#------------------------------------------------------------------------------ #$Date: 2024-08-05 20:57:26 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293741 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/19/1571961.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571961 loop_ _publ_author_name 'Zhao, Lingli' 'Wu, Zeng' 'Qin, Hanwen' 'Bin, Guangxiong' 'Gao, Junxiang' 'Zeng, Weixuan' 'Zhao, Yan' 'Chen, Huajie' _publ_section_title ; Ambipolar conjugated ladder polymers by room-temperature Knoevenagel polymerization. ; _journal_issue 29 _journal_name_full 'Chemical science' _journal_page_first 11594 _journal_page_last 11603 _journal_paper_doi 10.1039/d4sc03222e _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C112 H124 N8' _chemical_formula_sum 'C112 H124 N8' _chemical_formula_weight 1582.18 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-I 2ya' _space_group_name_H-M_alt 'I 1 2/a 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-04-18 _audit_creation_method ; Olex2 1.5-beta (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6439) ; _audit_update_record ; 2024-05-04 deposited with the CCDC. 2024-06-20 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90.107(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.0671(3) _cell_length_b 13.6045(3) _cell_length_c 46.1940(9) _cell_measurement_reflns_used 8466 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 71.9090 _cell_measurement_theta_min 3.3830 _cell_volume 9468.8(3) _computing_cell_refinement 'CrysAlisPro 1.171.43.92a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.43.92a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.43.92a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -57.00 -19.00 0.50 20.00 -- -46.12 107.00 101.00 76 2 \w 18.00 73.00 0.50 20.00 -- 46.12-107.00 3.00 110 3 \w -129.00-103.00 0.50 10.00 -- -99.00-107.00 3.00 52 4 \w -107.00 -31.00 0.50 10.00 -- -99.00 107.00 101.00 152 5 \w 73.00 102.00 0.50 10.00 -- 99.00-107.00 3.00 58 6 \w 88.00 168.00 0.50 10.00 -- 99.00 107.00 101.00 160 7 \w -23.00 26.00 0.50 20.00 -- -46.12 19.00 90.00 98 8 \w -70.00 -31.00 0.50 20.00 -- -46.12 -57.00 -60.00 78 9 \w -117.00 -76.00 0.50 20.00 -- -46.12 -57.00 -60.00 82 10 \w -23.00 29.00 0.50 20.00 -- -46.12 19.00-150.00 104 11 \w -19.00 16.00 0.50 20.00 -- 46.12 -37.00-120.00 70 12 \w -55.00 -29.00 0.50 10.00 -- -99.00 61.00 90.00 52 13 \w -55.00 -30.00 0.50 10.00 -- -99.00 61.00 60.00 50 14 \w -149.00 -97.00 0.50 10.00 -- -99.00 -94.00 60.00 104 15 \w -57.00 -31.00 0.50 10.00 -- -99.00 61.00 120.00 52 16 \w -169.00 -75.00 0.50 10.00 -- -99.00-125.00 -60.00 188 17 \w -171.00 -76.00 0.50 10.00 -- -99.00 -77.00 30.00 190 18 \w -99.00 -50.00 0.50 10.00 -- -99.00 77.00 120.00 98 19 \w 27.00 52.00 0.50 10.00 -- 99.00 -45.00-150.00 50 20 \w 28.00 53.00 0.50 10.00 -- 99.00 -45.00 60.00 50 21 \w 28.00 66.00 0.50 10.00 -- 99.00 -94.00 -60.00 76 22 \w 27.00 52.00 0.50 10.00 -- 99.00 -45.00 0.00 50 23 \w 27.00 52.00 0.50 10.00 -- 99.00 -45.00-180.00 50 24 \w 74.00 99.00 0.50 10.00 -- 99.00 -94.00 -60.00 50 25 \w 28.00 53.00 0.50 10.00 -- 99.00 -45.00 150.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0517465000 _diffrn_orient_matrix_UB_12 -0.0676890000 _diffrn_orient_matrix_UB_13 0.0207751000 _diffrn_orient_matrix_UB_21 -0.0134799000 _diffrn_orient_matrix_UB_22 -0.0867373000 _diffrn_orient_matrix_UB_23 -0.0209881000 _diffrn_orient_matrix_UB_31 0.0871733000 _diffrn_orient_matrix_UB_32 0.0267346000 _diffrn_orient_matrix_UB_33 -0.0154902000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0629 _diffrn_reflns_av_unetI/netI 0.0542 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 54 _diffrn_reflns_limit_l_min -54 _diffrn_reflns_number 32783 _diffrn_reflns_point_group_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 66.599 _diffrn_reflns_theta_max 66.599 _diffrn_reflns_theta_min 3.387 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.487 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.67344 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.43.92a (Rigaku Oxford Diffraction, 2023) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'metallic light colourless' _exptl_crystal_density_diffrn 1.110 _exptl_crystal_description block _exptl_crystal_F_000 3408 _exptl_crystal_size_max 0.132 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.525 _refine_diff_density_min -0.524 _refine_diff_density_rms 0.094 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.448 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 599 _refine_ls_number_reflns 8304 _refine_ls_number_restraints 636 _refine_ls_restrained_S_all 69.141 _refine_ls_R_factor_all 0.1523 _refine_ls_R_factor_gt 0.1186 _refine_ls_shift/su_max 0.009 _refine_ls_shift/su_mean 0.207 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3478 _refine_ls_wR_factor_ref 0.3787 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5448 _reflns_number_total 8304 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03222e2.cif _cod_data_source_block n2 _cod_depositor_comments 'Adding full bibliography for 1571961.cif.' _cod_database_code 1571961 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C H O N S' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.962 _shelx_estimated_absorpt_t_min 0.938 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C54-C55 = C54-C53 1.54 with sigma of 0.01 C52-C53 1.54 with sigma of 0.01 C55-C56 1.54 with sigma of 0.01 C54-C55 1.54 with sigma of 0.01 C30-C31 = C30-C29 1.54 with sigma of 0.01 C44-C43 = C44-C45 1.54 with sigma of 0.01 C46-C45 1.54 with sigma of 0.01 C46A-C45A = C45A-C44A = C44A-C43A 1.5 with sigma of 0.01 C58-C57 = C62-C58 = C62-C59 = C60-C59 = C61-C60 1.54 with sigma of 0.01 C54-C56 2.4 with sigma of 0.01 C53-C51 2.4 with sigma of 0.01 C55-C53 2.4 with sigma of 0.01 C54-C52 2.45 with sigma of 0.01 C61-C59 2.4 with sigma of 0.01 C58-C50 2.42 with sigma of 0.01 3. Rigid bond restraints C55, C54, C53, C52, C51 with sigma for 1-2 distances of 0.00007 and sigma for 1-3 distances of 0.00007 C51, C50 with sigma for 1-2 distances of 0.006 and sigma for 1-3 distances of 0.006 C61, C60, C59, C62, C58, C57, C50 with sigma for 1-2 distances of 0.0008 and sigma for 1-3 distances of 0.0008 C60, C61 with sigma for 1-2 distances of 0.00009 and sigma for 1-3 distances of 0.00009 4. Uiso/Uaniso restraints and constraints C44 \\sim C45 \\sim C46: within 2A with sigma of 0.0007 and sigma for terminal atoms of 0.0014 within 2A C55 \\sim C54 \\sim C53 \\sim C52 \\sim C51: within 2A with sigma of 0.0006 and sigma for terminal atoms of 0.0012 within 2A C45 \\sim C46 \\sim C44: within 2A with sigma of 0.0004 and sigma for terminal atoms of 0.0008 within 2A C51 \\sim C50: within 2A with sigma of 0.0004 and sigma for terminal atoms of 0.0008 within 2A C59 \\sim C62 \\sim C58 \\sim C57 \\sim C50: within 2A with sigma of 0.0001 and sigma for terminal atoms of 0.0002 within 2A C59 \\sim C62: within 2A with sigma of 0.00008 and sigma for terminal atoms of 0.00016 within 2A C60 \\sim C59: within 2A with sigma of 0.00008 and sigma for terminal atoms of 0.00016 within 2A Uanis(C56) \\sim Ueq: with sigma of 0.0005 and sigma for terminal atoms of 0.001 Uanis(C44A) = Uanis(C45A) = Uanis(C46A) = Uanis(C43A) = Uanis(C42) Uanis(C50) = Uanis(C49) = Uanis(C48) 5. Rigid body (RIGU) restrains N1, N2, N3, N4, C1, C2, C3, C4, C5, C6, C7, C8, C9, C10, C11, C12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25, C26, C27, C28, C29, C30, C31, C32, C33, C34, C35, C36, C37, C38, C39, C40, C41, C42, C43, C44, C45, C46, C47, C48, C49, C50, C51, C52, C53, C54, C55, C56 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.004 N1, N2, N3, N4, C1, C2, C3, C4, C5, C6, C7, C8, C9, C10, C11, C12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25, C26, C27, C28, C29, C30, C31, C32, C33, C34, C35, C36, C37, C38, C39, C40, C41, C42, C43, C44, C45, C46, C47, C48, C49, C50, C51, C52, C53, C54, C55, C56 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.005 C44, N1, C11, C10, C1, C9, C2, C6, C8, C12, C3, C5, C7, C18, C13, C17, C4, C32, C19, C14, C16, N2, C20, C15, C21, N3, C22, C23, C33, C24, C34, N4, C35, C47, C25, C36, C48, C26, C37, C49, C27, C31, C38, C50, C28, C30, C39, C51, C29, C40, C52, C41, C53, C42, C54, C43, C55, C56, C45, C46 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.007 C41, C42, C43, C44, C45, C46, C44A, C45A, C46A, C43A with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.005 C41, C42, C43A, C44A, C45A, C46A, C40 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.006 C46, N1, C11, C10, C1, C9, C2, C6, C8, C12, H2, C3, C5, C7, C18, C13, C17, H3, C4, H5, C32, C19, H13, C14, C16, H4, N2, H19, C20, H14, C15, C21, N3, H15, C22, C23, C33, C24, H33A, H33B, C34, N4, H34, C35, C47, C25, H35A, H35B, C36, H47A, H47B, C48, C26, H36A, H36B, C37, H48A, H48B, C49, C27, C31, H37A, H37B, C38, H49A, H49B, C50, H27, C28, H31, C30, H38A, H38B, C39, C51, H28, C29, H30, H39A, H39B, C40, C52, H29, H40A, H40B, C41, C53, H41A, H41B, C42, C54, H42A, H42B, H42C, H42D, C43, C43A, C55, H43A, H43B, C44, C44A, H43C, H43D, C56, H44A, H44B, C45, H44C, H44D, C45A, H45A, H45B, H45C, H45D, C46A, H46A, H46B, H46C, H46D, H46E, H46F with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.007 C52, N1, C11, C10, C1, C9, C2, C6, C8, C12, H2, C3, C5, C7, C18, C13, C17, H3, C4, H5, C32, C19, H13, C14, C16, H4, N2, H19, C20, H14, C15, C21, N3, H15, C22, C23, C33, C24, H33A, H33B, C34, N4, H34, C35, C47, C25, H35A, H35B, C36, H47A, H47B, C48, C26, H36A, H36B, C37, H48A, H48B, C49, C27, C31, H37A, H37B, C38, H49A, H49B, C50, H27, C28, C30, H31, H38A, H38B, C39, H50B, H50A, C51, C57, H28, C29, H30, H39A, H39B, C40, H51A, H51B, H57A, H57B, C58, H29, H40A, H40B, C41, H52A, H52B, C53, C62, H41A, H41B, C42, H53A, H53B, C54, C59, H62A, H62B, H42A, H42B, H42C, H42D, C43, C43A, H54A, H54B, C55, C60, H43A, H43B, C44, C44A, H43C, H43D, H55A, H55B, C56, H60A, H60B, C61, H44A, H44B, C45, H44C, H44D, C45A, H56A, H56B, H56C, H45A, H45B, C46, H45C, H45D, C46A, H46A, H46B, H46C, H46D, H46E, H46F with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.004 6. Others Fixed Sof: H42A(0.5) H42B(0.5) H42C(0.5) H42D(0.5) C43(0.5) H43A(0.5) H43B(0.5) C44(0.5) H44A(0.5) H44B(0.5) C45(0.5) H45A(0.5) H45B(0.5) C46(0.5) H46A(0.5) H46B(0.5) H46C(0.5) H50A(0.5) H50B(0.5) H50C(0.5) H50D(0.5) C51(0.5) H51A(0.5) H51B(0.5) C52(0.5) H52A(0.5) H52B(0.5) C53(0.5) H53A(0.5) H53B(0.5) C54(0.5) H54A(0.5) H54B(0.5) C55(0.5) H55A(0.5) H55B(0.5) C56(0.5) H56A(0.5) H56B(0.5) H56C(0.5) C44A(0.5) H44C(0.5) H44D(0.5) C45A(0.5) H45C(0.5) H45D(0.5) C46A(0.5) H46D(0.5) H46E(0.5) H46F(0.5) C43A(0.5) H43C(0.5) H43D(0.5) C60(0.5) H60A(0.5) H60B(0.5) C59(0.5) H59A(0.5) H59B(0.5) C57(0.5) H57A(0.5) H57B(0.5) C61(0.5) H61A(0.5) H61B(0.5) H61C(0.5) C58(0.5) H58A(0.5) H58B(0.5) C62(0.5) H62A(0.5) H62B(0.5) 7.a Ternary CH refined with riding coordinates: C34(H34) 7.b Secondary CH2 refined with riding coordinates: C33(H33A,H33B), C35(H35A,H35B), C36(H36A,H36B), C37(H37A,H37B), C38(H38A, H38B), C39(H39A,H39B), C40(H40A,H40B), C41(H41A,H41B), C42(H42A,H42B), C42(H42C,H42D), C43(H43A,H43B), C44(H44A,H44B), C45(H45A,H45B), C47(H47A,H47B), C48(H48A,H48B), C49(H49A,H49B), C50(H50A,H50B), C50(H50C,H50D), C51(H51A, H51B), C52(H52A,H52B), C53(H53A,H53B), C54(H54A,H54B), C55(H55A,H55B), C44A(H44C,H44D), C45A(H45C,H45D), C43A(H43C,H43D), C60(H60A,H60B), C59(H59A, H59B), C57(H57A,H57B), C58(H58A,H58B), C62(H62A,H62B) 7.c Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C4(H4), C5(H5), C13(H13), C14(H14), C15(H15), C19(H19), C27(H27), C28(H28), C29(H29), C30(H30), C31(H31) 7.d Idealised Me refined as rotating group: C46(H46A,H46B,H46C), C56(H56A,H56B,H56C), C46A(H46D,H46E,H46F), C61(H61A,H61B, H61C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL n2_a.res in I2/a n2.res created by SHELXL-2018/3 at 19:18:31 on 18-Apr-2024 REM Old TITL n1_2_auto_a.res in I2/a REM SHELXT solution in I2/a: R1 0.278, Rweak 0.015, Alpha 0.042 REM 0.346 for 416 systematic absences, Orientation as input REM Formula found by SHELXT: C40 N11 CELL 1.54184 15.0671 13.6045 46.194 90 90.107 90 ZERR 4 0.0003 0.0003 0.0009 0 0.002 0 LATT 2 SYMM 0.5-X,+Y,-Z SFAC C H N UNIT 448 496 32 DFIX 1.54 0.01 C54 C55 C54 C53 DFIX 1.54 0.01 C52 C53 DFIX 1.54 0.01 C55 C56 DFIX 1.54 0.01 C54 C55 DFIX 1.54 0.01 C30 C31 C30 C29 DANG 2.4 0.01 C54 C56 DANG 2.4 0.01 C53 C51 RIGU 0.001 0.004 N1 > C56 RIGU 0.001 0.005 N1 > C2 C3 C4 C5 C6 > C13 C14 C15 C16 > C19 C20 > C27 C28 = C29 C30 C31 C32 C33 C34 C35 C36 C37 C38 C39 C40 C41 C42 C43 C44 C45 C46 C47 = C48 C49 C50 C51 C52 C53 C54 C55 C56 DANG 2.4 0.01 C55 C53 SIMU 0.0007 0.0014 2 C44 C45 C46 DELU 0.00007 0.00007 C55 C54 C53 C52 C51 SIMU 0.0006 0.0012 2 C55 C54 C53 C52 C51 ISOR 0.0005 0.001 C56 SIMU 0.0004 0.0008 2 C45 C46 C44 SIMU 0.0004 0.0008 2 C51 C50 DELU 0.006 0.006 C51 C50 RIGU 0.001 0.007 C44 N1 C11 C10 C1 C9 C2 C6 C8 C12 C3 C5 C7 C18 C13 C17 C4 = C32 C19 C14 C16 N2 C20 C15 C21 N3 C22 C23 C33 C24 C34 N4 C35 C47 C25 C36 = C48 C26 C37 C49 C27 C31 C38 C50 C28 C30 C39 C51 C29 C40 C52 C41 C53 C42 C54 = C43 C55 C56 C45 C46 DFIX 1.54 0.01 C44 C43 C44 C45 DFIX 1.54 0.01 C46 C45 RIGU 0.001 0.005 C41 C42 C43 C44 C45 C46 C44A C45A C46A C43A RIGU 0.001 0.006 C41 C42 C43A C44A C45A C46A C40 DFIX 1.5 0.01 C46A C45A C45A C44A C44A C43A EADP C44A C45A C46A C43A C42 DANG 2.45 0.01 C54 C52 RIGU 0.001 0.007 C46 N1 C11 C10 C1 C9 C2 C6 C8 C12 H2 C3 C5 C7 C18 C13 C17 = H3 C4 H5 C32 C19 H13 C14 C16 H4 N2 H19 C20 H14 C15 C21 N3 H15 C22 C23 C33 = C24 H33A H33B C34 N4 H34 C35 C47 C25 H35A H35B C36 H47A H47B C48 C26 H36A = H36B C37 H48A H48B C49 C27 C31 H37A H37B C38 H49A H49B C50 H27 C28 H31 C30 = H38A H38B C39 C51 H28 C29 H30 H39A H39B C40 C52 H29 H40A H40B C41 C53 H41A = H41B C42 C54 H42A H42B H42C H42D C43 C43A C55 H43A H43B C44 C44A H43C H43D = C56 H44A H44B C45 H44C H44D C45A H45A H45B H45C H45D C46A H46A H46B H46C = H46D H46E H46F EADP C50 C49 C48 DFIX 1.54 0.01 C58 C57 C62 C58 C62 C59 C60 C59 C61 C60 RIGU 0.001 0.004 C52 N1 C11 C10 C1 C9 C2 C6 C8 C12 H2 C3 C5 C7 C18 C13 C17 = H3 C4 H5 C32 C19 H13 C14 C16 H4 N2 H19 C20 H14 C15 C21 N3 H15 C22 C23 C33 = C24 H33A H33B C34 N4 H34 C35 C47 C25 H35A H35B C36 H47A H47B C48 C26 H36A = H36B C37 H48A H48B C49 C27 C31 H37A H37B C38 H49A H49B C50 H27 C28 C30 H31 = H38A H38B C39 H50B H50A C51 C57 H28 C29 H30 H39A H39B C40 H51A H51B H57A = H57B C58 H29 H40A H40B C41 H52A H52B C53 C62 H41A H41B C42 H53A H53B C54 = C59 H62A H62B H42A H42B H42C H42D C43 C43A H54A H54B C55 C60 H43A H43B C44 = C44A H43C H43D H55A H55B C56 H60A H60B C61 H44A H44B C45 H44C H44D C45A = H56A H56B H56C H45A H45B C46 H45C H45D C46A H46A H46B H46C H46D H46E H46F SIMU 0.0001 0.0002 2 C59 C62 C58 C57 C50 DELU 0.0008 0.0008 C61 C60 C59 C62 C58 C57 C50 SIMU 0.00008 0.00016 2 C59 C62 DELU 0.00009 0.00009 C60 C61 SIMU 0.00008 0.00016 2 C60 C59 DANG 2.4 0.01 C61 C59 DANG 2.42 0.01 C58 C50 L.S. 2 PLAN 10 SIZE 0.08 0.1 0.132 TEMP -173 CONF BIND C58 C62 FREE C58 C50 FREE C61 C59 FREE C62 C60 BIND C45A C46A FREE H50d H58a FREE C54 C56 FREE C54 C52 FREE C51 C53 FREE C55 C53 BOND list 4 MORE -1 BOND $H ABIN fmap 2 acta SHEL 999 0.84 OMIT 0 2 2 OMIT -1 4 7 OMIT 1 1 10 OMIT -2 1 11 OMIT 0 6 10 OMIT 3 2 13 OMIT 7 1 4 OMIT 0 3 13 OMIT 6 4 0 OMIT -4 5 15 OMIT 0 3 11 OMIT 2 4 2 OMIT 7 1 6 OMIT 3 1 10 OMIT -1 2 1 OMIT -2 1 13 OMIT -7 2 11 REM REM REM WGHT 0.200000 FVAR 0.06338 N1 3 0.019999 0.602538 0.708886 11.00000 0.09209 0.06179 = 0.03474 -0.00897 0.02313 0.00813 N2 3 0.146718 0.113701 0.624221 11.00000 0.14550 0.04650 = 0.04517 -0.00040 0.03799 0.00493 N3 3 0.227874 0.356428 0.534176 11.00000 0.04762 0.03067 = 0.02348 -0.00009 0.01207 0.00086 N4 3 0.202983 0.699421 0.525748 11.00000 0.04925 0.03097 = 0.02678 0.00004 0.00857 0.00083 C1 1 0.045802 0.352057 0.694775 11.00000 0.06496 0.04915 = 0.02918 0.00191 0.01408 0.00201 C2 1 0.013075 0.344361 0.723416 11.00000 0.07968 0.05950 = 0.03331 0.00615 0.02217 0.01025 AFIX 43 H2 2 -0.002396 0.402264 0.733735 11.00000 -1.20000 AFIX 0 C3 1 0.003519 0.255172 0.736329 11.00000 0.10932 0.06120 = 0.03311 0.00828 0.02808 0.00621 AFIX 43 H3 2 -0.019131 0.251079 0.755470 11.00000 -1.20000 AFIX 0 C4 1 0.027066 0.169117 0.721423 11.00000 0.12771 0.05580 = 0.04033 0.01118 0.03603 0.00561 AFIX 43 H4 2 0.021236 0.107136 0.730699 11.00000 -1.20000 AFIX 0 C5 1 0.058242 0.173664 0.693743 11.00000 0.11246 0.04903 = 0.03734 0.00818 0.02827 0.00474 AFIX 43 H5 2 0.073070 0.114761 0.683822 11.00000 -1.20000 AFIX 0 C6 1 0.068615 0.264731 0.679775 11.00000 0.07534 0.04740 = 0.02902 0.00482 0.01780 0.00341 C7 1 0.101860 0.271672 0.650638 11.00000 0.07113 0.04355 = 0.02708 0.00113 0.01549 -0.00086 C8 1 0.109546 0.361697 0.637088 11.00000 0.04973 0.04291 = 0.02690 0.00003 0.01047 0.00031 C9 1 0.084240 0.449968 0.652076 11.00000 0.05011 0.04153 = 0.02645 0.00056 0.00927 0.00164 C10 1 0.054213 0.444790 0.680427 11.00000 0.05560 0.04699 = 0.02622 0.00026 0.01184 0.00284 C11 1 0.034737 0.532404 0.696020 11.00000 0.06646 0.05282 = 0.02570 -0.00117 0.01657 0.00275 C12 1 0.096106 0.532961 0.632485 11.00000 0.04768 0.04037 = 0.02632 -0.00098 0.01054 0.00301 C13 1 0.079931 0.631845 0.634445 11.00000 0.06729 0.04093 = 0.02864 -0.00454 0.01067 0.00685 AFIX 43 H13 2 0.058397 0.660176 0.651868 11.00000 -1.20000 AFIX 0 C14 1 0.096074 0.689700 0.610043 11.00000 0.06563 0.03856 = 0.03562 -0.00105 0.01621 0.00706 AFIX 43 H14 2 0.084164 0.758173 0.611128 11.00000 -1.20000 AFIX 0 C15 1 0.128480 0.652063 0.584464 11.00000 0.05527 0.03600 = 0.03252 -0.00046 0.01219 0.00361 AFIX 43 H15 2 0.138286 0.694682 0.568496 11.00000 -1.20000 AFIX 0 C16 1 0.147312 0.550526 0.581736 11.00000 0.04191 0.03843 = 0.02508 -0.00117 0.00887 0.00285 C17 1 0.129074 0.493536 0.606234 11.00000 0.04892 0.03746 = 0.02481 -0.00144 0.00930 0.00079 C18 1 0.140115 0.390452 0.608071 11.00000 0.05121 0.03644 = 0.02492 -0.00020 0.00730 -0.00049 C19 1 0.173292 0.339517 0.584968 11.00000 0.05290 0.03502 = 0.02714 0.00080 0.01081 -0.00071 AFIX 43 H19 2 0.182080 0.270408 0.585662 11.00000 -1.20000 AFIX 0 C20 1 0.193861 0.395204 0.559956 11.00000 0.04722 0.03336 = 0.02500 -0.00204 0.01052 0.00045 C21 1 0.182782 0.497424 0.557170 11.00000 0.04445 0.03310 = 0.02368 -0.00175 0.00826 -0.00082 C22 1 0.212815 0.521956 0.528469 11.00000 0.04141 0.03390 = 0.02401 -0.00073 0.00820 0.00167 C23 1 0.236714 0.433206 0.514887 11.00000 0.04059 0.03204 = 0.02269 0.00093 0.00906 -0.00099 C24 1 0.228345 0.613577 0.513781 11.00000 0.04349 0.03187 = 0.02360 -0.00186 0.00650 0.00008 C25 1 0.223589 0.783478 0.512629 11.00000 0.04966 0.03116 = 0.02890 -0.00058 0.00623 -0.00008 C26 1 0.187230 0.874146 0.525810 11.00000 0.05185 0.03019 = 0.03871 -0.00292 0.01407 -0.00200 C27 1 0.141687 0.942531 0.509087 11.00000 0.05384 0.03413 = 0.04521 0.00208 0.01408 -0.00181 AFIX 43 H27 2 0.135907 0.932836 0.488804 11.00000 -1.20000 AFIX 0 C28 1 0.104457 1.025390 0.522054 11.00000 0.06711 0.03479 = 0.06689 0.00139 0.02485 0.00191 AFIX 43 H28 2 0.073200 1.071628 0.510478 11.00000 -1.20000 AFIX 0 C29 1 0.112238 1.040920 0.550973 11.00000 0.08188 0.03562 = 0.06935 -0.00760 0.02879 0.00326 AFIX 43 H29 2 0.086127 1.097646 0.559401 11.00000 -1.20000 AFIX 0 C30 1 0.159288 0.972847 0.568875 11.00000 0.08888 0.03899 = 0.05148 -0.01214 0.02411 -0.00292 AFIX 43 H30 2 0.165620 0.983784 0.589086 11.00000 -1.20000 AFIX 0 C31 1 0.196294 0.888285 0.555481 11.00000 0.07156 0.03508 = 0.03837 -0.00428 0.01297 0.00006 AFIX 43 H31 2 0.227337 0.841241 0.566834 11.00000 -1.20000 AFIX 0 C32 1 0.126739 0.183259 0.636035 11.00000 0.09167 0.04244 = 0.02997 0.00437 0.02357 -0.00200 C33 1 0.283705 0.267273 0.534988 11.00000 0.05754 0.03261 = 0.02449 -0.00014 0.01078 0.00716 AFIX 23 H33A 2 0.293591 0.244355 0.514911 11.00000 -1.20000 H33B 2 0.251194 0.214859 0.545389 11.00000 -1.20000 AFIX 0 C34 1 0.374790 0.282526 0.549791 11.00000 0.06281 0.04689 = 0.03577 -0.01107 -0.00061 0.01404 AFIX 13 H34 2 0.363955 0.321088 0.567872 11.00000 -1.20000 AFIX 0 C35 1 0.437005 0.343273 0.530971 11.00000 0.05545 0.04543 = 0.05637 -0.00928 -0.00590 0.00562 AFIX 23 H35A 2 0.405673 0.404212 0.525228 11.00000 -1.20000 H35B 2 0.488777 0.362811 0.542879 11.00000 -1.20000 AFIX 0 C36 1 0.470711 0.293771 0.503962 11.00000 0.04784 0.04192 = 0.05695 -0.00084 0.00439 0.00074 AFIX 23 H36A 2 0.421075 0.258672 0.494426 11.00000 -1.20000 H36B 2 0.516178 0.244494 0.509353 11.00000 -1.20000 AFIX 0 C37 1 0.510478 0.366120 0.482909 11.00000 0.04801 0.05075 = 0.06668 0.00862 -0.00192 -0.00708 AFIX 23 H37A 2 0.558980 0.401969 0.492816 11.00000 -1.20000 H37B 2 0.464426 0.414845 0.477613 11.00000 -1.20000 AFIX 0 C38 1 0.546938 0.321465 0.455424 11.00000 0.04694 0.06802 = 0.06761 0.01100 0.00511 -0.00186 AFIX 23 H38A 2 0.500700 0.280089 0.446265 11.00000 -1.20000 H38B 2 0.598042 0.278714 0.460244 11.00000 -1.20000 AFIX 0 C39 1 0.576660 0.400751 0.434009 11.00000 0.05935 0.09174 = 0.07226 0.02153 0.00262 -0.01450 AFIX 23 H39A 2 0.525694 0.444809 0.430158 11.00000 -1.20000 H39B 2 0.623621 0.440670 0.443337 11.00000 -1.20000 AFIX 0 C40 1 0.610885 0.364383 0.405856 11.00000 0.06336 0.14165 = 0.07952 0.01016 0.01219 -0.00900 AFIX 23 H40A 2 0.565426 0.321653 0.396823 11.00000 -1.20000 H40B 2 0.664322 0.323780 0.409426 11.00000 -1.20000 AFIX 0 C41 1 0.634771 0.447091 0.384617 11.00000 0.06621 0.20870 = 0.08186 0.04938 -0.00130 -0.02227 AFIX 23 H41A 2 0.582405 0.490251 0.382135 11.00000 -1.20000 H41B 2 0.682934 0.487205 0.393188 11.00000 -1.20000 AFIX 0 C42 1 0.663109 0.412767 0.356236 11.00000 0.09789 0.31468 = 0.08872 0.02832 0.01637 -0.03760 PART 1 AFIX 23 H42A 2 0.613230 0.373277 0.348501 10.50000 -1.20000 H42B 2 0.712312 0.366084 0.359834 10.50000 -1.20000 AFIX 23 PART 2 H42C 2 0.617909 0.368481 0.347733 10.50000 -1.20000 H42D 2 0.719922 0.376570 0.357777 10.50000 -1.20000 AFIX 0 PART 1 C43 1 0.692522 0.476076 0.332254 10.50000 0.05749 0.44854 = 0.10164 0.09838 -0.01000 -0.04520 AFIX 23 H43A 2 0.744134 0.515515 0.338687 10.50000 -1.20000 H43B 2 0.644125 0.522114 0.327097 10.50000 -1.20000 AFIX 0 C44 1 0.718629 0.415994 0.305194 10.50000 0.21415 0.54598 = 0.14049 0.06925 0.05110 0.00420 AFIX 23 H44A 2 0.768797 0.374497 0.311721 10.50000 -1.20000 H44B 2 0.668296 0.370353 0.302147 10.50000 -1.20000 AFIX 0 C45 1 0.744525 0.448812 0.274862 10.50000 0.21416 0.54599 = 0.14051 0.06923 0.05111 0.00422 AFIX 23 H45A 2 0.795850 0.493179 0.277781 10.50000 -1.20000 H45B 2 0.695045 0.491427 0.268404 10.50000 -1.20000 AFIX 0 C46 1 0.768820 0.387020 0.247916 10.50000 0.21420 0.54605 = 0.14057 0.06923 0.05112 0.00427 AFIX 137 H46A 2 0.719541 0.388691 0.234048 10.50000 -1.50000 H46B 2 0.780133 0.318913 0.253765 10.50000 -1.50000 H46C 2 0.822180 0.414300 0.238859 10.50000 -1.50000 AFIX 0 PART 0 C47 1 0.413548 0.183514 0.558969 11.00000 0.07552 0.05562 = 0.04743 -0.00440 0.00107 0.02244 AFIX 23 H47A 2 0.403665 0.135607 0.543157 11.00000 -1.20000 H47B 2 0.478462 0.191011 0.561487 11.00000 -1.20000 AFIX 0 C48 1 0.375213 0.141926 0.586561 11.00000 0.14176 0.18324 = 0.12931 0.08872 0.03702 0.03935 AFIX 23 H48A 2 0.310097 0.136117 0.584220 11.00000 -1.20000 H48B 2 0.386486 0.189090 0.602468 11.00000 -1.20000 AFIX 0 C49 1 0.412170 0.041624 0.595402 11.00000 0.14176 0.18324 = 0.12931 0.08872 0.03702 0.03935 AFIX 23 H49A 2 0.399470 -0.006649 0.579901 11.00000 -1.20000 H49B 2 0.477408 0.046433 0.597567 11.00000 -1.20000 AFIX 0 C50 1 0.372517 0.005543 0.623468 11.00000 0.14176 0.18324 = 0.12931 0.08872 0.03702 0.03935 PART 1 AFIX 23 H50A 2 0.308945 0.023463 0.624653 10.50000 -1.20000 H50B 2 0.404035 0.034601 0.640232 10.50000 -1.20000 AFIX 23 PART 2 H50C 2 0.308150 0.019614 0.622263 10.50000 -1.20000 H50D 2 0.396486 0.048822 0.638836 10.50000 -1.20000 AFIX 0 PART 1 C51 1 0.385179 -0.121184 0.623111 10.50000 0.19695 0.18464 = 0.21485 0.08861 0.03691 0.03926 AFIX 23 H51A 2 0.340814 -0.153901 0.610552 10.50000 -1.20000 H51B 2 0.445751 -0.141263 0.617316 10.50000 -1.20000 AFIX 0 C52 1 0.366529 -0.140731 0.657371 10.50000 0.19736 0.18493 = 0.21524 0.08844 0.03672 0.03902 AFIX 23 H52A 2 0.406431 -0.191818 0.665366 10.50000 -1.20000 H52B 2 0.372346 -0.079755 0.668916 10.50000 -1.20000 AFIX 0 C53 1 0.270286 -0.176104 0.655866 10.50000 0.19774 0.18519 = 0.21571 0.08816 0.03652 0.03885 AFIX 23 H53A 2 0.265561 -0.245150 0.662453 10.50000 -1.20000 H53B 2 0.247251 -0.171497 0.635826 10.50000 -1.20000 AFIX 0 C54 1 0.218042 -0.106765 0.676301 10.50000 0.19789 0.18535 = 0.21615 0.08788 0.03638 0.03884 AFIX 23 H54A 2 0.222189 -0.128901 0.696674 10.50000 -1.20000 H54B 2 0.239940 -0.038325 0.674889 10.50000 -1.20000 AFIX 0 C55 1 0.123056 -0.115563 0.664842 10.50000 0.19801 0.18539 = 0.21641 0.08769 0.03626 0.03876 AFIX 23 H55A 2 0.115243 -0.176222 0.653275 10.50000 -1.20000 H55B 2 0.106801 -0.058003 0.652839 10.50000 -1.20000 AFIX 0 C56 1 0.067840 -0.119224 0.692809 10.50000 0.18140 0.18123 = 0.18069 0.00044 0.00106 -0.00038 AFIX 137 H56A 2 0.004533 -0.118056 0.687914 10.50000 -1.50000 H56B 2 0.082260 -0.062211 0.704902 10.50000 -1.50000 H56C 2 0.081560 -0.179734 0.703422 10.50000 -1.50000 AFIX 0 PART 2 C44A 1 0.707177 0.479963 0.306114 10.50000 0.09789 0.31468 = 0.08872 0.02832 0.01637 -0.03760 AFIX 23 H44C 2 0.762239 0.440921 0.308279 10.50000 -1.20000 H44D 2 0.661505 0.437515 0.297079 10.50000 -1.20000 AFIX 0 C45A 1 0.724574 0.566967 0.287079 10.50000 0.09789 0.31468 = 0.08872 0.02832 0.01637 -0.03760 AFIX 23 H45C 2 0.770420 0.604131 0.297873 10.50000 -1.20000 H45D 2 0.669658 0.606410 0.288922 10.50000 -1.20000 AFIX 0 C46A 1 0.750693 0.581581 0.255921 10.50000 0.09789 0.31468 = 0.08872 0.02832 0.01637 -0.03760 AFIX 137 H46D 2 0.701161 0.562720 0.243313 10.50000 -1.50000 H46E 2 0.802469 0.540675 0.251509 10.50000 -1.50000 H46F 2 0.765447 0.650858 0.252666 10.50000 -1.50000 AFIX 0 C43A 1 0.675528 0.513604 0.335653 10.50000 0.09789 0.31468 = 0.08872 0.02832 0.01637 -0.03760 AFIX 23 H43C 2 0.618335 0.548923 0.333854 10.50000 -1.20000 H43D 2 0.719570 0.558544 0.344498 10.50000 -1.20000 AFIX 0 C60 1 0.176792 -0.196979 0.698570 10.50000 0.14656 0.18250 = 0.12778 0.09159 0.03433 0.04066 AFIX 23 H60A 2 0.163933 -0.246885 0.713585 10.50000 -1.20000 H60B 2 0.161691 -0.224202 0.679306 10.50000 -1.20000 AFIX 0 C59 1 0.273619 -0.163997 0.699849 10.50000 0.21323 0.22447 = 0.39693 0.14759 0.04468 -0.04150 AFIX 23 H59A 2 0.313970 -0.221427 0.700016 10.50000 -1.20000 H59B 2 0.284857 -0.124003 0.717381 10.50000 -1.20000 AFIX 0 C57 1 0.380488 -0.097666 0.634766 10.50000 0.23519 0.17789 = 0.12613 0.08879 0.02325 -0.02941 AFIX 23 H57A 2 0.413945 -0.099483 0.653224 10.50000 -1.20000 H57B 2 0.410007 -0.141090 0.620534 10.50000 -1.20000 AFIX 0 C61 1 0.126261 -0.100997 0.704400 10.50000 0.33289 0.16799 = 0.30246 0.12499 0.20758 0.06604 AFIX 137 H61A 2 0.082514 -0.090187 0.689000 10.50000 -1.50000 H61B 2 0.168210 -0.045964 0.704842 10.50000 -1.50000 H61C 2 0.095811 -0.105586 0.723079 10.50000 -1.50000 AFIX 0 C58 1 0.282205 -0.127637 0.639275 10.50000 0.14522 0.18317 = 0.13074 0.08869 0.03417 0.04041 AFIX 23 H58A 2 0.270837 -0.198197 0.635563 10.50000 -1.20000 H58B 2 0.239832 -0.086146 0.628341 10.50000 -1.20000 AFIX 0 C62 1 0.287191 -0.101699 0.671991 10.50000 0.14548 0.18317 = 0.13075 0.08879 0.03357 0.04041 AFIX 23 H62A 2 0.245139 -0.046308 0.674213 10.50000 -1.20000 H62B 2 0.346996 -0.072688 0.674437 10.50000 -1.20000 AFIX 0 HKLF 4 REM n2_a.res in I2/a REM wR2 = 0.3787, GooF = S = 1.448, Restrained GooF = 69.141 for all data REM R1 = 0.1186 for 5448 Fo > 4sig(Fo) and 0.1523 for all 8304 data REM 599 parameters refined using 636 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 0.425, deepest hole -0.424, 1-sigma level 0.094 Q1 1 0.7500 0.7500 0.2500 10.50000 0.05 0.42 Q2 1 0.7853 0.6312 0.2343 11.00000 0.05 0.34 Q3 1 0.7267 0.6834 0.2792 11.00000 0.05 0.22 Q4 1 0.3894 0.0857 0.6523 11.00000 0.05 0.19 Q5 1 0.6119 0.2858 0.3995 11.00000 0.05 0.15 ; _shelx_res_checksum 90113 _shelx_fab_file ; 0 0 -54 1.0072 0.0066 0 0 -52 -1.4309 -0.0175 0 0 -50 -0.1891 0.0027 0 0 -48 2.3698 0.0280 0 0 -46 -2.4480 -0.0308 0 0 -44 0.8704 0.0008 0 0 -42 -0.4396 0.0179 0 0 -40 1.7723 -0.0079 0 0 -38 -2.4518 0.0001 0 0 -36 0.9216 -0.0081 0 0 -34 0.9532 0.0071 0 0 -32 -0.5357 0.0076 0 0 -30 -1.1235 -0.0088 0 0 -28 0.2958 -0.0057 0 0 -26 2.5859 0.0057 0 0 -24 -1.7388 0.0111 0 0 -22 -3.9791 -0.0086 0 0 -20 6.3562 -0.0263 0 0 -18 -0.9654 0.0558 0 0 -16 -3.4436 -0.0404 0 0 -14 1.3282 -0.0109 0 0 -12 -6.4660 0.0502 0 0 -10 31.9641 -0.0453 0 0 -8 -59.2901 0.0188 0 0 -6 50.1253 -0.0187 0 0 -4 7.1095 0.0464 0 1 -53 0.3499 0.0005 0 1 -51 0.4340 0.0012 0 1 -49 -1.2637 -0.0040 0 1 -47 1.4435 0.0014 0 1 -45 -0.7170 0.0092 0 1 -43 -0.4886 -0.0130 0 1 -41 1.4735 -0.0004 0 1 -39 -1.7369 0.0134 0 1 -37 1.0503 -0.0082 0 1 -35 0.3082 -0.0023 0 1 -33 -1.2143 -0.0002 0 1 -31 0.5237 0.0050 0 1 -29 1.2559 0.0012 0 1 -27 -1.9866 -0.0050 0 1 -25 0.2588 -0.0022 0 1 -23 2.7344 0.0004 0 1 -21 -4.0498 0.0171 0 1 -19 1.6256 -0.0212 0 1 -17 3.7414 -0.0033 0 1 -15 -8.9883 0.0266 0 1 -13 11.3951 -0.0223 0 1 -11 -9.5238 0.0062 0 1 -9 1.4029 -0.0028 0 1 -7 14.1514 0.0093 0 1 -5 -30.7991 -0.0099 0 1 -3 33.9831 0.0007 0 1 -1 -15.0464 0.0113 0 2 -54 -0.5729 0.0035 0 2 -52 -0.0017 0.0059 0 2 -50 1.3613 -0.0075 0 2 -48 -2.1879 -0.0099 0 2 -46 1.0476 0.0193 0 2 -44 0.8435 -0.0030 0 2 -42 -0.8140 -0.0117 0 2 -40 -1.5944 0.0022 0 2 -38 3.8808 0.0087 0 2 -36 -3.3900 0.0006 0 2 -34 0.1730 -0.0100 0 2 -32 2.8916 0.0010 0 2 -30 -3.1468 0.0060 0 2 -28 1.0010 0.0040 0 2 -26 1.5374 -0.0091 0 2 -24 -3.5918 -0.0037 0 2 -22 3.8334 0.0094 0 2 -20 0.5339 0.0078 0 2 -18 -7.8628 -0.0248 0 2 -16 9.8439 0.0168 0 2 -14 -3.4642 0.0097 0 2 -12 -0.2928 -0.0308 0 2 -10 -8.8902 0.0271 0 2 -8 21.8494 0.0005 0 2 -6 -18.8336 -0.0180 0 2 -4 -4.8925 -0.0067 0 2 0 -45.0860 -0.0377 0 3 -53 0.8272 0.0033 0 3 -51 -1.6277 -0.0053 0 3 -49 1.7751 0.0006 0 3 -47 -1.0730 0.0001 0 3 -45 -0.0978 0.0020 0 3 -43 0.9289 -0.0004 0 3 -41 -1.1833 -0.0005 0 3 -39 1.5588 -0.0032 0 3 -37 -2.2537 0.0035 0 3 -35 2.2478 0.0027 0 3 -33 -1.0872 -0.0038 0 3 -31 -0.0517 -0.0032 0 3 -29 0.2668 0.0049 0 3 -27 -0.3529 0.0015 0 3 -25 1.2214 -0.0031 0 3 -23 -2.1520 -0.0003 0 3 -21 1.3364 -0.0031 0 3 -19 2.1196 0.0071 0 3 -17 -6.2303 0.0043 0 3 -15 6.9696 -0.0194 0 3 -9 3.5248 -0.0132 0 3 -7 -10.1533 -0.0090 0 3 -5 22.3068 0.0235 0 3 -3 -27.5228 -0.0131 0 3 -1 12.9560 -0.0071 0 4 -52 0.9460 0.0096 0 4 -50 -0.4801 0.0011 0 4 -48 -0.3803 0.0001 0 4 -46 1.2093 -0.0083 0 4 -44 -1.2055 0.0054 0 4 -42 -0.0526 0.0050 0 4 -40 2.1043 -0.0060 0 4 -38 -3.9164 -0.0005 0 4 -36 3.9528 0.0011 0 4 -34 -0.9448 0.0022 0 4 -32 -3.6209 -0.0003 0 4 -30 5.1991 -0.0021 0 4 -28 -1.2279 -0.0017 0 4 -26 -4.4131 0.0040 0 4 -24 5.0262 0.0006 0 4 -22 0.8457 -0.0035 0 4 -20 -7.1825 -0.0000 0 4 -18 6.9722 0.0037 0 4 -16 -0.3362 -0.0051 0 4 -14 -4.8676 0.0063 0 4 -12 2.2088 -0.0015 0 4 -10 4.4331 -0.0097 0 4 -8 -5.4904 0.0123 0 4 -6 -0.6240 -0.0018 0 4 -4 5.3763 -0.0010 0 4 -2 -3.7891 -0.0109 0 5 -51 0.4610 0.0048 0 5 -49 -0.2812 0.0017 0 5 -47 0.4737 -0.0028 0 5 -45 -0.8280 -0.0040 0 5 -43 1.0673 0.0040 0 5 -41 -0.7975 0.0035 0 5 -39 -0.8426 -0.0035 0 5 -37 3.7826 -0.0032 0 5 -35 -5.7821 0.0019 0 5 -33 4.5407 0.0041 0 5 -31 -0.6375 -0.0006 0 5 -29 -2.9807 -0.0052 0 5 -27 3.8711 -0.0002 0 5 -25 -2.0760 0.0060 0 5 -23 0.1021 0.0022 0 5 -21 -0.2501 -0.0098 0 5 -19 1.2822 0.0004 0 5 -17 -0.2055 0.0104 0 5 -15 -1.9899 -0.0051 0 5 -13 1.0679 -0.0041 0 5 -11 2.7955 0.0034 0 5 -9 -4.4413 -0.0022 0 5 -7 2.4318 0.0057 0 5 -5 -0.9548 -0.0017 0 5 -3 1.5352 -0.0081 0 5 -1 -1.0234 0.0061 0 6 -50 0.1578 0.0032 0 6 -48 0.0667 0.0023 0 6 -46 -0.2141 -0.0013 0 6 -44 0.1640 -0.0021 0 6 -42 -0.0955 0.0010 0 6 -40 0.0827 0.0039 0 6 -38 0.3048 -0.0052 0 6 -36 -1.1802 0.0005 0 6 -34 1.5524 0.0034 0 6 -32 -0.6078 -0.0011 0 6 -30 -0.4589 -0.0029 0 6 -28 -0.3861 0.0013 0 6 -26 2.5337 0.0037 0 6 -24 -2.3829 -0.0033 0 6 -22 -1.7269 -0.0026 0 6 -20 5.6850 0.0054 0 6 -18 -3.9266 -0.0020 0 6 -16 -2.4076 -0.0017 0 6 -14 5.5545 0.0004 0 6 -12 -1.1977 0.0034 0 6 -8 5.8430 0.0012 0 6 -6 -0.7012 0.0044 0 6 -4 -3.2478 -0.0082 0 6 -2 2.6891 0.0081 0 6 0 -1.4412 -0.0054 0 7 -49 -0.0430 -0.0010 0 7 -47 -0.2611 0.0042 0 7 -45 0.6063 -0.0010 0 7 -43 -0.2676 -0.0009 0 7 -41 -0.6246 -0.0023 0 7 -39 1.5288 0.0022 0 7 -37 -2.2349 0.0026 0 7 -35 2.5871 -0.0019 0 7 -33 -2.1499 -0.0036 0 7 -31 0.5761 0.0018 0 7 -29 1.6522 0.0052 0 7 -27 -2.8443 -0.0037 0 7 -25 1.5922 -0.0042 0 7 -23 0.4948 0.0037 0 7 -21 0.2526 0.0035 0 7 -19 -3.8784 -0.0030 0 7 -17 5.1150 -0.0046 0 7 -15 -0.6751 0.0063 0 7 -13 -5.0089 -0.0007 0 7 -11 5.5929 -0.0032 0 7 -9 -1.5001 0.0035 0 7 -7 -1.7271 -0.0026 0 7 -5 1.4364 -0.0003 0 7 -3 0.1111 0.0034 0 7 -1 -0.3571 -0.0011 0 8 -46 -0.2368 0.0049 0 8 -44 -0.7953 -0.0022 0 8 -42 1.1947 -0.0033 0 8 -40 -0.5335 0.0030 0 8 -38 -0.5003 0.0025 0 8 -36 1.1539 -0.0035 0 8 -34 -1.6579 -0.0015 0 8 -32 2.2005 0.0040 0 8 -30 -1.7555 -0.0017 0 8 -28 -0.1550 -0.0000 0 8 -26 1.5139 0.0002 0 8 -24 -0.3281 -0.0016 0 8 -22 -1.6716 0.0020 0 8 -20 0.9560 0.0011 0 8 -18 2.5242 -0.0030 0 8 -16 -4.9563 0.0005 0 8 -14 3.6001 0.0023 0 8 -12 0.2084 -0.0027 0 8 -10 -3.0860 0.0032 0 8 -8 3.0904 -0.0020 0 8 -6 -1.0952 -0.0036 0 8 -4 -0.6052 0.0070 0 8 -2 0.9175 -0.0020 0 8 0 -0.7460 -0.0034 0 9 -45 0.6918 0.0015 0 9 -43 -0.4724 0.0026 0 9 -41 0.8931 -0.0033 0 9 -39 -1.0370 0.0005 0 9 -37 0.1243 0.0002 0 9 -35 0.6132 0.0015 0 9 -33 0.4089 -0.0014 0 9 -31 -2.0854 -0.0007 0 9 -29 1.4980 0.0014 0 9 -27 1.7100 -0.0004 0 9 -25 -4.0980 0.0004 0 9 -23 2.9266 -0.0013 0 9 -21 0.0140 0.0010 0 9 -19 -1.0775 -0.0002 0 9 -17 -0.1423 0.0006 0 9 -15 0.8756 -0.0012 0 9 -13 0.3384 0.0003 0 9 -11 -1.9140 0.0004 0 9 -9 2.2066 0.0018 0 9 -7 -1.8294 -0.0037 0 9 -5 1.9525 0.0008 0 9 -3 -2.0603 0.0037 0 9 -1 0.9557 -0.0034 0 10 -42 -0.7814 -0.0007 0 10 -40 -0.0997 -0.0045 0 10 -38 1.3977 0.0030 0 10 -36 -1.6003 0.0020 0 10 -34 0.9603 -0.0028 0 10 -32 -1.1425 -0.0003 0 10 -30 2.0137 0.0017 0 10 -28 -1.4974 -0.0005 0 10 -26 -0.6557 -0.0009 0 10 -24 1.9772 0.0013 0 10 -22 -1.3366 -0.0000 0 10 -20 0.8992 -0.0026 0 10 -18 -2.3437 0.0033 0 10 -16 3.6797 0.0003 0 10 -14 -2.0612 -0.0040 0 10 -12 -1.7016 0.0029 0 10 -10 3.7204 0.0008 0 10 -8 -1.9736 -0.0024 0 10 -6 -1.0373 0.0019 0 10 -4 1.4855 -0.0013 0 10 -2 0.8169 -0.0001 0 10 0 -2.3304 0.0018 0 11 -39 0.5047 -0.0065 0 11 -37 0.1211 -0.0002 0 11 -35 -1.1875 0.0016 0 11 -33 0.7525 0.0001 0 11 -31 0.9381 0.0003 0 11 -29 -1.6357 -0.0017 0 11 -27 0.4876 0.0009 0 11 -25 0.9725 0.0005 0 11 -23 -1.2054 0.0003 0 11 -21 0.3460 -0.0016 0 11 -19 0.4521 0.0009 0 11 -17 -0.3028 0.0007 0 11 -15 -0.5449 -0.0007 0 11 -13 0.7298 -0.0004 0 11 -11 0.6444 0.0012 0 11 -9 -2.3876 -0.0019 0 11 -7 2.3382 0.0026 0 11 -5 -0.2949 -0.0016 0 11 -3 -1.4316 -0.0008 0 11 -1 0.9119 0.0014 0 12 -36 2.3442 -0.0071 0 12 -34 -2.0609 0.0044 0 12 -32 0.1744 0.0011 0 12 -30 1.1099 -0.0009 0 12 -28 -0.6563 -0.0024 0 12 -26 -0.1738 0.0017 0 12 -24 -0.2821 0.0016 0 12 -22 1.6502 -0.0018 0 12 -20 -2.3127 -0.0006 0 12 -18 1.6346 0.0011 0 12 -16 -0.4016 -0.0000 0 12 -14 -0.4715 -0.0004 0 12 -12 0.8239 0.0009 0 12 -10 -0.9895 -0.0015 0 12 -8 1.1665 -0.0001 0 12 -6 -1.1215 0.0027 0 12 -4 0.5178 -0.0016 0 12 -2 0.4233 -0.0025 0 12 0 -0.8954 0.0034 0 13 -31 -1.4754 0.0001 0 13 -29 0.9340 0.0001 0 13 -27 -0.2656 0.0007 0 13 -25 0.2888 -0.0006 0 13 -23 -0.1779 -0.0006 0 13 -21 -0.5721 0.0012 0 13 -19 0.8116 -0.0001 0 13 -17 0.0576 -0.0016 0 13 -15 -0.6117 0.0016 0 13 -13 -0.1415 0.0010 0 13 -11 0.8265 -0.0033 0 13 -9 -0.0588 0.0020 0 13 -7 -1.0598 0.0012 0 13 -5 0.8056 -0.0017 0 13 -3 0.2522 -0.0003 0 13 -1 -0.3598 0.0013 0 14 -26 1.3744 -0.0053 0 14 -24 -1.2952 0.0000 0 14 -22 -1.0163 0.0016 0 14 -20 2.2538 -0.0004 0 14 -18 -0.6210 0.0002 0 14 -16 -1.5657 -0.0008 0 14 -14 1.3830 0.0009 0 14 -12 0.7594 -0.0010 0 14 -10 -2.0888 0.0012 0 14 -8 1.1583 -0.0005 0 14 -6 0.7451 -0.0003 0 14 -4 -1.5945 -0.0000 0 14 -2 1.0833 -0.0000 0 14 0 -0.6090 0.0008 0 15 -19 -0.7272 0.0011 0 15 -17 0.0580 -0.0022 0 15 -15 1.3453 0.0004 0 15 -13 -1.5117 0.0016 0 15 -11 0.2306 -0.0018 0 15 -9 1.2238 0.0007 0 15 -7 -2.1452 0.0006 0 15 -5 2.6427 -0.0014 0 15 -3 -2.4393 0.0014 0 15 -1 1.0346 -0.0007 0 16 -8 1.2142 -0.0006 0 16 -6 -1.1861 -0.0009 0 16 -4 0.2244 0.0014 0 16 -2 0.7638 0.0004 0 16 0 -1.1447 -0.0026 1 1 -54 -0.6459 0.0013 1 1 -52 1.2528 0.0031 1 1 -50 -0.4742 -0.0095 1 1 -48 -1.7173 -0.0008 1 1 -46 2.6832 0.0160 1 1 -44 -1.3188 -0.0137 1 1 -42 0.1910 0.0014 1 1 -40 -1.7077 0.0009 1 1 -38 4.1756 0.0011 1 1 -36 -3.8570 0.0063 1 1 -34 0.4444 -0.0121 1 1 -32 1.9632 0.0015 1 1 -30 -0.8665 0.0110 1 1 -28 -0.3614 -0.0065 1 1 -26 -1.6402 -0.0045 1 1 -24 2.9866 0.0026 1 1 -22 1.1965 0.0043 1 1 -20 -5.7979 0.0039 1 1 -18 2.2948 -0.0245 1 1 -16 5.0713 0.0324 1 1 -14 -4.6107 -0.0134 1 1 -12 -0.3415 -0.0155 1 1 -10 -7.9635 0.0219 1 1 -8 32.6392 0.0006 1 1 -6 -49.1871 -0.0142 1 1 -4 30.9091 -0.0149 1 1 -2 20.0773 0.0591 1 1 0 -71.0245 -0.0610 1 1 2 84.0300 0.0171 1 1 4 -47.7956 0.0198 1 1 6 -9.1019 -0.0222 1 1 8 42.5376 0.0187 1 1 12 14.3252 0.0500 1 1 14 -3.6005 -0.0348 1 1 16 5.1343 -0.0072 1 1 18 -4.9452 0.0394 1 1 20 -0.2359 -0.0320 1 1 22 3.3389 -0.0022 1 1 24 -2.0288 0.0198 1 1 26 0.2805 -0.0044 1 1 28 -0.0277 -0.0116 1 1 30 -0.0986 0.0033 1 1 32 0.5197 0.0075 1 1 34 -0.2268 -0.0004 1 1 36 -0.9685 -0.0055 1 1 38 1.9784 -0.0021 1 1 40 -1.6735 -0.0012 1 1 42 0.3137 0.0219 1 1 44 0.3469 -0.0220 1 1 46 0.6470 -0.0119 1 1 48 -1.7422 0.0345 1 1 50 1.1362 -0.0150 1 1 52 0.4043 -0.0136 1 1 54 -0.9913 0.0137 1 2 -53 0.2987 0.0032 1 2 -51 -0.9518 -0.0036 1 2 -49 1.5616 0.0010 1 2 -47 -1.8982 -0.0011 1 2 -45 1.5156 -0.0016 1 2 -43 -0.2324 0.0074 1 2 -41 -1.4066 -0.0043 1 2 -39 2.5503 -0.0070 1 2 -37 -2.6018 0.0086 1 2 -35 1.4709 0.0018 1 2 -33 0.0636 -0.0047 1 2 -31 -0.5606 -0.0033 1 2 -29 -0.5790 0.0039 1 2 -27 1.9768 0.0048 1 2 -25 -1.4182 -0.0056 1 2 -23 -1.6470 0.0005 1 2 -21 4.7194 -0.0067 1 2 -19 -3.8977 0.0167 1 2 -17 -1.7717 -0.0068 1 2 -15 8.2149 -0.0165 1 2 -13 -11.1164 0.0226 1 2 -11 11.1664 -0.0074 1 2 -9 -9.4278 -0.0016 1 2 -7 0.1640 -0.0101 1 2 -5 21.1974 0.0258 1 2 -3 -42.5093 -0.0247 1 2 1 -11.4504 0.0177 1 2 3 -23.8969 -0.0309 1 2 5 39.0323 0.0325 1 2 7 -30.5105 -0.0278 1 2 9 13.0922 0.0176 1 2 11 0.6470 -0.0018 1 2 13 -8.0057 -0.0114 1 2 15 10.2070 0.0156 1 2 17 -8.1129 -0.0166 1 2 19 3.2497 0.0180 1 2 21 1.4617 -0.0103 1 2 23 -3.1841 -0.0065 1 2 25 1.3678 0.0118 1 2 27 1.3661 0.0012 1 2 29 -1.7807 -0.0100 1 2 31 -0.0993 0.0015 1 2 33 1.3844 0.0051 1 2 35 -0.6144 0.0029 1 2 37 -0.7904 -0.0070 1 2 39 1.4334 -0.0047 1 2 41 -1.5672 0.0134 1 2 43 1.4482 -0.0059 1 2 45 -0.5130 -0.0016 1 2 47 -1.1323 -0.0039 1 2 49 2.1424 0.0085 1 2 51 -1.5571 0.0002 1 2 53 0.0447 -0.0104 1 3 -52 0.7191 0.0107 1 3 -50 -1.2124 0.0002 1 3 -48 1.2083 -0.0054 1 3 -46 -0.3196 -0.0041 1 3 -44 -0.9718 0.0095 1 3 -42 1.1635 -0.0022 1 3 -40 0.8074 -0.0023 1 3 -38 -4.1061 -0.0018 1 3 -36 5.9142 0.0014 1 3 -34 -3.5774 0.0055 1 3 -32 -1.9765 -0.0047 1 3 -30 6.0176 -0.0030 1 3 -28 -4.8865 0.0024 1 3 -26 -0.0571 0.0054 1 3 -24 4.4489 -0.0053 1 3 -22 -4.8027 -0.0032 1 3 -20 0.0837 0.0067 1 3 -18 6.9316 -0.0012 1 3 -16 -9.9555 -0.0058 1 3 -14 5.7975 0.0074 1 3 -12 -0.0102 0.0000 1 3 -10 -0.0978 -0.0098 1 3 -8 -3.5701 0.0052 1 3 -6 3.3062 0.0128 1 3 -4 2.3142 -0.0130 1 3 -2 -8.0932 -0.0179 1 3 0 11.1854 0.0406 1 3 2 -11.6930 -0.0189 1 3 4 7.7659 -0.0210 1 3 6 0.6981 0.0304 1 3 8 -6.9432 -0.0100 1 3 10 4.9208 -0.0037 1 3 12 1.1017 -0.0019 1 3 14 -2.2146 0.0084 1 3 16 -2.8967 -0.0030 1 3 18 7.7635 -0.0069 1 3 20 -7.2786 0.0077 1 3 22 2.1350 0.0017 1 3 24 3.3777 -0.0066 1 3 26 -4.8797 -0.0022 1 3 28 1.3881 0.0097 1 3 30 3.2562 -0.0011 1 3 32 -4.2898 -0.0093 1 3 34 1.2083 0.0029 1 3 36 2.6401 0.0067 1 3 38 -4.2784 -0.0006 1 3 40 3.1143 -0.0074 1 3 42 -0.4343 -0.0008 1 3 44 -1.5037 0.0092 1 3 46 1.2412 0.0005 1 3 48 0.2992 -0.0114 1 3 50 -1.1570 0.0025 1 3 52 0.8554 0.0123 1 4 -53 -1.5179 -0.0011 1 4 -51 1.7014 0.0063 1 4 -49 -1.1342 -0.0013 1 4 -47 0.6029 -0.0021 1 4 -45 -0.3262 -0.0020 1 4 -43 0.1339 0.0038 1 4 -41 0.0046 0.0004 1 4 -39 -0.5788 -0.0014 1 4 -37 2.3314 -0.0019 1 4 -35 -4.6244 0.0007 1 4 -33 5.3864 0.0035 1 4 -31 -3.4087 -0.0016 1 4 -29 -0.1811 -0.0026 1 4 -27 2.9713 -0.0003 1 4 -25 -3.4844 0.0038 1 4 -23 2.4604 0.0022 1 4 -21 -1.3644 -0.0080 1 4 -19 -0.3341 0.0014 1 4 -17 3.7422 0.0063 1 4 -15 -6.0424 -0.0012 1 4 -13 2.7064 -0.0059 1 4 -11 4.0973 0.0009 1 4 -9 -6.6245 0.0049 1 4 -5 -3.6644 -0.0139 1 4 -3 8.2595 0.0116 1 4 -1 -9.2668 -0.0007 1 4 1 2.0891 -0.0072 1 4 3 5.5899 0.0117 1 4 5 -6.4799 -0.0138 1 4 7 4.2539 0.0088 1 4 9 -4.7693 0.0001 1 4 11 6.1962 -0.0023 1 4 13 -4.3258 -0.0032 1 4 15 0.2635 0.0062 1 4 17 2.3598 -0.0008 1 4 19 -2.5852 -0.0078 1 4 21 1.4700 0.0112 1 4 23 -0.0012 -0.0064 1 4 25 -1.0526 -0.0002 1 4 27 1.5115 0.0012 1 4 29 -1.6956 0.0011 1 4 31 1.0368 0.0006 1 4 33 1.2249 -0.0034 1 4 35 -3.5880 0.0005 1 4 37 3.4789 0.0029 1 4 39 -1.1543 0.0011 1 4 41 -0.5562 -0.0056 1 4 43 0.3968 0.0004 1 4 45 0.1681 0.0068 1 4 47 0.1923 -0.0036 1 4 49 -1.0194 -0.0045 1 4 51 1.2992 0.0056 1 4 53 -0.8145 -0.0011 1 5 -52 -1.2763 -0.0139 1 5 -50 0.5457 0.0097 1 5 -48 0.8544 -0.0006 1 5 -46 -1.5002 0.0006 1 5 -44 0.7821 -0.0050 1 5 -42 0.2689 0.0028 1 5 -40 -0.6919 0.0032 1 5 -38 1.1986 -0.0040 1 5 -36 -2.4352 0.0001 1 5 -34 2.7277 0.0015 1 5 -32 -0.2767 0.0001 1 5 -30 -2.8678 -0.0016 1 5 -28 2.3696 0.0006 1 5 -26 2.0669 0.0024 1 5 -24 -4.8373 -0.0040 1 5 -22 1.0259 0.0017 1 5 -20 6.3609 0.0013 1 5 -18 -8.4976 -0.0009 1 5 -16 1.4149 0.0008 1 5 -14 7.4832 -0.0056 1 5 -12 -7.3377 0.0091 1 5 -10 -1.9618 -0.0035 1 5 -8 8.8102 -0.0038 1 5 -6 -5.1679 0.0025 1 5 -4 -3.1842 0.0013 1 5 -2 6.2027 0.0046 1 5 0 -3.7029 -0.0146 1 5 2 2.6901 0.0128 1 5 4 -4.2603 0.0008 1 5 6 2.2708 -0.0106 1 5 8 4.8447 0.0093 1 5 10 -9.3758 -0.0047 1 5 12 4.9528 0.0049 1 5 14 3.6747 -0.0073 1 5 16 -6.3854 0.0047 1 5 18 0.7487 0.0039 1 5 20 5.4983 -0.0098 1 5 22 -4.9930 0.0066 1 5 24 -0.4689 -0.0001 1 5 26 3.7467 -0.0012 1 5 28 -1.9491 -0.0001 1 5 30 -1.3345 -0.0021 1 5 32 2.1647 0.0034 1 5 34 -0.6558 0.0019 1 5 36 -1.0916 -0.0067 1 5 38 2.0539 0.0021 1 5 40 -2.0976 0.0045 1 5 42 1.1804 -0.0035 1 5 44 0.0906 -0.0003 1 5 46 -0.6922 -0.0019 1 5 48 0.5177 0.0060 1 5 50 -0.2466 -0.0039 1 5 52 0.0371 -0.0028 1 6 -47 -0.2653 0.0009 1 6 -45 0.9445 -0.0010 1 6 -43 -0.8747 -0.0010 1 6 -41 0.0474 -0.0026 1 6 -39 1.0678 0.0047 1 6 -37 -2.5812 0.0008 1 6 -35 4.2933 -0.0037 1 6 -33 -4.7957 -0.0017 1 6 -31 2.7333 0.0038 1 6 -29 1.1985 0.0024 1 6 -27 -3.9999 -0.0042 1 6 -25 3.0403 -0.0022 1 6 -23 0.1469 0.0030 1 6 -21 -0.6031 0.0044 1 6 -19 -3.1728 -0.0045 1 6 -17 5.7691 -0.0056 1 6 -15 -2.2655 0.0095 1 6 -13 -3.8838 -0.0012 1 6 -11 5.5665 -0.0070 1 6 -9 -1.8672 0.0076 1 6 -7 -2.2322 -0.0037 1 6 -5 3.4163 -0.0025 1 6 -3 -2.2885 0.0078 1 6 -1 0.4874 -0.0043 1 6 1 0.5719 -0.0063 1 6 3 -0.3766 0.0097 1 6 5 0.5264 -0.0012 1 6 7 -2.2215 -0.0075 1 6 9 2.8513 0.0087 1 6 11 0.2691 -0.0065 1 6 13 -4.0179 0.0027 1 6 15 3.1759 0.0031 1 6 17 1.2970 -0.0065 1 6 19 -3.7199 0.0040 1 6 21 2.1920 -0.0006 1 6 23 -0.0968 0.0006 1 6 25 0.1879 -0.0009 1 6 27 -1.7088 -0.0002 1 6 29 2.5794 0.0002 1 6 31 -1.4481 0.0003 1 6 33 -1.4850 0.0006 1 6 35 4.1479 -0.0012 1 6 37 -4.3249 0.0007 1 6 39 2.1889 -0.0013 1 6 41 0.1755 0.0025 1 6 43 -1.3826 -0.0017 1 6 45 1.5149 0.0001 1 6 47 -1.0826 0.0007 1 6 49 0.5188 -0.0028 1 7 -48 0.2311 0.0004 1 7 -46 0.1540 0.0050 1 7 -44 -0.2689 -0.0036 1 7 -42 0.5021 -0.0017 1 7 -40 -0.9857 0.0025 1 7 -38 0.8453 0.0019 1 7 -36 0.5162 -0.0035 1 7 -34 -2.1991 -0.0007 1 7 -32 2.6944 0.0033 1 7 -30 -1.5787 -0.0002 1 7 -28 0.0316 -0.0017 1 7 -26 0.2568 -0.0013 1 7 -24 0.8897 0.0029 1 7 -22 -1.3897 0.0007 1 7 -20 -0.5548 -0.0033 1 7 -18 3.4040 0.0005 1 7 -16 -3.8180 0.0031 1 7 -14 1.2896 -0.0024 1 7 -12 1.1906 -0.0018 1 7 -10 -1.4657 0.0069 1 7 -8 0.7107 -0.0084 1 7 -6 -0.8091 0.0027 1 7 -4 1.4119 0.0061 1 7 -2 -0.9720 -0.0088 1 7 0 -0.4804 0.0054 1 7 2 1.1791 -0.0037 1 7 4 -0.2792 0.0036 1 7 6 -0.7267 0.0014 1 7 8 0.3250 -0.0082 1 7 10 0.5106 0.0076 1 7 12 -0.1496 -0.0011 1 7 14 -0.4282 -0.0020 1 7 16 -0.8338 -0.0002 1 7 18 2.9469 0.0018 1 7 20 -2.8779 -0.0011 1 7 22 0.5112 0.0000 1 7 24 1.0992 0.0013 1 7 26 -0.6272 -0.0023 1 7 28 0.0248 0.0014 1 7 30 -0.7128 0.0003 1 7 32 1.5251 0.0000 1 7 34 -1.2481 -0.0016 1 7 36 0.4904 0.0010 1 7 38 -0.0839 0.0014 1 7 40 -0.2768 -0.0020 1 7 42 0.8346 0.0006 1 7 44 -0.8234 0.0010 1 7 46 -0.2089 -0.0023 1 7 48 1.2443 0.0030 1 8 -47 -0.2706 0.0006 1 8 -45 0.3379 0.0005 1 8 -43 -0.5638 0.0012 1 8 -41 1.2525 -0.0001 1 8 -39 -1.6373 -0.0025 1 8 -37 1.0964 0.0009 1 8 -35 -0.3816 0.0020 1 8 -33 0.7036 -0.0006 1 8 -31 -1.6095 -0.0019 1 8 -29 1.0247 -0.0000 1 8 -27 1.5793 0.0025 1 8 -25 -3.4483 -0.0004 1 8 -23 2.1478 -0.0024 1 8 -21 0.2831 0.0006 1 8 -19 0.0343 0.0026 1 8 -17 -2.6812 -0.0015 1 8 -15 3.2778 -0.0023 1 8 -13 -0.1437 0.0038 1 8 -11 -3.2127 -0.0021 1 8 -9 3.3259 0.0006 1 8 -7 -1.3417 -0.0010 1 8 -5 0.6614 0.0016 1 8 -3 -1.9780 -0.0002 1 8 -1 2.6864 -0.0021 1 8 1 -0.9163 0.0027 1 8 3 -1.6056 -0.0021 1 8 5 2.0409 0.0023 1 8 7 -0.8326 -0.0021 1 8 9 1.0010 -0.0007 1 8 11 -2.9271 0.0034 1 8 13 3.2946 -0.0017 1 8 15 -0.5802 -0.0020 1 8 17 -2.0513 0.0011 1 8 19 1.6740 0.0036 1 8 21 -0.0922 -0.0045 1 8 23 0.4840 -0.0009 1 8 25 -2.2784 0.0060 1 8 27 2.5653 -0.0045 1 8 29 -0.7918 -0.0011 1 8 31 -0.9085 0.0042 1 8 33 1.1535 -0.0020 1 8 35 -0.7214 -0.0013 1 8 37 0.7257 0.0015 1 8 39 -1.0375 -0.0001 1 8 41 0.9383 0.0003 1 8 43 -0.4630 -0.0006 1 8 45 0.2767 -0.0014 1 8 47 -0.4175 0.0021 1 9 -44 0.5034 0.0057 1 9 -42 -0.8048 -0.0036 1 9 -40 0.5480 -0.0025 1 9 -38 0.4680 0.0027 1 9 -36 -1.3562 0.0023 1 9 -34 1.4793 -0.0036 1 9 -32 -1.6577 -0.0003 1 9 -30 2.2802 0.0030 1 9 -28 -1.7898 -0.0019 1 9 -26 -0.5793 -0.0004 1 9 -24 2.3826 0.0019 1 9 -22 -1.2260 -0.0015 1 9 -20 -1.0561 -0.0012 1 9 -18 0.6569 0.0029 1 9 -16 2.5213 -0.0002 1 9 -14 -4.3806 -0.0040 1 9 -12 2.1027 0.0041 1 9 -10 2.0096 -0.0012 1 9 -8 -3.3946 -0.0012 1 9 -6 1.0511 0.0036 1 9 -4 1.3449 -0.0050 1 9 -2 -0.6371 0.0016 1 9 0 -1.5446 0.0040 1 9 2 1.5832 -0.0028 1 9 4 0.5986 -0.0053 1 9 6 -1.5350 0.0088 1 9 8 -0.6398 -0.0023 1 9 10 3.4489 -0.0057 1 9 12 -3.0924 0.0071 1 9 14 -0.8562 -0.0043 1 9 16 4.5726 0.0024 1 9 18 -4.2481 -0.0016 1 9 20 0.8583 0.0001 1 9 22 1.0665 0.0016 1 9 24 0.2692 -0.0021 1 9 26 -1.6976 0.0011 1 9 28 0.4476 0.0001 1 9 30 1.6515 0.0000 1 9 32 -1.7341 -0.0013 1 9 34 0.5447 0.0018 1 9 36 -0.4586 -0.0010 1 9 38 1.2506 0.0002 1 9 40 -0.9924 -0.0005 1 9 42 -0.3384 0.0012 1 9 44 0.9406 -0.0008 1 10 -43 0.0681 -0.0004 1 10 -41 -0.0349 0.0049 1 10 -39 0.7274 -0.0033 1 10 -37 -0.6261 -0.0006 1 10 -35 -0.5852 0.0004 1 10 -33 1.0255 0.0021 1 10 -31 0.3809 -0.0017 1 10 -29 -1.7868 -0.0010 1 10 -27 0.9482 0.0015 1 10 -25 1.4918 0.0003 1 10 -23 -2.9163 -0.0005 1 10 -21 2.1061 -0.0013 1 10 -19 -0.3078 0.0016 1 10 -17 -0.6697 0.0004 1 10 -15 0.4382 -0.0017 1 10 -13 -0.0968 0.0011 1 10 -11 0.6986 0.0001 1 10 -9 -1.8888 -0.0018 1 10 -7 2.3669 0.0043 1 10 -5 -1.5832 -0.0046 1 10 -3 0.3488 0.0009 1 10 -1 0.2641 0.0025 1 10 1 -0.0057 -0.0018 1 10 3 -0.5017 0.0004 1 10 5 0.2969 -0.0021 1 10 7 1.0067 0.0036 1 10 9 -2.3974 -0.0007 1 10 11 2.2460 -0.0034 1 10 13 -0.4969 0.0035 1 10 15 -0.8088 -0.0002 1 10 17 0.0873 -0.0022 1 10 19 1.4509 0.0019 1 10 21 -1.1995 -0.0003 1 10 23 -1.2728 -0.0003 1 10 25 3.2652 -0.0004 1 10 27 -2.2407 0.0009 1 10 29 -0.7106 -0.0003 1 10 31 2.1229 0.0006 1 10 33 -0.7677 -0.0030 1 10 35 -0.9015 0.0041 1 10 37 0.5984 -0.0009 1 10 39 0.6676 -0.0036 1 10 41 -0.8356 0.0053 1 10 43 0.1590 -0.0041 1 11 -40 -0.9996 0.0026 1 11 -38 0.4634 -0.0038 1 11 -36 1.2422 -0.0020 1 11 -34 -2.1119 0.0062 1 11 -32 1.3008 -0.0035 1 11 -30 -0.3093 -0.0011 1 11 -28 0.3978 0.0018 1 11 -26 -0.7280 0.0000 1 11 -24 0.0888 -0.0011 1 11 -22 1.1522 0.0010 1 11 -20 -1.9465 0.0000 1 11 -18 2.1731 -0.0012 1 11 -16 -2.1803 0.0010 1 11 -14 1.6101 0.0008 1 11 -12 0.0095 -0.0012 1 11 -10 -1.8647 -0.0007 1 11 -8 2.3489 0.0013 1 11 -6 -1.1450 0.0007 1 11 -4 -0.2199 -0.0018 1 11 -2 0.3691 0.0001 1 11 0 0.1971 0.0013 1 11 2 -0.0868 -0.0008 1 11 4 -0.7827 0.0010 1 11 6 0.9098 -0.0026 1 11 8 0.7130 0.0023 1 11 10 -2.8935 0.0003 1 11 12 3.3107 -0.0016 1 11 14 -1.3079 0.0007 1 11 16 -1.2106 -0.0001 1 11 18 2.2237 0.0004 1 11 20 -2.0099 -0.0002 1 11 22 1.9923 0.0004 1 11 24 -2.1124 -0.0011 1 11 26 1.2542 0.0005 1 11 28 0.2262 0.0017 1 11 30 -0.7200 -0.0025 1 11 32 0.1706 0.0004 1 11 34 -0.3048 0.0025 1 11 36 1.6005 -0.0035 1 11 38 -2.2788 0.0022 1 11 40 1.1666 0.0008 1 12 -35 0.9987 -0.0020 1 12 -33 -0.8520 -0.0007 1 12 -31 0.1218 0.0030 1 12 -29 0.3897 -0.0024 1 12 -27 -0.4851 0.0006 1 12 -25 0.6252 0.0006 1 12 -23 -0.6059 -0.0010 1 12 -21 -0.0006 0.0008 1 12 -19 0.4913 0.0004 1 12 -17 -0.0725 -0.0018 1 12 -15 -0.4019 0.0017 1 12 -13 -0.1904 0.0006 1 12 -11 0.9137 -0.0035 1 12 -9 -0.1046 0.0041 1 12 -7 -1.5963 -0.0018 1 12 -5 1.9070 -0.0006 1 12 -3 -0.4417 0.0011 1 12 -1 -0.6391 -0.0004 1 12 1 -0.0424 -0.0004 1 12 3 0.9901 0.0011 1 12 5 -0.1963 -0.0010 1 12 7 -1.7038 -0.0012 1 12 9 2.3246 0.0043 1 12 11 -1.0143 -0.0045 1 12 13 -0.4698 0.0006 1 12 15 0.7614 0.0034 1 12 17 -0.4052 -0.0033 1 12 19 0.2796 -0.0002 1 12 21 -0.3961 0.0023 1 12 23 0.6204 -0.0005 1 12 25 -0.8428 -0.0022 1 12 27 0.3875 0.0016 1 12 29 0.9935 0.0016 1 12 31 -1.9407 -0.0036 1 12 33 1.2127 0.0029 1 12 35 0.1718 -0.0016 1 13 -32 -1.2875 -0.0019 1 13 -30 -1.6021 0.0025 1 13 -28 2.6597 0.0028 1 13 -26 -0.4527 -0.0049 1 13 -24 -1.6604 0.0017 1 13 -22 0.6145 0.0007 1 13 -20 1.8253 0.0005 1 13 -18 -2.0044 -0.0018 1 13 -16 -0.2283 0.0012 1 13 -14 1.7286 0.0001 1 13 -12 -0.6841 -0.0019 1 13 -10 -1.2883 0.0032 1 13 -8 1.6872 -0.0014 1 13 -6 -0.2422 -0.0022 1 13 -4 -1.1543 0.0030 1 13 -2 1.0611 -0.0004 1 13 0 -0.1800 -0.0015 1 13 2 0.0925 0.0005 1 13 4 -0.9589 0.0003 1 13 6 1.4101 0.0010 1 13 8 -0.5962 -0.0028 1 13 10 -0.5987 0.0034 1 13 12 0.6869 -0.0021 1 13 14 0.5252 -0.0008 1 13 16 -1.5212 0.0030 1 13 18 0.7605 -0.0016 1 13 20 1.2486 -0.0023 1 13 22 -2.2768 0.0041 1 13 24 1.2347 -0.0022 1 13 26 0.2876 -0.0007 1 13 28 -0.2993 0.0024 1 13 30 -0.8019 -0.0026 1 13 32 1.0906 0.0020 1 14 -27 -0.3355 0.0021 1 14 -25 -0.2030 -0.0001 1 14 -23 0.9932 -0.0021 1 14 -21 -0.5487 0.0024 1 14 -19 -0.5219 -0.0009 1 14 -17 0.3896 -0.0005 1 14 -15 0.9143 0.0003 1 14 -13 -1.4936 0.0002 1 14 -11 0.5890 0.0005 1 14 -9 0.5003 -0.0012 1 14 -7 -0.7720 0.0003 1 14 -5 0.8497 0.0008 1 14 -3 -1.2918 -0.0002 1 14 -1 1.3222 -0.0007 1 14 1 -0.3284 0.0001 1 14 3 -0.7866 0.0012 1 14 5 1.0410 -0.0013 1 14 7 -0.9393 0.0008 1 14 9 1.1368 -0.0013 1 14 11 -0.8028 0.0021 1 14 13 -0.7674 -0.0010 1 14 15 2.0371 -0.0013 1 14 17 -1.1279 0.0014 1 14 19 -0.9391 0.0015 1 14 21 1.5288 -0.0027 1 14 23 -0.4086 -0.0015 1 14 25 -0.2960 0.0069 1 14 27 -0.1349 -0.0062 1 15 -20 -0.5197 -0.0017 1 15 -18 0.9169 0.0011 1 15 -16 0.3579 0.0010 1 15 -14 -0.8808 -0.0017 1 15 -12 -0.3150 0.0014 1 15 -10 1.5713 -0.0010 1 15 -8 -1.2852 0.0000 1 15 -6 -0.0789 0.0004 1 15 -4 1.0101 0.0009 1 15 -2 -0.8695 -0.0013 1 15 0 0.2536 -0.0006 1 15 2 0.0120 0.0020 1 15 4 0.2775 -0.0007 1 15 6 -0.6867 -0.0006 1 15 8 0.6427 0.0001 1 15 10 -0.1008 0.0001 1 15 12 -0.2137 0.0012 1 15 14 -0.2807 -0.0017 1 15 16 0.8452 0.0006 1 15 18 -0.2087 0.0004 1 15 20 -1.2332 0.0000 1 16 -7 1.5374 0.0004 1 16 -5 -2.4191 0.0017 1 16 -3 2.6472 -0.0012 1 16 -1 -1.9037 0.0004 1 16 1 0.3680 -0.0008 1 16 3 1.1405 0.0004 1 16 5 -1.8761 0.0013 1 16 7 1.8859 -0.0012 2 0 -54 -0.1256 0.0002 2 0 -52 1.1561 -0.0012 2 0 -50 -1.8949 -0.0038 2 0 -48 0.4490 0.0040 2 0 -46 1.6228 0.0018 2 0 -44 -1.7538 -0.0070 2 0 -42 0.7884 0.0110 2 0 -40 -1.8641 -0.0122 2 0 -38 5.0546 0.0035 2 0 -36 -6.1137 0.0110 2 0 -34 2.4727 -0.0142 2 0 -32 1.7062 0.0022 2 0 -30 -0.8267 0.0090 2 0 -28 -2.6571 -0.0089 2 0 -26 1.1179 0.0034 2 0 -12 -1.8104 0.0099 2 0 -10 2.0854 -0.0018 2 0 -8 17.3579 0.0110 2 0 -6 -47.7626 -0.0166 2 0 -4 58.0902 -0.0059 2 0 -2 -25.4449 0.0317 2 0 2 88.9285 0.0088 2 0 4 -86.0069 -0.0234 2 0 6 32.7402 0.0498 2 0 8 24.2935 -0.0359 2 0 10 -43.9652 -0.0174 2 0 12 29.7012 0.0595 2 0 14 -11.7285 -0.0594 2 0 16 5.5002 0.0249 2 0 18 -4.1365 0.0180 2 0 20 0.6823 -0.0364 2 0 22 2.2129 0.0147 2 0 24 -1.8943 0.0178 2 0 26 0.5164 -0.0211 2 0 28 -0.0026 0.0026 2 0 30 -0.0354 0.0046 2 0 32 -0.0572 -0.0016 2 0 34 0.3511 0.0059 2 0 36 -0.6310 -0.0058 2 0 38 0.9477 -0.0098 2 0 40 -1.3815 0.0121 2 0 42 1.3629 0.0171 2 0 44 -0.7450 -0.0371 2 0 46 0.4248 0.0109 2 0 48 -0.6494 0.0286 2 0 52 0.5500 0.0032 2 0 54 -1.0913 0.0117 2 1 -53 -0.0159 0.0041 2 1 -51 -0.1144 -0.0016 2 1 -49 0.4410 -0.0009 2 1 -47 -1.0645 -0.0030 2 1 -45 1.6079 0.0008 2 1 -43 -1.3639 0.0111 2 1 -41 0.1212 -0.0113 2 1 -39 1.4193 -0.0071 2 1 -37 -2.1363 0.0164 2 1 -35 1.4144 -0.0023 2 1 -33 0.1898 -0.0092 2 1 -31 -1.2036 0.0010 2 1 -29 0.5112 0.0053 2 1 -27 1.4340 0.0037 2 1 -25 -2.7239 -0.0073 2 1 -23 1.5675 -0.0029 2 1 -21 1.7281 0.0029 2 1 -19 -4.3144 0.0147 2 1 -17 3.3672 -0.0223 2 1 -15 0.6980 0.0060 2 1 -9 -12.3905 0.0062 2 1 -7 11.2353 -0.0062 2 1 -5 0.7360 0.0137 2 1 -3 -20.9760 -0.0217 2 1 -1 34.1785 0.0212 2 1 1 -26.7181 -0.0095 2 1 3 2.8008 -0.0050 2 1 5 19.4444 0.0155 2 1 7 -26.3709 -0.0255 2 1 9 18.8285 0.0323 2 1 11 -6.2614 -0.0235 2 1 13 -3.2880 0.0026 2 1 15 7.1403 0.0105 2 1 17 -6.4909 -0.0123 2 1 19 3.6113 0.0159 2 1 21 -0.3436 -0.0170 2 1 23 -1.7313 0.0024 2 1 25 1.4594 0.0127 2 1 27 0.4562 -0.0053 2 1 29 -1.5610 -0.0104 2 1 31 0.5758 0.0070 2 1 33 0.9708 0.0059 2 1 35 -1.1497 -0.0032 2 1 37 0.1785 -0.0061 2 1 39 0.6313 -0.0003 2 1 41 -0.9366 0.0122 2 1 43 1.0163 -0.0076 2 1 45 -0.6054 -0.0042 2 1 47 -0.5178 0.0013 2 1 49 1.5212 0.0093 2 1 51 -1.3110 -0.0061 2 1 53 0.0523 -0.0082 2 2 -54 0.6012 0.0062 2 2 -52 -0.3782 0.0079 2 2 -50 -0.0182 -0.0059 2 2 -48 1.0368 -0.0047 2 2 -46 -1.5834 0.0054 2 2 -44 0.5724 0.0029 2 2 -42 0.7579 -0.0074 2 2 -40 0.2002 0.0059 2 2 -38 -3.8713 -0.0031 2 2 -36 6.8779 -0.0011 2 2 -34 -5.4075 0.0064 2 2 -32 0.3213 -0.0063 2 2 -30 3.4669 -0.0008 2 2 -28 -3.5935 0.0057 2 2 -26 2.4837 -0.0018 2 2 -24 -1.4657 -0.0052 2 2 -22 -1.4476 0.0063 2 2 -20 4.8315 -0.0012 2 2 -18 -2.5689 -0.0028 2 2 -16 -5.6070 0.0006 2 2 -14 10.4761 0.0030 2 2 -12 -6.7348 0.0002 2 2 -10 2.1297 -0.0057 2 2 -8 -6.0003 -0.0023 2 2 -6 15.1129 0.0210 2 2 -4 -17.1235 -0.0218 2 2 -2 4.0253 -0.0079 2 2 0 19.8192 0.0375 2 2 2 -38.4715 -0.0341 2 2 4 35.4584 0.0086 2 2 6 -11.3857 0.0070 2 2 8 -12.8023 -0.0066 2 2 10 18.1794 0.0059 2 2 12 -8.6550 -0.0104 2 2 14 1.2547 0.0124 2 2 16 -2.6780 -0.0063 2 2 18 6.1264 -0.0057 2 2 20 -5.6115 0.0122 2 2 22 2.2325 -0.0029 2 2 24 1.0358 -0.0122 2 2 26 -2.5585 0.0116 2 2 28 1.5315 0.0018 2 2 30 1.0024 -0.0044 2 2 32 -2.2621 -0.0043 2 2 34 1.0088 0.0037 2 2 36 1.2650 0.0041 2 2 38 -2.7768 -0.0002 2 2 40 2.8310 -0.0072 2 2 42 -1.4053 -0.0036 2 2 44 -0.4856 0.0186 2 2 46 1.0736 -0.0090 2 2 48 -0.0333 -0.0136 2 2 50 -0.9756 0.0146 2 2 52 0.7720 0.0042 2 2 54 0.0292 -0.0121 2 3 -53 -1.2392 0.0003 2 3 -51 1.8865 0.0036 2 3 -49 -1.7473 -0.0002 2 3 -47 1.4635 -0.0014 2 3 -45 -1.3230 -0.0001 2 3 -43 0.8840 -0.0016 2 3 -41 0.0391 0.0027 2 3 -39 -1.1569 0.0026 2 3 -37 2.2762 -0.0063 2 3 -35 -3.2235 0.0006 2 3 -33 3.5478 0.0051 2 3 -31 -2.9251 -0.0010 2 3 -29 1.6216 -0.0026 2 3 -27 -0.2805 -0.0032 2 3 -25 -0.7981 0.0073 2 3 -23 2.0763 -0.0006 2 3 -21 -3.5558 -0.0049 2 3 -19 3.0170 -0.0008 2 3 -17 1.7296 0.0060 2 3 -15 -7.6096 -0.0003 2 3 -13 8.0829 -0.0053 2 3 -11 -3.0626 0.0001 2 3 -9 0.3072 0.0054 2 3 -7 -1.9546 0.0029 2 3 -5 -1.5083 -0.0198 2 3 -3 15.2915 0.0276 2 3 -1 -27.0797 -0.0181 2 3 1 21.4745 -0.0021 2 3 3 -1.6125 0.0189 2 3 5 -15.1381 -0.0229 2 3 7 18.7161 0.0159 2 3 9 -13.3937 -0.0062 2 3 11 6.9239 -0.0005 2 3 13 -2.2784 0.0023 2 3 15 -0.8491 0.0013 2 3 17 2.8960 -0.0046 2 3 19 -3.5362 0.0001 2 3 21 2.1570 0.0072 2 3 23 0.3405 -0.0053 2 3 25 -1.3084 -0.0024 2 3 27 -0.0949 0.0012 2 3 29 1.2388 0.0063 2 3 31 -0.3151 -0.0045 2 3 33 -0.6531 -0.0039 2 3 35 -0.2827 0.0017 2 3 37 1.4816 0.0072 2 3 39 -0.9523 -0.0039 2 3 41 -0.1011 -0.0081 2 3 43 -0.1965 0.0076 2 3 45 0.9643 0.0038 2 3 47 -0.3051 -0.0053 2 3 49 -1.3628 -0.0042 2 3 51 1.9932 0.0072 2 3 53 -0.9656 -0.0003 2 4 -52 -1.2162 -0.0053 2 4 -50 1.5002 0.0109 2 4 -48 -0.3530 -0.0023 2 4 -46 -1.1104 -0.0016 2 4 -44 1.5145 -0.0035 2 4 -42 -0.8509 0.0050 2 4 -40 -0.1754 0.0000 2 4 -38 1.8140 -0.0017 2 4 -36 -4.2368 -0.0013 2 4 -34 5.2712 0.0013 2 4 -32 -2.3032 0.0026 2 4 -30 -3.0856 -0.0037 2 4 -28 5.5912 0.0010 2 4 -26 -2.4978 0.0013 2 4 -24 -2.7134 -0.0013 2 4 -22 4.0673 0.0010 2 4 -20 0.5332 -0.0025 2 4 -18 -6.6552 0.0055 2 4 -16 7.3883 -0.0048 2 4 -14 -1.5850 -0.0029 2 4 -12 -3.4371 0.0086 2 4 -10 1.1303 -0.0020 2 4 -8 4.3791 -0.0071 2 4 -6 -3.7708 0.0001 2 4 -4 -3.5150 0.0155 2 4 -2 8.7108 -0.0129 2 4 0 -7.0458 -0.0098 2 4 4 -1.8383 -0.0112 2 4 6 1.1572 -0.0058 2 4 8 1.8139 0.0078 2 4 10 -4.9217 0.0001 2 4 12 4.2161 -0.0023 2 4 14 -0.1757 -0.0047 2 4 16 -2.4858 0.0110 2 4 18 0.5469 -0.0069 2 4 20 3.6676 -0.0043 2 4 22 -4.8066 0.0090 2 4 24 1.1622 -0.0035 2 4 26 2.9404 -0.0008 2 4 28 -2.8291 -0.0012 2 4 30 -0.6050 -0.0001 2 4 32 3.0060 0.0059 2 4 34 -2.3703 -0.0042 2 4 36 0.0082 -0.0048 2 4 38 2.3113 0.0053 2 4 40 -3.4121 0.0037 2 4 42 2.5386 -0.0058 2 4 44 -0.3868 -0.0012 2 4 46 -1.0141 0.0027 2 4 48 0.7709 0.0040 2 4 50 -0.0214 -0.0063 2 4 52 -0.1924 0.0005 2 5 -51 -1.6416 -0.0073 2 5 -49 0.8014 0.0091 2 5 -47 -0.3128 -0.0026 2 5 -45 0.5024 -0.0002 2 5 -43 -0.5988 -0.0013 2 5 -41 0.3286 -0.0002 2 5 -39 0.1210 0.0027 2 5 -37 -1.2887 -0.0007 2 5 -35 3.7004 -0.0022 2 5 -33 -6.1417 0.0002 2 5 -31 6.1539 0.0022 2 5 -29 -2.6940 -0.0003 2 5 -27 -2.0294 -0.0011 2 5 -25 4.2164 -0.0012 2 5 -23 -2.9012 0.0004 2 5 -21 1.3951 0.0052 2 5 -19 -2.1230 -0.0055 2 5 -17 2.3192 -0.0030 2 5 -15 0.9825 0.0085 2 5 -13 -4.4240 -0.0036 2 5 -11 2.8435 -0.0037 2 5 -9 2.1026 0.0058 2 5 -7 -4.6148 -0.0045 2 5 -5 3.6310 0.0019 2 5 -3 -2.2704 0.0018 2 5 -1 1.3423 -0.0025 2 5 1 -0.0280 -0.0017 2 5 3 -0.3155 0.0035 2 5 5 -0.9610 0.0009 2 5 7 0.9347 -0.0038 2 5 9 1.8859 0.0010 2 5 11 -4.1044 0.0003 2 5 13 2.9687 0.0040 2 5 15 -0.6040 -0.0072 2 5 17 -0.2630 0.0037 2 5 19 0.0722 0.0032 2 5 21 0.0581 -0.0074 2 5 23 -0.2851 0.0057 2 5 25 0.5668 0.0003 2 5 27 -0.6455 -0.0037 2 5 29 1.0711 0.0014 2 5 31 -1.5865 0.0009 2 5 33 0.3565 0.0010 2 5 35 2.7255 -0.0019 2 5 37 -4.5479 -0.0003 2 5 39 2.9668 -0.0003 2 5 41 0.0722 0.0040 2 5 43 -1.5689 -0.0029 2 5 45 1.2797 -0.0024 2 5 47 -0.8407 0.0027 2 5 49 0.9547 0.0008 2 5 51 -0.9880 0.0006 2 6 -50 -0.8307 -0.0105 2 6 -48 -0.4266 0.0061 2 6 -46 1.5590 0.0007 2 6 -44 -0.9286 -0.0016 2 6 -42 -0.4486 -0.0009 2 6 -40 0.4065 0.0012 2 6 -38 0.6822 0.0007 2 6 -36 -0.4181 -0.0006 2 6 -34 -1.4983 -0.0019 2 6 -32 2.4679 0.0027 2 6 -30 -1.0158 0.0007 2 6 -28 -0.6999 -0.0032 2 6 -26 -0.1840 -0.0002 2 6 -24 2.8560 0.0048 2 6 -22 -3.0582 -0.0028 2 6 -20 -1.5048 -0.0028 2 6 -18 6.8926 0.0023 2 6 -16 -6.5036 0.0034 2 6 -14 -0.3037 -0.0044 2 6 -12 6.1389 -0.0014 2 6 -10 -4.5220 0.0067 2 6 -8 -1.7152 -0.0071 2 6 -6 4.4751 0.0055 2 6 -4 -1.0667 -0.0035 2 6 -2 -3.4257 -0.0005 2 6 0 4.1308 0.0066 2 6 2 -2.3218 -0.0116 2 6 4 1.5829 0.0110 2 6 6 -1.5006 -0.0032 2 6 8 -0.9646 -0.0057 2 6 10 4.9930 0.0080 2 6 12 -5.5670 -0.0043 2 6 14 1.0207 0.0020 2 6 16 3.3509 -0.0028 2 6 18 -2.3218 0.0017 2 6 20 -1.9667 0.0016 2 6 22 3.6333 -0.0019 2 6 24 -1.4260 -0.0006 2 6 26 -0.9520 0.0006 2 6 28 1.2254 0.0015 2 6 30 -0.6779 -0.0006 2 6 32 0.5094 -0.0023 2 6 34 -0.1991 0.0014 2 6 36 -0.3147 0.0025 2 6 38 0.1246 -0.0035 2 6 40 0.5889 0.0004 2 6 42 -0.5948 0.0021 2 6 44 -0.0615 -0.0017 2 6 46 0.0751 -0.0002 2 6 48 0.6561 0.0018 2 6 50 -0.8010 -0.0011 2 7 -49 -0.4194 -0.0085 2 7 -47 0.4418 0.0047 2 7 -45 -0.7422 -0.0016 2 7 -43 0.2750 0.0027 2 7 -41 1.1040 -0.0014 2 7 -39 -2.2195 -0.0028 2 7 -37 2.3102 0.0024 2 7 -35 -2.0111 0.0019 2 7 -33 2.1640 -0.0017 2 7 -31 -2.2400 -0.0021 2 7 -29 0.7349 0.0015 2 7 -27 2.2527 0.0019 2 7 -25 -3.7725 -0.0007 2 7 -23 1.5937 -0.0028 2 7 -21 1.4640 0.0010 2 7 -19 -0.4287 0.0036 2 7 -17 -4.1964 -0.0029 2 7 -15 6.1038 -0.0026 2 7 -13 -1.8809 0.0052 2 7 -11 -4.1550 -0.0018 2 7 -9 5.8033 -0.0030 2 7 -7 -2.3946 0.0036 2 7 -5 -1.5488 0.0013 2 7 -3 2.0442 -0.0059 2 7 -1 0.3458 0.0034 2 7 1 -1.8329 0.0042 2 7 3 0.5372 -0.0075 2 7 5 0.9283 0.0034 2 7 7 0.1475 0.0019 2 7 9 -1.5989 -0.0038 2 7 11 -0.2232 0.0038 2 7 13 3.7293 -0.0023 2 7 15 -3.9502 -0.0014 2 7 17 0.2892 0.0037 2 7 19 2.8401 -0.0009 2 7 21 -2.7911 -0.0031 2 7 23 1.3192 0.0024 2 7 25 -0.5765 0.0020 2 7 27 0.5663 -0.0046 2 7 29 -0.6599 0.0029 2 7 31 0.5916 0.0008 2 7 33 0.0607 -0.0030 2 7 35 -1.3939 0.0019 2 7 37 2.4609 -0.0000 2 7 39 -2.2530 0.0001 2 7 41 0.9711 -0.0006 2 7 43 0.3136 0.0006 2 7 45 -0.8347 -0.0031 2 7 47 0.7132 0.0067 2 7 49 -0.5789 -0.0034 2 8 -46 -0.5588 0.0024 2 8 -44 0.8037 0.0026 2 8 -42 -0.6683 -0.0031 2 8 -40 0.7192 -0.0009 2 8 -38 -0.5411 0.0019 2 8 -36 -0.4503 0.0016 2 8 -34 1.7552 -0.0026 2 8 -32 -2.5979 -0.0008 2 8 -30 2.7116 0.0021 2 8 -28 -1.7199 0.0004 2 8 -26 -0.4228 -0.0014 2 8 -24 2.0821 -0.0005 2 8 -22 -1.3489 0.0012 2 8 -20 -0.8239 0.0000 2 8 -18 1.2170 -0.0001 2 8 -16 1.3091 -0.0007 2 8 -14 -3.9684 0.0002 2 8 -12 3.3955 0.0015 2 8 -10 0.2500 -0.0034 2 8 -8 -3.4508 0.0048 2 8 -6 3.4547 -0.0021 2 8 -4 -1.3035 -0.0045 2 8 -2 -0.0922 0.0068 2 8 0 -0.0006 -0.0012 2 8 2 -0.0813 -0.0032 2 8 4 1.0241 -0.0008 2 8 6 -1.4215 0.0055 2 8 8 0.2280 -0.0025 2 8 10 1.6977 -0.0031 2 8 12 -2.6149 0.0034 2 8 14 1.2459 -0.0007 2 8 16 2.0482 0.0004 2 8 18 -4.5345 -0.0022 2 8 20 3.4376 0.0031 2 8 22 0.0700 -0.0019 2 8 24 -1.8266 -0.0011 2 8 26 0.5301 0.0035 2 8 28 0.7038 -0.0022 2 8 30 0.2673 -0.0015 2 8 32 -1.4997 0.0029 2 8 34 0.9314 -0.0009 2 8 36 0.2138 -0.0009 2 8 38 -0.1660 0.0002 2 8 40 -0.2731 0.0015 2 8 42 -0.3065 -0.0023 2 8 44 1.0895 0.0011 2 8 46 -0.4951 0.0027 2 9 -45 -0.6803 0.0014 2 9 -43 0.6865 -0.0028 2 9 -41 -0.8147 0.0034 2 9 -39 1.1852 -0.0001 2 9 -37 -0.9595 -0.0025 2 9 -35 -0.1292 0.0007 2 9 -33 0.7264 0.0019 2 9 -31 0.3360 -0.0010 2 9 -29 -1.7619 -0.0011 2 9 -27 1.1497 0.0008 2 9 -25 1.4352 0.0010 2 9 -23 -3.2473 -0.0007 2 9 -21 2.5982 -0.0014 2 9 -19 -0.9018 0.0019 2 9 -17 0.2834 0.0007 2 9 -15 -0.7605 -0.0031 2 9 -13 0.8003 0.0019 2 9 -11 0.2802 0.0006 2 9 -9 -1.5360 -0.0016 2 9 -7 1.9197 0.0023 2 9 -5 -1.7864 -0.0037 2 9 -3 2.1232 0.0034 2 9 -1 -2.6152 -0.0008 2 9 1 1.9118 -0.0005 2 9 3 -0.0360 -0.0000 2 9 5 -1.3028 -0.0014 2 9 7 1.4155 0.0045 2 9 9 -1.5482 -0.0041 2 9 11 2.2045 -0.0005 2 9 13 -1.9487 0.0034 2 9 15 0.2344 -0.0018 2 9 17 0.9287 -0.0007 2 9 19 0.0104 0.0005 2 9 21 -1.3493 0.0012 2 9 23 0.4935 -0.0009 2 9 25 2.0403 -0.0016 2 9 27 -3.1563 0.0031 2 9 29 1.4487 -0.0005 2 9 31 0.9654 -0.0031 2 9 33 -1.4475 0.0022 2 9 35 0.2264 0.0019 2 9 37 0.4799 -0.0026 2 9 39 0.1429 -0.0001 2 9 41 -0.8150 0.0002 2 9 43 0.6920 0.0022 2 9 45 -0.5197 -0.0006 2 10 -42 -0.3340 0.0046 2 10 -40 0.0058 -0.0030 2 10 -38 0.0926 -0.0022 2 10 -36 0.6559 0.0013 2 10 -34 -1.2151 0.0036 2 10 -32 0.8371 -0.0045 2 10 -30 -0.6164 0.0008 2 10 -28 1.2955 0.0021 2 10 -26 -1.4724 -0.0015 2 10 -24 -0.0322 -0.0009 2 10 -22 1.7658 0.0019 2 10 -20 -1.7076 -0.0003 2 10 -18 0.5010 -0.0019 2 10 -16 -0.4425 0.0011 2 10 -14 1.7393 0.0023 2 10 -12 -1.9872 -0.0039 2 10 -10 -0.0646 0.0014 2 10 -8 2.1603 0.0019 2 10 -6 -1.5822 -0.0027 2 10 -4 -0.6933 0.0016 2 10 -2 1.2480 0.0003 2 10 0 0.7273 -0.0025 2 10 2 -2.2412 0.0026 2 10 4 0.9346 0.0018 2 10 6 1.5151 -0.0071 2 10 8 -1.6976 0.0064 2 10 10 -1.0130 -0.0000 2 10 12 3.5621 -0.0048 2 10 14 -2.8401 0.0041 2 10 16 -0.5143 -0.0013 2 10 18 2.8633 0.0001 2 10 20 -2.2639 -0.0005 2 10 22 0.7848 0.0008 2 10 24 -0.9258 -0.0007 2 10 26 1.7266 0.0003 2 10 28 -0.8930 0.0002 2 10 30 -0.8942 -0.0004 2 10 32 1.1063 0.0004 2 10 34 0.1621 -0.0008 2 10 36 -0.3755 0.0014 2 10 38 -1.0557 -0.0009 2 10 40 1.9008 -0.0002 2 10 42 -0.9246 -0.0000 2 11 -39 -0.0437 0.0037 2 11 -37 0.4936 -0.0000 2 11 -35 -0.2599 -0.0026 2 11 -33 -0.5251 0.0002 2 11 -31 0.8972 0.0027 2 11 -29 -0.5840 -0.0024 2 11 -27 0.0473 0.0006 2 11 -25 0.2955 -0.0000 2 11 -23 -0.0538 0.0003 2 11 -21 -0.8997 0.0005 2 11 -19 1.6317 -0.0016 2 11 -17 -0.9764 0.0004 2 11 -15 -0.5094 0.0025 2 11 -13 1.0991 -0.0035 2 11 -11 -0.5915 0.0009 2 11 -9 0.5268 0.0027 2 11 -7 -1.4459 -0.0044 2 11 -5 1.9046 0.0037 2 11 -3 -0.8261 -0.0013 2 11 -1 -0.6891 -0.0012 2 11 1 0.7685 0.0020 2 11 3 0.7007 -0.0009 2 11 5 -1.7371 -0.0003 2 11 7 0.6424 0.0000 2 11 9 1.7325 0.0010 2 11 11 -2.8787 -0.0007 2 11 13 1.7356 -0.0011 2 11 15 0.1607 0.0027 2 11 17 -0.8443 -0.0018 2 11 19 0.1573 -0.0010 2 11 21 0.5000 0.0024 2 11 23 0.0959 -0.0009 2 11 25 -1.5832 -0.0011 2 11 27 2.1174 0.0008 2 11 29 -0.5399 0.0013 2 11 31 -1.6164 -0.0034 2 11 33 1.8306 0.0049 2 11 35 -0.2468 -0.0047 2 11 37 -0.6292 0.0019 2 11 39 -0.0508 0.0024 2 12 -36 0.8498 -0.0007 2 12 -32 -2.6739 0.0029 2 12 -30 0.3000 -0.0004 2 12 -28 2.1104 -0.0004 2 12 -26 -1.3917 -0.0002 2 12 -24 -0.9249 0.0005 2 12 -22 1.2026 -0.0011 2 12 -20 0.8904 0.0019 2 12 -18 -2.4040 -0.0016 2 12 -16 1.6584 0.0007 2 12 -14 -0.0590 -0.0004 2 12 -12 -0.5762 -0.0003 2 12 -10 0.2961 0.0023 2 12 -8 -0.1428 -0.0028 2 12 -6 0.4626 -0.0002 2 12 -4 -0.7508 0.0033 2 12 -2 0.5184 -0.0023 2 12 0 0.1287 -0.0006 2 12 2 -0.6382 0.0009 2 12 4 0.5946 0.0011 2 12 6 -0.0580 -0.0016 2 12 8 -0.6477 -0.0003 2 12 10 1.1906 0.0025 2 12 12 -1.2847 -0.0032 2 12 14 0.9390 0.0020 2 12 16 -0.5908 0.0002 2 12 18 0.4410 -0.0012 2 12 20 0.0597 -0.0001 2 12 22 -1.2387 0.0014 2 12 24 2.1290 -0.0014 2 12 26 -1.5739 0.0018 2 12 28 0.1762 -0.0030 2 12 30 0.2752 0.0020 2 12 32 0.5692 0.0017 2 12 34 -1.0114 -0.0042 2 12 36 -0.1318 0.0041 2 13 -31 0.1030 -0.0022 2 13 -29 -0.1689 0.0025 2 13 -27 -0.3923 -0.0007 2 13 -25 0.1898 -0.0012 2 13 -23 0.7355 0.0014 2 13 -21 -0.8100 0.0003 2 13 -19 -0.2208 -0.0018 2 13 -17 0.6179 0.0020 2 13 -15 0.3700 -0.0014 2 13 -13 -1.1075 0.0003 2 13 -11 0.3174 0.0020 2 13 -9 0.7622 -0.0041 2 13 -7 -0.4406 0.0030 2 13 -5 -0.7260 0.0003 2 13 -3 0.9911 -0.0015 2 13 -1 -0.2172 -0.0002 2 13 1 -0.2014 0.0012 2 13 3 -0.1694 -0.0004 2 13 5 0.2861 -0.0002 2 13 7 0.2430 0.0005 2 13 9 -0.4547 -0.0026 2 13 11 0.0750 0.0051 2 13 13 -0.2646 -0.0037 2 13 15 1.3095 -0.0015 2 13 17 -1.6119 0.0046 2 13 19 0.3055 -0.0017 2 13 21 1.1619 -0.0034 2 13 23 -1.4715 0.0036 2 13 25 1.3020 0.0016 2 13 27 -1.3165 -0.0053 2 13 29 0.6598 0.0029 2 13 31 0.9351 0.0018 2 14 -26 2.1275 0.0046 2 14 -24 1.4356 -0.0008 2 14 -22 -2.6953 -0.0017 2 14 -20 0.3940 -0.0005 2 14 -18 1.7093 0.0031 2 14 -16 -0.7279 -0.0034 2 14 -14 -1.5023 0.0020 2 14 -12 1.6814 0.0008 2 14 -10 0.4374 -0.0035 2 14 -8 -2.3491 0.0028 2 14 -6 2.2223 0.0009 2 14 -4 -0.6231 -0.0026 2 14 -2 -0.7644 0.0008 2 14 0 1.1176 0.0008 2 14 2 -0.8951 -0.0006 2 14 4 0.7880 0.0002 2 14 6 -0.8424 -0.0002 2 14 8 0.6422 0.0001 2 14 10 -0.0302 -0.0012 2 14 12 -0.4537 0.0028 2 14 14 0.0087 -0.0021 2 14 16 1.1809 -0.0011 2 14 18 -1.5410 0.0024 2 14 20 -0.0109 -0.0002 2 14 22 2.1013 -0.0021 2 14 24 -2.3324 0.0026 2 14 26 0.5587 -0.0020 2 15 -19 -1.1796 0.0009 2 15 -17 0.7578 0.0020 2 15 -15 -0.6776 -0.0028 2 15 -13 1.1169 0.0012 2 15 -11 -1.3360 0.0010 2 15 -9 0.7697 -0.0018 2 15 -7 0.3236 0.0011 2 15 -5 -1.4227 -0.0004 2 15 -3 2.2319 0.0002 2 15 -1 -2.3746 0.0002 2 15 1 1.4871 -0.0004 2 15 3 -0.0009 -0.0009 2 15 5 -1.1021 0.0025 2 15 7 1.5942 -0.0016 2 15 9 -1.8967 -0.0009 2 15 11 1.6138 0.0010 2 15 13 0.0264 0.0018 2 15 15 -1.9807 -0.0028 2 15 17 1.9247 0.0005 2 15 19 0.2249 0.0006 2 16 -4 -0.4866 -0.0005 2 16 -2 0.2318 0.0015 2 16 0 -0.0424 -0.0007 2 16 2 -0.1250 -0.0012 2 16 4 0.5892 0.0015 3 1 -54 -0.1026 0.0101 3 1 -52 -0.2544 0.0006 3 1 -50 1.3184 -0.0085 3 1 -48 -1.2220 0.0034 3 1 -46 -0.0442 0.0075 3 1 -44 0.5754 -0.0083 3 1 -42 0.1420 -0.0046 3 1 -40 0.2038 0.0154 3 1 -38 -3.5228 -0.0092 3 1 -36 7.3696 -0.0053 3 1 -34 -6.8691 0.0095 3 1 -32 1.8243 -0.0033 3 1 -30 1.6998 -0.0006 3 1 -28 -0.1773 0.0019 3 1 -26 -1.5255 -0.0057 3 1 -24 -1.3023 0.0048 3 1 -22 4.1065 0.0066 3 1 -20 -0.8881 -0.0135 3 1 -18 -3.8688 0.0035 3 1 -16 1.7995 0.0097 3 1 -14 4.4817 -0.0099 3 1 -12 -5.0844 0.0041 3 1 -10 0.1202 -0.0004 3 1 -8 -1.9308 -0.0087 3 1 -6 17.7264 0.0207 3 1 -4 -36.2639 -0.0174 3 1 -2 35.0945 0.0034 3 1 0 -2.9687 -0.0043 3 1 4 64.8685 0.0017 3 1 6 -45.0336 -0.0399 3 1 8 3.6246 0.0508 3 1 12 -22.3385 -0.0154 3 1 14 11.1968 0.0202 3 1 16 -5.3710 -0.0086 3 1 18 4.5706 -0.0019 3 1 20 -3.2810 0.0095 3 1 22 1.1124 -0.0079 3 1 24 0.3875 -0.0072 3 1 26 -1.1476 0.0187 3 1 28 0.8940 -0.0124 3 1 30 0.4813 0.0018 3 1 32 -1.3858 -0.0006 3 1 34 0.6940 0.0003 3 1 36 0.4758 0.0027 3 1 38 -1.0642 0.0032 3 1 40 1.5043 -0.0116 3 1 42 -1.8838 0.0001 3 1 44 1.4727 0.0223 3 1 46 -0.4926 -0.0215 3 1 48 -0.0188 -0.0038 3 1 50 -0.0116 0.0179 3 1 52 -0.1148 -0.0067 3 1 54 0.4201 -0.0063 3 2 -53 -0.3558 -0.0019 3 2 -51 0.6608 0.0021 3 2 -49 -0.7545 0.0019 3 2 -47 1.1704 0.0009 3 2 -45 -2.0303 -0.0046 3 2 -43 2.4773 -0.0032 3 2 -41 -1.6381 0.0107 3 2 -39 -0.3470 -0.0009 3 2 -37 2.3700 -0.0124 3 2 -35 -3.1467 0.0064 3 2 -33 2.2234 0.0072 3 2 -31 -0.5168 -0.0049 3 2 -29 -0.3788 -0.0044 3 2 -27 -0.3521 0.0001 3 2 -25 1.8491 0.0087 3 2 -23 -2.0128 -0.0035 3 2 -21 -0.4101 -0.0050 3 2 -19 3.4286 -0.0005 3 2 -17 -3.0965 0.0101 3 2 -15 -1.0707 -0.0078 3 2 -13 4.6357 0.0009 3 2 -11 -5.2865 -0.0019 3 2 -9 7.1348 0.0057 3 2 -7 -12.0170 -0.0019 3 2 -5 11.1440 -0.0092 3 2 -3 4.5724 0.0216 3 2 -1 -27.3949 -0.0279 3 2 1 36.8308 0.0201 3 2 3 -22.8116 -0.0027 3 2 5 -3.1356 -0.0097 3 2 7 21.6091 0.0132 3 2 9 -23.6738 -0.0162 3 2 11 14.2358 0.0165 3 2 15 -2.7959 -0.0038 3 2 17 4.2164 0.0023 3 2 19 -3.6864 0.0020 3 2 21 2.2304 0.0023 3 2 23 0.1292 -0.0047 3 2 25 -1.5692 -0.0031 3 2 27 0.3296 0.0053 3 2 29 1.7458 0.0055 3 2 31 -1.5502 -0.0095 3 2 33 -0.3733 -0.0018 3 2 35 1.0622 0.0064 3 2 37 -0.0950 0.0051 3 2 39 -0.4976 -0.0100 3 2 41 0.2546 -0.0025 3 2 43 -0.5124 0.0104 3 2 45 1.1791 -0.0016 3 2 47 -0.6159 -0.0050 3 2 49 -1.2199 -0.0025 3 2 51 2.2035 0.0086 3 2 53 -1.1352 -0.0018 3 3 -52 -0.1150 0.0049 3 3 -50 1.0157 0.0093 3 3 -48 -1.2626 -0.0069 3 3 -46 0.6133 -0.0031 3 3 -44 0.5383 0.0043 3 3 -42 -1.5027 0.0015 3 3 -40 1.3715 -0.0030 3 3 -38 0.9320 -0.0001 3 3 -36 -5.0584 0.0002 3 3 -34 7.7624 0.0019 3 3 -32 -5.6379 -0.0001 3 3 -30 -0.2029 -0.0044 3 3 -28 4.8882 0.0043 3 3 -26 -5.4101 0.0004 3 3 -24 2.7206 -0.0016 3 3 -22 0.9343 -0.0032 3 3 -20 -3.2464 0.0052 3 3 -18 1.8469 0.0011 3 3 -16 2.8969 -0.0083 3 3 -14 -6.7613 0.0068 3 3 -12 6.8977 -0.0014 3 3 -10 -5.5050 0.0030 3 3 -8 5.0929 -0.0076 3 3 -6 -4.0148 0.0013 3 3 -4 0.1089 0.0134 3 3 -2 5.3522 -0.0176 3 3 0 -10.0283 0.0056 3 3 2 12.5151 0.0068 3 3 4 -10.7772 -0.0073 3 3 6 3.9303 0.0012 3 3 8 3.7213 0.0020 3 3 10 -6.0877 0.0003 3 3 12 3.0880 -0.0064 3 3 14 -0.0520 0.0098 3 3 16 0.1185 -0.0039 3 3 18 -1.9523 -0.0051 3 3 20 3.4819 0.0043 3 3 22 -3.5278 0.0035 3 3 24 1.4636 -0.0041 3 3 26 1.3663 -0.0019 3 3 28 -1.9894 0.0031 3 3 30 -0.2129 -0.0015 3 3 32 2.3843 0.0046 3 3 34 -2.2578 -0.0060 3 3 36 0.4897 -0.0009 3 3 38 1.4884 0.0045 3 3 40 -2.9049 0.0028 3 3 42 2.9057 -0.0074 3 3 44 -1.2120 0.0001 3 3 46 -0.6501 0.0059 3 3 48 0.9492 -0.0006 3 3 50 -0.0136 -0.0046 3 3 52 -0.6524 0.0001 3 4 -51 -2.4359 -0.0001 3 4 -49 2.0636 0.0029 3 4 -47 -1.2675 -0.0014 3 4 -45 0.8372 -0.0002 3 4 -43 -0.6299 0.0016 3 4 -41 0.4405 -0.0023 3 4 -39 -0.3147 -0.0002 3 4 -37 -0.2457 0.0033 3 4 -35 2.0133 -0.0018 3 4 -33 -4.6541 -0.0019 3 4 -31 6.4187 0.0015 3 4 -29 -5.5717 0.0004 3 4 -27 2.2209 0.0017 3 4 -25 1.4675 -0.0040 3 4 -23 -3.6031 0.0007 3 4 -21 4.4758 0.0046 3 4 -19 -4.3930 -0.0042 3 4 -17 1.3629 -0.0001 3 4 -15 4.9803 0.0021 3 4 -13 -9.0188 -0.0020 3 4 -11 5.1645 0.0028 3 4 -9 2.8235 -0.0025 3 4 -7 -6.1230 -0.0020 3 4 -5 3.7138 0.0078 3 4 -3 -2.4925 -0.0098 3 4 -1 5.0545 0.0068 3 4 1 -6.5413 0.0000 3 4 3 4.0021 -0.0081 3 4 5 -0.3486 0.0114 3 4 7 -1.7702 -0.0053 3 4 9 3.0590 -0.0058 3 4 11 -4.1773 0.0119 3 4 13 4.4358 -0.0087 3 4 15 -3.5767 -0.0008 3 4 17 1.7654 0.0096 3 4 19 0.6387 -0.0098 3 4 21 -1.9519 0.0008 3 4 23 0.7492 0.0062 3 4 25 1.1258 -0.0018 3 4 27 -0.8792 -0.0051 3 4 29 -0.5595 0.0029 3 4 31 0.4754 0.0024 3 4 33 0.4093 -0.0003 3 4 35 0.5237 -0.0029 3 4 37 -2.4751 -0.0006 3 4 39 2.3544 0.0025 3 4 41 -0.1789 0.0038 3 4 43 -1.0616 -0.0063 3 4 45 0.3479 -0.0021 3 4 47 0.2786 0.0084 3 4 49 0.5175 -0.0031 3 4 51 -1.4909 -0.0031 3 5 -50 -1.4908 -0.0029 3 5 -48 0.3659 0.0065 3 5 -46 1.7639 -0.0025 3 5 -44 -2.2365 0.0004 3 5 -42 0.5889 -0.0006 3 5 -40 0.7248 -0.0007 3 5 -38 -0.4129 0.0019 3 5 -36 0.3418 0.0005 3 5 -34 -1.8570 -0.0038 3 5 -32 2.8765 0.0033 3 5 -30 -1.1019 0.0010 3 5 -28 -1.7790 -0.0040 3 5 -26 1.8353 0.0014 3 5 -24 1.5812 0.0035 3 5 -22 -4.0441 -0.0040 3 5 -20 0.9041 -0.0003 3 5 -18 6.1654 0.0011 3 5 -16 -9.3474 0.0035 3 5 -14 3.7360 -0.0052 3 5 -12 5.1507 0.0003 3 5 -10 -7.1062 0.0026 3 5 -8 0.3811 0.0011 3 5 -6 5.9577 -0.0015 3 5 -4 -4.0976 -0.0078 3 5 -2 -3.1380 0.0159 3 5 0 7.6229 -0.0097 3 5 2 -6.4646 -0.0060 3 5 4 3.3280 0.0154 3 5 6 -1.4350 -0.0120 3 5 8 -0.3425 0.0032 3 5 10 3.6690 0.0011 3 5 12 -6.2863 -0.0001 3 5 14 4.5275 0.0008 3 5 16 0.5328 -0.0061 3 5 18 -3.2691 0.0088 3 5 20 0.9458 -0.0029 3 5 22 2.6046 -0.0043 3 5 24 -2.7873 0.0040 3 5 26 0.3264 0.0001 3 5 28 1.1900 -0.0000 3 5 30 -0.7797 -0.0012 3 5 32 -0.0964 -0.0020 3 5 34 0.7272 0.0049 3 5 36 -1.0941 -0.0010 3 5 38 0.5060 -0.0043 3 5 40 1.0887 0.0033 3 5 42 -2.0428 0.0011 3 5 44 1.3063 -0.0018 3 5 46 -0.1474 -0.0003 3 5 48 -0.0191 0.0009 3 5 50 -0.2568 0.0009 3 6 -49 -0.7042 -0.0076 3 6 -47 0.6285 0.0070 3 6 -45 -1.0950 -0.0022 3 6 -43 0.9626 0.0015 3 6 -41 0.2104 -0.0023 3 6 -39 -1.4169 0.0002 3 6 -37 1.9490 0.0014 3 6 -35 -2.4542 0.0007 3 6 -33 3.6022 -0.0025 3 6 -31 -4.5145 0.0010 3 6 -29 3.3074 0.0007 3 6 -27 0.3096 -0.0000 3 6 -25 -3.4295 -0.0002 3 6 -23 2.8968 -0.0012 3 6 -21 -0.1742 0.0007 3 6 -19 0.0884 0.0020 3 6 -17 -3.5072 -0.0022 3 6 -15 5.3019 -0.0017 3 6 -13 -1.8327 0.0048 3 6 -9 5.3117 -0.0029 3 6 -7 -2.2930 0.0059 3 6 -5 -2.0439 -0.0019 3 6 -3 3.8568 -0.0054 3 6 -1 -1.9936 0.0064 3 6 1 -0.9606 0.0015 3 6 3 1.2259 -0.0085 3 6 5 1.0402 0.0059 3 6 7 -1.6279 0.0014 3 6 9 -0.9887 -0.0046 3 6 11 2.8926 0.0032 3 6 13 -1.1543 -0.0019 3 6 15 -1.5741 0.0010 3 6 17 1.7503 0.0007 3 6 19 0.0892 -0.0019 3 6 21 -1.6047 0.0022 3 6 23 2.0451 -0.0018 3 6 25 -1.5078 0.0001 3 6 27 0.1805 0.0012 3 6 29 0.6916 0.0002 3 6 31 -0.0318 -0.0020 3 6 33 -0.7868 0.0003 3 6 35 -0.3401 0.0024 3 6 37 2.6855 -0.0021 3 6 39 -3.4958 0.0008 3 6 41 1.8935 -0.0009 3 6 43 0.2891 0.0005 3 6 45 -1.2916 -0.0006 3 6 47 1.2496 0.0052 3 6 49 -1.1504 -0.0088 3 7 -48 -0.1424 -0.0044 3 7 -46 -1.2082 0.0036 3 7 -44 1.5448 -0.0003 3 7 -42 -0.4268 -0.0014 3 7 -40 -0.2605 -0.0003 3 7 -38 -0.4344 0.0017 3 7 -36 0.9758 -0.0003 3 7 -34 0.0748 -0.0003 3 7 -32 -1.9128 -0.0022 3 7 -30 2.7337 0.0031 3 7 -28 -1.8622 0.0011 3 7 -26 0.2991 -0.0038 3 7 -24 0.2827 0.0001 3 7 -22 0.5557 0.0035 3 7 -20 -1.0498 -0.0007 3 7 -18 -0.6771 -0.0029 3 7 -16 3.5931 0.0006 3 7 -14 -4.5308 0.0038 3 7 -12 2.1887 -0.0034 3 7 -10 1.2659 -0.0016 3 7 -8 -2.9431 0.0065 3 7 -6 2.3549 -0.0066 3 7 -4 -1.3510 0.0010 3 7 -2 1.5033 0.0050 3 7 0 -2.1706 -0.0052 3 7 2 1.6865 0.0014 3 7 4 -0.0292 -0.0003 3 7 6 -1.2402 0.0011 3 7 8 1.5571 0.0010 3 7 10 -1.6211 -0.0036 3 7 12 1.2043 0.0014 3 7 14 0.3260 0.0028 3 7 16 -1.4306 -0.0034 3 7 18 0.0013 0.0011 3 7 20 2.5098 0.0010 3 7 22 -2.5999 -0.0028 3 7 24 0.2961 0.0035 3 7 26 1.0400 -0.0007 3 7 28 -0.3829 -0.0030 3 7 30 0.0472 0.0022 3 7 32 -0.9286 0.0021 3 7 34 1.1712 -0.0041 3 7 36 -0.0615 0.0020 3 7 38 -0.7156 0.0005 3 7 40 0.3901 -0.0003 3 7 42 -0.2681 -0.0024 3 7 44 0.8506 0.0047 3 7 46 -0.7697 -0.0025 3 7 48 -0.5124 -0.0048 3 8 -45 0.6509 0.0029 3 8 -43 -0.0879 -0.0056 3 8 -41 -1.2646 0.0066 3 8 -39 2.5206 -0.0022 3 8 -37 -2.4922 -0.0024 3 8 -35 1.1941 0.0013 3 8 -33 -0.0935 0.0019 3 8 -31 0.3889 -0.0015 3 8 -29 -1.1598 -0.0006 3 8 -27 0.3483 0.0008 3 8 -25 2.0011 -0.0000 3 8 -23 -3.1872 0.0008 3 8 -21 1.7074 -0.0021 3 8 -19 0.2019 0.0015 3 8 -17 0.2873 0.0014 3 8 -15 -2.4320 -0.0033 3 8 -13 3.0050 0.0014 3 8 -11 -0.7546 0.0016 3 8 -9 -2.0288 -0.0010 3 8 -7 2.5074 -0.0021 3 8 -5 -0.8979 0.0017 3 8 -3 0.1746 0.0026 3 8 -1 -1.8691 -0.0050 3 8 1 3.5800 0.0032 3 8 3 -2.4317 -0.0008 3 8 5 -0.4013 -0.0002 3 8 7 1.5856 0.0016 3 8 9 -0.9401 -0.0028 3 8 11 1.1028 0.0020 3 8 13 -2.4642 -0.0007 3 8 15 2.5349 0.0011 3 8 17 -0.5096 -0.0014 3 8 19 -1.3221 -0.0006 3 8 21 1.3454 0.0034 3 8 23 -0.7017 -0.0034 3 8 25 0.8102 -0.0002 3 8 27 -1.2105 0.0042 3 8 29 0.8377 -0.0041 3 8 31 0.1302 -0.0004 3 8 33 -0.6974 0.0039 3 8 35 0.5815 -0.0024 3 8 37 -0.4463 -0.0001 3 8 39 0.7010 -0.0004 3 8 41 -0.8565 0.0001 3 8 45 -0.1166 -0.0040 3 9 -44 -1.0752 0.0080 3 9 -42 0.5247 -0.0008 3 9 -40 0.0600 -0.0026 3 9 -38 -0.4086 0.0006 3 9 -36 0.9643 0.0003 3 9 -34 -1.3862 0.0013 3 9 -32 1.1400 -0.0011 3 9 -30 -0.9990 -0.0006 3 9 -28 1.6559 0.0003 3 9 -26 -1.7668 0.0015 3 9 -24 -0.1324 -0.0014 3 9 -22 2.5883 -0.0005 3 9 -20 -2.6931 0.0017 3 9 -18 0.3577 -0.0015 3 9 -16 1.1932 0.0000 3 9 -14 0.1872 0.0024 3 9 -12 -2.3995 -0.0037 3 9 -10 1.8840 0.0026 3 9 -8 1.1847 -0.0008 3 9 -6 -2.8722 -0.0009 3 9 -4 1.1564 0.0030 3 9 -2 1.1110 -0.0036 3 9 0 -0.6218 -0.0003 3 9 2 -1.5206 0.0049 3 9 4 1.8891 -0.0029 3 9 6 0.0932 -0.0046 3 9 8 -1.7063 0.0080 3 9 10 0.8167 -0.0036 3 9 12 1.6407 -0.0024 3 9 14 -2.7814 0.0040 3 9 16 0.8383 -0.0022 3 9 18 2.5235 0.0005 3 9 20 -3.6579 -0.0004 3 9 22 1.5279 0.0008 3 9 24 0.8082 -0.0003 3 9 26 -0.7187 -0.0010 3 9 28 -0.3543 0.0011 3 9 30 -0.0077 0.0008 3 9 32 1.0176 -0.0022 3 9 34 -0.5972 0.0012 3 9 36 -0.6425 0.0007 3 9 38 0.6229 -0.0007 3 9 40 0.4536 -0.0013 3 9 42 -0.6748 0.0033 3 9 44 -0.1690 -0.0030 3 10 -41 0.3576 -0.0022 3 10 -39 -0.3680 0.0029 3 10 -37 0.6694 -0.0003 3 10 -35 -0.6103 -0.0014 3 10 -33 0.0003 0.0002 3 10 -31 0.4518 0.0011 3 10 -29 -0.2448 -0.0004 3 10 -27 -0.2251 -0.0008 3 10 -25 0.2809 -0.0000 3 10 -23 0.4347 0.0018 3 10 -21 -1.7754 -0.0009 3 10 -19 2.8187 -0.0030 3 10 -17 -2.4014 0.0043 3 10 -15 0.6748 0.0002 3 10 -13 0.7805 -0.0055 3 10 -11 -1.0578 0.0054 3 10 -9 0.9486 -0.0010 3 10 -7 -1.3024 -0.0029 3 10 -5 1.7636 0.0044 3 10 -3 -1.6903 -0.0037 3 10 -1 1.0987 0.0012 3 10 1 -0.4103 0.0010 3 10 3 0.1420 -0.0011 3 10 5 -0.5393 0.0006 3 10 7 0.8490 -0.0014 3 10 9 0.0945 0.0017 3 10 11 -1.8846 0.0002 3 10 13 2.5212 -0.0029 3 10 15 -1.1667 0.0036 3 10 17 -0.4974 -0.0016 3 10 19 0.5401 -0.0015 3 10 21 0.6929 0.0028 3 10 23 -1.1448 -0.0010 3 10 25 -0.2997 -0.0012 3 10 27 2.2431 0.0009 3 10 29 -2.2667 0.0002 3 10 31 0.1328 0.0001 3 10 33 1.5927 0.0004 3 10 35 -1.0294 -0.0029 3 10 37 -0.4155 0.0031 3 10 39 0.5236 0.0004 3 10 41 0.3611 -0.0016 3 11 -38 -0.0089 -0.0003 3 11 -36 0.4931 -0.0015 3 11 -34 0.7238 -0.0001 3 11 -32 -1.5100 0.0028 3 11 -30 0.3018 -0.0030 3 11 -28 1.1254 0.0005 3 11 -26 -0.5437 0.0019 3 11 -24 -1.0267 -0.0015 3 11 -22 0.9334 -0.0012 3 11 -20 0.9445 0.0026 3 11 -18 -2.1815 -0.0009 3 11 -16 1.5950 -0.0008 3 11 -14 -0.5793 -0.0004 3 11 -12 0.3521 0.0024 3 11 -10 -0.2077 -0.0014 3 11 -8 -0.5842 -0.0017 3 11 -6 1.1627 0.0028 3 11 -4 -0.6698 -0.0009 3 11 -2 -0.0762 -0.0010 3 11 0 -0.0824 0.0011 3 11 2 0.6937 -0.0008 3 11 4 -0.4451 0.0008 3 11 6 -0.6992 -0.0005 3 11 8 1.2857 -0.0001 3 11 10 -0.3110 0.0002 3 11 12 -1.3702 0.0001 3 11 14 2.0202 0.0005 3 11 16 -1.1758 -0.0015 3 11 18 0.1013 0.0018 3 11 20 0.1780 -0.0011 3 11 22 -0.3062 -0.0004 3 11 24 1.1411 0.0020 3 11 26 -1.8577 -0.0019 3 11 28 1.1278 -0.0010 3 11 30 0.3593 0.0035 3 11 32 -0.5719 -0.0025 3 11 34 -0.6520 -0.0003 3 11 36 1.1713 0.0008 3 11 38 0.1185 0.0000 3 12 -35 -0.2390 0.0027 3 12 -33 -0.0682 -0.0026 3 12 -31 0.1788 -0.0007 3 12 -29 0.5093 0.0030 3 12 -27 -1.4250 -0.0021 3 12 -25 1.1637 -0.0002 3 12 -23 0.2067 0.0011 3 12 -21 -0.6990 -0.0002 3 12 -19 -0.5381 -0.0005 3 12 -17 1.5398 0.0004 3 12 -15 -0.5309 -0.0011 3 12 -13 -1.1889 0.0026 3 12 -11 1.3258 -0.0019 3 12 -9 -0.1001 -0.0020 3 12 -7 -0.4070 0.0045 3 12 -5 -0.4612 -0.0028 3 12 -3 1.2509 -0.0002 3 12 -1 -0.8482 0.0008 3 12 1 0.0707 -0.0001 3 12 3 -0.2432 -0.0003 3 12 5 1.1014 0.0008 3 12 7 -1.1811 -0.0015 3 12 9 0.0207 -0.0001 3 12 11 1.2933 0.0036 3 12 13 -1.8602 -0.0044 3 12 15 1.8419 0.0002 3 12 17 -1.4335 0.0043 3 12 19 0.5280 -0.0037 3 12 21 0.4382 -0.0003 3 12 23 -0.9166 0.0022 3 12 25 1.3353 -0.0003 3 12 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2.4751 -0.0090 4 3 -1 5.1940 0.0123 4 3 1 -14.8143 -0.0090 4 3 3 16.1783 -0.0031 4 3 5 -7.6880 0.0123 4 3 7 -3.3753 -0.0071 4 3 9 9.4963 -0.0039 4 3 11 -8.8185 0.0084 4 3 13 4.7939 -0.0089 4 3 15 -1.8040 0.0093 4 3 17 0.7080 -0.0027 4 3 19 0.4788 -0.0091 4 3 21 -1.8609 0.0105 4 3 23 1.2530 -0.0006 4 3 25 1.0051 -0.0026 4 3 27 -1.5868 -0.0042 4 3 29 -0.2382 0.0049 4 3 31 1.3654 0.0018 4 3 33 -0.4240 -0.0015 4 3 35 -0.2358 -0.0042 4 3 37 -0.6513 0.0011 4 3 39 1.1321 0.0059 4 3 41 -0.1259 -0.0017 4 3 43 -0.4887 -0.0072 4 3 45 -0.4938 0.0037 4 3 47 1.2772 0.0070 4 3 49 -0.1760 -0.0075 4 3 51 -1.4979 -0.0004 4 4 -50 -1.2865 0.0052 4 4 -48 1.6305 0.0040 4 4 -46 -0.3457 -0.0041 4 4 -44 -1.2084 0.0008 4 4 -42 1.5529 0.0004 4 4 -40 -1.1011 -0.0020 4 4 -38 0.5994 0.0049 4 4 -36 0.7668 -0.0036 4 4 -34 -3.4465 -0.0027 4 4 -32 5.2059 0.0060 4 4 -30 -3.4682 -0.0011 4 4 -28 -0.7802 -0.0054 4 4 -26 3.6432 0.0045 4 4 -24 -2.6480 0.0013 4 4 -22 -0.6333 -0.0030 4 4 -20 2.0603 -0.0006 4 4 -18 0.7359 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-0.0007 4 5 -27 -4.1212 -0.0009 4 5 -25 0.3399 0.0009 4 5 -23 2.3129 0.0015 4 5 -21 -2.9672 -0.0020 4 5 -19 3.4522 -0.0005 4 5 -17 -4.1661 0.0016 4 5 -13 2.2392 0.0001 4 5 -11 -5.7081 -0.0020 4 5 -9 4.0774 0.0013 4 5 -7 0.7576 0.0026 4 5 -5 -4.2255 -0.0045 4 5 -3 4.4082 0.0018 4 5 -1 -2.2131 0.0012 4 5 1 -0.4323 -0.0014 4 5 3 1.1195 0.0015 4 5 5 0.9726 -0.0033 4 5 7 -3.0307 0.0037 4 5 9 1.8467 -0.0007 4 5 11 1.5051 -0.0033 4 5 13 -3.4711 0.0052 4 5 15 2.9718 -0.0047 4 5 17 -1.3895 0.0016 4 5 19 -0.2215 0.0017 4 5 21 1.0271 -0.0004 4 5 23 -0.0806 -0.0044 4 5 25 -1.5928 0.0040 4 5 27 1.4527 0.0029 4 5 29 0.4644 -0.0058 4 5 31 -1.2704 0.0009 4 5 33 0.1194 0.0024 4 5 35 0.3902 0.0008 4 5 37 1.1587 -0.0036 4 5 39 -2.6310 0.0028 4 5 41 1.9823 -0.0027 4 5 43 -0.2608 0.0026 4 5 45 -0.5378 0.0012 4 5 47 0.4064 -0.0035 4 5 49 -0.5602 -0.0008 4 6 -48 -0.6143 0.0012 4 6 -46 -1.2981 0.0017 4 6 -44 2.5442 -0.0017 4 6 -42 -1.3314 -0.0002 4 6 -40 -0.7014 0.0015 4 6 -38 0.8873 -0.0007 4 6 -36 0.5477 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-1.6470 -0.0025 4 7 -41 0.1074 0.0055 4 7 -39 2.1449 -0.0045 4 7 -37 -3.2793 0.0003 4 7 -35 2.8298 0.0012 4 7 -33 -1.9890 0.0014 4 7 -31 1.9071 -0.0035 4 7 -29 -2.0170 0.0026 4 7 -27 0.6679 -0.0009 4 7 -25 2.0822 -0.0003 4 7 -23 -3.5539 0.0016 4 7 -21 1.9682 -0.0029 4 7 -19 0.3727 0.0024 4 7 -17 0.0906 0.0004 4 7 -15 -2.9802 -0.0023 4 7 -13 4.2813 0.0005 4 7 -11 -1.6610 0.0027 4 7 -9 -2.5881 -0.0018 4 7 -7 4.2122 -0.0032 4 7 -5 -1.7516 0.0054 4 7 -3 -1.6667 -0.0010 4 7 -1 1.8638 -0.0043 4 7 1 1.0241 0.0041 4 7 3 -2.7204 0.0001 4 7 5 1.0963 -0.0023 4 7 7 0.9036 0.0009 4 7 9 -0.4390 0.0016 4 7 11 -0.7547 -0.0027 4 7 13 -0.1007 0.0009 4 7 15 2.0322 0.0029 4 7 17 -2.2339 -0.0045 4 7 19 0.4049 0.0018 4 7 21 1.5671 0.0022 4 7 23 -2.4593 -0.0032 4 7 25 2.1979 0.0013 4 7 27 -0.9842 0.0012 4 7 29 -0.5058 -0.0031 4 7 31 1.1471 0.0031 4 7 33 -0.6497 -0.0005 4 7 35 0.0779 -0.0019 4 7 37 -0.4672 0.0018 4 7 39 1.4549 -0.0016 4 7 41 -1.7872 0.0013 4 7 43 0.9733 0.0022 4 7 45 0.1036 -0.0054 4 7 47 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-5 -0.3803 0.0020 4 13 -3 -0.1361 0.0010 4 13 -1 0.6936 -0.0008 4 13 1 -0.6181 -0.0021 4 13 3 0.2409 0.0027 4 13 5 -0.1722 -0.0005 4 13 7 0.4854 -0.0006 4 13 9 -1.0283 -0.0000 4 13 11 1.5371 -0.0011 4 13 13 -1.0912 0.0037 4 13 15 -1.0390 -0.0036 4 13 17 3.4849 -0.0001 4 13 19 -3.6656 0.0026 4 13 21 1.3319 -0.0011 4 13 23 0.9454 -0.0013 4 13 25 -1.5626 0.0009 4 13 27 1.5764 0.0013 4 13 29 -1.8036 -0.0012 4 14 -24 1.8582 0.0004 4 14 -22 0.8690 0.0042 4 14 -20 -1.9506 -0.0035 4 14 -18 0.4885 -0.0005 4 14 -16 1.1525 0.0030 4 14 -14 -0.9684 -0.0038 4 14 -12 -0.5020 0.0031 4 14 -10 1.5609 -0.0000 4 14 -8 -1.2567 -0.0024 4 14 -6 -0.1867 0.0007 4 14 -4 1.7201 0.0027 4 14 -2 -2.1318 -0.0032 4 14 0 1.0769 0.0013 4 14 2 0.4330 0.0007 4 14 4 -1.0163 -0.0024 4 14 6 0.5106 0.0027 4 14 8 -0.1067 0.0002 4 14 10 0.5923 -0.0029 4 14 12 -1.1352 0.0006 4 14 14 0.6968 0.0039 4 14 16 0.0494 -0.0037 4 14 18 0.2143 -0.0007 4 14 20 -0.9293 0.0031 4 14 22 0.3196 -0.0025 4 14 24 1.4699 0.0018 4 15 -15 1.4981 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1.1734 -0.0078 5 5 -48 -1.6342 0.0054 5 5 -46 0.4339 -0.0006 5 5 -44 1.4296 -0.0026 5 5 -42 -1.8227 0.0019 5 5 -40 0.5879 0.0020 5 5 -38 0.3719 -0.0049 5 5 -36 -0.0620 0.0043 5 5 -34 -0.3835 -0.0012 5 5 -32 -0.2051 -0.0018 5 5 -30 1.1517 0.0028 5 5 -28 -0.9240 -0.0013 5 5 -26 -0.4636 -0.0007 5 5 -24 0.8828 0.0005 5 5 -22 1.1476 0.0014 5 5 -20 -3.3423 -0.0017 5 5 -18 1.5441 -0.0001 5 5 -16 4.1062 0.0012 5 5 -14 -7.6769 -0.0009 5 5 -12 4.6754 0.0005 5 5 -10 1.6043 0.0006 5 5 -8 -4.1292 -0.0039 5 5 -6 0.8588 0.0060 5 5 -4 3.5394 -0.0027 5 5 -2 -3.6708 -0.0039 5 5 0 -1.1250 0.0069 5 5 2 6.7142 -0.0040 5 5 4 -8.3880 -0.0005 5 5 6 5.3410 0.0013 5 5 8 -0.7881 0.0015 5 5 10 -2.2929 -0.0034 5 5 12 3.6380 0.0001 5 5 14 -3.5867 0.0058 5 5 16 1.7546 -0.0071 5 5 18 0.8251 0.0021 5 5 20 -1.5612 0.0024 5 5 22 -0.0443 -0.0010 5 5 24 1.5509 -0.0016 5 5 26 -1.4560 -0.0001 5 5 28 0.8646 0.0027 5 5 30 -0.6651 -0.0006 5 5 32 0.2646 -0.0026 5 5 34 0.3426 0.0007 5 5 36 -0.2492 0.0037 5 5 38 -0.2877 -0.0035 5 5 40 0.0581 -0.0003 5 5 42 0.7826 0.0014 5 5 44 -0.9166 0.0007 5 5 46 0.2015 -0.0009 5 5 48 0.2344 -0.0016 5 6 -47 -0.4303 0.0026 5 6 -45 1.1936 -0.0016 5 6 -43 -1.8653 0.0025 5 6 -41 1.1533 -0.0014 5 6 -39 0.4928 -0.0011 5 6 -37 -1.6843 0.0019 5 6 -35 2.0126 -0.0003 5 6 -33 -2.2678 0.0000 5 6 -31 3.1047 -0.0023 5 6 -29 -3.9089 0.0037 5 6 -27 3.1786 -0.0019 5 6 -25 -0.5575 0.0004 5 6 -23 -1.9367 -0.0012 5 6 -21 2.1860 0.0008 5 6 -19 -1.1136 0.0023 5 6 -17 1.3904 -0.0035 5 6 -15 -3.1615 0.0009 5 6 -13 3.6051 0.0007 5 6 -11 -1.0497 0.0011 5 6 -9 -2.6168 -0.0020 5 6 -7 4.0858 -0.0008 5 6 -5 -2.0150 0.0034 5 6 -3 -1.5957 -0.0024 5 6 -1 3.0968 0.0000 5 6 1 -1.1656 0.0008 5 6 3 -1.2820 -0.0003 5 6 5 0.8922 -0.0004 5 6 7 1.3449 0.0005 5 6 9 -1.8100 0.0013 5 6 11 -0.1968 -0.0046 5 6 13 1.9052 0.0050 5 6 15 -1.5253 0.0001 5 6 17 0.1191 -0.0055 5 6 19 0.6856 0.0050 5 6 21 -0.3219 -0.0011 5 6 23 -0.9961 0.0003 5 6 25 2.2605 -0.0015 5 6 27 -1.9940 0.0006 5 6 29 0.0576 0.0009 5 6 31 1.6585 0.0009 5 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-0.0112 12 1 9 0.0425 0.0080 12 1 11 -1.1087 0.0049 12 1 13 1.8454 -0.0069 12 1 15 -1.8012 -0.0015 12 1 17 0.8057 0.0029 12 1 19 0.4274 0.0029 12 1 21 -0.8540 -0.0028 12 1 23 0.3744 -0.0016 12 1 25 0.1088 0.0015 12 1 27 0.0483 -0.0004 12 1 29 -0.5360 0.0027 12 1 31 0.7418 -0.0026 12 1 33 -0.5747 -0.0010 12 1 35 0.3957 0.0006 12 1 37 -0.3582 0.0033 12 1 39 0.1654 -0.0029 12 2 -40 0.2244 -0.0089 12 2 -38 -0.2273 0.0090 12 2 -36 0.3726 -0.0024 12 2 -34 -0.6151 0.0042 12 2 -32 0.8812 -0.0075 12 2 -30 -0.7753 0.0004 12 2 -28 -0.2568 0.0083 12 2 -26 1.8674 -0.0061 12 2 -24 -2.5579 -0.0008 12 2 -22 1.5652 0.0013 12 2 -20 -0.2340 0.0016 12 2 -18 0.0343 -0.0010 12 2 -16 -0.2317 -0.0009 12 2 -14 -0.4977 -0.0000 12 2 -12 1.3613 0.0020 12 2 -10 -0.8526 -0.0023 12 2 -8 -0.3349 0.0009 12 2 -6 0.4650 0.0010 12 2 -4 0.3039 -0.0010 12 2 -2 -0.6585 -0.0008 12 2 0 0.6295 0.0006 12 2 2 -1.1208 0.0032 12 2 4 2.0004 -0.0068 12 2 6 -2.2627 0.0067 12 2 8 1.2045 -0.0032 12 2 10 1.0882 -0.0027 12 2 12 -3.3397 0.0078 12 2 14 3.5924 -0.0066 12 2 16 -1.5322 0.0008 12 2 18 -0.6477 0.0003 12 2 20 1.0498 0.0037 12 2 22 -0.2667 -0.0030 12 2 24 -0.3181 -0.0030 12 2 26 0.4015 0.0042 12 2 28 0.0072 0.0003 12 2 30 -0.9886 -0.0009 12 2 32 1.6586 -0.0032 12 2 34 -0.9040 0.0042 12 2 36 -0.5706 -0.0017 12 2 38 1.0226 0.0009 12 2 40 -0.3179 -0.0004 12 3 -39 0.0485 -0.0059 12 3 -37 -0.5403 0.0092 12 3 -35 0.8366 -0.0012 12 3 -33 -0.5380 -0.0039 12 3 -31 -0.3501 -0.0016 12 3 -29 1.1453 0.0056 12 3 -27 -1.0711 -0.0009 12 3 -25 0.2003 -0.0022 12 3 -23 0.5481 -0.0015 12 3 -21 -0.5494 0.0021 12 3 -19 0.2500 0.0030 12 3 -17 -0.5090 -0.0040 12 3 -15 1.3712 -0.0006 12 3 -13 -1.7734 0.0018 12 3 -11 0.6561 0.0005 12 3 -9 1.5298 0.0005 12 3 -7 -2.8681 -0.0029 12 3 -5 2.1242 0.0009 12 3 -3 -0.3136 0.0026 12 3 -1 -0.7667 -0.0023 12 3 1 0.8416 -0.0001 12 3 3 -0.8159 0.0012 12 3 5 0.9892 -0.0016 12 3 7 -0.9585 0.0011 12 3 9 0.5269 0.0017 12 3 11 0.3348 -0.0040 12 3 13 -1.5262 0.0031 12 3 15 2.2274 -0.0013 12 3 17 -1.5291 0.0011 12 3 19 -0.0069 -0.0001 12 3 21 0.8470 -0.0023 12 3 23 -0.6517 0.0036 12 3 25 0.4644 -0.0031 12 3 27 -0.7927 0.0025 12 3 29 0.9691 -0.0016 12 3 31 -0.4757 0.0002 12 3 33 -0.2275 -0.0003 12 3 35 0.3955 0.0011 12 3 37 0.0320 0.0013 12 3 39 -0.3665 -0.0040 12 4 -38 0.4757 -0.0119 12 4 -36 0.2203 0.0043 12 4 -34 -0.4154 0.0005 12 4 -32 0.2580 -0.0008 12 4 -30 -0.1147 0.0015 12 4 -28 0.3845 -0.0031 12 4 -26 -1.3651 0.0033 12 4 -24 2.4141 -0.0018 12 4 -22 -2.0555 0.0003 12 4 -20 -0.0618 0.0003 12 4 -18 2.1429 -0.0005 12 4 -16 -2.1882 0.0025 12 4 -14 0.3304 -0.0052 12 4 -12 1.5025 0.0038 12 4 -10 -1.7918 0.0026 12 4 -8 0.7945 -0.0069 12 4 -6 0.1505 0.0046 12 4 -4 -0.4453 -0.0005 12 4 -2 0.8807 -0.0002 12 4 0 -2.0264 -0.0002 12 4 2 2.8312 -0.0004 12 4 4 -2.0489 0.0014 12 4 6 0.2394 -0.0038 12 4 8 1.1878 0.0070 12 4 10 -1.9986 -0.0053 12 4 12 2.5004 -0.0020 12 4 14 -2.0786 0.0059 12 4 16 0.3618 -0.0028 12 4 18 1.2960 0.0002 12 4 20 -1.4486 -0.0013 12 4 22 0.6017 0.0008 12 4 24 -0.0981 0.0014 12 4 26 0.2385 -0.0000 12 4 28 -0.6570 -0.0022 12 4 30 1.0541 -0.0000 12 4 32 -0.7767 0.0026 12 4 34 -0.6299 -0.0012 12 4 36 2.0527 0.0018 12 4 38 -1.8578 -0.0064 12 5 -37 -1.0825 -0.0002 12 5 -35 1.0823 -0.0056 12 5 -33 -0.2596 0.0022 12 5 -31 -0.5303 0.0033 12 5 -29 0.2344 -0.0027 12 5 -27 0.7795 -0.0003 12 5 -25 -0.9947 -0.0015 12 5 -23 -0.3025 0.0042 12 5 -21 2.0557 -0.0016 12 5 -19 -2.5896 -0.0017 12 5 -17 1.4138 0.0002 12 5 -15 0.3132 0.0014 12 5 -13 -1.2007 0.0017 12 5 -11 1.1867 -0.0046 12 5 -9 -1.0619 0.0029 12 5 -7 0.8591 -0.0001 12 5 -5 -0.0108 -0.0003 12 5 -3 -1.0939 -0.0003 12 5 -1 1.3013 -0.0008 12 5 1 -0.4376 0.0039 12 5 3 -0.5347 -0.0063 12 5 5 0.8939 0.0041 12 5 7 -0.5372 0.0016 12 5 9 -0.3957 -0.0037 12 5 11 1.2309 0.0010 12 5 13 -0.9809 -0.0009 12 5 15 -0.3086 0.0051 12 5 17 1.4102 -0.0055 12 5 19 -1.4880 0.0004 12 5 21 0.7296 0.0027 12 5 23 0.4271 -0.0022 12 5 25 -1.3759 0.0025 12 5 27 1.1463 -0.0025 12 5 29 0.4317 -0.0001 12 5 31 -1.9189 -0.0004 12 5 33 1.8355 0.0062 12 5 35 -0.4291 -0.0067 12 5 37 -0.9456 -0.0031 12 6 -34 -0.6588 -0.0009 12 6 -32 0.4513 -0.0012 12 6 -30 0.5058 0.0012 12 6 -28 -0.9529 0.0018 12 6 -26 0.5647 -0.0037 12 6 -24 -0.1911 0.0012 12 6 -22 0.1759 0.0022 12 6 -20 0.0707 -0.0017 12 6 -18 -0.5870 -0.0006 12 6 -16 0.3636 -0.0002 12 6 -14 0.9192 0.0023 12 6 -12 -1.7631 -0.0012 12 6 -10 0.7389 -0.0019 12 6 -8 1.1436 0.0023 12 6 -6 -1.6181 0.0005 12 6 -4 0.5055 -0.0025 12 6 -2 0.1159 0.0013 12 6 0 0.6844 0.0021 12 6 2 -1.3505 -0.0042 12 6 4 0.6635 0.0016 12 6 6 0.3331 0.0034 12 6 8 -0.4299 -0.0045 12 6 10 0.2674 0.0012 12 6 12 -0.7995 0.0007 12 6 14 1.4104 0.0003 12 6 16 -1.0730 0.0001 12 6 18 0.0818 -0.0017 12 6 20 0.6601 0.0006 12 6 22 -0.9308 0.0012 12 6 24 0.7998 0.0004 12 6 26 -0.2007 -0.0017 12 6 28 -0.3533 -0.0019 12 6 30 0.0466 0.0043 12 6 32 0.6843 0.0010 12 6 34 -0.5028 -0.0064 12 7 -33 0.6572 0.0012 12 7 -31 0.6038 -0.0042 12 7 -29 -1.4705 0.0015 12 7 -27 0.9936 -0.0007 12 7 -25 0.0254 0.0039 12 7 -23 -0.2771 -0.0046 12 7 -21 -0.3537 0.0001 12 7 -19 0.7881 0.0033 12 7 -17 -0.2595 -0.0007 12 7 -15 -0.6197 -0.0027 12 7 -13 0.6902 0.0016 12 7 -11 0.0890 0.0015 12 7 -9 -0.6134 -0.0023 12 7 -7 0.3026 0.0014 12 7 -5 0.1685 -0.0013 12 7 -3 -0.0616 0.0011 12 7 -1 -0.3854 0.0003 12 7 1 0.4571 -0.0019 12 7 3 0.0755 0.0021 12 7 5 -0.6875 -0.0013 12 7 7 0.5808 0.0009 12 7 9 0.3907 -0.0014 12 7 11 -1.2839 0.0013 12 7 13 1.0710 0.0001 12 7 15 0.0686 -0.0016 12 7 17 -1.1319 0.0018 12 7 19 1.5299 -0.0020 12 7 21 -1.1394 0.0020 12 7 23 -0.0444 -0.0004 12 7 25 1.2504 -0.0013 12 7 27 -1.0329 -0.0006 12 7 29 -0.7045 0.0031 12 7 31 1.9740 0.0002 12 7 33 -1.2617 -0.0058 12 8 -30 -0.0612 -0.0061 12 8 -28 1.1597 -0.0005 12 8 -26 -1.2453 0.0034 12 8 -24 0.6530 -0.0004 12 8 -22 -0.3622 -0.0026 12 8 -20 0.4366 0.0012 12 8 -18 -0.0874 0.0010 12 8 -16 -0.7448 -0.0002 12 8 -14 1.0877 -0.0014 12 8 -12 -0.5783 0.0006 12 8 -10 0.0944 0.0005 12 8 -8 -0.2010 0.0003 12 8 -6 0.3483 -0.0008 12 8 -4 -0.1931 -0.0008 12 8 -2 0.2091 0.0031 12 8 0 -0.4125 -0.0043 12 8 2 0.0861 0.0032 12 8 4 0.6925 0.0008 12 8 6 -0.8867 -0.0042 12 8 8 0.3198 0.0036 12 8 10 -0.0212 -0.0019 12 8 12 0.3871 0.0030 12 8 14 -0.6203 -0.0032 12 8 16 0.3161 -0.0011 12 8 18 -0.0073 0.0047 12 8 20 -0.1186 -0.0027 12 8 22 0.4499 0.0007 12 8 24 -0.7062 -0.0025 12 8 26 0.1589 0.0017 12 8 28 0.6679 0.0032 12 8 30 -0.3550 -0.0029 12 9 -27 -0.2668 -0.0023 12 9 -25 1.0561 0.0016 12 9 -23 -1.4444 0.0001 12 9 -21 1.1049 0.0000 12 9 -19 -0.2101 -0.0011 12 9 -17 -0.6138 -0.0000 12 9 -15 0.7888 0.0030 12 9 -13 -0.3504 -0.0038 12 9 -11 -0.1498 0.0008 12 9 -9 0.3060 0.0031 12 9 -7 -0.1694 -0.0047 12 9 -5 -0.0203 0.0034 12 9 -3 0.0867 -0.0001 12 9 -1 -0.0532 -0.0025 12 9 1 0.2632 0.0012 12 9 3 -0.9226 0.0015 12 9 5 1.3285 0.0010 12 9 7 -0.4385 -0.0066 12 9 9 -1.3727 0.0053 12 9 11 2.2791 0.0030 12 9 13 -1.3869 -0.0061 12 9 15 -0.0999 0.0004 12 9 17 0.8462 0.0032 12 9 19 -1.0431 0.0010 12 9 21 1.1532 -0.0051 12 9 23 -0.6711 0.0040 12 9 25 -0.5274 -0.0033 12 9 27 1.1373 0.0042 12 10 -22 1.1739 0.0067 12 10 -20 -2.0853 -0.0044 12 10 -18 1.4864 -0.0007 12 10 -16 0.5960 0.0025 12 10 -14 -2.4286 0.0001 12 10 -12 2.4106 -0.0025 12 10 -10 -0.9802 0.0019 12 10 -8 -0.1950 0.0001 12 10 -6 0.4101 -0.0022 12 10 -4 -0.3165 0.0043 12 10 -2 0.5538 -0.0049 12 10 0 -0.9688 0.0024 12 10 2 1.0215 0.0003 12 10 4 -0.4011 0.0007 12 10 6 -0.5355 -0.0028 12 10 8 0.8407 0.0001 12 10 10 -0.0742 0.0060 12 10 12 -0.8047 -0.0080 12 10 14 0.5941 0.0037 12 10 16 0.3167 0.0014 12 10 18 -0.5477 -0.0033 12 10 20 -0.0360 0.0038 12 10 22 0.2732 -0.0046 12 11 -15 -0.2438 -0.0006 12 11 -13 -0.1224 0.0031 12 11 -11 0.0177 -0.0015 12 11 -9 0.6963 -0.0046 12 11 -7 -1.2395 0.0080 12 11 -5 1.1582 -0.0033 12 11 -3 -0.6405 -0.0043 12 11 -1 -0.0577 0.0045 12 11 1 0.5348 0.0031 12 11 3 -0.2288 -0.0061 12 11 5 -0.5509 -0.0028 12 11 7 0.5065 0.0128 12 11 9 0.7317 -0.0097 12 11 11 -1.7404 -0.0025 12 11 13 1.3804 0.0080 12 11 15 -0.3706 -0.0033 12 12 -2 0.4654 0.0055 12 12 0 0.2137 -0.0030 12 12 2 -0.7935 -0.0001 13 1 -36 0.6856 0.0009 13 1 -34 -1.1463 0.0009 13 1 -32 0.7857 -0.0111 13 1 -30 -0.1036 0.0101 13 1 -28 -0.8828 0.0039 13 1 -26 2.1661 -0.0093 13 1 -24 -2.6138 0.0004 13 1 -22 1.2934 0.0052 13 1 -20 0.4473 0.0000 13 1 -18 -0.5041 -0.0048 13 1 -16 -0.6012 0.0031 13 1 -14 0.4398 -0.0009 13 1 -12 1.2699 0.0007 13 1 -10 -2.1864 -0.0001 13 1 -8 1.1893 -0.0004 13 1 -6 0.1358 -0.0005 13 1 -4 -0.3793 0.0003 13 1 -2 0.1686 0.0007 13 1 0 -0.4578 0.0001 13 1 2 0.7820 -0.0008 13 1 4 0.0458 -0.0026 13 1 6 -2.1418 0.0063 13 1 8 3.7222 -0.0033 13 1 10 -2.6192 -0.0040 13 1 12 -0.7378 0.0059 13 1 14 3.1289 0.0003 13 1 16 -2.6053 -0.0057 13 1 18 0.9203 0.0026 13 1 20 -0.3330 0.0047 13 1 22 0.4641 -0.0062 13 1 24 -0.2464 0.0005 13 1 26 0.1916 0.0035 13 1 28 -0.6271 -0.0012 13 1 30 0.4129 -0.0025 13 1 32 0.7584 0.0026 13 1 34 -1.3682 -0.0009 13 1 36 0.6940 0.0003 13 2 -37 -0.2089 0.0037 13 2 -35 0.4181 -0.0065 13 2 -33 -0.2008 0.0011 13 2 -31 -0.4167 -0.0020 13 2 -29 0.8458 0.0073 13 2 -27 -0.4361 -0.0047 13 2 -25 -0.6402 -0.0018 13 2 -23 1.3453 0.0010 13 2 -21 -0.9059 0.0021 13 2 -19 -0.1676 0.0017 13 2 -17 0.5588 -0.0054 13 2 -15 0.3130 0.0009 13 2 -13 -1.5141 0.0034 13 2 -11 1.5583 -0.0001 13 2 -9 -0.0847 -0.0033 13 2 -7 -1.6730 0.0001 13 2 -5 2.2608 0.0032 13 2 -3 -1.5534 -0.0020 13 2 -1 0.5194 0.0005 13 2 1 0.1994 0.0000 13 2 3 -0.7482 -0.0022 13 2 5 1.3240 0.0029 13 2 7 -1.7515 0.0007 13 2 9 1.6759 -0.0024 13 2 11 -0.7488 -0.0015 13 2 13 -0.9498 0.0038 13 2 15 2.4272 -0.0005 13 2 17 -2.5143 -0.0015 13 2 19 1.3328 -0.0012 13 2 21 -0.1377 0.0025 13 2 23 -0.3587 -0.0001 13 2 25 0.5063 -0.0013 13 2 27 -0.6713 0.0004 13 2 29 0.7527 -0.0002 13 2 31 -0.6841 0.0004 13 2 33 0.5833 -0.0000 13 2 35 -0.4857 0.0007 13 2 37 0.3682 -0.0018 13 3 -36 -0.5780 0.0060 13 3 -34 0.3035 -0.0027 13 3 -32 -0.1100 0.0045 13 3 -30 0.3195 -0.0038 13 3 -28 -0.3977 -0.0018 13 3 -26 -0.6302 0.0053 13 3 -24 2.4212 -0.0036 13 3 -22 -3.1369 0.0011 13 3 -20 1.7751 -0.0012 13 3 -18 0.4259 0.0022 13 3 -16 -1.6461 -0.0016 13 3 -14 1.4602 -0.0016 13 3 -12 -0.5592 0.0047 13 3 -10 -0.3683 -0.0032 13 3 -8 0.8990 -0.0014 13 3 -6 -0.8712 0.0029 13 3 -4 0.4471 -0.0010 13 3 -2 0.2352 0.0013 13 3 0 -1.1901 -0.0041 13 3 2 2.1011 0.0044 13 3 4 -2.4254 -0.0016 13 3 6 2.0811 -0.0021 13 3 8 -1.1543 0.0061 13 3 10 -0.6291 -0.0078 13 3 12 2.8510 0.0039 13 3 14 -3.7280 0.0014 13 3 16 2.2457 -0.0017 13 3 18 0.0365 0.0001 13 3 20 -1.0641 -0.0022 13 3 22 0.8949 0.0036 13 3 24 -0.6380 -0.0005 13 3 26 0.4874 -0.0006 13 3 28 -0.3886 -0.0031 13 3 30 0.7936 0.0039 13 3 32 -1.3628 0.0007 13 3 34 0.8365 -0.0031 13 3 36 0.7424 0.0019 13 4 -35 0.3873 -0.0011 13 4 -33 -0.0041 0.0035 13 4 -31 -0.0637 0.0019 13 4 -29 -0.5731 -0.0054 13 4 -27 1.3457 0.0006 13 4 -25 -1.2516 0.0036 13 4 -23 0.1165 -0.0005 13 4 -21 1.2000 -0.0028 13 4 -19 -1.8532 0.0010 13 4 -17 1.7649 0.0004 13 4 -15 -1.3073 0.0012 13 4 -13 0.6684 -0.0009 13 4 -11 0.2483 -0.0017 13 4 -9 -1.2983 0.0023 13 4 -7 1.7256 -0.0017 13 4 -5 -0.8901 0.0025 13 4 -3 -0.6039 -0.0026 13 4 -1 1.3147 -0.0001 13 4 1 -0.6996 0.0034 13 4 3 -0.3611 -0.0050 13 4 5 0.8289 0.0051 13 4 7 -0.4614 -0.0027 13 4 9 -0.3444 -0.0012 13 4 11 0.8493 0.0028 13 4 13 -0.4387 -0.0021 13 4 15 -0.6003 0.0024 13 4 17 1.2937 -0.0035 13 4 19 -1.2040 0.0028 13 4 21 0.6226 -0.0015 13 4 23 0.2739 0.0009 13 4 25 -1.2768 0.0009 13 4 27 1.5556 -0.0028 13 4 29 -0.5823 0.0015 13 4 31 -0.7806 -0.0004 13 4 33 1.2864 0.0044 13 4 35 -0.8311 -0.0077 13 5 -32 -0.2888 0.0001 13 5 -30 0.8003 0.0009 13 5 -28 -0.7136 0.0002 13 5 -26 0.3781 -0.0028 13 5 -24 -0.5672 0.0032 13 5 -22 1.0069 -0.0005 13 5 -20 -0.6045 -0.0012 13 5 -18 -0.7284 -0.0003 13 5 -16 1.5399 0.0019 13 5 -14 -0.6601 -0.0003 13 5 -12 -1.0190 -0.0019 13 5 -10 1.4558 0.0010 13 5 -8 -0.1962 0.0012 13 5 -6 -0.8872 -0.0011 13 5 -4 0.3061 -0.0012 13 5 -2 0.7857 0.0026 13 5 0 -0.4257 -0.0011 13 5 2 -1.1287 -0.0026 13 5 4 2.0117 0.0053 13 5 6 -1.5488 -0.0034 13 5 8 0.5240 -0.0018 13 5 10 0.6063 0.0046 13 5 12 -1.7955 -0.0031 13 5 14 2.3219 0.0009 13 5 16 -1.4889 -0.0002 13 5 18 -0.0381 -0.0004 13 5 20 1.0341 0.0007 13 5 22 -1.2360 0.0005 13 5 24 0.9970 -0.0012 13 5 26 -0.4427 -0.0005 13 5 28 -0.0484 0.0008 13 5 30 -0.2068 0.0017 13 5 32 0.8579 -0.0015 13 6 -31 -0.2117 -0.0010 13 6 -29 -0.5287 0.0041 13 6 -27 0.3672 -0.0021 13 6 -25 0.1155 0.0010 13 6 -23 -0.0105 -0.0014 13 6 -21 -0.7295 -0.0002 13 6 -19 1.4187 0.0018 13 6 -17 -1.4609 0.0002 13 6 -15 0.8316 -0.0026 13 6 -13 0.0336 0.0013 13 6 -11 -0.7399 0.0007 13 6 -9 1.2046 -0.0003 13 6 -7 -1.3336 0.0004 13 6 -5 0.8373 -0.0021 13 6 -3 0.2510 0.0020 13 6 -1 -1.2495 0.0001 13 6 1 1.4164 -0.0007 13 6 3 -0.6467 -0.0001 13 6 5 -0.4778 -0.0006 13 6 7 1.0592 0.0020 13 6 9 -0.5368 -0.0023 13 6 11 -0.6497 0.0018 13 6 13 1.3658 -0.0011 13 6 15 -0.9794 -0.0001 13 6 17 -0.1604 0.0007 13 6 19 1.2900 -0.0011 13 6 21 -1.5962 0.0020 13 6 23 0.5300 -0.0016 13 6 25 1.2155 -0.0011 13 6 27 -1.7428 0.0008 13 6 29 0.1952 0.0042 13 7 -28 1.0231 0.0035 13 7 -26 -1.0105 0.0021 13 7 -24 0.1355 -0.0043 13 7 -22 0.5124 0.0017 13 7 -20 -0.4277 0.0008 13 7 -18 0.1683 -0.0011 13 7 -16 -0.1400 0.0007 13 7 -14 -0.1877 0.0001 13 7 -12 1.0237 -0.0016 13 7 -10 -1.2588 0.0007 13 7 -8 0.1189 0.0030 13 7 -6 1.1991 -0.0044 13 7 -4 -1.2318 0.0010 13 7 -2 0.5373 0.0022 13 7 0 -0.4498 -0.0030 13 7 2 0.6988 0.0037 13 7 4 -0.2608 -0.0035 13 7 6 -0.5192 0.0001 13 7 8 0.6428 0.0035 13 7 10 -0.3357 -0.0036 13 7 12 0.4509 0.0033 13 7 14 -0.8572 -0.0039 13 7 16 0.8679 0.0015 13 7 18 -0.4423 0.0028 13 7 20 -0.1261 -0.0026 13 7 22 0.7720 -0.0003 13 7 24 -1.1004 -0.0015 13 7 26 0.4579 0.0048 13 7 28 0.6832 -0.0011 13 8 -25 1.2366 0.0006 13 8 -23 -1.5009 -0.0013 13 8 -21 0.9258 0.0017 13 8 -19 0.2511 -0.0010 13 8 -17 -1.1479 -0.0013 13 8 -15 1.0890 0.0037 13 8 -13 -0.3258 -0.0044 13 8 -11 -0.3496 0.0036 13 8 -9 0.5426 -0.0020 13 8 -7 -0.4622 -0.0013 13 8 -5 0.3643 0.0051 13 8 -3 -0.2949 -0.0049 13 8 -1 0.2585 0.0004 13 8 1 -0.0932 0.0021 13 8 3 -0.5499 0.0004 13 8 5 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0.3383 -0.0071 13 10 5 -1.3394 0.0040 13 10 7 1.3890 0.0087 13 10 9 0.3833 -0.0143 13 10 11 -2.3655 0.0041 13 10 13 2.3725 0.0074 13 10 15 -0.7682 -0.0055 13 11 -6 0.1413 -0.0005 13 11 -4 -0.3749 -0.0034 13 11 -2 0.1280 0.0067 13 11 2 -0.8994 -0.0000 13 11 4 0.5916 -0.0007 13 11 6 0.1480 0.0059 14 0 -34 -1.4529 -0.0071 14 0 -32 0.9092 -0.0046 14 0 -30 0.0735 0.0120 14 0 -28 -1.0139 -0.0027 14 0 -26 2.1898 -0.0074 14 0 -24 -3.1797 0.0029 14 0 -22 2.7105 0.0047 14 0 -20 -0.7531 -0.0019 14 0 -18 -0.8754 -0.0037 14 0 -16 0.9020 0.0025 14 0 -14 -0.2100 0.0005 14 0 -12 0.2133 -0.0003 14 0 -10 -0.8513 0.0011 14 0 -8 1.1062 -0.0024 14 0 -6 -0.6358 -0.0008 14 0 -4 0.0716 0.0041 14 0 -2 -0.0067 -0.0008 14 0 0 0.1270 -0.0035 14 0 2 0.3298 0.0017 14 0 4 -1.0056 0.0006 14 0 6 0.2807 0.0021 14 0 8 2.0684 -0.0014 14 0 10 -3.4286 -0.0066 14 0 12 1.7977 0.0090 14 0 14 0.8302 0.0024 14 0 16 -1.4240 -0.0134 14 0 18 0.5488 0.0089 14 0 20 -0.6185 0.0035 14 0 22 1.4054 -0.0076 14 0 24 -1.1179 0.0018 14 0 26 0.1868 0.0036 14 0 28 -0.2128 -0.0033 14 0 30 0.7333 -0.0004 14 0 32 -0.3158 0.0038 14 0 34 -0.6476 -0.0051 14 1 -33 0.2060 0.0018 14 1 -31 -0.4340 -0.0035 14 1 -29 0.6674 0.0075 14 1 -27 -0.5362 -0.0070 14 1 -25 -0.1255 0.0015 14 1 -23 0.9392 0.0003 14 1 -21 -1.2204 0.0024 14 1 -19 0.6979 -0.0014 14 1 -17 0.0885 -0.0022 14 1 -15 -0.3364 0.0006 14 1 -13 -0.0907 0.0030 14 1 -11 0.5453 0.0002 14 1 -9 -0.4308 -0.0062 14 1 -7 -0.1422 0.0048 14 1 -5 0.6525 0.0014 14 1 -3 -0.8231 -0.0034 14 1 -1 0.7285 0.0021 14 1 1 -0.4762 -0.0017 14 1 3 0.0994 0.0001 14 1 5 0.3563 0.0024 14 1 7 -0.8660 -0.0004 14 1 9 1.3458 -0.0039 14 1 11 -1.4070 0.0017 14 1 13 0.6308 0.0048 14 1 15 0.6785 -0.0050 14 1 17 -1.5622 -0.0005 14 1 19 1.5087 0.0022 14 1 21 -0.9316 0.0002 14 1 23 0.3778 -0.0010 14 1 25 0.0555 0.0005 14 1 27 -0.3630 -0.0016 14 1 29 0.4184 0.0021 14 1 31 -0.3024 -0.0007 14 1 33 0.2730 0.0001 14 2 -32 -0.6169 0.0063 14 2 -30 0.1415 -0.0116 14 2 -28 -0.0231 0.0049 14 2 -26 -0.5305 0.0037 14 2 -24 1.8859 -0.0032 14 2 -22 -2.8565 -0.0011 14 2 -20 2.2393 0.0003 14 2 -18 -0.5691 0.0036 14 2 -16 -0.6777 -0.0052 14 2 -14 0.9236 0.0036 14 2 -12 -0.6652 0.0000 14 2 -10 0.3975 -0.0031 14 2 -8 -0.1398 0.0027 14 2 -6 -0.2064 -0.0005 14 2 -4 0.4567 0.0004 14 2 -2 -0.2148 -0.0010 14 2 0 -0.4949 -0.0014 14 2 2 0.9819 0.0040 14 2 4 -0.9665 -0.0027 14 2 6 1.2842 0.0001 14 2 8 -2.2277 -0.0001 14 2 10 2.1774 0.0010 14 2 12 0.0398 -0.0002 14 2 14 -2.5365 -0.0024 14 2 16 2.7393 0.0049 14 2 18 -1.2292 -0.0049 14 2 20 0.3543 0.0010 14 2 22 -0.3658 0.0024 14 2 24 -0.0107 -0.0011 14 2 26 0.5937 -0.0011 14 2 28 -0.4105 -0.0015 14 2 30 0.0019 0.0047 14 2 32 -0.3625 -0.0027 14 3 -31 0.1067 0.0032 14 3 -29 -0.7608 -0.0081 14 3 -27 1.4365 0.0041 14 3 -25 -1.2147 0.0048 14 3 -23 -0.0164 -0.0057 14 3 -21 1.2240 -0.0003 14 3 -19 -1.4234 0.0025 14 3 -17 0.8666 -0.0003 14 3 -15 -0.5241 0.0002 14 3 -13 0.6597 -0.0012 14 3 -11 -0.6076 -0.0001 14 3 -9 -0.0421 0.0012 14 3 -7 0.7235 -0.0008 14 3 -5 -0.6864 0.0018 14 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0.3546 -0.0003 14 4 22 -0.8542 0.0003 14 4 24 1.0337 -0.0011 14 4 26 -0.9540 0.0009 14 4 28 0.5272 0.0012 14 4 30 -0.4007 -0.0018 14 5 -29 0.3572 0.0054 14 5 -27 -0.9761 -0.0049 14 5 -25 1.3977 -0.0005 14 5 -23 -0.8046 0.0034 14 5 -21 -0.4292 -0.0028 14 5 -19 1.3926 0.0008 14 5 -17 -1.8251 0.0024 14 5 -15 1.9431 -0.0037 14 5 -13 -1.6160 0.0006 14 5 -11 0.5212 0.0021 14 5 -9 1.0336 0.0002 14 5 -7 -2.0498 -0.0017 14 5 -5 1.7680 -0.0021 14 5 -3 -0.4424 0.0045 14 5 -1 -0.9384 -0.0010 14 5 1 1.5456 -0.0015 14 5 3 -1.1890 -0.0006 14 5 5 0.2239 0.0012 14 5 7 0.6436 0.0020 14 5 9 -0.7638 -0.0038 14 5 11 0.1941 0.0019 14 5 13 0.3405 -0.0002 14 5 15 -0.3596 0.0004 14 5 17 -0.0132 -0.0009 14 5 19 0.5633 0.0005 14 5 21 -0.9750 0.0016 14 5 23 0.5343 -0.0033 14 5 25 0.8968 0.0012 14 5 27 -1.9244 0.0014 14 5 29 1.1425 0.0015 14 6 -26 -1.0837 -0.0006 14 6 -24 0.1122 -0.0022 14 6 -22 0.6346 0.0021 14 6 -20 -0.7750 -0.0007 14 6 -18 0.6761 0.0001 14 6 -16 -0.6123 -0.0004 14 6 -14 0.1753 0.0016 14 6 -12 0.8828 -0.0037 14 6 -10 -1.5987 0.0033 14 6 -8 0.8392 0.0016 14 6 -6 0.7139 -0.0055 14 6 -4 -1.2309 0.0033 14 6 -2 0.4356 0.0007 14 6 0 0.1662 -0.0008 14 6 2 0.1774 -0.0002 14 6 4 -0.6357 -0.0015 14 6 6 0.5772 0.0029 14 6 8 -0.2872 -0.0012 14 6 10 -0.1249 -0.0008 14 6 12 0.8353 0.0015 14 6 14 -1.4108 -0.0020 14 6 16 1.2240 0.0016 14 6 18 -0.4826 0.0006 14 6 20 -0.2405 -0.0012 14 6 22 0.8619 -0.0013 14 6 24 -1.2423 0.0016 14 6 26 0.7928 0.0021 14 7 -23 -1.3300 -0.0023 14 7 -21 1.3069 0.0060 14 7 -19 -0.2799 -0.0045 14 7 -17 -0.7432 -0.0016 14 7 -15 0.6574 0.0053 14 7 -13 0.2302 -0.0030 14 7 -11 -0.6819 0.0008 14 7 -9 0.2132 -0.0033 14 7 -7 0.4942 0.0042 14 7 -5 -0.7171 0.0010 14 7 -3 0.4155 -0.0052 14 7 -1 0.1632 0.0020 14 7 1 -0.7572 0.0021 14 7 3 0.8530 0.0003 14 7 5 -0.0869 -0.0039 14 7 7 -0.9024 0.0010 14 7 9 0.9469 0.0035 14 7 11 0.0979 -0.0016 14 7 13 -1.1665 -0.0033 14 7 15 1.4146 0.0019 14 7 17 -0.8845 0.0044 14 7 19 -0.1061 -0.0058 14 7 21 1.0911 0.0007 14 7 23 -1.2206 0.0021 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0.1595 0.0098 15 1 -26 -0.7816 0.0008 15 1 -24 1.9060 -0.0031 15 1 -22 -3.0529 -0.0021 15 1 -20 3.0267 0.0028 15 1 -18 -1.3817 0.0014 15 1 -16 -0.7950 -0.0033 15 1 -14 1.7394 0.0027 15 1 -12 -0.8678 -0.0023 15 1 -10 -0.4283 0.0008 15 1 -8 0.5280 0.0013 15 1 -6 0.2163 -0.0005 15 1 -4 -0.3165 -0.0012 15 1 -2 -0.1956 -0.0000 15 1 0 0.0096 0.0021 15 1 2 0.7237 -0.0018 15 1 4 -0.5739 0.0017 15 1 6 -0.1166 -0.0029 15 1 8 -0.4735 0.0003 15 1 10 1.9405 0.0073 15 1 12 -1.8103 -0.0111 15 1 14 -0.0556 0.0045 15 1 16 1.0281 0.0061 15 1 18 -0.3107 -0.0094 15 1 20 0.0025 0.0040 15 1 22 -0.9062 0.0013 15 1 24 1.2444 -0.0004 15 1 26 -0.2851 -0.0029 15 1 28 -0.4044 0.0025 15 2 -29 -0.6683 -0.0085 15 2 -27 1.3383 0.0080 15 2 -25 -1.5240 0.0004 15 2 -23 0.5839 -0.0055 15 2 -21 1.0559 0.0020 15 2 -19 -2.0465 0.0020 15 2 -17 1.6191 -0.0017 15 2 -15 -0.4644 0.0010 15 2 -13 -0.3084 -0.0013 15 2 -11 0.4719 -0.0006 15 2 -9 -0.4057 0.0033 15 2 -7 0.2099 -0.0025 15 2 -5 0.1550 0.0003 15 2 -3 -0.3576 -0.0007 15 2 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0.0014 15 3 28 0.9128 0.0004 15 4 -25 2.0417 0.0001 15 4 -23 -1.7567 0.0071 15 4 -21 0.2778 -0.0069 15 4 -19 1.0590 0.0019 15 4 -17 -1.3938 0.0035 15 4 -15 1.2291 -0.0058 15 4 -13 -1.1481 0.0021 15 4 -11 0.8222 0.0028 15 4 -9 0.0520 -0.0011 15 4 -7 -0.8397 -0.0031 15 4 -5 0.8103 0.0006 15 4 -1 -0.3256 -0.0041 15 4 1 0.5958 -0.0007 15 4 3 -0.7522 0.0005 15 4 5 0.6298 0.0022 15 4 7 -0.1886 0.0000 15 4 9 -0.0537 -0.0041 15 4 11 -0.1559 0.0031 15 4 13 0.1898 0.0007 15 4 15 0.4100 -0.0012 15 4 17 -1.0436 -0.0020 15 4 19 1.0559 0.0040 15 4 21 -0.6842 -0.0015 15 4 23 0.2347 -0.0035 15 4 25 0.5046 0.0048 15 5 -24 0.2403 -0.0015 15 5 -22 0.2857 -0.0021 15 5 -20 -0.0656 0.0038 15 5 -18 -0.2169 -0.0010 15 5 -16 0.0764 -0.0023 15 5 -14 0.1007 0.0033 15 5 -12 0.1834 -0.0034 15 5 -10 -0.4931 0.0034 15 5 -8 -0.0093 -0.0014 15 5 -6 1.0004 -0.0017 15 5 -4 -1.1402 0.0024 15 5 -2 0.1106 -0.0004 15 5 0 0.8108 -0.0003 15 5 2 -0.6636 -0.0019 15 5 4 -0.1047 0.0034 15 5 6 0.8066 -0.0011 15 5 8 -1.2282 -0.0025 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0.6079 -0.0003 15 7 12 -0.6217 -0.0008 15 7 14 0.6763 0.0020 15 7 16 -0.4939 -0.0026 15 7 18 0.2881 0.0009 15 8 -13 1.0114 0.0051 15 8 -11 0.0180 -0.0004 15 8 -9 -0.1381 0.0012 15 8 -7 -0.2185 -0.0055 15 8 -5 0.0505 0.0035 15 8 -3 0.4052 0.0036 15 8 -1 -0.4347 -0.0048 15 8 1 0.2329 -0.0011 15 8 3 -0.1916 0.0032 15 8 5 -0.0817 0.0014 15 8 7 0.7690 -0.0025 15 8 9 -1.0055 -0.0026 15 8 11 0.2239 0.0030 15 8 13 0.7647 0.0043 16 0 -22 -2.4536 -0.0006 16 0 -20 3.8154 0.0020 16 0 -18 -3.4244 0.0012 16 0 -16 0.6519 -0.0011 16 0 -14 2.4111 -0.0017 16 0 -12 -2.5950 0.0006 16 0 -10 -0.0011 0.0023 16 0 -8 1.7271 -0.0011 16 0 -6 -0.6874 -0.0008 16 0 -4 -0.6716 -0.0013 16 0 -2 0.0854 0.0032 16 0 0 0.8427 -0.0004 16 0 2 -0.0833 -0.0032 16 0 4 -1.0353 0.0038 16 0 6 0.6375 -0.0042 16 0 8 0.1248 0.0042 16 0 10 0.4004 0.0016 16 0 12 -1.0555 -0.0107 16 0 14 0.3464 0.0110 16 0 16 0.4469 0.0001 16 0 18 0.2191 -0.0089 16 0 20 -1.0630 0.0055 16 0 22 0.3686 0.0021 16 0 24 0.8634 -0.0029 16 1 -21 -0.2835 0.0014 16 1 -19 -1.0889 -0.0008 16 1 -17 1.7777 -0.0001 16 1 -15 -1.3400 0.0019 16 1 -13 0.3257 -0.0038 16 1 -11 0.5481 0.0022 16 1 -9 -0.9475 0.0026 16 1 -7 0.7618 -0.0048 16 1 -5 -0.1259 0.0023 16 1 -3 -0.4011 -0.0003 16 1 -1 0.3351 0.0012 16 1 1 0.0709 -0.0006 16 1 3 -0.2381 -0.0030 16 1 5 0.1605 0.0037 16 1 7 -0.1935 -0.0009 16 1 9 0.1652 0.0012 16 1 11 0.3833 -0.0044 16 1 13 -1.1401 0.0019 16 1 15 1.1952 0.0059 16 1 17 -0.3718 -0.0071 16 1 19 -0.5082 -0.0008 16 1 21 0.8023 0.0065 16 1 23 -0.6695 -0.0037 16 2 -22 0.5373 0.0006 16 2 -20 -1.8113 -0.0059 16 2 -18 2.4363 0.0036 16 2 -16 -1.2292 0.0021 16 2 -14 -0.6520 -0.0047 16 2 -12 0.8136 0.0037 16 2 -10 0.7622 -0.0010 16 2 -8 -1.4275 -0.0005 16 2 -6 0.0561 -0.0007 16 2 -4 1.1193 0.0009 16 2 -2 -0.3387 0.0018 16 2 0 -0.8248 -0.0033 16 2 2 0.4646 0.0013 16 2 4 0.5363 -0.0013 16 2 6 -0.7301 0.0042 16 2 8 0.8206 -0.0027 16 2 10 -1.6278 -0.0046 16 2 12 1.8322 0.0086 16 2 14 -0.3629 -0.0056 16 2 16 -1.2242 0.0014 16 2 18 1.2052 0.0004 16 2 20 -0.4281 -0.0018 16 2 22 0.4127 0.0031 16 3 -21 1.1723 -0.0077 16 3 -19 0.8620 0.0041 16 3 -17 -1.9789 0.0015 16 3 -15 1.5635 -0.0051 16 3 -13 -0.5039 0.0034 16 3 -11 -0.4098 0.0020 16 3 -9 0.9940 -0.0034 16 3 -7 -0.9363 -0.0010 16 3 -5 0.0773 0.0030 16 3 -3 0.7647 0.0011 16 3 -1 -0.6540 -0.0037 16 3 1 0.0214 0.0007 16 3 3 0.0250 0.0016 16 3 5 0.4536 0.0007 16 3 7 -0.5281 -0.0022 16 3 9 0.2263 -0.0011 16 3 11 -0.3877 0.0035 16 3 13 0.8410 -0.0004 16 3 15 -0.5042 -0.0036 16 3 17 -0.6307 0.0015 16 3 19 1.3094 0.0049 16 3 21 -0.9554 -0.0069 16 4 -18 -0.6147 -0.0053 16 4 -16 1.0101 -0.0022 16 4 -14 -0.8554 0.0056 16 4 -12 0.9054 -0.0032 16 4 -10 -1.0391 -0.0001 16 4 -8 0.2628 0.0007 16 4 -6 1.2852 0.0004 16 4 -4 -1.9198 -0.0005 16 4 -2 0.8331 -0.0004 16 4 0 0.5980 0.0000 16 4 4 0.3758 0.0023 16 4 6 0.2399 -0.0050 16 4 8 -0.9680 0.0021 16 4 10 1.5735 0.0035 16 4 12 -1.0683 -0.0038 16 4 14 -0.5324 0.0000 16 4 16 1.6396 -0.0001 16 4 18 -1.2922 0.0036 16 4 20 0.3966 -0.0036 16 5 -15 0.1079 0.0082 16 5 -13 0.4743 -0.0070 16 5 -11 -1.2961 -0.0028 16 5 -9 1.2653 0.0058 16 5 -7 -0.4377 0.0013 16 5 -5 -0.2912 -0.0043 16 5 -3 0.6859 -0.0008 16 5 -1 -1.0172 0.0021 16 5 1 0.9525 0.0024 16 5 3 -0.0130 -0.0015 16 5 5 -1.1919 -0.0053 16 5 11 0.1085 -0.0040 16 5 13 0.2233 -0.0006 16 5 15 -0.4129 0.0037 16 5 17 0.5591 -0.0009 16 6 -10 0.2704 -0.0050 16 6 -8 -0.2692 0.0052 16 6 -6 0.0977 0.0024 16 6 -4 0.0064 -0.0070 16 6 -2 -0.0145 0.0010 16 6 0 0.2466 0.0068 16 6 2 -0.6626 -0.0058 16 6 4 0.7212 -0.0007 16 6 6 -0.3758 0.0044 16 6 8 0.1990 -0.0037 16 7 -7 0.2677 -0.0006 16 7 -5 0.3397 0.0042 16 7 -3 -0.5330 -0.0000 16 7 -1 0.6400 -0.0029 16 7 1 -0.5525 -0.0012 16 7 3 -0.0885 0.0038 16 7 5 0.8298 0.0003 16 7 7 -0.8445 -0.0032 17 1 -16 -2.4546 -0.0018 17 1 -14 -0.5656 0.0002 17 1 -12 2.4866 0.0008 17 1 -10 -0.8254 -0.0017 17 1 -8 -1.8089 0.0015 17 1 -6 1.5413 -0.0012 17 1 -4 0.6791 0.0017 17 1 -2 -1.0245 -0.0012 17 1 0 -0.7508 -0.0005 17 1 2 1.4625 0.0010 17 1 4 -0.1808 -0.0009 17 1 6 -0.8647 0.0033 17 1 8 0.6937 -0.0056 17 1 10 -0.6242 0.0029 17 1 12 0.9629 0.0029 17 1 14 -0.4750 -0.0058 17 1 16 -0.6909 0.0044 17 2 -15 2.5270 -0.0011 17 2 -13 -1.7319 0.0025 17 2 -11 0.1789 -0.0003 17 2 -9 1.2676 -0.0025 17 2 -7 -1.8202 0.0018 17 2 -5 1.0464 0.0007 17 2 -3 0.2788 -0.0008 17 2 -1 -0.7246 -0.0013 17 2 1 0.1272 0.0014 17 2 3 0.2324 0.0012 17 2 5 0.2245 -0.0017 17 2 7 -0.5124 -0.0010 17 2 9 0.0001 0.0016 17 2 11 0.3602 0.0024 17 2 13 0.2720 -0.0040 17 2 15 -1.0564 -0.0018 17 3 -14 -0.5002 0.0051 17 3 -12 0.4920 -0.0045 17 3 -10 -1.5538 -0.0005 17 3 -8 2.1299 0.0034 17 3 -6 -0.6474 -0.0012 17 3 -4 -1.4728 -0.0017 17 3 -2 1.7062 0.0005 17 3 0 -0.2250 0.0013 17 3 2 -0.7770 0.0008 17 3 4 0.5795 -0.0017 17 3 6 -0.1516 -0.0026 17 3 8 -0.2493 0.0052 17 3 10 1.0688 -0.0010 17 3 12 -1.6749 -0.0022 17 3 14 0.9990 -0.0003 17 4 -11 -0.0313 0.0005 17 4 -9 -0.2255 0.0050 17 4 -7 0.3897 -0.0010 17 4 -5 0.0594 -0.0036 17 4 -3 -0.6885 0.0008 17 4 -1 0.3695 0.0024 17 4 1 0.7193 0.0007 17 4 3 -0.9846 -0.0023 17 4 5 -0.1543 -0.0027 17 4 7 1.3115 0.0058 17 4 9 -1.2703 -0.0008 17 4 11 0.5860 -0.0043 17 5 -4 1.0478 -0.0025 17 5 -2 -0.7317 0.0008 17 5 0 0.1544 0.0038 17 5 2 -0.0548 -0.0064 17 5 4 0.1509 0.0032 0 0 0 0.0 0.0 ; _shelx_fab_checksum 27048 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.042 _oxdiff_exptl_absorpt_empirical_full_min 0.506 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.0200(3) 0.6025(3) 0.70889(7) 0.0628(10) Uani 1 1 d . . . . . N2 N 0.1467(4) 0.1137(3) 0.62422(9) 0.0790(14) Uani 1 1 d . . . . . N3 N 0.22787(19) 0.3564(2) 0.53418(6) 0.0339(7) Uani 1 1 d . . . . . N4 N 0.20298(19) 0.6994(2) 0.52575(6) 0.0357(7) Uani 1 1 d . . . . . C1 C 0.0458(3) 0.3521(3) 0.69477(8) 0.0477(9) Uani 1 1 d . . . . . C2 C 0.0131(3) 0.3444(4) 0.72342(9) 0.0575(11) Uani 1 1 d . . . . . H2 H -0.002396 0.402264 0.733735 0.069 Uiso 1 1 calc R U . . . C3 C 0.0035(4) 0.2552(4) 0.73633(9) 0.0678(13) Uani 1 1 d . . . . . H3 H -0.019131 0.251079 0.755470 0.081 Uiso 1 1 calc R U . . . C4 C 0.0271(4) 0.1691(4) 0.72142(10) 0.0746(16) Uani 1 1 d . . . . . H4 H 0.021236 0.107136 0.730699 0.089 Uiso 1 1 calc R U . . . C5 C 0.0582(4) 0.1737(4) 0.69374(9) 0.0662(14) Uani 1 1 d . . . . . H5 H 0.073070 0.114761 0.683822 0.079 Uiso 1 1 calc R U . . . C6 C 0.0686(3) 0.2647(3) 0.67977(8) 0.0506(10) Uani 1 1 d . . . . . C7 C 0.1019(3) 0.2717(3) 0.65064(8) 0.0472(9) Uani 1 1 d . . . . . C8 C 0.1095(2) 0.3617(3) 0.63709(8) 0.0398(8) Uani 1 1 d . . . . . C9 C 0.0842(2) 0.4500(3) 0.65208(7) 0.0394(8) Uani 1 1 d . . . . . C10 C 0.0542(3) 0.4448(3) 0.68043(8) 0.0429(9) Uani 1 1 d . . . . . C11 C 0.0347(3) 0.5324(3) 0.69602(8) 0.0483(10) Uani 1 1 d . . . . . C12 C 0.0961(2) 0.5330(3) 0.63248(7) 0.0381(8) Uani 1 1 d . . . . . C13 C 0.0799(3) 0.6318(3) 0.63445(8) 0.0456(9) Uani 1 1 d . . . . . H13 H 0.058397 0.660176 0.651868 0.055 Uiso 1 1 calc R U . . . C14 C 0.0961(3) 0.6897(3) 0.61004(8) 0.0466(10) Uani 1 1 d . . . . . H14 H 0.084164 0.758173 0.611128 0.056 Uiso 1 1 calc R U . . . C15 C 0.1285(3) 0.6521(3) 0.58446(8) 0.0412(9) Uani 1 1 d . . . . . H15 H 0.138286 0.694682 0.568496 0.049 Uiso 1 1 calc R U . . . C16 C 0.1473(2) 0.5505(3) 0.58174(7) 0.0351(8) Uani 1 1 d . . . . . C17 C 0.1291(2) 0.4935(3) 0.60623(7) 0.0371(8) Uani 1 1 d . . . . . C18 C 0.1401(2) 0.3905(3) 0.60807(7) 0.0375(8) Uani 1 1 d . . . . . C19 C 0.1733(2) 0.3395(3) 0.58497(7) 0.0383(8) Uani 1 1 d . . . . . H19 H 0.182080 0.270408 0.585662 0.046 Uiso 1 1 calc R U . . . C20 C 0.1939(2) 0.3952(3) 0.55996(7) 0.0352(8) Uani 1 1 d . . . . . C21 C 0.1828(2) 0.4974(3) 0.55717(7) 0.0337(8) Uani 1 1 d . . . . . C22 C 0.2128(2) 0.5220(3) 0.52847(7) 0.0331(7) Uani 1 1 d . . . . . C23 C 0.2367(2) 0.4332(3) 0.51489(7) 0.0318(7) Uani 1 1 d . . . . . C24 C 0.2283(2) 0.6136(3) 0.51378(7) 0.0330(7) Uani 1 1 d . . . . . C25 C 0.2236(2) 0.7835(3) 0.51263(7) 0.0366(8) Uani 1 1 d . . . . . C26 C 0.1872(3) 0.8741(3) 0.52581(8) 0.0402(8) Uani 1 1 d . . . . . C27 C 0.1417(3) 0.9425(3) 0.50909(9) 0.0444(9) Uani 1 1 d . . . . . H27 H 0.135907 0.932836 0.488804 0.053 Uiso 1 1 calc R U . . . C28 C 0.1045(3) 1.0254(3) 0.52205(10) 0.0562(10) Uani 1 1 d . . . . . H28 H 0.073200 1.071628 0.510478 0.067 Uiso 1 1 calc R U . . . C29 C 0.1122(3) 1.0409(3) 0.55097(10) 0.0622(11) Uani 1 1 d D . . . . H29 H 0.086127 1.097646 0.559401 0.075 Uiso 1 1 calc R U . . . C30 C 0.1593(3) 0.9728(3) 0.56888(10) 0.0598(11) Uani 1 1 d D . . . . H30 H 0.165620 0.983784 0.589086 0.072 Uiso 1 1 calc R U . . . C31 C 0.1963(3) 0.8883(3) 0.55548(9) 0.0483(10) Uani 1 1 d D . . . . H31 H 0.227337 0.841241 0.566834 0.058 Uiso 1 1 calc R U . . . C32 C 0.1267(3) 0.1833(3) 0.63604(8) 0.0547(11) Uani 1 1 d . . . . . C33 C 0.2837(2) 0.2673(3) 0.53499(7) 0.0382(8) Uani 1 1 d . . . . . H33A H 0.293591 0.244355 0.514911 0.046 Uiso 1 1 calc R U . . . H33B H 0.251194 0.214859 0.545389 0.046 Uiso 1 1 calc R U . . . C34 C 0.3748(3) 0.2825(3) 0.54979(8) 0.0485(9) Uani 1 1 d . . . . . H34 H 0.363955 0.321088 0.567872 0.058 Uiso 1 1 calc R U . . . C35 C 0.4370(3) 0.3433(3) 0.53097(10) 0.0524(10) Uani 1 1 d . . . . . H35A H 0.405673 0.404212 0.525228 0.063 Uiso 1 1 calc R U . . . H35B H 0.488777 0.362811 0.542879 0.063 Uiso 1 1 calc R U . . . C36 C 0.4707(3) 0.2938(3) 0.50396(9) 0.0489(9) Uani 1 1 d . . . . . H36A H 0.421075 0.258672 0.494426 0.059 Uiso 1 1 calc R U . . . H36B H 0.516178 0.244494 0.509353 0.059 Uiso 1 1 calc R U . . . C37 C 0.5105(3) 0.3661(3) 0.48291(10) 0.0551(10) Uani 1 1 d . . . . . H37A H 0.558980 0.401969 0.492816 0.066 Uiso 1 1 calc R U . . . H37B H 0.464426 0.414845 0.477613 0.066 Uiso 1 1 calc R U . . . C38 C 0.5469(3) 0.3215(4) 0.45542(11) 0.0609(11) Uani 1 1 d . . . . . H38A H 0.500700 0.280089 0.446265 0.073 Uiso 1 1 calc R U . . . H38B H 0.598042 0.278714 0.460244 0.073 Uiso 1 1 calc R U . . . C39 C 0.5767(3) 0.4008(5) 0.43401(12) 0.0744(14) Uani 1 1 d . . . . . H39A H 0.525694 0.444809 0.430158 0.089 Uiso 1 1 calc R U . . . H39B H 0.623621 0.440670 0.443337 0.089 Uiso 1 1 calc R U . . . C40 C 0.6109(4) 0.3644(6) 0.40586(14) 0.0948(18) Uani 1 1 d . . . . . H40A H 0.565426 0.321653 0.396823 0.114 Uiso 1 1 calc R U . . . H40B H 0.664322 0.323780 0.409426 0.114 Uiso 1 1 calc R U . . . C41 C 0.6348(4) 0.4471(7) 0.38462(14) 0.119(2) Uani 1 1 d . . . . . H41A H 0.582405 0.490251 0.382135 0.143 Uiso 1 1 calc R U . . . H41B H 0.682934 0.487205 0.393188 0.143 Uiso 1 1 calc R U . . . C42 C 0.6631(6) 0.4128(10) 0.35624(18) 0.167(3) Uani 1 1 d . . . . . H42A H 0.613230 0.373277 0.348501 0.200 Uiso 0.5 1 calc R U P A 1 H42B H 0.712312 0.366084 0.359834 0.200 Uiso 0.5 1 calc R U P A 1 H42C H 0.617909 0.368481 0.347733 0.200 Uiso 0.5 1 calc R U P B 2 H42D H 0.719922 0.376570 0.357777 0.200 Uiso 0.5 1 calc R U P B 2 C43 C 0.6925(14) 0.476(3) 0.3323(5) 0.203(5) Uani 0.5 1 d D . P C 1 H43A H 0.744134 0.515515 0.338687 0.243 Uiso 0.5 1 calc R U P C 1 H43B H 0.644125 0.522114 0.327097 0.243 Uiso 0.5 1 calc R U P C 1 C44 C 0.719(3) 0.416(3) 0.3052(5) 0.300(5) Uani 0.5 1 d D U P C 1 H44A H 0.768797 0.374497 0.311721 0.360 Uiso 0.5 1 calc R U P C 1 H44B H 0.668296 0.370353 0.302147 0.360 Uiso 0.5 1 calc R U P C 1 C45 C 0.745(2) 0.449(3) 0.2749(5) 0.300(5) Uani 0.5 1 d D U P C 1 H45A H 0.795850 0.493179 0.277781 0.360 Uiso 0.5 1 calc R U P C 1 H45B H 0.695045 0.491427 0.268404 0.360 Uiso 0.5 1 calc R U P C 1 C46 C 0.769(2) 0.387(3) 0.2479(6) 0.300(5) Uani 0.5 1 d D U P C 1 H46A H 0.719541 0.388691 0.234048 0.450 Uiso 0.5 1 calc R U P C 1 H46B H 0.780133 0.318913 0.253765 0.450 Uiso 0.5 1 calc R U P C 1 H46C H 0.822180 0.414300 0.238859 0.450 Uiso 0.5 1 calc R U P C 1 C47 C 0.4135(3) 0.1835(4) 0.55897(10) 0.0595(11) Uani 1 1 d . . . . . H47A H 0.403665 0.135607 0.543157 0.071 Uiso 1 1 calc R U . . . H47B H 0.478462 0.191011 0.561487 0.071 Uiso 1 1 calc R U . . . C48 C 0.3752(6) 0.1419(8) 0.5866(2) 0.1514(6) Uani 1 1 d . . . . . H48A H 0.310097 0.136117 0.584220 0.182 Uiso 1 1 calc R U . . . H48B H 0.386486 0.189090 0.602468 0.182 Uiso 1 1 calc R U . . . C49 C 0.4122(6) 0.0416(8) 0.5954(2) 0.1514(6) Uani 1 1 d . . . . . H49A H 0.399470 -0.006649 0.579901 0.182 Uiso 1 1 calc R U . . . H49B H 0.477408 0.046433 0.597567 0.182 Uiso 1 1 calc R U . . . C50 C 0.3725(6) 0.0055(7) 0.6235(2) 0.1514(6) Uani 1 1 d D U . . . H50A H 0.308945 0.023463 0.624653 0.182 Uiso 0.5 1 calc R U P D 1 H50B H 0.404035 0.034601 0.640232 0.182 Uiso 0.5 1 calc R U P D 1 H50C H 0.308150 0.019614 0.622263 0.182 Uiso 0.5 1 calc R U P E 2 H50D H 0.396486 0.048822 0.638836 0.182 Uiso 0.5 1 calc R U P E 2 C51 C 0.3852(17) -0.121(2) 0.6231(6) 0.1988(7) Uani 0.5 1 d D U P F 1 H51A H 0.340814 -0.153901 0.610552 0.239 Uiso 0.5 1 calc R U P F 1 H51B H 0.445751 -0.141263 0.617316 0.239 Uiso 0.5 1 calc R U P F 1 C52 C 0.3665(11) -0.1407(18) 0.6574(5) 0.1991(7) Uani 0.5 1 d D U P F 1 H52A H 0.406431 -0.191818 0.665366 0.239 Uiso 0.5 1 calc R U P F 1 H52B H 0.372346 -0.079755 0.668916 0.239 Uiso 0.5 1 calc R U P F 1 C53 C 0.2703(11) -0.1761(14) 0.6559(5) 0.1995(8) Uani 0.5 1 d D U P F 1 H53A H 0.265561 -0.245150 0.662453 0.239 Uiso 0.5 1 calc R U P F 1 H53B H 0.247251 -0.171497 0.635826 0.239 Uiso 0.5 1 calc R U P F 1 C54 C 0.2180(11) -0.1068(16) 0.6763(4) 0.1998(9) Uani 0.5 1 d D U P F 1 H54A H 0.222189 -0.128901 0.696674 0.240 Uiso 0.5 1 calc R U P F 1 H54B H 0.239940 -0.038325 0.674889 0.240 Uiso 0.5 1 calc R U P F 1 C55 C 0.1231(11) -0.1156(19) 0.6648(4) 0.1999(10) Uani 0.5 1 d D U P F 1 H55A H 0.115243 -0.176222 0.653275 0.240 Uiso 0.5 1 calc R U P F 1 H55B H 0.106801 -0.058003 0.652839 0.240 Uiso 0.5 1 calc R U P F 1 C56 C 0.0678(13) -0.119(2) 0.6928(5) 0.181(3) Uani 0.5 1 d D U P F 1 H56A H 0.004533 -0.118056 0.687914 0.272 Uiso 0.5 1 calc R U P F 1 H56B H 0.082260 -0.062211 0.704902 0.272 Uiso 0.5 1 calc R U P F 1 H56C H 0.081560 -0.179734 0.703422 0.272 Uiso 0.5 1 calc R U P F 1 C44A C 0.7072(13) 0.4800(15) 0.3061(3) 0.167(3) Uani 0.5 1 d D . P C 2 H44C H 0.762239 0.440921 0.308279 0.200 Uiso 0.5 1 calc R U P C 2 H44D H 0.661505 0.437515 0.297079 0.200 Uiso 0.5 1 calc R U P C 2 C45A C 0.7246(11) 0.5670(17) 0.2871(3) 0.167(3) Uani 0.5 1 d D . P C 2 H45C H 0.770420 0.604131 0.297873 0.200 Uiso 0.5 1 calc R U P C 2 H45D H 0.669658 0.606410 0.288922 0.200 Uiso 0.5 1 calc R U P C 2 C46A C 0.7507(11) 0.582(2) 0.2559(3) 0.167(3) Uani 0.5 1 d D . P C 2 H46D H 0.701161 0.562720 0.243313 0.251 Uiso 0.5 1 calc R U P C 2 H46E H 0.802469 0.540675 0.251509 0.251 Uiso 0.5 1 calc R U P C 2 H46F H 0.765447 0.650858 0.252666 0.251 Uiso 0.5 1 calc R U P C 2 C43A C 0.676(2) 0.514(3) 0.3357(5) 0.167(3) Uani 0.5 1 d D . P C 2 H43C H 0.618335 0.548923 0.333854 0.200 Uiso 0.5 1 calc R U P C 2 H43D H 0.719570 0.558544 0.344498 0.200 Uiso 0.5 1 calc R U P C 2 C60 C 0.1768(11) -0.1970(13) 0.6986(4) 0.1522(6) Uani 0.5 1 d D U P F 2 H60A H 0.163933 -0.246885 0.713585 0.183 Uiso 0.5 1 calc R U P F 2 H60B H 0.161691 -0.224202 0.679306 0.183 Uiso 0.5 1 calc R U P F 2 C59 C 0.2736(11) -0.164(2) 0.6998(5) 0.2782(6) Uani 0.5 1 d D U P F 2 H59A H 0.313970 -0.221427 0.700016 0.334 Uiso 0.5 1 calc R U P F 2 H59B H 0.284857 -0.124003 0.717381 0.334 Uiso 0.5 1 calc R U P F 2 C57 C 0.3805(12) -0.098(2) 0.6348(5) 0.1797(6) Uani 0.5 1 d D U P F 2 H57A H 0.413945 -0.099483 0.653224 0.216 Uiso 0.5 1 calc R U P F 2 H57B H 0.410007 -0.141090 0.620534 0.216 Uiso 0.5 1 calc R U P F 2 C61 C 0.1263(17) -0.1010(17) 0.7044(6) 0.268(13) Uani 0.5 1 d D U P F 2 H61A H 0.082514 -0.090187 0.689000 0.401 Uiso 0.5 1 calc R U P F 2 H61B H 0.168210 -0.045964 0.704842 0.401 Uiso 0.5 1 calc R U P F 2 H61C H 0.095811 -0.105586 0.723079 0.401 Uiso 0.5 1 calc R U P F 2 C58 C 0.2822(10) -0.1276(11) 0.6393(3) 0.1530(6) Uani 0.5 1 d D U P F 2 H58A H 0.270837 -0.198197 0.635563 0.184 Uiso 0.5 1 calc R U P F 2 H58B H 0.239832 -0.086146 0.628341 0.184 Uiso 0.5 1 calc R U P F 2 C62 C 0.2872(13) -0.1017(15) 0.6720(3) 0.1531(6) Uani 0.5 1 d D U P F 2 H62A H 0.245139 -0.046308 0.674213 0.184 Uiso 0.5 1 calc R U P F 2 H62B H 0.346996 -0.072688 0.674437 0.184 Uiso 0.5 1 calc R U P F 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.092(3) 0.062(2) 0.0347(18) -0.0090(15) 0.0231(18) 0.0081(19) N2 0.146(4) 0.046(2) 0.045(2) -0.0004(16) 0.038(2) 0.005(2) N3 0.0476(16) 0.0307(14) 0.0235(13) -0.0001(10) 0.0121(11) 0.0009(11) N4 0.0493(16) 0.0310(13) 0.0268(14) 0.0000(10) 0.0086(12) 0.0008(12) C1 0.065(2) 0.0491(19) 0.0292(17) 0.0019(13) 0.0141(16) 0.0020(17) C2 0.080(3) 0.060(2) 0.0333(18) 0.0061(17) 0.0222(18) 0.010(2) C3 0.109(4) 0.061(2) 0.033(2) 0.0083(17) 0.028(2) 0.006(2) C4 0.128(4) 0.056(2) 0.040(2) 0.0112(19) 0.036(2) 0.006(3) C5 0.112(4) 0.049(2) 0.0373(19) 0.0082(17) 0.028(2) 0.005(2) C6 0.075(3) 0.0474(19) 0.0290(17) 0.0048(14) 0.0178(16) 0.0034(18) C7 0.071(2) 0.0436(17) 0.0271(16) 0.0011(13) 0.0155(16) -0.0009(17) C8 0.050(2) 0.0429(17) 0.0269(15) 0.0000(12) 0.0105(14) 0.0003(15) C9 0.050(2) 0.0415(18) 0.0264(14) 0.0006(12) 0.0093(13) 0.0016(15) C10 0.056(2) 0.0470(18) 0.0262(15) 0.0003(12) 0.0118(14) 0.0028(16) C11 0.066(2) 0.0528(19) 0.0257(17) -0.0012(14) 0.0166(16) 0.0027(18) C12 0.0477(19) 0.0404(16) 0.0263(15) -0.0010(12) 0.0105(13) 0.0030(14) C13 0.067(2) 0.0409(17) 0.0286(17) -0.0045(13) 0.0107(16) 0.0068(16) C14 0.066(2) 0.039(2) 0.0356(16) -0.0010(13) 0.0162(16) 0.0071(18) C15 0.055(2) 0.0360(17) 0.0325(17) -0.0005(14) 0.0122(15) 0.0036(15) C16 0.0419(18) 0.0384(16) 0.0251(14) -0.0012(12) 0.0089(12) 0.0028(14) C17 0.0489(19) 0.0375(16) 0.0248(14) -0.0014(12) 0.0093(13) 0.0008(14) C18 0.051(2) 0.0364(16) 0.0249(14) -0.0002(12) 0.0073(13) -0.0005(15) C19 0.053(2) 0.0350(19) 0.0271(15) 0.0008(12) 0.0108(14) -0.0007(15) C20 0.0472(19) 0.0334(15) 0.0250(14) -0.0020(11) 0.0105(13) 0.0004(14) C21 0.0444(18) 0.0331(15) 0.0237(14) -0.0017(12) 0.0083(12) -0.0008(14) C22 0.0414(18) 0.0339(15) 0.0240(14) -0.0007(11) 0.0082(12) 0.0017(13) C23 0.0406(18) 0.0320(15) 0.0227(15) 0.0009(11) 0.0091(12) -0.0010(13) C24 0.0435(18) 0.0319(15) 0.0236(16) -0.0019(11) 0.0065(13) 0.0001(13) C25 0.0497(19) 0.0312(15) 0.0289(16) -0.0006(12) 0.0062(14) -0.0001(14) C26 0.052(2) 0.0302(17) 0.0387(16) -0.0029(13) 0.0141(14) -0.0020(14) C27 0.054(2) 0.0341(18) 0.045(2) 0.0021(14) 0.0141(15) -0.0018(14) C28 0.067(3) 0.035(2) 0.067(2) 0.0014(18) 0.0248(19) 0.0019(18) C29 0.082(3) 0.036(2) 0.069(2) -0.0076(18) 0.029(2) 0.003(2) C30 0.089(3) 0.039(2) 0.051(2) -0.0121(16) 0.024(2) -0.0029(19) C31 0.072(3) 0.035(2) 0.0384(16) -0.0043(15) 0.0130(16) 0.0001(18) C32 0.092(3) 0.0424(19) 0.0300(19) 0.0044(15) 0.0236(19) -0.002(2) C33 0.0575(18) 0.0326(18) 0.0245(16) -0.0001(14) 0.0108(13) 0.0072(14) C34 0.0628(19) 0.047(2) 0.0358(19) -0.0111(15) -0.0006(14) 0.0140(15) C35 0.055(2) 0.045(2) 0.056(2) -0.0093(17) -0.0059(16) 0.0056(17) C36 0.048(2) 0.042(2) 0.057(2) -0.0008(16) 0.0044(16) 0.0007(17) C37 0.048(2) 0.051(2) 0.067(2) 0.0086(18) -0.0019(17) -0.0071(18) C38 0.047(2) 0.068(3) 0.068(2) 0.0110(19) 0.0051(18) -0.002(2) C39 0.059(3) 0.092(4) 0.072(3) 0.022(2) 0.003(2) -0.014(2) C40 0.063(3) 0.142(5) 0.080(3) 0.010(3) 0.012(3) -0.009(3) C41 0.066(3) 0.209(7) 0.082(3) 0.049(4) -0.001(3) -0.022(4) C42 0.098(4) 0.315(10) 0.089(3) 0.028(4) 0.016(3) -0.038(5) C43 0.057(11) 0.449(16) 0.102(7) 0.098(8) -0.010(7) -0.045(14) C44 0.214(9) 0.546(9) 0.140(7) 0.069(9) 0.051(7) 0.004(9) C45 0.214(9) 0.546(9) 0.141(7) 0.069(9) 0.051(7) 0.004(9) C46 0.214(9) 0.546(10) 0.141(7) 0.069(9) 0.051(7) 0.004(9) C47 0.076(3) 0.056(2) 0.047(2) -0.0044(17) 0.0011(18) 0.022(2) C48 0.1418(11) 0.1832(12) 0.1293(11) 0.0887(10) 0.0370(11) 0.0394(11) C49 0.1418(11) 0.1832(12) 0.1293(11) 0.0887(10) 0.0370(11) 0.0394(11) C50 0.1418(11) 0.1832(12) 0.1293(11) 0.0887(10) 0.0370(11) 0.0394(11) C51 0.1970(12) 0.1846(12) 0.2148(12) 0.0886(11) 0.0369(11) 0.0393(12) C52 0.1974(13) 0.1849(14) 0.2152(13) 0.0884(13) 0.0367(13) 0.0390(13) C53 0.1977(15) 0.1852(15) 0.2157(14) 0.0882(14) 0.0365(14) 0.0389(14) C54 0.1979(16) 0.1853(16) 0.2161(16) 0.0879(15) 0.0364(15) 0.0388(16) C55 0.1980(17) 0.1854(17) 0.2164(17) 0.0877(16) 0.0363(16) 0.0388(17) C56 0.181(4) 0.181(4) 0.181(3) 0.0004(10) 0.0011(10) -0.0004(10) C44A 0.098(4) 0.315(10) 0.089(3) 0.028(4) 0.016(3) -0.038(5) C45A 0.098(4) 0.315(10) 0.089(3) 0.028(4) 0.016(3) -0.038(5) C46A 0.098(4) 0.315(10) 0.089(3) 0.028(4) 0.016(3) -0.038(5) C43A 0.098(4) 0.315(10) 0.089(3) 0.028(4) 0.016(3) -0.038(5) C60 0.1466(11) 0.1825(12) 0.1278(11) 0.0916(10) 0.0343(11) 0.0407(11) C59 0.2132(11) 0.2245(11) 0.3969(11) 0.1476(10) 0.0447(11) -0.0415(11) C57 0.2352(11) 0.1779(11) 0.1261(11) 0.0888(10) 0.0233(10) -0.0294(11) C61 0.333(10) 0.168(11) 0.30(3) 0.125(16) 0.21(2) 0.066(14) C58 0.1452(11) 0.1832(11) 0.1307(11) 0.0887(10) 0.0342(10) 0.0404(11) C62 0.1455(11) 0.1832(11) 0.1307(11) 0.0888(10) 0.0336(11) 0.0404(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C20 N3 C33 119.8(3) . . ? C23 N3 C20 107.5(3) . . ? C23 N3 C33 125.6(3) . . ? C25 N4 C24 119.4(3) . . ? C2 C1 C6 118.7(4) . . ? C2 C1 C10 121.9(4) . . ? C6 C1 C10 119.4(3) . . ? C1 C2 H2 119.5 . . ? C3 C2 C1 120.9(4) . . ? C3 C2 H2 119.6 . . ? C2 C3 H3 119.9 . . ? C2 C3 C4 120.1(4) . . ? C4 C3 H3 119.9 . . ? C3 C4 H4 119.7 . . ? C5 C4 C3 120.6(5) . . ? C5 C4 H4 119.7 . . ? C4 C5 H5 119.7 . . ? C4 C5 C6 120.6(4) . . ? C6 C5 H5 119.7 . . ? C1 C6 C7 119.1(4) . . ? C5 C6 C1 119.1(4) . . ? C5 C6 C7 121.7(4) . . ? C8 C7 C6 120.8(4) . . ? C8 C7 C32 120.7(3) . . ? C32 C7 C6 118.5(4) . . ? C7 C8 C9 120.0(3) . . ? C7 C8 C18 132.5(3) . . ? C9 C8 C18 107.5(3) . . ? C8 C9 C12 108.4(3) . . ? C10 C9 C8 119.9(3) . . ? C10 C9 C12 131.7(3) . . ? C9 C10 C1 120.7(3) . . ? C9 C10 C11 120.2(4) . . ? C11 C10 C1 119.0(3) . . ? N1 C11 C10 179.0(5) . . ? C13 C12 C9 134.2(3) . . ? C13 C12 C17 119.4(3) . . ? C17 C12 C9 106.4(3) . . ? C12 C13 H13 121.0 . . ? C12 C13 C14 118.0(3) . . ? C14 C13 H13 121.0 . . ? C13 C14 H14 118.5 . . ? C15 C14 C13 123.0(4) . . ? C15 C14 H14 118.5 . . ? C14 C15 H15 119.7 . . ? C14 C15 C16 120.7(3) . . ? C16 C15 H15 119.7 . . ? C15 C16 C21 129.1(3) . . ? C17 C16 C15 115.4(3) . . ? C17 C16 C21 115.5(3) . . ? C16 C17 C12 123.5(4) . . ? C16 C17 C18 125.1(3) . . ? C18 C17 C12 111.4(3) . . ? C17 C18 C8 106.3(3) . . ? C19 C18 C8 133.8(4) . . ? C19 C18 C17 119.9(3) . . ? C18 C19 H19 121.8 . . ? C18 C19 C20 116.5(4) . . ? C20 C19 H19 121.7 . . ? N3 C20 C19 125.0(3) . . ? N3 C20 C21 109.8(3) . . ? C21 C20 C19 125.3(3) . . ? C20 C21 C16 117.7(3) . . ? C20 C21 C22 106.0(3) . . ? C22 C21 C16 136.3(3) . . ? C23 C22 C21 107.0(3) . . ? C23 C22 C24 119.4(3) . . ? C24 C22 C21 133.3(3) . . ? N3 C23 C22 109.7(3) . . ? N3 C23 C23 130.34(18) . 2_556 ? C22 C23 C23 120.0(2) . 2_556 ? N4 C24 C22 120.7(3) . . ? N4 C24 C24 119.66(19) . 2_556 ? C24 C24 C22 119.62(19) 2_556 . ? N4 C25 C25 120.52(19) . 2_556 ? N4 C25 C26 116.2(3) . . ? C25 C25 C26 123.3(2) 2_556 . ? C27 C26 C25 120.8(3) . . ? C27 C26 C31 120.2(4) . . ? C31 C26 C25 119.0(3) . . ? C26 C27 H27 120.0 . . ? C26 C27 C28 120.1(4) . . ? C28 C27 H27 120.0 . . ? C27 C28 H28 119.5 . . ? C29 C28 C27 121.0(4) . . ? C29 C28 H28 119.5 . . ? C28 C29 H29 119.7 . . ? C28 C29 C30 120.7(4) . . ? C30 C29 H29 119.6 . . ? C29 C30 H30 121.1 . . ? C31 C30 C29 117.9(4) . . ? C31 C30 H30 121.1 . . ? C26 C31 C30 120.2(4) . . ? C26 C31 H31 119.9 . . ? C30 C31 H31 119.9 . . ? N2 C32 C7 179.3(5) . . ? N3 C33 H33A 108.8 . . ? N3 C33 H33B 108.8 . . ? N3 C33 C34 114.0(3) . . ? H33A C33 H33B 107.6 . . ? C34 C33 H33A 108.7 . . ? C34 C33 H33B 108.8 . . ? C33 C34 H34 107.1 . . ? C35 C34 C33 111.5(3) . . ? C35 C34 H34 107.1 . . ? C35 C34 C47 113.7(4) . . ? C47 C34 C33 110.1(4) . . ? C47 C34 H34 107.1 . . ? C34 C35 H35A 108.3 . . ? C34 C35 H35B 108.3 . . ? H35A C35 H35B 107.4 . . ? C36 C35 C34 116.0(4) . . ? C36 C35 H35A 108.3 . . ? C36 C35 H35B 108.3 . . ? C35 C36 H36A 109.2 . . ? C35 C36 H36B 109.2 . . ? C35 C36 C37 112.2(4) . . ? H36A C36 H36B 107.9 . . ? C37 C36 H36A 109.2 . . ? C37 C36 H36B 109.2 . . ? C36 C37 H37A 108.5 . . ? C36 C37 H37B 108.5 . . ? C36 C37 C38 115.1(4) . . ? H37A C37 H37B 107.5 . . ? C38 C37 H37A 108.5 . . ? C38 C37 H37B 108.5 . . ? C37 C38 H38A 109.3 . . ? C37 C38 H38B 109.3 . . ? C37 C38 C39 111.5(4) . . ? H38A C38 H38B 108.0 . . ? C39 C38 H38A 109.3 . . ? C39 C38 H38B 109.3 . . ? C38 C39 H39A 108.3 . . ? C38 C39 H39B 108.4 . . ? H39A C39 H39B 107.4 . . ? C40 C39 C38 115.7(5) . . ? C40 C39 H39A 108.4 . . ? C40 C39 H39B 108.4 . . ? C39 C40 H40A 108.9 . . ? C39 C40 H40B 108.9 . . ? C39 C40 C41 113.4(6) . . ? H40A C40 H40B 107.7 . . ? C41 C40 H40A 108.9 . . ? C41 C40 H40B 108.9 . . ? C40 C41 H41A 108.7 . . ? C40 C41 H41B 108.7 . . ? H41A C41 H41B 107.6 . . ? C42 C41 C40 114.2(9) . . ? C42 C41 H41A 108.8 . . ? C42 C41 H41B 108.7 . . ? C41 C42 H42A 105.9 . . ? C41 C42 H42B 106.0 . . ? C41 C42 H42C 110.5 . . ? C41 C42 H42D 110.5 . . ? C41 C42 C43 125.4(17) . . ? C41 C42 C43A 106.3(12) . . ? H42A C42 H42B 106.2 . . ? H42C C42 H42D 108.6 . . ? C43 C42 H42A 105.9 . . ? C43 C42 H42B 106.1 . . ? C43A C42 H42C 110.5 . . ? C43A C42 H42D 110.5 . . ? C42 C43 H43A 109.2 . . ? C42 C43 H43B 109.3 . . ? C42 C43 C44 112(2) . . ? H43A C43 H43B 107.9 . . ? C44 C43 H43A 109.2 . . ? C44 C43 H43B 109.1 . . ? C43 C44 H44A 104.4 . . ? C43 C44 H44B 104.5 . . ? H44A C44 H44B 105.6 . . ? C45 C44 C43 131(3) . . ? C45 C44 H44A 104.2 . . ? C45 C44 H44B 104.9 . . ? C44 C45 H45A 104.9 . . ? C44 C45 H45B 104.3 . . ? C44 C45 C46 130(3) . . ? H45A C45 H45B 105.6 . . ? C46 C45 H45A 105.2 . . ? C46 C45 H45B 104.8 . . ? C45 C46 H46A 120.3 . . ? C45 C46 H46B 118.4 . . ? C45 C46 H46C 118.6 . . ? H46A C46 H46B 98.5 . . ? H46A C46 H46C 97.8 . . ? H46B C46 H46C 98.7 . . ? C34 C47 H47A 108.6 . . ? C34 C47 H47B 108.6 . . ? H47A C47 H47B 107.6 . . ? C48 C47 C34 114.7(5) . . ? C48 C47 H47A 108.7 . . ? C48 C47 H47B 108.5 . . ? C47 C48 H48A 108.5 . . ? C47 C48 H48B 108.6 . . ? C47 C48 C49 114.8(7) . . ? H48A C48 H48B 107.5 . . ? C49 C48 H48A 108.5 . . ? C49 C48 H48B 108.6 . . ? C48 C49 H49A 109.3 . . ? C48 C49 H49B 109.2 . . ? H49A C49 H49B 107.9 . . ? C50 C49 C48 112.0(8) . . ? C50 C49 H49A 109.3 . . ? C50 C49 H49B 109.2 . . ? C49 C50 H50A 110.6 . . ? C49 C50 H50B 110.7 . . ? C49 C50 H50C 106.2 . . ? C49 C50 H50D 106.3 . . ? C49 C50 C51 105.7(10) . . ? C49 C50 C57 124.8(12) . . ? H50A C50 H50B 108.8 . . ? H50C C50 H50D 106.4 . . ? C51 C50 H50A 110.9 . . ? C51 C50 H50B 110.1 . . ? C57 C50 H50C 106.2 . . ? C57 C50 H50D 105.9 . . ? C50 C51 H51A 111.9 . . ? C50 C51 H51B 112.6 . . ? H51A C51 H51B 109.9 . . ? C52 C51 C50 97.7(19) . . ? C52 C51 H51A 111.6 . . ? C52 C51 H51B 112.7 . . ? C51 C52 H52A 112.1 . . ? C51 C52 H52B 111.4 . . ? H52A C52 H52B 109.8 . . ? C53 C52 C51 99.9(16) . . ? C53 C52 H52A 111.8 . . ? C53 C52 H52B 111.6 . . ? C52 C53 H53A 111.0 . . ? C52 C53 H53B 109.8 . . ? C52 C53 C54 105.3(9) . . ? H53A C53 H53B 108.8 . . ? C54 C53 H53A 110.8 . . ? C54 C53 H53B 111.2 . . ? C53 C54 H54A 111.5 . . ? C53 C54 H54B 111.6 . . ? H54A C54 H54B 109.1 . . ? C55 C54 C53 102.6(8) . . ? C55 C54 H54A 111.0 . . ? C55 C54 H54B 111.0 . . ? C54 C55 H55A 110.8 . . ? C54 C55 H55B 111.3 . . ? C54 C55 C56 102.6(8) . . ? H55A C55 H55B 109.2 . . ? C56 C55 H55A 111.5 . . ? C56 C55 H55B 111.3 . . ? C55 C56 H56A 109.2 . . ? C55 C56 H56B 109.7 . . ? C55 C56 H56C 109.5 . . ? H56A C56 H56B 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? H44C C44A H44D 108.1 . . ? C45A C44A H44C 109.6 . . ? C45A C44A H44D 109.7 . . ? C45A C44A C43A 110.2(17) . . ? C43A C44A H44C 109.7 . . ? C43A C44A H44D 109.6 . . ? C44A C45A H45C 103.4 . . ? C44A C45A H45D 103.2 . . ? C44A C45A C46A 135.4(19) . . ? H45C C45A H45D 105.2 . . ? C46A C45A H45C 103.7 . . ? C46A C45A H45D 103.1 . . ? C45A C46A H46D 110.0 . . ? C45A C46A H46E 109.3 . . ? C45A C46A H46F 109.5 . . ? H46D C46A H46E 109.4 . . ? H46D C46A H46F 109.3 . . ? H46E C46A H46F 109.3 . . ? C42 C43A H43C 110.3 . . ? C42 C43A H43D 110.3 . . ? C44A C43A C42 107(2) . . ? C44A C43A H43C 110.3 . . ? C44A C43A H43D 110.2 . . ? H43C C43A H43D 108.5 . . ? H60A C60 H60B 109.2 . . ? C59 C60 H60A 111.5 . . ? C59 C60 H60B 110.5 . . ? C59 C60 C61 102.5(9) . . ? C61 C60 H60A 111.4 . . ? C61 C60 H60B 111.6 . . ? C60 C59 H59A 111.2 . . ? C60 C59 H59B 110.1 . . ? C60 C59 C62 104.8(14) . . ? H59A C59 H59B 108.9 . . ? C62 C59 H59A 111.1 . . ? C62 C59 H59B 110.7 . . ? C50 C57 H57A 111.6 . . ? C50 C57 H57B 111.0 . . ? C50 C57 C58 102.5(14) . . ? H57A C57 H57B 109.2 . . ? C58 C57 H57A 112.1 . . ? C58 C57 H57B 110.2 . . ? C60 C61 H61A 109.1 . . ? C60 C61 H61B 110.0 . . ? C60 C61 H61C 109.5 . . ? H61A C61 H61B 109.4 . . ? H61A C61 H61C 109.4 . . ? H61B C61 H61C 109.4 . . ? C57 C58 H58A 114.1 . . ? C57 C58 H58B 113.2 . . ? C57 C58 C62 91.5(13) . . ? H58A C58 H58B 110.5 . . ? C62 C58 H58A 113.3 . . ? C62 C58 H58B 113.1 . . ? C59 C62 H62A 104.3 . . ? C59 C62 H62B 104.0 . . ? C58 C62 C59 132.5(19) . . ? C58 C62 H62A 104.1 . . ? C58 C62 H62B 104.1 . . ? H62A C62 H62B 105.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C11 1.146(5) . ? N2 C32 1.133(6) . ? N3 C20 1.400(4) . ? N3 C23 1.380(4) . ? N3 C33 1.477(5) . ? N4 C24 1.348(4) . ? N4 C25 1.331(5) . ? C1 C2 1.417(5) . ? C1 C6 1.418(6) . ? C1 C10 1.431(6) . ? C2 H2 0.9500 . ? C2 C3 1.360(7) . ? C3 H3 0.9500 . ? C3 C4 1.404(7) . ? C4 H4 0.9500 . ? C4 C5 1.364(6) . ? C5 H5 0.9500 . ? C5 C6 1.406(6) . ? C6 C7 1.440(5) . ? C7 C8 1.380(6) . ? C7 C32 1.429(6) . ? C8 C9 1.438(5) . ? C8 C18 1.471(5) . ? C9 C10 1.388(5) . ? C9 C12 1.458(5) . ? C10 C11 1.424(6) . ? C12 C13 1.370(5) . ? C12 C17 1.417(5) . ? C13 H13 0.9500 . ? C13 C14 1.397(5) . ? C14 H14 0.9500 . ? C14 C15 1.378(5) . ? C15 H15 0.9500 . ? C15 C16 1.416(5) . ? C16 C17 1.399(5) . ? C16 C21 1.448(5) . ? C17 C18 1.415(5) . ? C18 C19 1.368(5) . ? C19 H19 0.9500 . ? C19 C20 1.416(5) . ? C20 C21 1.407(5) . ? C21 C22 1.441(4) . ? C22 C23 1.408(5) . ? C22 C24 1.439(5) . ? C23 C23 1.433(6) 2_556 ? C24 C24 1.432(6) 2_556 ? C25 C25 1.414(7) 2_556 ? C25 C26 1.481(5) . ? C26 C27 1.390(6) . ? C26 C31 1.391(6) . ? C27 H27 0.9500 . ? C27 C28 1.395(6) . ? C28 H28 0.9500 . ? C28 C29 1.357(7) . ? C29 H29 0.9500 . ? C29 C30 1.429(6) . ? C30 H30 0.9500 . ? C30 C31 1.421(5) . ? C31 H31 0.9500 . ? C33 H33A 0.9900 . ? C33 H33B 0.9900 . ? C33 C34 1.546(6) . ? C34 H34 1.0000 . ? C34 C35 1.523(6) . ? C34 C47 1.528(6) . ? C35 H35A 0.9900 . ? C35 H35B 0.9900 . ? C35 C36 1.507(6) . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C36 C37 1.509(6) . ? C37 H37A 0.9900 . ? C37 H37B 0.9900 . ? C37 C38 1.512(7) . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C38 C39 1.531(7) . ? C39 H39A 0.9900 . ? C39 H39B 0.9900 . ? C39 C40 1.485(9) . ? C40 H40A 0.9900 . ? C40 H40B 0.9900 . ? C40 C41 1.536(9) . ? C41 H41A 0.9900 . ? C41 H41B 0.9900 . ? C41 C42 1.456(12) . ? C42 H42A 0.9900 . ? C42 H42B 0.9900 . ? C42 H42C 0.9900 . ? C42 H42D 0.9900 . ? C42 C43 1.47(3) . ? C42 C43A 1.68(4) . ? C43 H43A 0.9900 . ? C43 H43B 0.9900 . ? C43 C44 1.545(10) . ? C44 H44A 0.9900 . ? C44 H44B 0.9900 . ? C44 C45 1.522(10) . ? C45 H45A 0.9900 . ? C45 H45B 0.9900 . ? C45 C46 1.547(10) . ? C46 H46A 1.0885 . ? C46 H46B 1.0745 . ? C46 H46C 1.0755 . ? C47 H47A 0.9900 . ? C47 H47B 0.9900 . ? C47 C48 1.510(9) . ? C48 H48A 0.9900 . ? C48 H48B 0.9900 . ? C48 C49 1.529(12) . ? C49 H49A 0.9900 . ? C49 H49B 0.9900 . ? C49 C50 1.511(10) . ? C50 H50A 0.9900 . ? C50 H50B 0.9900 . ? C50 H50C 0.9900 . ? C50 H50D 0.9900 . ? C50 C51 1.73(3) . ? C50 C57 1.50(3) . ? C51 H51A 0.9900 . ? C51 H51B 0.9900 . ? C51 C52 1.63(3) . ? C52 H52A 0.9900 . ? C52 H52B 0.9900 . ? C52 C53 1.529(10) . ? C53 H53A 0.9900 . ? C53 H53B 0.9900 . ? C53 C54 1.550(10) . ? C54 H54A 0.9900 . ? C54 H54B 0.9900 . ? C54 C55 1.530(7) . ? C55 H55A 0.9900 . ? C55 H55B 0.9900 . ? C55 C56 1.539(10) . ? C56 H56A 0.9801 . ? C56 H56B 0.9801 . ? C56 H56C 0.9801 . ? C44A H44C 0.9900 . ? C44A H44D 0.9900 . ? C44A C45A 1.498(10) . ? C44A C43A 1.517(10) . ? C45A H45C 0.9900 . ? C45A H45D 0.9900 . ? C45A C46A 1.506(9) . ? C46A H46D 0.9812 . ? C46A H46E 0.9812 . ? C46A H46F 0.9812 . ? C43A H43C 0.9900 . ? C43A H43D 0.9900 . ? C60 H60A 0.9900 . ? C60 H60B 0.9900 . ? C60 C59 1.527(10) . ? C60 C61 1.536(10) . ? C59 H59A 0.9900 . ? C59 H59B 0.9900 . ? C59 C62 1.555(10) . ? C57 H57A 0.9900 . ? C57 H57B 0.9900 . ? C57 C58 1.550(10) . ? C61 H61A 0.9806 . ? C61 H61B 0.9807 . ? C61 H61C 0.9806 . ? C58 H58A 0.9900 . ? C58 H58B 0.9900 . ? C58 C62 1.554(10) . ? C62 H62A 0.9900 . ? C62 H62B 0.9900 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N3 C20 C21 C16 179.5(3) . . . . ? N3 C20 C21 C22 -0.9(4) . . . . ? N3 C33 C34 C35 -72.3(4) . . . . ? N3 C33 C34 C47 160.6(3) . . . . ? N4 C25 C26 C27 -129.2(4) . . . . ? N4 C25 C26 C31 48.4(5) . . . . ? C1 C2 C3 C4 0.7(8) . . . . ? C1 C6 C7 C8 -1.6(7) . . . . ? C1 C6 C7 C32 178.4(4) . . . . ? C2 C1 C6 C5 -0.1(7) . . . . ? C2 C1 C6 C7 179.9(4) . . . . ? C2 C1 C10 C9 -178.3(4) . . . . ? C2 C1 C10 C11 4.3(6) . . . . ? C2 C3 C4 C5 -1.1(9) . . . . ? C3 C4 C5 C6 0.9(9) . . . . ? C4 C5 C6 C1 -0.3(8) . . . . ? C4 C5 C6 C7 179.6(5) . . . . ? C5 C6 C7 C8 178.5(4) . . . . ? C5 C6 C7 C32 -1.5(7) . . . . ? C6 C1 C2 C3 -0.1(7) . . . . ? C6 C1 C10 C9 0.1(6) . . . . ? C6 C1 C10 C11 -177.4(4) . . . . ? C6 C7 C8 C9 0.0(6) . . . . ? C6 C7 C8 C18 -179.6(4) . . . . ? C7 C8 C9 C10 1.6(6) . . . . ? C7 C8 C9 C12 -178.0(4) . . . . ? C7 C8 C18 C17 177.5(4) . . . . ? C7 C8 C18 C19 -2.0(8) . . . . ? C8 C9 C10 C1 -1.7(6) . . . . ? C8 C9 C10 C11 175.8(4) . . . . ? C8 C9 C12 C13 177.1(4) . . . . ? C8 C9 C12 C17 -0.6(4) . . . . ? C8 C18 C19 C20 178.7(4) . . . . ? C9 C8 C18 C17 -2.2(4) . . . . ? C9 C8 C18 C19 178.3(4) . . . . ? C9 C12 C13 C14 -176.8(4) . . . . ? C9 C12 C17 C16 178.7(3) . . . . ? C9 C12 C17 C18 -0.8(4) . . . . ? C10 C1 C2 C3 178.3(5) . . . . ? C10 C1 C6 C5 -178.5(4) . . . . ? C10 C1 C6 C7 1.5(7) . . . . ? C10 C9 C12 C13 -2.5(8) . . . . ? C10 C9 C12 C17 179.9(4) . . . . ? C12 C9 C10 C1 177.8(4) . . . . ? C12 C9 C10 C11 -4.7(7) . . . . ? C12 C13 C14 C15 -1.0(6) . . . . ? C12 C17 C18 C8 1.9(4) . . . . ? C12 C17 C18 C19 -178.6(3) . . . . ? C13 C12 C17 C16 0.6(6) . . . . ? C13 C12 C17 C18 -178.9(4) . . . . ? C13 C14 C15 C16 0.0(6) . . . . ? C14 C15 C16 C17 1.2(5) . . . . ? C14 C15 C16 C21 -178.8(4) . . . . ? C15 C16 C17 C12 -1.5(5) . . . . ? C15 C16 C17 C18 177.9(4) . . . . ? C15 C16 C21 C20 -178.9(4) . . . . ? C15 C16 C21 C22 1.7(7) . . . . ? C16 C17 C18 C8 -177.6(4) . . . . ? C16 C17 C18 C19 1.9(6) . . . . ? C16 C21 C22 C23 -177.9(4) . . . . ? C16 C21 C22 C24 8.1(7) . . . . ? C17 C12 C13 C14 0.7(6) . . . . ? C17 C16 C21 C20 1.1(5) . . . . ? C17 C16 C21 C22 -178.3(4) . . . . ? C17 C18 C19 C20 -0.8(5) . . . . ? C18 C8 C9 C10 -178.7(3) . . . . ? C18 C8 C9 C12 1.7(4) . . . . ? C18 C19 C20 N3 -179.6(3) . . . . ? C18 C19 C20 C21 0.0(6) . . . . ? C19 C20 C21 C16 -0.2(5) . . . . ? C19 C20 C21 C22 179.5(3) . . . . ? C20 N3 C23 C22 2.9(4) . . . . ? C20 N3 C23 C23 -175.8(4) . . . 2_556 ? C20 N3 C33 C34 -67.6(4) . . . . ? C20 C21 C22 C23 2.6(4) . . . . ? C20 C21 C22 C24 -171.4(4) . . . . ? C21 C16 C17 C12 178.5(3) . . . . ? C21 C16 C17 C18 -2.1(5) . . . . ? C21 C22 C23 N3 -3.4(4) . . . . ? C21 C22 C23 C23 175.4(4) . . . 2_556 ? C21 C22 C24 N4 -9.2(6) . . . . ? C21 C22 C24 C24 170.4(4) . . . 2_556 ? C23 N3 C20 C19 178.5(3) . . . . ? C23 N3 C20 C21 -1.2(4) . . . . ? C23 N3 C33 C34 79.2(4) . . . . ? C23 C22 C24 N4 177.4(3) . . . . ? C23 C22 C24 C24 -3.0(6) . . . 2_556 ? C24 N4 C25 C25 -4.0(6) . . . 2_556 ? C24 N4 C25 C26 175.2(3) . . . . ? C24 C22 C23 N3 171.6(3) . . . . ? C24 C22 C23 C23 -9.6(6) . . . 2_556 ? C25 N4 C24 C22 175.4(3) . . . . ? C25 N4 C24 C24 -4.2(6) . . . 2_556 ? C25 C25 C26 C27 50.0(6) 2_556 . . . ? C25 C25 C26 C31 -132.4(5) 2_556 . . . ? C25 C26 C27 C28 177.2(4) . . . . ? C25 C26 C31 C30 -177.7(4) . . . . ? C26 C27 C28 C29 0.3(6) . . . . ? C27 C26 C31 C30 -0.2(6) . . . . ? C27 C28 C29 C30 0.3(7) . . . . ? C28 C29 C30 C31 -0.8(7) . . . . ? C29 C30 C31 C26 0.8(6) . . . . ? C31 C26 C27 C28 -0.4(6) . . . . ? C32 C7 C8 C9 -180.0(4) . . . . ? C32 C7 C8 C18 0.4(7) . . . . ? C33 N3 C20 C19 -29.4(5) . . . . ? C33 N3 C20 C21 151.0(3) . . . . ? C33 N3 C23 C22 -147.2(3) . . . . ? C33 N3 C23 C23 34.1(7) . . . 2_556 ? C33 C34 C35 C36 -69.9(5) . . . . ? C33 C34 C47 C48 -79.1(7) . . . . ? C34 C35 C36 C37 164.5(3) . . . . ? C34 C47 C48 C49 178.5(8) . . . . ? C35 C34 C47 C48 155.0(6) . . . . ? C35 C36 C37 C38 179.2(4) . . . . ? C36 C37 C38 C39 173.9(4) . . . . ? C37 C38 C39 C40 -178.1(4) . . . . ? C38 C39 C40 C41 176.8(4) . . . . ? C39 C40 C41 C42 -176.3(6) . . . . ? C40 C41 C42 C43 -177.8(12) . . . . ? C40 C41 C42 C43A 174.3(13) . . . . ? C41 C42 C43 C44 179.6(18) . . . . ? C41 C42 C43A C44A 178.7(16) . . . . ? C42 C43 C44 C45 174(3) . . . . ? C43 C44 C45 C46 -179(3) . . . . ? C47 C34 C35 C36 55.2(5) . . . . ? C47 C48 C49 C50 178.7(8) . . . . ? C48 C49 C50 C51 157.2(14) . . . . ? C48 C49 C50 C57 166.9(12) . . . . ? C49 C50 C51 C52 164.6(11) . . . . ? C49 C50 C57 C58 -124.7(13) . . . . ? C50 C51 C52 C53 101.0(16) . . . . ? C50 C57 C58 C62 -97.3(15) . . . . ? C51 C52 C53 C54 -124.3(19) . . . . ? C52 C53 C54 C55 157.4(17) . . . . ? C53 C54 C55 C56 139.1(19) . . . . ? C45A C44A C43A C42 -176.8(17) . . . . ? C43A C44A C45A C46A -175(2) . . . . ? C60 C59 C62 C58 -63(3) . . . . ? C57 C58 C62 C59 -120(2) . . . . ? C61 C60 C59 C62 -71(2) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.161 0.208 0.322 76.1 14.5 ? 2 0.161 0.292 0.822 76.1 14.5 ? 3 -0.161 0.708 0.178 76.1 14.5 ? 4 -0.161 0.792 0.678 76.1 14.5 ? 5 0.339 0.208 0.678 76.1 14.5 ? 6 0.339 0.292 0.178 76.1 14.5 ? 7 0.661 0.708 0.822 76.1 14.5 ? 8 0.661 0.792 0.322 76.1 14.5 ?