#------------------------------------------------------------------------------ #$Date: 2024-06-25 01:17:35 +0300 (Tue, 25 Jun 2024) $ #$Revision: 292546 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/19/1571966.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571966 loop_ _publ_author_name 'Chen, Jia-Wei' 'Ji, Wen-Jun' 'Huang, Xue-Ying' 'Ge, Danhua' 'Shen, Zhi-Liang' 'Guo, Kai' 'Chu, Xue-Qiang' _publ_section_title ; Chemo-, Regio-, and Stereoselective Tetrafunctionalization of Fluoroalkynes Enables Divergent Synthesis of 5--7-Membered Azacycles ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC03230F _journal_year 2024 _chemical_formula_moiety '1(C25 H15 F7 N2 O)' _chemical_formula_sum 'C25 H15 F7 N2 O' _chemical_formula_weight 492.39 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-09-05 _audit_creation_method ; Olex2 1.5-beta (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6439) ; _audit_update_record ; 2023-09-05 deposited with the CCDC. 2024-06-23 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 118.699(4) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 10.8721(3) _cell_length_b 42.5797(9) _cell_length_c 10.9151(3) _cell_measurement_reflns_used 7411 _cell_measurement_temperature 150.00(10) _cell_measurement_theta_max 73.5870 _cell_measurement_theta_min 4.0990 _cell_volume 4432.2(3) _computing_cell_refinement 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43f (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.5-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.5368 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 78.00 111.00 0.75 1.00 -- 40.73 38.00 30.00 44 2 \w 39.00 129.00 0.75 2.50 -- 106.95 -61.00 120.00 120 3 \w 76.00 115.00 0.75 2.50 -- 106.95-125.00 -30.00 52 4 \w 49.00 96.25 0.75 1.00 -- 40.73-125.00 60.00 63 5 \w 34.00 127.00 0.75 2.50 -- 106.95 -45.00 0.00 124 6 \w 142.00 167.50 0.75 2.50 -- 106.95 30.00-180.00 34 7 \w 81.00 106.50 0.75 2.50 -- 106.95 30.00-180.00 34 8 \w -114.00 -21.75 0.75 1.00 -- -40.73 -38.00 -90.00 123 9 \w -52.00 10.25 0.75 1.00 -- -41.23 77.00-180.00 83 10 \w 34.00 60.25 0.75 1.00 -- 41.23-125.00 60.00 35 11 \w 78.00 107.25 0.75 2.50 -- 106.95 -94.00-180.00 39 12 \w 91.00 118.00 0.75 2.50 -- 106.95 45.00 90.00 36 13 \w 139.00 177.25 0.75 2.50 -- 106.95 45.00 90.00 51 14 \w 37.00 95.50 0.75 2.50 -- 106.95 -94.00 -30.00 78 15 \w 82.00 148.00 0.75 2.50 -- 106.95 45.00 -90.00 88 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0618444000 _diffrn_orient_matrix_UB_12 0.0233845000 _diffrn_orient_matrix_UB_13 -0.0635462000 _diffrn_orient_matrix_UB_21 -0.0889560000 _diffrn_orient_matrix_UB_22 0.0265316000 _diffrn_orient_matrix_UB_23 0.0137564000 _diffrn_orient_matrix_UB_31 0.1197918000 _diffrn_orient_matrix_UB_32 0.0076067000 _diffrn_orient_matrix_UB_33 0.1472554000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0510 _diffrn_reflns_av_unetI/netI 0.0485 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 50 _diffrn_reflns_limit_k_min -50 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 18370 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 66.593 _diffrn_reflns_theta_max 66.593 _diffrn_reflns_theta_min 4.153 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.154 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.42645 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43f (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'light colourless' _exptl_crystal_density_diffrn 1.476 _exptl_crystal_description block _exptl_crystal_F_000 2000 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.502 _refine_diff_density_min -0.451 _refine_diff_density_rms 0.088 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.080 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 722 _refine_ls_number_reflns 7804 _refine_ls_number_restraints 694 _refine_ls_restrained_S_all 1.116 _refine_ls_R_factor_all 0.1053 _refine_ls_R_factor_gt 0.0938 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1422P)^2^+7.7380P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2539 _refine_ls_wR_factor_ref 0.2686 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6511 _reflns_number_total 7804 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03230f2.cif _cod_data_source_block 1096_2 _cod_original_cell_volume 4432.2(2) _cod_database_code 1571966 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2. Restrained distances C43-C42 1.54 with sigma of 0.01 N2-C20 \\sim N2-C01F with sigma of 0.02 C20-C21 \\sim C01F-C01S with sigma of 0.02 C20-C25 \\sim C01F-C01U with sigma of 0.02 C23-C24 \\sim C01P-C51 with sigma of 0.02 C23-C21 \\sim C01P-C01S with sigma of 0.04 C23-C22 \\sim C01P-C01Y with sigma of 0.02 C24-C22 \\sim C51-C01Y with sigma of 0.04 C21-C22 \\sim C01S-C01Y with sigma of 0.02 C25-C24 \\sim C01U-C51 with sigma of 0.02 C23-C25 \\sim C01P-C01U with sigma of 0.04 C21-C25 \\sim C01S-C01U with sigma of 0.04 N2-C21 \\sim N2-C01S with sigma of 0.04 N2-C25 \\sim N2-C01U with sigma of 0.04 C20-C24 \\sim C01F-C51 with sigma of 0.04 C20-C22 \\sim C01F-C01Y with sigma of 0.04 3. Uiso/Uaniso restraints and constraints F6 \\sim C18: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.004 within 2A F7 \\sim C18: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.004 within 2A C18 \\sim F5: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.004 within 2A 4. Rigid body (RIGU) restrains F10, F12, F8, F13, F14, F11, F16, F9, F17, O2, N4, N3, C26, C27, C28, C29, C30, C31, C32, C33, C34, C35, C36, C37, C38, C39, C40, C41, C42, C43, C44, C45, C46, C47, C48, C49, C50, C52 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.003 F4, F3, F1, F6, F7, F5, F2, O1, N1, N2, C1, C01F, C01P, C01S, C01U, C01Y, C2, C3, C4, C5, C6, C7, C8, C9, C10, C11, C12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25, C51 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.004 F10, F12, F8, F13, F14, F11, F16, F9, F15, F17, O2, N4, N3, C26, C27, C28, C29, C30, C31, C32, C33, C34, C35, C36, C37, C38, C39, C40, C41, C42, C43, C44, C45, C46, C47, C48, C49, C50, C52 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.004 5. Others Sof(C01F)=Sof(C01P)=Sof(H01P)=Sof(C01S)=Sof(H01S)=Sof(C01U)=Sof(H01U)= Sof(C01Y)=Sof(H01Y)=Sof(C51)=Sof(H51)=Sof(F16)=Sof(F15)=Sof(F17)=Sof(C43)=1- FVAR(1) Sof(C20)=Sof(C21)=Sof(H21)=Sof(C22)=Sof(H22)=Sof(C23)=Sof(H23)=Sof(C24)= Sof(H24)=Sof(C25)=Sof(H25)=Sof(F12)=Sof(F13)=Sof(F14)=Sof(C52)=FVAR(1) 6.a Aromatic/amide H refined with riding coordinates: C01P(H01P), C01S(H01S), C01U(H01U), C01Y(H01Y), C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C9(H9), C10(H10), C11(H11), C12(H12), C13(H13), C21(H21), C22(H22), C23(H23), C24(H24), C25(H25), C51(H51), C27(H27), C28(H28), C29(H29), C30(H30), C31(H31), C33(H33), C34(H34), C35(H35), C36(H36), C37(H37), C46(H46), C47(H47), C48(H48), C49(H49), C50(H50) ; _shelx_res_file ; TITL 1096_2_a.res in P2(1)/c 1096_2.res created by SHELXL-2018/3 at 20:21:28 on 05-Sep-2023 REM Old TITL 1096_2 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.295, Rweak 0.081, Alpha 0.051 REM 1.045 for 149 systematic absences, Orientation as input REM Formula found by SHELXT: C54 N7 O3 F16 CELL 1.54184 10.8721 42.5797 10.9151 90 118.699 90 ZERR 8 0.0003 0.0009 0.0003 0 0.004 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H F N O UNIT 200 120 56 16 8 SADI N2 C20 N2 C01F SADI C20 C21 C01F C01S SADI C20 C25 C01F C01U SADI C23 C24 C01P C51 SADI 0.04 C23 C21 C01P C01S SADI C23 C22 C01P C01Y SADI 0.04 C24 C22 C51 C01Y SADI C21 C22 C01S C01Y SADI C25 C24 C01U C51 SADI 0.04 C23 C25 C01P C01U SADI 0.04 C21 C25 C01S C01U SADI 0.04 N2 C21 N2 C01S SADI 0.04 N2 C25 N2 C01U SADI 0.04 C20 C24 C01F C51 SADI 0.04 C20 C22 C01F C01Y RIGU 0.001 0.003 F10 > F9 F17 > C52 RIGU 0.001 0.004 F4 > C51 RIGU 0.001 0.004 F10 > C52 DFIX 1.54 0.01 C43 C42 SIMU 0.001 0.004 2 F6 C18 SIMU 0.001 0.004 2 F7 C18 SIMU 0.001 0.004 2 C18 F5 L.S. 20 PLAN 8 CONF FREE F17 C51 FREE F17 F11 FREE F17 H51 BIND C42 C43 FREE F11 C52 FREE F11 C43 LIST 4 MORE -1 fmap 2 acta BOND $H SHEL 999 0.84 OMIT 0 2 0 REM REM REM WGHT 0.142200 7.738000 FVAR 0.38215 0.53684 F4 3 0.278037 0.535217 0.703068 11.00000 0.07506 0.06080 = 0.19653 0.02629 0.08205 -0.01048 F3 3 0.289017 0.528221 0.512551 11.00000 0.06227 0.05287 = 0.13741 -0.01776 0.01209 -0.03037 F1 3 0.474889 0.562508 0.480557 11.00000 0.06284 0.03292 = 0.04762 -0.01590 0.01434 -0.00635 F6 3 0.387410 0.479349 0.683024 11.00000 0.06676 0.03470 = 0.29245 0.02920 0.03385 -0.01149 F7 3 0.549454 0.502812 0.662778 11.00000 0.06907 0.04367 = 0.29497 -0.00183 0.05955 0.00782 F5 3 0.533542 0.509402 0.845751 11.00000 0.08440 0.05906 = 0.27145 0.05236 0.02467 -0.00867 F2 3 0.465385 0.578347 0.792692 11.00000 0.10068 0.03944 = 0.09010 -0.00581 0.07138 -0.01297 O1 5 0.841852 0.655590 0.685028 11.00000 0.02515 0.03391 = 0.05251 -0.00592 0.01859 -0.00368 N1 4 0.620719 0.657811 0.670905 11.00000 0.01989 0.02253 = 0.03426 -0.00286 0.01044 -0.00105 N2 4 0.691244 0.612536 0.630670 11.00000 0.02208 0.02601 = 0.03916 -0.00524 0.01424 0.00029 C1 1 0.606051 0.691407 0.662680 11.00000 0.02265 0.02219 = 0.03420 -0.00147 0.01233 -0.00124 PART 2 C01F 1 0.770895 0.592239 0.586671 -21.00000 0.02257 0.01833 = 0.02989 -0.00093 0.01291 -0.00198 C01P 1 0.920203 0.551447 0.514738 -21.00000 0.04934 0.03575 = 0.03995 -0.00474 0.02298 0.00465 AFIX 43 H01P 2 0.969125 0.537327 0.489161 -21.00000 -1.20000 AFIX 0 C01S 1 0.844977 0.568496 0.676629 -21.00000 0.08606 0.04956 = 0.03840 0.01636 0.03700 0.03896 AFIX 43 H01S 2 0.843199 0.566033 0.760424 -21.00000 -1.20000 AFIX 0 C01U 1 0.769517 0.595726 0.461137 -21.00000 0.05658 0.03222 = 0.03952 0.00737 0.03127 0.01033 AFIX 43 H01U 2 0.717302 0.611683 0.400056 -21.00000 -1.20000 AFIX 0 C01Y 1 0.922331 0.548256 0.641544 -21.00000 0.11680 0.08215 = 0.05436 0.02458 0.05465 0.06600 AFIX 43 H01Y 2 0.975754 0.532506 0.703237 -21.00000 -1.20000 AFIX 0 PART 0 C2 1 0.680776 0.709383 0.779762 11.00000 0.04678 0.02987 = 0.03543 -0.00332 0.00424 -0.00373 AFIX 43 H2 2 0.740119 0.699975 0.864930 11.00000 -1.20000 AFIX 0 C3 1 0.666618 0.741672 0.769353 11.00000 0.07325 0.02919 = 0.04685 -0.01016 0.00416 -0.00634 AFIX 43 H3 2 0.714359 0.754120 0.848419 11.00000 -1.20000 AFIX 0 C4 1 0.581124 0.755517 0.640859 11.00000 0.05978 0.02649 = 0.05551 0.00054 0.01442 0.00175 AFIX 43 H4 2 0.574299 0.777279 0.633471 11.00000 -1.20000 AFIX 0 C5 1 0.506814 0.737293 0.524966 11.00000 0.03947 0.03252 = 0.04692 0.00572 0.01188 0.00578 AFIX 43 H5 2 0.448151 0.746651 0.439461 11.00000 -1.20000 AFIX 0 C6 1 0.519151 0.704717 0.535236 11.00000 0.02931 0.03133 = 0.03265 -0.00148 0.01076 0.00016 AFIX 43 H6 2 0.469282 0.692163 0.456952 11.00000 -1.20000 AFIX 0 C7 1 0.512510 0.636381 0.639584 11.00000 0.02120 0.02497 = 0.02676 -0.00196 0.00874 -0.00225 C8 1 0.382196 0.644754 0.640367 11.00000 0.02180 0.02527 = 0.02709 0.00238 0.00883 0.00080 C9 1 0.254229 0.631970 0.541432 11.00000 0.02284 0.02983 = 0.03031 -0.00116 0.00755 -0.00114 AFIX 43 H9 2 0.250955 0.618945 0.471530 11.00000 -1.20000 AFIX 0 C10 1 0.132574 0.638599 0.547035 11.00000 0.02252 0.03674 = 0.03822 0.00731 0.01024 0.00067 AFIX 43 H10 2 0.048018 0.629956 0.480802 11.00000 -1.20000 AFIX 0 C11 1 0.135208 0.657929 0.649978 11.00000 0.02766 0.04674 = 0.04093 0.01020 0.01929 0.00750 AFIX 43 H11 2 0.053278 0.661911 0.654313 11.00000 -1.20000 AFIX 0 C12 1 0.260445 0.671299 0.746426 11.00000 0.03611 0.04684 = 0.03798 -0.00056 0.01995 0.00648 AFIX 43 H12 2 0.262526 0.684762 0.814490 11.00000 -1.20000 AFIX 0 C13 1 0.382772 0.664672 0.741815 11.00000 0.02661 0.03569 = 0.02967 -0.00307 0.01016 0.00053 AFIX 43 H13 2 0.466690 0.673665 0.807514 11.00000 -1.20000 AFIX 0 C14 1 0.557056 0.608442 0.617036 11.00000 0.02088 0.02636 = 0.03577 -0.00637 0.01106 -0.00271 C15 1 0.489301 0.577820 0.593883 11.00000 0.02369 0.02281 = 0.04390 -0.00709 0.00846 -0.00120 C16 1 0.442689 0.564528 0.672449 11.00000 0.03514 0.02407 = 0.06895 -0.00204 0.02496 -0.00340 C17 1 0.365552 0.533804 0.648195 11.00000 0.03025 0.03505 = 0.12832 0.00089 0.02492 -0.01297 C18 1 0.457323 0.505571 0.708892 11.00000 0.05180 0.03783 = 0.27952 0.02638 0.04230 -0.00571 C19 1 0.731745 0.643337 0.665149 11.00000 0.02042 0.02786 = 0.03119 -0.00334 0.00994 -0.00058 PART 1 C20 1 0.779030 0.586790 0.630578 21.00000 0.02215 0.02838 = 0.02871 -0.00348 0.01141 0.00224 C21 1 0.790707 0.558748 0.696509 21.00000 0.02654 0.03025 = 0.02750 -0.00206 0.01068 0.00156 AFIX 43 H21 2 0.743008 0.555507 0.746926 21.00000 -1.20000 AFIX 0 C22 1 0.874292 0.535153 0.687621 21.00000 0.03166 0.03865 = 0.04872 -0.00464 0.01564 0.00712 AFIX 43 H22 2 0.881605 0.515821 0.730253 21.00000 -1.20000 AFIX 0 C23 1 0.946652 0.540815 0.614345 21.00000 0.03426 0.04276 = 0.05182 -0.01446 0.01916 -0.00279 AFIX 43 H23 2 1.002594 0.525110 0.607683 21.00000 -1.20000 AFIX 0 C24 1 0.936806 0.569212 0.551715 21.00000 0.04034 0.04189 = 0.06234 -0.01423 0.03240 -0.00287 AFIX 43 H24 2 0.988005 0.572850 0.505091 21.00000 -1.20000 AFIX 0 C25 1 0.850953 0.592608 0.557320 21.00000 0.03521 0.03519 = 0.04034 -0.00936 0.02335 -0.00527 AFIX 43 H25 2 0.841939 0.611766 0.512857 21.00000 -1.20000 AFIX 0 PART 2 C51 1 0.845950 0.575433 0.426658 -21.00000 0.06386 0.03956 = 0.05446 0.00700 0.04287 0.01145 AFIX 43 H51 2 0.847368 0.577984 0.342726 -21.00000 -1.20000 AFIX 0 PART 0 F10 3 0.811338 0.545360 -0.013954 11.00000 0.09387 0.06414 = 0.09860 -0.04552 0.02796 -0.02535 PART 1 F12 3 1.061904 0.538876 0.010304 21.00000 0.11339 0.06842 = 0.07235 -0.00073 0.05046 0.01029 PART 0 F8 3 0.810345 0.605815 -0.056392 11.00000 0.05397 0.05940 = 0.04160 -0.02074 0.00791 -0.01081 PART 1 F13 3 1.156979 0.524677 0.224160 21.00000 0.10245 0.09769 = 0.06959 -0.00406 0.02590 0.03667 F14 3 0.990764 0.497280 0.066827 21.00000 0.14373 0.04401 = 0.11290 -0.01066 0.07091 -0.00246 PART 0 F11 3 0.921842 0.531776 0.227691 11.00000 0.19077 0.05581 = 0.11741 0.00856 0.06350 -0.01618 PART 2 F16 3 0.715784 0.515473 0.102143 -21.00000 0.24452 0.14688 = 0.05353 -0.02387 0.05334 -0.14389 PART 0 F9 3 1.054776 0.583688 0.285877 11.00000 0.11730 0.05116 = 0.03460 -0.00231 0.02060 -0.02892 PART 2 F15 3 0.667711 0.561312 0.086634 -21.00000 0.12775 0.16938 = 0.25427 -0.04372 0.11486 -0.08702 F17 3 0.799494 0.549226 0.267044 -21.00000 0.32874 0.38028 = 0.13064 -0.15372 0.17239 -0.29960 PART 0 O2 5 1.266851 0.686600 0.227198 11.00000 0.02544 0.03895 = 0.04068 -0.00755 0.01462 -0.00361 N4 4 1.111006 0.644504 0.138572 11.00000 0.02722 0.03516 = 0.03189 -0.00774 0.01521 -0.00290 N3 4 1.050412 0.684352 0.225162 11.00000 0.02251 0.02840 = 0.02906 -0.00077 0.01026 0.00092 C26 1 1.052507 0.715932 0.275264 11.00000 0.02635 0.02790 = 0.03095 -0.00004 0.01519 -0.00054 C27 1 0.962506 0.737977 0.184052 11.00000 0.04739 0.03503 = 0.03924 0.00686 0.01630 0.00857 AFIX 43 H27 2 0.900941 0.732666 0.091858 11.00000 -1.20000 AFIX 0 C28 1 0.965305 0.768245 0.232123 11.00000 0.06545 0.03334 = 0.06300 0.00560 0.03342 0.01149 AFIX 43 H28 2 0.904621 0.783366 0.171964 11.00000 -1.20000 AFIX 0 C29 1 1.057078 0.776018 0.367922 11.00000 0.05796 0.03218 = 0.06939 -0.00805 0.04207 -0.00394 AFIX 43 H29 2 1.058570 0.796419 0.399045 11.00000 -1.20000 AFIX 0 C30 1 1.147104 0.753828 0.458612 11.00000 0.04558 0.04311 = 0.05136 -0.01528 0.02568 -0.00963 AFIX 43 H30 2 1.208691 0.759158 0.550774 11.00000 -1.20000 AFIX 0 C31 1 1.145172 0.723348 0.411206 11.00000 0.03403 0.03827 = 0.03380 -0.00450 0.01357 -0.00096 AFIX 43 H31 2 1.206023 0.708210 0.471070 11.00000 -1.20000 AFIX 0 C32 1 0.816656 0.665245 0.198834 11.00000 0.02394 0.02640 = 0.02844 0.00523 0.00971 0.00240 C33 1 0.687699 0.653190 0.098268 11.00000 0.02919 0.03577 = 0.03070 -0.00202 0.01073 -0.00143 AFIX 43 H33 2 0.678690 0.645366 0.014800 11.00000 -1.20000 AFIX 0 C34 1 0.573848 0.652779 0.121531 11.00000 0.02659 0.03573 = 0.04151 0.00228 0.01175 -0.00216 AFIX 43 H34 2 0.489051 0.644401 0.054470 11.00000 -1.20000 AFIX 0 C35 1 0.585286 0.664763 0.244030 11.00000 0.03295 0.03475 = 0.04699 0.00566 0.02225 0.00107 AFIX 43 H35 2 0.508180 0.664556 0.259307 11.00000 -1.20000 AFIX 0 C36 1 0.711794 0.677104 0.344235 11.00000 0.03562 0.02836 = 0.04063 0.00381 0.02165 0.00386 AFIX 43 H36 2 0.719581 0.685106 0.426945 11.00000 -1.20000 AFIX 0 C37 1 0.826417 0.677560 0.321684 11.00000 0.02526 0.02629 = 0.02825 0.00439 0.00988 0.00281 AFIX 43 H37 2 0.910676 0.686134 0.388843 11.00000 -1.20000 AFIX 0 C38 1 0.940122 0.662839 0.177708 11.00000 0.02288 0.03234 = 0.02319 0.00085 0.00754 -0.00023 C39 1 0.978033 0.638193 0.124009 11.00000 0.02561 0.03843 = 0.02795 -0.00469 0.01210 -0.00298 C40 1 0.912176 0.607796 0.075542 11.00000 0.03565 0.04707 = 0.03250 -0.01340 0.01970 -0.01245 C41 1 0.952066 0.581860 0.153710 11.00000 0.07281 0.04677 = 0.03525 -0.01258 0.02822 -0.02428 C42 1 0.903790 0.547950 0.113223 11.00000 0.11037 0.05500 = 0.08122 -0.02151 0.04287 -0.04176 PART 2 C43 1 0.774222 0.542823 0.140640 -21.00000 0.11901 0.15244 = 0.08101 -0.07685 0.04897 -0.10249 PART 0 C44 1 1.157310 0.673327 0.202410 11.00000 0.02229 0.03291 = 0.02390 -0.00211 0.00813 0.00093 C45 1 1.187807 0.623941 0.096013 11.00000 0.03034 0.03080 = 0.03120 -0.00293 0.01759 -0.00229 C46 1 1.308070 0.609448 0.196263 11.00000 0.03622 0.04149 = 0.03357 0.00228 0.01894 0.00433 AFIX 43 H46 2 1.341710 0.613784 0.290517 11.00000 -1.20000 AFIX 0 C47 1 1.377919 0.588330 0.154254 11.00000 0.04613 0.04409 = 0.05094 0.00418 0.02979 0.00978 AFIX 43 H47 2 1.459081 0.578476 0.220528 11.00000 -1.20000 AFIX 0 C48 1 1.326894 0.581985 0.014320 11.00000 0.05734 0.04046 = 0.05416 -0.00191 0.03832 0.00541 AFIX 43 H48 2 1.372580 0.567441 -0.013301 11.00000 -1.20000 AFIX 0 C49 1 1.209789 0.596892 -0.084022 11.00000 0.06020 0.05090 = 0.03989 -0.00635 0.03160 0.00202 AFIX 43 H49 2 1.177837 0.592869 -0.178260 11.00000 -1.20000 AFIX 0 C50 1 1.137752 0.618086 -0.044331 11.00000 0.04344 0.04757 = 0.03120 -0.00227 0.01947 0.00187 AFIX 43 H50 2 1.057428 0.628101 -0.111180 11.00000 -1.20000 AFIX 0 PART 1 C52 1 1.016048 0.528845 0.120509 21.00000 0.09943 0.04344 = 0.04686 0.00130 0.01358 -0.02520 HKLF 4 REM 1096_2_a.res in P2(1)/c REM wR2 = 0.2686, GooF = S = 1.080, Restrained GooF = 1.116 for all data REM R1 = 0.0938 for 6511 Fo > 4sig(Fo) and 0.1053 for all 7804 data REM 722 parameters refined using 694 restraints END WGHT 0.1448 8.3202 REM Highest difference peak 0.502, deepest hole -0.451, 1-sigma level 0.088 Q1 1 0.9776 0.5326 0.1600 11.00000 0.05 0.50 Q2 1 0.6413 0.5735 0.0154 11.00000 0.05 0.35 Q3 1 0.5128 0.5204 0.8977 11.00000 0.05 0.22 Q4 1 0.5200 0.5064 0.5969 11.00000 0.05 0.16 Q5 1 0.5891 0.5077 0.8022 11.00000 0.05 0.11 ; _shelx_res_checksum 40951 _shelx_hkl_file ; 0 0 1 0.16 0.21 0 0 2 5787.79 54.59 0 0 3 0.06 0.67 0 0 3 -0.25 0.79 0 0 4 6.30 2.37 0 0 4 10.90 2.97 0 0 5 -0.68 1.71 0 0 6 146.09 13.42 0 0 7 0.10 0.65 0 0 7 0.78 0.96 0 0 7 1.10 1.03 0 0 8 10.11 2.37 0 0 8 10.38 2.18 0 0 8 7.34 3.29 0 0 9 2.83 1.44 0 0 10 13.12 2.55 0 -1 1 82.39 2.35 0 1 1 75.97 3.89 0 -1 1 74.83 3.99 0 1 2 9999.00 75.89 0 -1 2 9905.39 75.49 0 1 3 328.90 13.76 0 1 3 337.40 13.40 0 -1 3 337.93 14.25 0 -1 3 355.71 13.84 0 1 4 1426.74 32.31 0 1 4 1371.94 33.12 0 -1 4 1408.21 34.16 0 -1 5 317.63 18.03 0 1 5 312.13 17.64 0 1 5 315.86 17.11 0 1 6 87.90 10.18 0 -1 6 93.40 10.91 0 1 7 96.36 6.77 0 1 7 114.79 6.85 0 -1 7 89.21 11.36 0 -1 7 96.52 6.76 0 1 7 95.15 11.56 0 -1 8 53.76 5.37 0 1 8 49.32 5.13 0 -1 8 37.11 7.78 0 1 8 59.22 5.12 0 1 8 44.61 8.48 0 -1 9 36.79 4.51 0 1 9 39.45 4.65 0 1 10 11.62 2.41 0 -1 10 10.18 2.40 0 2 0 334.87 4.25 0 -2 1 2.44 0.44 0 2 1 1.60 0.50 0 2 -1 1.08 0.22 0 2 1 1.90 0.61 0 2 2 1663.17 26.26 0 -2 2 1671.16 27.40 0 2 2 1734.64 26.45 0 2 3 945.33 23.44 0 2 3 1035.73 24.23 0 -2 3 924.39 23.97 0 -2 3 1076.09 24.39 0 2 4 13.70 3.03 0 2 4 10.66 2.68 0 -2 4 10.16 2.83 0 -2 5 1.68 0.69 0 2 5 1.52 1.48 0 2 5 0.18 0.69 0 2 6 44.35 7.19 0 -2 6 37.83 7.05 0 -2 7 127.74 13.77 0 2 7 156.36 8.06 0 2 7 116.26 7.40 0 -2 7 130.87 7.87 0 2 7 142.40 14.05 0 2 8 6.99 1.98 0 -2 8 0.85 0.93 0 2 8 5.70 1.64 0 -2 8 4.67 1.49 0 2 9 71.42 6.20 0 -2 9 72.28 6.35 0 -2 10 39.40 4.45 0 2 10 35.11 4.01 0 3 0 0.39 0.20 0 3 -1 83.03 2.40 0 3 1 87.61 4.13 0 3 1 78.95 3.87 0 -3 2 8690.95 73.24 0 3 2 8624.98 69.43 0 3 3 45.81 5.08 0 -3 3 41.81 5.02 0 3 3 50.33 5.35 0 3 4 81.96 7.81 0 3 4 77.29 7.55 0 -3 4 81.81 8.18 0 3 5 21.77 4.63 0 -3 5 19.15 4.55 0 3 5 21.27 4.44 0 3 6 850.16 31.56 0 -3 6 819.43 32.86 0 -3 7 227.61 10.45 0 3 7 182.33 9.26 0 3 7 192.00 16.23 0 -3 7 196.72 17.52 0 3 8 1.32 1.35 0 3 8 1.09 0.85 0 -3 8 0.58 0.55 0 -3 8 1.37 0.91 0 3 9 113.79 7.73 0 -3 9 126.49 8.37 0 -3 10 -0.50 0.65 0 3 11 2.44 1.38 0 -3 11 2.23 1.04 0 4 0 1085.17 11.25 0 4 -1 625.47 8.13 0 -4 1 628.15 9.21 0 -4 2 420.92 8.99 0 4 2 474.14 13.25 0 4 2 380.52 11.93 0 -4 2 416.72 13.70 0 4 3 38.82 4.59 0 -4 3 37.85 4.90 0 4 3 39.88 4.88 0 -4 4 1425.22 35.41 0 4 4 1450.59 33.67 0 4 4 1445.90 33.02 0 4 5 1.43 1.50 0 4 5 0.57 0.64 0 -4 5 3.84 2.06 0 4 6 6.85 3.03 0 -4 6 2.35 1.72 0 4 7 17.05 4.93 0 -4 7 17.24 2.87 0 4 7 11.14 2.36 0 4 7 17.45 2.64 0 -4 7 13.91 4.80 0 -4 8 37.01 4.43 0 4 8 46.41 4.57 0 4 8 30.77 4.04 0 -4 8 26.75 6.82 0 -4 9 181.42 10.08 0 4 9 158.12 9.07 0 -4 10 22.27 3.40 0 -4 11 7.19 1.60 0 4 11 5.13 1.84 0 -5 0 0.41 0.25 0 5 1 467.13 10.52 0 -5 1 406.23 7.84 0 5 2 1651.21 26.14 0 5 2 1647.50 25.43 0 -5 3 56.00 6.17 0 5 3 53.65 5.74 0 5 3 59.59 5.65 0 5 4 127.60 9.62 0 5 4 131.75 10.31 0 -5 4 122.37 10.28 0 5 5 12.79 3.60 0 -5 5 14.08 4.04 0 5 5 12.04 3.48 0 5 6 45.72 7.50 0 -5 6 37.36 7.17 0 5 6 42.56 6.99 0 5 7 30.01 3.43 0 -5 7 20.71 5.77 0 -5 7 26.82 3.54 0 -5 8 6.71 1.92 0 5 8 11.52 2.58 0 -5 8 5.33 3.31 0 5 8 6.43 1.92 0 -5 9 242.36 11.63 0 -5 10 34.45 4.19 0 5 11 18.28 3.41 0 -5 11 18.21 2.54 0 -6 0 698.71 9.82 0 -6 1 226.28 6.25 0 -6 -1 246.64 5.27 0 -6 -2 7192.79 43.20 0 6 2 7422.62 63.96 0 6 3 90.17 7.33 0 6 3 83.72 6.67 0 -6 3 91.02 8.03 0 -6 4 191.93 13.13 0 6 4 206.16 13.03 0 6 4 187.77 11.52 0 6 5 89.54 9.47 0 6 5 104.29 9.72 0 -6 5 92.56 10.27 0 -6 6 62.43 9.57 0 6 6 75.61 9.82 0 6 6 68.71 8.94 0 -6 7 -1.15 2.38 0 -6 7 1.14 0.93 0 6 7 1.02 0.88 0 6 8 27.86 3.74 0 -6 8 23.13 3.59 0 -6 9 31.34 4.32 0 -6 10 15.67 2.84 0 -6 11 8.85 1.82 0 6 11 5.31 1.82 0 -7 0 0.71 0.42 0 -7 1 198.23 6.20 0 -7 -1 224.07 5.49 0 -7 -2 1146.14 13.26 0 -7 2 1174.03 18.47 0 7 3 544.61 17.38 0 -7 3 571.03 20.62 0 7 3 548.80 18.38 0 7 4 379.97 18.22 0 7 4 422.94 17.77 0 7 5 336.93 17.71 0 -7 5 314.59 19.38 0 7 5 324.46 18.43 0 7 6 637.45 28.91 0 -7 6 661.03 31.16 0 -7 7 156.57 8.67 0 7 7 164.57 8.06 0 -7 8 112.01 7.78 0 7 8 129.34 7.44 0 -7 9 106.60 7.68 0 -7 10 16.73 2.94 0 -7 11 14.44 2.26 0 -8 0 0.82 0.47 0 -8 -1 163.36 5.07 0 -8 1 142.14 5.55 0 -8 2 1729.60 23.94 0 -8 -2 1743.31 18.30 0 8 3 350.69 14.82 0 -8 3 379.08 17.25 0 -8 4 2057.93 45.93 0 8 4 2096.26 43.69 0 -8 5 138.91 12.93 0 8 5 134.04 12.20 0 8 6 120.86 12.78 0 -8 6 124.43 13.74 0 -8 7 212.25 10.13 0 8 7 248.43 9.90 0 8 8 9.79 2.64 0 -8 8 1.77 1.13 0 -8 8 4.55 3.43 0 -8 9 7.07 2.33 0 -8 10 23.22 3.47 0 -8 11 42.02 3.87 0 -9 0 1.46 0.65 0 -9 -1 465.56 9.32 0 -9 1 419.52 10.24 0 -9 -2 5838.19 42.07 0 9 2 5952.18 59.29 0 -9 3 359.84 12.69 0 9 3 334.93 14.77 0 -9 4 331.73 18.65 0 9 4 303.91 16.63 0 9 5 5.02 2.62 0 -9 5 7.76 3.33 0 -9 6 1.67 1.31 0 9 6 0.41 1.94 0 -9 7 0.59 2.03 0 -9 7 3.99 1.60 0 9 7 6.28 1.68 0 -9 8 4.86 1.73 0 -9 8 4.68 3.11 0 -9 9 209.52 10.78 0 -9 10 14.38 2.72 0 -9 11 13.79 2.20 0 -10 0 3321.45 31.64 0 -10 1 609.02 13.09 0 -10 -1 707.86 12.54 0 10 2 2.27 1.25 0 -10 -2 6.38 1.68 0 -10 3 2.99 1.36 0 -10 -3 2.33 0.78 0 10 3 1.25 0.92 0 10 4 10.08 3.30 0 -10 4 6.48 2.89 0 -10 5 57.86 8.78 0 10 5 58.15 8.23 0 -10 6 646.13 32.58 0 10 6 622.46 29.92 0 -10 7 219.24 10.29 0 10 7 244.48 9.73 0 -10 8 122.13 8.06 0 10 8 135.97 7.68 0 -10 9 92.06 7.19 0 -10 10 2.52 1.29 0 -10 11 15.92 2.36 0 -11 0 4.44 1.24 0 -11 -1 113.11 5.28 0 -11 1 100.31 5.49 0 -11 -2 1692.65 21.72 0 11 2 1859.04 33.14 0 -11 -3 9.67 1.66 0 11 3 4.32 1.62 0 -11 3 9.90 2.52 0 11 3 5.98 2.11 0 11 4 430.77 20.50 0 -11 4 452.22 23.10 0 11 5 531.88 26.02 0 -11 5 540.35 27.39 0 -11 6 7.21 3.48 0 11 6 6.95 4.01 0 -11 7 91.66 13.39 0 -11 7 97.28 6.88 0 11 7 76.14 11.70 0 11 7 116.41 6.67 0 -11 8 15.96 2.96 0 11 8 41.87 4.65 0 -11 9 5.93 2.06 0 -11 10 30.30 3.83 0 -11 11 1.94 0.91 0 -12 0 3871.42 37.75 0 -12 1 1836.16 25.97 0 -12 -1 2063.87 25.23 0 12 2 4790.96 57.84 0 -12 -2 4845.12 42.50 0 12 3 2784.48 48.11 0 12 3 2732.01 46.84 0 -12 4 2.91 2.40 0 12 4 1.93 1.42 0 12 5 1.25 1.36 0 -12 5 4.08 2.75 0 12 6 4.47 1.74 0 -12 6 5.16 3.07 0 12 7 150.89 7.67 0 12 7 109.04 14.15 0 -12 7 137.96 8.18 0 -12 7 98.93 14.16 0 -12 8 108.46 7.58 0 -12 9 0.37 0.84 0 -12 10 0.52 0.51 0 -12 11 6.33 1.51 0 -13 0 0.44 0.89 0 -13 -1 39.96 3.54 0 -13 1 33.71 3.45 0 -13 2 193.09 9.49 0 -13 -2 221.47 8.42 0 13 3 217.22 13.44 0 13 3 192.03 12.61 0 -13 -3 200.82 8.42 0 -13 3 211.64 11.04 0 13 4 221.01 15.31 0 -13 4 226.62 17.26 0 -13 5 91.82 11.93 0 13 5 92.41 11.16 0 -13 6 62.53 10.69 0 13 6 60.95 9.60 0 -13 7 273.81 23.96 0 13 7 252.60 21.60 0 -13 7 348.18 13.06 0 13 7 373.25 11.87 0 -13 8 147.52 8.88 0 -13 9 -0.39 0.96 0 -13 10 3.83 1.45 0 -13 11 1.21 0.79 0 -14 0 504.20 13.47 0 -14 1 101.34 6.38 0 -14 -1 103.46 5.88 0 -14 2 150.85 8.72 0 -14 -2 127.83 6.69 0 14 3 26.35 4.95 0 -14 -3 18.34 2.68 0 -14 3 18.01 3.40 0 14 4 486.67 23.06 0 -14 4 587.70 28.88 0 -14 5 83.20 11.76 0 14 5 84.29 11.00 0 14 6 46.05 4.49 0 -14 6 40.61 4.20 0 14 6 45.80 3.98 0 -14 6 41.60 8.94 0 14 6 37.83 7.91 0 14 7 149.98 7.58 0 -14 7 100.61 14.72 0 14 7 98.60 13.94 0 -14 7 133.47 8.07 0 -14 8 8.14 2.47 0 -14 9 -0.19 0.96 0 -14 10 0.32 0.76 0 -14 11 4.45 1.23 0 -14 11 6.11 2.14 0 -15 0 73.60 5.31 0 -15 1 692.41 17.43 0 -15 -1 728.46 16.62 0 -15 2 264.43 11.85 0 -15 -2 303.83 10.98 0 -15 3 76.84 7.06 0 15 3 69.83 7.92 0 15 3 76.03 8.50 0 -15 -3 84.45 6.11 0 -15 4 510.19 27.73 0 15 4 462.03 23.19 0 15 5 77.27 10.62 0 -15 5 86.18 12.30 0 -15 6 57.15 10.57 0 15 6 67.08 5.41 0 15 6 75.10 5.11 0 -15 6 67.49 5.56 0 15 6 51.46 9.80 0 -15 7 11.47 2.41 0 -15 7 8.66 4.94 0 15 7 8.58 4.38 0 -15 8 570.70 17.61 0 -15 9 61.28 5.64 0 -15 10 35.24 3.91 0 -15 11 2.92 1.02 0 -15 11 1.96 1.08 0 -16 0 1609.73 26.95 0 -16 1 223.30 10.30 0 -16 -1 230.00 9.71 0 -16 2 571.00 18.11 0 -16 -2 585.57 15.95 0 16 3 27.71 5.05 0 -16 3 27.24 4.56 0 -16 -3 18.48 2.89 0 16 4 109.25 11.38 0 -16 4 131.38 14.48 0 16 5 122.32 13.61 0 -16 5 129.54 15.43 0 -16 6 -0.28 0.79 0 -16 6 0.52 1.05 0 16 6 4.48 1.81 0 16 6 3.23 2.85 0 16 6 0.05 0.88 0 16 7 135.97 16.32 0 -16 7 141.62 18.19 0 -16 8 13.09 2.75 0 -16 9 157.24 9.00 0 -16 10 8.01 1.88 0 -16 11 0.90 0.65 0 -16 11 0.99 0.57 0 -17 0 2.45 1.18 0 -17 -1 140.96 7.94 0 -17 1 142.26 8.68 0 -17 -2 127.52 7.85 0 -17 2 122.57 8.60 0 -17 -3 10.83 2.37 0 -17 3 10.12 2.70 0 17 3 7.50 2.73 0 17 3 3.35 1.64 0 17 4 606.04 27.41 0 17 5 38.79 8.33 0 -17 5 37.05 8.47 0 -17 6 -0.92 0.71 0 -17 6 1.13 1.31 0 17 6 2.54 2.19 0 17 6 -0.33 1.10 0 17 6 4.08 1.82 0 17 7 211.32 20.71 0 -17 7 238.22 23.95 0 -17 8 7.26 2.04 0 -17 9 31.22 4.06 0 -17 10 5.05 1.32 0 -17 11 8.52 1.50 0 -17 11 7.90 2.01 0 -18 0 205.92 10.25 0 -18 -1 556.70 16.79 0 -18 1 555.30 17.77 0 -18 -2 39.39 4.62 0 -18 2 41.30 5.29 0 -18 -3 2.74 1.49 0 18 3 2.23 1.15 0 -18 3 5.24 3.04 0 18 4 9.31 3.69 0 -18 5 16.88 6.21 0 18 5 16.10 5.14 0 18 6 52.62 6.80 0 -18 6 56.37 11.41 0 -18 6 70.36 5.71 0 18 6 41.19 9.22 0 -18 7 48.38 4.95 0 -18 7 31.18 8.95 0 18 7 25.45 7.09 0 -18 8 32.29 4.18 0 -18 9 4.95 1.60 0 -18 10 38.81 3.92 0 -18 11 2.55 1.15 0 -18 11 2.53 0.82 0 -19 0 7.26 2.26 0 -19 -1 501.41 16.82 0 -19 1 486.31 17.53 0 -19 2 2356.63 41.88 0 -19 -2 2352.52 38.60 0 -19 -3 537.23 18.63 0 -19 3 549.26 21.98 0 19 3 475.49 22.97 0 19 3 469.68 23.23 0 19 4 1.55 1.74 0 -19 5 161.09 18.91 0 19 5 134.68 15.09 0 -19 6 194.34 9.64 0 19 6 140.85 11.31 0 19 6 121.38 15.31 0 -19 6 174.99 20.34 0 -19 7 35.21 9.47 0 -19 7 43.10 4.71 0 19 7 30.55 8.03 0 -19 8 216.71 10.67 0 -19 9 50.80 4.99 0 -19 10 8.85 1.90 0 -19 11 5.16 1.11 0 -20 0 16.03 3.03 0 -20 1 525.18 18.85 0 -20 -1 568.82 18.83 0 -20 2 866.60 25.75 0 -20 -2 875.42 23.86 0 -20 3 56.73 7.37 0 -20 -3 54.18 6.22 0 20 3 65.46 8.66 0 20 3 54.68 8.04 0 20 4 364.14 22.73 0 -20 5 107.80 15.90 0 20 5 88.64 12.36 0 20 5 102.78 6.42 0 20 6 36.67 8.53 0 -20 6 55.83 5.25 0 -20 6 41.14 10.14 0 20 6 43.94 6.34 0 -20 7 1.14 0.85 0 -20 8 2.14 1.32 0 -20 9 19.59 3.06 0 -20 10 4.19 1.30 0 -21 0 27.93 4.33 0 -21 -1 286.41 13.84 0 -21 1 295.45 14.55 0 21 2 162.08 13.12 0 -21 2 187.28 12.45 0 -21 -2 185.43 11.29 0 21 3 11.51 3.68 0 -21 -3 15.70 3.49 0 21 3 8.29 3.12 0 -21 3 16.36 3.87 0 21 4 402.98 24.20 0 21 5 14.98 5.23 0 21 5 10.90 2.91 0 21 5 11.08 2.08 0 -21 5 14.36 2.44 0 -21 5 14.76 6.09 0 -21 6 96.11 6.91 0 21 6 74.61 8.40 0 -21 6 86.80 14.82 0 21 6 59.23 10.78 0 -21 7 7.80 1.88 0 -21 8 9.77 2.18 0 -21 9 19.49 2.99 0 -21 10 52.72 4.25 0 -22 0 37.47 5.26 0 -22 -1 503.61 19.00 0 -22 1 515.38 19.91 0 -22 -2 4.23 1.60 0 22 2 7.57 3.06 0 -22 2 2.37 1.37 0 22 3 4.14 2.24 0 22 3 3.44 2.07 0 22 4 11.08 4.08 0 -22 5 4.57 4.14 0 22 5 2.00 1.25 0 -22 5 1.50 0.70 0 22 5 0.51 0.74 0 -22 6 0.56 0.44 0 -22 6 -2.81 4.65 0 22 6 -2.65 1.65 0 22 6 -0.69 1.43 0 -22 7 146.69 8.77 0 22 7 116.25 10.78 0 -22 8 46.57 4.82 0 -22 9 3.99 1.37 0 -22 10 5.50 1.45 0 -22 10 3.64 1.48 0 -23 0 4.04 1.56 0 -23 1 81.92 8.26 0 -23 -1 80.09 7.80 0 -23 -2 189.28 12.35 0 -23 2 207.60 14.10 0 23 2 179.71 14.45 0 23 3 16.76 4.42 0 23 3 19.62 5.25 0 23 4 2.96 2.73 0 -23 5 160.23 8.85 0 23 5 134.09 10.91 0 -23 5 158.10 20.79 0 23 5 119.47 14.90 0 -23 6 -3.39 4.44 0 -23 6 1.75 0.96 0 23 6 2.65 2.71 0 23 6 1.94 1.17 0 -23 7 353.84 13.71 0 23 7 312.87 17.90 0 -23 8 10.71 2.29 0 -23 9 2.27 0.95 0 -23 10 39.73 3.47 0 -23 10 30.38 3.79 0 -24 0 62.56 7.11 0 -24 1 286.38 15.76 0 -24 -1 288.07 15.46 0 -24 2 170.78 13.15 0 -24 -2 155.45 11.72 0 24 2 161.87 13.96 0 24 3 62.31 9.28 0 24 3 39.65 7.36 0 24 4 246.99 19.87 0 24 5 34.18 8.22 0 -24 5 42.93 4.67 0 -24 5 42.44 11.04 0 24 5 34.07 5.57 0 -24 6 -0.74 0.89 0 24 6 -0.44 1.17 0 -24 6 0.12 4.05 0 24 7 4.53 1.98 0 -24 7 5.38 1.61 0 -24 8 1.24 0.55 0 -24 9 0.98 0.88 0 -24 10 3.08 1.05 0 -24 10 0.89 0.61 0 -25 0 0.84 1.14 0 -25 1 343.44 18.12 0 -25 -1 338.96 17.52 0 -25 2 600.15 25.87 0 -25 -2 575.14 23.80 0 25 3 46.19 8.35 0 25 3 50.58 8.35 0 25 4 434.69 18.98 0 -25 4 427.54 14.43 0 -25 5 126.00 19.39 0 25 5 117.67 10.54 0 -25 5 135.50 8.32 0 25 6 17.82 4.33 0 -25 6 17.56 2.96 0 -25 6 8.48 5.07 0 25 7 40.39 6.42 0 -25 7 42.16 4.67 0 -25 8 23.78 3.40 0 -25 9 31.18 3.47 0 -25 10 5.97 1.34 0 -26 0 675.35 25.72 0 -26 -1 176.06 12.95 0 -26 1 185.13 13.87 0 -26 -2 132.28 11.68 0 -26 2 127.66 12.49 0 26 3 53.50 8.96 0 26 3 54.15 8.87 0 -26 4 93.24 6.82 0 26 4 77.32 11.26 0 26 4 81.93 8.32 0 -26 5 354.73 33.29 0 26 5 382.98 19.27 0 -26 5 392.02 14.37 0 26 6 15.76 4.15 0 -26 6 14.77 2.83 0 26 7 14.16 3.83 0 -26 7 12.01 2.56 0 -26 8 0.92 1.00 0 -26 9 13.15 2.18 0 -26 10 20.84 2.26 0 -27 0 3.24 2.04 0 -27 -1 16.77 4.08 0 -27 1 12.51 3.58 0 27 2 96.99 11.34 0 27 3 525.30 28.21 0 27 3 610.04 30.59 0 27 4 0.33 0.85 0 -27 4 -2.10 1.10 0 -27 5 82.65 6.69 0 27 5 72.00 8.38 0 -27 5 60.59 14.28 0 27 6 1.55 1.68 0 -27 6 1.76 1.15 0 -27 7 1.14 0.60 0 27 7 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6 12.02 2.74 0 30 6 9.06 3.28 0 30 7 83.93 9.02 0 -30 7 94.88 6.75 0 -30 8 35.34 3.70 0 -30 9 13.30 1.90 0 31 0 1.37 0.67 0 31 -1 233.78 11.26 0 31 1 210.80 11.08 0 31 -2 7.04 1.96 0 31 2 5.61 1.80 0 31 3 1.83 0.45 0 31 -3 2.09 1.14 0 -31 4 3.77 1.52 0 31 4 0.82 0.67 0 31 -4 3.56 1.56 0 -31 5 131.41 8.50 0 31 5 122.35 10.99 0 -31 6 43.09 4.79 0 31 6 43.97 6.66 0 -31 7 2.59 1.18 0 31 7 0.32 0.63 0 -31 8 20.15 2.80 0 -31 9 3.74 1.03 0 32 0 14.48 2.91 0 32 1 646.67 19.59 0 32 -1 669.69 19.44 0 32 -2 11.45 2.58 0 32 3 -0.61 0.78 0 32 -3 1.97 1.22 0 -32 4 4.58 1.63 0 32 4 2.56 1.39 0 32 -4 3.28 1.54 0 -32 5 110.82 7.83 0 32 5 105.76 10.10 0 -32 6 0.43 0.99 0 32 6 0.11 0.67 0 -32 7 2.64 1.10 0 32 7 1.45 0.72 0 -32 8 9.44 1.79 0 -32 9 6.89 1.27 0 33 0 -0.33 0.67 0 33 -1 43.19 4.97 0 33 1 38.30 4.90 0 33 2 0.98 1.13 0 33 -2 0.04 0.58 0 33 -3 0.65 0.46 0 33 3 0.35 0.80 0 33 4 291.79 16.18 0 -33 4 304.00 13.26 0 33 -4 274.31 12.85 0 33 5 219.36 14.52 0 -33 5 244.18 11.58 0 33 6 42.63 6.38 0 -33 6 39.81 4.49 0 -33 7 9.02 2.00 0 33 7 9.89 2.86 0 -33 8 3.98 1.07 0 -33 9 10.90 1.51 0 34 0 79.22 6.87 0 34 1 53.12 5.63 0 34 -1 55.59 5.66 0 34 -2 3.88 1.69 0 34 2 7.95 2.62 0 34 -3 42.71 5.10 0 34 3 44.40 6.00 0 34 -4 1.39 0.75 0 34 4 0.26 0.75 0 34 5 35.57 5.80 0 -34 5 37.39 4.51 0 34 6 34.32 5.66 0 -34 6 32.10 3.88 0 -34 7 48.39 4.42 0 34 7 50.52 6.29 0 -34 8 -0.53 0.44 0 35 0 2.35 1.09 0 35 1 57.61 5.91 0 35 -1 69.02 6.39 0 35 -2 1.26 0.54 0 35 2 1.34 0.64 0 35 3 0.68 0.79 0 35 -3 0.07 1.22 0 35 4 -0.97 1.68 0 35 -4 -0.27 0.55 0 -35 4 1.60 1.04 0 35 5 0.00 1.29 0 -35 5 2.29 0.98 0 35 6 3.07 1.78 0 -35 6 1.06 0.54 0 -35 7 -0.22 0.73 0 35 7 -0.58 0.88 0 -35 8 11.22 1.76 0 36 0 251.46 12.30 0 36 -1 109.57 8.10 0 36 1 94.51 7.65 0 36 -2 35.40 4.62 0 36 2 38.35 5.47 0 36 3 45.64 6.12 0 36 -3 39.03 4.85 0 36 4 13.42 3.23 0 36 -4 13.75 2.84 0 36 5 -0.70 1.22 0 -36 5 0.43 0.65 0 -36 6 -1.23 1.30 0 36 6 0.32 0.74 0 -36 7 37.18 3.62 0 36 7 37.53 5.02 0 -36 8 5.74 1.16 0 37 0 3.22 1.60 0 37 1 1.09 1.37 0 37 -1 1.31 0.94 0 37 2 77.37 7.77 0 37 -2 75.40 6.79 0 37 3 13.27 3.32 0 37 -3 12.45 2.83 0 37 4 140.75 10.85 0 37 -4 128.72 8.80 0 -37 5 49.11 4.98 0 37 5 48.52 6.47 0 -37 6 11.50 2.12 0 37 6 12.93 3.19 0 -37 7 27.84 3.00 0 37 7 27.59 4.15 0 -37 8 3.87 0.88 0 38 0 152.84 9.64 0 38 -1 20.05 3.49 0 38 1 24.30 4.36 0 38 2 42.49 5.74 0 38 -2 39.70 5.03 0 38 3 82.23 8.07 0 38 -3 74.02 6.72 0 38 -4 43.45 5.04 0 38 4 55.88 6.86 0 -38 5 78.29 6.21 0 38 5 78.84 8.10 0 -38 6 1.97 0.55 0 38 6 2.27 1.41 0 -38 7 6.55 1.38 0 38 7 4.07 1.40 0 39 0 1.37 1.10 0 39 0 4.24 1.98 0 39 -1 1.75 0.81 0 39 1 3.52 1.82 0 39 2 364.53 16.76 0 39 -2 325.44 14.24 0 39 -3 0.65 0.95 0 39 3 1.06 1.05 0 39 4 27.26 4.66 0 39 -4 24.49 3.76 0 39 5 31.11 4.96 0 -39 6 1.40 0.61 0 39 6 2.19 1.15 0 -39 7 5.14 1.17 0 39 7 6.29 1.79 0 40 0 158.16 10.78 0 40 -1 39.89 4.90 0 40 -1 48.00 5.86 0 40 1 48.20 5.98 0 40 2 142.99 10.42 0 40 -2 127.44 8.80 0 40 3 -0.39 1.49 0 40 -3 0.82 0.69 0 40 4 47.73 6.12 0 40 -4 36.65 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2.44 0 46 3 8.20 2.14 0 46 4 11.71 2.55 0 46 5 9.40 2.02 0 47 0 -0.14 0.74 0 47 1 5.31 1.79 0 47 2 6.65 1.82 0 47 3 18.46 3.09 0 47 4 13.00 2.43 0 -47 -5 2.50 1.24 0 47 5 1.27 0.66 0 48 0 0.74 0.74 0 48 1 0.22 0.49 0 48 2 6.21 1.75 0 48 3 0.52 0.55 0 48 4 32.33 3.69 0 48 5 0.65 0.55 0 49 0 0.03 0.61 0 49 1 23.10 3.34 0 49 2 8.34 1.95 0 49 3 0.35 0.40 0 49 4 2.46 0.99 0 50 0 11.51 2.11 0 50 1 18.04 2.83 0 50 2 0.75 0.60 0 50 3 0.55 0.49 0 -51 0 0.79 0.50 0 51 1 25.98 3.00 0 51 2 1.67 0.78 0 -51 -3 90.03 6.45 0 51 3 66.38 4.52 -1 0 12 60.20 5.60 -1 0 11 3.08 1.21 -1 0 10 113.82 7.95 -1 0 9 -1.05 0.74 -1 0 8 84.54 11.57 -1 0 8 107.85 7.51 -1 0 7 0.01 1.16 -1 0 6 36.32 6.42 -1 0 5 0.24 1.50 -1 0 4 16.97 3.54 -1 0 3 2.75 0.41 -1 0 3 4.04 0.44 -1 0 2 374.60 7.46 -1 0 2 372.07 11.29 -1 0 1 0.58 0.32 -1 0 1 2.46 0.64 -1 0 0 97.41 4.18 1 0 1 0.53 0.41 1 0 1 0.12 0.38 -1 0 -2 566.72 10.99 1 0 2 599.16 16.25 -1 0 -3 0.56 0.20 1 0 3 0.74 0.50 1 0 4 91.36 8.52 1 0 4 92.49 8.85 1 0 5 1.42 1.64 1 0 5 0.66 1.05 1 0 6 690.02 29.30 1 0 7 0.17 0.75 1 0 7 2.12 1.30 1 0 7 2.38 1.91 1 0 8 165.94 9.27 1 0 8 187.27 9.34 1 0 9 16.94 3.08 1 0 11 0.75 1.07 -1 -1 12 10.61 2.45 -1 1 12 8.52 2.09 -1 1 11 1.37 0.78 -1 -1 11 1.57 1.05 -1 -1 10 5.50 1.97 -1 1 10 6.29 2.26 -1 1 9 14.34 2.83 -1 -1 9 15.17 2.98 -1 1 8 120.44 7.94 -1 1 8 104.88 12.85 -1 -1 8 110.99 13.46 -1 -1 8 128.99 8.20 -1 -1 7 390.49 23.79 -1 1 7 376.29 22.67 -1 -1 6 546.15 25.44 -1 1 6 533.49 24.84 -1 -1 5 294.39 16.74 -1 1 5 303.62 16.64 -1 1 4 2398.94 42.68 -1 -1 4 2298.18 42.30 -1 1 3 392.46 13.24 -1 1 3 327.18 13.12 -1 -1 3 322.26 5.22 -1 -1 3 332.87 13.28 -1 1 2 1330.59 22.06 -1 -1 2 1325.77 22.38 -1 1 2 1304.59 14.37 -1 1 1 2197.81 21.50 -1 1 1 2198.06 20.97 -1 1 0 327.71 7.86 1 -1 0 355.06 6.26 1 -1 1 3508.41 35.50 1 -1 1 3592.56 34.00 -1 1 -1 3511.98 30.91 1 1 1 3501.80 32.81 1 1 1 3564.67 35.19 1 -1 2 4.88 1.48 -1 -1 -2 3.50 0.82 -1 1 -2 4.23 0.82 1 -1 2 3.20 1.04 1 1 2 3.13 1.01 1 1 2 3.39 1.41 -1 -1 -3 7.79 0.97 1 1 3 12.73 2.85 1 -1 3 11.04 2.71 -1 1 -3 7.31 0.74 1 1 3 12.41 2.81 1 -1 3 9.73 2.47 1 1 4 26.81 4.62 1 -1 4 19.83 4.21 1 1 4 25.65 4.63 1 -1 4 25.45 4.38 1 1 5 3.61 1.72 1 -1 5 4.12 2.16 1 1 5 4.81 2.33 1 -1 6 21.52 5.34 1 1 6 20.26 5.15 1 -1 7 15.96 2.85 1 -1 7 16.07 4.76 1 1 7 15.62 2.74 1 -1 7 23.09 3.24 1 1 7 24.80 3.29 1 -1 8 0.73 0.96 1 -1 8 -0.06 1.33 1 1 8 1.30 1.03 1 1 8 0.07 1.00 1 -1 9 18.09 3.06 1 1 9 21.23 3.21 1 -1 11 11.09 2.46 1 1 11 11.41 2.36 -1 2 12 2.44 1.14 -1 -2 11 13.58 2.49 -1 2 11 11.86 2.26 -1 -2 10 71.84 6.33 -1 2 10 67.79 6.10 -1 -2 9 0.51 1.44 -1 2 9 0.53 1.02 -1 2 8 131.16 8.32 -1 2 8 111.41 13.06 -1 2 8 160.05 8.22 -1 -2 8 114.19 13.98 -1 -2 8 149.37 8.83 -1 2 7 130.57 13.23 -1 -2 7 140.58 14.29 -1 2 6 0.84 0.72 -1 -2 6 1.17 1.28 -1 2 5 825.97 27.61 -1 -2 5 841.03 28.55 -1 -2 4 136.61 10.18 -1 2 4 128.91 9.53 -1 2 4 139.92 9.36 -1 2 3 870.41 8.80 -1 -2 3 934.13 10.48 -1 -2 3 975.10 23.23 -1 2 3 1124.34 22.51 -1 2 3 981.25 22.79 -1 -2 2 1693.76 25.97 -1 2 2 1665.82 25.03 -1 2 2 1640.76 16.69 -1 2 1 3300.08 27.72 -1 2 1 3254.17 26.83 1 -2 0 600.61 8.36 -1 2 0 573.56 10.63 1 2 1 5469.42 47.20 1 2 1 5590.79 47.12 -1 2 -1 5519.16 41.45 1 2 1 5505.74 43.61 1 -2 2 711.45 18.49 1 2 2 726.99 18.65 -1 2 -2 675.68 11.12 1 -2 2 729.10 18.60 1 2 2 698.21 17.41 1 -2 3 2623.78 41.22 1 -2 3 2558.66 41.94 1 2 3 2642.19 42.04 1 2 3 2707.02 41.41 1 2 4 1.69 0.83 1 -2 4 1.27 1.34 1 -2 4 -0.45 0.81 1 2 4 0.24 0.65 1 2 5 95.25 9.75 1 -2 5 91.66 10.02 1 2 5 84.37 9.33 1 -2 6 32.93 6.47 1 2 6 43.39 7.20 1 2 7 6.78 1.92 1 -2 7 4.96 1.54 1 -2 7 1.30 1.50 1 -2 7 4.48 1.32 1 -2 8 -0.19 1.32 1 2 8 2.95 1.15 1 -2 8 3.99 1.76 1 -2 9 12.92 2.55 1 2 9 36.55 4.29 1 2 11 15.95 2.79 1 -2 11 16.56 2.98 -1 3 11 0.56 0.48 -1 -3 11 0.39 0.53 -1 3 10 1.73 1.19 -1 -3 10 -0.05 0.86 -1 -3 9 76.61 6.59 -1 3 9 71.58 6.42 -1 3 8 81.56 11.24 -1 -3 8 71.25 11.08 -1 3 8 100.10 6.60 -1 -3 8 98.40 7.21 -1 3 8 80.48 6.51 -1 3 7 4.57 2.21 -1 -3 7 5.33 2.48 -1 3 6 114.37 11.27 -1 -3 6 127.72 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11.72 4 8 1 38.31 6.53 -4 8 -1 34.52 4.81 4 8 2 24.62 5.55 -4 8 -2 23.51 3.88 -4 -8 -2 26.48 5.56 4 8 2 22.12 5.34 4 8 3 156.59 15.45 4 8 4 78.83 8.60 4 8 4 70.21 5.40 4 -8 4 65.04 5.82 4 8 4 60.98 10.80 4 8 4 71.65 5.09 4 -8 5 21.81 3.42 4 8 5 24.31 3.26 4 8 5 19.14 6.34 4 8 5 26.08 5.24 4 8 5 25.94 3.30 4 -8 6 63.40 6.04 4 8 6 68.49 8.30 4 -8 6 56.08 8.01 4 -8 6 49.87 5.08 4 8 6 70.84 5.68 4 8 7 -0.83 0.95 4 -8 7 -0.22 0.78 4 8 7 -0.78 1.63 4 -8 7 -0.85 2.13 4 8 7 0.96 0.53 4 -8 8 13.11 3.24 4 8 8 12.51 2.85 4 -8 9 10.40 2.50 -4 -9 13 0.15 0.30 -4 9 12 1.01 0.80 -4 -9 12 1.94 0.89 -4 9 11 46.80 5.33 -4 -9 11 52.77 5.08 -4 -9 10 1.01 0.74 -4 9 10 0.55 0.60 -4 9 9 34.70 5.12 -4 -9 9 29.88 7.70 -4 -9 9 41.29 4.52 4 9 -9 32.89 4.20 -4 9 8 57.23 6.67 4 9 -8 47.69 4.78 -4 -9 8 55.39 10.22 -4 -9 7 21.81 5.80 -4 -9 6 28.44 6.04 -4 -9 5 240.89 16.32 -4 9 5 255.89 11.19 -4 9 4 74.66 6.39 -4 9 3 216.65 11.34 -4 9 2 43.71 5.08 -4 9 1 60.50 6.32 -4 9 0 31.36 4.54 4 9 1 12.05 3.68 -4 9 -1 0.63 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19.44 -4 12 -1 272.44 13.10 4 12 2 71.50 10.56 -4 12 -2 61.24 6.11 4 12 2 77.07 10.79 4 12 3 17.94 5.74 4 -12 4 88.54 6.91 4 12 4 87.85 5.88 4 12 4 83.44 13.44 4 12 4 95.58 5.88 4 12 5 11.18 2.22 4 -12 5 15.11 4.12 4 -12 5 11.37 2.62 4 12 5 13.75 2.62 4 12 6 2.34 1.09 4 -12 6 0.43 1.57 4 -12 6 0.39 0.80 4 -12 6 -0.12 1.18 4 12 6 0.75 0.58 4 -12 7 37.48 6.14 4 -12 7 29.48 3.68 4 12 7 34.80 3.82 4 -12 8 -0.15 1.25 4 -12 9 3.96 1.44 -4 13 12 9.69 1.80 -4 -13 12 10.44 1.93 -4 -13 11 0.95 0.88 -4 13 11 2.23 1.00 -4 -13 10 5.61 1.82 -4 13 10 4.19 2.31 -4 13 9 32.53 5.37 4 13 -9 27.46 3.78 -4 -13 9 30.56 3.91 -4 13 8 11.63 3.22 -4 -13 8 12.22 2.42 -4 -13 8 7.48 3.58 4 13 -8 10.08 2.24 -4 -13 7 202.26 19.15 -4 13 7 198.49 13.11 4 13 -7 167.49 8.55 -4 -13 6 3.69 2.51 -4 -13 6 8.35 2.30 -4 -13 5 528.25 27.24 -4 13 5 512.93 16.34 -4 13 4 10.52 2.38 -4 13 3 5.55 1.84 -4 13 2 280.62 12.91 -4 13 1 137.52 9.21 -4 13 0 620.74 19.78 4 13 1 2.18 2.33 -4 13 -1 1.70 1.07 4 13 2 0.96 1.48 4 13 2 3.27 1.96 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18 3 22.93 7.32 4 -18 4 41.42 6.43 4 -18 4 48.75 5.26 4 18 4 42.81 10.55 4 18 4 45.08 4.10 4 18 4 51.29 4.47 4 18 5 6.91 1.43 4 -18 5 6.02 1.78 4 18 5 13.43 2.73 4 -18 5 7.03 3.00 4 -18 6 24.54 4.84 4 -18 6 25.17 3.65 4 18 6 27.33 3.52 4 18 6 30.06 3.40 4 -18 7 30.63 4.89 4 -18 7 31.00 3.60 4 -18 8 13.06 2.78 4 -18 8 11.68 1.85 -4 -19 12 3.12 0.90 -4 19 11 1.27 1.01 -4 -19 11 3.12 1.18 -4 -19 10 9.14 2.11 -4 19 10 5.69 2.08 -4 19 9 0.22 0.65 -4 -19 9 1.30 1.00 -4 -19 8 11.54 2.42 -4 19 8 11.98 3.62 -4 -19 8 6.64 4.64 -4 -19 7 0.68 0.79 4 -19 -7 1.11 1.51 -4 19 7 0.19 0.89 -4 -19 7 1.47 2.09 4 19 -7 1.74 0.95 -4 -19 6 7.36 2.65 -4 -19 6 9.40 4.97 -4 19 6 6.28 2.50 4 19 -6 5.21 1.43 -4 -19 5 178.74 10.94 -4 19 5 170.38 10.50 -4 19 4 47.12 5.46 -4 19 3 -0.22 0.79 -4 19 2 497.89 18.14 -4 19 1 1.93 1.32 -4 19 0 138.98 9.83 4 19 1 156.58 17.38 -4 19 -1 140.63 9.86 -4 19 -2 16.20 3.50 4 19 2 21.83 6.92 4 -19 2 16.45 2.80 4 19 2 13.94 2.04 4 19 2 19.22 6.40 4 -19 3 26.89 5.06 4 -19 3 40.63 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21.85 3.26 4 22 4 19.09 2.64 4 -22 5 159.17 11.91 4 -22 5 172.77 9.72 4 22 5 175.03 7.83 4 -22 6 10.81 2.71 4 -22 6 9.97 2.27 4 22 6 8.51 1.85 4 -22 7 2.39 0.94 4 -22 7 0.10 0.68 4 -22 8 10.78 1.61 -4 23 11 1.29 1.03 -4 -23 11 0.96 0.53 -4 23 10 4.49 1.70 -4 -23 10 7.24 1.85 -4 23 9 16.23 4.13 -4 -23 9 19.34 3.10 -4 23 8 21.89 5.03 -4 -23 8 24.52 3.62 4 -23 -7 5.36 2.93 -4 23 7 7.66 3.05 -4 -23 7 7.00 5.15 -4 -23 6 24.17 5.00 -4 -23 6 26.24 9.15 -4 23 6 19.87 4.71 -4 23 5 100.60 10.33 -4 -23 5 113.81 9.83 -4 -23 4 292.43 14.65 -4 23 4 271.19 14.46 -4 23 3 437.08 18.09 -4 23 2 68.69 7.12 -4 23 1 0.66 1.25 -4 23 0 31.23 4.97 -4 23 -1 0.48 0.70 4 23 1 0.22 0.37 4 -23 1 1.95 1.26 4 23 2 20.85 7.60 4 -23 2 40.51 4.62 4 23 2 34.74 3.45 4 23 2 20.77 7.35 4 23 3 329.29 11.23 4 -23 3 325.73 13.39 4 -23 4 198.73 10.53 4 23 4 184.00 8.00 4 -23 5 139.00 10.87 4 -23 5 150.96 9.02 4 23 5 155.96 7.26 4 23 5 161.33 8.17 4 -23 6 7.19 2.24 4 -23 6 6.33 1.82 4 23 6 4.52 1.21 4 -23 7 10.84 1.94 4 -23 7 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39.48 6.60 5 3 3 26.82 6.19 5 -3 3 32.10 6.23 5 3 3 31.06 3.41 5 3 4 15.32 5.12 5 3 4 32.33 5.98 5 -3 4 27.75 5.54 5 3 4 27.64 3.41 5 -3 5 194.10 10.49 5 3 5 203.92 15.02 5 -3 5 187.01 14.67 5 3 5 183.37 9.74 5 3 5 191.65 9.38 5 -3 6 4.37 1.88 5 3 6 2.77 2.47 5 -3 6 6.80 2.70 5 3 6 5.91 1.88 5 3 7 4.93 1.55 5 3 7 0.22 1.16 5 -3 7 1.48 0.99 5 -3 7 3.23 1.12 5 3 8 6.28 2.03 5 -3 8 6.29 1.94 5 -3 8 12.08 1.85 -5 -4 13 66.97 4.57 -5 4 13 65.11 4.66 -5 -4 12 1.42 0.68 -5 4 12 0.27 0.98 5 4 -11 192.22 9.56 -5 -4 11 219.51 10.85 -5 4 11 210.46 11.13 5 -4 -11 164.37 9.19 -5 4 11 162.68 9.54 5 4 -10 34.36 4.44 -5 4 10 39.01 5.11 -5 -4 9 18.99 5.69 -5 4 9 16.04 4.78 -5 -4 9 21.56 3.71 -5 4 9 20.10 3.75 -5 -4 8 1.96 1.23 -5 4 8 2.70 1.63 -5 -4 8 2.31 1.87 -5 4 8 0.65 2.28 -5 -4 7 34.70 6.73 -5 4 7 34.13 6.05 -5 -4 6 14.74 3.95 -5 4 6 15.72 3.63 -5 -4 6 10.41 2.84 -5 4 6 13.97 2.92 -5 -4 5 62.72 7.36 -5 4 5 71.29 6.95 -5 -4 5 68.84 7.37 -5 4 5 75.82 7.27 -5 -4 4 21.45 3.78 -5 4 4 24.00 3.28 -5 -4 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3.24 5 5 -10 16.10 3.00 -5 -5 10 17.00 3.09 -5 -5 9 1.12 0.83 -5 5 9 2.19 1.56 -5 -5 9 0.43 0.99 -5 -5 8 1.36 0.89 -5 5 8 1.19 1.43 -5 -5 8 0.75 1.37 -5 5 8 0.23 1.36 -5 -5 7 0.63 1.64 -5 5 7 2.03 1.78 -5 -5 6 74.61 9.07 -5 5 6 81.66 8.35 -5 -5 6 76.40 7.73 -5 5 6 89.15 7.42 -5 -5 5 191.67 13.02 -5 5 5 222.42 12.13 -5 -5 5 201.81 12.94 -5 5 5 208.34 11.99 -5 -5 4 0.56 1.23 -5 -5 4 0.63 1.23 -5 5 4 1.29 1.14 -5 -5 3 106.50 7.62 -5 -5 3 127.37 10.68 -5 5 3 123.62 9.56 -5 -5 2 4.79 0.96 -5 5 2 6.02 2.26 5 5 -1 55.67 7.03 -5 -5 1 44.18 6.83 -5 5 1 38.03 5.64 5 5 0 102.12 9.81 -5 -5 0 120.55 11.68 -5 5 0 117.50 10.35 5 -5 0 93.52 7.41 5 5 1 107.63 10.99 -5 -5 -1 107.59 11.65 -5 5 -1 112.49 10.32 5 -5 1 99.77 8.61 5 5 1 111.82 11.10 5 -5 2 10.02 3.10 -5 -5 -2 1.85 1.50 5 5 2 7.88 3.47 5 -5 3 105.50 10.72 5 5 3 86.63 11.82 5 5 3 101.40 6.09 5 5 4 18.06 4.42 5 -5 4 14.57 4.21 5 5 4 11.10 2.17 5 5 4 9.31 4.46 5 5 4 16.71 2.68 5 5 5 3.76 2.16 5 -5 5 5.68 2.82 5 5 5 3.02 0.87 5 5 5 3.78 1.30 5 5 6 2.27 1.85 5 -5 6 1.99 1.13 5 -5 6 1.62 1.36 5 5 6 2.52 1.03 5 5 6 0.99 1.48 5 5 7 0.40 1.17 5 -5 7 1.25 0.91 5 -5 7 -0.67 0.94 5 5 7 -1.50 1.28 5 -5 8 12.46 2.83 5 -5 8 13.11 1.78 -5 -6 13 1.60 0.73 -5 6 13 -0.43 0.37 -5 -6 12 5.97 1.58 -5 6 12 4.21 1.55 -5 -6 11 0.82 0.88 -5 6 11 0.27 0.40 5 6 -11 -0.65 1.14 -5 6 10 96.27 8.18 5 6 -10 108.17 7.64 -5 -6 10 121.87 7.98 -5 -6 9 79.73 6.95 -5 -6 9 61.30 10.59 -5 6 9 77.97 7.57 5 6 -9 70.33 6.22 -5 -6 8 60.60 9.90 -5 6 8 72.47 9.61 -5 6 8 83.98 7.85 -5 -6 8 74.44 6.76 -5 -6 7 51.48 8.49 -5 6 7 54.30 7.52 -5 -6 6 186.40 14.67 -5 6 6 197.35 13.01 -5 -6 6 176.29 12.20 -5 6 6 200.65 11.10 -5 -6 5 186.56 13.05 -5 6 5 225.70 12.29 -5 -6 5 198.67 12.94 -5 6 5 213.44 12.01 -5 -6 4 4.97 2.03 -5 -6 4 2.33 0.96 -5 6 4 2.03 1.13 -5 -6 3 229.80 11.71 -5 -6 3 257.95 15.54 -5 6 3 263.01 13.97 -5 -6 2 -1.69 2.33 -5 6 2 1.74 1.11 -5 6 1 20.75 4.19 -5 -6 1 20.46 4.75 5 6 0 58.45 7.65 -5 -6 0 48.66 7.62 -5 6 0 50.21 6.78 5 6 1 132.77 12.52 -5 -6 -1 168.04 14.62 -5 6 -1 164.13 12.32 5 -6 1 128.60 9.72 5 6 1 141.45 12.86 5 -6 2 118.41 10.36 5 6 2 116.89 12.71 5 6 3 15.89 4.07 5 -6 3 12.46 3.99 5 6 3 12.80 2.14 5 6 3 10.43 4.03 5 6 4 172.98 13.60 5 -6 4 127.38 12.25 5 6 4 105.97 14.12 5 6 4 127.01 7.79 5 6 4 155.55 7.98 5 6 5 11.40 3.78 5 -6 5 8.93 3.49 5 6 5 11.11 2.17 5 6 5 8.46 2.01 5 -6 6 17.20 2.91 5 -6 6 16.53 4.51 5 6 6 21.84 3.30 5 6 6 19.56 3.01 5 6 6 15.39 3.93 5 6 7 -0.74 0.68 5 -6 7 0.05 1.34 5 -6 7 1.56 0.91 5 6 7 0.45 0.57 5 -6 8 12.86 2.75 5 -6 8 13.20 1.70 -5 -7 13 0.95 0.61 -5 7 13 1.70 0.84 -5 -7 12 7.22 1.76 -5 7 12 7.59 1.98 -5 -7 11 46.77 4.91 5 7 -11 41.62 4.34 -5 7 11 33.22 4.44 -5 7 10 62.59 6.65 -5 -7 10 72.94 6.16 5 7 -10 63.92 5.98 -5 7 9 13.01 3.23 -5 -7 9 13.05 5.27 5 7 -9 16.37 2.97 -5 7 8 28.45 4.73 -5 -7 8 27.09 6.74 -5 -7 8 24.49 3.90 -5 -7 7 5.63 2.93 -5 7 6 7.51 2.14 -5 -7 6 5.57 2.79 -5 -7 6 5.74 2.21 -5 -7 5 388.73 19.55 -5 -7 5 379.80 18.39 -5 7 5 423.16 16.80 -5 -7 4 59.85 7.14 -5 -7 4 53.62 7.30 -5 7 4 57.49 6.41 -5 7 3 0.97 0.68 -5 7 2 111.22 9.43 -5 -7 1 13.28 3.95 -5 7 1 18.99 3.97 5 7 0 745.25 28.58 -5 -7 0 730.35 29.81 -5 7 0 743.30 25.88 5 7 1 42.33 7.21 -5 -7 -1 46.95 7.85 -5 7 -1 53.71 6.97 5 7 1 38.70 6.86 -5 -7 -2 42.03 7.63 5 7 2 48.07 8.40 5 -7 3 166.08 13.51 5 7 3 136.38 15.69 5 7 3 156.63 7.57 5 7 4 22.93 3.22 5 7 4 28.01 3.38 5 7 4 26.78 5.36 5 -7 4 23.69 5.46 5 7 4 16.20 5.07 5 7 5 72.19 8.66 5 -7 5 54.60 7.79 5 7 5 69.93 5.71 5 7 5 60.48 5.29 5 7 6 13.92 3.70 5 -7 6 10.89 3.47 5 -7 6 13.23 2.80 5 7 6 16.47 2.92 5 7 6 17.68 2.85 5 7 7 7.73 1.69 5 -7 7 6.26 2.31 5 7 7 7.13 2.28 5 -7 7 8.82 1.84 5 -7 8 2.17 1.55 5 7 8 24.46 2.61 -5 -8 13 53.00 3.83 -5 8 13 45.76 3.60 -5 8 12 12.47 2.54 -5 -8 12 14.54 2.49 -5 8 11 1.35 0.70 -5 -8 11 1.81 1.01 5 8 -11 1.60 1.11 5 8 -10 6.02 1.82 -5 8 10 6.77 2.22 -5 -8 10 9.22 2.17 -5 8 9 4.05 1.76 -5 -8 9 0.57 1.23 5 8 -9 2.17 1.06 -5 -8 8 156.41 16.50 5 8 -8 144.71 8.58 -5 8 8 177.20 11.82 -5 -8 8 170.96 10.35 -5 -8 7 96.10 11.86 -5 8 6 5.91 2.11 -5 -8 6 4.17 2.11 -5 -8 6 2.88 1.35 -5 -8 5 140.98 12.09 -5 -8 5 132.59 11.16 -5 8 5 147.53 9.78 -5 -8 4 200.62 13.34 -5 -8 4 192.49 13.80 -5 8 4 202.69 11.97 -5 8 3 390.72 17.19 -5 8 2 13.61 3.25 -5 8 1 59.52 6.98 5 8 0 3.25 2.89 -5 -8 0 4.06 2.67 -5 8 0 5.78 2.45 5 8 1 1.44 1.77 5 8 1 -0.60 1.78 -5 -8 -1 -0.20 1.70 -5 8 -1 1.63 1.48 -5 -8 -2 115.44 12.88 5 8 2 113.40 13.04 5 8 3 63.98 7.91 5 -8 3 49.37 7.42 5 8 3 50.52 9.73 5 8 3 52.80 4.33 5 8 4 37.44 6.30 5 -8 4 28.45 5.69 5 8 4 21.53 6.78 5 8 4 23.38 3.26 5 8 4 31.33 3.57 5 8 5 2.44 1.26 5 8 5 2.45 1.66 5 -8 5 -0.03 1.31 5 8 5 3.82 1.37 5 8 6 117.81 7.12 5 -8 6 94.86 10.07 5 8 6 105.82 9.91 5 -8 6 105.78 7.47 5 8 6 115.73 7.53 5 8 7 6.44 1.62 5 -8 7 5.72 1.52 5 8 7 6.35 2.21 5 -8 7 3.60 1.83 5 -8 8 2.39 1.17 -5 9 13 1.16 0.72 -5 -9 13 0.44 0.48 -5 9 12 0.55 0.94 -5 -9 12 0.44 0.59 -5 -9 11 9.21 2.14 -5 9 11 9.10 2.35 5 9 -11 9.27 2.07 -5 9 10 17.26 3.57 5 9 -10 20.25 3.29 -5 -9 10 20.40 3.27 -5 9 9 6.03 2.55 -5 -9 9 9.57 5.26 -5 -9 9 7.58 2.12 5 9 -9 5.06 1.71 -5 -9 8 34.25 7.95 -5 9 8 39.76 5.78 5 9 -8 35.92 4.23 -5 -9 7 13.87 4.47 -5 -9 6 150.03 13.98 -5 -9 6 144.08 11.61 -5 9 6 168.11 9.90 -5 -9 5 440.99 22.24 -5 -9 5 417.19 20.43 -5 9 5 432.23 16.80 -5 -9 4 165.62 12.40 -5 9 4 170.87 10.95 -5 9 3 845.94 25.51 -5 9 2 1195.62 30.95 -5 9 1 349.72 17.06 5 9 0 1138.14 37.57 -5 9 0 989.50 29.46 5 9 1 5.81 2.78 5 9 1 12.79 4.34 -5 -9 -1 11.03 4.07 -5 9 -1 13.46 3.60 -5 -9 -2 123.30 13.32 5 9 2 113.29 13.57 5 9 3 16.35 4.50 5 -9 3 7.94 2.83 5 9 3 7.05 1.62 5 -9 3 6.06 1.83 5 9 3 6.60 3.69 5 9 3 8.50 1.77 5 9 4 38.08 4.10 5 -9 4 43.05 7.04 5 -9 4 33.37 4.28 5 9 4 38.81 9.11 5 9 4 42.06 4.14 5 9 4 48.28 7.09 5 -9 5 0.82 1.27 5 9 5 2.79 1.60 5 9 5 -0.48 2.01 5 9 5 1.09 0.98 5 9 6 5.93 2.35 5 -9 6 6.62 1.82 5 -9 6 3.33 2.16 5 9 6 7.92 2.12 5 9 6 3.72 1.45 5 9 7 3.14 1.23 5 -9 7 1.51 0.88 5 9 7 -0.60 0.84 5 -9 7 2.39 1.48 5 -9 8 18.44 3.24 -5 -10 13 1.09 0.63 -5 10 12 0.84 0.67 -5 -10 12 2.45 1.11 -5 -10 11 55.67 5.09 5 10 -11 53.35 4.94 -5 10 11 46.42 5.33 -5 10 10 2.29 1.42 -5 -10 10 3.99 1.58 5 10 -10 4.34 1.63 5 10 -9 217.87 10.72 -5 10 9 208.76 13.18 -5 -10 9 218.15 10.24 5 10 -8 27.38 3.67 -5 -10 8 28.19 7.40 -5 10 8 27.59 4.83 -5 -10 7 82.24 11.47 5 10 -7 71.12 5.60 -5 10 7 91.71 8.60 -5 -10 6 103.26 11.86 -5 -10 6 88.70 9.30 -5 10 6 115.90 8.27 -5 -10 5 7.01 3.23 -5 -10 5 3.77 2.02 -5 10 5 4.47 1.63 -5 -10 4 87.02 9.30 -5 10 4 92.34 7.99 -5 10 3 203.65 12.27 -5 10 2 469.33 19.10 -5 10 1 103.41 9.18 5 10 0 -0.36 0.86 -5 10 0 -0.83 1.16 5 10 1 435.14 25.46 -5 -10 -1 380.85 23.17 -5 10 -1 420.03 18.78 5 10 1 396.05 24.00 -5 -10 -2 97.68 11.97 5 10 2 123.79 14.45 5 10 3 0.30 1.17 5 -10 3 -0.31 1.17 5 10 3 -3.32 1.24 5 -10 3 0.07 0.36 5 10 3 0.70 0.48 5 10 3 -1.19 1.82 5 10 4 -0.97 0.95 5 10 4 1.69 1.10 5 -10 4 0.05 1.70 5 -10 4 -0.08 1.00 5 10 4 -1.10 1.70 5 10 4 0.74 0.49 5 10 5 9.40 2.14 5 10 5 6.40 2.18 5 -10 5 6.88 2.87 5 -10 5 3.49 1.41 5 10 5 11.36 2.39 5 10 6 11.90 2.28 5 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5 -11 4 46.00 7.15 5 -11 4 36.83 4.53 5 11 4 53.29 5.00 5 11 4 59.33 4.95 5 11 5 31.08 5.46 5 -11 5 21.89 5.02 5 -11 5 17.87 3.04 5 11 5 26.09 3.46 5 11 5 21.96 3.11 5 -11 6 25.01 3.40 5 11 6 24.97 4.52 5 -11 6 23.23 4.81 5 11 6 28.77 3.35 5 11 6 27.78 3.65 5 -11 7 -0.50 0.58 5 -11 7 0.17 1.12 5 -11 8 -0.11 0.90 -5 -12 13 5.75 1.17 -5 12 12 7.15 1.79 -5 -12 12 7.48 1.67 -5 -12 11 10.12 2.14 -5 12 11 6.50 1.98 -5 12 10 8.91 2.73 5 12 -10 9.94 2.24 -5 -12 10 8.33 2.03 5 12 -9 1.44 0.95 -5 12 9 2.09 1.33 -5 -12 9 2.15 0.97 -5 12 8 -0.12 1.02 -5 -12 8 -0.45 2.12 -5 -12 8 1.83 1.01 5 12 -8 0.14 0.43 -5 12 7 0.91 1.31 -5 -12 7 2.55 1.35 -5 12 7 1.25 1.01 5 12 -7 -0.13 0.47 -5 -12 6 25.75 6.32 -5 12 6 33.66 4.53 -5 -12 6 26.76 5.37 -5 -12 5 147.10 14.09 -5 12 5 153.94 9.96 -5 12 4 152.87 10.26 -5 12 3 42.19 5.49 -5 12 2 424.88 17.99 -5 12 1 1.35 1.08 5 12 0 489.96 27.26 -5 12 0 411.82 18.36 -5 12 -1 1.03 1.39 5 12 1 0.51 2.27 5 12 1 2.58 2.63 5 12 2 28.24 3.02 -5 -12 -2 25.85 6.51 5 12 2 29.55 7.73 5 12 3 38.26 6.05 5 -12 3 34.43 6.17 5 -12 3 30.58 4.10 5 12 3 33.82 8.77 5 12 3 37.74 3.68 5 12 3 35.80 3.91 5 12 4 -0.25 0.85 5 12 4 -1.17 1.35 5 -12 4 1.20 1.05 5 -12 4 1.32 0.94 5 12 4 2.90 1.17 5 12 5 3.98 1.50 5 -12 5 1.39 0.95 5 -12 5 2.13 0.89 5 12 5 4.11 1.51 5 12 5 0.87 1.56 5 -12 6 16.55 2.73 5 -12 6 13.52 3.56 5 12 6 16.15 2.43 5 -12 6 8.78 1.92 5 12 6 16.30 2.69 5 -12 7 0.76 1.09 5 12 7 11.81 2.22 5 -12 8 0.24 0.64 -5 -13 13 11.00 1.56 -5 13 12 12.79 2.36 -5 -13 12 14.07 2.26 -5 13 11 -0.39 0.80 -5 -13 11 1.47 1.20 5 13 -10 20.51 3.33 -5 13 10 14.96 3.61 -5 -13 10 16.51 2.93 -5 13 9 4.26 2.05 -5 -13 9 4.76 1.55 5 13 -9 4.57 1.51 -5 13 8 66.72 7.90 -5 -13 8 56.66 10.87 -5 13 8 60.89 7.04 -5 -13 8 62.51 5.38 5 13 -8 65.09 5.73 -5 13 7 62.63 7.54 -5 -13 7 49.31 9.56 5 13 -7 52.82 4.86 -5 13 7 47.27 5.94 -5 -13 6 -1.95 1.91 -5 13 6 2.24 1.37 -5 -13 5 60.66 9.31 -5 13 5 57.69 6.05 -5 13 4 64.93 6.62 -5 13 3 2.97 1.29 -5 13 2 64.98 6.94 -5 13 1 527.59 20.48 5 13 0 15.82 5.45 -5 13 0 19.32 4.00 5 13 1 29.38 7.28 -5 13 -1 30.92 5.01 5 -13 2 2.81 1.53 5 -13 2 0.96 0.92 5 13 2 0.48 1.56 -5 -13 -2 -1.21 1.52 5 13 2 -2.85 2.42 5 13 2 0.29 0.54 5 13 3 1.34 0.78 5 -13 3 2.24 1.58 5 -13 3 2.99 1.56 5 13 3 1.58 1.89 5 13 3 2.93 1.17 5 -13 4 22.89 5.07 5 -13 4 19.83 3.40 5 13 4 20.46 2.94 5 13 4 24.02 3.13 5 -13 5 11.26 3.78 5 -13 5 8.22 2.16 5 13 5 9.55 2.23 5 13 5 9.52 2.11 5 -13 6 48.31 6.79 5 -13 6 39.21 4.18 5 13 6 48.54 4.21 5 13 6 58.75 5.11 5 -13 6 50.43 4.80 5 13 7 16.39 2.57 5 -13 7 3.03 1.63 5 -13 8 13.49 2.62 -5 -14 12 41.64 3.67 -5 14 12 41.49 4.05 -5 14 11 5.50 1.91 -5 -14 11 6.98 1.68 -5 14 10 149.18 11.14 5 14 -10 178.08 9.57 -5 -14 10 168.32 8.89 5 14 -9 0.49 0.66 -5 -14 9 0.29 0.71 -5 14 9 -0.86 1.70 5 14 -8 0.95 0.96 -5 14 8 2.68 1.65 -5 14 8 0.70 1.02 -5 -14 8 -1.26 3.56 -5 -14 8 2.31 1.38 -5 14 7 24.36 4.79 -5 -14 7 24.83 7.23 5 14 -7 25.88 3.42 -5 14 7 21.09 4.03 -5 -14 7 21.58 3.07 -5 -14 6 105.57 13.65 -5 14 6 118.02 8.58 -5 -14 5 183.57 16.80 -5 14 5 203.59 11.54 -5 14 4 2.25 1.31 -5 14 3 773.77 23.61 -5 14 2 279.55 14.36 -5 14 1 91.15 8.46 5 14 0 140.36 15.25 -5 14 0 124.25 9.94 5 14 1 5.74 3.48 -5 14 -1 7.15 2.48 5 14 2 0.65 0.41 5 14 2 -0.12 0.78 5 -14 2 1.97 1.83 5 -14 2 -0.28 0.49 5 14 2 0.99 2.03 5 14 2 1.08 2.18 5 14 3 36.92 3.85 5 -14 3 37.09 6.33 5 -14 3 35.50 4.42 5 14 3 39.24 9.83 5 14 3 37.88 3.64 5 14 4 4.48 1.44 5 -14 4 4.50 2.10 5 -14 4 5.34 1.70 5 14 4 4.83 1.40 5 -14 5 77.37 9.10 5 -14 5 64.94 5.85 5 14 5 78.66 5.61 5 -14 6 2.92 1.30 5 14 6 5.81 1.50 5 -14 6 4.39 1.37 5 -14 6 2.06 1.28 5 14 6 6.33 1.68 5 -14 7 18.48 3.62 5 14 7 37.19 3.41 5 -14 8 17.56 2.82 -5 -15 12 17.69 2.38 -5 15 12 19.44 2.70 -5 15 11 0.52 0.55 -5 -15 11 3.24 1.35 -5 -15 10 8.70 2.31 -5 15 10 12.87 3.66 -5 15 9 2.53 1.68 5 15 -9 0.93 0.64 5 15 -8 39.06 4.37 -5 15 8 41.95 6.43 -5 -15 8 32.81 8.75 -5 -15 8 36.96 4.22 -5 15 8 36.67 5.39 -5 15 7 68.46 8.10 -5 -15 7 51.88 10.38 -5 15 7 60.90 6.83 5 15 -7 57.62 5.10 5 -15 -7 56.09 7.84 -5 -15 7 52.69 4.84 -5 -15 6 67.94 11.44 -5 15 6 66.18 6.43 -5 -15 5 23.33 5.90 -5 15 5 26.20 4.19 -5 15 4 103.24 8.55 -5 15 3 23.53 4.16 -5 15 2 17.18 3.69 -5 15 1 312.22 15.53 5 15 0 14.56 5.17 -5 15 0 20.58 3.96 5 15 1 222.49 20.53 -5 15 -1 210.50 12.97 5 15 2 -2.18 1.90 5 15 2 -0.13 0.55 5 -15 2 -0.09 1.41 5 -15 2 -0.12 0.41 5 15 2 -0.61 1.18 5 15 2 0.00 0.30 5 15 3 11.28 5.73 5 15 3 7.03 1.73 5 -15 3 10.35 3.17 5 -15 3 7.16 2.04 5 15 3 8.18 1.65 5 15 4 8.36 1.94 5 -15 4 9.98 3.17 5 -15 4 8.77 2.18 5 15 4 9.28 1.77 5 -15 5 73.01 8.76 5 -15 5 57.41 5.57 5 15 5 71.35 5.29 5 15 6 2.97 1.31 5 -15 6 -0.06 0.41 5 -15 6 0.47 1.15 5 15 6 1.32 0.82 5 15 7 51.26 3.86 5 -15 7 27.37 4.46 5 -15 8 25.15 3.24 -5 -16 12 59.70 4.23 -5 16 12 57.33 4.41 -5 -16 11 11.22 2.15 -5 16 11 9.57 2.45 -5 16 10 175.62 12.25 -5 -16 10 194.84 9.44 5 16 -9 16.95 3.03 -5 16 9 14.47 3.88 -5 -16 9 16.37 2.89 -5 16 8 25.09 5.06 5 16 -8 22.40 3.36 -5 -16 8 19.95 7.04 -5 -16 8 23.55 3.39 -5 16 8 24.01 4.41 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149.09 8.47 -5 18 9 147.04 12.12 -5 -18 8 5.61 1.61 -5 18 8 7.42 3.15 -5 -18 8 6.40 4.20 5 18 -8 4.69 1.71 -5 18 8 6.45 2.40 -5 18 7 41.48 6.59 -5 -18 7 33.35 9.01 5 18 -7 36.04 4.09 5 -18 -7 35.62 6.68 -5 18 7 29.12 5.00 -5 18 6 152.59 12.47 5 18 -6 143.75 7.75 5 -18 -6 164.46 14.03 -5 -18 6 142.01 17.87 -5 18 6 137.09 9.81 -5 18 6 122.89 9.84 -5 18 5 44.58 5.62 -5 18 4 237.30 13.06 -5 18 3 729.81 23.30 -5 18 2 49.73 6.21 -5 18 1 624.76 22.56 -5 18 0 87.91 8.46 5 18 0 76.77 12.67 5 -18 1 22.53 3.58 -5 18 -1 22.98 4.44 5 18 1 17.15 6.22 5 18 1 19.51 2.40 5 -18 2 33.06 5.51 5 18 2 28.66 8.33 5 -18 2 40.19 4.79 5 18 2 29.04 3.27 5 18 2 20.84 7.22 5 18 2 36.82 3.45 5 18 3 38.96 3.70 5 -18 3 35.85 5.98 5 -18 3 36.17 4.63 5 18 3 35.98 3.68 5 18 3 31.76 8.97 5 -18 4 258.38 16.26 5 -18 4 248.64 12.00 5 18 4 259.61 10.02 5 18 5 0.44 0.63 5 -18 5 1.31 1.07 5 -18 5 1.26 0.90 5 -18 6 2.00 0.99 5 -18 6 1.28 1.72 5 18 6 0.94 0.89 5 -18 7 17.56 3.19 5 -18 7 11.00 1.78 -5 -19 12 3.48 0.92 -5 19 11 0.84 1.10 -5 -19 11 0.95 0.68 -5 19 10 126.40 10.48 -5 -19 10 135.25 7.60 -5 19 9 15.76 4.05 -5 -19 9 14.37 2.65 -5 19 8 92.41 9.99 -5 19 8 85.92 8.46 5 19 -8 103.67 7.32 -5 -19 8 91.91 6.83 5 19 -7 0.98 0.82 5 -19 -7 -0.24 1.29 -5 19 7 0.29 0.92 -5 -19 7 0.55 2.64 -5 19 7 2.37 1.56 -5 19 6 1.88 1.22 5 -19 -6 3.60 2.63 -5 19 6 3.03 2.26 -5 -19 6 2.23 2.29 -5 -19 6 -0.88 0.85 5 19 -6 0.90 0.73 -5 19 6 2.13 1.65 -5 19 5 16.25 3.39 -5 19 4 319.69 15.24 -5 19 3 188.39 11.86 -5 19 2 0.96 0.73 -5 19 1 47.81 6.29 5 19 0 50.64 10.51 -5 19 0 52.63 6.52 5 -19 1 4.12 1.71 5 19 1 4.32 3.19 5 19 1 4.30 1.07 -5 19 -1 5.55 2.39 5 19 2 6.20 1.49 5 -19 2 6.61 2.86 5 19 2 9.22 4.97 5 -19 2 5.67 1.81 5 19 2 9.38 5.55 5 19 2 8.14 1.64 5 -19 3 1.92 1.32 5 -19 3 2.66 1.29 5 19 3 5.13 1.88 5 19 3 1.70 1.01 5 -19 4 33.65 5.79 5 -19 4 36.53 4.59 5 19 4 35.74 3.91 5 19 4 34.11 3.69 5 -19 5 16.82 3.92 5 -19 5 21.48 3.40 5 19 5 25.30 3.50 5 19 5 22.43 2.88 5 -19 6 111.16 9.17 5 -19 6 99.99 6.61 5 19 6 133.30 6.28 5 19 6 124.11 6.73 5 -19 7 1.25 0.64 5 -19 7 3.35 1.36 -5 -20 12 0.42 0.25 -5 20 11 1.87 1.33 -5 -20 11 1.09 0.57 -5 20 10 19.78 4.13 -5 -20 10 18.96 2.87 -5 -20 9 60.06 5.33 -5 20 9 59.88 7.91 -5 20 8 31.14 5.09 -5 20 8 43.01 6.88 -5 -20 8 32.75 4.00 -5 20 7 117.11 11.43 5 -20 -7 119.37 12.56 -5 -20 7 109.44 17.20 -5 20 7 99.89 9.12 5 20 -7 127.06 7.86 5 -20 -6 254.07 17.91 -5 -20 6 228.52 13.61 5 20 -6 241.23 10.24 -5 -20 6 248.57 25.08 -5 20 6 202.69 12.46 -5 20 6 196.85 12.69 -5 20 6 223.04 15.36 -5 20 5 76.69 8.60 5 -20 -5 101.15 10.72 -5 20 5 85.27 7.98 -5 20 5 71.62 7.56 5 20 -5 84.89 5.76 -5 20 4 131.72 9.88 -5 20 3 130.84 10.05 -5 20 2 20.47 4.00 -5 20 1 3.63 1.88 5 20 0 63.90 11.80 5 -20 0 70.89 6.24 -5 20 0 75.23 7.86 5 20 1 62.82 12.11 5 -20 1 66.02 6.07 -5 20 -1 55.61 6.87 5 20 1 55.95 4.11 5 20 2 78.67 14.25 5 -20 2 101.94 7.66 5 20 2 83.31 5.41 5 20 2 93.21 5.53 5 20 2 93.29 15.96 5 -20 3 -0.26 0.78 5 -20 3 -0.38 0.67 5 20 3 0.44 0.88 5 -20 4 102.18 9.86 5 -20 4 96.00 7.39 5 20 4 120.65 7.20 5 20 4 92.56 5.88 5 -20 5 55.71 6.94 5 -20 5 54.78 5.33 5 20 5 72.08 5.67 5 20 5 61.52 4.56 5 -20 6 10.23 2.07 5 -20 6 12.15 2.97 5 20 6 11.42 2.11 5 -20 7 1.50 1.00 5 -20 7 2.71 0.92 -5 -21 12 7.51 1.28 -5 21 11 -0.18 0.41 -5 -21 11 -0.13 0.55 -5 -21 10 4.01 1.42 -5 21 10 3.78 1.99 -5 21 9 35.13 6.07 -5 -21 9 38.31 4.24 5 -21 -8 18.04 4.61 -5 21 8 14.35 3.99 -5 -21 8 19.05 3.12 -5 21 8 14.28 3.35 5 -21 -7 12.61 4.28 -5 21 7 13.07 4.07 -5 -21 7 3.99 4.41 -5 21 7 9.92 2.79 -5 21 6 -0.24 0.96 -5 21 6 -2.58 1.46 5 -21 -6 -1.27 1.43 -5 21 6 0.07 0.67 -5 -21 6 2.06 1.75 -5 -21 6 0.16 1.16 5 -21 -5 1.80 1.30 -5 21 5 0.63 0.84 -5 21 5 2.31 1.24 -5 21 5 -0.04 1.20 -5 21 4 5.08 2.03 -5 21 3 95.98 8.64 -5 21 2 104.98 9.10 -5 21 1 286.67 15.42 5 21 0 91.36 14.28 5 -21 0 76.37 6.56 -5 21 0 77.31 8.04 5 21 1 103.52 15.71 5 -21 1 119.90 8.22 -5 21 -1 107.83 9.74 5 21 1 103.48 5.67 5 21 2 18.09 7.25 5 -21 2 17.59 3.15 5 21 2 11.49 5.43 5 21 2 17.19 2.41 5 21 2 16.15 2.45 5 -21 3 87.24 8.90 5 -21 3 90.34 7.24 5 21 3 89.29 5.76 5 21 3 87.31 5.62 5 -21 4 129.77 10.95 5 -21 4 131.26 8.62 5 21 4 159.78 8.37 5 21 4 132.24 6.82 5 -21 5 17.57 2.94 5 -21 5 18.57 3.95 5 21 5 23.45 3.05 5 21 5 20.69 2.79 5 -21 6 16.18 3.26 5 -21 6 16.99 2.66 5 21 6 19.67 2.56 5 -21 7 -0.01 0.22 5 -21 7 0.09 0.46 -5 -22 12 20.78 1.98 -5 22 11 20.75 3.42 -5 -22 11 23.63 2.70 -5 22 10 32.84 5.29 -5 -22 10 34.22 3.72 -5 22 9 29.87 5.59 -5 -22 9 30.26 3.82 -5 22 8 100.57 10.67 5 -22 -8 91.76 10.78 -5 22 8 88.74 8.43 -5 22 7 68.87 7.58 -5 22 7 68.95 8.99 5 -22 -7 80.34 10.46 -5 -22 7 66.65 14.03 -5 22 6 56.20 8.05 5 -22 -6 44.44 7.98 -5 -22 6 34.69 10.15 -5 22 6 30.91 5.13 -5 -22 6 27.64 4.97 5 -22 -5 56.59 8.19 -5 22 5 38.15 6.27 -5 22 5 45.34 6.04 -5 22 5 39.63 5.69 5 -22 -4 107.04 10.73 -5 22 4 94.06 8.56 -5 22 4 101.33 9.19 -5 22 3 78.99 7.85 -5 22 2 5.78 2.19 5 -22 -1 465.55 16.43 -5 22 1 526.62 21.00 5 22 0 5.35 4.12 5 22 0 5.58 1.27 -5 22 0 6.90 2.35 5 -22 0 7.66 2.12 5 22 1 88.57 5.26 5 22 1 91.43 15.20 5 -22 1 97.93 7.50 -5 22 -1 87.87 8.97 5 22 2 291.14 10.07 5 22 2 294.83 28.30 5 -22 2 298.46 13.27 5 22 2 247.79 26.03 5 -22 3 28.95 4.96 5 -22 3 31.94 4.37 5 22 3 31.68 3.53 5 22 3 25.95 3.04 5 22 4 5.16 1.54 5 -22 4 3.70 1.85 5 -22 4 4.10 2.40 5 22 4 8.83 2.26 5 -22 5 7.87 1.94 5 -22 5 5.52 1.96 5 22 5 7.71 1.63 5 -22 6 15.97 3.12 5 -22 6 15.72 2.54 5 -22 7 7.96 1.40 -5 23 11 9.29 2.30 -5 -23 11 7.42 1.45 -5 -23 10 46.84 4.29 -5 23 10 41.17 5.85 -5 23 9 81.62 9.23 -5 -23 9 100.08 6.80 5 -23 -8 5.09 2.56 -5 23 8 1.20 1.96 -5 23 8 0.86 1.09 5 -23 -7 1.77 1.59 -5 23 7 0.16 1.48 -5 -23 7 4.85 3.64 -5 23 7 0.84 0.71 5 -23 -6 21.00 5.35 -5 23 6 13.24 3.95 -5 -23 6 20.69 8.01 -5 -23 6 11.36 3.25 -5 23 6 12.38 3.35 -5 23 5 82.03 8.27 -5 23 5 81.54 9.37 5 -23 -5 100.87 11.12 -5 -23 5 97.48 9.08 -5 23 5 81.11 8.33 -5 23 4 28.79 5.00 -5 23 4 24.22 4.81 5 -23 -4 33.64 6.10 -5 23 4 30.08 4.94 -5 23 3 1074.68 29.89 -5 23 3 998.50 29.07 5 -23 -2 54.71 7.19 -5 23 2 75.74 7.85 -5 23 2 68.93 7.66 5 -23 -1 89.15 7.20 -5 23 1 96.96 9.04 5 23 0 13.56 5.68 5 -23 0 22.82 3.70 -5 23 0 22.19 4.46 5 23 0 16.53 2.19 5 -23 1 -0.28 1.01 5 23 1 -2.48 3.97 -5 23 -1 1.26 1.89 5 23 1 4.92 1.31 5 23 2 17.69 6.82 5 -23 2 18.29 3.25 5 23 2 14.31 5.79 5 23 2 15.32 2.40 5 23 3 5.57 1.71 5 -23 3 2.52 1.02 5 23 3 5.75 1.68 5 -23 4 58.64 6.96 5 -23 4 61.00 5.83 5 23 4 65.95 4.72 5 -23 5 14.82 3.21 5 -23 5 15.85 2.78 5 23 5 18.04 2.62 5 -23 6 15.16 2.43 5 -23 6 16.83 3.11 5 -23 7 4.28 0.97 -5 24 11 16.25 2.94 -5 -24 11 12.30 1.82 -5 24 10 2.54 1.46 -5 -24 10 3.74 1.13 -5 24 9 13.64 3.63 -5 -24 9 15.26 2.67 -5 24 8 141.40 12.72 5 -24 -8 142.63 13.61 5 -24 -7 5.78 3.34 -5 24 7 5.96 2.75 -5 24 7 3.69 1.45 -5 24 6 27.32 5.57 5 -24 -6 35.30 6.85 -5 -24 6 26.44 5.23 -5 -24 6 23.46 8.87 -5 24 6 30.32 5.10 -5 24 5 6.75 2.55 -5 24 5 6.52 2.43 5 -24 -5 5.23 2.40 -5 -24 5 8.77 2.92 -5 24 5 4.74 2.16 5 -24 -4 143.95 12.74 -5 24 4 146.82 11.14 -5 24 4 149.66 11.24 5 -24 -3 5.29 2.00 -5 24 3 3.12 1.78 -5 24 3 5.40 2.57 -5 24 2 1.49 1.34 -5 24 2 2.55 2.32 5 -24 -2 -0.61 1.33 5 -24 -1 62.83 6.11 -5 24 1 74.29 8.08 5 -24 0 31.20 4.26 -5 24 0 25.21 4.92 5 24 0 23.54 2.67 5 24 1 64.03 12.73 5 -24 1 52.23 5.54 -5 24 -1 51.23 7.17 5 24 1 53.77 4.23 5 24 2 35.37 3.55 5 -24 2 36.60 4.65 5 -24 3 54.74 5.64 5 24 3 61.59 5.06 5 24 3 50.00 4.18 5 -24 4 37.81 4.52 5 24 4 51.30 4.80 5 24 4 42.11 3.76 5 -24 5 -0.01 0.63 5 -24 5 -1.83 0.92 5 24 5 -0.47 0.89 5 -24 6 1.13 0.65 5 -24 6 0.18 0.57 -5 24 -6 0.42 0.47 -5 25 11 2.72 1.01 -5 -25 11 2.50 0.75 -5 25 10 8.60 2.75 -5 -25 10 7.31 1.60 -5 25 9 15.68 4.04 -5 25 8 86.48 9.88 5 -25 -8 86.90 10.57 -5 25 7 21.20 4.14 5 -25 -7 24.60 5.93 -5 25 7 21.45 5.24 -5 25 6 115.61 11.75 -5 -25 6 114.79 19.24 -5 -25 6 116.90 11.08 -5 25 6 115.84 9.86 5 -25 -6 120.46 12.86 5 -25 -5 0.89 1.28 -5 25 5 1.72 1.04 -5 -25 5 1.72 1.42 -5 25 5 1.25 1.39 -5 25 5 0.67 1.01 -5 -25 4 60.10 7.21 -5 25 4 58.16 7.24 5 -25 -4 51.64 7.72 -5 25 4 41.28 6.34 -5 25 4 51.92 6.62 5 -25 -3 5.79 2.52 -5 25 3 6.02 2.56 -5 25 3 7.93 2.65 5 -25 -2 69.05 8.21 -5 25 2 92.40 9.15 -5 25 2 91.42 8.84 5 -25 -1 61.90 6.09 5 -25 -1 50.84 6.96 -5 25 1 77.14 8.46 -5 25 1 83.81 8.59 5 25 0 62.48 12.53 5 -25 0 66.29 6.29 -5 25 0 62.76 7.95 5 25 0 51.32 4.01 5 25 1 145.81 19.47 5 -25 1 140.65 9.11 -5 25 -1 122.68 11.17 5 25 1 147.10 7.04 5 -25 2 9.38 2.24 5 25 2 10.35 1.99 5 -25 3 131.36 8.72 5 25 3 112.65 6.12 5 -25 4 1.25 0.91 5 25 4 0.57 0.64 5 -25 5 22.00 3.29 5 25 5 21.84 2.75 5 -25 6 7.33 1.56 -5 25 -6 5.71 1.58 -5 26 11 0.17 0.43 -5 -26 11 0.11 0.24 -5 26 10 53.34 6.34 -5 -26 10 54.22 4.23 -5 26 9 5.41 2.46 -5 26 8 1.81 1.07 5 -26 -8 2.64 1.82 5 -26 -7 1.92 1.12 -5 26 7 2.76 2.29 -5 26 7 4.34 1.70 -5 26 6 141.91 10.89 -5 26 6 155.96 13.64 5 -26 -6 158.25 14.78 -5 -26 6 127.01 20.37 -5 -26 6 140.93 12.43 5 -26 -5 5.28 2.75 -5 26 5 4.52 2.56 -5 -26 5 7.61 2.80 -5 26 5 6.14 2.34 5 -26 -4 40.90 6.92 -5 -26 4 41.14 6.15 -5 26 4 40.84 5.79 -5 26 4 36.24 5.84 -5 26 4 27.59 5.22 5 -26 -3 25.11 5.15 -5 26 3 27.72 5.13 -5 26 3 34.07 5.53 5 -26 -2 29.69 5.47 -5 26 2 37.73 5.97 -5 26 2 42.85 6.06 5 -26 -1 368.23 14.88 -5 26 1 396.42 19.64 -5 26 1 425.40 19.41 5 26 0 69.67 13.22 5 -26 0 53.94 5.71 -5 26 0 56.97 7.74 5 26 0 46.96 3.88 5 -26 1 1.35 1.13 5 26 1 2.74 2.69 5 26 1 0.86 0.59 5 -26 2 -0.02 0.94 5 26 2 0.53 0.61 5 -26 3 74.14 6.51 5 26 3 97.60 6.74 5 -26 4 37.51 4.42 5 26 4 40.67 4.00 5 -26 5 36.55 4.00 5 26 5 37.65 3.56 -5 26 -6 -0.51 0.54 5 -26 6 -0.19 0.39 -5 27 11 3.11 1.20 -5 27 10 53.92 6.31 -5 27 9 13.83 3.45 -5 27 8 52.02 7.55 5 -27 -8 39.89 6.95 5 -27 -7 3.76 2.32 -5 27 7 6.34 2.67 5 -27 -6 22.35 5.63 -5 27 6 22.21 5.18 -5 27 6 19.34 3.90 5 -27 -5 4.42 3.67 -5 27 5 1.17 0.86 -5 -27 5 4.04 2.57 -5 27 5 2.88 1.63 5 -27 -4 40.69 6.95 -5 27 4 42.54 6.39 -5 27 4 34.99 5.54 -5 27 4 31.42 5.58 -5 -27 4 45.12 6.54 -5 27 3 107.90 9.63 5 -27 -3 84.41 9.70 -5 -27 3 108.00 10.01 -5 27 3 106.54 10.30 5 -27 -2 89.95 9.64 -5 27 2 118.55 10.90 -5 27 2 124.91 10.43 5 -27 -1 11.59 3.35 -5 27 1 21.26 4.47 -5 27 1 14.27 3.89 5 -27 -1 14.82 2.91 -5 27 0 9.61 3.32 5 27 0 6.99 3.34 -5 -27 0 11.14 3.51 5 27 0 8.77 1.73 5 -27 0 9.09 2.35 5 -27 1 97.30 7.61 5 27 1 102.82 6.10 5 -27 2 5.11 1.97 5 27 2 4.07 1.44 5 -27 3 18.26 3.26 5 27 3 20.22 3.07 5 -27 4 10.63 2.32 5 27 4 11.68 2.07 5 -27 5 29.58 3.57 5 27 5 27.85 2.98 5 -27 6 3.37 1.04 -5 27 -6 2.64 1.07 -5 28 11 -0.04 0.25 -5 28 10 6.16 2.06 -5 28 9 39.53 6.04 5 -28 -8 11.64 3.83 -5 28 8 9.15 3.13 5 -28 -7 7.71 3.28 -5 28 7 10.73 3.64 5 -28 -6 0.75 0.96 -5 28 6 0.45 0.54 -5 28 6 -0.13 1.58 5 -28 -5 36.12 6.85 -5 -28 5 35.83 6.19 -5 28 5 32.22 5.24 -5 28 5 39.20 6.62 5 -28 -4 15.30 4.33 -5 28 4 11.69 3.33 -5 28 4 14.41 3.46 -5 -28 4 16.58 4.13 5 -28 -3 9.67 3.31 -5 -28 3 9.21 3.17 -5 28 3 12.67 3.66 -5 28 3 9.98 2.91 -5 28 2 93.92 9.01 5 -28 -2 77.54 9.06 -5 -28 2 112.81 10.78 -5 28 2 103.56 10.31 5 28 -1 126.65 8.23 5 -28 -1 126.56 8.83 -5 -28 1 153.11 12.71 -5 28 1 140.39 12.15 -5 28 1 144.28 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2.43 6 13 6 7.17 1.56 -6 -14 12 78.44 4.91 -6 14 12 83.59 5.95 -6 -14 11 13.78 2.37 -6 14 11 12.69 2.89 6 14 -10 21.68 3.39 -6 14 10 17.68 4.02 -6 -14 10 18.07 2.88 -6 14 9 5.55 2.76 -6 -14 9 1.49 0.81 6 14 -9 2.83 1.48 -6 14 8 15.71 3.65 -6 14 8 11.20 3.23 -6 -14 8 11.43 4.17 -6 -14 8 11.80 2.46 6 14 -8 13.70 2.66 6 14 -7 195.06 9.54 -6 14 7 189.65 12.29 -6 14 7 231.20 14.87 6 -14 -7 208.27 15.00 -6 -14 7 172.62 18.34 -6 14 6 101.18 9.47 6 -14 -6 108.52 10.66 -6 -14 6 92.06 12.78 -6 -14 6 91.48 11.78 -6 14 6 104.19 8.89 6 14 -6 92.38 6.27 -6 14 6 85.25 7.97 -6 -14 5 402.54 25.60 -6 -14 5 398.78 25.49 -6 14 5 389.94 17.69 -6 14 4 117.91 9.81 -6 14 3 53.78 6.82 -6 14 2 39.17 6.02 6 14 -1 160.60 17.11 -6 14 1 219.56 14.39 6 14 0 36.61 8.26 -6 -14 0 52.03 9.68 -6 14 0 44.24 6.73 6 14 0 34.15 3.37 6 -14 1 0.36 0.60 6 -14 1 0.78 1.31 6 14 1 -0.43 0.98 6 14 1 0.03 1.52 -6 -14 -1 2.27 2.60 -6 14 -1 0.47 1.01 6 14 1 -1.78 3.06 6 14 1 1.00 0.84 6 14 2 60.86 5.12 6 -14 2 75.94 9.03 6 -14 2 57.97 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265.08 15.18 7 9 -9 244.63 11.65 -7 9 8 35.29 5.61 -7 9 8 33.13 4.99 7 9 -8 29.45 4.00 -7 9 7 43.59 6.04 -7 9 7 36.15 5.14 7 9 -7 33.22 4.01 7 9 -6 3.42 1.32 -7 9 6 4.97 2.01 -7 -9 6 6.24 2.69 -7 9 6 4.03 1.77 -7 9 6 5.33 1.96 7 9 -6 5.05 1.50 -7 -9 5 160.02 15.68 -7 9 5 145.92 11.89 -7 9 4 33.93 5.99 -7 -9 4 32.87 7.19 -7 -9 3 142.41 15.34 -7 9 3 143.01 12.62 7 9 -2 136.66 14.15 -7 -9 2 132.28 15.10 -7 9 2 119.83 11.92 7 9 -1 70.71 10.57 -7 -9 1 86.97 12.59 -7 9 1 94.71 10.81 7 9 -1 73.64 5.62 7 9 0 222.24 19.52 -7 -9 0 237.52 21.14 -7 9 0 250.64 17.77 7 9 0 234.10 20.30 7 9 0 234.54 9.56 7 9 0 226.20 9.86 7 9 1 155.51 17.40 7 9 1 201.14 9.02 7 -9 2 28.44 6.00 7 9 2 26.54 3.37 7 9 3 35.46 4.05 7 -9 3 32.26 6.10 7 9 3 34.90 3.88 7 9 4 7.38 1.76 7 -9 4 10.14 3.33 7 9 4 8.08 1.77 7 -9 5 111.48 7.02 7 -9 5 102.33 9.18 7 9 5 119.30 6.34 7 -9 6 9.83 1.60 7 9 6 12.25 1.80 -7 10 13 2.06 0.88 -7 -10 13 2.28 0.74 -7 -10 12 0.59 0.64 -7 10 12 2.05 1.32 7 -10 -12 0.29 0.66 -7 10 11 2.42 1.56 -7 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5 79.97 5.09 7 10 6 6.82 1.42 7 -10 6 1.98 0.82 -7 -11 13 11.15 1.57 -7 11 13 14.66 2.09 -7 -11 12 16.59 2.35 7 -11 -12 12.59 2.27 -7 11 12 14.35 2.77 7 11 -11 28.34 3.67 -7 -11 11 23.63 3.13 -7 11 11 25.90 4.25 -7 11 10 0.27 0.79 -7 -11 10 0.42 0.48 -7 11 9 27.05 5.06 7 11 -9 24.32 3.64 -7 -11 9 24.37 3.38 -7 11 8 9.29 2.82 -7 11 8 10.50 3.42 7 11 -8 7.36 1.97 -7 11 7 222.67 13.05 7 11 -7 219.37 10.44 -7 11 6 34.93 5.24 -7 11 6 34.95 5.12 -7 11 6 32.86 5.49 -7 -11 6 36.29 7.58 7 11 -6 33.64 3.90 7 11 -6 27.59 3.59 7 11 -5 9.55 2.20 -7 -11 5 7.30 3.31 -7 11 5 11.38 2.83 -7 11 5 7.08 2.60 -7 -11 4 20.26 5.92 -7 11 4 20.25 4.48 -7 -11 3 40.67 8.60 -7 11 3 37.50 6.32 7 11 -2 253.07 20.53 -7 -11 2 270.38 22.16 -7 11 2 289.03 18.18 7 11 -2 227.31 9.91 7 -11 -1 45.66 5.13 7 11 -1 69.28 10.97 -7 -11 1 61.51 10.62 -7 11 1 62.88 8.64 -7 11 1 55.20 6.83 7 11 -1 56.34 4.88 7 11 0 25.18 6.96 7 -11 0 23.30 3.72 7 11 0 24.92 7.02 -7 11 0 31.45 6.17 -7 -11 0 18.33 5.97 7 11 0 29.22 3.38 7 -11 1 5.43 2.57 7 11 1 6.63 3.42 7 11 1 4.66 1.41 7 11 2 94.05 6.64 7 -11 2 109.58 11.42 7 11 2 108.28 6.63 7 11 3 21.90 3.08 7 -11 3 20.82 4.92 7 11 3 27.86 3.54 7 11 4 -0.44 0.71 7 -11 4 -1.44 1.50 7 11 4 0.32 0.56 7 11 5 5.73 1.49 7 -11 5 5.07 2.20 7 -11 5 2.68 1.19 7 11 5 4.29 1.48 7 11 6 5.63 1.32 7 -11 6 0.15 0.30 -7 -12 13 12.99 1.64 -7 12 13 16.25 2.13 -7 12 12 0.66 1.27 -7 -12 12 0.61 0.36 7 12 -11 84.77 6.34 -7 -12 11 75.59 5.53 -7 12 11 71.16 7.03 -7 -12 10 0.06 0.54 7 12 -10 0.02 0.58 -7 12 9 144.98 11.59 7 12 -9 133.44 8.51 -7 -12 9 116.35 7.38 -7 12 8 178.13 12.92 -7 12 8 161.38 11.52 7 12 -8 155.56 9.05 -7 12 7 56.12 6.65 -7 12 7 64.97 7.71 7 12 -7 59.65 5.36 -7 12 6 49.76 6.44 -7 -12 6 49.28 9.20 -7 12 6 47.11 6.48 7 12 -6 46.10 4.59 -7 12 6 46.99 5.96 7 12 -6 42.49 4.45 -7 12 5 5.01 1.86 7 12 -5 5.56 1.59 -7 -12 5 9.08 4.20 7 12 -5 6.35 1.58 -7 12 5 6.09 2.44 -7 -12 4 47.60 9.22 -7 12 4 49.67 7.05 -7 12 4 46.02 5.93 7 12 -4 45.85 4.54 -7 12 3 34.07 5.97 -7 -12 3 29.35 7.36 7 12 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7 13 4 1.46 0.71 7 -13 4 -0.19 1.27 7 13 4 1.45 1.05 7 -13 5 49.39 4.40 7 13 5 51.86 3.83 7 13 6 8.61 1.55 -7 -14 12 86.24 4.95 -7 14 12 80.82 6.25 -7 -14 11 11.75 2.13 -7 14 11 11.54 2.93 -7 -14 10 -0.69 1.15 -7 14 10 1.21 1.37 7 14 -10 1.62 1.16 -7 14 9 22.84 5.10 7 14 -9 21.64 3.43 -7 -14 9 18.67 2.97 -7 14 8 20.47 4.57 7 14 -8 19.69 3.21 -7 14 8 20.42 4.27 -7 14 7 166.23 12.44 -7 14 7 137.65 10.74 7 14 -7 154.70 8.73 -7 14 6 151.73 11.35 7 -14 -6 180.70 13.74 -7 -14 6 134.84 15.76 -7 14 6 144.31 11.15 -7 14 6 148.34 10.94 7 14 -6 154.34 8.35 7 14 -6 143.60 8.23 7 14 -5 3.40 1.21 7 -14 -5 5.67 2.26 -7 14 5 5.15 2.03 -7 -14 5 5.22 3.32 -7 14 5 7.59 2.63 -7 14 5 5.03 1.72 7 14 -5 4.12 1.30 7 -14 -4 29.21 5.13 -7 14 4 26.97 5.04 -7 -14 4 26.23 7.28 -7 14 4 28.60 4.92 7 14 -4 26.16 3.45 7 14 -3 0.58 0.45 -7 -14 3 0.22 1.31 -7 14 3 -0.94 1.54 -7 14 3 0.88 0.78 7 14 -2 64.36 11.02 -7 -14 2 67.60 11.64 -7 14 2 61.05 8.11 -7 14 2 57.41 7.18 7 14 -2 59.78 5.10 7 -14 -1 36.98 4.80 7 14 -1 43.88 9.36 -7 -14 1 45.74 9.80 -7 14 1 46.89 7.39 -7 14 1 42.36 6.38 7 14 -1 42.79 3.93 7 -14 0 23.28 3.90 7 14 0 34.94 8.78 -7 -14 0 20.87 6.26 -7 14 0 30.82 5.39 7 14 0 33.79 8.31 7 14 0 34.95 3.60 -7 14 0 29.38 5.85 7 14 1 26.48 3.41 7 -14 1 23.62 3.82 -7 14 -1 25.23 4.75 7 14 1 20.51 7.02 7 14 1 31.10 3.48 7 14 2 130.30 7.62 7 -14 2 144.13 12.65 7 14 2 151.21 7.68 7 -14 3 87.51 9.75 7 14 3 96.86 6.33 7 14 3 87.44 5.97 7 14 4 1.55 0.87 7 -14 4 1.83 1.99 7 14 4 1.74 1.07 7 -14 5 31.76 3.42 7 14 5 39.61 3.76 7 14 5 33.75 3.06 -7 15 12 1.08 1.12 -7 -15 12 1.37 0.69 -7 15 11 10.96 2.77 -7 -15 11 10.08 1.93 7 15 -10 2.39 1.24 -7 -15 10 0.74 0.55 -7 15 10 3.98 2.27 -7 15 9 9.20 3.28 7 15 -9 6.42 1.97 -7 15 8 14.74 3.82 7 15 -8 15.55 2.86 -7 15 8 14.11 3.59 -7 15 7 122.89 10.81 -7 15 7 123.98 10.23 7 15 -7 121.95 7.75 -7 15 6 69.00 7.73 7 -15 -6 76.11 9.05 -7 -15 6 59.11 10.65 -7 15 6 55.12 6.81 7 15 -6 73.73 5.78 -7 15 6 68.30 7.54 7 15 -6 62.22 5.43 7 -15 -5 27.99 5.33 -7 15 5 17.56 3.69 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222.25 17.59 8 10 -1 240.56 10.07 8 10 -1 250.44 10.93 8 10 0 147.17 7.87 8 10 1 1.10 0.78 8 10 1 3.68 1.23 8 -10 1 3.89 1.44 8 10 2 17.53 2.77 8 10 2 19.34 2.88 8 10 3 3.04 0.85 8 10 3 6.47 1.61 8 -10 4 15.60 2.49 8 10 4 19.78 2.66 8 10 4 18.08 2.38 8 10 5 23.01 2.17 8 10 5 26.43 2.37 8 -10 5 27.72 2.59 -8 11 13 48.68 3.65 -8 11 12 3.62 1.54 8 -11 -12 1.57 0.89 -8 -11 12 2.04 0.86 8 11 -11 23.51 3.29 -8 -11 11 18.96 2.66 -8 11 11 20.67 4.03 8 11 -10 27.77 3.82 -8 -11 10 22.01 3.06 -8 11 10 28.15 4.76 -8 11 9 1.90 1.49 8 11 -9 1.88 0.97 -8 11 8 22.23 4.57 -8 11 8 23.03 4.36 8 11 -8 17.98 3.08 -8 11 7 133.90 10.59 -8 11 7 128.61 10.25 8 11 -7 136.84 8.32 8 11 -7 116.29 7.77 -8 11 6 40.08 5.50 -8 11 6 35.93 6.16 -8 -11 6 38.60 8.91 -8 11 6 37.13 5.55 8 11 -6 38.77 4.22 8 11 -6 40.97 4.61 -8 11 5 30.20 5.68 -8 -11 5 26.29 7.39 -8 11 5 32.72 5.18 8 11 -5 25.45 3.27 8 11 -5 28.69 3.91 -8 11 4 3.82 2.22 8 11 -4 3.99 1.32 -8 -11 4 2.65 2.77 -8 11 4 4.18 1.90 -8 -11 3 25.27 7.00 -8 11 3 29.73 6.11 -8 11 3 25.61 4.68 8 11 -3 25.88 3.62 8 11 -2 7.20 1.97 -8 -11 2 3.34 2.49 -8 11 2 2.49 0.64 8 -11 -1 174.11 10.39 -8 -11 1 189.65 20.20 -8 11 1 222.77 17.62 8 11 -1 226.81 9.76 8 11 0 316.75 11.58 8 11 1 7.54 1.74 8 11 1 12.35 2.49 8 -11 1 10.52 2.31 8 11 2 2.15 0.90 8 11 2 6.27 1.86 8 11 3 2.33 1.09 8 11 3 4.23 1.19 8 11 4 1.54 0.92 8 -11 4 -0.98 0.97 8 11 4 -0.29 0.66 8 11 5 3.14 0.91 8 -11 5 1.70 0.68 -8 12 13 7.05 1.42 -8 12 12 5.72 1.85 -8 -12 12 4.15 1.05 -8 -12 11 27.04 3.12 8 12 -11 36.66 4.11 -8 12 11 35.21 4.86 -8 12 10 1.43 1.98 -8 -12 10 0.65 0.61 8 12 -10 2.17 1.24 -8 12 9 9.79 2.97 8 12 -9 10.55 2.42 -8 12 8 20.19 4.35 8 12 -8 17.45 3.03 -8 12 8 15.29 3.73 8 12 -7 0.33 0.53 -8 12 7 0.14 1.12 8 12 -7 1.10 0.75 -8 12 7 0.61 0.71 -8 12 6 197.79 12.20 -8 -12 6 216.07 21.01 -8 12 6 185.65 13.61 8 12 -6 242.91 10.62 -8 12 6 240.95 14.20 8 12 -6 234.74 11.06 8 12 -5 0.46 0.60 -8 -12 5 -0.93 3.10 8 12 -5 0.08 0.74 -8 12 5 0.65 0.88 -8 12 5 0.55 1.65 8 12 -4 -0.06 0.64 -8 -12 4 -0.86 3.89 -8 12 4 -0.38 0.96 -8 12 4 0.71 0.88 -8 -12 3 463.10 31.94 -8 12 3 432.19 23.14 -8 12 3 419.15 19.52 8 12 -3 449.36 15.00 8 12 -2 3.06 1.27 -8 -12 2 5.30 3.57 -8 12 2 3.87 1.84 -8 12 2 2.79 1.76 8 -12 -1 0.72 0.93 -8 -12 1 -0.71 1.68 -8 12 1 2.74 1.89 -8 12 1 0.14 0.75 8 12 -1 1.24 1.12 8 12 0 3.14 1.25 8 12 1 87.25 6.36 8 12 1 97.18 6.28 8 12 2 -1.55 1.23 8 12 2 0.59 0.69 8 12 3 6.53 1.51 8 12 3 7.49 1.72 8 12 4 7.28 1.45 8 -12 4 4.76 1.53 8 12 4 5.06 1.42 8 -12 5 2.34 0.76 8 12 5 2.21 0.64 -8 -13 12 20.90 2.34 -8 13 12 22.47 3.35 -8 -13 11 2.63 0.99 -8 13 11 4.88 1.89 8 13 -11 6.37 1.82 8 13 -10 142.45 8.44 -8 -13 10 112.89 6.82 -8 13 10 135.22 10.49 -8 13 9 86.41 8.82 8 13 -9 88.14 6.85 -8 13 8 40.40 6.21 -8 13 8 41.20 5.93 8 13 -8 41.22 4.65 8 13 -7 0.53 0.74 -8 13 7 2.17 1.82 -8 13 7 0.99 0.68 8 13 -7 1.49 0.94 8 13 -6 1.17 0.87 -8 13 6 2.93 1.78 -8 13 6 2.19 1.39 -8 -13 6 1.00 1.73 -8 13 6 0.95 1.10 8 13 -6 2.30 1.13 -8 -13 5 133.14 17.09 -8 13 5 119.80 11.18 -8 13 5 132.11 10.78 8 13 -5 122.01 7.24 8 13 -5 139.01 8.52 8 13 -4 1.85 1.13 -8 -13 4 1.11 1.39 -8 13 4 0.98 0.80 -8 13 4 0.97 1.03 8 13 -3 6.46 1.80 -8 -13 3 7.37 5.48 -8 13 3 4.34 2.61 -8 13 3 6.54 2.92 -8 13 2 37.59 7.01 -8 -13 2 42.46 9.62 -8 13 2 34.54 5.63 8 13 -2 46.89 4.84 8 -13 -1 57.23 5.99 -8 -13 1 63.53 11.96 -8 13 1 79.21 10.19 -8 13 1 81.16 8.61 8 13 -1 98.86 6.33 8 13 0 4.00 1.64 8 13 1 2.29 1.15 8 13 1 4.31 1.55 8 13 2 31.16 3.42 8 13 2 28.65 3.39 8 13 3 45.61 4.11 8 13 3 37.16 3.61 8 13 4 8.70 1.48 8 -13 4 9.32 1.97 8 13 5 9.82 1.36 8 13 5 3.61 0.86 -8 14 12 0.27 0.81 -8 -14 12 0.29 0.34 -8 -14 11 0.30 0.43 -8 14 11 0.53 1.11 -8 14 10 0.32 1.67 8 14 -10 3.01 1.59 -8 14 9 9.96 3.25 8 14 -9 11.66 2.55 -8 14 8 73.14 8.20 8 14 -8 84.42 6.64 -8 14 8 69.30 7.79 8 14 -7 6.06 1.75 -8 14 7 6.71 2.36 -8 14 7 6.14 2.21 8 14 -7 6.00 1.79 8 14 -6 10.09 2.36 -8 14 6 12.07 3.02 -8 -14 6 10.28 4.32 -8 14 6 8.49 2.93 8 14 -6 13.28 2.52 -8 14 6 6.76 2.46 8 14 -5 5.05 1.56 -8 -14 5 6.04 2.58 -8 14 5 8.81 3.25 8 14 -5 5.84 1.56 -8 14 5 5.72 2.06 8 14 -4 3.38 1.41 -8 -14 4 4.29 3.99 -8 14 4 4.57 2.51 -8 14 4 2.26 1.57 8 14 -3 13.28 5.32 -8 14 3 30.78 5.92 -8 -14 3 30.27 8.75 -8 14 3 28.34 5.29 8 14 -3 29.95 3.94 8 14 -2 1.59 1.49 -8 -14 2 5.66 4.33 -8 14 2 4.17 2.46 -8 14 2 7.15 2.58 8 14 -2 5.14 1.39 -8 14 1 22.22 4.62 -8 14 1 19.11 4.91 8 14 -1 29.02 3.41 8 14 0 171.03 8.30 8 14 1 169.13 8.54 8 14 1 183.87 8.54 8 14 2 183.86 8.38 8 14 2 161.37 7.97 8 14 3 7.25 1.61 8 14 3 7.02 1.65 8 -14 4 131.91 6.99 8 14 4 128.46 5.72 8 14 5 13.64 1.55 -8 15 12 25.30 3.49 -8 15 11 1.03 1.43 -8 15 10 66.15 7.40 8 15 -10 81.17 6.31 -8 15 9 7.93 2.96 -8 15 9 7.45 2.45 8 15 -9 6.26 1.80 -8 15 8 7.25 3.04 -8 15 8 9.45 2.87 8 15 -8 8.02 2.03 -8 15 7 28.48 4.99 -8 15 7 25.12 4.63 8 15 -7 25.42 3.57 -8 15 6 44.34 5.78 -8 15 6 34.47 5.74 -8 -15 6 35.29 8.78 -8 15 6 50.72 6.69 8 15 -6 58.46 5.25 8 15 -6 57.02 5.41 -8 15 5 37.24 6.33 -8 -15 5 43.26 10.07 -8 15 5 43.56 6.35 8 15 -5 45.78 4.49 8 15 -5 45.69 4.89 -8 -15 4 10.53 4.45 -8 15 4 15.80 4.35 -8 15 4 15.77 3.99 8 15 -4 13.86 2.73 -8 -15 3 392.92 30.45 -8 15 3 399.03 21.78 -8 15 3 426.98 20.55 8 15 -3 467.14 15.38 8 15 -2 42.95 9.94 -8 15 2 48.01 7.73 -8 -15 2 40.39 9.56 -8 15 2 59.82 7.66 8 15 -2 54.17 4.65 -8 15 1 37.88 6.00 8 15 -1 42.31 4.12 -8 15 0 61.12 7.29 8 15 0 77.95 5.55 8 15 1 10.23 2.08 8 15 1 12.85 2.46 8 15 2 154.88 7.63 8 15 2 135.87 7.20 8 15 3 2.92 1.20 8 15 3 1.41 1.09 8 -15 4 36.37 3.58 8 15 4 37.44 3.04 -8 16 12 12.63 2.40 -8 16 11 74.96 6.90 -8 16 10 28.05 4.78 8 16 -10 31.18 3.93 -8 16 9 7.79 2.67 -8 16 9 3.00 1.57 8 16 -9 4.80 1.66 -8 16 8 0.55 0.75 -8 16 8 0.22 0.66 8 16 -8 0.37 0.78 -8 16 7 28.13 4.94 -8 16 7 27.71 5.07 8 16 -7 34.88 4.16 8 16 -6 2.38 1.25 -8 16 6 0.55 0.60 -8 -16 6 1.37 1.91 -8 16 6 -1.14 1.12 -8 16 6 2.40 1.37 8 16 -6 2.66 1.13 -8 16 5 9.24 2.88 -8 -16 5 4.78 3.54 -8 16 5 8.62 3.04 8 16 -5 12.92 2.67 -8 -16 4 60.77 12.31 -8 16 4 62.63 8.32 -8 16 4 65.67 7.92 8 16 -4 86.14 6.64 8 16 -3 269.44 24.03 -8 -16 3 317.44 27.61 -8 16 3 351.43 20.44 -8 16 3 368.60 19.31 8 16 -3 310.96 11.00 8 16 -2 57.88 11.35 -8 -16 2 59.76 11.85 -8 16 2 71.26 9.25 -8 16 2 73.82 8.60 8 16 -2 76.22 5.47 -8 16 1 90.45 9.43 8 16 -1 98.81 6.21 -8 16 0 1.16 1.34 8 16 0 0.50 0.51 8 16 1 4.39 1.41 8 16 1 5.00 1.59 8 16 2 17.98 2.71 8 16 2 14.30 2.28 8 16 3 137.45 6.98 8 16 3 105.43 5.59 8 -16 4 37.68 3.58 8 16 4 39.54 2.99 -8 17 12 43.26 4.40 -8 17 11 3.77 1.86 -8 17 10 15.36 3.59 -8 17 9 1.77 1.68 -8 17 9 1.02 0.97 8 17 -9 0.70 0.85 -8 17 8 4.33 2.18 -8 17 8 6.60 2.96 8 17 -8 7.97 2.14 -8 17 7 3.41 2.13 -8 17 7 2.60 1.52 8 17 -7 4.95 1.68 -8 17 6 1.42 1.72 8 17 -6 2.60 1.30 -8 17 5 -1.38 1.24 -8 17 5 1.31 1.24 -8 -17 4 12.44 5.53 -8 17 4 15.85 4.25 -8 17 4 14.22 3.98 8 17 -3 33.35 8.46 -8 -17 3 60.89 12.23 -8 17 3 54.88 7.99 -8 17 3 63.89 8.09 8 17 -3 52.62 4.45 8 17 -2 20.64 6.96 -8 17 2 26.90 5.45 8 17 -2 25.99 3.14 -8 17 1 77.42 8.82 8 17 -1 87.33 5.82 -8 17 0 21.87 4.55 8 17 0 27.70 3.31 8 17 1 130.62 7.04 8 17 2 27.43 3.22 8 17 2 24.98 2.94 8 17 3 72.00 5.09 8 17 3 49.22 3.74 8 -17 4 15.37 2.16 8 17 4 18.52 2.49 8 17 4 15.76 1.88 -8 18 12 63.25 5.14 -8 18 11 10.41 2.66 -8 18 10 0.45 1.27 -8 18 9 6.68 2.48 -8 18 9 3.90 1.63 -8 18 8 99.95 9.73 -8 18 8 92.48 9.03 8 18 -7 2.85 1.49 -8 18 7 3.23 1.92 -8 18 7 3.62 2.03 -8 18 6 190.27 12.16 -8 18 6 232.24 14.77 -8 18 5 36.41 6.21 -8 -18 5 36.48 9.64 -8 18 5 48.02 6.90 -8 -18 4 276.70 27.04 -8 18 4 261.95 16.97 -8 18 4 310.00 17.78 8 18 -3 5.16 2.82 -8 -18 3 14.57 6.58 -8 18 3 10.02 3.55 -8 18 3 8.74 3.25 8 18 -3 10.37 1.95 -8 18 2 29.03 5.56 8 18 -2 38.01 3.82 -8 18 1 4.16 1.83 8 18 -1 4.00 1.33 -8 18 0 425.70 19.76 8 18 0 568.05 14.78 -8 18 -1 73.22 7.33 8 18 1 134.86 7.10 8 18 2 1.42 0.89 8 18 2 1.37 1.07 8 18 3 6.21 1.38 8 18 3 11.77 2.17 8 -18 4 65.31 4.24 8 18 4 62.45 3.42 -8 19 12 0.01 0.47 -8 19 11 39.79 4.83 -8 19 10 -0.40 1.04 -8 19 9 19.66 4.31 -8 19 9 20.21 4.05 -8 19 8 8.47 3.09 -8 19 8 11.00 3.20 -8 19 7 114.21 10.05 -8 19 7 116.04 10.43 -8 19 6 0.26 1.47 -8 19 6 0.98 1.20 -8 19 5 113.67 10.60 -8 19 4 203.47 14.47 -8 19 3 61.50 8.12 8 19 -3 56.98 4.57 -8 19 2 254.03 16.44 8 19 -2 266.29 9.98 -8 19 1 4.31 2.12 8 19 -1 6.78 1.55 -8 19 0 2.51 1.91 8 19 0 4.74 1.62 -8 19 -1 1.41 1.16 8 19 1 1.58 1.02 8 19 2 200.08 8.43 8 19 2 147.50 6.63 8 19 3 6.04 1.29 8 19 3 7.50 1.81 8 -19 4 2.28 0.76 8 19 4 2.77 0.92 -8 20 12 3.18 1.05 -8 20 11 2.83 1.48 -8 20 10 9.64 2.58 -8 20 9 41.97 6.16 -8 20 9 37.41 5.48 -8 20 8 19.32 4.31 -8 20 8 20.12 4.25 -8 20 7 1.72 1.55 -8 20 7 1.06 1.54 -8 20 6 -0.56 0.77 -8 20 6 -0.47 1.70 -8 20 5 5.53 2.76 -8 20 4 116.81 11.01 -8 20 3 79.32 9.25 8 20 -3 78.82 5.32 -8 20 2 82.75 9.45 8 20 -2 95.37 5.93 -8 20 1 21.79 4.75 8 20 -1 30.89 3.36 -8 20 0 0.77 0.73 8 20 0 3.18 1.34 -8 20 -1 47.24 5.91 8 20 1 87.07 5.61 8 20 2 2.06 1.05 8 20 3 105.42 6.04 8 20 3 66.81 3.84 8 -20 4 32.76 2.58 8 20 4 54.86 3.64 -8 21 12 4.72 1.25 -8 21 11 3.72 1.53 -8 21 10 0.44 0.90 -8 21 9 45.96 6.49 -8 21 9 49.16 6.13 -8 21 8 3.08 1.83 -8 21 8 4.16 1.93 -8 21 7 8.61 2.83 -8 21 7 7.40 2.76 -8 21 6 4.61 1.86 -8 21 6 6.07 2.22 -8 21 5 28.97 5.33 -8 21 4 62.52 8.18 -8 21 3 187.91 14.30 -8 21 2 378.42 20.23 8 21 -2 387.88 11.85 -8 21 1 9.90 3.33 8 21 -1 11.18 2.09 -8 21 0 6.39 2.28 8 21 0 7.95 1.71 -8 21 -1 23.23 4.15 8 21 1 37.79 3.64 8 21 2 47.75 4.09 8 21 3 0.46 0.85 8 21 4 -0.17 0.41 -8 22 12 10.70 1.82 -8 22 11 2.74 1.35 -8 22 10 -0.31 0.83 -8 22 9 2.24 1.35 -8 22 9 1.30 1.17 -8 22 8 11.14 3.24 -8 22 8 7.62 2.55 -8 22 7 4.46 2.23 -8 22 7 8.19 2.83 -8 22 6 8.00 2.40 -8 22 6 8.86 2.48 -8 22 5 10.28 3.16 -8 22 4 228.67 15.53 -8 22 3 31.22 5.76 -8 22 2 22.18 4.95 8 22 -2 20.73 2.70 -8 22 1 85.68 9.44 8 22 -1 98.12 5.91 -8 22 0 88.01 8.96 8 22 0 97.92 5.89 -8 22 -1 83.45 7.86 8 22 1 129.16 6.73 -8 22 -2 1.08 0.78 8 22 2 6.51 1.53 8 22 3 1.43 0.72 8 22 4 -0.31 0.49 -8 23 11 40.24 4.50 -8 23 10 7.34 2.44 -8 23 9 8.35 2.72 -8 23 9 9.55 2.66 -8 23 8 31.15 5.28 -8 23 8 39.24 5.65 -8 23 7 2.48 1.74 -8 23 7 3.99 2.20 -8 23 6 1.40 1.64 -8 23 6 0.64 0.85 -8 23 5 33.60 5.77 -8 23 4 19.15 4.49 -8 23 3 47.18 7.02 -8 23 2 154.85 12.98 8 23 -2 155.19 7.30 -8 23 1 19.33 4.60 8 23 -1 21.71 2.81 -8 23 0 0.08 1.05 8 23 0 0.19 0.81 -8 23 -1 0.75 0.94 8 23 1 0.70 0.49 -8 23 -2 6.22 1.96 8 23 2 13.37 2.12 8 23 3 37.06 3.28 8 23 4 -0.54 0.57 -8 24 11 1.50 1.01 -8 24 10 17.42 3.42 -8 24 9 -2.37 1.44 -8 24 8 3.28 1.70 -8 24 8 2.60 1.65 -8 24 7 0.36 0.71 -8 24 7 1.33 1.61 -8 24 6 80.90 7.77 -8 24 6 132.73 11.15 -8 24 5 168.90 12.95 -8 24 4 33.88 5.90 -8 24 3 27.61 5.41 -8 24 2 47.04 7.14 8 24 -2 41.64 3.77 -8 24 1 78.01 8.80 8 24 -1 84.19 5.37 -8 24 0 3.38 1.67 8 24 0 5.84 1.37 -8 24 -1 3.48 1.62 8 24 1 7.81 1.69 -8 24 -2 5.91 1.78 8 24 2 10.61 2.00 8 24 3 4.27 0.99 -8 25 11 27.38 3.42 -8 25 10 29.58 4.27 -8 25 9 3.34 1.56 -8 25 8 15.72 3.70 -8 25 8 19.13 3.83 -8 25 7 3.24 1.71 -8 25 7 2.50 1.56 -8 25 6 3.55 1.75 -8 25 6 5.62 2.49 -8 25 5 315.96 17.64 -8 25 4 34.00 5.92 -8 25 3 79.66 9.09 -8 25 2 36.21 6.05 8 25 -2 34.96 3.36 -8 25 1 37.37 6.13 8 25 -1 38.59 3.59 -8 25 0 35.87 5.52 8 25 0 41.23 3.78 -8 25 -1 2.40 1.33 8 25 1 2.68 0.98 -8 25 -2 0.35 0.62 8 25 2 -0.55 0.72 8 25 3 7.13 1.28 -8 26 11 -0.12 0.37 -8 26 10 22.06 3.72 -8 26 9 4.92 2.09 -8 26 8 164.12 11.59 -8 26 8 164.48 10.91 -8 26 7 1.25 1.45 -8 26 7 1.13 1.08 -8 26 6 13.50 3.16 -8 26 6 28.90 5.11 -8 26 5 15.46 4.09 -8 26 4 19.66 4.55 -8 26 3 105.24 10.47 -8 26 2 147.30 12.24 -8 26 1 1.41 0.85 8 26 -1 1.95 0.84 -8 26 0 13.14 3.30 8 26 0 12.51 2.08 -8 26 -1 31.48 4.58 8 26 1 50.63 4.13 -8 26 -2 3.55 1.36 8 26 2 8.37 1.64 8 26 3 0.03 0.59 -8 27 11 15.67 2.39 -8 27 10 0.20 0.67 -8 27 9 -0.62 0.57 -8 27 8 16.75 3.58 -8 27 8 13.26 3.08 -8 27 7 8.83 2.71 -8 27 7 11.39 2.90 -8 27 6 2.07 1.55 -8 27 5 41.31 6.18 -8 27 4 31.36 5.54 -8 27 3 20.64 4.59 -8 27 2 123.14 11.04 -8 27 1 135.47 11.20 8 27 -1 140.27 6.81 -8 27 0 32.78 5.17 8 27 0 36.57 3.51 -8 27 -1 27.25 4.19 8 27 1 48.04 4.15 -8 27 -2 1.33 0.74 8 27 2 2.62 0.85 8 27 3 1.34 0.43 -8 28 11 0.53 0.64 -8 28 10 1.26 0.95 -8 28 9 70.91 6.81 -8 28 8 12.65 3.17 -8 28 8 9.35 2.54 -8 28 7 -0.23 0.50 -8 28 7 -0.69 1.14 -8 28 6 59.30 7.11 -8 28 5 3.89 1.92 -8 28 4 74.63 8.34 -8 28 3 9.60 3.19 -8 28 2 27.12 5.07 -8 28 1 9.04 3.06 8 28 -1 8.28 1.68 -8 28 0 16.23 3.52 8 28 0 21.11 2.62 -8 28 -1 11.19 2.85 8 28 1 16.47 2.41 -8 28 -2 -0.36 0.57 8 28 2 -0.40 0.61 -8 29 10 6.36 1.73 -8 29 9 2.75 1.38 -8 29 8 13.77 3.15 -8 29 8 12.67 2.78 -8 29 7 2.45 1.11 -8 29 7 3.11 1.51 -8 29 6 80.96 7.99 -8 29 5 79.41 8.26 -8 29 4 182.98 12.82 -8 29 3 17.26 4.25 -8 29 2 7.22 2.77 -8 29 1 50.57 6.61 -8 29 0 0.03 0.75 8 29 0 1.48 0.91 -8 29 -1 38.24 4.85 8 29 1 55.11 4.06 -8 29 -2 0.30 0.55 8 29 2 -0.38 0.42 -8 30 10 1.28 0.85 -8 30 9 1.09 0.71 -8 30 8 58.35 6.18 -8 30 8 61.30 5.79 -8 30 7 1.96 1.09 -8 30 7 2.01 1.19 -8 30 6 1.53 1.25 -8 30 5 3.47 1.80 -8 30 4 65.87 7.71 -8 30 3 1.59 1.85 -8 30 2 38.62 5.83 -8 30 1 1.87 1.43 -8 30 0 30.51 4.67 8 30 0 31.94 3.18 -8 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178.72 12.49 9 11 -3 201.51 10.41 9 -11 -2 16.27 3.22 9 11 -2 22.03 3.11 9 11 -1 8.14 2.07 9 11 0 22.90 3.15 9 11 0 28.29 3.42 9 11 1 66.55 5.20 9 11 1 81.23 5.56 9 11 2 20.62 2.67 9 11 2 15.55 2.29 9 -11 3 13.39 2.19 9 11 3 19.29 2.44 9 11 3 16.42 2.07 9 -11 4 17.57 1.90 9 -12 -12 5.44 1.39 9 12 -11 16.92 2.68 -9 12 11 15.24 3.24 -9 12 10 10.42 2.73 9 12 -10 11.66 2.38 9 -12 -9 30.77 4.61 9 12 -9 38.55 4.48 -9 12 9 42.60 5.98 9 12 -8 8.46 2.11 -9 12 8 11.06 3.05 -9 12 8 9.10 2.88 9 12 -8 8.28 2.08 -9 12 7 139.05 11.02 9 12 -7 151.27 8.66 9 12 -7 157.50 9.05 -9 12 7 126.55 9.56 9 12 -6 26.35 3.52 -9 12 6 22.30 4.34 9 12 -6 28.60 4.04 -9 12 5 40.93 5.99 9 12 -5 42.91 4.88 9 12 -4 1.74 1.19 -9 12 4 -0.28 0.81 9 -12 -3 194.30 11.71 -9 12 3 223.37 14.19 9 -12 -2 132.26 9.16 -9 12 2 147.18 11.17 9 12 -2 166.63 8.46 9 12 -1 425.10 13.49 9 12 0 15.22 2.54 9 12 0 18.65 2.88 9 12 1 64.37 4.94 9 12 1 49.27 4.37 9 12 2 8.85 1.73 9 12 2 9.42 1.93 9 -12 3 18.95 2.56 9 12 3 22.38 2.31 9 -13 -12 1.50 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10 -1 -1 45.42 4.53 10 1 -1 54.19 4.94 10 -1 -1 46.75 4.50 10 1 0 1.29 0.93 10 -1 0 1.16 0.78 10 1 1 5.24 1.43 10 1 1 5.86 1.49 10 -1 1 4.87 1.37 10 1 2 38.70 3.46 10 -1 2 41.42 3.65 10 1 2 42.52 3.32 10 -1 2 37.27 3.01 10 1 3 8.40 1.30 10 -1 3 10.35 1.49 -10 -2 12 2.66 0.85 -10 2 12 2.71 0.92 10 2 -12 4.16 1.30 10 -2 -12 3.40 1.16 -10 -2 11 3.33 1.11 10 2 -11 4.39 2.00 10 -2 -11 2.32 1.07 10 2 -10 17.25 3.04 10 -2 -10 16.47 2.86 10 2 -9 12.79 2.57 10 -2 -9 11.31 2.50 10 2 -9 13.02 2.63 10 -2 -9 11.94 2.53 10 2 -8 26.90 3.92 10 -2 -8 28.17 4.29 10 2 -8 25.98 3.64 10 2 -7 34.82 4.68 10 -2 -7 31.34 4.57 10 2 -7 31.38 3.88 10 -2 -7 25.37 3.52 10 2 -6 30.99 4.44 10 -2 -6 29.97 4.52 -10 2 6 26.57 4.35 10 2 -5 0.60 0.73 10 -2 -5 1.33 1.19 10 2 -4 65.86 6.29 10 -2 -4 66.76 6.46 10 -2 -3 27.46 4.05 10 2 -3 28.03 3.97 10 2 -2 35.35 4.18 10 -2 -2 31.81 4.03 10 -2 -1 7.04 1.88 10 2 -1 8.97 1.94 10 -2 -1 7.87 1.98 10 2 0 8.99 1.89 10 -2 0 8.17 1.79 10 2 1 2.01 1.02 10 2 1 3.77 1.35 10 -2 1 2.34 1.07 10 2 2 2.29 0.98 10 -2 2 0.97 0.73 10 2 2 1.70 0.92 10 -2 2 1.33 0.73 10 2 3 65.25 3.44 10 -2 3 66.04 3.62 -10 -3 12 3.03 0.89 -10 3 12 2.96 0.89 10 3 -12 3.02 1.06 10 -3 -12 2.88 1.03 -10 -3 11 3.32 0.85 10 3 -11 4.13 1.39 10 -3 -11 2.60 0.77 10 3 -10 13.69 2.72 10 -3 -10 12.18 2.74 10 3 -9 0.21 0.40 10 -3 -9 0.91 0.77 10 3 -8 24.20 3.68 10 -3 -8 22.43 3.83 10 3 -8 22.72 3.37 10 3 -7 37.01 4.74 10 -3 -7 38.82 5.15 -10 3 7 34.97 5.04 10 3 -7 34.98 4.06 10 3 -6 -1.13 1.28 10 -3 -6 2.14 0.98 -10 3 6 0.49 1.15 10 3 -5 7.91 2.36 10 -3 -5 6.45 2.11 10 3 -4 117.16 8.23 10 -3 -4 107.17 8.43 10 3 -3 8.32 2.04 10 -3 -3 8.47 2.26 10 3 -2 2.61 1.12 10 -3 -2 1.36 0.84 10 3 -1 18.55 2.82 10 3 0 2.92 1.16 10 -3 0 1.56 0.91 10 3 1 43.80 4.09 10 3 1 52.76 4.26 10 -3 1 45.69 3.94 10 -3 2 16.42 2.32 10 3 2 20.76 2.32 10 -3 2 15.17 1.83 10 3 2 16.21 2.16 10 3 3 36.06 2.52 10 -3 3 36.23 2.71 -10 -4 12 2.10 0.75 -10 4 12 1.43 0.45 10 -4 -12 2.68 1.02 -10 -4 11 1.13 0.69 10 4 -11 1.90 0.93 10 -4 -11 3.74 2.06 10 4 -10 16.49 2.76 10 -4 -10 11.80 2.47 10 4 -9 11.45 2.39 10 -4 -9 12.51 2.63 10 4 -9 10.69 2.22 10 4 -8 112.27 7.89 10 -4 -8 110.87 8.52 10 4 -8 118.19 7.63 10 4 -7 5.84 2.04 10 -4 -7 2.78 1.35 -10 4 7 3.48 1.54 10 4 -7 2.85 1.02 10 4 -6 5.12 2.04 10 -4 -6 4.78 1.85 -10 4 6 3.67 1.97 10 4 -5 8.54 2.33 10 -4 -5 7.33 2.13 10 4 -4 375.70 14.69 10 -4 -4 335.08 14.72 10 4 -3 -0.01 0.56 10 -4 -3 -0.28 0.83 10 -4 -2 12.07 2.56 10 4 -2 13.69 2.72 10 4 -1 57.20 4.91 10 4 0 37.30 3.85 10 -4 0 32.75 3.66 10 4 1 203.87 8.73 10 -4 1 208.23 8.22 10 -4 2 12.63 2.06 10 4 2 16.04 2.07 10 4 2 15.58 2.11 10 4 3 37.85 2.51 10 -4 3 40.07 2.84 -10 5 12 1.54 0.61 10 5 -12 3.61 1.15 10 -5 -12 3.24 1.04 10 5 -11 36.19 3.79 10 -5 -11 29.88 3.93 10 5 -10 0.30 0.45 10 -5 -9 16.04 3.08 10 5 -9 19.49 3.12 10 5 -9 18.78 2.87 10 -5 -8 173.77 10.80 10 5 -8 177.94 9.34 10 5 -8 182.37 9.87 10 5 -7 41.45 4.94 10 -5 -7 37.86 5.11 -10 5 7 36.89 5.33 10 5 -7 40.72 4.32 10 5 -6 622.77 19.33 10 -5 -6 580.17 20.37 -10 5 6 589.91 21.21 10 5 -5 14.31 3.00 10 -5 -5 12.06 2.90 -10 5 5 14.34 3.30 10 5 -4 12.99 2.72 10 -5 -4 11.99 2.95 10 5 -3 3.18 1.43 10 -5 -3 1.54 0.70 10 -5 -2 36.75 4.42 10 5 -2 43.39 4.71 10 5 -1 23.40 3.13 10 5 0 71.44 5.25 10 -5 0 60.62 4.94 10 5 1 41.70 3.90 10 5 1 51.25 4.17 10 -5 1 40.63 3.62 10 5 2 9.72 1.63 10 -5 2 8.05 1.64 10 5 2 11.48 1.80 10 -5 3 4.46 0.99 10 6 -12 1.82 0.85 10 -6 -12 2.71 1.01 10 6 -11 27.89 3.31 10 -6 -11 24.87 3.39 10 6 -10 198.54 9.45 10 6 -9 4.69 1.45 10 -6 -9 5.01 1.55 10 6 -9 5.56 1.67 10 -6 -8 45.08 5.58 10 6 -8 45.35 4.69 10 6 -8 46.52 4.89 10 -6 -7 20.54 3.93 10 6 -7 22.11 3.19 -10 6 7 18.20 3.75 10 6 -7 22.07 3.66 10 6 -6 42.93 5.21 10 -6 -6 39.70 5.85 -10 6 6 42.73 5.75 10 -6 -5 78.46 7.37 -10 6 5 71.61 7.33 10 6 -5 82.15 6.97 10 -6 -4 14.48 3.11 10 6 -4 16.91 3.21 10 6 -3 2.50 1.42 10 -6 -3 1.88 1.17 10 -6 -2 44.71 4.84 10 6 -2 49.72 4.57 10 6 -2 51.85 5.10 10 6 -1 45.13 4.39 10 6 0 0.62 0.50 10 6 0 2.87 1.29 10 -6 0 2.62 1.11 10 6 1 29.64 3.24 10 6 1 36.87 3.50 10 -6 1 31.78 3.13 10 6 2 0.99 0.68 10 -6 2 0.29 0.49 10 6 2 1.24 0.69 10 -6 3 0.94 0.51 10 -7 -12 1.61 0.72 10 7 -11 6.77 1.67 10 -7 -11 4.18 1.30 10 7 -10 11.49 2.39 10 -7 -9 14.41 2.89 10 7 -9 16.25 2.78 10 7 -8 8.70 2.18 10 -7 -8 9.34 2.67 10 7 -8 7.64 1.93 10 -7 -7 38.32 5.22 -10 7 7 44.32 5.94 10 7 -7 40.35 4.29 10 7 -7 41.51 4.80 10 -7 -6 136.50 9.99 -10 7 6 135.58 10.33 10 7 -6 144.68 9.19 10 -7 -5 17.51 3.59 -10 7 5 16.19 3.57 10 7 -5 17.78 3.35 10 -7 -4 292.74 13.95 10 7 -4 348.65 14.01 10 -7 -3 51.59 5.56 10 7 -3 64.94 5.92 10 -7 -2 46.94 4.96 10 7 -2 53.20 4.85 10 7 -1 -0.20 0.88 10 7 0 0.58 0.51 10 7 0 2.15 1.21 10 -7 0 0.69 0.51 10 7 1 46.89 3.94 10 7 1 57.90 4.35 10 -7 1 47.25 3.71 10 -7 2 28.08 2.98 10 7 2 34.77 2.99 10 7 2 28.55 2.60 10 -7 3 11.39 1.48 10 -8 -12 5.29 1.32 10 8 -11 0.25 0.56 10 -8 -11 -0.70 0.96 10 8 -10 1.27 1.06 10 -8 -9 0.74 0.69 -10 8 9 1.88 1.74 10 8 -9 0.44 0.39 10 8 -8 0.47 0.50 10 -8 -8 2.33 1.15 -10 8 8 0.84 1.21 -10 8 8 0.78 1.38 10 8 -8 1.62 1.03 10 8 -7 0.83 0.80 10 -8 -7 0.80 0.62 -10 8 7 0.13 1.19 10 8 -7 0.08 0.60 10 8 -6 12.93 2.77 10 -8 -6 9.68 2.77 -10 8 6 6.90 2.48 10 -8 -5 29.37 4.56 -10 8 5 33.11 5.14 10 8 -5 39.24 4.80 10 -8 -4 22.05 3.90 10 8 -4 26.71 3.89 10 8 -3 3.59 1.58 10 -8 -3 2.23 1.45 10 -8 -2 33.95 4.25 10 8 -2 41.26 4.17 10 8 -1 168.91 8.34 10 8 0 4.65 1.21 10 -8 0 2.42 0.79 10 8 1 0.44 0.40 10 8 1 0.03 0.43 10 -8 1 1.35 0.87 10 8 2 3.90 0.98 10 -8 2 2.10 0.66 10 8 2 2.80 0.91 10 -9 -12 5.00 1.37 10 9 -11 5.80 1.60 10 -9 -11 2.90 1.06 10 9 -10 68.06 5.44 10 -9 -9 19.33 3.45 10 9 -9 26.09 3.48 -10 9 9 26.81 4.50 10 9 -8 3.66 1.61 10 -9 -8 4.64 1.69 -10 9 8 5.94 2.84 -10 9 8 2.94 1.93 10 9 -8 2.35 1.05 10 -9 -7 185.95 11.84 -10 9 7 205.65 12.88 10 9 -7 206.91 9.64 10 9 -7 209.64 10.66 10 9 -6 1.25 0.96 10 -9 -6 0.03 0.74 -10 9 6 0.05 0.86 10 9 -5 1.26 1.10 10 -9 -5 1.48 1.31 -10 9 5 0.87 0.65 10 9 -4 10.24 2.41 10 -9 -4 5.00 1.67 -10 9 4 7.18 2.18 10 9 -3 1.84 1.29 10 -9 -3 2.07 1.37 10 -9 -2 17.28 3.04 10 9 -2 22.78 3.10 10 9 -1 29.69 3.45 10 9 0 0.25 0.73 10 9 0 0.42 0.78 10 -9 0 -0.86 0.78 10 9 1 0.08 0.41 10 9 1 0.11 0.48 10 9 2 0.86 0.53 10 -9 2 -0.54 0.76 10 9 2 1.51 0.71 10 -10 -12 27.26 2.91 10 10 -11 15.25 2.39 10 10 -10 17.36 2.90 -10 10 10 20.88 3.94 10 -10 -9 16.15 3.28 10 10 -9 17.60 2.83 -10 10 9 17.83 3.72 10 -10 -8 224.94 12.72 -10 10 8 253.39 14.17 10 10 -8 250.31 10.87 -10 10 8 224.35 12.37 10 10 -8 242.63 10.84 10 10 -7 5.12 1.68 10 -10 -7 3.64 1.76 -10 10 7 5.81 1.96 -10 10 7 4.60 2.36 10 10 -7 4.92 1.49 10 -10 -6 15.91 3.49 -10 10 6 22.38 4.48 10 10 -6 20.40 3.53 10 -10 -5 21.25 3.83 -10 10 5 25.36 4.59 10 10 -5 27.84 3.97 10 10 -4 1.38 1.19 10 -10 -4 0.47 0.68 -10 10 4 1.23 0.73 10 10 -3 110.42 6.90 10 10 -3 129.29 8.31 10 -10 -2 2.72 1.30 10 10 -2 4.86 1.45 10 10 -1 14.54 2.34 10 10 0 1.59 0.79 10 10 0 2.53 1.16 10 -10 0 0.60 0.47 10 10 1 9.48 1.63 10 10 1 12.29 1.94 10 -10 2 18.58 2.35 10 10 2 23.31 2.43 10 10 2 16.94 1.83 10 -11 -12 1.15 0.91 10 -11 -10 9.82 2.09 10 11 -10 17.16 2.77 -10 11 10 15.67 3.28 10 -11 -9 8.96 2.45 -10 11 9 11.04 2.96 10 11 -9 12.99 2.43 10 11 -8 0.78 0.92 10 -11 -8 1.98 1.44 -10 11 8 0.49 1.20 -10 11 8 -0.07 1.32 10 11 -8 0.70 0.87 10 -11 -7 18.57 3.72 -10 11 7 21.50 4.28 10 11 -7 25.59 3.38 -10 11 7 18.12 3.32 10 11 -7 24.33 3.59 10 -11 -6 167.91 11.31 -10 11 6 177.56 12.30 10 -11 -5 18.25 3.62 -10 11 5 21.21 4.36 10 11 -5 26.86 3.93 10 -11 -4 96.47 8.05 -10 11 4 103.45 9.12 10 -11 -3 101.10 7.83 10 11 -3 131.15 7.43 10 -11 -2 0.31 0.37 10 11 -2 0.16 0.57 10 11 -1 0.36 0.75 10 11 0 0.56 0.75 10 -11 0 0.07 0.62 10 11 1 49.58 3.81 10 11 1 36.26 3.03 10 -11 2 12.85 1.91 10 11 2 12.80 1.53 10 -12 -12 22.92 2.55 10 -12 -10 1.00 0.73 -10 12 10 4.12 2.37 10 12 -10 2.87 1.28 10 -12 -9 0.32 0.44 -10 12 9 0.21 0.50 10 12 -9 1.61 1.04 10 -12 -8 21.88 4.08 -10 12 8 26.14 4.76 10 12 -8 25.16 3.44 -10 12 8 16.77 3.32 10 12 -7 4.68 1.64 10 -12 -7 5.41 2.07 -10 12 7 4.28 1.71 -10 12 7 4.70 2.09 10 12 -7 6.42 1.76 10 12 -6 2.66 1.51 10 -12 -6 1.23 1.78 -10 12 6 -0.03 0.95 10 -12 -5 23.87 4.23 -10 12 5 29.71 5.15 10 12 -5 37.43 4.57 10 12 -4 11.81 2.78 10 -12 -4 9.38 2.73 -10 12 4 7.91 2.74 10 -12 -3 20.25 3.53 -10 12 3 22.35 4.05 10 12 -3 31.01 3.60 10 -12 -2 8.09 2.10 10 12 -2 12.02 2.19 10 12 -1 156.68 7.62 10 12 0 22.20 2.70 10 -12 0 17.81 2.42 10 12 1 18.18 2.26 10 12 1 13.14 1.77 10 -12 2 9.98 1.69 10 12 2 15.51 1.96 10 -13 -12 3.19 0.98 10 -13 -10 56.09 5.02 -10 13 10 74.19 6.82 10 -13 -9 -0.06 0.98 -10 13 9 0.10 0.81 10 13 -9 1.67 1.09 10 -13 -8 56.56 6.51 -10 13 8 60.93 7.08 10 13 -8 69.85 5.71 -10 13 8 51.69 5.73 -10 13 7 27.38 4.78 10 13 -6 11.45 2.54 -10 13 6 5.31 2.03 10 -13 -5 164.34 10.95 -10 13 5 191.46 12.96 10 -13 -4 47.44 5.64 -10 13 4 49.02 6.45 10 13 -4 62.75 5.10 10 -13 -3 47.46 5.34 -10 13 3 49.03 6.09 10 13 -3 64.22 5.14 10 -13 -2 46.65 4.85 10 13 -2 69.68 5.21 10 13 -1 14.11 2.32 10 13 0 5.97 1.51 10 13 1 12.67 1.89 10 -13 2 10.58 1.69 10 13 2 18.95 2.19 10 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0.72 10 15 2 0.49 0.60 10 -16 -10 11.27 2.31 -10 16 10 13.29 2.85 10 -16 -9 3.69 1.56 -10 16 9 5.91 1.84 -10 16 8 0.43 0.92 -10 16 8 0.89 1.10 -10 16 7 0.27 0.71 -10 16 6 -0.56 1.05 -10 16 5 0.01 1.19 10 16 -5 0.40 0.41 10 -16 -4 8.51 2.49 -10 16 4 15.23 3.66 10 16 -4 11.49 2.04 10 -16 -3 0.82 0.64 -10 16 3 0.42 0.53 10 16 -3 1.69 0.86 10 -16 -2 1.90 1.10 -10 16 2 1.43 0.98 10 16 -2 2.64 0.97 10 16 -1 9.40 1.88 10 16 0 0.13 0.85 10 16 1 25.67 2.64 10 -16 2 -1.40 0.68 10 16 2 0.55 0.45 10 -17 -10 3.22 1.37 -10 17 10 4.18 1.55 10 -17 -9 -0.65 0.81 -10 17 9 0.64 0.91 -10 17 8 5.08 1.86 -10 17 8 6.87 2.17 -10 17 7 2.11 1.01 -10 17 6 7.10 2.46 -10 17 5 29.06 5.28 10 -17 -4 0.02 1.00 -10 17 4 1.55 0.60 10 17 -4 2.00 1.04 10 -17 -3 2.57 1.13 -10 17 3 3.44 1.73 10 17 -3 6.04 1.49 -10 17 2 2.07 0.67 10 17 -2 6.91 1.52 10 17 -1 0.92 0.82 10 17 0 2.50 0.97 10 17 1 19.08 2.24 10 -17 2 8.38 1.32 10 17 2 13.19 1.70 10 -18 -10 2.35 1.07 -10 18 10 1.30 0.89 10 -18 -9 4.93 1.73 -10 18 9 4.35 1.72 -10 18 8 20.83 4.02 -10 18 8 21.65 3.45 -10 18 7 0.76 1.17 -10 18 6 45.88 6.38 -10 18 5 18.95 4.27 10 -18 -4 6.89 2.14 -10 18 4 7.28 2.41 10 18 -4 12.35 2.12 10 -18 -3 8.45 2.19 -10 18 3 11.40 3.01 10 18 -3 16.91 2.45 -10 18 2 27.08 4.17 10 18 -2 47.35 3.98 10 18 -1 3.25 1.12 10 18 0 6.65 1.44 10 18 1 15.00 2.01 10 18 2 0.09 0.40 10 -19 -10 2.67 1.13 -10 19 10 3.23 1.35 10 -19 -9 5.30 1.60 -10 19 9 3.74 1.48 -10 19 8 0.80 1.17 -10 19 8 0.57 0.69 -10 19 7 68.82 7.55 -10 19 6 9.23 2.94 -10 19 5 29.53 5.21 10 -19 -4 83.41 7.23 -10 19 4 100.01 9.35 10 -19 -3 85.94 6.90 -10 19 3 102.67 9.05 -10 19 2 1.13 1.06 10 19 -2 4.14 1.23 10 19 -1 45.28 3.69 10 19 0 5.20 1.17 10 19 1 34.84 2.95 10 -20 -10 9.69 2.00 -10 20 10 14.07 2.66 10 -20 -9 0.35 0.81 -10 20 9 -0.22 0.64 -10 20 8 6.30 1.85 -10 20 8 10.31 2.73 -10 20 7 1.96 1.51 -10 20 6 1.53 1.55 -10 20 5 13.09 3.28 10 -20 -4 1.34 1.03 -10 20 4 2.13 1.47 10 -20 -3 -0.09 0.41 -10 20 3 0.90 0.73 10 20 -3 0.73 0.61 -10 20 2 12.45 2.91 10 20 -2 19.90 2.48 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1.73 -11 20 4 5.40 1.68 -11 20 3 1.99 0.96 11 20 -3 2.19 0.77 11 20 -2 16.49 1.92 11 20 -1 12.26 1.59 11 -21 -9 1.59 0.73 11 -21 -8 9.87 2.14 -11 21 8 12.98 2.80 11 -21 -7 6.80 1.91 -11 21 7 8.14 2.32 11 -21 -6 0.14 0.63 -11 21 6 1.44 1.09 11 -21 -5 -0.22 0.55 -11 21 5 0.23 0.79 11 -21 -4 -0.95 0.91 -11 21 4 -2.70 1.27 -11 21 3 3.85 1.33 11 21 -3 9.90 1.49 11 21 -2 6.30 1.19 11 21 -1 1.32 0.61 11 -22 -9 5.23 1.30 11 -22 -8 15.33 2.59 -11 22 8 26.41 3.80 11 -22 -7 -0.46 0.71 -11 22 7 0.26 0.91 11 -22 -6 0.39 0.39 -11 22 6 0.79 1.00 11 -22 -5 20.20 3.00 -11 22 5 27.65 4.16 11 -22 -4 -0.52 0.70 -11 22 4 -0.03 0.43 -11 22 3 6.98 1.69 11 22 -3 18.45 1.91 11 22 -2 28.66 2.37 11 22 -1 1.17 0.56 11 -23 -9 14.19 2.14 11 -23 -8 2.76 1.17 -11 23 8 5.01 1.71 11 -23 -7 11.44 2.27 -11 23 7 14.32 2.92 11 -23 -6 57.44 5.18 -11 23 6 83.91 7.13 11 -23 -5 10.26 2.12 -11 23 5 14.37 2.93 11 -23 -4 -0.19 0.76 -11 23 4 0.37 0.81 -11 23 3 4.53 1.34 11 23 -2 20.80 1.95 11 -24 -9 1.13 0.71 11 -24 -8 12.99 2.37 -11 24 8 22.98 3.39 11 -24 -7 7.60 1.83 -11 24 7 9.59 2.26 11 -24 -6 -0.52 0.67 -11 24 6 1.48 1.17 11 -24 -5 5.62 1.51 -11 24 5 11.95 2.55 11 -24 -4 1.40 0.55 -11 24 4 0.90 0.41 -11 24 3 0.42 0.62 11 -25 -9 5.94 1.29 11 -25 -8 0.88 0.44 11 -25 -7 1.96 0.97 -11 25 7 3.74 1.32 11 -25 -6 11.58 2.20 -11 25 6 16.78 3.00 11 -25 -5 7.33 1.62 -11 25 5 10.65 2.42 11 -25 -4 -0.06 0.46 -11 25 4 -0.18 0.70 -11 25 3 0.35 0.62 11 -26 -8 11.85 2.01 11 -26 -7 1.98 0.91 -11 26 7 3.10 1.17 11 -26 -6 8.19 1.77 -11 26 6 10.35 2.30 11 -26 -5 1.46 0.77 -11 26 5 1.34 0.94 11 -26 -4 7.00 1.34 -11 26 4 11.28 2.26 -11 26 3 8.36 1.70 11 -27 -8 1.39 0.71 11 -27 -7 17.43 2.46 -11 27 7 24.48 3.24 11 -27 -6 1.55 0.82 -11 27 6 2.61 1.17 11 -27 -5 8.65 1.65 -11 27 5 11.84 2.36 -11 27 4 11.52 2.19 11 -28 -8 2.99 1.01 11 -28 -7 0.77 0.49 -11 28 7 0.83 0.42 11 -28 -6 2.55 0.95 -11 28 6 3.54 1.31 11 -28 -5 3.10 0.99 -11 28 5 4.16 1.36 -11 28 4 0.73 0.61 11 -29 -7 0.27 0.32 -11 29 7 0.58 0.48 11 -29 -6 4.69 1.23 -11 29 6 5.06 1.36 11 -29 -5 13.10 1.76 -11 29 5 19.56 2.70 -11 29 4 29.53 3.12 11 -30 -6 1.47 0.69 -11 30 6 1.21 0.61 -11 30 5 1.14 0.84 12 0 -10 10.86 1.68 12 0 -9 0.41 0.59 12 0 -8 10.39 2.12 12 0 -7 1.41 0.95 12 0 -6 20.00 2.98 12 0 -5 0.89 0.83 12 0 -4 90.98 5.89 12 0 -3 -0.80 0.72 12 0 -2 82.49 4.33 12 0 -2 123.78 5.60 12 0 -1 0.72 0.49 12 1 -10 15.30 1.95 12 -1 -10 12.39 1.75 12 1 -9 3.58 1.16 12 -1 -9 3.59 1.30 12 1 -8 9.11 1.94 12 -1 -8 8.90 2.01 12 1 -7 6.93 1.81 12 -1 -7 5.71 1.71 12 1 -6 3.97 1.60 12 -1 -6 2.93 1.41 12 1 -5 10.34 2.36 12 -1 -5 10.20 2.35 12 1 -4 24.76 2.86 12 1 -4 29.19 3.37 12 -1 -4 29.20 3.40 12 1 -3 3.96 1.02 12 -1 -3 3.10 0.87 12 1 -2 2.80 1.01 12 -1 -2 2.79 1.03 12 1 -1 2.83 0.86 12 -1 -1 3.24 0.88 12 -2 -10 5.56 1.18 12 2 -9 13.86 2.20 12 -2 -9 13.56 2.26 12 2 -8 0.42 0.62 12 -2 -8 1.03 1.03 12 2 -7 7.04 1.84 12 -2 -7 5.78 1.61 12 2 -6 11.92 2.26 12 -2 -6 8.65 1.95 12 2 -5 43.18 4.20 12 -2 -5 38.84 4.03 12 -2 -4 3.67 1.82 12 2 -4 3.79 1.10 12 2 -3 0.65 0.46 12 -2 -3 0.89 0.46 12 2 -2 -0.04 0.48 12 -2 -2 -0.26 0.57 12 2 -1 50.97 3.12 12 -2 -1 47.70 2.96 12 -3 -10 -0.34 0.42 12 3 -9 8.36 1.73 12 -3 -9 8.29 1.80 12 3 -8 18.45 2.72 12 -3 -8 16.59 2.68 12 3 -7 1.63 1.18 12 -3 -7 0.34 0.93 12 3 -6 48.18 4.49 12 -3 -6 42.97 4.37 12 3 -5 5.43 1.74 12 -3 -5 4.17 1.54 12 3 -4 84.47 5.23 12 -3 -4 78.64 5.41 12 3 -3 5.14 1.28 12 -3 -3 2.44 0.78 12 3 -2 0.55 0.64 12 -3 -2 -0.34 0.49 12 -3 -1 2.12 0.62 12 3 -1 4.27 1.02 12 -3 -1 3.77 0.92 12 -4 -10 1.30 0.75 12 -4 -9 11.90 2.09 12 4 -8 3.30 1.29 12 -4 -8 2.48 1.29 12 4 -7 3.18 1.25 12 -4 -7 4.77 1.73 12 -4 -6 13.49 2.62 12 4 -6 16.27 2.82 12 -4 -5 9.65 2.01 12 4 -5 15.50 2.63 12 4 -4 18.81 2.48 12 -4 -4 20.08 2.77 12 4 -3 6.70 1.43 12 -4 -3 5.02 1.19 12 4 -2 6.01 1.24 12 -4 -2 4.61 1.13 12 4 -1 9.13 1.34 12 -4 -1 6.96 1.11 12 -5 -10 15.94 1.90 12 -5 -10 14.54 1.89 12 -5 -9 0.88 0.56 12 -5 -8 19.56 2.93 12 5 -8 24.02 3.08 12 -5 -7 17.48 2.89 12 5 -7 20.10 2.88 12 -5 -6 26.73 3.47 12 5 -6 33.82 3.82 12 5 -5 0.41 0.88 12 -5 -5 0.09 0.41 12 5 -5 -0.40 0.56 12 5 -4 11.24 1.90 12 -5 -4 10.92 2.05 12 5 -3 20.01 2.41 12 -5 -3 18.27 2.37 12 5 -2 7.60 1.42 12 -5 -2 3.90 1.13 12 5 -1 0.03 0.31 12 -5 -1 0.72 0.42 12 -6 -10 1.48 0.68 12 -6 -10 0.81 0.57 12 -6 -9 12.66 2.19 12 -6 -8 12.08 2.35 12 -6 -7 44.48 4.60 12 6 -7 60.69 4.95 12 -6 -6 10.37 2.32 12 6 -6 14.58 2.57 12 -6 -5 2.34 0.94 12 6 -5 4.61 1.15 12 -6 -4 0.80 0.73 12 6 -4 0.49 0.46 12 6 -3 9.46 1.61 12 -6 -3 5.69 1.19 12 -6 -3 8.88 1.63 12 6 -2 32.75 2.77 12 -6 -2 27.15 2.54 12 -6 -1 0.31 0.32 12 6 -1 2.36 0.78 12 -7 -10 12.74 1.78 12 -7 -9 0.68 0.88 12 -7 -8 4.49 1.57 12 -7 -7 20.49 3.13 12 -7 -6 4.18 1.51 12 7 -6 2.23 0.76 12 -7 -5 -0.02 0.35 12 7 -5 -0.45 0.62 12 -7 -4 6.11 1.75 12 7 -4 6.60 1.44 12 -7 -3 1.39 0.82 12 7 -3 0.33 0.49 12 -7 -3 -0.91 0.78 12 7 -2 1.19 0.59 12 -7 -2 0.38 0.35 12 -7 -1 28.34 2.41 12 7 -1 45.05 2.86 12 -8 -10 0.32 0.61 12 -8 -9 76.82 5.28 12 -8 -8 15.33 2.58 12 -8 -7 7.41 1.86 12 8 -7 6.88 1.36 12 -8 -6 0.05 0.61 12 8 -6 -0.77 0.74 12 -8 -5 3.15 1.20 12 8 -5 1.61 0.60 12 8 -4 34.48 3.15 12 -8 -4 28.06 3.10 12 -8 -3 14.07 1.98 12 -8 -3 15.01 2.02 12 8 -2 2.09 0.73 12 -8 -2 1.32 0.58 12 8 -1 5.00 1.00 12 -9 -9 3.91 1.35 12 -9 -8 1.13 0.80 12 -9 -7 2.75 1.27 12 9 -7 0.92 0.41 12 -9 -6 0.09 0.72 12 9 -6 0.02 0.46 12 -9 -5 1.99 1.05 12 9 -5 1.62 0.69 12 -9 -4 0.54 0.74 12 9 -4 0.85 0.61 12 -9 -3 0.73 0.49 12 9 -3 1.86 0.82 12 -9 -3 0.60 0.39 12 9 -2 1.61 0.72 12 -9 -2 0.17 0.25 12 9 -1 1.10 0.44 12 -10 -9 3.07 1.10 12 -10 -8 1.36 0.82 12 -10 -7 6.02 1.67 12 -10 -6 0.01 0.46 12 10 -6 -0.04 0.30 12 -10 -5 3.29 1.24 12 10 -5 1.17 0.47 12 -10 -4 -0.17 0.54 12 10 -4 0.03 0.32 12 10 -3 19.46 2.17 12 -10 -3 12.61 1.76 12 10 -2 2.53 0.74 12 -10 -2 1.75 0.64 12 10 -1 1.03 0.44 12 -11 -9 0.60 0.72 12 -11 -8 2.28 1.13 12 -11 -7 2.87 1.11 12 -11 -6 0.84 0.86 12 11 -6 -0.73 0.55 12 -11 -5 6.99 1.74 12 11 -5 6.89 1.42 12 -11 -4 0.16 0.35 12 11 -4 0.39 0.30 12 11 -3 1.60 0.68 12 -11 -3 -0.30 0.48 12 11 -2 0.91 0.45 12 -11 -2 0.81 0.44 12 11 -1 0.19 0.28 12 -12 -9 34.94 3.46 12 -12 -8 5.15 1.53 12 -12 -7 1.18 0.90 12 -12 -6 7.51 1.83 12 12 -6 7.61 1.34 12 -12 -5 1.48 0.95 12 12 -5 2.56 0.81 12 -12 -4 5.95 1.37 12 12 -4 8.15 1.40 12 12 -3 0.21 0.50 12 -12 -3 -0.47 0.75 12 12 -2 9.32 1.33 12 -12 -2 6.79 1.10 12 12 -1 21.14 1.80 12 -13 -9 9.14 1.85 12 -13 -8 24.00 3.14 12 -13 -7 7.95 1.98 12 -13 -6 3.88 1.29 12 -13 -5 11.07 2.06 12 13 -5 13.05 1.74 12 -13 -4 2.34 0.88 12 13 -4 3.37 0.87 12 13 -3 1.69 0.62 12 -13 -3 0.24 0.40 12 13 -2 -0.15 0.32 12 -14 -9 28.23 3.02 12 -14 -8 7.44 1.82 12 -14 -7 31.15 3.53 12 -14 -6 1.40 0.74 12 -14 -5 5.83 1.51 12 14 -5 8.94 1.42 12 -14 -4 6.36 1.35 12 14 -4 9.95 1.52 12 14 -3 -0.53 0.46 12 -14 -3 0.12 0.31 12 14 -2 0.50 0.40 12 -15 -9 54.87 4.13 12 -15 -8 1.22 0.84 12 -15 -7 0.96 0.84 12 -15 -6 1.39 0.78 -12 15 6 1.76 0.77 12 -15 -5 0.89 0.74 12 15 -5 0.29 0.21 12 15 -4 13.72 1.71 12 -15 -4 8.35 1.56 12 15 -3 0.49 0.39 12 -15 -3 -0.09 0.36 12 15 -2 12.14 1.41 12 -16 -9 1.53 0.73 12 -16 -8 17.03 2.51 12 -16 -7 20.97 2.86 12 -16 -6 5.38 1.46 -12 16 6 5.58 1.62 12 -16 -5 2.60 0.97 12 -16 -4 6.18 1.29 12 16 -4 9.28 1.30 12 16 -3 -0.03 0.24 12 -16 -3 -0.07 0.22 12 16 -2 0.27 0.22 12 -17 -9 0.52 0.45 12 -17 -8 0.99 0.62 12 -17 -7 11.37 2.08 12 -17 -6 0.82 0.40 -12 17 6 1.78 0.98 12 -17 -5 1.48 0.80 12 -17 -4 -0.12 0.46 12 17 -4 0.16 0.21 12 17 -3 3.10 0.71 12 -18 -9 18.77 2.22 12 -18 -8 0.31 0.39 12 -18 -7 12.49 2.13 12 -18 -6 5.85 1.45 -12 18 6 4.97 1.53 12 -18 -5 1.90 0.92 12 -18 -4 6.28 1.16 12 -19 -8 0.41 0.46 12 -19 -7 1.44 0.80 12 -19 -6 1.10 0.66 -12 19 6 1.03 0.77 12 -19 -5 14.15 2.02 12 -20 -8 -0.34 0.49 12 -20 -7 5.67 1.40 12 -20 -6 8.66 1.65 -12 20 6 9.77 1.99 12 -20 -5 1.37 0.68 12 -21 -8 -0.08 0.47 12 -21 -7 8.36 1.63 12 -21 -6 1.97 0.79 -12 21 6 1.58 0.71 12 -21 -5 4.64 1.08 12 -22 -8 19.60 2.22 12 -22 -7 27.79 2.78 12 -22 -6 0.18 0.23 -12 22 6 0.60 0.47 12 -23 -7 4.03 1.04 12 -23 -6 0.40 0.39 13 0 -7 -0.69 0.49 13 0 -6 30.61 2.66 13 0 -5 -0.69 0.52 13 0 -4 1.72 0.58 13 0 -3 0.81 0.50 13 1 -8 1.68 0.60 13 -1 -8 6.31 1.73 13 -1 -7 4.26 1.24 13 1 -7 1.61 0.51 13 1 -6 1.37 0.50 13 -1 -6 1.71 0.51 13 1 -5 1.02 0.43 13 -1 -5 0.19 0.38 13 1 -4 2.67 0.72 13 -1 -4 3.78 0.86 13 1 -3 5.68 0.95 13 -2 -8 34.76 3.13 13 -2 -7 1.21 0.96 13 2 -7 0.53 0.30 13 -2 -6 4.86 1.30 13 2 -6 4.47 0.99 13 -2 -6 4.35 1.03 13 2 -5 1.80 0.66 13 -2 -5 1.15 0.44 13 2 -4 16.58 1.76 13 -2 -4 16.44 1.78 13 2 -3 16.10 1.58 13 -3 -8 2.38 0.98 13 3 -7 12.72 1.60 13 -3 -7 19.34 2.41 13 -3 -6 4.76 1.26 13 3 -6 3.03 0.86 13 3 -5 31.37 2.56 13 -3 -5 25.89 2.39 13 3 -4 1.07 0.51 13 -3 -4 0.12 0.37 13 -4 -8 2.92 1.00 13 -4 -7 0.64 0.65 13 4 -7 -0.60 0.58 13 4 -6 15.90 1.83 13 -4 -6 20.25 2.39 13 4 -5 3.22 0.87 13 -4 -5 1.22 0.36 13 4 -4 8.12 1.27 13 -4 -4 4.62 0.95 13 -5 -8 1.20 0.67 13 -5 -7 6.42 1.38 13 5 -7 3.78 0.81 13 5 -6 4.80 0.98 13 -5 -6 8.08 1.62 13 5 -5 57.19 3.38 13 -5 -5 44.80 3.14 13 5 -4 14.98 1.62 13 -5 -4 10.71 1.41 13 -6 -8 9.50 1.64 13 -6 -7 0.82 0.51 13 6 -6 22.97 2.12 13 -6 -6 22.10 2.47 13 6 -5 16.60 1.78 13 -6 -5 12.19 1.62 13 6 -4 10.50 1.34 13 -6 -4 6.48 1.10 13 -7 -8 27.36 2.69 13 -7 -7 8.85 1.60 13 -7 -6 4.33 1.10 13 7 -6 3.47 0.78 13 -7 -5 4.44 1.09 13 7 -5 4.56 0.93 13 -7 -5 2.74 0.78 13 7 -4 1.85 0.62 13 -7 -4 0.39 0.24 13 -8 -8 10.65 1.69 13 -8 -7 5.03 1.25 13 8 -6 8.35 1.19 13 -8 -6 9.36 1.60 13 8 -5 11.17 1.41 13 -8 -5 8.80 1.35 13 -8 -5 9.48 1.48 13 8 -4 5.93 0.98 13 -8 -4 2.89 0.73 13 -9 -8 3.61 1.04 13 -9 -7 3.42 1.04 13 -9 -6 10.38 1.66 13 -9 -5 87.99 4.21 13 -9 -5 91.46 4.41 13 -9 -4 7.48 1.10 13 -10 -8 -0.07 0.45 13 -10 -7 28.70 2.76 13 -10 -6 0.20 0.39 13 -10 -5 7.76 1.22 13 -10 -5 9.29 1.38 13 -11 -8 0.45 0.46 13 -11 -7 9.88 1.60 13 -11 -6 1.66 0.69 13 -11 -5 6.18 1.07 13 -12 -8 3.14 0.85 13 -12 -7 8.02 1.40 13 -12 -6 1.39 0.63 13 -12 -5 12.91 1.51 13 -13 -7 0.07 0.33 13 -13 -6 5.12 1.04 13 -14 -7 7.23 1.25 0 0 0 0.00 0.00 TITL 1096_2 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 10.872091 42.579691 10.915139 90.0000 118.6993 90.0000 ZERR 38.00 0.000286 0.000855 0.000322 0.0000 0.0036 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 418.00 380.00 38.00 38.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 15530 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.073 _oxdiff_exptl_absorpt_empirical_full_min 0.457 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group F4 F 0.2780(4) 0.53522(8) 0.7031(5) 0.1038(14) Uani 1 1 d . . . . . F3 F 0.2890(4) 0.52822(8) 0.5126(5) 0.0991(12) Uani 1 1 d . . . . . F1 F 0.4749(3) 0.56251(6) 0.4806(3) 0.0529(6) Uani 1 1 d . . . . . F6 F 0.3874(4) 0.47935(8) 0.6830(7) 0.153(2) Uani 1 1 d . U . . . F7 F 0.5495(4) 0.50281(9) 0.6628(8) 0.1475(18) Uani 1 1 d . U . . . F5 F 0.5335(5) 0.50940(10) 0.8458(8) 0.164(2) Uani 1 1 d . U . . . F2 F 0.4654(4) 0.57835(6) 0.7927(3) 0.0661(8) Uani 1 1 d . . . . . O1 O 0.8419(2) 0.65559(6) 0.6850(3) 0.0372(6) Uani 1 1 d . . . . . N1 N 0.6207(3) 0.65781(6) 0.6709(3) 0.0266(6) Uani 1 1 d . . . . . N2 N 0.6912(3) 0.61254(7) 0.6307(3) 0.0293(6) Uani 1 1 d D . . . . C1 C 0.6061(3) 0.69141(8) 0.6627(4) 0.0269(6) Uani 1 1 d . . . . . C01F C 0.7709(11) 0.59224(19) 0.5867(11) 0.0235(16) Uani 0.463(4) 1 d D . P A 2 C01P C 0.9202(10) 0.5514(2) 0.5147(10) 0.0410(19) Uani 0.463(4) 1 d D . P A 2 H01P H 0.969125 0.537327 0.489161 0.049 Uiso 0.463(4) 1 calc R U P A 2 C01S C 0.8450(14) 0.5685(3) 0.6766(10) 0.055(3) Uani 0.463(4) 1 d D . P A 2 H01S H 0.843199 0.566033 0.760424 0.066 Uiso 0.463(4) 1 calc R U P A 2 C01U C 0.7695(10) 0.59573(19) 0.4611(9) 0.0394(19) Uani 0.463(4) 1 d D . P A 2 H01U H 0.717302 0.611683 0.400056 0.047 Uiso 0.463(4) 1 calc R U P A 2 C01Y C 0.9223(19) 0.5483(4) 0.6415(14) 0.079(6) Uani 0.463(4) 1 d D . P A 2 H01Y H 0.975754 0.532506 0.703237 0.095 Uiso 0.463(4) 1 calc R U P A 2 C2 C 0.6808(4) 0.70938(9) 0.7798(4) 0.0438(9) Uani 1 1 d . . . . . H2 H 0.740119 0.699975 0.864930 0.053 Uiso 1 1 calc R U . . . C3 C 0.6666(6) 0.74167(10) 0.7694(5) 0.0600(13) Uani 1 1 d . . . . . H3 H 0.714359 0.754120 0.848419 0.072 Uiso 1 1 calc R U . . . C4 C 0.5811(5) 0.75552(10) 0.6409(5) 0.0528(11) Uani 1 1 d . . . . . H4 H 0.574299 0.777279 0.633471 0.063 Uiso 1 1 calc R U . . . C5 C 0.5068(4) 0.73729(10) 0.5250(4) 0.0433(9) Uani 1 1 d . . . . . H5 H 0.448151 0.746651 0.439461 0.052 Uiso 1 1 calc R U . . . C6 C 0.5192(4) 0.70472(9) 0.5352(4) 0.0328(7) Uani 1 1 d . . . . . H6 H 0.469282 0.692163 0.456952 0.039 Uiso 1 1 calc R U . . . C7 C 0.5125(3) 0.63638(8) 0.6396(3) 0.0255(6) Uani 1 1 d . . . . . C8 C 0.3822(3) 0.64475(8) 0.6404(3) 0.0259(6) Uani 1 1 d . . . . . C9 C 0.2542(3) 0.63197(8) 0.5414(4) 0.0298(7) Uani 1 1 d . . . . . H9 H 0.250955 0.618945 0.471530 0.036 Uiso 1 1 calc R U . . . C10 C 0.1326(4) 0.63860(9) 0.5470(4) 0.0343(7) Uani 1 1 d . . . . . H10 H 0.048018 0.629956 0.480802 0.041 Uiso 1 1 calc R U . . . C11 C 0.1352(4) 0.65793(10) 0.6500(4) 0.0373(8) Uani 1 1 d . . . . . H11 H 0.053278 0.661911 0.654313 0.045 Uiso 1 1 calc R U . . . C12 C 0.2604(4) 0.67130(10) 0.7464(4) 0.0394(8) Uani 1 1 d . . . . . H12 H 0.262526 0.684762 0.814490 0.047 Uiso 1 1 calc R U . . . C13 C 0.3828(4) 0.66467(9) 0.7418(4) 0.0321(7) Uani 1 1 d . . . . . H13 H 0.466690 0.673665 0.807514 0.038 Uiso 1 1 calc R U . . . C14 C 0.5571(3) 0.60844(8) 0.6170(4) 0.0287(7) Uani 1 1 d . . . . . C15 C 0.4893(3) 0.57782(8) 0.5939(4) 0.0334(7) Uani 1 1 d . . . . . C16 C 0.4427(4) 0.56453(9) 0.6724(5) 0.0427(8) Uani 1 1 d . . . . . C17 C 0.3656(5) 0.53380(11) 0.6482(7) 0.0700(11) Uani 1 1 d . . . . . C18 C 0.4573(8) 0.50557(15) 0.7089(15) 0.1385(17) Uani 1 1 d . U . . . C19 C 0.7317(3) 0.64334(8) 0.6651(3) 0.0275(6) Uani 1 1 d . . . . . C20 C 0.7790(9) 0.5868(2) 0.6306(9) 0.0267(16) Uani 0.537(4) 1 d D . P A 1 C21 C 0.7907(7) 0.55875(16) 0.6965(7) 0.0290(13) Uani 0.537(4) 1 d D . P A 1 H21 H 0.743008 0.555507 0.746926 0.035 Uiso 0.537(4) 1 calc R U P A 1 C22 C 0.8743(7) 0.53515(18) 0.6876(9) 0.0412(16) Uani 0.537(4) 1 d D . P A 1 H22 H 0.881605 0.515821 0.730253 0.049 Uiso 0.537(4) 1 calc R U P A 1 C23 C 0.9467(9) 0.5408(2) 0.6143(10) 0.0436(17) Uani 0.537(4) 1 d D . P A 1 H23 H 1.002594 0.525110 0.607683 0.052 Uiso 0.537(4) 1 calc R U P A 1 C24 C 0.9368(8) 0.5692(2) 0.5517(10) 0.0450(18) Uani 0.537(4) 1 d D . P A 1 H24 H 0.988005 0.572850 0.505091 0.054 Uiso 0.537(4) 1 calc R U P A 1 C25 C 0.8510(7) 0.59261(17) 0.5573(8) 0.0347(15) Uani 0.537(4) 1 d D . P A 1 H25 H 0.841939 0.611766 0.512857 0.042 Uiso 0.537(4) 1 calc R U P A 1 C51 C 0.8459(11) 0.5754(2) 0.4267(10) 0.047(2) Uani 0.463(4) 1 d D . P A 2 H51 H 0.847368 0.577984 0.342726 0.056 Uiso 0.463(4) 1 calc R U P A 2 F10 F 0.8113(4) 0.54536(9) -0.0140(4) 0.0931(11) Uani 1 1 d . . . . . F12 F 1.0619(8) 0.53888(16) 0.0103(7) 0.0823(19) Uani 0.537(4) 1 d . . P A 1 F8 F 0.8103(3) 0.60581(7) -0.0564(3) 0.0579(7) Uani 1 1 d . . . . . F13 F 1.1570(8) 0.52468(19) 0.2242(7) 0.096(2) Uani 0.537(4) 1 d . . P A 1 F14 F 0.9908(9) 0.49728(15) 0.0668(8) 0.096(2) Uani 0.537(4) 1 d . . P A 1 F11 F 0.9218(7) 0.53178(10) 0.2277(5) 0.1257(16) Uani 1 1 d . . . . . F16 F 0.7158(15) 0.5155(3) 0.1021(8) 0.156(5) Uani 0.463(4) 1 d . . P A 2 F9 F 1.0548(4) 0.58369(7) 0.2859(3) 0.0743(10) Uani 1 1 d . . . . . F15 F 0.6677(15) 0.5613(4) 0.0866(19) 0.174(5) Uani 0.463(4) 1 d . . P A 2 F17 F 0.799(2) 0.5492(5) 0.2670(14) 0.254(9) Uani 0.463(4) 1 d . . P A 2 O2 O 1.2669(2) 0.68660(6) 0.2272(3) 0.0355(6) Uani 1 1 d . . . . . N4 N 1.1110(3) 0.64450(7) 0.1386(3) 0.0310(6) Uani 1 1 d . . . . . N3 N 1.0504(3) 0.68435(7) 0.2252(3) 0.0275(6) Uani 1 1 d . . . . . C26 C 1.0525(3) 0.71593(8) 0.2753(4) 0.0278(6) Uani 1 1 d . . . . . C27 C 0.9625(4) 0.73798(10) 0.1841(4) 0.0424(9) Uani 1 1 d . . . . . H27 H 0.900941 0.732666 0.091858 0.051 Uiso 1 1 calc R U . . . C28 C 0.9653(5) 0.76825(10) 0.2321(5) 0.0529(10) Uani 1 1 d . . . . . H28 H 0.904621 0.783366 0.171964 0.063 Uiso 1 1 calc R U . . . C29 C 1.0571(5) 0.77602(10) 0.3679(5) 0.0484(9) Uani 1 1 d . . . . . H29 H 1.058570 0.796419 0.399045 0.058 Uiso 1 1 calc R U . . . C30 C 1.1471(5) 0.75383(10) 0.4586(5) 0.0457(9) Uani 1 1 d . . . . . H30 H 1.208691 0.759158 0.550774 0.055 Uiso 1 1 calc R U . . . C31 C 1.1452(4) 0.72335(9) 0.4112(4) 0.0365(8) Uani 1 1 d . . . . . H31 H 1.206023 0.708210 0.471070 0.044 Uiso 1 1 calc R U . . . C32 C 0.8167(3) 0.66525(8) 0.1988(3) 0.0275(6) Uani 1 1 d . . . . . C33 C 0.6877(4) 0.65319(9) 0.0983(4) 0.0334(7) Uani 1 1 d . . . . . H33 H 0.678690 0.645366 0.014800 0.040 Uiso 1 1 calc R U . . . C34 C 0.5738(4) 0.65278(9) 0.1215(4) 0.0365(8) Uani 1 1 d . . . . . H34 H 0.489051 0.644401 0.054470 0.044 Uiso 1 1 calc R U . . . C35 C 0.5853(4) 0.66476(9) 0.2440(4) 0.0370(7) Uani 1 1 d . . . . . H35 H 0.508180 0.664556 0.259307 0.044 Uiso 1 1 calc R U . . . C36 C 0.7118(4) 0.67710(8) 0.3442(4) 0.0335(7) Uani 1 1 d . . . . . H36 H 0.719581 0.685106 0.426945 0.040 Uiso 1 1 calc R U . . . C37 C 0.8264(3) 0.67756(8) 0.3217(3) 0.0278(7) Uani 1 1 d . . . . . H37 H 0.910676 0.686134 0.388843 0.033 Uiso 1 1 calc R U . . . C38 C 0.9401(3) 0.66284(8) 0.1777(3) 0.0276(6) Uani 1 1 d . . . . . C39 C 0.9780(3) 0.63819(9) 0.1240(4) 0.0310(7) Uani 1 1 d . . . . . C40 C 0.9122(4) 0.60780(10) 0.0755(4) 0.0370(7) Uani 1 1 d . . . . . C41 C 0.9521(5) 0.58186(11) 0.1537(4) 0.0507(10) Uani 1 1 d . . . . . C42 C 0.9038(8) 0.54795(15) 0.1132(7) 0.0835(13) Uani 1 1 d D . . . . C43 C 0.7742(17) 0.5428(5) 0.1406(18) 0.117(3) Uani 0.463(4) 1 d D . P A 2 C44 C 1.1573(3) 0.67333(8) 0.2024(3) 0.0276(6) Uani 1 1 d . . . . . C45 C 1.1878(4) 0.62394(8) 0.0960(4) 0.0296(7) Uani 1 1 d . . . . . C46 C 1.3081(4) 0.60945(9) 0.1963(4) 0.0362(8) Uani 1 1 d . . . . . H46 H 1.341710 0.613784 0.290517 0.043 Uiso 1 1 calc R U . . . C47 C 1.3779(5) 0.58833(10) 0.1543(5) 0.0444(9) Uani 1 1 d . . . . . H47 H 1.459081 0.578476 0.220528 0.053 Uiso 1 1 calc R U . . . C48 C 1.3269(5) 0.58198(10) 0.0143(5) 0.0459(9) Uani 1 1 d . . . . . H48 H 1.372580 0.567441 -0.013301 0.055 Uiso 1 1 calc R U . . . C49 C 1.2098(5) 0.59689(11) -0.0840(4) 0.0472(9) Uani 1 1 d . . . . . H49 H 1.177837 0.592869 -0.178260 0.057 Uiso 1 1 calc R U . . . C50 C 1.1378(4) 0.61809(10) -0.0443(4) 0.0401(8) Uani 1 1 d . . . . . H50 H 1.057428 0.628101 -0.111180 0.048 Uiso 1 1 calc R U . . . C52 C 1.0160(13) 0.5288(2) 0.1205(10) 0.0722(17) Uani 0.537(4) 1 d . . P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F4 0.075(2) 0.061(2) 0.197(4) 0.026(2) 0.082(3) -0.0105(17) F3 0.0623(19) 0.0529(18) 0.137(3) -0.0178(19) 0.0121(18) -0.0304(15) F1 0.0628(15) 0.0329(12) 0.0476(13) -0.0159(10) 0.0143(12) -0.0063(11) F6 0.067(2) 0.0347(15) 0.292(5) 0.029(2) 0.034(3) -0.0115(14) F7 0.069(2) 0.0437(17) 0.295(5) -0.002(3) 0.060(3) 0.0078(16) F5 0.084(3) 0.059(2) 0.271(5) 0.052(3) 0.025(3) -0.0087(19) F2 0.101(2) 0.0394(14) 0.0901(19) -0.0058(13) 0.0714(18) -0.0130(14) O1 0.0252(11) 0.0339(13) 0.0525(16) -0.0059(11) 0.0186(11) -0.0037(9) N1 0.0199(12) 0.0225(12) 0.0343(15) -0.0029(10) 0.0104(11) -0.0010(9) N2 0.0221(12) 0.0260(12) 0.0392(16) -0.0052(11) 0.0142(11) 0.0003(9) C1 0.0226(14) 0.0222(13) 0.0342(14) -0.0015(11) 0.0123(11) -0.0012(11) C01F 0.023(4) 0.018(3) 0.030(4) -0.001(2) 0.013(3) -0.002(2) C01P 0.049(5) 0.036(4) 0.040(4) -0.005(3) 0.023(3) 0.005(3) C01S 0.086(7) 0.050(5) 0.038(4) 0.016(4) 0.037(5) 0.039(5) C01U 0.057(5) 0.032(4) 0.040(4) 0.007(3) 0.031(4) 0.010(3) C01Y 0.117(11) 0.082(9) 0.054(5) 0.025(5) 0.055(7) 0.066(9) C2 0.047(2) 0.0299(16) 0.0354(18) -0.0033(13) 0.0042(15) -0.0037(15) C3 0.073(3) 0.0292(17) 0.047(2) -0.0102(15) 0.004(2) -0.0063(17) C4 0.060(3) 0.0265(19) 0.056(2) 0.0005(14) 0.0144(17) 0.0017(17) C5 0.039(2) 0.0325(16) 0.047(2) 0.0057(14) 0.0119(16) 0.0058(14) C6 0.0293(16) 0.0313(15) 0.0327(16) -0.0015(12) 0.0108(13) 0.0002(13) C7 0.0212(13) 0.0250(13) 0.0268(15) -0.0020(11) 0.0087(12) -0.0022(10) C8 0.0218(13) 0.0253(15) 0.0271(14) 0.0024(11) 0.0088(11) 0.0008(11) C9 0.0228(13) 0.0298(17) 0.0303(16) -0.0012(13) 0.0075(12) -0.0011(12) C10 0.0225(14) 0.0367(18) 0.0382(17) 0.0073(13) 0.0102(14) 0.0007(13) C11 0.0277(15) 0.047(2) 0.0409(17) 0.0102(14) 0.0193(13) 0.0075(14) C12 0.0361(16) 0.047(2) 0.0380(18) -0.0006(16) 0.0200(14) 0.0065(14) C13 0.0266(15) 0.0357(17) 0.0297(16) -0.0031(13) 0.0102(13) 0.0005(13) C14 0.0209(13) 0.0264(13) 0.0358(18) -0.0064(12) 0.0111(13) -0.0027(11) C15 0.0237(15) 0.0228(14) 0.0439(16) -0.0071(12) 0.0085(13) -0.0012(12) C16 0.0351(19) 0.0241(16) 0.069(2) -0.0020(14) 0.0250(17) -0.0034(14) C17 0.0302(19) 0.0350(19) 0.128(3) 0.001(2) 0.0249(18) -0.0130(14) C18 0.052(2) 0.0378(18) 0.280(4) 0.026(2) 0.042(2) -0.0057(15) C19 0.0204(12) 0.0279(14) 0.0312(16) -0.0033(12) 0.0099(12) -0.0006(10) C20 0.022(3) 0.028(3) 0.029(4) -0.003(2) 0.011(3) 0.002(2) C21 0.027(3) 0.030(3) 0.027(3) -0.002(2) 0.011(2) 0.002(2) C22 0.032(3) 0.039(3) 0.049(4) -0.005(3) 0.016(3) 0.007(2) C23 0.034(4) 0.043(3) 0.052(5) -0.014(3) 0.019(3) -0.003(3) C24 0.040(4) 0.042(3) 0.062(5) -0.014(3) 0.032(4) -0.003(3) C25 0.035(3) 0.035(3) 0.040(4) -0.009(3) 0.023(3) -0.005(2) C51 0.064(5) 0.040(4) 0.054(5) 0.007(3) 0.043(4) 0.011(3) F10 0.094(2) 0.064(2) 0.099(2) -0.0455(19) 0.0280(18) -0.0253(18) F12 0.113(5) 0.068(4) 0.072(4) -0.001(3) 0.050(4) 0.010(3) F8 0.0540(14) 0.0594(16) 0.0416(12) -0.0207(11) 0.0079(10) -0.0108(12) F13 0.102(4) 0.098(5) 0.070(3) -0.004(3) 0.026(3) 0.037(4) F14 0.144(6) 0.044(3) 0.113(5) -0.011(3) 0.071(5) -0.002(3) F11 0.191(5) 0.056(2) 0.117(3) 0.009(2) 0.064(3) -0.016(3) F16 0.245(12) 0.147(7) 0.054(4) -0.024(5) 0.053(6) -0.144(8) F9 0.117(2) 0.0512(16) 0.0346(12) -0.0023(11) 0.0206(13) -0.0289(16) F15 0.128(6) 0.169(10) 0.254(13) -0.044(8) 0.115(8) -0.087(5) F17 0.329(15) 0.38(2) 0.131(6) -0.154(9) 0.172(8) -0.300(15) O2 0.0254(11) 0.0390(14) 0.0407(14) -0.0076(11) 0.0146(10) -0.0036(9) N4 0.0272(13) 0.0352(14) 0.0319(14) -0.0077(11) 0.0152(11) -0.0029(10) N3 0.0225(12) 0.0284(12) 0.0291(14) -0.0008(10) 0.0103(11) 0.0009(9) C26 0.0263(14) 0.0279(14) 0.0309(14) 0.0000(11) 0.0152(11) -0.0005(11) C27 0.047(2) 0.0350(17) 0.0392(19) 0.0069(13) 0.0163(16) 0.0086(15) C28 0.065(3) 0.0333(18) 0.063(2) 0.0056(16) 0.0334(18) 0.0115(18) C29 0.058(2) 0.0322(19) 0.069(2) -0.0080(15) 0.0421(17) -0.0039(15) C30 0.046(2) 0.0431(18) 0.051(2) -0.0153(14) 0.0257(17) -0.0096(15) C31 0.0340(17) 0.0383(17) 0.0338(15) -0.0045(13) 0.0136(13) -0.0010(14) C32 0.0239(13) 0.0264(16) 0.0284(14) 0.0052(11) 0.0097(11) 0.0024(11) C33 0.0292(14) 0.0358(18) 0.0307(16) -0.0020(14) 0.0107(12) -0.0014(13) C34 0.0266(15) 0.0357(19) 0.0415(17) 0.0023(14) 0.0118(14) -0.0022(14) C35 0.0329(16) 0.0347(18) 0.0470(17) 0.0057(14) 0.0223(14) 0.0011(14) C36 0.0356(15) 0.0284(17) 0.0406(18) 0.0038(14) 0.0217(13) 0.0039(13) C37 0.0253(14) 0.0263(16) 0.0283(14) 0.0044(12) 0.0099(12) 0.0028(12) C38 0.0229(13) 0.0323(15) 0.0232(15) 0.0008(12) 0.0075(12) -0.0002(11) C39 0.0256(14) 0.0384(15) 0.0279(16) -0.0047(13) 0.0121(13) -0.0030(12) C40 0.0356(17) 0.0471(17) 0.0325(14) -0.0134(12) 0.0197(12) -0.0125(13) C41 0.073(2) 0.0468(18) 0.0352(15) -0.0126(13) 0.0282(15) -0.0243(17) C42 0.110(3) 0.055(2) 0.081(2) -0.0215(19) 0.043(2) -0.042(2) C43 0.119(5) 0.152(8) 0.081(5) -0.077(5) 0.049(5) -0.102(5) C44 0.0223(12) 0.0329(15) 0.0239(15) -0.0021(11) 0.0081(11) 0.0009(10) C45 0.0303(15) 0.0308(16) 0.0312(14) -0.0029(12) 0.0176(12) -0.0023(12) C46 0.0362(17) 0.0415(19) 0.0336(17) 0.0023(14) 0.0189(14) 0.0043(14) C47 0.046(2) 0.044(2) 0.0509(18) 0.0042(16) 0.0298(17) 0.0098(17) C48 0.057(2) 0.040(2) 0.0542(18) -0.0019(16) 0.0383(17) 0.0054(17) C49 0.060(2) 0.051(2) 0.0399(19) -0.0064(16) 0.0316(17) 0.0020(17) C50 0.043(2) 0.048(2) 0.0312(15) -0.0023(15) 0.0195(15) 0.0019(16) C52 0.099(4) 0.043(3) 0.047(4) 0.001(3) 0.014(3) -0.025(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C7 N1 C1 125.5(3) . . ? C19 N1 C1 120.9(3) . . ? C19 N1 C7 110.4(3) . . ? C14 N2 C01F 130.0(5) . . ? C14 N2 C20 123.7(5) . . ? C19 N2 C01F 119.5(5) . . ? C19 N2 C14 109.1(3) . . ? C19 N2 C20 126.5(5) . . ? C2 C1 N1 119.9(3) . . ? C2 C1 C6 121.7(3) . . ? C6 C1 N1 118.4(3) . . ? C01S C01F N2 116.1(8) . . ? C01S C01F C01U 121.1(7) . . ? C01U C01F N2 122.8(7) . . ? C01Y C01P H01P 120.1 . . ? C51 C01P H01P 120.1 . . ? C51 C01P C01Y 119.9(9) . . ? C01F C01S H01S 120.4 . . ? C01F C01S C01Y 119.3(9) . . ? C01Y C01S H01S 120.4 . . ? C01F C01U H01U 120.4 . . ? C51 C01U C01F 119.3(8) . . ? C51 C01U H01U 120.4 . . ? C01P C01Y C01S 119.9(10) . . ? C01P C01Y H01Y 120.1 . . ? C01S C01Y H01Y 120.1 . . ? C1 C2 H2 120.5 . . ? C1 C2 C3 119.1(4) . . ? C3 C2 H2 120.5 . . ? C2 C3 H3 120.0 . . ? C2 C3 C4 120.0(4) . . ? C4 C3 H3 120.0 . . ? C3 C4 H4 119.8 . . ? C5 C4 C3 120.3(4) . . ? C5 C4 H4 119.8 . . ? C4 C5 H5 120.0 . . ? C4 C5 C6 119.9(4) . . ? C6 C5 H5 120.0 . . ? C1 C6 C5 119.0(3) . . ? C1 C6 H6 120.5 . . ? C5 C6 H6 120.5 . . ? N1 C7 C8 122.9(3) . . ? C14 C7 N1 106.7(3) . . ? C14 C7 C8 130.4(3) . . ? C9 C8 C7 120.5(3) . . ? C13 C8 C7 121.2(3) . . ? C13 C8 C9 118.3(3) . . ? C8 C9 H9 119.8 . . ? C10 C9 C8 120.3(3) . . ? C10 C9 H9 119.8 . . ? C9 C10 H10 119.6 . . ? C9 C10 C11 120.7(3) . . ? C11 C10 H10 119.6 . . ? C10 C11 H11 120.2 . . ? C12 C11 C10 119.5(3) . . ? C12 C11 H11 120.2 . . ? C11 C12 H12 120.0 . . ? C11 C12 C13 120.1(4) . . ? C13 C12 H12 120.0 . . ? C8 C13 H13 119.5 . . ? C12 C13 C8 121.0(3) . . ? C12 C13 H13 119.5 . . ? N2 C14 C15 122.8(3) . . ? C7 C14 N2 108.4(3) . . ? C7 C14 C15 128.6(3) . . ? F1 C15 C14 114.9(3) . . ? C16 C15 F1 118.8(3) . . ? C16 C15 C14 126.3(4) . . ? F2 C16 C17 112.1(4) . . ? C15 C16 F2 119.9(3) . . ? C15 C16 C17 128.0(5) . . ? F4 C17 C16 109.6(5) . . ? F4 C17 C18 107.6(7) . . ? F3 C17 F4 107.8(4) . . ? F3 C17 C16 110.5(5) . . ? F3 C17 C18 106.1(7) . . ? C18 C17 C16 115.0(4) . . ? F6 C18 C17 113.4(6) . . ? F7 C18 F6 108.1(9) . . ? F7 C18 C17 111.6(8) . . ? F5 C18 F6 109.5(9) . . ? F5 C18 F7 105.2(6) . . ? F5 C18 C17 108.8(8) . . ? O1 C19 N1 127.0(3) . . ? O1 C19 N2 127.6(3) . . ? N2 C19 N1 105.4(3) . . ? C21 C20 N2 123.6(7) . . ? C21 C20 C25 121.7(7) . . ? C25 C20 N2 114.8(7) . . ? C20 C21 H21 120.2 . . ? C20 C21 C22 119.5(8) . . ? C22 C21 H21 120.2 . . ? C21 C22 H22 120.5 . . ? C23 C22 C21 119.1(8) . . ? C23 C22 H22 120.5 . . ? C22 C23 H23 119.6 . . ? C24 C23 C22 120.8(8) . . ? C24 C23 H23 119.6 . . ? C23 C24 H24 119.8 . . ? C23 C24 C25 120.4(7) . . ? C25 C24 H24 119.8 . . ? C20 C25 C24 118.4(7) . . ? C20 C25 H25 120.8 . . ? C24 C25 H25 120.8 . . ? C01P C51 C01U 120.6(8) . . ? C01P C51 H51 119.7 . . ? C01U C51 H51 119.7 . . ? C52 F12 F14 88.7(6) . 3_765 ? F14 F14 F12 80.7(5) 3_765 3_765 ? C52 F14 F12 172.5(9) . 3_765 ? C52 F14 F14 98.9(7) . 3_765 ? C39 N4 C45 125.2(3) . . ? C44 N4 C39 109.5(3) . . ? C44 N4 C45 125.4(3) . . ? C38 N3 C26 127.2(3) . . ? C44 N3 C26 121.4(3) . . ? C44 N3 C38 110.9(3) . . ? C27 C26 N3 118.9(3) . . ? C31 C26 N3 119.5(3) . . ? C31 C26 C27 121.6(4) . . ? C26 C27 H27 120.6 . . ? C26 C27 C28 118.8(4) . . ? C28 C27 H27 120.6 . . ? C27 C28 H28 119.8 . . ? C29 C28 C27 120.4(4) . . ? C29 C28 H28 119.8 . . ? C28 C29 H29 119.7 . . ? C28 C29 C30 120.5(4) . . ? C30 C29 H29 119.7 . . ? C29 C30 H30 120.2 . . ? C29 C30 C31 119.5(4) . . ? C31 C30 H30 120.2 . . ? C26 C31 C30 119.2(4) . . ? C26 C31 H31 120.4 . . ? C30 C31 H31 120.4 . . ? C33 C32 C38 119.9(3) . . ? C37 C32 C33 118.5(3) . . ? C37 C32 C38 121.5(3) . . ? C32 C33 H33 119.6 . . ? C34 C33 C32 120.7(3) . . ? C34 C33 H33 119.6 . . ? C33 C34 H34 119.9 . . ? C35 C34 C33 120.2(3) . . ? C35 C34 H34 119.9 . . ? C34 C35 H35 120.0 . . ? C34 C35 C36 119.9(3) . . ? C36 C35 H35 120.0 . . ? C35 C36 H36 119.9 . . ? C37 C36 C35 120.2(3) . . ? C37 C36 H36 119.9 . . ? C32 C37 H37 119.8 . . ? C36 C37 C32 120.5(3) . . ? C36 C37 H37 119.8 . . ? N3 C38 C32 125.6(3) . . ? C39 C38 N3 106.4(3) . . ? C39 C38 C32 127.6(3) . . ? N4 C39 C40 120.9(3) . . ? C38 C39 N4 108.2(3) . . ? C38 C39 C40 130.4(3) . . ? F8 C40 C39 117.3(4) . . ? F8 C40 C41 119.0(4) . . ? C41 C40 C39 123.6(4) . . ? F9 C41 C42 111.1(4) . . ? C40 C41 F9 119.2(4) . . ? C40 C41 C42 129.5(4) . . ? F10 C42 F11 130.7(5) . . ? F10 C42 C41 112.4(6) . . ? F10 C42 C43 83.5(7) . . ? F10 C42 C52 102.5(6) . . ? F11 C42 C41 109.6(5) . . ? F11 C42 C43 60.4(10) . . ? F11 C42 C52 85.3(7) . . ? C41 C42 C43 106.7(8) . . ? C52 C42 C41 110.8(6) . . ? F16 C43 F17 110.7(15) . . ? F16 C43 C42 113.8(14) . . ? F15 C43 F16 102.0(13) . . ? F15 C43 F17 92.5(18) . . ? F15 C43 C42 120.9(18) . . ? F17 C43 C42 114.6(11) . . ? O2 C44 N4 127.0(3) . . ? O2 C44 N3 128.0(3) . . ? N4 C44 N3 105.0(3) . . ? C46 C45 N4 119.5(3) . . ? C50 C45 N4 119.3(3) . . ? C50 C45 C46 121.1(3) . . ? C45 C46 H46 120.4 . . ? C45 C46 C47 119.1(4) . . ? C47 C46 H46 120.4 . . ? C46 C47 H47 120.0 . . ? C48 C47 C46 120.0(4) . . ? C48 C47 H47 120.0 . . ? C47 C48 H48 119.8 . . ? C49 C48 C47 120.5(4) . . ? C49 C48 H48 119.8 . . ? C48 C49 H49 119.7 . . ? C48 C49 C50 120.5(4) . . ? C50 C49 H49 119.7 . . ? C45 C50 C49 118.8(4) . . ? C45 C50 H50 120.6 . . ? C49 C50 H50 120.6 . . ? F13 C52 F12 91.5(9) . . ? F13 C52 F14 97.5(9) . . ? F13 C52 C42 133.0(9) . . ? F14 C52 F12 90.6(8) . . ? F14 C52 C42 121.0(9) . . ? C42 C52 F12 112.2(7) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag F4 C17 1.347(7) . ? F3 C17 1.326(8) . ? F1 C15 1.339(4) . ? F6 C18 1.303(7) . ? F7 C18 1.325(13) . ? F5 C18 1.325(14) . ? F2 C16 1.349(5) . ? O1 C19 1.226(4) . ? N1 C1 1.437(4) . ? N1 C7 1.395(4) . ? N1 C19 1.383(4) . ? N2 C01F 1.458(8) . ? N2 C14 1.404(4) . ? N2 C19 1.377(5) . ? N2 C20 1.454(7) . ? C1 C2 1.372(5) . ? C1 C6 1.374(5) . ? C01F C01S 1.369(12) . ? C01F C01U 1.371(12) . ? C01P H01P 0.9300 . ? C01P C01Y 1.380(14) . ? C01P C51 1.369(12) . ? C01S H01S 0.9300 . ? C01S C01Y 1.381(13) . ? C01U H01U 0.9300 . ? C01U C51 1.371(11) . ? C01Y H01Y 0.9300 . ? C2 H2 0.9300 . ? C2 C3 1.382(6) . ? C3 H3 0.9300 . ? C3 C4 1.388(6) . ? C4 H4 0.9300 . ? C4 C5 1.369(6) . ? C5 H5 0.9300 . ? C5 C6 1.393(6) . ? C6 H6 0.9300 . ? C7 C8 1.465(4) . ? C7 C14 1.351(5) . ? C8 C9 1.398(5) . ? C8 C13 1.392(5) . ? C9 H9 0.9300 . ? C9 C10 1.382(5) . ? C10 H10 0.9300 . ? C10 C11 1.382(6) . ? C11 H11 0.9300 . ? C11 C12 1.382(6) . ? C12 H12 0.9300 . ? C12 C13 1.384(5) . ? C13 H13 0.9300 . ? C14 C15 1.459(5) . ? C15 C16 1.315(6) . ? C16 C17 1.507(6) . ? C17 C18 1.498(9) . ? C20 C21 1.368(11) . ? C20 C25 1.383(10) . ? C21 H21 0.9300 . ? C21 C22 1.389(9) . ? C22 H22 0.9300 . ? C22 C23 1.386(12) . ? C23 H23 0.9300 . ? C23 C24 1.368(12) . ? C24 H24 0.9300 . ? C24 C25 1.386(10) . ? C25 H25 0.9300 . ? C51 H51 0.9300 . ? F10 C42 1.269(8) . ? F12 F14 1.716(9) 3_765 ? F12 C52 1.566(13) . ? F8 C40 1.332(5) . ? F13 C52 1.412(13) . ? F14 F14 1.582(15) 3_765 ? F14 C52 1.439(11) . ? F11 C42 1.356(8) . ? F16 C43 1.296(19) . ? F9 C41 1.337(5) . ? F15 C43 1.29(3) . ? F17 C43 1.300(16) . ? O2 C44 1.225(4) . ? N4 C39 1.402(4) . ? N4 C44 1.381(5) . ? N4 C45 1.433(5) . ? N3 C26 1.448(4) . ? N3 C38 1.396(4) . ? N3 C44 1.382(4) . ? C26 C27 1.376(5) . ? C26 C31 1.371(5) . ? C27 H27 0.9300 . ? C27 C28 1.386(6) . ? C28 H28 0.9300 . ? C28 C29 1.372(7) . ? C29 H29 0.9300 . ? C29 C30 1.378(7) . ? C30 H30 0.9300 . ? C30 C31 1.394(6) . ? C31 H31 0.9300 . ? C32 C33 1.399(5) . ? C32 C37 1.396(5) . ? C32 C38 1.471(5) . ? C33 H33 0.9300 . ? C33 C34 1.378(5) . ? C34 H34 0.9300 . ? C34 C35 1.380(6) . ? C35 H35 0.9300 . ? C35 C36 1.385(6) . ? C36 H36 0.9300 . ? C36 C37 1.382(5) . ? C37 H37 0.9300 . ? C38 C39 1.359(5) . ? C39 C40 1.450(5) . ? C40 C41 1.334(7) . ? C41 C42 1.527(7) . ? C42 C43 1.589(9) . ? C42 C52 1.437(15) . ? C45 C46 1.383(5) . ? C45 C50 1.380(5) . ? C46 H46 0.9300 . ? C46 C47 1.389(6) . ? C47 H47 0.9300 . ? C47 C48 1.378(6) . ? C48 H48 0.9300 . ? C48 C49 1.365(7) . ? C49 H49 0.9300 . ? C49 C50 1.393(6) . ? C50 H50 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag F4 C17 C18 F6 59.2(12) . . . . ? F4 C17 C18 F7 -178.5(7) . . . . ? F4 C17 C18 F5 -62.9(7) . . . . ? F3 C17 C18 F6 -56.0(12) . . . . ? F3 C17 C18 F7 66.3(8) . . . . ? F3 C17 C18 F5 -178.1(6) . . . . ? F1 C15 C16 F2 175.0(3) . . . . ? F1 C15 C16 C17 -3.4(6) . . . . ? F2 C16 C17 F4 32.0(6) . . . . ? F2 C16 C17 F3 150.7(4) . . . . ? F2 C16 C17 C18 -89.3(8) . . . . ? N1 C1 C2 C3 179.2(4) . . . . ? N1 C1 C6 C5 -178.3(3) . . . . ? N1 C7 C8 C9 142.9(3) . . . . ? N1 C7 C8 C13 -39.3(5) . . . . ? N1 C7 C14 N2 -1.5(4) . . . . ? N1 C7 C14 C15 173.6(3) . . . . ? N2 C01F C01S C01Y 179.7(13) . . . . ? N2 C01F C01U C51 -179.2(9) . . . . ? N2 C14 C15 F1 -57.1(5) . . . . ? N2 C14 C15 C16 123.0(4) . . . . ? N2 C20 C21 C22 178.3(7) . . . . ? N2 C20 C25 C24 -179.8(7) . . . . ? C1 N1 C7 C8 -21.6(5) . . . . ? C1 N1 C7 C14 160.9(3) . . . . ? C1 N1 C19 O1 18.0(5) . . . . ? C1 N1 C19 N2 -161.2(3) . . . . ? C1 C2 C3 C4 -2.0(8) . . . . ? C01F N2 C14 C7 -164.4(6) . . . . ? C01F N2 C14 C15 20.2(7) . . . . ? C01F N2 C19 O1 -12.3(7) . . . . ? C01F N2 C19 N1 166.9(5) . . . . ? C01F C01S C01Y C01P -2(3) . . . . ? C01F C01U C51 C01P 1.6(16) . . . . ? C01S C01F C01U C51 -1.3(17) . . . . ? C01U C01F C01S C01Y 2(2) . . . . ? C01Y C01P C51 C01U -2.3(19) . . . . ? C2 C1 C6 C5 0.0(6) . . . . ? C2 C3 C4 C5 2.2(9) . . . . ? C3 C4 C5 C6 -1.3(8) . . . . ? C4 C5 C6 C1 0.2(6) . . . . ? C6 C1 C2 C3 0.9(7) . . . . ? C7 N1 C1 C2 120.3(4) . . . . ? C7 N1 C1 C6 -61.4(5) . . . . ? C7 N1 C19 O1 178.8(3) . . . . ? C7 N1 C19 N2 -0.4(4) . . . . ? C7 C8 C9 C10 176.5(3) . . . . ? C7 C8 C13 C12 -176.8(3) . . . . ? C7 C14 C15 F1 128.5(4) . . . . ? C7 C14 C15 C16 -51.4(6) . . . . ? C8 C7 C14 N2 -178.7(3) . . . . ? C8 C7 C14 C15 -3.6(6) . . . . ? C8 C9 C10 C11 0.1(5) . . . . ? C9 C8 C13 C12 1.1(5) . . . . ? C9 C10 C11 C12 1.4(6) . . . . ? C10 C11 C12 C13 -1.7(6) . . . . ? C11 C12 C13 C8 0.4(6) . . . . ? C13 C8 C9 C10 -1.3(5) . . . . ? C14 N2 C01F C01S -83.8(12) . . . . ? C14 N2 C01F C01U 94.2(10) . . . . ? C14 N2 C19 O1 -179.7(3) . . . . ? C14 N2 C19 N1 -0.5(4) . . . . ? C14 N2 C20 C21 -40.1(10) . . . . ? C14 N2 C20 C25 139.6(6) . . . . ? C14 C7 C8 C9 -40.2(5) . . . . ? C14 C7 C8 C13 137.5(4) . . . . ? C14 C15 C16 F2 -5.1(6) . . . . ? C14 C15 C16 C17 176.5(4) . . . . ? C15 C16 C17 F4 -149.5(5) . . . . ? C15 C16 C17 F3 -30.8(6) . . . . ? C15 C16 C17 C18 89.2(9) . . . . ? C16 C17 C18 F6 -178.4(9) . . . . ? C16 C17 C18 F7 -56.1(11) . . . . ? C16 C17 C18 F5 59.5(10) . . . . ? C19 N1 C1 C2 -81.9(4) . . . . ? C19 N1 C1 C6 96.4(4) . . . . ? C19 N1 C7 C8 178.7(3) . . . . ? C19 N1 C7 C14 1.2(4) . . . . ? C19 N2 C01F C01S 111.8(10) . . . . ? C19 N2 C01F C01U -70.2(11) . . . . ? C19 N2 C14 C7 1.3(4) . . . . ? C19 N2 C14 C15 -174.1(3) . . . . ? C19 N2 C20 C21 129.0(8) . . . . ? C19 N2 C20 C25 -51.3(9) . . . . ? C20 N2 C14 C7 172.1(5) . . . . ? C20 N2 C14 C15 -3.4(6) . . . . ? C20 N2 C19 O1 9.8(7) . . . . ? C20 N2 C19 N1 -171.0(5) . . . . ? C20 C21 C22 C23 1.4(11) . . . . ? C21 C20 C25 C24 -0.1(13) . . . . ? C21 C22 C23 C24 0.2(12) . . . . ? C22 C23 C24 C25 -1.8(14) . . . . ? C23 C24 C25 C20 1.7(13) . . . . ? C25 C20 C21 C22 -1.4(12) . . . . ? C51 C01P C01Y C01S 3(2) . . . . ? F10 C42 C43 F16 64.3(16) . . . . ? F10 C42 C43 F15 -57.7(13) . . . . ? F10 C42 C43 F17 -167(2) . . . . ? F10 C42 C52 F12 54.8(8) . . . . ? F10 C42 C52 F13 169.6(10) . . . . ? F10 C42 C52 F14 -50.3(10) . . . . ? F8 C40 C41 F9 179.6(4) . . . . ? F8 C40 C41 C42 4.0(8) . . . . ? F14 F12 C52 F13 105.0(6) 3_765 . . . ? F14 F12 C52 F14 7.5(8) 3_765 . . . ? F14 F12 C52 C42 -116.6(7) 3_765 . . . ? F14 F14 C52 F12 -8.2(9) 3_765 . . . ? F14 F14 C52 F13 -99.9(9) 3_765 . . . ? F14 F14 C52 C42 108.4(10) 3_765 . . . ? F11 C42 C43 F16 -80.8(18) . . . . ? F11 C42 C43 F15 157.2(15) . . . . ? F11 C42 C43 F17 48.0(19) . . . . ? F11 C42 C52 F12 -174.5(7) . . . . ? F11 C42 C52 F13 -59.7(11) . . . . ? F11 C42 C52 F14 80.4(9) . . . . ? F9 C41 C42 F10 -176.6(5) . . . . ? F9 C41 C42 F11 29.8(7) . . . . ? F9 C41 C42 C43 93.7(10) . . . . ? F9 C41 C42 C52 -62.6(7) . . . . ? N4 C39 C40 F8 -103.3(4) . . . . ? N4 C39 C40 C41 73.8(5) . . . . ? N4 C45 C46 C47 176.8(4) . . . . ? N4 C45 C50 C49 -177.0(4) . . . . ? N3 C26 C27 C28 -179.6(4) . . . . ? N3 C26 C31 C30 179.7(3) . . . . ? N3 C38 C39 N4 0.1(4) . . . . ? N3 C38 C39 C40 171.8(4) . . . . ? C26 N3 C38 C32 -14.9(5) . . . . ? C26 N3 C38 C39 171.9(3) . . . . ? C26 N3 C44 O2 4.7(5) . . . . ? C26 N3 C44 N4 -172.3(3) . . . . ? C26 C27 C28 C29 0.5(7) . . . . ? C27 C26 C31 C30 0.8(6) . . . . ? C27 C28 C29 C30 -0.4(7) . . . . ? C28 C29 C30 C31 0.5(7) . . . . ? C29 C30 C31 C26 -0.7(6) . . . . ? C31 C26 C27 C28 -0.7(6) . . . . ? C32 C33 C34 C35 1.0(6) . . . . ? C32 C38 C39 N4 -173.0(3) . . . . ? C32 C38 C39 C40 -1.2(6) . . . . ? C33 C32 C37 C36 1.5(5) . . . . ? C33 C32 C38 N3 148.5(3) . . . . ? C33 C32 C38 C39 -39.7(5) . . . . ? C33 C34 C35 C36 -0.3(6) . . . . ? C34 C35 C36 C37 0.2(5) . . . . ? C35 C36 C37 C32 -0.9(5) . . . . ? C37 C32 C33 C34 -1.6(5) . . . . ? C37 C32 C38 N3 -35.7(5) . . . . ? C37 C32 C38 C39 136.1(4) . . . . ? C38 N3 C26 C27 -64.6(5) . . . . ? C38 N3 C26 C31 116.4(4) . . . . ? C38 N3 C44 O2 177.5(3) . . . . ? C38 N3 C44 N4 0.5(4) . . . . ? C38 C32 C33 C34 174.4(3) . . . . ? C38 C32 C37 C36 -174.4(3) . . . . ? C38 C39 C40 F8 85.9(5) . . . . ? C38 C39 C40 C41 -97.0(5) . . . . ? C39 N4 C44 O2 -177.5(3) . . . . ? C39 N4 C44 N3 -0.4(4) . . . . ? C39 N4 C45 C46 -110.7(4) . . . . ? C39 N4 C45 C50 67.0(5) . . . . ? C39 C40 C41 F9 2.5(7) . . . . ? C39 C40 C41 C42 -173.0(5) . . . . ? C40 C41 C42 F10 -0.7(9) . . . . ? C40 C41 C42 F11 -154.3(6) . . . . ? C40 C41 C42 C43 -90.4(11) . . . . ? C40 C41 C42 C52 113.3(8) . . . . ? C41 C42 C43 F16 175.7(14) . . . . ? C41 C42 C43 F15 53.8(14) . . . . ? C41 C42 C43 F17 -55(2) . . . . ? C41 C42 C52 F12 -65.3(8) . . . . ? C41 C42 C52 F13 49.5(13) . . . . ? C41 C42 C52 F14 -170.4(7) . . . . ? C44 N4 C39 C38 0.2(4) . . . . ? C44 N4 C39 C40 -172.5(3) . . . . ? C44 N4 C45 C46 68.1(5) . . . . ? C44 N4 C45 C50 -114.2(4) . . . . ? C44 N3 C26 C27 106.9(4) . . . . ? C44 N3 C26 C31 -72.1(4) . . . . ? C44 N3 C38 C32 172.9(3) . . . . ? C44 N3 C38 C39 -0.3(4) . . . . ? C45 N4 C39 C38 179.2(3) . . . . ? C45 N4 C39 C40 6.5(5) . . . . ? C45 N4 C44 O2 3.6(6) . . . . ? C45 N4 C44 N3 -179.4(3) . . . . ? C45 C46 C47 C48 -0.2(6) . . . . ? C46 C45 C50 C49 0.7(6) . . . . ? C46 C47 C48 C49 1.6(7) . . . . ? C47 C48 C49 C50 -1.8(7) . . . . ? C48 C49 C50 C45 0.6(7) . . . . ? C50 C45 C46 C47 -0.9(6) . . . . ?