#------------------------------------------------------------------------------ #$Date: 2024-08-05 21:07:34 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293766 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/19/1571965.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571965 loop_ _publ_author_name 'Chen, Jia-Wei' 'Ji, Wen-Jun' 'Huang, Xue-Ying' 'Ge, Danhua' 'Shen, Zhi-Liang' 'Guo, Kai' 'Chu, Xue-Qiang' _publ_section_title ; Chemo-, regio-, and stereoselective tetrafunctionalization of fluoroalkynes enables divergent synthesis of 5-7-membered azacycles. ; _journal_issue 30 _journal_name_full 'Chemical science' _journal_page_first 12026 _journal_page_last 12035 _journal_paper_doi 10.1039/d4sc03230f _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C21 H18 Br F7 N2' _chemical_formula_sum 'C21 H18 Br F7 N2' _chemical_formula_weight 511.28 _chemical_name_systematic CXQ-220602-2 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2022-06-02 _audit_creation_method ; Olex2 1.5 (compiled 2021.12.09 svn.r5202d8cf for OlexSys, GUI svn.r6439) ; _audit_update_record ; 2022-06-02 deposited with the CCDC. 2024-06-23 downloaded from the CCDC. ; _cell_angle_alpha 80.233(4) _cell_angle_beta 78.910(4) _cell_angle_gamma 79.201(4) _cell_formula_units_Z 2 _cell_length_a 9.0199(4) _cell_length_b 9.6664(5) _cell_length_c 12.1317(5) _cell_measurement_reflns_used 6279 _cell_measurement_temperature 100.01(10) _cell_measurement_theta_max 74.7700 _cell_measurement_theta_min 3.8030 _cell_volume 1009.79(8) _computing_cell_refinement 'CrysAlisPro 1.171.41.110a (Rigaku OD, 2021)' _computing_data_collection 'CrysAlisPro 1.171.41.110a (Rigaku OD, 2021)' _computing_data_reduction 'CrysAlisPro 1.171.41.110a (Rigaku OD, 2021)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.01(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.977 _diffrn_measured_fraction_theta_max 0.964 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 20.00 67.12 0.38 0.04 -- 43.34 49.00 -77.00 124 2 \w 74.00 102.88 0.38 0.04 -- 43.34 49.00 -77.00 76 3 \w 126.00 173.88 0.38 0.10 -- 109.59 45.00-150.00 126 4 \w 122.00 176.34 0.38 0.10 -- 109.59 61.00-120.00 143 5 \w 87.00 176.30 0.38 0.10 -- 109.59 49.00 -77.00 235 6 \w 102.00 127.08 0.38 0.10 -- 109.59 45.00 -30.00 66 7 \w 132.00 177.22 0.38 0.10 -- 109.59 45.00 -30.00 119 8 \w 88.00 173.12 0.38 0.10 -- 109.59 45.00 0.00 224 9 \w -78.00 -44.94 0.38 0.10 -- -96.00 77.00-180.00 87 10 \w -55.00 -19.66 0.38 0.10 -- -96.00 49.00 -77.00 93 11 \w -59.00 -28.98 0.38 0.10 -- -96.00 61.00 -60.00 79 12 \w -47.00 -18.88 0.38 0.10 -- -96.00 45.00 90.00 74 13 \w -51.00 -25.92 0.38 0.10 -- -96.00 45.00 120.00 66 14 \w -50.00 -21.88 0.38 0.10 -- -96.00 45.00 150.00 74 15 \w -25.00 35.04 0.38 0.04 -- -43.34 19.00 30.00 158 16 \w -11.00 33.46 0.38 0.04 -- -43.34 37.00 60.00 117 17 \w -45.00 31.00 0.38 0.04 -- -43.34 49.00 -77.00 200 18 \w 40.00 69.64 0.38 0.10 -- 109.59 -61.00 -90.00 78 19 \w 93.00 147.34 0.38 0.10 -- 109.59 125.00 120.00 143 20 \w 1.00 27.22 0.38 0.04 -- 43.34 -49.00 135.00 69 21 \w 37.00 65.12 0.38 0.10 -- 109.59 -61.00 150.00 74 22 \w 52.00 99.88 0.38 0.10 -- 109.59 -94.00 60.00 126 23 \w 90.00 115.08 0.38 0.10 -- 109.59-125.00 60.00 66 24 \w 68.00 103.72 0.38 0.10 -- 109.59-125.00 0.00 94 25 \w 37.00 98.56 0.38 0.04 -- 43.34-125.00 -60.00 162 26 \w 71.00 115.08 0.38 0.10 -- 109.59-125.00-180.00 116 27 \w 45.00 104.28 0.38 0.10 -- 109.59-125.00-120.00 156 28 \w 38.00 106.02 0.38 0.10 -- 109.59 -94.00-120.00 179 29 \w -87.00 -31.14 0.38 0.10 -- -96.00 125.00 0.00 147 30 \w -86.00 -40.78 0.38 0.10 -- -96.00 125.00 -30.00 119 31 \w -56.00 -28.64 0.38 0.04 -- -43.34 -49.00 135.00 72 32 \w -116.00 -55.96 0.38 0.04 -- -43.34 -49.00 135.00 158 33 \w -159.00-132.02 0.38 0.10 -- -96.00 -49.00 135.00 71 34 \w -115.00 -72.06 0.38 0.10 -- -96.00 -49.00 135.00 113 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.1294223000 _diffrn_orient_matrix_UB_12 0.0115089000 _diffrn_orient_matrix_UB_13 -0.0690717000 _diffrn_orient_matrix_UB_21 0.0085511000 _diffrn_orient_matrix_UB_22 0.1590348000 _diffrn_orient_matrix_UB_23 -0.0382766000 _diffrn_orient_matrix_UB_31 0.1194337000 _diffrn_orient_matrix_UB_32 -0.0376109000 _diffrn_orient_matrix_UB_33 -0.1041018000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0275 _diffrn_reflns_av_unetI/netI 0.0308 _diffrn_reflns_Laue_measured_fraction_full 0.977 _diffrn_reflns_Laue_measured_fraction_max 0.964 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 8740 _diffrn_reflns_point_group_measured_fraction_full 0.977 _diffrn_reflns_point_group_measured_fraction_max 0.964 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 69.966 _diffrn_reflns_theta_min 3.749 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 3.472 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.80804 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.110a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear whiteish white' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier whiteish _exptl_crystal_colour_primary white _exptl_crystal_density_diffrn 1.682 _exptl_crystal_description needle _exptl_crystal_F_000 512 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.328 _refine_diff_density_min -0.421 _refine_diff_density_rms 0.055 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 280 _refine_ls_number_reflns 3689 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.045 _refine_ls_R_factor_all 0.0271 _refine_ls_R_factor_gt 0.0260 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0299P)^2^+0.5241P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0653 _refine_ls_wR_factor_ref 0.0662 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3530 _reflns_number_total 3689 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03230f2.cif _cod_data_source_block zyw-220602-2_auto _cod_depositor_comments 'Adding full bibliography for 1571965--1571967.cif.' _cod_database_code 1571965 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C N F Br' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.723 _shelx_estimated_absorpt_t_min 0.723 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2.a Secondary CH2 refined with riding coordinates: C00N(H00A,H00B), C00O(H00C,H00D), C00P(H00F,H00G), C00R(H00H,H00K), C00S(H00L, H00N), C00T(H00O,H00P), C00U(H00Q,H00R) 2.b Aromatic/amide H refined with riding coordinates: C00E(H00E), C00I(H00I), C00J(H00J), C00M(H00M) ; _shelx_res_file ; TITL zyw-220602-2_auto_a.res in P-1 zyw-220602-2_auto.res created by SHELXL-2018/3 at 19:38:15 on 02-Jun-2022 REM Old TITL ZYW-220602-2_auto in P1 REM SHELXT solution in P-1: R1 0.123, Rweak 0.010, Alpha 0.027 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C21 N2 F7 Br CELL 1.54184 9.0199 9.6664 12.1317 80.233 78.91 79.201 ZERR 2 0.0004 0.0005 0.0005 0.004 0.004 0.004 LATT 1 SFAC C H Br F N UNIT 42 36 2 14 4 L.S. 4 0 0 PLAN 4 SIZE 0.1 0.1 0.1 TEMP -173 CONF list 4 fmap 2 53 ACTA MORE -1 BOND $H OMIT 0 140 REM REM REM WGHT 0.029900 0.524100 FVAR 0.61106 BR01 3 0.359107 0.740185 0.063403 11.00000 0.02728 0.03751 = 0.01710 0.00580 -0.00584 -0.01205 F002 4 0.472533 0.196661 0.438817 11.00000 0.02222 0.03224 = 0.02399 -0.00964 -0.00083 -0.00902 F003 4 0.497438 -0.032006 0.345690 11.00000 0.04101 0.02735 = 0.02794 -0.00994 -0.01039 0.01117 F004 4 0.083907 0.151353 0.498298 11.00000 0.02398 0.04052 = 0.03860 -0.02178 0.00136 -0.01356 F005 4 0.402115 0.054656 0.145982 11.00000 0.04599 0.04440 = 0.02362 -0.01905 -0.00759 0.00446 F006 4 0.250438 -0.017169 0.357556 11.00000 0.04520 0.04355 = 0.04208 -0.02604 0.01013 -0.02465 F007 4 0.487181 0.218663 0.203536 11.00000 0.06659 0.05430 = 0.02133 -0.00116 0.00113 -0.03099 F008 4 0.245320 0.229012 0.211978 11.00000 0.05870 0.05388 = 0.03404 -0.01800 -0.02600 0.02633 N009 5 0.215710 0.492293 0.652482 11.00000 0.01708 0.01799 = 0.01579 -0.00462 -0.00226 -0.00408 N00A 5 0.143557 0.424490 0.855299 11.00000 0.02014 0.02443 = 0.01496 -0.00561 -0.00270 -0.00450 C00B 1 0.230022 0.437101 0.552801 11.00000 0.01569 0.02055 = 0.01648 -0.00507 -0.00281 -0.00204 C00C 1 0.201850 0.299381 0.582138 11.00000 0.01806 0.01923 = 0.01701 -0.00361 -0.00235 -0.00299 C00D 1 0.177957 0.389956 0.743904 11.00000 0.01447 0.02253 = 0.01392 -0.00301 -0.00248 -0.00241 C00E 1 0.407520 0.667354 0.293114 11.00000 0.01691 0.01634 = 0.02113 -0.00174 -0.00255 -0.00282 AFIX 43 H00E 2 0.486145 0.724400 0.270659 11.00000 -1.20000 AFIX 0 C00F 1 0.167886 0.267697 0.702659 11.00000 0.01800 0.01831 = 0.01606 -0.00285 -0.00212 -0.00253 C00G 1 0.320652 0.648619 0.215572 11.00000 0.02004 0.02001 = 0.01640 -0.00132 -0.00319 -0.00074 C00H 1 0.340798 0.152173 0.434713 11.00000 0.02308 0.01940 = 0.01636 -0.00145 -0.00390 -0.00708 C00I 1 0.174999 0.502701 0.357312 11.00000 0.01781 0.01941 = 0.02172 -0.00339 -0.00303 -0.00411 AFIX 43 H00I 2 0.094375 0.447898 0.379384 11.00000 -1.20000 AFIX 0 C00J 1 0.204484 0.567229 0.245998 11.00000 0.01805 0.02320 = 0.01828 -0.00324 -0.00525 -0.00264 AFIX 43 H00J 2 0.146137 0.555809 0.191720 11.00000 -1.20000 AFIX 0 C00K 1 0.261849 0.516639 0.438200 11.00000 0.01774 0.01685 = 0.01646 -0.00395 -0.00294 -0.00009 C00L 1 0.214403 0.199130 0.502340 11.00000 0.02363 0.01893 = 0.01738 -0.00171 -0.00384 -0.00762 C00M 1 0.377367 0.601083 0.404313 11.00000 0.01811 0.01788 = 0.01816 -0.00472 -0.00572 -0.00086 AFIX 43 H00M 2 0.436057 0.613302 0.458103 11.00000 -1.20000 AFIX 0 C00N 1 0.171618 0.077985 0.877800 11.00000 0.02654 0.02336 = 0.02134 0.00262 -0.00041 -0.00181 AFIX 23 H00A 2 0.138306 -0.014917 0.908517 11.00000 -1.20000 H00B 2 0.284853 0.062961 0.866144 11.00000 -1.20000 AFIX 0 C00O 1 0.233645 0.637417 0.661429 11.00000 0.02725 0.01895 = 0.02223 -0.00636 -0.00206 -0.00629 AFIX 23 H00C 2 0.191725 0.704935 0.599716 11.00000 -1.20000 H00D 2 0.343457 0.643607 0.654461 11.00000 -1.20000 AFIX 0 C00P 1 0.193095 0.556292 0.868032 11.00000 0.02504 0.03030 = 0.02054 -0.01102 -0.00148 -0.00734 AFIX 23 H00F 2 0.305591 0.539991 0.863876 11.00000 -1.20000 H00G 2 0.145571 0.584285 0.943279 11.00000 -1.20000 AFIX 0 C00Q 1 0.363979 0.059128 0.343826 11.00000 0.02413 0.02311 = 0.02331 -0.00763 -0.00310 -0.00358 C00R 1 0.118916 0.130732 0.763766 11.00000 0.02695 0.02054 = 0.01774 -0.00188 -0.00033 -0.00592 AFIX 23 H00H 2 0.158209 0.056139 0.713972 11.00000 -1.20000 H00K 2 0.005757 0.143145 0.776000 11.00000 -1.20000 AFIX 0 C00S 1 0.187233 0.311153 0.945997 11.00000 0.02200 0.03467 = 0.01525 -0.00233 -0.00449 -0.00581 AFIX 23 H00L 2 0.165341 0.352138 1.017971 11.00000 -1.20000 H00N 2 0.299192 0.279874 0.929181 11.00000 -1.20000 AFIX 0 C00T 1 0.109219 0.180660 0.964359 11.00000 0.02383 0.03088 = 0.01432 0.00160 -0.00263 -0.00423 AFIX 23 H00O 2 -0.001320 0.212557 0.962671 11.00000 -1.20000 H00P 2 0.119524 0.128753 1.040890 11.00000 -1.20000 AFIX 0 C00U 1 0.148121 0.674947 0.776053 11.00000 0.03210 0.02237 = 0.02430 -0.01004 -0.00123 -0.00538 AFIX 23 H00Q 2 0.173805 0.765097 0.789733 11.00000 -1.20000 H00R 2 0.036397 0.687990 0.776972 11.00000 -1.20000 AFIX 0 C00V 1 0.375570 0.141649 0.223641 11.00000 0.03329 0.03365 = 0.02168 -0.01080 -0.00878 0.00528 HKLF 4 REM zyw-220602-2_auto_a.res in P-1 REM wR2 = 0.0662, GooF = S = 1.045, Restrained GooF = 1.045 for all data REM R1 = 0.0260 for 3530 Fo > 4sig(Fo) and 0.0271 for all 3689 data REM 280 parameters refined using 0 restraints END WGHT 0.0299 0.5241 REM Highest difference peak 0.328, deepest hole -0.421, 1-sigma level 0.055 Q1 1 0.3560 0.6918 0.1583 11.00000 0.05 0.33 Q2 1 0.3783 0.6450 0.0671 11.00000 0.05 0.32 Q3 1 0.3546 0.7514 -0.0386 11.00000 0.05 0.29 Q4 1 0.1852 0.6610 0.7199 11.00000 0.05 0.28 ; _shelx_res_checksum 74037 _shelx_hkl_file ; -11 -4 -5 6.49 0.71 -11 -3 -6 172.00 5.71 -11 -2 -6 1.15 0.40 -10 -6 -5 95.53 4.62 -10 -6 -3 10.47 1.44 -10 -6 -2 7.25 1.19 -10 -6 -1 79.30 4.01 -10 -5 -8 21.61 1.45 -10 -5 -7 0.96 0.43 -10 -5 -6 38.45 2.20 -10 -5 -6 28.97 2.43 -10 -5 -5 31.01 2.61 -10 -5 -3 51.92 3.58 -10 -5 -2 129.35 6.12 -10 -5 -1 69.58 4.06 -10 -5 0 44.32 2.91 -10 -4 -7 164.43 6.13 -10 -4 -6 125.11 5.82 -10 -4 -5 23.22 2.35 -10 -4 -4 7.20 1.37 -10 -4 -3 16.01 2.09 -10 -4 -2 32.51 2.90 -10 -4 -1 6.13 1.28 -10 -4 0 31.83 2.62 -10 -4 1 147.99 6.09 -10 -3 -9 88.95 3.57 -10 -3 -8 37.85 2.24 -10 -3 -6 7.23 1.33 -10 -3 -5 16.63 2.09 -10 -3 -4 233.47 9.72 -10 -3 -3 43.02 3.52 -10 -3 -2 55.51 4.01 -10 -3 -1 9.20 1.60 -10 -3 0 3.33 0.93 -10 -3 1 40.59 2.91 -10 -2 -9 1.17 0.40 -10 -2 -8 70.14 3.25 -10 -2 -6 73.60 4.28 -10 -2 -5 136.60 6.64 -10 -2 -4 77.89 4.87 -10 -2 -2 0.39 0.64 -10 -2 -1 44.38 3.56 -10 -2 0 64.03 4.20 -10 -2 1 57.74 3.68 -10 -1 -8 5.04 0.74 -10 -1 -7 0.65 0.43 -10 -1 -5 0.49 0.63 -10 -1 -4 26.40 2.69 -10 -1 0 0.34 0.57 -10 -1 1 19.75 2.09 -10 0 -7 111.79 4.19 -10 0 1 94.04 4.89 -9 -7 -6 3.56 0.95 -9 -7 -5 32.44 2.75 -9 -7 -3 158.27 7.19 -9 -7 -2 43.30 3.27 -9 -7 -1 57.58 3.69 -9 -6 -6 186.80 8.05 -9 -6 -5 59.94 4.18 -9 -6 -3 19.84 2.38 -9 -6 -2 8.36 1.59 -9 -6 -1 0.89 0.74 -9 -6 0 3.47 0.98 -9 -6 1 13.49 1.67 -9 -5 -10 70.43 3.17 -9 -5 -9 94.65 4.15 -9 -5 -8 148.01 5.90 -9 -5 -7 5.17 0.99 -9 -5 -6 92.62 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3 -8 19.49 2.26 0 3 -8 19.95 2.37 0 3 -7 117.86 5.74 0 3 -7 123.46 8.23 0 3 -6 56.82 3.43 0 3 -6 65.42 5.31 0 3 -5 38.93 3.87 0 3 -4 1168.19 35.00 0 3 -3 4362.65 120.90 0 3 -2 6.95 1.26 0 3 -1 43.19 3.17 0 3 1 1280.85 37.84 0 3 2 2304.23 65.37 0 3 3 9.08 1.47 0 3 5 243.50 9.57 0 4 -13 109.01 4.25 0 4 -12 1.86 0.71 0 4 -11 -0.17 0.58 0 4 -10 101.76 5.73 0 4 -10 96.49 5.59 0 4 -9 0.94 0.69 0 4 -9 3.25 1.20 0 4 -9 1.98 0.91 0 4 -8 452.81 15.66 0 4 -8 433.85 15.45 0 4 -8 430.63 16.15 0 4 -8 410.16 19.12 0 4 -7 713.51 23.78 0 4 -7 726.02 22.94 0 4 -7 706.22 27.09 0 4 -6 84.61 4.58 0 4 -6 81.32 6.61 0 4 -5 207.35 10.86 0 4 -4 616.52 21.38 0 4 -2 261.71 11.18 0 4 -1 75.00 5.01 0 4 1 791.12 25.76 0 4 2 140.91 7.32 0 4 3 1349.61 41.10 0 5 -12 89.04 4.10 0 5 -12 90.89 3.82 0 5 -11 357.90 12.32 0 5 -11 350.50 12.36 0 5 -10 161.31 7.27 0 5 -10 162.83 7.51 0 5 -9 87.83 5.11 0 5 -9 79.66 5.33 0 5 -8 122.65 6.28 0 5 -8 119.66 6.35 0 5 -8 110.17 6.68 0 5 -7 13.44 2.97 0 5 -7 17.36 2.15 0 5 -7 15.83 2.10 0 5 -7 15.49 2.34 0 5 -6 0.44 0.64 0 5 -6 0.98 0.72 0 5 -6 0.43 0.67 0 5 -5 111.24 5.38 0 5 -5 92.32 7.47 0 5 -4 323.54 14.24 0 5 -1 509.40 19.36 0 5 1 1.70 1.09 0 5 2 95.71 6.50 0 5 3 328.39 14.08 0 5 5 760.12 26.73 0 6 -11 13.00 1.34 0 6 -11 12.02 1.35 0 6 -11 9.08 1.01 0 6 -10 14.52 1.70 0 6 -10 17.55 1.96 0 6 -9 77.55 4.49 0 6 -9 72.65 4.83 0 6 -9 76.04 4.65 0 6 -8 91.38 5.25 0 6 -8 104.03 6.21 0 6 -8 99.06 5.50 0 6 -8 94.49 5.56 0 6 -7 130.77 6.61 0 6 -7 126.98 6.75 0 6 -7 132.13 7.40 0 6 -6 266.84 10.47 0 6 -6 252.22 14.31 0 6 -5 336.19 13.47 0 6 -5 353.99 12.55 0 6 -5 317.40 16.56 0 6 -4 17.67 2.36 0 6 -4 19.62 3.28 0 6 -3 153.80 7.35 0 6 -3 155.92 9.91 0 6 5 15.11 2.91 0 7 -10 128.58 5.33 0 7 -9 160.32 6.65 0 7 -9 176.95 7.18 0 7 -9 172.08 7.42 0 7 -8 5.89 1.14 0 7 -8 5.91 1.43 0 7 -8 6.91 1.35 0 7 -7 3.64 1.04 0 7 -7 3.16 0.96 0 7 -7 3.34 1.24 0 7 -6 86.74 5.04 0 7 -6 92.11 5.73 0 7 -6 93.70 5.95 0 7 -5 100.91 5.47 0 7 -5 116.59 6.68 0 7 -4 144.30 6.64 0 7 -4 144.60 7.56 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54.22 3.68 0 10 -1 75.65 4.65 0 10 0 83.70 5.17 0 10 2 52.35 4.12 0 10 3 4.08 1.26 0 10 4 13.53 1.97 0 10 5 7.52 1.42 0 10 6 19.76 2.01 0 11 -3 9.98 1.14 0 11 -2 245.06 8.67 0 11 -1 28.44 2.25 0 11 -1 28.72 2.19 0 11 0 4.89 1.04 0 11 0 3.31 0.83 0 11 1 37.03 2.49 0 11 2 8.48 1.40 0 11 3 1.33 0.71 0 11 4 18.23 1.89 0 11 5 156.84 6.20 1 -11 -5 85.92 3.78 1 -11 -4 44.23 2.55 1 -11 -4 44.68 2.68 1 -11 -3 10.91 1.27 1 -11 -3 10.99 1.27 1 -11 -2 10.06 1.20 1 -11 -1 7.02 1.09 1 -11 0 11.59 1.29 1 -10 -7 63.28 3.51 1 -10 -7 65.52 3.46 1 -10 -6 39.83 2.83 1 -10 -5 3.75 0.91 1 -10 -5 3.24 0.97 1 -10 -4 50.25 3.53 1 -10 -4 50.43 3.37 1 -10 -3 0.91 0.77 1 -10 -3 2.37 0.93 1 -10 -2 20.52 2.18 1 -10 -1 5.56 1.20 1 -10 -1 7.10 1.43 1 -10 0 64.32 4.02 1 -10 1 211.31 8.38 1 -10 2 37.37 2.70 1 -9 -9 7.39 1.02 1 -9 -8 21.34 2.03 1 -9 -8 20.81 1.88 1 -9 -8 24.27 2.23 1 -9 -7 13.52 1.82 1 -9 -7 11.05 1.47 1 -9 -7 13.39 1.80 1 -9 -6 7.33 1.53 1 -9 -5 0.78 0.75 1 -9 -4 14.80 2.15 1 -9 -3 649.69 21.58 1 -9 -2 178.01 8.16 1 -9 -1 24.51 2.63 1 -9 0 76.44 4.61 1 -9 2 0.49 0.75 1 -9 3 314.23 11.35 1 -8 -11 15.95 1.51 1 -8 -10 5.07 1.06 1 -8 -10 5.88 1.14 1 -8 -9 58.95 3.72 1 -8 -9 54.26 3.65 1 -8 -9 54.14 3.59 1 -8 -8 61.15 4.09 1 -8 -8 60.98 4.12 1 -8 -8 63.83 4.10 1 -8 -8 64.59 4.09 1 -8 -7 253.14 10.17 1 -8 -7 243.62 9.93 1 -8 -6 73.91 4.64 1 -8 -6 76.38 4.46 1 -8 -6 77.24 4.96 1 -8 -5 103.56 5.57 1 -8 -4 0.82 0.99 1 -8 -3 23.78 2.84 1 -8 -3 27.28 4.33 1 -8 -2 0.98 0.97 1 -8 -1 182.81 8.10 1 -8 -1 164.18 7.82 1 -8 0 8.77 1.66 1 -8 0 13.44 2.03 1 -8 0 8.72 2.51 1 -8 1 405.93 14.06 1 -8 1 377.34 18.39 1 -7 -11 291.45 10.53 1 -7 -10 91.87 5.11 1 -7 -10 96.66 5.31 1 -7 -10 92.36 4.99 1 -7 -9 117.41 6.06 1 -7 -9 101.84 5.87 1 -7 -9 100.67 5.68 1 -7 -8 57.96 3.96 1 -7 -8 52.16 4.02 1 -7 -8 49.63 3.95 1 -7 -7 0.93 0.95 1 -7 -7 0.78 0.78 1 -7 -6 121.49 6.43 1 -7 -6 128.14 6.66 1 -7 -6 114.98 9.30 1 -7 -5 44.36 5.57 1 -7 -5 42.33 3.46 1 -7 -5 42.66 4.93 1 -7 -4 212.91 12.89 1 -7 -4 207.83 8.92 1 -7 -4 210.10 12.00 1 -7 -4 222.56 9.01 1 -7 -3 207.07 11.90 1 -7 -3 212.24 8.81 1 -7 -3 194.44 12.17 1 -7 -2 552.71 22.61 1 -7 -1 2.24 0.94 1 -7 -1 -0.41 0.90 1 -7 0 240.23 9.63 1 -7 0 228.43 9.44 1 -7 0 229.83 12.77 1 -7 1 36.33 2.97 1 -7 1 35.72 3.16 1 -7 1 38.25 4.74 1 -7 2 55.76 5.77 1 -7 2 62.19 4.10 1 -7 3 437.02 18.93 1 -6 -13 34.85 2.19 1 -6 -12 147.26 6.38 1 -6 -11 -0.17 0.80 1 -6 -11 0.34 0.73 1 -6 -10 4.45 1.38 1 -6 -10 5.32 1.25 1 -6 -9 98.72 5.88 1 -6 -9 96.90 5.68 1 -6 -9 101.06 5.99 1 -6 -8 13.29 1.88 1 -6 -8 19.53 2.56 1 -6 -8 16.74 2.23 1 -6 -7 222.39 13.56 1 -6 -7 246.50 9.89 1 -6 -7 232.28 10.04 1 -6 -6 549.77 21.97 1 -6 -6 614.00 24.84 1 -6 -6 621.27 20.11 1 -6 -5 193.80 7.64 1 -6 -5 163.33 10.84 1 -6 -5 172.93 10.01 1 -6 -5 176.41 7.95 1 -6 -4 139.44 9.47 1 -6 -4 144.39 8.92 1 -6 -4 150.05 6.58 1 -6 -3 17.75 2.02 1 -6 -3 18.50 3.09 1 -6 -2 162.51 7.09 1 -6 -2 167.01 9.70 1 -6 -1 429.49 14.83 1 -6 -1 459.06 18.38 1 -6 0 200.70 8.22 1 -6 0 208.11 10.98 1 -6 1 511.85 16.94 1 -6 1 557.27 21.00 1 -6 1 531.11 17.26 1 -6 2 282.12 10.43 1 -6 2 278.57 13.37 1 -6 3 0.77 0.56 1 -6 3 1.69 0.76 1 -6 3 1.67 1.11 1 -5 -13 30.78 2.28 1 -5 -12 2.48 0.96 1 -5 -11 209.78 8.94 1 -5 -11 184.98 7.73 1 -5 -11 196.13 8.79 1 -5 -10 229.08 10.16 1 -5 -10 240.56 10.40 1 -5 -10 237.72 9.98 1 -5 -9 14.98 2.20 1 -5 -9 12.19 2.04 1 -5 -9 14.95 2.12 1 -5 -8 74.38 4.89 1 -5 -8 62.73 6.80 1 -5 -8 67.03 4.57 1 -5 -7 39.97 3.40 1 -5 -7 39.27 3.08 1 -5 -7 34.90 4.79 1 -5 -7 39.41 3.19 1 -5 -7 35.06 3.15 1 -5 -6 153.56 9.90 1 -5 -6 150.63 6.97 1 -5 -6 130.48 7.81 1 -5 -5 582.54 18.37 1 -5 -5 614.98 23.42 1 -5 -5 603.05 21.48 1 -5 -4 519.13 20.53 1 -5 -4 521.05 19.39 1 -5 -3 516.73 19.25 1 -5 -2 855.09 28.64 1 -5 0 372.17 15.08 1 -5 1 32.65 3.59 1 -5 2 86.21 5.95 1 -5 3 234.48 8.60 1 -5 3 234.49 10.96 1 -5 4 371.56 15.01 1 -4 -13 22.18 2.02 1 -4 -13 19.76 1.83 1 -4 -12 78.68 4.71 1 -4 -11 79.00 5.08 1 -4 -11 85.26 5.30 1 -4 -10 6.39 1.55 1 -4 -10 5.37 1.53 1 -4 -9 178.97 8.24 1 -4 -9 166.32 8.19 1 -4 -9 170.89 12.05 1 -4 -9 174.30 8.43 1 -4 -9 170.03 8.04 1 -4 -8 84.97 5.16 1 -4 -8 80.55 7.63 1 -4 -8 85.82 4.99 1 -4 -8 88.17 5.17 1 -4 -7 794.36 30.14 1 -4 -7 840.66 25.92 1 -4 -7 809.48 25.51 1 -4 -6 82.14 4.52 1 -4 -6 99.81 7.32 1 -4 -5 2.56 1.18 1 -4 -5 2.65 0.96 1 -4 -4 6.52 1.64 1 -4 -4 5.94 1.39 1 -4 -3 560.16 19.29 1 -4 -2 11.82 1.94 1 -4 0 1399.00 42.10 1 -4 1 113.40 6.26 1 -4 2 971.09 30.49 1 -4 3 187.40 8.56 1 -4 4 1253.34 38.10 1 -3 -14 -0.83 0.69 1 -3 -13 3.18 0.85 1 -3 -12 220.70 9.35 1 -3 -12 212.05 9.00 1 -3 -11 53.52 4.24 1 -3 -11 54.39 4.20 1 -3 -11 60.64 4.43 1 -3 -10 583.36 20.92 1 -3 -10 630.53 21.33 1 -3 -10 655.29 21.53 1 -3 -10 638.89 21.40 1 -3 -9 99.99 5.78 1 -3 -9 94.13 8.66 1 -3 -9 104.25 5.95 1 -3 -9 99.05 5.77 1 -3 -9 88.64 5.42 1 -3 -9 99.66 5.61 1 -3 -9 94.62 5.26 1 -3 -8 253.67 10.12 1 -3 -8 244.76 9.92 1 -3 -8 249.59 9.62 1 -3 -8 274.96 14.43 1 -3 -8 240.03 9.90 1 -3 -8 242.73 9.85 1 -3 -7 20.51 2.17 1 -3 -7 24.33 2.38 1 -3 -7 26.44 3.90 1 -3 -6 413.40 17.19 1 -3 -5 80.42 4.48 1 -3 -5 83.64 5.87 1 -3 -4 826.28 27.07 1 -3 -4 815.05 25.24 1 -3 -3 1.40 0.83 1 -3 -3 2.35 0.78 1 -3 -2 2415.26 68.24 1 -3 0 8.26 1.38 1 -3 1 344.67 12.22 1 -3 2 336.87 12.00 1 -3 3 433.66 14.67 1 -3 4 1126.40 33.50 1 -2 -14 311.80 10.22 1 -2 -13 57.51 3.82 1 -2 -12 26.95 2.82 1 -2 -12 19.75 2.39 1 -2 -12 23.13 2.41 1 -2 -11 1.52 1.07 1 -2 -11 0.41 0.75 1 -2 -11 0.79 0.72 1 -2 -11 1.83 0.73 1 -2 -10 115.17 6.46 1 -2 -10 112.16 6.28 1 -2 -10 112.34 6.31 1 -2 -10 120.00 5.84 1 -2 -10 120.91 6.48 1 -2 -10 109.12 5.56 1 -2 -9 39.35 3.46 1 -2 -9 39.35 3.37 1 -2 -9 37.23 3.29 1 -2 -9 43.99 3.19 1 -2 -9 39.87 3.43 1 -2 -9 38.33 2.93 1 -2 -9 34.22 3.19 1 -2 -8 93.48 7.98 1 -2 -8 108.50 5.64 1 -2 -8 103.08 5.48 1 -2 -8 98.42 5.33 1 -2 -8 103.03 5.52 1 -2 -8 94.87 5.30 1 -2 -7 606.73 19.21 1 -2 -7 580.93 18.96 1 -2 -7 618.99 23.45 1 -2 -6 528.93 20.14 1 -2 -5 33.36 3.48 1 -2 -5 29.49 2.09 1 -2 -4 162.01 6.26 1 -2 -4 163.57 7.81 1 -2 -3 708.99 22.86 1 -2 -3 727.84 21.57 1 -2 -2 1645.66 46.45 1 -2 0 4710.04 128.83 1 -2 1 19.33 1.67 1 -2 2 1515.76 42.96 1 -2 3 24.74 1.94 1 -2 4 1109.83 32.00 1 -1 -14 20.06 1.74 1 -1 -13 42.03 3.21 1 -1 -13 39.03 3.07 1 -1 -12 124.44 6.49 1 -1 -12 113.40 5.52 1 -1 -12 110.74 6.12 1 -1 -11 7.05 1.52 1 -1 -11 7.45 1.45 1 -1 -11 8.92 1.49 1 -1 -10 1280.57 38.93 1 -1 -10 1333.87 38.77 1 -1 -10 1244.01 37.47 1 -1 -9 289.12 11.34 1 -1 -9 285.44 11.26 1 -1 -9 291.94 11.30 1 -1 -9 280.03 11.33 1 -1 -9 300.24 10.64 1 -1 -8 118.42 5.81 1 -1 -7 567.13 18.22 1 -1 -7 604.21 23.04 1 -1 -6 68.53 5.50 1 -1 -5 530.04 16.53 1 -1 -5 621.99 20.09 1 -1 -4 8.10 1.52 1 -1 -3 75.67 6.91 1 -1 -3 897.06 10.17 1 -1 -2 26.65 1.63 1 -1 -1 17.19 1.26 1 -1 0 188.86 6.33 1 -1 1 3483.33 95.01 1 -1 2 912.61 25.93 1 -1 3 566.45 16.62 1 -1 4 4051.56 110.19 1 0 -14 116.05 4.60 1 0 -13 219.86 8.72 1 0 -13 216.39 8.73 1 0 -13 216.68 8.10 1 0 -12 47.78 3.76 1 0 -12 45.83 3.63 1 0 -12 43.44 3.27 1 0 -11 171.35 8.15 1 0 -11 159.90 7.84 1 0 -11 155.97 7.43 1 0 -10 14.47 2.27 1 0 -10 17.54 2.38 1 0 -10 15.75 2.00 1 0 -9 94.02 5.51 1 0 -9 96.48 5.40 1 0 -9 95.60 5.12 1 0 -9 97.08 5.28 1 0 -8 374.44 13.36 1 0 -8 377.14 13.14 1 0 -8 364.19 12.75 1 0 -7 202.07 7.97 1 0 -7 193.20 7.69 1 0 -5 150.21 5.48 1 0 -5 155.95 8.09 1 0 -4 451.47 14.28 1 0 -4 438.92 13.17 1 0 -4 479.93 16.08 1 0 -3 14.31 1.23 1 0 -3 13.27 0.85 1 0 -2 6.53 0.63 1 0 -2 4.83 0.59 1 0 -1 100.38 3.62 1 0 0 1056.28 29.09 1 0 2 4.17 0.55 1 0 3 492.96 14.18 1 1 -13 3.82 1.03 1 1 -13 4.45 0.94 1 1 -12 107.45 5.73 1 1 -12 108.71 5.83 1 1 -12 104.61 5.53 1 1 -11 241.94 10.22 1 1 -11 244.56 10.31 1 1 -10 110.13 6.12 1 1 -10 106.75 6.00 1 1 -10 103.00 5.64 1 1 -9 246.26 10.14 1 1 -9 245.72 10.03 1 1 -9 240.37 9.69 1 1 -8 375.69 13.29 1 1 -8 372.57 13.12 1 1 -8 350.35 12.70 1 1 -8 375.89 12.91 1 1 -7 142.18 7.77 1 1 -7 158.13 6.60 1 1 -7 145.63 6.16 1 1 -7 141.64 6.12 1 1 -6 195.42 8.79 1 1 -5 641.01 20.63 1 1 -4 1471.11 41.68 1 1 -4 1741.21 44.02 1 1 -3 1862.35 52.14 1 1 1 460.46 13.74 1 2 -13 360.48 12.28 1 2 -13 356.90 11.90 1 2 -12 107.68 5.68 1 2 -11 217.56 9.17 1 2 -10 18.11 2.28 1 2 -10 21.63 2.41 1 2 -9 1.81 0.92 1 2 -9 2.78 0.93 1 2 -8 218.17 11.10 1 2 -8 217.45 8.88 1 2 -8 211.84 8.76 1 2 -8 220.87 8.85 1 2 -7 47.24 4.41 1 2 -7 52.92 3.39 1 2 -7 47.09 3.23 1 2 -7 52.58 3.34 1 2 -6 888.05 26.49 1 2 -6 886.26 26.37 1 2 -6 905.89 28.93 1 2 -5 951.46 29.75 1 2 -4 38.46 3.02 1 2 -3 137.12 5.56 1 2 -2 746.69 22.42 1 2 -1 37.29 2.50 1 2 1 3193.16 88.27 1 2 2 4957.02 135.66 1 2 3 526.01 16.48 1 2 4 36.78 2.46 1 3 -13 0.17 0.34 1 3 -12 36.36 2.79 1 3 -11 313.32 11.68 1 3 -10 442.27 15.65 1 3 -10 484.91 16.56 1 3 -10 458.77 16.16 1 3 -9 400.34 14.52 1 3 -9 434.95 15.28 1 3 -9 422.73 15.10 1 3 -9 432.85 15.13 1 3 -9 407.10 15.01 1 3 -8 4.92 1.57 1 3 -8 6.45 1.27 1 3 -8 5.56 1.21 1 3 -8 6.67 1.43 1 3 -8 5.84 1.27 1 3 -8 5.52 1.25 1 3 -7 414.70 14.08 1 3 -7 416.88 14.45 1 3 -7 431.06 14.47 1 3 -7 418.90 17.21 1 3 -6 3.31 1.22 1 3 -5 21.88 2.77 1 3 -4 10.72 1.54 1 3 -3 436.78 15.05 1 3 -2 1789.15 51.82 1 3 -1 1622.77 47.41 1 3 2 4.95 1.15 1 3 3 22.85 2.40 1 3 4 207.41 8.59 1 3 5 3279.95 91.69 1 4 -12 86.93 4.46 1 4 -12 97.43 4.42 1 4 -11 146.61 6.73 1 4 -11 141.49 6.53 1 4 -11 151.57 6.72 1 4 -10 -0.18 0.53 1 4 -10 0.18 0.52 1 4 -9 36.23 3.21 1 4 -9 31.09 3.03 1 4 -9 30.23 2.91 1 4 -9 30.30 3.11 1 4 -8 28.00 3.92 1 4 -8 29.09 2.84 1 4 -8 29.77 2.87 1 4 -8 23.62 2.82 1 4 -7 245.20 9.56 1 4 -7 224.15 10.07 1 4 -7 220.55 11.99 1 4 -6 843.57 25.04 1 4 -6 777.59 25.77 1 4 -6 772.00 28.21 1 4 -5 1039.58 30.74 1 4 -5 1077.58 34.78 1 4 -4 579.40 20.04 1 4 -3 187.50 8.98 1 4 -2 46.21 3.99 1 4 -1 43.53 3.88 1 4 2 322.93 13.09 1 4 3 239.56 10.59 1 4 4 10.24 1.86 1 4 5 262.20 11.18 1 5 -12 0.70 0.35 1 5 -11 134.17 5.84 1 5 -11 129.31 5.74 1 5 -11 131.10 5.56 1 5 -10 162.79 7.17 1 5 -10 156.22 7.13 1 5 -9 665.27 21.83 1 5 -9 684.82 22.09 1 5 -9 665.27 22.47 1 5 -8 160.33 7.44 1 5 -8 159.58 7.55 1 5 -8 148.38 7.97 1 5 -7 257.40 10.22 1 5 -7 258.17 10.31 1 5 -7 239.88 10.24 1 5 -7 260.42 11.25 1 5 -7 238.87 13.20 1 5 -6 3.56 1.46 1 5 -6 3.67 1.10 1 5 -6 4.33 1.32 1 5 -6 2.32 0.94 1 5 -5 7.78 2.06 1 5 -5 6.67 1.16 1 5 -4 347.13 14.92 1 5 -4 357.80 11.97 1 5 -3 433.07 13.96 1 5 -3 471.29 18.06 1 5 -2 497.64 19.42 1 5 -1 1313.40 42.09 1 5 0 10.11 2.24 1 5 1 566.62 21.30 1 5 2 1508.89 47.21 1 5 3 33.59 3.81 1 5 4 2.72 1.25 1 5 5 850.40 29.08 1 5 6 1437.98 45.00 1 6 -11 49.36 2.32 1 6 -10 59.39 3.49 1 6 -10 62.51 3.69 1 6 -10 58.05 3.18 1 6 -9 1.18 0.67 1 6 -9 1.31 0.77 1 6 -9 0.89 0.57 1 6 -8 60.27 3.99 1 6 -8 61.74 4.18 1 6 -8 56.44 4.12 1 6 -8 60.15 4.59 1 6 -7 449.39 15.77 1 6 -7 442.05 16.24 1 6 -7 472.01 16.22 1 6 -7 467.80 17.27 1 6 -6 508.41 17.21 1 6 -6 497.80 17.83 1 6 -6 475.82 21.24 1 6 -5 206.51 9.52 1 6 -5 187.31 11.60 1 6 -4 334.02 11.63 1 6 -4 331.83 15.37 1 6 -4 326.18 12.95 1 6 -3 20.58 3.39 1 6 -3 25.26 2.09 1 6 -3 21.54 2.51 1 6 -2 102.43 4.58 1 6 -2 107.41 7.90 1 6 -1 21.45 3.50 1 6 0 121.87 8.61 1 6 1 8.08 2.23 1 6 2 1339.70 44.23 1 6 3 667.21 25.46 1 6 4 183.41 10.71 1 6 5 505.72 20.74 1 6 6 319.48 15.02 1 7 -10 74.24 3.58 1 7 -9 299.78 10.84 1 7 -9 312.88 11.26 1 7 -8 55.11 3.71 1 7 -8 63.03 4.39 1 7 -7 87.62 4.76 1 7 -7 92.42 5.14 1 7 -7 84.58 5.23 1 7 -6 62.31 4.01 1 7 -6 63.92 4.23 1 7 -6 69.78 4.89 1 7 -6 64.71 4.93 1 7 -5 8.34 1.53 1 7 -5 9.88 1.98 1 7 -5 8.15 1.80 1 7 -4 122.61 6.92 1 7 -3 822.73 30.80 1 7 -3 800.98 25.91 1 7 -3 809.67 26.35 1 7 -2 1181.61 40.35 1 7 -2 1143.47 34.90 1 7 -2 1094.52 34.55 1 7 -1 237.88 13.38 1 7 -1 208.02 8.99 1 7 0 3.29 1.65 1 7 2 308.01 15.95 1 7 3 0.47 0.89 1 7 4 13.00 3.02 1 7 5 263.21 14.67 1 7 5 290.97 11.47 1 8 -7 22.81 2.19 1 8 -7 28.52 2.77 1 8 -6 282.28 10.85 1 8 -6 292.30 11.66 1 8 -6 318.81 12.21 1 8 -5 114.51 5.86 1 8 -5 131.91 7.00 1 8 -5 122.45 6.85 1 8 -4 6.72 1.29 1 8 -4 7.42 1.68 1 8 -4 5.40 1.48 1 8 -3 770.22 25.48 1 8 -3 815.80 26.08 1 8 -2 62.57 4.56 1 8 -2 74.26 5.06 1 8 -1 0.22 0.60 1 8 -1 1.60 1.45 1 8 -1 1.34 0.77 1 8 0 58.82 6.68 1 8 0 51.78 4.29 1 8 2 127.97 10.21 1 8 3 579.68 25.49 1 8 3 589.59 20.55 1 8 4 111.61 9.60 1 8 4 128.59 7.01 1 8 5 120.95 9.66 1 8 5 114.26 6.53 1 8 6 52.18 4.02 1 9 -7 32.12 2.26 1 9 -6 16.09 1.61 1 9 -6 19.05 2.00 1 9 -6 20.02 2.12 1 9 -5 8.78 1.26 1 9 -5 10.15 1.65 1 9 -5 9.14 1.67 1 9 -4 1.02 0.58 1 9 -4 0.75 0.90 1 9 -3 1.54 0.76 1 9 -3 1.72 0.97 1 9 -3 2.16 1.07 1 9 -3 2.51 0.78 1 9 -2 229.23 10.00 1 9 -2 204.95 9.05 1 9 -2 203.98 9.28 1 9 -1 252.23 10.83 1 9 0 329.60 13.29 1 9 2 213.05 9.92 1 9 3 21.18 2.78 1 9 4 387.76 14.88 1 9 5 13.85 2.14 1 9 6 63.92 4.41 1 10 -5 250.21 8.99 1 10 -3 2.11 0.90 1 10 -2 319.47 11.98 1 10 -2 307.47 11.41 1 10 -1 2.46 1.01 1 10 -1 1.27 0.88 1 10 0 25.35 2.78 1 10 0 28.61 2.92 1 10 1 60.26 4.15 1 10 2 33.27 2.89 1 10 2 31.09 3.20 1 10 3 141.98 7.31 1 10 4 1.15 0.88 1 10 5 96.57 5.46 1 10 6 154.79 6.90 1 11 -3 6.18 0.94 1 11 -2 1.08 0.63 1 11 -1 113.99 5.19 1 11 0 23.90 2.12 1 11 0 26.53 2.31 1 11 1 30.77 2.39 1 11 1 39.07 2.90 1 11 2 14.47 1.81 1 11 3 -0.43 0.62 1 11 4 64.09 3.85 1 11 5 23.90 2.08 1 11 6 26.89 1.95 1 12 3 7.49 0.89 2 -10 -6 1.65 0.72 2 -10 -5 12.87 1.59 2 -10 -4 18.56 1.97 2 -10 -4 20.63 1.91 2 -10 -3 -0.13 0.65 2 -10 -3 0.52 0.53 2 -10 -2 5.54 1.18 2 -10 -1 50.59 3.40 2 -10 -1 46.41 3.11 2 -10 0 29.64 2.55 2 -10 1 94.85 4.71 2 -10 2 52.91 3.10 2 -9 -9 13.38 1.19 2 -9 -8 28.04 2.06 2 -9 -7 25.55 2.21 2 -9 -7 32.83 2.60 2 -9 -6 32.61 2.60 2 -9 -6 34.38 2.92 2 -9 -6 32.41 2.67 2 -9 -5 2.41 0.81 2 -9 -5 0.83 0.65 2 -9 -4 22.92 2.61 2 -9 -4 26.42 2.57 2 -9 -3 279.91 11.11 2 -9 -3 282.64 11.02 2 -9 -2 -0.18 0.89 2 -9 -1 128.54 6.40 2 -9 -1 124.29 6.49 2 -9 0 36.85 3.04 2 -9 0 38.07 3.33 2 -9 1 2.57 1.06 2 -9 2 13.93 1.87 2 -9 3 0.13 0.51 2 -8 -10 127.46 5.27 2 -8 -9 14.33 1.71 2 -8 -8 17.33 2.01 2 -8 -8 14.20 1.78 2 -8 -7 10.21 1.68 2 -8 -7 11.22 1.81 2 -8 -7 11.15 1.66 2 -8 -6 185.87 8.41 2 -8 -6 188.81 8.30 2 -8 -5 325.52 12.33 2 -8 -5 322.63 12.03 2 -8 -4 41.89 3.51 2 -8 -4 47.50 3.99 2 -8 -4 50.48 3.78 2 -8 -3 10.46 1.76 2 -8 -3 8.41 1.82 2 -8 -3 9.23 1.75 2 -8 -2 2.24 0.92 2 -8 -2 3.22 1.30 2 -8 -1 4.65 1.35 2 -8 0 4.02 1.25 2 -8 1 44.69 3.67 2 -8 1 42.43 3.36 2 -8 2 209.98 9.08 2 -8 3 16.64 2.10 2 -7 -12 7.37 0.84 2 -7 -11 34.58 2.47 2 -7 -11 36.19 2.48 2 -7 -10 107.54 5.29 2 -7 -10 105.78 5.30 2 -7 -9 77.59 4.68 2 -7 -9 72.68 4.51 2 -7 -8 84.33 5.14 2 -7 -8 80.70 4.70 2 -7 -8 83.22 5.04 2 -7 -8 78.55 4.69 2 -7 -7 23.51 2.70 2 -7 -7 22.61 2.55 2 -7 -7 22.13 2.52 2 -7 -7 21.17 2.40 2 -7 -6 213.17 9.40 2 -7 -6 230.76 9.54 2 -7 -6 203.29 8.97 2 -7 -6 202.76 8.46 2 -7 -5 127.03 6.60 2 -7 -5 120.46 6.08 2 -7 -5 119.61 6.54 2 -7 -5 101.36 8.17 2 -7 -4 155.41 7.28 2 -7 -4 156.20 7.46 2 -7 -4 145.45 10.79 2 -7 -4 128.02 9.61 2 -7 -3 83.49 5.07 2 -7 -3 83.67 7.87 2 -7 -3 84.32 5.34 2 -7 -3 74.78 7.12 2 -7 -2 18.15 2.26 2 -7 -2 25.13 2.81 2 -7 -2 22.61 3.89 2 -7 -1 240.57 9.80 2 -7 -1 222.14 9.36 2 -7 -1 213.07 12.85 2 -7 0 390.28 13.99 2 -7 0 364.67 17.99 2 -7 1 134.85 6.50 2 -7 1 123.81 9.40 2 -7 2 38.30 3.43 2 -7 2 35.86 4.81 2 -7 3 88.35 5.10 2 -7 3 89.46 5.33 2 -7 4 5.71 1.23 2 -7 4 4.37 1.20 2 -7 5 106.24 5.65 2 -6 -11 164.62 7.10 2 -6 -10 1.94 1.03 2 -6 -10 1.80 0.94 2 -6 -9 2.39 1.10 2 -6 -9 0.40 0.90 2 -6 -9 0.82 0.68 2 -6 -8 33.72 2.93 2 -6 -8 34.33 3.32 2 -6 -8 35.89 3.32 2 -6 -8 30.65 2.92 2 -6 -7 125.91 6.27 2 -6 -7 122.51 6.41 2 -6 -7 135.81 6.98 2 -6 -7 127.30 6.81 2 -6 -7 120.14 6.36 2 -6 -6 2.85 1.09 2 -6 -6 3.08 1.61 2 -6 -6 3.95 1.27 2 -6 -5 1.48 1.34 2 -6 -5 0.94 0.98 2 -6 -5 0.31 0.59 2 -6 -5 1.17 0.86 2 -6 -5 0.75 0.83 2 -6 -4 1123.57 34.20 2 -6 -4 1124.24 39.77 2 -6 -4 1137.02 34.37 2 -6 -4 1081.60 37.90 2 -6 -3 205.75 12.43 2 -6 -3 225.96 9.31 2 -6 -3 230.24 12.32 2 -6 -2 -0.17 0.74 2 -6 -2 0.77 0.95 2 -6 -1 134.30 6.52 2 -6 0 26.74 2.57 2 -6 0 28.90 2.77 2 -6 0 24.18 3.78 2 -6 1 66.12 4.05 2 -6 1 65.23 4.30 2 -6 1 62.96 6.06 2 -6 2 140.21 6.84 2 -6 2 154.72 9.62 2 -6 3 868.51 27.00 2 -6 3 842.38 30.67 2 -6 4 178.52 7.46 2 -6 4 162.68 7.63 2 -6 5 4.10 1.09 2 -5 -12 73.33 4.10 2 -5 -11 9.99 1.75 2 -5 -10 42.98 3.17 2 -5 -9 20.79 2.62 2 -5 -9 17.44 2.13 2 -5 -9 18.66 2.51 2 -5 -9 20.26 2.32 2 -5 -8 1202.80 36.75 2 -5 -8 1183.45 36.86 2 -5 -8 1211.63 35.41 2 -5 -8 1155.30 35.87 2 -5 -7 45.85 3.56 2 -5 -7 43.67 5.66 2 -5 -7 47.89 3.55 2 -5 -7 46.53 3.29 2 -5 -7 47.27 3.67 2 -5 -7 41.96 3.40 2 -5 -7 48.35 3.88 2 -5 -6 197.47 8.34 2 -5 -6 209.25 12.62 2 -5 -6 216.49 8.68 2 -5 -6 198.68 8.81 2 -5 -6 185.02 8.29 2 -5 -5 8.00 1.48 2 -5 -5 7.04 1.29 2 -5 -5 12.70 2.96 2 -5 -5 9.79 1.63 2 -5 -5 8.28 1.29 2 -5 -5 9.01 2.05 2 -5 -4 25.63 2.53 2 -5 -4 25.49 3.87 2 -5 -4 30.69 3.75 2 -5 -3 20.35 3.31 2 -5 -3 25.14 3.40 2 -5 -2 766.24 24.13 2 -5 -2 827.56 27.70 2 -5 -2 773.30 23.82 2 -5 -1 121.66 5.71 2 -5 0 388.84 13.26 2 -5 0 416.22 16.67 2 -5 0 386.26 13.23 2 -5 1 143.34 8.50 2 -5 1 140.96 6.17 2 -5 2 196.08 10.33 2 -5 3 400.68 16.59 2 -5 4 294.60 13.39 2 -5 5 1.87 0.77 2 -4 -13 67.45 3.23 2 -4 -12 124.33 5.51 2 -4 -12 122.83 5.93 2 -4 -11 50.75 3.87 2 -4 -11 54.33 4.06 2 -4 -11 52.56 3.61 2 -4 -10 230.66 9.95 2 -4 -10 225.62 10.10 2 -4 -9 182.38 8.74 2 -4 -9 201.93 8.57 2 -4 -9 187.36 9.07 2 -4 -9 186.24 8.27 2 -4 -8 403.70 14.25 2 -4 -8 366.10 18.95 2 -4 -8 358.52 13.46 2 -4 -7 0.54 0.60 2 -4 -7 3.21 0.99 2 -4 -7 0.48 0.93 2 -4 -7 1.18 0.79 2 -4 -7 1.28 0.71 2 -4 -6 618.69 19.81 2 -4 -6 637.70 25.04 2 -4 -6 610.77 19.66 2 -4 -6 634.23 20.48 2 -4 -5 24.03 2.25 2 -4 -5 32.05 4.09 2 -4 -5 25.49 3.02 2 -4 -4 791.18 27.90 2 -4 -4 763.10 25.93 2 -4 -3 460.63 18.11 2 -4 -3 447.01 17.00 2 -4 -2 1551.76 47.16 2 -4 0 158.18 8.20 2 -4 1 2.14 1.02 2 -4 2 643.74 22.31 2 -4 3 1130.72 35.67 2 -4 4 1301.39 40.29 2 -3 -13 7.72 1.20 2 -3 -12 22.62 2.33 2 -3 -12 20.60 2.26 2 -3 -11 20.38 2.43 2 -3 -11 23.83 2.65 2 -3 -10 172.52 8.31 2 -3 -10 177.56 7.92 2 -3 -10 192.15 8.78 2 -3 -10 161.43 8.31 2 -3 -9 152.68 7.92 2 -3 -9 163.26 7.92 2 -3 -9 164.63 7.55 2 -3 -9 149.68 11.67 2 -3 -9 169.84 8.24 2 -3 -8 475.86 16.23 2 -3 -8 475.77 22.05 2 -3 -8 479.90 17.01 2 -3 -8 463.18 16.64 2 -3 -8 511.26 16.97 2 -3 -8 464.96 16.85 2 -3 -8 453.04 15.97 2 -3 -7 737.75 24.51 2 -3 -7 799.93 24.73 2 -3 -7 793.28 29.90 2 -3 -7 775.78 24.62 2 -3 -7 788.41 24.83 2 -3 -6 182.69 7.92 2 -3 -6 204.27 11.32 2 -3 -5 73.57 5.94 2 -3 -5 72.91 4.66 2 -3 -4 6.21 1.34 2 -3 -4 3.75 1.40 2 -3 -3 5.06 1.51 2 -3 -3 3.92 1.14 2 -3 -2 679.28 22.22 2 -3 0 921.19 28.71 2 -3 1 306.74 11.81 2 -3 2 201.29 8.79 2 -3 3 749.99 24.10 2 -3 4 22.08 2.47 2 -2 -14 36.85 2.05 2 -2 -13 103.66 4.81 2 -2 -12 43.45 3.30 2 -2 -11 450.46 16.45 2 -2 -11 477.87 16.51 2 -2 -11 446.88 15.08 2 -2 -10 3.38 1.30 2 -2 -10 1.07 0.92 2 -2 -10 2.57 1.12 2 -2 -10 3.15 1.03 2 -2 -10 4.32 1.05 2 -2 -9 484.94 17.62 2 -2 -9 482.66 17.38 2 -2 -9 489.59 17.20 2 -2 -9 512.60 16.79 2 -2 -9 468.66 16.22 2 -2 -9 511.92 17.67 2 -2 -8 22.81 2.61 2 -2 -8 18.24 2.34 2 -2 -8 20.29 2.35 2 -2 -8 22.15 2.26 2 -2 -8 22.10 4.07 2 -2 -8 24.86 2.65 2 -2 -8 18.06 1.96 2 -2 -7 127.19 6.19 2 -2 -7 126.19 9.13 2 -2 -7 124.80 6.25 2 -2 -6 1207.83 35.15 2 -2 -6 1139.85 34.81 2 -2 -6 1238.50 39.72 2 -2 -5 1611.91 49.89 2 -2 -4 2308.03 66.13 2 -2 -4 2217.61 63.56 2 -2 -3 93.53 4.80 2 -2 -2 221.67 8.60 2 -2 -1 1483.17 42.94 2 -2 0 1050.99 31.27 2 -2 1 2.54 0.77 2 -2 2 1.62 0.69 2 -2 3 235.92 9.05 2 -2 4 89.30 4.67 2 -2 5 3938.71 108.94 2 -1 -14 61.17 2.81 2 -1 -13 19.33 1.94 2 -1 -12 2.19 1.09 2 -1 -12 1.63 0.83 2 -1 -12 1.50 0.64 2 -1 -11 21.09 2.62 2 -1 -11 21.15 2.64 2 -1 -11 18.71 2.32 2 -1 -11 19.42 2.04 2 -1 -11 20.23 2.21 2 -1 -10 284.23 11.64 2 -1 -10 273.77 11.36 2 -1 -10 275.92 11.14 2 -1 -10 264.43 10.26 2 -1 -10 258.43 10.45 2 -1 -9 388.84 14.70 2 -1 -9 381.15 14.45 2 -1 -9 379.55 14.06 2 -1 -9 390.19 13.61 2 -1 -9 405.82 14.58 2 -1 -9 389.55 13.87 2 -1 -8 263.95 10.74 2 -1 -8 264.61 10.27 2 -1 -8 263.22 9.88 2 -1 -8 262.20 10.55 2 -1 -8 248.33 9.92 2 -1 -8 270.64 10.59 2 -1 -8 271.31 10.63 2 -1 -7 435.44 15.08 2 -1 -7 471.39 20.08 2 -1 -6 160.10 9.45 2 -1 -6 154.91 6.57 2 -1 -5 927.93 30.88 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59.49 3.87 4 0 -11 70.49 3.90 4 0 -10 36.87 2.90 4 0 -10 32.90 3.11 4 0 -10 39.58 3.17 4 0 -9 339.30 13.86 4 0 -9 369.43 13.13 4 0 -9 364.00 13.75 4 0 -9 382.09 13.68 4 0 -8 33.07 3.28 4 0 -8 32.11 2.87 4 0 -8 25.49 2.92 4 0 -8 32.73 3.01 4 0 -8 38.78 3.35 4 0 -7 56.77 4.32 4 0 -7 63.55 4.37 4 0 -7 70.87 4.25 4 0 -7 60.83 4.39 4 0 -7 71.20 4.46 4 0 -7 67.94 3.86 4 0 -6 349.51 13.01 4 0 -6 360.92 12.93 4 0 -6 339.78 12.30 4 0 -6 371.34 13.18 4 0 -6 348.71 12.71 4 0 -6 344.09 11.95 4 0 -5 542.62 18.20 4 0 -5 593.64 22.93 4 0 -5 558.95 17.41 4 0 -4 25.38 3.48 4 0 -4 27.59 2.07 4 0 -3 179.76 9.12 4 0 -3 166.58 8.16 4 0 -2 54.45 4.14 4 0 -2 58.71 4.29 4 0 -1 898.04 28.19 4 0 -1 938.05 29.21 4 0 0 488.14 15.95 4 0 1 3744.02 104.94 4 0 1 3974.82 107.50 4 0 2 481.81 15.01 4 0 2 517.51 17.62 4 0 3 404.42 14.96 4 0 4 208.98 9.30 4 0 8 107.23 5.71 4 0 9 1177.77 35.77 4 0 10 77.60 4.85 4 0 11 517.90 17.47 4 1 -12 100.18 4.17 4 1 -12 102.36 4.38 4 1 -11 39.22 2.82 4 1 -11 37.24 2.82 4 1 -10 121.48 6.40 4 1 -10 113.71 5.83 4 1 -9 451.08 16.42 4 1 -9 461.89 15.35 4 1 -9 440.05 15.84 4 1 -8 105.44 6.04 4 1 -8 106.10 5.41 4 1 -8 89.83 5.49 4 1 -7 7.62 1.56 4 1 -7 6.79 1.37 4 1 -7 6.49 1.29 4 1 -7 8.91 1.40 4 1 -6 50.48 3.70 4 1 -6 49.09 3.56 4 1 -6 53.70 3.82 4 1 -6 58.80 3.48 4 1 -5 587.28 18.51 4 1 -5 544.67 17.06 4 1 -5 582.82 17.82 4 1 -4 192.00 7.15 4 1 -4 181.34 8.47 4 1 -3 605.71 21.50 4 1 -3 587.41 20.29 4 1 -2 284.89 11.50 4 1 -2 270.60 11.33 4 1 -1 656.29 21.38 4 1 -1 684.45 22.53 4 1 0 482.64 15.43 4 1 1 7.90 0.90 4 1 3 5.27 1.29 4 1 4 1301.39 39.61 4 1 5 466.37 16.71 4 1 6 809.78 26.01 4 1 8 98.10 5.42 4 1 9 14.43 2.00 4 1 10 174.04 8.11 4 1 11 7.63 1.44 4 1 12 70.03 4.18 4 2 -11 63.73 3.27 4 2 -11 57.77 3.55 4 2 -10 13.03 1.90 4 2 -10 12.13 1.69 4 2 -10 15.94 2.06 4 2 -9 15.97 2.23 4 2 -9 14.84 1.74 4 2 -9 13.61 1.96 4 2 -9 16.27 2.17 4 2 -8 247.43 10.35 4 2 -8 232.33 9.30 4 2 -8 249.39 9.81 4 2 -8 238.50 10.23 4 2 -7 258.84 10.24 4 2 -7 226.88 8.83 4 2 -7 236.07 9.53 4 2 -7 237.62 10.04 4 2 -6 336.39 12.15 4 2 -6 316.39 12.08 4 2 -6 333.74 11.22 4 2 -6 321.36 11.19 4 2 -6 335.05 11.90 4 2 -6 317.17 12.27 4 2 -5 146.81 6.63 4 2 -5 155.37 6.08 4 2 -4 833.98 24.55 4 2 -4 861.93 25.01 4 2 -4 805.43 26.83 4 2 6 1.10 0.81 4 2 10 748.78 24.46 4 2 11 87.96 5.29 4 2 12 242.03 9.64 4 3 -12 16.18 1.25 4 3 -11 163.12 6.52 4 3 -10 75.78 4.52 4 3 -10 90.10 4.79 4 3 -9 180.30 8.30 4 3 -9 196.36 8.50 4 3 -8 456.16 16.35 4 3 -8 465.52 15.50 4 3 -8 449.54 15.21 4 3 -8 483.82 16.66 4 3 -7 62.79 4.23 4 3 -7 63.51 4.34 4 3 -7 68.31 4.03 4 3 -7 68.88 4.57 4 3 -6 41.59 3.31 4 3 -6 47.72 3.63 4 3 -6 43.24 2.98 4 3 -6 41.50 3.03 4 3 -6 42.21 3.44 4 3 -5 38.42 2.97 4 3 -5 48.59 3.01 4 3 -5 43.80 3.49 4 3 -5 40.22 3.18 4 3 -5 43.64 3.01 4 3 -4 571.53 17.68 4 3 -4 569.64 17.84 4 3 -3 233.80 8.34 4 3 8 180.14 8.00 4 3 9 3.42 1.08 4 3 11 78.89 5.06 4 3 12 19.26 2.22 4 3 13 368.78 12.42 4 4 -11 67.88 3.26 4 4 -10 23.09 2.11 4 4 -9 24.43 2.44 4 4 -8 323.54 12.53 4 4 -8 335.33 12.28 4 4 -7 147.72 7.19 4 4 -7 155.10 7.46 4 4 -7 166.10 7.21 4 4 -7 164.04 7.59 4 4 -6 21.48 2.27 4 4 -6 18.97 2.40 4 4 -6 20.03 2.12 4 4 -6 19.89 2.34 4 4 -5 920.87 27.35 4 4 -5 942.57 28.89 4 4 -5 851.74 27.59 4 4 -4 474.87 15.35 4 4 -4 465.43 16.64 4 4 -4 471.06 15.29 4 4 -3 5.68 0.98 4 4 -2 114.16 4.80 4 4 10 386.51 14.11 4 4 12 29.64 2.79 4 4 13 16.46 1.76 4 5 -10 206.51 7.28 4 5 -9 127.81 5.63 4 5 -8 119.97 5.77 4 5 -8 111.84 5.59 4 5 -7 167.72 7.84 4 5 -7 166.78 7.47 4 5 -7 165.48 7.37 4 5 -6 44.71 3.35 4 5 -6 46.70 3.44 4 5 -6 46.71 3.96 4 5 -5 4.34 1.27 4 5 -4 175.74 8.59 4 5 -3 9.71 1.40 4 5 -3 8.39 1.75 4 5 -3 9.86 1.28 4 5 -2 916.10 26.83 4 5 10 65.46 4.49 4 5 12 127.13 6.31 4 5 13 114.72 5.16 4 6 -8 32.40 2.63 4 6 -7 108.44 5.88 4 6 -7 110.18 5.61 4 6 -6 19.38 2.53 4 6 -6 25.40 2.52 4 6 -5 17.41 2.12 4 6 -5 20.98 2.76 4 6 -4 1162.90 34.29 4 6 -4 1116.99 36.08 4 6 -3 124.53 5.89 4 6 -2 2.83 0.84 4 6 -2 3.47 1.18 4 6 -2 6.27 1.32 4 6 -1 8.49 1.73 4 6 -1 5.71 1.32 4 6 0 627.27 21.70 4 6 0 682.54 22.01 4 6 1 87.75 5.41 4 6 3 157.87 7.72 4 6 4 320.57 12.50 4 6 5 329.85 12.66 4 6 6 10.60 1.69 4 6 11 84.29 4.80 4 6 13 28.04 2.11 4 7 -8 297.15 10.24 4 7 -7 110.79 5.36 4 7 -6 19.34 2.42 4 7 -6 21.81 2.34 4 7 -5 1.68 0.76 4 7 -5 -0.23 0.73 4 7 -4 279.85 10.79 4 7 -4 299.07 12.54 4 7 -3 14.39 1.85 4 7 -3 13.59 1.94 4 7 -2 53.93 3.49 4 7 -2 41.05 3.97 4 7 -2 49.50 3.97 4 7 -1 510.37 19.56 4 7 -1 538.37 19.33 4 7 0 497.23 18.21 4 7 0 516.87 18.41 4 7 1 8.67 1.66 4 7 1 10.50 1.89 4 7 2 1.74 0.84 4 7 2 14.17 2.21 4 7 3 36.93 3.56 4 7 4 3.79 1.34 4 7 5 55.16 4.31 4 7 6 612.86 20.80 4 7 11 10.45 1.52 4 7 13 5.42 0.82 4 8 -6 244.84 9.61 4 8 -5 221.18 8.83 4 8 -5 216.08 9.48 4 8 -4 17.40 1.90 4 8 -3 168.54 7.17 4 8 -3 169.59 8.65 4 8 -2 47.64 3.27 4 8 -2 50.88 4.32 4 8 -2 41.77 3.68 4 8 -1 1.46 0.94 4 8 -1 1.79 1.00 4 8 0 101.93 5.05 4 8 0 111.79 6.57 4 8 0 112.65 6.62 4 8 1 1.11 0.85 4 8 1 0.48 0.93 4 8 2 617.93 20.87 4 8 3 11.14 2.01 4 8 4 485.00 17.93 4 8 5 207.82 9.62 4 8 6 144.57 7.43 4 8 7 84.54 5.13 4 8 11 94.20 4.56 4 9 -6 2.59 0.63 4 9 -6 1.70 0.61 4 9 -5 15.64 1.84 4 9 -5 15.74 1.63 4 9 -4 55.98 3.46 4 9 -3 105.20 5.99 4 9 -2 166.83 6.95 4 9 -2 191.04 8.71 4 9 -2 183.45 7.95 4 9 -1 65.48 3.69 4 9 -1 69.86 4.92 4 9 -1 69.72 4.72 4 9 0 119.48 5.33 4 9 0 120.52 6.71 4 9 0 126.42 6.84 4 9 1 196.91 9.03 4 9 1 203.81 9.48 4 9 2 134.80 6.83 4 9 3 15.14 2.39 4 9 4 54.14 4.36 4 9 5 6.64 1.49 4 9 6 136.75 6.96 4 9 7 122.25 6.07 4 9 11 0.15 0.31 4 10 -5 35.41 2.06 4 10 -4 68.46 3.27 4 10 -3 114.18 5.43 4 10 -3 111.43 4.83 4 10 -2 36.66 2.98 4 10 -1 3.29 1.02 4 10 -1 2.31 0.84 4 10 0 51.50 3.74 4 10 0 54.37 3.81 4 10 1 37.16 3.06 4 10 1 35.36 3.17 4 10 2 93.43 4.98 4 10 3 98.54 5.67 4 10 4 107.14 5.93 4 10 5 25.56 2.65 4 10 6 58.50 3.81 4 10 7 6.71 1.17 4 10 10 33.13 2.03 4 11 -2 50.51 2.70 4 11 -1 153.38 5.94 4 11 0 13.74 1.44 4 11 0 11.43 1.36 4 11 1 175.23 6.87 4 11 1 220.83 7.82 4 11 3 3.43 0.94 4 11 4 109.01 5.18 4 11 5 5.38 1.02 4 11 6 34.26 2.27 5 -9 -4 58.53 2.76 5 -9 -3 1.80 0.53 5 -9 -2 74.93 3.48 5 -9 -1 77.60 3.55 5 -9 0 0.08 0.38 5 -8 -7 41.61 2.29 5 -8 -6 23.75 1.90 5 -8 -5 1.25 0.67 5 -8 -4 125.10 5.70 5 -8 -3 4.91 1.12 5 -8 -3 4.91 1.04 5 -8 -2 2.06 0.85 5 -8 -2 3.62 0.99 5 -8 -1 2.69 0.94 5 -8 0 12.07 1.70 5 -8 0 12.54 1.79 5 -8 1 84.10 4.55 5 -8 1 79.56 4.57 5 -8 2 203.93 8.09 5 -8 2 212.60 8.31 5 -8 3 236.97 8.69 5 -8 4 29.67 2.12 5 -7 -7 87.63 4.42 5 -7 -6 41.65 3.08 5 -7 -5 11.40 1.76 5 -7 -4 64.64 4.30 5 -7 -4 62.71 3.94 5 -7 -3 220.61 9.53 5 -7 -3 230.11 9.34 5 -7 -2 212.95 9.10 5 -7 -2 206.40 9.16 5 -7 -1 78.32 5.01 5 -7 0 68.16 4.63 5 -7 0 70.75 4.72 5 -7 1 2.48 1.12 5 -7 2 0.36 0.72 5 -7 3 4.43 1.17 5 -7 3 2.83 1.07 5 -7 4 26.87 2.42 5 -7 4 29.70 2.85 5 -7 5 235.08 9.38 5 -7 6 1.83 0.77 5 -6 -9 1.40 0.62 5 -6 -8 4.22 1.01 5 -6 -7 10.43 1.48 5 -6 -6 23.69 2.35 5 -6 -5 419.04 14.65 5 -6 -4 27.22 2.94 5 -6 -4 25.56 2.56 5 -6 -4 24.31 2.54 5 -6 -3 25.25 2.92 5 -6 -3 28.53 2.70 5 -6 -3 27.70 2.87 5 -6 -2 4.34 1.35 5 -6 -2 5.82 1.50 5 -6 0 93.48 5.70 5 -6 0 92.97 5.66 5 -6 1 4.95 1.34 5 -6 1 5.30 1.31 5 -6 2 145.18 7.31 5 -6 3 161.32 7.73 5 -6 3 174.20 8.31 5 -6 4 10.70 1.93 5 -6 4 10.19 1.63 5 -6 5 105.42 5.97 5 -6 6 1.23 0.85 5 -6 7 22.94 2.32 5 -6 8 0.23 0.45 5 -5 -9 24.62 2.17 5 -5 -8 145.85 6.69 5 -5 -8 143.75 6.62 5 -5 -7 32.32 3.00 5 -5 -7 28.54 2.81 5 -5 -7 27.86 2.64 5 -5 -6 0.60 0.86 5 -5 -6 0.56 0.78 5 -5 -6 0.93 0.82 5 -5 -6 0.82 0.68 5 -5 -5 72.26 4.92 5 -5 -5 76.27 4.81 5 -5 -5 65.31 4.21 5 -5 -4 164.48 7.86 5 -5 -4 155.41 7.04 5 -5 -4 181.93 7.76 5 -5 -3 6.53 1.42 5 -5 -3 3.93 1.20 5 -5 -2 121.16 6.64 5 -5 -2 115.86 6.14 5 -5 -2 103.23 9.00 5 -5 -2 113.91 6.23 5 -5 -1 313.99 11.97 5 -5 -1 313.64 16.76 5 -5 -1 316.21 12.34 5 -5 -1 317.76 12.22 5 -5 -1 292.12 16.07 5 -5 0 16.97 2.10 5 -5 0 15.09 3.31 5 -5 0 14.83 2.22 5 -5 0 16.09 2.21 5 -5 1 16.58 3.40 5 -5 1 19.10 2.47 5 -5 1 18.36 2.39 5 -5 1 21.36 3.89 5 -5 2 5.37 1.34 5 -5 2 4.10 1.30 5 -5 2 4.39 1.88 5 -5 3 14.87 2.06 5 -5 4 20.37 2.39 5 -5 4 20.22 2.56 5 -5 5 164.54 8.02 5 -5 6 802.32 25.93 5 -5 7 144.33 7.05 5 -5 8 3.45 1.03 5 -5 9 61.93 3.57 5 -4 -9 111.95 5.40 5 -4 -8 13.09 1.90 5 -4 -8 10.69 1.84 5 -4 -8 15.86 2.01 5 -4 -8 11.82 1.87 5 -4 -8 12.70 2.38 5 -4 -7 58.44 4.16 5 -4 -7 58.40 4.29 5 -4 -7 55.51 3.92 5 -4 -7 48.73 3.91 5 -4 -7 60.30 4.25 5 -4 -6 84.48 5.32 5 -4 -6 92.55 5.60 5 -4 -6 91.01 5.09 5 -4 -6 71.70 4.90 5 -4 -6 91.66 5.21 5 -4 -5 41.77 3.69 5 -4 -5 45.18 3.84 5 -4 -5 52.60 3.66 5 -4 -5 39.13 3.37 5 -4 -4 51.88 4.04 5 -4 -4 50.36 3.94 5 -4 -4 40.67 3.18 5 -4 -4 42.29 5.69 5 -4 -4 49.15 3.53 5 -4 -3 133.09 6.97 5 -4 -3 132.61 6.82 5 -4 -3 128.37 9.79 5 -4 -3 143.48 6.70 5 -4 -3 130.16 6.43 5 -4 -2 11.35 1.80 5 -4 -2 16.41 3.30 5 -4 -2 14.29 1.98 5 -4 -2 11.37 1.72 5 -4 -2 11.67 1.73 5 -4 -1 67.75 4.48 5 -4 -1 70.89 6.87 5 -4 -1 72.02 4.54 5 -4 -1 63.14 4.11 5 -4 -1 71.94 4.41 5 -4 -1 77.04 7.03 5 -4 0 0.69 0.64 5 -4 0 1.89 0.81 5 -4 0 1.23 0.73 5 -4 0 2.12 1.33 5 -4 0 0.91 0.73 5 -4 1 306.90 15.68 5 -4 1 341.92 12.58 5 -4 1 338.13 11.99 5 -4 1 333.79 12.53 5 -4 1 318.60 16.15 5 -4 2 215.73 9.40 5 -4 2 227.18 9.30 5 -4 2 207.95 8.58 5 -4 2 230.47 9.46 5 -4 3 84.55 5.16 5 -4 3 77.95 4.74 5 -4 3 77.45 4.35 5 -4 4 271.97 10.98 5 -4 4 252.60 10.35 5 -4 4 289.71 11.22 5 -4 5 18.69 2.31 5 -4 5 16.08 2.22 5 -4 6 9.29 1.78 5 -4 6 8.17 1.57 5 -4 7 36.59 3.10 5 -4 7 36.39 3.31 5 -4 8 69.19 4.51 5 -4 9 11.88 1.70 5 -4 10 338.10 11.56 5 -3 -10 89.16 4.58 5 -3 -9 17.29 2.11 5 -3 -9 25.21 2.99 5 -3 -8 4.14 1.17 5 -3 -8 2.92 1.11 5 -3 -8 4.24 1.22 5 -3 -8 4.92 1.31 5 -3 -7 175.97 8.21 5 -3 -7 182.97 8.67 5 -3 -7 186.78 8.22 5 -3 -7 166.53 8.39 5 -3 -7 206.39 8.70 5 -3 -7 183.26 7.65 5 -3 -6 3.91 1.22 5 -3 -6 5.76 1.47 5 -3 -6 6.94 1.46 5 -3 -6 4.57 1.27 5 -3 -6 6.41 1.27 5 -3 -5 2.15 0.90 5 -3 -5 1.87 0.89 5 -3 -5 1.79 0.87 5 -3 -5 1.05 1.30 5 -3 -5 0.77 0.77 5 -3 -5 4.64 2.22 5 -3 -4 47.82 3.77 5 -3 -4 48.90 3.84 5 -3 -4 45.99 3.27 5 -3 -4 42.32 5.44 5 -3 -4 36.63 3.18 5 -3 -4 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154.80 7.15 6 2 -7 6.06 1.27 6 2 -7 7.98 1.95 6 2 -7 6.02 1.39 6 2 -6 15.15 2.42 6 2 -6 11.98 1.89 6 2 -5 13.11 2.35 6 2 -5 9.28 1.75 6 2 -4 156.11 6.20 6 2 -4 143.54 7.15 6 2 -4 156.29 6.87 6 2 -3 210.27 8.52 6 2 -3 202.44 8.77 6 2 -3 228.39 8.63 6 2 -3 212.27 11.30 6 2 -2 441.19 15.08 6 2 -2 441.69 15.10 6 2 -2 443.41 18.54 6 2 -1 56.33 5.43 6 2 0 444.44 18.81 6 2 2 76.70 6.51 6 2 3 86.60 6.83 6 2 4 865.75 30.83 6 2 5 121.15 8.45 6 2 5 143.42 6.64 6 2 6 229.45 9.58 6 2 6 201.22 11.24 6 2 6 219.78 9.37 6 2 7 90.66 5.52 6 2 7 95.58 5.63 6 2 8 88.82 5.45 6 2 9 67.03 4.79 6 2 10 9.86 1.81 6 2 10 6.42 1.37 6 2 11 4.67 1.18 6 2 12 127.28 6.03 6 2 13 290.66 9.93 6 3 -10 1.48 0.51 6 3 -9 20.08 1.90 6 3 -8 177.34 7.17 6 3 -8 187.82 7.75 6 3 -7 175.23 7.59 6 3 -7 195.05 8.29 6 3 -6 47.24 3.04 6 3 -6 44.93 3.63 6 3 -6 49.86 3.50 6 3 -5 164.36 6.80 6 3 -5 153.88 7.57 6 3 -5 176.89 7.47 6 3 -4 505.94 17.93 6 3 -4 482.37 15.99 6 3 -4 480.06 16.97 6 3 -4 524.89 16.73 6 3 -3 60.11 4.44 6 3 -3 48.78 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134.39 6.26 6 5 11 118.90 6.35 6 5 12 56.72 3.65 6 5 13 31.68 2.22 6 6 -6 3.98 1.12 6 6 -5 149.34 7.50 6 6 -5 147.75 6.52 6 6 -4 70.31 5.14 6 6 -4 74.92 4.33 6 6 -3 196.12 8.30 6 6 -2 46.48 4.24 6 6 -2 48.14 3.82 6 6 -1 521.36 19.64 6 6 -1 569.15 19.29 6 6 0 297.99 12.65 6 6 0 309.88 12.55 6 6 1 34.32 3.44 6 6 1 40.05 3.71 6 6 2 0.21 0.57 6 6 3 64.16 4.82 6 6 4 22.93 2.84 6 6 5 636.84 21.78 6 6 6 0.21 1.04 6 6 7 188.82 8.47 6 6 8 46.60 4.05 6 6 9 389.58 14.81 6 6 10 15.97 2.18 6 6 11 76.79 4.48 6 6 11 83.24 4.82 6 6 12 81.70 4.30 6 6 13 26.59 1.83 6 7 -5 183.30 7.98 6 7 -5 168.45 6.97 6 7 -4 69.58 4.82 6 7 -3 52.18 3.47 6 7 -2 0.45 0.47 6 7 -2 0.25 0.73 6 7 -2 0.37 0.58 6 7 -1 213.36 8.56 6 7 -1 211.23 9.97 6 7 -1 198.59 9.29 6 7 0 204.54 9.71 6 7 0 199.35 9.45 6 7 1 290.35 12.07 6 7 1 280.78 12.14 6 7 2 153.52 7.71 6 7 3 46.49 4.15 6 7 4 74.44 5.31 6 7 5 365.48 14.30 6 7 6 19.00 2.49 6 7 7 305.66 11.89 6 7 8 30.41 3.24 6 7 9 49.73 3.90 6 7 10 5.35 1.21 6 7 11 138.38 5.99 6 7 11 132.09 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4.95 1.38 7 -1 5 7.20 1.23 7 -1 6 24.60 2.79 7 -1 6 31.35 3.05 7 -1 7 181.65 8.42 7 -1 8 146.76 7.14 7 -1 8 146.41 7.29 7 -1 9 41.03 3.23 7 -1 9 43.57 3.53 7 -1 10 200.20 7.82 7 -1 10 208.99 8.51 7 -1 11 93.98 4.61 7 -1 12 83.33 3.66 7 0 -9 34.38 2.23 7 0 -7 485.01 16.53 7 0 -7 520.74 16.63 7 0 -6 101.83 5.59 7 0 -6 109.80 5.51 7 0 -6 96.60 4.92 7 0 -5 63.19 4.41 7 0 -5 65.08 4.17 7 0 -5 62.25 3.87 7 0 -4 23.74 2.68 7 0 -4 23.54 2.48 7 0 -4 19.91 2.18 7 0 -4 22.48 2.14 7 0 -3 75.35 4.98 7 0 -3 68.14 4.24 7 0 -3 77.24 4.32 7 0 -2 479.53 17.09 7 0 -1 76.78 5.03 7 0 0 1110.32 33.32 7 0 1 85.97 4.93 7 0 2 151.87 7.18 7 0 3 66.02 4.42 7 0 3 63.15 4.05 7 0 4 22.81 2.60 7 0 4 21.70 2.35 7 0 5 5.35 1.27 7 0 5 3.87 1.18 7 0 6 40.73 3.56 7 0 6 35.74 3.27 7 0 7 441.36 16.26 7 0 7 462.27 16.37 7 0 8 470.06 16.69 7 0 9 41.85 3.36 7 0 9 40.78 3.45 7 0 10 91.17 4.83 7 0 10 94.97 5.26 7 0 11 51.86 3.46 7 0 12 212.09 7.71 7 1 -9 28.52 1.95 7 1 -8 178.25 6.99 7 1 -8 173.38 7.18 7 1 -7 18.91 2.17 7 1 -6 51.92 3.61 7 1 -6 58.43 3.85 7 1 -6 55.33 3.99 7 1 -6 61.79 3.73 7 1 -5 738.70 24.50 7 1 -5 796.53 24.62 7 1 -5 782.26 25.07 7 1 -5 790.36 24.32 7 1 -4 236.94 9.81 7 1 -4 232.42 9.95 7 1 -4 243.55 9.47 7 1 -4 229.87 8.78 7 1 -3 185.00 8.44 7 1 -3 194.21 8.63 7 1 -2 64.41 4.42 7 1 -1 51.94 3.94 7 1 -1 57.11 4.00 7 1 -1 50.83 5.73 7 1 0 43.27 3.44 7 1 0 39.80 5.00 7 1 1 93.24 5.08 7 1 2 306.23 11.65 7 1 2 311.49 11.93 7 1 2 298.54 15.38 7 1 3 681.56 21.86 7 1 3 652.41 21.80 7 1 3 703.66 26.71 7 1 3 651.94 21.00 7 1 4 180.80 8.31 7 1 4 178.72 8.20 7 1 4 177.57 11.25 7 1 4 188.60 7.98 7 1 5 552.51 18.44 7 1 5 531.48 18.30 7 1 6 120.69 6.65 7 1 6 131.36 6.69 7 1 7 61.68 4.45 7 1 7 60.14 4.39 7 1 8 -0.21 0.60 7 1 9 187.20 8.36 7 1 9 175.05 8.36 7 1 10 113.64 5.79 7 1 10 118.91 6.21 7 1 11 122.67 5.96 7 1 12 125.31 5.47 7 1 13 45.61 2.32 7 2 -8 60.94 3.38 7 2 -8 65.26 3.68 7 2 -7 85.93 4.51 7 2 -7 82.02 4.65 7 2 -6 161.29 7.47 7 2 -5 154.75 7.42 7 2 -4 243.06 10.36 7 2 -4 269.44 10.19 7 2 -3 38.84 3.15 7 2 -3 37.40 3.07 7 2 -3 36.58 3.23 7 2 -3 45.23 3.28 7 2 -2 304.93 11.86 7 2 -2 333.48 12.22 7 2 -2 328.12 11.82 7 2 -2 320.64 15.74 7 2 -1 141.97 6.89 7 2 -1 144.16 7.04 7 2 -1 148.68 10.05 7 2 0 616.57 20.66 7 2 0 653.23 21.17 7 2 0 642.79 25.56 7 2 1 655.29 20.95 7 2 1 654.30 21.65 7 2 2 253.80 10.48 7 2 2 253.33 13.86 7 2 3 60.80 4.25 7 2 3 56.98 6.09 7 2 4 17.01 2.21 7 2 4 18.12 3.43 7 2 4 21.24 2.27 7 2 5 4.87 1.17 7 2 5 1.73 1.27 7 2 5 2.22 0.96 7 2 6 147.45 7.07 7 2 6 141.17 9.71 7 2 6 157.54 7.50 7 2 7 353.58 13.59 7 2 8 253.30 10.78 7 2 9 522.28 18.16 7 2 10 4.98 1.30 7 2 10 4.11 1.11 7 2 11 288.56 10.49 7 2 11 300.30 11.22 7 2 12 48.14 3.14 7 2 13 24.23 1.73 7 3 -8 6.02 0.93 7 3 -8 7.11 1.10 7 3 -7 22.21 2.08 7 3 -7 21.67 2.15 7 3 -6 26.29 2.45 7 3 -6 23.82 2.46 7 3 -5 211.58 9.00 7 3 -5 220.36 8.77 7 3 -4 118.09 5.23 7 3 -4 107.72 5.89 7 3 -4 115.35 5.72 7 3 -3 1094.45 32.43 7 3 -3 1083.35 33.15 7 3 -3 1113.83 33.65 7 3 -3 1131.11 33.26 7 3 -2 71.77 4.60 7 3 -2 79.22 4.65 7 3 -2 78.62 4.45 7 3 -2 64.39 6.36 7 3 -1 432.15 15.26 7 3 -1 420.40 14.40 7 3 -1 405.33 19.06 7 3 0 125.68 6.54 7 3 0 117.59 9.11 7 3 1 83.91 5.22 7 3 1 79.77 7.47 7 3 2 86.17 5.02 7 3 2 88.46 5.32 7 3 2 74.95 7.32 7 3 3 141.69 7.27 7 3 3 131.25 9.87 7 3 4 988.41 31.02 7 3 4 979.99 30.92 7 3 4 1004.63 36.13 7 3 4 991.21 30.16 7 3 5 95.93 5.87 7 3 5 100.33 5.68 7 3 5 99.12 8.18 7 3 5 99.54 5.55 7 3 6 194.43 8.47 7 3 6 176.19 11.26 7 3 6 189.98 8.64 7 3 7 72.26 5.08 7 3 7 71.04 4.87 7 3 8 46.90 4.01 7 3 8 47.92 4.00 7 3 9 1.69 0.91 7 3 10 52.08 3.79 7 3 11 382.37 13.28 7 3 11 394.99 13.92 7 3 12 193.34 7.68 7 3 13 63.67 3.12 7 4 -7 151.09 6.17 7 4 -7 167.69 6.43 7 4 -6 72.10 4.11 7 4 -6 79.15 4.22 7 4 -5 106.03 4.92 7 4 -5 107.22 5.39 7 4 -4 1.67 0.67 7 4 -4 1.87 0.83 7 4 -4 2.35 0.91 7 4 -3 39.13 2.94 7 4 -3 50.44 3.47 7 4 -3 47.86 3.40 7 4 -3 45.04 3.23 7 4 -2 0.99 0.95 7 4 -2 1.01 0.68 7 4 -2 -0.18 0.45 7 4 -1 408.53 15.75 7 4 -1 418.46 15.06 7 4 -1 406.42 13.91 7 4 -1 394.24 19.01 7 4 0 554.25 19.42 7 4 0 556.05 18.95 7 4 0 537.29 17.40 7 4 0 499.82 23.12 7 4 1 688.65 22.46 7 4 1 599.85 26.64 7 4 2 297.34 11.26 7 4 2 255.26 15.17 7 4 3 356.26 13.31 7 4 3 343.26 13.47 7 4 3 338.08 17.68 7 4 4 23.20 2.69 7 4 4 22.65 2.69 7 4 4 18.33 3.66 7 4 5 82.29 5.35 7 4 5 82.67 5.17 7 4 5 78.08 7.47 7 4 5 70.02 4.65 7 4 6 25.09 2.66 7 4 6 24.32 2.77 7 4 7 535.31 18.86 7 4 7 501.36 17.47 7 4 7 524.78 18.35 7 4 8 51.95 4.21 7 4 8 53.79 4.26 7 4 9 154.68 7.79 7 4 9 157.51 7.82 7 4 11 70.40 4.07 7 4 11 66.64 4.28 7 4 12 48.15 2.75 7 4 12 55.15 3.35 7 4 13 0.62 0.40 7 5 -6 5.71 1.02 7 5 -5 322.82 11.13 7 5 -4 8.22 1.29 7 5 -3 584.66 18.82 7 5 -3 589.05 18.75 7 5 -2 153.92 8.23 7 5 -2 154.78 7.34 7 5 -2 155.38 6.64 7 5 -1 190.44 9.53 7 5 -1 201.52 9.07 7 5 -1 204.60 7.93 7 5 0 2.92 1.15 7 5 0 5.11 0.98 7 5 0 6.34 1.48 7 5 1 2.08 1.03 7 5 1 2.05 0.95 7 5 2 21.87 2.41 7 5 3 204.45 9.22 7 5 3 212.70 9.75 7 5 4 565.95 20.12 7 5 4 599.77 20.45 7 5 5 812.56 26.93 7 5 5 853.57 26.79 7 5 5 792.82 25.83 7 5 6 24.29 2.88 7 5 6 16.45 2.26 7 5 6 20.15 2.44 7 5 7 41.14 3.36 7 5 7 37.48 3.48 7 5 8 26.56 3.03 7 5 8 26.35 2.93 7 5 9 23.35 2.71 7 5 9 18.98 2.39 7 5 10 47.28 3.63 7 5 10 47.59 3.66 7 5 12 74.61 3.57 7 5 12 89.34 4.24 7 5 13 110.05 4.27 7 6 -5 74.88 3.81 7 6 -4 2.13 0.68 7 6 -3 23.38 2.20 7 6 -2 62.37 4.92 7 6 -2 75.38 4.24 7 6 -2 77.37 4.65 7 6 -1 326.56 13.93 7 6 -1 374.52 13.66 7 6 0 26.77 3.13 7 6 0 33.39 3.29 7 6 1 352.54 14.05 7 6 1 363.93 14.25 7 6 2 43.55 3.74 7 6 2 36.33 3.15 7 6 3 101.48 5.86 7 6 3 104.11 6.40 7 6 4 35.96 3.42 7 6 4 36.52 3.56 7 6 5 44.37 3.91 7 6 5 46.11 3.95 7 6 6 85.66 5.63 7 6 6 88.32 5.45 7 6 7 22.35 2.47 7 6 8 478.77 17.14 7 6 8 454.31 16.50 7 6 9 272.98 10.78 7 6 9 239.20 10.21 7 6 10 81.26 4.67 7 6 10 74.65 4.54 7 6 12 18.04 1.40 7 6 12 23.58 1.84 7 7 -4 201.64 7.58 7 7 -3 160.89 7.73 7 7 -2 172.34 8.37 7 7 -1 23.50 2.81 7 7 -1 22.55 2.19 7 7 -1 23.42 2.55 7 7 0 14.48 2.23 7 7 0 13.65 2.11 7 7 1 33.82 3.36 7 7 1 39.92 3.65 7 7 2 30.71 3.06 7 7 3 247.83 10.07 7 7 3 236.80 10.70 7 7 4 108.48 6.11 7 7 4 108.10 6.47 7 7 5 66.27 4.72 7 7 5 68.95 4.87 7 7 6 495.06 17.89 7 7 6 510.54 17.65 7 7 7 25.99 2.90 7 7 7 29.97 2.75 7 7 8 69.94 4.41 7 7 9 26.65 2.63 7 7 9 21.57 2.27 7 7 10 33.98 2.70 7 7 10 29.59 2.53 7 7 11 31.82 2.33 7 8 -3 4.81 0.85 7 8 -3 3.54 1.04 7 8 -2 6.13 1.06 7 8 -2 7.85 1.44 7 8 -1 47.71 3.73 7 8 -1 54.38 3.22 7 8 0 93.60 5.47 7 8 0 99.11 4.70 7 8 0 89.82 5.25 7 8 1 291.55 11.39 7 8 1 290.29 11.62 7 8 2 49.51 3.64 7 8 3 171.58 8.28 7 8 4 6.24 1.25 7 8 4 5.17 1.37 7 8 5 11.12 1.73 7 8 5 13.38 1.97 7 8 6 2.90 1.01 7 8 6 1.21 0.79 7 8 7 122.43 6.28 7 8 7 128.55 5.94 7 8 9 110.97 5.25 7 8 9 98.25 4.76 7 8 10 28.30 2.17 7 8 10 27.39 2.02 7 8 11 23.08 1.56 7 9 -2 116.18 4.61 7 9 -1 40.12 2.84 7 9 -1 38.89 2.37 7 9 0 77.52 4.23 7 9 0 76.61 3.66 7 9 0 74.65 4.10 7 9 1 2.56 0.66 7 9 1 2.09 0.71 7 9 1 1.64 0.86 7 9 2 32.39 2.24 7 9 2 34.73 2.95 7 9 3 44.88 2.66 7 9 3 41.34 3.34 7 9 4 30.98 2.78 7 9 5 41.23 3.15 7 9 6 46.90 3.17 7 9 6 44.72 3.11 7 9 7 95.40 4.69 7 9 7 90.91 4.29 7 9 8 13.07 1.50 7 10 1 55.72 2.96 7 10 2 58.87 3.27 7 10 4 17.63 1.70 7 10 5 0.49 0.47 7 10 6 4.78 0.79 8 -6 -3 3.64 0.64 8 -6 -2 54.59 2.88 8 -6 -1 1.51 0.59 8 -6 0 22.86 1.92 8 -6 3 31.29 2.22 8 -6 4 114.87 4.70 8 -6 5 4.23 0.71 8 -5 -5 2.23 0.54 8 -5 -4 7.71 1.05 8 -5 -3 60.74 3.33 8 -5 -3 59.82 3.27 8 -5 -2 115.12 5.26 8 -5 -2 114.54 5.11 8 -5 -1 23.24 2.22 8 -5 -1 26.02 2.20 8 -5 0 197.26 7.99 8 -5 0 190.87 7.57 8 -5 1 14.46 1.86 8 -5 1 12.49 1.55 8 -5 2 14.86 1.91 8 -5 2 10.87 1.40 8 -5 3 24.52 2.02 8 -5 3 27.44 2.26 8 -5 4 153.34 6.01 8 -5 4 169.19 6.67 8 -5 5 62.94 3.48 8 -5 6 39.10 2.50 8 -5 7 17.93 1.45 8 -4 -6 3.55 0.71 8 -4 -5 68.21 3.63 8 -4 -4 14.11 1.67 8 -4 -3 110.95 5.47 8 -4 -2 36.18 2.90 8 -4 -2 37.84 3.01 8 -4 -1 0.16 0.56 8 -4 -1 0.82 0.73 8 -4 0 206.29 8.76 8 -4 0 208.46 8.75 8 -4 1 51.05 3.69 8 -4 2 358.87 13.00 8 -4 3 28.54 2.66 8 -4 3 23.20 2.33 8 -4 4 84.83 4.67 8 -4 4 82.35 4.67 8 -4 5 3.18 0.98 8 -4 5 3.30 0.91 8 -4 6 9.30 1.41 8 -4 6 8.91 1.29 8 -4 7 14.01 1.37 8 -4 8 34.04 2.27 8 -3 -6 0.71 0.41 8 -3 -5 37.93 2.86 8 -3 -5 32.77 2.19 8 -3 -4 453.03 15.49 8 -3 -3 17.61 2.21 8 -3 -2 186.67 8.08 8 -3 -2 194.01 8.63 8 -3 -2 192.07 7.37 8 -3 -2 205.23 8.17 8 -3 -1 61.05 4.16 8 -3 -1 70.19 4.63 8 -3 0 8.43 1.61 8 -3 0 9.19 1.79 8 -3 0 11.43 1.77 8 -3 1 27.23 2.92 8 -3 1 33.31 2.84 8 -3 2 4.99 1.13 8 -3 2 4.61 1.25 8 -3 2 5.39 1.44 8 -3 2 4.74 1.18 8 -3 3 0.66 0.69 8 -3 3 0.58 0.68 8 -3 3 0.86 0.71 8 -3 4 59.44 4.24 8 -3 4 53.10 3.45 8 -3 4 60.77 4.03 8 -3 5 34.51 3.16 8 -3 5 40.37 3.23 8 -3 6 548.74 18.45 8 -3 6 559.63 18.41 8 -3 7 31.69 2.69 8 -3 7 34.11 2.79 8 -3 9 55.84 3.10 8 -2 -7 175.83 6.54 8 -2 -7 174.65 6.28 8 -2 -6 117.82 5.44 8 -2 -6 120.63 5.05 8 -2 -5 171.24 7.32 8 -2 -5 158.11 6.50 8 -2 -4 0.70 0.58 8 -2 -4 1.47 0.58 8 -2 -3 26.16 2.23 8 -2 -3 29.23 2.38 8 -2 -3 31.30 2.63 8 -2 -2 23.40 2.33 8 -2 -1 3.22 1.00 8 -2 -1 5.75 1.48 8 -2 -1 4.68 1.16 8 -2 0 142.62 6.95 8 -2 0 150.72 7.57 8 -2 0 154.83 6.92 8 -2 1 424.84 15.42 8 -2 1 444.65 16.08 8 -2 1 424.21 14.97 8 -2 2 42.28 3.61 8 -2 2 44.05 3.33 8 -2 2 44.40 3.33 8 -2 3 12.17 1.79 8 -2 3 11.66 1.90 8 -2 3 14.61 1.87 8 -2 4 227.14 9.00 8 -2 4 237.81 9.67 8 -2 5 109.70 5.99 8 -2 5 94.90 4.86 8 -2 5 110.71 5.82 8 -2 6 2.11 0.92 8 -2 6 1.30 0.82 8 -2 7 61.91 4.10 8 -2 7 63.58 4.13 8 -2 8 87.40 4.68 8 -2 9 58.97 3.31 8 -2 9 58.48 3.52 8 -2 10 95.58 4.32 8 -1 -8 31.97 1.89 8 -1 -7 144.67 5.68 8 -1 -6 5.49 1.11 8 -1 -6 6.52 1.13 8 -1 -5 4.35 1.13 8 -1 -5 3.80 1.05 8 -1 -5 4.09 0.86 8 -1 -4 9.93 1.72 8 -1 -4 11.14 1.53 8 -1 -4 13.23 1.60 8 -1 -4 10.99 1.46 8 -1 -3 347.52 13.16 8 -1 -3 347.46 12.00 8 -1 -3 328.74 11.96 8 -1 -3 339.86 12.10 8 -1 -2 41.72 3.64 8 -1 -2 37.72 2.81 8 -1 -2 38.93 3.05 8 -1 -1 173.06 8.46 8 -1 -1 177.42 7.72 8 -1 0 97.40 5.33 8 -1 0 94.13 5.90 8 -1 1 474.87 16.32 8 -1 1 450.92 15.85 8 -1 2 634.28 20.60 8 -1 2 586.33 19.74 8 -1 3 37.39 3.38 8 -1 3 29.43 2.71 8 -1 3 37.25 3.06 8 -1 4 278.45 11.55 8 -1 4 285.15 10.64 8 -1 4 288.78 11.12 8 -1 5 133.03 6.99 8 -1 5 133.44 6.06 8 -1 5 141.24 6.86 8 -1 6 71.64 4.78 8 -1 6 69.35 4.54 8 -1 7 199.99 8.81 8 -1 7 200.89 8.73 8 -1 8 91.88 5.10 8 -1 8 92.59 5.14 8 -1 9 50.06 3.34 8 -1 10 5.83 1.09 8 -1 10 3.24 0.78 8 -1 11 34.14 2.17 8 0 -8 61.31 2.92 8 0 -7 68.28 3.53 8 0 -6 50.34 3.18 8 0 -6 52.87 3.04 8 0 -5 77.28 4.55 8 0 -5 81.96 4.42 8 0 -5 80.17 4.23 8 0 -4 54.00 3.90 8 0 -4 53.20 3.53 8 0 -4 50.85 3.38 8 0 -3 2.54 1.08 8 0 -3 1.64 0.81 8 0 -3 2.66 0.88 8 0 -3 1.37 0.70 8 0 -2 35.47 3.30 8 0 -2 35.55 2.86 8 0 -2 42.73 3.14 8 0 -1 0.65 0.79 8 0 -1 0.28 0.53 8 0 -1 0.48 0.62 8 0 0 246.85 9.84 8 0 0 260.77 10.93 8 0 1 164.99 7.56 8 0 2 286.25 11.33 8 0 3 157.42 7.56 8 0 3 146.83 6.80 8 0 4 8.66 1.48 8 0 4 4.74 1.36 8 0 5 377.48 13.78 8 0 6 2.61 1.02 8 0 6 1.65 0.97 8 0 7 170.25 8.10 8 0 7 174.17 7.97 8 0 8 252.43 10.08 8 0 8 238.46 9.93 8 0 9 40.21 3.11 8 0 10 136.27 5.86 8 0 10 142.31 6.28 8 0 11 81.13 3.99 8 1 -7 21.30 1.84 8 1 -6 25.57 2.20 8 1 -6 19.53 1.89 8 1 -5 10.86 1.57 8 1 -5 9.64 1.40 8 1 -4 24.26 2.43 8 1 -4 19.63 2.21 8 1 -4 19.11 2.08 8 1 -3 393.85 14.28 8 1 -3 398.49 13.50 8 1 -2 27.71 2.84 8 1 -1 295.76 11.82 8 1 0 32.28 3.20 8 1 1 387.31 13.86 8 1 2 181.88 8.21 8 1 3 364.82 13.74 8 1 4 344.47 13.31 8 1 4 343.97 12.54 8 1 5 171.66 8.36 8 1 5 180.70 7.99 8 1 6 99.28 5.89 8 1 6 93.31 5.46 8 1 7 58.46 4.32 8 1 7 54.48 4.01 8 1 8 110.35 6.00 8 1 8 99.24 5.67 8 1 9 100.88 5.49 8 1 9 109.71 5.72 8 1 10 16.24 1.88 8 1 11 52.58 2.89 8 1 11 59.68 3.38 8 1 12 3.02 0.67 8 2 -8 4.44 0.67 8 2 -5 37.78 2.92 8 2 -4 19.14 2.07 8 2 -3 248.96 9.72 8 2 -2 45.61 3.44 8 2 -2 48.95 3.47 8 2 -1 143.59 7.03 8 2 -1 152.17 7.39 8 2 -1 153.50 6.93 8 2 0 2.41 0.95 8 2 0 3.24 1.15 8 2 1 772.83 24.06 8 2 1 736.35 24.48 8 2 1 778.19 25.07 8 2 2 31.64 2.96 8 2 2 29.09 3.06 8 2 3 444.93 16.14 8 2 3 464.69 16.57 8 2 4 2.48 1.15 8 2 4 2.69 1.08 8 2 5 32.67 3.22 8 2 5 31.49 3.12 8 2 5 29.47 2.78 8 2 6 56.21 4.06 8 2 7 0.38 0.74 8 2 7 2.55 1.20 8 2 8 89.79 5.49 8 2 8 96.40 5.50 8 2 9 176.05 7.84 8 2 9 162.32 7.63 8 2 10 25.61 2.38 8 2 11 61.33 3.36 8 2 11 68.52 3.77 8 2 12 163.63 6.13 8 3 -7 128.95 5.06 8 3 -6 0.11 0.50 8 3 -5 1.61 0.73 8 3 -4 4.85 1.09 8 3 -3 351.04 12.47 8 3 -2 250.22 9.20 8 3 -2 251.21 10.20 8 3 -2 277.13 10.14 8 3 -1 4.60 1.14 8 3 -1 6.73 1.44 8 3 0 35.29 3.31 8 3 0 39.14 3.00 8 3 1 8.09 1.70 8 3 2 36.17 3.12 8 3 3 102.45 5.80 8 3 3 100.43 6.04 8 3 4 296.73 12.04 8 3 5 538.00 18.41 8 3 5 515.05 17.63 8 3 6 5.90 1.35 8 3 6 4.54 1.28 8 3 7 338.68 12.90 8 3 8 157.63 7.68 8 3 8 148.92 7.34 8 3 9 49.48 3.69 8 3 9 39.37 3.34 8 3 10 1.25 0.73 8 3 10 0.75 0.62 8 3 11 170.85 6.70 8 3 12 58.18 3.04 8 4 -6 171.28 6.52 8 4 -5 131.37 5.78 8 4 -4 186.14 7.44 8 4 -3 8.92 1.27 8 4 -3 10.61 1.51 8 4 -2 110.58 5.15 8 4 -2 111.04 5.72 8 4 -2 107.34 5.30 8 4 -1 89.67 5.31 8 4 -1 86.82 4.63 8 4 0 6.37 1.18 8 4 0 6.03 1.41 8 4 1 172.41 8.30 8 4 1 162.13 6.92 8 4 2 12.39 1.80 8 4 3 40.85 3.70 8 4 4 305.97 12.42 8 4 5 92.67 5.81 8 4 5 96.93 5.71 8 4 5 88.53 5.01 8 4 6 15.96 2.31 8 4 6 16.37 2.19 8 4 6 15.51 2.07 8 4 7 29.28 2.72 8 4 7 24.14 2.65 8 4 8 62.09 4.28 8 4 9 212.00 8.93 8 4 10 260.64 9.90 8 4 10 251.79 9.86 8 4 11 13.65 1.50 8 4 12 53.22 2.82 8 5 -5 35.89 2.46 8 5 -3 38.84 2.60 8 5 -3 35.10 2.57 8 5 -2 36.88 2.70 8 5 -2 35.20 2.58 8 5 -1 468.99 16.34 8 5 -1 462.62 15.08 8 5 0 128.53 6.71 8 5 0 119.27 5.40 8 5 1 19.10 2.53 8 5 3 251.01 10.22 8 5 3 242.72 10.75 8 5 4 82.32 5.23 8 5 4 82.14 5.39 8 5 5 296.20 12.19 8 5 5 308.61 12.21 8 5 6 181.82 8.54 8 5 6 175.76 8.07 8 5 6 158.39 7.42 8 5 7 38.34 3.52 8 5 7 38.46 3.18 8 5 7 35.29 3.07 8 5 8 4.45 1.14 8 5 8 3.80 1.18 8 5 9 169.97 7.49 8 5 10 18.41 2.00 8 5 11 20.36 1.80 8 5 11 20.93 1.88 8 6 -4 240.18 8.26 8 6 -3 27.48 2.13 8 6 -2 22.20 2.00 8 6 -1 111.94 5.23 8 6 -1 104.62 5.60 8 6 0 37.97 3.31 8 6 1 219.05 9.72 8 6 3 29.75 3.18 8 6 4 139.95 7.05 8 6 4 145.39 7.47 8 6 5 45.02 3.77 8 6 5 53.37 4.04 8 6 6 5.70 1.38 8 6 6 6.64 1.47 8 6 7 2.37 1.01 8 6 7 4.68 1.08 8 6 8 55.77 3.68 8 6 9 24.64 2.44 8 6 9 23.87 2.25 8 6 10 51.12 3.13 8 6 11 113.52 4.56 8 6 11 99.89 4.41 8 7 -3 85.48 3.88 8 7 -2 159.81 6.29 8 7 0 365.05 13.19 8 7 1 86.96 5.18 8 7 3 0.40 0.78 8 7 4 13.25 2.04 8 7 5 198.44 8.60 8 7 5 207.91 8.93 8 7 6 167.52 7.83 8 7 6 191.17 7.99 8 7 7 80.02 4.69 8 7 7 71.62 4.13 8 7 9 6.82 1.22 8 8 -1 3.29 0.70 8 8 0 11.54 1.31 8 8 0 9.76 1.43 8 8 1 53.67 3.04 8 8 1 53.78 3.57 8 8 2 233.12 9.38 8 8 3 83.18 4.83 8 8 4 63.26 4.09 8 8 5 70.02 4.23 8 8 6 11.65 1.53 8 8 6 10.50 1.59 8 8 7 0.38 0.53 8 8 7 -0.42 0.76 8 8 8 2.41 0.73 8 9 1 22.56 1.58 8 9 1 22.98 1.86 8 9 2 70.00 3.15 8 9 2 64.93 3.63 8 9 3 0.78 0.38 8 9 4 2.03 0.50 8 9 4 1.65 0.67 8 9 5 8.54 1.19 8 9 6 198.13 7.16 8 10 4 16.17 1.25 9 -5 2 0.81 0.40 9 -5 3 12.14 1.17 9 -4 -3 46.71 2.55 9 -4 -2 20.49 1.72 9 -4 -1 6.09 1.03 9 -4 0 70.00 3.70 9 -4 1 41.67 2.75 9 -4 2 28.18 2.26 9 -4 2 28.89 2.24 9 -4 3 23.17 2.03 9 -4 3 24.62 2.03 9 -4 4 0.72 0.48 9 -4 5 68.85 3.18 9 -3 -4 2.19 0.64 9 -3 -3 0.11 0.53 9 -3 -2 22.37 2.10 9 -3 -1 62.24 3.79 9 -3 0 22.31 2.28 9 -3 1 166.02 7.28 9 -3 2 23.19 2.38 9 -3 3 7.10 1.33 9 -3 4 34.44 2.76 9 -3 5 15.53 1.73 9 -3 6 79.63 4.01 9 -3 6 79.76 3.92 9 -3 7 56.92 3.01 9 -3 7 64.43 3.19 9 -3 8 64.16 2.94 9 -2 -5 39.01 2.38 9 -2 -4 1.02 0.59 9 -2 -3 29.18 2.49 9 -2 -2 154.18 6.17 9 -2 -2 135.30 5.65 9 -2 -1 12.37 1.57 9 -2 -1 7.69 1.20 9 -2 0 6.54 1.45 9 -2 0 6.79 1.24 9 -2 1 3.10 1.14 9 -2 1 2.07 0.81 9 -2 2 47.57 3.44 9 -2 2 42.23 3.53 9 -2 2 44.79 3.16 9 -2 3 346.16 12.47 9 -2 3 337.79 12.64 9 -2 3 322.51 11.60 9 -2 4 47.47 3.46 9 -2 4 43.68 2.90 9 -2 5 254.48 8.82 9 -2 6 0.13 0.50 9 -2 6 0.71 0.63 9 -2 7 9.80 1.40 9 -2 7 11.01 1.47 9 -2 8 73.78 3.66 9 -2 9 12.91 1.21 9 -1 -5 52.78 2.89 9 -1 -5 46.84 2.51 9 -1 -4 0.74 0.58 9 -1 -4 0.33 0.44 9 -1 -4 0.50 0.38 9 -1 -3 52.41 3.52 9 -1 -3 46.64 2.75 9 -1 -3 53.45 3.11 9 -1 -3 52.57 3.01 9 -1 -2 75.90 4.56 9 -1 -2 67.74 3.81 9 -1 -2 76.85 4.07 9 -1 -1 46.09 3.59 9 -1 -1 41.44 3.01 9 -1 0 132.50 6.82 9 -1 1 159.78 7.27 9 -1 1 181.92 8.25 9 -1 1 172.87 7.41 9 -1 2 156.05 7.22 9 -1 2 158.57 6.93 9 -1 3 7.70 1.50 9 -1 3 7.78 1.41 9 -1 4 39.82 3.28 9 -1 4 37.35 2.81 9 -1 5 56.66 3.33 9 -1 6 12.85 1.83 9 -1 6 12.39 1.66 9 -1 7 177.38 7.42 9 -1 7 169.21 7.13 9 -1 8 206.87 7.86 9 -1 8 196.30 7.70 9 -1 9 42.88 2.58 9 -1 9 45.00 2.69 9 0 -6 37.57 2.10 9 0 -5 142.93 5.50 9 0 -5 137.67 5.30 9 0 -4 136.66 5.63 9 0 -4 139.31 5.66 9 0 -3 268.79 10.30 9 0 -3 280.28 9.73 9 0 -3 283.75 9.94 9 0 -2 69.90 4.40 9 0 -2 68.79 3.73 9 0 -2 73.57 4.11 9 0 -2 77.21 4.10 9 0 -1 27.64 2.76 9 0 -1 29.79 2.55 9 0 0 2.54 1.13 9 0 1 63.09 4.46 9 0 1 61.93 3.97 9 0 2 6.42 1.38 9 0 2 8.12 1.66 9 0 2 6.33 1.33 9 0 3 456.10 15.61 9 0 3 424.30 14.87 9 0 4 22.08 2.50 9 0 4 21.21 2.16 9 0 5 175.99 7.88 9 0 5 159.24 6.81 9 0 6 128.65 5.45 9 0 6 128.54 6.08 9 0 7 98.46 5.18 9 0 7 81.58 4.62 9 0 8 0.92 0.60 9 0 8 0.98 0.69 9 0 9 91.33 4.37 9 0 9 85.96 4.31 9 0 10 6.39 0.95 9 0 10 4.28 0.71 9 1 -6 141.27 5.26 9 1 -5 110.65 4.68 9 1 -5 104.46 4.49 9 1 -4 30.99 2.36 9 1 -4 31.53 2.32 9 1 -3 9.34 1.37 9 1 -2 52.00 3.55 9 1 -2 51.45 3.30 9 1 -2 53.78 3.36 9 1 -1 186.59 8.09 9 1 -1 180.94 7.34 9 1 -1 182.00 7.72 9 1 -1 191.47 7.74 9 1 0 111.82 6.05 9 1 1 45.50 3.76 9 1 2 633.09 20.22 9 1 2 597.54 20.68 9 1 3 71.70 4.59 9 1 4 0.19 0.69 9 1 5 1.14 0.87 9 1 6 54.10 3.28 9 1 6 53.79 3.62 9 1 7 153.11 7.21 9 1 7 149.33 6.73 9 1 8 51.86 3.58 9 1 8 52.91 3.47 9 1 9 457.63 14.77 9 1 9 436.92 14.59 9 1 10 12.04 1.32 9 1 10 13.08 1.41 9 2 -6 3.99 0.71 9 2 -5 338.03 11.13 9 2 -4 51.32 3.10 9 2 -4 47.96 2.95 9 2 -3 199.09 7.78 9 2 -3 195.12 7.72 9 2 -2 256.17 9.48 9 2 -2 244.74 9.15 9 2 -1 66.27 4.00 9 2 0 41.26 3.10 9 2 1 64.21 4.23 9 2 2 46.87 3.44 9 2 2 45.35 3.60 9 2 3 46.31 3.56 9 2 4 253.97 10.45 9 2 5 114.96 6.24 9 2 6 335.07 12.80 9 2 7 79.59 4.51 9 2 8 101.57 5.41 9 2 8 97.76 5.00 9 2 9 44.71 3.09 9 2 9 37.94 2.81 9 2 10 7.56 1.13 9 2 10 4.46 0.94 9 2 11 62.08 2.97 9 3 -5 38.15 2.39 9 3 -4 21.33 1.95 9 3 -4 21.10 1.84 9 3 -3 3.70 0.88 9 3 -2 50.25 3.22 9 3 -1 193.21 7.79 9 3 0 382.55 13.16 9 3 1 178.26 8.24 9 3 1 171.04 7.24 9 3 3 245.73 9.91 9 3 3 248.96 10.51 9 3 4 106.86 5.78 9 3 4 100.86 5.89 9 3 5 123.65 6.49 9 3 6 0.57 0.79 9 3 8 35.02 3.00 9 3 8 31.86 2.64 9 3 9 100.74 4.99 9 3 9 88.24 4.58 9 3 10 328.72 10.92 9 3 10 312.95 10.75 9 3 11 127.37 4.87 9 4 -4 83.22 4.01 9 4 -3 51.64 2.96 9 4 -2 100.40 4.67 9 4 -1 324.05 11.16 9 4 0 71.65 4.50 9 4 0 65.91 3.70 9 4 1 5.97 1.06 9 4 1 7.34 1.51 9 4 2 9.56 1.32 9 4 3 265.10 10.42 9 4 3 219.49 8.38 9 4 4 383.91 14.12 9 4 4 405.45 14.67 9 4 5 84.26 5.08 9 4 5 87.59 5.21 9 4 6 306.59 11.99 9 4 6 315.33 11.74 9 4 7 66.79 4.37 9 4 9 0.27 0.52 9 4 10 6.26 0.97 9 4 10 4.71 0.95 9 4 11 3.30 0.59 9 5 -5 52.16 2.39 9 5 -2 32.05 2.13 9 5 -1 147.79 5.79 9 5 -1 135.06 5.53 9 5 0 97.39 5.16 9 5 0 82.33 3.98 9 5 1 103.61 5.72 9 5 3 260.87 10.76 9 5 4 30.05 2.72 9 5 4 39.09 3.34 9 5 5 2.70 0.97 9 5 5 1.25 0.82 9 5 6 97.14 5.41 9 5 6 102.65 5.32 9 5 7 7.02 1.40 9 5 7 6.54 1.18 9 5 9 88.79 4.52 9 5 10 63.42 3.30 9 6 -4 125.79 4.50 9 6 -1 15.90 1.50 9 6 0 3.72 0.80 9 6 0 2.25 0.78 9 6 1 1.30 0.82 9 6 2 8.71 1.56 9 6 3 19.29 2.33 9 6 4 64.31 4.26 9 6 5 49.37 3.57 9 6 6 176.12 7.40 9 6 7 154.49 6.33 9 6 8 152.76 6.48 9 6 10 28.48 1.88 9 7 -1 65.84 3.11 9 7 0 42.76 2.48 9 7 1 69.25 3.35 9 7 1 56.52 3.57 9 7 2 45.22 3.24 9 7 3 146.48 6.64 9 7 4 63.05 3.91 9 7 5 40.78 2.95 9 7 6 5.86 1.07 9 7 7 23.81 1.83 9 7 8 71.24 3.58 9 8 1 3.28 0.59 9 8 1 3.91 0.76 9 8 2 10.32 1.07 9 8 2 10.45 1.30 9 8 3 0.15 0.30 9 8 4 51.35 3.10 9 8 5 110.41 4.81 9 8 6 46.38 2.57 9 9 4 4.86 0.72 10 -3 -1 0.93 0.42 10 -3 0 9.52 1.07 10 -3 1 194.61 6.89 10 -3 2 0.41 0.45 10 -3 3 12.13 1.22 10 -3 4 105.94 4.18 10 -2 -2 9.06 1.07 10 -2 0 27.33 1.78 10 -2 1 129.31 5.03 10 -2 2 169.91 6.82 10 -2 3 2.64 0.81 10 -2 4 0.97 0.55 10 -2 5 67.38 3.46 10 -2 6 31.52 2.03 10 -1 -2 4.29 0.82 10 -1 -1 38.33 2.64 10 -1 -1 39.55 2.43 10 -1 -1 36.97 2.27 10 -1 0 1.12 0.62 10 -1 0 1.50 0.55 10 -1 1 24.65 2.32 10 -1 1 27.16 2.14 10 -1 2 402.99 14.02 10 -1 2 423.56 13.50 10 -1 3 1.10 0.53 10 -1 4 52.19 3.17 10 -1 4 43.43 2.63 10 -1 5 30.16 2.35 10 -1 6 4.31 0.95 10 -1 7 5.44 0.92 10 0 -2 2.35 0.60 10 0 -1 90.26 4.47 10 0 -1 90.11 4.22 10 0 0 17.41 1.90 10 0 0 20.74 1.87 10 0 1 6.71 1.26 10 0 1 4.51 0.96 10 0 2 89.13 4.82 10 0 2 88.63 4.41 10 0 3 83.34 4.70 10 0 3 89.60 4.34 10 0 4 18.29 1.93 10 0 4 18.66 2.09 10 0 4 18.42 1.72 10 0 5 24.97 2.27 10 0 5 24.12 2.30 10 0 5 21.77 1.76 10 0 6 166.21 6.81 10 0 7 114.12 5.02 10 0 8 47.77 2.64 10 1 -3 59.77 2.77 10 1 -3 67.99 3.10 10 1 -1 23.55 1.93 10 1 -1 25.13 1.99 10 1 0 1.25 0.55 10 1 0 0.68 0.49 10 1 1 26.37 2.19 10 1 2 99.85 5.16 10 1 2 101.88 4.89 10 1 3 376.72 13.70 10 1 3 419.52 13.48 10 1 4 29.76 2.49 10 1 4 25.47 2.47 10 1 4 28.11 2.28 10 1 5 0.55 0.57 10 1 5 1.01 0.68 10 1 5 0.90 0.51 10 1 6 27.54 2.36 10 1 6 28.89 1.93 10 1 8 4.32 0.86 10 1 9 44.21 2.36 10 2 -3 0.69 0.42 10 2 -3 0.23 0.36 10 2 -2 196.37 6.97 10 2 -2 203.32 7.23 10 2 -1 62.26 3.14 10 2 -1 65.09 3.34 10 2 -1 57.60 3.26 10 2 0 68.08 3.67 10 2 0 70.32 3.74 10 2 1 40.29 2.72 10 2 2 0.25 0.51 10 2 2 -0.11 0.46 10 2 4 70.22 4.01 10 2 4 69.08 3.83 10 2 5 155.53 6.68 10 2 5 149.62 6.12 10 2 6 88.02 4.56 10 2 6 80.84 3.82 10 2 7 19.33 1.97 10 2 8 66.09 3.51 10 2 9 0.95 0.48 10 3 -3 8.13 0.96 10 3 -2 5.24 0.86 10 3 -2 6.61 0.92 10 3 -1 39.15 2.48 10 3 -1 40.61 2.49 10 3 0 4.20 0.85 10 3 0 2.47 0.69 10 3 1 8.70 1.16 10 3 2 45.19 2.77 10 3 3 39.74 2.54 10 3 5 16.07 1.83 10 3 6 7.97 1.30 10 3 7 1.73 0.75 10 3 9 85.69 3.81 10 4 -3 48.30 2.39 10 4 -2 47.02 2.57 10 4 -1 143.17 5.33 10 4 0 29.05 1.95 10 4 1 4.63 0.78 10 4 2 26.91 1.87 10 4 6 121.49 5.50 10 4 7 143.81 6.04 10 4 8 23.51 1.93 10 4 9 65.71 3.14 10 5 -2 11.27 1.10 10 5 7 0.59 0.42 10 5 8 22.06 1.71 10 6 2 6.59 0.86 10 6 4 0.92 0.56 10 7 4 75.63 3.55 11 0 2 80.36 3.32 11 0 3 76.58 3.15 11 1 0 12.65 1.06 11 1 2 3.28 0.62 11 1 3 16.74 1.34 11 1 4 84.99 3.44 11 2 0 104.23 3.89 11 2 1 89.18 3.68 11 2 2 64.99 3.06 11 2 3 37.86 2.19 11 2 4 27.75 1.77 11 3 1 1.94 0.48 11 3 3 60.69 2.91 11 3 4 106.98 4.20 11 3 5 38.84 2.00 11 4 2 102.75 3.99 11 4 3 217.47 7.25 11 4 4 5.24 0.72 11 4 5 5.91 0.69 0 0 0 0.00 0.00 TITL ZYW-220602-2_auto in P1 REM P1 (#1 in standard setting) CELL 1.54184 9.019918 9.666450 12.131659 80.2331 78.9102 79.2010 ZERR 14.00 0.000425 0.000470 0.000511 0.0038 0.0037 0.0040 LATT -1 SFAC C N F Br UNIT 14.00 14.00 14.00 14.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.1; aver:100.0 TEMP -173 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 40129 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.401 _oxdiff_exptl_absorpt_empirical_full_min 0.686 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br01 Br 0.35911(2) 0.74018(2) 0.06340(2) 0.02724(8) Uani 1 1 d . . . . . F002 F 0.47253(12) 0.19666(11) 0.43882(9) 0.0253(2) Uani 1 1 d . . . . . F003 F 0.49744(14) -0.03201(12) 0.34569(10) 0.0329(3) Uani 1 1 d . . . . . F004 F 0.08391(12) 0.15135(13) 0.49830(10) 0.0322(3) Uani 1 1 d . . . . . F005 F 0.40211(15) 0.05466(14) 0.14598(10) 0.0376(3) Uani 1 1 d . . . . . F006 F 0.25044(15) -0.01717(14) 0.35756(11) 0.0412(3) Uani 1 1 d . . . . . F007 F 0.48718(17) 0.21866(15) 0.20354(10) 0.0462(3) Uani 1 1 d . . . . . F008 F 0.24532(17) 0.22901(16) 0.21198(11) 0.0496(4) Uani 1 1 d . . . . . N009 N 0.21571(15) 0.49229(15) 0.65248(12) 0.0166(3) Uani 1 1 d . . . . . N00A N 0.14356(16) 0.42449(16) 0.85530(12) 0.0194(3) Uani 1 1 d . . . . . C00B C 0.23002(18) 0.43710(18) 0.55280(14) 0.0174(3) Uani 1 1 d . . . . . C00C C 0.20185(19) 0.29938(18) 0.58214(14) 0.0180(3) Uani 1 1 d . . . . . C00D C 0.17796(18) 0.38996(18) 0.74390(14) 0.0170(3) Uani 1 1 d . . . . . C00E C 0.40752(19) 0.66735(17) 0.29311(14) 0.0183(3) Uani 1 1 d . . . . . H00E H 0.486145 0.724400 0.270659 0.022 Uiso 1 1 calc R U . . . C00F C 0.16789(19) 0.26770(18) 0.70266(14) 0.0175(3) Uani 1 1 d . . . . . C00G C 0.32065(19) 0.64862(18) 0.21557(14) 0.0193(3) Uani 1 1 d . . . . . C00H C 0.3408(2) 0.15217(18) 0.43471(14) 0.0192(3) Uani 1 1 d . . . . . C00I C 0.17500(19) 0.50270(18) 0.35731(15) 0.0195(3) Uani 1 1 d . . . . . H00I H 0.094375 0.447898 0.379384 0.023 Uiso 1 1 calc R U . . . C00J C 0.20448(19) 0.56723(18) 0.24600(14) 0.0196(3) Uani 1 1 d . . . . . H00J H 0.146137 0.555809 0.191720 0.024 Uiso 1 1 calc R U . . . C00K C 0.26185(19) 0.51664(17) 0.43820(14) 0.0172(3) Uani 1 1 d . . . . . C00L C 0.2144(2) 0.19913(18) 0.50234(14) 0.0195(3) Uani 1 1 d . . . . . C00M C 0.37737(19) 0.60108(17) 0.40431(14) 0.0177(3) Uani 1 1 d . . . . . H00M H 0.436057 0.613302 0.458103 0.021 Uiso 1 1 calc R U . . . C00N C 0.1716(2) 0.0780(2) 0.87780(15) 0.0252(4) Uani 1 1 d . . . . . H00A H 0.138306 -0.014917 0.908517 0.030 Uiso 1 1 calc R U . . . H00B H 0.284853 0.062961 0.866144 0.030 Uiso 1 1 calc R U . . . C00O C 0.2336(2) 0.63742(18) 0.66143(15) 0.0223(4) Uani 1 1 d . . . . . H00C H 0.191725 0.704935 0.599716 0.027 Uiso 1 1 calc R U . . . H00D H 0.343457 0.643607 0.654461 0.027 Uiso 1 1 calc R U . . . C00P C 0.1931(2) 0.5563(2) 0.86803(15) 0.0243(4) Uani 1 1 d . . . . . H00F H 0.305591 0.539991 0.863876 0.029 Uiso 1 1 calc R U . . . H00G H 0.145571 0.584285 0.943279 0.029 Uiso 1 1 calc R U . . . C00Q C 0.3640(2) 0.05913(19) 0.34383(15) 0.0231(4) Uani 1 1 d . . . . . C00R C 0.1189(2) 0.13073(19) 0.76377(15) 0.0220(4) Uani 1 1 d . . . . . H00H H 0.158209 0.056139 0.713972 0.026 Uiso 1 1 calc R U . . . H00K H 0.005757 0.143145 0.776000 0.026 Uiso 1 1 calc R U . . . C00S C 0.1872(2) 0.3112(2) 0.94600(15) 0.0238(4) Uani 1 1 d . . . . . H00L H 0.165341 0.352138 1.017971 0.029 Uiso 1 1 calc R U . . . H00N H 0.299192 0.279874 0.929181 0.029 Uiso 1 1 calc R U . . . C00T C 0.1092(2) 0.1807(2) 0.96436(15) 0.0237(4) Uani 1 1 d . . . . . H00O H -0.001320 0.212557 0.962671 0.028 Uiso 1 1 calc R U . . . H00P H 0.119524 0.128753 1.040890 0.028 Uiso 1 1 calc R U . . . C00U C 0.1481(2) 0.6749(2) 0.77605(16) 0.0258(4) Uani 1 1 d . . . . . H00Q H 0.173805 0.765097 0.789733 0.031 Uiso 1 1 calc R U . . . H00R H 0.036397 0.687990 0.776972 0.031 Uiso 1 1 calc R U . . . C00V C 0.3756(2) 0.1416(2) 0.22364(16) 0.0295(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br01 0.02728(12) 0.03751(13) 0.01710(11) 0.00580(8) -0.00584(7) -0.01205(8) F002 0.0222(5) 0.0322(6) 0.0240(5) -0.0096(4) -0.0008(4) -0.0090(4) F003 0.0410(7) 0.0273(6) 0.0279(6) -0.0099(5) -0.0104(5) 0.0112(5) F004 0.0240(5) 0.0405(6) 0.0386(6) -0.0218(5) 0.0014(5) -0.0136(5) F005 0.0460(7) 0.0444(7) 0.0236(6) -0.0191(5) -0.0076(5) 0.0045(6) F006 0.0452(7) 0.0435(7) 0.0421(7) -0.0260(6) 0.0101(6) -0.0247(6) F007 0.0666(9) 0.0543(8) 0.0213(6) -0.0012(5) 0.0011(6) -0.0310(7) F008 0.0587(9) 0.0539(8) 0.0340(7) -0.0180(6) -0.0260(6) 0.0263(7) N009 0.0171(7) 0.0180(7) 0.0158(7) -0.0046(5) -0.0023(5) -0.0041(5) N00A 0.0201(7) 0.0244(7) 0.0150(7) -0.0056(6) -0.0027(5) -0.0045(6) C00B 0.0157(8) 0.0206(8) 0.0165(8) -0.0051(6) -0.0028(6) -0.0020(6) C00C 0.0181(8) 0.0192(8) 0.0170(8) -0.0036(6) -0.0023(6) -0.0030(6) C00D 0.0145(8) 0.0225(8) 0.0139(8) -0.0030(6) -0.0025(6) -0.0024(6) C00E 0.0169(8) 0.0163(8) 0.0211(8) -0.0017(6) -0.0026(6) -0.0028(6) C00F 0.0180(8) 0.0183(8) 0.0161(8) -0.0028(6) -0.0021(6) -0.0025(6) C00G 0.0200(8) 0.0200(8) 0.0164(8) -0.0013(6) -0.0032(6) -0.0007(6) C00H 0.0231(8) 0.0194(8) 0.0164(8) -0.0014(6) -0.0039(7) -0.0071(7) C00I 0.0178(8) 0.0194(8) 0.0217(9) -0.0034(7) -0.0030(7) -0.0041(6) C00J 0.0181(8) 0.0232(8) 0.0183(8) -0.0032(7) -0.0052(6) -0.0026(6) C00K 0.0177(8) 0.0169(8) 0.0165(8) -0.0039(6) -0.0029(6) -0.0001(6) C00L 0.0236(9) 0.0189(8) 0.0174(8) -0.0017(6) -0.0038(7) -0.0076(7) C00M 0.0181(8) 0.0179(8) 0.0182(8) -0.0047(6) -0.0057(6) -0.0009(6) C00N 0.0265(9) 0.0234(9) 0.0213(9) 0.0026(7) -0.0004(7) -0.0018(7) C00O 0.0272(9) 0.0189(8) 0.0222(9) -0.0064(7) -0.0021(7) -0.0063(7) C00P 0.0250(9) 0.0303(9) 0.0205(9) -0.0110(7) -0.0015(7) -0.0073(7) C00Q 0.0241(9) 0.0231(9) 0.0233(9) -0.0076(7) -0.0031(7) -0.0036(7) C00R 0.0269(9) 0.0205(8) 0.0177(8) -0.0019(7) -0.0003(7) -0.0059(7) C00S 0.0220(9) 0.0347(10) 0.0153(8) -0.0023(7) -0.0045(7) -0.0058(7) C00T 0.0238(9) 0.0309(9) 0.0143(8) 0.0016(7) -0.0026(7) -0.0042(7) C00U 0.0321(10) 0.0224(9) 0.0243(9) -0.0100(7) -0.0012(7) -0.0054(7) C00V 0.0333(10) 0.0336(10) 0.0217(9) -0.0108(8) -0.0088(8) 0.0053(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00B N009 C00D 109.46(14) . . ? C00B N009 C00O 125.54(14) . . ? C00D N009 C00O 124.98(14) . . ? C00D N00A C00P 114.48(14) . . ? C00D N00A C00S 116.82(14) . . ? C00P N00A C00S 109.83(14) . . ? N009 C00B C00K 125.01(15) . . ? C00C C00B N009 106.84(15) . . ? C00C C00B C00K 128.08(15) . . ? C00B C00C C00F 109.50(15) . . ? C00B C00C C00L 124.97(15) . . ? C00F C00C C00L 125.42(15) . . ? N009 C00D N00A 120.40(15) . . ? C00F C00D N009 108.56(14) . . ? C00F C00D N00A 130.74(16) . . ? C00G C00E H00E 120.6 . . ? C00G C00E C00M 118.80(15) . . ? C00M C00E H00E 120.6 . . ? C00C C00F C00R 123.75(15) . . ? C00D C00F C00C 105.63(15) . . ? C00D C00F C00R 130.41(15) . . ? C00E C00G Br01 119.31(13) . . ? C00J C00G Br01 118.76(13) . . ? C00J C00G C00E 121.92(16) . . ? F002 C00H C00Q 110.70(14) . . ? C00L C00H F002 119.12(15) . . ? C00L C00H C00Q 130.07(16) . . ? C00J C00I H00I 119.3 . . ? C00J C00I C00K 121.40(16) . . ? C00K C00I H00I 119.3 . . ? C00G C00J C00I 118.63(16) . . ? C00G C00J H00J 120.7 . . ? C00I C00J H00J 120.7 . . ? C00I C00K C00B 118.07(15) . . ? C00M C00K C00B 123.68(15) . . ? C00M C00K C00I 118.21(15) . . ? F004 C00L C00C 116.07(14) . . ? C00H C00L F004 118.22(15) . . ? C00H C00L C00C 125.71(16) . . ? C00E C00M C00K 121.03(15) . . ? C00E C00M H00M 119.5 . . ? C00K C00M H00M 119.5 . . ? H00A C00N H00B 107.8 . . ? C00R C00N H00A 109.0 . . ? C00R C00N H00B 109.0 . . ? C00T C00N H00A 109.0 . . ? C00T C00N H00B 109.0 . . ? C00T C00N C00R 113.06(15) . . ? N009 C00O H00C 110.0 . . ? N009 C00O H00D 110.0 . . ? N009 C00O C00U 108.51(14) . . ? H00C C00O H00D 108.4 . . ? C00U C00O H00C 110.0 . . ? C00U C00O H00D 110.0 . . ? N00A C00P H00F 109.5 . . ? N00A C00P H00G 109.5 . . ? N00A C00P C00U 110.77(15) . . ? H00F C00P H00G 108.1 . . ? C00U C00P H00F 109.5 . . ? C00U C00P H00G 109.5 . . ? F003 C00Q C00H 109.85(15) . . ? F003 C00Q C00V 105.75(14) . . ? F006 C00Q F003 108.32(15) . . ? F006 C00Q C00H 111.79(15) . . ? F006 C00Q C00V 107.27(16) . . ? C00H C00Q C00V 113.55(15) . . ? C00F C00R C00N 115.62(15) . . ? C00F C00R H00H 108.4 . . ? C00F C00R H00K 108.4 . . ? C00N C00R H00H 108.4 . . ? C00N C00R H00K 108.4 . . ? H00H C00R H00K 107.4 . . ? N00A C00S H00L 108.2 . . ? N00A C00S H00N 108.2 . . ? N00A C00S C00T 116.34(15) . . ? H00L C00S H00N 107.4 . . ? C00T C00S H00L 108.2 . . ? C00T C00S H00N 108.2 . . ? C00N C00T H00O 108.6 . . ? C00N C00T H00P 108.6 . . ? C00S C00T C00N 114.84(15) . . ? C00S C00T H00O 108.6 . . ? C00S C00T H00P 108.6 . . ? H00O C00T H00P 107.5 . . ? C00O C00U H00Q 109.8 . . ? C00O C00U H00R 109.8 . . ? C00P C00U C00O 109.20(15) . . ? C00P C00U H00Q 109.8 . . ? C00P C00U H00R 109.8 . . ? H00Q C00U H00R 108.3 . . ? F005 C00V F008 107.97(16) . . ? F005 C00V C00Q 111.39(17) . . ? F007 C00V F005 108.54(16) . . ? F007 C00V F008 108.20(18) . . ? F007 C00V C00Q 110.64(16) . . ? F008 C00V C00Q 110.00(16) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br01 C00G 1.9042(17) . ? F002 C00H 1.349(2) . ? F003 C00Q 1.354(2) . ? F004 C00L 1.355(2) . ? F005 C00V 1.326(2) . ? F006 C00Q 1.340(2) . ? F007 C00V 1.324(3) . ? F008 C00V 1.329(2) . ? N009 C00B 1.377(2) . ? N009 C00D 1.390(2) . ? N009 C00O 1.466(2) . ? N00A C00D 1.410(2) . ? N00A C00P 1.467(2) . ? N00A C00S 1.470(2) . ? C00B C00C 1.376(2) . ? C00B C00K 1.474(2) . ? C00C C00F 1.427(2) . ? C00C C00L 1.457(2) . ? C00D C00F 1.383(2) . ? C00E H00E 0.9500 . ? C00E C00G 1.388(2) . ? C00E C00M 1.391(2) . ? C00F C00R 1.503(2) . ? C00G C00J 1.384(3) . ? C00H C00L 1.323(3) . ? C00H C00Q 1.499(2) . ? C00I H00I 0.9500 . ? C00I C00J 1.386(2) . ? C00I C00K 1.405(2) . ? C00J H00J 0.9500 . ? C00K C00M 1.400(2) . ? C00M H00M 0.9500 . ? C00N H00A 0.9900 . ? C00N H00B 0.9900 . ? C00N C00R 1.524(3) . ? C00N C00T 1.524(3) . ? C00O H00C 0.9900 . ? C00O H00D 0.9900 . ? C00O C00U 1.521(2) . ? C00P H00F 0.9900 . ? C00P H00G 0.9900 . ? C00P C00U 1.514(3) . ? C00Q C00V 1.533(3) . ? C00R H00H 0.9900 . ? C00R H00K 0.9900 . ? C00S H00L 0.9900 . ? C00S H00N 0.9900 . ? C00S C00T 1.521(3) . ? C00T H00O 0.9900 . ? C00T H00P 0.9900 . ? C00U H00Q 0.9900 . ? C00U H00R 0.9900 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br01 C00G C00J C00I -178.90(12) . . . . ? F002 C00H C00L F004 -178.91(14) . . . . ? F002 C00H C00L C00C 1.2(3) . . . . ? F002 C00H C00Q F003 42.56(19) . . . . ? F002 C00H C00Q F006 162.85(15) . . . . ? F002 C00H C00Q C00V -75.61(19) . . . . ? F003 C00Q C00V F005 57.0(2) . . . . ? F003 C00Q C00V F007 -63.86(19) . . . . ? F003 C00Q C00V F008 176.65(16) . . . . ? F006 C00Q C00V F005 -58.5(2) . . . . ? F006 C00Q C00V F007 -179.31(15) . . . . ? F006 C00Q C00V F008 61.2(2) . . . . ? N009 C00B C00C C00F 0.49(19) . . . . ? N009 C00B C00C C00L -175.97(16) . . . . ? N009 C00B C00K C00I -134.72(17) . . . . ? N009 C00B C00K C00M 47.7(2) . . . . ? N009 C00D C00F C00C 0.29(18) . . . . ? N009 C00D C00F C00R -174.57(16) . . . . ? N009 C00O C00U C00P 49.4(2) . . . . ? N00A C00D C00F C00C 173.86(16) . . . . ? N00A C00D C00F C00R -1.0(3) . . . . ? N00A C00P C00U C00O -64.60(19) . . . . ? N00A C00S C00T C00N 77.2(2) . . . . ? C00B N009 C00D N00A -174.35(14) . . . . ? C00B N009 C00D C00F 0.01(18) . . . . ? C00B N009 C00O C00U 157.05(16) . . . . ? C00B C00C C00F C00D -0.48(19) . . . . ? C00B C00C C00F C00R 174.80(16) . . . . ? C00B C00C C00L F004 -118.15(19) . . . . ? C00B C00C C00L C00H 61.8(3) . . . . ? C00B C00K C00M C00E 176.39(15) . . . . ? C00C C00B C00K C00I 41.9(2) . . . . ? C00C C00B C00K C00M -135.70(19) . . . . ? C00C C00F C00R C00N 146.95(17) . . . . ? C00D N009 C00B C00C -0.31(18) . . . . ? C00D N009 C00B C00K 176.90(15) . . . . ? C00D N009 C00O C00U -21.4(2) . . . . ? C00D N00A C00P C00U 46.8(2) . . . . ? C00D N00A C00S C00T -63.2(2) . . . . ? C00D C00F C00R C00N -39.0(3) . . . . ? C00E C00G C00J C00I -0.1(3) . . . . ? C00F C00C C00L F004 65.9(2) . . . . ? C00F C00C C00L C00H -114.2(2) . . . . ? C00G C00E C00M C00K 0.1(2) . . . . ? C00H C00Q C00V F005 177.49(15) . . . . ? C00H C00Q C00V F007 56.7(2) . . . . ? C00H C00Q C00V F008 -62.8(2) . . . . ? C00I C00K C00M C00E -1.2(2) . . . . ? C00J C00I C00K C00B -176.04(15) . . . . ? C00J C00I C00K C00M 1.7(2) . . . . ? C00K C00B C00C C00F -176.61(16) . . . . ? C00K C00B C00C C00L 6.9(3) . . . . ? C00K C00I C00J C00G -1.0(2) . . . . ? C00L C00C C00F C00D 175.96(16) . . . . ? C00L C00C C00F C00R -8.8(3) . . . . ? C00L C00H C00Q F003 -141.39(19) . . . . ? C00L C00H C00Q F006 -21.1(3) . . . . ? C00L C00H C00Q C00V 100.4(2) . . . . ? C00M C00E C00G Br01 179.37(12) . . . . ? C00M C00E C00G C00J 0.6(3) . . . . ? C00O N009 C00B C00C -178.94(15) . . . . ? C00O N009 C00B C00K -1.7(3) . . . . ? C00O N009 C00D N00A 4.3(2) . . . . ? C00O N009 C00D C00F 178.64(15) . . . . ? C00P N00A C00D N009 -16.7(2) . . . . ? C00P N00A C00D C00F 170.36(17) . . . . ? C00P N00A C00S C00T 164.32(15) . . . . ? C00Q C00H C00L F004 5.3(3) . . . . ? C00Q C00H C00L C00C -174.57(17) . . . . ? C00R C00N C00T C00S -75.9(2) . . . . ? C00S N00A C00D N009 -147.09(15) . . . . ? C00S N00A C00D C00F 40.0(2) . . . . ? C00S N00A C00P C00U -179.52(14) . . . . ? C00T C00N C00R C00F 61.8(2) . . . . ?