemical_formula_sum 'C7 H12 I6 N2 Pb2' _chemical_formula_weight 1299.97 _space_group_crystal_system orthorhombic _space_group_IT_number 64 _space_group_name_Hall '-C 2ac 2' _space_group_name_H-M_alt 'C m c e' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2024-01-05 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2024-01-05 deposited with the CCDC. 2024-06-13 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 12.9548(6) _cell_length_b 18.8648(9) _cell_length_c 17.6101(7) _cell_measurement_reflns_used 4263 _cell_measurement_temperature 299.13(10) _cell_measurement_theta_max 30.7780 _cell_measurement_theta_min 2.1960 _cell_volume 4303.7(3) _computing_cell_refinement 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment air _diffrn_ambient_temperature 299.13(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.819 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -26.00 6.00 0.50 1.50 -- 5.69 94.00 61.00 64 2 \w -20.00 44.00 0.50 1.50 -- -6.24 38.00 -60.00 128 3 \w -18.00 31.00 0.50 1.50 -- 5.69 -99.00-180.00 98 4 \w -13.00 32.00 0.50 1.50 -- 5.69 -94.00 -49.00 90 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0153755000 _diffrn_orient_matrix_UB_12 -0.0505868000 _diffrn_orient_matrix_UB_13 0.0006706000 _diffrn_orient_matrix_UB_21 -0.0079125000 _diffrn_orient_matrix_UB_22 -0.0054840000 _diffrn_orient_matrix_UB_23 -0.0366875000 _diffrn_orient_matrix_UB_31 0.0363751000 _diffrn_orient_matrix_UB_32 0.0201836000 _diffrn_orient_matrix_UB_33 -0.0082485000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0394 _diffrn_reflns_av_unetI/netI 0.0380 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.819 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 13562 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.819 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.555 _diffrn_reflns_theta_min 2.159 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 24.222 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.11415 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.84a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'metallic reddish red' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier reddish _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 4.013 _exptl_crystal_description block _exptl_crystal_F_000 4400 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _refine_diff_density_max 2.491 _refine_diff_density_min -4.696 _refine_diff_density_rms 0.325 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 96 _refine_ls_number_reflns 2819 _refine_ls_number_restraints 66 _refine_ls_restrained_S_all 1.048 _refine_ls_R_factor_all 0.0762 _refine_ls_R_factor_gt 0.0517 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0321P)^2^+157.0801P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1058 _refine_ls_wR_factor_ref 0.1151 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2076 _reflns_number_total 2819 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc00954a2.cif _cod_data_source_block 2Rac _cod_original_sg_symbol_Hall '-C 2bc 2' _cod_database_code 1571905 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C1 H1 N1 Pb1 I1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.085 _shelx_estimated_absorpt_t_min 0.085 _reflns_odcompleteness_completeness 99.63 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; 1. Shared sites {C1, N1} 2. Restrained distances C2-N1 1.51 with sigma of 0.01 C1-C2 1.51 with sigma of 0.01 C2-C3 1.51 with sigma of 0.01 3. Uiso/Uaniso restraints and constraints Uanis(C1) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(C2) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C1) = Uanis(N1) 4. Rigid body (RIGU) restrains C4, C5, C6, C7, N2, C3, C2, N1 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Fixed Sof: C1(0.5) H1A(0.5) H1B(0.5) H1C(0.5) N1(0.5) H1D(0.5) H1E(0.5) H1F(0.5) 6.a Riding coordinates: C1(H1A,H1B,H1C), N1(H1D,H1E,H1F) 6.b Aromatic/amide H refined with riding coordinates: N2(H2), C7(H7), C5(H5), C6(H6), C4(H4) ; _shelx_res_file ; TITL fcc-124-01_a.res in Cmca fcc-124-01.res created by SHELXL-2018/3 at 13:00:07 on 05-Jan-2024 CELL 0.71073 12.9548 18.8648 17.6101 90 90 90 ZERR 8 0.0006 0.0009 0.0007 0 0 0 LATT 7 SYMM -X,0.5-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM +X,-Y,-Z SFAC C H I N Pb UNIT 56 96 48 16 16 DFIX 1.51 0.01 C2 N1 DFIX 1.51 0.01 C1 C2 ISOR 0.001 0.002 C1 DFIX 1.51 0.01 C2 C3 EADP C1 N1 ISOR 0.01 0.02 C2 RIGU C4 C5 C6 C7 N2 C3 C2 N1 EXYZ C1 N1 L.S. 30 PLAN 1 SIZE 0.2 0.2 0.2 TEMP 6.13 CONF BOND LIST 4 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.032100 157.080109 FVAR 0.03687 PB1 5 0.254051 0.375948 0.619926 11.00000 0.04180 0.03812 = 0.02825 0.00014 -0.00095 -0.00241 I4 3 0.285219 0.500000 0.500000 10.50000 0.06355 0.06044 = 0.04338 0.02342 0.00000 0.00000 I1 3 0.250000 0.493764 0.750000 10.50000 0.04250 0.03796 = 0.03563 0.00000 -0.00298 0.00000 I5 3 0.000000 0.402011 0.605500 10.50000 0.03357 0.05534 = 0.06519 -0.00713 0.00000 0.00000 I2 3 0.250000 0.257785 0.750000 10.50000 0.03924 0.04170 = 0.03579 0.00000 0.00378 0.00000 I6 3 0.250000 0.250000 0.500000 10.50000 0.17402 0.11420 = 0.06312 -0.05823 0.02526 -0.06227 I3 3 0.500000 0.359824 0.636851 10.50000 0.02756 0.04892 = 0.06372 0.01067 0.00000 0.00000 N2 4 0.000000 0.191929 0.724132 10.50000 0.04423 0.03965 = 0.07630 -0.01818 0.00000 0.00000 AFIX 43 H2 2 0.000000 0.230321 0.750465 10.50000 -1.20000 AFIX 0 C7 1 0.000000 0.194161 0.646608 10.50000 0.05134 0.05261 = 0.07692 0.01174 0.00000 0.00000 AFIX 43 H7 2 0.000000 0.237507 0.621452 10.50000 -1.20000 AFIX 0 C5 1 0.000000 0.070599 0.643003 10.50000 0.04621 0.05988 = 0.07457 0.00171 0.00000 0.00000 AFIX 43 H5 2 0.000000 0.028673 0.615222 10.50000 -1.20000 AFIX 0 C2 1 0.000000 0.134120 0.843851 10.50000 0.09772 0.12395 = 0.08478 0.00464 0.00000 0.00000 H2A 2 0.000000 0.175874 0.883718 10.50000 -1.20000 C6 1 0.000000 0.133414 0.606981 10.50000 0.03895 0.06829 = 0.05255 0.00489 0.00000 0.00000 AFIX 43 H6 2 0.000000 0.134781 0.554191 10.50000 -1.20000 AFIX 0 C3 1 0.000000 0.127051 0.758794 10.50000 0.02467 0.06262 = 0.07655 0.00667 0.00000 0.00000 C4 1 0.000000 0.068599 0.717914 10.50000 0.03948 0.04558 = 0.07620 0.01769 0.00000 0.00000 AFIX 43 H4 2 0.000000 0.024915 0.742390 10.50000 -1.20000 AFIX 0 PART 9 C1 1 0.098319 0.115290 0.883643 10.50000 0.09524 0.09727 = 0.09451 0.00082 -0.00161 0.00036 AFIX 3 H1A 2 0.154789 0.135980 0.856163 10.50000 -1.50000 H1B 2 0.107169 0.064820 0.885963 10.50000 -1.50000 H1C 2 0.096609 0.134290 0.934203 10.50000 -1.50000 AFIX 0 PART 10 N1 4 0.098319 0.115290 0.883643 10.50000 0.09524 0.09727 = 0.09451 0.00082 -0.00161 0.00036 AFIX 3 H1D 2 0.130999 0.155400 0.895073 10.50000 -1.20000 H1E 2 0.137909 0.089110 0.853323 10.50000 -1.20000 H1F 2 0.085049 0.091360 0.926083 10.50000 -1.20000 AFIX 0 HKLF 4 REM fcc-124-01_a.res in Cmca REM wR2 = 0.1151, GooF = S = 1.054, Restrained GooF = 1.048 for all data REM R1 = 0.0517 for 2076 Fo > 4sig(Fo) and 0.0762 for all 2819 data REM 96 parameters refined using 66 restraints END WGHT 0.0321 157.0596 REM Highest difference peak 2.491, deepest hole -4.696, 1-sigma level 0.325 Q1 1 0.2238 0.2682 0.4917 11.00000 0.05 2.49 ; _shelx_res_checksum 31384 _shelx_hkl_file ; 0 0 2 2.72 0.26 0 0 -2 3.32 0.29 0 0 -3 0.54 0.29 0 0 3 -0.32 0.26 0 0 -4 314.67 15.53 0 0 4 320.93 15.54 0 0 4 316.70 15.37 0 0 -5 0.51 0.62 0 0 5 0.24 0.52 0 0 5 0.24 0.22 0 0 6 167.25 8.45 0 0 -6 166.16 8.43 0 0 6 167.35 8.17 0 0 7 -0.34 0.83 0 0 -7 0.23 0.72 0 0 7 0.72 0.31 0 0 -8 7422.91 350.41 0 0 8 7294.09 350.44 0 0 8 7192.55 350.07 0 0 9 0.11 1.02 0 0 9 0.18 0.36 0 0 -9 -0.61 1.07 0 0 -10 72.23 4.24 0 0 10 74.39 3.76 0 0 11 0.11 0.45 0 0 -11 -0.63 1.36 0 0 12 10.62 0.87 0 0 -12 10.18 1.80 0 0 13 -0.08 0.53 0 0 -13 -0.92 1.68 0 0 -14 141.03 7.93 0 0 14 144.20 7.18 0 0 -15 -0.18 1.98 0 0 15 0.42 0.64 0 0 -16 1130.06 54.93 0 0 16 1113.67 54.14 0 0 -17 -0.62 2.20 0 0 17 1.01 0.74 0 0 18 35.21 2.11 0 0 19 -0.71 0.82 0 0 20 4.20 0.99 0 0 -20 2.07 2.68 0 0 21 -0.29 0.95 0 0 -21 1.87 2.69 0 2 0 5.26 0.32 0 2 1 1742.02 84.12 0 2 -2 5.54 0.76 0 -2 2 4.94 0.76 0 2 2 5.55 0.37 0 2 -2 5.36 0.36 0 2 -3 2106.37 104.81 0 -2 3 2139.18 104.79 0 2 3 2190.58 104.49 0 2 -4 2.40 0.82 0 -2 -4 4.33 0.61 0 2 4 3.29 0.52 0 2 5 1140.99 53.48 0 -2 -5 1085.53 53.49 0 2 -5 1090.87 53.74 0 2 5 1094.61 53.34 0 2 6 7.72 0.88 0 -2 -6 8.27 0.94 0 2 -6 7.20 1.01 0 2 6 8.63 0.62 0 2 -6 6.89 1.13 0 2 -7 1693.41 86.22 0 2 -7 1801.53 86.20 0 2 7 1760.99 86.01 0 -2 -7 1812.78 86.02 0 -2 7 1776.18 85.69 0 2 7 1775.92 85.81 0 -2 -8 1.47 0.91 0 2 -8 1.17 1.07 0 2 -8 0.46 1.13 0 2 8 0.95 0.85 0 2 8 1.49 0.46 0 -2 8 1.45 0.24 0 2 9 362.87 17.54 0 2 -9 352.37 17.69 0 -2 -9 350.01 17.53 0 2 9 358.09 17.22 0 -2 9 348.98 17.09 0 -2 -10 18.08 1.75 0 2 10 17.14 1.56 0 2 -10 19.17 1.83 0 2 10 16.97 1.15 0 -2 10 17.80 0.98 0 2 -11 711.18 35.49 0 -2 11 716.87 34.74 0 2 11 716.72 35.28 0 -2 -11 727.88 35.28 0 2 -11 736.04 35.42 0 2 11 712.03 34.87 0 -2 -12 2.41 1.55 0 2 12 1.68 0.69 0 2 -12 2.49 1.43 0 -2 12 2.84 0.47 0 2 -12 0.77 1.62 0 2 12 0.56 1.32 0 2 -13 99.17 5.68 0 -2 13 93.19 4.70 0 2 13 93.86 5.46 0 -2 -13 98.51 5.49 0 2 -13 95.55 5.57 0 2 13 93.07 4.86 0 -2 -14 3.02 1.75 0 2 14 1.36 0.73 0 2 -14 3.29 1.74 0 -2 14 0.94 0.48 0 2 14 0.68 1.60 0 2 -14 -1.41 2.05 0 2 -15 423.85 22.73 0 -2 15 455.27 21.76 0 2 15 444.52 22.59 0 -2 -15 446.15 22.53 0 2 -15 457.38 22.67 0 2 15 437.74 21.90 0 2 16 1.01 0.85 0 2 -16 -1.18 1.92 0 2 -16 -3.25 2.30 0 -2 -16 -0.19 1.99 0 -2 16 0.49 0.60 0 2 17 17.84 1.41 0 2 -17 11.79 2.60 0 -2 -17 15.92 2.58 0 2 -17 19.19 2.73 0 2 -18 3.49 2.36 0 2 18 5.10 1.03 0 2 -19 122.22 7.51 0 2 19 118.62 6.18 0 2 20 1.58 1.03 0 2 -20 3.65 2.80 0 2 21 4.33 1.18 0 2 -21 3.23 2.79 0 2 22 0.08 1.18 0 4 0 375.80 18.25 0 4 1 3.85 0.37 0 4 -1 3.95 0.34 0 -4 2 12.43 0.95 0 4 -2 13.13 0.75 0 4 2 12.85 0.84 0 4 -3 31.08 1.90 0 -4 3 33.36 1.77 0 4 -3 34.69 1.70 0 4 3 33.33 1.82 0 -4 3 32.02 2.45 0 4 -4 9122.90 440.77 0 -4 4 8995.68 440.73 0 4 -4 9140.79 440.05 0 4 -5 7.87 1.64 0 -4 5 7.64 1.44 0 4 5 9.21 0.92 0 4 -5 7.46 0.65 0 4 6 70.79 3.77 0 -4 6 69.83 4.40 0 4 -6 68.00 3.53 0 4 -6 68.28 4.37 0 4 6 70.55 3.59 0 4 7 19.69 1.51 0 4 7 19.26 1.25 0 4 -7 21.78 2.39 0 4 8 58.63 3.93 0 4 -8 54.24 4.44 0 4 -9 11.85 1.90 0 4 -9 12.07 1.80 0 4 9 13.25 1.01 0 4 9 12.35 1.33 0 4 10 127.97 6.61 0 4 -10 120.53 7.01 0 -4 -10 132.16 6.67 0 4 -10 107.35 6.94 0 4 10 124.99 6.30 0 4 -11 16.20 2.25 0 4 -11 17.17 2.15 0 4 11 15.89 1.66 0 4 11 15.09 1.24 0 -4 -11 21.51 1.93 0 4 -12 2811.36 127.67 0 4 12 2601.51 127.32 0 -4 -12 2617.20 127.32 0 4 -12 2536.05 127.69 0 4 12 2607.31 126.94 0 4 -13 17.42 2.49 0 4 13 20.80 2.02 0 4 -13 18.19 2.43 0 4 13 15.32 1.35 0 -4 -13 20.73 2.19 0 4 -14 60.32 4.05 0 4 14 55.30 3.67 0 -4 -14 53.61 3.72 0 4 -14 50.83 3.96 0 4 14 50.76 3.00 0 4 15 -0.29 0.87 0 4 -15 -0.25 1.99 0 -4 -15 1.53 1.89 0 4 15 0.71 1.60 0 4 -15 -0.21 2.07 0 4 16 5.79 1.09 0 4 -16 9.84 2.36 0 -4 -16 8.93 2.25 0 4 16 5.81 1.92 0 4 -16 6.47 2.42 0 4 -17 5.19 2.52 0 4 17 3.23 1.10 0 4 17 2.32 2.00 0 4 18 82.57 5.60 0 4 18 90.56 4.71 0 4 -18 74.47 5.84 0 4 -19 -0.31 2.54 0 4 19 0.59 1.12 0 4 -20 332.33 17.96 0 4 20 335.59 16.65 0 4 -21 0.34 3.00 0 4 21 3.32 1.30 0 4 22 18.93 1.83 0 6 0 22.30 1.31 0 6 -1 1038.50 50.24 0 6 1 1037.19 50.28 0 6 -2 5.94 0.50 0 6 2 6.20 0.60 0 -6 3 1913.97 94.05 0 6 -3 1954.81 93.88 0 6 3 1944.78 93.99 0 6 -4 22.96 1.78 0 6 -4 28.49 1.45 0 6 4 26.66 1.62 0 -6 4 26.18 2.51 0 -6 4 27.54 1.52 0 6 -5 981.00 48.73 0 6 -5 1012.21 48.46 0 -6 5 944.99 49.47 0 6 -6 59.87 3.10 0 -6 6 57.17 4.08 0 6 -6 55.33 4.16 0 6 -6 56.31 2.80 0 6 -7 561.08 26.63 0 6 7 533.10 26.82 0 -6 7 529.32 27.57 0 6 -7 559.70 27.80 0 6 7 538.88 26.64 0 6 -8 0.60 0.66 0 6 8 -0.13 0.64 0 6 -8 -0.27 2.06 0 -6 8 2.50 1.76 0 6 8 0.82 0.86 0 6 -9 292.60 14.39 0 6 -9 294.31 15.57 0 6 9 292.63 14.44 0 6 9 288.83 14.69 0 6 -10 43.45 2.46 0 6 -10 43.93 3.76 0 6 10 41.99 2.50 0 6 10 42.17 2.84 0 6 -11 964.18 46.61 0 6 11 951.02 46.94 0 6 -11 957.41 47.71 0 6 11 958.20 46.65 0 6 12 -0.97 1.34 0 6 -12 0.69 2.38 0 6 -12 0.73 0.80 0 6 12 0.76 0.90 0 6 -12 -0.27 2.13 0 6 13 104.94 6.31 0 6 -13 114.25 6.94 0 6 -13 107.92 7.04 0 6 13 128.61 5.98 0 6 -13 106.60 5.88 0 6 14 27.79 2.48 0 6 -14 28.54 3.24 0 6 14 28.53 1.99 0 6 -14 28.83 3.38 0 6 -14 30.88 2.01 0 6 15 116.22 6.77 0 6 -15 118.90 7.30 0 6 -15 118.96 6.22 0 6 -15 120.43 7.47 0 6 15 119.62 6.25 0 6 16 5.59 1.21 0 6 -16 5.53 1.24 0 6 -16 5.67 2.77 0 6 16 3.88 1.93 0 6 -16 3.04 2.62 0 6 17 17.80 2.53 0 6 -17 20.67 1.85 0 6 -17 23.18 3.31 0 6 17 21.19 1.73 0 6 18 3.80 1.26 0 6 -18 2.24 1.34 0 6 -18 4.81 2.80 0 6 18 2.89 2.09 0 6 19 203.93 11.69 0 6 -19 205.79 10.92 0 6 -19 230.11 12.38 0 6 19 222.32 10.92 0 6 20 3.37 2.54 0 6 -20 1.04 3.17 0 6 20 0.81 1.35 0 6 21 1.11 2.63 0 6 21 5.31 1.47 0 6 -21 3.24 3.30 0 6 22 2.68 1.45 0 6 23 30.28 2.49 0 8 0 6425.78 310.28 0 8 -1 2.52 0.56 0 8 1 2.44 0.58 0 -8 2 3.78 0.73 0 8 -2 5.12 0.57 0 -8 3 20.72 1.70 0 8 -3 21.39 1.30 0 8 3 22.38 1.43 0 -8 4 42.43 2.39 0 8 -4 41.24 2.20 0 8 4 42.15 2.39 0 -8 4 36.00 3.21 0 -8 5 12.14 0.86 0 -8 5 10.20 2.24 0 8 -5 11.20 1.22 0 8 5 12.33 1.04 0 8 -5 10.46 0.75 0 8 -6 39.56 2.61 0 8 -6 39.90 2.05 0 -8 6 33.68 3.41 0 8 -7 63.31 3.75 0 -8 7 64.97 4.77 0 8 -7 65.81 3.27 0 8 -8 3296.68 159.57 0 8 8 3296.55 159.51 0 -8 8 3278.25 160.60 0 8 8 3309.89 159.74 0 -8 9 37.12 3.78 0 8 9 40.12 2.72 0 8 -9 38.03 2.47 0 8 -9 39.88 4.06 0 8 9 39.43 2.42 0 8 -10 17.11 1.58 0 8 10 18.87 1.51 0 8 -10 14.22 3.36 0 8 10 17.96 1.83 0 8 11 8.92 1.29 0 8 11 5.97 1.58 0 8 -12 8.01 1.20 0 8 12 8.35 1.22 0 8 12 11.00 1.65 0 8 -13 19.18 1.71 0 8 13 21.58 1.73 0 8 13 20.03 2.16 0 8 14 68.27 4.54 0 8 -14 73.20 5.34 0 8 -14 76.62 4.17 0 8 -14 72.31 5.67 0 8 14 73.36 4.14 0 8 15 10.31 1.43 0 8 -15 13.19 1.56 0 8 -15 11.30 2.93 0 8 15 15.23 2.11 0 8 16 744.86 37.41 0 8 -16 747.83 36.93 0 8 -16 741.51 38.16 0 8 16 769.52 36.94 0 8 17 15.29 1.63 0 8 -17 8.21 1.57 0 8 -17 11.65 3.24 0 8 17 10.72 2.28 0 8 18 18.36 2.75 0 8 -18 22.94 2.13 0 8 18 24.49 2.03 0 8 -18 19.24 3.64 0 8 -19 1.30 1.56 0 8 19 -0.96 2.28 0 8 19 -0.67 1.36 0 8 20 2.30 2.45 0 8 20 4.14 1.62 0 8 -20 6.27 3.59 0 8 21 1.41 1.56 0 8 22 35.40 2.77 0 8 23 0.75 1.77 0 10 0 35.62 2.10 0 10 -1 947.41 45.85 0 10 1 939.82 45.89 0 10 2 12.07 1.14 0 10 -2 14.12 1.03 0 -10 2 13.27 1.15 0 10 -3 182.92 9.10 0 10 3 185.23 9.22 0 -10 3 178.13 9.46 0 10 4 -0.47 0.76 0 10 -4 0.43 0.54 0 -10 4 -1.21 1.02 0 10 -5 279.52 13.20 0 10 5 258.94 13.38 0 -10 5 235.74 14.26 0 -10 5 269.03 13.31 0 10 -6 32.10 1.79 0 10 6 30.92 2.08 0 -10 6 29.60 3.53 0 -10 6 31.69 1.83 0 10 -7 879.81 41.97 0 10 -7 850.64 42.36 0 -10 7 789.75 43.33 0 10 -8 5.61 0.57 0 10 -8 6.14 1.59 0 -10 8 4.19 2.67 0 10 -9 258.31 13.41 0 10 9 260.56 13.45 0 -10 9 276.36 14.62 0 10 9 263.28 13.19 0 10 10 53.26 3.67 0 10 -10 53.09 3.53 0 -10 10 46.56 4.68 0 10 10 60.77 3.33 0 10 11 69.55 4.36 0 10 -11 73.86 4.14 0 -10 11 68.07 5.52 0 10 11 67.70 3.98 0 10 -12 2.93 1.41 0 10 12 1.15 1.10 0 10 -13 72.78 4.25 0 10 13 73.08 4.60 0 10 13 72.06 4.16 0 10 14 15.99 2.22 0 10 -14 21.57 3.94 0 10 -14 19.62 2.01 0 10 14 15.41 1.72 0 10 15 378.06 19.56 0 10 -15 377.16 19.16 0 10 -15 409.89 20.73 0 10 15 385.86 19.14 0 10 -16 -0.24 1.59 0 10 16 2.61 1.92 0 10 -16 1.12 3.55 0 10 16 1.99 1.41 0 10 -17 13.57 1.98 0 10 17 17.82 2.59 0 10 17 14.66 1.83 0 10 -18 7.06 1.85 0 10 18 6.66 2.32 0 10 -18 12.16 3.86 0 10 18 9.07 1.61 0 10 -19 22.21 2.48 0 10 -19 24.21 4.24 0 10 19 27.16 2.24 0 10 19 25.53 3.10 0 10 20 1.29 1.62 0 10 21 6.19 1.92 0 10 22 1.34 1.80 0 10 23 95.51 5.61 0 12 0 18.81 1.48 0 12 -1 -0.44 0.76 0 12 1 0.89 0.80 0 12 2 4.92 0.94 0 12 -2 5.13 0.84 0 -12 2 4.58 0.97 0 12 -3 20.96 1.43 0 12 3 18.66 1.58 0 -12 3 17.71 1.96 0 12 -4 2128.28 101.99 0 12 4 2097.16 102.14 0 -12 4 2076.67 102.35 0 -12 5 8.90 1.19 0 12 -5 7.51 0.94 0 12 5 9.83 1.29 0 -12 5 11.45 2.64 0 12 -6 1.02 0.69 0 12 6 0.40 1.06 0 -12 6 2.50 2.53 0 -12 6 1.13 0.70 0 12 -7 7.08 0.82 0 -12 7 7.66 2.86 0 12 7 7.74 1.26 0 12 -8 9.34 0.87 0 -12 8 3.86 3.02 0 12 -9 16.93 1.11 0 -12 9 14.35 3.41 0 12 10 13.90 2.03 0 12 10 12.05 1.56 0 12 -10 14.54 2.02 0 12 -11 29.95 2.59 0 12 11 23.40 2.53 0 -12 11 21.79 3.85 0 12 11 28.01 2.21 0 12 12 840.31 42.88 0 12 -12 892.68 42.76 0 12 12 889.38 42.58 0 -12 12 812.58 43.85 0 12 -13 18.34 2.28 0 12 13 16.11 1.86 0 12 13 13.81 2.29 0 12 -14 11.91 2.10 0 12 14 12.16 1.72 0 12 14 14.46 2.32 0 12 -15 2.08 1.91 0 12 15 2.47 1.51 0 12 15 -0.41 1.97 0 12 -16 6.08 1.90 0 12 16 2.52 1.44 0 12 16 4.93 2.16 0 12 -17 3.58 1.88 0 12 17 3.26 1.60 0 12 17 4.45 2.21 0 12 18 28.62 2.49 0 12 18 21.22 2.94 0 12 19 3.94 1.81 0 12 20 178.72 9.48 0 12 21 6.18 1.98 0 14 0 10.70 1.29 0 14 -1 29.39 2.10 0 14 1 32.37 2.17 0 14 2 2.31 1.18 0 14 -2 -1.03 0.95 0 -14 2 0.10 1.02 0 -14 3 464.85 23.13 0 14 3 466.77 22.87 0 14 -3 457.43 22.74 0 14 -4 3.50 0.95 0 -14 4 3.28 1.63 0 14 4 6.79 1.27 0 -14 5 307.29 14.12 0 14 -5 269.73 13.85 0 14 5 269.70 14.05 0 -14 5 270.40 15.09 0 -14 6 30.25 3.77 0 14 -6 27.68 1.85 0 14 6 25.17 2.14 0 -14 6 27.14 1.85 0 14 7 10.83 1.55 0 -14 7 10.16 3.20 0 14 -7 12.21 1.15 0 14 8 4.65 1.34 0 -14 8 2.96 3.16 0 14 -8 4.50 0.86 0 14 -9 48.91 2.74 0 -14 9 55.42 5.24 0 14 -10 14.63 1.16 0 -14 10 10.82 3.91 0 14 11 375.30 18.07 0 -14 11 324.67 19.35 0 14 11 352.52 18.37 0 14 12 3.00 1.49 0 14 12 2.80 2.08 0 14 13 47.72 3.91 0 14 -13 52.85 3.78 0 14 13 56.02 3.52 0 14 -14 16.82 2.40 0 14 14 15.66 2.58 0 14 14 15.08 2.01 0 14 -15 14.62 2.34 0 14 15 14.05 2.55 0 14 15 11.26 1.95 0 14 16 4.80 2.37 0 14 16 2.84 1.67 0 14 17 9.74 2.57 0 14 17 9.76 1.91 0 14 18 5.26 1.84 0 14 19 155.56 8.51 0 16 0 753.10 36.92 0 16 -1 -0.42 1.18 0 16 1 0.79 1.15 0 16 -2 8.42 1.39 0 16 2 7.22 1.41 0 -16 2 8.65 1.52 0 16 3 0.60 1.23 0 16 -3 1.38 1.10 0 -16 3 -0.34 1.76 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65.50 4.06 0 18 -10 6.29 1.26 0 18 10 5.55 1.79 0 18 11 5.70 2.56 0 18 12 -0.24 2.52 0 18 13 5.46 2.51 0 18 13 7.84 2.03 0 18 14 4.80 2.54 0 18 14 5.69 2.14 0 20 0 3.76 1.60 0 -20 1 5.76 1.73 0 20 -1 -0.14 1.55 0 20 1 2.96 1.64 0 -20 2 4.34 2.09 0 20 -2 5.52 1.68 0 20 2 3.78 1.73 0 -20 3 -1.26 2.45 0 20 3 2.63 1.63 0 20 -3 -0.68 1.48 0 20 -4 191.93 9.91 0 20 4 196.82 10.06 0 -20 4 174.59 10.18 0 20 5 1.46 1.76 0 20 -5 2.94 1.49 0 -20 5 0.78 1.42 0 20 -6 0.25 1.42 0 20 6 0.33 1.72 0 -20 6 2.27 1.07 0 20 7 0.51 1.70 0 20 -7 1.34 1.52 0 20 -8 7.95 1.59 0 20 8 4.50 1.87 0 20 9 0.35 1.73 0 20 10 6.68 1.98 0 20 11 0.92 1.92 0 -22 0 11.91 1.98 0 22 0 7.71 1.96 0 -22 1 0.92 2.03 0 22 -1 1.61 1.70 0 22 1 3.33 1.77 0 -22 2 -2.22 2.68 0 22 2 -2.54 1.82 0 22 -2 0.16 1.73 0 22 -3 81.28 5.32 0 22 3 96.98 5.56 0 -22 3 95.10 5.96 0 22 -4 1.21 1.63 0 22 4 1.23 1.86 0 -22 4 -1.99 1.87 0 -22 5 49.28 3.14 0 22 -5 48.66 3.45 0 22 5 47.68 3.63 0 22 6 2.57 1.97 0 22 -6 2.50 1.79 0 -22 6 1.96 0.96 0 22 7 2.62 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2.76 -2 8 17 9.82 1.63 -2 8 18 35.71 3.69 2 8 18 32.24 3.12 2 8 -18 33.40 2.46 -2 8 -18 36.26 2.89 -2 8 -18 34.36 4.11 2 8 -18 30.97 4.80 -2 8 18 40.16 2.68 2 8 18 37.15 2.64 2 8 -19 1.09 1.38 2 8 -19 2.62 3.74 -2 8 -19 0.63 2.91 -2 8 19 -1.13 2.69 2 8 19 3.36 2.11 2 8 19 2.07 1.51 -2 8 19 0.12 1.47 2 8 -20 8.97 4.24 -2 8 -20 2.63 3.13 2 8 20 4.95 1.53 -2 8 20 1.51 2.80 2 8 20 4.46 2.32 -2 8 20 2.97 1.62 -2 8 21 4.12 1.70 2 8 21 4.13 1.67 2 8 22 50.14 3.49 -2 8 22 50.16 3.37 -2 8 23 0.88 1.69 2 8 23 0.91 1.80 -2 -10 0 2.61 0.70 2 10 0 3.23 0.70 -2 -10 1 524.81 25.72 -2 -10 -1 519.85 25.75 2 10 1 526.47 25.79 2 10 -1 538.54 25.76 2 10 -2 3.56 0.66 2 10 2 2.18 0.73 2 -10 2 4.21 1.01 -2 -10 2 3.15 0.59 -2 -10 -2 2.87 0.78 -2 -10 2 2.45 0.68 -2 -10 3 149.93 7.12 2 -10 3 139.42 7.76 2 10 3 142.82 7.38 2 10 -3 140.23 7.27 -2 -10 3 141.67 7.23 2 10 -4 0.58 0.56 2 10 4 0.15 0.73 -2 -10 4 1.01 0.52 2 10 5 44.59 2.80 2 10 -5 46.74 2.65 2 -10 5 47.63 3.29 -2 -10 5 46.79 4.31 2 -10 6 34.59 3.64 2 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16.05 1.64 -2 10 14 16.62 1.83 -2 10 -14 21.72 2.25 2 10 14 16.77 1.81 2 10 15 436.89 22.72 -2 10 15 464.09 23.06 2 10 -15 451.48 22.32 -2 10 -15 443.97 22.60 2 10 15 444.59 22.42 -2 10 15 465.94 22.50 -2 10 -15 473.36 23.64 -2 10 -16 8.23 3.09 2 10 16 11.21 1.60 2 10 16 9.24 2.12 -2 10 16 13.93 2.54 2 10 -16 7.68 1.47 -2 10 -16 10.65 2.01 -2 10 16 11.40 1.65 -2 10 -17 2.26 2.98 2 10 -17 15.92 4.53 2 10 17 14.82 1.65 2 10 17 1.90 1.99 -2 10 17 0.50 2.34 2 10 -17 5.45 1.44 -2 10 -17 3.91 1.96 -2 10 17 4.10 1.58 2 10 18 4.19 1.59 -2 10 18 2.07 1.59 -2 10 18 -0.27 2.61 2 10 18 3.06 2.10 2 10 -18 4.67 1.56 -2 10 -18 3.73 2.02 2 10 -18 4.20 4.38 -2 10 -18 2.63 3.21 2 10 19 35.99 3.40 -2 10 19 32.41 3.79 2 10 19 38.18 2.82 2 10 -19 43.96 5.72 -2 10 -19 40.19 4.51 -2 10 19 33.02 2.73 2 10 20 1.83 1.67 -2 10 20 3.10 1.77 -2 10 21 0.82 1.72 2 10 21 2.00 1.72 -2 10 22 -0.69 1.76 2 10 22 2.47 1.86 2 10 23 98.81 5.70 -2 10 23 95.15 5.66 2 12 0 10.33 1.13 2 12 -1 4.41 0.92 2 12 1 3.64 0.93 2 -12 2 35.57 2.41 -2 -12 2 39.44 2.15 2 12 -2 32.92 2.21 2 12 2 36.17 2.30 -2 -12 3 -1.52 0.86 -2 12 3 1.58 1.10 2 -12 3 0.91 1.37 2 12 3 0.35 0.88 2 12 -3 1.16 0.82 2 -12 4 1899.16 93.05 -2 12 4 1906.58 92.61 2 12 4 1909.64 92.56 2 12 -4 1912.08 92.42 2 12 -5 23.69 1.56 2 12 5 22.02 1.76 2 -12 5 21.18 2.46 -2 12 -5 20.97 1.60 -2 12 5 20.48 1.87 -2 -12 5 25.42 3.60 2 -12 5 18.36 2.79 2 12 -6 18.14 1.44 2 12 6 22.43 1.79 2 -12 6 25.92 2.22 -2 12 -6 22.62 1.54 -2 12 6 19.42 1.79 2 -12 6 20.43 2.92 -2 -12 6 24.93 3.77 -2 12 7 11.41 1.54 -2 12 -7 10.50 1.07 2 -12 7 9.57 1.45 2 12 7 9.45 1.33 2 -12 7 5.58 2.66 -2 -12 7 10.71 3.39 2 12 -7 10.05 1.06 -2 12 -8 8.08 0.95 2 -12 8 10.96 2.77 -2 -12 8 6.27 3.36 2 12 -8 8.63 1.10 2 -12 8 11.15 1.25 -2 12 -9 32.83 1.96 2 -12 9 33.37 3.73 -2 12 10 118.82 6.86 -2 12 -10 117.42 5.89 2 12 10 114.88 6.32 -2 12 10 116.22 6.41 2 12 -10 117.49 6.31 -2 12 -10 129.44 6.74 -2 -12 10 107.85 7.99 2 -12 10 121.08 7.62 -2 12 11 1.27 1.39 -2 12 11 2.19 2.06 2 -12 11 2.29 2.86 -2 -12 11 1.94 3.24 -2 12 -11 0.65 1.93 2 12 -11 1.97 1.58 -2 12 -11 0.35 0.35 2 12 11 -0.34 1.21 2 12 12 726.32 36.79 -2 12 12 741.88 37.06 -2 12 -12 772.52 36.88 2 12 -12 707.11 36.65 -2 12 12 757.50 36.67 2 12 12 762.97 36.58 2 -12 12 710.57 37.71 -2 -12 12 802.15 38.19 2 12 13 10.99 2.16 -2 12 13 11.73 2.56 2 12 13 18.78 1.86 2 12 -13 14.24 2.00 -2 12 -13 13.69 2.32 -2 12 13 13.89 1.85 2 12 -14 39.88 3.13 -2 12 -14 48.67 3.61 -2 12 14 45.05 3.88 2 12 14 50.39 3.58 2 12 14 49.92 3.16 -2 12 14 44.64 3.20 2 12 15 2.68 1.42 2 12 15 3.98 1.85 -2 12 15 1.87 2.16 -2 12 -15 3.22 2.20 2 12 -15 3.89 1.59 -2 12 15 0.98 1.61 2 12 16 2.09 1.59 -2 12 16 5.42 2.45 2 12 16 1.34 2.04 2 12 -16 4.65 1.61 -2 12 -16 2.05 2.12 -2 12 16 4.56 1.64 2 12 17 9.30 1.75 -2 12 17 5.40 2.70 2 12 17 8.94 2.18 -2 12 -17 11.75 2.43 -2 12 17 7.39 1.86 -2 12 -18 48.48 3.91 2 12 18 50.51 3.48 -2 12 18 48.64 3.54 -2 12 18 54.29 4.44 2 12 18 54.20 3.98 2 12 19 1.82 1.77 -2 12 19 1.95 1.94 2 12 20 152.73 8.33 -2 12 20 155.54 8.40 -2 12 21 0.15 1.83 2 12 21 4.27 2.09 -2 14 0 2.40 1.12 2 14 0 3.76 1.06 2 14 1 92.12 4.79 2 14 -1 82.91 4.68 -2 14 -1 88.16 4.80 -2 14 1 84.55 4.83 2 14 -2 8.07 1.16 2 14 2 6.52 1.27 2 -14 2 8.23 1.39 -2 -14 2 7.27 1.11 -2 14 -2 6.08 1.20 -2 14 2 6.45 1.33 -2 14 3 665.75 32.86 -2 14 -3 648.11 32.74 2 14 3 666.98 32.80 2 14 -3 661.43 32.69 -2 -14 3 708.05 32.71 2 -14 3 648.79 33.11 -2 -14 4 31.83 1.71 -2 14 4 31.58 2.39 -2 14 -4 34.24 2.18 2 14 -4 28.53 2.04 2 14 4 33.38 2.27 2 -14 5 193.60 10.75 2 14 -5 199.98 10.06 2 14 5 209.52 10.25 -2 14 5 204.50 10.33 -2 14 -5 187.89 10.08 2 -14 5 196.18 11.01 -2 -14 5 212.84 11.91 -2 14 -6 7.36 1.13 -2 14 6 6.04 1.43 2 14 6 7.91 1.46 2 -14 6 4.89 1.76 2 -14 6 7.68 2.55 -2 -14 6 8.04 3.65 2 14 -6 9.33 1.12 2 -14 7 97.46 5.48 2 14 -7 93.02 5.04 -2 14 7 100.46 5.42 -2 14 -7 92.05 5.05 2 14 7 94.72 5.29 -2 -14 7 99.38 7.36 2 -14 7 102.32 6.43 -2 14 8 3.06 1.41 -2 14 -8 3.63 0.93 2 -14 8 2.70 1.10 2 14 -8 2.41 0.99 -2 -14 8 0.87 3.59 2 -14 8 2.15 2.58 2 14 8 2.88 1.24 -2 14 -9 11.86 1.16 -2 -14 9 12.30 3.89 2 -14 9 9.58 3.21 -2 14 -10 17.86 1.31 2 14 10 16.81 2.28 -2 14 10 14.23 2.51 -2 -14 10 13.03 4.03 2 -14 10 15.67 3.46 -2 14 11 528.68 25.13 2 14 11 513.89 25.02 -2 14 -11 495.60 24.50 2 14 11 499.22 25.26 -2 14 11 490.53 25.50 -2 -14 11 566.03 26.96 2 -14 11 493.20 26.17 2 14 12 10.73 1.65 -2 14 12 11.14 2.55 2 14 12 10.31 2.15 -2 14 12 9.11 1.80 2 14 13 15.58 1.90 -2 14 13 16.79 2.75 2 14 13 18.27 2.38 -2 14 -13 18.07 2.56 -2 14 13 12.48 2.00 2 14 14 4.46 1.58 -2 14 -14 9.95 2.35 -2 14 14 3.54 1.71 -2 14 14 5.89 2.55 2 14 14 2.68 2.00 2 14 15 31.46 2.99 -2 14 15 29.58 3.39 -2 14 -15 24.88 2.92 -2 14 15 25.48 2.55 2 14 15 26.15 2.45 -2 14 16 1.82 2.64 2 14 16 -0.40 2.01 -2 14 16 0.96 1.87 2 14 16 0.88 1.60 -2 14 17 -2.18 2.72 2 14 17 1.06 2.11 -2 14 17 3.55 1.84 2 14 17 0.74 1.65 2 14 18 4.23 1.86 -2 14 18 3.48 2.09 2 14 19 153.19 8.49 -2 14 19 157.88 8.53 -2 16 0 971.66 47.55 2 16 0 972.79 47.48 2 16 -1 8.12 1.34 2 16 1 10.16 1.49 -2 16 -1 6.57 1.44 -2 16 1 6.74 1.56 2 16 -2 2.45 1.14 2 16 2 0.46 1.19 -2 16 2 1.03 1.32 -2 16 -2 -0.11 1.15 -2 -16 2 0.21 1.25 2 -16 2 1.56 1.38 2 16 -3 2.87 1.15 2 16 3 1.06 1.21 -2 -16 3 0.29 1.25 2 -16 3 6.21 1.93 -2 16 3 4.89 1.44 -2 16 -3 3.07 1.28 2 -16 4 55.07 4.02 -2 -16 4 50.79 2.68 -2 16 4 51.16 3.37 -2 16 -4 51.02 3.16 2 16 4 51.98 3.28 2 16 -4 46.80 3.06 2 16 -5 15.44 1.51 2 16 5 16.08 1.76 -2 16 5 11.25 1.78 -2 16 -5 14.49 1.59 2 -16 5 9.61 2.35 -2 -16 5 17.66 3.78 2 -16 5 16.49 2.90 2 16 6 51.59 3.29 -2 16 6 50.88 3.38 -2 16 -6 50.90 3.06 2 -16 6 43.36 3.60 2 16 -6 48.69 3.03 2 -16 6 55.05 4.54 -2 -16 6 50.99 5.58 -2 16 -7 3.48 1.21 -2 16 7 0.73 1.56 2 16 7 1.45 1.39 2 -16 7 0.78 1.51 2 16 -7 2.72 1.15 2 -16 7 6.61 2.88 -2 -16 7 1.79 3.77 2 16 -8 636.66 30.87 2 16 8 651.19 31.13 -2 16 8 619.82 31.19 -2 16 -8 612.50 30.84 2 -16 8 644.22 32.14 -2 -16 8 658.98 33.07 2 -16 8 621.78 31.05 2 16 9 9.00 1.74 -2 16 -9 11.13 1.34 2 16 -9 8.99 1.43 -2 16 9 10.73 1.87 -2 16 -10 29.87 2.01 -2 16 -11 0.68 0.85 2 16 11 1.53 1.93 -2 16 11 1.22 2.36 -2 16 12 6.76 1.95 2 16 12 11.98 1.91 -2 16 12 11.09 2.62 2 16 12 6.50 2.14 -2 16 13 6.22 1.95 2 16 13 10.02 1.88 -2 16 13 6.93 2.62 2 16 13 6.22 2.17 2 16 14 45.46 3.78 -2 16 14 44.34 4.29 -2 16 14 45.69 3.56 2 16 14 52.86 3.51 -2 16 15 -2.10 2.01 2 16 15 2.55 1.80 -2 16 15 3.84 2.81 2 16 15 -1.07 2.05 2 16 16 176.50 9.33 -2 16 16 186.74 9.50 2 16 16 158.32 9.63 -2 16 16 164.59 10.06 2 18 0 50.46 3.32 -2 18 0 54.30 3.50 2 -18 1 291.53 14.32 -2 -18 1 266.82 14.03 -2 18 -1 273.49 14.26 2 18 -1 292.84 14.24 -2 18 1 282.25 14.31 2 18 1 281.44 14.23 2 18 -2 2.03 1.40 2 18 2 1.43 1.34 -2 18 2 2.34 1.55 -2 18 -2 -1.18 1.43 2 -18 2 1.48 1.71 -2 -18 2 1.27 1.72 2 -18 3 47.41 3.68 -2 -18 3 46.81 2.89 -2 18 3 40.37 3.12 2 18 3 44.60 3.04 2 18 -3 42.25 2.93 -2 18 -3 41.77 3.01 -2 -18 4 5.55 0.69 2 18 -4 5.59 1.42 2 18 4 1.91 1.43 2 -18 4 3.35 2.34 -2 18 -4 4.33 1.49 -2 18 4 3.07 1.58 -2 18 -5 15.80 1.87 -2 18 5 16.29 2.11 2 18 -5 15.99 1.75 2 18 5 19.20 1.99 2 -18 5 16.56 2.70 2 18 6 1.87 1.54 2 -18 6 3.16 1.94 -2 18 6 3.37 1.71 -2 18 -6 5.07 1.52 2 18 -6 2.77 1.36 2 18 -7 409.23 19.65 -2 18 -7 400.83 19.65 -2 18 7 372.23 19.90 2 18 7 406.09 19.86 2 -18 7 375.22 19.87 -2 18 -8 20.09 1.90 2 18 8 19.45 2.18 -2 18 8 23.73 2.40 2 18 -8 20.38 1.96 2 -18 8 18.06 1.95 2 18 9 50.58 3.52 -2 18 -9 54.64 3.18 -2 18 9 50.08 3.65 2 18 -9 46.90 3.24 -2 18 10 1.23 1.80 -2 18 -10 2.03 1.25 2 18 10 2.05 1.64 -2 18 11 19.37 3.18 2 18 11 21.31 2.76 2 18 12 -0.43 2.14 -2 18 12 -1.11 2.77 2 18 13 3.08 2.33 -2 18 13 -0.28 2.74 -2 18 13 2.41 1.94 2 18 13 1.02 1.85 2 18 14 2.48 2.29 -2 18 14 -1.15 2.98 -2 18 14 6.81 2.25 2 18 14 0.86 1.87 2 20 0 66.91 3.97 2 -20 0 62.09 3.85 2 20 1 4.34 1.60 2 20 -1 7.55 1.76 -2 20 1 7.78 1.89 -2 20 -1 7.43 1.79 2 -20 1 7.60 2.00 -2 -20 1 6.38 1.77 2 20 2 9.73 1.81 2 20 -2 11.05 1.82 -2 -20 2 8.49 2.14 2 -20 2 9.53 2.21 -2 20 -2 10.89 1.88 -2 20 2 5.95 1.84 -2 -20 3 8.72 1.36 2 20 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1.38 6 -16 1 6.42 1.89 6 16 1 5.83 1.51 6 16 -1 7.21 1.61 -6 -16 -1 5.93 0.94 -6 -16 -2 6.47 1.60 -6 -16 2 6.83 1.37 6 -16 2 6.14 1.98 6 16 -2 6.12 1.63 6 16 2 8.58 1.58 -6 -16 -2 7.28 0.97 -6 -16 -3 1.53 1.41 -6 -16 3 0.09 1.28 -6 -16 -3 2.51 0.88 6 -16 3 5.36 2.24 6 16 -3 0.97 1.52 6 16 3 1.36 1.36 -6 -16 -4 74.67 3.75 6 -16 4 63.72 4.80 -6 -16 -4 65.61 4.12 -6 -16 4 63.10 3.92 6 -16 4 71.11 4.66 6 16 4 63.14 4.17 6 16 -4 71.86 4.26 6 -16 5 11.77 2.49 -6 -16 5 7.94 4.76 -6 -16 5 12.03 1.45 6 -16 5 7.44 2.63 6 16 5 13.97 1.81 6 -16 6 79.46 5.16 6 16 6 70.61 4.37 -6 -16 6 69.16 3.98 6 -16 6 67.62 4.93 -6 -16 7 3.77 1.12 6 -16 7 5.38 2.54 6 16 7 1.59 1.58 -6 -16 7 -1.03 4.82 6 -16 7 0.45 2.48 6 16 8 335.60 16.66 -6 -16 8 325.05 16.23 6 -16 8 326.04 17.14 6 16 9 6.19 1.79 -6 -16 9 5.82 1.19 6 -16 9 6.06 2.22 -6 16 10 11.22 3.37 6 16 10 6.50 1.99 6 -16 10 6.64 2.16 6 16 11 5.67 1.91 -6 16 11 2.43 3.27 6 -16 11 -3.42 2.01 -6 16 12 9.86 2.40 6 16 12 16.54 2.18 -6 16 12 14.93 3.53 6 16 12 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20.97 2.72 -10 -2 -2 12.12 2.68 10 2 2 18.24 2.36 10 2 -3 24.90 2.57 -10 -2 -3 21.09 2.53 10 -2 -3 19.25 2.15 -10 -2 -3 20.53 2.86 10 2 3 21.07 2.32 -10 -2 -4 9.05 2.08 10 2 -4 14.88 2.01 10 -2 -4 13.35 1.73 -10 -2 -4 10.76 0.80 -10 -2 -4 7.48 2.18 10 -2 -4 10.23 0.78 10 2 4 7.85 1.78 10 -2 4 10.91 2.37 -10 -2 -5 11.55 0.95 -10 -2 -5 9.76 2.27 10 -2 5 10.25 2.18 10 2 5 7.20 1.62 10 2 -5 12.55 1.77 -10 -2 -5 14.67 2.32 -10 2 -5 13.80 2.32 10 -2 -5 12.12 1.26 -10 -2 -6 2.98 1.87 -10 2 -6 3.40 1.28 10 2 -6 2.28 0.60 10 -2 6 3.12 1.96 -10 -2 -6 -0.54 1.89 10 2 -6 6.97 1.45 -10 2 -6 2.26 2.06 -10 -2 -6 2.32 0.78 10 -2 -6 1.25 1.32 10 2 -7 83.60 4.27 -10 2 -7 77.40 4.76 10 -2 7 89.54 5.26 -10 -2 -7 76.38 5.26 -10 2 -7 71.71 5.55 -10 -2 -7 86.36 5.22 -10 2 -7 89.66 5.33 10 -2 -7 89.27 5.08 -10 -2 -7 83.80 4.40 -10 2 -8 8.68 1.86 10 2 -8 8.55 0.90 -10 2 -8 5.58 1.31 10 2 -8 5.55 1.53 -10 2 -8 5.77 2.34 -10 -2 -8 8.00 2.05 10 -2 8 4.77 1.71 -10 -2 -8 5.31 1.95 -10 -2 -8 6.06 1.09 10 -2 -8 5.66 2.03 10 -2 -9 20.95 2.99 10 2 -9 29.35 2.80 -10 -2 -9 26.76 1.99 -10 2 -9 28.85 2.62 10 2 -9 26.91 1.73 -10 -2 -9 23.23 2.62 -10 -2 -9 27.72 2.79 -10 2 -9 21.09 2.85 -10 2 -9 28.66 2.19 -10 2 -10 13.19 2.41 -10 2 -10 11.84 2.37 10 2 -10 12.73 1.31 10 -2 -10 16.24 2.87 10 2 -10 11.37 2.63 -10 2 -10 14.22 1.80 -10 -2 -10 16.41 1.55 -10 -2 -10 17.09 2.21 -10 -2 -10 15.60 2.37 10 -2 -11 69.92 5.50 -10 -2 -11 66.09 4.00 -10 2 -11 63.56 4.64 10 2 -11 73.19 3.82 -10 2 -11 67.74 4.64 -10 -2 -11 70.48 4.54 10 2 -11 66.92 5.41 -10 2 -11 67.50 4.18 -10 -2 -11 73.11 4.62 -10 -2 -12 4.98 2.09 10 -2 -12 6.56 3.29 10 2 -12 4.24 3.12 -10 2 -12 5.21 1.72 -10 -2 -12 6.04 1.52 -10 2 -12 9.09 2.02 -10 2 -12 4.00 2.44 10 2 -12 4.71 1.19 -10 -2 -13 8.26 2.20 -10 2 -13 6.22 2.16 10 -2 -13 11.51 3.86 -10 -2 -13 9.74 1.73 10 2 -13 6.19 3.70 -10 2 -13 7.96 1.92 -10 2 -13 8.48 2.71 10 2 -13 11.03 1.36 -10 2 -14 0.35 2.05 -10 -2 -14 0.58 2.09 10 -2 -14 5.09 3.78 10 2 -14 4.23 4.20 -10 -2 -14 3.30 1.62 -10 2 -14 -2.39 1.84 -10 2 -14 -3.18 2.62 10 2 -14 2.54 1.29 -10 -2 -15 86.37 5.09 10 2 -15 71.37 7.52 -10 2 -15 86.08 5.91 10 2 -15 86.44 4.84 -10 2 -15 87.12 5.42 -10 2 -15 92.66 5.34 10 -2 -15 82.83 7.19 -10 -2 -16 0.86 1.84 10 -2 -16 5.04 4.42 10 2 -16 -1.73 5.20 -10 2 -16 1.35 2.09 -10 2 -16 -0.23 3.09 10 2 -16 0.72 1.48 -10 2 -16 2.03 2.15 10 -2 -17 6.56 5.12 10 2 -17 3.13 5.57 -10 -2 -17 5.14 1.90 -10 2 -17 4.78 2.26 10 -2 -18 5.91 5.71 -10 -2 -18 1.58 2.06 10 2 -18 -0.67 6.24 -10 2 -18 3.71 2.44 -10 2 -19 57.09 4.16 -10 -2 -19 44.86 3.70 10 -2 -19 47.95 7.64 10 2 -19 49.55 8.33 -10 -2 -20 1.53 2.28 10 2 -20 -0.76 7.44 -10 2 -20 -0.20 2.66 10 -2 -20 2.76 6.76 10 4 0 23.60 2.46 10 -4 0 23.63 2.61 10 4 1 0.16 1.45 10 4 -1 -0.20 1.80 10 -4 -1 1.44 1.59 10 -4 1 -0.22 1.92 -10 -4 1 -0.71 2.10 10 4 -2 207.82 9.58 10 -4 2 195.59 9.60 10 -4 -2 176.31 9.08 10 4 2 173.02 8.97 -10 4 -2 156.44 8.26 -10 -4 2 140.59 9.39 -10 -4 -2 178.45 8.31 10 4 -3 0.02 0.39 -10 4 3 0.54 0.98 -10 4 -3 0.09 0.85 10 4 3 1.72 1.21 10 -4 3 5.00 2.15 10 -4 -3 5.11 1.49 10 4 -3 -3.55 2.33 -10 -4 -3 1.37 1.81 -10 -4 -3 3.49 1.93 10 4 -4 275.89 13.50 10 -4 4 286.78 13.70 -10 -4 -4 270.16 13.32 -10 -4 -4 231.21 13.32 10 4 4 250.55 12.41 -10 4 4 289.98 12.83 -10 4 -4 231.52 12.62 10 4 -4 253.54 12.39 10 4 5 0.87 0.59 -10 4 5 0.46 1.50 -10 4 -5 1.64 1.23 10 4 -5 1.45 0.56 10 -4 5 6.09 2.26 10 4 -5 2.08 1.81 -10 -4 -5 5.85 2.00 -10 -4 -5 2.55 1.73 -10 -4 -6 68.82 4.70 10 4 -6 77.19 4.50 -10 -4 -6 72.22 4.69 10 -4 6 81.77 5.06 10 4 6 73.09 3.82 -10 4 -6 64.89 4.22 10 4 -6 72.66 3.79 -10 4 -7 5.51 1.66 10 4 -7 4.76 0.83 10 -4 7 10.51 2.17 10 4 -7 8.90 1.50 -10 -4 -7 4.60 2.01 -10 -4 -7 8.19 1.87 10 -4 8 2.70 1.85 -10 -4 -8 10.47 2.10 -10 -4 -8 6.57 1.76 -10 4 -8 7.80 1.77 10 4 -8 4.26 0.87 -10 4 -9 8.26 1.97 10 4 -9 7.26 1.03 10 -4 9 6.06 1.95 -10 4 -9 5.95 2.36 -10 -4 -9 9.17 1.94 -10 4 -9 9.13 2.28 -10 -4 -9 10.24 2.04 -10 4 -10 156.80 9.02 -10 4 -10 180.07 9.10 -10 -4 -10 157.74 8.75 -10 4 -10 152.62 8.72 10 4 -10 164.06 8.18 -10 -4 -10 158.35 8.91 -10 -4 -11 -1.74 2.09 -10 4 -11 1.75 1.65 -10 4 -11 1.18 2.01 10 4 -11 2.51 2.32 -10 -4 -11 -0.17 1.78 -10 4 -11 0.97 2.04 10 4 -11 0.14 1.01 -10 4 -12 190.32 10.70 10 4 -12 207.34 10.10 -10 4 -12 181.59 10.67 -10 -4 -12 182.65 10.69 10 4 -12 220.88 11.57 -10 4 -12 211.85 10.54 -10 4 -13 7.85 2.44 10 4 -13 3.19 1.35 -10 4 -13 3.37 1.90 10 4 -13 3.73 3.51 -10 4 -13 2.47 1.95 10 4 -14 7.92 3.89 -10 4 -14 7.16 2.27 -10 4 -14 9.74 2.57 10 4 -14 5.04 1.39 -10 4 -14 7.33 2.01 10 4 -15 -1.01 4.56 -10 4 -15 0.17 2.06 -10 4 -15 1.99 2.56 10 4 -15 1.01 1.46 -10 4 -15 -1.30 1.93 10 4 -16 16.37 5.42 -10 4 -16 16.01 2.63 10 4 -17 1.24 5.73 -10 4 -17 4.16 2.32 10 -4 -17 5.75 4.53 -10 4 -18 72.77 5.05 10 -4 -18 83.33 8.02 10 4 -19 -3.60 6.86 -10 4 -19 1.64 2.72 10 -4 -19 4.90 5.78 -10 -4 -19 -0.15 1.99 -10 4 -20 59.50 4.53 10 -4 -20 56.58 8.20 -10 -4 -20 49.06 3.82 10 4 -20 50.56 8.89 -10 -6 0 4.79 1.77 10 6 0 5.23 1.27 10 -6 0 2.73 1.79 10 -6 0 4.25 0.83 -10 -6 0 4.89 1.06 10 -6 -1 11.21 1.09 10 -6 1 12.51 1.14 -10 -6 1 13.32 1.21 -10 6 1 13.93 1.34 10 6 1 12.88 0.88 10 6 1 9.20 1.33 10 6 -1 10.96 1.64 10 -6 -1 13.61 2.00 10 -6 1 14.20 2.39 -10 -6 -1 12.69 1.41 -10 -6 1 11.43 2.03 -10 -6 2 -0.57 1.78 10 6 2 2.02 0.58 -10 6 2 3.34 1.11 10 6 -2 2.61 1.47 10 -6 -2 1.93 1.49 10 -6 2 2.67 2.02 -10 -6 -2 4.83 1.92 -10 -6 2 4.48 0.89 -10 -6 3 95.71 6.30 -10 -6 -3 106.84 6.34 10 6 -3 116.19 6.35 10 -6 3 110.42 6.68 10 -6 -3 112.55 6.16 10 6 3 108.18 5.45 -10 6 3 111.69 5.75 10 6 4 12.10 0.94 -10 6 4 8.84 1.46 10 6 -4 11.71 2.30 10 -6 4 13.28 2.51 -10 -6 -4 11.06 2.09 -10 -6 4 10.82 2.05 -10 -6 -4 14.68 2.04 10 -6 5 46.50 3.87 -10 -6 -5 45.65 3.38 10 6 -5 46.13 3.66 -10 -6 -5 44.78 3.23 -10 -6 5 34.14 3.27 -10 6 -5 47.59 2.84 10 6 -5 39.22 2.39 10 6 5 42.47 2.34 -10 6 5 45.56 2.88 10 -6 6 39.29 3.42 -10 -6 -6 33.51 2.81 10 6 -6 41.11 3.28 -10 -6 -6 38.93 2.97 -10 6 -6 38.11 2.55 10 6 -6 32.98 2.03 10 6 6 32.04 1.96 -10 6 6 33.00 2.57 10 -6 7 56.53 4.19 10 6 -7 57.54 3.84 -10 -6 -7 50.33 3.68 -10 6 -7 53.23 3.43 10 6 -7 50.77 2.92 10 6 7 52.30 2.88 -10 6 7 53.02 3.58 -10 -6 -7 49.64 3.68 -10 -6 7 49.49 3.88 10 6 8 10.00 1.14 -10 6 -8 6.25 1.78 -10 6 8 9.58 2.12 10 6 -8 10.99 1.20 -10 6 -8 12.89 2.45 -10 -6 -8 11.17 1.90 10 6 -8 11.62 1.81 -10 -6 8 8.28 2.08 -10 -6 -8 7.49 1.98 10 6 -9 4.98 1.07 10 6 9 2.67 1.00 -10 6 9 6.17 2.22 -10 6 -9 1.96 1.76 -10 6 -9 6.97 2.31 -10 -6 -9 3.47 1.76 10 6 -9 6.31 1.46 -10 -6 9 -0.98 2.24 -10 -6 -9 3.74 1.91 -10 6 10 2.52 2.15 -10 6 -10 2.35 1.88 10 6 -10 4.98 1.11 10 6 10 1.82 1.04 -10 -6 -10 0.19 2.07 -10 -6 -10 2.56 1.85 -10 -6 10 0.19 2.01 -10 6 -10 2.84 2.12 10 6 11 121.53 6.78 -10 6 11 160.70 8.04 -10 6 -11 148.89 7.33 10 6 -11 126.58 6.75 -10 -6 11 114.09 7.33 -10 6 -11 130.83 7.47 -10 -6 -11 136.25 7.36 -10 -6 12 -3.20 2.06 -10 6 -12 -0.54 1.86 -10 6 -12 -0.15 1.88 10 6 12 1.74 1.25 -10 6 12 -1.33 2.82 10 6 -12 0.61 1.18 10 6 13 9.33 1.55 -10 6 13 13.91 3.47 -10 6 -13 16.34 2.39 10 6 -13 9.71 1.56 -10 -6 13 8.61 2.07 -10 6 -13 10.76 2.20 -10 6 -14 16.01 2.62 10 6 -14 10.55 1.71 -10 6 -14 15.72 2.32 -10 6 -15 59.44 4.19 10 6 -15 55.96 3.46 -10 -6 15 47.32 3.63 -10 6 -16 5.25 2.39 -10 6 -17 2.75 2.63 10 6 -17 -3.33 5.14 -10 6 -18 4.70 2.86 10 6 -18 1.83 5.65 -10 6 -19 57.98 4.62 10 6 -19 50.13 7.68 10 -8 0 297.92 16.06 -10 -8 0 333.23 15.81 10 -8 0 307.41 15.48 -10 -8 0 308.42 15.93 -10 -8 1 1.44 1.52 -10 -8 -1 0.16 1.51 10 -8 -1 1.05 1.67 10 -8 1 1.26 1.90 -10 -8 1 -0.12 1.51 10 -8 1 2.06 1.05 10 -8 2 75.24 5.38 10 -8 -2 84.33 5.14 -10 -8 -2 86.40 5.17 -10 -8 -2 90.96 5.13 -10 -8 2 85.30 5.03 -10 -8 2 90.87 4.85 10 -8 2 79.11 4.61 -10 -8 3 7.43 1.64 10 8 -3 4.86 0.97 10 8 3 5.63 0.87 -10 8 3 5.37 1.54 10 -8 3 3.41 2.14 10 -8 -3 6.14 1.63 -10 -8 -3 6.43 1.90 10 -8 3 4.97 1.21 -10 -8 3 4.50 1.39 -10 -8 4 8.36 1.77 10 8 4 10.49 1.06 -10 8 4 11.25 1.72 10 8 -4 7.01 1.19 -10 -8 -4 14.14 2.21 -10 -8 4 11.75 1.51 10 8 5 9.48 1.08 -10 8 5 7.28 1.75 10 8 -5 10.08 1.46 -10 -8 5 7.50 1.76 -10 -8 -5 11.51 2.14 -10 -8 -5 6.98 1.88 -10 -8 6 135.85 8.12 10 8 -6 151.79 8.08 -10 -8 -6 150.74 8.26 10 8 6 159.88 7.68 -10 8 6 154.01 8.17 -10 -8 -6 144.75 8.31 10 8 7 1.14 0.90 -10 8 7 0.29 1.80 10 8 -7 0.64 2.01 -10 -8 7 1.36 1.44 -10 -8 -7 0.46 1.56 -10 -8 -7 -1.96 1.84 -10 -8 -8 228.76 12.48 10 8 -8 273.04 12.80 -10 8 -8 266.24 12.38 10 8 -8 230.08 12.10 10 8 8 236.40 12.00 -10 8 8 249.29 12.59 -10 -8 8 225.53 12.43 -10 8 9 9.84 2.23 -10 8 -9 13.92 1.94 10 8 -9 9.69 1.48 10 8 9 10.47 1.27 10 8 -9 13.52 2.42 -10 -8 9 11.37 1.83 -10 -8 -9 10.96 2.02 -10 8 -10 9.04 1.93 10 8 -10 6.66 1.41 10 8 10 8.02 1.25 -10 8 10 5.47 2.33 10 8 -10 8.51 1.86 -10 -8 10 5.29 1.64 -10 -8 -10 5.33 1.97 10 -8 10 6.11 2.20 -10 8 -11 5.01 1.96 10 8 -11 6.58 1.50 10 8 11 3.94 1.27 -10 8 11 9.77 2.57 10 8 -11 5.75 1.61 -10 -8 11 5.91 1.60 -10 8 -11 5.71 2.07 10 -8 11 1.47 2.03 10 8 12 15.34 1.75 -10 8 12 16.37 3.05 -10 8 -12 20.17 2.33 10 8 -12 15.79 1.78 -10 8 -12 15.35 2.32 -10 -8 12 13.43 1.83 10 8 -12 18.65 1.83 10 8 13 14.09 1.73 -10 8 13 16.50 3.15 -10 8 -13 16.55 2.41 10 8 -13 14.21 1.82 -10 -8 13 11.33 1.82 -10 8 -13 14.97 2.36 -10 -8 14 92.22 5.42 10 8 14 95.32 5.46 -10 8 -14 105.82 5.93 10 8 -14 96.10 5.53 10 8 15 -1.20 1.67 -10 8 15 -2.22 3.38 10 8 16 90.14 5.49 -10 8 16 122.09 7.74 -10 -10 0 1.66 1.60 10 -10 0 4.03 1.28 10 -10 -1 116.50 6.68 -10 -10 1 107.71 6.46 -10 -10 -1 117.60 6.55 -10 -10 1 133.23 6.92 10 -10 1 115.01 6.28 -10 -10 2 8.09 2.16 10 -10 2 10.09 1.61 10 -10 -2 11.80 2.10 -10 -10 -2 8.27 1.98 -10 -10 -2 8.97 1.93 -10 -10 2 13.10 1.75 -10 -10 -3 34.60 3.06 -10 -10 3 37.07 2.85 -10 -10 -3 39.68 3.30 10 -10 -3 47.73 3.19 -10 -10 3 46.16 3.35 10 -10 3 40.27 2.81 10 10 4 8.14 1.22 -10 10 4 10.06 1.99 -10 -10 -4 10.07 2.15 -10 -10 4 7.63 1.99 10 -10 4 6.02 1.61 -10 -10 4 12.81 1.82 10 10 5 6.55 1.19 -10 10 5 8.04 2.05 -10 -10 5 8.94 1.71 -10 -10 -5 3.56 1.95 10 -10 5 7.31 1.63 -10 -10 5 7.60 1.95 10 10 6 1.85 1.11 -10 10 6 3.18 2.05 -10 -10 6 4.03 1.53 10 -10 6 3.92 2.39 -10 -10 -6 0.76 1.64 -10 -10 6 -0.30 1.78 -10 -10 -7 183.09 10.04 -10 -10 7 182.24 9.89 10 -10 7 219.92 10.79 10 10 7 190.29 9.63 -10 10 7 191.47 10.22 10 -10 8 0.24 2.27 -10 -10 8 3.16 1.39 -10 -10 -8 -0.30 1.94 10 10 8 -0.74 1.15 -10 10 8 -0.54 2.14 10 -10 9 29.20 3.25 -10 -10 -9 29.23 2.78 -10 -10 9 31.46 2.42 10 10 9 32.31 2.20 -10 10 9 29.36 3.04 10 10 -9 28.79 1.64 -10 -10 -10 25.97 2.68 10 -10 10 24.71 2.97 -10 -10 10 23.60 2.09 -10 10 -10 27.99 2.45 10 10 10 23.37 1.92 10 10 -10 22.89 2.25 -10 10 10 20.70 2.94 10 10 -10 19.48 1.50 -10 -10 11 45.96 3.06 -10 10 -11 50.19 3.35 10 10 -11 45.32 3.24 10 10 11 48.26 2.99 -10 10 11 49.37 3.96 10 -10 11 38.51 3.67 -10 -10 12 10.42 1.51 10 10 -12 8.36 1.96 10 10 12 8.00 1.59 -10 10 12 10.10 2.87 -10 10 -12 11.36 2.07 -10 10 -12 9.56 2.07 -10 -10 13 1.77 1.28 -10 10 -13 1.86 2.01 10 10 -13 1.88 1.83 10 10 13 1.90 1.49 -10 10 13 0.51 2.90 10 10 14 1.20 1.58 -10 10 14 2.53 3.12 10 10 15 96.21 5.71 -10 10 15 118.49 7.28 10 10 16 -0.13 1.68 -10 10 16 9.10 3.75 10 10 17 7.14 1.99 -10 10 17 4.25 4.09 10 10 18 2.42 1.99 -10 10 18 -5.37 4.99 -10 -12 0 39.21 3.01 10 -12 1 1.79 1.53 -10 -12 1 -1.19 2.69 10 -12 1 -0.22 2.18 -10 -12 -1 2.12 1.77 -10 -12 1 0.29 1.65 10 -12 2 83.73 5.62 -10 -12 -2 89.04 5.19 -10 -12 2 82.48 5.04 -10 -12 2 89.10 5.83 10 -12 2 86.54 4.99 -10 -12 3 0.66 2.52 10 -12 3 2.33 1.56 -10 -12 -3 1.19 1.89 10 -12 3 1.86 2.30 -10 -12 3 2.21 1.66 -10 -12 -4 262.71 13.74 10 -12 4 258.09 14.11 -10 -12 4 250.56 13.51 -10 -12 4 288.20 14.14 10 -12 4 271.79 13.55 -10 12 5 12.77 2.50 10 12 5 8.96 1.44 -10 -12 5 9.03 1.77 10 -12 5 11.60 2.68 -10 -12 -5 9.09 1.93 -10 -12 5 5.26 2.40 10 -12 5 7.39 1.82 -10 12 6 12.49 2.49 10 12 6 11.89 1.53 -10 -12 6 4.70 1.62 10 -12 6 17.03 2.77 -10 -12 -6 11.14 2.01 10 -12 6 9.61 1.90 -10 -12 6 11.36 2.49 10 12 7 4.07 1.36 -10 12 7 9.93 2.57 -10 -12 7 3.19 1.53 10 -12 7 6.15 2.64 -10 -12 -7 7.52 1.97 -10 -12 7 6.38 2.35 10 -12 7 5.90 1.89 10 -12 8 33.24 3.35 -10 -12 -8 23.00 2.54 -10 -12 8 24.93 2.28 10 12 8 26.35 2.15 -10 12 8 32.85 3.25 10 -12 9 18.60 2.86 -10 -12 -9 11.91 2.22 -10 -12 9 10.87 1.75 10 12 9 17.14 1.75 -10 12 9 12.40 2.81 10 -12 10 93.34 6.43 -10 -12 -10 108.49 6.14 10 12 10 108.19 5.68 -10 12 10 114.74 6.72 -10 -12 10 96.86 5.67 10 -12 11 0.45 2.40 10 12 11 -1.42 1.51 -10 12 11 1.16 2.68 -10 -12 11 -0.61 1.45 10 12 12 118.36 6.31 -10 12 12 120.06 7.41 -10 -12 12 110.77 6.14 10 12 13 6.86 1.82 -10 12 13 8.89 3.17 10 12 14 -0.89 1.75 -10 12 14 1.12 3.29 10 12 15 -0.68 1.71 -10 12 15 -1.81 3.39 10 12 16 9.78 2.05 -10 12 16 10.44 4.08 10 12 17 3.60 2.29 -10 12 17 0.69 4.14 10 -14 0 11.39 2.32 10 -14 1 17.75 2.24 -10 -14 1 28.20 3.96 10 -14 -1 18.43 2.55 10 -14 1 26.80 2.99 -10 -14 -2 1.82 1.71 10 -14 -2 0.19 1.91 10 -14 2 2.58 2.45 -10 -14 2 -0.61 3.37 10 -14 2 -2.13 1.84 -10 -14 3 163.09 8.55 -10 -14 -3 157.09 8.73 10 -14 3 159.43 9.14 10 -14 -3 154.46 8.75 -10 -14 3 183.44 9.83 10 -14 3 152.88 8.57 -10 -14 4 -1.11 3.14 10 -14 4 1.34 1.88 10 -14 4 -2.64 2.52 -10 -14 -4 2.05 1.91 -10 -14 4 1.33 1.59 10 -14 5 75.52 5.06 -10 -14 -5 60.86 4.33 -10 -14 5 68.94 4.17 -10 -14 5 72.11 5.31 10 -14 5 67.99 4.39 -10 14 6 12.01 2.94 10 14 6 10.19 1.69 10 -14 6 11.89 2.79 -10 -14 6 10.61 3.11 10 -14 6 8.23 2.10 -10 -14 -6 13.48 2.08 -10 -14 6 10.51 1.84 -10 -14 7 42.87 4.17 10 14 7 41.63 2.92 10 -14 7 49.06 4.08 -10 -14 -7 36.78 3.24 10 -14 7 42.61 3.37 -10 -14 7 44.30 3.05 10 -14 8 12.30 2.86 -10 -14 -8 4.23 1.94 -10 -14 8 9.99 1.70 10 -14 8 6.08 2.24 -10 -14 8 7.21 2.88 10 14 8 9.95 1.73 -10 14 8 10.57 2.96 10 14 9 2.76 1.58 -10 14 9 1.44 2.79 -10 -14 9 0.87 1.54 10 -14 9 3.64 2.57 -10 -14 -9 1.84 1.97 10 14 10 -0.36 1.64 -10 14 10 -1.74 3.04 -10 -14 10 0.52 1.49 10 -14 10 1.65 2.49 10 14 11 122.95 6.68 10 -14 11 105.08 7.23 10 -14 12 2.66 2.44 10 14 12 -0.38 1.73 -10 14 12 -2.38 3.25 10 14 13 11.43 2.04 -10 14 13 16.06 3.69 -10 14 14 5.79 3.52 10 14 14 7.37 2.01 10 14 15 23.19 2.63 -10 14 15 28.40 4.53 10 -16 0 160.43 9.10 10 -16 1 5.02 2.00 -10 -16 1 6.14 4.24 10 -16 1 3.78 2.46 10 -16 -1 4.68 2.40 10 -16 2 10.95 2.18 -10 -16 2 14.26 4.49 10 -16 -2 8.06 2.33 10 -16 2 4.87 2.56 10 -16 -3 5.81 2.26 10 -16 3 -0.24 2.51 -10 -16 -3 0.62 1.89 -10 -16 3 -1.48 4.26 10 -16 3 1.43 2.05 -10 -16 4 49.35 5.54 10 -16 4 46.91 3.73 -10 -16 -4 52.35 3.73 10 -16 4 52.40 4.35 -10 -16 -5 4.58 1.98 10 -16 5 8.79 2.78 -10 -16 5 3.40 3.71 10 -16 5 8.50 2.27 10 -16 6 54.30 4.42 -10 -16 -6 49.76 3.66 10 -16 6 48.89 3.87 10 -16 7 1.48 2.72 -10 -16 7 3.13 1.66 -10 -16 -7 -0.46 1.99 10 16 7 1.35 1.66 -10 16 7 4.95 3.08 -10 -16 -8 96.27 6.30 10 16 8 105.06 6.13 -10 16 8 135.72 7.43 -10 -16 8 111.37 6.06 10 -16 8 122.13 7.04 10 -16 9 9.68 2.95 -10 -16 -9 2.04 2.06 -10 -16 9 6.06 1.59 10 16 9 3.07 1.77 -10 16 9 8.92 3.36 10 -16 10 2.35 2.76 10 16 10 0.79 1.87 -10 16 10 1.36 3.37 10 -16 11 2.29 2.54 10 16 11 0.27 1.88 -10 16 11 0.28 3.40 10 16 12 18.12 2.30 -10 16 12 18.11 4.00 10 16 13 4.71 2.16 -10 16 13 6.19 3.73 10 16 14 34.99 3.08 10 -18 0 4.08 2.74 10 -18 -1 83.54 5.52 10 -18 1 78.25 5.66 10 -18 -2 5.93 2.55 10 -18 2 3.28 2.87 10 -18 3 15.90 3.18 10 -18 -3 19.73 2.88 10 -18 -4 8.62 2.40 10 -18 4 13.57 3.16 10 -18 5 4.31 2.88 10 -18 6 4.76 2.76 10 -18 7 98.00 6.68 10 18 7 94.80 5.88 10 -18 8 1.95 2.92 10 18 8 3.08 1.93 -10 18 8 9.42 3.54 10 -18 9 34.14 3.65 10 18 9 25.84 2.76 -10 18 9 35.52 4.34 10 18 10 4.92 2.09 -10 18 10 12.24 3.84 10 18 11 16.88 2.58 -10 18 11 16.49 3.96 10 20 8 19.80 2.69 -10 20 8 23.51 4.23 11 -1 0 -0.90 2.20 11 1 0 0.47 1.96 11 1 -1 32.57 3.33 11 -1 -1 36.25 3.20 11 1 1 37.28 3.33 11 -1 1 37.39 3.35 11 -1 -2 2.01 1.92 11 1 -2 4.52 2.16 11 -1 2 10.41 2.24 11 1 2 4.48 2.21 11 -1 -3 3.42 1.65 11 1 -3 2.80 2.02 -11 -1 -3 0.29 2.50 11 -1 3 6.75 2.27 11 1 3 4.04 1.98 11 1 -4 15.09 2.13 11 -1 -4 10.34 1.85 -11 -1 -4 5.81 2.47 11 -1 4 9.52 2.34 11 1 4 12.30 2.23 -11 -1 -5 9.63 2.27 11 -1 -5 7.63 1.70 11 1 -5 13.64 1.91 -11 -1 -5 7.70 2.43 11 -1 5 11.34 2.19 11 1 5 3.60 1.80 -11 1 -6 2.70 2.06 11 -1 -6 2.62 1.37 -11 -1 -6 4.35 2.22 11 1 -6 3.17 1.50 -11 -1 -6 1.96 0.84 -11 1 -6 0.27 2.37 -11 -1 -6 -0.25 2.14 11 1 6 1.59 1.69 11 -1 6 2.27 1.91 -11 1 -7 3.09 2.36 -11 -1 -7 0.73 2.24 11 1 -7 1.31 1.43 -11 1 -7 1.74 2.07 -11 -1 -7 2.85 2.12 11 -1 -7 1.37 1.06 -11 -1 -7 -0.30 0.91 11 -1 7 -0.39 1.79 -11 1 -8 12.74 1.52 -11 -1 -8 12.84 2.47 -11 1 -8 12.94 2.62 -11 -1 -8 16.28 2.55 -11 1 -8 12.41 2.40 11 -1 -8 15.50 1.84 -11 -1 -8 12.75 1.38 11 -1 -9 41.99 3.17 -11 -1 -9 38.50 2.52 -11 -1 -9 33.08 3.34 11 1 -9 37.91 2.88 -11 1 -9 37.58 2.63 -11 1 -9 43.40 3.48 -11 -1 -9 40.90 3.47 -11 1 -9 43.13 3.65 11 -1 -10 2.44 2.18 11 1 -10 2.12 1.89 -11 -1 -10 1.98 1.25 -11 1 -10 1.10 1.39 -11 -1 -10 0.44 2.04 -11 1 -10 2.71 2.30 -11 -1 -11 17.33 2.76 11 -1 -11 17.29 2.91 11 1 -11 13.97 2.71 -11 -1 -11 16.99 1.79 -11 1 -11 14.31 1.83 -11 1 -11 13.32 2.61 -11 1 -12 23.88 2.83 11 -1 -12 21.91 3.45 11 1 -12 20.66 3.19 -11 -1 -12 21.47 2.08 -11 1 -12 19.91 2.19 -11 1 -13 5.52 2.35 11 -1 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20.61 2.52 -11 -3 -5 19.94 2.47 11 -3 -5 24.89 2.09 11 -3 -5 15.31 1.26 -11 -3 -5 18.31 1.19 -11 -3 -5 18.66 2.72 11 -3 -6 16.80 1.52 -11 3 -6 12.88 1.46 11 3 -6 15.91 1.02 11 -3 6 17.53 2.66 11 3 -6 12.38 2.01 -11 -3 -6 15.80 2.40 -11 -3 -6 12.01 2.29 -11 -3 -6 16.49 1.19 11 -3 -7 19.64 1.94 -11 -3 -7 20.83 1.46 -11 3 -7 16.56 1.90 11 3 -7 18.64 1.24 11 3 -7 22.06 2.18 11 -3 7 14.60 2.43 -11 -3 -7 14.74 2.48 -11 3 -7 17.96 2.77 -11 -3 -7 23.25 2.67 -11 -3 -8 29.73 2.09 -11 3 -8 30.32 2.55 11 3 -8 34.44 1.94 11 -3 8 37.56 3.16 -11 -3 -8 31.21 3.11 11 3 -8 39.15 2.69 11 -3 -8 36.46 2.82 -11 -3 -8 30.89 3.17 -11 3 -8 30.01 3.35 -11 3 -9 0.95 2.40 -11 3 -9 1.38 1.82 11 3 -9 0.24 0.79 -11 -3 -9 3.05 2.10 11 -3 9 -4.39 2.07 -11 -3 -9 2.63 2.22 11 -3 -9 0.73 1.97 -11 -3 -9 1.29 1.06 -11 -3 -10 1.73 2.10 11 -3 -10 4.56 2.35 -11 -3 -10 2.99 1.21 -11 3 -10 1.13 2.13 -11 3 -10 2.67 1.93 11 3 -10 2.72 0.93 11 -3 -11 1.75 2.53 -11 -3 -11 3.13 1.30 -11 3 -11 0.72 1.62 -11 3 -11 2.58 2.28 -11 3 -11 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5.81 2.10 11 5 2 3.30 1.46 -11 -5 2 5.79 2.33 11 -5 2 5.54 2.26 11 -5 -2 11.59 1.99 -11 -5 -2 7.53 0.68 11 5 -3 15.34 0.86 -11 5 -3 13.03 1.20 -11 -5 -3 17.51 2.31 11 -5 3 16.46 2.61 11 -5 -3 15.67 2.08 -11 -5 3 16.43 2.69 -11 -5 -3 12.13 2.36 11 5 -3 18.12 2.63 -11 5 -4 3.12 1.03 11 5 -4 2.48 0.50 -11 5 4 4.95 1.25 11 -5 4 5.82 2.35 11 5 -4 4.03 2.42 11 -5 -4 5.27 1.66 -11 -5 -4 4.53 2.09 -11 -5 -4 4.11 1.91 -11 -5 4 -1.85 2.53 -11 -5 -5 50.64 3.88 11 -5 5 69.42 4.44 -11 -5 -5 52.62 3.87 11 5 -5 59.37 4.16 -11 5 5 65.94 3.40 -11 5 -5 48.78 3.08 11 5 -5 51.34 2.74 -11 -5 5 42.34 4.27 -11 5 -6 2.99 1.32 -11 5 6 3.17 1.68 11 5 -6 1.79 0.64 11 -5 6 5.25 2.43 -11 -5 -6 5.02 2.09 11 5 -6 3.62 2.10 -11 -5 -6 2.54 1.84 -11 -5 6 -1.09 2.67 11 -5 7 1.40 2.14 -11 -5 -7 3.59 2.14 -11 -5 -7 2.96 2.04 11 5 -7 2.98 1.88 -11 5 -7 3.16 1.51 11 5 -7 0.58 0.72 11 -5 8 9.22 2.32 -11 -5 -8 5.47 2.11 11 5 -8 10.12 1.86 -11 -5 -8 7.33 2.22 -11 5 -8 8.73 1.70 11 5 -8 8.59 1.00 11 -5 9 19.03 2.64 11 5 -9 21.18 2.02 -11 -5 -9 19.35 2.52 -11 5 -9 21.27 2.87 -11 5 -9 18.31 2.23 11 5 -9 14.41 1.35 11 5 -10 2.64 1.47 -11 5 -10 2.22 1.87 11 5 -10 -0.30 0.98 -11 5 -10 0.65 2.22 -11 5 -11 -0.14 1.92 11 5 -11 0.48 1.04 -11 5 -11 1.65 2.21 -11 5 -12 9.64 2.32 11 5 -12 4.90 1.23 -11 5 -12 10.02 2.29 -11 5 -13 19.48 2.69 -11 5 -13 16.25 2.54 11 5 -13 20.95 1.80 -11 5 -14 -1.60 2.08 11 5 -14 1.68 1.36 11 5 -15 3.24 1.50 -11 5 -16 4.49 2.32 11 5 -17 -2.17 4.20 -11 5 -17 4.35 2.50 11 -5 -17 5.87 4.75 11 5 -18 -4.80 5.09 -11 -5 -18 2.09 1.96 11 -5 -18 -1.46 4.88 11 5 -19 -1.05 5.26 11 -5 -19 4.72 5.63 11 -7 0 0.64 2.03 -11 -7 0 -0.13 0.98 11 -7 0 -0.50 0.78 11 7 1 0.64 0.56 -11 7 1 0.56 1.02 -11 -7 -1 2.96 1.84 -11 -7 1 1.21 1.87 11 7 -1 2.18 1.21 11 -7 -1 5.07 2.05 11 -7 1 -1.80 2.28 -11 -7 1 1.47 0.92 -11 -7 -1 0.68 1.07 11 -7 -1 0.97 0.82 11 7 2 30.30 1.68 -11 7 2 30.10 2.05 11 -7 -2 30.12 2.77 11 7 -2 29.80 2.37 11 -7 2 28.96 3.17 -11 -7 2 27.46 2.86 11 -7 -2 30.03 1.86 11 7 3 24.04 1.42 -11 7 3 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0.69 2.58 -12 0 -13 1.18 1.66 12 0 -14 85.98 6.02 -12 0 -14 84.83 5.02 12 0 -15 -3.65 3.45 12 0 -16 69.50 6.15 12 0 -17 -4.14 4.04 12 0 -18 0.82 4.49 12 -2 0 3.21 2.33 12 2 0 12.88 2.60 12 2 1 246.69 13.41 12 2 -1 255.02 13.51 12 -2 1 262.87 13.56 12 -2 -1 243.47 13.37 12 2 2 5.25 2.19 12 -2 2 2.17 2.19 12 2 -2 3.27 2.26 12 -2 -2 2.14 2.21 -12 -2 -2 0.31 2.75 12 -2 3 266.57 13.56 12 2 -3 262.76 13.47 12 -2 -3 265.15 13.32 12 2 3 262.52 13.37 12 2 4 13.19 2.29 12 -2 4 11.21 2.55 12 -2 -4 10.68 2.21 12 2 -4 9.98 2.41 -12 -2 -4 8.65 2.68 12 -2 -5 132.48 7.31 12 2 -5 135.90 7.53 -12 -2 -5 113.52 7.78 -12 -2 -5 139.58 7.58 12 -2 5 145.33 7.79 12 2 5 117.19 7.29 12 -2 6 14.16 2.58 12 -2 -6 17.36 2.09 12 2 -6 8.58 2.18 -12 -2 -6 16.25 2.50 -12 -2 -6 8.76 2.60 -12 2 -6 14.60 3.07 12 -2 7 199.01 10.59 -12 -2 -7 221.39 10.61 12 2 -7 198.31 10.23 -12 2 -7 191.41 10.90 12 -2 -7 203.04 10.19 -12 -2 -7 195.47 9.57 12 -2 -7 177.14 9.58 -12 2 -8 2.35 2.59 12 2 -8 7.83 1.81 12 -2 -8 4.94 1.27 -12 -2 -8 2.86 1.09 12 -2 8 3.10 2.05 12 -2 -9 61.21 3.81 -12 -2 -9 61.14 3.52 12 2 -9 63.93 3.98 12 -2 -10 1.49 1.88 -12 -2 -10 0.33 1.20 12 -2 -11 94.24 5.90 -12 -2 -11 98.52 5.31 -12 2 -12 3.25 1.72 12 2 -12 0.35 1.92 12 -2 -12 4.07 2.40 -12 -2 -12 1.32 1.45 -12 2 -13 14.30 2.07 12 2 -13 10.03 2.54 12 -2 -13 14.84 3.02 -12 -2 -13 11.58 1.79 12 2 -14 4.68 2.80 -12 2 -14 2.47 1.95 -12 -2 -14 3.46 1.76 12 2 -15 43.02 4.41 12 -2 -15 42.34 4.71 12 2 -16 -0.65 3.34 12 -2 -16 2.77 3.80 12 -2 -17 1.14 4.09 12 2 -17 3.64 3.70 12 -2 -18 1.65 4.58 12 2 -18 -2.00 4.49 12 -4 0 273.53 13.45 12 4 0 278.05 13.33 12 4 -1 -2.65 2.21 12 4 1 2.53 2.03 12 -4 1 1.63 2.37 12 -4 -1 0.88 2.12 -12 -4 1 -4.29 2.83 12 4 -2 129.51 7.07 12 -4 2 124.82 7.09 12 -4 -2 110.64 6.76 12 4 2 122.63 6.61 12 4 -3 4.95 2.52 12 4 3 3.16 1.65 12 -4 3 9.25 2.49 12 -4 -3 7.40 2.12 -12 -4 -3 1.60 2.20 12 -4 4 677.26 30.79 12 4 -4 685.47 30.75 12 -4 -4 575.95 30.27 -12 -4 -4 526.50 30.58 -12 -4 -5 0.19 2.10 12 4 -5 0.65 2.37 12 -4 -5 2.54 1.73 -12 -4 -5 1.35 0.52 12 -4 5 2.18 2.36 12 -4 6 35.66 3.53 -12 -4 -6 39.32 3.43 12 -4 -6 40.12 3.10 12 4 -6 40.59 3.48 12 -4 -6 37.58 2.26 -12 -4 -6 38.00 2.15 -12 4 -7 2.35 1.29 12 4 -7 2.54 0.66 12 -4 7 3.23 2.29 12 4 -7 2.79 2.09 -12 -4 -7 4.63 2.29 12 -4 -7 2.43 1.22 -12 -4 -7 3.59 0.93 12 4 -8 104.59 5.33 -12 4 -8 108.04 5.75 12 -4 8 108.67 6.52 -12 4 -8 111.78 6.82 12 4 -8 107.84 6.16 -12 -4 -8 110.06 6.45 12 -4 -8 103.55 5.81 -12 -4 -8 103.78 5.48 -12 4 -9 1.15 1.62 12 4 -9 3.01 0.84 12 -4 9 -0.64 2.04 -12 4 -9 6.24 2.54 12 4 -9 3.12 1.71 -12 -4 -9 2.31 1.12 12 -4 -9 2.91 1.77 -12 4 -10 104.08 5.78 12 4 -10 95.31 5.20 12 4 -10 104.59 5.80 12 -4 -10 108.09 6.07 -12 -4 -10 103.92 5.40 12 4 -11 6.07 1.60 -12 -4 -11 4.17 1.42 12 -4 -11 8.04 2.43 12 4 -11 1.90 1.00 -12 -4 -12 166.39 8.61 12 -4 -12 173.65 9.50 12 4 -12 163.68 8.39 12 4 -13 3.25 1.16 -12 -4 -13 3.59 1.53 12 -4 -13 0.76 2.73 12 4 -14 7.28 1.42 -12 -4 -14 9.06 1.74 12 -4 -14 7.59 3.22 12 -4 -15 2.49 3.39 12 -4 -16 21.45 4.04 12 -4 -17 0.37 4.10 12 -4 -18 39.76 5.61 12 6 0 15.24 1.98 12 -6 0 11.64 2.61 -12 -6 0 15.58 2.56 12 -6 -1 111.63 6.54 -12 -6 -1 100.24 6.52 -12 -6 1 94.07 6.50 12 6 -1 107.72 6.11 12 6 1 100.83 5.90 12 6 -2 13.22 2.20 12 -6 2 9.00 2.61 12 -6 -2 7.84 2.24 -12 -6 2 7.97 2.55 12 6 -3 227.27 9.66 -12 -6 3 164.42 9.66 12 -6 3 238.20 10.01 12 -6 -3 205.00 9.43 -12 6 -3 179.03 8.33 12 6 -3 155.43 8.20 -12 -6 -3 196.13 8.40 -12 6 -4 2.17 0.96 12 6 -4 0.27 0.45 12 -6 4 -0.98 2.33 12 6 -4 1.27 2.33 12 -6 -4 3.21 1.75 -12 -6 -4 0.37 2.16 -12 -6 4 -0.26 2.59 -12 -6 5 108.03 8.25 12 -6 5 170.21 8.55 12 6 -5 181.90 8.57 -12 -6 -5 148.05 8.12 12 -6 -5 130.55 7.83 -12 6 -5 152.48 7.28 12 6 -5 138.24 7.02 -12 6 -6 2.92 1.26 12 6 -6 0.29 0.64 12 -6 6 1.46 2.35 12 6 -6 0.23 2.59 -12 -6 -6 0.95 2.30 -12 -6 6 -1.08 2.56 -12 -6 -7 80.33 5.39 12 6 -7 102.17 5.78 -12 -6 7 72.25 5.67 12 -6 7 87.72 5.66 -12 6 -7 90.72 4.71 12 6 -7 81.39 4.30 12 -6 8 4.21 2.38 -12 6 -8 7.06 1.60 12 6 -8 3.23 0.82 -12 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35.93 3.18 13 11 5 31.81 2.03 -13 -11 -6 0.40 2.36 13 -11 -6 4.64 2.21 13 11 6 1.55 0.92 -13 -11 -7 7.30 2.60 13 11 7 6.45 1.13 13 11 8 0.65 1.06 13 -11 8 6.56 2.68 13 11 9 2.92 1.18 13 11 10 0.77 1.22 13 -13 -2 32.54 3.63 13 13 2 36.40 2.33 13 -13 -3 0.67 2.30 13 13 3 -0.06 1.12 13 -13 -4 2.99 2.26 13 13 4 -1.11 1.10 13 -13 4 -1.02 2.63 13 -13 -5 2.29 2.25 13 13 5 0.88 1.13 13 -13 5 0.50 2.55 13 13 6 21.47 1.79 13 13 7 0.51 1.18 13 13 8 -0.76 1.21 13 15 3 6.56 1.43 13 15 4 2.65 1.37 14 0 0 31.27 3.42 14 0 -1 -0.73 2.40 14 0 1 1.45 2.38 14 0 2 57.02 4.45 14 0 -2 54.06 4.48 14 0 3 3.08 2.48 14 0 -3 -2.06 2.36 14 0 4 4.16 2.45 14 0 -4 9.69 2.71 14 0 5 -1.35 2.36 14 0 -5 -1.32 2.39 14 0 6 57.37 4.24 14 0 -6 57.47 4.34 14 0 -7 0.99 2.26 14 0 -8 45.56 3.68 14 0 -9 2.29 1.96 14 0 -10 19.05 2.46 14 0 -11 1.49 1.87 14 0 -12 5.35 2.02 14 -2 0 8.08 2.78 14 2 0 4.54 2.61 14 -2 1 13.22 2.75 14 2 1 10.75 2.68 14 2 -1 14.23 2.68 14 -2 -1 4.30 2.53 14 -2 2 1.95 2.46 14 2 -2 2.89 2.55 14 2 2 6.64 2.44 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3.59 2.05 14 4 -7 -1.11 2.53 14 -4 8 2.05 2.22 14 4 -8 3.88 2.59 14 -4 -8 4.40 2.09 14 -4 9 3.78 2.27 14 -4 -9 6.18 1.94 14 4 -9 -1.02 2.36 14 4 -10 53.98 4.17 14 4 -11 0.36 2.19 14 6 0 1.03 1.78 14 -6 0 -0.72 2.40 14 6 -1 0.74 1.98 14 -6 1 -0.74 2.55 14 -6 -1 4.08 2.58 14 -6 2 1.50 2.59 14 6 -2 1.17 2.14 14 -6 -2 -1.18 2.48 14 6 -3 24.90 2.94 14 -6 3 23.09 3.06 14 -6 -3 17.18 2.84 14 -6 4 0.99 2.47 14 6 -4 3.71 2.45 14 -6 -4 4.38 2.39 14 -6 5 9.10 2.62 14 6 -5 11.38 2.78 14 -6 -5 9.23 2.43 14 -6 6 11.90 2.76 14 6 -6 13.14 2.95 14 -6 -6 8.24 2.43 14 6 -7 18.12 3.17 14 -6 7 22.61 3.04 14 -6 8 1.88 2.38 14 6 -8 -1.67 2.82 14 -6 -8 4.83 2.03 14 -6 9 2.28 2.48 14 -6 -9 8.63 2.26 14 -8 0 69.55 5.14 14 -8 1 -0.74 2.47 14 -8 -1 -1.22 2.69 14 -8 -2 20.23 3.10 14 -8 2 29.65 3.37 14 -8 3 3.25 2.68 14 8 -3 1.82 1.57 14 -8 -3 5.72 2.48 14 8 -4 6.59 1.79 14 -8 4 6.46 2.61 14 -8 -4 2.38 2.23 14 8 -5 3.24 1.86 14 -8 5 7.66 2.72 14 -8 -5 2.68 2.34 14 -8 6 56.18 4.48 14 -8 -6 53.50 4.11 14 -8 7 4.62 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5 -5 7.83 2.94 15 -5 5 16.25 2.96 15 -5 -5 14.51 2.90 15 5 -6 3.11 2.84 15 -5 6 0.24 2.48 15 -5 -6 3.66 2.32 15 5 -7 0.72 2.78 15 -5 7 -0.71 2.45 15 -5 -7 -1.03 2.31 15 -5 -8 7.92 2.43 15 -5 -9 14.13 2.65 15 -5 -10 2.84 2.33 15 -7 0 -3.22 2.73 15 -7 1 -1.52 2.68 15 -7 -1 0.24 2.64 15 7 -2 12.25 2.25 15 -7 -2 10.11 2.84 15 7 -3 0.18 2.00 15 -7 3 3.99 2.79 15 -7 -3 -0.73 2.70 15 -7 4 6.18 2.82 15 -7 -4 1.41 2.46 15 -7 5 3.44 2.64 15 -7 -5 2.72 2.54 15 -7 -6 8.98 2.56 15 -7 -7 0.41 2.34 15 -9 0 1.49 2.70 15 -9 1 7.89 2.97 15 -9 -1 0.75 2.63 15 -9 -2 3.51 2.79 15 -9 -3 1.46 2.63 16 0 0 266.54 14.27 16 0 -1 2.65 2.69 16 0 1 2.86 2.82 16 0 2 37.89 3.90 16 0 -2 36.55 3.92 16 0 -3 0.72 2.81 16 0 3 -1.86 2.63 16 0 4 56.71 4.68 16 0 -4 72.40 4.95 16 0 5 0.66 2.40 16 0 -5 0.23 2.73 16 0 6 36.57 3.57 16 0 -6 29.80 3.58 16 0 -7 2.49 2.66 16 0 -8 121.36 7.42 16 0 -9 4.32 2.70 16 0 -10 6.65 2.76 16 0 -11 -1.79 2.48 16 2 0 6.79 2.86 16 -2 0 0.73 2.58 16 2 -1 65.79 5.14 16 2 1 64.40 4.91 16 -2 1 75.18 5.11 16 -2 -1 65.93 5.11 16 -2 2 -3.15 2.78 16 2 2 -2.71 2.75 16 2 -2 0.48 2.84 16 -2 -2 -0.25 2.80 16 -2 3 81.16 5.50 16 2 3 75.36 5.28 16 2 -3 81.49 5.38 16 -2 -3 67.81 5.30 16 2 4 0.43 2.37 16 2 -4 0.47 2.72 16 -2 4 0.95 2.67 16 -2 -4 1.88 2.77 16 2 -5 47.03 4.22 16 -2 5 44.65 4.12 16 -2 -5 40.48 3.97 16 -2 6 0.23 2.48 16 2 -6 0.23 2.79 16 -2 -6 2.57 2.54 16 -2 -7 47.95 4.23 16 2 -7 49.35 4.29 16 -2 -8 3.08 2.63 16 2 -8 -2.64 2.74 16 -2 -9 21.52 3.35 16 -2 -10 0.81 2.34 16 4 0 69.77 5.06 16 -4 0 75.48 5.46 16 4 1 2.12 2.34 16 -4 1 5.68 2.98 16 4 -1 1.58 2.70 16 -4 -1 4.00 2.70 16 -4 2 31.37 3.59 16 4 -2 36.12 3.64 16 4 2 20.31 3.10 16 -4 -2 24.80 3.49 16 4 -3 1.63 2.68 16 -4 3 2.93 2.66 16 -4 -3 -2.89 2.74 16 -4 4 161.19 9.36 16 4 -4 170.72 9.42 16 -4 -4 155.48 9.37 16 -4 -5 -2.40 2.78 16 4 -5 -3.78 2.85 16 -4 -6 9.58 2.96 16 4 -6 13.92 3.14 16 -4 -7 4.98 2.84 16 -4 -8 25.06 3.25 16 -6 0 3.30 3.06 16 -6 -1 45.06 3.93 16 6 -1 26.60 3.20 16 -6 -2 -2.70 2.85 16 6 -2 0.79 2.39 16 -6 -3 61.68 4.85 17 1 0 0.23 2.75 17 -1 0 5.73 2.95 17 -1 -1 7.42 2.92 17 -1 1 1.42 2.66 17 1 -1 -2.58 2.82 17 1 1 1.85 2.75 17 -1 2 6.84 2.90 17 1 2 5.91 2.63 17 1 -2 6.11 2.74 17 -1 -2 7.41 3.02 17 -1 -3 6.71 2.97 17 1 -3 9.40 3.08 17 1 3 7.36 2.75 17 -1 -4 4.57 2.92 17 1 -4 1.88 2.81 17 1 4 -1.73 2.56 17 -1 -5 -4.95 2.81 17 1 -5 5.63 2.94 17 1 -6 10.26 3.18 17 -1 -6 8.07 2.93 17 1 -7 6.15 2.98 17 -1 -7 0.69 2.85 17 3 0 0.67 2.63 17 3 1 6.60 2.72 17 3 -1 9.10 2.95 17 3 -2 4.13 2.75 17 3 2 4.03 2.53 17 3 -3 6.48 2.91 17 3 -4 3.49 2.89 17 5 0 -3.01 2.48 18 2 -1 0.45 2.82 18 2 -2 4.29 2.69 0 0 0 0.00 0.00 TITL FCC-124-01 in Pbca REM Pbca (#61, found as Pcab in ba-c setting) CELL 0.71073 17.610100 12.954830 18.864803 90.0000 90.0000 90.0000 ZERR 60.00 0.000749 0.000596 0.000938 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N I Pb UNIT 60.00 60.00 60.00 60.00 60.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 95600 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 3.736 _oxdiff_exptl_absorpt_empirical_full_min 0.443 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.25405(3) 0.37595(2) 0.61993(2) 0.03606(14) Uani 1 1 d . . . . . I4 I 0.28522(10) 0.500000 0.500000 0.0558(3) Uani 1 2 d S T P . . I1 I 0.250000 0.49376(5) 0.750000 0.0387(2) Uani 1 2 d S T P . . I5 I 0.000000 0.40201(7) 0.60550(7) 0.0514(3) Uani 1 2 d S T P . . I2 I 0.250000 0.25778(5) 0.750000 0.0389(2) Uani 1 2 d S T P . . I6 I 0.250000 0.250000 0.500000 0.1171(8) Uani 1 2 d S . P . . I3 I 0.500000 0.35982(6) 0.63685(7) 0.0467(3) Uani 1 2 d S T P . . N2 N 0.000000 0.1919(8) 0.7241(9) 0.053(3) Uani 1 2 d S T P . . H2 H 0.000000 0.230321 0.750465 0.064 Uiso 1 2 calc R U P . . C7 C 0.000000 0.1942(10) 0.6466(12) 0.060(4) Uani 1 2 d S T P . . H7 H 0.000000 0.237507 0.621452 0.072 Uiso 1 2 calc R U P . . C5 C 0.000000 0.0706(11) 0.6430(12) 0.060(4) Uani 1 2 d S T P A . H5 H 0.000000 0.028673 0.615222 0.072 Uiso 1 2 calc R U P . . C2 C 0.000000 0.1341(16) 0.8439(10) 0.102(6) Uani 1 2 d DS TU P . . H2A H 0.000000 0.176(14) 0.884(14) 0.123 Uiso 1 2 d S U P . . C6 C 0.000000 0.1334(10) 0.6070(11) 0.053(4) Uani 1 2 d S T P . . H6 H 0.000000 0.134781 0.554191 0.064 Uiso 1 2 calc R U P . . C3 C 0.000000 0.1271(10) 0.7588(10) 0.055(3) Uani 1 2 d DS T P A . C4 C 0.000000 0.0686(10) 0.7179(11) 0.054(4) Uani 1 2 d S T P . . H4 H 0.000000 0.024915 0.742390 0.065 Uiso 1 2 calc R U P A . C1 C 0.0983(11) 0.1153(8) 0.8836(9) 0.096(5) Uani 0.5 1 d D U P A 9 H1A H 0.154789 0.135980 0.856163 0.144 Uiso 0.5 1 d R U P A 9 H1B H 0.107169 0.064820 0.885963 0.144 Uiso 0.5 1 d R U P A 9 H1C H 0.096609 0.134290 0.934203 0.144 Uiso 0.5 1 d R U P A 9 N1 N 0.0983(11) 0.1153(8) 0.8836(9) 0.096(5) Uani 0.5 1 d D . P A 10 H1D H 0.130999 0.155400 0.895073 0.115 Uiso 0.5 1 d R U P A 10 H1E H 0.137909 0.089110 0.853323 0.115 Uiso 0.5 1 d R U P A 10 H1F H 0.085049 0.091360 0.926083 0.115 Uiso 0.5 1 d R U P A 10 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.0418(3) 0.0381(2) 0.0282(2) 0.00014(14) -0.00095(16) -0.00241(18) I4 0.0636(8) 0.0604(7) 0.0434(6) 0.0234(5) 0.000 0.000 I1 0.0425(5) 0.0380(5) 0.0356(5) 0.000 -0.0030(4) 0.000 I5 0.0336(6) 0.0553(7) 0.0652(7) -0.0071(6) 0.000 0.000 I2 0.0392(5) 0.0417(5) 0.0358(5) 0.000 0.0038(4) 0.000 I6 0.174(2) 0.1142(14) 0.0631(10) -0.0582(10) 0.0253(11) -0.0623(14) I3 0.0276(5) 0.0489(6) 0.0637(7) 0.0107(5) 0.000 0.000 N2 0.044(8) 0.040(6) 0.076(7) -0.018(6) 0.000 0.000 C7 0.051(11) 0.053(8) 0.077(8) 0.012(7) 0.000 0.000 C5 0.046(10) 0.060(8) 0.075(8) 0.002(7) 0.000 0.000 C2 0.098(9) 0.124(11) 0.085(7) 0.005(7) 0.000 0.000 C6 0.039(9) 0.068(8) 0.053(8) 0.005(6) 0.000 0.000 C3 0.025(7) 0.063(7) 0.077(7) 0.007(6) 0.000 0.000 C4 0.039(9) 0.046(7) 0.076(8) 0.018(6) 0.000 0.000 C1 0.095(5) 0.097(5) 0.095(5) 0.001(2) -0.002(2) 0.000(2) N1 0.095(5) 0.097(5) 0.095(5) 0.001(2) -0.002(2) 0.000(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag I4 Pb1 I1 88.065(16) . . ? I4 Pb1 I5 88.06(3) . . ? I4 Pb1 I2 172.64(3) . . ? I4 Pb1 I6 96.372(10) . . ? I4 Pb1 I3 90.31(3) . . ? I1 Pb1 I5 86.32(2) . . ? I1 Pb1 I2 88.34(2) . . ? I1 Pb1 I3 90.90(2) . . ? I2 Pb1 I5 98.11(3) . . ? I2 Pb1 I3 83.33(2) . . ? I6 Pb1 I1 175.367(18) . . ? I6 Pb1 I5 92.48(2) . . ? I6 Pb1 I2 87.397(17) . . ? I6 Pb1 I3 90.41(2) . . ? I3 Pb1 I5 176.82(3) . . ? Pb1 I4 Pb1 165.40(5) . 4_566 ? Pb1 I1 Pb1 91.74(3) . 7_546 ? Pb1 I5 Pb1 160.91(5) . 12 ? Pb1 I2 Pb1 91.58(3) 7_546 . ? Pb1 I6 Pb1 180.000(16) 13_556 . ? Pb1 I3 Pb1 164.77(4) 12_655 . ? C7 N2 H2 120.9 . . ? C7 N2 C3 118.3(15) . . ? C3 N2 H2 120.9 . . ? N2 C7 H7 120.2 . . ? C6 C7 N2 119.6(18) . . ? C6 C7 H7 120.2 . . ? C6 C5 H5 120.1 . . ? C4 C5 H5 120.1 . . ? C4 C5 C6 120(2) . . ? C3 C2 H2A 137(10) . . ? C1 C2 H2A 82(7) 12 . ? C1 C2 H2A 82(7) . . ? C1 C2 C3 116.4(12) 12 . ? C1 C2 C3 116.4(12) . . ? C1 C2 C1 117(2) 12 . ? N1 C2 H2A 82(7) . . ? N1 C2 C3 116.4(12) . . ? C7 C6 C5 120(2) . . ? C7 C6 H6 119.8 . . ? C5 C6 H6 119.7 . . ? N2 C3 C2 111.4(18) . . ? C4 C3 N2 120.4(17) . . ? C4 C3 C2 128(2) . . ? C5 C4 H4 119.2 . . ? C3 C4 C5 121.5(19) . . ? C3 C4 H4 119.2 . . ? C2 C1 H1A 108.4 . . ? C2 C1 H1B 110.9 . . ? C2 C1 H1C 109.0 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C2 N1 H1D 108.0 . . ? C2 N1 H1E 110.0 . . ? C2 N1 H1F 110.4 . . ? H1D N1 H1E 109.5 . . ? H1D N1 H1F 109.5 . . ? H1E N1 H1F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 I4 3.1780(4) . ? Pb1 I1 3.1921(8) . ? Pb1 I5 3.3374(5) . ? Pb1 I2 3.1967(8) . ? Pb1 I6 3.1793(4) . ? Pb1 I3 3.2146(5) . ? N2 H2 0.8600 . ? N2 C7 1.37(2) . ? N2 C3 1.37(2) . ? C7 H7 0.9300 . ? C7 C6 1.34(3) . ? C5 H5 0.9300 . ? C5 C6 1.34(3) . ? C5 C4 1.32(3) . ? C2 H2A 1.1(3) . ? C2 C3 1.504(10) . ? C2 C1 1.497(7) . ? C2 C1 1.496(7) 12 ? C2 N1 1.497(7) . ? C6 H6 0.9300 . ? C3 C4 1.32(2) . ? C4 H4 0.9300 . ? C1 H1A 0.9601 . ? C1 H1B 0.9599 . ? C1 H1C 0.9601 . ? N1 H1D 0.8901 . ? N1 H1E 0.8900 . ? N1 H1F 0.8899 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N2 C7 C6 C5 0.000(7) . . . . ? N2 C3 C4 C5 0.000(6) . . . . ? C7 N2 C3 C2 180.000(6) . . . . ? C7 N2 C3 C4 0.000(6) . . . . ? C2 C3 C4 C5 180.000(6) . . . . ? C6 C5 C4 C3 0.000(6) . . . . ? C3 N2 C7 C6 0.000(6) . . . . ? C4 C5 C6 C7 0.000(6) . . . . ? C1 C2 C3 N2 108(2) 12 . . . ? C1 C2 C3 N2 -108(2) . . . . ? C1 C2 C3 C4 72(2) . . . . ? C1 C2 C3 C4 -72(2) 12 . . . ? N1 C2 C3 N2 -108(2) . . . . ? N1 C2 C3 C4 72(2) . . . . ?