Crystallography Open Database

Information card for entry 1571951

1571950 << 1571951 >> 1571952

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Coordinates	1571951.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H20 Cu F10 P
Calculated formula	C28 H20 Cu F10 P
Title of publication	Synthesis and application of well-defined [Ph<sub>4</sub>P]<sup>+</sup>[Cu(CF<sub>2</sub>CF<sub>3</sub>)<sub>2</sub>]<sup>-</sup> complex as a versatile pentafluoroethylating reagent.
Authors of publication	Dong, Tao; Shen, Qilong; Tsui, Gavin Chit
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	29
Pages of publication	11550 - 11556
a	18.025 ± 0.004 Å
b	7.2972 ± 0.0018 Å
c	22.077 ± 0.007 Å
α	90°
β	112.088 ± 0.006°
γ	90°
Cell volume	2690.7 ± 1.2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1435
Residual factor for significantly intense reflections	0.0898
Weighted residual factors for significantly intense reflections	0.2473
Weighted residual factors for all reflections included in the refinement	0.2839
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
293738 (current)	2024-08-05	cif/ Updating files of 1571951 Original log message: Adding full bibliography for 1571951.cif.	1571951.cif
292478	2024-06-21	cif/ Adding structures of 1571951 via cif-deposit CGI script.	1571951.cif