#------------------------------------------------------------------------------ #$Date: 2024-06-25 01:19:48 +0300 (Tue, 25 Jun 2024) $ #$Revision: 292548 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/19/1571977.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571977 loop_ _publ_author_name 'Soldatova, Natalia S.' 'Radzhabov, Amirbek' 'Ivanov, Daniil' 'Burguera Pi\~na, Sergi' 'Frontera, Antonio' 'Abramov, Pavel A.' 'Postnikov, Pavel S.' 'Kukushkin, Vadim Yu.' _publ_section_title ; Key-to-Lock Halogen Bond-Based Tetragonal Pyramidal Association of Iodonium Cations with the Lacune Rims of Beta-Octamolybdate ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC01695E _journal_year 2024 _chemical_formula_moiety '4(C12 H10 I), 0.14(I), Mo8 O26, 2(C3 H7 N O)' _chemical_formula_sum 'C54 H54 I4 Mo8 N2 O28' _chemical_formula_weight 2454.11 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_date 2024-02-19 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _audit_update_record ; 2024-02-21 deposited with the CCDC. 2024-06-17 downloaded from the CCDC. ; _cell_angle_alpha 69.875(2) _cell_angle_beta 64.408(2) _cell_angle_gamma 68.367(2) _cell_formula_units_Z 1 _cell_length_a 12.7533(3) _cell_length_b 12.7583(3) _cell_length_c 13.1803(3) _cell_measurement_reflns_used 8572 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 28.8010 _cell_measurement_theta_min 2.7600 _cell_volume 1753.70(8) _computing_cell_refinement 'CrysAlisPro 1.171.41.123a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.41.123a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.41.123a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 150(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.6 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.832 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'New Xcalibur, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0222 _diffrn_reflns_av_unetI/netI 0.0351 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.832 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 16766 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.832 _diffrn_reflns_theta_full 25.500 _diffrn_reflns_theta_max 29.049 _diffrn_reflns_theta_min 1.833 _diffrn_source 'sealed X-ray tube' _exptl_absorpt_coefficient_mu 3.223 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.91751 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.123a (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 2.324 _exptl_crystal_description block _exptl_crystal_F_000 1164 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 2.451 _refine_diff_density_min -0.943 _refine_diff_density_rms 0.130 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 439 _refine_ls_number_reflns 7792 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.040 _refine_ls_R_factor_all 0.0417 _refine_ls_R_factor_gt 0.0304 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0319P)^2^+4.4419P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0740 _refine_ls_wR_factor_ref 0.0780 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6488 _reflns_number_total 7792 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc01695e2.cif _cod_data_source_block 1_a _cod_original_cell_volume 1753.71(8) _cod_database_code 1571977 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.739 _shelx_estimated_absorpt_t_min 0.445 _olex2_refinement_description ; 1. Others Fixed Sof: I1B(0.93) I1C(0.07) 2.a Aromatic/amide H refined with riding coordinates: C12A(H12A), C11A(H11A), C10A(H10A), C9A(H9A), C8A(H8A), C6A(H6A), C5A(H5A), C4A(H4A), C3A(H3A), C2A(H2A), C12B(H12B), C11B(H11B), C10B(H10B), C9B(H9B), C8B(H8B), C6B(H6B), C5B(H5B), C4B(H4B), C3B(H3B), C2B(H2B), C1S(H1S) 2.b Idealised Me refined as rotating group: C3S(H3SA,H3SB,H3SC), C2S(H2SA,H2SB,H2SC) ; _shelx_res_file ; TITL akl627b_auto_a.res in P-1 1_a.res created by SHELXL-2017/1 at 22:27:12 on 30-Nov-2022 REM Old TITL akl627b_auto in P-1 REM SHELXT solution in P-1 REM R1 0.081, Rweak 0.004, Alpha 0.046, Orientation as input REM Formula found by SHELXT: C3B N3 O10 Mo4 I1B CELL 0.71073 12.7533 12.7583 13.1803 69.875 64.408 68.367 ZERR 1 0.0003 0.0003 0.0003 0.002 0.002 0.002 LATT 1 SFAC C H N O Mo I UNIT 54 54 2 28 8 4 TEMP -123 L.S. 10 PLAN 9 BOND $H LIST 4 fmap 2 acta 51 OMIT 0 OMIT 3 2 1 OMIT -1 1 2 OMIT -3 1 3 OMIT -2 -2 3 OMIT 4 3 3 OMIT 1 4 4 OMIT 3 1 3 SIZE 0.3 0.2 0.1 WGHT 0.031900 4.441900 FVAR 0.23327 I1A 6 0.363150 0.589058 0.647236 11.00000 0.01924 0.02933 = 0.02403 -0.00012 -0.00871 -0.00926 C7A 1 0.190284 0.565080 0.701546 11.00000 0.01683 0.02572 = 0.02847 -0.00243 -0.00944 -0.00872 C12A 1 0.113672 0.571967 0.812318 11.00000 0.02821 0.04519 = 0.02824 -0.00467 -0.01298 -0.01563 AFIX 43 H12A 2 0.136193 0.590089 0.862970 11.00000 -1.20000 AFIX 0 C11A 1 0.001865 0.551433 0.847654 11.00000 0.02427 0.06930 = 0.02881 -0.00271 -0.00579 -0.02038 AFIX 43 H11A 2 -0.053399 0.556128 0.923576 11.00000 -1.20000 AFIX 0 C10A 1 -0.029216 0.524733 0.774806 11.00000 0.03380 0.06643 = 0.03777 0.00760 -0.01503 -0.03219 AFIX 43 H10A 2 -0.106092 0.511365 0.800294 11.00000 -1.20000 AFIX 0 C9A 1 0.049632 0.516822 0.664244 11.00000 0.04161 0.04833 = 0.04068 -0.00228 -0.02565 -0.02214 AFIX 43 H9A 2 0.027279 0.496951 0.614590 11.00000 -1.20000 AFIX 0 C8A 1 0.161884 0.537910 0.625330 11.00000 0.02943 0.03777 = 0.02801 -0.00479 -0.01224 -0.01070 AFIX 43 H8A 2 0.216857 0.533759 0.549206 11.00000 -1.20000 AFIX 0 C1A 1 0.341532 0.746322 0.527267 11.00000 0.02502 0.02217 = 0.02588 -0.00348 -0.00935 -0.00760 C6A 1 0.373510 0.746212 0.413745 11.00000 0.03022 0.02695 = 0.02914 -0.00524 -0.00887 -0.01219 AFIX 43 H6A 2 0.401512 0.675688 0.389426 11.00000 -1.20000 AFIX 0 C5A 1 0.363961 0.851796 0.335109 11.00000 0.03527 0.03719 = 0.02641 0.00020 -0.01186 -0.01616 AFIX 43 H5A 2 0.383649 0.854167 0.256262 11.00000 -1.20000 AFIX 0 C4A 1 0.326323 0.951977 0.371171 11.00000 0.03223 0.02714 = 0.04555 0.00486 -0.01535 -0.00838 AFIX 43 H4A 2 0.321219 1.023960 0.316983 11.00000 -1.20000 AFIX 0 C3A 1 0.295445 0.949507 0.486395 11.00000 0.05193 0.02464 = 0.05742 -0.01344 -0.02029 -0.00172 AFIX 43 H3A 2 0.269036 1.019918 0.510521 11.00000 -1.20000 AFIX 0 C2A 1 0.302574 0.847254 0.565313 11.00000 0.04475 0.03568 = 0.03540 -0.01262 -0.01462 -0.00510 AFIX 43 H2A 2 0.281379 0.845248 0.644353 11.00000 -1.20000 AFIX 0 PART 2 I1B 6 0.755496 0.872447 0.934277 10.93000 0.02972 0.03810 = 0.04175 -0.01191 -0.01119 -0.01711 C7B 1 0.696666 0.873383 1.111172 11.00000 0.02724 0.03644 = 0.04489 -0.00861 -0.01443 -0.01549 C12B 1 0.724559 0.769982 1.186727 11.00000 0.03512 0.02386 = 0.06850 -0.01227 -0.02338 -0.00919 AFIX 43 H12B 2 0.766530 0.700206 1.160192 11.00000 -1.20000 AFIX 0 C11B 1 0.690485 0.770131 1.300599 11.00000 0.04273 0.02927 = 0.05440 0.00330 -0.02656 -0.01453 AFIX 43 H11B 2 0.706722 0.699619 1.354163 11.00000 -1.20000 AFIX 0 C10B 1 0.632571 0.872625 1.337631 11.00000 0.02800 0.04332 = 0.04383 -0.00388 -0.01357 -0.01405 AFIX 43 H10B 2 0.610926 0.872479 1.416275 11.00000 -1.20000 AFIX 0 C9B 1 0.606130 0.974559 1.261613 11.00000 0.02530 0.03561 = 0.04989 -0.01306 -0.01063 -0.00278 AFIX 43 H9B 2 0.566903 1.044412 1.288239 11.00000 -1.20000 AFIX 0 C8B 1 0.635805 0.977361 1.146136 11.00000 0.02789 0.02884 = 0.04361 -0.00464 -0.01227 -0.00583 AFIX 43 H8B 2 0.615344 1.047263 1.093599 11.00000 -1.20000 AFIX 0 PART 0 C1B 1 0.891794 0.953721 0.887729 11.00000 0.02427 0.03997 = 0.03837 -0.01042 -0.00741 -0.01638 C6B 1 0.861306 1.072777 0.864302 11.00000 0.03030 0.03891 = 0.04017 -0.00639 -0.01421 -0.01068 AFIX 43 H6B 2 0.782232 1.116988 0.866516 11.00000 -1.20000 AFIX 0 C5B 1 0.950692 1.125786 0.837287 11.00000 0.04521 0.03979 = 0.03997 -0.00729 -0.01171 -0.01862 AFIX 43 H5B 2 0.932638 1.207693 0.821368 11.00000 -1.20000 AFIX 0 C4B 1 1.064914 1.060536 0.833461 11.00000 0.03426 0.05636 = 0.03712 -0.01261 -0.00605 -0.02500 AFIX 43 H4B 2 1.125430 1.097778 0.813971 11.00000 -1.20000 AFIX 0 C3B 1 1.092433 0.941713 0.857612 11.00000 0.02366 0.05087 = 0.04647 -0.01997 -0.00760 -0.00701 AFIX 43 H3B 2 1.171385 0.897532 0.855859 11.00000 -1.20000 AFIX 0 C2B 1 1.005024 0.885792 0.884651 11.00000 0.03179 0.03918 = 0.04363 -0.01184 -0.00937 -0.01026 AFIX 43 H2B 2 1.023088 0.803899 0.900333 11.00000 -1.20000 AFIX 0 PART 1 I1C 6 0.590533 0.836018 1.483839 10.07000 0.03740 PART 0 MO1 5 0.482097 0.337876 0.906456 11.00000 0.01986 0.01900 = 0.02140 -0.00328 -0.00807 -0.00881 MO2 5 0.698448 0.457557 0.713224 11.00000 0.01677 0.02523 = 0.02062 -0.00583 -0.00506 -0.00759 MO3 5 0.560502 0.690955 0.813715 11.00000 0.02046 0.01860 = 0.02078 0.00023 -0.00750 -0.00973 MO4 5 0.350158 0.573318 1.000109 11.00000 0.01410 0.01803 = 0.01996 -0.00274 -0.00656 -0.00619 O2 4 0.617762 0.512724 0.622324 11.00000 0.02281 0.02986 = 0.02458 -0.00504 -0.00815 -0.00954 O3 4 0.476376 0.741900 0.727115 11.00000 0.02868 0.02566 = 0.02720 0.00019 -0.01275 -0.00953 O4 4 0.269990 0.630876 0.911312 11.00000 0.02302 0.02485 = 0.02764 -0.00361 -0.01250 -0.00626 O1 4 0.397973 0.398010 0.818537 11.00000 0.02675 0.02661 = 0.02846 -0.00400 -0.01332 -0.01062 O7 4 0.841212 0.405314 0.627893 11.00000 0.01930 0.03984 = 0.02791 -0.01062 -0.00506 -0.00572 O8 4 0.704679 0.600110 0.725281 11.00000 0.01943 0.02535 = 0.02415 -0.00320 -0.00463 -0.01108 O9 4 0.607623 0.805160 0.800338 11.00000 0.02790 0.02358 = 0.02928 -0.00092 -0.00880 -0.01220 O10 4 0.425728 0.695614 0.965051 11.00000 0.01956 0.01700 = 0.02348 -0.00304 -0.00837 -0.00631 O11 4 0.244314 0.600890 1.133977 11.00000 0.01548 0.02355 = 0.02482 -0.00682 -0.00654 -0.00623 O12 4 0.358930 0.409671 1.037393 11.00000 0.01936 0.01773 = 0.02056 -0.00003 -0.00706 -0.00982 O5 4 0.471983 0.198307 0.957700 11.00000 0.03170 0.02113 = 0.02874 -0.00344 -0.01166 -0.01150 O13 4 0.523499 0.510609 0.883680 11.00000 0.01606 0.01885 = 0.02261 -0.00259 -0.00642 -0.00773 O6 4 0.639693 0.321391 0.797182 11.00000 0.01867 0.02293 = 0.02471 -0.00829 -0.00515 -0.00680 O1S 4 0.907768 0.850153 0.706478 11.00000 0.04260 0.05829 = 0.05197 -0.01996 -0.01476 -0.01281 N1S 3 0.935295 0.803161 0.544543 11.00000 0.02499 0.03485 = 0.04142 -0.01175 -0.00431 -0.00905 C1S 1 0.883241 0.803469 0.655554 11.00000 0.02458 0.04516 = 0.04545 -0.01285 -0.00494 -0.00781 AFIX 43 H1S 2 0.821603 0.764156 0.699537 11.00000 -1.20000 AFIX 0 C3S 1 0.893918 0.750297 0.491510 11.00000 0.02985 0.04967 = 0.04878 -0.01782 -0.00294 -0.01485 AFIX 137 H3SA 2 0.961526 0.691636 0.453816 11.00000 -1.50000 H3SB 2 0.861780 0.809821 0.434093 11.00000 -1.50000 H3SC 2 0.830646 0.713917 0.550990 11.00000 -1.50000 AFIX 0 C2S 1 1.035274 0.855452 0.470250 11.00000 0.04091 0.05262 = 0.05034 -0.01824 0.00242 -0.02506 AFIX 137 H2SA 2 1.101987 0.799708 0.427692 11.00000 -1.50000 H2SB 2 1.062135 0.877436 0.517552 11.00000 -1.50000 H2SC 2 1.008854 0.924336 0.415604 11.00000 -1.50000 AFIX 0 HKLF 4 REM akl627b_auto_a.res in P-1 REM R1 = 0.0304 for 6488 Fo > 4sig(Fo) and 0.0417 for all 7792 data REM 439 parameters refined using 0 restraints END WGHT 0.0319 4.4443 REM Highest difference peak 2.451, deepest hole -0.943, 1-sigma level 0.130 Q1 1 0.7659 0.8882 0.8808 11.00000 0.05 2.45 Q2 1 0.7525 0.8982 0.9480 11.00000 0.05 1.82 Q3 1 0.7951 0.8405 0.9428 11.00000 0.05 1.80 Q4 1 0.7697 0.8249 0.9513 11.00000 0.05 1.78 Q5 1 0.6231 0.7948 1.4776 11.00000 0.05 0.80 Q6 1 0.5734 0.8768 1.4871 11.00000 0.05 0.75 Q7 1 0.7351 0.8346 1.0165 11.00000 0.05 0.70 Q8 1 0.3204 0.5589 0.9287 11.00000 0.05 0.69 Q9 1 0.6370 0.4815 0.6754 11.00000 0.05 0.67 ; _shelx_res_checksum 1417 _shelx_hkl_file ; 0 0 -2 19.34 1.79 0 0 2 14.95 1.48 0 0 -2 16.92 1.54 0 0 2 17.53 1.42 0 0 -2 21.93 2.33 0 0 3 410.34 9.13 0 0 -3 407.20 9.20 0 0 -3 416.19 8.68 0 0 3 416.81 8.62 0 0 -3 435.97 10.38 0 0 -4 266.60 7.76 0 0 4 269.38 7.71 0 0 -4 278.45 7.25 0 0 4 281.60 7.19 0 0 -4 268.52 8.86 0 0 -5 136.40 5.81 0 0 5 138.55 5.82 0 0 5 145.06 5.38 0 0 -5 145.80 5.48 0 0 -5 145.34 6.98 0 0 6 317.77 9.96 0 0 -6 321.46 9.96 0 0 6 326.91 9.15 0 0 -6 312.99 11.28 0 0 -7 160.99 7.29 0 0 7 151.49 7.20 0 0 7 152.87 6.38 0 0 -7 156.63 8.50 0 0 8 27.54 3.07 0 0 -8 22.16 3.26 0 0 8 22.81 3.45 0 0 -8 25.09 4.35 0 0 -9 11.35 2.93 0 0 9 18.80 3.51 0 0 9 18.30 2.82 0 0 -9 13.11 3.84 0 0 -10 108.52 7.28 0 0 10 115.08 7.60 0 0 10 121.26 6.71 0 0 -10 94.75 8.20 0 0 -11 880.40 23.73 0 0 11 893.15 21.79 0 0 -11 857.09 26.88 0 0 -12 2.65 3.05 0 0 12 7.32 2.63 0 0 -12 6.59 4.32 0 0 -13 31.62 5.04 0 0 -13 31.26 6.09 0 0 -14 137.00 9.72 0 0 -15 1.85 3.44 0 1 -14 258.62 13.34 0 1 -14 277.54 16.96 0 1 -13 8.02 3.42 0 1 -13 1.72 4.28 0 1 -12 24.67 4.31 0 1 -12 14.75 4.64 0 1 -11 856.65 23.19 0 -1 11 874.96 22.28 0 1 -11 884.78 27.69 0 1 -10 381.05 13.65 0 -1 10 386.97 13.06 0 1 -10 394.87 16.78 0 -1 9 40.30 4.06 0 1 -9 37.92 4.25 0 1 -9 50.16 6.16 0 1 -8 195.78 8.45 0 -1 8 188.62 8.13 0 1 -8 199.09 8.30 0 1 -8 199.77 10.49 0 1 -7 118.32 6.07 0 -1 7 109.10 6.06 0 -1 7 114.36 5.81 0 1 -7 114.59 5.97 0 1 -7 108.51 7.39 0 -1 6 3.14 1.69 0 -1 6 6.56 2.47 0 1 -6 1.94 1.94 0 1 -6 2.26 1.90 0 1 -6 6.19 3.46 0 -1 5 108.96 5.08 0 1 -5 104.02 4.98 0 -1 5 99.38 4.83 0 1 -5 97.80 4.88 0 1 -4 4.39 1.86 0 -1 4 3.89 1.63 0 -1 4 7.34 2.06 0 1 -4 2.19 1.81 0 1 -3 1470.42 24.39 0 1 -3 1505.46 24.97 0 -1 3 1516.74 25.02 0 1 -2 419.03 8.03 0 1 -2 410.09 8.67 0 -1 2 402.35 8.59 0 1 -1 278.13 6.02 0 -1 1 284.50 6.04 0 -1 -1 380.85 7.11 0 1 1 372.38 7.05 0 1 2 530.82 10.37 0 -1 -2 540.58 10.42 0 1 3 1630.82 26.87 0 -1 -3 1615.57 26.84 0 1 3 1596.52 27.49 0 -1 -4 16.08 2.71 0 1 4 24.53 2.72 0 1 4 21.17 2.01 0 1 4 20.02 2.92 0 -1 -4 10.12 2.57 0 -1 -5 264.60 8.59 0 1 5 276.69 8.78 0 1 5 279.37 7.50 0 1 5 284.86 9.71 0 -1 -5 264.20 9.37 0 1 6 1773.88 32.50 0 -1 -6 1723.18 32.08 0 1 6 1750.10 29.90 0 -1 -6 1757.73 33.92 0 -1 -7 737.60 18.00 0 1 7 723.69 18.04 0 1 7 724.78 15.84 0 -1 -7 734.56 19.55 0 1 8 211.80 9.27 0 -1 -8 203.14 8.99 0 1 8 208.43 7.67 0 -1 -8 193.65 9.93 0 1 9 122.00 7.45 0 -1 -9 113.92 7.08 0 1 9 122.54 6.12 0 -1 -9 120.18 8.30 0 -1 -10 42.14 4.89 0 1 10 47.20 5.28 0 1 10 46.64 4.12 0 -1 -10 35.74 5.42 0 -1 -11 247.38 11.73 0 1 11 255.99 10.04 0 1 12 16.63 3.19 0 -1 -12 18.78 4.10 0 -1 -13 83.08 7.64 0 -1 -14 -1.10 3.06 0 -1 -15 47.01 6.45 0 2 -13 6.07 2.83 0 2 -13 10.54 4.70 0 2 -12 180.00 10.00 0 2 -12 184.29 13.07 0 -2 11 25.86 3.93 0 2 -11 24.55 3.70 0 2 -11 24.93 5.66 0 -2 10 44.91 4.65 0 2 -10 42.85 4.70 0 2 -10 41.89 4.78 0 2 -10 45.35 6.59 0 2 -9 270.31 10.53 0 -2 9 260.85 10.68 0 2 -9 272.31 10.94 0 2 -9 249.55 12.91 0 2 -8 470.67 13.81 0 2 -8 487.81 14.51 0 -2 8 479.85 14.41 0 2 -8 501.63 17.28 0 2 -7 2.33 1.97 0 -2 7 2.37 2.02 0 2 -7 1.91 2.06 0 -2 6 32.53 3.36 0 2 -6 36.52 3.37 0 2 -6 37.06 3.65 0 2 -5 595.49 13.48 0 -2 5 595.42 14.43 0 2 -5 613.22 14.63 0 2 -4 217.68 6.60 0 2 -4 227.00 7.62 0 -2 4 227.65 7.54 0 2 -3 2544.89 39.58 0 2 -3 2630.75 41.67 0 -2 3 2581.71 41.53 0 2 -2 533.03 11.68 0 -2 2 543.56 11.66 0 2 -1 96.27 4.00 0 -2 1 85.38 3.77 0 2 0 415.83 8.78 0 2 0 404.05 8.29 0 -2 0 421.42 8.36 0 -2 0 411.16 7.61 0 -2 0 409.89 8.37 0 -2 -1 57.51 2.22 0 2 1 55.61 2.13 0 -2 -1 52.35 2.42 0 2 1 53.42 2.44 0 2 2 2031.65 31.90 0 2 2 2007.83 31.99 0 -2 -2 2010.68 31.99 0 -2 -2 2006.77 29.94 0 2 2 2001.24 29.90 0 -2 -3 232.56 7.15 0 2 3 237.19 7.05 0 -2 -3 224.66 5.51 0 2 4 856.78 17.70 0 -2 -4 871.54 17.79 0 2 4 871.71 18.21 0 2 5 1502.57 28.16 0 -2 -5 1499.86 28.02 0 2 5 1517.78 29.10 0 2 6 698.14 17.06 0 -2 -6 694.20 16.90 0 2 6 695.65 14.64 0 2 6 707.67 17.99 0 2 7 1261.69 26.73 0 -2 -7 1215.51 26.24 0 2 7 1262.18 23.50 0 2 7 1259.58 27.89 0 -2 -8 406.98 13.57 0 2 8 418.79 13.95 0 2 8 427.97 11.50 0 2 8 438.32 15.40 0 2 9 508.11 16.26 0 -2 -9 484.97 15.72 0 2 9 503.33 13.33 0 2 10 2.22 2.52 0 -2 -10 5.70 2.83 0 2 10 4.96 2.01 0 2 11 -0.74 2.08 0 -2 -11 7.35 3.38 0 -2 -12 36.03 5.15 0 2 12 42.47 4.29 0 -2 -13 56.81 6.68 0 -2 -14 49.33 6.42 0 2 15 -7.93 4.43 0 3 -13 92.34 9.90 0 3 -12 53.40 5.39 0 3 -12 59.80 8.14 0 3 -11 1.79 2.50 0 3 -11 2.10 3.02 0 3 -10 108.06 6.88 0 3 -10 108.63 7.59 0 -3 10 107.49 7.44 0 3 -10 123.06 9.89 0 3 -9 216.78 9.35 0 3 -9 229.71 10.49 0 -3 9 228.50 10.39 0 3 -9 231.99 12.78 0 -3 8 217.23 9.73 0 3 -8 201.32 9.41 0 3 -8 204.89 8.60 0 3 -7 94.30 6.18 0 -3 7 97.91 6.31 0 3 -7 103.85 5.61 0 3 -6 414.30 12.78 0 -3 6 395.00 12.62 0 3 -6 406.94 11.14 0 -3 5 39.71 3.83 0 3 -5 40.49 3.16 0 3 -5 39.89 3.92 0 3 -4 100.39 5.53 0 -3 4 99.51 5.45 0 3 -4 105.82 4.66 0 3 -3 6.58 2.24 0 -3 3 8.32 2.17 0 -3 2 192.80 6.93 0 3 -2 190.56 6.92 0 -3 1 364.86 9.63 0 3 -1 377.50 9.90 0 3 -1 376.47 9.57 0 3 0 264.33 7.58 0 3 0 260.93 6.96 0 -3 0 255.68 6.94 0 -3 0 248.46 6.96 0 -3 0 251.77 6.05 0 3 1 139.32 4.42 0 -3 -1 147.06 4.50 0 3 1 148.39 4.58 0 3 1 136.62 4.72 0 -3 -1 145.17 4.63 0 3 2 0.26 1.76 0 -3 -2 1.71 1.50 0 3 2 2.69 1.51 0 3 2 2.18 1.19 0 -3 -2 1.23 1.24 0 3 3 3540.45 55.25 0 3 3 3621.07 55.59 0 -3 -3 3515.40 52.26 0 3 3 3537.26 52.22 0 3 4 1697.61 30.54 0 3 4 1745.97 30.71 0 -3 -4 1712.57 30.59 0 -3 -4 1675.02 27.25 0 3 5 191.41 7.68 0 -3 -5 177.56 7.50 0 -3 -5 180.20 5.85 0 3 6 378.86 12.08 0 -3 -6 370.38 11.88 0 3 6 395.10 12.76 0 -3 -7 73.53 5.62 0 3 7 76.14 5.55 0 3 7 78.42 5.98 0 3 8 288.48 11.50 0 -3 -8 266.33 10.98 0 3 8 286.99 9.16 0 3 8 284.45 12.00 0 -3 -9 1.39 2.63 0 3 9 -3.35 3.27 0 3 9 2.67 1.97 0 3 9 4.45 3.31 0 -3 -10 28.97 4.54 0 3 10 27.79 3.25 0 -3 -11 575.09 19.31 0 3 11 596.42 15.86 0 -3 -12 69.02 6.93 0 3 12 68.85 5.18 0 -3 -13 6.30 3.33 0 3 14 58.95 7.77 0 4 -12 79.84 6.41 0 4 -12 87.67 7.85 0 4 -12 81.80 9.37 0 4 -11 12.01 3.04 0 4 -11 11.82 3.77 0 4 -11 12.62 5.51 0 4 -10 6.20 2.58 0 4 -10 2.92 2.79 0 4 -10 5.72 4.32 0 4 -9 235.15 11.15 0 -4 9 224.71 11.01 0 4 -9 222.88 9.42 0 4 -8 580.31 17.64 0 -4 8 589.76 18.12 0 4 -8 584.64 15.62 0 -4 7 995.79 24.30 0 4 -7 984.35 23.99 0 4 -7 976.97 21.09 0 4 -6 11.45 2.25 0 -4 6 10.51 2.76 0 4 -6 8.85 2.72 0 -4 5 255.69 10.24 0 4 -5 269.71 10.26 0 4 -5 264.80 8.21 0 -4 4 37.62 3.94 0 4 -4 32.14 3.75 0 4 -3 1271.11 25.73 0 -4 3 1270.09 25.86 0 4 -2 111.97 5.88 0 -4 2 103.50 5.56 0 4 -2 106.98 5.66 0 4 -1 1308.12 25.38 0 4 -1 1335.89 24.94 0 4 0 1232.47 23.38 0 4 0 1221.35 22.33 0 -4 0 1190.70 20.72 0 -4 0 1219.92 22.41 0 -4 -1 578.57 12.26 0 4 1 599.40 12.40 0 -4 -1 546.79 11.96 0 -4 -1 594.38 12.83 0 4 1 595.87 12.84 0 4 1 587.85 12.06 0 -4 -2 1284.55 22.95 0 4 2 1281.35 23.43 0 4 2 1261.89 21.55 0 -4 -2 1248.97 21.59 0 4 2 1286.43 22.98 0 4 2 1294.92 22.86 0 4 3 125.76 5.71 0 -4 -3 119.68 4.19 0 4 3 135.21 4.28 0 4 3 131.42 5.76 0 4 4 994.08 20.60 0 4 4 1000.86 20.90 0 -4 -4 962.20 17.27 0 4 5 5.68 2.39 0 4 5 5.21 2.50 0 -4 -5 5.05 1.41 0 4 6 164.25 8.02 0 -4 -6 161.34 7.92 0 4 6 176.21 8.14 0 -4 -6 172.68 6.00 0 4 7 100.29 6.58 0 -4 -7 109.77 6.91 0 4 7 104.13 6.84 0 -4 -7 101.52 4.91 0 4 7 112.46 7.12 0 4 8 401.72 14.21 0 -4 -8 390.81 13.89 0 4 8 419.77 15.02 0 -4 -8 382.45 11.22 0 4 9 15.24 3.51 0 -4 -9 19.90 3.77 0 4 9 19.77 2.95 0 4 9 21.18 4.35 0 -4 -10 132.58 8.66 0 4 10 138.12 6.82 0 -4 -11 317.19 14.20 0 4 11 315.61 10.93 0 4 11 308.40 14.61 0 -4 -12 47.62 6.21 0 4 12 51.22 6.69 0 4 13 -1.82 3.52 0 4 14 0.14 3.38 0 5 -12 51.73 6.75 0 5 -12 53.83 8.27 0 5 -11 1.01 2.20 0 5 -11 2.36 2.99 0 5 -11 8.99 5.38 0 5 -10 14.81 4.20 0 5 -10 15.16 3.10 0 5 -9 333.92 14.13 0 5 -9 332.15 11.63 0 5 -8 4.58 3.30 0 5 -8 1.93 2.08 0 5 -7 22.68 4.02 0 -5 7 18.15 3.49 0 5 -7 21.64 2.83 0 -5 6 337.23 13.02 0 5 -6 343.24 12.92 0 5 -6 363.33 14.31 0 5 -6 322.38 10.04 0 5 -5 30.92 4.16 0 -5 5 33.40 4.10 0 5 -5 30.82 4.03 0 5 -4 -0.78 2.35 0 5 -4 -0.24 2.59 0 -5 4 -0.70 1.98 0 -5 3 1447.39 29.96 0 5 -3 1439.41 29.73 0 5 -3 1488.31 30.30 0 5 -2 40.20 4.24 0 5 -2 38.81 3.81 0 5 -1 455.96 13.00 0 5 -1 446.11 12.53 0 -5 1 432.83 10.21 0 -5 0 3.81 1.45 0 5 0 -0.56 2.56 0 5 0 0.25 1.71 0 -5 0 5.11 2.50 0 5 1 190.84 6.74 0 -5 -1 186.39 6.68 0 -5 -1 194.17 6.50 0 5 1 194.34 6.33 0 5 1 197.21 7.08 0 -5 -1 193.82 7.10 0 -5 -2 17.83 2.46 0 5 2 8.60 1.57 0 -5 -2 16.36 2.19 0 5 2 14.99 1.98 0 5 2 15.88 2.29 0 -5 -3 334.67 10.05 0 5 3 341.12 10.48 0 -5 -3 326.72 8.48 0 5 3 349.55 8.45 0 5 3 364.36 10.34 0 5 4 123.56 6.30 0 -5 -4 111.42 4.38 0 5 4 112.36 4.28 0 5 4 116.89 6.06 0 5 5 765.23 18.58 0 -5 -5 745.34 14.96 0 5 5 826.58 19.58 0 5 6 372.68 12.71 0 -5 -6 364.24 9.42 0 5 6 416.18 13.44 0 5 7 263.55 11.02 0 5 7 265.94 11.10 0 -5 -7 244.94 7.83 0 5 8 1852.36 39.20 0 5 8 1991.64 39.88 0 -5 -8 1866.18 33.67 0 5 8 2009.35 40.66 0 5 9 22.01 4.27 0 -5 -9 23.46 2.85 0 5 10 320.20 14.45 0 5 10 327.40 11.19 0 -5 -10 329.74 11.13 0 5 11 21.63 4.47 0 5 11 12.42 2.69 0 -5 -11 17.22 3.00 0 5 12 15.44 4.48 0 -5 -12 10.21 2.77 0 5 13 112.91 9.95 0 -5 -13 117.73 7.70 0 5 14 34.62 6.30 0 6 -12 7.61 4.32 0 6 -11 3.18 3.59 0 6 -11 9.15 5.14 0 6 -10 131.91 9.65 0 6 -10 157.30 7.99 0 6 -9 -1.02 3.39 0 6 -9 3.31 2.10 0 6 -8 184.28 10.67 0 6 -8 193.65 8.31 0 6 -7 200.25 10.71 0 6 -7 197.58 8.01 0 -6 6 1426.25 32.67 0 6 -6 1412.53 32.15 0 6 -6 1371.72 26.83 0 -6 5 239.70 11.13 0 6 -5 223.36 10.63 0 6 -5 253.09 11.78 0 6 -4 -1.20 2.73 0 6 -4 -0.15 2.63 0 6 -3 1941.67 38.95 0 6 -3 2059.61 39.73 0 6 -2 788.35 20.40 0 6 -2 811.99 20.26 0 -6 1 10.72 1.86 0 6 -1 7.76 2.71 0 6 -1 11.77 2.68 0 -6 1 9.25 2.56 0 6 0 78.65 5.50 0 6 0 83.56 5.12 0 -6 0 80.31 4.22 0 -6 0 87.98 5.46 0 6 1 245.86 9.52 0 -6 -1 236.72 8.27 0 6 1 260.23 8.61 0 -6 -1 231.93 8.58 0 -6 -1 229.76 7.73 0 -6 -2 484.77 12.52 0 6 2 497.11 12.16 0 -6 -2 475.91 12.09 0 6 2 491.79 12.41 0 6 2 500.32 13.20 0 -6 -3 72.50 4.72 0 6 3 79.06 5.09 0 6 3 76.56 4.05 0 -6 -3 76.46 4.13 0 6 3 76.54 4.80 0 6 3 70.79 4.54 0 6 4 142.16 7.16 0 -6 -4 129.44 5.20 0 6 4 137.66 5.18 0 6 4 139.41 6.85 0 6 5 87.22 5.94 0 -6 -5 74.94 3.90 0 6 5 81.90 3.86 0 6 5 87.23 5.87 0 6 6 7.43 2.54 0 -6 -6 12.53 1.87 0 6 6 15.03 3.04 0 6 7 8.33 2.97 0 -6 -7 9.98 1.76 0 6 7 11.02 2.88 0 6 8 465.35 16.24 0 -6 -8 472.76 12.11 0 6 9 101.06 7.75 0 -6 -9 99.73 5.37 0 6 10 20.38 4.37 0 -6 -10 26.46 3.24 0 6 11 86.75 6.07 0 6 11 83.17 7.86 0 -6 -11 92.13 5.85 0 6 12 39.36 5.98 0 -6 -12 31.63 3.71 0 6 13 3.39 3.50 0 6 14 223.82 14.55 0 7 -12 7.10 4.95 0 7 -11 74.18 8.18 0 7 -10 14.45 4.71 0 7 -9 9.43 4.01 0 7 -9 13.68 2.77 0 7 -8 23.75 5.00 0 7 -8 21.97 3.07 0 7 -7 91.27 7.64 0 7 -7 89.02 5.53 0 7 -6 618.28 20.32 0 7 -6 619.34 15.55 0 7 -5 7.02 3.47 0 7 -4 457.39 16.19 0 7 -3 154.93 8.90 0 7 -3 175.59 9.39 0 7 -2 109.25 7.40 0 7 -2 112.68 7.15 0 -7 2 110.04 5.29 0 -7 1 21.60 2.41 0 7 -1 21.87 3.83 0 7 -1 19.67 3.29 0 -7 1 25.01 3.49 0 7 0 1006.13 24.55 0 7 0 1039.77 23.18 0 -7 0 1016.41 22.97 0 -7 0 1020.74 20.70 0 7 1 349.67 12.56 0 7 1 351.49 11.12 0 -7 -1 341.45 10.29 0 -7 -1 334.31 11.25 0 7 2 5.22 1.89 0 -7 -2 3.57 1.93 0 7 2 3.16 2.39 0 7 2 4.37 1.77 0 -7 -2 2.32 1.79 0 7 2 0.89 1.75 0 -7 -3 1080.29 23.36 0 7 3 1113.16 24.38 0 7 3 1094.44 21.67 0 -7 -3 1074.12 21.78 0 7 3 1109.69 23.80 0 7 3 1106.01 23.21 0 7 4 2653.21 47.49 0 7 4 2625.77 42.55 0 -7 -4 2508.97 42.70 0 7 4 2614.41 46.01 0 7 4 2636.58 46.05 0 7 5 858.07 21.57 0 7 5 819.09 16.59 0 -7 -5 778.53 16.74 0 7 5 825.15 20.52 0 7 6 95.58 6.78 0 -7 -6 93.20 4.58 0 7 6 96.84 6.65 0 -7 -7 45.78 3.31 0 7 7 56.60 5.51 0 7 8 48.29 5.43 0 -7 -8 47.41 3.47 0 7 9 0.08 2.78 0 -7 -9 4.51 1.44 0 7 10 146.99 10.03 0 -7 -10 145.07 6.69 0 7 11 51.75 6.67 0 -7 -11 44.25 4.03 0 7 12 26.11 5.46 0 -7 -12 24.06 3.27 0 7 13 41.55 6.52 0 8 -11 117.07 10.47 0 8 -10 236.77 14.06 0 8 -9 36.47 6.21 0 8 -8 27.33 3.53 0 8 -8 36.83 6.15 0 8 -7 53.31 6.33 0 8 -7 45.12 4.30 0 8 -6 334.34 15.15 0 8 -5 251.86 12.76 0 8 -4 99.60 7.86 0 8 -3 3.02 2.85 0 -8 3 10.24 2.34 0 -8 2 20.13 2.68 0 8 -2 21.74 4.33 0 8 -2 23.85 3.85 0 -8 2 15.73 3.38 0 8 -1 234.19 11.29 0 8 -1 252.46 10.94 0 -8 1 226.65 10.25 0 -8 1 241.39 8.52 0 8 0 272.66 11.99 0 8 0 274.23 10.88 0 -8 0 273.82 9.25 0 -8 0 263.36 10.73 0 8 1 673.48 19.59 0 8 1 683.28 17.79 0 -8 -1 639.36 17.75 0 -8 -1 670.45 16.42 0 8 2 119.93 7.67 0 -8 -2 109.97 6.11 0 8 2 118.85 6.31 0 8 2 120.47 6.23 0 -8 -3 21.66 2.96 0 8 3 24.16 3.20 0 8 3 25.00 3.50 0 8 3 23.17 2.85 0 -8 -3 20.96 2.83 0 8 3 25.06 3.38 0 8 4 1132.83 25.82 0 -8 -4 1031.46 21.70 0 8 4 1032.30 21.35 0 8 4 1082.22 24.44 0 8 4 1063.67 24.10 0 8 5 489.04 15.91 0 8 5 455.79 11.77 0 -8 -5 460.17 12.13 0 8 5 454.80 14.72 0 8 5 464.04 14.66 0 -8 -6 403.07 10.98 0 8 6 423.40 14.66 0 8 6 415.94 10.75 0 -8 -7 132.14 5.75 0 8 7 135.19 8.53 0 8 8 3.82 2.87 0 -8 -8 0.19 1.31 0 8 9 1.75 2.94 0 -8 -9 0.10 1.63 0 8 10 31.44 5.41 0 -8 -10 33.01 3.18 0 -8 -11 202.42 8.18 0 8 11 235.41 13.45 0 8 12 159.22 11.64 0 8 13 28.67 5.86 0 9 -10 209.20 13.89 0 9 -9 0.68 3.78 0 9 -8 11.91 4.70 0 9 -7 25.00 3.42 0 9 -7 20.18 4.99 0 9 -6 80.58 8.08 0 9 -5 34.37 5.55 0 9 -4 65.86 7.12 0 -9 4 63.95 4.80 0 9 -3 122.77 8.98 0 -9 3 119.62 8.55 0 -9 3 124.11 6.44 0 9 -2 160.29 10.12 0 -9 2 144.04 9.02 0 -9 2 150.42 7.01 0 -9 1 -0.12 1.49 0 9 -1 -0.53 2.91 0 9 -1 1.44 2.02 0 -9 1 -1.40 2.55 0 9 0 300.64 13.28 0 9 0 312.80 12.39 0 -9 0 278.04 11.86 0 -9 0 295.22 10.23 0 9 1 1450.14 34.30 0 9 1 1555.90 32.16 0 -9 -1 1512.69 30.08 0 -9 -1 1484.09 32.27 0 -9 -2 36.53 3.88 0 9 2 34.91 4.89 0 9 2 38.39 4.32 0 9 2 36.30 3.97 0 9 3 31.55 3.82 0 -9 -3 27.35 3.55 0 9 3 27.54 4.24 0 9 3 26.53 3.85 0 9 3 30.05 3.49 0 9 3 32.27 3.91 0 9 4 1.62 2.05 0 9 4 1.82 2.34 0 9 4 1.37 1.55 0 -9 -4 0.60 1.61 0 9 4 3.74 2.25 0 -9 -5 498.35 13.31 0 9 5 478.56 12.86 0 9 5 482.50 15.68 0 9 5 485.20 15.72 0 9 6 47.55 5.21 0 -9 -6 49.74 3.84 0 9 6 55.58 3.80 0 9 6 48.79 4.94 0 -9 -7 128.72 5.93 0 9 7 139.69 8.86 0 -9 -8 79.73 4.60 0 9 8 78.30 7.06 0 9 9 4.00 3.60 0 -9 -9 1.35 1.43 0 -9 -10 78.01 4.62 0 9 10 86.55 8.21 0 9 11 185.76 12.26 0 9 12 358.06 17.73 0 9 13 44.79 7.09 0 10 -9 9.10 5.01 0 10 -8 3.97 3.79 0 10 -7 -5.68 4.44 0 10 -6 376.87 17.90 0 10 -5 234.49 13.82 0 10 -4 8.49 4.01 0 -10 4 8.12 2.42 0 -10 4 6.53 3.60 0 10 -3 4.97 3.75 0 -10 3 13.97 2.96 0 -10 3 10.52 4.08 0 10 -2 63.78 7.14 0 -10 2 58.20 4.68 0 -10 2 61.55 6.38 0 10 -1 28.49 5.06 0 -10 1 29.40 3.52 0 -10 1 31.17 4.77 0 -10 0 0.62 1.76 0 10 0 5.03 3.54 0 10 0 3.77 2.69 0 -10 0 -0.13 2.43 0 10 1 57.47 6.29 0 10 1 54.12 5.36 0 -10 -1 54.07 4.77 0 -10 -1 50.30 5.39 0 -10 -2 1.44 1.82 0 10 2 2.25 2.14 0 10 2 3.69 2.32 0 10 2 -2.83 3.29 0 -10 -3 6.64 2.54 0 10 3 0.77 2.82 0 10 3 6.78 2.78 0 10 3 5.13 2.11 0 10 4 198.62 11.03 0 10 4 221.00 8.99 0 10 4 204.46 9.81 0 10 5 375.44 15.31 0 10 5 406.54 12.15 0 -10 -5 393.46 12.23 0 10 5 397.80 14.56 0 10 6 45.41 5.30 0 10 6 41.23 3.66 0 -10 -6 45.40 3.93 0 -10 -7 500.15 13.40 0 10 7 510.05 17.97 0 10 8 31.02 5.12 0 -10 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161.41 7.72 -2 6 2 168.94 7.83 2 -6 -1 2.62 1.79 2 -6 -1 1.93 2.01 -2 6 1 1.33 1.86 -2 6 0 456.50 13.81 2 -6 0 438.08 13.66 2 -6 0 464.44 13.22 2 -6 0 445.66 12.42 -2 6 -1 40.98 4.32 2 -6 1 44.86 4.45 2 -6 1 39.77 3.66 2 -6 1 38.02 3.80 -2 6 -2 64.83 5.64 -2 6 -2 73.44 5.76 2 -6 2 65.98 5.46 2 -6 2 70.33 4.82 -2 6 -3 39.21 4.64 -2 6 -3 29.02 4.17 -2 6 -4 257.99 11.50 -2 6 -4 278.33 12.23 -2 6 -5 155.21 8.90 -2 6 -6 500.33 17.04 -2 6 -7 118.37 8.14 -2 6 -8 256.32 10.85 -2 6 -8 238.77 12.00 -2 6 -9 229.16 10.63 -2 6 -9 227.70 11.92 -2 6 -10 6.95 3.02 -2 6 -10 9.94 4.01 -2 6 -11 -7.78 3.74 -2 6 -11 2.02 3.21 -2 6 -12 5.82 3.81 -2 5 13 9.88 4.35 2 -5 -13 11.75 3.53 -2 5 12 78.48 8.46 2 -5 -12 76.60 6.65 -2 5 11 -1.18 3.28 2 -5 -11 -0.27 2.59 -2 5 10 10.61 3.83 2 -5 -10 10.50 2.83 2 -5 -9 94.17 6.43 -2 5 9 90.15 7.74 -2 5 8 19.67 4.00 2 -5 -8 24.74 3.43 2 -5 -7 178.16 8.03 -2 5 7 167.60 9.47 -2 5 6 320.92 12.42 2 -5 -6 282.16 9.96 -2 5 6 283.49 11.90 -2 5 5 1692.34 33.88 2 -5 -5 1539.81 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32.32 4.01 -2 4 -3 32.75 3.75 -2 4 -4 128.46 6.82 -2 4 -4 133.57 7.39 -2 4 -5 339.34 11.75 -2 4 -5 362.09 13.11 -2 4 -6 0.36 2.15 -2 4 -6 -0.44 2.44 -2 4 -7 2.43 2.54 -2 4 -7 0.09 2.45 -2 4 -8 173.78 8.60 -2 4 -8 166.22 8.78 -2 4 -9 27.77 3.91 -2 4 -9 33.36 4.55 -2 4 -10 237.09 10.93 -2 4 -10 222.88 10.85 -2 4 -11 533.04 17.66 -2 4 -11 527.06 17.85 -2 4 -12 -1.34 2.69 -2 4 -12 2.69 2.82 -2 4 -12 7.70 5.06 -2 4 -13 2.96 3.22 -2 4 -13 7.91 5.04 2 -3 -14 141.88 10.52 -2 3 13 1.35 3.24 2 -3 -13 -2.44 3.38 -2 3 12 72.16 7.90 2 -3 -12 65.83 6.75 -2 3 11 371.49 14.01 -2 3 11 373.63 16.67 2 -3 -11 356.56 14.59 -2 3 10 46.49 4.95 -2 3 10 42.64 5.79 2 -3 -10 44.13 5.06 -2 3 9 -2.27 3.20 -2 3 9 2.24 2.52 2 -3 -9 0.86 2.15 -2 3 8 137.02 8.20 -2 3 8 130.51 7.38 -2 3 8 119.68 8.07 2 -3 -8 127.13 7.19 -2 3 7 137.56 7.88 -2 3 7 120.64 7.66 -2 3 7 147.10 9.05 2 -3 -7 129.15 6.87 -2 3 6 171.39 8.34 2 -3 -6 176.15 7.63 -2 3 6 175.15 8.74 -2 3 6 181.87 9.37 -2 3 5 34.87 3.72 -2 3 5 32.56 3.98 2 -3 -5 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1604.57 32.06 2 7 1 1583.67 28.11 2 7 1 1594.67 29.70 -2 -7 -1 1617.56 31.67 2 7 2 17.78 2.16 2 7 2 16.34 3.13 2 7 2 14.11 2.34 2 7 2 15.97 2.29 2 7 2 18.13 2.98 2 7 3 216.23 8.90 2 7 3 216.33 8.22 2 7 3 221.57 6.88 2 7 3 214.32 7.29 2 7 3 220.81 9.03 2 7 4 140.84 6.96 2 7 4 158.96 7.38 2 7 4 144.74 4.75 2 7 4 145.50 7.34 2 7 4 148.84 6.42 2 7 5 677.86 16.74 2 7 5 684.59 16.84 2 7 5 693.81 12.07 2 7 5 725.85 18.40 2 7 6 81.21 5.49 2 7 6 90.85 5.22 -2 -7 -6 87.45 6.24 2 7 6 85.24 6.01 2 7 7 548.20 16.39 -2 -7 -7 544.01 16.94 2 7 7 589.55 17.61 2 7 8 1.51 2.74 2 7 8 2.50 2.57 -2 -7 -8 -1.49 3.06 2 7 9 15.81 3.69 -2 -7 -9 14.48 1.38 -2 -7 -9 17.07 4.04 2 7 10 37.47 5.33 -2 -7 -10 34.79 2.37 -2 -7 -10 42.26 5.59 2 7 11 54.72 6.51 -2 -7 -11 62.37 3.52 -2 -7 -11 55.91 6.47 2 7 12 18.69 4.32 -2 -7 -12 14.05 2.12 -2 -7 -12 20.49 4.76 -2 -7 -13 12.92 4.28 2 7 13 13.46 4.50 -2 -7 -14 -7.07 4.83 2 7 14 -5.14 3.51 2 8 -11 14.29 4.96 2 8 -10 -3.87 3.91 2 8 -9 233.98 14.04 2 8 -8 -0.69 3.92 2 8 -7 400.20 17.43 2 8 -6 0.19 1.19 2 8 -6 2.11 3.69 2 8 -5 43.66 2.64 2 8 -5 47.41 6.16 2 8 -4 83.98 3.81 2 8 -4 86.68 7.47 2 8 -3 5.14 3.19 2 8 -2 53.62 5.63 -2 -8 2 54.66 5.49 2 8 -2 59.71 5.53 -2 -8 2 58.29 5.64 -2 -8 2 57.79 3.17 -2 -8 1 53.82 5.26 2 8 -1 51.95 5.46 2 8 -1 57.75 5.11 -2 -8 1 45.85 4.99 -2 -8 1 52.90 2.93 2 8 0 805.72 21.71 2 8 0 790.75 16.77 2 8 0 838.09 20.24 -2 -8 0 773.75 15.31 -2 -8 0 797.56 20.88 -2 -8 -1 617.38 13.42 2 8 1 650.34 18.39 2 8 1 639.23 15.00 2 8 1 650.16 16.64 -2 -8 -1 636.94 17.77 2 8 2 1731.94 35.45 2 8 2 1774.73 32.41 2 8 2 1772.26 32.34 2 8 2 1724.79 30.20 2 8 3 106.73 6.80 2 8 3 116.35 6.28 2 8 3 117.01 5.41 2 8 3 114.82 5.47 2 8 3 110.89 6.80 2 8 4 943.24 22.40 2 8 4 984.49 22.38 2 8 4 923.28 18.14 2 8 4 956.61 22.88 2 8 4 952.28 20.52 2 8 5 6.95 2.29 2 8 5 6.97 2.57 2 8 5 6.84 2.48 2 8 5 9.15 1.37 2 8 5 7.72 2.08 2 8 6 20.21 2.98 2 8 6 23.92 3.60 2 8 6 17.37 2.88 2 8 7 823.07 19.74 2 8 7 808.79 21.28 2 8 7 880.10 23.07 2 8 8 190.88 9.86 2 8 9 53.69 5.78 2 8 10 221.03 11.76 -2 -8 -10 178.76 4.20 2 8 11 132.84 9.74 -2 -8 -11 119.84 3.99 2 8 12 236.69 13.50 2 8 13 53.89 7.25 2 8 14 13.57 4.70 2 9 -10 8.32 4.43 2 9 -9 399.09 19.33 2 9 -8 303.17 16.24 2 9 -7 209.93 13.03 2 9 -6 11.14 4.29 2 9 -5 6.58 4.16 2 9 -5 5.29 1.39 2 9 -4 81.87 7.72 2 9 -3 28.91 5.00 -2 -9 3 27.24 2.50 -2 -9 3 31.32 4.90 2 9 -2 11.04 3.70 -2 -9 2 14.15 1.84 -2 -9 2 10.70 3.43 2 9 -1 62.21 6.23 2 9 -1 63.61 4.03 2 9 -1 70.66 5.98 -2 -9 1 60.51 5.89 -2 -9 1 63.73 3.51 -2 -9 0 12.77 1.83 2 9 0 8.66 2.04 2 9 0 12.19 3.61 2 9 0 10.87 2.69 -2 -9 0 12.76 3.30 -2 -9 -1 101.01 4.79 2 9 1 95.43 7.26 2 9 1 102.80 5.59 2 9 1 102.70 6.36 -2 -9 -1 100.66 7.03 2 9 2 784.75 21.69 2 9 2 798.16 18.92 2 9 2 781.96 18.90 2 9 3 411.67 14.75 2 9 3 427.44 13.37 2 9 3 430.07 12.15 2 9 3 425.76 11.89 2 9 3 438.46 14.83 2 9 4 471.57 15.54 2 9 4 488.44 15.02 2 9 4 464.25 12.00 2 9 4 501.19 15.91 2 9 4 470.15 13.47 2 9 5 64.08 5.52 2 9 5 65.56 5.51 2 9 5 61.10 3.41 2 9 5 59.85 4.88 2 9 5 59.57 5.34 2 9 6 354.97 12.80 2 9 6 365.43 13.74 2 9 6 357.45 8.13 2 9 6 335.41 12.28 2 9 6 360.58 13.66 2 9 7 -2.36 2.68 2 9 7 -0.81 2.13 2 9 8 269.65 10.68 2 9 8 277.06 12.14 2 9 9 284.02 10.88 2 9 9 263.34 12.58 2 9 10 199.29 8.96 2 9 10 199.90 11.46 2 9 11 45.74 6.10 2 9 12 210.61 12.99 2 9 13 1.10 3.45 2 9 14 3.34 3.90 2 10 -8 185.18 13.25 2 10 -7 43.97 6.89 2 10 -6 4.92 4.52 2 10 -5 191.36 12.51 2 10 -4 -0.73 3.74 -2 -10 4 -0.73 3.05 2 10 -3 436.32 17.92 -2 -10 3 420.68 17.29 -2 -10 3 403.05 10.58 2 10 -2 1165.10 22.95 2 10 -2 1175.60 31.46 -2 -10 2 1185.84 30.67 -2 -10 2 1159.10 21.98 2 10 -1 25.94 4.65 2 10 -1 28.02 3.06 -2 -10 1 27.18 2.59 -2 -10 1 28.26 4.50 -2 -10 0 -0.75 1.31 2 10 0 -0.57 1.96 2 10 0 -1.78 3.49 2 10 0 -3.43 2.59 -2 -10 0 -2.56 2.90 -2 -10 -1 3.31 1.53 2 10 1 5.61 3.23 2 10 1 1.70 1.79 2 10 1 2.22 2.10 -2 -10 -1 3.43 2.68 2 10 2 26.10 3.58 2 10 2 29.83 4.84 2 10 2 25.41 3.46 2 10 3 24.49 2.96 2 10 3 25.07 4.34 2 10 3 20.23 3.29 2 10 3 23.00 3.13 2 10 4 236.86 11.40 2 10 4 239.13 10.57 2 10 4 233.36 8.57 2 10 4 234.84 9.27 2 10 5 154.56 9.12 2 10 5 156.37 8.88 2 10 5 154.70 6.21 2 10 5 170.05 8.20 2 10 6 45.16 5.15 2 10 6 54.03 3.09 2 10 6 51.76 4.93 2 10 7 -1.15 2.67 2 10 7 -0.19 2.15 2 10 8 635.71 18.73 2 10 8 626.07 19.77 2 10 9 1000.10 24.86 2 10 9 1035.75 27.80 2 10 10 11.59 3.14 2 10 10 7.15 3.44 2 10 11 21.65 3.53 2 10 11 13.30 4.06 2 10 12 222.94 9.98 2 10 12 244.21 14.06 2 10 13 13.94 4.72 2 11 -7 -0.40 3.84 2 11 -6 23.27 5.93 -2 -11 6 23.09 5.12 2 11 -5 167.49 12.15 -2 -11 5 173.96 12.34 2 11 -4 62.18 7.70 -2 -11 4 70.32 7.88 2 11 -3 71.96 7.95 -2 -11 3 80.29 7.93 2 11 -2 800.44 18.31 2 11 -2 818.28 26.37 -2 -11 2 803.24 25.23 2 11 -1 37.10 6.01 2 11 -1 30.91 3.56 -2 -11 1 32.63 5.00 -2 -11 1 31.43 2.95 2 11 0 120.51 6.66 -2 -11 0 111.30 5.45 2 11 0 115.42 9.19 -2 -11 0 121.73 8.85 2 11 1 59.57 6.73 2 11 1 54.76 4.82 2 11 1 55.58 5.43 -2 -11 -1 46.84 5.64 2 11 2 27.30 4.94 2 11 2 17.76 3.25 2 11 2 23.44 3.70 2 11 3 57.20 6.26 2 11 3 61.94 5.45 2 11 3 56.42 4.89 2 11 4 344.47 14.80 2 11 4 369.36 13.90 2 11 4 369.66 11.79 2 11 4 349.21 12.08 2 11 5 152.98 9.64 2 11 5 170.66 7.11 2 11 5 165.32 8.46 2 11 6 141.50 9.08 2 11 6 145.52 5.85 2 11 6 145.54 8.31 2 11 7 6.67 3.05 2 11 7 2.64 2.84 2 11 7 7.98 1.36 2 11 8 99.72 7.55 2 11 8 104.81 7.84 2 11 9 212.07 10.72 2 11 9 224.44 12.04 2 11 10 33.00 4.43 2 11 10 27.75 4.92 2 11 11 54.30 5.51 2 11 11 39.02 5.93 2 11 12 16.21 4.86 2 11 13 54.81 7.33 2 12 -5 468.81 21.58 -2 -12 5 492.98 21.80 2 12 -4 4.82 4.17 -2 -12 4 -1.56 3.60 2 12 -3 10.18 4.45 -2 -12 3 3.27 3.54 2 12 -2 209.68 13.42 -2 -12 2 203.62 12.72 2 12 -1 16.59 4.90 -2 -12 1 12.05 4.10 2 12 0 51.43 4.74 2 12 0 44.72 6.62 -2 -12 0 41.28 5.69 2 12 1 3.48 3.46 2 12 1 2.02 2.34 -2 -12 -1 -0.17 3.17 2 12 2 163.11 11.02 2 12 2 170.25 9.36 2 12 2 168.11 8.99 2 12 3 37.29 4.42 2 12 3 30.82 4.24 2 12 3 35.02 5.63 2 12 4 260.23 13.50 2 12 4 261.40 10.42 2 12 5 557.28 20.02 2 12 5 568.65 15.18 2 12 5 541.99 16.87 2 12 6 355.11 15.49 2 12 6 349.50 10.41 2 12 6 339.23 13.50 2 12 7 96.77 7.97 2 12 7 100.51 7.42 2 12 8 24.67 4.62 2 12 8 19.85 3.66 2 12 9 143.86 9.40 2 12 9 142.87 9.67 2 12 10 17.02 3.81 2 12 10 24.07 4.78 2 12 11 3.47 2.64 2 12 11 6.72 3.76 2 12 12 19.52 5.28 2 13 -3 0.70 3.74 -2 -13 3 1.54 3.56 2 13 -2 60.08 7.86 -2 -13 2 55.83 7.39 2 13 -1 4.74 3.95 -2 -13 1 0.39 3.15 2 13 0 3.97 4.27 -2 -13 0 -0.95 3.16 2 13 1 348.27 17.40 2 13 2 5.03 4.04 2 13 3 44.91 6.32 2 13 4 84.98 8.54 2 13 5 36.46 5.93 2 13 5 25.15 3.74 2 13 6 6.05 3.63 2 13 6 2.03 2.21 2 13 7 0.82 3.16 2 13 7 -5.59 3.04 2 13 8 48.82 6.27 2 13 8 46.93 5.73 2 13 9 22.03 4.44 2 13 9 20.31 4.22 2 13 10 14.68 3.89 2 13 10 -0.26 4.20 2 13 11 10.60 3.06 2 13 11 2.54 3.99 2 13 12 203.40 13.56 -2 -14 2 3.79 3.65 2 14 -1 21.13 5.69 -2 -14 1 26.31 5.57 2 14 0 22.64 5.73 -2 -14 0 19.15 5.21 2 14 1 470.76 21.45 2 14 2 216.76 14.18 2 14 3 -0.25 3.77 2 14 4 104.43 9.86 2 14 5 25.30 5.76 2 14 6 9.29 4.06 2 14 6 9.38 3.00 2 14 7 26.68 5.41 2 14 7 29.73 4.76 2 14 8 1.39 3.56 2 14 8 -1.06 3.27 2 14 9 112.62 9.66 2 14 9 110.24 9.09 2 14 10 25.28 5.05 2 14 10 28.30 5.13 2 14 11 -5.89 4.38 2 15 2 27.25 6.06 2 15 3 74.09 9.04 2 15 4 -0.82 3.73 2 15 5 22.97 5.66 2 15 6 246.52 15.08 2 15 7 -5.16 3.86 2 15 7 8.29 4.39 2 15 8 67.71 7.18 2 15 8 83.77 8.85 2 15 9 -6.20 3.93 2 15 9 1.85 3.71 2 15 10 4.44 3.23 2 15 10 19.24 5.21 2 16 7 48.51 7.94 2 16 8 6.23 4.05 2 16 9 10.54 4.77 -3 13 5 162.31 13.06 -3 13 4 89.94 10.02 3 -13 -4 91.33 8.19 -3 13 3 36.16 6.59 -3 13 2 34.62 6.56 -3 13 1 20.93 6.09 -3 13 0 2.98 4.18 3 -13 2 65.73 7.60 3 -13 3 24.01 5.38 3 -13 4 37.25 6.20 -3 12 8 151.79 11.96 -3 12 7 25.27 5.67 -3 12 6 40.61 6.43 3 -12 -5 174.67 10.51 3 -12 -4 66.59 6.59 -3 12 3 107.95 10.36 3 -12 -3 111.86 8.87 -3 12 2 -0.94 3.90 -3 12 1 20.15 5.67 -3 12 0 -2.38 3.68 -3 12 -1 1.37 3.59 3 -12 1 3.20 3.04 -3 12 -2 147.21 12.25 3 -12 2 122.37 9.52 -3 12 -3 172.60 13.02 3 -12 3 157.01 11.06 -3 12 -4 36.31 6.96 3 -12 4 31.88 5.48 3 -12 5 3.65 3.74 3 -12 6 45.85 7.20 -3 11 9 5.14 3.77 -3 11 8 228.20 14.08 -3 11 7 35.23 6.00 3 -11 -7 28.17 4.34 -3 11 6 2.73 3.39 3 -11 -6 2.16 2.43 -3 11 5 4.28 3.59 3 -11 -5 5.19 2.68 3 -11 -4 182.40 10.54 3 -11 -3 27.17 4.66 3 -11 -2 17.96 4.30 -3 11 1 11.96 4.75 3 -11 -1 25.40 4.60 -3 11 0 -6.41 4.60 -3 11 -1 -1.20 3.57 3 -11 1 -5.82 3.41 -3 11 -2 162.79 12.09 3 -11 2 156.13 10.06 -3 11 -3 558.63 22.92 3 -11 3 529.97 19.67 -3 11 -4 20.72 5.66 3 -11 4 19.39 4.69 -3 11 -5 9.46 5.19 3 -11 5 11.12 4.28 -3 11 -6 6.28 4.69 3 -11 6 -0.37 3.25 -3 11 -7 158.27 12.81 3 -11 7 156.81 11.99 -3 10 10 24.15 5.48 -3 10 9 -3.36 3.87 -3 10 8 79.65 8.37 3 -10 -8 66.63 6.05 -3 10 7 1.48 3.24 3 -10 -7 1.09 2.36 -3 10 6 0.48 3.00 3 -10 -6 0.43 2.21 -3 10 5 12.18 4.00 3 -10 -5 14.99 3.41 -3 10 5 13.81 3.26 -3 10 5 12.06 2.92 3 -10 -4 430.70 16.03 -3 10 4 463.35 17.56 3 -10 -3 189.93 10.47 3 -10 -2 39.86 5.22 3 -10 -1 4.44 2.97 -3 10 0 55.31 7.01 3 -10 0 66.97 6.74 -3 10 -1 9.26 4.01 3 -10 1 3.21 2.48 -3 10 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34.32 6.15 -3 9 -10 -6.24 4.37 -3 9 -11 4.60 4.70 -3 8 11 30.21 6.11 -3 8 10 10.95 4.26 3 -8 -10 14.33 3.48 -3 8 9 15.43 4.66 3 -8 -9 15.71 3.46 3 -8 -8 108.33 7.27 -3 8 8 128.77 9.87 3 -8 -7 263.30 11.45 -3 8 7 295.31 14.27 -3 8 7 276.88 11.38 3 -8 -6 213.06 10.18 -3 8 6 238.41 10.27 -3 8 6 227.96 12.08 -3 8 6 224.16 9.76 -3 8 5 5.77 3.19 3 -8 -5 10.05 3.07 -3 8 5 9.27 2.69 -3 8 5 10.20 2.64 3 -8 -4 83.33 6.32 -3 8 4 100.94 6.65 -3 8 4 89.24 5.87 -3 8 4 105.50 7.73 3 -8 -3 279.97 11.90 -3 8 3 337.68 12.55 -3 8 3 336.42 13.39 3 -8 -2 14.51 3.34 -3 8 2 12.58 2.85 3 -8 -2 9.04 2.89 3 -8 -1 217.06 10.53 -3 8 1 218.24 10.49 3 -8 -1 215.89 10.31 3 -8 0 210.86 10.73 -3 8 0 222.45 10.79 3 -8 0 222.65 10.29 3 -8 0 217.59 9.35 -3 8 -1 129.43 8.56 3 -8 1 123.15 8.31 3 -8 1 136.39 7.55 3 -8 1 129.13 7.82 -3 8 -2 135.80 9.39 3 -8 2 141.17 9.05 3 -8 2 141.50 8.08 3 -8 2 157.14 8.48 -3 8 -3 848.91 25.19 3 -8 3 855.05 22.24 3 -8 3 811.77 22.28 -3 8 -4 49.73 6.12 3 -8 4 43.25 4.69 -3 8 -5 10.45 4.11 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2.66 4 14 9 186.19 11.36 4 14 9 200.66 11.39 4 14 10 15.08 4.07 4 14 10 21.59 4.70 4 14 11 -0.57 3.36 4 14 12 172.18 11.97 4 14 13 204.01 13.71 4 15 1 83.43 9.61 4 15 2 111.87 10.58 4 15 3 257.64 15.62 4 15 4 47.65 7.11 4 15 5 43.05 6.82 4 15 6 0.54 3.72 4 15 7 0.34 3.59 4 15 8 1.34 3.67 4 15 8 3.07 2.66 4 15 9 192.16 12.48 4 15 9 196.87 11.41 4 15 10 29.74 5.22 4 15 10 21.59 4.87 4 15 11 11.86 4.46 4 15 12 29.84 5.30 4 16 4 6.09 4.06 4 16 5 13.70 4.87 4 16 6 79.94 9.33 4 16 7 47.19 7.35 4 16 8 55.75 7.76 4 16 9 321.02 16.86 5 -13 -3 99.42 9.81 5 -13 -2 27.38 5.99 5 -12 -4 21.64 5.19 5 -12 -3 42.80 6.50 5 -12 -2 27.19 5.63 5 -12 -1 11.30 4.72 5 -12 0 -1.11 3.46 5 -12 3 194.36 11.86 5 -12 4 66.71 7.65 5 -12 5 22.57 5.02 5 -12 6 2.39 4.17 5 -11 -6 113.65 9.37 5 -11 -5 3.31 3.22 5 -11 -4 0.67 3.12 5 -11 -3 88.09 8.36 5 -11 -2 -2.85 3.46 5 -11 -1 80.78 8.04 5 -11 0 130.80 10.41 -5 11 -1 30.43 6.24 5 -11 1 28.24 5.41 -5 11 -2 7.40 4.70 5 -11 2 10.82 3.58 -5 11 -3 137.78 11.95 5 -11 3 150.10 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79.98 7.07 10 1 0 1.49 3.01 -10 -1 0 1.02 2.57 10 1 1 567.50 19.33 -10 -1 -1 473.55 15.78 10 1 2 315.14 13.99 -10 -1 -2 262.33 10.60 10 1 3 139.85 9.31 10 1 4 102.33 7.81 10 1 4 89.72 3.52 10 1 5 109.19 8.14 10 1 6 361.66 14.91 10 1 7 49.62 5.75 10 1 8 16.76 3.91 10 1 9 240.20 12.29 10 1 10 92.26 7.99 -10 -1 -11 -2.31 1.88 10 1 11 -1.39 3.08 -10 -1 -12 470.84 20.07 -10 -1 -12 477.43 15.19 -10 -1 -13 31.56 6.46 -10 -1 -14 5.63 4.04 -10 -2 8 62.55 7.49 -10 -2 7 12.37 4.33 -10 -2 6 20.25 4.60 10 2 -6 25.67 5.63 -10 -2 5 45.34 5.66 10 2 -5 54.12 7.36 10 2 -4 4.95 3.40 -10 -2 4 1.51 1.74 10 2 -3 94.47 8.68 -10 -2 3 96.86 4.92 10 2 -2 1227.19 33.31 -10 -2 1 16.61 4.11 10 2 -1 9.94 3.65 10 2 0 24.47 3.87 10 2 0 23.49 4.47 -10 -2 0 24.76 4.21 10 2 1 785.40 23.50 -10 -2 -1 685.64 19.14 10 2 1 779.96 20.81 10 2 2 42.58 4.67 10 2 2 41.51 5.34 -10 -2 -2 39.07 4.13 10 2 3 3.38 2.42 10 2 3 -0.63 2.75 -10 -2 -3 1.94 1.93 10 2 4 9.40 3.21 10 2 4 14.40 1.75 -10 -2 -4 11.88 2.15 10 2 5 543.79 18.20 10 2 6 129.30 8.57 10 2 7 11.86 3.48 10 2 8 62.79 6.37 10 2 9 498.70 17.57 -10 -2 -10 62.80 7.39 10 2 10 54.61 5.83 -10 -2 -10 64.55 4.26 -10 -2 -11 4.66 3.93 10 2 11 3.92 2.93 -10 -2 -11 8.39 2.57 -10 -2 -12 675.48 24.30 -10 -2 -12 688.39 17.68 -10 -2 -13 77.71 8.59 -10 -2 -14 1.85 4.05 -10 -2 -15 87.05 9.83 -10 -3 7 -0.87 3.22 10 3 -6 153.12 12.12 -10 -3 6 158.79 10.13 10 3 -5 82.09 8.98 -10 -3 5 68.91 5.70 10 3 -4 156.03 11.46 -10 -3 4 149.88 7.54 10 3 -3 2.90 3.26 -10 -3 3 2.81 1.76 10 3 -2 677.23 19.91 10 3 -2 725.27 24.08 -10 -3 2 732.02 16.60 10 3 -1 134.77 9.58 10 3 -1 144.57 8.17 10 3 0 66.82 6.74 10 3 0 68.55 5.64 10 3 1 124.42 8.73 10 3 1 125.78 7.28 10 3 2 4.28 2.36 10 3 2 4.67 3.37 -10 -3 -3 37.74 4.98 10 3 3 39.28 5.03 10 3 3 43.50 4.50 -10 -3 -3 48.76 3.97 -10 -3 -4 605.67 18.93 10 3 4 660.08 19.74 10 3 4 598.36 13.83 -10 -3 -4 606.53 13.49 -10 -3 -4 640.32 19.49 10 3 5 44.00 5.03 -10 -3 -5 35.12 4.51 -10 -3 -5 45.12 2.68 10 3 6 2.48 2.48 -10 -3 -6 0.79 2.08 10 3 7 102.69 7.37 -10 -3 -7 94.64 7.12 -10 -3 -8 23.67 3.95 10 3 8 24.59 4.23 -10 -3 -9 106.06 8.73 10 3 9 90.90 7.02 -10 -3 -9 83.65 6.75 -10 -3 -9 77.63 2.76 -10 -3 -10 11.18 4.48 -10 -3 -10 7.60 2.90 10 3 10 2.12 2.34 -10 -3 -10 -0.96 1.48 -10 -3 -11 195.77 7.14 -10 -3 -11 237.14 13.27 10 3 11 227.44 11.22 -10 -3 -11 231.03 7.43 -10 -3 -12 13.80 4.84 10 3 12 15.84 3.82 -10 -3 -12 7.32 2.00 -10 -3 -13 38.79 6.61 -10 -3 -14 126.83 10.82 -10 -3 -15 133.78 11.48 -10 -4 6 22.77 4.08 10 4 -6 16.20 4.91 10 4 -5 41.50 6.58 -10 -4 5 36.64 4.58 10 4 -4 20.95 4.73 -10 -4 4 16.73 3.21 -10 -4 3 67.55 5.30 10 4 -3 62.37 7.36 10 4 -2 41.45 6.20 -10 -4 2 36.31 3.72 10 4 -1 3.13 2.00 10 4 -1 -1.59 3.34 -10 -4 1 0.83 1.72 10 4 0 547.21 19.42 10 4 0 547.19 15.89 10 4 1 33.34 3.87 10 4 1 40.31 5.40 10 4 2 601.59 19.30 10 4 2 565.34 16.06 -10 -4 -3 1959.14 41.49 10 4 3 2045.07 41.83 10 4 3 1961.44 37.88 -10 -4 -4 242.91 11.32 10 4 4 240.22 11.15 10 4 4 231.07 8.22 -10 -4 -5 210.77 10.17 10 4 5 225.65 10.66 -10 -4 -5 214.20 10.42 10 4 5 218.54 8.27 -10 -4 -6 20.95 3.58 10 4 6 25.02 3.93 -10 -4 -6 26.58 4.19 -10 -4 -7 335.31 11.97 -10 -4 -7 318.52 12.72 10 4 7 357.52 13.32 -10 -4 -8 62.96 4.82 10 4 8 63.61 5.60 -10 -4 -8 58.00 5.46 -10 -4 -8 73.26 7.03 -10 -4 -9 103.18 5.67 -10 -4 -9 114.26 7.46 10 4 9 117.11 7.58 -10 -4 -9 122.25 9.01 -10 -4 -10 229.76 7.85 10 4 10 240.82 10.99 -10 -4 -10 229.57 10.72 -10 -4 -10 251.36 13.12 -10 -4 -11 3.84 1.24 -10 -4 -11 7.89 3.97 -10 -4 -11 0.75 2.41 10 4 11 5.06 2.82 -10 -4 -12 62.82 7.51 -10 -4 -12 52.47 5.79 10 4 12 59.68 5.75 -10 -4 -13 271.31 15.17 -10 -4 -14 359.22 18.18 -10 -4 -15 45.74 7.42 10 5 -6 26.73 5.98 -10 -5 6 30.52 5.21 10 5 -5 -0.25 3.55 -10 -5 5 3.29 2.93 -10 -5 4 80.40 6.51 10 5 -4 93.50 9.28 10 5 -3 12.88 4.09 -10 -5 3 12.66 2.86 10 5 -2 10.19 3.74 -10 -5 2 17.18 3.12 10 5 -1 1.70 2.11 10 5 -1 1.41 2.77 -10 -5 1 3.83 1.97 10 5 0 39.32 3.89 10 5 0 48.67 5.88 10 5 1 69.25 6.70 10 5 1 68.03 4.90 10 5 2 285.43 12.83 10 5 2 274.96 10.02 -10 -5 -3 1887.92 40.19 10 5 3 1985.85 40.23 10 5 3 1833.03 35.43 -10 -5 -4 4.72 3.13 10 5 4 1.58 2.38 10 5 4 6.45 2.13 -10 -5 -5 214.00 10.14 10 5 5 229.05 10.44 10 5 5 211.66 8.62 -10 -5 -6 224.90 9.97 10 5 6 247.38 10.72 -10 -5 -6 221.85 10.22 -10 -5 -7 6.39 2.29 -10 -5 -7 14.72 4.24 10 5 7 7.67 2.54 -10 -5 -7 8.58 2.63 -10 -5 -8 346.72 11.34 10 5 8 374.26 13.19 -10 -5 -8 322.16 12.38 -10 -5 -8 365.58 14.65 -10 -5 -9 973.52 20.71 -10 -5 -9 1007.13 27.25 10 5 9 1055.74 24.52 -10 -5 -9 919.54 23.44 -10 -5 -10 43.75 3.20 -10 -5 -10 47.22 6.25 10 5 10 57.32 5.26 -10 -5 -10 43.44 4.68 -10 -5 -11 0.27 3.52 -10 -5 -11 1.09 0.89 10 5 11 0.29 2.03 -10 -5 -11 -3.27 2.72 -10 -5 -12 -0.05 4.32 10 5 12 4.66 2.33 -10 -5 -12 1.16 2.23 -10 -5 -13 14.23 4.78 -10 -5 -14 67.30 8.21 -10 -5 -15 101.03 9.89 -10 -6 6 5.77 3.53 10 6 -5 257.34 15.63 -10 -6 5 228.63 12.22 10 6 -4 12.09 4.52 -10 -6 4 16.62 3.74 10 6 -3 125.97 10.09 -10 -6 3 109.31 7.59 -10 -6 2 839.52 22.37 10 6 -2 875.35 27.23 10 6 -1 441.49 18.04 -10 -6 1 459.23 14.97 10 6 0 360.11 11.08 10 6 0 375.97 15.84 10 6 1 5.37 1.84 10 6 1 4.96 2.72 10 6 2 171.95 9.84 10 6 2 167.14 7.11 10 6 3 50.41 5.38 10 6 3 41.02 3.71 -10 -6 -4 103.63 7.54 -10 -6 -4 103.35 6.70 10 6 4 101.45 7.14 10 6 4 95.95 6.04 -10 -6 -5 162.96 8.78 -10 -6 -5 175.59 8.95 10 6 5 170.79 8.93 10 6 5 164.86 7.98 -10 -6 -6 51.52 4.97 -10 -6 -6 62.40 5.93 10 6 6 64.97 5.47 10 6 6 60.23 5.09 -10 -6 -7 8.93 2.39 -10 -6 -7 10.93 3.66 10 6 7 3.90 2.10 -10 -6 -8 12.08 2.63 -10 -6 -8 10.54 3.68 10 6 8 8.09 2.63 -10 -6 -8 6.47 2.17 -10 -6 -9 1234.42 24.41 10 6 9 1303.39 27.46 -10 -6 -9 1165.05 26.46 -10 -6 -9 1218.54 30.82 -10 -6 -10 320.01 8.90 -10 -6 -10 354.95 15.37 10 6 10 349.41 11.99 -10 -6 -10 300.92 11.37 -10 -6 -11 27.61 1.62 -10 -6 -11 36.43 5.70 10 6 11 37.55 4.00 -10 -6 -11 31.36 3.68 -10 -6 -12 81.13 8.16 -10 -6 -12 81.78 5.93 -10 -6 -13 19.89 5.08 -10 -6 -14 61.07 7.74 -10 -6 -15 28.83 6.15 -10 -7 7 18.54 4.85 -10 -7 6 2.06 3.45 -10 -7 5 362.97 16.24 10 7 -5 407.79 19.93 10 7 -5 331.40 17.82 10 7 -4 23.57 5.32 10 7 -4 21.47 5.18 -10 -7 4 25.44 4.85 10 7 -3 45.34 6.79 10 7 -3 49.40 6.30 -10 -7 3 45.80 5.64 -10 -7 2 200.50 10.51 10 7 -2 191.07 12.32 10 7 -2 186.30 11.18 -10 -7 1 185.59 5.44 10 7 -1 216.21 12.41 10 7 -1 203.54 10.97 -10 -7 1 204.23 10.22 -10 -7 0 120.01 5.02 10 7 0 121.74 7.93 -10 -7 0 131.99 7.89 10 7 0 113.24 8.72 10 7 1 125.03 5.45 -10 -7 -1 118.58 5.63 10 7 1 119.53 8.70 10 7 1 123.72 7.38 -10 -7 -2 5.26 2.39 10 7 2 2.00 1.65 10 7 2 4.01 2.85 10 7 2 -0.13 2.55 -10 -7 -3 129.28 6.76 10 7 3 122.09 8.07 10 7 3 115.20 5.55 -10 -7 -4 138.68 8.57 -10 -7 -4 135.98 7.26 10 7 4 135.46 8.24 10 7 4 134.52 7.58 -10 -7 -5 208.62 10.20 -10 -7 -5 198.85 9.36 10 7 5 213.06 9.83 10 7 5 200.36 9.48 -10 -7 -6 1328.50 29.55 -10 -7 -6 1313.70 29.83 10 7 6 1368.92 29.21 10 7 6 1353.85 29.96 -10 -7 -7 24.03 4.18 -10 -7 -7 22.77 3.29 10 7 7 21.26 3.07 10 7 7 17.82 3.17 -10 -7 -8 186.71 8.21 10 7 8 195.10 8.56 -10 -7 -8 188.86 10.35 -10 -7 -9 267.56 9.27 -10 -7 -9 279.23 13.12 10 7 9 302.92 10.63 -10 -7 -10 53.28 3.50 -10 -7 -10 45.33 5.95 10 7 10 54.62 4.40 -10 -7 -10 43.05 3.96 -10 -7 -11 98.82 8.41 10 7 11 110.23 6.00 -10 -7 -11 95.90 5.74 -10 -7 -12 -0.79 3.52 -10 -7 -13 32.56 5.89 -10 -7 -14 26.87 5.61 -10 -7 -15 135.25 11.28 -10 -8 6 3.93 4.07 -10 -8 5 736.48 24.96 10 8 -5 712.85 27.01 -10 -8 4 306.54 15.00 10 8 -4 316.02 16.62 -10 -8 3 65.32 6.85 10 8 -3 60.77 7.31 -10 -8 2 3.75 2.72 10 8 -2 6.77 3.64 10 8 -1 -1.26 3.45 -10 -8 1 3.93 2.58 10 8 -1 2.16 3.31 10 8 0 167.62 10.71 10 8 0 171.68 9.83 -10 -8 0 160.12 9.44 -10 -8 -1 9.61 1.66 10 8 1 4.27 2.88 10 8 1 9.42 3.38 -10 -8 -2 8.64 1.83 10 8 2 13.94 1.82 10 8 2 9.56 3.06 10 8 2 9.31 2.81 -10 -8 -3 1.79 1.97 10 8 3 8.00 1.78 10 8 3 7.58 3.21 10 8 3 6.46 2.25 -10 -8 -4 56.22 4.56 10 8 4 61.64 5.64 10 8 4 63.60 4.11 10 8 4 59.96 3.87 -10 -8 -5 167.44 9.34 -10 -8 -5 161.90 8.19 10 8 5 170.93 8.75 10 8 5 172.18 9.11 10 8 5 166.74 5.37 -10 -8 -6 1409.19 31.50 -10 -8 -6 1421.48 31.14 10 8 6 1487.87 30.64 10 8 6 1403.99 32.04 -10 -8 -7 767.16 20.33 10 8 7 827.45 19.78 -10 -8 -7 744.68 21.39 10 8 8 3.45 1.83 -10 -8 -8 -0.36 1.94 -10 -8 -9 266.74 9.51 10 8 9 281.60 9.76 -10 -8 -9 266.01 12.74 -10 -8 -10 122.54 5.54 -10 -8 -10 116.44 8.84 10 8 10 120.89 5.96 -10 -8 -11 37.31 6.03 10 8 11 28.08 2.98 -10 -8 -12 82.05 8.19 -10 -8 -13 40.12 6.57 -10 -8 -14 165.44 12.19 -10 -8 -15 2.47 3.98 -10 -9 6 53.12 7.70 -10 -9 5 153.09 11.45 10 9 -5 138.05 12.15 -10 -9 4 213.66 13.08 10 9 -4 208.98 14.06 -10 -9 3 27.82 5.23 10 9 -3 23.43 5.31 10 9 -2 124.39 9.81 -10 -9 2 102.27 8.55 -10 -9 1 45.73 5.70 10 9 -1 48.03 6.10 10 9 0 62.15 6.45 -10 -9 0 61.83 6.40 10 9 1 287.45 14.80 10 9 1 266.48 13.35 10 9 1 293.27 12.44 -10 -9 -2 440.52 10.61 10 9 2 444.31 18.10 10 9 2 441.16 14.63 10 9 2 446.49 16.74 -10 -9 -3 13.79 2.42 10 9 3 16.89 1.54 10 9 3 21.97 4.71 10 9 3 17.13 3.60 10 9 3 18.28 3.48 10 9 4 63.43 6.50 -10 -9 -4 60.99 4.67 10 9 4 60.79 5.62 10 9 4 58.91 3.36 10 9 4 60.01 4.52 -10 -9 -5 3.92 2.00 10 9 5 8.48 2.62 10 9 5 10.58 2.25 -10 -9 -6 -4.42 3.17 -10 -9 -6 -2.72 2.70 10 9 6 0.34 1.94 10 9 6 5.11 1.56 10 9 7 28.95 3.54 -10 -9 -7 14.15 2.89 -10 -9 -7 19.94 3.72 -10 -9 -8 196.79 9.04 10 9 8 207.62 8.28 -10 -9 -8 198.69 10.49 -10 -9 -9 49.58 4.30 -10 -9 -9 39.67 5.27 10 9 9 48.56 3.76 -10 -9 -10 0.43 1.47 -10 -9 -10 0.62 3.17 10 9 10 1.84 1.55 -10 -9 -11 147.05 10.37 -10 -9 -12 363.04 16.85 -10 -9 -13 498.29 20.71 -10 -9 -14 3.02 3.76 -10 -9 -15 49.81 7.31 -10 -10 5 28.23 5.93 -10 -10 4 20.76 5.33 10 10 -4 13.31 4.99 -10 -10 3 205.90 13.02 10 10 -3 212.14 13.74 -10 -10 2 3.38 3.12 10 10 -2 3.47 3.90 10 10 -1 6.85 4.86 -10 -10 1 1.74 3.29 10 10 -1 8.12 4.45 10 10 0 348.13 17.31 10 10 0 352.00 15.20 -10 -10 0 343.91 15.44 10 10 1 79.37 8.41 10 10 1 84.03 7.32 10 10 2 693.79 23.69 10 10 2 659.73 21.60 10 10 2 721.15 20.49 -10 -10 -3 139.22 5.73 10 10 3 152.36 10.48 10 10 3 132.96 8.69 10 10 4 299.32 14.00 -10 -10 -4 296.40 9.96 10 10 4 300.98 12.49 10 10 4 275.28 6.02 10 10 5 136.91 9.26 10 10 5 127.58 7.66 -10 -10 -5 131.11 7.01 10 10 6 62.59 6.28 10 10 6 58.29 4.99 -10 -10 -6 48.08 4.74 10 10 7 31.50 4.66 -10 -10 -7 34.34 4.31 -10 -10 -7 28.18 4.15 10 10 7 29.01 3.46 -10 -10 -8 8.86 2.74 -10 -10 -8 3.89 2.61 10 10 8 4.48 1.82 -10 -10 -9 0.22 2.04 -10 -10 -9 3.48 2.94 10 10 9 1.07 1.52 -10 -10 -10 22.29 4.47 10 10 10 15.90 1.82 -10 -10 -11 131.41 9.85 -10 -10 -12 42.16 6.37 -10 -10 -13 137.94 10.94 -10 -10 -14 27.08 5.52 -10 -10 -15 -2.77 3.98 10 11 -4 36.84 7.44 10 11 -3 101.53 9.99 -10 -11 3 91.05 9.12 10 11 -2 33.28 6.87 -10 -11 2 28.60 5.60 10 11 -2 28.69 6.16 10 11 -1 165.48 12.76 10 11 -1 180.92 12.14 -10 -11 1 158.18 11.41 10 11 0 257.46 15.24 10 11 0 250.57 13.48 -10 -11 0 248.49 13.73 10 11 1 74.37 8.69 10 11 2 3.50 3.72 10 11 3 275.25 14.46 10 11 3 275.14 12.92 -10 -11 -4 20.83 2.63 10 11 4 22.11 4.95 10 11 4 19.65 3.46 -10 -11 -5 3.52 1.78 10 11 5 2.50 0.96 10 11 5 4.97 3.23 10 11 5 0.00 2.29 10 11 6 519.78 18.57 10 11 6 534.51 15.94 -10 -11 -6 524.83 16.05 10 11 7 193.71 10.58 10 11 7 202.05 8.54 -10 -11 -7 190.72 9.82 10 11 8 34.06 4.48 10 11 8 39.62 3.43 -10 -11 -8 36.10 4.85 -10 -11 -8 38.72 4.63 -10 -11 -9 220.35 11.65 -10 -11 -9 228.13 10.28 10 11 9 235.18 10.65 -10 -11 -10 307.50 14.58 -10 -11 -11 73.49 7.70 -10 -11 -12 3.07 3.80 -10 -11 -13 70.24 8.07 -10 -11 -14 39.54 8.40 10 12 -3 87.44 9.76 -10 -12 2 9.81 4.08 10 12 -2 9.13 5.44 10 12 -1 189.59 14.04 10 12 -1 160.75 11.85 -10 -12 1 150.80 11.61 10 12 0 6.33 4.48 -10 -12 0 -5.05 4.21 10 12 1 6.06 4.56 10 12 2 1.34 4.08 10 12 3 263.16 14.75 10 12 3 275.78 13.14 10 12 4 102.41 9.02 10 12 4 99.13 7.39 -10 -12 -5 42.82 3.94 10 12 5 46.57 6.50 10 12 5 41.32 4.78 10 12 6 324.24 14.86 10 12 6 333.37 12.20 -10 -12 -6 312.04 11.92 10 12 7 626.36 15.29 10 12 7 671.63 21.41 10 12 7 658.68 16.90 -10 -12 -7 616.68 18.83 -10 -12 -8 50.70 5.57 10 12 8 75.62 6.79 -10 -12 -9 15.25 3.91 10 12 9 19.46 3.95 -10 -12 -10 -4.60 3.79 10 12 10 0.38 2.49 -10 -12 -11 3.13 3.05 -10 -12 -12 22.07 5.15 -10 -12 -13 10.59 4.27 -10 -12 -14 91.59 9.49 10 13 -2 160.58 12.99 10 13 1 150.22 12.22 10 13 2 23.15 5.81 10 13 3 468.13 20.57 10 13 4 311.94 16.21 10 13 4 314.34 13.65 10 13 5 282.32 14.98 10 13 5 284.34 12.20 10 13 6 35.38 5.69 10 13 6 31.40 4.04 10 13 7 51.25 6.19 -10 -13 -7 48.88 5.02 10 13 8 67.40 6.91 -10 -13 -8 67.61 6.30 10 13 9 35.26 5.24 -10 -13 -9 35.21 5.23 10 13 10 89.12 7.01 -10 -13 -10 76.70 7.59 -10 -13 -11 -0.31 3.32 -10 -13 -12 109.37 9.71 -10 -13 -13 361.27 18.11 10 14 2 11.30 5.32 10 14 3 224.38 14.69 10 14 4 335.59 17.45 10 14 5 0.10 3.89 10 14 6 13.21 4.74 10 14 7 63.68 7.53 10 14 8 58.48 6.86 10 14 9 56.84 6.61 -10 -14 -9 43.84 5.60 -10 -14 -10 328.50 15.61 -10 -14 -11 3.87 3.69 -10 -14 -12 4.13 3.47 10 14 13 19.55 4.89 -10 -14 -13 25.76 5.74 10 14 14 -0.91 3.47 10 15 4 5.61 4.33 10 15 5 10.73 4.90 10 15 6 15.90 5.21 10 15 7 144.50 11.27 10 15 8 7.60 4.17 10 15 9 79.20 8.05 -10 -15 -12 24.41 5.40 10 16 6 18.31 5.46 10 16 7 145.92 11.64 10 16 8 13.83 5.00 11 -6 -1 2.05 4.81 11 -6 0 0.73 3.52 11 -6 1 15.43 5.42 11 -6 2 33.68 6.50 11 -6 3 12.57 4.88 11 -6 4 25.73 5.99 -11 6 -9 240.67 15.16 -11 6 -10 9.38 4.66 11 -5 -3 141.39 12.14 11 -5 -2 409.28 20.34 11 -5 -1 11.18 4.60 11 -5 0 51.44 7.78 11 -5 1 13.31 4.78 11 -5 2 -1.23 3.64 11 -5 3 114.34 10.87 11 -5 4 16.89 5.04 11 -5 5 64.47 8.41 11 -5 6 75.43 8.90 11 -5 7 29.65 6.97 -11 5 -9 272.06 15.44 -11 5 -10 24.32 5.57 11 -4 -4 66.29 8.65 11 -4 -3 0.31 3.62 11 -4 -2 7.33 4.41 11 -4 -1 107.26 10.40 11 -4 0 36.45 6.49 11 -4 1 93.63 9.51 11 -4 2 14.39 4.83 11 -4 3 269.63 15.56 11 -4 4 260.02 15.50 11 -4 5 329.05 17.42 11 -4 6 360.97 18.56 11 -4 7 11.17 4.53 11 -4 8 4.25 3.62 11 -4 9 84.58 9.33 -11 4 -10 23.27 5.29 11 -3 -4 3.66 3.52 11 -3 -3 -6.69 4.24 11 -3 -2 14.74 4.86 11 -3 -1 250.60 15.04 11 -3 0 43.93 6.82 11 -3 1 575.27 22.73 11 -3 2 21.95 5.53 11 -3 3 6.96 4.03 11 -3 4 23.02 5.24 11 -3 5 3.84 3.60 11 -3 6 61.80 7.72 11 -3 7 0.68 3.70 11 -3 8 6.10 4.34 11 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593.43 21.47 11 0 4 16.59 4.20 11 0 5 283.68 14.47 11 0 6 852.68 26.31 11 0 7 3.26 3.58 11 0 8 6.60 3.31 11 0 9 7.59 4.02 11 0 10 106.77 9.25 11 0 11 4.42 3.51 -11 0 -12 65.50 8.55 11 0 12 52.68 7.12 -11 0 -13 0.10 3.84 11 1 -5 201.54 14.10 11 1 -4 8.43 4.28 11 1 -3 66.59 7.94 11 1 -2 48.87 7.05 11 1 -1 2.54 3.34 11 1 0 162.84 11.04 -11 -1 0 141.66 9.19 11 1 1 50.04 6.45 -11 -1 -1 43.76 5.12 11 1 2 315.35 14.86 -11 -1 -2 266.70 11.43 11 1 3 330.28 15.03 -11 -1 -3 266.52 10.79 11 1 4 294.92 14.25 11 1 5 125.91 9.35 11 1 6 165.54 10.62 11 1 7 25.82 4.76 11 1 8 51.88 6.20 11 1 9 302.05 14.62 11 1 10 3.99 3.10 11 1 11 116.58 9.37 -11 -1 -12 407.87 19.01 11 1 12 388.17 17.33 -11 -1 -13 199.67 13.78 -11 -1 -14 69.45 8.68 11 2 -5 13.08 5.17 11 2 -4 94.13 9.51 11 2 -3 19.73 5.08 11 2 -2 842.03 27.57 11 2 -1 197.24 13.25 11 2 0 249.92 13.65 -11 -2 0 228.77 11.33 11 2 1 263.41 13.55 -11 -2 -1 248.27 11.05 11 2 2 357.73 15.62 -11 -2 -2 325.42 12.16 11 2 3 663.22 21.44 -11 -2 -3 548.61 15.63 11 2 4 -0.28 2.62 -11 -2 -4 0.12 1.80 11 2 5 169.09 10.36 -11 -2 -5 150.90 6.30 11 2 5 147.99 5.68 11 2 6 101.22 8.12 11 2 7 20.36 4.43 11 2 8 3.31 3.09 11 2 9 489.94 18.31 11 2 10 6.43 3.23 -11 -2 -11 57.45 7.66 11 2 11 38.04 5.51 -11 -2 -12 276.44 15.39 11 2 12 244.07 13.13 -11 -2 -13 154.33 11.97 -11 -2 -14 46.94 7.69 11 3 -5 165.07 12.77 11 3 -4 64.34 8.00 11 3 -3 13.82 4.71 11 3 -2 320.50 16.38 11 3 -1 35.06 5.83 11 3 0 15.26 4.02 11 3 1 6.84 2.73 11 3 1 4.22 3.15 11 3 2 34.91 4.39 11 3 2 32.57 5.10 11 3 3 193.59 11.22 11 3 3 193.80 9.79 -11 -3 -3 191.71 8.19 11 3 4 64.57 6.65 -11 -3 -4 70.11 4.43 -11 -3 -5 90.19 7.25 11 3 5 99.88 7.82 -11 -3 -5 97.36 4.39 11 3 5 97.76 4.98 11 3 6 239.91 11.82 -11 -3 -6 219.42 5.64 11 3 7 265.92 12.70 11 3 8 398.14 15.64 11 3 9 1459.80 34.52 -11 -3 -10 180.90 11.75 11 3 10 163.78 10.02 -11 -3 -11 32.00 6.01 11 3 11 17.06 3.95 -11 -3 -12 50.16 7.20 11 3 12 37.64 5.46 -11 -3 -13 22.05 5.98 -11 -3 -14 71.82 8.86 11 4 -5 488.26 22.17 11 4 -4 30.61 6.20 11 4 -3 0.25 3.24 -11 -4 3 2.09 1.94 11 4 -2 657.04 23.93 -11 -4 2 656.12 16.74 11 4 -1 210.12 10.11 11 4 -1 220.24 12.99 11 4 0 0.40 2.07 11 4 0 1.78 2.97 11 4 1 29.02 3.82 11 4 1 25.09 4.59 11 4 2 245.84 12.67 11 4 2 237.86 10.45 11 4 3 1025.43 27.59 11 4 3 1007.80 24.56 11 4 4 5.76 2.42 11 4 4 6.78 3.01 11 4 4 7.40 1.93 -11 -4 -5 183.88 10.22 11 4 5 186.20 10.41 11 4 5 192.45 7.62 -11 -4 -6 120.83 7.90 11 4 6 117.12 8.07 11 4 6 107.83 6.00 -11 -4 -7 42.54 4.79 11 4 7 42.53 5.17 -11 -4 -8 4.20 2.69 11 4 8 3.84 2.66 -11 -4 -9 182.96 8.63 11 4 9 201.56 10.55 -11 -4 -9 213.13 12.11 -11 -4 -10 98.60 5.79 -11 -4 -10 121.26 9.58 11 4 10 103.47 7.65 -11 -4 -11 8.11 4.43 11 4 11 5.68 2.72 -11 -4 -12 157.94 11.44 11 4 12 132.12 8.73 -11 -4 -13 3.29 4.43 -11 -4 -14 72.74 8.81 11 5 -4 -0.38 4.00 -11 -5 4 5.65 2.83 11 5 -3 172.92 12.56 -11 -5 3 176.59 9.01 11 5 -2 4.04 3.66 -11 -5 2 3.31 1.96 11 5 -1 37.56 4.27 11 5 -1 44.98 6.40 11 5 0 159.40 10.94 11 5 0 152.66 7.99 11 5 1 248.10 13.03 11 5 1 241.96 10.11 11 5 2 119.13 8.79 11 5 2 113.33 6.74 11 5 3 210.79 11.44 11 5 3 220.48 9.55 11 5 4 316.99 13.52 11 5 4 304.07 11.59 -11 -5 -5 362.85 14.38 11 5 5 382.56 14.77 11 5 5 367.97 11.85 -11 -5 -6 135.23 8.33 11 5 6 146.82 8.82 11 5 6 138.83 7.18 -11 -5 -7 37.21 4.45 11 5 7 37.97 4.77 -11 -5 -7 28.95 4.32 -11 -5 -8 112.02 6.90 -11 -5 -8 100.32 7.27 11 5 8 122.94 7.89 -11 -5 -8 121.94 8.93 -11 -5 -9 123.62 6.84 -11 -5 -9 115.51 7.67 11 5 9 130.65 8.20 -11 -5 -9 139.64 9.74 -11 -5 -10 61.91 4.46 -11 -5 -10 71.45 7.42 11 5 10 62.82 5.71 -11 -5 -10 59.77 5.61 -11 -5 -11 322.09 15.60 11 5 11 302.11 12.60 -11 -5 -11 286.47 12.56 -11 -5 -12 17.55 5.10 11 5 12 14.89 3.25 -11 -5 -13 -1.64 4.08 -11 -5 -14 209.79 14.02 -11 -5 -15 170.82 13.02 11 6 -4 41.65 6.81 -11 -6 4 26.27 4.53 11 6 -3 90.64 9.36 -11 -6 3 85.13 6.71 11 6 -2 34.12 5.89 -11 -6 2 34.30 4.32 11 6 -1 108.03 9.35 -11 -6 1 114.84 7.22 11 6 0 1084.15 24.09 11 6 0 1132.73 31.31 11 6 1 0.16 1.97 11 6 1 -1.94 3.03 11 6 2 107.56 8.41 11 6 2 103.73 6.12 11 6 3 378.94 15.34 11 6 3 363.44 12.06 11 6 4 3.74 2.24 11 6 4 5.24 2.81 -11 -6 -5 153.21 9.21 11 6 5 148.73 9.04 11 6 5 156.77 7.84 -11 -6 -6 47.10 5.07 -11 -6 -6 61.84 6.10 11 6 6 50.96 5.44 11 6 6 49.92 4.62 -11 -6 -7 158.30 8.52 -11 -6 -7 171.80 9.98 11 6 7 172.99 9.21 11 6 7 151.47 8.29 -11 -6 -8 70.08 5.49 -11 -6 -8 67.29 6.95 11 6 8 76.19 6.07 -11 -6 -8 65.25 5.65 -11 -6 -9 56.76 4.60 -11 -6 -9 55.13 7.03 11 6 9 56.07 5.28 -11 -6 -9 50.98 5.05 -11 -6 -10 40.68 3.57 -11 -6 -10 41.36 6.11 11 6 10 44.72 4.79 -11 -6 -10 39.88 4.59 -11 -6 -11 69.50 7.74 11 6 11 83.19 6.34 -11 -6 -11 64.72 5.63 -11 -6 -12 48.61 6.78 11 6 12 44.42 4.68 -11 -6 -13 189.90 12.85 -11 -6 -14 114.36 10.53 -11 -6 -15 7.36 4.53 -11 -7 5 168.42 11.05 11 7 -4 23.58 5.56 -11 -7 4 25.24 4.65 11 7 -3 5.51 3.42 -11 -7 3 10.41 3.15 11 7 -2 95.97 9.33 -11 -7 2 75.39 6.53 11 7 -1 131.90 10.35 -11 -7 1 119.49 7.90 -11 -7 0 206.24 7.52 11 7 0 187.91 11.82 -11 -7 -1 37.92 3.74 11 7 1 28.86 3.16 11 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22.93 5.32 11 10 0 65.61 7.66 11 10 0 62.68 6.99 11 10 1 7.75 3.73 11 10 1 2.08 2.88 11 10 2 5.92 3.29 11 10 2 6.51 3.10 -11 -10 -3 131.64 6.85 11 10 3 143.27 9.53 11 10 3 154.95 8.24 -11 -10 -4 279.12 10.00 11 10 4 300.04 13.27 11 10 4 305.39 10.77 -11 -10 -5 43.08 4.43 11 10 5 40.38 4.96 11 10 5 42.51 3.74 -11 -10 -6 24.02 3.50 11 10 6 27.83 4.05 11 10 6 25.58 2.46 11 10 7 214.13 9.63 -11 -10 -7 211.58 10.44 11 10 8 -2.85 1.92 -11 -10 -8 0.57 2.42 -11 -10 -8 2.64 2.78 -11 -10 -9 309.89 12.15 -11 -10 -9 317.94 14.29 11 10 9 349.52 11.16 -11 -10 -10 420.46 17.28 11 10 10 417.44 11.65 -11 -10 -11 25.22 5.18 -11 -10 -12 188.91 12.43 -11 -10 -13 280.59 15.61 -11 -10 -14 19.17 5.18 -11 -11 3 59.61 7.73 11 11 -3 69.62 8.87 11 11 -2 222.90 14.20 -11 -11 2 219.17 13.79 11 11 -1 524.20 20.93 -11 -11 1 532.21 21.46 11 11 0 2.10 3.69 11 11 0 0.87 3.71 11 11 1 27.93 6.45 11 11 1 22.74 4.82 11 11 1 30.80 5.10 11 11 2 96.74 9.48 11 11 2 87.86 7.94 11 11 2 109.48 8.02 11 11 3 3.79 3.74 11 11 3 6.03 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5.83 -12 -2 -2 36.15 5.16 12 2 3 836.56 25.82 -12 -2 -3 705.71 19.28 12 2 4 3.39 3.52 -12 -2 -4 0.84 2.08 12 2 5 32.41 5.51 -12 -2 -5 25.55 3.15 12 2 5 23.43 2.08 12 2 6 178.45 11.14 -12 -2 -6 147.18 6.16 12 2 6 151.91 6.16 12 2 7 4.21 3.31 12 2 8 30.02 5.14 12 2 9 435.90 18.01 12 2 10 40.96 5.88 -12 -2 -11 17.01 5.59 12 2 11 1.62 3.36 -12 -2 -12 2.24 4.03 12 2 12 0.41 3.30 -12 -2 -13 3.75 4.36 12 2 13 -1.34 3.35 12 3 -3 52.45 7.44 12 3 -2 299.92 16.46 12 3 -1 212.52 13.47 12 3 0 248.55 14.20 12 3 1 116.99 9.78 12 3 2 477.29 19.28 12 3 3 81.37 7.66 12 3 4 43.70 5.96 12 3 5 8.49 3.28 12 3 5 8.86 1.78 -12 -3 -5 13.16 2.22 12 3 6 472.57 18.16 12 3 6 440.94 12.24 12 3 7 1.70 2.79 12 3 8 22.48 4.69 12 3 9 1292.70 33.14 12 3 10 404.54 16.76 -12 -3 -11 112.63 10.18 12 3 11 96.21 8.11 -12 -3 -12 58.32 8.01 12 3 12 54.42 6.43 -12 -3 -13 23.76 6.01 12 3 13 20.73 4.70 -12 -3 -14 7.11 4.47 12 4 -3 -0.34 3.88 12 4 -2 161.27 12.16 12 4 -1 89.21 9.01 12 4 0 303.30 15.84 12 4 1 146.36 10.71 12 4 2 7.22 3.44 12 4 3 79.63 7.73 12 4 4 32.41 5.23 12 4 5 23.47 4.46 12 4 5 22.85 2.68 12 4 6 900.50 25.65 12 4 6 815.63 19.27 -12 -4 -7 4.22 2.98 12 4 7 4.30 3.07 -12 -4 -8 173.26 9.50 12 4 8 166.35 10.24 -12 -4 -9 156.54 8.71 12 4 9 186.83 10.79 -12 -4 -10 63.91 7.64 12 4 10 53.40 5.93 -12 -4 -11 55.68 7.62 12 4 11 41.63 5.41 -12 -4 -12 36.55 6.57 12 4 12 29.03 4.82 -12 -4 -13 6.53 4.19 12 4 13 4.98 3.15 -12 -4 -14 3.33 4.15 12 5 -3 37.69 6.66 12 5 -2 0.23 3.72 12 5 -1 148.24 11.29 12 5 0 118.30 9.93 12 5 1 39.06 4.68 12 5 1 45.19 6.49 12 5 2 2.67 2.48 12 5 2 1.61 3.07 12 5 3 24.75 3.90 12 5 3 29.64 5.38 12 5 4 47.84 5.87 12 5 4 58.56 5.44 12 5 5 154.09 9.85 12 5 5 148.27 7.15 12 5 6 1712.77 37.98 12 5 6 1568.96 31.87 -12 -5 -7 628.44 19.50 12 5 7 637.34 20.34 12 5 7 594.11 17.08 -12 -5 -8 81.25 6.56 12 5 8 93.03 7.57 -12 -5 -8 97.10 8.41 -12 -5 -9 54.77 5.08 -12 -5 -9 64.77 7.29 12 5 9 58.04 6.07 -12 -5 -10 4.79 4.26 12 5 10 -1.33 2.74 -12 -5 -11 126.68 10.28 12 5 11 122.81 8.63 -12 -5 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140.11 9.74 12 7 3 130.74 7.06 -12 -7 -4 287.97 11.79 12 7 4 277.23 13.38 12 7 4 271.88 10.58 12 7 5 1.86 1.99 -12 -7 -5 2.83 3.22 12 7 5 -1.85 2.57 12 7 5 -1.85 2.14 -12 -7 -6 80.48 6.94 12 7 6 76.56 6.73 12 7 6 73.54 5.91 -12 -7 -7 22.42 3.95 -12 -7 -7 24.72 4.65 12 7 7 22.39 3.98 12 7 7 22.12 3.56 -12 -7 -8 109.15 7.43 12 7 8 104.92 7.47 -12 -7 -8 105.07 8.47 -12 -7 -9 12.60 2.92 -12 -7 -9 13.37 4.17 12 7 9 15.52 3.52 -12 -7 -10 2.63 3.66 12 7 10 0.69 2.25 -12 -7 -11 441.65 18.86 12 7 11 456.29 15.35 -12 -7 -12 -2.98 4.63 12 7 12 -1.02 2.33 -12 -7 -13 290.73 16.16 -12 -7 -14 0.55 3.90 -12 -8 3 74.73 7.33 12 8 -2 90.05 9.61 -12 -8 2 81.01 7.39 12 8 -1 233.20 14.44 12 8 0 118.85 10.01 12 8 1 64.50 7.42 -12 -8 -2 -4.24 2.34 12 8 2 -1.10 3.30 12 8 3 382.72 16.29 -12 -8 -3 334.48 11.92 12 8 4 26.94 3.30 12 8 4 22.55 4.32 -12 -8 -4 22.21 3.64 12 8 5 27.21 3.50 12 8 5 37.86 5.34 -12 -8 -5 25.25 4.10 12 8 6 255.83 11.95 -12 -8 -6 235.07 11.28 12 8 7 4.89 2.49 -12 -8 -7 0.22 2.88 -12 -8 -8 65.52 5.89 12 8 8 68.67 5.99 -12 -8 -8 63.82 6.66 -12 -8 -9 162.46 8.50 -12 -8 -9 152.83 10.14 12 8 9 167.49 8.91 -12 -8 -10 383.58 16.97 12 8 10 412.87 14.12 -12 -8 -11 10.77 4.00 12 8 11 10.99 3.11 -12 -8 -12 17.03 5.27 -12 -8 -13 14.81 4.73 -12 -8 -14 165.04 12.56 -12 -9 3 3.70 3.25 12 9 -2 20.48 5.57 -12 -9 2 21.15 4.50 12 9 -2 8.17 4.03 12 9 -1 367.19 18.51 12 9 -1 366.77 16.63 12 9 0 13.74 4.96 12 9 0 -2.43 3.51 12 9 1 15.19 4.94 12 9 1 10.74 3.02 12 9 2 8.03 3.61 -12 -9 -3 710.55 17.72 12 9 3 747.45 23.91 -12 -9 -4 391.46 13.14 12 9 4 406.60 16.47 -12 -9 -5 1.79 2.88 12 9 5 2.68 2.51 -12 -9 -6 330.39 13.28 12 9 6 360.35 14.33 -12 -9 -7 166.48 9.76 12 9 7 187.40 9.75 -12 -9 -8 -7.03 4.03 -12 -9 -8 -0.02 2.57 12 9 8 1.54 2.42 -12 -9 -9 12.24 3.63 12 9 9 16.05 3.08 -12 -9 -10 41.73 6.10 12 9 10 42.08 4.40 -12 -9 -11 0.15 3.18 12 9 11 2.57 2.02 -12 -9 -12 1.96 3.56 -12 -9 -13 2.56 3.94 -12 -9 -14 158.82 12.41 -12 -10 3 15.81 5.04 12 10 -3 12.45 4.55 12 10 -2 128.33 10.65 -12 -10 2 135.47 10.68 12 10 -1 22.23 5.62 12 10 -1 17.23 4.83 12 10 0 103.06 9.70 12 10 0 110.91 9.02 12 10 1 43.66 6.56 12 10 1 44.20 5.41 12 10 2 24.37 4.91 12 10 2 22.35 4.06 12 10 3 338.77 15.67 12 10 3 367.79 13.11 -12 -10 -4 159.89 7.61 12 10 4 162.23 10.25 12 10 4 162.29 7.67 -12 -10 -5 364.13 12.90 12 10 5 387.93 15.48 -12 -10 -6 84.58 6.51 12 10 6 93.05 7.19 -12 -10 -7 3.72 2.48 12 10 7 6.59 2.77 -12 -10 -8 35.10 5.13 12 10 8 38.28 4.49 -12 -10 -9 260.29 13.14 12 10 9 279.50 10.93 -12 -10 -10 269.97 13.93 -12 -10 -11 50.73 6.73 -12 -10 -12 194.74 12.61 -12 -10 -13 114.00 10.18 -12 -10 -14 373.45 18.86 -12 -11 2 54.86 7.31 12 11 -2 50.83 7.46 12 11 -1 218.57 13.58 12 11 0 192.89 12.12 12 11 0 203.68 13.69 12 11 1 137.05 9.51 12 11 1 143.91 11.14 12 11 2 1.44 3.24 12 11 2 -0.69 2.95 12 11 3 244.92 13.32 12 11 4 396.57 16.56 12 11 5 8.87 3.44 -12 -11 -6 38.59 4.47 12 11 6 33.37 4.58 -12 -11 -7 13.00 3.24 12 11 7 13.51 3.44 -12 -11 -8 131.07 8.78 12 11 8 132.40 7.71 -12 -11 -9 95.41 7.99 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13.64 -12 -14 -12 74.25 8.50 -12 -14 -13 58.05 7.67 12 15 6 19.26 6.00 12 15 7 6.10 4.27 12 15 8 4.16 3.94 -12 -15 -12 32.59 6.17 12 16 7 390.91 19.75 12 16 8 193.61 13.72 13 -3 3 224.50 15.32 13 -3 4 11.59 4.95 13 -3 5 49.00 7.80 13 -3 6 224.59 15.27 13 -2 0 2.59 4.23 13 -2 1 -3.32 3.54 13 -2 2 71.26 8.50 13 -2 3 235.94 15.26 13 -2 4 98.24 10.24 13 -2 5 15.27 5.22 13 -2 6 98.34 10.08 13 -2 7 7.68 4.70 13 -2 8 8.15 4.50 13 -2 9 362.28 19.18 13 -1 -1 238.54 15.63 13 -1 0 144.76 12.14 13 -1 1 49.38 7.28 13 -1 2 59.56 8.13 13 -1 3 176.81 12.90 13 -1 4 17.71 4.82 13 -1 5 72.38 8.52 13 -1 6 3.27 3.86 13 -1 7 114.29 10.40 13 -1 8 0.06 3.67 13 -1 9 672.41 26.17 13 -1 10 43.44 7.11 13 -1 11 -3.53 4.31 13 0 -1 72.66 8.76 13 0 0 -3.28 4.20 13 0 1 8.62 4.08 13 0 2 -0.06 3.83 13 0 3 81.09 8.96 13 0 4 175.64 12.65 13 0 5 23.66 5.64 13 0 6 417.62 19.27 13 0 7 -3.65 3.70 13 0 8 0.55 3.47 13 0 9 738.62 26.62 13 0 10 94.95 9.57 13 0 11 52.73 7.50 13 0 12 23.67 5.78 13 1 -1 26.69 5.94 13 1 0 21.86 5.62 13 1 1 30.75 6.14 13 1 2 93.03 9.30 13 1 3 63.05 7.65 13 1 4 52.06 7.01 13 1 5 25.18 5.79 13 1 6 220.05 13.58 13 1 7 50.66 6.86 13 1 8 19.27 5.04 13 1 9 458.19 19.92 13 1 10 115.32 10.18 13 1 11 0.50 3.44 13 1 12 84.82 8.92 13 1 13 1.78 3.44 13 2 -2 14.59 4.68 13 2 -1 19.91 5.60 13 2 0 66.83 8.36 13 2 1 527.00 21.93 13 2 2 136.23 10.93 13 2 3 -5.36 4.23 13 2 4 110.66 9.65 13 2 5 56.22 6.95 13 2 6 44.28 6.52 13 2 7 69.09 7.67 13 2 8 286.40 14.99 13 2 9 58.62 7.44 13 2 10 48.25 6.55 13 2 11 147.29 11.04 -13 -2 -12 143.80 12.02 13 2 12 116.09 10.00 13 2 13 26.13 5.62 13 3 -2 26.43 6.04 13 3 -1 232.62 14.97 13 3 0 598.63 24.00 13 3 1 97.47 9.43 13 3 2 244.48 14.17 13 3 3 56.47 7.33 13 3 4 62.85 7.37 13 3 5 40.02 6.22 13 3 6 -1.43 3.27 13 3 7 81.12 8.14 13 3 8 0.69 3.10 13 3 9 99.46 8.71 13 3 10 62.39 7.22 -13 -3 -11 154.52 11.88 13 3 11 138.02 10.47 -13 -3 -12 156.52 12.26 13 3 12 127.16 10.03 -13 -3 -13 92.83 10.06 13 3 13 74.66 7.91 13 4 -2 48.96 7.59 13 4 -1 23.94 5.92 13 4 0 199.40 13.48 13 4 1 23.14 5.40 13 4 2 160.03 11.68 13 4 3 283.98 14.98 13 4 4 18.44 4.76 13 4 5 153.79 10.69 13 4 6 1007.69 29.20 13 4 7 106.82 8.79 13 4 8 -1.90 3.00 13 4 9 15.39 3.91 -13 -4 -10 22.26 5.92 13 4 10 16.10 4.33 -13 -4 -11 16.50 5.19 13 4 11 3.21 3.05 -13 -4 -12 31.60 6.42 13 4 12 21.03 4.79 -13 -4 -13 141.66 11.93 13 4 13 128.52 9.69 13 4 14 5.47 3.34 13 5 -2 -0.53 3.94 13 5 -1 55.82 7.69 13 5 0 13.48 4.60 13 5 1 -0.69 3.28 13 5 2 15.55 4.77 13 5 3 200.99 12.49 13 5 4 39.62 5.87 13 5 5 201.64 12.06 13 5 6 693.92 23.10 13 5 7 158.84 10.39 13 5 7 137.87 7.41 13 5 8 -0.65 3.09 13 5 8 2.91 2.45 -13 -5 -9 133.64 10.36 13 5 9 129.31 9.34 -13 -5 -10 13.53 5.07 13 5 10 8.56 3.35 -13 -5 -11 12.57 5.23 13 5 11 11.06 3.52 -13 -5 -12 194.94 13.48 13 5 12 200.95 11.52 -13 -5 -13 22.54 5.78 13 5 13 22.00 4.60 13 5 14 83.86 7.69 13 6 -1 -2.54 4.02 13 6 0 74.27 8.47 13 6 1 210.89 13.53 13 6 2 263.84 14.61 13 6 3 1098.76 31.58 13 6 4 211.69 12.42 13 6 5 183.19 11.28 13 6 6 156.90 10.30 13 6 6 144.20 7.76 -13 -6 -7 48.08 6.45 13 6 7 32.34 4.88 13 6 7 23.17 3.59 -13 -6 -8 329.77 15.20 13 6 8 302.09 14.07 -13 -6 -9 10.25 4.58 13 6 9 8.20 3.15 -13 -6 -10 34.20 6.13 13 6 10 25.98 4.49 -13 -6 -11 114.38 9.91 13 6 11 98.46 7.74 -13 -6 -12 95.98 9.58 13 6 12 93.77 7.62 -13 -6 -13 372.88 18.71 13 6 13 322.90 14.12 13 7 -1 54.72 7.73 13 7 0 0.94 4.01 13 7 1 23.04 5.57 13 7 2 18.13 4.47 13 7 3 564.45 21.29 13 7 4 449.85 18.29 -13 -7 -4 426.84 15.46 13 7 5 37.62 4.60 -13 -7 -5 49.50 5.96 13 7 5 39.83 5.69 -13 -7 -6 78.67 7.23 13 7 6 77.78 7.19 13 7 6 77.70 6.23 -13 -7 -7 125.45 9.15 13 7 7 128.92 8.95 -13 -7 -8 12.84 4.42 13 7 8 11.56 3.52 -13 -7 -9 364.26 16.49 13 7 9 380.12 15.25 -13 -7 -10 294.12 15.23 13 7 10 296.26 13.12 -13 -7 -11 60.97 7.53 13 7 11 62.39 6.09 -13 -7 -12 1.63 3.72 13 7 12 -1.42 2.95 -13 -7 -13 42.15 6.86 -13 -7 -14 13.91 4.85 13 8 -1 634.22 25.53 13 8 0 72.10 8.38 13 8 1 49.75 7.12 13 8 2 13.59 4.31 -13 -8 -3 0.37 2.15 13 8 3 7.61 3.81 -13 -8 -4 7.93 3.04 13 8 4 5.38 3.69 -13 -8 -5 154.98 9.17 13 8 5 160.78 10.61 -13 -8 -6 31.64 4.78 13 8 6 30.61 5.13 -13 -8 -7 3.86 3.30 13 8 7 -1.00 2.72 -13 -8 -8 26.58 5.05 13 8 8 35.10 4.80 -13 -8 -9 312.54 15.04 13 8 9 332.58 13.82 -13 -8 -10 723.22 24.66 13 8 10 753.37 21.60 -13 -8 -11 0.10 4.01 13 8 11 16.24 3.51 -13 -8 -12 37.27 6.35 -13 -8 -13 129.30 11.21 -13 -8 -14 0.20 3.85 13 9 0 18.77 5.28 13 9 1 16.55 4.83 13 9 2 14.01 4.94 13 9 3 55.01 7.04 -13 -9 -4 7.40 2.51 13 9 4 7.35 3.23 -13 -9 -5 67.05 5.85 13 9 5 67.82 7.12 -13 -9 -6 87.06 7.05 13 9 6 98.36 7.84 -13 -9 -7 123.26 8.68 13 9 7 137.80 8.96 -13 -9 -8 30.95 4.95 13 9 8 41.50 5.16 -13 -9 -9 -2.72 3.87 13 9 9 0.35 2.56 -13 -9 -10 120.91 9.66 13 9 10 120.12 7.72 -13 -9 -11 51.99 6.99 -13 -9 -12 32.40 6.10 -13 -9 -13 1.53 4.23 -13 -9 -14 201.98 13.95 13 10 0 134.56 11.45 13 10 1 102.30 9.85 13 10 2 0.75 3.44 13 10 3 442.04 18.88 13 10 4 154.28 10.54 -13 -10 -5 42.76 4.57 13 10 5 39.73 5.52 -13 -10 -6 176.43 9.62 13 10 6 190.15 10.98 -13 -10 -7 265.29 12.52 13 10 7 284.05 12.90 -13 -10 -8 124.82 8.97 13 10 8 127.47 8.25 -13 -10 -9 2.30 3.03 13 10 9 1.43 2.56 -13 -10 -10 34.89 5.59 -13 -10 -11 16.12 4.77 -13 -10 -12 22.72 5.14 -13 -10 -13 1.76 3.59 -13 -10 -14 244.23 15.43 13 11 1 60.00 7.90 13 11 2 140.21 11.11 13 11 3 29.87 5.46 13 11 4 251.67 13.79 13 11 5 -1.35 3.44 13 11 6 50.45 5.87 -13 -11 -7 26.03 4.24 13 11 7 30.57 4.69 -13 -11 -8 1.94 2.55 13 11 8 3.78 2.70 -13 -11 -9 264.45 13.44 -13 -11 -10 178.29 11.46 -13 -11 -11 78.46 8.36 -13 -11 -12 11.29 4.57 -13 -11 -13 163.15 12.25 13 12 1 165.13 12.71 13 12 2 88.13 9.12 13 12 3 58.22 7.45 13 12 4 4.18 3.50 13 12 5 125.71 9.56 13 12 6 33.90 4.99 13 12 7 180.87 10.23 -13 -12 -8 1.91 2.66 -13 -12 -9 51.98 6.10 -13 -12 -10 294.43 14.72 -13 -12 -11 207.38 12.91 -13 -12 -12 105.76 9.82 -13 -12 -13 3.75 3.42 13 13 2 0.19 3.31 13 13 3 43.71 6.83 13 13 4 100.08 9.05 13 13 5 14.68 4.30 -13 -13 -10 -0.05 3.39 -13 -13 -11 29.37 5.52 -13 -13 -12 -3.08 4.24 -13 -13 -13 13.77 4.95 13 14 3 38.92 6.63 -13 -14 -11 6.96 3.78 -13 -14 -12 3.04 3.74 -13 -14 -13 83.50 9.20 13 15 7 -2.65 4.78 14 -1 4 11.70 5.08 14 -1 5 1.37 3.88 14 -1 6 22.20 5.91 14 -1 7 47.01 7.72 14 0 2 84.00 9.76 14 0 3 71.77 8.70 14 0 4 10.70 4.80 14 0 5 7.98 4.63 14 0 6 382.60 19.32 14 0 7 5.88 3.86 14 0 8 4.80 4.01 14 0 9 523.06 22.94 14 0 10 135.27 11.75 14 1 1 -0.40 4.02 14 1 2 5.38 4.44 14 1 3 150.68 12.18 14 1 4 6.02 4.17 14 1 5 6.97 4.28 14 1 6 450.40 20.75 14 1 7 13.47 4.79 14 1 8 69.37 8.29 14 1 9 110.52 10.22 14 1 10 13.34 4.93 14 1 11 4.78 3.56 14 1 12 38.39 6.68 14 2 1 111.57 10.61 14 2 2 174.79 12.78 14 2 3 269.92 16.00 14 2 4 146.84 11.81 14 2 5 11.78 4.79 14 2 6 794.80 27.57 14 2 7 240.43 14.51 14 2 8 37.45 6.38 14 2 9 43.24 6.92 14 2 10 9.40 4.19 14 2 11 97.70 9.61 14 2 12 149.79 11.56 14 2 13 39.00 6.70 14 2 14 -2.34 3.85 14 3 0 114.63 10.80 14 3 1 69.37 8.53 14 3 2 119.71 10.71 14 3 3 70.66 8.28 14 3 4 9.58 4.28 14 3 5 105.77 9.82 14 3 6 15.98 5.20 14 3 7 38.48 6.25 14 3 8 29.97 5.87 14 3 9 159.88 11.71 14 3 10 27.21 5.77 -14 -3 -11 57.23 8.10 14 3 11 32.65 6.35 14 3 12 562.93 22.37 14 3 13 326.01 16.85 14 3 14 -4.74 3.62 14 4 0 45.26 7.30 14 4 1 172.53 12.80 14 4 2 369.01 18.48 14 4 3 47.10 7.02 14 4 4 99.82 9.65 14 4 5 31.94 5.87 14 4 6 163.59 11.52 14 4 7 15.94 4.65 14 4 8 161.18 11.36 14 4 9 41.52 6.41 -14 -4 -10 67.63 8.43 14 4 10 53.60 6.99 -14 -4 -11 152.61 12.05 14 4 11 115.44 9.64 -14 -4 -12 65.22 8.70 14 4 12 44.81 6.42 14 4 13 213.36 13.09 14 4 14 1.77 3.73 14 5 0 88.23 9.62 14 5 1 6.99 4.03 14 5 2 0.48 3.50 14 5 3 179.73 12.52 14 5 4 37.63 6.17 14 5 5 50.83 6.88 14 5 6 7.02 3.65 14 5 7 3.56 3.40 14 5 8 0.39 3.08 -14 -5 -9 174.55 12.42 14 5 9 173.08 11.43 -14 -5 -10 276.69 15.48 14 5 10 267.19 14.13 -14 -5 -11 49.14 7.25 14 5 11 31.53 5.55 -14 -5 -12 29.67 6.44 14 5 12 13.65 4.33 14 5 13 8.67 3.92 14 6 0 21.83 6.05 14 6 1 13.54 4.82 14 6 2 -0.54 3.63 14 6 3 832.48 27.96 14 6 4 348.34 16.96 14 6 5 3.88 3.91 14 6 6 77.63 7.94 14 6 7 46.58 6.25 -14 -6 -8 6.29 4.35 14 6 8 3.04 2.91 -14 -6 -9 9.89 4.65 14 6 9 -0.31 3.24 -14 -6 -10 87.37 8.88 14 6 10 94.58 8.16 -14 -6 -11 2.02 3.99 14 6 11 3.41 3.17 -14 -6 -12 3.71 3.81 14 6 12 8.34 3.87 -14 -6 -13 4.73 4.36 14 6 13 -2.27 3.12 14 7 1 30.96 6.19 14 7 2 40.80 6.65 14 7 3 294.83 15.99 14 7 4 83.18 8.62 -14 -7 -5 366.94 15.19 14 7 5 364.89 16.87 -14 -7 -6 8.83 4.14 14 7 6 -0.67 3.16 -14 -7 -7 8.54 4.30 14 7 7 -0.85 3.21 -14 -7 -8 3.19 3.88 14 7 8 0.95 2.94 -14 -7 -9 283.39 15.04 14 7 9 298.35 14.28 -14 -7 -10 287.71 15.42 14 7 10 281.33 13.66 -14 -7 -11 111.95 10.20 14 7 11 106.79 8.28 -14 -7 -12 97.10 9.88 14 7 12 101.98 8.14 -14 -7 -13 23.17 5.86 14 8 1 329.02 17.80 14 8 2 17.60 5.11 14 8 3 78.73 8.64 -14 -8 -4 208.75 10.68 14 8 4 207.29 13.01 -14 -8 -5 53.99 5.96 14 8 5 51.48 6.78 -14 -8 -6 25.47 4.62 14 8 6 28.41 5.09 -14 -8 -7 23.12 4.98 14 8 7 18.75 4.30 -14 -8 -8 162.17 10.81 14 8 8 172.40 10.79 -14 -8 -9 48.57 6.67 14 8 9 65.32 6.79 -14 -8 -10 229.91 13.76 14 8 10 254.23 12.64 -14 -8 -11 35.72 6.62 14 8 11 36.02 5.17 -14 -8 -12 10.15 4.44 -14 -8 -13 0.29 4.70 14 9 1 70.36 8.51 14 9 2 73.49 8.87 14 9 3 10.88 4.38 14 9 4 93.99 8.97 -14 -9 -5 8.49 2.89 14 9 5 14.86 4.23 -14 -9 -6 380.99 15.39 14 9 6 400.13 17.17 -14 -9 -7 769.81 23.97 14 9 7 858.05 25.60 -14 -9 -8 4.54 3.37 14 9 8 6.82 2.84 -14 -9 -9 171.88 11.40 14 9 9 194.93 10.85 -14 -9 -10 484.99 20.11 14 9 10 520.79 18.03 -14 -9 -11 -6.10 4.86 -14 -9 -12 -8.60 5.15 -14 -9 -13 5.47 3.69 14 10 2 -1.56 4.06 14 10 3 50.48 7.27 14 10 4 22.53 5.42 14 10 5 59.66 7.11 14 10 6 140.01 10.13 -14 -10 -7 460.91 17.33 14 10 7 466.05 18.06 -14 -10 -8 -2.58 3.30 14 10 8 0.91 2.54 -14 -10 -9 7.15 3.48 14 10 9 7.15 2.98 -14 -10 -10 180.81 11.90 -14 -10 -11 8.97 4.49 -14 -10 -12 29.45 6.04 -14 -10 -13 142.60 11.73 14 11 2 122.72 10.69 14 11 3 72.84 8.33 14 11 4 46.13 7.01 14 11 5 -2.14 3.75 14 11 6 36.08 5.39 14 11 7 219.90 12.01 -14 -11 -8 23.95 4.63 14 11 8 21.96 4.33 -14 -11 -9 94.95 8.50 -14 -11 -10 8.87 3.96 -14 -11 -11 246.42 14.26 -14 -11 -12 166.51 12.16 -14 -11 -13 157.21 12.32 14 12 3 7.65 4.54 14 12 4 0.37 3.84 14 12 5 -2.80 3.88 14 12 6 15.02 4.37 -14 -12 -9 0.53 2.90 -14 -12 -10 62.54 7.18 -14 -12 -11 18.60 4.88 -14 -12 -12 79.84 8.87 -14 -12 -13 123.78 10.82 14 13 3 -1.86 3.94 14 13 4 103.67 9.66 -14 -13 -11 12.01 4.41 -14 -13 -12 32.15 6.03 15 1 6 477.79 22.34 15 1 7 30.71 6.38 15 1 8 1.29 3.79 15 1 9 22.55 5.90 15 2 4 11.75 4.93 15 2 5 -9.47 5.00 15 2 6 486.70 22.09 15 2 7 159.99 12.58 15 2 8 5.73 4.06 15 2 9 23.21 5.83 15 2 10 -5.72 4.30 15 2 11 22.35 5.73 15 3 3 633.64 25.69 15 3 4 33.72 6.43 15 3 5 127.27 11.12 15 3 6 2.22 3.93 15 3 7 -3.52 3.97 15 3 8 43.42 6.93 15 3 9 49.07 7.24 15 3 10 11.56 4.87 15 3 11 0.12 3.53 15 3 12 243.98 15.00 15 3 13 225.30 14.61 15 4 3 353.88 18.60 15 4 4 229.69 14.79 15 4 5 1.89 3.85 15 4 6 60.75 7.71 15 4 7 8.60 4.22 15 4 8 46.14 7.03 15 4 9 206.65 13.45 15 4 10 252.22 14.99 15 4 11 15.78 4.79 15 4 12 34.76 6.17 15 4 13 108.08 9.97 15 4 14 19.21 5.55 15 5 2 7.25 4.65 15 5 3 28.69 6.17 15 5 4 9.37 3.86 15 5 5 86.96 9.02 15 5 6 16.28 4.89 15 5 7 12.15 4.65 15 5 8 132.82 10.69 15 5 9 318.92 16.35 -15 -5 -10 934.76 30.87 15 5 10 926.17 29.33 -15 -5 -11 18.11 5.79 15 5 11 14.62 4.94 15 5 12 60.39 7.50 15 5 13 59.29 7.32 15 6 2 4.69 3.64 15 6 3 58.06 7.64 15 6 4 -0.88 3.52 15 6 5 10.55 4.43 15 6 6 36.84 6.17 15 6 7 37.49 6.34 -15 -6 -8 209.78 13.23 15 6 8 188.11 12.47 -15 -6 -9 8.24 4.46 15 6 9 2.63 3.78 -15 -6 -10 147.12 11.79 15 6 10 161.45 11.27 -15 -6 -11 38.83 6.96 15 6 11 43.26 6.38 15 6 12 2.79 3.33 15 7 2 12.82 5.25 15 7 3 61.66 8.08 15 7 4 4.86 3.46 -15 -7 -5 109.42 8.73 15 7 5 97.82 9.51 -15 -7 -6 106.14 8.95 15 7 6 101.24 9.38 -15 -7 -7 280.56 14.54 15 7 7 272.94 14.89 -15 -7 -8 17.29 5.29 15 7 8 3.01 3.23 -15 -7 -9 -0.80 3.84 15 7 9 -2.69 4.04 -15 -7 -10 25.67 6.12 15 7 10 10.79 3.99 -15 -7 -11 169.88 12.71 15 7 11 181.98 11.49 -15 -7 -12 63.20 8.31 15 7 12 47.94 6.28 15 8 3 23.87 5.61 15 8 4 105.54 9.81 -15 -8 -5 14.56 3.92 15 8 5 9.20 4.05 -15 -8 -6 45.74 6.01 15 8 6 41.46 6.30 -15 -8 -7 9.89 4.47 15 8 7 9.57 4.02 -15 -8 -8 9.34 4.00 15 8 8 2.70 3.18 -15 -8 -9 40.16 6.27 15 8 9 54.95 6.56 -15 -8 -10 3.88 3.98 15 8 10 9.44 3.52 -15 -8 -11 172.13 12.60 15 8 11 184.76 11.23 -15 -8 -12 12.21 4.64 15 9 3 37.37 6.25 15 9 4 -0.63 3.56 15 9 5 24.71 5.24 15 9 6 112.87 9.74 -15 -9 -7 281.44 14.02 15 9 7 293.43 15.11 -15 -9 -8 38.20 5.93 15 9 8 31.82 5.36 -15 -9 -9 172.77 11.78 15 9 9 180.96 11.26 -15 -9 -10 153.39 11.53 15 9 10 172.49 10.72 -15 -9 -11 222.03 14.13 -15 -9 -12 142.50 11.75 15 10 3 35.84 6.43 15 10 4 165.89 12.29 15 10 5 21.89 5.31 15 10 6 72.11 7.91 15 10 7 412.82 17.95 -15 -10 -8 -6.35 4.53 15 10 8 4.00 3.58 -15 -10 -9 -3.28 4.71 -15 -10 -10 -8.71 4.71 -15 -10 -11 36.81 6.42 -15 -10 -12 26.41 5.82 15 11 4 363.87 18.23 15 11 5 -0.19 3.48 15 11 6 30.57 5.63 15 11 7 553.91 20.92 -15 -11 -9 5.64 3.34 -15 -11 -10 30.59 5.99 -15 -11 -11 86.58 8.97 -15 -11 -12 12.29 4.72 15 12 4 183.67 13.17 15 12 5 12.06 4.57 15 12 6 112.94 9.84 -15 -12 -11 6.08 3.72 -15 -12 -12 3.24 3.57 16 4 6 10.91 4.72 16 4 7 6.16 3.97 16 4 8 0.93 3.99 16 4 9 226.77 14.79 16 4 10 175.25 13.09 16 4 11 118.57 10.81 16 4 12 35.76 6.61 16 5 5 82.17 9.20 16 5 6 12.36 4.79 16 5 7 8.86 4.40 16 5 8 86.52 9.06 16 5 9 12.23 4.41 16 5 10 278.90 15.97 16 5 11 139.91 11.42 16 5 12 69.98 8.27 16 5 13 15.50 5.15 16 6 5 -6.63 4.68 16 6 6 298.00 16.73 16 6 7 460.52 20.82 -16 -6 -8 7.66 4.87 16 6 8 -3.87 4.24 -16 -6 -9 12.27 5.54 16 6 9 14.76 5.01 -16 -6 -10 106.34 10.53 16 6 10 87.61 8.97 16 6 11 4.65 3.88 16 6 12 -1.23 3.51 16 7 5 23.76 5.44 -16 -7 -6 57.30 7.50 16 7 6 47.41 7.24 -16 -7 -7 471.94 19.79 16 7 7 454.05 20.42 -16 -7 -8 6.12 4.65 16 7 8 0.23 3.60 -16 -7 -9 6.39 4.78 16 7 9 -0.44 3.57 -16 -7 -10 139.84 11.77 16 7 10 141.87 10.97 -16 -7 -11 -1.39 4.28 16 7 11 -6.03 4.00 16 8 5 4.24 4.00 16 8 6 4.75 3.82 -16 -8 -7 65.10 7.81 16 8 7 63.76 7.84 -16 -8 -8 13.14 4.90 16 8 8 18.07 4.95 -16 -8 -9 74.16 8.55 16 8 9 70.27 7.91 -16 -8 -10 -2.40 3.98 16 8 10 4.30 3.77 -16 -8 -11 261.02 15.92 16 9 5 18.49 4.79 16 9 6 33.97 6.19 16 9 7 6.04 3.91 -16 -9 -8 -3.24 4.40 16 9 8 4.63 4.05 -16 -9 -9 4.72 3.87 16 9 9 5.60 4.10 -16 -9 -10 26.49 5.50 -16 -9 -11 51.41 7.42 16 10 5 22.31 5.14 16 10 6 158.22 11.87 16 10 7 225.62 13.83 16 10 8 53.70 7.11 -16 -10 -9 -3.10 4.57 -16 -10 -10 111.72 10.07 -16 -10 -11 22.96 5.44 16 11 5 9.47 4.46 16 11 6 -2.59 3.70 -16 -11 -11 -7.49 4.51 -17 -6 -8 43.93 7.38 17 6 9 18.86 5.48 17 6 10 11.28 4.87 17 6 11 81.35 9.37 -17 -7 -7 217.20 13.76 -17 -7 -8 9.78 5.03 17 7 8 1.43 3.80 -17 -7 -9 8.52 4.87 17 7 9 1.22 3.52 17 7 10 6.65 4.62 -17 -8 -8 0.91 4.08 17 8 8 4.34 3.72 -17 -8 -9 -3.11 4.59 17 8 9 7.20 4.04 17 9 7 37.48 6.80 17 9 8 4.78 4.54 -17 -9 -10 313.85 17.35 0 0 0 0.00 0.00 TITL akl627b_auto in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 12.753315 12.758267 13.180311 69.8749 64.4079 68.3670 ZERR 2.00 0.000267 0.000341 0.000326 0.0024 0.0022 0.0022 LATT 1 SFAC C H N O Mo I UNIT 60.00 80.00 4.00 52.00 16.00 4.00 REM CrysAlisPro recorded range (K): Min=150.0; max=150.0; aver:150.0 TEMP -123 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 95491 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1A I 0.36315(3) 0.58906(3) 0.64724(2) 0.02450(8) Uani 1 1 d . . . . . C7A C 0.1903(4) 0.5651(4) 0.7015(4) 0.0231(9) Uani 1 1 d . . . . . C12A C 0.1137(4) 0.5720(5) 0.8123(4) 0.0318(11) Uani 1 1 d . . . . . H12A H 0.136193 0.590089 0.862970 0.038 Uiso 1 1 calc R U . . . C11A C 0.0019(5) 0.5514(5) 0.8477(5) 0.0419(14) Uani 1 1 d . . . . . H11A H -0.053399 0.556128 0.923576 0.050 Uiso 1 1 calc R U . . . C10A C -0.0292(5) 0.5247(5) 0.7748(5) 0.0446(14) Uani 1 1 d . . . . . H10A H -0.106092 0.511365 0.800294 0.053 Uiso 1 1 calc R U . . . C9A C 0.0496(5) 0.5168(5) 0.6642(5) 0.0382(13) Uani 1 1 d . . . . . H9A H 0.027279 0.496951 0.614590 0.046 Uiso 1 1 calc R U . . . C8A C 0.1619(5) 0.5379(4) 0.6253(4) 0.0310(11) Uani 1 1 d . . . . . H8A H 0.216857 0.533759 0.549206 0.037 Uiso 1 1 calc R U . . . C1A C 0.3415(4) 0.7463(4) 0.5273(4) 0.0243(9) Uani 1 1 d . . . . . C6A C 0.3735(4) 0.7462(4) 0.4137(4) 0.0281(10) Uani 1 1 d . . . . . H6A H 0.401512 0.675688 0.389426 0.034 Uiso 1 1 calc R U . . . C5A C 0.3640(5) 0.8518(4) 0.3351(4) 0.0325(11) Uani 1 1 d . . . . . H5A H 0.383649 0.854167 0.256262 0.039 Uiso 1 1 calc R U . . . C4A C 0.3263(5) 0.9520(4) 0.3712(5) 0.0378(12) Uani 1 1 d . . . . . H4A H 0.321219 1.023960 0.316983 0.045 Uiso 1 1 calc R U . . . C3A C 0.2954(6) 0.9495(5) 0.4864(5) 0.0455(14) Uani 1 1 d . . . . . H3A H 0.269036 1.019918 0.510521 0.055 Uiso 1 1 calc R U . . . C2A C 0.3026(5) 0.8473(5) 0.5653(5) 0.0387(12) Uani 1 1 d . . . . . H2A H 0.281379 0.845248 0.644353 0.046 Uiso 1 1 calc R U . . . I1B I 0.75550(3) 0.87245(3) 0.93428(3) 0.03354(9) Uani 0.93 1 d . . P A 2 C7B C 0.6967(5) 0.8734(4) 1.1112(5) 0.0334(11) Uani 1 1 d . . . A 2 C12B C 0.7246(5) 0.7700(4) 1.1867(5) 0.0394(13) Uani 1 1 d . . . A 2 H12B H 0.766530 0.700206 1.160192 0.047 Uiso 1 1 calc R U . A 2 C11B C 0.6905(5) 0.7701(5) 1.3006(5) 0.0405(13) Uani 1 1 d . . . A 2 H11B H 0.706722 0.699619 1.354163 0.049 Uiso 1 1 calc R U . A 2 C10B C 0.6326(5) 0.8726(5) 1.3376(5) 0.0382(12) Uani 1 1 d . . . A 2 H10B H 0.610926 0.872479 1.416275 0.046 Uiso 1 1 calc R U . A 2 C9B C 0.6061(5) 0.9746(5) 1.2616(5) 0.0384(12) Uani 1 1 d . . . A 2 H9B H 0.566903 1.044412 1.288239 0.046 Uiso 1 1 calc R U . A 2 C8B C 0.6358(5) 0.9774(4) 1.1461(5) 0.0350(12) Uani 1 1 d . . . A 2 H8B H 0.615344 1.047263 1.093599 0.042 Uiso 1 1 calc R U . A 2 C1B C 0.8918(4) 0.9537(5) 0.8877(4) 0.0325(11) Uani 1 1 d . . . . . C6B C 0.8613(5) 1.0728(5) 0.8643(5) 0.0359(12) Uani 1 1 d . . . . . H6B H 0.782232 1.116988 0.866516 0.043 Uiso 1 1 calc R U . . . C5B C 0.9507(5) 1.1258(5) 0.8373(5) 0.0409(13) Uani 1 1 d . . . . . H5B H 0.932638 1.207693 0.821368 0.049 Uiso 1 1 calc R U . . . C4B C 1.0649(5) 1.0605(5) 0.8335(5) 0.0402(13) Uani 1 1 d . . . . . H4B H 1.125430 1.097778 0.813971 0.048 Uiso 1 1 calc R U . . . C3B C 1.0924(5) 0.9417(5) 0.8576(5) 0.0403(13) Uani 1 1 d . . . . . H3B H 1.171385 0.897532 0.855859 0.048 Uiso 1 1 calc R U . . . C2B C 1.0050(5) 0.8858(5) 0.8847(5) 0.0385(12) Uani 1 1 d . . . . . H2B H 1.023088 0.803899 0.900333 0.046 Uiso 1 1 calc R U . . . I1C I 0.5905(5) 0.8360(4) 1.4838(4) 0.0374(11) Uiso 0.07 1 d . . P B 1 Mo1 Mo 0.48210(3) 0.33788(3) 0.90646(3) 0.01893(9) Uani 1 1 d . . . . . Mo2 Mo 0.69845(3) 0.45756(3) 0.71322(3) 0.02054(9) Uani 1 1 d . . . . . Mo3 Mo 0.56050(3) 0.69095(3) 0.81372(3) 0.01970(9) Uani 1 1 d . . . . . Mo4 Mo 0.35016(3) 0.57332(3) 1.00011(3) 0.01692(8) Uani 1 1 d . . . . . O2 O 0.6178(3) 0.5127(3) 0.6223(3) 0.0252(7) Uani 1 1 d . . . . . O3 O 0.4764(3) 0.7419(3) 0.7271(3) 0.0270(7) Uani 1 1 d . . . . . O4 O 0.2700(3) 0.6309(3) 0.9113(3) 0.0244(7) Uani 1 1 d . . . . . O1 O 0.3980(3) 0.3980(3) 0.8185(3) 0.0253(7) Uani 1 1 d . . . . . O7 O 0.8412(3) 0.4053(3) 0.6279(3) 0.0299(7) Uani 1 1 d . . . . . O8 O 0.7047(3) 0.6001(3) 0.7253(3) 0.0231(7) Uani 1 1 d . . . . . O9 O 0.6076(3) 0.8052(3) 0.8003(3) 0.0271(7) Uani 1 1 d . . . . . O10 O 0.4257(3) 0.6956(2) 0.9651(2) 0.0196(6) Uani 1 1 d . . . . . O11 O 0.2443(3) 0.6009(3) 1.1340(3) 0.0207(6) Uani 1 1 d . . . . . O12 O 0.3589(3) 0.4097(2) 1.0374(2) 0.0188(6) Uani 1 1 d . . . . . O5 O 0.4720(3) 0.1983(3) 0.9577(3) 0.0259(7) Uani 1 1 d . . . . . O13 O 0.5235(2) 0.5106(2) 0.8837(2) 0.0189(6) Uani 1 1 d . . . . . O6 O 0.6397(3) 0.3214(3) 0.7972(3) 0.0217(6) Uani 1 1 d . . . . . O1S O 0.9078(4) 0.8502(4) 0.7065(4) 0.0495(10) Uani 1 1 d . . . . . N1S N 0.9353(4) 0.8032(4) 0.5445(4) 0.0351(10) Uani 1 1 d . . . . . C1S C 0.8832(5) 0.8035(5) 0.6556(5) 0.0407(13) Uani 1 1 d . . . . . H1S H 0.821603 0.764156 0.699537 0.049 Uiso 1 1 calc R U . . . C3S C 0.8939(5) 0.7503(5) 0.4915(5) 0.0434(14) Uani 1 1 d . . . . . H3SA H 0.961526 0.691636 0.453816 0.065 Uiso 1 1 calc R U . . . H3SB H 0.861780 0.809821 0.434093 0.065 Uiso 1 1 calc R U . . . H3SC H 0.830646 0.713917 0.550990 0.065 Uiso 1 1 calc R U . . . C2S C 1.0353(5) 0.8555(5) 0.4702(5) 0.0489(16) Uani 1 1 d . . . . . H2SA H 1.101987 0.799708 0.427692 0.073 Uiso 1 1 calc R U . . . H2SB H 1.062135 0.877436 0.517552 0.073 Uiso 1 1 calc R U . . . H2SC H 1.008854 0.924336 0.415604 0.073 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1A 0.01924(15) 0.02933(16) 0.02403(15) -0.00012(12) -0.00871(11) -0.00926(12) C7A 0.017(2) 0.026(2) 0.028(2) -0.0024(19) -0.0094(18) -0.0087(18) C12A 0.028(3) 0.045(3) 0.028(2) -0.005(2) -0.013(2) -0.016(2) C11A 0.024(3) 0.069(4) 0.029(3) -0.003(3) -0.006(2) -0.020(3) C10A 0.034(3) 0.066(4) 0.038(3) 0.008(3) -0.015(2) -0.032(3) C9A 0.042(3) 0.048(3) 0.041(3) -0.002(3) -0.026(3) -0.022(3) C8A 0.029(3) 0.038(3) 0.028(2) -0.005(2) -0.012(2) -0.011(2) C1A 0.025(2) 0.022(2) 0.026(2) -0.0035(18) -0.0093(19) -0.0076(19) C6A 0.030(3) 0.027(2) 0.029(2) -0.005(2) -0.009(2) -0.012(2) C5A 0.035(3) 0.037(3) 0.026(2) 0.000(2) -0.012(2) -0.016(2) C4A 0.032(3) 0.027(3) 0.046(3) 0.005(2) -0.015(2) -0.008(2) C3A 0.052(4) 0.025(3) 0.057(4) -0.013(3) -0.020(3) -0.002(3) C2A 0.045(3) 0.036(3) 0.035(3) -0.013(2) -0.015(2) -0.005(3) I1B 0.02972(19) 0.0381(2) 0.0418(2) -0.01191(16) -0.01119(15) -0.01711(16) C7B 0.027(3) 0.036(3) 0.045(3) -0.009(2) -0.014(2) -0.015(2) C12B 0.035(3) 0.024(3) 0.069(4) -0.012(3) -0.023(3) -0.009(2) C11B 0.043(3) 0.029(3) 0.054(4) 0.003(2) -0.027(3) -0.015(2) C10B 0.028(3) 0.043(3) 0.044(3) -0.004(3) -0.014(2) -0.014(2) C9B 0.025(3) 0.036(3) 0.050(3) -0.013(3) -0.011(2) -0.003(2) C8B 0.028(3) 0.029(3) 0.044(3) -0.005(2) -0.012(2) -0.006(2) C1B 0.024(3) 0.040(3) 0.038(3) -0.010(2) -0.007(2) -0.016(2) C6B 0.030(3) 0.039(3) 0.040(3) -0.006(2) -0.014(2) -0.011(2) C5B 0.045(3) 0.040(3) 0.040(3) -0.007(2) -0.012(3) -0.019(3) C4B 0.034(3) 0.056(4) 0.037(3) -0.013(3) -0.006(2) -0.025(3) C3B 0.024(3) 0.051(3) 0.046(3) -0.020(3) -0.008(2) -0.007(2) C2B 0.032(3) 0.039(3) 0.044(3) -0.012(2) -0.009(2) -0.010(2) Mo1 0.0199(2) 0.01900(18) 0.02140(18) -0.00328(14) -0.00807(15) -0.00881(15) Mo2 0.0168(2) 0.0252(2) 0.02062(19) -0.00583(15) -0.00506(15) -0.00759(15) Mo3 0.0205(2) 0.01860(18) 0.02078(18) 0.00023(14) -0.00750(15) -0.00973(15) Mo4 0.01410(18) 0.01803(18) 0.01996(18) -0.00274(14) -0.00656(14) -0.00619(14) O2 0.0228(17) 0.0299(17) 0.0246(16) -0.0050(13) -0.0081(13) -0.0095(14) O3 0.0287(18) 0.0257(16) 0.0272(17) 0.0002(13) -0.0128(14) -0.0095(14) O4 0.0230(17) 0.0248(16) 0.0276(17) -0.0036(13) -0.0125(13) -0.0063(13) O1 0.0268(18) 0.0266(17) 0.0285(17) -0.0040(14) -0.0133(14) -0.0106(14) O7 0.0193(17) 0.0398(19) 0.0279(17) -0.0106(15) -0.0051(14) -0.0057(15) O8 0.0194(16) 0.0253(16) 0.0242(16) -0.0032(13) -0.0046(13) -0.0111(13) O9 0.0279(18) 0.0236(16) 0.0293(17) -0.0009(13) -0.0088(14) -0.0122(14) O10 0.0196(16) 0.0170(14) 0.0235(15) -0.0030(12) -0.0084(12) -0.0063(12) O11 0.0155(15) 0.0235(15) 0.0248(16) -0.0068(13) -0.0065(12) -0.0062(12) O12 0.0194(16) 0.0177(14) 0.0206(15) 0.0000(12) -0.0071(12) -0.0098(12) O5 0.0317(18) 0.0211(16) 0.0287(17) -0.0034(13) -0.0117(14) -0.0115(14) O13 0.0161(15) 0.0189(15) 0.0226(15) -0.0026(12) -0.0064(12) -0.0077(12) O6 0.0187(16) 0.0229(15) 0.0247(16) -0.0083(13) -0.0052(12) -0.0068(13) O1S 0.043(2) 0.058(3) 0.052(2) -0.020(2) -0.015(2) -0.013(2) N1S 0.025(2) 0.035(2) 0.041(3) -0.012(2) -0.0043(19) -0.0090(19) C1S 0.025(3) 0.045(3) 0.045(3) -0.013(3) -0.005(2) -0.008(2) C3S 0.030(3) 0.050(3) 0.049(3) -0.018(3) -0.003(2) -0.015(3) C2S 0.041(3) 0.053(4) 0.050(4) -0.018(3) 0.002(3) -0.025(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1A I1A C7A 98.54(17) . . ? C12A C7A I1A 118.6(3) . . ? C12A C7A C8A 123.2(4) . . ? C8A C7A I1A 118.1(3) . . ? C7A C12A H12A 121.2 . . ? C7A C12A C11A 117.6(4) . . ? C11A C12A H12A 121.2 . . ? C12A C11A H11A 119.6 . . ? C10A C11A C12A 120.8(5) . . ? C10A C11A H11A 119.6 . . ? C11A C10A H10A 119.6 . . ? C11A C10A C9A 120.8(5) . . ? C9A C10A H10A 119.6 . . ? C10A C9A H9A 119.9 . . ? C10A C9A C8A 120.1(5) . . ? C8A C9A H9A 119.9 . . ? C7A C8A C9A 117.5(5) . . ? C7A C8A H8A 121.2 . . ? C9A C8A H8A 121.2 . . ? C6A C1A I1A 119.6(3) . . ? C6A C1A C2A 122.3(5) . . ? C2A C1A I1A 117.9(4) . . ? C1A C6A H6A 120.8 . . ? C1A C6A C5A 118.4(4) . . ? C5A C6A H6A 120.8 . . ? C6A C5A H5A 120.0 . . ? C4A C5A C6A 120.0(5) . . ? C4A C5A H5A 120.0 . . ? C5A C4A H4A 119.8 . . ? C5A C4A C3A 120.4(5) . . ? C3A C4A H4A 119.8 . . ? C4A C3A H3A 119.7 . . ? C2A C3A C4A 120.7(5) . . ? C2A C3A H3A 119.7 . . ? C1A C2A H2A 120.9 . . ? C3A C2A C1A 118.2(5) . . ? C3A C2A H2A 120.9 . . ? C1B I1B C7B 92.85(19) . . ? C12B C7B I1B 118.2(4) . . ? C12B C7B C8B 122.6(5) . . ? C8B C7B I1B 119.2(4) . . ? C7B C12B H12B 120.6 . . ? C11B C12B C7B 118.7(5) . . ? C11B C12B H12B 120.6 . . ? C12B C11B H11B 119.9 . . ? C12B C11B C10B 120.1(5) . . ? C10B C11B H11B 119.9 . . ? C11B C10B H10B 119.8 . . ? C9B C10B C11B 120.4(5) . . ? C9B C10B H10B 119.8 . . ? C10B C9B H9B 119.5 . . ? C10B C9B C8B 121.1(5) . . ? C8B C9B H9B 119.5 . . ? C7B C8B C9B 117.0(5) . . ? C7B C8B H8B 121.5 . . ? C9B C8B H8B 121.5 . . ? C6B C1B I1B 117.8(4) . . ? C2B C1B I1B 118.6(4) . . ? C2B C1B C6B 123.6(5) . . ? C1B C6B H6B 121.3 . . ? C1B C6B C5B 117.5(5) . . ? C5B C6B H6B 121.3 . . ? C6B C5B H5B 119.8 . . ? C4B C5B C6B 120.5(5) . . ? C4B C5B H5B 119.8 . . ? C5B C4B H4B 119.7 . . ? C5B C4B C3B 120.6(5) . . ? C3B C4B H4B 119.7 . . ? C4B C3B H3B 119.8 . . ? C4B C3B C2B 120.4(5) . . ? C2B C3B H3B 119.8 . . ? C1B C2B C3B 117.5(5) . . ? C1B C2B H2B 121.3 . . ? C3B C2B H2B 121.3 . . ? O1 Mo1 O10 165.00(12) . 2_667 ? O1 Mo1 O12 95.74(14) . . ? O1 Mo1 O13 94.76(12) . . ? O1 Mo1 O6 101.28(14) . . ? O10 Mo1 O13 72.67(10) 2_667 . ? O12 Mo1 O10 73.03(11) . 2_667 ? O12 Mo1 O13 72.75(10) . . ? O5 Mo1 O1 103.91(15) . . ? O5 Mo1 O10 88.34(13) . 2_667 ? O5 Mo1 O12 101.44(13) . . ? O5 Mo1 O13 161.00(13) . . ? O5 Mo1 O6 101.97(14) . . ? O6 Mo1 O10 84.25(12) . 2_667 ? O6 Mo1 O12 146.66(12) . . ? O6 Mo1 O13 77.41(11) . . ? O2 Mo2 O8 98.50(14) . . ? O2 Mo2 O11 164.89(13) . 2_667 ? O2 Mo2 O13 94.53(12) . . ? O2 Mo2 O6 97.52(14) . . ? O7 Mo2 O2 104.13(15) . . ? O7 Mo2 O8 102.45(14) . . ? O7 Mo2 O11 90.95(14) . 2_667 ? O7 Mo2 O13 161.34(13) . . ? O7 Mo2 O6 103.79(15) . . ? O8 Mo2 O11 78.81(12) . 2_667 ? O8 Mo2 O13 73.98(11) . . ? O8 Mo2 O6 144.73(12) . . ? O11 Mo2 O13 70.40(10) 2_667 . ? O6 Mo2 O11 77.60(12) . 2_667 ? O6 Mo2 O13 73.59(11) . . ? O3 Mo3 Mo4 86.09(10) . . ? O3 Mo3 O8 101.94(15) . . ? O3 Mo3 O10 98.17(14) . . ? O3 Mo3 O12 165.00(12) . 2_667 ? O3 Mo3 O13 94.80(12) . . ? O8 Mo3 Mo4 119.73(9) . . ? O8 Mo3 O10 146.42(12) . . ? O8 Mo3 O12 82.89(12) . 2_667 ? O8 Mo3 O13 78.25(11) . . ? O9 Mo3 Mo4 134.94(11) . . ? O9 Mo3 O3 105.09(15) . . ? O9 Mo3 O8 100.80(14) . . ? O9 Mo3 O10 99.55(13) . . ? O9 Mo3 O12 87.70(13) . 2_667 ? O9 Mo3 O13 159.77(13) . . ? O10 Mo3 Mo4 35.41(8) . . ? O10 Mo3 O12 71.52(11) . 2_667 ? O10 Mo3 O13 73.48(11) . . ? O12 Mo3 Mo4 79.25(7) 2_667 . ? O13 Mo3 Mo4 41.48(7) . . ? O13 Mo3 O12 72.09(10) . 2_667 ? O4 Mo4 Mo3 91.07(10) . . ? O4 Mo4 O10 101.47(13) . . ? O4 Mo4 O11 104.03(15) . . ? O4 Mo4 O12 102.58(13) . . ? O4 Mo4 O13 100.60(13) . . ? O4 Mo4 O13 176.30(13) . 2_667 ? O10 Mo4 Mo3 36.35(8) . . ? O10 Mo4 O13 78.81(11) . . ? O10 Mo4 O13 77.36(11) . 2_667 ? O11 Mo4 Mo3 131.76(9) . . ? O11 Mo4 O10 95.43(12) . . ? O11 Mo4 O12 96.30(13) . . ? O11 Mo4 O13 155.36(13) . . ? O11 Mo4 O13 79.62(12) . 2_667 ? O12 Mo4 Mo3 125.09(9) . . ? O12 Mo4 O10 149.73(12) . . ? O12 Mo4 O13 78.93(11) . . ? O12 Mo4 O13 77.46(11) . 2_667 ? O13 Mo4 Mo3 85.94(6) 2_667 . ? O13 Mo4 Mo3 46.19(7) . . ? O13 Mo4 O13 75.75(12) . 2_667 ? Mo3 O8 Mo2 117.18(14) . . ? Mo3 O10 Mo1 104.21(12) . 2_667 ? Mo4 O10 Mo1 111.67(13) . 2_667 ? Mo4 O10 Mo3 108.24(13) . . ? Mo4 O11 Mo2 119.78(15) . 2_667 ? Mo1 O12 Mo3 101.98(12) . 2_667 ? Mo4 O12 Mo1 110.05(13) . . ? Mo4 O12 Mo3 110.39(12) . 2_667 ? Mo1 O13 Mo2 86.10(9) . . ? Mo1 O13 Mo4 95.53(10) . 2_667 ? Mo3 O13 Mo1 164.71(14) . . ? Mo3 O13 Mo2 85.66(9) . . ? Mo3 O13 Mo4 97.35(10) . 2_667 ? Mo4 O13 Mo1 92.45(10) . . ? Mo4 O13 Mo2 90.20(9) 2_667 . ? Mo4 O13 Mo2 165.55(15) . . ? Mo4 O13 Mo3 92.33(11) . . ? Mo4 O13 Mo4 104.25(12) . 2_667 ? Mo1 O6 Mo2 118.86(15) . . ? C1S N1S C3S 120.7(4) . . ? C1S N1S C2S 121.8(5) . . ? C3S N1S C2S 117.4(4) . . ? O1S C1S N1S 125.5(5) . . ? O1S C1S H1S 117.3 . . ? N1S C1S H1S 117.3 . . ? N1S C3S H3SA 109.5 . . ? N1S C3S H3SB 109.5 . . ? N1S C3S H3SC 109.5 . . ? H3SA C3S H3SB 109.5 . . ? H3SA C3S H3SC 109.5 . . ? H3SB C3S H3SC 109.5 . . ? N1S C2S H2SA 109.5 . . ? N1S C2S H2SB 109.5 . . ? N1S C2S H2SC 109.5 . . ? H2SA C2S H2SB 109.5 . . ? H2SA C2S H2SC 109.5 . . ? H2SB C2S H2SC 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1A C7A 2.109(4) . ? I1A C1A 2.095(5) . ? C7A C12A 1.374(7) . ? C7A C8A 1.381(6) . ? C12A H12A 0.9500 . ? C12A C11A 1.392(7) . ? C11A H11A 0.9500 . ? C11A C10A 1.360(8) . ? C10A H10A 0.9500 . ? C10A C9A 1.380(8) . ? C9A H9A 0.9500 . ? C9A C8A 1.393(7) . ? C8A H8A 0.9500 . ? C1A C6A 1.371(7) . ? C1A C2A 1.383(7) . ? C6A H6A 0.9500 . ? C6A C5A 1.390(7) . ? C5A H5A 0.9500 . ? C5A C4A 1.363(7) . ? C4A H4A 0.9500 . ? C4A C3A 1.386(8) . ? C3A H3A 0.9500 . ? C3A C2A 1.361(8) . ? C2A H2A 0.9500 . ? I1B C7B 2.121(5) . ? I1B C1B 2.108(4) . ? C7B C12B 1.384(8) . ? C7B C8B 1.388(7) . ? C12B H12B 0.9500 . ? C12B C11B 1.371(8) . ? C11B H11B 0.9500 . ? C11B C10B 1.382(8) . ? C10B H10B 0.9500 . ? C10B C9B 1.371(8) . ? C9B H9B 0.9500 . ? C9B C8B 1.391(8) . ? C8B H8B 0.9500 . ? C1B C6B 1.378(7) . ? C1B C2B 1.374(7) . ? C6B H6B 0.9500 . ? C6B C5B 1.391(7) . ? C5B H5B 0.9500 . ? C5B C4B 1.374(8) . ? C4B H4B 0.9500 . ? C4B C3B 1.377(8) . ? C3B H3B 0.9500 . ? C3B C2B 1.395(7) . ? C2B H2B 0.9500 . ? Mo1 O1 1.714(3) . ? Mo1 O10 2.299(3) 2_667 ? Mo1 O12 1.992(3) . ? Mo1 O5 1.706(3) . ? Mo1 O13 2.343(3) . ? Mo1 O6 1.885(3) . ? Mo2 O2 1.715(3) . ? Mo2 O7 1.696(3) . ? Mo2 O8 1.912(3) . ? Mo2 O11 2.232(3) 2_667 ? Mo2 O13 2.467(3) . ? Mo2 O6 1.930(3) . ? Mo3 Mo4 3.1972(5) . ? Mo3 O3 1.706(3) . ? Mo3 O8 1.895(3) . ? Mo3 O9 1.701(3) . ? Mo3 O10 1.995(3) . ? Mo3 O12 2.364(3) 2_667 ? Mo3 O13 2.309(3) . ? Mo4 O4 1.686(3) . ? Mo4 O10 1.951(3) . ? Mo4 O11 1.755(3) . ? Mo4 O12 1.945(3) . ? Mo4 O13 2.119(3) . ? Mo4 O13 2.413(3) 2_667 ? O1S C1S 1.224(7) . ? N1S C1S 1.321(7) . ? N1S C3S 1.459(7) . ? N1S C2S 1.459(6) . ? C1S H1S 0.9500 . ? C3S H3SA 0.9800 . ? C3S H3SB 0.9800 . ? C3S H3SC 0.9800 . ? C2S H2SA 0.9800 . ? C2S H2SB 0.9800 . ? C2S H2SC 0.9800 . ?