#------------------------------------------------------------------------------ #$Date: 2024-08-05 21:11:07 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293772 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/19/1571950.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571950 loop_ _publ_author_name 'Arnold, Robert E.' 'Saska, Jan' 'Mesquita-Ribeiro, Raquel' 'Dajas-Bailador, Federico' 'Taylor, Laurence' 'Lewis, William' 'Argent, Stephen' 'Shao, Huiling' 'Houk, Kendall N.' 'Denton, Ross M.' _publ_section_title ; Total synthesis, biological evaluation and biosynthetic re-evaluation of Illicium-derived neolignans. ; _journal_issue 30 _journal_name_full 'Chemical science' _journal_page_first 11783 _journal_page_last 11793 _journal_paper_doi 10.1039/d4sc03232b _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C27 H26 O3' _chemical_formula_sum 'C27 H26 O3' _chemical_formula_weight 398.48 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary iterative _atom_sites_solution_secondary difmap _audit_creation_date 2018-09-05 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-01-23 deposited with the CCDC. 2024-06-13 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 102.695(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.6576(9) _cell_length_b 11.7041(5) _cell_length_c 10.0865(3) _cell_measurement_reflns_used 3332 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 73.7140 _cell_measurement_theta_min 4.4780 _cell_volume 2148.75(16) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_environment 'N2 gas' _diffrn_ambient_temperature 120(2) _diffrn_crystal_treatment 'flash frozen in gaseous N2' _diffrn_detector 'CCD area detector' _diffrn_detector_area_resol_mean 4.2207 _diffrn_detector_type 'Agilent Diffraction Titan S2 detector' _diffrn_measured_fraction_theta_full 0.979 _diffrn_measured_fraction_theta_max 0.949 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -113.00 -25.00 1.00 20.00 -- -42.81 -38.00 30.00 88 2 \w -49.00 -22.00 1.00 20.00 -- -42.81 38.00-180.00 27 3 \w -92.00 -2.00 1.00 20.00 -- -42.81 125.00-180.00 90 4 \w 94.00 170.00 1.00 80.00 -- 103.32 125.00-150.00 76 5 \w 143.00 175.00 1.00 80.00 -- 103.32 77.00 -90.00 32 6 \w 40.00 110.00 1.00 80.00 -- 103.32 -94.00-150.00 70 7 \w 88.00 117.00 1.00 80.00 -- 103.32-125.00 60.00 29 8 \w 32.00 63.00 1.00 80.00 -- 103.32-125.00 60.00 31 9 \w 43.00 87.00 1.00 80.00 -- 103.32 -45.00-180.00 44 10 \w 74.00 127.00 1.00 80.00 -- 103.32 77.00 -90.00 53 11 \w 54.00 84.00 1.00 80.00 -- 103.32 -94.00 150.00 30 12 \w 31.00 97.00 1.00 80.00 -- 103.32 0.00 60.00 66 ; _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'SuperNova, Titan S2' _diffrn_measurement_method '\w scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0074255000 _diffrn_orient_matrix_UB_12 -0.1310418000 _diffrn_orient_matrix_UB_13 -0.0019116000 _diffrn_orient_matrix_UB_21 -0.0841561000 _diffrn_orient_matrix_UB_22 -0.0111960000 _diffrn_orient_matrix_UB_23 -0.0444180000 _diffrn_orient_matrix_UB_31 0.0053994000 _diffrn_orient_matrix_UB_32 0.0050157000 _diffrn_orient_matrix_UB_33 -0.1501017000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0423 _diffrn_reflns_av_unetI/netI 0.0505 _diffrn_reflns_Laue_measured_fraction_full 0.979 _diffrn_reflns_Laue_measured_fraction_max 0.949 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 7 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 8284 _diffrn_reflns_point_group_measured_fraction_full 0.979 _diffrn_reflns_point_group_measured_fraction_max 0.949 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.821 _diffrn_reflns_theta_min 2.427 _diffrn_source 'microfocus sealed tube' _diffrn_source_type 'Agilent Diffraction microfocus tube' _exptl_absorpt_coefficient_mu 0.625 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.745 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.232 _exptl_crystal_description needle _exptl_crystal_F_000 848 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: diethyl ether, pentane' _exptl_crystal_size_max 0.402 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.026 _refine_diff_density_max 0.400 _refine_diff_density_min -0.351 _refine_diff_density_rms 0.065 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.133 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 331 _refine_ls_number_reflns 4132 _refine_ls_number_restraints 180 _refine_ls_restrained_S_all 1.155 _refine_ls_R_factor_all 0.0934 _refine_ls_R_factor_gt 0.0584 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0828P)^2^+1.5833P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1526 _refine_ls_wR_factor_ref 0.2029 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2758 _reflns_number_total 4132 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03232b2.cif _cod_data_source_block 3-simonsol-F _cod_depositor_comments 'Adding full bibliography for 1571943--1571950.cif.' _cod_original_cell_volume 2148.74(16) _cod_database_code 1571950 _nottingham_internal_coll_name REARDI _nottingham_internal_coll_number 17626 _nottingham_internal_coll_client REA/RD _nottingham_internal_coll_type custom _nottingham_internal_coll_frame_method '\w scans' _nottingham_internal_coll_frame_time '20.00, 80.00' _nottingham_internal_coll_frame_width 1.00 _nottingham_internal_coll_user pczwl _nottingham_internal_coll_date 10/04/2018 _nottingham_internal_coll_location NOTTS _nottingham_internal_coll_instrument 'GVA, PL13110002' _nottingham_internal_process_date 12/04/2018 _nottingham_internal_process_user pczwl _nottingham_internal_solution_date 25/4/2018 _nottingham_internal_solution_user pczwl _nottingham_internal_refinement_date 25/4/2018 _nottingham_internal_refinement_user pczwl _nottingham_internal_validation_date 7/6/2018 _nottingham_internal_validation_user pczwl _nottingham_internal_archive_date 7/6/2018 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C27 H26 O3' _chemical_oxdiff_usercomment 'REARDI #17626 GVA-1420 IN FOMBLIN FILM ON A MICROMOUNT FOR REA/RD' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.984 _shelx_estimated_absorpt_t_min 0.787 _reflns_odcompleteness_completeness 97.88 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 67.13 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups At 1.5 times of: All O(H) groups 2. Restrained distances C22-C21 \\sim C22A-C21 \\sim C26-C25 \\sim C29-C28 \\sim C28-C29A \\sim C25-C26A with sigma of 0.02 C27-C26 \\sim C30A-C29A \\sim C30-C29 \\sim C23A-C22A \\sim C23-C22 \\sim C26A-C27A with sigma of 0.02 3. Uiso/Uaniso restraints and constraints C25 \\sim C26 \\sim C26A \\sim C27 \\sim C27A \\sim C28 \\sim C29 \\sim C29A \\sim C30 \\sim C30A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 4. Rigid body (RIGU) restrains C21, C22, C22A, C23, C23A, C25, C26, C26A, C27, C27A, C28, C29, C29A, C30, C30A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Sof(H28D)=Sof(H28C)=Sof(C29A)=Sof(H29A)=Sof(C30A)=Sof(H30C)=Sof(H30D)=1-FVAR(1) Sof(H28a)=Sof(H28b)=Sof(C29)=Sof(H29)=Sof(C30)=Sof(H30a)=Sof(H30b)=FVAR(1) Sof(H21C)=Sof(H21D)=Sof(C22A)=Sof(H22A)=Sof(C23A)=Sof(H23C)=Sof(H23D)=1-FVAR(2) Sof(H21a)=Sof(H21b)=Sof(C22)=Sof(H22)=Sof(C23)=Sof(H23a)=Sof(H23b)=FVAR(2) Sof(H25C)=Sof(H25D)=Sof(C26A)=Sof(H26A)=Sof(C27A)=Sof(H27C)=Sof(H27D)=1-FVAR(3) Sof(H25a)=Sof(H25b)=Sof(C26)=Sof(H26)=Sof(C27)=Sof(H27a)=Sof(H27b)=FVAR(3) 6.a Ternary CH refined with riding coordinates: C13(H13) 6.b Secondary CH2 refined with riding coordinates: C1(H1a,H1b), C21(H21a,H21b), C21(H21C,H21D), C25(H25a,H25b), C25(H25C,H25D), C28(H28a,H28b), C28(H28D,H28C) 6.c Aromatic/amide H refined with riding coordinates: C4(H4), C7(H7), C9(H9), C10(H10), C16(H16), C18(H18), C19(H19), C22(H22), C22A(H22A), C26(H26), C26A(H26A), C29(H29), C29A(H29A) 6.d X=CH2 refined with riding coordinates: C23(H23a,H23b), C23A(H23C,H23D), C27(H27a,H27b), C27A(H27C,H27D), C30(H30a, H30b), C30A(H30C,H30D) ; _shelx_res_file ; TITL reardi.res created by SHELXL-2018/3 at 10:45:38 on 07-Jun-2018 CELL 1.54184 18.657562 11.704094 10.086468 90 102.6946 90 ZERR 4 0.000949 0.000473 0.00034 0 0.0041 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H O UNIT 108 104 12 SADI C22 C21 C22A C21 C26 C25 C29 C28 C28 C29A C25 C26A SADI C27 C26 C30A C29A C30 C29 C23A C22A C23 C22 C26A C27A SIMU 0.01 0.02 2 C25 > C30A RIGU C21 > C23A C25 > C30A L.S. 12 0 0 PLAN 20 SIZE 0.026 0.05 0.402 TEMP -153(2) HTAB O24 O14 bond $h conf htab more -1 fmap 2 53 acta OMIT 15 5 0 REM REM REM WGHT 0.082800 1.583300 FVAR 1.70515 0.80579 0.72314 0.42542 C1 1 0.637042 0.460452 0.541758 11.00000 0.03657 0.03434 = 0.03291 -0.00067 0.00570 0.00978 AFIX 23 H1A 2 0.612506 0.525683 0.575875 11.00000 -1.20000 H1B 2 0.626167 0.465383 0.441338 11.00000 -1.20000 AFIX 0 C2 1 0.605649 0.351782 0.582010 11.00000 0.03660 0.04030 = 0.02222 -0.00428 0.00490 0.00337 C3 1 0.650198 0.245982 0.589107 11.00000 0.03264 0.03340 = 0.02232 -0.00049 0.00467 0.00040 C4 1 0.722066 0.255328 0.584994 11.00000 0.03431 0.02725 = 0.02234 -0.00298 0.00565 0.00218 AFIX 43 H4 2 0.749181 0.186222 0.589189 11.00000 -1.20000 AFIX 0 C5 1 0.763138 0.364345 0.574442 11.00000 0.04754 0.02428 = 0.02463 -0.00029 0.00745 -0.00119 C6 1 0.824709 0.372644 0.700778 11.00000 0.04261 0.02650 = 0.02521 -0.00064 0.00924 -0.00627 C7 1 0.893510 0.320747 0.736916 11.00000 0.03983 0.03665 = 0.03083 -0.00490 0.00890 0.00157 AFIX 43 H7 2 0.910197 0.272323 0.674368 11.00000 -1.20000 AFIX 0 C8 1 0.937744 0.340466 0.865790 11.00000 0.03888 0.04291 = 0.03953 -0.00615 0.00281 0.00009 C9 1 0.910958 0.409896 0.956352 11.00000 0.04858 0.03871 = 0.02953 -0.00576 0.00161 -0.00638 AFIX 43 H9 2 0.940686 0.421844 1.044600 11.00000 -1.20000 AFIX 0 C10 1 0.842085 0.462638 0.922453 11.00000 0.04589 0.03183 = 0.03033 -0.00706 0.00767 -0.00498 AFIX 43 H10 2 0.824257 0.509284 0.985250 11.00000 -1.20000 AFIX 0 C11 1 0.801532 0.443124 0.792803 11.00000 0.04427 0.02410 = 0.02981 -0.00016 0.00765 -0.00349 O12 3 0.732997 0.488906 0.742229 11.00000 0.04810 0.03224 = 0.02754 -0.00587 0.00519 0.00373 C13 1 0.718519 0.470805 0.594751 11.00000 0.04739 0.02762 = 0.02513 -0.00054 0.00706 0.00078 AFIX 13 H13 2 0.737100 0.538007 0.551076 11.00000 -1.20000 AFIX 0 O14 3 0.543412 0.351224 0.606187 11.00000 0.04240 0.05207 = 0.04462 0.00056 0.01850 0.00952 C15 1 0.618159 0.130076 0.595665 11.00000 0.03037 0.03673 = 0.02705 0.00289 0.00149 -0.00308 C16 1 0.633676 0.044412 0.510580 11.00000 0.03174 0.03626 = 0.03278 0.00420 0.00382 -0.00398 AFIX 43 H16 2 0.661671 0.063302 0.445549 11.00000 -1.20000 AFIX 0 C17 1 0.609876 -0.068046 0.516693 11.00000 0.04194 0.03490 = 0.04049 0.00425 -0.00291 -0.00529 C18 1 0.568460 -0.094137 0.611297 11.00000 0.04690 0.04106 = 0.03917 0.01081 -0.00481 -0.01639 AFIX 43 H18 2 0.552360 -0.170419 0.618601 11.00000 -1.20000 AFIX 0 C19 1 0.550347 -0.010679 0.694947 11.00000 0.03897 0.05968 = 0.03270 0.01055 0.00209 -0.01662 AFIX 43 H19 2 0.521369 -0.030119 0.758184 11.00000 -1.20000 AFIX 0 C20 1 0.573829 0.101074 0.688005 11.00000 0.03884 0.05052 = 0.02444 0.00277 0.00159 -0.00788 C21 1 0.629258 -0.159334 0.425107 11.00000 0.05975 0.03099 = 0.06906 -0.00406 0.01129 -0.00822 PART 1 AFIX 23 H21A 2 0.637457 -0.124720 0.340114 31.00000 -1.20000 H21B 2 0.588691 -0.215328 0.401318 31.00000 -1.20000 AFIX 23 PART 0 PART 2 H21C 2 0.590117 -0.217234 0.420640 -31.00000 -1.20000 H21D 2 0.619233 -0.122869 0.334337 -31.00000 -1.20000 AFIX 0 PART 0 PART 1 C22 1 0.699204 -0.218642 0.501325 31.00000 0.05519 0.02464 = 0.04442 -0.00413 0.01191 -0.00495 AFIX 43 H22 2 0.699843 -0.248696 0.589069 31.00000 -1.20000 AFIX 0 PART 0 PART 2 C22A 1 0.695014 -0.226927 0.427852 -31.00000 0.07559 0.03044 = 0.06667 -0.00282 0.00923 -0.00093 AFIX 43 H22A 2 0.703642 -0.270151 0.353175 -31.00000 -1.20000 AFIX 0 PART 0 PART 1 C23 1 0.759210 -0.230591 0.451882 31.00000 0.06161 0.03200 = 0.06413 -0.00364 0.00739 0.00047 AFIX 93 H23A 2 0.760176 -0.201397 0.364409 31.00000 -1.20000 H23B 2 0.801128 -0.268325 0.504020 31.00000 -1.20000 AFIX 0 PART 0 PART 2 C23A 1 0.741267 -0.220543 0.547576 -31.00000 0.05568 0.04049 = 0.08434 -0.00229 0.00211 -0.01388 AFIX 93 H23C 2 0.729206 -0.175645 0.618058 -31.00000 -1.20000 H23D 2 0.786539 -0.260857 0.563056 -31.00000 -1.20000 AFIX 0 PART 0 O24 3 0.555301 0.177948 0.777826 11.00000 0.05510 0.05641 = 0.03334 0.00143 0.01598 -0.00275 H24 2 0.552442 0.244647 0.732371 11.00000 -1.50000 C25 1 0.786155 0.362368 0.436190 11.00000 0.04680 0.03417 = 0.02740 -0.00113 0.01398 -0.00029 PART 1 AFIX 23 H25A 2 0.818897 0.296114 0.434260 41.00000 -1.20000 H25B 2 0.741783 0.351704 0.362753 41.00000 -1.20000 AFIX 23 PART 0 PART 2 H25C 2 0.810090 0.288125 0.427308 -41.00000 -1.20000 H25D 2 0.741186 0.366416 0.362898 -41.00000 -1.20000 AFIX 0 PART 0 PART 1 C26 1 0.824290 0.467432 0.409061 41.00000 0.05446 0.03762 = 0.03781 0.00005 0.01691 0.00121 AFIX 43 H26 2 0.868999 0.489485 0.468549 41.00000 -1.20000 AFIX 0 PART 0 PART 2 C26A 1 0.837493 0.456734 0.413892 -41.00000 0.05765 0.03845 = 0.03946 -0.00134 0.03134 -0.00423 AFIX 43 H26A 2 0.881475 0.466486 0.481204 -41.00000 -1.20000 AFIX 0 PART 0 PART 1 C27 1 0.795790 0.531352 0.300744 41.00000 0.04082 0.04508 = 0.04415 0.00882 0.02776 -0.00240 AFIX 93 H27A 2 0.751077 0.509195 0.241343 41.00000 -1.20000 H27B 2 0.820215 0.599015 0.283033 41.00000 -1.20000 AFIX 0 PART 0 PART 2 C27A 1 0.826310 0.527329 0.307952 -41.00000 0.04627 0.05181 = 0.05347 0.00468 0.03411 -0.01323 AFIX 93 H27C 2 0.783037 0.520557 0.238291 -41.00000 -1.20000 H27D 2 0.861599 0.584509 0.301965 -41.00000 -1.20000 AFIX 0 PART 0 C28 1 1.013334 0.290320 0.905809 11.00000 0.04523 0.08013 = 0.05777 -0.02184 -0.00611 0.01898 PART 1 AFIX 23 H28A 2 1.047138 0.338385 0.866617 21.00000 -1.20000 H28B 2 1.029600 0.294604 1.005949 21.00000 -1.20000 AFIX 23 PART 0 PART 2 H28D 2 1.041578 0.343609 0.973969 -21.00000 -1.20000 H28C 2 1.007638 0.219266 0.955743 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C29 1 1.020577 0.174739 0.865056 21.00000 0.04142 0.05434 = 0.06555 0.00020 -0.00613 0.01325 AFIX 43 H29 2 0.990576 0.117849 0.892639 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C29A 1 1.060371 0.262028 0.820631 -21.00000 0.04818 0.06769 = 0.05917 -0.01174 0.00008 0.02360 AFIX 43 H29A 2 1.094217 0.311818 0.791932 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C30 1 1.070055 0.142075 0.786214 21.00000 0.06882 0.10865 = 0.05972 -0.02882 -0.02171 0.06837 AFIX 93 H30A 2 1.100544 0.197672 0.757597 21.00000 -1.20000 H30B 2 1.073198 0.064276 0.761242 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C30A 1 1.048787 0.149597 0.786135 -21.00000 0.06578 0.07815 = 0.07580 -0.02702 -0.01276 0.02358 AFIX 93 H30C 2 1.013518 0.106724 0.820227 -21.00000 -1.20000 H30D 2 1.076000 0.114288 0.728055 -21.00000 -1.20000 AFIX 0 HKLF 4 REM REM wR2 = 0.2029, GooF = S = 1.133, Restrained GooF = 1.155 for all data REM R1 = 0.0584 for 2758 Fo > 4sig(Fo) and 0.0934 for all 4132 data REM 331 parameters refined using 180 restraints END WGHT 0.0828 1.5833 REM Instructions for potential hydrogen bonds EQIV $1 x, -y+1/2, z-1/2 HTAB C1 O24_$1 EQIV $2 -x+1, y-1/2, -z+3/2 HTAB C19 O14_$2 HTAB O24 O14 REM Highest difference peak 0.400, deepest hole -0.351, 1-sigma level 0.065 Q1 1 0.8001 0.3644 0.6417 11.00000 0.05 0.40 Q2 1 0.9974 0.2175 0.9216 11.00000 0.05 0.33 Q3 1 0.9999 0.1457 0.9479 11.00000 0.05 0.27 Q4 1 0.8167 0.3911 0.7549 11.00000 0.05 0.27 Q5 1 0.7763 0.3652 0.5111 11.00000 0.05 0.26 Q6 1 0.7442 0.3114 0.5791 11.00000 0.05 0.26 Q7 1 0.5954 0.1220 0.6264 11.00000 0.05 0.25 Q8 1 1.0209 0.0820 0.8434 11.00000 0.05 0.24 Q9 1 0.7031 0.4745 0.6807 11.00000 0.05 0.24 Q10 1 0.6777 0.2543 0.5196 11.00000 0.05 0.24 Q11 1 0.7405 0.4082 0.5738 11.00000 0.05 0.23 Q12 1 0.8229 0.4608 0.8569 11.00000 0.05 0.22 Q13 1 0.9019 0.3164 0.6220 11.00000 0.05 0.21 Q14 1 0.6605 0.4579 0.7503 11.00000 0.05 0.21 Q15 1 0.8407 0.3594 0.6015 11.00000 0.05 0.21 Q16 1 0.8195 0.4841 1.0082 11.00000 0.05 0.20 Q17 1 0.7201 0.4223 0.7754 11.00000 0.05 0.20 Q18 1 0.8173 0.5041 0.7668 11.00000 0.05 0.20 Q19 1 0.5997 0.1606 0.8570 11.00000 0.05 0.19 Q20 1 0.5609 0.3369 0.5163 11.00000 0.05 0.19 ; _shelx_res_checksum 83570 _shelx_hkl_file ; -1 0 010814.60 54.66 2 -2 0 0 4247.78 48.86 2 -3 0 0 1106.46 33.00 2 -4 0 0 1242.62 41.22 2 -5 0 028511.74 203.65 2 -6 0 015093.76 165.50 2 -7 0 0 416.72 36.22 2 -8 0 0 392.90 38.69 2 8 0 0 407.46 54.67 1 9 0 0 1621.89 96.03 1 10 0 0 2602.55 124.55 1 11 0 024894.58 273.74 3 11 0 024158.58 389.94 1 12 0 0 1315.04 103.23 1 13 0 0 561.49 77.61 1 13 0 0 621.50 38.93 9 14 0 0 120.43 24.72 9 14 0 0 93.43 45.66 1 15 0 0 546.84 39.33 9 15 0 0 -2.36 27.19 10 17 0 0 26.86 30.72 10 -20 0 0 -2.35 17.53 4 -21 0 0 44.05 16.58 4 -22 0 0 1.44 12.66 4 0 1 0 4.59 10.16 1 1 1 027782.25 157.45 1 2 1 0 211.61 22.70 1 3 1 0 6113.82 100.13 1 4 1 014865.37 173.06 1 5 1 0 66.90 30.01 1 -6 1 0 1777.62 62.06 2 6 1 0 1879.95 81.25 1 7 1 0 142.62 40.21 1 -7 1 0 149.68 28.00 2 -8 1 0 5566.55 123.74 2 8 1 0 5639.65 158.31 1 9 1 0 94.71 38.97 1 -9 1 0 89.05 27.24 2 10 1 0 2511.48 122.67 1 10 -1 0 2511.79 72.83 3 -10 1 0 2550.11 96.96 2 -11 1 0 598.95 54.04 2 11 1 0 609.24 72.32 1 11 -1 0 557.25 69.57 1 12 1 0 774.16 83.82 1 12 -1 0 746.00 81.73 1 12 1 0 840.61 62.59 3 13 1 0 606.97 57.41 3 13 1 0 576.90 77.41 1 13 -1 0 707.06 41.67 9 13 1 0 698.04 41.43 9 13 -1 0 653.08 81.01 1 14 -1 0 64.75 22.36 9 14 -1 0 80.28 48.97 1 14 -1 0 -5.21 26.59 10 14 1 0 84.27 23.39 9 14 1 0 65.86 45.72 1 15 -1 0 20.41 28.15 10 15 1 0 113.23 25.70 9 16 1 0 13.67 20.23 9 16 1 0 -1.80 24.92 10 16 -1 0 -3.95 24.52 10 -20 1 0 10.58 16.35 4 -21 1 0 26.06 14.78 4 -21 -1 0 13.44 16.93 4 -22 -1 0 23.24 13.49 4 0 2 0 1342.59 47.72 1 1 2 0 2994.37 71.38 1 2 2 0 9376.26 127.82 1 3 2 017645.34 188.59 1 4 2 0 8672.33 146.53 1 5 2 0 4353.94 116.36 1 6 -2 0 752.89 19.18 3 6 2 0 782.96 60.48 1 7 -2 0 4.98 9.58 3 7 2 0 -10.31 33.41 1 8 2 0 27.61 36.20 1 9 2 0 6829.93 193.22 1 -9 2 0 6676.90 146.94 2 10 2 0 262.81 52.48 1 -10 2 0 264.85 39.08 2 -11 2 0 1455.13 81.46 2 11 2 0 1443.08 104.66 1 -12 2 0 -12.72 25.49 2 12 2 0 -12.67 37.72 1 13 -2 0 280.56 59.91 1 13 2 0 354.05 34.56 9 13 2 0 297.85 49.67 3 13 2 0 363.76 66.85 1 14 2 0 35.31 30.25 3 14 -2 0 40.42 45.94 1 14 2 0 7.59 42.63 1 14 2 0 15.93 21.98 9 14 -2 0 -12.13 25.08 10 15 2 0 12.30 19.69 9 15 -2 0 -4.71 24.81 10 17 -2 0 6.38 23.40 10 18 -2 0 24.16 23.05 10 -19 2 0 339.84 27.03 4 -21 -2 0 -0.44 16.48 4 -22 -2 0 91.41 16.63 4 0 3 0 10.97 27.17 1 1 3 027230.05 248.06 1 2 3 0 3666.94 98.23 1 -2 3 0 3481.54 44.35 3 3 3 0 1523.75 69.43 1 4 3 0 437.01 48.37 1 5 3 0 -5.75 31.50 1 6 3 0 2011.88 94.84 1 7 3 0 38.28 35.79 1 8 3 0 26.55 34.53 1 9 3 0 -17.69 40.22 1 -10 3 0 206.52 38.11 2 10 3 0 190.69 49.62 1 -11 3 0 63.46 23.13 2 11 3 0 135.48 49.55 1 -12 3 0 49.74 29.05 2 12 -3 0 -37.97 25.29 10 12 3 0 63.24 24.40 9 12 3 0 66.84 44.05 1 -13 3 0 190.33 42.74 2 13 3 0 167.34 52.22 1 13 3 0 213.63 46.39 3 13 3 0 182.11 27.67 9 14 -3 0 1335.49 119.81 1 14 3 0 1354.20 117.70 1 14 3 0 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32.96 1 -2 5 0 4.52 14.03 3 2 5 0 -1.87 34.62 1 3 5 0 883.70 69.63 1 4 5 012486.29 237.55 1 5 5 015531.16 278.41 1 6 5 0 316.86 53.74 1 7 5 0 102.74 41.00 1 8 5 0 479.33 65.07 1 9 5 0 1097.82 95.87 1 10 5 0 2408.69 142.32 1 10 -5 0 114.33 25.68 10 11 5 0 223.13 60.56 1 11 -5 0 13.47 25.81 10 -12 5 0 4039.03 157.85 2 12 5 0 3670.54 186.09 1 12 5 0 3939.44 164.86 3 13 5 0 661.75 79.69 3 13 5 0 627.53 89.00 1 13 5 0 673.85 45.04 9 -13 5 0 627.45 70.34 2 14 5 0 353.22 87.68 1 14 5 0 457.15 39.45 9 14 5 0 454.03 67.54 3 15 -5 0 9.00 25.11 10 16 -5 0 -13.82 25.12 10 18 -5 0 5.91 21.28 10 -20 -5 0 263.50 23.67 4 -21 5 0 441.60 23.88 12 -21 -5 0 458.76 23.10 4 0 6 0 5467.73 112.24 3 1 6 0 8.04 31.96 1 -1 6 0 1.82 16.09 3 2 6 0 1440.41 88.73 1 3 6 0 1322.62 89.00 1 4 6 0 1109.91 83.80 1 5 6 0 29.36 38.88 1 6 6 0 184.86 46.87 1 7 6 0 30.32 36.12 1 8 -6 0 -2.10 23.35 10 8 6 0 86.16 45.54 1 9 6 0 -13.62 40.68 1 10 6 0 1124.45 106.61 1 11 6 0 747.89 90.83 1 11 6 0 681.80 75.81 3 12 6 0 667.06 91.44 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1 13 2 3 803.48 108.03 1 -13 2 -3 873.42 46.86 4 -14 -2 -3 724.00 49.62 4 -14 2 -3 808.36 45.26 4 -15 2 -3 -26.59 21.69 4 -15 -2 -3 11.04 26.99 4 -16 -2 -3 76.21 34.67 4 -16 2 -3 68.77 22.43 4 -17 2 -3 49.52 19.79 4 -17 -2 -3 53.50 26.65 4 -18 2 -3 6.13 15.88 4 -18 -2 -3 -12.15 20.96 4 -19 -2 -3 562.79 33.23 4 -20 -2 -3 11.30 13.58 4 22 3 -3 -4.24 14.96 10 22 -3 -3 -13.61 16.64 10 21 -3 -3 -3.34 18.89 10 21 3 -3 33.78 26.28 10 20 3 -3 31.90 20.55 9 20 3 -3 31.40 25.67 10 20 -3 -3 3.15 22.52 10 19 3 -3 600.17 43.29 9 19 -3 -3 3.37 24.62 10 18 -3 -3 -4.56 25.38 10 18 3 -3 121.31 29.31 9 17 -3 -3 5.80 26.13 10 17 3 -3 4.61 26.88 9 16 3 -3 359.23 41.10 9 16 -3 -3 19.69 27.66 10 15 3 -3 1369.30 106.71 3 15 3 -3 1424.36 67.40 9 14 3 -3 210.27 50.58 3 14 3 -3 213.55 34.18 9 13 3 -3 2.04 23.93 9 13 3 -3 0.76 33.22 3 12 3 -3 357.71 36.74 9 12 3 -3 376.62 56.20 3 12 -3 -3 407.23 34.24 9 12 -3 -3 461.93 32.49 6 11 -3 -3 1.10 24.69 10 11 3 -3 29.20 35.03 3 11 -3 -3 -12.17 20.01 9 10 3 -3 763.12 70.82 3 9 3 -3 5443.63 170.70 3 8 3 -3 264.37 47.27 3 8 3 -3 273.70 33.56 1 7 3 -3 1102.56 55.42 1 7 3 -3 1135.07 77.71 3 6 3 -3 58.16 36.02 3 5 3 -3 2856.66 103.96 3 4 3 -3 241.80 40.19 3 -3 3 3 107.44 25.25 1 3 3 -3 133.88 33.69 3 -2 3 3 1917.21 72.79 1 2 3 -3 1871.73 76.69 3 -1 3 3 189.08 32.96 1 1 3 -3 182.21 33.54 3 0 3 -3 952.82 55.35 3 0 3 3 959.54 60.60 1 -1 3 -3 916.19 54.64 3 1 3 3 891.75 62.40 1 -2 3 -311239.00 167.49 3 2 3 311190.30 210.01 1 3 3 3 518.19 58.59 1 -3 3 -3 548.34 41.48 3 4 3 3 1987.24 107.05 1 5 3 3 6816.35 198.50 1 6 3 3 304.22 57.53 1 7 3 3 874.61 89.59 1 -7 3 -3 901.93 69.80 2 8 3 3 366.59 66.47 1 -8 3 -3 367.04 50.35 2 -9 3 -3 122.36 36.41 2 9 3 3 112.71 53.09 1 10 3 3 -3.13 45.21 1 -10 3 -3 -6.56 20.24 4 -10 3 -3 -11.63 28.44 2 -11 3 -3 1462.39 55.13 4 -11 3 -3 1671.21 110.49 2 11 3 3 1520.82 133.26 1 -12 3 -3 15.03 31.19 2 12 3 3 -34.61 52.66 1 -12 3 -3 -3.42 19.29 4 -13 3 -3 75.06 40.76 2 13 3 3 160.82 68.63 1 -13 3 -3 53.91 22.36 4 -13 -3 -3 64.37 27.48 4 13 -3 3 42.05 56.98 1 -14 3 -3 136.16 24.49 4 -14 -3 -3 138.85 30.57 4 -15 -3 -3 158.88 32.16 4 -15 3 -3 128.93 22.78 4 -16 -3 -3 258.20 36.16 4 -17 -3 -3 70.16 25.94 4 -18 -3 -3 141.32 26.49 4 -19 -3 -3 26.77 17.68 4 -20 -3 -3 147.40 17.44 4 22 -4 -3 -4.89 14.41 10 21 4 -3 -18.07 19.65 10 21 -4 -3 7.00 17.29 10 20 4 -3 -0.80 22.45 10 20 -4 -3 7.27 21.88 10 19 -4 -3 1.03 24.40 10 19 4 -3 189.78 28.53 9 18 4 -3 27.23 24.88 9 18 -4 -3 -0.68 24.28 10 17 4 -3 62.50 28.63 9 17 -4 -3 9.92 26.39 10 16 4 -3 4.05 27.10 9 15 4 -3 2299.78 85.93 9 15 4 -3 2242.37 142.98 3 14 4 -3 -8.16 37.61 3 14 4 -3 -3.88 25.99 9 14 -4 -3 -7.25 26.45 10 13 -4 -3 0.57 24.89 10 13 4 -3 57.84 38.24 3 13 4 -3 65.02 26.48 9 12 -4 -3 -0.12 24.36 10 12 4 -3 249.71 52.14 3 11 -4 -3 -1.20 23.26 10 11 4 -3 -3.59 37.55 3 10 4 -3 577.78 65.74 3 9 4 -3 101.16 43.61 3 9 4 -3 123.69 30.40 1 8 4 -3 1822.88 104.62 3 8 4 -3 1771.38 83.58 1 7 4 -3 72.30 34.16 3 7 4 -3 132.02 29.46 1 6 4 -3 1.63 34.15 3 5 4 -3 1407.40 81.16 3 4 4 -321234.91 281.12 3 3 4 -3 2801.40 103.42 3 -3 4 3 2778.59 94.46 1 -2 4 3 1870.07 82.26 1 2 4 -3 1896.59 82.46 3 -1 4 3 334.27 46.87 1 1 4 -3 340.38 39.96 3 0 4 -3 126.79 30.20 3 0 4 3 121.38 37.70 1 -1 4 -3 34.18 25.09 3 1 4 3 46.70 37.00 1 2 4 3 122.57 39.38 1 -2 4 -3 145.12 28.20 3 3 4 3 480.79 62.00 1 -3 4 -3 529.58 41.11 3 4 4 3 124.60 43.77 1 5 4 3 144.71 44.75 1 6 4 3 25.66 39.47 1 7 4 3 36.76 41.31 1 -8 4 -3 1456.03 95.70 2 8 4 3 1405.24 116.07 1 9 4 3 120.44 55.33 1 -9 4 -3 96.06 37.09 2 -10 4 -3 90.63 39.22 2 10 4 3 56.52 50.59 1 -11 4 -3 438.33 63.46 2 11 4 3 394.96 77.82 1 -12 4 -3 8.11 34.14 2 -12 -4 -3 7.32 22.50 4 12 4 3 54.63 54.06 1 -13 -4 -3 106.53 27.70 4 -14 -4 -3 486.67 41.63 4 -15 -4 -3 304.00 35.26 4 -16 -4 -3 311.92 34.79 4 -17 -4 -3 66.50 23.97 4 -18 -4 -3 35.84 19.69 4 -19 -4 -3 251.12 22.01 4 21 5 -3 0.76 15.71 10 21 -5 -3 0.71 16.96 10 20 5 -3 165.88 22.32 9 20 5 -3 6.54 20.27 10 20 -5 -3 5.00 19.28 10 -20 5 3 168.30 20.41 12 19 5 -3 291.50 30.50 9 -19 5 3 264.03 27.69 12 18 5 -3 9.34 22.63 9 17 -5 -3 -4.72 25.44 10 17 5 -3 10.65 25.30 9 16 -5 -3 0.76 25.23 10 16 5 -3 13.40 27.75 9 15 5 -3 685.52 52.37 9 14 5 -3 614.33 82.72 3 14 5 -3 675.06 52.06 9 13 -5 -3 1.20 25.65 10 13 5 -3 3214.42 164.02 3 12 -5 -3 49.09 42.81 10 12 5 -3 223.92 56.40 3 11 5 -3 70.77 42.70 3 11 -5 -3 57.73 27.49 10 10 -5 -3 -3.96 23.88 10 10 5 -3 4.90 35.13 3 9 -5 -3 1.32 23.68 10 9 5 -3 29.84 27.55 1 9 5 -3 7.49 36.84 3 8 5 -3 7.19 35.53 3 7 5 -3 6458.02 191.25 3 6 5 -3 62.49 36.99 3 5 5 -3 174.55 42.97 3 4 5 -3 1459.24 83.89 3 3 5 -3 1083.41 74.48 3 2 5 -3 4705.60 134.36 3 -2 5 3 4740.28 142.58 1 1 5 -3 224.05 35.29 3 -1 5 3 233.10 39.57 1 0 5 3 560.54 57.17 1 0 5 -3 524.05 47.06 3 1 5 3 1296.46 85.81 1 -1 5 -3 1376.85 68.23 3 2 5 3 626.46 66.72 1 -2 5 -3 596.60 45.22 3 3 5 3 545.95 63.37 1 4 5 3 3982.99 162.65 1 5 5 3 78.09 43.17 1 6 5 3 372.37 62.69 1 -7 -5 -3 123.12 22.67 4 7 5 3 131.38 49.94 1 -8 -5 -3 167.80 25.08 4 8 5 3 171.93 55.69 1 -9 -5 -3 301.74 31.64 4 -9 5 -3 356.42 58.64 2 9 5 3 318.41 70.79 1 10 5 3 109.64 53.90 1 -10 -5 -3 51.46 22.05 4 -10 5 -3 68.30 36.14 2 11 5 3 21.12 47.17 1 -11 -5 -3 43.94 23.26 4 -11 5 -3 23.28 33.16 2 -12 -5 -3 163.39 28.99 4 -13 -5 -3 184.64 30.69 4 -14 -5 -3 -6.56 23.06 4 -15 -5 -3 33.62 23.77 4 -16 -5 -3 36.10 21.97 4 -17 -5 -3 6.92 19.23 4 -18 5 -3 98.24 18.16 12 -18 -5 -3 96.90 19.31 4 -19 -5 -3 6.42 11.75 4 20 -6 -3 7.14 17.36 10 20 6 -3 238.57 21.66 9 -19 6 3 38.08 17.12 12 19 6 -3 26.14 18.09 9 18 6 -3 310.87 33.79 9 -18 6 3 351.89 30.96 12 17 6 -3 140.96 30.57 9 -17 6 3 129.69 25.36 12 -16 6 3 82.83 24.98 12 16 6 -3 102.69 30.70 9 15 -6 -3 2.01 25.89 10 15 6 -3 258.29 41.30 9 14 6 -3 304.96 40.54 9 14 -6 -3 -3.71 25.15 10 13 6 -3 858.29 94.97 3 13 -6 -3 12.33 28.17 10 12 6 -3 143.32 52.16 3 12 -6 -3 1.99 25.25 10 11 6 -3 810.80 87.35 3 11 -6 -3 10.76 26.42 10 10 6 -3 4.86 40.37 3 10 -6 -3 -5.82 24.72 10 -10 6 3 3.97 21.25 12 9 6 -3 1169.20 96.87 3 -9 6 3 1056.46 52.88 12 8 6 -3 713.06 76.29 3 -8 6 3 603.33 40.25 12 7 6 -3 1032.10 85.22 3 6 6 -3 1871.95 107.12 3 5 6 -3 284.49 50.73 3 4 6 -3 1014.94 76.35 3 3 6 -3 50.87 30.31 3 -2 6 3 253.82 42.95 1 2 6 -3 278.24 42.38 3 1 6 -3 625.41 55.85 3 -1 6 3 691.42 66.47 1 0 6 -3 274.77 39.05 3 0 6 3 287.33 50.94 1 1 6 3 444.13 60.88 1 -1 6 -3 470.36 45.10 3 2 6 3 136.46 43.00 1 3 6 3 2512.65 132.85 1 4 6 3 35.72 37.90 1 -5 6 -3 624.47 40.92 12 5 6 3 649.21 79.69 1 6 6 3 961.63 101.24 1 7 6 3 17.17 48.63 1 8 6 3 81.11 50.86 1 -8 -6 -3 150.20 25.62 4 9 6 3 47.24 48.19 1 -9 -6 -3 59.70 22.25 4 10 6 3 230.71 68.80 1 -10 -6 -3 217.11 28.84 4 -10 6 -3 282.08 56.82 2 -11 -6 -3 -0.49 21.62 4 -12 -6 -3 320.77 33.24 4 -13 -6 -3 50.71 23.59 4 -14 -6 -3 228.96 29.11 4 -15 -6 -3 0.39 19.38 4 -16 6 -3 78.77 20.88 12 -16 -6 -3 103.43 21.55 4 -17 6 -3 88.82 18.20 12 -17 -6 -3 94.93 18.90 4 -18 6 -3 22.18 13.23 12 -18 -6 -3 -9.62 12.97 4 -19 7 3 20.41 13.63 12 19 7 -3 33.14 16.98 9 -18 7 3 281.83 25.34 12 18 7 -3 275.86 28.73 9 17 -7 -3 4.43 22.87 10 -17 7 3 14.68 19.07 12 17 7 -3 1.10 21.11 9 16 7 -3 28.61 26.48 9 -16 7 3 38.66 21.37 12 -15 7 3 60.77 25.63 12 15 7 -3 56.83 28.88 9 15 -7 -3 26.37 43.29 10 14 -7 -3 1.85 25.73 10 -14 7 3 275.32 33.30 12 -13 7 3 713.97 49.39 12 -12 7 3 87.89 28.03 12 12 -7 -3 9.76 27.24 10 11 7 -3 435.13 71.96 3 -11 7 3 388.18 38.51 12 -10 7 3 22.19 24.24 12 10 7 -3 35.86 37.19 3 -9 7 3 280.54 45.65 12 9 7 -3 210.65 54.06 3 8 7 -3 701.90 85.07 3 -8 7 3 718.75 43.87 12 -7 7 3 951.40 48.98 12 7 7 -3 944.48 87.63 3 6 7 -3 614.52 37.00 12 -6 7 3 618.13 40.39 12 6 7 -3 598.46 68.93 3 5 7 -3 599.77 36.69 12 -5 7 3 660.61 43.10 12 5 7 -3 587.21 66.37 3 -4 7 3 454.40 35.04 12 4 7 -3 455.95 58.17 3 3 7 -3 74.60 34.13 3 2 7 -3 704.17 63.63 3 1 7 -3 49.65 26.85 3 -1 7 3 42.26 29.70 1 0 7 3 263.78 49.52 1 1 7 3 89.84 40.77 1 1 7 3 127.50 23.70 12 -1 7 -3 143.70 32.43 5 2 7 3 584.43 71.79 1 2 7 3 607.37 37.12 12 -2 7 -3 651.99 39.92 12 -2 7 -3 583.86 41.50 5 3 7 3 3744.48 84.93 12 -3 7 -3 3709.27 94.35 5 -3 7 -3 3826.72 87.41 12 3 7 3 3545.02 164.47 1 -4 7 -3 1352.42 55.41 12 4 7 3 1290.09 109.32 1 -5 7 -3 22.19 23.39 12 5 7 3 6.74 36.71 1 -6 7 -3 188.37 29.46 12 6 7 3 98.30 47.49 1 -7 7 -3 30.59 22.02 12 7 7 3 39.23 43.64 1 -8 7 -3 52.96 25.44 12 8 7 3 58.11 50.56 1 9 7 3 37.62 42.65 1 -9 7 -3 52.81 23.96 12 -10 7 -3 209.16 31.98 12 -11 7 -3 13.78 23.55 12 -11 -7 -3 9.37 19.27 4 -12 -7 -3 120.66 23.51 4 -12 7 -3 1024.01 67.19 12 -13 -7 -3 356.11 30.31 4 -13 7 -3 359.69 33.49 12 -14 7 -3 45.54 20.89 12 -14 -7 -3 33.76 18.29 4 -15 7 -3 108.10 21.18 12 -15 -7 -3 106.00 19.31 4 -16 7 -3 5.93 15.91 12 -17 7 -3 2.69 16.28 5 -17 7 -3 27.18 14.26 12 18 8 -3 10.29 15.21 9 -18 8 3 21.21 13.53 12 17 8 -3 858.73 50.99 9 -17 8 3 612.18 32.16 12 -16 8 3 12.64 18.96 12 16 8 -3 9.02 23.32 9 -15 8 3 289.11 30.36 12 15 8 -3 343.57 36.92 9 -14 8 3 181.82 28.50 12 14 -8 -3 -0.67 24.12 10 13 -8 -3 -1.48 24.65 10 -13 8 3 675.92 45.25 12 12 -8 -3 -0.42 27.20 10 -12 8 3 91.58 25.48 12 11 8 -3 327.12 35.12 6 -11 8 3 315.19 36.08 12 -10 8 3 879.62 52.53 12 10 -8 -3 4.20 25.50 10 -9 8 3 276.64 34.55 12 9 8 -3 293.92 62.79 3 8 8 -3 498.61 74.09 3 -8 8 3 525.28 41.32 12 7 8 -3 -10.41 34.98 3 -7 8 3 -7.10 21.71 12 6 8 -3 1039.89 48.12 12 6 8 -3 981.76 93.32 3 -6 8 3 1064.56 52.46 12 5 8 -3 489.67 34.77 12 -5 8 3 481.68 37.96 12 5 8 -3 477.35 64.90 3 4 8 -3 266.49 50.60 3 -4 8 3 256.89 29.74 12 4 8 -3 275.54 29.56 12 -3 8 3 97.44 24.55 12 3 8 -3 71.22 22.78 12 3 8 -3 66.17 31.47 3 2 8 -3 1686.99 60.41 12 2 8 -3 1570.37 58.98 5 1 8 -3 454.05 36.85 5 -1 8 3 449.50 34.51 12 0 8 -3 40.42 23.56 5 0 8 -3 67.09 23.12 12 0 8 3 35.95 20.68 12 0 8 3 14.30 33.08 1 1 8 3 98.92 43.35 1 -1 8 -3 120.43 28.20 5 -1 8 -3 109.53 24.57 12 1 8 3 98.48 24.81 12 -2 8 -3 947.12 51.51 5 2 8 3 929.29 47.01 12 2 8 3 877.47 89.11 1 -2 8 -3 1022.08 54.75 12 -3 8 -3 71.04 26.69 5 -3 8 -3 66.92 23.23 12 3 8 3 56.48 42.79 1 3 8 3 48.36 21.11 12 -4 8 -3 112.08 30.03 5 4 8 3 91.56 51.74 1 -4 8 -3 73.60 24.48 12 -5 8 -3 124.27 32.19 5 5 8 3 73.41 40.70 1 -5 8 -3 145.58 28.28 12 6 8 3 799.03 95.45 1 -6 8 -3 776.31 47.78 12 -7 8 -3 7.49 21.26 12 7 8 3 21.33 41.32 1 -8 8 -3 55.94 27.04 12 -9 8 -3 21.97 22.34 12 -10 8 -3 215.67 32.32 12 -11 8 -3 91.67 29.76 12 -12 8 -3 5.29 19.50 12 -13 8 -3 261.54 28.32 12 -14 8 -3 -3.29 16.88 12 -15 8 -3 -3.11 14.81 12 -15 8 -3 4.75 18.79 5 -16 8 -3 164.67 20.88 5 -16 8 -3 191.05 17.69 12 17 9 -3 11.04 14.31 9 -17 9 3 17.94 12.17 12 16 9 -3 25.97 18.25 9 -16 9 3 30.76 16.61 12 -15 9 3 36.33 19.07 12 15 9 -3 27.31 21.72 9 14 9 -3 7.17 22.89 9 -14 9 3 22.78 20.52 12 -13 9 3 15.39 20.88 12 -12 9 3 12.85 23.68 12 -11 9 3 16.11 21.53 12 -10 9 3 467.07 39.94 12 -9 9 3 1355.39 61.00 12 -8 9 3 711.01 45.91 12 7 9 -3 276.07 60.66 3 -7 9 3 298.74 34.29 12 -6 9 3 -1.97 22.17 12 6 9 -3 -28.12 42.68 3 5 9 -3 356.97 57.95 3 5 9 -3 389.58 35.45 12 -5 9 3 412.55 36.55 12 4 9 -3 245.71 29.62 12 -4 9 3 238.90 30.54 12 3 9 -3 313.08 30.14 12 2 9 -3 -8.53 20.92 12 -2 9 3 12.76 22.15 12 -1 9 3 219.10 29.18 12 1 9 -3 189.08 28.03 5 1 9 -3 207.81 27.95 12 0 9 -3 14.96 22.89 5 0 9 3 6.64 20.52 12 0 9 -3 11.46 19.36 12 -1 9 -3 1435.99 59.94 5 -1 9 -3 1466.48 59.83 12 1 9 3 1502.52 60.24 12 -2 9 -3 3243.22 87.06 5 2 9 3 3254.68 84.73 12 2 9 3 3154.15 167.30 1 -2 9 -3 3224.53 88.28 12 3 9 3 93.33 46.23 1 -3 9 -3 137.92 28.06 12 -3 9 -3 115.03 27.72 5 3 9 3 172.00 28.73 12 -4 9 -3 179.92 29.88 5 4 9 3 147.28 48.73 1 -4 9 -3 168.69 29.73 12 -5 9 -3 123.87 28.86 12 -5 9 -3 126.01 30.88 5 -6 9 -3 162.87 33.29 5 -6 9 -3 121.24 26.56 12 -7 9 -3 88.98 30.03 5 -7 9 -3 92.79 27.12 12 -8 -9 -3 23.22 19.06 8 -8 9 -3 8.12 26.78 5 -8 9 -3 34.51 25.55 12 -9 9 -3 67.10 29.00 5 -9 9 -3 39.16 24.57 12 -10 9 -3 42.08 22.86 12 -10 9 -3 19.98 24.15 5 -11 9 -3 64.17 21.95 12 -11 9 -3 48.11 26.17 5 -12 9 -3 53.55 23.27 5 -12 9 -3 72.95 20.56 12 -13 9 -3 60.74 21.65 5 -13 9 -3 66.49 19.08 12 -14 9 -3 16.72 13.96 12 -14 9 -3 3.58 16.69 5 -15 9 -3 33.56 14.83 5 -15 9 -3 31.51 11.82 12 16 10 -3 202.44 19.30 9 -15 10 3 22.93 13.28 12 15 10 -3 15.99 16.26 9 14 10 -3 174.24 26.13 9 -14 10 3 170.83 21.06 12 -13 10 3 126.77 21.75 12 -12 10 3 49.18 21.20 12 -11 10 3 73.13 24.73 12 -10 10 3 167.56 26.98 12 -9 10 3 5.20 20.59 12 8 -10 -3 20.00 20.29 8 -8 10 3 19.45 23.27 12 -7 10 3 -5.44 21.91 12 -6 10 3 52.81 26.93 12 -4 10 3 59.42 24.03 12 4 10 -3 56.40 22.56 12 3 10 -3 45.31 22.11 12 -3 10 3 37.46 23.08 12 -2 10 3 12.99 21.68 12 2 10 -3 14.62 20.77 12 1 10 -3 359.72 33.29 12 -1 10 3 357.60 34.35 12 0 10 -3 152.35 28.09 12 0 10 3 149.03 26.57 12 -1 10 -3 84.02 24.52 5 1 10 3 84.19 24.04 12 -1 10 -3 87.55 24.35 12 -2 10 -3 -7.00 22.02 5 2 10 3 -1.37 20.71 12 -2 10 -3 0.02 15.58 12 -3 10 -3 364.78 34.76 5 -3 10 -3 347.39 35.88 12 -4 10 -3 0.36 21.68 12 -4 10 -3 7.51 21.92 5 -5 10 -3 299.18 32.48 5 -5 10 -3 364.65 35.26 12 -6 10 -3 240.37 32.29 12 -6 10 -3 255.11 31.79 5 -7 10 -3 109.88 27.14 12 -7 10 -3 103.28 25.81 5 -8 10 -3 658.33 42.11 5 -8 -10 -3 676.97 36.42 8 -8 10 -3 681.54 42.50 12 -9 10 -3 19.05 21.16 5 -9 10 -3 31.15 20.28 12 -10 10 -3 58.31 21.89 5 -10 10 -3 52.98 20.14 12 -11 10 -3 14.05 17.04 12 -11 10 -3 -1.66 18.09 5 -12 10 -3 11.69 15.32 12 -12 10 -3 -3.06 16.53 5 -13 10 -3 5.66 12.27 12 -13 10 -3 7.83 14.17 5 14 11 -3 1.22 13.77 9 -14 11 3 -2.52 10.86 12 13 11 -3 26.11 16.97 9 -12 11 3 -0.62 14.82 12 10 11 -3 2.08 19.83 6 -9 11 3 18.90 16.76 12 8 -11 -3 -8.05 18.17 8 7 -11 -3 65.67 22.63 8 -7 11 3 84.04 23.78 12 -6 11 3 297.29 30.98 12 -5 11 3 123.31 24.44 12 -4 11 3 92.93 25.15 12 3 11 -3 232.23 28.23 12 -3 11 3 253.57 31.22 12 -2 11 3 151.87 27.01 12 2 11 -3 180.53 27.48 12 1 11 -3 -3.04 20.30 12 -1 11 3 -7.41 20.88 12 0 11 3 56.87 22.69 12 0 11 -3 45.91 22.99 12 1 11 3 583.18 40.53 12 -1 11 -3 533.64 38.43 12 -2 11 -3 13.48 20.44 12 -3 11 -3 64.21 21.90 12 -4 11 -3 80.38 25.00 12 -5 11 -3 98.42 21.98 5 -5 11 -3 34.56 15.32 12 -6 11 -3 524.14 34.10 5 -6 -11 -3 475.28 33.53 8 -7 -11 -3 1150.88 45.55 8 -7 11 -3 1031.78 43.64 5 -7 11 -3 1085.66 46.25 12 -8 11 -3 223.19 24.38 5 -8 11 -3 260.27 25.54 12 -9 11 -3 521.14 32.93 5 -9 11 -3 264.24 24.08 12 -10 11 -3 90.11 17.34 5 -10 11 -3 121.99 19.09 12 -11 11 -3 33.67 13.73 5 12 12 -3 13.13 13.30 9 -11 12 3 52.66 13.31 12 -10 12 3 5.29 13.92 12 9 12 -3 210.58 23.67 6 -9 12 3 188.18 21.37 12 -8 12 3 38.57 16.09 12 7 -12 -3 19.00 17.07 8 -7 12 3 29.92 17.08 12 6 -12 -3 37.36 19.36 8 -6 12 3 44.24 19.63 12 -5 12 3 -0.64 18.07 12 -4 12 3 40.71 19.37 12 -3 12 3 18.41 18.15 12 2 12 -3 14.38 18.78 12 -2 12 3 13.54 19.20 12 -1 12 3 312.87 29.76 12 1 12 -3 325.31 28.05 12 0 12 -3 -1.40 16.37 12 -1 12 -3 105.37 22.24 12 -2 12 -3 34.81 18.52 12 -3 12 -3 11.51 17.72 12 -4 12 -3 11.25 16.42 12 -5 -12 -3 283.49 26.39 8 -5 12 -3 313.14 25.97 12 -6 12 -3 141.63 19.62 12 -6 -12 -3 124.36 19.69 8 -7 -12 -3 91.32 16.38 8 -7 12 -3 99.30 17.05 12 -8 12 -3 112.60 15.68 12 -9 12 -3 5.90 10.85 12 -8 13 3 49.37 12.57 12 7 13 -3 14.18 16.93 6 -7 13 3 5.50 12.57 12 -6 13 3 -3.05 13.22 12 5 -13 -3 -6.34 15.62 8 -5 13 3 7.80 13.99 12 4 -13 -3 1.56 17.02 8 -4 13 3 5.31 14.76 12 3 -13 -3 422.52 30.00 8 -3 13 3 417.33 27.67 12 2 -13 -3 -11.04 18.65 8 1 -13 -3 3.35 18.35 8 0 -13 -3 13.38 19.97 8 -1 -13 -3 108.62 21.58 8 -1 13 -3 104.59 16.68 12 -2 13 -3 -0.46 12.79 12 -2 -13 -3 4.47 16.81 8 -3 -13 -3 51.53 22.76 8 -3 13 -3 26.36 13.72 12 -4 -13 -3 26.94 15.05 8 -4 13 -3 43.43 13.34 12 -5 -13 -3 4.39 12.94 8 -5 13 -3 -13.10 11.52 12 2 -14 -3 16.84 12.43 8 1 -14 -3 4.77 11.77 8 0 -14 -3 32.55 12.98 8 -1 -14 -3 14.18 11.72 8 23 0 -4 3.04 13.67 10 21 0 -4 -1.63 20.89 10 20 0 -4 7.78 25.16 10 19 0 -4 530.43 42.97 9 19 0 -4 1.44 26.64 10 18 0 -4 13.55 28.31 10 18 0 -4 1731.01 71.16 9 17 0 -4 313.67 38.53 9 17 0 -4 -7.71 29.90 10 16 0 -4 105.60 31.03 9 15 0 -4 -10.22 24.29 9 14 0 -4 93.61 28.16 9 13 0 -4 11.35 21.46 9 13 0 -4 -20.71 22.12 6 12 0 -4 411.76 51.04 3 12 0 -4 432.11 36.12 9 12 0 -4 410.04 33.44 6 11 0 -4 672.32 63.25 3 10 0 -4 2236.20 101.78 3 9 0 -4 945.65 68.60 3 8 0 -4 186.83 38.37 3 7 0 -4 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7 4 160.35 44.86 1 0 7 -4 203.43 30.82 5 0 7 4 198.32 25.45 12 1 7 4 2510.63 68.89 12 1 7 4 2366.21 136.29 1 -1 7 -4 2529.29 79.83 5 2 7 4 3527.88 168.20 1 2 7 4 3613.78 82.30 12 -2 7 -4 3683.07 95.80 5 -3 7 -4 21.61 27.38 5 3 7 4 -28.21 41.98 1 -3 7 -4 9.01 20.20 12 -4 7 -4 275.85 37.09 5 -4 7 -4 278.82 30.38 12 4 7 4 268.44 62.07 1 5 7 4 333.96 69.51 1 -5 7 -4 342.29 32.80 12 -6 -7 -4 926.26 47.35 8 6 7 4 925.23 103.83 1 -6 7 -4 882.56 47.34 12 7 7 4 172.83 62.69 1 -7 -7 -4 170.37 25.34 8 -7 7 -4 263.86 32.96 12 -8 7 -4 19.09 21.99 12 -9 7 -4 92.95 25.54 12 -10 7 -4 25.74 23.46 12 -11 7 -4 -5.79 19.27 12 -11 -7 -4 1.89 18.16 4 -12 -7 -4 1049.52 44.18 4 -12 7 -4 1050.52 47.93 12 -13 7 -4 23.37 17.65 12 -13 -7 -4 17.29 18.27 4 -14 7 -4 27.53 16.98 12 -14 -7 -4 21.13 15.86 4 -15 7 -4 39.54 14.57 12 -15 7 -4 27.27 20.20 5 -16 7 -4 117.19 19.07 5 18 8 -4 128.81 20.20 9 17 8 -4 130.65 25.07 9 -16 8 4 54.98 16.75 12 16 8 -4 82.86 26.25 9 15 8 -4 65.17 26.42 9 -15 8 4 48.25 18.44 12 -14 8 4 14.01 18.94 12 14 8 -4 19.28 27.00 9 14 -8 -4 -3.86 23.66 10 13 -8 -4 29.46 29.39 10 -13 8 4 230.75 28.84 12 12 8 -4 893.11 49.54 6 -12 8 4 879.71 47.67 12 -11 8 4 45.38 21.75 12 11 -8 -4 0.52 25.56 10 11 8 -4 43.69 28.41 6 -10 8 4 132.79 28.89 12 10 -8 -4 2.29 25.45 10 -9 8 4 713.21 44.83 12 8 8 -4 274.08 59.34 3 8 -8 -4 291.82 31.31 8 -8 8 4 279.07 30.60 12 -7 8 4 1796.32 64.82 12 7 8 -4 1862.03 127.84 3 6 8 -4 413.13 64.50 3 -6 8 4 448.67 36.50 12 -5 8 4 190.89 26.77 12 5 8 -4 184.80 49.44 3 4 8 -4 42.13 35.19 3 -4 8 4 35.73 20.23 12 -3 8 4 36.50 21.50 12 3 8 -4 55.52 38.86 3 -2 8 4 46.09 20.92 12 2 8 -4 39.50 24.69 5 1 8 -4 1118.84 55.39 5 -1 8 4 1176.14 50.30 12 0 8 -4 835.45 50.79 5 0 8 4 815.72 44.21 12 -1 8 -4 692.42 46.58 5 1 8 4 650.47 80.31 1 1 8 4 716.87 40.80 12 -1 8 -4 708.34 41.03 12 -2 8 -4 267.11 36.35 5 2 8 4 297.82 61.52 1 2 8 4 311.64 30.65 12 -2 8 -4 285.55 30.63 12 -3 8 -4 64.75 29.75 5 -3 8 -4 58.65 21.31 12 3 8 4 85.52 46.97 1 -4 8 -4 4542.91 113.14 5 -4 8 -4 4435.33 97.66 12 -5 8 -4 507.47 46.95 5 5 8 4 447.60 74.41 1 -5 8 -4 505.07 38.81 12 -6 8 -4 -3.96 21.27 12 -6 8 -4 11.83 29.21 5 -6 -8 -4 17.89 22.04 8 -7 8 -4 43.59 23.56 12 -7 -8 -4 81.49 24.47 8 -7 8 -4 47.96 30.74 5 -8 8 -4 6.62 20.96 12 -8 8 -4 5.69 29.14 5 -9 8 -4 97.12 31.72 5 -9 8 -4 91.22 24.10 12 -10 8 -4 120.17 24.59 12 -10 8 -4 112.43 31.50 5 -11 8 -4 83.21 20.90 12 -11 8 -4 71.63 30.12 5 -12 8 -4 142.52 21.31 12 -12 8 -4 175.74 30.68 5 -13 8 -4 16.32 22.88 5 -13 8 -4 0.87 15.21 12 -14 8 -4 14.21 19.09 5 -15 8 -4 214.42 21.90 5 17 9 -4 245.12 22.51 9 16 9 -4 10.89 18.12 9 15 9 -4 3.20 20.86 9 -15 9 4 20.71 14.42 12 -14 9 4 8.84 15.18 12 14 9 -4 -11.56 24.55 9 -13 9 4 5.49 16.78 12 12 9 -4 288.41 31.47 6 -12 9 4 272.23 27.77 12 -11 9 4 100.13 25.58 12 11 9 -4 95.16 27.56 6 -10 9 4 79.16 22.93 12 -9 9 4 40.10 26.26 12 8 -9 -4 585.61 40.02 8 -8 9 4 586.36 41.16 12 7 -9 -4 339.83 33.49 8 -7 9 4 326.46 32.53 12 -5 9 4 1582.90 60.00 12 -4 9 4 3.04 19.44 12 4 9 -4 10.99 18.96 12 3 9 -4 732.03 40.24 12 -3 9 4 767.44 44.01 12 2 9 -4 34.34 21.34 12 -2 9 4 34.70 21.24 12 1 9 -4 2482.96 78.66 5 -1 9 4 2507.57 73.62 12 1 9 -4 2476.77 70.27 12 0 9 -4 1249.71 59.06 5 0 9 -4 1313.79 52.44 12 0 9 4 1283.22 54.92 12 -1 9 -4 49.91 20.31 12 1 9 4 33.61 22.09 12 -1 9 -4 56.62 26.12 5 -2 9 -4 227.67 33.35 5 2 9 4 267.94 64.15 1 -2 9 -4 248.60 32.18 12 -3 9 -4 3616.41 97.73 5 -3 9 -4 3580.89 88.08 12 -4 9 -4 146.93 25.63 12 -4 9 -4 116.05 30.20 5 -5 9 -4 54.44 23.24 12 -5 9 -4 40.36 28.16 5 -5 -9 -4 53.79 24.96 8 -6 9 -4 2306.65 80.30 5 -6 -9 -4 2347.11 72.02 8 -6 9 -4 2274.59 71.47 12 -7 9 -4 37.95 27.25 5 -7 -9 -4 -15.35 19.57 8 -7 9 -4 18.72 20.48 12 -8 9 -4 396.00 33.43 12 -8 9 -4 436.67 41.77 5 -9 9 -4 13.02 18.26 12 -9 9 -4 33.25 27.43 5 -10 9 -4 17.05 16.74 12 -10 9 -4 -4.47 22.87 5 -11 9 -4 35.00 17.10 12 -11 9 -4 43.49 23.17 5 -12 9 -4 -2.49 19.96 5 -12 9 -4 -8.86 13.62 12 -13 9 -4 -0.48 16.77 5 -14 9 -4 153.18 18.05 5 16 10 -4 49.14 14.01 9 15 10 -4 87.65 19.70 9 14 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14.80 23.81 4 10 0 5 12.98 50.22 1 -10 0 -5 -0.78 24.44 4 11 0 5 4.08 55.42 1 -11 0 -5 -17.00 24.97 4 -12 0 -5 6.99 27.10 4 -13 0 -5 -0.55 24.61 4 -14 0 -5 4.95 23.80 4 -15 0 -5 4.29 23.99 4 -16 0 -5 -7.17 19.94 4 -17 0 -5 -7.75 16.65 4 -18 0 -5 8.34 12.98 4 22 -1 -5 1.80 16.73 10 22 1 -5 2.21 16.12 10 21 -1 -5 6.53 21.24 10 21 1 -5 3.68 19.80 10 20 -1 -5 -4.60 23.21 10 20 1 -5 0.49 23.46 10 19 -1 -5 -3.20 24.95 10 19 1 -5 1.48 25.00 10 18 1 -5 7.26 27.28 10 18 -1 -5 -46.90 27.68 10 17 -1 -5 -12.23 29.36 10 17 1 -5 22.33 27.33 9 17 -1 -5 7.55 25.50 9 16 -1 -5 296.21 36.52 9 16 1 -5 315.11 38.31 9 15 -1 -5 308.58 35.60 9 15 1 -5 318.46 38.69 9 15 -1 -5 300.68 31.30 6 15 1 -5 329.86 32.91 6 14 -1 -5 6.63 23.52 9 14 1 -5 1.69 24.30 9 14 1 -5 12.80 20.66 6 13 1 -5 536.78 67.15 3 13 -1 -5 497.06 39.46 9 13 1 -5 503.28 41.46 9 13 -1 -5 485.93 37.09 6 13 1 -5 550.67 39.96 6 12 -1 -5 6.71 19.62 9 12 1 -5 14.55 23.62 9 12 1 -5 -4.41 36.95 3 12 -1 -5 5.24 21.34 6 12 1 -5 -2.99 21.83 6 11 -1 -5 136.85 25.14 9 11 1 -5 166.17 28.28 9 11 1 -5 115.35 41.08 3 11 -1 -5 133.04 34.55 3 11 -1 -5 137.55 25.23 6 11 1 -5 148.70 26.94 6 10 1 -5 102.90 23.46 9 10 1 -5 86.42 37.11 3 10 -1 -5 87.58 31.01 3 10 -1 -5 92.30 23.32 6 10 1 -5 88.13 23.73 6 9 1 -5 536.74 60.78 3 9 -1 -5 553.29 55.47 3 8 1 -5 98.63 38.68 3 8 -1 -5 93.54 31.83 3 7 1 -5 1887.85 99.36 3 7 -1 -5 1807.97 89.47 3 6 1 -5 2648.62 115.01 3 6 -1 -5 2534.62 102.55 3 5 1 -5 374.99 51.10 3 5 -1 -5 378.22 45.91 3 4 1 -5 2095.24 99.27 3 4 -1 -5 2120.04 92.76 3 3 1 -5 14.50 31.41 3 3 -1 -5 14.57 29.61 3 2 1 -5 194.22 42.17 3 -2 1 5 147.69 27.52 1 2 -1 -5 164.79 37.74 3 2 1 -5 169.33 22.10 2 -1 1 5 61.54 24.95 1 1 1 -5 82.92 35.70 3 1 -1 -5 73.92 30.94 3 1 1 -5 53.88 18.84 2 0 1 5 1755.79 85.36 1 0 1 -5 1688.08 85.62 3 0 1 -5 1665.25 68.17 2 1 1 512228.89 236.34 1 -1 1 -512375.89 221.28 3 -1 1 -512015.49 190.66 2 2 1 5 57.61 34.46 1 -2 1 -5 58.34 26.96 2 3 1 5 236.30 51.67 1 -3 1 -5 226.43 36.35 2 4 1 5 19.91 41.19 1 -4 1 -5 20.59 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42.81 1 -3 4 -5 27.16 25.08 5 3 4 5 -33.15 44.89 1 -4 -4 -5 257.60 28.03 4 -4 -4 -5 265.45 28.16 8 -4 4 -5 263.02 46.23 2 4 4 5 266.44 57.00 1 -5 -4 -5 43.72 20.13 8 -5 4 -5 148.66 27.40 4 -5 -4 -5 62.26 21.46 4 5 4 5 65.19 48.91 1 -5 4 -5 103.57 37.44 2 -6 -4 -5 312.13 32.53 4 -6 4 -5 358.60 56.16 2 6 4 5 293.79 66.90 1 -7 -4 -5 6.46 21.41 4 7 4 5 -24.75 51.72 1 -7 4 -5 9.83 28.91 2 -8 -4 -5 307.77 35.17 4 8 4 5 305.48 72.34 1 -8 4 -5 327.70 56.27 2 -9 -4 -5 1122.53 57.66 4 9 4 5 972.25 115.02 1 -9 4 -5 1175.93 99.76 2 -10 -4 -5 81.32 27.74 4 -11 -4 -5 7.19 24.95 4 -12 -4 -5 634.21 46.57 4 -13 -4 -5 63.82 27.67 4 -14 -4 -5 40.11 24.23 4 -15 -4 -5 35.51 21.64 4 -16 4 -5 173.15 23.43 5 -16 -4 -5 182.02 23.30 4 -17 -4 -5 40.75 15.40 4 21 -5 -5 1.44 14.75 10 21 5 -5 -11.65 16.54 10 21 5 -5 2.35 11.94 9 20 5 -5 5.67 20.99 10 20 5 -5 44.55 18.15 9 19 -5 -5 -3.14 20.36 10 19 5 -5 0.90 20.29 9 18 5 -5 0.54 23.40 9 17 -5 -5 -1.34 23.53 10 17 5 -5 17.69 27.62 9 16 -5 -5 -8.80 25.14 10 16 5 -5 12.06 29.13 9 15 -5 -5 8.11 25.10 10 15 5 -5 76.83 31.85 9 14 5 -5 394.94 44.65 9 14 5 -5 354.93 36.17 6 13 -5 -5 11.60 25.20 10 13 5 -5 25.04 29.56 9 13 5 -5 11.93 26.00 6 12 -5 -5 4.80 26.98 10 12 5 -5 88.15 45.95 3 12 5 -5 95.06 29.51 6 11 5 -5 279.71 65.55 3 11 5 -5 356.19 39.68 6 10 5 -5 369.62 67.42 3 10 5 -5 311.06 38.58 6 9 5 -5 85.30 30.67 6 9 -5 -5 8.22 21.55 10 9 5 -5 97.01 47.12 3 8 5 -5 44.64 41.93 3 8 -5 -5 7.29 22.04 8 8 5 -5 1.62 18.73 11 7 5 -5 147.79 46.90 3 7 5 -5 214.69 26.68 11 7 -5 -5 216.14 27.18 8 7 -5 -5 193.77 25.88 6 6 5 -5 121.12 22.45 11 6 5 -5 118.30 45.31 3 6 -5 -5 146.94 25.24 8 6 -5 -5 170.38 23.98 6 5 -5 -5 828.61 42.67 8 5 5 -5 845.03 43.35 11 5 5 -5 912.43 83.84 3 4 5 -5 213.61 27.54 11 4 -5 -5 170.44 25.29 8 3 5 -5 710.93 70.71 3 3 5 -5 758.83 44.82 5 3 -5 -5 765.48 41.14 8 2 5 -5 163.22 42.60 3 2 -5 -5 155.62 25.83 8 2 5 -5 160.68 28.04 5 1 5 -5 150.52 28.45 5 -1 5 5 143.10 38.66 1 1 5 -5 106.05 35.20 3 1 -5 -5 120.12 23.46 8 0 5 -5 60.83 23.06 5 0 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9 19 6 -5 51.82 19.49 9 18 -6 -5 11.26 21.76 10 18 6 -5 25.96 22.58 9 17 6 -5 350.73 37.40 9 17 -6 -5 2.30 21.70 10 16 6 -5 55.56 30.19 9 15 -6 -5 2.26 25.21 10 15 6 -5 56.79 29.46 9 14 6 -5 615.80 50.79 9 14 6 -5 569.27 41.17 6 13 -6 -5 1.35 24.54 10 13 6 -5 439.97 39.23 6 12 -6 -5 21.88 25.27 10 12 6 -5 1780.41 72.45 6 11 6 -5 255.64 61.72 3 11 6 -5 298.86 39.38 6 10 6 -5 1991.33 76.82 6 10 6 -5 1951.08 139.19 3 9 6 -5 8.31 39.80 3 9 -6 -5 3.25 22.94 10 8 -6 -5 -6.26 23.19 10 8 6 -5 96.48 47.67 3 8 -6 -5 112.10 23.81 8 7 6 -5 451.36 38.65 11 7 -6 -5 442.43 35.93 8 7 6 -5 450.20 69.43 3 6 -6 -5 527.19 38.10 8 6 6 -5 541.21 73.82 3 6 6 -5 551.00 37.07 11 5 6 -5 1846.88 63.14 11 5 -6 -5 1794.14 61.90 8 5 6 -5 1895.54 120.35 3 4 6 -5 7.98 18.95 11 4 6 -5 -6.40 34.82 3 4 -6 -5 -8.39 22.27 8 3 6 -5 1459.75 99.25 3 3 6 -5 1442.17 60.66 5 3 -6 -5 1459.00 57.26 8 3 6 -5 1541.81 59.55 11 2 6 -5 920.54 80.35 3 2 6 -5 947.05 51.89 5 2 -6 -5 869.36 47.96 8 1 6 -5 6.60 24.85 5 1 6 -5 34.74 31.49 3 1 -6 -5 30.60 23.18 8 -1 6 5 10.98 31.18 1 0 6 5 233.00 46.92 1 0 6 -5 218.95 42.98 3 0 -6 -5 227.51 30.44 8 0 6 -5 211.93 32.87 5 1 6 5 306.10 57.20 1 -1 -6 -5 282.62 31.16 8 -1 6 -5 274.60 34.52 5 -2 6 -5 195.91 33.73 5 -2 -6 -5 220.20 31.22 8 2 6 5 216.29 53.87 1 -3 -6 -5 577.63 40.16 8 3 6 5 581.28 78.92 1 -3 6 -5 558.32 44.56 5 -4 6 -5 2.47 28.50 5 4 6 5 9.02 39.36 1 -4 -6 -5 9.27 21.49 8 -5 -6 -5 1262.27 54.12 8 5 6 5 1238.38 116.78 1 -5 6 -5 1330.60 66.26 5 -6 -6 -5 1072.97 49.42 8 6 6 5 1170.99 120.21 1 -6 6 -5 1166.11 96.55 2 7 6 5 103.09 53.92 1 -7 -6 -5 50.80 21.62 4 -7 6 -5 75.37 41.90 2 -8 -6 -5 291.24 31.19 4 -9 -6 -5 93.99 24.42 4 -10 -6 -5 683.05 42.15 4 -11 -6 -5 872.51 45.03 4 -12 -6 -5 60.89 21.88 4 -13 6 -5 19.27 24.09 5 -13 -6 -5 -0.19 18.16 4 -14 6 -5 13.04 22.31 5 -14 -6 -5 -13.33 17.19 4 -15 6 -5 41.03 19.28 5 -15 -6 -5 39.56 15.25 4 -16 6 -5 23.75 14.11 5 19 7 -5 105.41 17.96 9 18 7 -5 56.00 19.77 9 17 -7 -5 -28.07 20.97 10 17 7 -5 10.82 23.01 9 16 7 -5 142.46 29.83 9 15 7 -5 46.38 28.42 9 14 -7 -5 11.71 24.27 10 14 7 -5 54.21 30.39 9 14 7 -5 43.78 22.49 6 13 -7 -5 8.06 23.60 10 13 7 -5 521.50 40.28 6 12 -7 -5 4.70 24.70 10 12 7 -5 -20.66 26.86 6 11 7 -5 32.73 28.45 6 11 -7 -5 11.26 24.32 10 10 -7 -5 -6.15 23.71 10 10 7 -5 1312.17 65.11 6 9 -7 -5 4970.90 100.29 8 9 7 -5 5169.54 217.72 3 8 -7 -5 652.36 42.13 8 8 7 -5 822.32 91.26 3 7 7 -5 13.72 19.65 11 7 7 -5 47.07 46.77 3 7 -7 -5 11.73 24.69 10 7 -7 -5 26.02 22.41 8 6 7 -5 95.10 22.01 11 6 7 -5 63.77 40.39 3 6 -7 -5 72.20 24.33 8 5 7 -5 65.04 23.38 11 5 7 -5 37.92 37.65 3 5 -7 -5 43.98 24.99 8 4 7 -5 1286.95 101.12 3 4 7 -5 1295.54 54.81 11 4 -7 -5 1252.62 57.23 8 3 7 -5 465.11 64.93 3 3 7 -5 489.93 37.43 11 3 -7 -5 463.38 39.89 8 2 7 -5 17.05 25.87 5 2 7 -5 40.07 30.93 3 2 -7 -5 34.46 25.46 8 1 7 -5 73.62 27.58 5 0 7 5 103.09 41.38 1 0 -7 -5 107.30 28.82 8 0 7 -5 127.54 32.09 5 -1 7 -5 425.60 44.14 5 -1 -7 -5 408.42 38.95 8 1 7 5 432.26 67.52 1 -2 7 -5 1943.27 75.33 5 -2 -7 -5 1909.14 68.35 8 3 7 5 25.50 43.37 1 -3 7 -5 4.40 28.03 5 -3 -7 -5 8.42 24.53 8 -4 7 -5 699.99 51.91 5 -4 -7 -5 765.05 51.47 8 4 7 5 676.26 89.87 1 -5 7 -5 1.58 30.06 5 -5 -7 -5 -3.00 23.00 8 5 7 5 -46.75 51.19 1 -6 7 -5 26.08 29.08 5 -6 -7 -5 35.11 21.85 8 -7 7 -5 1031.74 62.16 5 -8 7 -5 300.95 42.27 5 -9 7 -5 502.59 48.26 5 -10 7 -5 13.88 28.87 5 -11 7 -5 15.53 29.44 5 -11 -7 -5 -0.98 16.73 4 -12 7 -5 7.29 24.34 5 -13 7 -5 31.11 22.90 5 -14 7 -5 6.49 18.13 5 -15 7 -5 47.26 15.76 5 18 8 -5 270.10 22.70 9 17 8 -5 184.28 24.64 9 16 8 -5 35.26 21.92 9 15 8 -5 6.87 23.67 9 14 8 -5 73.21 29.02 9 13 8 -5 1.92 22.05 6 12 8 -5 228.65 32.07 6 11 8 -5 1007.14 56.70 6 10 8 -5 735.17 52.26 6 9 -8 -5 36.03 21.90 8 8 -8 -5 956.75 48.91 8 7 8 -5 129.95 50.42 3 7 -8 -5 137.63 27.26 8 6 8 -5 105.77 50.95 3 6 -8 -5 93.11 26.99 8 5 8 -5 187.66 25.88 11 5 8 -5 181.04 52.12 3 5 -8 -5 196.24 32.48 8 4 8 -5 -55.24 45.20 3 4 8 -5 24.08 20.34 11 3 8 -5 796.97 43.75 11 3 -8 -5 700.30 46.49 8 2 8 -5 165.92 28.20 11 2 -8 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27.27 6 14 4 -6 1919.94 77.21 9 14 4 -6 1947.19 72.55 6 13 4 -6 4223.59 110.62 9 13 4 -6 4248.76 104.93 6 12 4 -6 2286.02 149.54 3 12 4 -6 2222.38 80.57 9 12 -4 -6 2256.39 68.62 6 12 4 -6 2264.00 80.37 6 11 4 -6 1592.77 127.76 3 11 4 -6 1499.31 66.99 9 11 -4 -6 1582.62 58.68 6 11 4 -6 1644.84 69.93 6 10 4 -6 141.72 53.75 3 10 -4 -6 130.46 28.74 6 10 4 -6 133.02 34.17 6 9 4 -6 276.54 36.95 6 9 4 -6 297.54 63.15 3 9 -4 -6 224.90 29.06 6 8 4 -6 746.17 83.56 3 8 4 -6 699.23 42.00 11 8 -4 -6 701.14 41.09 8 8 -4 -6 696.42 40.39 6 8 4 -6 644.40 47.92 6 7 4 -6 1433.25 108.55 3 7 4 -6 1460.87 58.36 11 7 -4 -6 1367.01 53.74 8 7 4 -6 1381.36 44.38 7 7 -4 -6 1445.91 53.22 6 7 4 -6 1356.01 62.87 6 6 4 -6 16.38 25.67 6 6 4 -6 7.08 21.28 11 6 4 -6 7.27 36.17 3 6 4 -6 -41.16 21.46 7 6 -4 -6 3.11 20.06 6 5 4 -6 477.47 65.89 3 5 4 -6 483.23 37.83 11 5 -4 -6 452.24 40.07 8 5 4 -6 405.40 27.03 7 5 -4 -6 502.03 33.90 6 5 4 -6 428.40 38.33 6 4 4 -6 161.75 27.85 11 4 4 -6 143.50 45.03 3 4 -4 -6 151.62 26.13 8 4 4 -6 102.25 21.90 7 4 -4 -6 151.92 23.37 6 3 4 -6 1974.77 68.64 5 3 4 -6 1984.27 114.90 3 3 4 -6 2061.88 70.12 11 3 -4 -6 2035.27 65.71 8 3 4 -6 2063.27 50.56 7 3 -4 -6 2153.41 58.49 6 2 4 -6 5106.26 105.46 5 2 4 -6 5252.57 178.76 3 2 4 -6 5231.05 87.66 4 2 -4 -6 5141.84 101.05 8 2 4 -6 5326.33 78.01 7 1 4 -6 362.51 34.94 5 1 4 -6 390.29 54.26 3 1 4 -6 366.07 29.36 4 1 -4 -6 391.79 33.25 8 1 4 -6 361.91 27.22 7 1 4 -6 402.74 44.58 2 0 4 -6 25.27 23.74 5 0 4 -6 22.14 17.08 4 0 -4 -6 23.77 22.01 8 0 -4 -6 61.34 22.37 4 0 4 -6 -9.99 30.43 3 0 4 -6 11.10 20.49 7 0 4 -6 18.80 22.07 2 -1 4 -6 757.66 46.32 5 -1 4 -6 759.19 70.72 3 -1 4 -6 793.93 39.41 4 -1 -4 -6 784.52 41.42 4 -1 -4 -6 792.37 43.75 8 1 4 6 711.61 75.15 1 -1 4 -6 731.63 32.48 7 -1 4 -6 860.09 67.34 2 2 4 6 8.27 35.05 1 -2 4 -6 12.33 24.24 5 -2 4 -6 32.72 19.06 4 -2 -4 -6 34.38 26.63 8 -2 -4 -6 20.14 20.70 4 -2 4 -6 61.91 25.52 7 -2 4 -6 44.61 28.38 2 3 4 6 -10.95 39.41 1 -3 4 -6 7.88 24.05 5 -3 4 -6 22.39 16.08 4 -3 -4 -6 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702.19 45.18 11 3 5 -6 406.05 40.22 5 3 5 -6 391.53 37.64 11 3 -5 -6 412.65 35.94 8 3 5 -6 377.05 59.87 3 2 5 -6 -0.92 25.93 5 2 5 -6 -4.20 34.00 3 2 -5 -6 4.08 23.02 8 1 5 -6 3239.58 90.95 5 1 5 -6 3271.91 142.08 3 1 5 -6 3169.69 67.94 4 1 -5 -6 3248.95 85.29 8 0 5 -6 -16.46 17.52 4 0 -5 -6 7.43 21.69 8 0 5 -6 -17.11 31.58 3 0 5 -6 -17.39 25.35 5 -1 5 -6 104.07 30.91 5 -1 -5 -6 96.81 24.69 8 -1 5 -6 66.97 30.88 3 -2 5 -6 539.32 43.81 5 -2 -5 -6 490.50 34.66 4 -2 -5 -6 591.53 40.55 8 2 5 6 528.47 71.96 1 -2 5 -6 558.53 61.32 2 -3 5 -6 415.76 41.43 5 -3 -5 -6 401.13 32.99 4 3 5 6 422.73 71.43 1 -3 -5 -6 441.74 37.65 8 -3 5 -6 431.56 56.35 2 -4 5 -6 552.11 46.57 5 4 5 6 474.97 78.52 1 -4 -5 -6 533.54 37.47 4 -4 5 -6 565.14 65.47 2 -5 5 -6 255.81 36.32 5 5 5 6 226.18 59.75 1 -5 -5 -6 248.20 30.32 4 -5 -5 -6 313.00 31.51 8 -5 5 -6 329.79 56.25 2 6 5 6 521.71 84.76 1 -6 -5 -6 505.51 38.56 4 -6 -5 -6 549.18 37.06 8 -6 5 -6 472.47 66.19 2 -6 5 -6 557.13 48.49 5 -7 5 -6 181.02 37.02 5 -7 -5 -6 139.84 27.22 4 -8 5 -6 978.12 58.73 5 -8 -5 -6 1090.51 52.97 4 -9 5 -6 53.32 29.45 5 -9 -5 -6 69.29 25.94 4 -10 5 -6 1628.00 70.65 5 -10 -5 -6 1802.14 64.08 4 -11 5 -6 304.13 38.62 5 -11 -5 -6 247.06 30.30 4 -12 5 -6 5.22 23.73 5 -12 -5 -6 5.27 20.33 4 -13 5 -6 -3.38 20.15 5 -13 -5 -6 11.33 18.55 4 -14 5 -6 62.76 19.49 5 -14 -5 -6 82.71 18.29 4 -15 5 -6 136.01 17.15 5 -15 -5 -6 140.09 17.06 4 20 6 -6 12.01 15.23 10 20 6 -6 -2.42 11.13 9 19 -6 -6 -0.75 16.47 10 19 6 -6 12.92 15.88 9 18 6 -6 51.14 21.66 9 17 -6 -6 -2.93 20.96 10 17 6 -6 102.56 25.79 9 16 -6 -6 1.52 21.58 10 16 6 -6 -18.54 24.51 9 15 -6 -6 2.11 22.43 10 15 6 -6 -5.58 27.16 9 15 6 -6 19.04 21.80 6 14 6 -6 915.24 56.97 9 14 6 -6 857.82 48.01 6 13 6 -6 267.09 38.27 9 13 6 -6 288.21 36.13 6 12 6 -6 150.27 32.60 6 11 -6 -6 3.14 24.16 10 11 6 -6 271.40 38.51 6 10 6 -6 45.39 34.30 6 10 -6 -6 10.15 23.41 10 9 6 -6 453.79 74.92 3 9 -6 -6 379.35 33.51 8 9 6 -6 409.52 43.30 6 8 6 -6 -12.84 30.12 6 8 6 -6 -2.60 20.27 11 8 6 -6 -18.94 45.60 3 7 6 -6 105.27 24.06 11 7 6 -6 75.93 45.97 3 7 -6 -6 101.98 25.47 8 6 6 -6 1213.04 106.54 3 6 6 -6 1188.72 54.94 11 6 -6 -6 1176.73 55.36 8 5 6 -6 298.60 33.19 11 5 6 -6 214.30 55.23 3 5 -6 -6 265.56 32.77 8 4 6 -6 394.49 37.82 11 4 -6 -6 343.93 35.83 8 4 6 -6 347.54 61.44 3 3 6 -6 134.15 29.08 11 3 6 -6 102.84 41.23 3 3 -6 -6 110.45 29.16 8 2 6 -6 718.74 49.46 5 2 6 -6 709.70 74.28 3 2 -6 -6 692.57 46.70 8 1 6 -6 -0.59 26.99 5 1 -6 -6 4.30 23.33 8 1 6 -6 20.93 38.38 3 0 6 -6 1553.19 68.37 5 0 -6 -6 1579.14 64.11 8 -1 6 -6 862.86 53.63 5 -1 -6 -6 832.29 48.69 8 -2 6 -6 729.64 51.89 5 -2 -6 -6 741.45 46.24 8 -3 6 -6 72.58 29.09 5 -3 -6 -6 80.89 25.51 8 3 6 6 99.93 58.41 1 -3 6 -6 59.00 35.99 2 -4 6 -6 681.13 52.51 5 -4 -6 -6 716.86 44.36 8 4 6 6 620.99 88.67 1 -4 6 -6 791.76 79.25 2 -5 6 -6 18.22 28.29 5 -5 -6 -6 17.81 20.41 8 5 6 6 -15.34 48.19 1 -5 6 -6 2.63 36.41 2 -6 6 -6 593.38 49.46 5 -6 -6 -6 488.71 36.73 4 -6 -6 -6 559.93 36.86 8 -7 6 -6 137.96 35.21 5 -7 -6 -6 106.30 23.63 4 -8 6 -6 733.03 52.49 5 -8 -6 -6 713.27 40.88 4 -9 6 -6 -3.62 28.42 5 -9 -6 -6 -14.32 20.51 4 -10 6 -6 349.27 39.49 5 -10 -6 -6 358.95 31.26 4 -11 6 -6 182.81 31.88 5 -11 -6 -6 184.94 24.21 4 -12 6 -6 32.71 22.87 5 -12 -6 -6 49.34 18.28 4 -13 6 -6 91.86 21.65 5 -13 -6 -6 102.83 18.06 4 -14 6 -6 122.71 18.79 5 19 7 -6 0.66 11.70 9 18 7 -6 -2.49 15.69 9 17 7 -6 405.03 32.93 9 16 -7 -6 -26.94 20.25 10 16 7 -6 34.51 22.36 9 15 -7 -6 4.03 21.73 10 15 7 -6 46.62 25.21 9 15 7 -6 31.59 18.73 6 14 -7 -6 -6.25 22.61 10 14 7 -6 21.70 26.09 9 14 7 -6 13.45 22.40 6 13 7 -6 391.14 40.05 9 13 7 -6 369.20 36.79 6 12 -7 -6 7.04 23.35 10 12 7 -6 108.82 30.48 6 11 -7 -6 -11.16 22.44 10 11 7 -6 339.75 40.15 6 10 7 -6 -10.25 30.86 6 10 -7 -6 0.89 21.50 10 9 7 -6 77.23 32.18 6 9 -7 -6 65.81 24.78 8 8 7 -6 0.47 31.30 6 8 -7 -6 -2.38 26.65 8 7 7 -6 2520.69 152.97 3 7 7 -6 2434.38 71.50 11 7 -7 -6 2385.67 75.29 8 6 7 -6 2870.26 158.68 3 6 7 -6 2835.74 78.43 11 5 7 -6 548.46 76.07 3 5 7 -6 533.12 39.95 11 5 -7 -6 477.53 41.28 8 4 7 -6 339.71 35.76 11 4 -7 -6 273.51 35.90 8 4 7 -6 372.64 65.93 3 3 -7 -6 403.58 41.13 8 3 7 -6 388.10 63.27 3 3 7 -6 458.70 39.77 11 2 7 -6 633.67 49.17 5 2 7 -6 596.02 44.39 11 2 -7 -6 638.46 51.95 8 1 7 -6 288.60 37.94 5 1 -7 -6 277.03 36.88 8 0 7 -6 -1.54 27.15 5 0 -7 -6 127.78 45.06 8 -1 7 -6 1384.54 67.81 5 -1 -7 -6 1388.12 62.62 8 -2 7 -6 826.27 54.75 5 -2 -7 -6 860.97 50.12 8 -3 7 -6 1211.87 64.72 5 -3 -7 -6 1236.99 57.87 8 -4 7 -6 2121.94 82.97 5 -4 -7 -6 2133.40 71.60 8 -5 7 -6 37.92 30.02 5 -6 7 -6 381.05 44.07 5 -6 -7 -6 436.10 34.42 8 -7 7 -6 355.65 42.43 5 -8 7 -6 1909.93 75.23 5 -9 7 -6 598.44 46.17 5 -10 7 -6 122.71 29.16 5 -11 7 -6 19.34 22.51 5 -12 7 -6 -0.93 18.66 5 -13 7 -6 238.98 23.79 5 -14 7 -6 26.49 12.83 5 18 8 -6 74.17 13.66 9 17 8 -6 12.96 15.62 9 16 8 -6 30.31 19.92 9 15 8 -6 57.10 23.00 9 14 8 -6 112.63 27.56 9 14 8 -6 78.16 21.92 6 13 8 -6 1.90 23.74 9 13 8 -6 14.65 21.37 6 12 8 -6 55.61 26.63 6 11 8 -6 45.96 29.00 6 10 8 -6 5.33 28.33 6 9 -8 -6 423.70 34.86 8 9 8 -6 559.14 48.28 6 8 -8 -6 980.76 52.92 8 8 8 -6 1042.24 62.03 6 7 -8 -6 245.06 31.71 8 6 8 -6 699.19 41.54 11 6 -8 -6 629.26 45.33 8 5 8 -6 916.97 47.08 11 5 -8 -6 901.58 53.10 8 4 8 -6 45.06 21.76 11 4 -8 -6 10.09 25.08 8 3 8 -6 792.04 46.45 11 3 -8 -6 686.90 50.13 8 2 8 -6 283.80 33.87 11 2 -8 -6 254.02 38.46 8 1 8 -6 267.38 37.30 5 1 8 -6 230.68 32.47 11 1 -8 -6 299.61 39.21 8 0 8 -6 1132.65 61.27 5 0 -8 -6 1128.31 59.36 8 -1 8 -6 1025.04 58.85 5 -1 -8 -6 1023.49 55.14 8 -2 8 -6 1675.61 72.30 5 -2 -8 -6 1698.48 67.84 8 -3 8 -6 946.18 57.29 5 -3 -8 -6 957.86 52.30 8 -4 8 -6 586.24 49.50 5 -4 -8 -6 586.31 42.01 8 -5 8 -6 24.54 31.71 5 -6 8 -6 39.90 36.71 5 -6 -8 -6 17.77 17.85 8 -7 8 -6 1162.13 59.43 5 -8 8 -6 343.12 37.37 5 -9 8 -6 117.11 28.10 5 -10 8 -6 14.26 21.88 5 -11 8 -6 123.70 23.05 5 -12 8 -6 442.60 27.63 5 -13 8 -6 15.82 12.16 5 16 9 -6 3.26 13.85 9 15 9 -6 599.80 33.69 9 14 9 -6 145.42 24.16 9 13 9 -6 18.20 22.02 9 13 9 -6 9.96 17.49 6 12 9 -6 64.74 23.88 6 11 9 -6 273.98 32.88 6 10 9 -6 83.81 28.76 6 9 9 -6 294.07 39.29 6 9 -9 -6 255.01 27.37 8 8 9 -6 224.52 37.52 6 7 -9 -6 273.03 31.85 8 6 -9 -6 148.70 28.18 8 5 9 -6 130.31 21.55 11 5 -9 -6 157.67 31.21 8 4 9 -6 30.25 19.09 11 4 -9 -6 7.37 25.78 8 3 9 -6 105.60 22.76 11 3 -9 -6 138.12 31.37 8 2 9 -6 2.98 18.67 11 2 -9 -6 24.44 29.65 8 1 9 -6 1157.19 51.62 11 1 -9 -6 1175.81 60.71 8 0 9 -6 10.89 20.81 11 0 -9 -6 2.64 26.24 8 -1 9 -6 2338.64 80.52 5 -1 9 -6 2282.92 73.05 11 -1 -9 -6 2510.90 79.91 8 -2 9 -6 513.13 44.82 5 -2 -9 -6 499.96 39.84 8 -3 9 -6 472.54 42.51 5 -3 -9 -6 454.99 38.00 8 -4 9 -6 501.23 42.67 5 -4 -9 -6 458.81 37.11 8 -5 9 -6 160.42 31.99 5 -5 -9 -6 49.10 21.04 8 -6 9 -6 -2.13 24.07 5 -6 -9 -6 -1.89 17.39 8 -7 9 -6 213.05 30.51 5 -8 9 -6 326.05 32.27 5 -9 9 -6 -7.91 19.36 5 -10 9 -6 30.69 18.18 5 -11 9 -6 14.78 13.89 5 14 10 -6 160.94 19.54 9 13 10 -6 295.76 26.13 9 13 10 -6 118.50 17.22 6 12 10 -6 65.13 21.43 9 12 10 -6 90.79 19.26 6 11 10 -6 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32.01 6 6 -11 -6 24.03 17.75 8 5 -11 -6 245.44 28.96 8 4 -11 -6 56.35 23.06 8 3 -11 -6 11.02 21.21 8 2 -11 -6 283.31 31.39 8 1 -11 -6 104.10 25.83 8 0 -11 -6 186.22 27.36 8 -1 -11 -6 8.62 20.24 8 -2 -11 -6 9.60 22.38 8 -4 -11 -6 2.07 14.24 8 -5 -11 -6 132.58 16.43 8 8 12 -6 24.57 15.11 6 7 12 -6 32.60 18.28 6 6 12 -6 1.40 17.20 6 6 -12 -6 13.10 13.19 8 5 12 -6 45.04 20.11 6 5 -12 -6 44.19 15.60 8 4 12 -6 30.13 20.64 6 4 -12 -6 21.50 15.81 8 3 12 -6 5.60 18.51 6 2 12 -6 1.26 18.98 6 2 -12 -6 17.75 15.66 8 1 -12 -6 11.18 14.35 8 1 12 -6 233.48 25.64 6 0 12 -6 23.00 18.09 6 -1 12 -6 48.25 16.11 6 -1 -12 -6 55.84 16.41 8 -2 -12 -6 81.25 16.23 8 -3 -12 -6 321.75 20.19 8 20 0 -7 16.34 19.01 10 19 0 -7 -3.77 21.66 10 18 0 -7 -0.48 21.59 10 18 0 -7 12.63 15.41 6 17 0 -7 1.85 25.87 10 17 0 -7 21.16 24.37 9 17 0 -7 2.69 18.76 6 16 0 -7 1.45 24.86 10 16 0 -7 15.37 21.25 9 16 0 -7 39.80 25.59 6 15 0 -7 -6.06 26.96 10 15 0 -7 -7.93 22.80 9 15 0 -7 10.28 25.21 6 14 0 -7 -2.35 26.35 10 14 0 -7 -6.93 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26.02 4 -4 0 -10 119.50 18.81 7 -5 0 -10 -7.08 20.00 4 -6 0 -10 331.95 29.19 4 -7 0 -10 491.51 29.18 4 -8 0 -10 335.76 22.81 4 -9 0 -10 5.46 11.25 4 16 1 -10 45.07 16.06 6 15 -1 -10 34.89 17.75 6 15 1 -10 16.11 17.47 6 14 -1 -10 44.13 20.33 6 14 1 -10 31.08 20.18 6 13 -1 -10 -6.70 20.78 6 12 -1 -10 45.34 23.47 6 12 1 -10 30.28 23.44 6 11 1 -10 132.38 21.67 7 11 -1 -10 126.97 21.57 7 11 -1 -10 154.67 27.91 6 11 1 -10 131.45 27.82 6 10 1 -10 12.08 20.31 7 10 -1 -10 24.74 21.80 7 10 -1 -10 22.04 22.79 6 10 1 -10 30.36 25.08 6 9 1 -10 506.12 32.96 7 9 -1 -10 570.26 36.62 7 9 -1 -10 607.84 45.64 6 9 1 -10 543.04 41.55 6 8 1 -10 130.72 27.28 7 8 -1 -10 130.45 26.90 7 8 -1 -10 125.69 27.15 6 8 1 -10 134.27 29.75 6 7 1 -10 34.26 27.80 7 7 -1 -10 -4.88 26.09 7 7 -1 -10 23.91 21.80 6 7 1 -10 -2.68 23.39 6 6 1 -10 563.80 41.85 7 6 -1 -10 569.65 45.06 7 6 -1 -10 508.37 35.93 6 6 1 -10 547.50 39.20 6 5 1 -10 93.29 30.97 7 5 -1 -10 94.27 29.70 7 5 -1 -10 98.68 21.53 6 5 1 -10 90.88 24.49 6 4 1 -10 275.50 34.09 7 4 -1 -10 269.02 35.14 7 4 -1 -10 247.49 25.70 6 4 1 -10 225.52 26.33 6 3 1 -10 276.53 27.51 11 3 1 -10 354.68 36.22 7 3 -1 -10 346.73 37.30 7 2 1 -10 477.46 34.03 11 2 -1 -10 517.07 37.75 4 2 1 -10 519.46 40.43 7 2 -1 -10 514.30 40.03 7 1 1 -10 981.09 43.59 11 1 1 -10 938.39 47.25 4 1 -1 -10 964.77 45.92 4 1 1 -10 1005.50 45.33 7 1 -1 -10 999.68 50.17 7 0 1 -10 1029.75 44.14 11 0 1 -10 990.96 48.94 4 0 -1 -10 1057.84 48.70 4 0 1 -10 981.70 42.13 7 -1 1 -10 26.19 17.88 11 -1 1 -10 22.00 22.86 4 -1 -1 -10 22.30 23.14 4 -1 1 -10 8.13 22.63 7 -2 1 -10 309.29 26.41 11 -2 1 -10 297.54 30.29 4 -2 -1 -10 328.95 32.90 4 -2 1 -10 265.07 24.90 7 -2 -1 -10 285.36 27.15 7 -3 1 -10 162.85 26.82 4 -3 -1 -10 160.02 27.42 4 -3 1 -10 129.32 20.02 7 -3 -1 -10 146.36 22.24 7 -4 1 -10 214.48 27.27 4 -4 -1 -10 209.21 27.65 4 -4 -1 -10 172.48 20.26 7 -5 1 -10 3.37 19.71 4 -5 -1 -10 29.51 20.99 4 -6 1 -10 222.33 24.00 4 -6 -1 -10 214.74 25.64 4 -7 1 -10 20.24 16.12 4 -7 -1 -10 26.90 17.04 4 -8 1 -10 5.91 13.22 4 -8 -1 -10 5.76 14.43 4 -9 1 -10 4.74 10.13 4 -9 -1 -10 2.79 11.06 4 16 2 -10 62.96 15.33 6 15 2 -10 136.79 21.53 6 14 2 -10 114.22 25.96 6 13 -2 -10 63.63 20.66 6 13 2 -10 56.36 23.01 6 12 -2 -10 89.94 22.80 6 12 2 -10 90.91 27.11 6 11 -2 -10 221.59 23.99 7 11 -2 -10 268.72 29.81 6 11 2 -10 285.77 33.47 6 10 -2 -10 634.91 35.00 7 10 -2 -10 617.35 39.80 6 10 2 -10 645.38 43.84 6 9 2 -10 187.16 27.70 7 9 -2 -10 168.55 27.57 6 9 2 -10 218.40 32.03 6 8 2 -10 1598.05 50.85 7 8 -2 -10 1126.01 48.96 7 8 -2 -10 1124.43 48.82 6 8 2 -10 1514.40 70.05 6 7 2 -10 -11.29 26.54 7 7 -2 -10 10.08 25.96 7 7 -2 -10 19.85 20.62 6 7 2 -10 4.53 23.54 6 6 2 -10 -5.01 25.97 7 6 -2 -10 46.18 29.97 7 6 -2 -10 -9.78 18.05 6 6 2 -10 -25.32 23.70 6 5 2 -10 605.91 40.47 7 5 -2 -10 558.35 34.30 6 5 2 -10 550.18 38.68 6 4 2 -10 37.96 24.35 11 4 2 -10 -8.59 20.56 6 3 2 -10 937.69 45.39 11 3 2 -10 1075.50 45.13 7 2 2 -10 134.12 24.36 11 2 -2 -10 160.37 25.45 4 1 2 -10 244.41 28.60 11 1 -2 -10 262.91 29.35 4 1 2 -10 249.35 28.71 7 1 -2 -10 283.92 34.75 7 0 2 -10 25.96 20.55 11 0 2 -10 12.11 20.73 4 0 -2 -10 29.87 25.06 4 0 2 -10 21.29 22.79 7 0 -2 -10 19.61 26.52 7 -1 2 -10 533.18 35.56 11 -1 2 -10 543.21 36.52 4 -1 -2 -10 558.85 35.93 4 -1 2 -10 494.81 30.10 7 -1 -2 -10 569.68 36.93 7 -2 2 -10 64.74 20.61 11 -2 2 -10 84.20 22.98 4 -2 -2 -10 104.98 23.92 4 -2 2 -10 90.88 20.42 7 -3 2 -10 361.04 29.00 11 -3 2 -10 346.28 29.76 4 -3 -2 -10 376.86 31.10 4 -3 -2 -10 348.67 26.73 7 -4 2 -10 32.39 17.51 11 -4 2 -10 30.06 19.31 4 -4 -2 -10 34.39 19.85 4 -4 -2 -10 23.87 17.24 7 -5 2 -10 31.31 17.79 4 -5 -2 -10 55.51 20.51 4 -6 2 -10 -4.44 14.90 4 -6 -2 -10 12.97 17.83 4 -7 2 -10 17.72 14.13 4 -7 -2 -10 17.43 16.61 4 -8 2 -10 6.87 10.96 4 -8 -2 -10 -1.52 13.07 4 -9 -2 -10 196.06 15.67 4 16 3 -10 285.03 19.65 6 14 3 -10 268.50 26.59 6 13 3 -10 9.83 20.24 6 12 3 -10 74.07 24.66 6 11 -3 -10 623.15 30.44 7 11 3 -10 645.93 41.23 6 10 -3 -10 333.38 30.28 6 10 3 -10 379.52 35.96 6 9 -3 -10 169.74 26.50 7 9 -3 -10 142.27 24.05 6 9 3 -10 171.83 29.40 6 8 -3 -10 294.11 31.87 7 8 -3 -10 273.20 28.12 6 8 3 -10 234.85 32.43 6 7 -3 -10 204.36 24.49 6 7 3 -10 205.99 30.09 6 6 3 -10 401.79 32.68 7 6 3 -10 423.45 36.78 6 5 3 -10 371.82 33.59 11 5 3 -10 356.83 33.22 7 5 3 -10 356.28 33.94 6 4 3 -10 343.27 32.13 11 4 3 -10 361.07 32.17 7 4 3 -10 326.97 31.71 6 3 3 -10 46.03 39.97 11 3 3 -10 20.34 24.79 7 3 3 -10 21.52 20.01 6 2 3 -10 89.48 23.41 11 2 3 -10 114.58 26.94 7 1 3 -10 8.13 20.40 11 1 -3 -10 9.09 18.11 4 1 3 -10 19.68 23.43 7 0 3 -10 -9.72 19.29 11 0 -3 -10 -6.40 18.19 4 -1 3 -10 8.82 19.90 11 -1 -3 -10 -3.35 18.18 4 -2 3 -10 196.59 26.26 11 -2 3 -10 226.73 25.26 4 -2 -3 -10 227.51 25.49 4 -2 -3 -10 198.33 26.26 7 -3 3 -10 23.27 19.12 11 -3 3 -10 -5.00 17.37 4 -3 -3 -10 18.48 17.75 4 -4 3 -10 195.27 24.23 11 -4 3 -10 212.93 22.59 4 -4 -3 -10 178.76 23.10 4 -4 -3 -10 211.81 21.06 7 -5 3 -10 23.57 15.64 11 -5 3 -10 -2.36 14.40 4 -5 -3 -10 -9.23 17.23 4 -6 3 -10 287.64 20.88 4 -6 -3 -10 301.56 23.59 4 -7 3 -10 76.87 13.43 4 -7 -3 -10 78.29 15.75 4 -8 -3 -10 90.39 13.75 4 15 4 -10 160.15 21.15 6 14 4 -10 52.37 18.76 6 13 4 -10 502.97 32.49 6 12 4 -10 57.34 21.60 6 11 4 -10 253.74 29.44 6 10 -4 -10 128.39 24.02 7 10 4 -10 124.05 26.77 6 9 -4 -10 37.14 22.33 7 9 4 -10 54.15 26.08 6 8 4 -10 368.35 35.68 6 7 4 -10 4.39 23.51 6 6 4 -10 90.27 26.11 6 5 4 -10 157.73 26.96 11 5 4 -10 136.00 27.43 6 4 4 -10 208.54 29.52 11 4 4 -10 190.56 26.59 6 3 4 -10 16.94 21.45 11 3 4 -10 29.68 19.64 6 2 4 -10 96.49 25.57 11 1 4 -10 79.89 24.81 11 0 4 -10 2.87 20.51 11 0 -4 -10 -17.05 16.45 4 -1 4 -10 331.57 30.83 11 -1 -4 -10 325.34 25.04 4 -2 4 -10 29.54 19.47 11 -2 -4 -10 34.16 17.89 4 -3 4 -10 74.66 22.12 11 -3 -4 -10 92.86 18.36 4 -3 -4 -10 91.68 20.72 7 -4 4 -10 4.06 17.78 11 -4 -4 -10 17.01 15.72 4 -5 4 -10 161.89 21.15 11 -5 -4 -10 176.66 18.75 4 -6 4 -10 157.55 18.71 11 -6 -4 -10 148.88 16.47 4 -7 -4 -10 201.07 15.64 4 15 5 -10 78.12 16.07 6 14 5 -10 409.60 24.64 6 13 5 -10 116.98 19.79 6 12 5 -10 261.69 26.50 6 11 5 -10 97.66 24.37 6 10 -5 -10 284.02 24.20 7 10 5 -10 288.65 30.28 6 9 5 -10 260.27 32.09 6 8 5 -10 12.08 23.87 6 7 5 -10 6.53 23.79 6 6 5 -10 -5.54 22.25 6 5 5 -10 230.03 27.88 11 5 5 -10 267.10 36.27 6 4 5 -10 37.32 21.69 11 4 5 -10 12.74 18.80 6 3 5 -10 308.49 31.36 11 3 5 -10 332.53 28.36 6 2 5 -10 589.98 37.35 11 1 5 -10 78.14 22.52 11 0 5 -10 187.28 26.23 11 -1 5 -10 26.77 18.98 11 -2 5 -10 12.73 19.12 11 -3 5 -10 336.09 28.50 11 -3 -5 -10 322.22 24.82 7 -4 5 -10 415.92 28.71 11 -5 5 -10 84.54 18.41 11 -6 5 -10 18.19 13.12 11 13 6 -10 446.40 25.17 6 12 6 -10 408.22 26.53 6 11 6 -10 11.70 18.21 6 10 6 -10 4.25 19.38 6 9 6 -10 2.00 20.04 6 8 6 -10 -9.17 21.47 6 7 6 -10 10.41 21.36 6 6 6 -10 6.81 20.80 6 5 6 -10 21.38 21.10 6 4 6 -10 196.16 25.18 11 4 6 -10 233.72 25.48 6 3 6 -10 19.85 19.86 11 2 6 -10 17.39 19.15 11 1 6 -10 121.14 22.78 11 0 6 -10 66.57 20.41 11 -1 6 -10 75.53 20.19 11 -2 6 -10 370.23 27.57 11 -3 6 -10 341.32 25.95 11 -3 -6 -10 305.76 21.19 7 -4 6 -10 96.99 17.99 11 -5 6 -10 62.88 13.56 11 12 7 -10 -6.12 12.63 6 11 7 -10 165.44 18.57 6 10 7 -10 49.53 17.60 6 9 -7 -10 131.55 17.73 7 9 7 -10 88.74 19.80 6 8 7 -10 90.72 19.90 6 7 7 -10 80.97 20.63 6 6 7 -10 -13.19 19.84 6 5 7 -10 27.36 19.70 6 4 7 -10 229.93 22.92 6 3 7 -10 18.79 16.58 11 2 7 -10 25.28 16.54 11 1 7 -10 88.45 18.49 11 0 7 -10 227.53 22.62 11 -1 7 -10 -9.31 15.39 11 -2 7 -10 194.46 19.61 11 -3 7 -10 5.72 12.12 11 -4 7 -10 137.93 14.76 11 9 8 -10 53.57 14.25 6 8 8 -10 -3.55 13.35 6 7 8 -10 57.39 16.53 6 6 8 -10 98.89 18.10 6 5 8 -10 265.46 20.72 6 1 8 -10 51.35 13.16 11 0 8 -10 172.83 16.52 11 -1 8 -10 322.82 18.95 11 14 0 -11 -3.72 13.42 6 13 0 -11 16.55 15.08 6 12 0 -11 -3.09 16.65 6 11 0 -11 15.14 17.67 6 10 0 -11 -30.74 18.80 7 10 0 -11 -2.09 17.55 6 9 0 -11 27.32 20.76 7 9 0 -11 7.34 18.49 6 8 0 -11 -9.11 22.08 7 8 0 -11 -0.86 18.14 6 7 0 -11 15.61 23.16 7 7 0 -11 2.34 16.89 6 6 0 -11 6.95 23.85 7 6 0 -11 -3.34 16.15 6 5 0 -11 -5.93 24.22 7 4 0 -11 8.30 24.66 7 3 0 -11 87.12 34.90 7 2 0 -11 25.51 22.67 7 1 0 -11 -25.30 22.56 7 0 0 -11 29.04 19.59 7 -1 0 -11 -2.10 17.53 7 -2 0 -11 8.42 16.77 4 -2 0 -11 23.79 16.84 7 -3 0 -11 2.90 15.41 4 -4 0 -11 18.58 15.39 4 -5 0 -11 -0.61 12.07 4 15 1 -11 6.35 10.91 6 14 1 -11 9.96 13.43 6 13 1 -11 108.25 20.32 6 12 -1 -11 177.29 21.28 6 12 1 -11 184.18 22.23 6 11 -1 -11 185.69 22.06 6 11 1 -11 192.87 23.37 6 10 -1 -11 119.80 18.95 7 10 -1 -11 142.62 21.21 6 9 1 -11 9.56 20.95 7 9 -1 -11 17.60 20.72 7 9 -1 -11 0.58 17.44 6 8 1 -11 -25.07 21.32 7 8 -1 -11 -13.12 22.36 7 8 -1 -11 -11.43 17.93 6 8 1 -11 -10.14 15.66 6 7 1 -11 390.02 29.91 7 7 -1 -11 396.64 31.74 7 7 -1 -11 385.15 26.82 6 6 1 -11 41.94 23.42 7 6 -1 -11 19.21 24.14 7 6 -1 -11 26.93 15.77 6 5 1 -11 29.77 24.13 7 5 -1 -11 16.82 24.53 7 4 1 -11 77.88 24.26 7 4 -1 -11 85.74 25.85 7 3 1 -11 46.85 24.71 7 3 -1 -11 30.78 25.80 7 2 1 -11 771.70 35.00 7 2 -1 -11 858.54 38.06 7 1 1 -11 852.26 34.98 7 1 -1 -11 936.42 38.85 7 0 1 -11 137.97 21.59 7 0 -1 -11 132.50 23.65 7 -1 1 -11 21.20 17.25 7 -1 -1 -11 23.52 16.99 7 -2 -1 -11 93.27 18.33 4 -2 -1 -11 242.72 20.30 7 -3 -1 -11 316.49 23.88 4 -3 -1 -11 314.41 18.45 7 -4 -1 -11 204.34 19.52 4 -5 -1 -11 216.62 18.29 4 -6 -1 -11 40.69 11.06 4 14 2 -11 10.02 12.87 6 13 2 -11 77.73 16.72 6 10 -2 -11 59.76 19.14 7 10 2 -11 35.79 19.75 6 9 -2 -11 5.11 19.85 7 9 2 -11 2.50 18.68 6 8 -2 -11 142.23 23.64 7 8 2 -11 193.00 23.94 6 7 -2 -11 14.83 22.08 7 7 2 -11 -5.95 16.82 6 6 -2 -11 280.80 29.27 7 6 2 -11 264.92 27.14 7 6 2 -11 290.68 26.11 6 5 2 -11 450.58 31.36 7 5 -2 -11 436.96 33.06 7 4 2 -11 318.33 28.50 7 3 2 -11 196.73 24.98 7 2 2 -11 112.44 24.38 7 2 -2 -11 133.64 26.15 7 1 -2 -11 19.56 22.85 7 0 -2 -11 79.88 21.84 7 -1 -2 -11 18.99 19.27 7 -2 -2 -11 225.34 20.03 7 -3 -2 -11 71.31 15.94 4 -3 -2 -11 74.99 14.35 7 -4 -2 -11 72.86 14.45 4 -5 -2 -11 -9.20 11.27 4 14 3 -11 48.84 13.49 6 12 3 -11 4.99 18.81 6 11 3 -11 52.83 19.43 6 10 -3 -11 -17.04 17.15 7 10 3 -11 -6.42 17.77 6 9 -3 -11 160.16 21.81 7 9 3 -11 129.01 22.57 6 8 -3 -11 72.71 20.53 7 8 3 -11 77.43 19.93 6 7 3 -11 1002.65 41.11 6 6 3 -11 -3.78 17.81 6 4 -3 -11 53.58 29.06 7 3 -3 -11 65.11 28.99 7 1 3 -11 132.97 18.86 11 1 -3 -11 26.85 19.39 7 0 3 -11 20.26 15.59 11 0 -3 -11 23.86 19.99 7 -1 3 -11 9.61 13.85 11 -1 -3 -11 4.31 16.37 7 -2 -3 -11 95.28 16.53 7 13 4 -11 10.94 9.90 6 12 4 -11 23.50 14.64 6 11 4 -11 12.90 15.59 6 10 4 -11 246.26 23.49 6 9 -4 -11 22.72 16.99 7 9 4 -11 27.64 19.06 6 8 4 -11 200.00 23.73 6 7 4 -11 44.60 19.48 6 6 -4 -11 738.11 35.57 7 6 4 -11 779.02 33.52 6 5 -4 -11 101.16 22.54 7 4 -4 -11 103.72 24.38 7 3 -4 -11 60.83 23.49 7 2 4 -11 72.85 17.85 11 2 -4 -11 85.37 22.20 7 1 4 -11 11.50 14.89 11 1 -4 -11 1.24 21.36 7 0 4 -11 48.51 15.87 11 0 -4 -11 29.18 17.59 7 -1 4 -11 4.76 14.23 11 -1 -4 -11 1.97 15.39 7 -2 4 -11 77.71 15.02 11 -2 -4 -11 37.32 13.53 7 -3 4 -11 5.36 11.06 11 12 5 -11 167.03 15.76 6 11 5 -11 77.14 15.16 6 10 5 -11 42.07 15.21 6 9 -5 -11 149.79 16.66 7 9 5 -11 161.63 20.15 6 8 -5 -11 14.45 14.59 7 8 5 -11 22.55 17.19 6 7 -5 -11 111.77 25.54 7 7 5 -11 84.92 19.10 6 6 -5 -11 81.44 21.17 7 6 5 -11 54.84 16.43 6 5 -5 -11 141.39 22.89 7 4 -5 -11 18.07 23.27 7 3 -5 -11 34.35 20.24 7 2 -5 -11 33.56 19.02 7 1 5 -11 1.47 13.67 11 1 -5 -11 11.99 16.83 7 0 5 -11 130.00 17.41 11 -1 5 -11 328.09 21.43 11 -1 -5 -11 351.21 20.27 7 -2 5 -11 229.34 17.13 11 9 6 -11 122.53 15.07 6 8 6 -11 291.46 19.82 6 7 -6 -11 18.60 16.34 7 7 6 -11 -1.30 13.12 6 6 -6 -11 247.01 20.02 7 5 -6 -11 153.27 19.52 7 4 -6 -11 51.71 17.99 7 3 -6 -11 0.01 16.65 7 2 -6 -11 -2.52 15.31 7 1 -6 -11 31.34 14.68 7 0 -6 -11 7.56 11.98 7 4 -7 -11 -12.71 12.33 7 7 0 -12 84.76 17.63 7 6 0 -12 -1.24 17.06 7 5 0 -12 234.17 20.88 7 4 0 -12 357.37 22.77 7 3 0 -12 -16.03 16.89 7 2 0 -12 34.82 16.46 7 8 -1 -12 199.46 18.44 7 7 -1 -12 311.86 20.27 7 6 -1 -12 12.47 16.64 7 5 -1 -12 20.99 16.02 7 4 -1 -12 9.37 15.27 7 3 -1 -12 80.81 17.40 7 2 -1 -12 76.95 17.36 7 1 -1 -12 -6.64 13.99 7 8 -2 -12 -7.37 13.66 7 7 -2 -12 443.17 22.54 7 6 -2 -12 27.96 16.03 7 5 -2 -12 16.76 16.42 7 4 -2 -12 55.02 16.69 7 3 -2 -12 336.42 22.05 7 2 -2 -12 3.83 14.16 7 1 -2 -12 37.18 13.37 7 8 -3 -12 100.57 13.91 7 7 -3 -12 4.43 13.20 7 6 -3 -12 1.91 14.15 7 5 -3 -12 41.89 14.46 7 4 -3 -12 54.34 15.46 7 3 -3 -12 10.62 13.89 7 2 -3 -12 20.23 13.07 7 6 -4 -12 157.39 14.77 7 5 -4 -12 203.00 16.40 7 4 -4 -12 161.81 15.71 7 3 -4 -12 104.16 14.18 7 0 0 0 0.00 0.00 0 17 1 -1 -0.17 24.96 10 ; _shelx_hkl_checksum 12038 _olex2_date_sample_data_collection 2018-04-12 _olex2_date_sample_submission 2018-04-09 _olex2_exptl_crystal_mounting_method 'in fomblin film on a micromount' _olex2_submission_original_sample_id RA-308-004 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.355 _oxdiff_exptl_absorpt_empirical_full_min 0.703 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.63704(16) 0.4605(3) 0.5418(3) 0.0349(6) Uani 1 1 d . . . . . H1A H 0.612506 0.525683 0.575875 0.042 Uiso 1 1 calc R . . . . H1B H 0.626167 0.465383 0.441338 0.042 Uiso 1 1 calc R . . . . C2 C 0.60565(16) 0.3518(3) 0.5820(3) 0.0333(6) Uani 1 1 d . . . . . C3 C 0.65020(15) 0.2460(2) 0.5891(2) 0.0297(6) Uani 1 1 d . . . . . C4 C 0.72207(15) 0.2553(2) 0.5850(2) 0.0281(6) Uani 1 1 d . . . . . H4 H 0.749181 0.186222 0.589189 0.034 Uiso 1 1 calc R . . . . C5 C 0.76314(17) 0.3643(2) 0.5744(3) 0.0322(6) Uani 1 1 d . . . . . C6 C 0.82471(17) 0.3726(2) 0.7008(3) 0.0312(6) Uani 1 1 d . . . . . C7 C 0.89351(17) 0.3207(3) 0.7369(3) 0.0356(7) Uani 1 1 d . . . . . H7 H 0.910197 0.272323 0.674368 0.043 Uiso 1 1 calc R . . . . C8 C 0.93774(18) 0.3405(3) 0.8658(3) 0.0413(7) Uani 1 1 d . . . . . C9 C 0.91096(18) 0.4099(3) 0.9564(3) 0.0400(7) Uani 1 1 d . . . . . H9 H 0.940686 0.421844 1.044600 0.048 Uiso 1 1 calc R . . . . C10 C 0.84208(17) 0.4626(3) 0.9225(3) 0.0361(7) Uani 1 1 d . . . . . H10 H 0.824257 0.509284 0.985250 0.043 Uiso 1 1 calc R . . . . C11 C 0.80153(17) 0.4431(2) 0.7928(3) 0.0328(6) Uani 1 1 d . . . . . O12 O 0.73300(12) 0.48891(17) 0.74223(18) 0.0364(5) Uani 1 1 d . . . . . C13 C 0.71852(17) 0.4708(2) 0.5948(3) 0.0335(6) Uani 1 1 d . . . . . H13 H 0.737100 0.538007 0.551076 0.040 Uiso 1 1 calc R . . . . O14 O 0.54341(13) 0.3512(2) 0.6062(2) 0.0450(6) Uani 1 1 d . . . . . C15 C 0.61816(16) 0.1301(3) 0.5957(3) 0.0321(6) Uani 1 1 d . . . . . C16 C 0.63368(16) 0.0444(3) 0.5106(3) 0.0341(6) Uani 1 1 d . . . . . H16 H 0.661671 0.063302 0.445549 0.041 Uiso 1 1 calc R . . . . C17 C 0.60988(18) -0.0680(3) 0.5167(3) 0.0410(7) Uani 1 1 d . . . . . C18 C 0.56846(19) -0.0941(3) 0.6113(3) 0.0446(8) Uani 1 1 d . . . . . H18 H 0.552360 -0.170419 0.618601 0.053 Uiso 1 1 calc R . . . . C19 C 0.55035(18) -0.0107(3) 0.6949(3) 0.0447(8) Uani 1 1 d . . . . . H19 H 0.521369 -0.030119 0.758184 0.054 Uiso 1 1 calc R . . . . C20 C 0.57383(17) 0.1011(3) 0.6880(3) 0.0388(7) Uani 1 1 d . . . . . C21 C 0.6293(2) -0.1593(3) 0.4251(4) 0.0537(9) Uani 1 1 d D U . . . H21A H 0.637457 -0.124720 0.340114 0.064 Uiso 0.723(10) 1 calc R . P A 1 H21B H 0.588691 -0.215328 0.401318 0.064 Uiso 0.723(10) 1 calc R . P A 1 H21C H 0.590117 -0.217234 0.420640 0.064 Uiso 0.277(10) 1 calc R . P A 2 H21D H 0.619233 -0.122869 0.334337 0.064 Uiso 0.277(10) 1 calc R . P A 2 C22 C 0.6992(3) -0.2186(4) 0.5013(7) 0.0413(13) Uani 0.723(10) 1 d D U P A 1 H22 H 0.699843 -0.248696 0.589069 0.050 Uiso 0.723(10) 1 calc R . P A 1 C22A C 0.6950(8) -0.2269(12) 0.4279(19) 0.059(4) Uani 0.277(10) 1 d D U P A 2 H22A H 0.703642 -0.270151 0.353175 0.070 Uiso 0.277(10) 1 calc R . P A 2 C23 C 0.7592(3) -0.2306(4) 0.4519(6) 0.0536(16) Uani 0.723(10) 1 d D U P A 1 H23A H 0.760176 -0.201397 0.364409 0.064 Uiso 0.723(10) 1 calc R . P A 1 H23B H 0.801128 -0.268325 0.504020 0.064 Uiso 0.723(10) 1 calc R . P A 1 C23A C 0.7413(11) -0.2205(13) 0.5476(17) 0.062(5) Uani 0.277(10) 1 d D U P A 2 H23C H 0.729206 -0.175645 0.618058 0.075 Uiso 0.277(10) 1 calc R . P A 2 H23D H 0.786539 -0.260857 0.563056 0.075 Uiso 0.277(10) 1 calc R . P A 2 O24 O 0.55530(14) 0.1779(2) 0.7778(2) 0.0473(6) Uani 1 1 d . . . . . H24 H 0.552(3) 0.245(4) 0.732(5) 0.071 Uiso 1 1 d R . . . . C25 C 0.78615(18) 0.3624(2) 0.4362(3) 0.0352(6) Uani 1 1 d D U . . . H25A H 0.818897 0.296114 0.434260 0.042 Uiso 0.43(4) 1 calc R . P B 1 H25B H 0.741783 0.351704 0.362753 0.042 Uiso 0.43(4) 1 calc R . P B 1 H25C H 0.810090 0.288125 0.427308 0.042 Uiso 0.57(4) 1 calc R . P B 2 H25D H 0.741186 0.366416 0.362898 0.042 Uiso 0.57(4) 1 calc R . P B 2 C26 C 0.8243(12) 0.4674(18) 0.409(2) 0.042(3) Uani 0.43(4) 1 d D U P B 1 H26 H 0.868999 0.489485 0.468549 0.051 Uiso 0.43(4) 1 calc R . P B 1 C26A C 0.8375(9) 0.4567(13) 0.4139(18) 0.042(2) Uani 0.57(4) 1 d D U P B 2 H26A H 0.881475 0.466486 0.481204 0.050 Uiso 0.57(4) 1 calc R . P B 2 C27 C 0.7958(14) 0.5314(12) 0.3007(13) 0.041(3) Uani 0.43(4) 1 d D U P B 1 H27A H 0.751077 0.509195 0.241343 0.049 Uiso 0.43(4) 1 calc R . P B 1 H27B H 0.820215 0.599015 0.283033 0.049 Uiso 0.43(4) 1 calc R . P B 1 C27A C 0.8263(12) 0.5273(10) 0.3080(11) 0.047(2) Uani 0.57(4) 1 d D U P B 2 H27C H 0.783037 0.520557 0.238291 0.056 Uiso 0.57(4) 1 calc R . P B 2 H27D H 0.861599 0.584509 0.301965 0.056 Uiso 0.57(4) 1 calc R . P B 2 C28 C 1.0133(2) 0.2903(4) 0.9058(4) 0.0637(11) Uani 1 1 d D U . . . H28A H 1.047138 0.338385 0.866617 0.076 Uiso 0.806(8) 1 calc R . P C 1 H28B H 1.029600 0.294604 1.005949 0.076 Uiso 0.806(8) 1 calc R . P C 1 H28D H 1.041578 0.343609 0.973969 0.076 Uiso 0.194(8) 1 calc R . P C 2 H28C H 1.007638 0.219266 0.955743 0.076 Uiso 0.194(8) 1 calc R . P C 2 C29 C 1.0206(3) 0.1747(4) 0.8651(5) 0.0565(13) Uani 0.806(8) 1 d D U P C 1 H29 H 0.990576 0.117849 0.892639 0.068 Uiso 0.806(8) 1 calc R . P C 1 C29A C 1.0604(10) 0.2620(18) 0.8206(17) 0.060(3) Uani 0.194(8) 1 d D U P C 2 H29A H 1.094217 0.311818 0.791932 0.072 Uiso 0.194(8) 1 calc R . P C 2 C30 C 1.0701(4) 0.1421(8) 0.7862(9) 0.085(2) Uani 0.806(8) 1 d D U P C 1 H30A H 1.100544 0.197672 0.757597 0.101 Uiso 0.806(8) 1 calc R . P C 1 H30B H 1.073198 0.064276 0.761242 0.101 Uiso 0.806(8) 1 calc R . P C 1 C30A C 1.049(2) 0.150(2) 0.786(5) 0.078(6) Uani 0.194(8) 1 d D U P C 2 H30C H 1.013518 0.106724 0.820227 0.093 Uiso 0.194(8) 1 calc R . P C 2 H30D H 1.076000 0.114288 0.728055 0.093 Uiso 0.194(8) 1 calc R . P C 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0366(16) 0.0343(15) 0.0329(14) -0.0007(11) 0.0057(11) 0.0098(13) C2 0.0366(16) 0.0403(16) 0.0222(12) -0.0043(11) 0.0049(10) 0.0034(13) C3 0.0326(14) 0.0334(14) 0.0223(11) -0.0005(10) 0.0047(10) 0.0004(12) C4 0.0343(15) 0.0273(13) 0.0223(11) -0.0030(10) 0.0056(10) 0.0022(12) C5 0.0475(17) 0.0243(13) 0.0246(12) -0.0003(10) 0.0075(11) -0.0012(12) C6 0.0426(16) 0.0265(13) 0.0252(12) -0.0006(10) 0.0092(11) -0.0063(12) C7 0.0398(16) 0.0367(16) 0.0308(13) -0.0049(11) 0.0089(12) 0.0016(13) C8 0.0389(17) 0.0429(17) 0.0395(15) -0.0062(13) 0.0028(13) 0.0001(14) C9 0.0486(19) 0.0387(16) 0.0295(13) -0.0058(12) 0.0016(12) -0.0064(14) C10 0.0459(18) 0.0318(15) 0.0303(13) -0.0071(11) 0.0077(12) -0.0050(13) C11 0.0443(17) 0.0241(13) 0.0298(13) -0.0002(10) 0.0077(12) -0.0035(12) O12 0.0481(13) 0.0322(10) 0.0275(9) -0.0059(8) 0.0052(8) 0.0037(9) C13 0.0474(18) 0.0276(14) 0.0251(13) -0.0005(10) 0.0071(11) 0.0008(13) O14 0.0424(13) 0.0521(14) 0.0446(12) 0.0006(10) 0.0185(10) 0.0095(11) C15 0.0304(14) 0.0367(15) 0.0271(12) 0.0029(11) 0.0015(10) -0.0031(12) C16 0.0317(14) 0.0363(15) 0.0328(14) 0.0042(12) 0.0038(11) -0.0040(12) C17 0.0419(17) 0.0349(16) 0.0405(15) 0.0043(12) -0.0029(13) -0.0053(14) C18 0.0469(19) 0.0411(17) 0.0392(15) 0.0108(14) -0.0048(13) -0.0164(15) C19 0.0390(17) 0.060(2) 0.0327(15) 0.0106(14) 0.0021(12) -0.0166(16) C20 0.0388(17) 0.0505(18) 0.0244(12) 0.0028(13) 0.0016(11) -0.0079(15) C21 0.060(2) 0.0310(16) 0.069(2) -0.0041(16) 0.0113(18) -0.0082(16) C22 0.055(3) 0.025(2) 0.044(3) -0.004(2) 0.012(3) -0.005(2) C22A 0.076(9) 0.030(7) 0.067(10) -0.003(8) 0.009(7) -0.001(6) C23 0.062(3) 0.032(2) 0.064(4) -0.004(2) 0.007(3) 0.000(2) C23A 0.056(9) 0.040(8) 0.084(11) -0.002(7) 0.002(8) -0.014(7) O24 0.0551(15) 0.0564(15) 0.0333(11) 0.0014(10) 0.0160(10) -0.0028(12) C25 0.0468(17) 0.0342(14) 0.0274(13) -0.0011(11) 0.0140(12) -0.0003(13) C26 0.054(6) 0.038(4) 0.038(4) 0.000(3) 0.017(4) 0.001(4) C26A 0.058(5) 0.038(4) 0.039(3) -0.001(3) 0.031(3) -0.004(4) C27 0.041(7) 0.045(4) 0.044(4) 0.009(3) 0.028(5) -0.002(5) C27A 0.046(6) 0.052(4) 0.053(4) 0.005(3) 0.034(4) -0.013(5) C28 0.045(2) 0.080(3) 0.058(2) -0.0218(19) -0.0061(16) 0.0190(19) C29 0.041(2) 0.054(3) 0.066(3) 0.000(2) -0.006(2) 0.013(2) C29A 0.048(6) 0.068(6) 0.059(6) -0.012(5) 0.000(4) 0.024(5) C30 0.069(4) 0.109(4) 0.060(3) -0.029(3) -0.022(3) 0.068(3) C30A 0.066(12) 0.078(8) 0.076(10) -0.027(8) -0.013(10) 0.024(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 1 -2 0 0.0211 -1 2 0 0.0221 1 0 -2 0.2001 -1 0 2 0.2001 1 0 0 0.0162 -1 0 0 0.0100 5 2 0 0.0174 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H1A C1 H1B 107.7 . . ? C2 C1 H1A 108.9 . . ? C2 C1 H1B 108.9 . . ? C2 C1 C13 113.5(2) . . ? C13 C1 H1A 108.9 . . ? C13 C1 H1B 108.9 . . ? C3 C2 C1 118.3(2) . . ? O14 C2 C1 119.9(3) . . ? O14 C2 C3 121.7(3) . . ? C2 C3 C15 122.4(2) . . ? C4 C3 C2 118.6(3) . . ? C4 C3 C15 119.0(3) . . ? C3 C4 H4 116.8 . . ? C3 C4 C5 126.4(3) . . ? C5 C4 H4 116.8 . . ? C4 C5 C6 107.3(2) . . ? C4 C5 C13 112.3(2) . . ? C4 C5 C25 107.3(2) . . ? C6 C5 C13 99.7(2) . . ? C6 C5 C25 116.6(3) . . ? C13 C5 C25 113.5(2) . . ? C7 C6 C5 132.4(2) . . ? C11 C6 C5 108.1(3) . . ? C11 C6 C7 119.4(3) . . ? C6 C7 H7 120.2 . . ? C6 C7 C8 119.5(3) . . ? C8 C7 H7 120.2 . . ? C7 C8 C28 121.0(3) . . ? C9 C8 C7 118.8(3) . . ? C9 C8 C28 120.2(3) . . ? C8 C9 H9 118.7 . . ? C8 C9 C10 122.6(3) . . ? C10 C9 H9 118.7 . . ? C9 C10 H10 121.9 . . ? C11 C10 C9 116.2(3) . . ? C11 C10 H10 121.9 . . ? C10 C11 C6 123.3(3) . . ? O12 C11 C6 112.7(2) . . ? O12 C11 C10 124.0(3) . . ? C11 O12 C13 105.6(2) . . ? C1 C13 C5 115.0(2) . . ? C1 C13 H13 109.2 . . ? C5 C13 H13 109.2 . . ? O12 C13 C1 108.6(2) . . ? O12 C13 C5 105.5(2) . . ? O12 C13 H13 109.2 . . ? C16 C15 C3 119.3(2) . . ? C16 C15 C20 117.6(3) . . ? C20 C15 C3 123.1(3) . . ? C15 C16 H16 118.6 . . ? C15 C16 C17 122.8(3) . . ? C17 C16 H16 118.6 . . ? C16 C17 C21 121.3(3) . . ? C18 C17 C16 118.0(3) . . ? C18 C17 C21 120.7(3) . . ? C17 C18 H18 119.6 . . ? C19 C18 C17 120.8(3) . . ? C19 C18 H18 119.6 . . ? C18 C19 H19 119.5 . . ? C18 C19 C20 121.0(3) . . ? C20 C19 H19 119.5 . . ? C19 C20 C15 119.7(3) . . ? O24 C20 C15 123.0(3) . . ? O24 C20 C19 117.2(3) . . ? C17 C21 H21A 110.1 . . ? C17 C21 H21B 110.1 . . ? C17 C21 H21C 103.8 . . ? C17 C21 H21D 103.8 . . ? C17 C21 C22 107.9(3) . . ? H21A C21 H21B 108.4 . . ? H21C C21 H21D 105.4 . . ? C22 C21 H21A 110.1 . . ? C22 C21 H21B 110.1 . . ? C22A C21 C17 133.5(7) . . ? C22A C21 H21C 103.8 . . ? C22A C21 H21D 103.8 . . ? C21 C22 H22 118.1 . . ? C23 C22 C21 123.8(6) . . ? C23 C22 H22 118.1 . . ? C21 C22A H22A 124.3 . . ? C23A C22A C21 111.4(16) . . ? C23A C22A H22A 124.3 . . ? C22 C23 H23A 120.0 . . ? C22 C23 H23B 120.0 . . ? H23A C23 H23B 120.0 . . ? C22A C23A H23C 120.0 . . ? C22A C23A H23D 120.0 . . ? H23C C23A H23D 120.0 . . ? C20 O24 H24 103(3) . . ? C5 C25 H25A 108.9 . . ? C5 C25 H25B 108.9 . . ? C5 C25 H25C 108.4 . . ? C5 C25 H25D 108.4 . . ? H25A C25 H25B 107.7 . . ? H25C C25 H25D 107.4 . . ? C26 C25 C5 113.3(12) . . ? C26 C25 H25A 108.9 . . ? C26 C25 H25B 108.9 . . ? C26A C25 C5 115.7(8) . . ? C26A C25 H25C 108.4 . . ? C26A C25 H25D 108.4 . . ? C25 C26 H26 120.1 . . ? C27 C26 C25 119.8(14) . . ? C27 C26 H26 120.1 . . ? C25 C26A H26A 117.2 . . ? C27A C26A C25 125.5(11) . . ? C27A C26A H26A 117.2 . . ? C26 C27 H27A 120.0 . . ? C26 C27 H27B 120.0 . . ? H27A C27 H27B 120.0 . . ? C26A C27A H27C 120.0 . . ? C26A C27A H27D 120.0 . . ? H27C C27A H27D 120.0 . . ? C8 C28 H28A 108.3 . . ? C8 C28 H28B 108.3 . . ? C8 C28 H28D 105.4 . . ? C8 C28 H28C 105.4 . . ? H28A C28 H28B 107.4 . . ? H28D C28 H28C 106.0 . . ? C29 C28 C8 115.9(4) . . ? C29 C28 H28A 108.3 . . ? C29 C28 H28B 108.3 . . ? C29A C28 C8 127.5(8) . . ? C29A C28 H28D 105.4 . . ? C29A C28 H28C 105.4 . . ? C28 C29 H29 118.7 . . ? C30 C29 C28 122.6(6) . . ? C30 C29 H29 118.7 . . ? C28 C29A H29A 126.3 . . ? C30A C29A C28 107(3) . . ? C30A C29A H29A 126.3 . . ? C29 C30 H30A 120.0 . . ? C29 C30 H30B 120.0 . . ? H30A C30 H30B 120.0 . . ? C29A C30A H30C 120.0 . . ? C29A C30A H30D 120.0 . . ? H30C C30A H30D 120.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? C1 C2 1.493(4) . ? C1 C13 1.501(4) . ? C2 C3 1.484(4) . ? C2 O14 1.238(4) . ? C3 C4 1.355(4) . ? C3 C15 1.490(4) . ? C4 H4 0.9500 . ? C4 C5 1.504(4) . ? C5 C6 1.520(4) . ? C5 C13 1.537(4) . ? C5 C25 1.547(4) . ? C6 C7 1.394(4) . ? C6 C11 1.380(4) . ? C7 H7 0.9500 . ? C7 C8 1.397(4) . ? C8 C9 1.395(4) . ? C8 C28 1.499(5) . ? C9 H9 0.9500 . ? C9 C10 1.399(4) . ? C10 H10 0.9500 . ? C10 C11 1.378(4) . ? C11 O12 1.377(4) . ? O12 C13 1.468(3) . ? C13 H13 1.0000 . ? C15 C16 1.391(4) . ? C15 C20 1.416(4) . ? C16 H16 0.9500 . ? C16 C17 1.395(4) . ? C17 C18 1.387(5) . ? C17 C21 1.507(5) . ? C18 H18 0.9500 . ? C18 C19 1.380(5) . ? C19 H19 0.9500 . ? C19 C20 1.386(5) . ? C20 O24 1.374(4) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 H21C 0.9900 . ? C21 H21D 0.9900 . ? C21 C22 1.528(7) . ? C21 C22A 1.455(12) . ? C22 H22 0.9500 . ? C22 C23 1.329(8) . ? C22A H22A 0.9500 . ? C22A C23A 1.323(14) . ? C23 H23A 0.9500 . ? C23 H23B 0.9500 . ? C23A H23C 0.9500 . ? C23A H23D 0.9500 . ? O24 H24 0.90(5) . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C25 H25C 0.9900 . ? C25 H25D 0.9900 . ? C25 C26 1.476(12) . ? C25 C26A 1.511(9) . ? C26 H26 0.9500 . ? C26 C27 1.334(12) . ? C26A H26A 0.9500 . ? C26A C27A 1.330(10) . ? C27 H27A 0.9500 . ? C27 H27B 0.9500 . ? C27A H27C 0.9500 . ? C27A H27D 0.9500 . ? C28 H28A 0.9900 . ? C28 H28B 0.9900 . ? C28 H28D 0.9900 . ? C28 H28C 0.9900 . ? C28 C29 1.429(6) . ? C28 C29A 1.396(13) . ? C29 H29 0.9500 . ? C29 C30 1.398(9) . ? C29A H29A 0.9500 . ? C29A C30A 1.366(16) . ? C30 H30A 0.9500 . ? C30 H30B 0.9500 . ? C30A H30C 0.9500 . ? C30A H30D 0.9500 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag O24 H24 O14 0.90(5) 1.76(5) 2.644(3) 165(4) . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 C2 C3 C4 12.6(3) . . . . ? C1 C2 C3 C15 -165.2(2) . . . . ? C2 C1 C13 C5 47.0(3) . . . . ? C2 C1 C13 O12 -70.9(3) . . . . ? C2 C3 C4 C5 0.4(4) . . . . ? C2 C3 C15 C16 132.7(3) . . . . ? C2 C3 C15 C20 -49.2(4) . . . . ? C3 C4 C5 C6 119.1(3) . . . . ? C3 C4 C5 C13 10.5(4) . . . . ? C3 C4 C5 C25 -114.8(3) . . . . ? C3 C15 C16 C17 175.7(3) . . . . ? C3 C15 C20 C19 -175.3(3) . . . . ? C3 C15 C20 O24 1.3(4) . . . . ? C4 C3 C15 C16 -45.1(4) . . . . ? C4 C3 C15 C20 133.0(3) . . . . ? C4 C5 C6 C7 79.0(4) . . . . ? C4 C5 C6 C11 -98.0(3) . . . . ? C4 C5 C13 C1 -34.0(3) . . . . ? C4 C5 C13 O12 85.7(3) . . . . ? C4 C5 C25 C26 177.3(10) . . . . ? C4 C5 C25 C26A -171.7(8) . . . . ? C5 C6 C7 C8 -176.5(3) . . . . ? C5 C6 C11 C10 175.2(3) . . . . ? C5 C6 C11 O12 -3.1(3) . . . . ? C5 C25 C26 C27 -120(2) . . . . ? C5 C25 C26A C27A -126.6(16) . . . . ? C6 C5 C13 C1 -147.4(2) . . . . ? C6 C5 C13 O12 -27.7(3) . . . . ? C6 C5 C25 C26 -62.3(10) . . . . ? C6 C5 C25 C26A -51.3(9) . . . . ? C6 C7 C8 C9 1.4(5) . . . . ? C6 C7 C8 C28 -177.2(3) . . . . ? C6 C11 O12 C13 -15.5(3) . . . . ? C7 C6 C11 C10 -2.3(4) . . . . ? C7 C6 C11 O12 179.4(2) . . . . ? C7 C8 C9 C10 -1.4(5) . . . . ? C7 C8 C28 C29 -41.9(6) . . . . ? C7 C8 C28 C29A 27.8(13) . . . . ? C8 C9 C10 C11 -0.5(5) . . . . ? C8 C28 C29 C30 123.6(5) . . . . ? C8 C28 C29A C30A -93(2) . . . . ? C9 C8 C28 C29 139.4(4) . . . . ? C9 C8 C28 C29A -150.9(12) . . . . ? C9 C10 C11 C6 2.4(4) . . . . ? C9 C10 C11 O12 -179.5(3) . . . . ? C10 C11 O12 C13 166.2(3) . . . . ? C11 C6 C7 C8 0.3(4) . . . . ? C11 O12 C13 C1 151.2(2) . . . . ? C11 O12 C13 C5 27.4(3) . . . . ? C13 C1 C2 C3 -36.2(3) . . . . ? C13 C1 C2 O14 145.1(3) . . . . ? C13 C5 C6 C7 -163.9(3) . . . . ? C13 C5 C6 C11 19.1(3) . . . . ? C13 C5 C25 C26 52.7(10) . . . . ? C13 C5 C25 C26A 63.7(9) . . . . ? O14 C2 C3 C4 -168.6(3) . . . . ? O14 C2 C3 C15 13.6(4) . . . . ? C15 C3 C4 C5 178.2(2) . . . . ? C15 C16 C17 C18 0.6(4) . . . . ? C15 C16 C17 C21 -178.5(3) . . . . ? C16 C15 C20 C19 2.8(4) . . . . ? C16 C15 C20 O24 179.4(3) . . . . ? C16 C17 C18 C19 1.2(5) . . . . ? C16 C17 C21 C22 93.3(4) . . . . ? C16 C17 C21 C22A 78.9(11) . . . . ? C17 C18 C19 C20 -0.9(5) . . . . ? C17 C21 C22 C23 -126.4(5) . . . . ? C17 C21 C22A C23A 14(2) . . . . ? C18 C17 C21 C22 -85.8(4) . . . . ? C18 C17 C21 C22A -100.2(11) . . . . ? C18 C19 C20 C15 -1.2(5) . . . . ? C18 C19 C20 O24 -178.0(3) . . . . ? C20 C15 C16 C17 -2.5(4) . . . . ? C21 C17 C18 C19 -179.7(3) . . . . ? C25 C5 C6 C7 -41.4(4) . . . . ? C25 C5 C6 C11 141.6(2) . . . . ? C25 C5 C13 C1 87.9(3) . . . . ? C25 C5 C13 O12 -152.4(2) . . . . ? C28 C8 C9 C10 177.3(3) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 0.9983 -1.9999 -0.0023 0.2695 -0.0615 -0.0043 -0.9983 1.9999 0.0023 -0.2695 0.0615 0.0043 0.9949 -0.0002 -1.9990 0.0112 0.0051 0.3054 -0.9949 0.0002 1.9990 -0.0112 -0.0051 -0.3054 0.9994 -0.0001 -0.0009 0.0074 -0.0841 0.0055 -0.9994 0.0001 0.0009 -0.0074 0.0841 -0.0055 4.9978 1.9994 -0.0029 -0.2249 -0.4429 0.0375