#------------------------------------------------------------------------------ #$Date: 2024-06-19 05:04:57 +0300 (Wed, 19 Jun 2024) $ #$Revision: 292464 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/19/1571941.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1571941 loop_ _publ_author_name 'Nazarov, Yusufjon Eshkobilovich' 'Turaev, Khayit Khudaynazarovich' 'Alimnazarov, Bekmurod Khurramovich' 'Suyunov, Jabbor Ruziboevich' 'Umirova, Gulnora Abdurakhmonovna' 'Ibragimov, Bakhtiyar Tulyaganovich' 'Ashurov, Jamshid Mengnorovich' _publ_section_title ; Bis(8-hydroxyquinolinium) naphthalene-1,5-disulfonate tetrahydrate ; _journal_coeditor_code WM4216 _journal_issue 6 _journal_name_full IUCrData _journal_paper_doi 10.1107/S2414314624005704 _journal_volume 9 _journal_year 2024 _chemical_formula_iupac '2C9 H8 N O +, C10 H6 O6 S2 2-, 4H2 O' _chemical_formula_moiety '2(C9 H8 N O +), C10 H6 O6 S2 2-, 4(H2 O)' _chemical_formula_sum 'C28 H30 N2 O12 S2' _chemical_formula_weight 650.66 _chemical_name_systematic ; Bis(8-hydroxyquinolinium) naphthalene-1,5-disulfonate tetrahydrate ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary 'intrinsic phasing' _atom_sites_solution_secondary difmap _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _cell_angle_alpha 90 _cell_angle_beta 94.7152(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 7.55855(8) _cell_length_b 12.16674(13) _cell_length_c 16.00467(17) _cell_measurement_reflns_used 9285 _cell_measurement_temperature 290(2) _cell_measurement_theta_max 71.2150 _cell_measurement_theta_min 2.7890 _cell_volume 1466.85(3) _computing_cell_refinement ; CrysAlisPro (Rigaku OD, 2022) ; _computing_data_collection ; CrysAlisPro (Rigaku OD, 2022) ; _computing_data_reduction ; CrysAlisPro (Rigaku OD, 2022) ; _computing_molecular_graphics ; Olex2 (Dolomanov et al., 2009) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 290 _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix3000' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0256 _diffrn_reflns_av_unetI/netI 0.0169 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 14094 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 71.395 _diffrn_reflns_theta_min 4.571 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 2.246 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.82038 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2022) ; _exptl_crystal_colour 'light yellow' _exptl_crystal_density_diffrn 1.473 _exptl_crystal_description block _exptl_crystal_F_000 680 _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.28 _refine_diff_density_max 0.199 _refine_diff_density_min -0.295 _refine_ls_extinction_coef 0.0023(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL-2019/2 (Sheldrick 2015b) ; _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 214 _refine_ls_number_reflns 2841 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.053 _refine_ls_R_factor_all 0.0328 _refine_ls_R_factor_gt 0.0307 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0501P)^2^+0.3030P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0869 _refine_ls_wR_factor_ref 0.0886 _reflns_number_gt 2621 _reflns_number_total 2841 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file wm4216.cif _cod_data_source_block I _cod_original_cell_volume 1466.86(3) _cod_database_code 1571941 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.533 _shelx_estimated_absorpt_t_max 0.572 _shelx_hkl_file ; 0 0 1 7.91307 2.55636 3 0 0 1 14.0590 3.56469 1 0 0 2 117.053 11.9256 3 0 0 2 148.281 13.4843 5 0 0 2 145.815 14.2971 11 0 0 3-1.52325 6.29865 5 0 0 3 6.98140 6.85892 3 0 0 3 8.54710 8.03765 1 0 0 4 256096. 4652.73 1 0 0 4 244330. 4642.49 5 0 0 4 245069. 4638.15 3 0 0 4 247045. 4653.86 11 0 0 5 20.6043 13.5214 1 0 0 5 19.2623 11.6059 11 0 0 6 35472.5 743.951 5 0 0 6 34990.1 759.360 11 0 0 6 35927.5 764.120 12 0 0 7 13.3966 14.1485 2 0 0 7 9.96907 14.9822 12 0 0 7 14.5811 16.8685 11 0 0 8 28467.9 657.938 2 0 0 8 28204.3 672.854 12 0 0 8 28423.3 667.816 11 0 0 9 6.82964 18.1024 11 0 0 9 6.96485 18.4607 12 0 0 10 46316.5 1064.73 12 0 0 10 46942.0 1062.58 11 0 0 11 18.4446 26.1334 12 0 0 11 9.08502 22.2959 11 0 0 11 39.7722 29.8844 19 0 0 12 19065.0 565.387 11 0 0 12 18706.7 565.010 12 0 0 12 18006.5 573.024 19 0 0 12 18248.2 640.327 39 0 0 13 22.5353 31.9270 12 0 0 13-12.0732 32.0000 19 0 0 13-16.6923 23.6490 39 0 0 -14 2759.59 217.651 55 0 0 14 2573.20 194.238 19 0 0 -15 15.0316 36.8858 55 0 0 15-12.6929 35.9653 19 0 0 -16 4679.91 282.913 55 0 0 16 4497.47 255.357 19 0 0 -17 24.7845 32.8488 55 0 0 18 34.2481 36.1663 47 0 0 18 8.67324 24.5770 23 0 0 -18 9.97540 26.4410 55 0 0 -19 14.1548 21.2711 55 0 0 19 8.20444 20.1336 47 0 -1 0-3.16665 3.07279 38 0 -1 0 2.83184 2.31792 37 0 -1 0 0.75584 2.93385 40 0 -1 0 3.31160 3.21334 53 0 -1 0 10.2907 4.46481 13 0 -1 0 10.9878 3.95273 7 0 -1 0 0.90061 3.37690 4 0 -1 1 3976.32 94.7427 13 0 -1 1 3788.46 90.6324 12 0 -1 -1 3884.77 87.3847 34 0 -1 1 3871.47 97.2925 5 0 -1 1 3850.21 94.5242 36 0 -1 1 3640.48 97.2181 39 0 -1 -1 3985.85 94.6163 36 0 -1 2 870.850 39.0078 12 0 1 2 988.159 38.6958 11 0 -1 2 950.587 43.2858 11 0 -1 -2 897.699 28.2674 34 0 -1 2 962.063 36.2397 3 0 -1 2 883.534 42.0358 5 0 1 2 926.453 41.3002 1 0 -1 2 959.739 47.2684 39 0 1 3 132382. 2430.96 1 0 -1 3 127761. 2424.93 2 0 -1 3 130381. 2436.91 5 0 -1 3 130757. 2432.15 12 0 -1 3 126260. 2436.21 11 0 1 3 133153. 2425.80 11 0 1 4 9442.66 217.200 5 0 -1 4 9763.05 236.272 2 0 -1 4 9229.03 220.647 3 0 -1 4 9728.25 243.458 5 0 1 4 10170.5 240.938 1 0 -1 4 9610.69 245.097 11 0 1 4 9641.72 235.139 11 0 -1 4 9730.00 243.148 12 0 -1 5 94131.9 1841.30 5 0 -1 5 90546.7 1830.10 2 0 -1 5 88840.9 1807.42 3 0 1 5 97238.7 1839.89 1 0 1 5 95920.4 1827.24 3 0 -1 5 95865.0 1841.54 12 0 -1 5 97496.1 1849.21 11 0 1 5 99792.2 1833.54 11 0 -1 6 24787.3 557.875 5 0 1 6 24609.5 543.776 3 0 1 6 25366.8 556.924 1 0 -1 6 23403.4 545.528 2 0 -1 6 23991.7 560.677 12 0 1 6 25501.9 555.115 11 0 -1 6 24942.7 566.166 11 0 -1 7 84.1979 23.9329 5 0 1 7 59.9306 23.1315 1 0 -1 7 57.0558 20.1943 2 0 -1 7 52.0894 22.1809 11 0 1 7 78.6661 25.0010 11 0 1 8 41944.6 912.454 11 0 -1 8 41133.6 918.830 11 0 -1 8 40699.7 917.221 12 0 1 9 3539.10 171.409 11 0 -1 9 3812.15 180.946 12 0 1 9 3393.42 175.968 12 0 -1 10 16283.9 477.862 11 0 -1 10 16107.6 472.713 12 0 1 10 15767.8 462.211 11 0 1 10 15597.9 473.337 12 0 -1 10 17185.5 548.828 39 0 -1 11 100.263 37.6725 12 0 1 11 104.110 40.2491 12 0 -1 11 47.2141 29.9443 11 0 -1 11 40.3684 31.9993 19 0 -1 11 121.188 48.6554 39 0 -1 12 10731.1 410.411 19 0 1 12 11424.9 415.924 19 0 1 12 10565.8 395.915 12 0 -1 -12 11509.3 454.274 55 0 -1 12 10017.3 442.575 39 0 -1 13 11892.3 447.502 19 0 1 13 12368.0 455.280 19 0 1 13 11443.9 430.962 12 0 -1 13 11532.1 487.145 39 0 -1 -13 12151.6 482.542 55 0 1 13 10616.8 458.751 54 0 -1 -14 2797.09 225.046 55 0 1 14 2774.24 200.739 19 0 -1 14 2291.23 183.943 19 0 1 -15 9776.65 429.304 55 0 -1 -15 9715.33 434.276 55 0 1 15 9893.07 403.313 19 0 -1 15 9355.26 395.259 19 0 1 -16 1956.63 179.442 55 0 -1 -16 2255.24 192.464 55 0 1 16 1886.70 162.129 19 0 -1 17 10757.3 447.093 47 0 1 -17 11628.3 433.494 55 0 -1 -17 11442.4 439.756 55 0 -1 17 10638.8 403.437 23 0 1 17 10706.1 399.304 19 0 -1 18 367.274 70.8270 47 0 1 18 427.968 78.4487 47 0 -1 18 519.007 75.3394 23 0 1 -18 303.415 61.1825 55 0 -1 -18 264.749 59.8501 55 0 -1 -19 116.150 36.4035 55 0 1 19 72.2681 30.1489 47 0 -1 19 103.100 34.6750 47 0 -2 0 476746. 8653.87 40 0 -2 0 454748. 8634.59 37 0 -2 0 454639. 8658.45 13 0 -2 0 461159. 8651.31 7 0 -2 0 462277. 8642.29 5 0 -2 0 454999. 8659.53 4 0 -2 -1 34140.1 692.804 4 0 -2 1 34126.1 683.434 5 0 -2 1 34320.0 684.437 4 0 -2 1 33778.6 687.580 53 0 -2 1 34061.4 683.402 38 0 -2 -1 34831.0 677.335 34 0 -2 1 34618.8 683.786 13 0 2 1 35248.1 674.275 54 0 -2 2 3485.19 102.817 13 0 -2 2 3234.85 104.539 5 0 2 2 3251.58 104.547 1 0 -2 3 4368.12 141.728 39 0 -2 3 4081.73 134.082 5 0 2 3 4200.32 132.068 1 0 -2 3 4112.38 132.503 11 0 2 3 4487.27 122.452 11 0 -2 3 4171.04 125.717 12 0 -2 4 12274.5 325.498 39 0 2 4 12835.0 309.911 1 0 -2 4 12815.7 315.118 5 0 -2 4 12335.3 301.795 12 0 -2 4 12819.1 314.822 11 0 2 4 12860.0 295.847 11 0 -2 5 2884.53 130.968 39 0 2 5 2616.86 108.973 1 0 -2 5 2551.95 113.985 5 0 -2 5 2336.04 110.133 11 0 2 5 2701.11 104.657 11 0 -2 5 2424.76 106.638 12 0 -2 6 51800.4 1074.94 39 0 -2 6 48188.4 1032.21 5 0 2 6 48329.6 1021.37 1 0 -2 6 48502.3 1038.87 11 0 2 6 49929.9 1010.50 11 0 -2 6 48634.9 1020.94 12 0 -2 7 1386.92 108.229 39 0 2 7 1635.21 92.8423 3 0 -2 7 1630.00 101.656 5 0 2 7 1446.66 92.8514 1 0 -2 7 1554.61 100.647 11 0 2 7 1465.71 88.7575 11 0 -2 7 1504.92 95.2706 12 0 -2 8 33650.6 823.115 39 0 2 8 33964.9 765.277 1 0 -2 8 31914.5 767.344 5 0 -2 8 33275.0 763.593 12 0 -2 8 32713.7 775.668 11 0 -2 9 111.633 41.9887 39 0 -2 9 134.930 35.6545 5 0 2 9 202.935 41.2923 1 0 -2 9 98.1487 29.8961 12 0 -2 9 138.235 39.3047 11 0 2 10 42098.4 1002.00 12 0 -2 10 43171.1 1008.07 11 0 -2 10 42037.4 1058.69 39 0 -2 11 3154.40 200.193 19 0 2 11 3767.51 207.682 12 0 -2 -11 3532.72 225.540 55 0 -2 11 3374.21 228.081 39 0 -2 12 25104.8 731.755 19 0 -2 -12 27640.3 797.751 55 0 2 12 25631.8 776.191 54 0 2 12 26225.8 729.786 12 0 -2 13 358.029 75.5559 19 0 2 13 364.985 80.9188 54 0 -2 -13 347.689 81.8524 55 0 2 13 440.773 79.4706 12 0 -2 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13 0 3 2 122210. 2332.36 54 0 -3 -2 120768. 2359.09 4 0 -3 2 123097. 2344.04 5 0 -3 -2 124997. 2326.45 34 0 -3 2 120804. 2344.20 38 0 -3 2 122107. 2342.79 13 0 -3 3 11675.3 303.690 5 0 3 3 12352.1 306.147 1 0 -3 -3 11913.5 314.009 4 0 3 3 11797.4 278.891 11 0 3 4 24094.6 543.994 1 0 -3 4 24105.3 547.738 5 0 -3 4 23933.5 534.202 13 0 -3 5 2427.12 122.475 39 0 -3 5 2019.30 108.292 5 0 3 5 2108.21 105.161 1 0 -3 5 2115.99 100.334 12 0 -3 5 2256.57 107.565 13 0 -3 6 2215.06 128.475 39 0 -3 6 2317.88 123.574 5 0 -3 6 2076.61 108.294 12 0 -3 7 87.3828 29.4442 5 0 3 7 163.789 33.0947 1 0 -3 7 225.070 45.1700 39 0 3 8 6.54511 16.0622 1 0 -3 8 21.4017 21.4409 5 0 -3 8 8.78486 17.6023 39 0 3 9 6678.61 256.153 1 0 -3 9 5989.59 252.418 5 0 -3 9 5870.64 273.759 39 0 -3 -10 14206.8 490.281 55 0 -3 10 14566.4 470.963 25 0 3 10 13875.2 431.562 1 0 -3 10 13202.3 448.971 19 0 -3 10 14268.6 475.517 16 0 3 11 636.732 98.8486 54 0 -3 -11 490.963 89.7962 55 0 3 11 543.264 82.4228 12 0 -3 11 721.993 99.7651 16 0 -3 11 500.474 84.3981 25 0 -3 11 586.385 87.6664 19 0 3 12 3041.50 228.659 54 0 -3 -12 3516.89 245.584 55 0 3 12 4234.55 237.955 12 0 -3 12 3799.11 233.330 25 0 3 13 2169.05 196.058 54 0 -3 -13 2095.96 192.192 55 0 -3 13 2005.82 200.266 37 0 3 13 2131.23 175.134 12 0 -3 13 2322.71 184.844 25 0 3 14 11867.6 454.097 19 0 -3 -14 11855.0 496.654 55 0 -3 14 11276.8 449.432 25 0 -3 14 12464.1 479.053 23 0 3 15 3285.91 218.762 19 0 -3 -15 3276.59 241.335 55 0 -3 15 3468.27 252.291 47 0 -3 15 3163.60 222.211 23 0 3 16 651.987 97.1447 19 0 -3 -16 738.225 112.832 55 0 -3 16 404.129 87.4110 47 0 -3 16 600.127 93.2476 23 0 3 17 3928.35 214.288 19 0 -3 -17 3859.24 237.351 55 0 -3 17 3551.06 224.817 47 0 -3 17 3504.94 209.629 23 0 3 18 515.284 69.4354 19 0 -3 18 351.221 62.6931 47 0 -3 18 529.976 71.8243 23 0 -3 -18 476.239 75.8979 55 0 3 19 381.775 54.3494 47 0 -3 19 324.401 47.8583 47 0 -3 -19 392.343 55.3414 55 0 -4 0 124026. 2382.84 4 0 -4 0 123296. 2371.01 34 0 -4 0 121471. 2376.49 53 0 -4 -1 82052.1 1598.92 53 0 -4 1 76163.4 1596.11 53 0 -4 1 80847.0 1597.31 4 0 -4 -1 78948.8 1585.62 7 0 -4 -1 83487.3 1610.81 4 0 -4 1 81005.1 1589.36 38 0 -4 -1 81356.4 1586.34 34 0 -4 1 79902.1 1597.45 34 0 -4 1 84273.0 1600.05 13 0 -4 -2 195.439 32.0074 53 0 -4 2 137.433 23.8401 37 0 -4 2 155.896 26.9920 38 0 -4 2 174.375 28.2308 13 0 -4 -2 176.893 26.5611 34 0 -4 -2 163.520 29.6088 7 0 -4 -2 168.928 32.8718 4 0 -4 2 184.386 28.6949 5 0 4 3 8425.00 249.982 1 0 -4 -3 8300.12 259.451 4 0 -4 3 8379.87 248.220 5 0 -4 3 8607.41 245.710 13 0 -4 3 8366.89 247.379 38 0 -4 3 9182.83 257.278 37 0 4 4 40958.1 876.802 1 0 -4 4 40873.8 881.141 5 0 -4 -4 40437.7 892.498 4 0 4 4 40631.4 870.390 54 0 -4 4 41296.7 869.859 13 0 4 5 4590.72 178.214 1 0 -4 5 4233.44 177.558 5 0 4 5 4496.09 180.289 54 0 -4 5 4055.17 170.994 34 0 -4 5 4429.35 171.672 13 0 -4 6 19368.2 503.136 34 0 -4 6 20361.2 523.358 5 0 4 6 21457.3 518.798 1 0 -4 -6 19346.0 524.260 4 0 4 6 20788.6 527.718 54 0 4 7 7494.89 261.587 1 0 -4 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169.162 63.2663 23 0 -4 14 249.002 65.7505 25 0 4 15 60.7451 48.6855 19 0 -4 -15 31.3584 49.6732 55 0 -4 15 14.7594 39.1226 47 0 -4 15 13.2917 37.6651 23 0 4 16 1317.19 128.781 19 0 -4 -16 1015.51 130.000 55 0 -4 16 1236.40 136.814 47 0 -4 16 1423.01 138.307 23 0 4 17 9.09020 25.7610 19 0 -4 17 38.6128 32.0767 23 0 -4 -17 35.3005 33.3443 55 0 -4 -18 3514.08 197.496 55 0 -4 18 3527.42 178.629 23 0 -5 0 9.22745 17.2940 34 0 -5 0-4.98635 18.0108 53 0 -5 0 4.95423 17.8948 4 0 -5 1 3069.31 139.965 53 0 -5 -1 2936.82 137.989 53 0 -5 1 3058.00 136.709 34 0 -5 -1 2813.49 126.739 34 0 -5 -1 3209.04 144.851 4 0 -5 1 2915.59 134.016 4 0 -5 -1 3105.86 130.904 7 0 -5 -2 60691.2 1285.63 4 0 -5 -2 61253.3 1265.83 7 0 -5 -2 61759.1 1274.44 53 0 -5 2 59338.3 1256.98 38 0 -5 -2 61011.2 1247.19 34 0 -5 2 62433.7 1276.65 34 0 -5 2 64020.4 1271.02 13 0 5 3 732.531 66.6359 1 0 -5 -3 831.860 75.3548 4 0 -5 -3 640.079 63.7424 7 0 -5 3 721.637 67.7749 34 0 -5 3 672.534 62.3002 13 0 -5 -3 618.049 63.5384 53 0 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1197.11 137.569 24 -1 -9 -4 3753.28 260.045 55 -1 -9 -4 3839.71 254.456 53 1 -9 4 3530.88 268.078 49 1 -9 4 3634.55 252.711 48 1 9 4 3404.29 214.972 1 -1 -9 -4 3843.65 239.753 4 1 -9 4 4180.13 248.166 34 1 -9 4 4056.52 256.363 33 1 -9 4 3952.45 251.095 24 1 -9 4 4034.47 248.988 22 1 9 5 5579.13 283.021 14 -1 -9 -5 5658.52 328.575 55 -1 -9 -5 6057.54 328.923 53 1 -9 5 6082.50 334.324 48 1 -9 5 5740.31 316.175 46 1 9 5 6085.43 298.603 1 -1 -9 -5 6311.23 319.973 4 -1 -9 -5 5991.40 319.927 21 1 -9 5 5967.63 307.510 34 1 -9 5 5799.09 319.103 33 1 -9 5 6451.02 322.640 23 1 -9 5 5860.00 319.379 24 1 -9 5 5976.04 310.956 22 1 9 6 3733.88 225.901 14 -1 -9 -6 3395.38 254.136 55 1 -9 6 3367.04 250.872 48 1 -9 6 3723.24 246.402 46 -1 -9 -6 3185.61 240.105 53 1 9 6 4029.50 235.514 1 -1 -9 -6 3780.71 246.899 4 -1 -9 -6 3906.17 259.382 21 1 -9 6 2903.26 215.178 34 1 -9 6 3448.67 245.920 33 1 -9 6 3820.39 255.219 24 1 -9 6 3594.20 239.729 22 1 -9 6 3786.52 247.022 23 1 9 7 20260.1 628.668 14 1 -9 7 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164.262 23 1 -9 12 2067.78 170.610 24 -1 -9 -13 11.1046 27.2508 21 1 9 13 18.4856 34.6465 8 1 -9 13-10.6539 33.7520 24 1 -9 13 41.6520 37.6129 23 -1 -9 -13 64.9317 48.6783 55 1 9 14 1257.36 104.720 8 -1 -9 -14 1314.59 128.267 55 1 -9 14 1154.03 107.806 24 1 -9 14 1363.64 114.915 23 1 9 15 3093.87 144.535 8 -1 -9 -15 2904.19 169.605 55 1 -9 15 3223.22 158.862 23 1 -9 15 3336.05 160.259 24 1 -10 -14 19.0987 20.1683 29 -1 -10 14-7.07824 21.2731 22 1 -10 -13 509.398 71.1535 29 1 -10 -13 489.946 77.3134 21 1 -10 -12 4133.00 238.691 21 -1 10 12 3922.41 205.111 17 -1 -10 12 4126.20 235.111 22 1 -10 -12 4104.93 221.397 29 -1 -10 11 13.0032 29.1290 22 1 -10 -11 11.1914 33.6352 29 1 -10 -11 13.4676 40.4757 21 1 -10 -10 10175.8 438.668 21 1 -10 -10 10506.4 413.135 29 -1 -10 10 9891.03 429.390 22 -1 -10 10 10009.8 412.569 24 1 -10 -9 2583.27 214.137 21 -1 -10 9 2455.53 199.525 48 1 -10 -9 2399.50 190.209 29 -1 -10 9 2198.92 198.872 22 -1 -10 9 2835.63 212.650 24 1 -10 -8 10749.5 464.442 21 1 -10 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107.181 47.8204 14 -1 -10 -8 238.665 76.4372 55 1 -10 8 124.443 51.7753 48 -1 -10 -8 171.329 69.8476 21 1 -10 8 145.725 56.6239 33 1 -10 8 213.205 65.3244 23 1 -10 8 315.817 79.7803 24 1 10 9 4826.31 257.030 14 -1 -10 -9 4664.54 301.388 55 1 -10 9 4835.49 286.486 48 1 10 9 4666.14 265.368 8 -1 -10 -9 4864.89 293.617 21 1 -10 9 4576.47 273.290 33 1 -10 9 4620.01 273.426 23 1 -10 9 4738.37 281.878 24 -1 -10 -10 717.676 119.735 55 1 -10 10 806.215 111.778 48 -1 -10 -10 853.968 119.995 21 1 10 10 622.824 95.7930 8 1 -10 10 666.512 101.933 31 1 -10 10 544.367 94.4665 33 1 -10 10 803.950 112.199 23 1 -10 10 709.371 108.046 24 -1 -10 -11 894.503 124.423 55 -1 -10 -11 1030.73 123.696 21 1 10 11 860.068 103.903 8 1 -10 11 972.155 112.195 31 1 -10 11 1061.18 115.984 33 1 -10 11 976.396 114.105 23 1 -10 11 863.152 112.103 24 1 10 12 2458.78 161.086 8 -1 -10 -12 2234.82 182.236 55 1 -10 12 2352.42 168.002 24 -1 -10 -12 2510.99 180.788 21 1 10 13 1080.18 97.0315 8 -1 -10 -13 1180.99 120.296 55 1 -10 13 1119.85 104.189 24 -1 -10 -13 1112.63 107.516 21 1 10 14 1349.53 90.7052 8 1 -10 14 1262.46 96.1002 24 -1 -10 -14 1422.15 112.687 55 -1 -11 13 530.003 64.5388 22 -1 -11 13 627.352 66.8582 31 1 -11 -13 577.266 76.3393 49 1 -11 -12 53.7360 32.3737 21 -1 -11 12 84.9495 35.1109 22 1 -11 -11 2141.26 163.808 21 -1 11 11 2304.57 147.670 17 -1 -11 11 2252.82 165.381 22 1 -11 -10 1136.78 130.554 21 -1 -11 10 1091.75 117.246 24 -1 -11 10 1452.86 142.542 22 1 -11 -9 2419.11 192.836 21 -1 -11 9 2116.75 174.313 24 -1 -11 9 2363.82 191.138 22 -1 -11 9 2333.89 181.669 48 1 -11 -8 1029.04 130.969 21 -1 -11 8 743.318 110.715 24 -1 -11 8 1237.69 143.198 22 -1 -11 8 1339.86 144.993 48 1 -11 -8 860.040 132.363 50 1 -11 -7 279.603 73.8225 21 -1 -11 7 121.132 54.8406 22 -1 -11 7 230.885 67.9259 24 -1 -11 7 299.821 75.1984 48 1 -11 -7 242.066 75.6106 50 -1 -11 6 2773.64 217.868 24 -1 -11 6 2528.52 212.327 22 -1 -11 6 2961.62 228.263 48 1 -11 -6 2658.02 235.859 50 -1 -11 5-15.8642 44.9513 22 -1 -11 5 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29.5046 39.1163 31 1 -11 3 89.9176 49.8050 24 1 -11 3 140.553 56.4196 48 -1 -11 -3 39.5717 48.5645 49 1 -11 3 39.3817 48.3314 49 1 11 4 1100.09 123.046 14 -1 -11 -4 895.833 137.958 55 1 -11 4 1140.23 134.200 30 1 -11 4 1057.06 135.699 31 1 -11 4 1159.52 144.491 24 1 -11 4 969.247 135.592 48 -1 -11 -4 1270.10 169.561 49 1 11 5 4496.89 254.126 14 1 -11 5 4897.93 300.450 48 -1 -11 -5 5097.38 334.412 49 -1 -11 -5 5152.88 317.429 55 1 -11 5 5288.16 302.912 31 1 -11 5 4826.30 291.810 24 1 11 6 11.5301 30.5612 14 -1 -11 -6 18.6343 41.7429 49 1 -11 6 15.6463 35.0495 48 -1 -11 -6 33.2965 47.1733 55 -1 -11 -6 14.5641 32.6254 21 1 -11 6 14.6373 38.7967 31 1 -11 6-14.7570 33.0575 24 1 11 7 6905.94 311.411 14 1 -11 7 6889.15 353.648 48 -1 -11 -7 6329.86 353.675 55 -1 -11 -7 6381.90 336.404 21 1 -11 7 7262.94 352.272 31 1 -11 7 6815.71 343.656 24 1 11 8 1342.13 128.296 14 -1 -11 -8 1222.85 148.949 55 1 -11 8 1377.01 146.011 48 -1 -11 -8 1146.99 137.846 21 1 -11 8 1175.95 137.199 31 1 -11 8 1296.11 141.839 24 1 11 9 5940.44 271.148 14 -1 -11 -9 5957.55 321.686 55 1 -11 9 5827.58 297.820 48 1 11 9 6148.79 290.226 8 -1 -11 -9 6079.15 310.835 21 1 -11 9 6035.12 301.335 31 1 -11 9 5508.78 290.668 24 -1 -11 -10 39.0155 39.0969 55 1 -11 10 52.7765 38.1376 48 -1 -11 -10 47.6462 33.7646 21 1 11 10 48.5358 36.3982 8 1 -11 10 64.3305 38.7386 31 1 -11 10 55.3341 38.4169 24 -1 -11 -11 5064.75 268.185 55 -1 -11 -11 5637.04 269.141 21 1 11 11 6004.45 249.604 8 1 -11 11 5259.43 244.184 31 1 -11 11 5413.18 253.017 24 1 11 12 6.56308 22.7893 8 -1 -11 -12 92.4369 35.7248 21 1 -11 12 68.2525 32.2417 24 -1 -11 -12 64.0488 34.3058 55 -1 -12 11 28.3743 24.6241 31 1 -12 -11 38.7612 32.2022 49 -1 -12 10 1503.67 123.529 31 1 -12 -10 1468.83 125.588 21 1 -12 -10 1826.07 157.745 49 -1 -12 9 597.163 85.5380 31 1 -12 -9 559.435 83.1019 21 -1 -12 9 605.449 84.0935 48 1 -12 -9 614.711 101.518 49 1 -12 -8 9707.70 390.492 21 -1 -12 8 10344.8 397.301 48 1 -12 -8 10784.7 462.758 49 1 -12 -7 202.802 69.8548 49 -1 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440.292 11 2 1 4 18478.7 469.066 6 2 -1 4 19230.1 480.144 39 2 1 4 18565.2 469.444 39 2 -1 4 19206.8 471.302 37 2 -1 5 400.830 46.0182 54 2 1 5 270.400 43.6532 54 2 1 5 346.885 45.0519 11 2 -1 5 386.971 45.2585 11 2 1 5 404.673 54.0954 6 2 -1 5 318.501 50.1579 39 2 -1 5 321.520 47.0279 37 2 -1 6 1828.98 106.702 54 2 1 6 1587.38 109.050 54 2 -1 6 1620.45 103.176 11 2 1 6 1890.92 110.021 11 2 1 6 1793.24 112.153 6 2 -1 6 1536.01 117.793 39 2 -1 6 1598.08 113.170 37 2 1 7 15421.1 428.643 11 2 -1 7 15063.8 423.162 11 2 1 7 14975.0 445.455 54 2 -1 7 15076.4 454.139 37 2 1 7 16013.1 487.000 39 2 -1 7 15029.1 474.033 39 2 -1 8 1040.00 93.4334 11 2 1 8 1015.77 93.2632 11 2 1 8 1232.57 110.255 54 2 1 8 1064.58 115.573 39 2 -1 8 1174.36 110.871 37 2 -1 8 1221.36 119.838 39 2 1 9 38556.3 952.140 54 2 -1 9 39223.7 925.363 11 2 1 9 39227.1 919.170 11 2 -1 9 37482.3 945.005 8 2 1 9 38771.8 946.272 8 2 1 9 38208.0 1003.98 39 2 -1 9 37775.7 997.345 39 2 -1 9 36937.0 958.944 37 2 1 10 2102.15 164.556 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6 55184.5 1126.41 3 -2 -2 6 50986.8 1125.15 3 -2 -2 6 52420.3 1132.15 5 -2 2 6 51933.1 1107.60 12 -2 2 5 12424.5 338.592 3 -2 -2 5 11792.5 340.517 3 -2 2 5 12340.1 325.262 12 2 2 -4 9138.57 253.590 41 -2 2 4 9505.14 269.012 3 -2 -2 4 9267.76 275.183 3 2 -2 -4 8954.36 270.577 7 -2 2 4 9334.24 249.902 12 2 2 -3 1385.93 78.7863 41 -2 2 3 1506.19 75.8599 1 -2 2 3 1544.36 83.1915 3 -2 -2 3 1509.48 89.1249 3 2 -2 -3 1366.20 82.0064 7 -2 -2 3 1513.11 88.5821 13 -2 2 2 21222.8 459.395 1 -2 2 2 21471.3 477.508 3 -2 -2 2 20997.4 490.959 3 2 -2 -2 21672.8 484.480 7 2 2 -2 20971.9 493.126 10 -2 -2 2 20855.7 488.665 13 -2 -2 1 233.122 31.6691 13 2 2 -1 174.364 28.5466 10 -2 2 1 167.670 23.8180 3 2 -2 0 32686.9 700.884 40 2 -2 0 31523.0 681.607 37 2 -2 0 33402.8 689.786 38 2 -2 0 32413.9 667.508 10 -2 -2 0 31654.0 679.276 13 2 2 0 33717.9 693.954 10 -2 -2 0 31315.2 688.589 53 2 -2 1 2932.98 122.973 38 2 -2 1 3029.52 123.734 37 2 -2 1 2988.08 133.630 40 -2 -2 -1 3002.23 117.368 13 2 -2 1 2984.35 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268.059 8 2 2 14 5139.72 266.769 19 2 -2 14 4275.37 259.211 33 2 -2 14 4608.47 273.636 25 2 2 15 362.524 71.7717 19 2 -2 15 479.946 90.3867 25 2 2 15 398.211 81.1885 8 2 -2 15 592.066 107.834 47 2 2 16 2075.83 151.951 19 2 2 16 1987.23 159.126 8 2 -2 16 1808.41 171.834 47 2 -2 16 2072.76 165.620 23 2 -2 16 1861.95 157.283 25 2 2 17 172.346 46.7321 8 2 -2 17 312.227 59.8102 25 2 -2 17 291.859 59.8410 23 2 -2 17 328.442 70.1027 47 2 -2 18 3240.40 164.669 23 2 -2 18 3191.70 161.921 25 2 2 18 2974.06 156.750 25 2 3 -19 806.573 75.0492 55 2 -3 -19 735.508 72.1541 55 -2 -3 18 3014.31 175.849 16 -2 3 18 3311.29 177.543 16 2 3 -18 3148.58 179.802 55 2 -3 -18 2919.68 175.724 55 -2 3 17 1348.63 127.159 16 -2 -3 17 1273.18 127.692 16 2 3 -17 1224.78 127.130 55 2 -3 -17 1269.26 129.836 55 -2 -3 16 39.2795 39.3503 16 2 -3 -16-13.1062 34.7383 55 -2 3 15 890.848 115.149 17 -2 -3 15 869.507 124.413 16 2 -3 -15 1101.21 137.031 55 -2 -3 14 1570.23 165.626 16 -2 3 14 2069.46 173.836 17 2 -3 -14 1817.78 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3 -2 -3 7 20205.9 543.379 5 -2 -3 7 18990.6 527.401 3 -2 -3 7 19517.0 551.764 13 -2 3 7 20096.6 513.120 12 -2 -3 6 6.49961 19.5361 3 -2 -3 6 40.1215 25.0668 5 -2 3 6 6.16022 18.5162 3 -2 3 6 22.9599 15.2167 1 2 -3 -6 7.00430 18.5673 7 -2 -3 6 36.5855 23.1821 13 -2 -3 5 8969.75 293.952 5 -2 3 5 9542.37 280.109 1 2 -3 -5 9198.68 299.974 7 -2 3 5 9639.96 291.243 3 -2 -3 5 9095.10 303.872 13 -2 -3 4 7496.75 242.790 5 -2 3 4 7485.29 240.010 3 -2 3 4 7174.64 222.660 1 2 -3 -4 7274.61 246.510 7 -2 -3 4 7351.68 250.665 13 2 -3 -4 7098.10 232.519 35 -2 3 3 30313.8 646.922 1 2 -3 -3 28711.5 675.736 7 -2 3 3 29903.4 663.678 3 2 3 -3 28967.0 663.485 10 -2 -3 3 30027.9 685.300 13 2 -3 -3 31568.1 680.701 35 -2 3 2 2728.09 116.765 3 2 -3 -2 2745.60 125.106 7 2 -3 -2 2773.60 128.130 35 2 -3 -2 2778.14 126.978 34 -2 -3 2 2648.01 126.989 13 2 3 -2 2964.73 123.552 10 -2 3 1 87243.4 1767.10 3 2 -3 -1 94394.1 1821.67 40 2 -3 -1 90589.0 1803.11 34 2 -3 -1 93353.4 1811.27 35 -2 -3 1 91505.3 1803.74 13 2 3 -1 89576.7 1786.37 10 2 -3 0 19576.5 470.171 38 2 -3 0 19336.1 456.209 37 2 -3 0 19432.8 483.236 40 -2 -3 0 18939.5 472.907 53 2 -3 0 18825.4 469.146 35 2 -3 0 19251.4 469.522 34 -2 -3 0 19288.0 464.428 13 2 -3 1 2679.39 127.665 35 2 -3 1 2830.82 129.139 34 -2 -3 -1 2704.66 126.920 53 2 -3 1 3001.47 133.092 38 2 -3 1 2630.93 122.198 37 2 -3 1 2551.76 133.821 40 2 -3 2 39378.0 849.127 38 2 -3 2 38756.1 870.584 40 2 -3 2 38502.6 843.236 37 -2 -3 -2 37714.1 832.308 53 2 -3 2 37596.9 837.596 35 2 -3 2 39121.6 837.088 34 2 -3 3 26898.1 629.134 37 2 -3 3 26657.6 613.755 35 2 -3 3 25501.0 606.656 34 -2 -3 -3 26517.6 610.920 53 -2 -3 -4 16.0488 17.7751 53 2 -3 4 6.40773 18.1570 37 2 3 4 4.46279 10.9524 1 2 -3 4 20.2863 16.0673 34 2 3 4 5.10150 14.4561 11 2 3 5 4610.48 172.728 1 2 -3 5 4362.95 199.917 37 2 -3 5 4484.33 177.389 11 2 3 5 4790.29 188.917 11 -2 -3 -5 4429.82 185.969 53 2 -3 6 3914.55 199.287 37 2 -3 6 3893.33 173.601 11 2 3 6 3931.04 176.791 11 2 3 6 3820.01 189.739 54 -2 -3 -6 4006.85 181.763 53 2 -3 7 54467.1 1263.98 37 2 -3 7 56371.8 1214.59 11 2 3 7 56678.5 1214.85 11 2 3 7 54805.0 1254.43 54 2 -3 8 1311.13 127.209 37 2 3 8 1391.67 125.371 54 2 -3 8 1322.31 111.037 11 2 3 8 1391.10 112.310 11 2 -3 9 17708.4 588.392 47 2 -3 9 17092.4 554.306 8 2 3 9 17071.3 547.638 8 2 -3 9 17972.4 580.595 37 2 3 9 18356.7 571.390 54 2 -3 9 18600.1 536.460 11 2 3 9 18168.1 528.044 11 2 -3 10 2117.11 183.746 47 2 -3 10 2351.07 179.495 8 2 3 10 2375.95 179.186 8 2 -3 10 2094.92 180.572 37 2 3 10 2215.68 178.023 54 2 -3 10 2435.56 170.044 11 2 3 10 2217.60 156.974 11 2 3 11 7699.14 366.554 54 2 -3 11 8124.22 394.049 47 2 -3 11 7918.36 359.347 8 2 3 11 7705.96 351.754 8 2 -3 11 7334.19 371.252 37 2 3 11 8214.50 405.447 39 2 -3 11 7526.13 353.272 33 2 -3 11 8166.41 343.971 11 2 3 11 7994.09 333.098 11 2 3 12 1946.32 171.258 8 2 -3 12 1859.43 188.282 47 2 3 12 1725.06 170.739 54 2 3 12 1782.22 190.301 39 2 -3 12 1537.17 168.595 37 2 -3 12 1979.17 174.468 33 2 -3 12 2037.83 178.369 25 2 -3 13 10595.1 483.373 47 2 3 13 11393.9 451.641 8 2 -3 13 10291.5 429.234 33 2 -3 13 11303.0 456.343 25 2 -3 14 902.002 135.306 47 2 3 14 1336.31 143.493 8 2 3 14 1026.80 118.687 19 2 -3 14 1297.23 138.782 33 2 -3 14 895.176 122.652 25 2 -3 14 1014.38 129.091 23 2 3 15 1496.40 137.463 19 2 -3 15 1525.72 153.649 23 2 -3 15 1748.16 159.126 25 2 3 15 1416.72 141.318 8 2 -3 15 1757.49 174.410 47 2 3 16 687.854 88.2645 19 2 -3 16 642.992 94.1340 25 2 -3 16 719.309 98.7231 23 2 3 16 713.231 92.3247 8 2 -3 16 650.966 100.394 47 2 3 17 1573.36 117.076 19 2 -3 17 1793.27 135.814 23 2 -3 17 1791.83 134.911 25 2 -3 17 1709.04 143.273 47 2 3 17 1649.29 125.198 8 2 -3 18 165.024 37.3444 25 2 -3 18 132.248 35.7924 23 2 3 18 147.024 33.9541 25 -2 -4 18 4014.11 196.561 16 -2 4 18 4159.92 190.384 16 2 4 -18 4273.55 199.961 55 2 -4 -18 3733.13 191.665 55 -2 4 17 5043.29 242.681 16 -2 -4 17 4941.02 249.980 16 2 -4 -17 4610.23 243.029 55 -2 -4 16 3163.71 216.835 16 2 -4 -16 3522.52 225.896 55 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261.418 13 -2 -4 8 1166.31 112.206 5 -2 4 8 1196.17 105.212 1 -2 4 8 1105.51 104.316 3 2 -4 -8 793.402 95.6219 7 -2 -4 8 923.041 104.234 13 -2 -4 7 33232.7 823.187 5 -2 4 7 34204.6 812.809 3 -2 4 7 33313.0 797.743 1 2 -4 -7 33303.0 833.860 7 -2 -4 7 33510.1 838.079 13 -2 -4 6 26179.0 655.640 5 -2 4 6 25222.3 642.729 3 -2 4 6 26744.7 637.702 1 2 -4 -6 25685.6 666.487 7 -2 -4 6 25196.6 665.676 13 -2 -4 5 2328.30 134.004 5 -2 4 5 2255.69 129.183 3 -2 4 5 2084.47 118.549 1 2 -4 -5 2343.99 139.944 7 -2 -4 5 2255.31 139.289 13 -2 -4 4 7704.68 260.082 5 -2 4 4 8187.91 263.405 3 2 -4 -4 7740.69 255.943 4 -2 4 4 7741.75 244.915 1 2 -4 -4 8095.54 277.289 7 2 -4 -4 8178.66 263.974 35 -2 -4 4 7946.37 281.185 13 -2 -4 4 7594.43 264.115 36 -2 -4 3 53869.3 1131.95 5 -2 4 3 54535.4 1130.55 3 2 -4 -3 53462.5 1152.63 7 2 -4 -3 56130.8 1150.25 35 2 -4 -3 52859.6 1136.94 34 -2 -4 3 54019.6 1162.82 13 -2 -4 3 52185.6 1150.52 36 -2 -4 2 52913.7 1090.39 5 -2 -4 2 50730.1 1126.02 36 2 -4 -2 53522.7 1132.59 40 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225.676 37 2 -4 4 5677.91 216.371 34 2 4 4 5033.18 200.452 11 2 -4 5 354.155 58.4836 37 2 4 5 410.699 53.2697 1 2 4 5 312.524 48.0987 11 -2 -4 -5 293.136 50.5285 53 2 -4 6 273.548 57.3632 37 2 4 6 310.684 48.1921 1 2 4 6 342.407 53.0395 11 -2 -4 -6 385.770 60.3670 53 2 -4 7 1979.11 152.410 37 -2 -4 -7 2060.41 142.915 53 2 4 7 1964.19 131.281 11 2 4 8 5105.03 230.509 11 2 4 8 4856.90 233.241 14 -2 -4 -8 4841.11 255.780 55 2 -4 8 5031.39 268.910 47 2 4 8 5323.11 258.347 8 2 -4 8 4647.81 254.414 37 2 -4 8 5396.85 266.270 33 2 -4 8 4862.88 239.727 28 2 -4 8 4839.84 250.144 25 2 4 9 29.2409 25.8343 14 2 4 9-9.24614 24.5069 11 2 -4 9 9.67891 21.6816 11 2 4 9 11.2603 27.6316 8 2 -4 9 53.4152 35.3942 47 -2 -4 -9-12.3785 32.8091 55 2 4 9 12.0182 24.0796 54 2 -4 9-13.0051 26.0569 37 2 -4 9 35.7515 37.7529 33 2 -4 9 72.3694 38.7524 28 2 -4 9 58.0751 36.7958 25 2 4 10 24.4881 40.6840 8 2 -4 10 14.6808 29.4175 47 -2 -4 -10 68.0209 40.8880 55 2 -4 10 14.3730 28.8008 37 2 -4 10 38.4626 28.7231 33 2 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-4 9 211.446 63.1603 37 3 -4 9 106.208 46.0802 33 3 4 9 182.349 51.5417 11 3 4 10 13669.5 500.106 8 3 -4 10 13430.7 493.913 25 3 -4 10 13696.4 538.829 47 3 4 10 13197.0 465.275 20 3 -4 10 13862.6 513.308 33 3 4 10 14393.7 480.693 11 3 -4 11 33.0302 37.0082 47 3 -4 11 72.1720 45.7379 33 3 -4 11 95.4527 45.3175 25 3 4 11 27.5009 41.3370 8 3 -4 12 3614.63 266.993 47 3 -4 12 3840.29 252.471 33 3 -4 12 4440.34 262.542 25 3 4 12 3481.49 237.779 8 3 -4 13 1190.62 150.531 47 3 -4 13 1220.47 138.917 25 3 4 13 1425.48 146.950 8 3 -4 13 1359.04 147.963 33 3 -4 14 3725.65 230.976 25 3 -4 14 3550.01 222.969 23 3 4 14 3818.49 234.596 8 3 -4 14 4035.52 239.854 33 3 -4 15 8884.52 352.353 25 3 -4 15 8663.69 343.626 23 3 4 15 9051.05 354.185 8 3 -4 15 9105.85 353.315 33 3 -4 16 6276.63 263.255 25 3 -4 16 6773.62 265.712 23 3 4 16 6668.49 269.115 8 3 -4 16 6581.29 261.620 33 3 -4 17 11.7762 20.4388 25 3 4 17 46.7201 26.1682 8 -3 5 17 1332.66 111.535 16 -3 -5 17 1119.60 105.254 16 -3 -5 16 401.390 74.3149 16 -3 5 16 279.152 56.9526 18 -3 5 15 3994.93 228.216 17 -3 -5 15 3746.32 237.283 16 -3 5 15 4465.54 237.356 18 -3 -5 14 241.621 74.0429 16 -3 5 14 135.371 56.5718 17 -3 -5 14 130.972 57.2662 18 -3 -5 13 45.3966 52.5134 16 -3 5 13-13.0673 43.4170 17 -3 -5 13 14.3947 38.1531 18 -3 -5 12 9489.12 431.119 16 -3 -5 12 8733.66 410.890 18 -3 5 12 10002.8 412.310 17 3 5 -11 18742.8 598.505 56 -3 -5 11 19752.9 660.123 16 -3 -5 11 18779.4 649.785 18 -3 5 11 18482.8 611.132 17 3 5 -10 3694.56 227.255 56 -3 -5 10 3281.78 223.350 5 -3 5 10 3672.05 222.606 2 -3 5 10 3584.40 224.141 3 -3 -5 10 3537.58 243.227 13 -3 -5 10 3462.09 242.290 16 3 -5 -10 3912.20 258.643 21 -3 -5 10 3393.28 241.444 18 3 5 -9 2161.26 170.162 56 -3 -5 9 2523.27 197.146 16 3 -5 -9 2201.24 190.313 21 -3 -5 9 1878.27 175.356 18 -3 -5 9 1969.11 165.308 5 3 -5 -9 2084.41 170.763 7 -3 5 9 2168.87 167.883 3 -3 -5 9 2021.61 177.530 13 3 -5 -8 1300.40 133.070 56 3 5 -8 1387.17 132.668 56 3 -5 -8 1296.79 143.816 21 -3 -5 8 1492.08 153.638 18 3 -5 -8 1211.18 125.974 52 -3 5 8 1466.30 131.832 3 -3 -5 8 1355.88 131.956 5 3 -5 -8 1255.74 130.035 7 -3 -5 8 1500.39 147.591 13 3 -5 -7 1839.33 155.837 56 3 -5 -7 1916.72 170.202 21 -3 -5 7 1531.30 149.249 18 3 -5 -7 1855.16 151.363 52 -3 5 7 1750.05 139.732 3 -3 -5 7 1989.39 152.343 5 3 -5 -7 1997.66 155.479 7 -3 -5 7 1649.98 153.056 13 3 -5 -6 14716.5 489.167 56 3 -5 -6 14482.6 481.965 52 3 -5 -6 15175.6 525.820 21 -3 -5 6 15563.7 517.363 18 -3 -5 6 14698.1 499.159 13 -3 -5 6 14780.9 489.735 15 -3 5 6 15379.0 467.048 3 -3 -5 6 15311.0 480.539 5 3 -5 -6 14625.3 480.665 7 -3 -5 5 3878.47 219.128 13 -3 5 5 4076.27 199.759 3 -3 -5 5 3857.37 200.560 5 3 -5 -5 4146.57 230.097 40 -3 -5 4 1603.13 134.309 13 -3 5 4 1773.08 122.190 3 3 -5 -4 1610.91 136.581 40 -3 -5 4 1934.82 140.826 36 -3 -5 3 864.344 95.5607 13 -3 -5 3 758.182 90.2245 36 3 -5 -3 616.107 83.8033 40 -3 -5 2 7763.25 306.086 13 3 -5 -2 7955.68 307.255 35 3 -5 -2 7539.91 313.971 40 -3 -5 2 7958.84 313.194 36 3 -5 -1 16064.4 479.838 34 -3 -5 1 16303.8 488.854 13 3 -5 -1 16541.9 494.195 35 3 -5 -1 16064.7 506.020 40 -3 -5 1 16868.6 499.828 36 3 -5 0 8324.19 309.905 34 -3 -5 0 8472.94 321.060 36 3 -5 0 7860.91 310.707 35 3 -5 0 8454.49 334.628 40 3 -5 1 359.275 61.1842 34 -3 -5 -1 482.466 73.6757 53 3 -5 1 647.317 81.1080 35 -3 -5 -1 505.405 73.9381 36 3 -5 1 378.447 71.1515 40 3 -5 2 67814.0 1466.67 34 3 -5 2 67045.9 1445.76 37 3 -5 2 70001.9 1481.34 38 -3 -5 -2 67791.1 1476.24 36 3 -5 3 5664.43 253.065 34 -3 -5 -3 5390.79 252.611 53 3 -5 3 5499.52 247.224 37 3 -5 3 6060.89 268.137 38 -3 -5 -3 6000.71 261.166 36 -3 -5 -4 54181.1 1267.49 53 3 -5 4 56599.6 1266.36 37 3 -5 4 56603.6 1290.99 38 3 -5 4 56788.9 1267.77 34 3 5 4 54495.2 1238.78 11 3 -5 5 13590.3 448.614 28 3 -5 5 13863.4 489.930 48 -3 -5 -5 14297.3 487.295 21 3 -5 5 15330.6 482.808 37 3 -5 5 14057.8 478.637 38 3 -5 5 13823.1 493.561 42 3 -5 5 13933.0 487.644 32 3 -5 5 15120.9 482.789 33 3 5 5 13807.3 440.871 11 3 5 6 10395.4 402.397 6 3 -5 6 10108.1 371.198 28 3 -5 6 9789.26 404.195 48 -3 -5 -6 9677.04 393.454 21 3 -5 6 9468.00 399.331 42 3 -5 6 9796.72 394.283 38 3 -5 6 10143.4 393.080 37 3 -5 6 9810.06 398.149 32 3 -5 6 9737.62 386.692 33 3 5 6 9487.38 355.351 11 3 5 7 5340.60 271.791 8 3 -5 7 5111.79 260.235 28 3 -5 7 5682.18 298.845 48 -3 -5 -7 5074.84 277.657 21 3 5 7 5387.42 255.358 20 3 -5 7 5417.77 291.324 38 3 -5 7 4887.68 281.063 42 3 -5 7 5362.68 281.611 37 3 -5 7 5279.07 283.407 32 3 -5 7 5181.41 277.778 33 3 5 7 5366.70 255.581 11 3 5 8 195.078 59.9110 8 3 -5 8 160.722 58.7175 28 3 -5 8 152.090 53.7276 48 -3 -5 -8 91.6861 45.5512 21 3 5 8 166.661 51.2070 20 3 -5 8 167.232 55.9228 38 3 -5 8 243.445 66.4426 37 3 -5 8 151.903 51.8476 42 3 -5 8 290.405 70.0372 33 3 5 8 125.861 42.1339 11 3 -5 9 12.1846 36.6217 28 3 -5 9 88.8672 45.8575 25 3 -5 9-14.0991 31.5859 48 3 -5 9 29.2519 32.7659 37 3 -5 9 14.8507 29.7575 38 -3 -5 -9 54.3771 40.8581 21 3 5 9 91.0549 48.7599 8 3 -5 9 13.9808 34.3099 33 3 -5 10 307.566 73.5283 25 3 5 10 299.178 75.9998 8 3 -5 10 188.392 63.4586 33 3 -5 11 4471.62 268.900 25 3 5 11 4613.90 273.479 8 3 -5 11 4669.69 281.818 33 3 -5 12 2735.43 207.319 25 3 5 12 3361.88 228.324 8 3 -5 12 2699.56 210.214 33 3 -5 13 2190.87 179.893 25 3 5 13 2592.55 192.231 8 3 -5 13 2390.44 188.882 33 3 -5 14 236.923 59.9608 25 3 5 14 260.417 64.3086 8 3 -5 14 205.056 59.4567 33 3 -5 15-9.41015 35.2728 25 3 -5 15 9.24583 24.5062 33 3 5 15 9.42110 29.8457 8 3 -5 16 662.306 72.8210 33 3 5 16 540.118 71.1892 8 -3 -6 17 2000.37 122.525 22 -3 -6 17 1965.80 125.921 16 -3 6 17 2082.07 125.747 16 -3 -6 16 4436.11 217.818 22 -3 -6 16 4081.56 215.472 16 -3 6 16 4224.22 200.790 18 -3 -6 15 1485.20 139.862 16 -3 6 15 1358.94 126.509 17 -3 6 15 1454.11 128.708 18 -3 6 14 6282.53 297.594 17 -3 -6 14 5891.14 307.732 16 -3 -6 14 6086.11 301.744 18 -3 -6 13 43.9103 41.4836 16 -3 6 13 37.7734 39.8988 17 -3 -6 13 83.1183 53.7568 18 -3 -6 12 431.833 94.4663 16 -3 6 12 528.448 97.7259 17 -3 -6 12 615.117 107.760 18 -3 -6 11 23979.8 767.473 18 -3 -6 11 22435.3 753.514 16 -3 6 11 24619.8 735.836 17 3 -6 -11 24369.1 723.995 29 3 6 -11 25106.6 721.583 56 3 -6 -10 13968.1 539.475 21 -3 -6 10 12781.2 520.790 18 -3 -6 10 13460.8 526.077 16 3 6 -10 13403.5 486.517 56 3 -6 -10 13866.0 499.269 29 -3 6 9 3290.01 215.780 3 -3 -6 9 3006.02 211.456 5 3 -6 -9 3002.91 215.348 7 3 -6 -9 3076.30 227.915 51 3 6 -9 3328.08 217.248 56 -3 -6 9 3264.52 239.598 18 3 -6 -9 3402.79 243.856 21 -3 -6 9 3493.23 242.131 16 3 -6 -9 2914.02 206.791 29 -3 -6 9 3369.05 238.671 13 3 -6 -8 7875.07 349.730 29 3 -6 -8 8114.34 372.534 51 3 -6 -8 8374.82 393.351 21 -3 -6 8 8238.82 386.216 18 -3 -6 8 7863.39 348.992 5 -3 6 8 7912.95 344.397 3 3 -6 -8 8052.14 359.632 7 -3 -6 8 7794.66 374.976 13 3 -6 -7 684.894 97.5437 29 3 -6 -7 902.363 118.186 51 3 -6 -7 925.126 123.619 21 -3 -6 7 954.704 124.715 18 3 -6 -7 744.372 105.722 40 -3 -6 7 690.829 104.229 13 -3 -6 7 680.403 93.8019 5 -3 6 7 664.355 92.0872 3 3 -6 -7 582.089 92.7140 7 -3 -6 6 1079.46 126.509 13 -3 -6 6 882.180 111.019 15 3 -6 -6 1078.62 119.992 52 3 -6 -6 1270.90 133.810 51 3 -6 -6 1143.91 134.027 21 -3 -6 6 1250.90 136.595 18 3 -6 -6 1220.52 132.613 40 3 -6 -6 1252.71 127.814 29 -3 -6 6 1096.02 113.362 5 -3 6 6 1040.46 107.523 3 -3 -6 5 1736.13 152.453 15 -3 -6 5 1669.13 152.392 13 3 -6 -5 1909.21 155.496 52 3 -6 -5 2157.17 169.734 51 3 -6 -5 1767.52 166.341 21 -3 -6 5 1791.86 160.674 18 3 -6 -5 1724.22 154.244 40 3 -6 -5 1893.50 151.533 29 -3 6 5 2051.00 146.139 3 3 -6 -4 17467.7 549.855 52 3 -6 -4 19661.9 587.489 51 3 -6 -4 16634.8 577.834 21 -3 -6 4 18007.7 580.404 18 -3 -6 4 19574.9 571.515 36 3 -6 -4 17400.4 577.673 40 -3 -6 4 19616.5 594.745 13 -3 -6 4 18799.7 577.794 15 3 -6 -4 19399.4 569.201 29 -3 -6 3 1973.93 152.567 36 3 -6 -3 1894.19 158.568 40 3 -6 -3 1908.19 147.142 35 -3 -6 3 1849.64 151.908 13 -3 -6 3 1853.39 150.897 15 3 -6 -3 1925.22 148.251 29 3 -6 -3 1616.11 144.455 31 -3 -6 2 5208.91 258.313 36 3 -6 -2 5059.36 264.715 40 -3 -6 2 5445.14 265.821 13 3 -6 -2 5297.65 256.878 35 3 -6 -1 13213.1 440.817 34 3 -6 -1 13993.3 458.187 35 3 -6 -1 12949.3 465.750 40 -3 -6 1 13297.2 452.223 36 3 -6 0 41060.7 1017.32 35 3 -6 0 42931.3 1012.76 34 -3 -6 0 43936.6 1033.73 36 3 -6 1 52.4265 36.4362 35 3 -6 1 138.378 44.3226 34 3 -6 1 121.113 51.5105 40 -3 -6 -1 123.468 42.5406 36 -3 -6 -2 144.094 48.5046 53 -3 -6 -2 245.054 57.0398 36 3 -6 2 147.680 40.0058 37 3 -6 2 311.510 66.4714 32 3 -6 2 171.121 50.3536 35 3 -6 2 162.058 45.4881 34 3 -6 2 126.999 42.7419 28 -3 -6 -3 850.401 107.987 55 -3 -6 -3 895.015 108.406 53 3 -6 3 894.341 108.626 48 -3 -6 -3 1052.25 117.067 21 3 -6 3 1021.71 103.493 37 -3 -6 -3 1155.76 115.405 36 3 -6 3 983.027 113.546 38 3 -6 3 1143.91 124.075 44 3 -6 3 946.233 117.047 42 3 -6 3 932.243 113.107 32 3 -6 3 811.154 98.8109 31 3 -6 3 947.729 106.373 34 3 -6 3 1058.69 107.278 28 3 6 4-9.22243 22.6307 11 3 6 4-8.92314 17.8783 1 -3 -6 -4-10.2832 23.0352 4 -3 -6 -4 134.618 50.5492 55 3 -6 4-12.2752 24.5945 48 -3 -6 -4 22.9931 30.4716 53 -3 -6 -4-11.6291 28.5364 21 3 -6 4 11.5476 23.1366 38 3 -6 4 24.0810 31.9133 44 3 -6 4 10.1343 17.5846 37 3 -6 4 26.1067 32.0313 42 3 -6 4-10.7208 18.6022 34 3 -6 4 12.4079 21.5296 32 3 -6 4-9.77732 29.3845 28 3 6 5 1097.35 109.015 14 3 6 5 867.689 97.1778 11 -3 -6 -5 1031.02 117.120 4 -3 -6 -5 1023.34 124.206 55 -3 -6 -5 939.985 114.484 53 3 -6 5 708.326 105.820 48 -3 -6 -5 776.562 109.124 21 3 -6 5 878.338 105.290 37 3 -6 5 903.084 113.466 44 3 -6 5 1009.08 127.937 42 3 -6 5 1282.14 131.920 38 3 -6 5 1186.16 132.926 32 3 -6 5 914.378 112.044 33 3 -6 5 1183.29 118.431 28 3 -6 6 27862.5 769.084 28 3 -6 6 29491.9 836.213 48 -3 -6 -6 29264.7 820.510 21 3 -6 6 26889.8 777.353 37 3 -6 6 29034.7 816.352 38 3 -6 6 29283.6 842.900 42 3 -6 6 28739.2 825.251 32 3 -6 6 28508.1 806.518 33 3 6 6 27054.0 746.070 14 3 6 6 28049.7 752.664 11 3 6 7 9359.24 385.477 8 3 -6 7 8921.57 368.547 28 3 -6 7 8854.24 403.836 48 -3 -6 -7 9299.85 401.543 21 3 -6 7 9371.40 394.392 37 3 -6 7 8474.54 389.474 38 3 -6 7 9233.20 408.902 42 3 -6 7 8511.16 388.917 32 3 -6 7 8236.31 379.641 33 3 6 7 9480.26 363.987 14 3 6 8 840.300 115.867 8 3 -6 8 1077.98 125.118 28 3 -6 8 1012.71 132.220 48 -3 -6 -8 840.562 118.281 21 3 -6 8 858.770 119.187 37 3 -6 8 1121.92 139.175 42 3 -6 8 1153.31 136.883 38 3 -6 8 1193.97 138.398 33 3 6 8 1044.66 115.575 14 3 -6 9 209.997 64.5158 25 3 -6 9 238.748 65.5111 28 3 -6 9 179.305 61.8249 48 -3 -6 -9 116.719 54.8086 21 3 6 9 288.667 65.5357 14 3 -6 9 189.384 62.0241 33 3 6 9 189.018 62.0879 8 -3 -6 -10 5512.97 308.777 21 3 -6 10 5356.98 295.733 25 3 6 10 5312.48 293.936 8 3 -6 10 5427.54 307.350 33 3 -6 11 1437.27 149.544 25 3 -6 11 1343.67 150.342 33 3 -6 12 1079.75 128.542 25 3 6 12 1372.52 145.368 8 3 -6 13 1089.37 122.659 25 3 6 13 955.034 115.266 8 3 -6 13 839.337 111.751 33 3 6 14 243.520 59.3708 8 3 -6 14 143.469 51.4463 33 3 6 15 1237.91 108.941 8 3 -6 15 1148.03 104.321 33 3 -6 16 5750.66 219.172 24 3 -6 16 5794.05 210.845 33 3 6 16 5917.61 220.381 8 -3 7 16 2373.18 132.367 18 -3 -7 16 2328.67 139.769 22 -3 -7 15 2317.28 162.211 16 -3 7 15 2276.58 151.412 17 -3 7 15 2295.38 150.380 18 -3 -7 15 2199.33 155.266 22 -3 -7 14 57.3898 41.4621 22 -3 7 14 30.8816 34.2063 17 -3 -7 14 11.8346 31.3723 16 3 -7 -13 2018.16 157.994 29 -3 -7 13 2046.19 173.617 18 -3 -7 13 2061.32 178.529 16 -3 7 13 2178.19 172.941 17 -3 -7 13 1886.89 169.859 22 -3 7 12 635.484 101.485 17 -3 -7 12 433.044 86.0508 22 -3 -7 12 430.700 87.9741 18 3 7 -12 555.179 89.1331 56 3 -7 -12 571.829 94.0782 29 -3 -7 12 413.224 95.1191 16 3 7 -11 2466.42 185.248 56 -3 -7 11 2141.14 194.668 18 -3 -7 11 2145.36 194.421 16 -3 7 11 2535.65 195.737 17 3 -7 -11 1991.36 172.892 29 -3 -7 11 2136.05 193.985 22 3 -7 -10 73.6911 51.1472 51 3 7 -10 25.3415 38.0817 56 -3 -7 10 46.0928 48.6742 22 3 -7 -10 16.2409 39.8545 21 -3 -7 10-15.8585 44.9361 18 3 -7 -10 13.3029 37.6950 29 -3 -7 10 15.5897 41.3218 16 3 -7 -9 6750.38 363.817 21 -3 -7 9 6509.23 356.551 18 -3 -7 9 6829.28 356.604 16 3 7 -9 7320.40 338.982 56 3 -7 -9 7330.36 346.475 29 3 -7 -9 7234.83 362.241 51 -3 -7 8 6052.05 337.547 13 3 -7 -8 6687.08 358.432 21 -3 -7 8 7314.29 368.147 18 3 -7 -8 7023.01 355.779 51 3 -7 -8 6522.03 326.054 29 -3 7 8 7412.56 334.791 3 -3 -7 7 9140.49 409.903 13 -3 -7 7 8558.38 377.537 15 -3 -7 7 8840.97 411.051 18 3 -7 -7 8038.97 396.612 21 3 -7 -7 7636.02 376.259 51 3 -7 -7 8793.48 380.393 29 -3 7 7 9425.67 375.916 3 -3 -7 6 15534.9 568.266 13 -3 -7 6 15830.2 552.449 15 3 -7 -6 15578.5 579.271 21 -3 -7 6 16316.1 581.426 18 3 -7 -6 17099.4 581.464 51 3 -7 -6 16503.6 551.930 29 -3 7 6 16583.8 528.713 3 3 -7 -5 9388.47 400.581 51 3 -7 -5 9192.30 409.410 21 -3 -7 5 9443.59 408.487 18 3 -7 -5 9495.87 388.417 29 -3 -7 5 9385.81 405.541 13 -3 -7 5 8993.09 387.610 15 -3 -7 4 4678.50 271.517 13 -3 -7 4 4830.15 266.835 15 3 -7 -4 4570.25 264.546 51 3 -7 -4 4935.25 286.515 21 -3 -7 4 4424.40 266.006 18 -3 -7 4 5415.70 272.032 36 3 -7 -4 4930.82 260.615 35 3 -7 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248.973 41 4 -8 2 4317.46 281.906 44 4 -8 2 3471.15 247.620 30 4 -8 2 3326.83 237.951 31 4 -8 2 3971.95 271.227 32 4 -8 2 3794.87 237.788 28 -4 -8 -3 7048.63 335.352 9 4 8 3 7092.28 345.181 57 4 -8 3 6676.33 355.337 46 4 -8 3 6694.17 344.865 45 4 -8 3 6722.65 345.196 48 -4 -8 -3 6148.10 332.276 21 4 -8 3 6780.22 361.953 44 4 -8 3 6641.83 359.944 32 4 -8 3 6429.44 336.127 30 4 -8 3 6647.38 340.824 31 4 -8 3 6820.60 329.570 28 4 -8 4 60.3054 50.1139 48 4 -8 4 62.7619 52.1535 46 -4 -8 -4 136.016 58.6556 21 4 -8 4 208.824 70.1596 44 4 -8 4 80.7522 53.6812 32 4 -8 4 25.9118 43.0722 28 4 -8 5 1310.40 155.573 46 4 -8 5 1659.05 170.758 48 -4 -8 -5 1282.74 153.948 21 4 -8 5 1266.94 152.567 44 4 -8 5 1445.63 163.830 32 4 -8 5 1597.35 155.612 28 4 -8 6 2542.73 213.850 48 4 -8 6 3170.00 241.887 46 -4 -8 -6 2493.07 212.960 21 4 8 6 3235.13 206.669 20 4 -8 6 2439.34 208.850 44 4 -8 6 2974.28 230.036 32 4 -8 6 2949.11 214.535 33 4 -8 6 2806.30 204.907 28 4 -8 7 5256.60 310.274 48 4 -8 7 4666.55 289.027 46 4 -8 7 5043.27 299.100 32 4 -8 7 5411.73 293.066 33 4 -8 7 5256.69 281.604 28 -4 -8 -7 4981.76 300.543 21 4 8 7 5113.91 264.507 20 4 -8 8 1057.30 133.808 48 4 -8 8 881.254 122.980 46 4 -8 8 887.363 121.890 32 4 -8 8 1075.53 130.213 33 4 -8 8 956.399 122.305 28 -4 -8 -8 999.881 133.255 21 4 -8 9 317.337 77.2486 48 4 -8 9 451.562 86.9612 46 4 -8 9 367.129 78.4653 33 4 -8 9 276.807 69.6485 28 -4 -8 -9 462.917 90.2315 21 -4 -8 -10 331.426 74.7165 21 4 -8 10 337.937 70.3145 33 4 -8 10 390.954 77.6530 48 4 -8 10 290.575 65.5743 46 -4 -8 -11 1243.48 126.128 21 4 8 11 1255.35 116.702 8 4 -8 11 1163.63 119.620 33 4 -8 11 1060.11 113.962 48 -4 -8 -12 17.7568 28.1270 21 4 -8 12-25.8201 29.8687 33 4 8 12-7.67822 23.0769 8 4 -8 13 160.096 38.4744 33 4 8 13 188.893 41.1890 32 4 8 13 94.4772 31.9588 8 4 9 -13 5.92122 17.7955 56 -4 9 13 6.55879 24.5847 17 4 -9 -13-8.90528 28.2114 50 4 9 -12 2275.92 143.531 56 -4 9 12 2253.76 146.905 17 4 -9 -12 2359.69 176.250 50 4 9 -11 623.898 83.7227 56 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325.908 28 4 -9 7 342.777 83.6291 48 4 -9 7 292.619 74.0910 46 -4 -9 -7 395.297 88.9988 55 -4 -9 -7 433.629 89.4490 21 4 -9 7 288.866 71.8368 32 4 -9 7 349.857 73.2162 33 4 -9 7 199.800 62.5698 28 -4 -9 -8 54.7679 43.3902 21 4 -9 8 142.791 55.0298 28 4 -9 8 71.4155 37.7237 33 4 -9 8 63.5987 40.3114 46 4 -9 8 26.7225 32.8064 48 4 -9 9 109.806 42.6407 33 -4 -9 -9 87.8977 45.3902 21 4 -9 9 89.1610 43.2787 46 4 -9 9 96.1238 43.4364 48 4 -9 10 1843.61 145.491 33 -4 -9 -10 2236.68 168.001 21 4 -9 10 2113.57 158.321 48 4 -9 10 1966.72 148.396 46 4 -9 11 148.108 43.7227 33 -4 -9 -11 184.144 49.7632 21 4 -9 11 163.365 44.9216 48 4 -9 12 619.980 68.6615 33 -4 -9 -12 725.457 77.5367 21 4 10 -12 407.784 53.0391 56 4 -10 -12 427.879 66.3786 50 -4 10 12 398.152 54.6061 17 4 10 -11 1164.77 100.230 56 4 -10 -11 1116.23 118.415 50 -4 10 11 1392.97 109.989 17 4 10 -10 143.734 42.3822 56 4 -10 -10 36.4245 36.5266 50 -4 10 10 102.312 40.0957 17 4 10 -9 1308.17 120.532 56 4 -10 -9 937.732 124.299 50 4 10 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1173.00 119.855 14 4 -10 6 54.3411 44.8932 28 -4 -10 -6 39.5323 37.3406 21 4 -10 6 13.0553 32.0388 46 4 -10 6 77.5307 44.8446 48 4 -10 6 12.9038 36.5652 32 4 -10 6 33.7169 31.8484 33 4 10 6-9.96734 29.9586 14 4 -10 7 2527.53 171.328 28 4 -10 7 2362.59 181.055 48 4 -10 7 2223.66 175.882 46 -4 -10 -7 2412.93 186.123 21 4 -10 7 1783.78 150.801 33 4 10 7 2155.84 152.675 14 4 -10 8 2220.87 155.206 28 4 -10 8 2290.89 170.265 48 4 -10 8 2507.79 174.597 46 -4 -10 -8 2392.71 179.997 21 4 10 8 2597.29 174.626 43 4 -10 8 2687.70 174.011 33 4 10 8 2563.16 158.287 14 -4 -10 -9 506.390 80.8852 21 4 -10 9 506.675 72.4065 33 -4 -10 -10 140.014 41.1588 21 4 -10 10 117.170 35.9061 48 4 -10 10 58.9922 31.3938 33 -4 -10 -11 2037.08 128.142 21 -4 11 10 151.054 36.4097 17 4 11 -10 128.734 34.8357 56 4 -11 -10 203.213 50.1365 50 4 -11 -10 113.025 32.7429 28 -4 11 9 229.635 49.4343 17 4 11 -9 218.543 46.8864 56 4 -11 -9 187.365 42.8819 28 4 -11 -9 197.994 55.3735 50 4 11 -8 1167.67 105.796 56 4 -11 -8 1212.86 109.087 28 4 -11 -8 855.132 112.515 50 4 11 -7 1949.49 141.735 56 -4 -11 7 1575.01 137.348 15 4 -11 -7 1618.60 131.528 28 -4 -11 7 1817.25 148.014 48 4 -11 -7 1535.90 154.754 50 4 11 -6 11722.8 407.370 56 -4 -11 6 11662.6 431.438 15 4 -11 -6 12498.5 424.901 28 4 -11 -6 12104.9 470.680 50 4 11 -5 408.705 71.4283 56 4 -11 -5 478.576 82.2332 28 -4 -11 5 559.734 93.1863 15 4 -11 -5 343.286 79.4340 50 -4 -11 4 10397.0 417.705 15 4 -11 -4 9546.22 384.935 30 4 -11 -4 10052.1 390.523 28 4 11 -4 10703.3 399.236 57 -4 -11 3 5582.54 298.549 15 4 -11 -3 5489.18 287.933 30 4 -11 -3 6192.93 292.553 28 4 11 -3 6146.99 298.622 57 -4 -11 2 26.5354 32.5672 15 4 -11 -2 114.166 47.5550 30 4 -11 -2 46.2122 38.3942 28 4 11 -2 24.8450 32.9356 57 -4 -11 1-13.1534 37.2701 15 4 -11 -1 25.9780 41.1485 30 4 -11 -1-23.1953 32.8620 28 4 11 -1 12.7640 36.1669 57 -4 -11 0 12.7649 31.3238 15 4 -11 0-13.0669 29.2712 30 4 -11 0 11.5309 36.5294 28 4 11 0-25.6608 36.3551 57 4 -11 1 477.391 88.2317 30 4 -11 1 556.508 88.6941 28 4 11 1 592.316 95.8379 57 4 11 2 1145.72 119.185 14 4 -11 2 1394.61 142.412 30 4 -11 2 1055.12 129.439 31 4 -11 2 1273.45 128.997 28 4 11 2 1346.41 137.219 57 4 11 3 7728.59 318.614 14 4 11 3 7817.11 335.085 57 4 -11 3 7128.87 329.144 30 4 -11 3 7454.61 346.050 31 4 -11 3 8143.97 333.808 28 4 -11 4 4841.06 252.033 48 4 -11 4 4704.30 260.323 31 4 11 4 4686.40 235.507 14 4 -11 4 4696.64 241.398 28 4 -11 5 3066.53 196.895 48 4 -11 5 2886.88 181.351 28 4 -11 5 3044.56 198.105 31 4 11 5 3049.64 180.178 14 -4 -11 -6 1156.93 120.465 21 4 -11 6 1570.08 128.223 28 4 11 6 1383.16 115.501 14 4 -11 6 1362.41 127.361 48 -4 -11 -7 117.718 42.9327 21 4 -11 7 155.261 44.0868 28 4 -11 7 168.999 48.9575 48 4 11 7 182.123 43.2706 14 4 -11 8 1454.24 118.157 48 -4 -11 -8 1369.70 119.257 21 4 -11 9 761.344 77.6417 48 -4 -11 -9 951.180 90.3736 21 4 12 -8 2858.84 141.777 56 4 -12 -8 2871.50 142.563 28 4 12 -7 2509.09 138.950 56 -4 -12 7 2174.11 137.992 15 4 -12 -7 2655.03 145.269 28 -4 -12 7 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396.842 57 5 0 -2 48.7914 35.2520 41 5 0 -2 61.2754 35.4457 57 5 0 -2 56.5680 29.9924 10 5 0 -2-10.5526 25.9016 26 5 0 -1 1454.36 130.146 57 5 0 -1 1406.02 130.771 26 5 0 -1 1507.84 128.843 41 5 0 0 92.5743 37.1623 57 5 0 0 21.3141 28.2582 26 5 0 0 20.1799 26.7559 27 5 0 0 68.8643 29.5775 41 5 0 1 4164.89 227.553 57 5 0 1 3743.44 217.983 27 5 0 1 4012.66 226.408 26 5 0 1 4095.83 220.499 41 5 0 2-10.3683 31.1625 57 5 0 2 22.1059 31.3202 26 5 0 2 32.7763 34.6127 27 5 0 2 39.9186 29.9943 41 5 0 2 34.0572 39.3976 43 5 0 3 48295.5 1177.56 27 5 0 3 47695.4 1141.85 41 5 0 3 49336.1 1194.49 43 5 0 4 23.6267 33.4732 44 5 0 4 13.0509 41.3446 43 5 0 4 35.8233 33.8351 27 5 0 4-22.7363 39.4510 32 5 0 5 48677.3 1204.07 32 5 0 5 48588.3 1240.47 43 5 0 6 26.5273 35.1570 32 5 0 6 14.6792 41.5949 43 5 0 7 12276.6 488.885 32 5 0 7 13476.8 520.803 43 5 0 8 14.8082 46.9123 32 5 0 9 19758.3 672.789 32 5 0 9 20501.8 689.998 43 5 0 10 15.0830 37.0129 32 5 0 11 259.485 76.5687 32 5 0 12-13.1230 34.7831 32 5 0 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8 392.655 77.0119 3 5 1 -8 342.921 70.7481 56 5 -1 -8 362.279 74.2929 56 5 1 -8 336.993 81.4320 10 5 -1 -8 245.767 72.4371 10 -5 -1 8 326.460 75.4000 15 -5 -1 7 7284.03 337.969 3 -5 1 7 7418.12 329.495 3 5 -1 -7 7862.15 339.876 56 5 1 -7 7867.75 337.132 56 5 1 -7 6921.81 354.494 10 5 -1 -7 6402.65 340.972 10 -5 -1 6 14587.1 507.776 3 -5 1 6 16208.4 514.339 3 5 -1 -6 15446.9 514.401 56 5 1 -6 16037.2 518.202 56 5 1 -6 13994.7 529.707 10 5 -1 -6 14941.4 542.260 10 -5 -1 5 1567.42 143.050 3 5 -1 -5 1673.05 156.187 10 5 1 -5 1741.36 159.703 10 5 -1 -5 1498.30 135.500 56 5 1 -5 1810.47 146.306 56 5 1 -4 7324.02 311.960 57 5 -1 -4 6820.40 302.321 57 5 1 -4 6868.45 326.213 10 5 -1 -4 7036.27 328.624 10 5 -1 -4 7129.99 322.035 26 5 1 -4 7592.03 307.491 41 5 -1 -3 6276.65 289.411 57 5 1 -3 6345.30 291.986 57 5 1 -3 6587.25 312.250 10 5 -1 -3 6685.70 308.214 10 5 -1 -3 6893.94 310.425 26 5 1 -3 6498.45 285.292 41 5 -1 -3 7203.00 300.340 41 5 -1 -2 13938.3 472.501 57 5 1 -2 14366.4 478.937 57 5 1 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27 5 -1 2 5521.97 276.426 26 5 1 2 5727.55 286.135 6 5 1 3 1499.70 131.339 41 5 1 3 1430.87 142.516 43 5 -1 3 1404.20 147.374 43 5 -1 3 1625.88 148.231 44 5 -1 3 1484.46 142.723 27 5 -1 3 1658.82 145.833 26 5 1 3 1601.19 151.037 6 5 -1 4 5053.11 268.277 44 5 1 4 4562.67 267.503 43 5 -1 4 4888.58 275.559 43 5 -1 4 4570.21 254.837 32 5 -1 4 4745.06 260.760 27 5 -1 5 845.484 111.683 44 5 1 5 876.300 123.364 43 5 -1 5 848.022 121.252 43 5 1 5 894.014 106.108 20 5 -1 5 832.970 112.145 32 5 1 5 939.927 119.059 32 5 -1 5 959.034 117.525 27 5 1 6 2230.06 192.586 43 5 -1 6 1862.29 180.641 43 5 1 6 2132.14 166.984 20 5 -1 6 2202.14 185.024 32 5 1 6 1884.70 170.262 32 5 1 7 809.039 122.036 43 5 -1 7 791.423 121.081 43 5 1 7 527.853 89.2170 20 5 -1 7 715.705 111.794 32 5 1 7 703.345 110.788 32 5 1 8 47261.1 1233.70 43 5 -1 8 46566.8 1234.88 43 5 -1 8 45843.3 1211.52 32 5 1 8 47853.0 1222.21 32 5 1 9 1291.96 157.214 43 5 -1 9 973.881 135.253 32 5 1 9 1030.34 136.389 32 5 1 10 3640.72 252.997 43 5 -1 10 4062.74 264.953 32 5 1 10 3767.14 256.570 32 5 -1 11 700.685 110.817 32 5 1 11 720.416 115.318 32 5 -1 12 1137.91 132.062 32 5 1 12 1049.72 127.362 32 5 -1 12 806.000 109.076 33 5 -1 13 186.691 53.9907 32 5 1 13 191.261 52.9614 32 5 -1 13 142.378 51.5615 33 5 1 14 115.671 40.9319 32 5 -1 14 154.254 45.5257 33 5 1 14 163.297 47.2970 33 5 -1 15 171.863 39.6750 33 5 1 15 151.070 40.8073 33 -5 -2 17 982.325 83.9074 18 -5 2 17 1162.95 90.3889 18 -5 2 16 296.737 56.8740 18 -5 -2 16 294.486 56.8071 18 -5 2 15 305.134 67.7901 18 -5 -2 15 264.414 60.1644 18 5 2 -14-10.1715 28.8210 56 -5 -2 14-12.3556 35.0096 18 -5 2 14 11.7588 39.0694 18 5 2 -13 1759.92 153.281 56 5 -2 -13 1973.93 161.908 56 -5 -2 13 1544.06 157.313 18 -5 2 13 2073.60 174.939 18 5 2 -12 12.5625 33.2985 56 5 -2 -12 25.6462 31.4681 56 -5 -2 12 14.4347 40.9019 18 -5 2 12 27.0035 35.7878 18 5 2 -11 221.481 63.9926 56 5 -2 -11 160.537 55.3194 56 -5 -2 11 44.0672 48.8748 18 -5 2 11 204.849 67.0739 18 5 2 -10 261.293 68.0802 56 5 -2 -10 202.323 64.8793 56 -5 -2 10 131.231 62.0535 18 -5 2 10 120.618 53.7964 18 5 -2 -9 9799.64 408.960 56 5 2 -9 9721.13 400.274 56 -5 -2 9 9851.16 419.020 18 -5 2 9 9876.23 401.978 18 5 2 -9 7795.78 396.024 10 -5 -2 9 9191.03 402.544 15 -5 -2 9 8883.54 393.806 5 -5 2 9 8581.18 381.886 3 5 -2 -8 23.6222 28.9864 52 -5 2 8 60.7863 38.5161 3 5 2 -8 12.3214 27.6045 56 5 -2 -8 90.3333 48.3737 56 5 2 -8 15.0748 33.7716 10 -5 -2 8-13.4091 35.5434 15 -5 2 7 19063.4 596.808 3 5 2 -7 17869.5 630.155 10 5 -2 -7 18351.4 637.328 10 -5 -2 7 19466.1 632.267 15 5 2 -7 19547.4 605.807 56 5 -2 -6 2123.08 181.023 10 -5 -2 6 1988.66 174.896 15 5 2 -6 2135.69 182.488 10 5 -2 -6 2309.39 175.301 56 5 2 -6 1941.22 158.356 56 5 -2 -6 2165.67 182.543 40 5 -2 -5 32407.7 904.339 10 -5 -2 5 34948.4 916.247 15 5 2 -5 31339.7 900.028 10 5 -2 -5 34279.4 887.326 56 5 2 -5 33348.9 863.943 56 5 -2 -5 34891.3 923.434 40 5 -2 -4 5111.67 256.020 56 5 -2 -4 5123.85 259.864 57 5 2 -4 5415.12 263.127 57 -5 -2 4 4996.86 270.439 15 5 2 -4 4923.76 274.291 10 5 -2 -4 4843.35 264.348 10 5 -2 -4 4784.65 264.830 26 5 2 -4 5544.83 259.560 41 5 -2 -4 5423.20 281.004 40 5 2 -3 63.0672 34.9308 57 5 -2 -3 10.8291 24.2676 57 5 2 -3 36.7147 27.4230 10 5 -2 -3 33.6034 29.6963 10 -5 -2 3 34.5641 39.9885 15 5 -2 -3 35.6946 33.7203 26 5 2 -3 91.4564 43.1956 41 5 -2 -2 736.870 95.7856 57 5 2 -2 855.901 102.604 57 -5 -2 2 662.350 94.9954 15 5 -2 -2 1027.85 117.358 26 5 -2 -2 839.398 104.082 27 5 2 -2 765.402 95.4094 41 5 2 -1 382.388 70.0951 57 5 -2 -1 347.014 67.2990 57 5 -2 -1 322.261 68.5372 26 5 -2 -1 353.403 69.4134 27 5 -2 -1 474.214 78.4052 44 5 2 -1 318.159 62.8948 41 5 2 0 566.034 84.4827 6 5 -2 0 543.259 84.0436 44 5 2 0 713.113 92.1010 41 5 2 0 427.653 74.2495 57 5 -2 0 683.820 92.9222 57 5 -2 0 740.360 99.4307 26 5 -2 0 627.788 93.2629 27 5 -2 1 2133.86 170.051 44 5 2 1 2244.48 173.508 6 5 2 1 2217.49 161.555 41 5 2 1 1913.32 155.684 57 5 -2 1 2117.33 162.344 57 5 -2 1 2361.50 174.620 27 5 -2 1 2347.87 173.294 26 5 -2 2 1844.33 155.437 44 5 2 2 1558.77 145.805 6 5 2 2 1067.48 114.538 41 5 2 2 1346.36 135.804 43 5 2 2 1555.65 139.000 57 5 -2 2 1625.45 140.255 57 5 -2 2 1281.22 131.043 27 5 -2 2 1442.88 137.236 26 5 2 3 14657.7 514.335 6 5 -2 3 13589.8 482.885 27 5 -2 3 13594.7 474.882 26 5 -2 3 13381.5 488.367 44 5 2 3 13228.1 454.915 41 5 2 3 13524.0 492.989 43 5 -2 3 13210.4 493.831 43 5 -2 3 14373.5 485.450 32 5 2 3 13282.0 442.183 11 5 2 4 1733.60 164.099 6 5 -2 4 1995.08 166.877 27 5 -2 4 1781.10 159.894 44 5 2 4 1571.87 138.017 20 5 2 4 1628.74 157.810 43 5 -2 4 1623.52 159.507 43 5 -2 4 1546.72 148.686 32 5 2 4 1500.07 131.961 11 5 2 5 2912.36 218.400 6 5 -2 5 2996.16 209.661 27 5 -2 5 2899.25 207.041 44 5 2 5 2827.56 192.303 20 5 2 5 3196.46 226.917 43 5 -2 5 2899.72 219.249 43 5 -2 5 2989.69 212.226 32 5 2 5 3402.50 202.416 11 5 -2 6 2522.69 192.051 27 5 2 6 2210.85 171.902 20 5 2 6 2429.06 178.141 11 5 2 6 2657.28 208.881 43 5 -2 6 2171.84 187.849 32 5 2 6 2135.39 182.360 32 5 2 6 2148.44 191.420 6 5 2 7 8056.75 387.930 43 5 2 7 8165.03 355.879 20 5 -2 7 7912.78 375.961 32 5 2 7 7280.14 361.907 32 5 2 7 7381.79 334.743 11 5 -2 8-15.1179 47.8928 32 5 2 8 29.5975 49.1701 32 5 2 8-12.7181 33.7093 20 5 2 8-15.6214 54.2112 43 5 -2 9 20002.3 680.275 32 5 2 9 22198.1 704.017 32 5 -2 9 21429.6 670.841 33 5 2 9 19523.5 679.250 43 5 -2 9 19329.3 674.576 42 5 2 10 1257.55 147.433 32 5 -2 10 971.161 131.037 32 5 -2 10 1165.17 133.676 33 5 2 10 944.568 128.628 43 5 -2 10 908.685 128.940 42 5 -2 11 3088.94 224.290 32 5 2 11 3406.55 236.239 32 5 -2 11 3080.11 216.934 33 5 -2 11 3464.41 231.978 42 5 -2 12 12.5351 28.0797 32 5 2 12-12.9154 31.6929 32 5 -2 12-12.1159 34.3306 33 5 -2 13 2983.83 192.441 32 5 2 13 3371.33 208.711 32 5 -2 13 3248.54 201.447 33 5 2 14 138.670 42.5983 32 5 -2 14 113.193 40.9793 33 5 -2 15 292.498 49.0071 33 5 2 15 272.172 47.9902 33 -5 3 16 167.424 45.8656 18 -5 -3 16 195.439 46.4535 18 -5 3 15 306.160 63.1568 18 -5 -3 15 372.841 70.9362 18 -5 -3 14 9160.35 380.996 18 -5 3 14 9753.54 380.640 18 5 3 -14 9093.50 350.808 56 -5 -3 13 81.0538 52.4165 18 -5 3 13 37.3097 41.3249 18 5 3 -13 11.2712 27.6636 56 -5 -3 12 3623.96 247.880 18 -5 3 12 4249.91 254.740 18 5 -3 -12 3645.70 232.369 56 5 3 -12 3717.51 231.534 56 -5 -3 11 478.969 95.4151 18 -5 3 11 539.235 94.1544 18 5 3 -11 543.544 93.1815 56 5 -3 -11 766.492 111.584 56 -5 -3 10 601.933 108.068 18 -5 3 10 373.559 81.8384 18 5 3 -10 563.406 96.9116 56 5 -3 -10 565.243 97.1328 56 -5 -3 9 14487.6 553.380 18 5 -3 -9 15638.2 528.100 52 -5 -3 9 15253.3 548.424 15 5 -3 -9 15798.7 556.977 56 5 3 -9 15391.2 537.134 56 5 -3 -8 602.562 98.2895 56 5 3 -8 676.630 102.584 56 5 -3 -8 542.854 90.6658 52 -5 -3 8 581.451 103.052 18 -5 -3 8 442.826 88.3815 15 -5 -3 8 602.172 94.9729 5 -5 3 8 852.948 107.546 3 5 -3 -7 2789.22 200.259 52 -5 -3 7 2618.17 193.930 5 5 -3 -7 3237.23 234.723 40 -5 -3 7 3004.65 218.390 15 5 -3 -7 2673.01 199.711 56 5 3 -7 2795.65 197.059 56 5 -3 -6 1436.16 154.522 40 5 -3 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178.624 6 5 3 0 1771.31 151.278 57 5 -3 0 2405.75 176.644 57 5 -3 0 1977.85 165.907 27 5 -3 0 2165.31 172.734 26 5 3 0 2061.31 161.001 41 5 -3 0 2161.84 180.098 40 5 3 1 757.301 105.388 6 5 3 1 611.953 88.2855 41 5 -3 1 544.865 92.6749 44 5 3 1 609.474 90.4349 57 5 -3 1 605.182 90.0346 57 5 -3 1 587.016 90.2634 26 5 -3 1 544.030 88.8734 27 5 -3 2 851.660 105.128 57 5 3 2 1008.89 116.593 57 5 -3 2 1068.82 124.837 44 5 -3 2 965.331 114.485 48 5 -3 2 868.359 112.342 27 5 -3 2 1000.37 116.699 26 5 3 2 966.640 109.804 41 5 3 2 1093.91 123.777 43 5 3 2 960.603 105.881 11 5 3 2 813.980 111.986 6 5 3 3 4287.51 262.787 6 5 -3 3 4408.54 254.845 27 5 -3 3 4426.64 248.234 26 5 -3 3 4705.50 266.530 44 5 -3 3 4976.90 272.581 48 5 3 3 4524.68 264.765 43 5 -3 3 4479.61 256.369 32 5 3 3 4006.52 224.923 11 5 3 4 4621.41 277.273 6 5 -3 4 4874.75 268.077 27 5 -3 4 4581.88 270.803 48 5 3 4 4126.83 234.070 20 5 -3 4 4636.53 269.098 44 5 3 4 4335.26 264.997 43 5 -3 4 4466.74 262.402 32 5 3 4 4836.88 249.630 11 5 3 5 1668.03 168.055 6 5 -3 5 1562.51 150.903 27 5 -3 5 1705.85 166.840 48 5 3 5 1445.42 139.275 20 5 -3 5 1579.25 155.231 44 5 3 5 1835.12 172.183 43 5 -3 5 1853.07 174.535 42 5 -3 5 1569.24 158.898 32 5 3 5 1596.94 143.905 11 5 3 6 2232.18 198.702 6 5 -3 6 2200.52 180.866 27 5 -3 6 2663.32 209.081 48 5 3 6 2594.59 212.060 43 5 -3 6 2240.49 199.032 42 -5 -3 -6 2744.10 211.269 21 5 3 6 2022.72 168.306 20 5 -3 6 2935.50 217.058 32 5 3 6 2471.45 182.722 11 5 -3 7 10962.7 462.911 32 -5 -3 -7 10809.2 449.541 21 5 3 7 10982.8 429.470 20 5 -3 7 10852.6 438.546 37 5 3 7 11118.8 472.188 43 5 -3 7 10888.6 474.061 42 5 -3 8 19648.3 673.591 32 5 3 8 21019.3 647.775 20 5 3 8 19618.1 677.082 43 5 -3 8 19700.8 682.514 42 5 -3 9 8596.64 404.637 32 5 3 9 8892.59 409.218 32 5 -3 9 8554.68 382.608 33 5 3 9 9170.43 388.639 20 5 3 9 8411.80 399.967 43 5 -3 9 8322.40 401.252 42 5 -3 10 132.405 55.2385 32 5 3 10 177.105 66.1997 32 5 -3 10 199.849 61.2489 33 5 3 10 230.982 66.3523 43 5 -3 10 147.688 61.0871 42 5 -3 11-27.1928 40.8625 32 5 3 11 55.6027 44.0366 32 5 -3 11 12.7354 33.7551 33 5 -3 11-13.2842 29.7577 42 5 -3 12 273.756 64.3794 32 5 3 12 187.058 58.7808 32 5 -3 12 313.833 69.0452 33 5 3 13 31.5519 31.6151 32 5 -3 13 40.1727 37.6510 33 5 3 14 391.296 63.8153 32 5 -3 14 534.263 71.1951 33 5 -3 15 40.9922 22.7352 33 5 3 15 46.6424 24.7933 33 -5 4 16-6.75718 22.4515 18 -5 -4 16 20.7574 22.9896 18 -5 -4 15 2662.05 172.742 18 -5 4 15 2989.32 175.284 18 5 4 -14 346.171 62.2604 56 -5 4 14 439.097 76.5437 18 -5 -4 14 317.487 73.9222 18 5 4 -13 32.3199 35.7965 56 -5 4 13 11.8204 33.4947 18 -5 -4 13 13.0392 36.9480 18 5 4 -12 370.781 73.0835 56 5 -4 -12 247.342 63.4028 56 -5 4 12 305.912 71.3000 18 -5 -4 12 257.169 71.7666 18 5 -4 -11 5169.43 286.817 56 5 4 -11 5524.62 289.060 56 -5 -4 11 5148.36 304.683 18 5 -4 -10 20392.1 661.111 56 5 4 -10 20460.6 645.168 56 -5 -4 10 19709.8 675.064 18 5 -4 -9 24785.8 721.352 52 -5 -4 9 23043.8 728.245 15 5 -4 -9 23433.1 731.419 56 5 4 -9 23780.4 716.889 56 -5 -4 9 23191.8 750.518 18 5 -4 -8 2868.91 205.610 52 -5 -4 8 2517.68 208.709 18 -5 -4 8 2932.99 220.351 15 5 -4 -8 2629.63 205.921 56 5 4 -8 2785.40 202.214 56 5 -4 -7 677.485 103.588 52 -5 -4 7 865.872 112.083 5 5 -4 -7 822.634 125.065 40 -5 -4 7 756.284 115.386 15 5 -4 -7 976.395 122.476 56 5 4 -7 932.946 118.311 56 5 -4 -6 45089.7 1185.40 40 5 -4 -6 44888.9 1120.76 52 -5 -4 6 43430.9 1144.56 15 5 -4 -6 43737.8 1127.61 56 5 4 -6 44081.6 1100.45 56 5 -4 -5 10563.7 454.189 40 5 -4 -5 11027.7 421.492 52 -5 -4 5 10586.1 439.984 15 5 -4 -5 10256.0 413.199 56 5 4 -5 9752.22 387.916 56 5 4 -4 6822.85 309.973 41 5 -4 -4 6733.66 347.849 40 5 -4 -4 7385.65 329.026 52 -5 -4 4 7029.86 341.093 15 5 -4 -4 6257.08 308.763 56 5 4 -4 6816.30 315.265 57 5 -4 -4 7021.00 323.672 57 5 4 -3 34.2866 30.3118 41 5 -4 -3 44.9260 42.4466 40 5 -4 -3 68.1085 34.1328 52 -5 -4 3 181.990 58.2488 15 5 4 -3 58.2979 35.0585 57 5 -4 -3 48.8351 34.6107 57 5 4 -2 16430.8 556.057 57 5 -4 -2 17059.2 564.090 57 5 4 -2 17508.5 558.421 41 5 -4 -2 16833.9 605.270 40 5 -4 -2 18420.5 559.414 52 -5 -4 2 18268.1 587.548 15 5 -4 -2 17216.3 580.831 26 5 -4 -1 4795.90 266.060 57 5 4 -1 4873.74 262.015 57 5 -4 -1 4641.34 266.800 26 5 -4 -1 4733.50 270.433 27 5 4 -1 4724.69 255.793 41 5 -4 -1 4582.60 262.645 44 5 -4 -1 4486.71 279.514 40 5 4 0 453.988 84.2226 6 5 4 0 334.448 73.2720 57 5 -4 0 500.366 85.9949 57 5 -4 0 460.165 84.0020 26 5 -4 0 540.339 93.3194 27 5 4 0 549.838 88.1053 41 5 -4 0 455.383 84.8906 44 5 -4 0 410.880 86.1312 40 5 4 1 7937.38 361.400 6 5 4 1 7796.41 340.651 41 5 -4 1 7227.67 349.026 44 5 -4 1 6402.45 346.067 40 5 4 1 7798.37 342.019 57 5 -4 1 7356.78 338.483 57 5 -4 1 7489.46 348.183 27 5 -4 1 7643.27 340.061 26 5 4 2 791.144 100.327 11 5 -4 2 949.582 116.453 57 5 4 2 589.299 92.9540 57 5 -4 2 825.128 109.278 48 5 -4 2 915.356 119.304 27 5 4 2 809.307 106.793 41 5 -4 2 844.757 115.165 44 5 -4 2 818.597 109.545 32 5 4 2 824.504 117.238 6 5 4 3 6205.85 330.336 6 5 -4 3 6409.62 322.268 48 5 -4 3 5998.39 308.676 27 5 -4 3 6666.99 333.088 44 5 -4 3 6414.97 328.861 42 5 -4 3 5664.68 303.442 32 5 4 3 5496.65 279.188 11 5 4 4 2128.18 190.314 6 5 -4 4 1963.14 171.434 27 5 -4 4 1921.64 176.103 48 5 -4 4 2248.71 190.064 44 5 4 4 1872.42 177.956 43 5 -4 4 2266.51 196.042 42 5 -4 4 2209.64 188.535 32 5 4 4 1903.29 158.391 11 5 4 5 5070.37 301.907 6 5 -4 5 4976.76 276.375 27 5 -4 5 4625.10 283.562 48 -5 -4 -5 4939.75 294.700 21 5 4 5 4938.11 265.728 20 5 -4 5 4713.02 279.840 44 5 4 5 4642.24 287.262 43 5 -4 5 5445.39 311.504 42 5 -4 5 5471.67 303.127 32 5 4 5 4384.00 252.740 11 5 -4 6 1953.75 178.468 44 5 4 6 2008.92 188.242 43 5 -4 6 2075.90 193.503 42 -5 -4 -6 1904.73 179.687 21 5 4 6 2188.15 175.598 20 5 -4 6 1941.24 183.391 32 5 -4 6 1883.01 181.204 48 5 4 7 2604.92 218.292 43 5 -4 7 2513.25 214.920 42 -5 -4 -7 2318.32 200.622 21 5 4 7 2303.52 184.794 20 5 -4 7 2633.33 217.045 32 5 -4 7 2694.86 219.331 48 5 4 8 2988.36 231.892 43 5 -4 8 2882.31 231.619 42 -5 -4 -8 2557.84 208.842 21 5 4 8 3259.74 220.127 20 5 -4 8 3357.55 243.200 32 5 -4 8 3360.75 243.344 48 5 -4 9 1618.24 168.225 32 5 -4 9 1334.63 144.590 33 5 4 9 1455.61 146.064 20 5 4 9 1596.30 164.789 43 5 -4 9 1475.78 162.559 42 5 -4 10 4225.05 268.709 32 5 4 10 4904.40 284.720 32 5 -4 10 4783.07 271.044 33 5 4 10 4414.08 268.671 43 5 -4 10 4988.39 291.168 42 5 -4 11 683.113 103.373 32 5 -4 11 850.009 109.640 33 5 4 11 745.081 108.307 32 5 -4 11 661.786 100.489 42 5 -4 12 76.8009 39.6556 32 5 4 12 70.4288 40.7604 32 5 -4 12 87.0926 42.2637 33 5 4 13 2946.85 182.476 32 5 -4 13 2717.57 171.679 33 5 4 14 66.0805 29.4521 32 5 -4 14 79.3632 31.5334 33 -5 -5 15 3312.41 183.277 18 -5 5 15 3892.02 191.085 18 5 5 -14 11038.0 376.882 56 -5 -5 14 11141.5 407.533 18 5 5 -13 588.303 84.8420 56 -5 5 13 536.356 86.3053 18 -5 -5 13 610.383 96.8835 18 5 -5 -12 13109.7 478.711 51 5 5 -12 12735.0 458.919 56 -5 -5 12 12482.8 489.716 18 5 -5 -11 150.277 51.2578 51 5 5 -11 110.535 49.2664 56 -5 -5 11 103.652 53.5319 18 5 -5 -10 2244.88 178.245 52 5 -5 -10 2336.25 191.767 56 5 5 -10 2527.01 192.035 56 -5 -5 10 2246.93 200.346 18 5 -5 -9 10624.2 424.866 52 -5 -5 9 10273.8 432.594 15 5 -5 -9 9755.08 427.193 56 5 5 -9 10647.7 425.037 56 -5 -5 9 10028.8 448.791 18 5 -5 -8 66.3850 39.9130 52 -5 -5 8 116.363 54.5290 15 5 -5 -8 14.3352 40.6293 56 5 5 -8 51.5006 40.7981 56 -5 -5 8 77.1790 55.7619 18 5 -5 -7 2249.90 184.340 52 -5 -5 7 2550.55 208.351 15 5 -5 -7 2124.82 188.665 56 5 5 -7 2715.24 195.654 56 5 -5 -6 1707.44 181.124 40 5 -5 -6 1917.65 167.785 52 -5 -5 6 1606.69 164.731 15 5 -5 -6 1491.49 154.099 56 5 5 -6 1726.39 155.649 56 5 -5 -5 11079.1 486.255 40 5 -5 -5 11941.4 451.573 52 -5 -5 5 10906.9 458.523 15 5 -5 -5 11175.2 448.584 56 5 5 -4 24419.2 710.380 41 -5 -5 4 24486.4 746.098 36 5 -5 -4 24113.0 787.213 40 5 -5 -4 25228.2 723.835 52 -5 -5 4 24804.8 756.195 15 5 -5 -4 21681.8 699.093 56 5 5 -4 24709.0 716.732 57 5 -5 -4 23913.6 719.924 57 5 5 -3 5554.97 282.641 41 -5 -5 3 5096.55 293.300 36 5 -5 -3 5037.57 311.054 40 5 -5 -3 5353.90 276.040 52 -5 -5 3 4959.16 286.877 15 5 5 -3 4968.48 272.336 57 5 -5 -3 5125.86 280.671 57 5 5 -2 7877.77 353.225 57 5 -5 -2 8370.93 368.179 57 5 5 -2 8097.63 354.803 41 5 -5 -2 7206.61 379.165 40 -5 -5 2 7526.94 366.114 36 5 -5 -2 7416.12 330.111 52 -5 -5 2 8404.80 374.257 15 5 -5 -2 7131.09 352.103 26 -5 -5 1 320.260 77.3589 36 5 5 -1 261.958 62.7185 41 5 -5 -1 259.465 69.9686 44 5 -5 -1 325.592 80.0810 40 5 5 -1 355.465 74.3563 57 5 -5 -1 222.688 61.7906 57 5 -5 -1 373.294 78.0665 26 5 5 0 6360.38 312.057 41 5 -5 0 6273.27 323.200 44 -5 -5 0 6496.46 336.263 36 5 -5 0 5157.22 318.636 40 5 5 0 6329.38 321.751 6 5 5 0 6213.85 308.861 57 5 -5 0 6040.97 307.491 57 5 -5 0 5572.50 296.688 26 5 -5 0 6163.53 319.398 27 5 -5 1 8009.40 364.774 57 5 5 1 8372.91 369.976 57 5 5 1 8768.94 394.933 6 5 5 1 8504.47 368.370 41 5 -5 1 8369.20 386.014 44 -5 -5 -1 8216.28 386.441 36 5 -5 1 7932.82 367.173 32 5 -5 1 8438.90 382.913 27 5 5 2 1578.18 149.260 11 5 5 2 1858.84 178.001 6 5 5 2 1742.43 160.385 57 5 -5 2 1849.60 163.749 57 5 -5 2 1456.94 147.874 48 5 5 2 1765.96 159.513 41 5 -5 2 1782.79 173.662 44 -5 -5 -2 1716.73 168.446 36 5 -5 2 1610.16 161.985 42 5 -5 2 1793.20 168.724 32 5 -5 2 1907.77 170.654 27 5 5 3 109.579 43.9780 11 5 5 3 15.5150 31.0857 6 5 -5 3 12.4677 33.0455 57 5 -5 3-13.7127 33.6493 48 5 -5 3-14.8394 33.2416 44 5 -5 3-14.8705 36.4906 42 5 -5 3-14.2548 31.9319 32 5 -5 3 13.3878 35.4843 27 5 5 4 208.060 71.8257 6 5 -5 4 290.015 71.2407 27 5 -5 4 274.910 76.8143 48 -5 -5 -4 276.445 75.4904 21 5 -5 4 119.102 53.9383 44 5 -5 4 201.988 66.1714 42 5 -5 4 280.874 75.6295 32 5 5 4 257.748 64.0280 11 5 -5 5 14.8127 36.3735 44 5 -5 5 80.2536 45.4996 42 -5 -5 -5 108.706 58.2255 21 5 5 5 99.9537 46.8521 20 5 -5 5 60.9780 45.8352 32 5 -5 5 135.829 52.3915 48 5 -5 6 3198.95 240.984 48 -5 -5 -6 3587.98 250.396 21 5 5 6 3088.81 213.777 20 5 -5 6 3100.76 226.756 44 5 5 6 3247.07 242.503 43 5 -5 6 3387.23 248.918 42 5 -5 6 3003.00 231.675 32 5 -5 6 2775.41 202.157 28 5 -5 7 25457.5 788.593 48 -5 -5 -7 25420.2 784.646 21 5 5 7 24016.7 726.503 20 5 5 7 24705.2 784.795 43 5 -5 7 25516.1 801.783 42 5 -5 7 24410.6 780.443 32 5 -5 7 23439.3 722.684 28 5 5 8 1328.85 154.471 43 5 -5 8 1359.32 157.305 42 -5 -5 -8 1329.10 152.909 21 5 5 8 1376.36 143.600 20 5 -5 8 1214.91 147.456 32 5 -5 8 1477.34 160.661 48 5 5 9 3986.77 257.227 43 5 -5 9 3903.45 260.207 42 -5 -5 -9 3646.36 241.645 21 5 5 9 3850.20 234.776 20 5 -5 9 3493.41 245.116 48 5 -5 9 3687.01 249.728 32 5 -5 9 3594.85 231.397 33 5 -5 10 635.320 101.748 32 5 -5 10 588.492 92.3654 33 5 5 10 499.520 89.7821 43 5 -5 10 343.767 77.2410 42 5 -5 11 177.632 54.4676 32 5 5 11 173.454 52.7650 32 5 -5 11 191.552 53.0510 33 5 5 12 10.6963 28.3511 32 5 -5 12 9.85999 24.1960 33 5 5 13 17.2536 27.3301 32 5 -5 13 8.10053 24.3462 33 5 5 14 12.4419 21.5892 32 5 -5 14 6.05798 18.2072 33 -5 -6 15 4506.89 198.419 18 -5 6 15 4998.33 202.583 18 5 6 -14 549.872 68.8386 56 -5 6 14 514.256 72.9121 18 -5 -6 14 561.972 79.5551 18 5 6 -13 97.9215 38.9618 56 -5 6 13 253.948 61.1627 18 -5 -6 13 142.397 50.3551 18 5 -6 -12 136.008 49.5639 51 5 6 -12 145.528 48.9163 56 -5 -6 12 152.064 53.9250 18 5 -6 -11 2470.56 192.528 51 5 6 -11 2669.27 187.368 56 -5 -6 11 2348.02 196.080 18 5 -6 -10 3100.20 223.361 51 5 6 -10 3034.57 207.896 56 -5 -6 10 2825.02 221.493 18 5 -6 -9 2783.07 217.594 51 -5 -6 9 2308.32 191.192 15 5 6 -9 2817.80 203.913 56 -5 -6 9 2427.94 211.092 18 5 -6 -8 147.400 57.1102 52 -5 -6 8 218.037 66.8648 15 5 6 -8 282.628 68.2315 56 -5 -6 8 188.452 65.0044 18 5 -6 -7 3089.12 218.670 52 5 -6 -7 3554.21 248.034 51 -5 -6 7 3155.92 233.800 15 5 6 -7 2791.04 203.302 56 -5 -6 7 2884.20 227.940 18 5 -6 -6 3605.97 236.259 52 5 6 -6 3651.21 229.760 56 -5 -6 6 3433.16 246.719 15 -5 -6 5 10621.3 460.588 15 5 -6 -5 11517.2 451.447 52 5 -6 -5 11666.5 467.265 51 5 6 -4 5085.41 277.996 41 5 -6 -4 5015.33 322.698 40 -5 -6 4 4670.01 284.472 36 5 -6 -4 5132.03 279.427 52 5 -6 -4 5068.94 287.953 51 -5 -6 4 4868.08 294.327 15 5 6 -4 4965.89 277.083 57 5 6 -3 103.840 41.1853 41 -5 -6 3 89.9128 47.5297 36 5 -6 -3 106.616 53.4541 40 5 -6 -3 199.946 58.7652 52 -5 -6 3 205.696 67.4903 15 5 6 -3 105.487 49.4799 57 5 -6 -3 138.116 53.6382 57 5 6 -2 683.581 105.672 57 -5 -6 2 754.984 113.112 15 5 6 -2 763.148 107.060 41 -5 -6 2 714.695 115.740 36 5 -6 -2 479.494 101.473 40 5 -6 -2 611.583 103.562 26 5 6 -1 4161.39 258.365 41 5 -6 -1 4326.59 272.439 44 5 -6 -1 4444.36 301.271 40 -5 -6 1 4705.50 286.978 36 5 6 -1 4239.06 258.844 57 5 -6 -1 4178.11 263.273 57 5 -6 -1 4399.08 265.204 26 5 6 0 27077.5 793.314 57 5 -6 0 26694.6 793.075 57 5 6 0 26207.6 806.505 6 5 6 0 27213.3 787.774 41 5 -6 0 26412.3 809.533 44 5 -6 0 24924.8 836.045 40 -5 -6 0 26847.5 820.453 36 5 -6 0 25956.9 785.675 32 5 -6 0 27843.3 814.053 27 5 6 1 13.6304 33.4484 57 5 -6 1 13.6896 27.4293 57 -5 -6 -1 14.6762 32.8768 21 5 6 1-15.3777 30.8116 6 5 6 1 13.4344 26.9182 41 -5 -6 -1 76.3162 45.8724 36 5 -6 1 30.7741 40.7840 44 5 -6 1 28.4663 37.7257 32 5 -6 1 28.5621 37.8526 27 5 6 2 64.1033 33.9973 11 5 6 2 127.585 59.7887 6 5 6 2 27.1198 35.9557 57 -5 -6 -2 105.945 54.6781 21 5 6 2 26.8456 35.5925 41 -5 -6 -2 90.2681 52.2203 36 5 -6 2 46.7788 41.3423 44 5 -6 2 44.6191 36.5118 42 5 -6 2 44.1443 41.7075 32 5 -6 2 84.0543 44.3923 27 5 6 3 5260.58 290.016 57 5 -6 3 5738.11 308.135 48 -5 -6 -3 5240.76 308.612 21 5 -6 3 5249.16 313.920 44 5 -6 3 5206.03 309.635 42 5 -6 3 5149.10 302.143 32 5 -6 3 4878.75 270.439 28 5 -6 3 5202.16 292.080 27 5 -6 4 4294.98 271.094 48 -5 -6 -4 4334.69 280.233 21 5 -6 4 4016.94 269.991 44 5 -6 4 4097.12 276.513 42 5 -6 4 3549.48 251.670 32 5 -6 4 3847.18 239.047 28 5 -6 5 183.808 66.9327 48 -5 -6 -5 79.3569 50.3411 21 5 6 5 127.643 55.7933 20 5 -6 5 76.5709 43.4638 44 5 -6 5 180.398 65.7637 42 5 -6 5 157.332 59.0262 32 5 -6 5 254.100 67.3949 28 5 -6 6 140.169 60.4335 48 -5 -6 -6 15.7659 38.6977 21 5 6 6 25.4928 42.3601 20 5 -6 6 29.5204 46.7679 44 5 6 6 32.0315 42.4588 43 5 -6 6 98.8059 52.1761 42 5 -6 6 31.5260 41.7891 32 5 -6 6 102.560 57.4423 28 5 -6 7 77.3702 51.5192 48 -5 -6 -7 184.632 70.7110 21 5 6 7 238.346 64.1642 20 5 6 7 187.871 62.8226 43 5 -6 7 307.603 81.1603 42 5 -6 7 217.082 72.9338 32 5 -6 7 152.841 59.9386 28 5 -6 8 1764.03 173.549 48 -5 -6 -8 1646.39 168.188 21 5 6 8 1608.52 151.110 20 5 6 8 1504.57 162.331 43 5 -6 8 1580.60 168.627 42 5 -6 8 1859.99 177.839 32 5 -6 8 1812.87 160.373 28 5 6 9 834.148 115.653 43 -5 -6 -9 856.658 118.197 21 5 6 9 807.068 106.729 20 5 -6 9 829.414 114.403 32 5 -6 9 841.998 109.547 33 5 -6 9 850.072 117.821 48 5 6 10 5897.74 291.549 43 5 -6 10 5999.74 300.100 32 5 -6 10 6115.43 287.819 33 -5 -6 -10 5697.74 289.841 21 5 -6 10 5116.50 276.156 46 5 -6 11 40.2490 30.2412 33 5 6 11-22.2078 27.2480 32 5 -6 11 9.93857 24.3884 46 5 6 12 717.191 90.3234 32 5 -6 12 613.864 78.7611 33 5 6 13 2306.24 142.237 32 5 -6 13 2193.79 132.422 33 -5 -7 14 956.006 90.7654 18 -5 7 14 1081.73 91.1072 18 5 7 -14 896.883 76.8263 56 -5 7 13 617.820 78.9126 18 -5 -7 13 490.582 76.5448 18 5 7 -13 509.292 67.8357 56 -5 -7 12 1640.30 145.296 18 5 7 -12 1494.23 127.266 56 5 -7 -12 1664.30 138.592 51 -5 -7 11 1197.32 135.825 18 5 7 -11 1345.52 128.794 56 5 -7 -11 1211.16 129.512 51 -5 -7 10 5191.78 294.077 18 5 7 -10 5372.30 273.204 56 5 -7 -10 5009.66 282.597 51 -5 -7 9 965.908 130.117 18 5 7 -9 891.031 115.149 56 -5 -7 9 1022.82 125.643 15 5 -7 -9 934.615 124.917 51 -5 -7 8 4109.57 268.243 18 5 7 -8 4150.04 245.472 56 -5 -7 8 3943.71 255.214 15 5 -7 -8 3699.37 251.786 51 -5 -7 7 61.7843 46.4223 18 5 -7 -7 14.9906 36.7865 51 5 7 -7-12.4900 30.6505 56 -5 -7 7 44.4685 46.9590 15 5 -7 -6 253.903 70.2600 51 -5 -7 6 198.707 70.2517 15 5 7 -6 135.650 51.0478 56 -5 -7 5 14827.3 556.749 15 -5 -7 5 14304.5 513.284 9 5 -7 -5 13383.7 507.122 52 5 -7 -5 14703.6 543.053 51 -5 -7 4 2749.05 220.169 15 5 -7 -4 2764.33 220.157 45 5 -7 -4 2600.78 199.590 52 5 -7 -4 2952.41 217.748 51 5 7 -4 3161.40 218.936 57 -5 -7 3 4475.68 284.881 15 5 -7 -3 4779.14 297.700 45 5 -7 -3 4501.80 259.976 52 5 7 -3 4615.19 273.481 57 5 -7 -2 400.492 91.0202 45 5 7 -2 307.955 75.8008 57 -5 -7 2 357.271 88.4698 15 5 -7 -2 370.555 84.7220 26 5 -7 -1 2895.60 230.195 44 5 7 -1 2876.82 216.723 57 -5 -7 1 3216.88 231.808 15 5 -7 -1 3373.22 247.980 45 5 7 0 313.642 75.7781 57 5 -7 0 363.213 85.3761 44 5 -7 0 271.386 76.8991 45 5 -7 0 322.576 77.9252 32 5 -7 0 287.143 72.0620 28 5 -7 0 268.409 70.2880 27 5 7 1 398.585 85.7932 57 5 -7 1 377.365 86.5030 45 5 -7 1 241.194 75.8145 44 5 -7 1 452.411 90.8607 32 5 -7 1 302.203 71.6321 28 5 -7 1 320.191 78.7664 27 5 7 2 421.219 84.6886 57 5 -7 2 433.679 87.1766 46 5 -7 2 382.945 84.3443 45 -5 -7 -2 348.843 86.2404 21 5 -7 2 421.414 92.1220 44 5 -7 2 308.646 79.1451 32 5 -7 2 292.212 70.0677 28 5 -7 2 535.798 97.0938 27 5 7 3 328.403 72.6958 57 5 -7 3 191.508 62.7971 45 5 -7 3 359.295 82.2857 46 5 -7 3 227.530 71.3934 48 -5 -7 -3 295.288 81.0439 21 5 -7 3 194.462 69.0443 44 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33.0196 32 7 -1 7 13.7206 36.3689 42 7 -1 8 1063.67 119.780 32 7 1 8 1148.80 122.988 32 7 -1 8 1164.26 132.167 42 7 -1 9 62.2812 38.9246 32 7 1 9 70.5353 36.4133 32 7 1 9 78.1769 38.7728 42 7 -1 9 33.5593 35.4555 42 7 -1 10 717.982 86.7101 32 7 1 10 727.039 85.5804 32 7 1 10 772.706 92.2651 42 7 -1 10 569.822 79.8771 42 7 -1 11 144.752 39.0943 32 7 1 11 135.058 37.0535 32 7 1 11 106.187 32.5573 42 7 -1 11 64.1850 29.5219 42 7 2 -13 5927.25 230.620 56 7 -2 -13 6087.07 233.743 51 -7 2 12 2035.87 138.604 15 7 2 -12 1985.06 136.664 56 7 -2 -12 2004.46 139.560 56 -7 -2 11 5216.00 246.792 15 -7 2 11 4867.36 241.020 15 7 2 -11 5280.12 244.816 56 7 -2 -11 4563.96 234.468 56 -7 -2 10 1095.45 121.384 15 -7 2 10 1183.83 123.732 15 7 2 -10 885.867 104.741 56 7 -2 -10 1080.95 116.520 56 7 -2 -10 945.891 101.291 52 -7 -2 9 12.3280 40.9631 15 -7 2 9 96.5411 48.3593 15 7 2 -9 10.8935 32.7422 56 7 -2 -9 68.8987 41.4798 56 7 -2 -9 10.4151 25.5615 52 -7 -2 8 903.281 124.245 15 7 2 -8 733.059 103.317 56 7 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34.2274 57 7 -2 1 163.167 61.2730 27 7 2 1 14.8606 42.1130 44 7 -2 1 90.7414 54.6309 44 7 2 2-27.1480 47.1059 57 7 -2 2-13.5195 38.3075 57 7 -2 2 29.7994 42.2182 27 7 2 2 14.8581 49.3670 44 7 -2 2 30.4288 37.3343 44 7 -2 3 12215.1 488.852 44 7 2 3 11336.5 471.742 44 7 -2 4 1562.24 162.806 44 7 2 4 1134.58 144.512 43 7 -2 4 1336.32 149.588 42 7 2 4 1399.24 149.906 44 7 -2 5 983.033 125.934 44 7 2 5 958.352 128.989 43 7 -2 5 619.166 104.346 42 -7 -2 -5 1019.74 128.772 21 7 2 5 1051.09 127.534 44 7 -2 6 100.274 46.9909 32 7 -2 6 38.1413 36.0348 44 7 2 6 57.6488 43.3227 43 7 -2 6 14.0838 37.3389 42 7 -2 7 3682.21 230.852 32 7 2 7 4088.95 254.212 43 7 -2 7 4108.15 252.428 42 7 -2 8 90.1594 42.2593 32 7 2 8 62.9138 36.4064 32 7 -2 8 36.8450 38.9244 42 7 -2 9 1103.15 113.850 32 7 2 9 1067.68 108.303 32 7 -2 9 1165.07 119.662 42 7 -2 10 69.1724 33.5700 32 7 2 10 49.3831 30.8749 32 7 2 10 53.2052 30.7971 42 7 -2 10 116.064 42.9110 42 7 -2 11 307.959 52.5949 32 7 2 11 455.490 59.4877 32 7 2 11 323.547 52.0501 42 7 -2 11 308.904 51.6238 42 7 3 -13 5.92483 18.7764 56 7 -3 -13 78.0835 28.8619 51 -7 3 12 492.428 66.4019 15 7 3 -12 524.103 68.8617 56 7 -3 -12 559.344 72.9778 51 -7 -3 11 1212.23 115.125 15 -7 3 11 1520.67 126.869 15 7 3 -11 1257.30 112.727 56 7 -3 -11 1240.27 115.526 56 -7 -3 10 2257.26 165.960 15 -7 3 10 2056.58 159.271 15 7 3 -10 1994.45 149.843 56 7 -3 -10 1915.42 153.119 56 7 -3 -10 1985.87 143.511 52 -7 -3 9 9131.28 376.683 15 7 3 -9 8726.74 349.674 56 7 -3 -9 9141.41 367.035 56 7 -3 -9 8926.16 350.229 52 -7 -3 8 16655.2 556.619 15 7 3 -8 15606.9 513.523 56 7 -3 -8 15189.2 522.131 56 7 -3 -8 15543.8 515.255 52 7 -3 -7 1397.47 141.123 56 -7 -3 7 1301.77 144.267 15 7 -3 -7 1241.89 136.312 26 7 -3 -7 1596.81 147.823 52 -7 -3 6 14.1850 37.5997 15 7 -3 -6 68.4226 47.4914 26 7 -3 -6 12.2779 38.8979 52 7 3 -5 1068.88 124.706 57 7 -3 -5 1132.95 127.523 57 -7 -3 5 834.713 122.951 15 7 -3 -5 1004.44 131.540 26 7 -3 -5 1087.68 127.286 52 7 3 -4 3166.30 220.696 57 7 -3 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7 -4 -10 1107.00 114.811 51 -7 -4 9 5410.15 271.008 15 7 4 -9 4997.07 246.087 56 7 -4 -9 5026.73 244.742 52 7 4 -8 10696.1 393.662 56 -7 -4 8 11156.0 431.039 15 7 -4 -8 11193.2 421.170 26 7 -4 -8 11483.0 410.983 52 -7 -4 7 52.7724 49.4526 15 7 -4 -7-25.2458 39.9887 26 7 -4 -7 11.3448 34.0955 52 -7 -4 6 744.076 111.447 15 7 -4 -6 823.591 114.954 26 7 -4 -6 864.903 109.171 52 7 4 -5 1107.13 125.637 57 7 -4 -5 1147.77 129.166 57 -7 -4 5 1506.09 156.154 15 7 -4 -5 1230.77 142.857 26 7 -4 -5 1293.16 134.044 52 7 4 -4 1872.88 163.070 57 7 -4 -4 1591.65 152.326 57 -7 -4 4 1549.79 159.858 15 7 -4 -4 1554.29 146.866 52 7 -4 -4 1356.17 153.213 26 7 -4 -3 8337.01 357.889 52 7 4 -3 7955.16 367.126 57 7 -4 -3 8323.34 377.974 57 7 -4 -3 8616.46 383.247 27 7 -4 -3 8542.78 397.553 26 7 4 -2 3056.22 216.736 57 7 -4 -2 3107.29 219.220 57 7 -4 -2 2745.57 211.389 27 7 -4 -2 2757.93 216.434 26 7 4 -1 1538.87 157.876 57 7 -4 -1 1177.98 141.921 57 7 -4 -1 1571.24 161.603 27 7 -4 -1 1318.93 149.978 26 7 -4 -1 1475.43 154.603 44 7 4 0 233.279 64.6636 57 7 -4 0 220.321 66.3375 57 7 -4 0 306.014 74.5967 26 7 -4 0 350.423 81.5868 27 7 -4 0 248.384 70.3663 44 7 4 1 2130.30 182.283 57 7 -4 1 2316.53 190.404 57 7 -4 1 2351.98 198.314 27 7 -4 1 2351.29 196.197 26 7 -4 1 2518.64 206.400 44 7 4 2 26.0660 29.1950 57 7 -4 2-12.9257 34.2597 57 7 -4 2-14.4220 38.2255 27 7 -4 2 44.5079 44.5877 44 -7 -4 -3-15.2979 34.2683 21 7 -4 3-14.5330 29.1181 44 7 4 3 82.3411 43.4753 43 7 -4 3-12.1090 34.3107 57 7 -4 3 28.0508 39.7409 27 7 -4 4 1132.30 135.277 44 7 4 4 1259.62 140.294 43 7 -4 4 1043.09 130.251 42 -7 -4 -4 995.620 132.097 21 7 4 4 1375.59 144.149 44 7 4 5 84.2937 43.5024 44 7 -4 5 26.0721 31.9979 44 7 4 5 40.9730 36.2076 43 7 -4 5 26.4633 35.0787 42 -7 -4 -5 13.7085 36.3423 21 7 4 5 52.2327 31.4050 20 7 -4 5 61.1612 38.7585 32 7 -4 6 177.285 55.6151 44 7 4 6 157.422 54.2675 43 7 -4 6 216.648 59.9557 42 -7 -4 -6 112.478 48.5810 21 7 4 6 120.261 43.8634 20 7 -4 6 248.067 62.6899 32 7 4 7 183.074 54.7198 43 7 -4 7 83.2138 41.3068 42 -7 -4 -7 66.0960 41.3448 21 7 -4 7 166.366 49.7337 32 7 4 8 1287.95 128.898 43 7 -4 8 1537.36 136.226 42 7 -4 8 1518.74 132.918 32 7 4 9 2314.75 158.776 43 7 -4 9 2343.55 158.392 42 7 -4 9 2093.29 147.909 32 7 4 10 437.974 58.4527 32 7 -4 10 481.412 64.4329 32 7 -4 10 514.181 64.1849 46 7 5 -12-5.42985 17.2015 56 7 -5 -12 5.95900 19.7992 51 -7 -5 11 2480.18 143.528 15 -7 5 11 2471.46 147.500 15 7 5 -11 2396.59 139.415 56 7 -5 -11 2395.97 147.684 51 -7 -5 10 449.387 69.1300 15 7 5 -10 354.893 59.8441 56 7 -5 -10 437.043 69.0461 51 7 5 -9 5913.61 257.072 56 -7 -5 9 6377.22 285.057 15 7 -5 -9 6358.11 277.672 26 7 -5 -9 6030.54 277.678 51 -7 -5 8 3022.86 201.140 15 7 -5 -8 2811.48 189.427 26 7 -5 -8 2677.06 174.864 52 7 -5 -8 3154.56 198.534 51 -7 -5 7 1209.55 133.753 15 7 -5 -7 1199.10 131.150 26 7 -5 -7 1081.16 115.881 52 7 -5 -7 1178.51 126.199 51 -7 -5 6 169.388 59.8990 15 7 -5 -6 115.696 49.9747 26 7 -5 -6 200.399 55.8538 52 7 -5 -6 208.214 59.1709 51 7 5 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122.037 21 7 5 2 743.756 106.499 57 7 -5 2 832.712 116.264 27 -7 -5 -3 100.843 52.0666 21 7 -5 3 104.954 52.6022 27 7 -5 3 96.9846 50.0768 44 7 5 3 90.9187 43.1926 43 -7 -5 -4 220.421 66.3442 21 7 5 4 227.153 56.8379 20 7 -5 4 271.934 63.9471 32 7 -5 4 209.574 63.1378 27 7 -5 4 285.856 68.3482 42 7 -5 4 277.513 68.9408 44 7 5 4 246.953 63.9515 43 7 -5 5 560.646 91.8224 42 7 5 5 649.656 91.4174 44 7 -5 5 342.589 74.1050 44 7 5 5 481.635 85.6616 43 -7 -5 -5 617.973 99.4853 21 7 5 5 428.742 74.6351 20 7 -5 5 495.954 83.8167 32 7 -5 6 545.560 87.7170 42 7 -5 6 457.679 77.9779 44 7 5 6 721.178 100.629 43 -7 -5 -6 596.444 92.9097 21 7 5 6 762.166 92.0561 20 7 -5 6 581.346 87.2248 32 7 5 7 99.0647 41.3013 43 7 -5 7 171.964 48.6353 32 -7 -5 -7 61.5848 37.1213 21 7 5 8 9.64251 25.5578 43 -7 -5 -8 8.57219 27.1566 21 7 -5 8-8.84063 23.4325 46 7 -5 8 44.8527 31.1309 32 7 5 9 428.462 64.5619 43 7 -5 9 369.476 60.4668 32 7 -5 9 484.209 66.6095 46 -7 6 11 348.231 51.0755 15 7 6 -11 342.068 47.0996 56 7 -6 -11 328.367 50.4331 51 7 6 -10 268.366 47.2244 56 -7 -6 10 151.482 42.3441 15 7 -6 -10 253.495 48.5416 26 7 -6 -10 257.381 52.1589 51 7 6 -9 115.016 34.6659 56 7 -6 -9 136.454 41.9618 26 7 -6 -9 190.839 47.6911 51 -7 -6 8 20.1520 31.9204 15 7 -6 -8-9.80666 29.4728 26 7 -6 -8-9.53484 28.6559 51 -7 -6 7 998.720 116.754 15 7 -6 -7 1032.88 113.944 26 7 -6 -7 1261.61 122.168 51 -7 -6 6 4367.06 248.540 15 7 -6 -6 4511.57 252.103 26 7 -6 -6 3893.22 218.007 52 7 6 -5 10.4312 29.5568 57 -7 -6 5 12.3412 30.2838 15 7 -6 -5-12.3473 34.9861 26 7 -6 -5 22.2716 31.5532 27 7 -6 -5-10.3519 25.4022 52 7 -6 -5 23.1981 28.4627 45 7 6 -4 505.830 84.7945 57 -7 -6 4 512.857 89.9859 15 7 -6 -4 509.718 89.8570 26 7 -6 -4 514.174 86.8950 27 7 -6 -4 468.736 77.2594 52 7 -6 -4 565.029 92.0588 45 7 6 -3 2832.70 198.358 57 -7 -6 3 2814.30 203.015 15 7 -6 -3 3028.23 215.140 45 7 -6 -3 2855.34 207.733 26 7 -6 -2 9290.30 398.258 45 7 6 -2 8961.19 378.210 57 7 -6 -2 8851.17 384.679 27 7 -6 -2 8439.08 376.471 26 7 -6 -1 55.0112 45.7171 45 7 -6 -1 76.5411 40.4384 44 7 6 -1 161.056 54.1179 57 7 -6 -1 37.9077 35.8325 26 7 -6 -1 118.428 54.3705 27 7 -6 0 598.934 102.035 45 -7 -6 0 628.815 100.005 21 7 -6 0 764.762 110.557 44 7 6 0 764.646 107.143 57 7 -6 0 893.828 121.446 27 7 -6 0 816.069 109.976 26 7 -6 1 3534.71 233.803 45 -7 -6 -1 3672.06 237.597 21 7 -6 1 3614.21 237.329 44 7 6 1 3767.27 229.842 57 7 -6 1 3653.44 232.884 27 7 -6 2 960.230 118.591 45 7 -6 2 897.616 118.930 44 -7 -6 -2 919.523 122.974 21 7 6 2 1022.61 109.224 20 7 6 2 1086.69 123.691 57 7 -6 2 995.871 122.263 27 -7 -6 -3 78.1758 43.3175 21 7 6 3 79.2963 39.7484 20 7 -6 3 47.0069 39.0756 27 7 -6 3 178.682 59.9905 44 7 6 3 83.2623 41.3061 43 -7 -6 -4 1556.16 151.807 21 7 6 4 1461.34 127.649 20 7 -6 4 1638.68 149.556 44 7 6 4 1436.32 139.936 43 7 -6 4 1642.50 143.643 32 7 -6 4 1494.60 137.593 27 7 -6 5 176.031 56.2651 44 7 6 5 158.802 52.1441 43 -7 -6 -5 139.108 52.0062 21 7 6 5 145.908 46.6618 20 7 -6 5 114.940 43.2453 32 7 -6 5 162.065 47.6720 46 7 -6 6 57.6576 33.3743 44 7 6 6 63.4949 36.7481 43 -7 -6 -6 104.695 45.7363 21 7 6 6 84.3809 34.8784 20 7 -6 6 97.5367 39.1068 32 7 -6 6 47.5229 30.1388 46 7 6 7 104.335 39.1852 43 -7 -6 -7 54.6128 34.1268 21 7 -6 7 8.78544 24.9055 32 7 -6 7 42.8606 28.4919 46 7 6 8 3373.91 180.645 43 7 -6 8 3093.82 168.656 32 -7 -6 -8 3162.47 169.735 21 7 -6 8 3040.23 165.175 46 7 -6 9 1669.61 107.762 46 7 -7 -10 1819.82 110.119 26 7 -7 -10 1480.96 102.733 51 -7 -7 9 1654.65 117.026 15 7 -7 -9 1565.32 114.555 26 7 -7 -9 1509.94 112.602 51 -7 -7 8 58.7630 34.6875 15 7 -7 -8 41.3421 31.0078 26 7 -7 -8 55.2610 27.4128 51 -7 -7 7 142.270 46.6181 15 7 -7 -7 120.663 41.6617 26 7 -7 -7 153.120 45.1655 51 -7 -7 6 1346.65 127.794 15 7 -7 -6 1123.44 110.099 27 7 -7 -6 1300.90 123.395 26 -7 -7 5 473.611 73.6920 9 7 7 -5 600.175 81.0900 57 -7 -7 5 529.894 83.8271 15 7 -7 -5 618.689 88.6996 26 7 -7 -5 539.255 81.2881 27 -7 -7 4 2216.52 159.420 9 7 7 -4 1969.41 152.060 57 -7 -7 4 2059.84 165.973 15 7 -7 -4 2454.09 174.389 27 7 -7 -4 2326.50 172.160 26 7 -7 -4 1939.91 160.461 45 7 7 -3 423.429 77.0311 57 -7 -7 3 474.529 79.9326 9 7 -7 -3 635.941 92.6315 26 7 -7 -3 452.796 79.9206 27 7 -7 -3 577.308 91.8935 45 7 7 -2 866.899 107.507 57 7 -7 -2 866.074 112.754 45 -7 -7 2 1000.05 116.176 9 7 -7 -2 1085.48 120.573 27 7 -7 -2 1038.60 115.880 26 7 7 -1 1536.40 141.906 57 7 -7 -1 1577.56 144.543 44 7 -7 -1 1541.12 149.040 45 -7 -7 1 1507.02 143.557 9 7 -7 -1 1769.61 154.606 27 7 7 0 11.0546 27.1276 57 7 -7 0 24.3415 36.5785 45 7 -7 0 11.7459 35.3016 44 -7 -7 0 11.3123 33.9987 9 7 -7 0 11.6726 30.9391 27 7 7 1 3568.72 211.016 57 7 -7 1 3118.63 209.446 45 -7 -7 -1 2908.96 198.991 21 7 7 1 3369.29 192.047 20 7 -7 1 3087.66 207.536 44 -7 -7 -1 3424.83 209.094 9 7 -7 1 3694.44 220.696 27 7 7 2 161.074 48.4221 57 7 -7 2 131.510 45.3258 45 7 -7 2 81.9213 40.6791 44 -7 -7 -2 91.0902 47.0878 21 7 7 2 127.740 44.8395 20 7 -7 2 225.865 59.0609 27 -7 -7 -2 112.071 42.1462 9 -7 -7 -3 1182.04 125.176 21 7 7 3 1307.75 115.373 20 7 -7 3 1058.27 110.887 32 7 -7 3 1144.42 116.460 27 7 -7 3 1193.11 124.797 44 7 7 3 986.265 109.130 43 7 -7 4 564.811 83.2559 44 7 7 4 629.799 87.6584 43 7 -7 4 646.445 84.3100 32 -7 -7 -4 521.624 82.6711 21 7 7 4 652.787 80.8949 20 7 -7 5 28.0961 26.5391 44 7 7 5 28.8917 23.6349 43 -7 -7 -5 29.5853 27.9456 21 7 7 5-7.88529 24.9827 20 7 -7 5 53.7189 31.0723 32 7 -7 5 16.8435 22.3247 46 7 -7 6 31.7285 27.5334 44 7 7 6 79.0755 36.2961 43 -7 -7 -6 52.8318 34.1691 21 7 7 6-7.10926 20.1529 20 7 -7 6 57.0604 34.6510 32 7 -7 6 54.2261 30.0621 46 7 7 7 175.177 41.9901 43 7 -7 7 241.102 47.2985 32 -7 -7 -7 202.199 44.5711 21 7 -7 7 284.882 50.0996 46 7 -8 -8 100.757 31.5752 26 -7 -8 8 57.6474 28.7321 15 7 -8 -7 188.278 45.4259 26 -7 -8 7 172.291 42.5810 15 7 -8 -6 786.772 83.4609 27 7 -8 -6 964.919 95.6838 26 -7 -8 6 691.643 84.7897 15 7 -8 -5 186.780 46.7621 26 7 -8 -5 234.072 51.7851 27 -7 -8 5 249.178 55.8235 15 -7 -8 5 220.960 47.4204 9 -7 -8 4 24.9856 28.9088 9 7 8 -4 16.5495 23.4541 57 -7 -8 4 45.8493 33.1270 15 7 -8 -4 52.7001 31.7313 26 7 -8 -4 9.07554 25.7225 27 7 -8 -4 101.027 41.1514 45 7 8 -3 3213.56 184.976 57 -7 -8 3 3197.03 186.479 9 7 -8 -3 3297.02 193.447 27 7 -8 -3 3235.45 185.710 26 7 -8 -3 3250.17 195.639 45 7 8 -2 1667.91 134.541 57 -7 -8 2 1911.60 144.197 9 7 -8 -2 2088.34 153.006 27 7 -8 -2 1601.94 140.197 45 7 8 -1 217.756 52.9475 57 7 -8 -1 293.028 65.5854 45 -7 -8 1 211.772 53.8286 9 7 -8 -1 148.491 48.7354 27 7 8 0 702.361 87.7222 57 7 -8 0 535.428 83.2807 45 7 8 0 599.533 75.8071 20 7 -8 0 599.238 83.6792 44 -7 -8 0 541.878 79.9015 9 7 -8 0 689.412 89.8569 27 7 8 1 98.8901 39.2878 57 7 -8 1 98.2296 36.8531 45 7 8 1 71.2328 31.7541 20 7 -8 1 79.5685 38.6215 44 -7 -8 -1 90.7944 39.6780 9 7 -8 1 74.2297 37.2141 27 7 8 2 107.817 39.0653 57 7 -8 2 189.984 48.8821 45 7 -8 2 97.5745 43.7996 44 -7 -8 -2 133.410 41.8541 9 7 8 2 170.970 42.7287 20 7 -8 2 223.576 51.7585 27 7 -8 3 120.369 40.4529 44 -7 -8 -3 70.3972 37.4232 21 7 8 3 44.7077 28.9396 20 7 -8 4 1623.12 120.905 32 7 -8 4 1692.67 130.476 44 7 8 4 1849.21 134.364 43 -7 -8 -4 2035.46 141.203 21 7 8 4 1975.40 127.618 20 7 -8 5 663.213 74.9047 32 -7 -8 -5 705.302 80.8424 21 7 8 5 778.790 75.5477 20 7 -8 5 696.907 77.7956 44 7 8 5 633.026 75.0789 43 -7 -8 -6 493.342 63.3606 21 7 8 6 529.115 65.2679 43 -7 -9 6 12.0704 20.9451 15 -7 -9 5 138.931 37.5574 15 7 -9 -5 107.459 31.1022 27 -7 -9 4 25.0204 24.2716 9 7 9 -4 12.4847 18.7637 57 7 -9 -4 27.8754 25.1739 27 -7 -9 4 13.8040 20.7459 15 7 9 -3 1391.29 105.487 57 7 -9 -3 1413.74 112.149 27 -7 -9 3 1493.25 111.647 9 7 9 -2 880.210 87.9003 57 -7 -9 2 1016.32 93.7173 9 7 -9 -2 880.848 90.0200 27 7 9 -1 853.905 85.8399 57 7 -9 -1 728.259 85.4290 45 7 -9 -1 793.987 84.7134 27 -7 -9 1 705.636 78.5493 9 7 9 -1 587.969 66.2697 20 7 9 0-6.26070 19.8338 20 7 9 0 14.5536 21.8697 57 7 -9 0 7.39979 18.1584 44 7 -9 0 7.28622 21.8980 27 -7 -9 0 14.7209 25.5432 9 7 9 1 1289.67 102.070 57 7 -9 1 1311.29 107.946 44 7 9 1 1312.77 98.6110 20 -7 -9 -1 1334.29 104.898 9 7 -9 1 1344.17 103.951 27 7 9 2 1261.94 94.7542 20 7 9 2 1178.37 92.4207 57 7 -9 2 1176.47 100.509 44 7 9 3 33.6738 21.7783 20 7 -9 3 6.85447 20.6034 44 8 0 -11-10.8344 17.1621 56 -8 0 11-5.80778 21.7702 15 8 0 -10 16170.8 460.586 56 -8 0 10 18306.7 490.681 15 8 0 -9-6.92971 19.6354 52 -8 0 9 8.55407 35.3326 15 8 0 -8 723.642 83.8779 52 -8 0 8 829.533 98.9036 15 8 0 -7 9.07087 28.7360 52 -8 0 7-10.2724 44.8567 15 8 0 -6-9.80484 29.4674 52 -8 0 6 10.7498 34.0550 15 8 0 -5-20.5870 34.2026 57 -8 0 5-10.9599 46.5835 15 8 0 -4 5997.70 285.937 57 8 0 -3 11.6410 32.9855 57 8 0 -2 7022.40 320.437 44 8 0 -2 6969.13 325.099 57 8 0 -1-24.1724 38.2911 57 8 0 0 717.958 103.349 57 8 0 0 779.005 107.696 44 8 0 1-46.3728 40.2377 57 8 0 1-25.2475 35.7757 44 8 0 2 2308.86 183.670 44 8 0 2 2372.61 174.105 57 8 0 3 23.8905 37.8445 44 8 0 4 3480.80 215.912 44 8 0 5 10.0226 30.1221 44 8 0 5 10.0423 28.4554 42 8 0 6 9694.53 358.317 42 8 0 7-8.48483 28.1919 42 8 0 8 1246.51 102.643 42 8 1 -11 369.944 48.9264 56 -8 -1 11 368.233 51.5703 15 -8 1 11 422.033 55.5549 15 8 1 -10-6.23717 24.9935 56 8 -1 -10 6.45303 22.3941 56 -8 -1 10 14.3805 28.8127 15 -8 1 10-28.8055 34.5985 15 8 -1 -9 2389.21 141.791 52 8 -1 -9 2228.03 141.464 56 -8 -1 9 2864.76 167.484 15 -8 1 9 2801.02 166.342 15 8 1 -8 212.724 47.5529 52 8 -1 -8 268.353 53.5941 52 -8 -1 8 199.042 56.3398 15 -8 1 8 262.233 61.6745 15 8 -1 -7 1338.12 118.682 52 -8 -1 7 1300.05 126.756 15 -8 1 7 1390.29 128.854 15 8 -1 -6 77.7580 37.7293 52 -8 -1 6 42.9871 40.2991 15 -8 1 6 63.0998 43.4540 15 8 -1 -5 2250.81 162.292 52 8 1 -5 1927.71 151.200 57 8 -1 -5 2172.61 159.278 57 -8 -1 5 2031.96 163.542 15 -8 1 5 2355.43 171.137 15 8 1 -4 318.612 66.3114 57 8 -1 -4 285.863 66.3599 57 8 -1 -4 376.101 69.6838 52 8 1 -3 11.5511 32.7300 57 8 -1 -3 34.6665 34.7288 57 8 -1 -3-10.5047 23.5315 52 8 1 -2 475.459 83.7665 57 8 -1 -2 487.444 83.7834 57 8 1 -2 395.077 75.8957 44 8 1 -1 108.009 43.3714 57 8 -1 -1 35.9894 31.8287 57 8 1 -1 85.0155 42.1714 44 8 -1 -1 133.560 53.0389 44 8 1 0 178.260 54.6649 57 8 -1 0 154.287 51.9390 57 8 1 0 211.354 59.8302 44 8 -1 0 211.963 61.2884 44 8 -1 1 978.093 120.980 44 8 1 1 805.377 106.934 57 8 -1 1 953.063 112.757 57 8 1 1 872.998 115.028 44 8 1 2 10.8542 34.3860 57 8 -1 2-10.8180 35.9440 57 8 1 2 24.5351 32.5154 44 8 -1 2-24.7552 39.2118 44 8 -1 3 7282.40 331.492 44 8 1 3 7374.44 329.360 44 8 -1 4 777.208 102.926 44 8 1 4 699.374 97.7201 44 -8 -1 -4 833.941 104.469 21 8 1 5 58.6116 39.1536 44 8 -1 5 29.9532 31.6414 44 8 1 5 69.7446 41.1630 42 8 -1 5 39.4267 31.2369 42 8 1 6 457.489 75.3842 42 8 -1 6 536.151 79.1100 42 8 1 7 3635.37 194.880 42 8 -1 7 3751.88 194.048 42 8 1 8 325.803 53.4497 42 8 -1 8 337.313 55.3245 42 8 -2 -11 1082.36 83.7955 51 -8 -2 10 11199.4 350.686 15 -8 2 10 11290.1 352.407 15 8 -2 -9 1933.93 125.551 52 -8 -2 9 2109.92 142.589 15 -8 2 9 2119.74 140.499 15 8 2 -8 59.2389 30.6001 52 8 -2 -8 63.1769 31.6590 52 -8 -2 8 18.3163 27.5396 15 -8 2 8 89.6292 43.0719 15 8 -2 -7 762.632 89.2816 52 -8 2 7 762.519 96.1861 15 -8 -2 7 668.051 90.3577 15 8 -2 -6-9.41362 28.2916 52 -8 -2 6 42.0761 37.9950 15 -8 2 6-20.1459 36.3838 15 8 -2 -5 19.7180 26.1332 52 8 2 -5 29.6827 29.7376 57 8 -2 -5 9.89680 26.2334 57 -8 -2 5 21.5764 32.4242 15 -8 2 5 10.2500 34.0578 15 8 2 -4 3163.49 200.577 57 8 -2 -4 3136.10 196.804 57 8 -2 -4 3050.35 189.119 52 8 2 -3 461.480 80.1255 57 8 -2 -3 360.640 72.7266 57 8 -2 -3 473.802 75.9891 52 8 2 -2 1715.89 149.850 57 8 -2 -2 1775.53 154.862 57 8 -2 -2 1461.56 130.086 52 8 2 -2 1499.85 141.589 44 8 2 -1-23.4190 31.0364 57 8 -2 -1 11.7070 26.2251 57 8 2 -1 11.8624 31.4416 44 8 -2 -1-11.8546 31.4211 44 8 -2 0 1621.92 151.269 44 8 2 0 1796.60 154.481 57 8 -2 0 1654.13 149.760 57 8 2 0 1575.99 147.444 44 8 2 1 11.2095 27.5069 57 8 -2 1 11.1679 31.6441 57 8 2 1-12.1327 32.1577 44 8 -2 1-12.2709 34.7697 44 8 2 2 2022.75 167.440 44 8 2 2 1909.80 153.951 57 8 -2 2 1960.84 157.670 57 8 2 3 181.458 54.5519 44 8 -2 3 104.499 48.0321 44 -8 -2 -3 154.466 53.2989 21 8 2 4 10.4862 25.7331 44 8 -2 4-21.6652 32.5571 44 -8 -2 -4 10.8239 30.6705 21 8 2 5 213.569 51.8981 44 8 -2 5 174.826 48.7621 44 -8 -2 -5 151.972 48.6312 21 8 -2 6 1439.44 118.245 44 8 2 6 1290.51 117.234 42 8 -2 6 1263.44 115.555 42 8 2 7 7.97946 23.9817 42 8 -2 7 7.83136 20.7575 42 8 2 8 39.9482 23.1080 42 8 -2 8 6.55270 17.3713 42 -8 -3 10 104.951 32.2384 15 -8 3 10 186.393 42.2924 15 8 -3 -10 145.740 36.5900 51 -8 -3 9 1479.71 114.927 15 -8 3 9 1592.25 118.393 15 8 -3 -9 1424.62 103.819 52 8 -3 -9 1453.75 110.946 51 -8 -3 8 2018.65 142.609 15 -8 3 8 1922.90 138.485 15 8 -3 -8 1925.60 129.763 52 -8 -3 7 217.144 55.3459 15 -8 3 7 324.043 60.6696 15 8 -3 -7 231.773 49.9727 52 -8 -3 6 4171.36 223.712 15 -8 3 6 4077.18 215.877 15 8 -3 -6 4009.99 216.734 26 8 -3 -6 4276.90 214.843 52 8 3 -5 3353.62 193.005 57 8 -3 -5 3428.65 193.465 57 -8 -3 5 3419.49 204.256 15 8 -3 -5 2970.53 180.983 52 8 -3 -5 3327.08 204.635 26 8 -3 -4 549.680 79.6663 52 8 -3 -4 608.663 94.4709 26 8 3 -4 640.831 87.7912 57 8 -3 -4 652.302 89.7237 57 8 3 -3 1160.77 119.781 57 8 -3 -3 936.855 109.880 57 8 -3 -3 859.610 99.0571 52 8 3 -2 144.165 49.7331 57 8 -3 -2 155.473 53.4009 57 8 3 -2 87.0779 39.3790 44 8 3 -1 44.8153 35.4930 57 8 -3 -1 11.2016 29.6897 57 8 -3 -1-33.4356 35.3074 27 8 3 -1-11.3572 27.8692 44 8 -3 -1 56.6270 39.3026 44 8 3 0 243.745 59.8825 57 8 -3 0 198.866 55.4602 57 8 3 0 196.967 54.5644 44 8 -3 0 163.469 51.1180 44 8 3 1 555.722 86.7182 57 8 -3 1 478.326 77.9705 57 8 3 1 404.601 78.1331 44 8 -3 1 387.820 76.7543 44 8 3 2 214.384 58.7787 44 8 -3 2 150.051 50.4529 44 -8 -3 -2 109.077 48.6183 21 8 3 2 80.1094 37.6031 57 8 -3 2 119.085 44.5174 57 8 -3 3 1328.76 130.355 44 -8 -3 -3 1232.35 127.729 21 8 3 3 1100.47 118.897 44 8 -3 4 911.838 104.304 44 -8 -3 -4 792.783 100.339 21 8 3 4 812.217 98.2745 44 8 -3 5 857.546 96.2470 44 -8 -3 -5 974.969 102.541 21 8 3 5 1120.56 105.455 44 8 -3 6 22.9693 23.0154 44 8 -3 6 24.0534 26.6440 42 -8 -3 -6 30.7853 25.5760 21 8 -3 7 70.6250 29.1988 42 8 3 7 65.5582 29.2164 42 -8 -4 9 1865.67 122.344 15 -8 4 9 2160.41 130.388 15 8 -4 -9 2145.28 126.973 51 -8 -4 8 1159.18 104.047 15 -8 4 8 1096.25 100.285 15 8 -4 -8 1166.78 95.0328 52 8 -4 -8 1198.29 99.9531 51 -8 -4 7 8.60935 25.8745 15 -8 4 7 16.2427 28.1838 15 8 -4 -7 24.1899 22.8475 26 8 -4 -7-7.52528 21.3231 52 -8 -4 6 239.912 56.4478 15 -8 4 6 222.122 53.6783 15 8 -4 -6 310.048 61.4835 26 8 -4 -6 316.530 57.7073 52 8 4 -5-8.59990 19.2644 57 -8 -4 5-9.56119 31.7677 15 8 -4 -5 33.9252 25.4895 52 8 -4 -5-9.96559 28.2374 26 8 -4 -4 181.409 46.6863 52 8 -4 -4 95.4190 45.1475 26 8 4 -4 169.520 48.1879 57 8 -4 -4 160.250 46.3464 57 8 -4 -3 2011.23 140.781 52 8 -4 -3 1840.91 153.662 26 8 4 -3 1940.20 150.251 57 8 -4 -3 1972.28 152.723 57 8 4 -2 843.368 101.131 44 8 4 -2 982.783 110.464 57 8 -4 -2 1003.90 110.510 57 8 -4 -2 818.371 101.795 27 8 4 -1 2492.00 173.353 44 -8 -4 1 1799.92 156.330 21 8 -4 -1 1807.28 149.426 44 8 4 -1 2091.14 159.073 57 8 -4 -1 2014.74 155.353 57 8 -4 -1 1988.74 156.659 27 8 4 0 4394.61 238.760 44 -8 -4 0 4196.40 242.533 21 8 4 0 4107.81 227.292 57 8 -4 0 4355.24 230.968 57 8 -4 0 4458.82 240.474 27 8 -4 0 4097.04 232.362 44 8 4 1 85.8440 41.6850 44 8 -4 1 131.292 49.0612 44 -8 -4 -1 103.671 47.6244 21 8 4 1 138.785 45.5565 57 8 -4 1 108.176 39.4616 57 8 -4 2 836.318 103.038 44 -8 -4 -2 692.281 98.7044 21 8 4 2 884.244 104.811 44 8 4 2 894.182 97.6170 57 8 -4 3 2558.86 175.034 44 -8 -4 -3 3077.48 193.232 21 8 4 3 2796.33 179.764 44 8 4 4 123.547 45.1323 44 8 -4 4 103.381 40.0062 44 -8 -4 -4 135.118 44.3619 21 8 -4 5 24.7827 24.8304 44 -8 -4 -5 17.0054 30.7144 21 8 -4 6 324.957 52.3958 44 -8 -4 -6 319.547 53.5299 21 8 -4 6 273.920 46.9957 46 8 4 7 545.700 63.6425 42 -8 -5 8 6.56005 25.4544 15 -8 5 8 12.6433 29.0229 15 8 -5 -8 30.0402 24.8181 26 -8 -5 7 559.750 72.4159 15 -8 5 7 490.011 66.9179 15 8 -5 -7 590.539 72.4855 26 -8 -5 6 8799.30 313.167 15 -8 5 6 8140.47 295.130 15 8 -5 -6 8358.48 308.094 26 8 -5 -6 7748.97 285.033 52 8 5 -5 521.842 67.5008 57 -8 -5 5 482.123 70.9442 15 8 -5 -5 444.302 64.8557 52 8 -5 -5 474.270 73.3679 26 8 -5 -4 165.124 42.6084 52 8 -5 -4 156.603 48.0182 45 8 -5 -4 95.0923 40.4944 26 8 5 -4 134.429 40.4439 57 8 -5 -3 4058.94 219.506 45 8 5 -3 4213.47 214.572 57 8 -5 -3 3860.78 206.641 27 8 -5 -3 4227.13 224.560 26 8 -5 -2 246.239 57.3848 45 8 5 -2 256.916 56.0738 44 8 5 -2 270.496 58.5085 57 8 -5 -2 169.574 48.3096 27 8 -5 -1 404.098 72.2882 45 -8 -5 1 417.929 72.5809 21 8 5 -1 460.091 73.4966 44 8 -5 -1 346.115 64.6631 44 8 5 -1 396.111 67.8705 57 8 -5 -1 370.511 70.8171 27 8 -5 0 264.490 59.6629 45 -8 -5 0 290.778 62.1507 21 8 5 0 350.780 66.4203 44 8 -5 0 243.133 56.2228 44 8 5 0 278.505 59.0618 57 8 -5 0 334.245 67.0084 27 8 5 1 38.5335 25.5448 44 8 -5 1 39.1945 32.5656 44 -8 -5 -1 100.509 41.5223 21 8 -5 1 38.7199 27.4389 45 8 5 1 26.5912 25.1271 57 8 -5 2 899.903 100.442 44 -8 -5 -2 823.065 98.9231 21 8 5 2 777.529 94.0504 44 8 -5 2 868.785 95.2921 45 8 5 2 878.507 91.3685 57 8 -5 3 1687.64 133.911 44 -8 -5 -3 1705.61 136.017 21 8 5 3 1720.18 130.738 44 8 -5 4 2180.80 145.150 44 -8 -5 -4 2042.29 142.747 21 8 5 4 2051.51 136.669 44 8 -5 5 1011.66 91.2452 44 8 5 5 1064.58 93.7835 43 -8 -5 -5 1135.04 99.1685 21 8 -6 -7 207.346 40.0305 26 -8 -6 7 257.658 44.3088 15 -8 6 7 217.866 41.7132 15 8 -6 -6 716.767 75.6716 26 -8 -6 6 704.394 76.3783 15 -8 6 6 643.479 70.6282 15 8 -6 -5 1322.91 107.267 26 -8 -6 5 1220.18 100.892 15 -8 -6 5 1136.43 91.8192 9 8 6 -4 14.2040 22.5106 57 -8 -6 4 85.1073 32.5673 9 8 -6 -4 55.9721 31.0325 26 8 -6 -4 31.0448 29.1010 45 8 6 -3 384.513 60.7308 57 -8 -6 3 495.210 68.5156 9 8 -6 -3 419.629 65.1875 27 8 -6 -3 505.712 72.1179 45 8 6 -2 675.751 79.6347 57 8 -6 -2 651.994 83.3637 45 8 6 -2 725.646 82.7776 44 -8 -6 2 714.394 83.1737 9 8 -6 -2 781.987 87.8609 27 8 6 -1 455.749 68.6765 57 8 6 -1 355.579 61.9511 44 8 -6 -1 445.229 71.2516 45 -8 -6 1 468.751 70.3582 9 8 -6 -1 449.082 69.4193 27 8 6 0 1337.19 112.205 57 8 -6 0 1610.11 126.463 45 8 6 0 1417.36 118.529 44 8 -6 0 1226.43 109.197 44 -8 -6 0 1398.95 114.705 9 8 -6 0 1261.67 113.761 27 8 -6 1 8.19937 23.2329 45 -8 -6 -1 16.3185 29.4713 21 8 6 1-16.4691 26.0866 44 8 -6 1 8.31091 22.0280 44 -8 -6 -1 22.6527 27.2740 9 8 6 1 7.51387 18.4381 57 8 -6 2 1735.56 128.911 44 -8 -6 -2 1907.03 133.882 21 8 6 2 1838.71 130.192 44 8 -6 2 2038.88 132.840 45 8 6 2 1760.37 119.857 57 8 -6 3 1341.03 108.355 44 -8 -6 -3 1343.23 109.583 21 8 6 3 1359.76 105.986 44 8 6 4-5.94789 16.8535 44 8 -6 4-13.4742 22.3846 44 -8 -6 -4 27.5575 25.8240 21 8 7 -4 27.4983 19.0866 57 8 -7 -4 22.6147 21.1929 27 -8 -7 4 21.7838 22.4954 9 8 -7 -4-5.98373 19.8823 45 8 -7 -3 4742.69 203.553 45 8 7 -3 4982.48 201.529 57 -8 -7 3 4922.59 200.334 9 8 -7 -3 4938.17 202.988 27 8 -7 -2 437.445 62.2014 45 8 7 -2 451.144 59.4309 57 8 7 -2 408.459 55.8892 44 -8 -7 2 458.313 61.2542 9 8 -7 -2 566.669 66.6582 27 8 -7 -1 1335.57 106.201 45 8 7 -1 1500.45 109.201 44 8 7 -1 1539.79 107.234 57 -8 -7 1 1360.75 103.223 9 8 -7 -1 1608.14 113.147 27 8 7 0 50.6703 26.9257 57 8 7 0 20.1630 21.2988 44 8 -7 0 31.8281 22.9993 44 8 -7 0 62.3276 30.2457 45 -8 -7 0 6.34046 19.0634 9 8 -7 0 40.4010 25.2456 27 8 -7 1 38.3169 23.9455 45 8 7 1 64.2784 26.1870 57 -8 -7 -1 5.81884 18.4441 9 8 7 1 39.1029 23.5481 44 8 -7 1 58.1935 25.9174 44 8 7 2 343.045 50.3908 44 8 -7 2 268.571 44.5935 44 9 0 -6-5.12355 14.5179 52 9 0 -5 123.766 30.4361 52 9 0 -4-24.8061 26.3597 57 9 0 -4-5.91551 16.7643 52 9 0 -3 452.374 62.9387 57 9 0 -3 466.399 57.4619 52 9 0 -1 4900.18 210.512 57 9 0 -1 4389.78 198.958 44 9 0 0-7.21164 19.1149 44 9 0 1 360.696 55.7668 57 9 0 1 458.452 63.0039 44 -9 0 -2-19.1460 23.0519 21 9 0 2 20.4541 20.4908 44 9 0 3 37.0731 24.7692 44 9 1 -6 1070.04 79.1263 52 9 -1 -6 996.113 76.6252 52 9 1 -5-11.1031 16.6846 52 9 -1 -5 5.45854 14.4680 52 9 1 -4 462.273 59.0949 57 9 -1 -4 424.999 57.0767 57 9 1 -4 530.039 61.0831 52 9 -1 -4 477.429 56.7539 52 9 1 -3 1160.84 95.7477 57 9 -1 -3 1053.17 91.6156 57 9 1 -3 983.584 84.2271 52 9 -1 -3 1041.38 84.4965 52 9 -1 -2 359.628 56.6545 57 9 1 -2 270.459 45.3191 52 9 1 -1 6.96461 30.4128 57 9 -1 -1-6.95091 26.0550 57 9 1 -1 13.7742 20.6990 44 9 -1 -1 20.3123 23.4972 44 9 1 0 376.919 57.4269 57 9 -1 0 443.350 61.8753 57 9 -1 0 549.046 68.5155 44 9 1 0 469.046 64.2248 44 9 1 1 330.715 54.7881 44 9 -1 1 259.381 49.3666 44 9 1 1 210.970 43.7461 57 9 -1 1 204.288 43.2022 57 -9 -1 -1 252.355 50.7622 21 -9 -1 -2 52.1433 26.9396 21 9 1 2 60.0217 28.3617 44 9 -1 2 46.9496 24.2454 44 9 1 3 282.151 45.8076 44 9 -1 3 389.275 53.1169 44 9 2 -5 10.4478 15.7009 52 9 -2 -5 10.0596 15.1177 52 9 2 -4 89.7762 26.9869 52 9 -2 -4 41.6359 20.2320 52 9 2 -4 97.1443 29.2169 57 9 2 -3 150.125 33.8104 52 9 2 -3 131.656 35.0476 57 9 -2 -3 99.9343 33.7774 57 9 2 -2 51.3735 21.4149 52 9 2 -2 45.9392 26.3131 57 9 -2 -2 45.7634 25.3811 57 9 2 -1 2436.55 138.231 44 9 2 -1 2618.67 143.760 57 9 -2 -1 2436.98 139.388 57 -9 -2 1 2139.64 138.716 21 9 2 0 800.598 79.0682 44 9 -2 0 667.218 73.3267 44 9 2 0 699.327 74.5640 57 9 -2 0 677.151 72.0356 57 -9 -2 0 640.076 74.5881 21 9 2 1 1412.65 105.618 44 9 -2 1 1088.35 93.1764 44 9 2 1 1152.29 89.7909 57 -9 -2 -1 1331.07 103.545 21 -9 -2 -2 37.5639 25.8604 21 9 2 2 6.23584 17.6705 44 9 -2 2 6.27981 15.4114 44 9 3 -4 725.591 66.2715 52 9 3 -3 299.331 46.3740 57 9 -3 -3 374.679 52.5730 45 -9 -3 2 1977.33 121.689 21 9 -3 -2 2267.43 133.389 45 9 3 -2 2221.74 125.330 57 9 3 -1 11.7945 19.5972 44 -9 -3 1 31.6101 24.5314 21 9 -3 -1 39.1074 25.2914 45 9 3 -1 5.96803 19.8323 57 9 3 0 424.802 55.5936 44 9 -3 0 386.731 52.4179 44 -9 -3 0 349.533 52.6843 21 9 3 0 480.257 57.2264 57 9 -3 0 474.999 60.2276 45 9 3 1 29.7135 19.7527 44 0 0 0 0.00 0.00 0 TITL exp_733 CELL 1.54184 7.558550 12.166744 16.004672 90.0000 94.7152 90.0000 ZERR 6.00 0.000083 0.000129 0.000171 0.0000 0.0010 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O UNIT 66.00 60.00 6.00 6.00 TREF HKLF 4 END ; _shelx_hkl_checksum 63813 _shelx_res_file ; TITL exp_733_y2_znast_y3_a.res in P2(1)/n 733.res created by SHELXL-2019/2 at 23:04:53 on 10-Apr-2024 REM Old TITL exp_733_Y2_Znast_Y3 in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.110, Rweak 0.008, Alpha 0.031 REM 0.703 for 72 systematic absences, Orientation as input REM Formula found by SHELXT: C14 N O6 Cl CELL 1.54184 7.55855 12.166744 16.004672 90 94.7152 90 ZERR 2 0.000083 0.000129 0.000171 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O S UNIT 56 60 4 24 4 EQIV $1 0.5-X,0.5+Y,0.5-Z EQIV $2 0.5-X,-0.5+Y,0.5-Z EQIV $3 -1+X,+Y,+Z EQIV $4 1-X,1-Y,-Z EQIV $5 0.5+X,1.5-Y,-0.5+Z DFIX 0.86 0.01 N1 H1a DFIX 0.82 0.01 O1 H1 L.S. 4 PLAN 5 SIZE 0.32 0.3 0.28 TEMP 18 CONF HTAB C12 O2 HTAB C12 O3 HTAB C14 O1_$3 HTAB O1 O1W HTAB N1 O2W HTAB C4 O4_$4 HTAB C6 O3_$5 HTAB O1W O2 HTAB O1W O4_$2 HTAB O2W O2_$1 HTAB O2W O3 BOND LIST 4 MORE -1 BOND $H fmap 2 acta NOHKL REM REM REM WGHT 0.050100 0.303000 EXTI 0.002333 FVAR 5.01691 S1 5 0.126587 0.523662 0.298174 11.00000 0.04245 0.03805 = 0.02794 -0.00284 0.01084 -0.00473 O2 4 0.162572 0.408397 0.283878 11.00000 0.06338 0.04156 = 0.05987 -0.01350 0.02424 -0.00363 O3 4 0.286366 0.584611 0.323845 11.00000 0.04708 0.05402 = 0.03603 -0.00210 0.01422 -0.01400 O4 4 0.022393 0.574225 0.228747 11.00000 0.05841 0.07063 = 0.02907 0.00665 0.00781 -0.00197 C10 1 -0.009527 0.526072 0.384190 11.00000 0.03561 0.03080 = 0.02893 0.00007 0.00743 -0.00244 C11 1 0.059151 0.497555 0.467379 11.00000 0.03123 0.02846 = 0.02995 0.00018 0.00658 -0.00176 C12 1 0.238455 0.465557 0.487728 11.00000 0.03168 0.03930 = 0.03556 0.00264 0.01024 0.00176 AFIX 43 H12 2 0.315658 0.460895 0.445520 11.00000 -1.20000 AFIX 0 C13 1 0.298602 0.441650 0.568215 11.00000 0.03068 0.04888 = 0.04277 0.00539 0.00471 0.00523 AFIX 43 H13 2 0.417007 0.422577 0.580589 11.00000 -1.20000 AFIX 0 C14 1 -0.183132 0.554462 0.367088 11.00000 0.03851 0.04419 = 0.03088 0.00434 0.00213 0.00044 AFIX 43 H14 2 -0.225612 0.571361 0.312413 11.00000 -1.20000 AFIX 0 O1 4 0.604961 0.472096 0.188298 11.00000 0.07850 0.04596 = 0.03878 0.00567 0.01589 -0.00954 N1 3 0.684754 0.647736 0.098158 11.00000 0.04833 0.04031 = 0.03605 0.00424 0.00406 -0.00236 C1 1 0.662410 0.451789 0.112582 11.00000 0.04431 0.04368 = 0.03454 0.00493 0.00172 -0.00274 C2 1 0.682719 0.350028 0.078291 11.00000 0.05713 0.04074 = 0.05179 0.00594 0.00260 -0.00188 AFIX 43 H2 2 0.659051 0.287453 0.108831 11.00000 -1.20000 AFIX 0 C3 1 0.739220 0.339520 -0.002929 11.00000 0.06605 0.04736 = 0.05552 -0.00757 0.00562 0.00662 AFIX 43 H3 2 0.750754 0.269640 -0.025395 11.00000 -1.20000 AFIX 0 C4 1 0.777393 0.428433 -0.049459 11.00000 0.05989 0.06134 = 0.04094 -0.00434 0.00916 0.00706 AFIX 43 H4 2 0.814252 0.419332 -0.103052 11.00000 -1.20000 AFIX 0 C5 1 0.798111 0.631847 -0.058804 11.00000 0.05247 0.06492 = 0.03977 0.01359 0.01039 0.00067 AFIX 43 H5 2 0.836512 0.627362 -0.112434 11.00000 -1.20000 AFIX 0 C6 1 0.779057 0.732090 -0.023205 11.00000 0.05822 0.05319 = 0.05431 0.02099 0.00905 -0.00498 AFIX 43 H6 2 0.804189 0.795738 -0.052154 11.00000 -1.20000 AFIX 0 C7 1 0.721389 0.738486 0.057232 11.00000 0.05696 0.03956 = 0.05319 0.00763 0.00325 -0.00284 AFIX 43 H7 2 0.708614 0.806722 0.082224 11.00000 -1.20000 AFIX 0 C8 1 0.702894 0.545486 0.065438 11.00000 0.03702 0.04127 = 0.03210 0.00294 0.00002 -0.00181 C9 1 0.760684 0.534609 -0.015854 11.00000 0.04002 0.05332 = 0.03442 0.00457 0.00333 0.00133 AFIX 6 O1W 4 0.499487 0.310228 0.282094 11.00000 0.06474 0.05289 = 0.07219 0.01309 0.01713 0.00033 H1WA 2 0.392446 0.331508 0.282471 11.00000 -1.50000 H1WB 2 0.491769 0.242369 0.269682 11.00000 -1.50000 AFIX 6 O2W 4 0.535704 0.712601 0.240168 11.00000 0.06287 0.04512 = 0.06184 0.00692 0.02362 0.00573 H2WA 2 0.480634 0.773241 0.233271 11.00000 -1.50000 H2WB 2 0.460317 0.669091 0.258790 11.00000 -1.50000 AFIX 0 H1A 2 0.643238 0.656211 0.146739 11.00000 0.06865 H1 2 0.580521 0.414686 0.211415 11.00000 0.08550 HKLF 4 REM exp_733_y2_znast_y3_a.res in P2(1)/n REM wR2 = 0.0886, GooF = S = 1.054, Restrained GooF = 1.053 for all data REM R1 = 0.0307 for 2621 Fo > 4sig(Fo) and 0.0328 for all 2841 data REM 214 parameters refined using 2 restraints END WGHT 0.0501 0.3030 REM Highest difference peak 0.199, deepest hole -0.295, 1-sigma level 0.038 Q1 1 0.0000 0.5000 0.5000 10.50000 0.05 0.20 Q2 1 0.0357 0.5037 0.2258 11.00000 0.05 0.19 Q3 1 0.4506 0.7107 0.1981 11.00000 0.05 0.18 Q4 1 0.2862 0.5215 0.3228 11.00000 0.05 0.18 Q5 1 0.0182 0.5085 0.4246 11.00000 0.05 0.18 ; _shelx_res_checksum 25682 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S S1 0.12659(4) 0.52366(3) 0.29817(2) 0.03571(13) Uani d 1 . . O O2 0.16257(16) 0.40840(9) 0.28388(7) 0.0539(3) Uani d 1 . . O O3 0.28637(14) 0.58461(9) 0.32385(6) 0.0451(3) Uani d 1 . . O O4 0.02239(15) 0.57423(10) 0.22875(6) 0.0525(3) Uani d 1 . . C C10 -0.00953(17) 0.52607(10) 0.38419(8) 0.0315(3) Uani d 1 . . C C11 0.05915(16) 0.49755(10) 0.46738(8) 0.0297(3) Uani d 1 . . C C12 0.23846(17) 0.46556(11) 0.48773(9) 0.0351(3) Uani d 1 . . H H12 0.315658 0.460895 0.445520 0.042 Uiso calc 1 . . C C13 0.29860(18) 0.44165(13) 0.56821(9) 0.0407(3) Uani d 1 . . H H13 0.417007 0.422577 0.580589 0.049 Uiso calc 1 . . C C14 -0.18313(18) 0.55446(12) 0.36709(9) 0.0379(3) Uani d 1 . . H H14 -0.225612 0.571361 0.312413 0.045 Uiso calc 1 . . O O1 0.60496(18) 0.47210(9) 0.18830(7) 0.0538(3) Uani d 1 . . N N1 0.68475(17) 0.64774(10) 0.09816(8) 0.0415(3) Uani d 1 . . C C1 0.6624(2) 0.45179(12) 0.11258(9) 0.0409(3) Uani d 1 . . C C2 0.6827(2) 0.35003(13) 0.07829(10) 0.0500(4) Uani d 1 . . H H2 0.659051 0.287453 0.108831 0.060 Uiso calc 1 . . C C3 0.7392(2) 0.33952(15) -0.00293(11) 0.0563(4) Uani d 1 . . H H3 0.750754 0.269640 -0.025395 0.068 Uiso calc 1 . . C C4 0.7774(2) 0.42843(15) -0.04946(10) 0.0538(4) Uani d 1 . . H H4 0.814252 0.419332 -0.103052 0.065 Uiso calc 1 . . C C5 0.7981(2) 0.63185(15) -0.05880(10) 0.0520(4) Uani d 1 . . H H5 0.836512 0.627362 -0.112434 0.062 Uiso calc 1 . . C C6 0.7791(2) 0.73209(15) -0.02321(11) 0.0550(4) Uani d 1 . . H H6 0.804189 0.795738 -0.052154 0.066 Uiso calc 1 . . C C7 0.7214(2) 0.73849(13) 0.05723(11) 0.0500(4) Uani d 1 . . H H7 0.708614 0.806722 0.082224 0.060 Uiso calc 1 . . C C8 0.70289(18) 0.54549(12) 0.06544(9) 0.0370(3) Uani d 1 . . C C9 0.7607(2) 0.53461(13) -0.01585(9) 0.0426(3) Uani d 1 . . O O1W 0.49949(17) 0.31023(10) 0.28209(9) 0.0626(3) Uani d 1 . . H H1WA 0.392446 0.331508 0.282471 0.094 Uiso d 1 . . H H1WB 0.491769 0.242369 0.269682 0.094 Uiso d 1 . . O O2W 0.53570(16) 0.71260(10) 0.24017(8) 0.0556(3) Uani d 1 . . H H2WA 0.480634 0.773241 0.233271 0.083 Uiso d 1 . . H H2WB 0.460317 0.669091 0.258790 0.083 Uiso d 1 . . H H1A 0.643(3) 0.6562(18) 0.1467(8) 0.069(6) Uiso d 1 . . H H1 0.581(3) 0.4147(13) 0.2114(14) 0.086(7) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.0424(2) 0.0381(2) 0.02794(19) -0.00473(12) 0.01084(14) -0.00284(12) O2 0.0634(7) 0.0416(6) 0.0599(7) -0.0036(5) 0.0242(6) -0.0135(5) O3 0.0471(6) 0.0540(6) 0.0360(5) -0.0140(5) 0.0142(4) -0.0021(4) O4 0.0584(7) 0.0706(8) 0.0291(5) -0.0020(5) 0.0078(5) 0.0066(5) C10 0.0356(7) 0.0308(6) 0.0289(6) -0.0024(5) 0.0074(5) 0.0001(5) C11 0.0312(6) 0.0285(6) 0.0300(6) -0.0018(5) 0.0066(5) 0.0002(5) C12 0.0317(7) 0.0393(7) 0.0356(7) 0.0018(5) 0.0102(5) 0.0026(5) C13 0.0307(7) 0.0489(8) 0.0428(8) 0.0052(6) 0.0047(6) 0.0054(6) C14 0.0385(7) 0.0442(8) 0.0309(7) 0.0004(6) 0.0021(5) 0.0043(5) O1 0.0785(8) 0.0460(7) 0.0388(6) -0.0095(6) 0.0159(6) 0.0057(5) N1 0.0483(7) 0.0403(6) 0.0360(6) -0.0024(5) 0.0041(5) 0.0042(5) C1 0.0443(8) 0.0437(8) 0.0345(7) -0.0027(6) 0.0017(6) 0.0049(6) C2 0.0571(9) 0.0407(8) 0.0518(9) -0.0019(7) 0.0026(7) 0.0059(7) C3 0.0661(10) 0.0474(9) 0.0555(10) 0.0066(8) 0.0056(8) -0.0076(7) C4 0.0599(10) 0.0613(10) 0.0409(8) 0.0071(8) 0.0092(7) -0.0043(7) C5 0.0525(9) 0.0649(11) 0.0398(8) 0.0007(7) 0.0104(7) 0.0136(7) C6 0.0582(10) 0.0532(10) 0.0543(10) -0.0050(8) 0.0090(8) 0.0210(8) C7 0.0570(9) 0.0396(8) 0.0532(9) -0.0028(7) 0.0033(7) 0.0076(7) C8 0.0370(7) 0.0413(7) 0.0321(7) -0.0018(5) 0.0000(5) 0.0029(5) C9 0.0400(7) 0.0533(9) 0.0344(7) 0.0013(6) 0.0033(6) 0.0046(6) O1W 0.0647(8) 0.0529(7) 0.0722(8) 0.0003(6) 0.0171(7) 0.0131(6) O2W 0.0629(7) 0.0451(6) 0.0618(7) 0.0057(5) 0.0236(6) 0.0069(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O2 S1 C10 . . 105.37(6) ? O3 S1 O2 . . 112.16(7) ? O3 S1 C10 . . 107.03(6) ? O4 S1 O2 . . 112.81(7) ? O4 S1 O3 . . 112.91(7) ? O4 S1 C10 . . 105.88(6) ? C11 C10 S1 . . 121.69(10) ? C14 C10 S1 . . 117.11(10) ? C14 C10 C11 . . 121.19(12) ? C11 C11 C10 3_566 . 117.91(14) ? C12 C11 C10 . . 123.05(12) ? C12 C11 C11 . 3_566 119.03(14) ? C11 C12 H12 . . 119.6 ? C13 C12 C11 . . 120.86(12) ? C13 C12 H12 . . 119.6 ? C12 C13 H13 . . 119.7 ? C12 C13 C14 . 3_566 120.62(13) ? C14 C13 H13 3_566 . 119.7 ? C10 C14 C13 . 3_566 120.36(13) ? C10 C14 H14 . . 119.8 ? C13 C14 H14 3_566 . 119.8 ? C1 O1 H1 . . 110.6(17) ? C7 N1 C8 . . 122.67(13) ? C7 N1 H1A . . 116.7(15) ? C8 N1 H1A . . 120.6(15) ? O1 C1 C2 . . 125.70(14) ? O1 C1 C8 . . 115.67(13) ? C2 C1 C8 . . 118.63(14) ? C1 C2 H2 . . 119.8 ? C1 C2 C3 . . 120.36(15) ? C3 C2 H2 . . 119.8 ? C2 C3 H3 . . 119.0 ? C4 C3 C2 . . 121.91(16) ? C4 C3 H3 . . 119.0 ? C3 C4 H4 . . 120.3 ? C3 C4 C9 . . 119.43(15) ? C9 C4 H4 . . 120.3 ? C6 C5 H5 . . 119.4 ? C6 C5 C9 . . 121.12(15) ? C9 C5 H5 . . 119.4 ? C5 C6 H6 . . 120.4 ? C5 C6 C7 . . 119.28(15) ? C7 C6 H6 . . 120.4 ? N1 C7 C6 . . 120.25(15) ? N1 C7 H7 . . 119.9 ? C6 C7 H7 . . 119.9 ? N1 C8 C1 . . 119.89(13) ? N1 C8 C9 . . 119.25(13) ? C9 C8 C1 . . 120.85(14) ? C4 C9 C8 . . 118.80(14) ? C5 C9 C4 . . 123.77(15) ? C5 C9 C8 . . 117.43(14) ? H1WA O1W H1WB . . 104.5 ? H2WA O2W H2WB . . 104.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag S1 O2 . 1.4503(11) ? S1 O3 . 1.4476(10) ? S1 O4 . 1.4455(11) ? S1 C10 . 1.7853(13) ? C10 C11 . 1.4314(18) ? C10 C14 . 1.3627(19) ? C11 C11 3_566 1.431(2) ? C11 C12 . 1.4219(18) ? C12 H12 . 0.9300 ? C12 C13 . 1.362(2) ? C13 H13 . 0.9300 ? C13 C14 3_566 1.409(2) ? C14 H14 . 0.9300 ? O1 C1 . 1.3433(19) ? O1 H1 . 0.819(10) ? N1 C7 . 1.3246(19) ? N1 C8 . 1.3611(19) ? N1 H1A . 0.868(9) ? C1 C2 . 1.368(2) ? C1 C8 . 1.414(2) ? C2 H2 . 0.9300 ? C2 C3 . 1.407(2) ? C3 H3 . 0.9300 ? C3 C4 . 1.358(3) ? C4 H4 . 0.9300 ? C4 C9 . 1.409(2) ? C5 H5 . 0.9300 ? C5 C6 . 1.359(3) ? C5 C9 . 1.409(2) ? C6 H6 . 0.9300 ? C6 C7 . 1.395(2) ? C7 H7 . 0.9300 ? C8 C9 . 1.412(2) ? O1W H1WA . 0.8500 ? O1W H1WB . 0.8501 ? O2W H2WA . 0.8498 ? O2W H2WB . 0.8495 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O2W H2WA O2 2 0.85 1.98 2.8239(16) 176 yes O2W H2WB O3 . 0.85 2.02 2.8610(15) 168 yes O1W H1WA O2 . 0.85 1.98 2.8150(17) 169 yes O1W H1WB O4 2_545 0.85 2.05 2.8806(18) 166 yes O1 H1 O1W . 0.819(10) 1.840(12) 2.6390(16) 165(2) yes N1 H1A O2W . 0.868(9) 1.889(11) 2.7347(18) 164(2) yes C6 H6 O3 4_675 0.93 2.46 3.3153(19) 154 yes C4 H4 O4 3_665 0.93 2.45 3.352(2) 165 yes C14 H14 O1 1_455 0.93 2.57 3.3173(18) 137 yes C12 H12 O3 . 0.93 2.46 3.0439(17) 121 yes C7 H7 Cg1 2_555 0.93 2.82 3.6125(17) 144 yes C7 H7 Cg2 4_675 0.93 2.82 3.6125(17) 144 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag S1 C10 C11 C11 . . . 3_566 179.61(12) ? S1 C10 C11 C12 . . . . 0.00(18) ? S1 C10 C14 C13 . . . 3_566 -179.89(11) ? O2 S1 C10 C11 . . . . 69.66(12) ? O2 S1 C10 C14 . . . . -109.23(12) ? O3 S1 C10 C11 . . . . -49.90(12) ? O3 S1 C10 C14 . . . . 131.21(11) ? O4 S1 C10 C11 . . . . -170.60(10) ? O4 S1 C10 C14 . . . . 10.52(13) ? C10 C11 C12 C13 . . . . 178.45(13) ? C11 C10 C14 C13 . . . 3_566 1.2(2) ? C11 C11 C12 C13 3_566 . . . -1.1(2) ? C11 C12 C13 C14 . . . 3_566 1.5(2) ? C14 C10 C11 C11 . . . 3_566 -1.6(2) ? C14 C10 C11 C12 . . . . 178.84(13) ? O1 C1 C2 C3 . . . . 178.11(15) ? O1 C1 C8 N1 . . . . 0.9(2) ? O1 C1 C8 C9 . . . . -178.57(13) ? N1 C8 C9 C4 . . . . -179.40(14) ? N1 C8 C9 C5 . . . . 0.5(2) ? C1 C2 C3 C4 . . . . 0.8(3) ? C1 C8 C9 C4 . . . . 0.0(2) ? C1 C8 C9 C5 . . . . 179.91(14) ? C2 C1 C8 N1 . . . . -179.68(14) ? C2 C1 C8 C9 . . . . 0.9(2) ? C2 C3 C4 C9 . . . . 0.1(3) ? C3 C4 C9 C5 . . . . 179.58(16) ? C3 C4 C9 C8 . . . . -0.5(2) ? C5 C6 C7 N1 . . . . -0.4(3) ? C6 C5 C9 C4 . . . . 179.83(16) ? C6 C5 C9 C8 . . . . 0.0(2) ? C7 N1 C8 C1 . . . . 179.67(14) ? C7 N1 C8 C9 . . . . -0.9(2) ? C8 N1 C7 C6 . . . . 0.8(2) ? C8 C1 C2 C3 . . . . -1.3(2) ? C9 C5 C6 C7 . . . . 0.0(3) ?