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Information card for entry 1571962
Preview
| Coordinates | 1571962.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C21 H25 N O6 S |
|---|---|
| Calculated formula | C21 H25 N O6 S |
| Title of publication | Enantioselective phosphine-catalyzed [6 + 1] annulations of α-allyl allenoates with 1,1-bisnucleophiles. |
| Authors of publication | Lai, Jingxiong; Cai, Wei; Huang, You |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 29 |
| Pages of publication | 11515 - 11520 |
| a | 7.0682 ± 0.0006 Å |
| b | 8.2714 ± 0.0007 Å |
| c | 18.0737 ± 0.0016 Å |
| α | 93.27 ± 0.004° |
| β | 99.19 ± 0.004° |
| γ | 90.759 ± 0.004° |
| Cell volume | 1041.13 ± 0.16 Å3 |
| Cell temperature | 193 K |
| Ambient diffraction temperature | 193 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0709 |
| Residual factor for significantly intense reflections | 0.0627 |
| Weighted residual factors for significantly intense reflections | 0.1597 |
| Weighted residual factors for all reflections included in the refinement | 0.1655 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.08 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.34139 Å |
| Diffraction radiation type | GaKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 293727 (current) | 2024-08-05 | cif/ Updating files of 1571962 Original log message: Adding full bibliography for 1571962.cif. |
1571962.cif |
| 292521 | 2024-06-22 | cif/ Adding structures of 1571962 via cif-deposit CGI script. |
1571962.cif |
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Users of the data should acknowledge the original authors of the
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